WQ0000838_Modification_20190724

INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Project Number* WQ0000838
SUBMITTAL DATED: 7/24/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
r
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number WQ0000838
currently has project
Applicant\Permittee * Granville Farms, Inc
Facility Name * Multiple Facilities
Phone Number*
2528839301
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Hc.)
GFI WQ0000838 Permit Mod July'19.pdf 20.87MB
upload only 1 RDF docurrent. NUltiple documents rust be contained into one RDF file.

For new and modification permit applications, a paper copy may be required. If YGL' have any questions
about what is required, please contactthe reviewer or Tessa Monday. If a aaoe- a1,o1:cation is required,
be advised, applications accepted far pre -review until both the paper and eIect-c-i_ col. es -,ave been
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (cales, soils
report, specs, etc.)
o One full-size engineering plan set
o One 11x27" engineering plan set
o One extra set of specifications
o Fee (if required)
Mailing address:
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
By U.S. Postal Service
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
By Courier/Special Delivery:
�----------------------------------------------------------------------------
---------------------------
❑ivision of Water Resources
i Division of Water Resources
-------------- - ---- ----- -----------------------------------
Non -Discharge Branch
1---------
Non -Discharge Branch
1617 Mail Service Center
i Aft: Nathaniel Thornburg, 90 Floor, O f`uce #942W
Raleigh. NC 27699-1617
512 N. Salisbury St.
Far questions or problems contact Tessa Monday [e-mail] or 919.707.3560.
* I;W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
e _fa&X�Wl
Submission Date 7/24/2019

GRANVILLE FARMS, INC.
PERMIT MODIFICATION
CLASS B PROGRAM
WQ0000838
Submitted by:
Soil Plus
PO Box 1396
Oxford, North Carolina 27565
July 24, 2019
SOIL PLUS

SOIL PLUS
July 24, 2019
NCDEQ-DWR
Non -Discharge Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Attention: Mr. Nathaniel Thornburg
Reference: PERMIT MODIFICATION
Granville Farms, Inc. Residual Biosolids "Class B" Program
Permit # WQ0000838
Mr. Thornburg:
Soil Plus, LLC (Soil Plus) is submitting one paper copy and one electronic copy of this
permit modification application package for Granville Farms, Inc. (WQ0000838). This
package includes:
1. Completed Residual Land Application Program Application
2. Completed
Residual Source Certification Attachments
a.
Arbor Hills MHP WWTP (New)
b.
Ashley Hills WWTP (New)
c.
Birchwood RV Park WWTP (New)
d.
Chapel Ridge WWTP (New)
e.
Cottonwood/Baywood WWTP (New)
f.
Lake Royale WWTP (New)
g.
Town of Pittsboro WWTP (New)
h.
Henderson WRF (Modified)
This package is designed to add (7) new facilities, and increase the permitted dry tonnage
for (1) facility. A check for $395 is enclosed with this package per the Division of Water
Resources Land Application Unit's fee schedule for a major modification to a major non -
discharge permit.
Soil Plus will be responsible for completing this permit application for the Granville Farms,
Inc. If there is any further information required or questions regarding this permit
application, please do not hesitate to contact me for assistance.
Respectfully,
PO Box 1396
Oxford, NC 27565
Drew Matthews, Soil Plus
[phone]
Jason Smith, Granville Farms, Inc.
[e-mail]
www.soilplus.net

Granville Farms, Inc.
Permit Modification
WQ0000838
Residual Source Certification
Attachment
Arbor Hills MHP WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Ashley Hills WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Birchwood RV Park WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Chapel Ridge WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Cottonwood/Baywood WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Lake Royale WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Town of Pittsboro WWTP
Analytical/Field Loading Calculations
Residual Source Certification
Attachment
Henderson WRF
Analytical/Field Loading Calculations

2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Land Application Program Application
RLAP
Weighted Source PAN Calculations
Revised O&M Plan

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 03-15
I. APPLICANT INFORMATION:
1. Applicant's name: tranville Farms, Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Jason Smith Title: Vice President
Applicant's mailing address: P.O. Box 1396
City: Oxford State: NC Zip: 27565-__,=
Telephone number: [phone] Email Address:
2. Consultant's name: Drew Matthews License Number (for P.E.): _
Affiliation: ❑ On Staff ® Retained (Firm: Soil Plus, LLC)
Consultant's mailing address: P.O. Box 1396
City: Oxford State: NC Zip: 27565-
Telephone number: [phone] Email Address: dmatthewsgsoilplus.net
3. Agronomist's name: License Number:
Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: )
Agronomist's mailing address:
City: State: Zip: W__-M
Telephone number: (_) = Email Address:
In-
4. Soil Scientist's name: License Number:
Affiliation: ❑ N/A ❑ On Staff Retained (Firm: )
Soil Scientist's mailing address:
City: I State: Zip: �-
Telephone number: () - Email Address:
5. Fee submitted: (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WQ0000838
Date of most -recently issued permit: 10/11/2016
Date of most -recently certified Attachment A (if different than the permit): 04/20/18
Date of most -recently certified Attachment B (if different than the permit): 04/20/18
FORM: RLAP 03-15 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: NA
City: N State: Zip: -,
Coordinates: Latitude: _° Longitude: _° _'
Datum: —.&_ Level of accuracy:
Method of measurement:
m
County where residuals land application program is headquartered:
1. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Jason Smith
Granville Farms, Inc.
13266
Back -Up ORC
Bryan A. Smith
Granville Farms, Inc.
13265
Additional Back -Up
ORCs
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide
the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training
school and certification test:
2. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrozen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in
the following table:
Maximum amount of residuals to be certified: 8,638 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
41.14
57.66
355,395
498,096
Five -Year Maximum Adjusted
59.38
71.66
512,920
619,036
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified
and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
Hay
2,199.91
Pasture
2,199.91
Total:
2,199.91
Methods
Surface
2,199.91
Incorporation or Injection
0
Total:
2,199.91
FORM: RLAP 03-15 Page 2 of 5

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
7,107.9
9,961.91
10,258.39
12,380.72
100
3,353.95
4,980.96
5,129.2
6,190.36
150
2,369.3
3,320.64
3,419.46
4,126.91
200
1,776.97
2,490.48
2,564.6
3,095.18
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector
reduction practices not in place, etc.): Many of these sources will also maintain their current land application programin
coniunction with this one. Basicallv for most sources this Dermit will not serve as an exclusive land application Droeram. but
rather as a supplement
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than
agronomic rates, explain;
Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain; -A
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or
irrigation facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
Land Application Site
Certification. doc
FORM: RLAP 03-15 Page 3 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without
proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with
any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, Jason Smith Vice President
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Granville Farms Inc.
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water
Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes
unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate
enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the
Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this
application are not completed and that if all required supporting information and attachments are not included, this application
package will be returned to me as incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.613, any person who knowingly makes any
false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine
not to exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: 14c-, k 'S� Date: 7 -zI/ aV
FORM: RLAP 03-15 Page 4 of 5

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GRANVILLE FARMS, INC.
OPERATION AND MAINTENANCE PLAN
LAND APPLICATION OF CLASS B RESIDUAL BIOSIOLIDS
WQ#0000838
Revised June 2019

1.0 SUMMARY
Granville Farms, Inc. (GFI) is a privately owned company that is contracted to haul and land apply nutrient enriched
by-products such as Biosolids from Wastewater Treatment Plants, Residuals from Water Treatment Plants, Animal
Waste from Animal Production Facilities, and certain Construction Debris from Road Work (i.e. slurry water from
diamond cutting of concrete). GFI is unique in that it does not participate in the generation or treatment of the by-
products generated by any of the source types listed above. At times GFI is requested to provide lime stabilization
of Biosolids by smaller operating facilities, but this quantity is normally very small. GFI's main role is to provide
transportation and operational equipment to spread the nutrient enriched by-products listed above.
Another unique characteristic about GFI is that it owns and maintains permits to land apply these by-products. Given
that most generators are issued their own land application permit, they have direct oversight of the preparation,
removal, and application of their by-products. This creates some operational and permit challenges for GFI since
standard, state issued permits are typically issued to generators not land application companies. This Operation and
Maintenance Plan (O&M) addresses how GFI is able to manage by-products produced by multiple, independent
generators and land applies under their own land application permit.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
SAMPLING & ANALYTICAL

2.0 ANALYTICAL REQUIREMENTS
Prior to the hauling and land application event being schedule the generator must provide analytical results
documenting that all parameters listed in Condition IV. 2 — 4 and at the frequency listed in most recent copy of this
permit. If GFI does not collect the sample then it DOES NOT own the responsibility of the integrity of the sample
and the method it was collected, transported, submitted, and analyzed. Should the generating source elect to have
GFI collect the sample prior to land application, then it will be done in the following manner:
Four factors that may ultimately affect the integrity of reported data include: 1) obtaining a representative sample, 2)
preventing contamination of the sample, 3) providing legal documentation of the sampling event, and 4) protecting
the sample from chemical, physical or biological change prior to analysis.
A sample will be collected according to the schedule provided in the most recent copy of the Attachment of this
permit and prior to land application one composite sample should be pulled from a designated location from the
generating source. GFI has identified Meritech, Inc based in Reidsville, NC to be used as the Certified Laboratory.
The composite sample should be analyzed for:
• % Solids,
• Nitrogen Series (TKN, Ammonia, Nitrate, Nitrite, and Organic Nitrogen),
• Phosphorus,
• Potassium,
• Sulfur,
• Calcium,
• Magnesium,
• Sodium,
• Iron,
• Aluminum,
• Manganese,
• Copper,
• Zinc,
• and Remaining 503 Metals (i.e. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel,
Selenium)
Approximately 2 quarts of residual should be collected. The sample containers should be clean and sterile. They
should also be labeled so that they are easily identifiable in the lab. The samples should be pulled using the method
listed below:
Collect one sample from each digester(s) from which the material will be land applied using a "swing sampler"
o The swing sampler must be used with a sterile, plastic 960 ml container
Combine each sample in a stainless steel bucket
Mix thoroughly using a fiberglass rod
Collect each sample from the top of the access point at each digester. This access point is obtained by climbing
the installed ladder on the side of the digester.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

Once the sample is pulled, it should be placed in medium size cooler packed with ice. The sample should be collected
with an enough time so that it can be delivered to the laboratory.
Once per calendar year a sample should be collected and analyzed for:
• Full TCLP
• Ignitability, Corrosivity, and Reactivity
• Requires 5 Liters
A third should be submitted for a 30-Day Scale Bench test and Fecal Coliform Density Test. The 30-Day Scale Bench
Test also requires 1 quart of "clear" water from the Clarifier for Dilution if necessary. This sample would be analyzed
for:
• 30-Day Scale Bench Test (4 Quarts of Residuals and 1 Quart of Clarifier water)
• Fecal Coliform Density Test (seven samples)
The contact information for the lab is:
Mailing Address
Meritech, Inc.
642 Tamco Rd
Reidsville, NC 27320
[phone] (Phone)
Sampling frequency will be conducted in accordance with the Table listed in the most recent Attachment A of this
permit. The sample will be collected by a representative of Soil Plus, LLC. For further information please contact:
Drew Matthews
P.O. Box 1396
Oxford, NC 27565
252-883-9301
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
OPERATION, SPILL CONTROLL, & TRAINING

3.0 BIOSOLIDS REMOVAL, TRANSPORT, AND APPLICATION
Biosolids will be transported from the generators to suitable, permitted land application sites. Transport equipment
will be inspected, licensed and appropriately marked, as required, for the purpose of transporting biosolids. Biosolids
will be delivered to the application sites between sunrise to sunset.
Both liquid and dewatered biosolids distribution on the land application sites will be uniform throughout the
application area. To ensure adequate control of the application rate for each site, the equipment used for spreading
the sludge will be calibrated by measuring the amount handled on a known square footage. While the rate of discharge
from the application vehicle is fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to
achieve specific application rates. Spreading operations will be discontinued during periods of inclement weather and
will not be resumed until sufficient drying of the fields has occurred. This allows equipment access without causing
excessive soil compaction or rutting. To prevent adherence of the biosolids, transport vehicles will be equipped with
rear mud flaps, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap
will be scraped off in the field before the truck returns to the roadway. Examples of our application tracking and
summary form/reports can be provided upon request.
4.0 SITE OPERATION
Biosolids will be surface applied at the properly -calculated agronomic rate and in strict accordance with any state and
federal regulations for the land application of the biosolids. Buffer zone distances will be observed in accordance with
applicable state and federal regulations. Buffer zones will be flagged and no biosolids will be applied within those
areas. The most restrictive buffer will apply in combined situations. Operational provisions will be taken to prevent
soil loss through erosion. Provisions will include contour application and avoidance of areas where surface drainage
patterns result in concentrated flow of runoff from rainfall. In accordance with sound, industry standard agronomic
practice, areas which are unseasonably wet (and would produce rutting or damage to the field) will not be utilized for
biosolids application operations during those periods. Operations will be discontinued when soils are saturated and
will not be resumed until the field has sufficient dried. The amount of biosolids applied will not exceed the hydraulic
capacity of the soil at the time of each application. If a subsequent pass across a field is necessary to achieve the
desired application rate, sufficient drying time will be allowed between passes.
5.0 PROJECT CONTROL
To ensure biosolids are continuously applied at the correct application rate and in a manner consistent with the
Operations Plan, a GFI Project/Field Manager will be in direct charge of the field operations, controlling the amount
of biosolids delivered to each field, and conducting daily field inspections. Field inspections will include ensuring that
flags are in place, biosolids are applied uniformly at the designated application rate, setbacks are observed, trucks are
unloading at best location, trucks are not driving over biosolids, trucks are cleaned before leaving the field and the
land application equipment is maintained in working condition.
6.0 TRANSPORTATION SYSTEM ROUTING
Per the specifications, GFI transportation vehicles will be equipped with GPS devices that will guide drivers to the
land application sites. Transportation routes will follow primary highways and avoid residential areas where possible.
Designated routes are followed unless a detour is specified. In the event of a detour route, it shall be taken as specified
by the detour authority. There shall be no unscheduled stops when loaded. Transportation vehicles will be inspected,
licensed and appropriately marked as required with identification numbers for the purpose of this contract. All units
will be equipped with spill guards and full mud flaps. This will prevent the biosolids from adhering to the tires and
undercarriage of the transport vehicle, thereby preventing biosolids from being tracked onto roadways. Biosolids
adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. All federal OSHA
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

and DOT laws and regulations are complied with for the protection of our clients, the community and our drivers.
Examples of vehicle and driver transportation logs and inspection forms can be provided upon request.
7.0 DEWATERED BIOSOLIDS
Dewatered biosolids will be transported in standard end dump trailers. The dump trailers will be loaded per the
generator's specifications and standard protocols. The dump trailers used for transportation of dewatered cake
biosolids will be equipped with sealed tailgates and will be completely sealed to prevent leakage. All trucks will be fully
covered and will be fitted with positive lock tailgates.
8.0 LIQUID BIOSOLIDS
Liquid biosolids will be transported using liquid tankers that will be pulled by standard road tractors. The tankers
will be loaded per the generator's specifications and standard protocols. The tractor/tanker unit will transport its
load to a designated staging area inside the buffered area of a permitted land application site.
9.0 APPLICATION (SPREADING) — DEWATERED BIOSOLIDS
At the staging area each load will be unloaded in a designated area within the land application site. Biosolids will be
loaded into our Side Slinger cake box by a GFI employee using a front-end loader. This unit is capable of delivering
an accurate, calibrated application of dewatered biosolids over the application site. The uniform spread pattern ensures
that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each
site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the
biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual
PAN requirement.
10.0 APPLICATION (SPREADING) — LIQUID BIOSOLIDS
At the staging area each load will be transferred into a 4,000-gallon capacity pull behind or TerraGator for subsequent
land application. This unit is capable of delivering an accurate, calibrated application of liquid biosolids over the
application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and
hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on
the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver
between 75 and 100 percent of a crop's annual PAN requirement.
11.0 SPILL AND EMERGENCY RESPONSE PROGRAM
In the unlikely event of a spill, GFI will take the following actions immediately.
• Halt Source of Spill. Use of any leaking or damaged unit which is causing the spill will cease immediately. The
unit will be repaired before resuming its use.
• Contain Spill. In the event large quantities of biosolids have been spilled, straw bales will be used where
available and as necessary to either form a barrier or absorb biosolids.
• Clean -Up. Depending on the type and amount of biosolids spilled, a variety of equipment may be used to
remove the biosolids: front-end loader, shovels and brooms and vacuum equipment of a liquid biosolids
applicator. Any biosolids removed from the spill site will be spread on an approved application site, returned
to the WWTP, or disposed of in an approved landfill.
• Final Clean -Up. Flush roadways with water or sweep as necessary to clean. Allow to dry and incorporate if
spill occurs on non -paved and tillable area. In the event a spill occurs on private property, final clean-up
should be completed immediately to the satisfaction of the owner.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

Management of Clean -Up Efforts. The Operations Manager will take immediate charge and initiate clean-up
activities. GFI labor will be used, with additional labor secured as needed. The Operations Manager will also
communicate with the public on the scene, answering questions and advising of clean-up activities.
Reporting. All spills will be reported immediately to GFI offices and the client. State and local agencies will
be notified in accordance with their notification requirements. Within 24 hours of the spill, the Operations
Manager will send GFI office a written report detailing how the spill occurred and remedial action taken. This
report will be provided using the enclosed Spill Report form.
Spill Prevention. The Operations Manager will implement the following spill prevention measures:
o Ensure truck drivers watch trailer while loading and do not overload;
o Ensure trailer hatches are closed and latched while transporting;
o Ensure trailer seals are inspected on a daily basis and replaced as necessary; and
o Ensure unloading operations in the field are conducted to minimize any potential runoff or tracking.
All employees receive safety and spill response training as part to their new hire training and thereafter participate in
our monthly safety and spill response training program. In addition to our internal training and protocols, we also
contract with a regional emergency response firm - HEPACO - available to respond to an incident in the Central and
Eastern North Carolina area within two hours. A copy of our agreement with HEPACO can be provided upon
request.
Names and Titles of Inspection Personnel
Andy Smith, Area Supervisor
Jason Smith, Area Supervisor
JT Bryant, Regional Supervisor
Jay Bryant, Project Supervisor
Matt Foster Project Supervisor
BJ Bryant, Field operators
Jeff Bumpass, Field operators
Tammy Walston, Field operators
12.0 PREVENTION
The goal of a compliance assurance system is to prevent compliance issues from occurring. Prevention involves:
• Ensuring personnel understand their role in assuring compliance;
• Identifying compliance requirements at the federal, state and local levels;
• Implementing a system where compliance tasks are scheduled, assigned and tracked to completion;
• Developing standard operating procedures where appropriate; and
• Reviewing the compliance task list and standard operating procedures on an ongoing basis and modifying
them as appropriate to account for changes in regulations/requirements and operating methods, and to
address compliance deficiencies.
GFI ensures employees understand their role in assuring compliance through new employee orientation programs
and on the job training.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

13.0 Standard Operating Procedures (SOP's)
GFI develops and implements SOPS to ensure compliance tasks are completed consistently across the company.
The SOP provides standard forms to use, approved biosolids analytical methods, frequency of monitoring
information, etc. Another key SOP relative to preventing compliance issues from occurring is the use of a "Pre -
Operating and Buffer Checklist".
The Pre -Operating and Buffer Checklist ensures federal, state and local regulations and permit requirements are met
prior to initiating biosolids applications at field sites. Compliance items on the Checklist include:
• The field is permitted and suitable for the biosolids/residuals type being applied;
• Pre -application requirements are met;
• Farmer and landowner agreements are current and the crop to be grown has been verified;
• The field is flagged to prevent applications in buffer zones and restricted areas;
• The appropriate application rate and field capacity is calculated; and
• Any special permit or local requirements are met.
• A listing of the buffer zones and restricted areas where biosolids/residuals cannot be applied
• A listing of operating requirements including notification requirements,
• application method requirements, and inclement weather operating requirements
14.0 ASSESMENT
To help ensure compliance requirements are being met and the compliance assurance system is implemented and
working, periodic, consistent, objective and documented assessments of a project/facility's compliance status are
conducted. GFI personnel have clearly -defined compliance assessment responsibilities and time to conduct such
assessments. GFI conducts informal site inspections and formal audits on an ongoing basis.
15.0 CORRECTIVE ACTION
Once compliance issues have been identified during the course of day to day business and through internal audits and
inspections a system must be in place which ensures that appropriate and timely corrective action is taken, the cause
of the compliance issue is identified and actions are taken to prevent recurrence of the issue.
GFI's goal is to have no instances of non-compliance. However, issues and incidents may occur and when this
happens employees work to correct the incident in a timely and thorough manner. When compliance issues are
identified, the situation is examined to determine the root cause of the problem and the corrective and preventive
action that must be taken. The preventive action must address the root cause with the goal of preventing a recurrence.
Depending on the nature of the compliance issue, it is assigned to one or more responsible parties to ensure that the
corrective and preventive actions are implemented. A deadline for completion of the task is assigned and the issue is
tracked to completion by regional and corporate compliance personnel.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

16.0 TRAINING
An effective compliance training program involves:
• Identifying training needs and requirements;
• Assigning personnel to provide training and providing them the resources they need to conduct training;
• Documenting and tracking that mandatory t raining has occurred; and
• An employee's training needs and requirements, as well as their training responsibilities, are based on
his/her position within the company.
Revised 06/19 ©Granville Farms, Inc. Operation and Maintenance Plan

GRANVILLE FARMS O&M PLAN
PROCESS FLOW DIAGRAM

GRANVILLE FARMS CLASS B SOURCES (WWTP)
Amherst Subdivision
Knightdale MHP
Arbor Hills MHP
Lake Ridge
Avocet
Lake Royale
Ashley Hills
Little Creek WWTP
Barclay Downs
Mallard Crossing
Beachwood
Mallinckrodt
Birchwood MHP
Nature's Trail
Briar Chapel Development
Neuse Colony
Briarwood Farms
Neuse River Village
Carolina Meadows
Neuse River WWTP
Chapel Ridge
Pope Industrial Park
Cole Park Plaza
River Mill
Colvard Farms
Rock Bridge
Consolidated Diesel
SGWASA WWTP
Cottonwood/Baywood
Shearon Harris NPP
Crooked Creek
Tar River Regional WWTP
Cross Creek
The Legacy at Jordan Lake
Deerchase
The Preserve at Jordan Lake
Enfield WWTP
Town of Bunn
Fearrington Village
Town of Louisburg
Franklin County WWTP
Town of Pittsboro
Governor's Club
Town of Spring Hope
Hasentree Golf Comm.
Town of Warrenton
Hawthorne Subdivision
Tradewinds
Henderson WRF
Westfall
Johnston Co. WWTP
Whippoorwill Valley
Kenly Regional WWTP
Wildwood Green
King's Grant Subdivision
Willowbrook
Kittrell Job Corp.
Woodlake Country Club

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Enfield WTP
Kerr Lake Regional WTP
SGWASA WTP
Sunset WTP
Tar River WTP

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GRANVILLE FARMS O&M PLAN
MAXIMUM PRODUCTION
QUANTIFICATION & JUSTIFICATION

A
#of
Forecasted
Requested
Dry TonsVERAGE WWTP
Years Counted
Production
DT
43,229
2.69 Amherst WWTP
7
Amherst WWTP
5.37
10.00
13,350
1.14 Arbor Hill MHP
1
Arbor Hill MHP
2.28
10.00
97,900
5.47 Ashley Hills WWTP
1
Ashley Hills W6NP
10.94
30.00
60,075
5.06 Avocet WWTP
2
Avocet W WTP
10.12
10.00
21,614
0.53 Barclay Downs WWTP
7
Barclay Downs WWTP
1.07
10.00
24,920
1.84 Beachwood WWTP
5
Beachwood WWTP
3.68
10.00
48,950
2.47 Birchwood RV Park
1
Birchwood RV Park
4.94
10.00
282,750
19.80 Briar Chapel Development
2
Briar Chapel Development
39.60
30.00
77,319
4.85 Briarwood Farms WWTP
8
Briarwood Farms WWTP
9.70
30.00
403,444
35.87 Carolina Meadows WWTP
8
Carolina Meadows WWTP
71.74
75.00
18,450
3.99 Chapel Ridge WWTP
1
Chapel Ridge WWTP
7.98
10.00
75,094
6.81 Cole Park Plaza
8
Cale Park Plaza
13.62
10.00
43,875
2.31 Colvard Farms
2
Colvard Farms
4.62
10.00
97,660
6.22 Consolidated Diesel WWTP
5
Consolidated Diesel WWTP
12.45
20.00
-
0.00 Cottonwood/Baywood WWTP
1
Cottonwood/Baywood WWTP
0.00
10.00
125,563
10.86 Crooked Creek W WTP
8
Crooked Creek WWTP
21.72
40.00
49,269
2.10 Cross Creek Mobile Estates
8
Cross Creek Mobile Estates
4.20
10.00
71,363
3.27 Deerchase WWTP
8
Deerchase WWTP
6.55
10.00
115,219
11.55 Enfield WTP
8
Enfield WTP
23.09
50.00
203,500
20.99 Enfield WWTP
8
Enfield WWTP
41.97
100.00
249,000
32.02 Fearrington Utility WWTP
8
Fearrington Utility WWTP
64.05
100.00
994,000
127.69 Franklin County WWTP
8
Franklin County WWTP
255.38
319.00
191,979
8.22 Govenor's Club WWTP
7
Govenor's Club WWTP
16.43
40.00
37,200
3.27 Hasentree Golf Community
2
Hasentree Golf Community
6.53
50.00
300,806
24.94 Hawthorne Subdivision WWTP
8
Hawthorne Subdivision WWTP
49.87
80.00
2,893,188
446.51 Henderson WRF
8
Henderson WRF
893.02
1200.00
234,000
33.18 Johnston County WWTP
1
Johnston County WWTP
66.35
100.00
937,350
80.15 Kenly Regional WWTP
8
Kenly Regional WWTP
160.29
319.00
2,800,000
107.49 Kerr Lake Regional WTP
8
Kerr Lake Regional WTP
214.98
200.00
29,481
1.63 Kings Grant Subdivision
8
Kings Grant Subdivision
3.27
10.00
19,636
1.63 Kittrell Job Corp
7
Kittrell Job Corp
3.25
10.00
73,425
5.96 Knightdale Mobile Home Park
8
Knightdale Mobile Home Park
11.93
15.00
21,508
1.98 Lake Ridge WWTP
6
Lake Ridge WWTP
3.95
10.00
-
0.00 Lake Royale WWTP
1
Lake Royale WWTP
0.00
10.00
38,800
2.07 Legacy at Jordan Lake
1
Legacy at Jordan Lake
4.14
20.00
928,694
88.96 Little Creek WWTP
6
Little Creek WWTP
177.92
150.00
90,431
6.99 Mallard Crossing WWTP
8
Mallard Crossing WWTP
13.99
15.00
-
0.00 Mallinckrodt WWTP
1
Mallinckr.dt WWTP
0.00
790.00
147,486
6.07 Nature Trails MHP WWTP
7
Nature Trails MHP WWTP
12.14
20.00
886,571
62.25 Neuse Colony WWTP
7
Neuse Colony WWTP
124.49
150.00
82,325
4.10 Neuse River Village
8
Neuse River Village
8.20
15.00
4,567,920
650.92 Neuse River WWTP
6
Neuse River WWTP
1301.84
1000.00
10,383
0.26 Pope Industrial Park
3
Pope Industrial Park
0.52
10.00
155,500
8.57 Preserve at Jordan Lake
2
Preserve at Jordan Lake
17.13
20.00
4,450
0.50 Bi- Mil] WWTP
1
Rivcr MdI WWTP
1.00
10.00
51,338
1,10 Rock Bridge WWTP
4
Rock Bridge WWTP
6.79
10.00
1,937,250
133.36 SGWASA WTP
8
SGWASA WTP
266.72
319.00
2,409,690
295.77 SGWASA WWTP
8
SGWASA WWTP
591.54
650.00
400,425
3.91 Shearon Harris NPP
6
Shearon Harris NPP
7.82
15.00
495,408
87.55 Sunset WTP
6
Sunset WTP
175.10
319.00
1,632,313
158.03 Tar River Regional WWTP
8
Tar River Regional WWTP
316.05
800.00
842,625
108.47 Tar River WTP
8
Tar River WTP
216.95
319.00
32,500
1.90 Town of Bunn
1
Town of Bunn
3.79
75.00
1,199,000
142.79 Town of Louisburg
8
Town of Louisburg
285.57
319.00
527,000
96.90 Town of Pittsboro WWTP
I
Town of Pittsboro W WTP
193.80
200.00
93,450
9.81 Town of Spring Hope WWTP
5
Town of Spring Hope WWTP
19.62
50.00
971,188
155.05 Town of Warrenton WWTP
8
Town of Warrenton WWTP
310.10
319.00
82,438
4.12 Tradewinds WWTP
8
Tradewinds WWTP
8.24
10.00
57,850
3.52 Westfall WWTP
1
Westfall WWTP
7.04
10.00
44,263
1.98 Whippoorwill Valley WWTP
8
Whippoorwill Valley WWTP
3.96
15.00
85,825
7.10 Wildwood Green WWTP
8
Wildwood Green WWTP
14.20
15.00
72,471
3.39 Willowbrook WWTP
7
Willowbrook WWTP
6.77
10.00
113,467
10.64 Woodlake C- ry Club WWTP
3
Woodlxke C- ry Club WWTP
21.28
25.00
28,616,124
3,081
6,161.67
8,638.00

GRANVILLE FARMS O&M PLAN
SOURCE VICINITY MAPS

TABLE OF CONTENTS
SOURCE
FIGURE
SOURCE
FIGURE
Amherst Subdivision
1
Lake Ridge
18
Arbor Hills MHP
38
Lake Royale
29
Avocet
25
Little Creek WWTP
19
Ashley Hills
40
Mallard Crossing
20
Barclay Downs
2
Mallinckrodt
8
Beachwood
2
Nature's Trail
4
Birchwood MHP
38
Neuse Colony
21
Briar Chapel Development
5
Neuse River Village
2
Briarwood Farms
3
Neuse River WWTP
16
Carolina Meadows
4
Pope Industrial Park
22
Chapel Ridge
39
River Mill
23
Cole Park Plaza
5
Rock Bridge
16
Colvard Farms
6
SGWASA WTP
24
Consolidated Diesel
7
SGWASA WWTP
24
Cottonwood/Baywood
40
Shearon Harris NPP
25
Crooked Creek
1
Sunset WTP
26
Cross Creek
2
Tar River Regional WWTP
27
Deerchase
8
Tar River WTP
28
Enfield WTP
9
The Legacy at Jordan Lake
36
Enfield WWTP
9
The Preserve at Jordan Lake
36
Fearrington Village
5
Town of Bunn
29
Franklin County WWTP
10
Town of Louisburg
30
Governor's Club
4
Town of Pittsboro
39
Hasentree Golf Comm.
37
Town of Spring Hope
31
Hawthorne Subdivision
11
Town of Warrenton
32
Henderson WRF
12
Tradewinds
8/20
Johnston Co. WWTP
13
Westfall
4
Kenly Regional WWTP
14
Whippoorwill Valley
33
Kerr Lake WTP
15
Wildwood Green
11
King's Grant Subdivision
16
Willowbrook
34
Kittrell Job Corp.
17
Woodlake Country Club
35
Knightdale MHP
2

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LOCATION MAP
Figure
1
Drawn by: CSC
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Fuquay-Varina, North Carolina
Date: Sept'16
Soil Plus Project # 200705.G10

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Figure
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GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Raleigh, North Carolina
Date: Sept'16
Soil Plus Project # 200705.G10

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Date: Sept'16 Soil Plus Project # 200705.G10

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Chapel Hill, North Carolina
4
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Soil Plus Project # 200705.D10

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Reviewed hy: CSC
Chapel Hill, North Carolina
S
Date: April'17
Soil Plus Project # 200705.G10

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Reviewed by: CSC Durham, North Carolina 6
Date: Sept'16 Soil Plus Project # 200705.G10

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Date: Sept'16 Soil Plus Project # 200705.G10

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SOIL PLUS
GFI Land Application Permit
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Raleigh, North Carolina
8
Date: April '17
Soil Plus Project # 200705.G10

N
` W E
S
Coat
SRSR-12�R-
SR-1223
NC-48
NC-481
SR-1220
Legend
Source Location
— Road
Stream
J County Boundary
Municipal Boundary
Surface Water
HALIFAX
Enfield
5�
Enfield/WTP
s
NC-481
WWTP
0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Enfield, North Carolina 9
Date: Sept'16 Soil Plus Project # 200705.G10

E
S
h
SR-1133
Jy
V,
Fratildinton
4SR- 1157
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M
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h
Legend
Source Location srpJl
— Road
Stream
[_-_—],County Boundary sR 19�4 sg''
sg, L Municipal Boundary
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Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Franklinton, North Carolina 10
Date: Sept'16 Soil Plus Project # 200705.G10

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Raleigh
Stream
��
OJ
SR-330�s
rJ County Boundary
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s4 Miles
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Raleigh, North Carolina
11
Date: Sept'16
Soil Plus Project # 200705.G10

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Source Location
— Road
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J County Boundary
Municipal Boundary
cu_,ca2
0.5 0.25 0
0.5
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Miles
SR-1148
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Henderson, North Carolina
12
Date: Sept'16
Psoilplus Project # 200705.G10

N U,
00
N
W E
SR-1340
t
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M
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1343
Legend
Source Location
— Road
Stream Smithfield Smithfield
J County Boundary s� M
L Municipal Boundary
Surface Water 0.5 0.25 0 0.5
Miles'
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL U s GFI Land Application Permit (WQ000838)
Reviewed by: CSC Smithfield, North Carolina 13
Date: Sept'16 Soil Plus Project # 200705.G10

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7 Source Location SR-2341
a
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Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Kenly, North Carolina 14
Date: Sept'16 Soil Plus Project # 200705.G10

N
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S
SR-
SR-1366
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Legend
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— Road SR- - Stream 4'
RMP-2130 P
[__]County Boundary
[J Municipal Boundary �� of
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Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Middleburg, North Carolina 15
Date: Sept'16 Soil Plus Project # 200705.G10

114
SR,4j
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SR-4198 13p
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SR-2507
SR-2508
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Source Location
— Road
Stream —
Count Boundar %� JOHNSTON Clayton
�_J Y Y
L Municipal Boundary 1�rE
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Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Clayton, North Carolina 16
Date: Sept'16 Soil Plus Project # 200705.G10

N \ sg 1112
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Legend
Source Location
— Road
Stream
J County Boundary
L Municipal Boundary
r Surface Water 0.5 0.25 0 0.5
mmmiiiiil Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Kittrell, North Carolina 17
Date: Sept'16 Soil Plus Project # 200705.G10

SR-1221414
N
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1
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N
aCounty Boundary J��1114,
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-ham
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC Durham, North Carolina 18
Date: Sept'16 Soil Plus Project # 200705.G10

N
ti
W E
S
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SR-232o
. SR-2456
AS
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SR-2346
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Source Location
— Road
Stream /
J County Boundary
L Municipal Boundary SR-1723
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Zebulon, North Carolina 19
Date: Sept'16 Soil Plus Project # 200705.G10

N
Z �
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SR-4657
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Raleigh
Raleigh
N
N
0
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0
0
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N
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Source Location
— Road
Stream
r i_J County Boundary
Municipal Boundary
R 0.5 0.2 5 0 0.5
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iiiiii Miles
Knightdale nnigntaate
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Raleigh, North Carolina 20
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
i S
max. I
1 Clayton
Clayton
Clayton
SR-2641
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cc
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-� Us-70
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Clayton, North Carolina 21
Date: Sept'16 Soil Plus Project # 200705.G10

N SR-1466 � SR 2684
1' cn
Raleigh
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00
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r�
a�
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mo
J County Boundary
�J
Municipal Boundary
SR,4864
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531,9
0.5
54
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SR-2891
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LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Garner, North Carolina
22
Date: Sept'16
Soil Plus Project # 200705.G10

V (N
W E
S
O
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SR-362'4
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Raleigh
Wake Forest
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SR-2045
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Legend
Source Location
Wake Forest
— Road
Stream
[_-_—],County Boundary
L Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC4900EPPP�* Raleigh, North Carolina 23
Date: Sept'16 1 Soil Plus Project # 200705.G10

i
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er (including the Flat Riv
Source Location
R-1234
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r
Count Boundar
LJ Y Y
/
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0.5
Surface Water
r
Miles
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OIL PL U
S S
LOCATION MAP
Figure
24
Drawn by: CSC
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Butner, North Carolina
Date: Sept'16
Soil Plus Project # 200705.G10

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ee
68
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141
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SOURCE LOCATION MAP
Figure
Drawn by: CSC
SOIL
PLUS
GFI Land Application Permit (WQ000838)
Reviewed by:
Holly Springs, North Carolina
25
Date: Nov'17
Soil Plus Project # 200705.D10

RMP-172
/
Rocky Mount
Maple CreeJ
M
^ti
SR
Horn B
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0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Rocky Mount, North Carolina 26
Date: Sept'16 Soil Plus Project # 200705.G10

N
W E
S
SR-1404
00
Tar River
U i
Rocky Mount
Legend
Source Location
— Road
Stream
_IR J County Boundary
L Municipal Boundary
Surface Water
N
0
�ek
WWTP
SR-1414
0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed by: CSC Rocky Mount, North Carolina 27
Date: Sept'16 Soil Plus Project # 200705.G10

Z1707��t
Aofec
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rah �
SR-1709 c!l
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s
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ranch
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SR-1733
I V v
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Source Location
— Road
7�
Stream x
J County Boundary
L Municipal Boundary
0.5 0.25 0 0.5
Surface Water
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC4949swpw— Rocky Mount, North Carolina 28
Date: Sept'16 1 Soil Plus Project # 200705.G10

N
W E
S
R 1-17 NC-98
\S�
Town of
U
FRANKLIN
1609
.0
J
w
�98
Legend
V ��
❑Source Location
Z
SR-1736
— Road
— Stream
QCounty Boundary
❑Municipal Boundary
^Q, R1j
s
Surface Water
0.5 0.25 0
0.5
Miles
Scale: 1 inch = 0.5 miles
SOIL PL Us
LOCATION MAP
Figure
Drawn by: CSC
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Bunn, North Carolina
29
Date: Sept'16
Soil Plus Project # 200705.G10

c
N
N
10
W E \
c
6
� SR-1268
s
SR`1272
SR-1256
N
�
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Opole Creek
SR-1232
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SR-1420
SR-1231
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SR-1650 NC-56,581 U4¢ SR 1491
Louisburg
FRANKLIN
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00
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N
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SR-1645
Sg
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rd
Legend
Source Location
— Road
Stream
r �_J County Boundary
L Municipal Boundary
Surface Water
4�
0.5 0.25 0
0.5
SR-1604
Miles
Scale: 1 inch = 0.5 miles
SOIL PLUS
LOCATION MAP
Figure
30
Drawn by: CSC
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Louisburg, North Carolina
Date: Sept'16
Soil Plus Project # 200705.G10

i
N
'lam
W E�9
S
SR-
SR-1331
SR-1314
SR -
�10
'�'-1146
Lo
Spring Hope
ks Creek
s4s
Q
� SR-1180 c4
SR-1915
SR,
S�
Legend s'e
Source Location
— Road s
TAR RIVER
— Stream
r Count Boundar
LJ Y Y
❑ Municipal Boundary
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn hy: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed hy: CSC Spring Hope, North Carolina 31
FDa7tS7ept'l6 Soil Plus Project # 200705.G10

N
W E
S
tiI
Fishing
SR'1
0
ry SR-1332
SR-1107
SR-1`119 �S
M SR-1326
SR-1150
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SR-1142
x
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SR -I
SR-1601
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Legend oC, �ro�
Source Location
— Road°yy
Stream
County Boundary
L Municipal Boundary -
Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Warrenton, North Carolina 32
Date: Sept'16 Soil Plus Project # 200705.G10

'19
S4/
n
M
SR-1715
SR_2447
FRANKLIN
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N
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Legend
Source Location
1I25
Sg
— Road
Stream
N
�e
SR-2309 esva
F_JCounty Boundary
9�k
L Municipal Boundary
r
0.5 0.25 0
0.5
Surface Water
Miles
SR-2315
Scale: 1 inch = 0.5 miles
LOCATION MAP
Figure
Drawn by: CSC
SOIL PLUS
GFI Land Application Permit (WQ000838)
Reviewed by: CSC
Zebulon, North Carolina
33
Date: Sept'16
Soil Plus Project # 200705.G10

\ N.
W E
S
N
� N
G �
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N
^� N
0
SR-417R '
tihh� � N
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SR-52041
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M �
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SR-1771
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SR-1677
M Clayton
M
SR-1632
Legend Cn C
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Source Location N ��
— Road s�\IssJ
Stream SR-1550
r �_J County Boundary
s L Municipal Boundary
r hN Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC4949swpw— Garner, North Carolina 34
Date: Sept'16 1 Soil Plus Project # 200705.G10

N
W E
s
O
SR-2016
MOO
SR-2176
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N/
h
N
SR-2019
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N No
� N
Legend N
Source Location
— Road
Stream HOKE 4~��
FJCounty Boundary
[J Municipal Boundary
� Surface Water 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP Figure
Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838)
Reviewed by: CSC Vass, North Carolina 35
Date: Sept'16 Soil Plus Project # 200705.G10

of
N
W E
s
The Preserve at Jordan Lake 1749
0
The
0
J
Lf
rd
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CHATHAM 1746
0 0
gAl
Legend O
ElNC Sources
— Stream
0
— Road
NHDWaterbody
❑ <all other values>
yp 64
FT e JordancL-ake-SR"A=_Seaforth 64
❑ Estuary
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❑ Playa o
❑ Reservoir
❑ SwampMarsh O
j J! CountyBoundary
❑ MunicipalBoundaries_polys 0.5 0.25 0 0.5
Miles
Scale: 1 inch = 0.5 miles LOCATION MAP
Figure
Drawn hy: CSC SOIL PL Us GFI Land Application Permit (WQ000838)
Reviewed hy: CSC Pittshoro, North Carolina 36
Date: April'17 Soil Plus Project # 200705.G10

1909
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0
Hasentree Golff-Communify
Hasentree Golf Community, Phase 1
Q o
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Date: June '19 Soil Plus Project # 200705.D10

APPENDIX 1
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0035595)
Residual Source Certification Attachment
RS CA
Arbor Hills MHP WWTP
Analytical
Field Loading Calculations

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State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Arbor Hills Mobile Home Park WWTP
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or ® Private.
Facility permit issued by: ■ Div. of Water Resources, Div. of Environmental Health,
or ❑ Other (explain: `).
3. Facility contact person and title: Mr. Luther Thomas Harden III
Complete mailing address: 4228 US Highway
City: Durham State: NC Zip: 27705-
Telephone number: [phone] E-mail address: ltharden31954(a^,gmail.com
4. Facility physical address: 4228 US Highway
City: - State: NC Zip: 705-
Coordinates: Latitude: 36' 02' 57.0" Longitude: 79' 01' 26.0"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes ® No
7. Facility permitted/design flow: 0.006 MGD and facility average daily flow:.002 MGD
8. Average amount of residuals being generated at this facility < 5 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 6,000 Gallon Aeration Bas'�
Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Sludge Holding Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2
FORM: RSC 11-13 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Peritech Inc. and Date of analysis: -
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<2.45
Cadmium
85
39
1.59
Copper
4,300
1,500
288
Lead
840
300
7.94
Mercury
57
17
0.123
Molybdenum
75
n/a
5.25
Nickel
420
420
5.88
Selenium
100
100
24.6
Zinc
7,500
2,800
598
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
FORM: RSC 11-13 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory:lkeritech Inc. and Date of analysis: -
Parameter
Result
(mg/kg)
Aluminum
3,180
Ammonia -Nitrogen
9,020
Calcium
36,200
Magnesium
2,820
Nitrate -Nitrite Nitrogen
<490
pH (Standard Unit)
6.7
Phosphorus
12,000
Potassium
2,320
Sodium
2,990
Total Kjeldahl Nitrogen
53,400
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.58
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
18,314
27,346
Injection/Incorporation
22,824
30,695
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 11-13 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 11-13 Page 5 of 5

it,
Facility Arbor Hills MHP
FIELD LOADING ESTIMATES
Sampling Date 5/24/2019
% Solids 2.04
Mineralization Rate 0.3
Gallons per DT 11,755.30
pH 6.7
Sodium Absorpotion 0.58 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 53,400 lbs./1,000 gal 9.09
Ammonia Nitrogen (mg/Kg) 9,020.00 lbs./1,000 gal 1.53
Nitrate -Nitrite (mg/Kg) 490.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 18,314 lbs./1,000 gal 3.12
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 22,824 lbs./1,000 gal 3.88
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.39
Phosphorus lbs./1,000 gal 2.04
Calcium lbs./1,000 gal 6.16
Magnesium lbs./1,000 gal 0.48
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
2.45
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.59
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
288.00
Copper lbs./1,000 gal
0.05
Lead (mg/Kg)
7.94
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.12
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.88
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
24.60
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
598.00
Zinc lbs./1,000 gal
0.10
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
53,400
18,314
36.63
35,086
53,400
22,824 45.65
30,576
35,086
5,263
10.53
29,823
30,576
4,586 9.17
25,990
29,823
2,237
4.47
27,586
25,990
1,949 3.90
24,040
27,586
1,034
2.07
26,552
24,040
902 1.80
23,139
26,552
498
1.00
26,054
23,139
434 0.87
22,705
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 27,346 54.69
Total 30,695 61.39

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Work Order # 0524d949
Parameters
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Sample: AR052419 Grab
Results Analysis Date
Report Date: 6/11/2019
Project: Arbor Hills
Date Sample Rcvd: 5/24/2019
5/24/19
Reporting Limit Method
%Total Solids
2.04
%
5/29/19
0-100
%
SM 2540B
Ammonia, Nitrogen
9020
mg/kg
6/3/19
10
mg/kg
EPA
350A
TKN
53,400
mg/kg
6/3/19
20
mg/kg
EPA
351.1
Nitrate/Nitrite, Nitrogen
<490
mg/kg
5/29/19
490
mg/lcg
EPA
353.2
Aluminum, total
3,180
mg/kg
5/31/19
2.50
mg/kg
EPA
200.7
Arsenic, total
<2.45
mg/kg
5/31/19
2.45
mg/kg
EPA
2003
Cadmium, total
1.59
mg/kg
5/31/19
0.20
mg/kg
EPA
2003
Calcium, total
36,200
mg/kg
5/31/19
10.0
mg/kg
EPA
200.7
Copper, total
288
mg/kg
5/31/19
1.00
mg/kg
EPA
2003
Lead, total
7.94
mg/kg
5/31/19
0.500
mg/kg
EPA
2003
Magnesium, total
2,820
mg/kg
5/31/19
10.0
mg/k9
EPA
2003
Mercury, total
0.123
mg/kg
6/10/19
0.053
mg/kg
EPA
245.1
Molybdenum, total
5.25
mg/kg
5/31/19
0.500
mg/kg
EPA
200.7
Nickel, total
5.88
mg/kg
5/31/19
2.0
mg/kg
EPA
2003
Phosphorus, total
12,000
mg/kg
5/31/19
2.00
mg/kg
EPA
200.7
Potassium, total
2,320
mg/kg
5/31/19
20.0
mg/kg
EPA
200.7
Selenium, total
24.6
mg/kg
5/31/19
2.63
mg/kg
EPA
200.7
Sodium, total
2,990
mg/kg
5/31/19
20.0
mg/kg
EPA
200.7
Zinc, total
598
mg/kg
5/31/19
0.500
mg/kg
EPA
200.7
pH
6.7
S.U.
5/29/19
1.0 - 14.0
S.U.
SM 4500-HB
I hereby certify thatl have reviewed and approve these data. (�(� 4(�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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APPENDIX 2
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Ashley Hills WWTP
Analytical
Field Loading Calculations

DWR
Diivis on of Water ResoUKes
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Khley Hills WWTP
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or ® Private.
Facility permit issued by: ■ Div. of Water Resources, Div. of Environmental Health,
or ❑l Other (explain: Pp�).
3. Facility contact person and title: Wayne, Lead Operator
Complete mailing address: 815B Hwy 70 East
City: Garner
Telephone number: [phone]
4. Facility physical address: 320 Woods Run
City: m State: NC
Coordinates: Latitude: 35' 45' 19.4"
FORM: RSC 06-16
State: NC Zip: 27529-
E-mail address: Wayne.Leary_gcarolinawaterservicenc.com
Datum: NAD 83
Method of measurement:
Zip: 545-
Longitude: 78' 28' 1.72"
Level of accuracy: Sub -Meter
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0.25 MGD and facility average daily flow: M MGD
8. Average amount of residuals being generated at this facility — 10 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Extended Aeration 230,000 Gallo
Type and volume of residuals storage (i.e., outside of residuals treatment units): (3) Digesters Totaling 120,000 Gallons &
(2) Sludge Holding Tanks Totaling 70,000 Gallons
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: E yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: el yes 0 no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: L] yes A no. Flashpoint: _ OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: 11" mg/kg (<250) & HZS: _ mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(mg/l)
Result
(mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Environment Inc, and Date of analysis: 1/31/18
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
< 2.5
Cadmium
85
39
1.3
Copper
4,300
1,500
386
Lead
840
300
11
Mercury
57
17
0.09
Molybdenum
75
n/a
7
Nickel
420
420
9
Selenium
100
100
< 5.0
Zinc
7,500
2,800
684
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
0 > 25 but < 50
34
220
240
> 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: environment 1, A and Date of analysis: _
Parameter
Result
(mg/kg)
Aluminum
3,473
Ammonia -Nitrogen
2,990
Calcium
17,566
Magnesium
3,454
Nitrate -Nitrite Nitrogen
12.92
pH (Standard Unit)
5.9
Phosphorus
19,900
Potassium
6,246
Sodium
6,182
Total Kjeldahl Nitrogen
62,570
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
19,382
30,500
Injection/Incorporation
20,877
31,610
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

AGMAN
FIELD LOADING ESTIMATES
Facility Ashley Hills WWTP
Sampling Date 1 /31 /2018
% Solids 1.34
Mineralization Rate 0.30
Gallons per DT 17,896.13
PH 5.9
Sodium Absorpotion 1.29 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 62,570 lbs./1,000 gal 6.99
Ammonia Nitrogen (mg/Kg) 2,990.00 lbs./1,000 gal 0.33
Nitrate -Nitrite (mg/Kg) 12.92 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 19,382 lbs./1,000 gal 2.17
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 20,877 lbs./1,000 gal 2.33
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.70
Phosphorus lbs./1,000 gal 2.22
Calcium lbs./1,000 gal 1.96
Magnesium lbs./1,000 gal 0.39
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
386.00
Copper lbs./1,000 gal
0.04
Lead (mg/Ig)
11.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.09
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
9.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
684.00
Zinc lbs./1,000 gal
0.08
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
62,570
19,382
38.76
43,188
62,570
20,877 41.75
41,693
43,188
6,478
12.96
36,710
41,693
6,254 12.51
35,439
36,710
2,753
5.51
33,957
35,439
2,658 5.32
32,781
33,957
1,273
2.55
32,683
32,781
1,229 2.46
31,552
32,683
613
1.23
32,070
31,552
592 1.18
30,960
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 30,500 61.00
Total 31,610 63.22

EEWUhMUMM % hg@
i
P.O. BOX 7085, 114 QAKMONT D91VE
GREENVILLE, N-C, 27835-7085
ASHLEY HILLS (CWS)
C/O CAROLINA WATER SERVICE
315B HWY. 70 EAST
GARNER ,NC 27529
TOW
Sludge
Analysis
Method
PARAMETERS
Sample
Date
Analyst
Code
PH, Units
5.9
02/21/18
KDS
4500HB-11
Aluminum, (dry wt. basis), mg/kg
3473
02/26/18
LFJ .
EPA200.7
Arsenic (dry wt. basis), mgllig
C 2.5
02/26/18
MTM
3113B-04
Calcium (dry wt. basis), mg/kg
17566
02/26/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.3
02126/18
MTM
31131€3-04
Copper (dry wt, basis), mg/kg
386
02/26/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
7
02/26/18
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
11
02/23/18
MTM
3113E-04
Magnesium (dry wt. basis), mg/kg
3454
02126/18
LFJ
EPA200,7
Mercury (dry wt. basis), mg/kg
0.09
02/27/18
MTM
EPA7471B
Nickel (dry wt. basis), mg/kg
9
02/26/18
LFJ
EPA200.7
Potassium (dry wt, basis), mg/kg
6246
02/26/18
LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
C 5.0
02/22/18
MTM
3113E-04
Sodium (dry wt. basis), mg/kg
6192
02/26/18
LFJ
EPA200.7
Zinc (dry wt. basis), mg/kg
684
02/26/18
LFJ
EPA200.7
Total Solids, %
1.34
02/01/18
KAC
2540G-11
T1CN (dry wt.), mg/kg
c 62570
02/22/18
CML
351.2 R2-93
Ammonia Nitrogen (dry wt,),mg/kg
c 2990
03/06/18
MF
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
c 19900
02122/18
DTL
365.4-74
Nitrate -Nitrite (dry wt.), mg/kg
c 12.92
02/23/18
MF
353.2 112-93
Plant Available Nitrogen, mg/kg
19382
03/12/18
SEJ
Molybdenum (dry wt. basis), mg/kg
7
02/26/18
LFJ
EPA200.7
n
Dxirtking Water !Dz 3'715..
waote:rater ZD; 10
PHONE [phone]
FAX [phone]
ID#: 621 S
DATE COLLECTED: 01/31/18
DATES REPORTED : 03/1.3/18
REVIEWED BY:
0 Uncertifiad data. DWR doae not offer non-aquaoue certification for this analytical procedure.

Meritech, Inc.
°a
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Contact: Drew Matthews
Report Date:
5/3/2019
Client: Soil Plus
P.O. Box 1396
Project:
Ashley Hills
Oxford, NC 27565
Date Sample Rcvd:
4/23/2019
Meritech Work Order #
04231976
Sample:
AH042319 (001)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
1.36
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
117,647
col/g dry wt
4/23/19
208 col/g dry wt
SM 9222D
Meritech Work Order #
04231977
Sample:
AH042319 (002)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
0.95
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
452,632
col/g drywt
4/23/19
208 col/g dry wt
SM 9222D
Meritech Work Order #
04231978
Sample:
AH042319 (003)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
0.89
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
595,506
col/g dry wt
4/23/19
208 col/g dry wt
SM 9222D
Meritech Work Order #
04231979
Sample:
AH042319 (004)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
%Total Solids
1.00
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform (Sludge)
470,000
col/g dry wt
4/23/19
208 col/g dry wt
SM 9222D
Meritech Work Order #
04231980
Sample:
AH042319 (005)
Grab
4/23/19
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
Fecal Coliform (Sludge)
1.03
407,767
%
col/g dry wt
4/25/19
4/23/19
0-100
208
%
col/g dry wt
SM
SM
2540B
9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
Page 2
2019
Ashley Hills
4/23/2019
Meritech Work
Order #
04231881
Sample:
AH042319 (006)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
1.36
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform
(Sludge)
220,588
col/g dry wt
4/23/19
208
col/g dry wt
SM 9222D
Meritech Work
Order #
04231982
Sample:
AH042319 (007)
Grab
4/23/19
Parameters
Results
Analysis Date
Reporting
Limit
Method
% Total Solids
1.37
%
4/25/19
0-100
%
SM 2540B
Fecal Coliform
(Sludge)
204,380
col/g dry wt
4/23/19
208
col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data, r�a^i�
LaboratoryRepresentative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date:
Project:
Date Sample Rcvd:
5/30/2019
Ashley Hills
4/23/2019
Vector Attraction Reduction /Aerobically Digested Sludge (30 Day Test)
Meritech Work Order # 04231975
Week 1
Week 2
Week 3
Week 4
Week 5
Total
Solids
0.880
0.700
0.540
0.690
0.800
Sample: AH042319 Grab
Volatile Solids
0.740
0.560
0.450
0.510
0.590
4/23/19
Volatile Solids
0.834
0.799
0.825
0.738
0.742
Mass Balance Equation =11.07%Volatile Solids Reduction as per EPA Part 503 Biosolids Rule
I hereby certify' that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
teL[phone]fax.[phone]

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APPENDIX 3
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Birchwood RV Park WWTP
Analytical
Field Loading Calculations

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
DiivisIon of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Mchwood RV Park
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ® Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: �.
3. Facility contact person and title: Jay Murray
Complete mailing address: F901 Wilkins Dr
City: Durham State: NC Zip: 27705-
Telephone number: [phone] E-mail address: birchwoodrvparkgyahoo.com
4. Facility physical address: 5901 Wilkins Dr
City: - State: NC Zip: 705-
Coordinates: Latitude: 35' 59' 06.0" Longitude: 79' 00' 00.4"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: .018 MGD and facility average daily flow: M MGD
8. Average amount of residuals being generated at this facility < 5 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 18,000 Gallons Extended Aeration
Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Primary Sludge Storage
Tank & 10,000 Gallon Secondary Sludge Storage Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
FORM: RSC 11-13 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): _
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: E yes M no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: el yes 0 no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: L] yes A no. Flashpoint: _ OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: 11" mg/kg (<250) & HZS: _ mg/kg (<500)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(mg/l)
Result
(mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: eritech Inc and Date of analysis:
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<4.13
Cadmium
85
39
1.95
Copper
4,300
1,500
181
Lead
840
300
4.42
Mercury
57
17
0.372
Molybdenum
75
n/a
4.42
Nickel
420
420
7.25
Selenium
100
100
10.7
Zinc
7,500
2,800
740
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
0 > 25 but < 50
34
220
240
> 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory:lkeritech Inc. and Date of analysis: 05/29/19
Parameter
Result
(mg/kg)
Aluminum
2,790
Ammonia -Nitrogen
5,240
Calcium
13,700
Magnesium
3,140
Nitrate -Nitrite Nitrogen
<826
pH (Standard Unit)
6.5
Phosphorus
9,420
Potassium
3,540
Sodium
4,260
Total Kjeldahl Nitrogen
75,000
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.94
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
24,374
37,406
Injection/Incorporation
26,994
39,352
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

it,
Facility Birchwood
FIELD LOADING ESTIMATES
Sampling Date 5/29/2019
% Solids 1.21
Mineralization Rate 0.3
Gallons per DT 19,818.86
pH 6.5
Sodium Absorpotion 0.94 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 75,000 lbs./1,000 gal 7.57
Ammonia Nitrogen (mg/Kg) 5,240.00 lbs./1,000 gal 0.53
Nitrate -Nitrite (mg/Kg) 826.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 24,374 lbs./1,000 gal 2.46
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 26,994 lbs./1,000 gal 2.72
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.36
Phosphorus lbs./1,000 gal 0.95
Calcium lbs./1,000 gal 1.38
Magnesium lbs./1,000 gal 0.32
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
4.13
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.95
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
181.00
Copper lbs./1,000 gal
0.02
Lead (mg/Kg)
4.42
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.37
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
7.25
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
10.70
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
740.00
Zinc lbs./1,000 gal
0.07
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
75,000
24,374
48.75
50,626
75,000
26,994 53.99
48,006
50,626
7,594
15.19
43,032
48,006
7,201 14.40
40,805
43,032
3,227
6.45
39,805
40,805
3,060 6.12
37,745
39,805
1,493
2.99
38,312
37,745
1,415 2.83
36,329
38,312
718
1.44
37,594
36,329
681 1.36
35,648
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 37,406 74.81
Total 39,352 78.70

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Worlc Order # 05291978
Parameters
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Sample: TP052919 Grab
Results Analysis Date
Report Date: 6/11/2019
Project: Triangle RV Park
Date Sample Rcvd: 5/29/2019
5/29/19
Reporting Limit Method
%Total Solids
1.21
%
5/30/19
0-100
%
SM 2540B
Ammonia, Nitrogen
5,240
mg/kg
6/3/19
10
mg/kg
EPA
350A
TKN
75,000
mg/kg
6/3/19
20
mg/kg
EPA
351.1
Nitrate/Nitrite, Nitrogen
<826
mg/kg
5/30/19
826
mg/kg
EPA
353.2
Aluminum, total
2,790
mg/kg
6/5/19
2,50
mg/kg
EPA
200.7
Arsenic, total
<4.13
mg/kg
6/5/19
4.13
mg/kg
EPA
200.7
Cadmium, total
1.95
mg/kg
6/5/19
0.20
mg/kg
EPA
2003
Calcium, total
131700
mg/kg
6/5/19
10.0
mg/kg
EPA
2003
Copper, total
181
mg/kg
6/5/19
1.00
mg/kg
EPA
200.7
Lead, total
4.42
mg/kg
6/5/19
0.500
mg/kg
EPA
200.7
Magnesium, total
3,140
mg/kg
6/5/19
10.0
mg/kg
EPA
2003
Mercury, total
0.372
mg/kg
6/10/19
0.053
mg/kg
EPA
245A
Molybdenum, total
4.42
mg/kg
6/5/19
0.500
mg/kg
EPA
2003
Nickel, total
7.25
mg/kg
6/5/19
2.0
mg/kg
EPA
2003
Phosphorus, total
9,420
mg/kg
6/5/19
2.00
mg/kg
EPA
2003
Potassium, total
3,540
mg/kg
6/5/19
20.0
mg/kg
EPA
200.7
Selenium, total
10.7
mg/kg
6/5/19
2.63
mg/kg
EPA
200.7
Sodium, total
4,260
mg/kg
6/5/19
20.0
mg/kg
EPA
200.7
Zinc, total
740
mg/kg
6/5/19
0.500
mg/kg
EPA
2003
PH
6.5
S.U.
5/30/19
1.0 - 14.0
S.U.
SM 4500-HB
/hereby certify that I have reviewed and approve these data. � ''�?`} �(�, ��(�(`(� (�i (��
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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APPENDIX 4
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Chapel Ridge WWTP
Analytical
Field Loading Calculations

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ® Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: M.
3. Facility contact person and title: Roger Tupps, Area Manager
Complete mailing address: F02 MacKenan Court
City: = State: NC Zip: 27597-
Telephone number: [phone] E-mail address: RBTupTskaquaamerica.com
4. Facility physical address: Hardwood Forest Trail
City: - State: NC Zip: 7� 312-
Coordinates: Latitude: 35' 47' 7.4" Longitude: M° J4' 10.7"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0 MGD and facility average daily flow: 0.07 MGD
8. Average amount of residuals being generated at this facility E dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 70,000 gallon Aeration;
Type and volume of residuals storage (i.e., outside of residuals treatment units): 90,000 gallon Sludge Storage Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Peritech Inc. and Date of analysis: 06/19/19
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<0.963
Cadmium
85
39
1.89
Copper
4,300
1,500
717
Lead
840
300
29.5
Mercury
57
17
0.125
Molybdenum
75
n/a
1.95
Nickel
420
420
18.1
Selenium
100
100
1.38
Zinc
7,500
2,800
2,470
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory:lkeritech Inc. and Date of analysis: 06/19/19
Parameter
Result
(mg/kg)
Aluminum
19,500
Ammonia -Nitrogen
320
Calcium
25,600
Magnesium
3,240
Nitrate -Nitrite Nitrogen
102
pH (Standard Unit)
6.6
Phosphorus
20,200
Potassium
1,500
Sodium
3,510
Total Kjeldahl Nitrogen
16,600
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.25
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
5,146
8,095
Injection/Incorporation
5,306
8,213
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

it,
FIELD LOADING ESTIMATES
Facility Chapel Ridge WWTP
Sampling Date 6/19/2019
% Solids 5.19
Mineralization Rate 0.30
Gallons per DT 4,620.58
pH 6.6
Sodium Absorpotion 1.25 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 16,600 lbs./1,000 gal 7.19
Ammonia Nitrogen (mg/Kg) 320.00 lbs./1,000 gal 0.14
Nitrate -Nitrite (mg/Kg) 102.00 lbs./1,000 gal 0.04
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 5,146 lbs./1,000 gal 2.23
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 5,306 lbs./1,000 gal 2.30
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.65
Phosphorus lbs./1,000 gal 8.74
Calcium lbs./1,000 gal 11.08
Magnesium lbs./1,000 gal 1.40
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
0.96
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.89
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
717.00
Copper lbs./1,000 gal
0.31
Lead (mg/Kg)
29.50
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.13
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
18.10
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
1.38
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
2470.00
Zinc lbs./1,000 gal
1.07
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
16,600
5,146
10.29
11,454
16,600
5,306 10.61
11,294
11,454
1,718
3.44
9,736
11,294
1,694 3.39
9,600
9,736
730
1.46
9,006
9,600
720 1.44
8,880
9,006
338
0.68
8,668
8,880
333 0.67
8,547
8,668
163
0.33
8,505
8,547
160 0.32
8,387
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 8,095 16.19
Total 8,213 16.43

Meritech, Inc.
x;Environmental Laboratory
Laboratory Certification No. 165
Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Date
Report Date:
Project:
Sample Rcvd:
7/2/2019
Chapel Ridge
6/19/2019
Meritech Work Order # 061919114
Sample:
CR061919 Grab
6/19/19
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
5.19
%
6/21/19
0-100
%
SM 2540B
Ammonia, Nitrogen
320
mg/kg
6/25/19
10
mg/kg
EPA 350.1
TKN
16,600
mg/kg
6/27/19
20
mg/kg
EPA 351.1
Nitrate/Nitrite, Nitrogen
102
mg/kg
6/21/19
31.3
mg/kg
EPA 353.2
Aluminum, total
19,500
mg/kg
6/27/19
2.50
mg/kg
EPA 2003
Arsenic, total
<0.963
mg/kg
6/27/19
0.963
mg/kg
EPA 2003
Cadmium, total
1.89
mg/kg
6/27/19
0.20
mg/kg
EPA 2003
Calcium, total
25,600
mg/kg
6/27/19
10.0
mg/kg
EPA 2003
Copper, total
717
mg/kg
6/27/19
1.00
mg/kg
EPA 2003
Lead, total
29.5
mg/kg
6/27/19
0.500
mg/kg
EPA 200.7
Magnesium, total
3,240
mg/kg
6/27/19
10.0
mg/kg
EPA 2003
Mercury, total
0.125
mg/kg
6/25/19
0.02
mg/kg
EPA 245A
Molybdenum, total
1.95
mg/kg
6/27/19
0.500
mg/kg
EPA 2003
Nickel, total
18.1
mg/kg
6/27/19
2.0
mg/kg
EPA 2003
Phosphorus, total
20,200
mg/kg
6/27/19
2.00
mg/kg
EPA 2003
Potassium, total
1,500
mg/kg
6/27/19
20.0
mg/kg
EPA 200.7
Selenium, total
1.38
mg/kg
6/27/19
0.50
mg/kg
EPA 2003
Sodium, total
3,510
mg/kg
6/27/19
20.0
mg/kg
EPA 2003
Zinc, total
2,470
mg/kg
6/27/19
0.500
mg/kg
EPA 2003
pH
6.6
S.U.
6/20/19
1.0 - 14.0
S.U.
SM 4500-HB
I hereby certi/y that 1 have reviewed and approve these data. � (� ��
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.(336]342-1522

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APPENDIX 5
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Cottonwood/Baywood WWTP
Analytical
Field Loading Calculations

DWR
Division of Water ResoUKes
State of North Carolina
Department of Environment and Natural Resources
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Cottonwood/Baywood WWI
2. Facility permit holder is: ❑ Federal, A State, 0 Local Government, or ® Private.
Facility permit issued by: ■ Div. of Water Resources, Div. of Environmental Health,
or ❑ Other (explain: �.
3. Facility contact person and title: Lucille C. Ginsbere
Complete mailing address: 7536 NC HWY 39
City: Zebulon State: NC Zip: 27597
Telephone number: [phone] E-mail address: [e-mail]
4. Facility physical address: Bethlehem Road
City: m State: NC Zip: 545-
Coordinates: Latitude: 35' 45' 42.9" Longitude: 78' 28' 24.6"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: Q95A MGD and facility average daily flow: = MGD
8. Average amount of residuals being generated at this facility E dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 0.0575 MG Extended Aeration'
Type and volume of residuals storage (i.e., outside of residuals treatment units): 13,000 Gallon Sludge Holding Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: environment 1, A and Date of analysis: 3/26/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<2.5
Cadmium
85
39
1.3
Copper
4,300
1,500
208
Lead
840
300
11
Mercury
57
17
0.57
Molybdenum
75
n/a
13
Nickel
420
420
8
Selenium
100
100
<5.0
Zinc
7,500
2,800
1,166
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: environment 1, Ir>♦ and Date of analysis: 03/26/2019
Parameter
Result
(mg/kg)
Aluminum
3,157
Ammonia -Nitrogen
509.1
Calcium
16,306
Magnesium
3,008
Nitrate -Nitrite Nitrogen
113.4
pH (Standard Unit)
6.8
Phosphorus
25,610
Potassium
6,585
Sodium
21,932
Total Kjeldahl Nitrogen
46,270
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): -
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
14,096
22,379
Injection/Incorporation
14,351
22,568
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

it,
Facility Cottonwood/Baywood WWTP
FIELD LOADING ESTIMATES
Sampling Date 3/26/2019
% Solids 0.49
Mineralization Rate 0.3
Gallons per DT 48,940.44
pH 6.8
Sodium Absorpotion 2.89 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 46,270 lbs./1,000 gal 1.89
Ammonia Nitrogen (mg/Kg) 509.10 lbs./1,000 gal 0.02
Nitrate -Nitrite (mg/Kg) 113.40 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 14,096 lbs./1,000 gal 0.58
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 14,351 lbs./1,000 gal 0.59
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.27
Phosphorus lbs./1,000 gal 1.05
Calcium lbs./1,000 gal 0.67
Magnesium lbs./1,000 gal 0.12
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
208.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
11.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.57
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
8.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1166.00
Zinc lbs./1,000 gal
0.05
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
46,270
14,096
28.19
32,174
46,270
14,351 28.70
31,919
32,174
4,826
9.65
27,348
31,919
4,788 9.58
27,131
27,348
2,051
4.10
25,297
27,131
2,035 4.07
25,096
25,297
949
1.90
24,348
25,096
941 1.88
24,155
24,348
457
0.91
23,891
24,155
453 0.91
23,702
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 22,379 44.76
Total 22,568 45.14

114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
COTTONWOOD
ATTN: LUCI CROSBY
CROSBY WATER & SEWER
7536 NC HWY 39 SOUTH
ZEBULON ,NC 27807
PARAMETERS
PH (not to be used for reporting)
Aluminum, (dry wt. basis), mglkg
Arsenic (dry wt. basis), mglkg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mglkg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6.8
03/26/19
TCW
4500HB-11
3157
04/04/19
LFJ
EPA200.7
2.5
04/04/19
MTM
3113B-04
16306
04/04/19
LFJ
EPA200.7
1.3
04/08/19
MTM
3113B-04
208
04/04/19
LFJ
EPA200.7
6
04/04/19
LFJ
EPA200.7
11
04/05/19
MTM
3113B-04
3008
04/04/19
LFJ
EPA200.7
0.57
04/17/19
MTM
EPA7471B
8
04/04/19
LFJ
EPA200.7
6585
04/04/19
LFJ
EPA200.7
C5.0
04/10/19
MTM
3113B-04
21932
04/18/19
AKS
3111B-11
1166
04/04/19
LFJ
EPA200.7
0.49
03/28/19
KDS
254OG-11
c 46270
03/29/19
TLH
351.2 R2-93
c 509.1
04/01/19
CLO
350.1 R2-93
c 25610
04/02/19
CLO
365.4-74
c 113.4
04/02/19
DTL
353.2 R2-93
14096
04/05/19
SEJ
13
04/04/19
LFJ
EPA200.7
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
ID#: 339 C
DATE COLLECTED: 03/26/19
DATE REPORTED : 04/22/19
REVIEWED BY:
c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure.

APPENDIX 6
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Lake Royale WWTP
Analytical
Field Loading Calculations

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: Federal, 0 State, 11 Local Government, or ® Private.
Facility permit issued by: Div. of Water Resources, IN Div. of Environmental Health,
or Other (explain: `).
3. Facility contact person and title: Total Environmental Solutions, Inc.
Complete mailing address: P.O. Box 14059
City: Baton Rouge State: Zip: 70898-4059
Telephone number: 52) 478-4704 E-mail address: dhartgtesi-usa.com
4. Facility physical address: NCSR 1611
City: � State: NC Zip: 7549-
Coordinates: Latitude: 35' 57' 0111" Longitude: 78' 11' 27.0"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes ® No
7. Facility permitted/design flow: 0.080 MGD and facility average daily flow: 0.0027 MGD
8. Average amount of residuals being generated at this facility < 5 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 0.08 MG Aeration Tank(s)
Type and volume of residuals storage (i.e., outside of residuals treatment units): 5,000 Gallon Sludge Holding Tank
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: _ and Date of analysis: _
Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: Eyes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
Hexachlorobenzene
0.13
Barium
100.0
Hexachloro-1,3-Butadiene
0.5
Benzene
0.5
Hexachloroethane
3.0
Cadmium
1.0
Lead
5.0
Carbon Tetrachloride
0.5
Lindane
0.4
Chlordane
0.03
Mercury
0.2
Chlorobenzene
100.0
Methoxychlor
10.0
Chloroform
6.0
Methyl Ethyl Ketone
200.0
Chromium
5.0
Nitrobenzene
2.0
m-Cresol
200.0
Pentachlorophenol
100.0
o-Cresol
200.0
Pyridine
5.0
p-Cresol
200.0
Selenium
1.0
Cresol
200.0
Silver
5.0
2,4-D
10.0
Tetrachloroethylene
0.7
1,4-Dichlorobenzene
7.5
Toxaphene
0.5
1,2-Dichloroethane
0.5
Trichloroethylene
0.5
1,1-Dichloroethylene
0.7
2,4,5-Trichlorophenol
400.0
2,4-Dinitrotoluene
0.13
2,4,6-Trichlorophenol
2.0
Endrin
0.02
2,4,5-TP (Silvex)
1.0
Heptachlor and its Hydroxide
0.008
Vinyl Chloride
0.2

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Peritech Inc. and Date of analysis: -
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<1.81
Cadmium
85
39
3.97
Copper
4,300
1,500
750
Lead
840
300
42.8
Mercury
57
17
0.217
Molybdenum
75
n/a
5.29
Nickel
420
420
10.4
Selenium
100
100
2.22
Zinc
7,500
2,800
1,880
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory:lkeritech Inc. and Date of analysis: -
Parameter
Result
(mg/kg)
Aluminum
10,500
Ammonia -Nitrogen
2,620
Calcium
11,500
Magnesium
1,440
Nitrate -Nitrite Nitrogen
<361
pH (Standard Unit)
6.7
Phosphorus
10,300
Potassium
1,780
Sodium
2,380
Total Kjeldahl Nitrogen
20,600
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.92
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
7,065
10,549
Injection/Incorporation
8,375
11,522
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

it,
FIELD LOADING ESTIMATES
Facility Lake Royale
Sampling Date 5/31/2019
% Solids 2.77
Mineralization Rate 0.30
Gallons per DT 8,657.33
pH 6.7
Sodium Absorpotion 0.92 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 20,600 lbs./1,000 gal 4.76
Ammonia Nitrogen (mg/Kg) 2,620.00 lbs./1,000 gal 0.61
Nitrate -Nitrite (mg/Kg) 361.00 lbs./1,000 gal 0.08
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 7,065 lbs./1,000 gal 1.63
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 8,375 lbs./1,000 gal 1.93
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.41
Phosphorus lbs./1,000 gal 2.38
Calcium lbs./1,000 gal 2.66
Magnesium lbs./1,000 gal 0.33
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
1.81
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
3.97
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
750.00
Copper lbs./1,000 gal
0.17
Lead (mg/Kg)
42.80
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.22
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.40
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
2.22
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
1880.00
Zinc lbs./1,000 gal
0.43
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN
PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
20,600
7,065
14.13
13,535
20,600
8,375
16.75
12,225
13,535
2,030
4.06
11,505
12,225
1,834
3.67
10,391
11,505
863
1.73
10,642
10,391
779
1.56
9,612
10,642
399
0.80
10,243
9,612
360
0.72
9,251
10,243
192
0.38
10,051
9,251
173
0.35
9,078
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 10,549 21.10
Total 11,522 23.04

Contact: Drew Matthews
Client: Soil Plus
P.O. Box 1396
Oxford, NC 27565
Meritech Work Order # 05311923
Parameters
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Sample: LR053119 Grab
Results Analysis Date
Report Date:
Project:
Date Sample Rcvd:
6/12/2019
Lake Royale
5/31/2019
5/31/19
RenortingLimit Method
%Total Solids
2.77
%
6/5/19
0-100
%
SM 2540B
Ammonia, Nitrogen
2620
mg/kg
6/6/19
10
mg/kg
EPA
350.1
TKN
20,600
mg/kg
6/7/19
20
mg/kg
EPA
351.1
Nitrate/Nitrite, Nitrogen
<361
mg/kg
6/4/19
361
mg/kg
EPA
353.2
Aluminum, total
10,500
mg/kg
6/5/19
2,50
mg/kg
EPA
200.7
Arsenic, total
<1.81
mg/kg
6/5/19
1.81
mg/kg
EPA
200.7
Cadmium, total
3.97
mg/kg
6/5/19
0.20
mg/kg
EPA
200.7
Calcium, total
11,500
mg/kg
6/5/19
10.0
mg/kg
EPA
200.7
Copper, total
750
mg/kg
6/5/19
1.00
mg/kg
EPA
200.7
Lead, total
42.8
mg/kg
6/5/19
0.500
mg/kg
EPA
200.7
Magnesium, total
1,440
mg/kg
6/5/19
10.0
mg/kg
EPA
200.7
Mercury, total
0.217
mg/kg
6/10/19
0.02
mg/kg
EPA
245.1
Molybdenum, total
5.29
mg/kg
6/5/19
0.500
mg/kg
EPA
200.7
Nickel, total
10.4
mg/kg
6/5/19
2.0
mg/kg
EPA
200.7
Phosphorus, total
10,300
mg/kg
6/5/19
2.00
mg/kg
EPA
200.7
Potassium, total
1,780
mg/kg
6/5/19
20.0
mg/kg
EPA
2003
Selenium, total
2.22
mg/kg
6/5/19
2.63
mg/kg
EPA
200.7
Sodium, total
2,380
mg/kg
6/5/19
20.0
mg/kg
EPA
200.7
Zinc, total
1,880
mg/kg
6/5/19
0.500
mg/kg
EPA
2003
pH
6.7
S.U.
6/4/19
1.0 - 14.0
S.U.
SM 4500-HB
I hereby certify that 1 have reviewed and approve these data. �, (�(' �)
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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APPENDIX 7
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Town of Pittsboro WWTP
Analytical
Field Loading Calculations

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Town of Pittsboro WWTP
2. Facility permit holder is: ❑ Federal, 0 State, M Local Government, or ❑ Private.
Facility permit issued by: Div. of Water Resources, IN Div. of Environmental Health,
or Other (explain: `).
3. Facility contact person and title: Jamie McLaurin, WWTP Superintendent
Complete mailing address: P.O. Box 759
City: Pittsboro State: NC Zip: 27312-
Telephone number: 919) 542-2444 E-mail address: jmclaurinkpittsboronc.gov
4. Facility physical address: 485 Small St.
City: — State: NC Zip: 77312-
Coordinates: Latitude: 35' 42' 51.9" Longitude: M° JO' 12.5"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0.75 MGD and facility average daily flow: 0 MGD
8. Average amount of residuals being generated at this facility — 100 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 0.75 MG Extended Aeratio7
Type and volume of residuals storage (i.e., outside of residuals treatment units): 180,000 Gallon Sludge e T
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: lummit Environmental Technologies, In and Date of analysis: -
Passed corrosivity test: ® yes ❑ no. pH: 6.9 s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: Non -Flammable IF (> 140°F)
Passed reactivity test: ® yes Eno. HCN: � mg/kg (<250) & H2S: M mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
<1.25
Hexachlorobenzene
0.13
<0.0400
Barium
100.0
<12.5
Hexachloro-1,3-Butadiene
0.5
<0.0160
Benzene
0.5
<0.125
Hexachloroethane
3.0
<0.0800
Cadmium
1.0
<0.250
Lead
5.0
<1.25
Carbon Tetrachloride
0.5
<0.125
Lindane
0.4
<0.00500
Chlordane
0.03
<0.0250
Mercury
0.2
<0.00500
Chlorobenzene
100.0
<0.125
Methoxychlor
10.0
<0.00500
Chloroform
6.0
<0.125
Methyl Ethyl Ketone
200.0
<0.625
Chromium
5.0
<0.500
Nitrobenzene
2.0
<0.0800
m-Cresol
200.0
2.72
Pentachlorophenol
100.0
<0.200
o-Cresol
200.0
<0.200
Pyridine
5.0
<0.200
p-Cresol
200.0
2.72
Selenium
1.0
<0.125
Cresol
200.0
<4.00
Silver
5.0
<1.25
2,4-D
10.0
<0.500
Tetrachloroethylene
0.7
<0.125
1,4-Dichlorobenzene
7.5
<0.0800
Toxaphene
0.5
<0.0500
1,2-Dichloroethane
0.5
<0.125
Trichloroethylene
0.5
<0.125
1,1-Dichloroethylene
0.7
<0.125
2,4,5-Trichlorophenol
400.0
<0.200
2,4-Dinitrotoluene
0.13
<0.0400
2,4,6-Trichlorophenol
2.0
<0.200
Endrin
0.02
<0.00500
2,4,5-TP (Silvex)
1.0
<0.5
Heptachlor and its Hydroxide
0.008
<0.00500
Vinyl Chloride
0.2
<0.0500

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: lace Analytical and Date of analysis: 1/23/2019
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
<8.9
Cadmium
85
39
1.1
Copper
4,300
1,500
149
Lead
840
300
6.8
Mercury
57
17
0.40
Molybdenum
75
n/a
5.1
Nickel
420
420
17.2
Selenium
100
100
<8.9
Zinc
7,500
2,800
299
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 0 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: hce Analytical and Date of analysis: 1/23/2019
Parameter
Result
(mg/kg)
Aluminum
43,700
Ammonia -Nitrogen
14,600
Calcium
7,940
Magnesium
2,530
Nitrate -Nitrite Nitrogen
<25.5
pH (Standard Unit)
7.1
Phosphorus
21,900
Potassium
<4,440
Sodium
<4,440
Total Kjeldahl Nitrogen
67,900
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
23,316
34,793
Injection/Incorporation
30,616
40,213
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

it,
FIELD LOADING ESTIMATES
Facility Town of Pittsboro WWTP
Sampling Date 1/23/2019
% Solids 7.4
Mineralization Rate 0.30
Gallons per DT 3,240.65
pH 7.1
Sodium Absorpotion 3.01 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 67,900 lbs./1,000 gal 41.91
Ammonia Nitrogen (mg/Kg) 14,600.00 lbs./1,000 gal 9.01
Nitrate -Nitrite (mg/Kg) 25.50 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 23,316 lbs./1,000 gal 14.39
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 30,616 lbs./1,000 gal 18.89
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ceiling
Limits (mg/Kg) Limits (mg/Kg)
41 75
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
1 st Year
2nd Year
3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 2.74
Phosphorus lbs./1,000 gal 13.52
Calcium lbs./1,000 gal 4.90
Magnesium lbs./1,000 gal 1.56
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
8.90
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
1.10
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
149.00
Copper lbs./1,000 gal
0.09
Lead (mg/Kg)
6.80
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.40
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
17.20
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
8.90
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
299.00
Zinc lbs./1,000 gal
0.18
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
67,900
23,316
46.63
44,585
67,900
30,616 61.23
37,285
44,585
6,688
13.38
37,897
37,285
5,593 11.19
31,692
37,897
2,842
5.68
35,055
31,692
2,377 4.75
29,315
35,055
1,315
2.63
33,740
29,315
1,099 2.20
28,216
33,740
633
1.27
33,107
28,216
529 1.06
27,687
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 34,793 69.59
Total 40,213 80.43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 05, 2019
Ms. Melinda Boyd
Synagro
284 Boger Road
Mocksville, NC 27028
RE: Project: Pittsboro WWTP
Pace Project No.: 92415607
Dear Ms. Boyd:
Enclosed are the analytical results for sample(s) received by the laboratory on January 29, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
�pQ AC RFb
REPORT OF LABORATORY ANALYSIS
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Project: Pittsboro WWTP
Pace Project No.: 92415607
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Pittsboro WWTP
92415607
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92415607001
Pittsboro
EPA 601OD
SH1
13
PASI-A
EPA 7471 B
RDT
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271OB-2011
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
DMN
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
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ANALYTICAL RESULTS
Project: Pittsboro WWTP
Pace Project No.: 92415607
Sample: Pittsboro
Lab ID: 92415607001 Collected:
01/23/19
16:00
Received: 01/29/19 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
43700 mg/kg
88.8
1
01/31/19 10:25
01/31/19 22:51
7429-90-5
Arsenic
ND mg/kg
8.9
1
01/31/19 10:25
01/31/19 22:51
7440-38-2
Cadmium
1.1 mg/kg
0.89
1
01/31/19 10:25
01/31/19 22:51
7440-43-9
Calcium
7940 mg/kg
88.8
1
01/31/19 10:25
02/01/19 20:02
7440-70-2
Copper
149 mg/kg
4.4
1
01/31/19 10:25
01/31/19 22:51
7440-50-8
Lead
6.8 mg/kg
4.4
1
01/31/19 10:25
01/31/19 22:51
7439-92-1
Magnesium
2530 mg/kg
88.8
1
01/31/19 10:25
01/31/19 22:51
7439-95-4
Molybdenum
5.1 mg/kg
4.4
1
01/31/19 10:25
01/31/19 22:51
7439-98-7
Nickel
17.2 mg/kg
4.4
1
01/31/19 10:25
01/31/19 22:51
7440-02-0
Potassium
ND mg/kg
4440
1
01/31/19 10:25
01/31/19 22:51
7440-09-7
Selenium
ND mg/kg
8.9
1
01/31/19 10:25
01/31/19 22:51
7782-49-2
Sodium
ND mg/kg
4440
1
01/31/19 10:25
01/31/19 22:51
7440-23-5
Zinc
299 mg/kg
8.9
1
01/31/19 10:25
01/31/19 22:51
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Mercury
0.40 mg/kg
0.027
1
01/29/1918:07
01/30/1913:10
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
7.4 %
0.10
1
01/30/19 13:34
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
92.6 %
0.10
1
01/30/19 13:26
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
7.1 Std. Units
0.10
1
01/30/19 21:43
H3
Plant Available Nitrogen
Analytical Method: SM 271OB-2011
Plant Available Nitrogen
23300 mg/kg
0.12
1
02/05/19 15:35
N2
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0
1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
14600 mg/kg
260
2
02/03/19 13:33
02/03/19 18:10
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0
1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
67900 mg/kg
2600
5
02/02/19 02:22
02/05/19 00:53
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0
1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mg/kg
25.5
1
02/05/19 09:43
02/05/19 14:06
Nitrogen, Nitrate
ND mg/kg
25.5
1
02/05/19 09:43
02/05/19 14:06
14797-55-8
Nitrogen, Nitrite
ND mg/kg
12.7
1
02/05/19 09:43
02/05/19 14:06
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0
1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Phosphorus
21900 mg/kg
613
50
02/01/19 19:38
02/01/19 22:41
7723-14-0
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QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 455116
Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92415607001
METHOD BLANK: 2484636
Matrix: Solid
Associated Lab Samples: 92415607001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060
01/30/1912:24
LABORATORY CONTROL SAMPLE: 2484637
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
0.083 0.074
89 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2484698 2484699
MS MSD
92415499010
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.68
0.055 0.058 1.1
1.1 780 766 75-125 1 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 455551 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92415607001
METHOD BLANK: 2486503
Associated Lab Samples: 92415607001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
02/01/1919:41
Arsenic
mg/kg
ND
1.0
01/31/19 21:33
Cadmium
mg/kg
ND
0.10
01/31/19 21:33
Calcium
mg/kg
ND
10.0
02/01/1919:41
Copper
mg/kg
ND
0.50
01/31/19 21:33
Lead
mg/kg
ND
0.50
01/31/19 21:33
Magnesium
mg/kg
ND
10.0
01/31/19 21:33
Molybdenum
mg/kg
ND
0.50
01/31/19 21:33
Nickel
mg/kg
ND
0.50
01/31/19 21:33
Potassium
mg/kg
ND
500
01/31/19 21:33
Selenium
mg/kg
ND
1.0
01/31/19 21:33
Sodium
mg/kg
ND
500
01/31/19 21:33
Zinc
mg/kg
ND
1.0
01/31/19 21:33
LABORATORY CONTROL SAMPLE:
2486504
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Qualifiers
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
500
486
97
80-120
50
47.7
95
80-120
50
48.1
96
80-120
500
478
96
80-120
50
50.6
101
80-120
50
48.2
96
80-120
500
479
96
80-120
50
51.8
104
80-120
50
48.8
98
80-120
500
ND
97
80-120
50
44.0
88
80-120
500
474J
95
80-120
50
48.3
97
80-120
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2486505
2486506
MS
MSD
92415417001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Aluminum mg/kg
24000
17700
19200
58100
60400
192
189
75-125 4 M1
Arsenic mg/kg
ND
1770
1920
1680
1780
95
93
75-125 6
Cadmium mg/kg
ND
1770
1920
1680
1800
94
93
75-125 7
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Pittsboro WWTP
92415607
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2486505
2486506
MS
MSD
92415417001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
23400
17700
19200
39400
40700
90
90
75-125
3
Copper
mg/kg
1170
1770
1920
2940
3060
100
98
75-125
4
Lead
mg/kg
97.6
1770
1920
1740
1900
93
94
75-125
8
Magnesium
mg/kg
6320
17700
19200
23100
24800
95
96
75-125
7
Molybdenum
mg/kg
28.1
1770
1920
1810
1960
101
101
75-125
8
Nickel
mg/kg
90.3
1770
1920
1770
1910
95
95
75-125
8
Potassium
mg/kg
ND
17700
19200
28700
30100
98
98
75-125
5
Selenium
mg/kg
ND
1770
1920
1470
1580
82
81
75-125
7
Sodium
mg/kg
ND
17700
19200
21000
22400
93
93
75-125
6
Zinc
mg/kg
1150
1770
1920
2790
2950
93
94
75-125
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 455370 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92415607001
SAMPLE DUPLICATE: 2485661
92414482001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 50.1 54.8 9
SAMPLE DUPLICATE: 2485662
92415720001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 86.6 86.4 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 455326 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92415607001
SAMPLE DUPLICATE: 2485362
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 2485363
Parameter
pH at 25 Degrees C
92414839001 Dup
Units Result Result RPD Qualifiers
Std. Units 10.9 10.9 0 H3
92414876001 Dup
Units Result Result RPD Qualifiers
Std. Units 6.4 6.3 1 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 456068
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1
Ammonia
Associated Lab Samples: 92415607001
METHOD BLANK: 2488656
Matrix: Solid
Associated Lab Samples: 92415607001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 9.1
02/03/19 16:55
LABORATORY CONTROL SAMPLE: 2488657
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg
472 478
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2488658 2488659
MS MSD
92415467001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 236
633 519 803
722 90 94 90-110 11 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 456003
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Associated Lab Samples: 92415607001
METHOD BLANK: 2488444
Matrix: Solid
Associated Lab Samples: 92415607001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0
02/05/19 00:18
LABORATORY CONTROL SAMPLE: 2488445
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000 986
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2488448 2488449
MS MSD
92415609001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 32300
17200 18800 52900
57300 120 133 90-110 8 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 456360 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92415607001
METHOD BLANK: 2489788
Matrix:
Solid
Associated Lab Samples: 92415607001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND
2.0
02/05/19 14:00
Nitrogen, Nitrite
mg/kg
ND
1.0
02/05/19 14:00
Nitrogen, NO2 plus NO3
mg/kg
ND
2.0
02/05/19 14:00
LABORATORY CONTROL SAMPLE:
2489789
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
15
15.7
105 90-110
Nitrogen, Nitrite
mg/kg
10
10.3
103 90-110
Nitrogen, NO2 plus NO3
mg/kg
25
26.0
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2489790
2489791
MS
MSD
92415609001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
294
292
317
264
108
90
90-110
18 R1
Nitrogen, Nitrite
mg/kg
ND
196
196
220
218
105
105
90-110
1
Nitrogen, NO2 plus NO3
mg/kg
ND
490
488
536
483
105
94
90-110
11 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: Pittsboro WWTP
Pace Project No.: 92415607
QC Batch: 455771
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92415607001
METHOD BLANK: 2487394
Matrix: Solid
Associated Lab Samples: 92415607001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 1.0
02/01/19 22:34
LABORATORY CONTROL SAMPLE: 2487395
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
46.3 48.3
104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2487396 2487397
MS MSD
92415896001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 3010
49.9 51 2790
2900 -438 -219 90-110 4 H1,M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 13 of 18

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: Pittsboro WWTP
Pace Project No.: 92415607
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Pittsboro WWTP
92415607
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92415607001
Pittsboro
EPA 3050B
455551
EPA 6010D
455635
92415607001
Pittsboro
EPA 7471 B
455116
EPA 7471 B
455217
92415607001
Pittsboro
SM 2540G-2011
455639
92415607001
Pittsboro
ASTM D2974-87
455370
92415607001
Pittsboro
EPA 9045D
455326
92415607001
Pittsboro
SM 2710B-2011
456474
92415607001
Pittsboro
EPA 350.1 Rev 2.0
1993
456068
EPA 350.1 Rev 2.0
1993
456076
Mod.
Mod.
92415607001
Pittsboro
EPA 351.2 Rev 2.0
1993
456003
EPA 351.2 Rev 2.0
1993
456278
92415607001
Pittsboro
EPA 353.2 Rev 2.0
1993
456360
EPA 353.2 Rev 2.0
1993
456389
92415607001
Pittsboro
EPA 365.1 Rev 2.0
1993
455771
EPA 365.1 Rev 2.0
1993
455991
Date: 02/05/2019 04:23 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 18

Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality office
�_�,IOAWPWI'
Laboratory receiving samples:
Asheville, Eden❑
Greenwood ❑
HLfntersville ❑ Raleigh❑ Mechanicsville❑
SampleClient Name:
WO# • 92415607
p•
Project
#:
n�
�°
Courier: ❑Fed Ex
S ❑LISPS
[]Client
itIIIIIIIIIIIIIIIIIIII
❑ Commercial ❑Pace
❑Other:
92415607
Custody Seal Present? ❑Yes �No
Seals Intact? ❑Yes
❑No
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap
[]Bubble Bags None
❑ Other
Biological Tissue Frozen?
[:]yes ❑No ,UN/A
Thermometer: ?
j(�rGun ID: r
Type of Ice: Wet ❑Blue
❑None
Cooler Temp (°C): r 0 Correction
Factor: Add/Subtract (°C)
0,
Temp should be above freezing to ii°C
Cooler Temp Corrected ro.
[]samples out of temp criteria. Sampies on ice, cooling process
has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
inrliidina Hawaii and Puerto Rico)? nYes []No
Comments/Discrepancy:
Chain of Custody Present?
eYes
[]No
❑N/A
1.
Samples Arrived within Hold Time?
j2rYes
[]No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
ETNo
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
2rNo
❑NIA
4.
Sufficient Volume?
Zes
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
La� s
TYes
[:]No
[]No
❑N/A
❑N/A
6.
Containers Intact?
es
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
o
❑N/A
8.
Sample Labels Match COO
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Pfes
[]Yes
❑No
[]No
❑N/A
E]N A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
[]No
❑No
N/A
N/A
11.
CCIVIMENTS/SAMPLE DISCREPANCY[ h Field Data Required? ❑Yes C�N'. l
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date: r iJ�� II
Project Manager SRF Review: Date:
Page 16 of 18

Document Name:
Document Revised: February 7, 2018
' laceklalytical
Sample Condition Upon Receipt(SOUR)
Page 1 of 2
Document No.!
issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Dffice
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WOE
PM: UP
CLIENT:
:92415607
Due Date: 02/07/19
92-SYNAGRO
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Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.a.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 18

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SUMMIT
ENVIRONMENTAL IECHNOLOGIE3.IN
ArlafyNal Lab6ratarla2;
February 26, 2019
Melinda Boyd
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Pittsboro
Dear Melinda Boyd:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: htta://www.settek.com
Order No.: 19011562
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/29/2019 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 36

summly Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL IECHNOLgG1ES,INC. Cuyahoga Falls, Ohio44223 wo#: 19011562
Arralytacal Lahoraldrla; TEL: [phone] FAX: [phone]
Website: htW.-Ilwww.settek.com Date: 2/26/2019
CLIENT: Synagro
Project: Pittsboro
WorkOrder Narrative:
19011562: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
19011562-OOIA TCLP-SVOC_8270E: The associated CCV exhibited high recovery of Nitrobenzene,
Pyridine; sample is ND for these analytes.
Analytical Sequence QC Notes:
ccv 40ng 18589 SVOC-MSTR_S(8270): The 8270 CCV exhibited high recovery of Nitrobenzene,
Pyridine; Associated samples are ND for these analytes.
Original
Page 2 of 36

SUMMIT Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win
ENVIRONMEWAL TECHNOLOGIES, INN Cuyahoga Falls, Ohio 442� WO#: 19011562
ArWyacal Laboralonag TEL: [phone] FAX.- (330) 253-446
Website: httD://www.settekeo Date: 2/26/2019
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
* The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
NIB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 36

MM1 T Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWALrECHROLOG{r;S.JHC Cuyahoga Falls, Ohio44223
Arrzrlyf�cal Laboralorlas TEL: [phone] FAX.- [phone]
Website: hgp://www.settek.com
CLIENT: Synagro
Project: Pittsboro
Lab SampleID Client Sample ID
19011562-001 Pittsboro
Tag No Date Collected
1/23/2019 4:00:00 PM
Workorder
Sample Summary
WO#: 19011562
Date Received
1/29/2019 10:20:00 AM
26-Feb-19
Matrix
Sludge
Page 4 of 36

z
F
O O O O O O O O O
N N N N N N N N N
N N N N N N N N N
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MMIT Summit Environmental Technologies Inc.
SU3310 Win St.
ENVIRONMENTALIrEcHNOL4GIES,IMC Cuyahoga Falls, Ohio44223
Arralytacal Lab6ralorla2; TEL: [phone] FAX.- [phone]
Website: htto:llwww.settek.com
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
19011562-001A
Project:
Pittsboro
Client Sample ID Pittsboro
Analyses Result
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
TCLP Barium(Ba)
ND
TCLP Cadmium(Cd)
ND
TCLP Chromium(Cr)
ND
TCLP Lead(Pb)
ND
TCLP Selenium(Se)
ND
TCLP Silver(Ag)
ND
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Analytical Report
(base report)
WO#: 19011562
Date Reported: 2/26/2019
Tag Number:
Collection Date: 1/23/2019 4:00:00 PM
RL Qual Units DF Date Analyzed
SW7470A SW7470A Analyst: DNS
0.00500 mg/L 1 2/4/2019 4:47:00 PM
SW6010D SW3010A Analyst: KMO
1.25
mg/L
1
2/4/2019 4:03:17 PM
12.5
mg/L
1
2/4/2019 4:03:17 PM
0.250
mg/L
1
2/4/2019 4:03:17 PM
0.500
mg/L
1
2/4/2019 4:03:17 PM
1.25
mg/L
1
2/4/2019 4:03:17 PM
0.125
mg/L
1
2/4/2019 4:03:17 PM
1.25
mg/L
1
2/4/2019 4:03:17 PM
SW8270 SW3510C Analyst: BJH
1,4-Dichlorobenzene
ND
0.0800
mg/L
2
2/6/2019 8:41:00 PM
2,4,5-Trichlorophenol
ND
0.200
mg/L
2
2/6/2019 8:41:00 PM
2,4,6-Trichlorophenol
ND
0.200
mg/L
2
2/6/2019 8:41:00 PM
2,4-Dinitrotoluene
ND
0.0400
mg/L
2
2/6/2019 8:41:00 PM
o-Cresol
ND
0.200
mg/L
2
2/6/2019 8:41:00 PM
m/p-Cresol(s)
2.72
0.200
mg/L
2
2/6/2019 8:41:00 PM
Cresols, Total
ND
4.00
mg/L
2
2/6/2019 8:41:00 PM
Hexachloro-1,3-butadiene
ND
0.0160
mg/L
2
2/6/2019 8:41:00 PM
Hexachlorobenzene
ND
0.0400
mg/L
2
2/6/2019 8:41:00 PM
Hexachloroethane
ND
0.0800
mg/L
2
2/6/2019 8:41:00 PM
Nitrobenzene
ND
0.0800
QC+ mg/L
2
2/6/2019 8:41:00 PM
Pentachlorophenol
ND
0.200
mg/L
2
2/6/2019 8:41:00 PM
Pyridine
ND
0.200
QC+ mg/L
2
2/6/2019 8:41:00 PM
Surr: 2-Fluorophenol
42.3
10 - 109
%Rec
2
2/6/2019 8:41:00 PM
Surr: Phenol-d6
24.5
10 - 109
%Rec
2
2/6/2019 8:41:00 PM
Surr: Nitrobenzene-d5
47.2
19 - 120
%Rec
2
2/6/2019 8:41:00 PM
Surr: 2,4,6-Tribromophenol
58.3
10 - 120
%Rec
2
2/6/2019 8:41:00 PM
Surr: 2-Fluorobiphenyl
47.9
22 - 117
%Rec
2
2/6/2019 8:41:00 PM
*
Qualifiers:
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 6 of 36

MMIT Summit Environmental Technologies Inc.
SU3310 Win St.
ENVIRONMENTALIrEcHNOL4GIES,IMC Cuyahoga Falls, Ohio44223
Arrafytacal Laboralarta; TEL: [phone] FAX.- [phone]
Website: htto:llwww.settek.com
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
19011562-001A
Project:
Pittsboro
Client Sample ID Pittsboro
Analyses Result
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
Analytical Report
(base report)
WO#: 19011562
Date Reported: 2/26/2019
Tag Number:
Collection Date: 1/23/2019 4:00:00 PM
RL Qual Units DF Date Analyzed
SW8270 SW3510C Analyst: BJH
Surr: p-Terphenyl-d14 74.8
34 - 116
%Rec
2
2/6/2019 8:41:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
10
2/7/2019 7:39:00 PM
Toxaphene
ND
0.0500
mg/L
10
2/7/2019 7:39:00 PM
Endrin
ND
0.00500
d
mg/L
10
2/7/2019 7:39:00 PM
gamma-BHC
ND
0.00500
d
mg/L
10
2/7/2019 7:39:00 PM
Heptachlor
ND
0.00500
d
mg/L
10
2/7/2019 7:39:00 PM
Heptachlor epoxide
ND
0.00500
d
mg/L
10
2/7/2019 7:39:00 PM
Methoxychlor
ND
0.00500
d
mg/L
10
2/7/2019 7:39:00 PM
Surr: TCMX
36.3
10 - 119
%Rec
10
2/7/2019 7:39:00 PM
Surr: DCB
36.8
10 - 119
%Rec
10
2/7/2019 7:39:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8151A
SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW1311/8151)
2,4-D
ND
0.500
mg/L
10
2/7/2019 4:34:00 PM
2,4,5-TP
ND
0.500
mg/L
10
2/7/2019 4:34:00 PM
Surr: DCAA
86.4
20 - 140
%Rec
10
2/7/2019 4:34:00 PM
TCLP VOLATILES
ANALYSIS
SW8260
SW1311M Analyst: RMT
1,1-Dichloroethene
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
1,2-Dichloroethane
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
MEK
ND
0.625
mg/L
25
2/1/2019 6:48:00 PM
Benzene
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Carbon tetrachloride ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Chlorobenzene
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Chloroform
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Tetrachloroethene
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Trichloroethene
ND
0.125
mg/L
25
2/1/2019 6:48:00 PM
Vinyl chloride
ND
0.0500
mg/L
25
2/1/2019 6:48:00 PM
*
Qualifiers:
Value exceeds Maximum Contaminant Level.
E Value above quantitation range
H
Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC
Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND
Not Detected
0 RSD is greater than
RSDlimit
P
Second column confirmation exceeds
PL Permit Limit
Original
R
RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 7 of 36

MMIT Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTALIrEcHNOL4GIES,IMC Cuyahoga Falls, Ohio44223
Arrafytacal Laborafarta; TEL: [phone] FAX.- [phone]
Website: htto:llwww.settek.com
CLIENT:
Synagro
Matrix:
SLUDGE
Lab ID:
19011562-001A
Project:
Pittsboro
Client Sample ID Pittsboro
Analytical Report
(base report)
WO#: 19011562
Date Reported: 2/26/2019
Tag Number:
Collection Date: 1/23/2019 4:00:00 PM
Analyses
Result
RL
Qual Units
TCLP VOLATILES ANALYSIS
SW8260
Surr: 4-Bromofluorobenzene
96.1
70 - 130
%Rec
Sum Dibromofluoromethane
100
70 - 130
%Rec
Sum Toluene-d8
101
70 - 130
%Rec
RCI-SOLID-W/ IGNITABILITY1030
SW9014
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.495
mg/Kg
RCI-SOLID-W/ IGNITABILITY1030
SW1030
IGNITABILITY OF SOLIDS (SW-846: 1030)
Ignitability non-flammable
RCI-SOLID-W/ IGNITABILITY1030
SW9045D
PH (SW9045D)
pH
6.9
s.u.@20.5C
RCI-SOLID-W/ IGNITABILITY1030
SW9034
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0
mg/Kg
Qualifiers: *
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
DF Date Analyzed
SW1311M Analyst: RMT
25
2/1/2019 6:48:00 PM
25
2/1/2019 6:48:00 PM
25
2/1/2019 6:48:00 PM
Analyst: MS
1
2/1/2019 1:11:00 PM
Analyst: AJT
1
2/4/2019 1:00:00 PM
Analyst: DHC
1
2/6/2019 3:15:00 PM
Analyst: MS
1
2/1/2019 1:11:00 PM
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
ffISU
MM' T
3310 Win St.
v
Analte5 Report
p
EHYI#20Nt}G
MEUT.ALIECHHQL{�S,INC
, Cuyahoga Falls, Ohio
J
ArralyOal Laboralarlam
TEL: [phone] FAX.- [phone]
WO#:
19011562
Website: hgp://www.settek.com
26-Feb-19
Client: Synagro
State: NW
Project: Pittsboro
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
19011562-001A Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4,5-TP
A
Sludge
TCLP Herbicides Analysis (SW1311/8151)
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
NC WW SCM A Accredited
Version #3
Page 9 of 36

Summit Environmental Technologies, Inc.
Accreditation
Program
MM' T
ffISU3310 Win St.
v
Analte5 Report
p
EHYI#20NMEUT.ALIECHHQL{�S,INC
t}G , Cuyahoga Falls, Ohio
J
ArralyOal Laboralarlam
TEL: [phone] FAX.- [phone]
WO#:
19011562
Website: hgp://www.settek.com
26-Feb-19
Client: Synagro
State: NW
Project: Pittsboro
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
19011562-OOIA Sludge
TCLP Volatiles Analysis
1, 1 -Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited
Version #3
Page 10 of 36

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�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTALIECHNOLI)G1�3.ING Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arra/yt�caf L2boralorfas TEL: [phone] FAX: [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Chain of Custody
1. Is Chain of Custody complete?
2. How was the sample delivered?
Lop In
3, Coolers are present?
Work Order Number: 19011562
1/29/2019 10:20:00 AM
1/29/2019 12:07:33 PM
1/29/2019 3:31:43 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0° C to 6.0°C
7, Sample(s) in proper container(s)?
8. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
RcptNo: 1
��., rrr.•r�-�
Yes
❑
No ❑
Not Present ❑
UPS
Yes
❑
No ❑
NA ❑
Yes
d❑
No ❑
Yes
❑
No ❑
Not Present ❑d
Signed By:
Yes
❑
No ❑
NA ❑
Yes
❑
No ❑
NA ❑
Yes
❑
No ❑
Yes
d❑
No ❑
Yes
J❑
No ❑
Yes
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No
NA ❑
Yes
❑
No ❑
No VOA Vials ❑�
Yes
❑
No d❑
Yes
J❑
No ❑
Yes d❑ No ❑
Yes d❑ No ❑
Yes J❑ No ❑
Yes ❑ No ❑ NA ❑d
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No I Temp °C Condition Seal Intact Seal No Seal Date Signed
1 3.1 Good, Not Present
Page 36 of 36

Cameron Testing Services, Inc. Laboratory Report
NCDENR#654
NC PHHS #37799
Client:
Synagro CTs Proj.
190117
US EPA #NC01918
Project: _
Pittsboro WWTP Regulatory
Yes
Sample Information
Sampled
M. Boyd
Date 01/16/19 Received C. Cameron Date :`
01/16/19
Analyses and Results
Lab ID
Sample ID
k�
c` Analyte Result =
E
T
?+
Std. Methods
D
-'J
c d
Reference
Q
190117
1
31udgE cr Fec. Coliform-S 60900 CFUrg
15200
01/17/19 ERP
9222D - MF
2
106000 CFU/9
15100
3
30300 CFU19
15100
4
15300 CFUf9
15300
5
90000 CFUrg
15000
6
30600 CFU/g
15300
7
15300 CFU/g
15300
Geomean 38500
1
3ludge Gr TS (°/n) 6.57%
0.01
01/17/19 ERP
2540 G -TS.
2
6.61 %
0.01
3
6.61 %
0.01
4
6.52%
0.61
6
6.67%
0.01
6
6.54%
0.01
7
6.52%
0.01
Report
Review
C z9 /9
Protect �Manaqer Date
219 S. Steele Str.
Sanford NC 27330
919-208-4240
[e-mail]

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APPENDIX 8
2019 PERMIT MODIFICATION
Granville Farms, Inc. (WQ0000838)
Residual Source Certification Attachment
RS CA
Henderson WRF
Analytical
Field Loading Calculations

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Henderson WRF
2. Facility permit holder is: Federal, 0 State, 9 Local Government, or ❑ Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: PPpr ).
3. Facility contact person and title: H. Lamont Allen, Plant Director
Complete mailing address: PO Box 1434
City: henderson State: NC Zip: 27536-
Telephone number: [phone] E-mail address: hlallen(&ci.henderson.nc.us
4. Facility physical address: 1646 West Andrews Avenue
City: Henderso State: NC Zip: 536-
Coordinates: Latitude: 36' 20' 55.8" Longitude: 78' 24' 38.6"
Datum: NAD 83 Level of accuracy: Sub -Meter
Method of measurement:
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: M MGD and facility average daily flow: N MGD
8. Average amount of residuals being generated at this facility = dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 4.0 MG Conventional Activated Sludge
Type and volume of residuals storage (i.e., outside of residuals treatment units): 2.0 MG Aerobic Di esg tion
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: t Ana i and Date of analysis: MMUM
Passed corrosivity test: ® yes no. pH: 8_0 s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes no. Flashpoint: _ °F (> 140°F)
Passed reactivity test: ® yes Ono. HCN: _ mg/kg (<250) & H2S: _ mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
< 0.125
Hexachlorobenzene
0.13
< 0.02
Barium
100.0
0.217
Hexachloro-1,3-Butadiene
0.5
< 0.02
Benzene
0.5
< 0.01
Hexachloroethane
3.0
< 0.02
Cadmium
1.0
< 0.025
Lead
5.0
< 0.05
Carbon Tetrachloride
0.5
< 0.01
Lindane
0.4
< 0.0016
Chlordane
0.03
< 0.008
Mercury
0.2
< 0.02
Chlorobenzene
100.0
< 0.01
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.01
Methyl Ethyl Ketone
200.0
< 0.2
Chromium
5.0
< 0.05
Nitrobenzene
2.0
< 0.02
m-Cresol
200.0
< 0.04
Pentachlorophenol
100.0
< 0.04
o-Cresol
200.0
< 0.02
Pyridine
5.0
< 0.02
p-Cresol
200.0
< 0.04
Selenium
1.0
< 0.25
Cresol
200.0
< 0.04
Silver
5.0
< 0.25
2,4-D
10.0
< 0.02
Tetrachloroethylene
0.7
< 0.01
1,4-Dichlorobenzene
7.5
< 0.01
Toxaphene
0.5
< 0.012
1,2-Dichloroethane
0.5
< 0.01
Trichloroethylene
0.5
< 0.01
1,1-Dichloroethylene
0.7
< 0.01
2,4,5-Trichlorophenol
400.0
< 0.02
2,4-Dinitrotoluene
0.13
< 0.02
2,4,6-Trichlorophenol
2.0
< 0.02
Endrin
0.02
< 0.0016
2,4,5-TP (Silvex)
1.0
< 0.02
Heptachlor and its Hydroxide
0.008
< 0.0016
Vinyl Chloride
0.2
< 0.01

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: �YMoint Analytical and Date of analysis: -
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
8.43
Cadmium
85
39
< 1.0
Copper
4,300
1,500
292
Lead
840
300
22.0
Mercury
57
17
0.308
Molybdenum
75
n/a
7.75
Nickel
420
420
18.7
Selenium
100
100
8.72
Zinc
7,500
2,800
645
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: _ and Date of analysis: _
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: a %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Waypoint Analytical and Date of analysis: 4/10/2019
Parameter
Result
(mg/kg)
Aluminum
31,500
Ammonia -Nitrogen
10,100
Calcium
12,000
Magnesium
2,250
Nitrate -Nitrite Nitrogen
323
pH (Standard Unit)
7.6
Phosphorus
25,300
Potassium
2,680
Sodium
926
Total Kjeldahl Nitrogen
39,100
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): -
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
14,073
20,516
Injection/Incorporation
19,123
24,266
6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.

Waypointo
ANALYTICAL
4/19/2019
City of Henderson
Darrell Johnson
PO Box 1434
Henderson, NC, 27536
Ref: Analytical Testing
Report Number: 19-101-0213
Project Description: 2nd Quarter Aerobic
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Darrell Johnson:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/11/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�a f• c—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Virginia 460014
Z� l
Page 1 of 6

(2)
7621 Whitepine Road, Richmond, VA 23237
Waypoint, Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-101-0213
Client Project Description: 2nd Quarter Aerobic
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
65846
aerobic digester
Solids
04/10/2019
08:04
04/11/2019
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW-7471B
WTN
SM-4500-NH3C-TKN
WTN
SM-2540G
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6

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Waypoint.
ANALYTICAL
Customer Number: 46116
Customer Name: City of Henderson
Report Number: 19-101-0213
0 Fed Ex 0 US Postal
0 UPS 0 Client
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Shipping Method
0 Lab 0 Other:
0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments: F
0 Yes
0 No
Signature: IBrandi Watson Date & Time: 04/11/2019 13:44:25
Page 5 of 6

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Waypointo
ANALYTICAL
1 /22/2019
City of Henderson
Darrell Johnson
PO Box 1434
Henderson, NC, 27536
Ref: Analytical Testing
Report Number: 19-010-0200
Project Description: 1 st Qtr 2019
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Dear Darrell Johnson:
Waypoint Analytical Virginia, Inc. received sample(s) on 1/10/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�a f• c—r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Page 1 of 9

(2)
Waypoeint 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-010-0200
Client Project Description: 1st Qtr 2019
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
64365
Aerobic Digester
Solids
01/09/2019 08:17
01/10/2019
SW-7.3.3
WTN
64365
Aerobic Digester
Solids
01/09/2019 08:17
01/10/2019
SW-9045C
WTN
64365
Aerobic Digester
Solids
01/09/2019 08:17
01/10/2019
ASTM D93-80
WTN
64365
Aerobic Digester
Solids
01/09/2019 08:17
01/10/2019
SW-7.3.4
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
8270C
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
6010D
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
SW-1311 (ZHE)
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
8151A
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
SW-1311
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
8260E
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
8081A
WTN
64366
Aerobic Digester
TCLP
01/09/2019 08:17
01/10/2019
7470A
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 9

wavDoint,o
ANALYTICAL
46116
City of Henderson
Darrell Johnson
PO Box 1434
Henderson , NC 27536
Submitted By : Darrel Johnson
Report Number : 19-010-0200
Lab No : 64365
Sample ID : Aerobic Digester
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Darrel Johnson
Project 1st Qtr 2019
Information :
REPORT OF ANAL YSIS
Report Date : 01/22/2019
Received : 01/10/2019
Pam•« XF 6040r,
Pauric McGroary
Agronomist
Matrix: Solids
Sampled: 1/9/2019 8:17
pH
8.0
s.u.
1
01/21/19 07:54
JSL
SW-9045C
Test
Results
Units MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Cyanide (Reactivity)
<0.125
mg/Kg 0.125
1
01/18/19 09:05
EWB
SW-7.3.3
Ignitability
>96
degrees C
1
01/21/19 08:55
RXC
ASTM D93-80
Sulfide (Reactivity)
<25.0
mg/Kg 25.0
1
01/21/19 10:20
EWB
SW-7.3.4
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 9

wavDointo
ANALYTICAL
46116
City of Henderson
Darrell Johnson
PO Box 1434
Henderson, NC 27536
Submitted By : Darrel Johnson
Report Number : 19-010-0200
Lab No : 64366
Sample ID : Aerobic Digester
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Darrel Johnson
Project 1st Qtr 2019
Information :
REPORT OF ANAL YSIS
Report Date : 01/22/2019
Received : 01/10/2019
Pam•« XF 6040r,
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 1/9/2019 8:17
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
TCLP Herbicide Extraction
Combined
1
01/16/18 15:01
SAJ
SW-1311
TCLP Metals Extraction
Combined
1
01/16/18 15:01
SAJ
SW-1311
TCLP Pesticide Extraction
Combined
1
01/16/18 15:01
SAJ
SW-1311
TCLP SVOC Extraction
Combined
1
01/16/18 15:01
SAJ
SW-1311
TCLP VOC ZHE Extraction
Combined
1
01/16/19 15:12
SAJ
SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L417246
01/17/19 10:00
Prep Method: 3005A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Arsenic
<0.125
mg/L
0.125
1
01/18/19 17:11
KKM
L417509
TCLP Barium
0.217
mg/L
0.125
1
01/18/19 17:11
KKM
L417509
TCLP Cadmium
<0.0250
mg/L
0.0250
1
01/18/19 17:11
KKM
L417509
TCLP Chromium
<0.050
mg/L
0.050
1
01/18/19 17:11
KKM
L417509
TCLP Lead
<0.050
mg/L
0.050
1
01/18/19 17:11
KKM
L417509
TCLP Selenium
<0.250
mg/L
0.250
1
01/18/19 17:11
KKM
L417509
TCLP Silver
<0.025
mg/L
0.025
1
01/18/19 17:11
KKM
L417509
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 9

wavDointo
ANALYTICAL
46116
City of Henderson
Darrell Johnson
PO Box 1434
Henderson, NC 27536
Submitted By : Darrel Johnson
Report Number : 19-010-0200
Lab No : 64366
Sample ID : Aerobic Digester
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Darrel Johnson
Project 1st Qtr 2019
Information :
REPORT OF ANAL YSIS
Report Date : 01/22/2019
Received : 01/10/2019
Pam•« XF 6040r,
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 1/9/2019 8:17
Analytical Method: 7470A
Prep Batch(es):
L417251
01/17/19 10:10
Prep Method: 7470A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Mercury
<0.0200
mg/L
0.0200
1
01/17/19 14:26
TJS
L417336
Analytical Method: 8081A
Prep Batch(es):
L417777
01/21/19 16:00
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Endrin
<0.001600
mg/L
0.001600
10
01/21/19 19:24
BMP
L417877
TCLP gamma-BHC
<0.001600
mg/L
0.001600
10
01/21/19 19:24
BMP
L417877
TCLP Methoxychlor
<0.001600
mg/L
0.001600
10
01/21/19 19:24
BMP
L417877
TCLP Toxaphene
<0.01200
mg/L
0.01200
10
01/21/19 19:24
BMP
L417877
TCLP Chlordane
<0.008000
mg/L
0.008000
10
01/21/19 19:24
BMP
L417877
TCLP Heptachlor Epoxide
<0.001600
mg/L
0.001600
10
01/21/19 19:24
BMP
L417877
TCLP Heptachlor
<0.001600
mg/L
0.001600
10
01/21/19 19:24
BMP
L417877
Surrogate: Decachlorobiphenyl
45.25
Limits: 36-116%
10 01/21/19 19:24 BMP
L417877
Surrogate: Tetrachloro-m-xylene
50.75
Limits: 25-123%
10 01/21/19 19:24 BMP
L417877
Analytical Method: 8151A
Prep Batch(es):
L417785
01/21/19 17:40
Prep Method: 8151A
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1
01/22/19 13:45
BMP
L417964
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1
01/22/19 13:45
BMP
L417964
Surrogate: DCAA
44.40
Limits: 20-120%
1 01/22/19 13:45 BMP
L417964
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 5 of 9

Waypoint 7621 0 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46116
City of Henderson Darrel Johnson
Darrell Johnson
Project 1st Qtr 2019
Report Date : 01/22/2019
PO Box 1434
Information :
Received
: 01/10/2019
Henderson, NC 27536
Pam,«
/
m`
Submitted By : Darrel Johnson
Pauric McGroary
Report Number : 19-010-0200
REPOR T OF A
NA L YSIS
Agronomist
Lab No : 64366
Matrix:
TCLP
Sample ID : Aerobic Digester
Sampled:
1/9/2019
8:17
Analytical Method: 8260B
Prep Batch(es):
L417423 01/17/19 08:36
Prep Method: 5030E
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Chloroform
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
01/17/19 20:20
SPC
L417537
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
01/17/19 20:20
SPC
L417537
Surrogate: 4-Bromofluorobenzene
88.4
Limits: 71-137%
1 01/17/19 20:20 SPC
L417537
Surrogate: Dibromofluoromethane
97.4
Limits: 70-128%
1 01/17/19 20:20 SPC
L417537
Surrogate: 1,2-Dichloroethane - d4
110
Limits: 63-136%
1 01/17/19 20:20 SPC
L417537
Surrogate: Toluene-d8
89.2
Limits: 70-130%
1 01/17/19 20:20 SPC
L417537
Analytical Method: 8270C
Prep Batch(es):
L417541 01/18/19 15:30
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.020
mg/L
0.020
1
01/21/19 16:40
ATF
L417706
TCLP 3&4 Methylphenol
<0.040
mg/L
0.040
1
01/21/19 16:40
ATF
L417706
TCLP 2,4-Dinitrotoluene
<0.020
mg/L
0.020
1
01/21/19 16:40
ATF
L417706
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 6 of 9

Waypoint 7621 0 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
46116
City of Henderson Darrel Johnson
Darrell Johnson Project 1st Qtr 2019 Report Date : 01/22/2019
PO Box 1434 Information : Received : 01/10/2019
Henderson, NC 27536 /
Pam,« m`
Submitted By : Darrel Johnson
Report Number : 19-010-0200
Lab No : 64366
Sample ID : Aerobic Digester
REPOR T OF A NA L YSIS
Pauric McGroary
Agronomist
Matrix: TCLP
Sampled: 1/9/2019 8:17
Analytical Method: 8270C
Prep Batch(es):
L417541 01/18/19 15:30
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP Hexachlorobutadiene
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP Hexachloroethane
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP Nitrobenzene
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP Pentachlorophenol
<0.040
mg/L
0.040
1
01/21/19 16:40 ATF
L417706
TCLP Pyridine
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP 2,4,5-Trichlorophenol
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
TCLP 2,4,6-Trichlorophenol
<0.020
mg/L
0.020
1
01/21/19 16:40 ATF
L417706
Surrogate: TCLP 2,4,6-Tribromophenol
75.5
Limits: 40-125%
1 01/21/19 16:40 ATF
L417706
Surrogate: TCLP 2-Fluorobiphenyl
53.5
Limits: 38-107%
1 01/21/19 16:40 ATF
L417706
Surrogate: TCLP 2-Fluorophenol
23.5
Limits: 20-110%
1 01/21/19 16:40 ATF
L417706
Surrogate: TCLP 4-Terphenyl-d14
57.0
Limits: 33-122%
1 01/21/19 16:40 ATF
L417706
Surrogate: TCLP Nitrobenzene-d5
49.0
Limits: 29-110%
1 01/21/19 16:40 ATF
L417706
Surrogate: TCLP Phenol-d6
17.0
Limits: 10-115%
1 01/21/19 16:40 ATF
L417706
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 7 of 9

0 0
Waypoint.
ANALYTICAL
Customer Number: 46116
Customer Name: City of Henderson
Report Number: 19-010-0200
0 Fed Ex 0 US Postal
0 UPS 0 Client
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Cooler Receipt Form
Shipping Method
0 Lab 0 Other:
0 Courier Thermometer ID:
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
® N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments: F
0 Yes
0 No
Signature: Brandi Watson Date & Time: 01/10/2019 10:41:06
Page 8 of 9

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R&R
PROMPT- A CCU RATE • RELIAMLE
LABORATORIES, INC
W W W.PARLABS.COM
REPORT OF ANALYSES
Attn: DARREL JOHNSON
CITY OF HENDERSON WR1"
PO BOX 1434
HENDERSON, NC 27536-
PROJECT NAME: APR 19
DATE: 05/29/19
SAMPLE NUMBER-
135540
SAMPLE ID- AEROBIC DIGESTER
SAMPLE MATRIX- SO
DATE SAMPLED-
04/10/19
TIME SAMPLED- 0804
DATE RECEIVED-
04/11/19
SAMPLER- RR
RECEIVED BY- DJ
TIME RECEIVED-
1125
DELIVERED BY- UPS
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE TIME BY
RESULT UNITS
30 DAY BENCH SCALE
TEST
VAR
04/11/19 1250 RE
3.01 %
LABORATORY
DIRECTOR ml
_1 ,�-
2217 Graham Park Drive • Charlotte, NC 28273
Phone: [phone] • Fax: [phone]

PA&F;Z
c RoMPT• ACCu RATE • RE LIP, E]LE
LABORATdR :ESA INC
WWW. PARLABB. COM
30 Day Bench Scale Extended Aeration Test
Percent Volatile Solids Reduction
CITY OF HENDERSON
AEROBIC DIGESTER
135540
04/11/19
� � 05113119
Start: End:
TS
0.1953
0.1703
TS%
1.88%
1.89%
V5
0.1076
0.0905
VS%
55.09%
53.14%
y Mass Fraction of Volatile Solids in Liquid Sludge
0,0103562
0.0100432
x Mass Fraction of Fixed Solids in Liquid Sludge
0.0084409
0.0088557
FSVR (Mass Balance)
3.01%
FSVR Van Kleeck
3.01 %
FSVR (Mass Balance)<15%
YES
FSVR (Van Kleeck) <15%
YES
P.O. Box 411483 * Charlotte, N C 28241-1483
Phone: [phone] • Fax: [phone]

PLLR
PRC M PT, A C CU RATE• R ELI AE LE
LABORATORIES, INC
WWW.PARLABS.COM
Collected
D.O.
Crucible
Tare Wt (g)
Sample Wt +
Tare Wt (g)
Liquid Sludge
(g)
Oven Temp °C
Date/Time In
Date/Time Oul
Dried Sample
+ Tare Wt (g)
Dried Sludge Wt
Fixed Solids Wt
Furnace Temp
DatelTime In
Date/Time Ou-
Burned Sampl
Wt + Tare Wt
Volatile Solids Wt
TS%
VS%
30 Day Bench Scale Extended Aeration Test
VAR Clntinn 3 PPrGPnt Vnfatile Solids Reduction
CITY OF HENDERSON
AEROBIC DIGESTER
135540
04/11/19
05/13/19
As Received Day 0 Day 7 Day 14
04111/19 04/15/19 04122119 04129119
Day 21 Day 28
05106119 05113119
4.07
5.11
6.90
6,88
6.91
X2
X8
X6
X12
X8
X4
25.0655
24.7171
24.2903
19.3055
24.7178
20.3643
34.1403
35,1070
33.6193
28.6181
33.4329
29.3754
Nt
9.0748
10.3899
9.3290
9,3126
8.7151
9.0111
106
105
106
106
107
106
04/11/19 12750
104115119 09:45
04/22/19 10:30
04/29/19 09:20
05/06119 10:15
05/13/19 09:30
04/12/19 12:40
04/16/19 10:00
04/23/19 10:20
04/30/19 09:40
05/07/19 10:10
05/14/19 09:25
MCI
25.8871
24.9124
24.4666
19.4787
24.8808
20.5346
(g)
Q.8216
0.1953
0,1763
0.1732
0,1630
0.1703
(g)
0.0877
0.0809
0.0796
0.0749
0.0798
°C
550
550
550
550
550
04/16119 13:15
04/23/19 14715
04/30/19 12:10
05/07/19 13:45
05/14/19 14:00
04/16119 14:20
04/23/19 15:10
104130119 13:15
05/07/19 14:50
05/14/19 15:10
�g)
24.8048
24.3712
19.3851
24.7927
20.4441
(g)M
0.1076
0,0954
0.0936
0.0881
0.0905
1.88%
1,89%
1.86%
1.87%
1.89%
55.09%
1 54.11 %
1 54.04%
1 54.05%
53.14%
Yf Mass Fraction of Volatile Solids In Liquid (Feed)
Sludge at Star) of Test
0,0103562
Yb Mass Fraction of Voiatite Solids In Liquid (Bottom)
Sludge at end of To
0.0100432
Xf Mass Fraction of Fixed Solids in Liquid (Feed) Sludge
at Start of Test
0.0084409
Xb Mass Fraction of Fixed Solids in Liquid (Bottom)
Sludge at End of rest
0.0088557
T5
0.1953
TS
0.1703
VS )
0.1076
VS
0.0905
Volatile Fraction In: 1 0. 1 Volatile Fraction Out: 1 0.28116
t?O. Box 411483+Charlotte, NC 28241-1483
Phone: [phone] Fax: [phone]S

PiIR
PROM PT•AGCU RATE• RELIABLE
LABORATORIES INC
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
Phone [phone]
Fax [phone]
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information be recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carnhna rlenartment of FnvirnnrnPntRl and Nahiral Resnurcas
Company Name (billing)
Comments/ Special Instructions
Please return Cooler to:
City of Henderson WRF
Address
Henderson WRF
P.O. Box 1434
1546 West Andrews Ave.
Henderson, NC 27536Et.
City, State �zip code
Henderson, NC 27536
PO # 20190073
Point of Contact t3 Telephone Number
Darrel Johnson, (252)-431-6080 Cell 252-432-4590
Sample 1
Taken By: SIGNATURE � 6' PRINTED NAME .� 'fC br
ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO
*Sample Type: DW WW GWMW HW Soil other X
Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C
**Field Preserved: Yes No X Teflon Liner/Zero Headspace: Yes No n1a X
Residual Chlorine checked at time of sampling (YIN): N Dechlorination Necessary (YIN): N
Client Sample I.D.
(Sample Location 1 Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Date/Time
Analyses
Requested
Aerobic Digester
�° '`�
30-Day Scale Bench Test
k<e lsheci by- % uater l lme rteceivea oy: alm erne
art I -IOC
Relinquished by:
DatelTime Received by:
DatelTime
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste