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HomeMy WebLinkAboutNC0089885_Application_20190708NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. Mail the complete application to: N. C. Department of Environment and Natural Resources Division of Water Quality / NPDES Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 NPDES Permit Number INCH If you are completing this form in computer use the TAB key or the up - down arrows to moue from one field to the next. To check the boxes, click your mouse on top of the box. Otherwise, please print or type. 1. Contact Information: Owner Name Facility Name Mailing Address City State / Zip Code Telephone Number Fax Number e-mail Address Duke Energy Carolinas, LLC Charlotte Metro Office Tower Construction 526 S Church Street, EC03T RFCEIVFD/NODE /DWR Charlotte NC 28202 2019 (980)737-2663 Water Quality Richard. Powell2 a duke-energy.com 2. Location of facility producing discharge: Check here if same as above ❑ Street Address or State Road City State / Zip Code County 510, 518, 522 S College Street and 509, 515, 521, 525, 527 S Tryon Street Charlotte NC 28202 Mecklenburg 3. Operator Information: Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the Operator in Responsible Charge or ORC) Name Childress Klein Mailing Address 301 South College Street, Suite 2800 City Charlotte State / Zip Code NC 28202 Telephone Number (704)343-4396 Fax Number ( ) 4. Ownership Status: Federal ❑ State ❑ Private ® Public ❑ Page I of 3 C-GW 03/05 NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. 5. Products recovered: RECENED N Gasoline ® Diesel fuel ® Solvents ® Other Ct?E[p 6. Number of separate discharge points: 2 JUV 4 8 2019 Outfall Identification number(s) ULS004-0174 and ULS004-0172 water Quality Permitting Section 7. Frequency of discharge: Continuous ® Intermittent ❑ If intermittent: Days per week discharge occurs: 7 Duration: Approx. 4 Months 8. Treatment System Design flow 72,000 MGD 9. Name of receiving stream(s) (Provide a map shouting the exact location of each outfall, including latitude and longitude): Little Sugar Creek 10. Please list all additives to the treatment system, including chemicals or nutrients, that have the potential to be discharged. None 11. Is this facility located on Indian country? (check one) Yes ❑ No 12. Additional Information All applicants (including renewals): v A USGS topographical map (or copy of the relevant portion) which shows all outfalls y A summary of the most recent analytical results (effluent data, if available) containing the maximum values for each chemical detected NEW Applicants only: Engineering Alternative Analysis Description of remediation treatment system components, capacities, and removal efficiency for detected compounds. If the treatment system will discharge to a storm sewer, written approval from the municipality responsible for the sewer. A list of any chemicals found in detectable amounts at the site, with the maximum observed concentration reported for each chemical (the most recent sample must be collected less than one year prior to the date of this application) For petroleum -contaminated sites — Analyses for Volatile Organic Compounds (VOC) should be performed. Analyses for any fuel additives likely to be present at the site and for phenol and lead should also be performed. For sites contaminated with solvents or other contaminants - EPA Method 624/625 analysis should be performed. Page 2 of 3 C-GW 03105 NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. 13. Applicant Certification I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete, and accurate. K. CA \Vj Printed name of Pet Signature of Ntf �c_ CKA� rz� f< Title Za t 1 Date North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document files or required to be maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section 1001 provides a punishment by a fine of not more than $25,000 or imprisonment not more than 5 years, or both, for a similar offense.) RECEIVED/NCDEQ/DWR JUL 0 8 101g Water Quality Permitting Section Page 3 of 3 C-GW 03/05 TOPOGRAPHIC MAP 73mt1! GRATE - 736.63 �6 RIM - T36.53' r _*,�� -r INV - 734.23' �i O�' �- INV- - 73 U INV. - 731.37' —,-_,� ?, -- A Z INV - 73320 K' INV. - 732.58 136.3y - INV. - 73121' i► N* pp 0 ST. PETERS CATHOLIC CHURCH Z O U N Ro •(G \ _„l� MB. 332 PG- 378 U`0 NL� PC/25C 5305 �jNy ASPHALT "t� (DY Z 1GRATE - 736.43' rm,Ba W". �. Nv.-733.78 (t 9 N DUCT BANK _ 735 Y Rw • 736.1r + 73?Ar INV.- 7322r / n. SUE LEVEL C LOCATIONS _ t .` INV. -733 - O Q INV. - 73T-w \\\ a O GRATE - 73321' ���- 5-0p Z LEGEND 733.88 A T J4 9v * ' \ WV, - 730. , Sup"sy CONTROL POINT suw Er eENcrNMwc N TB.M.1EiA0 Nk O" MA03 NE W NAA. FOUND '� •� �\ G � W41407.24 OEF EAISTINO 04ON PIPE /, . ELj35.05' OEIR EAST•NG WNON ROO / A . 730.1 / • SET NRoP POD ♦ COMPUTED POT �7 ASP KPILT 736 ® STORM DRAN MANHOLE\d - 'T,,}W j/ I / o T35 STOFAN DRAIN INLET / I N:S41406.72 / - ,X. �OT 1 ■ STORM ORAiN CLRB "LLET E 1448064.15 �^ UIfO)=N6RGYJ1AR CLNAS. LL �%� BR1LK'hALt 0. f/ f 194)�PGS,661 - 664 Kz ® SANrrAcn SEINER MAN+OLE / 1���p II ON.RIM • ?29-1733A / --"1� _ � /` / , 3 t 66! r O SAMTAAN SEWER CLEANOUT � ` NV. • 72l.12 I TWO? - '_ / / �T : - _ W NCNOYN BANK Of DELAAPARE Q HYORANT fNY.-729.70 ° r +733,78'/ 0.9.11224PG2" U + � 9 PID I-IM5311 WWgAT10N CONTROL VALVE Q WATER a WATER METER O WATER WLLLT �vNv 44uarOiM413 WELL a DAB 'ALA .�.}. - - - _ - - — - ,%j' / z p am METER - � - - r - m� / - RIM . 727s' En O EIR / NV..116$2' w TELEPHONE MANHOLE _ Y_� - G TPA E7(ISTING BUILDING r _ - + l AB!'NALT (,. N:54 L'54.606' % Ll ® TELEPHONE PEi>iBTAL t f - r-- _. — _ E:1448511.393/CC ® ELECTRIC MANHOLE s� l - _ _- - - - r + 727Ar EL^6.SS a. 1� ^ SEE INSET MAP FOR CIETAL E60 ELECTRIC METER N B r 45' 28' W 4304121 GRID, NIP r _ 6'LANDSCAPE G 4305.39','GROUND; ® ELECTRIC SM ROC CORD ' I I _ - _i EMENT NEO FACTOR - 0.999644a7 D.B. 10220 PG. 507 I j % _ - . I G37 PG. 454i RN - 72627 D UnUTv POLE MB. 51 PG. 559 f NV. - 722.11' -- GLX WRE 12SH301 I I - /'` �- PAY . _ _ - .,y0 �'S CONCRETE O uoHT POLE .A ' ® mcnoN Boa j � !/ + 725.W p d`O - 734 �y i� Cn 6 TRAFFIC SGhAL .POST � 1 'ARATE - l' � J � c � U ZZ A r NV.tz �Itl.tO 61 T SIGN �� /J ASPHALT in O s ®RATE - 720..3B' Rpll t.. CBGEP • 723.l4' U rn OECED000B TREE r' - INV. - 721.13 L T LL v N m EvERGAEE3N TREE ? N � Cq In —O— CHAIN:M%k FENCE CiP V_ GRATE . T2032' RIM . 721135' � �GQ � � DUCT BANK � °10ni Z` o — 0— W000 FENCE INV.. IV4'.. TT7.71' �_ `7'� 2 CL m Z —T— Lar�ERGROVNO TELEPHONE LINET1895YB'CLAY1 /�%'.�.i � % - O TBAC WG NAIL ~ P' 3 Z u ui DUCT BANK r N:541132j671r aL _-'�— II.GERGROIJVD (iA8 JE WALL $1� � _J _ E-14LBf72.771' N d U --E— UNDERGROLNO ELECTRIC LIE ^ Rf3j f / EL72336' °� N ---,v— LOCERI(WOUNO'WATER LINE U 6j E — — &"°`A''# 'NE Outfall Structure ID: ULS004-0174 Outfall Structure ID: ULS004-0174 R&A' 7t7 tl.BB%� 0 S`°RI" DRAIN LINE Lat: 35 ° 13' 21.84" North I n6 Cat 35 ° 13' 22.04" North o 0- OVERHEAD'A1RE �/ 91 DUCT BANK Long 800 50' 49.83" West a `� Long: 80 ° 50' 49.93" West , �O CSQSC - T2049' 0 A+ NV. - 715.80' I- SCtECLLE 8 EXCEPTION F NV. - 715AIT GROUNDWATER RESULTS SUMMARY TABLE RECEIVED/NCDEQ/DWR N OVA CHARLOTTE METRO Charlotte, North Carolina Table 1: Groundwater Results Summary JUL 0 S 2019 Water Quality Permitting Section Hardness In Volatile Organic Compounds (VOCs) In pg/L Potynuclear Aromatic Hydrocarbons (PAHs) Metals in mg/L mg/L In pg/L m c E m m E m m m c E `m O` O O` N N N m m m L m L _� U O Q 0_ E '2 O r U E U O L U C m m C a m o �` m C m C m C m L L E U c� E U n c`� m J "+ m m Y U Z C N 'Cl m m o m N D 0 0 0 N O E T o m O �o O m S, X S rj 51 $ w m tp U C m ? L U C m > n pp U C m > m J C m ? m f C m > U Z C m C m _= !qq b m E o p r Q a o °° m �' m m = d m m ? N m c o o 0 =( 0 o 0 o 0 o m o O Sample ID Date Sampled r- m m U 0 0 Mn_ z E � N m 0 b 0 o 0 0 0 t 0 0 MW-1 4/3/2017 NA BRL BRL BRL BRL 1.0 BRL BRL BRL I BRL 2.5 0.75 BRL 9.2 J 1 7.2 J 28 1 8.2 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5/30/2019 360 BRL BRL BRL BRL 0.381 BRL BRL BRL BRL 0.72 BRL BRL BRL BRL BRL BRL 97 BRL 0.029 BRL BRL BRL BRL BRL 30 BRL 0.014 BRL BRL BRL MW 2 4/3/2017 NA 11 1.5 BRL 1.5 BRL BRL 0.61 17 1.2 BRL BRL BRL BRL BRL BRL BRL NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5/30/2019 Not Sampled. Well was dry. MW-3 4/3/2017 NA BRL BRL 1.1 4.3 BRL 0.64 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NA NA NALBR NA NA NA NA NA NA NA A 5/30/2019 210 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 44 BRL 0.0240.013 BRL 0.011 BRL 23 BRL BRL LMW-4 4/3/2017 NA BRL BRL 1.7 6.5 BRL 1.0 BRL BRL BRL BRL BRL 0.62 J BRL BRL 3.2 J BRL NA NA NA NA NA NA NA NA NA NA A5/30/2019 230 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 53 BRL 0.0200.017 BRL BRL BRL 24 BRL 0.020 LMW-5 4/3, 5 and 14/2017 ZEIR Not Sampled. Well was dry. 5/30/2019 Not Sampled. Well was dry. NCDEQ 02B Standards 100 NE 1.19 NE NE NE NE NE 0.7 2.5 NE NE NE NE NE NE NE 0.13608* 0.13608* 0.01688* 0.i; . 0.00559* 0.00559* NE NE 0.09742* 0.72US EPA NRWQC NE NE NE NE 60 NE NE NE NL NL NE NE NE NE NE 0.32 20 NE NE NE NE 1.3 NE NE NE NE NE NE E J - An estimated concentration detected below the reporting limit. BRL- Below Laboratory Reporting Limit NCDEQ 02B Standards - North Carolina Department of Environmental Quality 02B Water Quality Standards for Surface Waters (Most Stringent Freshwater Standard) US EPA NRWQC- United States Environmental Protection Agency Nationally Recommended Water Quality Criteria (Most Stringent Freshwater Standard) NE - Not Established NA- Not Analyzed * - Calculated using hardness of 210 mg/L Bold - Indicates a detection above laboratory reporting limits Bold & Highlighted - Indicates a detection above the applicable regulatory standard GROUNDWATER LABORATORY DATA Case Narrative Flf j��. V f e��'a S�. �IABORATORIE$ING Full -Service Analytical & Environmental Solutions Anchor QEA of North Carolina, PLLC Mike Falknor 231 Haywood Street Asheville, NC 28801 NC Certification No. 402 NC Drinking Water Cent No. 37735 SC Certification No. 99012 Project: Charlotte Metro Lab Submittal Date. 04/03/2017 Prism Work Order: 7040018 04/05/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: Reviewed By Robbi A. Jones President/Project Manager D RPD value outside of the control limits. J Detected but below the Reporting Limit, therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240543 -Charlotte, NC 28224-0643 _ Phone: 7041529-6364 • Toll Free Number: 1-8001529-6364 - Fax: 7041626-0409 Page 1 of 19 IS� %� Fun -Service Analytical �v� i Environmental Solutions Sample Receipt Summary 04/05/2017 Prism Work Order: 7040018 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received MW-1 7040018-01 Water 04/03/17 04/03/17 Samples were received in good condition at 1.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041626-0409 Page 2 of 19 Summary of Detections Full -Service Analytical P R I S M Environmental Solutions 04/05/2017 lvt, Prism Work Order: 7040018 Prism ID Client ID Parameter Method Result Units 7040018-01 MW-1 as- 1,2-Dichloroethylene 8260E 1.0 ug/L 7040018-01 MW-1 Tetrachloroethylene 6260E 2.5 ug/L 7040018-01 MW-1 Trichloroethylene 82606 0.75 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041626-0409 Page 3 of 19� F? R I S M Laboratory Report Full -Service RnalytiCal 6 Environmental Solutions 04/05/2017 icl!", ,._._�.i "'ueonnfoarekinc. Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-1 Attn: Mike Falknor Prism Sample ID: 7040018-01 231 Haywood Street Prism Work Order: 7040018 Asheville, NC 28801 Sample Matrix: Water Time Collected: 04/03/17 12:12 Time Submitted: 04/03/17 15:24 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 1.8 1 8270D 4/4/17 15:30 JMV P7D0004 1,2-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 4/4/17 15:30 JMV P7D00D4 1,3-Dichlorobenzene BRL ug/L 10 1.9 1 82700 414/17 15.30 JMV P7D00D4 1,4-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 414/17 15:30 JMV P7DD004 1-Methylnaphthalene BRL ug/L 1D 2.6 1 8270D 414/17 15:30 JMV P7D0004 2,4,5-Trichlorophenol BRL ug/L 10 1.6 1 5270D 4/4/17 15:30 JMV P71D0004 2,4,6-Trichtorophenol BRL ug/L 10 1.8 1 8270D 414/17 15:30 JMV P7D0004 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270D 414/17 15.30 JMV P7DO004 2,4-Dimethylphenol BRL ug]L 10 3A 1 8270D 4/4/17 15:30 JMV P7DOOD4 2,4-Dinitrophenol BRL ug/L 10 2.7 1 8270D 4/4/17 15:30 JMV P700004 2,4-Dinitrotoluene BRL ug/L 10 1.4 1 8270D 414117 15:30 JMV P7D0004 2,6-Dinitrotoluene BRL ug/L 10 1.1 1 8270D 414/17 15:30 JMV P7D0004 2-Chloronsphthalene BRL ug/L 10 2.7 1 8270D 4/4/17 15:30 JMV P7130004 2-Chlorophenol BRL ug/L 10 1.9 1 8270D 4/4/17 15:30 JMV P7D0004 2-Methylnaphthalene BRL ug/L 10 2.4 1 8270D 414117 15:30 JMV P7D0004 2-Methyiphenol BRL ug/L 10 1.8 1 8270D 414117 15:30 JMV P7D0004 2-Nitroaniline BRL ug/L 10 1.4 1 8270D 414117 15:30 JMV P7D0004 2-Nitrophenol BRL ug/L 10 2.4 1 8270D 414117 15:30 JMV P7D0004 3,3'-Dichlorobenzidine BRL ug/L 10 1.4 1 8270D 4/4117 15:30 JMV P7D0004 3/4-Methylphenol BRL ug/L 10 1.5 1 8270D 4/4/17 15:30 JMV P7D0004 3-Nitroaniline BRL ug/L 10 1.4 1 8270D 4/4117 15:30 JMV P7D0004 4,6-Dinitro-2-methylphenol BRL ug/L 10 1.4 1 8270D 414117 15:30 JMV P7D0004 4-Bromophenyi phenyl ether BRL ug/L 10 1.3 1 8270D 4/4/17 15:30 JMV P7D0004 4-Chloro-3-methylphenol BRL ug/L 10 2.4 1 8270D 4/4117 15:30 JMV P7DOOD4 4-Chloroaniline BRL ug/L 10 2.4 1 82700 4/4117 15:30 JMV P7DO004 4-Chlorophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 4/4117 15:30 JMV P7010004 4-Nitroaniline BRL ug/L 10 0.93 1 8270D 4/4117 15:30 JMV P7100004 4-Nitrophenol BRL ug/L 10 0.60 1 8270D 4/4117 15:30 JMV P7D0004 Acenaphthene BRL ug/L 10 1.8 1 8270D 4/4/17 15:30 JMV P7D0004 Acenaphthylene BRL ug/L 10 2.0 1 8270D 414/17 15:30 JMV P7D0004 Aniline BRIL ug/L 10 2.4 1 8270D 4/4117 15:30 JMV P7DOD04 Anthracene BRL ug/L 10 1.4 1 8270D 414117 15:30 JMV P7DODO4 Azobenzene BRL ug/L 10 1.8 1 8270D 414/17 15:30 JMV P7DOD04 Benzo(a)anthracene BRL ug/L 10 1.4 1 8270D 4/4117 15:30 JMV P7D0004 Benzo(a)pyrene BRL ug/L 10 1.4 1 8270D 414/17 15:30 JMV P7DOD04 Benzo(b)Ouoranthene BRL ug/L 10 1.1 1 8270D 4/4/17 15:30 JMV P7D0004 Benzo(g,hJ)perylene BRL ug/L 10 1.4 1 8270D 4/4117 15:3D JMV P7DOD04 Benzo(k)fluoranthene BRL ug/L 10 1.4 1 8270D 414/17 15:30 JMV P700004 Benzoic Acid BRL ug/L 100 4.7 1 8270D 414117 15:30 JMV P7100004 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 414117 15:30 JMV P7D0004 bis(2-Chloroethoxy)methane BRL ug/L 10 2.6 1 8270D 414/17 15:30 JMV P7DOD04 Bis(2-Chloroethyl)ether BRL ug/L 10 2.3 1 8270D 4/4117 15:30 JMV P7D0004 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories. Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364 -Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 4 of 19 , PRISMLaboratory Report Full -Service Analytical 8 Environmental Solutions 04/05/2017 tok „£is:"`i<a«nroka5 we Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-1 Attn: Mike Falknor Prism Sample ID: 7040018-01 231 Haywood Street Prism Work Order: 7040018 Asheville, NC 28801 Sample Matrix: Water Time Collected: 04/03/17 12:12 Time Submitted: 04/03/17 15:24 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis DateMme Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.0 1 8270D 414/17 15:30 JMV P7DOD04 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.3 1 8270D 4/4/17 15:30 JMV P700004 Butyl benzyl phthalate BRL ug/L 10 1.4 1 8270D 414/17 15:30 JMV P7130004 Chrysene BRL ug/L 10 1.4 1 8270D 4/4/17 15:30 JMV P7D0004 Dibenzo(a,h)anthracene BRL ug/L 10 1.2 1 8270D 4/4/17 15:30 JMV P7D0004 Dibenzoturan BRL ug/L 10 1.8 1 8270D 414/17 15:30 JMV P7D6004 Diethyl phthalate BRL ug/L 10 3.3 1 8270D 414/17 15:30 JMV P71)0004 Dimethyl phthalate BRL ug/L 10 1.4 1 8270D 414117 15:30 JMV P7DO004 Di-n-butyl phthalate BRL ug/L 10 13 1 8270D 414117 15:30 JMV P7130004 Di-n-Dctyl phthalate BRL ug/L 10 1.3 1 8270D 4/4/17 15:30 JMV P71)0004 Fluoranthene BRL ug/L 10 1.7 1 8270D 414/17 16:30 JMV P7D0004 Fluorene BRL ug/L 10 1.7 1 8270D 414117 15:30 JMV P7D0004 Hexachlorobenzene BRL ug/L 10 1.3 1 8270D 4/4117 15:30 JMV P7D0004 Hexachlorobutadiene BRL ug/L 10 2.1 1 8270D 4/4117 15:30 JMV P7D0004 Hexachlorocyclopentadiene BRL ug/L 10 1.7 1 8270D 4/4/17 15:30 JMV P700004 Hexachloroethane BRL ug/L 10 1.7 1 8270D 414/17 15:30 JMV P71)0004 Indeno(1,2,3-cd)pyrene BRL ug/L 10 3.9 1 8270D 414117 15:30 JMV P71)0004 Isophorone BRL ug/L 10 2.5 1 8270D 4/4/17 16:30 JMV P7D00D4 Naphthalene BRL ug/L 10 2.6 1 8270D 414/17 15:30 JMV P7D0004 Nitrobenzene BRL ug/L 10 2.6 1 8270D 4/4/17 15:30 JMV P7D0004 N-Nitroso-di-n-propylamine BRL ug/L 10 2.2 1 8270D 4/4/17 15:30 JMV P7D00D4 N-Nitrosodiphenylamine BRL ug/L 10 1.3 1 8270D 4/4/17 15:30 JMV P71)0004 Pentachlorophenol BRL ug/L 10 1.2 1 8270D 4/4/17 15:30 JMV P71)0004 Phenanthrene BRL ug/L 10 1.5 1 8270D 4/4/17 15:30 JMV P7D0004 Phenol BRL ug/L 10 0.98 1 8270D 4/4117 15:30 JMV P7D0004 Pyrene BRL ug/L 10 1.4 1 8270D 4/4/17 15:30 JMV P71)0004 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 78 % 43-140 2-Fluorobiphenyl 67 % 44-119 2-Fluorophenol 41 % 19-119 Nitrobenzene-d5 60 % 44-120 Pheno1-d5 29 % 11-52 Terphenyl-d14 98 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 4/4/17 12:23 KDM P7DO037 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 4/4/17 12:23 KDM P7DO037 1, 1, 2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 414117 12:23 KDM P7DO037 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 82608 414/17 12:23 KDM P700037 1, 1 -Dichloroethane BRL ug/L 0.50 0.083 1 82608 414117 12:23 KDM P7DO037 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 414/17 12:23 KDM P7DO037 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 4/4/17 12:23 KDM P71)0037 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 414/17 12:23 KDM P7D0037 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 4/4/17 12:23 KDM P7DOD37 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 _ Phone: 704/629-6364 - Toll Free Number: l-8001629-6364- Fax: 7041626-"09 Page 5 of 1971 Laboratory Report R Full -Service Analytical 8 I Environmental solutions 04/05/2017 '?��*='i "'tR00R410RIES INC. Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MWA Attn: Mike Falknor Prism Sample ID: 7040018-01 231 Haywood Street Prism Work Order: 7040018 Asheville, NC 28801 Sample Matrix: Water Time Collected: 04/03/17 12:12 Time Submitted: 04/03/17 15:24 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichiorobenzene BRL ug/L 1.0 0.13 1 8260B 4/4/17 12:23 KDM P7DD037 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 82608 4/4/17 12:23 KDM P7DO037 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 4/4/17 12:23 KDM P7DO037 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 414/17 12:23 KDM P71)0037 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 4/4/17 12:23 KDM P7DO037 1,2-Dichloroethane BRL ug/L 0.50 0,066 1 8260B 4/4/17 12:23 KDM P7DD037 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 4/4/17 12:23 KDM P7DO037 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 4/4/17 12:23 KDM P7DO037 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 4/4/17 12:23 KDM P7DO037 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 4/4/17 12:23 KDM P7DO037 1.4-Dichlorobenzene BRL ug/L 0.50 0.051) 1 8260B 4/4/17 12:23 KDM P7DO037 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 414/17 12:23 KDM P71)0037 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 414/17 12:23 KDM P71)0037 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 4/4/17 12:23 KDM P7130037 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 4/4/17 12:23 KDM P7DD037 Acetone BRL ug/L 5.0 0.31 1 8260B 4/4117 12:23 KDM P700037 Acrolein BRL ug/L 20 0,20 1 8260B 4/4/17 12.23 KDM P71)0037 Acrylonithle BRL ug1L 20 0.20 1 8260B 4/4/17 12:23 KDM P71)0037 Benzene BRL ug/L 0.50 0.048 1 8260B 4/4/17 12:23 KDM P71)0037 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 4/4/17 12:23 KDM P700037 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 414/17 12:23 KDM P700037 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 4/4117 12:23 KDM P71)0037 Bromoform BRL ug/L 1.0 0.040 1 8260B 414/17 12:23 KDM P7DO037 Bromomethane BRL ug/L 1.0 0.18 1 8260B 4/4/17 12:23 KDM P700037 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 4/4/17 12:23 KDM P700037 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 414117 12:23 KDM P7DO037 Chlorobenzene BRL ug/L 0.60 0.062 1 8260B 4/4/17 12:23 KDM P7DO037 Chloroethane BRL ug/L 0.50 0.22 1 8260B 4/4/17 12:23 KDM P71)0037 Chloroform BRL ug/L 0.50 0.076 1 8260B 4/4/17 12:23 KDM P7DO037 Chloromethane BRL ug/L 0.50 0.079 1 82608 414/17 12:23 KDM P7DO037 cts-1,2-Dichloroethylene 1.0 ug/L 0.60 0.066 1 8260B 414117 12:23 KDM P700037 cis- 1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 4/4/17 12:23 KDM P7DO037 Dibromochloromethane BRL ug/L 0.50 0.081 1 82608 414/17 12:23 KDM P71)0037 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 4/4/17 12:23 KDM P7DO037 Diichloroditiuoromethane BRL ug/L 1.0 0.11 1 8260B 4/4/17 12:23 KDM P7DO037 Ethylbenzene BRL ug/L 0.50 0,061 1 8260B 4/4/17 12:23 KDM P7DO037 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 4/4117 12:23 KDM P7DO037 Isopropyl Ether BRL ug/L 0.50 0.050 1 82608 4/4/17 12:23 KDM P7DO037 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 414/17 12:23 KDM P7DO037 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 414/17 12:23 KDM P7DOD37 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 414/17 12:23 KDM P7D0037 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 4/4/17 12:23 KDM P71)0037 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 4/4117 12:23 KDM P71)0037 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 44S Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364-Toll Free Number: 1-5001529.6364-Fax:704/626-0409 Page of 99 II t Laboratory Report s ix A I Service Analytical 8 t , V E Environmental Solutions 04105/2017 n�.�'-S; "':tAgpA4ipAl[E ING Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW 1 Attn: Mike Falknor Prism Sample ID: 7040018-01 231 Haywood Street Prism Work Order: 7040018 Asheville, NC 28801 Sample Matrix: Water Time Collected: 04/03/17 12:12 Time Submitted: 04/03/17 15:24 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/lime ID Methylene Chloride BRL ug/L Methyl-tert-Butyl Ether BRL ug/L Naphthalene BRL ug/L n-Butylbenzene BRL ug/L n-Propylbenzene BRL ug/L o-Xylene BRL ug/L sec-Butylbenzene BRL ug1L Styrene BRL ug/L tert-Butylbenzene BRL ug/L Tetrachloroethylene 2.6 ug/L Toluene BRL ug/L trans-1,2-Dichloroethylene BRL ug/L trans- 1,3-Dichloropropylene BRL ug/L Trichloroethylene 0.75 ug/L Trichlorofluoromethane BRL ug/L Vinyl acetate BRL ug/L Vinyl chloride BRL ug/L 1.0 0.083 1 8260B 4/4/17 12:23 KDM P7D0037 0.50 0.042 1 8260B 414/17 12:23 KDM P7D0037 1.0 0.19 1 8260B 414/17 12:23 KDM P700037 1.D 0,076 1 82608 414/17 12.23 KDM P700037 0.50 0.087 1 8260B 414117 12:23 KDM P7D0037 0.50 0.044 1 8260B 4/4/17 12:23 KDM P7DO037 0.50 0.076 1 8260B 4/4/17 12:23 KDM P7D0037 0.50 0,047 1 8260B 414117 12:23 KDM P7D0037 0.50 0.088 1 8260B 4/4/17 12:23 KDM P7130037 0.50 0.098 1 8260B 414117 12:23 KDM P7D0037 0.50 0.044 1 8260B 4/4117 12:23 KDM P7DOD37 0.50 0.094 1 8260B 414/17 12:23 KDM P7D0037 0.50 0.070 1 8260B 414/17 12:23 KDM P7D0037 0.50 0.078 1 8260B 414117 12:23 KDM P71110037 0.50 0.062 1 8260B 414/17 12:23 KDM P7D0037 2.0 0.060 1 8260B 4/4/17 12:23 KDM P7DO037 0.50 0.097 1 8260B 414/17 12:23 KDM P7D0037 Surrogate Recovery Control Limits 4-Bromofluorobenzene 111 % 80-124 Dibromofluoromethane 99 % 75-129 Toluene-d8 101 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/625-0409 Page 7 of 19 P I Is M I Full -Service Analytical s Environmental Solutions Level 11 QC Report 415/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0037 - 6030B Blank (P7D0037-BLKt) Prepared & Analyzed: 04/04/17 1, 1, 1,2-Tetrachioroethane BRL 0.50 ug/L 1, 1, 1 -Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1, 1, 2-Trichloroethane BRL 0.50 ug/L 1,1-Dichioroethane BRL 0.50 ug/L 1,1-Dichioroethylene BRL 0,50 ug/L 1,1-Dichioropropylene BRL 0,50 ug/L 1,2,3-Trichlorobenzene BRL 2-0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethylbenzene BRL 0.50 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0,50 ug/L 1,3,5-Trimethylbenzene BRL 0,50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 uglL Bromochioromethane BRL 0.50 ug/L 8romodichloromethane BRL 0,50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0,50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 1.0 ug/L Ethytbenzene BRL 0.50 ug/L Hexachlorobutadiene BRL 2.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629 6364 -Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 8 of 19 r] 1� %� j Euviron ice.anai Solutions s 1 v' I Environmentt�l $UiutiOns Level 11 QC Report 4/5/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GClMS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0037 - 6030B Blank (P7D0037.8LK1) _ _ Prepared & Analyzed: 04/04/17 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tart-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans-1,2-Dichloroethylene BRL 0.50 ug/L trans- 1, 3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Surrogate:4-Bromofluorobenzene 55.4 ug//- 50.00 111 80-124 Surrogate: Dibmmotluoromethane 50.2 ug/L 50.00 100 75-129 Surrogate: Toluene-0 49.6 ug/L 50.00 99 77-123 LCS (P7D0037-BSI) _ Prepared & Analyzed: 04/04/17 _ 1,1,1,2-Tetrachloroethane 19.9 0.50 ug/L 20.00 99 79-134 1,1,1-Trichloroethane 19.9 0.50 ug/L 20.00 99 75-136 1,1,2,2-Tetrachloroethane 22.4 0.50 ug/L 20.00 112 62-127 1,1,2-Trichloroethane 20.7 0.50 ug/L 20.00 103 70-140 1,1-Dichloroethane 19.7 0.5D ug/L 20.00 99 78-130 1,1-Dichloroethylene 18.7 0.50 ug/L 20.00 93 70-154 1,1-Dichloropropylene 22.9 0.50 ug/L 20.00 115 71-136 1,2,3-Tcchlorobenzene 20.9 2.0 ug/L 20.00 105 58-144 1,2,3-Trichloropropane 22.6 1.0 ug/L 20.DD 113 71-127 1,2,4-Trichlorobanzene 21.2 1.0 ug1L 20.00 106 66-139 1,2,4-Trimethylbenzene 21.9 0,50 ug/L 20.00 109 75-133 1,2-Dibromo-3-chloropropane 22.3 2.0 ug/L 20.00 112 63-134 1,2-Dibromoethane 22.5 0.50 ug/L 20.00 113 77-135 1,2-Dichlorobenzene 21.0 0.50 ug/L 20.00 105 78-128 1,2-Dichloroethane 20.6 0.50 ug/L 20.00 103 68-131 1,2-Dichloropropane 21.0 0.60 ug/L 20.00 105 77-130 1,3,5-Trimethylbenzene 21.6 0,50 ug/L 20.00 108 75-131 1,3-Dichlorobenzene 20.2 0,50 ug/L 20.00 101 77-125 1,3-Dichloropropane 22.8 0.6D ug/L 20.00 114 76-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1.800/629-6364 - Fax: 7041626-0409 "" pa9"" ge g of 19 Fun -Service Analytical R ISM I Envir ervice A Solutions Level 11 QC Report 4/5/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GCJMS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P71010037 - 6030B LCS (P7D0037-BS1) _ Prepared &Analyzed: 04104/17_- 1,4-Dichlorobenzene 20.5 0.50 ug/L 20.00 103 75-126 2,2-Dichicropropane 20.7 2.0 ug/L 20.00 103 29-149 2-Chlorotoluene 21.7 0.50 ug/L 20.00 109 74-126 4-Chlorotoluene 22.4 0.50 ug/L 20.00 112 78-129 4-Isopropyltoluene 20.4 0.50 ug/L 20,00 102 69-132 Acetone 39.6 5.0 ug/L 40.00 99 40-166 Acrolein 48.1 20 ug/L 40.00 120 70-130 Acrylonitrile 42A 20 ug/L 40.00 106 81-127 Benzene 20,2 0.50 ug/L 20.00 101 77-128 Bromobenzene 21.7 0.50 ug/L 20.00 108 78-129 Bromochloromethane 20.2 0.50 ug/L 20.00 101 78-135 Bromodichloromethane 20.8 0.50 ug/L 20.00 104 76-138 Bromoform 18A 1.0 ug/L 20,00 92 71-135 Bromomethane 15.5 1.0 ug/L 20.00 77 41-168 Carbon disulfide 19.7 5.0 ug/L 20.00 98 59-135 Carbon Tetrachloride 21.1 0.50 ug/L 20.00 106 72-142 Chiorobenzene 20.4 0.50 ug/L 20.00 102 78-119 Chloroethane 15.0 0.50 ug/L 20.00 75 57-142 Chloroform 20.3 0.50 ug/L 20.00 101 77-130 Chioromethane 15.0 0.50 ug/L 20.00 75 47-145 cis-1,2-Dichloroethylene 20.3 0.50 ug/L 20.00 102 76-141 cis-1,3-Dichloropropylene 20.5 0.50 ug/L 20.00 102 65-140 Dibromochloromethane 20.5 0.50 ug/L 20.00 102 75-134 Dibromomethane 20.8 0.50 ug/L 20.00 104 76-138 Dichlorodifluoromethene 21.6 1.0 ug/L 20.00 108 28-163 Ethylbenzene 20.9 0.50 ug/L 20.00 104 80-127 Hexachlorobutadiene 20.3 2.0 ug/L 20.00 101 61-134 Isopropyl Ether 19.5 0.50 ug/L 20.00 98 60-154 Isopropylbenzene (Cumene) 22.1 0.50 ug/L 20.00 110 70-130 m,p-Xylenes 43.2 1.0 ug/L 40.00 108 77-133 Methyl Butyl Ketone (2-Hexanone) 21.9 5.0 ug/L 20.00 110 64-137 Methyl Ethyl Ketone (2-Butanone) 21.7 5.0 ug/L 20.00 108 71-134 Methyl Isobutyl Ketone 20.3 5.0 ug/L 20.00 101 69-134 Methylene Chloride 18.9 1.0 ug/L 20.00 95 73-131 Methyl-tert-Butyl Ether 19,8 0.50 ug/L 20.00 99 68-135 Naphthalene 23.2 1.0 ug/L 20.00 116 64-136 n-Butytbenzene 21.1 1.0 ug/L 20.00 105 68-134 n-Propylbenzene 22.0 0.50 ug/L 20.00 110 72-132 o-Xylene 21.1 0.50 ug/L 20.00 105 78-128 sec-Butylbenzene 21.7 0.60 ug/L 20.00 108 71-131 Styrene 19.0 0.50 ug/L 20.00 95 78-129 tert-Butylbenzene 21A 0.50 ug/L 20.00 107 70-132 Tetrachloroethylene 20.5 0,50 ug/L 20.00 102 80-129 Toluene 20.0 0.50 ug/L 20.00 100 76-131 trans-1,2-Dichloroethylene 21.0 0.50 ug/L 20.00 105 76-135 Vans-1,3-Dichloropropylene 20.3 0.50 ug/L 20.00 101 67-140 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: l-8001629-6364- Fax: 7041626-0409 Page 10 of 19 , �^ Pk.R i S M ( EnviService Analytical Environmental Solutions Level 11 QC Report 4/5117 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GCIMS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P71010037 - 5030B LCS (P7D0037-BSI) Prepared & Analyzed: 04/04/17 _ Trichloroethytene 19.7 0.50 ug/L 20.00 99 77-133 Thchlorofluoromethane 16.8 0.50 ug/L 20.00 84 62-148 Vinyl acetate 20.9 2.0 ug/L 20.00 105 34-167 Vinyl chloride 19.6 0.50 ug/L 20.00 98 57-141 Surrogate:4-Bronlofluorobenzene 53.8 uglL 50.00 108 80-124 Surrogate: Dibromo/luoromethane 49.6 ug/L 50.00 99 75-129 Surrogate: Toluene-o'8 50.2 U94 50.00 100 77-123 LCS Dup (137130037-121SD1_)_ _ Prepared & Analyzed: 04/04/17 _ 1,1,1,2-Tetrachloroethane 20.4 0.50 ug/L 20.00 102 79-134 3 20 1,1,1-Trichloroethane 20.4 0.50 ug/L 20.00 102 75-136 3 20 1,1,2,2-Tetrachloroethane 22.4 0.50 ug/L 20.00 112 62-127 0.4 20 1,1,2-Trichloroethane 21.6 0.50 ug/L 20.00 108 70-140 4 20 1,1-Dichloroethane 20.4 0.50 ug/L 20.00 102 78-130 3 20 1,1-Dichloroethylene 19.1 0.50 ug/L 20.00 95 70-154 2 20 1,1-Dichloropropylene 23.4 0.50 ug/L 20.00 117 71-136 2 20 1,2,3-Trichlorobenzene 22.2 2.0 uglL 20.00 ill 58-144 6 20 1,2,3-Trichloropropane 22,6 1,0 ug/L 20,00 113 71-127 0.4 20 1,2,4-Trichlorobenzene 22,5 1.0 ug/L 20.00 113 66-139 6 20 1,2,4-Trimethylbenzene 22.3 0.50 ug/L 20.00 112 75-133 2 20 1,2-Dibromo-3-chloropropane 21.4 2.0 ug/L 20A0 107 63-134 4 20 1,2-Dibromoethane 2Z8 0.50 ug/L 20,00 114 77-135 1 20 1,2-Dichlorobenzene 21.4 0.50 ug/L 20.00 107 78-128 2 20 1,2-Dichloroethane 21.4 0.50 ug/L 20.00 107 68-131 4 20 1,2-Dichloropropane 21.4 0.50 ug/L 20.00 107 77-130 2 20 1,3,5-Trimethylbenzene 22.1 0.50 ug/L 20,00 110 75-131 2 20 1,3-Dichlorobenzene 20.8 0,50 ug/L 20.00 104 77-125 3 20 1,3-Dichloropropane 23.2 0.50 ug/L 20.00 116 76-132 2 20 1,4-Dichlorobenzene 20.8 0.50 ug/L 20.00 104 75-126 1 20 2,2-Dichloropropane 20,8 2.0 ug/L 20.00 104 29-149 0.4 20 2-Chbrotoluene 22.1 0.50 ug/L 20.00 110 74-126 2 20 4-Chbrotoluene 22.6 0.50 ug/L 20.00 113 78-129 1 20 4-Isopropyltoluene 20.9 0.50 ug/L 20.00 104 69-132 2 20 Acetone 38.0 5.0 ug/L 40.00 95 40-166 4 20 Acrolein 45.1 20 ug/L 40.00 113 70-130 7 20 Acrylonitrile 41.9 20 ug/L 40.00 105 81-127 1 20 Benzene 20.8 0.50 ug/L 20.00 104 77-128 3 20 Bromobenzene 22.5 0.50 ug/L 20,00 112 78-129 4 20 Bromochloromelhane 20.6 0.56 ug/L 20.00 103 78-135 2 20 Bromodichloromethane 21.3 0.50 ug/L 20.00 1D6 76-138 2 20 Bromoform 18.5 1.0 ug/L 20.00 93 71-135 0.6 20 Bromomethane 17.0 1.0 ug/L 20.00 85 41-168 10 20 Carbon disulfide 20.2 5.0 ug/L 20.00 1 D1 59-135 3 2D Carbon Tetrachloride 20.4 0.50 uglL 20.00 1 D2 72-142 3 2D Chlorobenzene 21,0 0.50 ug/L 20.00 105 78-119 3 20 Chloroethane 16.0 0.5D ug/L 20.00 80 57-142 6 20 Chloroform 20.8 0.50 ug/L 20.00 104 77-130 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toil Free Number:1-800/529-6364 - Fax: 7041526-0409 r Page 11 of 19 [� Analytical I Environmental Solutions Level II QC Report 415/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GCfMS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7DO037 - 6030B LCS Dup (P7D0037-BSD1) Prepared & Analyzed: 04/04/17 Chloromethane 16.5 0.50 ug/L 20.00 82 47-145 10 20 cis-1,2-Dichloroethylene 21.0 0.50 ug/L 20.00 105 76-141 3 20 cis-1,3-Dichloropropylene 21.0 0.50 ug/L 20.00 105 65-140 3 20 Dibromochloromethane 20.9 0.50 ug/L 20.00 104 75-134 2 20 Dibromomethane 21.2 0.50 ug/L 20.00 106 76-138 2 20 Dichlorodifluoromethane 22.0 1.0 ug/L 20.00 110 28-163 2 20 Ethylbenzene 21.3 0.50 ug/L 20.00 107 80-127 2 20 Hexachlorobutadiene 21.2 2.0 ug/L 20.00 106 61-134 4 20 Isopropyl Ether 20.1 0.50 ug/L 20.00 100 60-154 3 20 Isopropylbenzene (Cumene) 22.6 0.50 ug/L 20.00 113 70-130 2 20 m,p-Xylenes 43.8 1.0 ug/L 40.00 110 77-133 1 20 Methyl Butyl Ketone (2-Hexanone) 21.2 5.0 ug/L 20.00 106 64-137 3 20 Methyl Ethyl Ketone (2-Butanone) 21,7 5.0 ug/L 20.00 108 71-134 0.05 20 Methyl Isobutyl Ketone 20.0 5.0 ug/L 20.00 100 69-134 1 20 Methylene Chloride 19.5 1.0 ug/L 20.00 97 73-131 3 20 Methyl-tert-Butyl Ether 20.2 0.5D ug/L 20.00 101 68-135 2 20 Naphthalene 23.6 1.0 ug/L 20.00 118 64-136 2 20 n-Butylbenzene 21.3 1.0 ug/L 20.00 107 68-134 1 20 n-Propylbenzene 22.2 0.50 ug/L 20.00 111 72-132 0.9 20 o•Xylene 21.7 0,50 ug/L 20.00 109 78-128 3 20 sec-Butylbenzene 22.1 OM ug/L 20,00 110 71-131 2 20 Styrene 19.9 0.50 ug/L 20.00 100 7a-129 4 20 tert-Butylbenzene 22.0 0.50 ug/L 20.00 110 70-132 3 20 Tetrachloroethylene 20.5 0.50 ug/L 20.00 102 80-129 0.2 20 Toluene 20.4 D.50 ug/L 20.00 102 76-131 2 20 trans-1,2-Dichioroethylene 21.5 0.50 ug/L 20,00 108 76-135 2 20 trans-1,3-Dichloropropylene 20.8 OM ug/L 20.00 104 67-1140 3 20 Trichloroethylene 19.9 MD ug/L 20.00 10D 77-133 1 20 Trichiorofluoromethane 17.1 0,50 ug/L 20.00 86 62-148 2 2D Vinyl acetate 21.3 2.0 ug/L 20.00 107 34-167 2 20 Vinyl chloride 20.4 0.50 ug/L 20.00 102 57-141 4 20 Surrogate:4-Bromofluorobenzene 55.0 u94 50.00 110 80-124 Surrogate: Dibromotluoromethene 50.3 uglL 50.00 101 75-129 Surrogate: Toluene -de 51.6 U91L 50.00 103 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-800/629-6364 - Pax: 7041626-0409 Page 12 of 19 ISM Full- Service Analytical Environmental Solutions Level it QC Report 4/5/17 Anchor 0EA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0004 - 3510C MS Blank (P7d0004-BLK1) Prepared &Analyzed: 04/03/17 1,2,4-Tiichoorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methylnaphthalene BRL 10 ug/L 2,4,5-Trichlorophenof BRL 10 ug/L 2,4,6-Trichlorophenot BRL 10 ugJL 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthatene BRL 10 ug/L 2-Chlorophenot BRL 10 ug/L 2-Methylnaphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 uglL 314-Methylphenol BRL 10 ug/L 3-Nitroanifine BRL 10 ug/L 4,6-Dinilro-2-methylphenot BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitroaniline BRL 10 ugJL 4-Nitrophenoi BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug/L Aniline BRL 10 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Senzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Sis(2-chloroisopropypether BRL 10 ug/L Bis(2-EthylheW)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road • P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-0364-Toll Free Number: l-8001629.6364- Fax: 7041626-0409 Page 13 of 19 �` rF M Full-Service Analytical& P I Si Environmental solutions �tAAn11FTO Level II QC Report 4/5117 Anchor 0EA of North Carolina, PLLC Project Charlotte Metro Prism Work Order: 7040018 Attm Mike Falknor Time Submitted: 4/3/2017 3.24.00PM 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC1MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result % REC Limits RPD Limit Notes Batch P7D0004 - 3510C MS Blank (P7D0004-BLK1) _ _ _ Prepared & Analyzed: 04/03/17 u— Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 uglL Dt-n-butyl phthalate BRL 10 ug1L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachiorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocyciopentadiene BRL 10 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachiorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate. 2,4,6-Tribromophenol 85.3 ug/L 100.0 85 43-140 Surrogate: 2•Fluorobiphenyl 35.2 ug/L 50.00 70 44-119 Surrogate:2-Fluorophenol 49.0 ug/L 100.0 49 19-119 Surrogate: Nitrobenzene-d5 35.2 ug/L 50.00 70 44-120 Surrogate. Phenol-d5 31.7 ug/L 100.0 32 11-52 Surrogate. 7erphenyl-04 53.1 ug/L 50.00 106 50-134 This report should not be reproduced, except in its entirety without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704152M364 - Toll Free Number: 1-8001629-6364 - Fax: 704162"409 Page 14 of 19 Full -Service AnalyticalRISV I Environmental & Solutions Anchor QFA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GClMS - Quality Control Level II QC Report 4/5/17 Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD limit Notes Batch P7D0004 - 3510C MS LCS (P7D0004-BSI) _ Prepared &Analyzed: 04/03/17 1,2,4-Trichlorobenzene 26.7 10 ug/L 50.00 53 29-126 1,2-Dichlorobenzene 26.7 10 ug/L 50,00 53 32-111 1,3-Dichlorobenzene 24.4 10 ug/L 50.00 49 28-110 1,4-Dichlorobenzene 25.0 10 ug/L 50.00 50 29-112 1-Methylnaphthalene 351 10 ug/L 50.00 70 41-119 2,4,5-Trichlorophenol 42.2 10 ug/L 50.00 84 53-123 2,4,6-Trichlorophenol 43.1 10 ug/L 50.00 86 50-125 2,4-Dichlorophenol 36.1 10 ug/L 50.00 72 47-121 2,4-Dimethylphenol 44.3 10 ug/L 50.00 89 31-124 2,4-Dinitrophenol 56.7 10 ug/L 50.00 113 23-143 2,4-Dinitrotoluene 45.6 10 ug/L 50.00 91 57-128 2,6-Dinitrotoluene 46.4 10 ug/L 50.00 93 57-124 2-Chloronaphthalene 37.4 10 ug/L 50.00 75 40-116 2-Chlorophenol 36.7 10 ug/L 50.00 73 38-117 2-Methylnaphthalene 33.0 10 ug/L 50.00 66 40-121 2-Methylphenol 36.9 10 ug/L 50.00 74 3D-117 2-Nitreaniline 39.4 10 ug/L 50.00 79 55-127 2-Nitrophenol 36.1 10 ug/L 50.00 72 47-123 3,3'-Dichlorobenzidine 48.8 10 ug/L 50.00 98 27-129 3/4-Methylphenol 30.8 10 ug/L 50.00 62 29-110 3-Nitroanitine 40.2 10 ug/L 50.00 80 41-128 4,6-Dinitro-2-methylphenot 48.8 10 ug/L 50.00 98 44-137 4-Bromophenyl phenyl ether 42.2 10 ug/L 50.00 84 55-124 4-Chloro-3-methylphenol 39.4 10 ug/L 50.00 79 52-119 4-Chloroaniline 34.3 10 ug/L 50.00 69 33-117 4-Chlorophenyl phenyl ether 39.4 10 ug/L 50.00 79 53-121 4-Nitroaniline 38.7 10 ug/L 50,00 77 45-135 4-Nitrophenof 20.2 10 ug/L 50.00 40 10-77 Acenaphthene 42.9 10 ug/L 50.00 86 47-122 Acenaphthylene 39.9 10 ug/L 50.00 80 41-130 Aniline 44.8 10 ug/L 50.00 90 12-197 Anthrecene 45.7 10 ug/L 50.00 91 57-123 Azobenzene 45.8 10 ug/L 50.00 92 61-116 Benzo(a)anthracene 48.1 10 ug/L 50.00 96 58-125 Senzo(a)pyrene 45.2 10 ug/L 50.00 90 54-128 Benzo(b)fluoranthene 47.1 10 ug/L 50.00 94 53-131 Benzo(g,h,l)perylene 41.5 10 ug/L 50.00 83 50-134 Benzo(k)fluoranthene 43.8 10 ug/L 50,00 88 57-129 Benzoic Acid 15.1 100 ug/L 50.00 30 10-125 J Benzyl alcohol 34.6 10 ug/L 50.00 69 31-112 b>is(2-Chloroethoxy)methane 35.6 10 ug/L 50.00 71 48-120 Bis(2-ChioroethAether 33.3 10 ug/L 50.00 67 43-118 Bis(2-chloroisopropyoether 34.7 10 ug/L 50.00 69 37-130 Bis(2-Ethylhexyl)phthalale 48.5 10 ug/L 50.00 97 55-135 Butyl benzyl phthalate 47.8 10 ug/L 50.00 96 53-134 Chrysene 48.8 10 ug/L 50.00 98 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364 -Toll Free Number: 1-8001629-6364 - Fax: 704/626-0409 Page 15 of 19 ! Fulletce ORISM Environmental Solutions .di�1L�S:.Ya3.::.'.;;;: - 1A00RRTOkIES. !NL Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GCIMS - Quality Control Level 11 QC Report 415/17 Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0004 - 3610C MS LCS (P7t30004-BSI) _ _ _ _ Prepared 8 Analyzed: 04/03/17 Dibenzo(a,h)anthracene 44.9 10 ug/L 50.00 90 51-134 Dibenzofuran 41.6 10 ug/L 50,00 83 53-118 Diethyl phthalate 42.6 10 ug/L 50.00 85 56-125 Dimethyl phthalate 42.7 10 ug/L 50.00 85 45-127 Di-n-butyl phthalate 43.1 10 ug/L 50.00 86 59-127 Di-n-octyl phthalate 46.2 10 ug/L 50.00 92 51-140 Fluoranthene 44.6 10 ug/L 50.00 89 57-128 Fluorene 42.6 10 ug/L 50.00 85 52-124 Hexachiorobenzene 43.5 10 ug1L 50.00 87 53-125 Hexachlorobutadiene 24.6 10 uglL 50.00 49 22-124 Hexachlorocyclopentadiene 9.72 10 ug1L 50.00 19 32-117 L, J Hexachloroethane 23.3 10 ug1L 50.00 47 21-115 lndeno(1,2,3-0d)pyrene 44.4 10 uglL 50.00 89 52-134 Isophorone 37.8 10 ug/L 50.00 76 42-124 Naphthalene 31.4 10 ug/L 50.00 63 40-121 Nitrobenzene 33.4 10 ug/L 50.00 67 45-121 N-Nitroso-di-n-propylamine 37.6 10 ug/L 50.00 75 49-119 N-Nitrosodiphenylamine 54.0 10 ug/L 50.00 108 51-123 Pentachlorophenol 59.1 10 ug/L 50.00 118 35-138 Phenanthrene 45.6 10 ug/L 50.00 91 59-120 Phenol 18.6 10 ug/L 50.00 37 12-58 Pyrene 47.2 10 ug/L 50.00 94 57-126 Surrogate:2,4,8-Tribromophenot 86.4 ug/L 100.0 66 43-140 Surrogate:2-F/uorobiphenyl 38.0 ug/L 50.00 76 44-119 Surrogate:2-Fluorophenol 46.1 ug/L 100.0 46 19-119 Surrogate: Nitrobenzene-d5 32.8 ug/L 50.00 66 44-120 Surrogate: Phenol-d5 32.0 ug/L 100.0 32 11-52 Surrogate: Terphenyl-04 52.5 ug/L 50.00 105 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364-Toll Free Number: l-8001629-6364- Fax: 7041626-0409 Page 16 of 19 ��r Ir �w PR S M ! nvService Environmental Solutions Level 11 QC Report 4/5/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7D0004 - 3610C MS Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source Result Limit Units Level Result %REC %REC RPD Limits RPD Limit Notes LCS Dup (P7D0004-BSD1) _ Prepared &Analyzed: 04/03/17 1,2,4-Trichlorobenzene 23.7 10 ug/L 50.00 47 29-126 12 20 1,2-Dichlorobenzene 24.6 10 ug/L 50.00 49 32-111 9 20 1,3-Dichlorobenzene 22.7 10 ug/L 50.00 45 28-110 7 20 1,4-Dichlorobenzene 23.2 10 ug/L 50.00 46 29-112 8 20 1-Methylnaphthatene 31.0 10 uglL 50.00 62 41-119 12 20 2,4,5-Tdchlorophenol 38.2 10 ug/L 50.00 76 53-123 10 20 2,4,6-Trichlorophenol 39.5 10 ug/L 60.00 79 5D-125 9 2D 2,4-Dichlorophenol 31.9 10 ug/L 50.00 64 47-121 12 20 2,4-Dimethylphenol 39.5 10 ug/L 50.00 79 31-124 11 20 2,4-Dinitrophenol 60.0 10 ug/L 50,00 100 23-143 12 20 2,4-Dinitrotoluene 42.0 10 ug/L 50.00 84 57-128 8 20 2,6-Dinitrotoluene 42A 10 ug/L 50.00 84 57-124 10 20 2-Chloronaphthalene 33.7 10 ug/L 50.00 67 40-116 10 20 2-Chlorophenol 32.9 10 ug/L 60.00 66 38-117 11 20 2-Methylnaphthalene 29.3 10 ug/L 50.00 59 40-121 12 20 2-Methylphenol 32.4 10 ug/L 50.00 65 30-117 13 20 2-Nitroaniline 35.9 10 ug/L 50.00 72 55-127 9 20 2-Nitrophenol 31.3 10 ug/L 50.00 63 47-123 14 20 3,3'-Dichlorobenzidine 44.5 10 ug/L 50.00 89 27-129 9 20 3/4-Methylphenol 26.7 10 ug/L 50.00 53 29-110 14 20 3-Nitroaniline 36.8 10 ug/L 50.00 74 41-128 9 20 4,6-Dinitro-2-methylphenol 43.6 10 ug/L 50.00 87 44-137 11 20 4-Bromophenyl phenyl ether 38.2 10 ug/L 50.00 76 55-124 1D 20 4-Chloro-3-methylphenol 36.1 10 ug/L 50.00 72 52-119 9 20 4-Chloroaniline 29.8 10 ug/L 50.00 60 33-117 14 20 4-Chlorophenyl phenyl ether 37.0 10 ug/L 50.00 74 53-121 6 20 4-Nitroaniline 36.6 10 ug/L 50.00 73 45-135 6 20 4-Nitrophenol 18.2 10 ug/L 50,00 36 1D-77 10 20 Acenaphthene 38.5 10 ug/L 50.00 77 47-122 11 20 Acenaphthylene 36.2 10 ug/L 50.00 72 41-130 10 20 Aniline 30.1 10 ug/L 50.00 76 12-197 16 20 Anthracene 42.0 10 ug/L 50.00 84 57-123 8 20 Azobenzene 40.7 10 ug/L 50.00 81 61-116 12 20 Benzo(a)anthracene 43.9 10 ug/L 50.00 88 58-125 9 20 Benzo(a)pyrene 41.2 10 ug/L 50.00 82 54-128 9 20 Benzo(b)fluoranthene 41.4 10 ug/L 50.00 83 53-131 13 20 Benzo(g,h,i)perylene 37.5 10 ug/L 50.00 75 50-134 10 20 Benzo(k)fluoranthene 41.6 10 ug/L 60.00 83 57-129 5 20 Benzoic Acid 8.92 100 ug/L 50.00 18 10-125 51 20 D, J Benzyl alcohol 30.8 10 ug/L 50.00 62 31-112 12 20 bis(2-Chloroethoxy)methane 31.6 10 ug/L 50.00 63 48-120 12 20 Bis(2-Chloroethypether 3D.5 10 ug/L 50.00 61 43-118 9 20 Bis(2-chloroisopropyl)ether 31.1 10 ug/L 50.00 62 37-130 11 20 Bis(2-Ethylhexyl)phthalate 44.0 10 ug/L 50.00 88 55-135 10 20 Butyl benzyl phthalate 44.7 10 ug/L 50.00 89 53-134 7 20 Chrysene 45.6 10 ug/L 50.00 91 59-123 7 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 _ Phone: 7041629.6364-Toll Free Number. t-8001629-6364- Fax: 7041626-0409 Page 17 of 19 -YY��YYYY�� Full -Service Analytical Environmental Solutionsa /��P;�:� .... i I cna`oarcc KC. Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7D0004 - 3510C MS Level II QC Report 415117 Prism Work Order: 7040018 Time Submitted: 4/3/2017 3:24:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS Dup (P7D0004-BSD1) Prepared &Analyzed: 04/03/17 Dibenzo(a,h)anthracene 40.6 10 ug/L 50.00 81 51-134 10 20 Dibenzofuran 38.5 10 ug/L 50.00 77 53-118 8 20 Diethyl phthalate 39.5 10 ug/L 50.00 79 56-125 7 20 Dimethyl phthalate 38.6 10 ug/L 50.00 77 45-127 10 20 Di-n-butyl phthalate 39.4 10 ug/L 50.00 79 59-127 9 20 Di-n-octyl phthalate 42.3 10 ug/L 50.00 85 51-140 9 20 Fluoranthene 4D.6 10 ug/L 50.00 81 57-128 9 20 Fluorene $9.1 10 ug/L 50.00 78 52-124 8 20 Hexachlorobenzene 40.9 10 ug/L 50.00 82 53-125 6 20 Hexachlorobutadiene 22.5 10 ug/L 50.00 45 22-124 9 20 Hexachlorocyclopentediene 8.84 10 ug/L 50.00 18 32-117 9 20 L, J Hexachioroethane 21.6 10 ug/L 50.00 43 21-115 8 20 Indeno(1,2,3-ed)pyrene 41.5 10 ug/L 50.00 83 52-134 7 20 Isophorone 33.6 10 ug/L 50.00 67 42-124 12 20 Naphthalene 27.9 10 ug/L 50.00 56 40-121 12 20 Nitrobenzene 3D.1 10 ug/L 50.00 60 45-121 10 20 N-Nitroso-di-n-propylamine 34.0 10 ug/L 50.00 66 49-119 10 20 N-Nitrosodiphenylemine 48.2 10 ug/L 50.00 96 51-123 11 20 Pentachlorophenol 53.2 10 ug/L 50.00 106 35-138 11 20 Phenanthrene 41.8 10 ug/L 50.00 84 59-120 9 20 Phenol 16.1 10 ug/L 50.00 32 12-68 14 20 Pyrene 43.5 10 ug/L 50.00 87 57-126 8 20 Surrogate:2,4,6-Tribromophenol 77.1 uglL 100.0 77 43-140 Surrogate:2-Fluorobiphenyl 34.0 u91L 50.00 68 44-119 Surrogate: 2-Fluorophenol 40.6 ug/L 100.0 41 19-119 Surrogate: Nitrobenzene-d5 29.4 ug/L 50.00 59 44.120 Surrogate: Phenol-d5 27A ug/L 100.0 27 11-52 Surrogate: Terphenyt-04 48.1 uglL 50.00 96 50-134 Sample Extraction Data Prep Method: 3610C MS Lab Number Batch initial Final Datemme 7040010-01 P7D0004 1000 mL 1 mL 04/04/17 9:40 Prep Method: 6030B Lab Number Batch Initial Final Daterrime 7040018-01 P700037 10 mL 10 mL 04/04/17 9:49 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1.800/629.6364 - Fax: 7041626-0409 Page 18 of 19 iPR! Full -Service AnS0l1Al i { Environ�nentnt! Satly,utions �� �aoor�m'ertr , ulc. 40 Sprtnahrook Road • Charlotte, NC 2821 T Phone 7641529•k364 • Fax: 7041525-0409 Client Company Name: Report To/Contact Name: Reporting Address:,.- -�— CHAIN OF CUSTODY RECORD PAGE OF:_ QUOTE S TO ENSURE PROPER BILLING:. Project Name: Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) *Please ATTACH any p `t specific reporting (QC LEVEL 111111 IV) provisions and/or QC Requirements 1 Invoice To: -- Address: 1 -ke NO NIA. i" Phone"(;, Fax (Yes) urchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Address: �� ��s*���= C? t v' � £ � Pt R q ested Due Date J. Tl)ay D 2 Days ❑ 3 Days D 4 Days D 5 Pays Certification• NELAC DOD FL NC EDD Type: POF ',gr l�'CDiher 'Working Days" D 6-9 Days D Standard 10 days.4.08h Work M_Approved st Be SC OTiiER N/A Site Location Name:Samples received after 14:00 ndtl be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO, Site Location Physical Address: (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES_�-NO_ RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) I TIME MATRIX SAMPLE CONTAINER ANALYSIS REQUESTED PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA•j REMARKS LAB SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES N jJ ID NO. HOURS SLUDGE) SEE BELOWob �_.... . ..' I. (tt%'t`k AlboL i Sampler's Signature t ik ` Sampled By (Print Name) j Affiliation Upon relinquishing, this Chain of Custody is ya- authorization for Prism to proceed with the analyses as requ .- ed above. Any changes must be !PRISM ONLY submitted In writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. e!n igneture) Received By: (Signature) Date MilitarytHours Additional Comments: Sfte Amval TimB: t nquiffed By. (Signature) Received By. (Si Lure) Data -Site Depatiuro Tiine:. . - Field Tscli Fee: quished y: (Signature) Rpmved For Prisr Laboratories By. �...--^•.t cDe ' � 1 1•t � i, _ f. Jf ( 7,c+� tUtllpage: .,. hod af Shipment: : ALL SAMPLE COOLERS SHOULD BE TAPED WITH D EALS FOR TRANSPO ATION O ORATOR r Group o. ---�� - SA ARE NOT ACCEPTED AND VERIFIED AGAINST COC N RECEIVED AT THE LABORA RY. ) �111 �u � ) fD 0Ex 0 UPS O Prism Field Servba O Other o DES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCCERCLA LANDFILL OTHER: its mem jj , C❑SC) ❑SC ❑❑NC ❑SC ❑SC D❑NC ❑SC ( ❑❑NC ❑SC`❑❑NC ❑SC 0NC OSC ANC DNC 0NC❑SC� jj NTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) Case Narrative M � : ISM w ,11- ____'�,�.&,,:^� LARORATORiES, lNC Full -Service Analytical & Environmental Solutions Anchor QEA of North Carolina, PLLC Mike Falknor 231 Haywood Street Asheville, NC 28801 NC Certification No, 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Charlotte Metro Lab Submittal Date: 03/31/2017 Prism Work Order: 7030490 04/04/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. IL�_ (0:: �� V L. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: Reviewed By Robbi A. Jones President/Project Manager D RPD value outside of the control limits. J Detected but below the Reporting Limit, therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springibrook Road - P.O. Sox 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-0409 Page 1 of 23 �. i I Full•Service Analytical & Environmental Solutions �rJlt" > ` ueoH«cn en �wc Sample Receipt Summary 04/04/2017 Prism Work Order: 7030490 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received MW-2 7030490-01 Water 03/31/17 03/31/17 MW-3 7030490-02 Water 03/31/17 03/31/17 Samples were received in good condition at 5.2 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Chartotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001629-6364 • Fax: 7041626-0409 Page 2 7172771 1111,,,,� al Sol Analytical 8 ' \(I Environmental Solutions P R I V� n I Environmental - jy "IABORATORIE$IW, Summary of Detections 04/04/2017 Prism Work Order: 7030490 Prism ID Client ID Parameter Method Result Units 7030490-01 MW-2 1-Methylnaphthalene 8270D 9.2 J ug/L 7030490-01 MW-2 2-Methylnaphthalene 8270D 7.2 J ug/L 7030490-01 MW-2 Bis(2-Ethylhexyl)phthalate 8270D 28 ug/L 7030490-01 MW 2 Naphthalene 8270D 8,2 J ug/L 7030490-01 MW-2 Acetone 8260E 11 ug/L 7030490-01 MW-2 Benzene 8260E 1.6 ug/L 7030490-01 MW-2 Chloroform 8260E 1.5 ug/L 7030490-01 MW-2 Isopropylbenzene (Cumene) 8260E 0.61 ug/L 7030490-01 MW-2 Naphthalene 82606 17 ug/L 7030490-01 MW-2 sec-Butylbenzene 8260E 1.2 ug/L 7030490-02 MW-3 Bromodichloromethane 8260B 1.1 ug/L 7030490-02 MW-3 Chloroform 8260B 4.3 ug1L 7030490-02 MW-3 Dibromochloromethane 8260E 0.64 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529.6364-Toll Free Number, 1-8001629-6364- Fax: 7041526-M9 Page 3 tZf 23 i�� II III I I �•S I Laboratory Report Futl-Service Analytical 8 Environmental Solutions 04l04/2017 G�bNs `-"' I.ABGRATORIEi ING Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW 2 Attn: Mike Falknor Prism Sample ID: 7030490-01 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 12:15 Time Submitted: 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefrime ID Semivolatile Organic Compounds by GClMS 1,2,4-Trichlorobenzene BRL ug/L 11 2.0 1 8270D 413117 17:04 JMV P7DOD04 1,2-Dichlorobenzene BRL ug/L 11 1.9 1 8270D 4/3/17 17:04 JMV P7130004 1,3-Dichlorobenzene BRL ug1L 11 2.1 1 8270D 4/3117 17:04 JMV P7DOD04 1,4-Dichlorobenzene BRL ug/L 11 1.9 1 8270D 413117 17:04 JMV P7DO004 1-Methyinaphthalene 9.2 J ug/L 11 3.0 1 9270D 413117 17:04 JMV P7DO004 2,4,5-Trichlorophenol BRL ug/L 11 1.8 1 8270D 4/3/17 17:04 JMV P700004 2,4,6-Trichlorophenol BRL ug/L 11 2.1 1 8270D 4/3/17 17:04 JMV P7DO004 2,4-Dichlorophenol BRL ug/L 11 2.9 1 8270D 413/17 17:04 JMV P700Do4 2,4-Dimethylphenol BRL ug/L 11 3.9 1 8270D 4/3/17 17:04 JMV P7130004 2,4-Dinitrophenol BRL ug/L 11 3.1 1 8270D 413/17 17:04 JMV P71)0004 2,4-Dinitrotoluene BRL ug/L 11 1.6 1 8270D 4/3117 17:04 JMV P7DOD04 2,6-Dinitrotoluene BRL ug/L 11 1.3 1 8270D 4/3/17 17:04 JMV P700004 2-Chloronaphthalene BRL ug/L 11 3.1 1 8270D 4/3/17 17:04 JMV P7130004 2-Chlorophenol BRL ug1L 11 2.1 1 8270D 413117 17:04 JMV P7DO004 2-Methyinaphthalene 7.2 J ug/L 11 2.7 1 8270D 413117 17:04 JMV P7DO004 2-Methylphenol BRL ug1L 11 2A 1 8270D 413/17 17:04 JMV P700004 2-Nitroaniline BRL ug/L 11 1.6 1 8270D 4/3117 17:04 JMV P7DO004 2-Nitraphenol BRL ug/L 11 2.7 1 8270D 413/17 17:04 JMV P7DO004 3,3'-Dichlorobenzidine BRL ug/L 11 1.6 1 8270D 413/17 17:04 JMV P71)0004 3)4-Methylphenol BRL ug1L 11 1.8 1 8270D 413117 17:04 JMV P7DO004 3-Nitroaniline BRL ug1L 11 1.6 1 8270D 413/17 17:04 JMV P71)0004 4,6-Dinftro-2-methylphenol BRL ug/L 11 1.6 1 8270D 4/3/17 17:04 JMV P7DO004 4-Bromophenyl phenyl ether BRL ug/L 11 1.5 1 8270D 4/3/17 17:04 JMV P7DO004 4-Chloro-3-methylphenol BRL ug1L 11 2.7 1 8270D 4/3117 17:04 JMV P7DO004 4-Chioroaniline BRL ug/L 11 2.8 1 8270D 4/3/17 17:04 JMV P71)0004 4-Chiorophenyl phenyl ether BRL ug/L 11 1.5 1 8270D 413/17 17:04 JMV P7130004 4-Nitroaniline BRL ug/L 11 1.1 1 8270D 4/3/17 17:04 JMV P7DO004 4-Nitrophenol BRL ug/L 11 0.68 1 8270D 4/3/17 17:04 JMV P7DO004 Acenaphthene BRL ug/L 11 2.1 1 8270D 4/3/17 17:04 JMV P71)0004 Acenaphthylene BRL ug/L 11 2.3 1 8270D 413/17 17:04 JMV P71)0004 Aniline BRL ug/L 11 2.7 1 8270D 413/17 17:04 JMV P7D0004 Anthracene BRL ug1L 11 1.6 1 8270D 4/3/17 17:04 JMV P7DO004 Azobenzene BRL ug/L 11 2.0 1 8270D 413117 17,04 JMV P71)0004 Benzo(a)anthracene BRL ug/L 11 1.6 1 8270D 413117 17:04 JMV P7DD004 Benzo(a)pyrene BRL ug/L 11 1.6 1 8270D 413117 17:04 JMV P7130004 Benzo(b)fiuoranthene BRL ug/L 11 1.3 1 8270D 4/3/17 17:04 JMV P71)0004 Benzo(g,h,i)perylene BRL ug/L 11 1.6 1 8270D 413/17 17.04 JMV P71)0004 Benzo(k)tiuoranthene BRL ug/L 11 1.6 1 8270D 4/3/17 17:04 JMV P71)0004 Benzoic Acid BRL ug/L 110 5.3 1 8270D 4/3/17 17:04 JMV P71)0004 Benzyl alcohol BRL ug/L 11 2.4 1 8270D 413/17 17.04 JMV P7DO004 bis(2-Chloroethoxy)methane BRL ug/L 11 2.9 1 8270D 4/3/17 17:04 JMV P7DO004 Bis(2-Chloroethyl)ether BRL ug/L 11 2.6 1 8270D 413/17 17:04 JMV P7DD004 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 -Toll Free Number:1-8001629.6364 - Fax: 704/526-0409 Page 4 of 23 x P S M Laboratory Report Full -Service Analytical & Environmental Solutions 04/04/2017 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-2 Attn: Mike Falknor Prism Sample ID: 7030490-01 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 12:15 Time Submitted: 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateTme ID Bis(2-chloroisopropyl)ether BRL ug/L 11 2.2 1 8270D 4/3/17 17:04 JMV P7DO004 Bis(2-Ethyihexygphthalate 28 ug/L 11 1.6 1 8270D 413/17 17:04 JMV P7DO004 Butyl benzyl phthalate BRL ug/L 11 1.5 1 8270D 4/3/17 17:D4 JMV P7DOD04 Chrysene BRL ug/L 11 1.6 1 8270D 4/3/17 17:04 JMV P71)0004 Dibenzo(a,h)anthracene BRL ug/L 11 1.4 1 8270D 413/17 17:04 JMV P7DOD04 Dibenzofuran BRL ug/L 11 2.0 1 8270D 4/3/17 17:04 JMV P7DO004 Diethyl phthalate BRL ug/L 11 3.8 1 827DD 4/3/17 17:04 JMV P7D0004 Dimethyi phthalate BRL ug/L 11 1.6 1 82701) 4/3/17 17:04 JMV P7DO004 Di-n-butyl phthalate BRL ug/L 11 1.9 1 8270D 413117 17:04 JMV P7DO004 Di-n-octyl phthalate BRL ug/L 11 1.5 1 8270D 413117 17:04 JMV P7130004 Fluoranthene BRL ug/L 11 1.9 1 8270D 413/17 17:04 JMV P71)0004 Fluorene BRL ug/L 11 1.9 1 8270D 4/3/17 17:04 JMV P7DO004 Hexachlorobenzene BRL ug/L 11 1.5 1 8270D 413/17 17:04 JMV P71)0004 Hexachlorobuladlene BRL ug/L 11 2.4 1 8270D 413/17 17:04 JMV P7D0004 Hexachiorocyclopentadiene BRL ug/L 11 2.0 1 8270D 4/3117 17:04 JMV P7DO004 Hexachloroethane BRL ug/L 11 2.0 1 8270D 4/3/17 17:04 JMV P7DO004 Indeno(1,2,3-cd)pyrene BRL ug/L 11 4A 1 8270D 4/3/17 17:04 JMV P700004 Isophorone BRL ug/L 11 2.9 1 8270D 413117 17:04 JMV P700004 Naphthalene 8.2 J ug/L 11 2.9 1 8270D 4/3/17 17:04 JMV P7DO004 Nitrobenzene BRL ug/L 11 2.9 1 8270D 4/3/17 17:04 JMV P7130004 N-Nitroso-di-n-propylamine BRL uglL 11 2.5 1 8270D 4/3/17 17:04 JMV 137Do004 N-Nitrosodiphenylamine BRL ug/L 11 1.5 1 8270D 4/3117 17:04 JMV P70DO04 Pentachlorophenol BRL ug/L 11 1.4 1 8270D 413/17 17:04 JMV P7DD004 Phenanthrene BRL ug/L 11 1.7 1 8270D 4/3/17 17:04 JMV P7D0004 Phenol BRL ug/L 11 1.1 1 8270D 4/3/17 17:04 JMV P7DO004 Pyrene BRL ug/L 11 1.6 1 8270D 4/3/17 17:04 JMV P7DO004 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 55 % 43-140 2-Fluorobiphenyl 54 % 44-119 2-Fluorophenol 33 % 19-119 Nitrobenzene-d5 49 % 44-120 Phenol-d5 25 % 11-52 Terphenyl-d14 63 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachioroethane BRL ug/L 0.50 0.11 1 8260B 413117 13:03 KDM P7DO017 1,1,1-Trichioroethane BRL ug/L 0.50 0.061 1 8260B 4/3117 13:03 KDM P7DO017 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 4/3/17 13:03 KDM P71)0017 1,1,2-Trichioroethane BRL ug/L 0.50 0.066 1 8260B 4/3117 13:03 KDM 137DO017 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 4/3/17 13:03 KDM P7DO017 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 413117 13:03 KDM P7DO017 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 82608 4/3117 13:03 KDM P7DO017 1,2,3-Trichlorobenzene BRL ug/L 2.0 0,40 1 8260B 413117 13:03 KDM P7DO017 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 4/3117 13:03 KDM P7DO017 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041626-0409 page 5 Df 23 .�� PR I S M f Laboratory Report Full -Service Analytical & Environmental Solutions 04/04/2017 1A90AATGR'Ell WC - Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-2 Attn: Mike Falknor Prism Sample ID: 7030490-01 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 12:15 Time Submitted: 03/31/17 15:20 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 4/3/17 13:03 KOM P7D0017 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 8260B 4/3/17 13:03 KDM P7D0017 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 4/3/17 13:03 KDM P7D0017 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 4/3/17 13:03 KDM P700017 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 4/3/17 13:03 KDM P71)0017 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 4/3/17 13:03 KDM P7D0017 1,2-Dichloropropane BRL ug/L 0.60 0.11 1 8260B 4/3/17 13:03 KDM P7130017 1,3,5-Trimethyibenzene BRL ug/L 0.50 0.076 1 8260B 413117 13:03 KDM P7130017 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 4/3117 13:03 KDM P7130017 1,3-Dichloropropane BRL ug/L 0.50 0,043 1 8260B 4/3117 13:03 KDM P7130017 1,4-Dichlorobenzene BRL ug/L 0,50 0.050 1 8260B 4/3/17 13:03 KDM PTDD017 2,2-Dichloropropane BRL ug/L 2.0 0A1 1 8260B 4/3/17 13:03 KOM P7D0017 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 4/3/17 13:03 KDM P7D0017 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 4/3117 13:03 KDM P7D0017 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 4/3/17 13:03 KDM P7D0017 Acetone 11 ug1L 6.0 0.31 1 826013 413/17 13:03 KDM P7D0017 Acrolein BRL ug/L 20 0,20 1 8260B 4/3/17 13:03 KDM P71)0017 Acrylonitrile BRL ug/L 20 0.20 1 8260B 4/3117 13:03 KDM P7D0017 Benzene 1.s ug/L 0.60 0.048 1 8260B 413/17 13:03 KDM P7D0017 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 413/17 13:03 KDM P700017 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 4/3117 13:03 KOM P7D0017 Bromodichloromethane BRL ug/L 0.50 0,062 1 8260B 4/3117 13:03 KDM P71)0017 Bromoform BRL ug/L 1.0 0.040 1 82608 413117 13:03 KDM P7D0017 Bromomethane BRL ug/L 1.0 0.18 1 8260B 4/3117 13:03 KDM P7D0017 Carbon disulfide BRL ug/L 5.0 0.075 1 82605 413/17 13:03 KDM P7D0017 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 4/3/17 13:03 KDM P700017 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 413/17 13:03 KDM 137130017 Chloroethane BRL ug/L 0.50 0.22 1 8260B 4/3117 13:03 KDM P700017 Chloroform 1.6 ug/L 0.60 0.076 1 8260B 413117 13:03 KOM P700017 Chloromethane BRL ug/L 0.50 0.079 1 82608 413117 13:03 KDM P7D0017 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 4/3117 13:03 KDM P700017 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 4/3117 13:03 KDM P700017 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 4/3/17 13:03 KDM P700017 Dibromomethane BRL ug/L 0.50 0.065 1 82608 4/3117 13:03 KDM P70oD17 Dichbrodifluoromethane BRL ug/L 1.0 0.11 1 8260B 413/17 13:03 KDM 137D0017 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 4/3/17 13:03 KDM P7D0017 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 82608 4/3/17 13:03 KDM P7DOD17 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 4/3/17 13:03 KDM P7D0017 lsopropylbenzene (Cumene) 0.61 ug/L 0.60 0.064 1 8260E 4/3/17 13:03 KDM P700017 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 4/3117 13:03 KDM P71)0017 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 82608 4/3117 13:03 KDM P7D0017 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 413/17 13:03 KDM P7D0017 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 4/3/17 13:03 KOM P7D0017 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/626-0409 Page 6 of 23 Laboratory Report � %� f FullService Analytical a • ISv � I Environmental Solutions 04i0412017 .! �u1-.r.....,._ LhuufUTUHtES IHC. Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-2 Attn: Mike Falknor Prism Sample ID: 7030490-01 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 12:15 Time Submitted: 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 4/3/17 13:03 KDM 137D0017 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 4/3/17 13:03 KDM P700017 Naphthalene 17 ugfL 1.0 0.19 1 8260B 413/17 13:03 KDM P7D0017 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260D 413/17 13:03 KDM P7D0017 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 413/17 13:03 KDM P7D0017 o-Xylene BRL ug/L 0.50 0.044 1 8260B 413/17 13:03 KDM P7D0017 sec-Butylbenzene 1.2 ug/L 0.60 0.076 1 6260B 4/311713:03 KDM P7130017 Styrene BRL ug/L 0.50 0.047 1 8260B 4/3/17 13:03 KDM P7D0017 tert-Butylbenzene BRL ug/L 0.50 0,088 1 8260B 4/3/17 13:03 KDM P700017 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 4/3/17 13:03 KDM P7DOD17 Toluene BRL ug/L 0.50 0.044 1 8260B 4/3117 13:03 KDM P7D0017 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 4/3/17 13:03 KDM P7D0017 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 4/3/17 13:03 KDM 137D0017 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 4/3/17 13:03 KDM P700017 Trichlorofluoromethane BRL ug/L 0.50 0,062 1 8260B 4/3/17 13:03 KDM P7D0017 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 413/17 13:03 KDM P7DO017 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 413117 13:03 KDM P7D0017 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 88 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Tog Free Number: 1.300/629-6364 - Fax: 7041626-0409 Page 7 of 33� ORISM F A"A' ``{I F.Laboratory Report y.� Environmert.1 SOIuuonz 04/0412017 -:.`ram?'-`,.s,'"-G'-b'✓•;`: �nuow.i o�„F, �Nc Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-3 Attn: Mike Falknor Prism Sample ID: 7030490-02 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 13:10 Time Submitted: 03/31/17 15,20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateMme ID Semivotatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 1.8 1 8270D 4/3/17 1726 JMV P7D0004 1,2-Dichlorobenzene BRL ug/L 10 1.7 1 8270D 4/3/17 17:26 JMV P71)0004 1,3-Dichlorobenzene BRL ug/L 10 2.0 1 8270D 4/3117 17:26 JMV P7D0004 1,4-Dichlorobenzene BRL ug/L 10 1.7 1 8270D 4/3/17 17:26 JMV P7D0004 1-Methylnaphthalene BRL ug/L 10 2.7 1 8270D 4/3/17 17:26 JMV P7D0004 2,4,5-Trichlorophenol BRL ug/L 10 1.7 1 8270D 4/3/17 17:26 JMV P7D0004 2,4,6-Trichlorophenol BRL ug/L 10 1.9 1 8270D 4/3/17 17:26 JMV P71)0004 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270D 4/3/17 1726 JMV P7D0004 2,4-Dimethylphenol BRL ug/L 10 3.6 1 8270D 4/3/17 17:26 JMV P7D0004 2,4-Dinitrophenol BRL ug/L 10 2.8 1 8270D 4/3/17 17:26 JMV P71)0004 2,4-Dinitrotoluene BRL ug/L 10 1.5 1 8270D 413/17 17:26 JMV P7130004 2,6-Dinitrotoluene BRL ug/L 10 1.2 1 8270D 4/3/17 17:26 JMV P7D0004 2-Chloronaphthalene BRL ug/L 10 2.8 1 8270D 4/3117 1726 JMV P7D0004 2-Chlorophenol BRL ug/L 10 2.0 1 8270D 4/3/17 17:26 JMV P7130004 2-Methylnaphthalene BRL ug/L 10 2.5 1 8270D 413/17 17:26 JMV P7D0004 2-Methylphenol BRL ug/L 10 19 1 8270D 4/3117 17:26 JMV P7130004 2-Nitroaniline BRL ug/L 10 1.5 1 8270D 4/3/17 17:26 JMV P7D0004 2-Nitrophenol BRL ug/L 10 2.5 1 8270D 4/3/17 17:26 JMV P7D0004 3,3'-Dichlorobenzidine BRL ugll 10 1.5 1 8270D 4/3/17 17:26 JMV P7D0004 3/4-Methylphenol BRL ug/L 10 1.6 1 827DD 4/3117 17:26 JMV P7D0004 3-Nitroaniline BRL ug/L 10 1.4 1 8270D 4/3/17 17:26 JMV P7130004 4,6-Dinitro-2-methylphenol BRL ug/L 10 1.4 1 8270D 413/17 17:26 JMV P7D0004 4-Bromophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 4/3/17 17:26 JMV P7D0004 4-Chloro-3-methylphenol BRL ug/L 10 2.5 1 8270D 4/3117 17:26 JMV P7DD004 4-Chloroaniline BRL ug/L 10 2.6 1 8270D 4/3/17 17:26 JMV P7D0004 4-Chlorophenyl phenyl ether BRL ug/L 10 1.4 1 8270D 4/3/17 1726 JMV P7D0004 4-Nitroaniline BRL ug/L 10 0.97 1 8270D 4/3/17 1726 JMV P7D0004 4-Nitrophenol BRL ug/L 10 0.62 1 8270D 4/3/17 17:26 JMV P7D0004 Acenaphthene BRL ug/L 10 1.9 1 8270D 413117 1726 JMV P7D0004 Acenaphthylene BRL ug/L 10 2.1 1 8270D 4/3117 17:26 JMV P71)0004 Aniline BRL ug/L 10 2.5 1 8270D 4/3/17 17:26 JMV P7130004 Anthracene BRL ug/L 10 1.5 1 8270D 4/3/17 17:26 JMV P7D0004 Azobenzene BRL ug/L 10 1.9 1 8270D 4/3117 1726 JMV P7D0004 Benzo(a)anthrace ne BRL ug/L 10 1.5 1 8270D 413117 17:26 JMV P7D0004 Benzo(a)pyrene BRL ug/L 10 1.5 1 6270D 4/3117 17:26 JMV P7D0004 Benzo(b)fluoranthene BRL ug/L 10 1.2 1 8270D 4/3/17 17:26 JMV P7DOOD4 Benzo(g,h,i)perylene BRL ug/L 10 1.4 1 8270D 4/3/17 17:26 JMV P7D0004 Benzo(k)fluoranthene BRL ug/L 10 1.5 1 8270D 4/3/17 17:26 JMV P7D0004 Benzoic Acid BRL ug/L 100 4,9 1 8270D 4/3/17 17:26 JMV P7D0004 Benzyl alcohol BRL ug/L 10 2.2 1 8270D 4/3117 17:26 JMV P7D0004 bis(2-Chicroethoxy)methane BRL ug/L 10 2.7 1 8270D 4/3/17 17:26 JMV P7D0004 Bis(2-Chloroethyl)ether BRL ug/L 10 2.4 1 8270D 413/17 17:26 JMV P7D0004 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/62"409 Page 8 of 23 PRISM ` Fun -Service Analytical Environmental Solutions Laboratory Report 04/04/2017 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID. MW-3 Attn: Mike Falknor Prism Sample ID: 7030490-02 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix Water Time Collected, 03/31/17 13:10 Time Submitted 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bis(2-chloroisopropyl)ether BRL ug/L Bis(2-Ethylhexyl)phthalate BRL ug/L Butyl benzyl phthalate BRL ug/L Chrysene BRL ug/L Dibenzo(a,h)anthracene BRL ug/L Dibenzofuran BRL ug/L Diethyl phthalate BRL ug/L Dimethyl phthalate BRL ug/L Di-n-butyl phthalate BRL ug/L Di-n-octyl phthalate BRL ug/L Fluoranthene BRL ug/L Fluorene BRL ug/L Hexachlorobenzene BRL ug/L Hexachlorobutadiene BRL ug/L Hexachlorocyclopentadiene BRL ug/L Herachloroethane BRL ug/L Indeno(1,2,3-cd)pyrene BRL ug/L Isophorone BRL ug/L Naphthalene BRL uglL Nitrobenzene BRL ug/L N-Nitroso-di-n-propylemine BRL ug/L N-Nitrosodiphenylamine BRL ug/L Pentachlorophenol BRL ug/L Phenanthrene BRL ug/L Phenol BRL ug/L Pyrene BRL ug/L Volatile Organic Compounds by GC/MS 10 2.1 1 8270D 4/3117 17:26 JMV P7D0004 10 1.4 1 8270D 4/3/17 17:26 JMV P7D0004 10 1.4 1 8270D 4/3/17 17:26 JMV P71)0004 10 1.5 1 8270D 4/3117 17:26 JMV P7D0004 10 1.2 1 8270D 4/3117 1726 JMV P7D0004 10 1.8 1 82700 4/3/17 17:26 JMV P7D0004 10 3.5 1 8270D 4/3/17 17:26 JMV P7D0004 10 1.5 1 8270D 4/3117 17:26 JMV P7D0004 10 1.8 1 8270D 4/3/17 17.26 JMV P7D0004 10 1.4 1 8270D 4/3/17 17:26 JMV P71)0004 10 1.8 1 8270D 4/3/17 17:26 JMV P71)0004 10 1.8 1 8270D 4/3/17 17:26 JMV P7DOD04 10 1.3 1 8270D 413117 17:26 JMV P7D0004 10 2.2 1 8270D 4/3/17 17:26 JMV P71)0004 10 1.8 1 8270D 413/17 17:26 JMV P7D0004 10 1.8 1 8270D 413/17 17.26 JMV P7D0004 10 4.1 1 8270D 4/3/17 17:26 JMV P7D0004 10 2.6 1 8270D 4/3/17 17:26 JMV P7D0004 10 2.7 1 8270D 4/3/17 17:26 JMV P7D0004 10 2.7 1 8270D 4/3/17 17:26 JMV P7D0004 10 2.3 1 827DD 413/17 17:26 JMV P7D0004 10 1.4 1 8270D 4/3117 17:26 JMV P7D0004 10 13 1 8270D 413/17 17:26 JMV P7D0004 10 1.5 1 8270D 413117 17.26 JMV P7D0004 10 1.0 1 8270D 413117 17:26 JMV P7D0004 10 1.5 1 8270D 4/3/17 17:26 JMV P7D0004 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 86 % 43-140 2-Fluorobiphenyl 73 % 44-119 2-Fluorophenol 48 % 19-119 Nitrobenzene-d5 66 % 44-120 Phenokd5 32 % 11-52 Terphenyb04 103 % 50-134 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 82608 413/17 1337 KDM P7D0017 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 413117 13.37 KDM P7D0017 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 413/17 13:37 KDM P7D0017 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 4/3/17 13:37 KDM P7D0017 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 82606 413117 13:37 KDM P7D0017 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 4/3/17 13:37 KDM P7D0017 1,1-Dichloropropylene BRL ug/L 0,50 0.051 1 8260B 4/3117 13:37 KDM P7D0017 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 413/17 13:37 KDM P7130017 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 6260B 413/17 13:37 KDM P7D0017 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1.8001629-6364 - Fax: 7041625-0409 Page 9 of 23� :PRISM Laboratory Report Environmental al Solutions s 04/04/2017 Environments( Solutions Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-3 Attn Mike Falknor Prism Sample ID: 7030490-02 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 13:10 Time Submitted. 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 413117 13:37 KDM P7D0017 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 8260B 4/3117 13:37 KDM P7D0017 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 4/3/17 13:37 KDM P700017 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 4/3117 13:37 KDM P700017 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 4/3/17 13:37 KDM P7DO017 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 4/3/17 13:37 KDM P7D0017 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 413117 13:37 KDM P7D0017 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 4/3/17 13:37 KDM P7D0017 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 413117 13:37 KDM P7D0017 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 4/3117 13:37 KDM P7D0017 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 4/3/17 13:37 KDM P7D0017 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 4/3/17 1337 KDM P7D0017 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 4/3117 13:37 KDM P7D0017 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 4/3117 13:37 KDM P7D0017 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 4/3/17 13:37 KDM P7DO017 Acetone BRL uglL 5.0 0.31 1 82608 4/3117 13:37 KDM P7DO017 Acrolein BRL ug/L 20 0.20 1 8260B 4/3/17 13:37 KDM P7DO017 Acrylonitrile BRL ug/L 20 0.20 1 8260B 4/3/17 13:37 KDM P7D0017 Benzene BRL ug/L 0.50 0,048 1 8260B 413/17 13:37 KDM P7D0017 Bromobenzene BRL ug/L 0.50 0.057 1 8260E 4/3117 13:37 KDM P7D0017 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 413/17 1337 KDM P7D0017 Bromodichloromethane 1.1 ug/L 0.50 0.062 1 6260B 413117 13:37 KDM P7D0017 Bromoform BRL ug/L 1.0 0.040 1 8260B 4/3/17 13,37 KDM P7D0017 Bromomethane BRL ug/L 1.0 0.18 1 8260B 4/3/17 13:37 KDM P7DD017 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 4/3/17 13:37 KDM P71)0017 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 413/17 13.37 KDM P7D0017 Chlorobenzene BRL ug/L 0,50 0.062 1 8260B 413/17 13,37 KDM P71D0017 Chloroethane BRL ug/L 0.50 0,22 1 8260B 4/3/17 13 37 KDM P7D0017 Chloroform 4.3 ug/L 0.60 0.076 1 82608 4/3117 13:37 KDM P7D0017 Chlorornethane BRL ug/L 0.50 0.079 1 8260B 4/3117 13:37 KDM P7D0017 cis-1.2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 4/3/17 13:37 KDM P7D0017 cis- 1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 4/3/17 13.37 KDM P7D0017 Dibromochloromethane 0.64 ug/L 0.60 0.081 1 8260B 413117 13:37 KDM P7D0017 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 413117 1337 KDM P7D0017 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 4/3/17 1337 KDM P7D0017 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 4/3/17 13:37 KDM P7D0017 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 4/3/17 13:37 KDM P7D0017 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 4/3/17 1337 KDM P7D0017 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 413/17 13:37 KDM P7DO017 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 413117 13:37 KDM P7D0017 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 413117 13:37 KDM P7D0017 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 413/17 13:37 KDM P7D0017 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 4/3/17 13:37 KDM P7D0017 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041626-0409 Page 10 of 23 P R I S M I Fujiitonmee Analytical 8 = Environmental Solutions .LS�,—ry� ���'a "-IABORATOR�ES iuC Laboratory Report 04/04/2017 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-3 Attm Mike Falknor Prism Sample ID: 7030490-02 231 Haywood Street Prism Work Order: 7030490 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/31/17 13:10 Time Submitted: 03/31/17 15:20 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L Methyl-tert-Butyl Ether BRL ug/L Naphthalene BRL ug/L n-Butylbenzene BRL ug/L n-Propylbenzene BRL ug/L o-Xylene BRL ug/L sec-Butylbenzene BRL ug/L Styrene BRL ug/L tert-Butylbenzene BRL ug/L Tetrachloroethylene BRL ug/L Toluene BRL ug/L trans-1,2-Dichloroethylene BRL ug/L trans- 1, 3-Dichloropropylene BRL ug/L Trichloroethylene BRL ug/L Trichlorofluoromethane BRL ug/L Vinyl acetate BRL ug/L Vinyl chloride BRL ug/L 1.0 0.083 1 8260B 4/3/17 13:37 KDM P7DO017 0.50 0.042 1 8260B 4/3/17 13:37 KDM P7DO017 1.0 0.19 1 82606 4/3117 1337 KDM P7DO017 1.0 0.076 1 8260B 4/3/17 13:37 KDM P7DOD17 0.50 0.087 1 8260B 4/3/17 13:37 KDM P7DO017 0.50 0.044 1 8260B 4/3/17 13:37 KDM P7DO017 0,50 0.076 1 8260B 4/3/17 13:37 KDM P7DO017 0,50 0.047 1 8260B 4/3117 13:37 KDM P7DO017 0.50 0.088 1 8260B 4/3/17 13.37 KDM P7DO017 0.50 0.098 1 8260B 413/17 13.37 KDM P7DO017 0.50 0.044 1 8260B 4/3/17 13:37 KDM P7DO017 0.50 0.094 1 8260B 413/17 13:37 KDM P7DO017 0.50 0.070 1 8260B 4/3117 1137 KDM P7DO017 0.50 0.078 1 8260B 4/3117 13:37 KDM P7DO017 0.50 0.062 1 8260B 413/17 13:37 KDM P7DO017 2.0 0.060 1 8260B 4/3/17 13:37 KDM P7DO017 0.50 0.097 1 8260B 4/3/17 13:37 KDM P7DOD17 Surrogate Recovery Control Limits 4-Bromofluorobe nzene 99 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 90 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629.6364 - Toll Free Number: 1.800/529.6364 - Fax: 7041526-0409 Page 11 of 23 S M ! Full -Service Analytical 8 r� I Envlronmenla15o1v Solutions a Level II QC Report 4/4/17 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Prism Work Order: 7030490 Attn: Mike Falknor Time Submitted: 3/31/2017 3:20:OOPM 231 Haywood Street Asheville, NC 28801 Volatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0017 - 5030B Blank (P7D0017-BLK1) Prepared & Analyzed. 04/03/17_ 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1.1,2-Trichloroethane BRL 0.50 ug/L 1,1-Dichloroethane BRL 0.50 ug/L 1, 1 -Dichloroethylene BRL 0.50 ug/L 1, 1 -Dichloropropylene BRL 0.50 ug/L 1,2,3-Tnchlorobenzene BRL 2.0 ug/L 1,2,3-Trichloropropane BRL 1.0 ug/L 1,2,4-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethylbenzene BRL 0.50 ug/L 1,2-Dibromo-3-chlompropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3.5-Trimethylbenzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis- 1,2-D ichloroethylene BRL 0.50 ug/L cas-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 1.0 ug/L Ethylbenzene BRL 0.50 ug/L Hexachlorobutadiene BRL 2.0 ug/L This report should not be reproduced except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/62"364 -Toll Free Number: 1.8001529-6364 - Fax: 704/626-0409 Page 12 of 23 IC !` n I Full -Service Analytical 8 J' V I Environmental Solutions '�''�l�tKnM1TORIff. II:C Level II QC Report 4/4117 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Volatile Organic Compounds by GClMS - Quality Control Prism Work Order: 7030490 Time Submitted: 3/31/2017 3:20:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0017 - 5030B Blank (P71)(11017-BLM )i Prepared & Analyzed: 04/03/17 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0,50 ug/L trans-1,2-Dichloroethylene BRL 0.50 ug/L Vans-1,3-Dichloropropylene BRL 0.5D ug/L Trichloroethylene BRL 0,50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug!L Surrogate. 4-Bromolluorobenzene 506 ug/L 50.00 101 80-124 Surrogate. Dibromolluoromethane 54.2 ug/L 50.00 108 75-129 Surrogate: Toluene-0`8 45.0 ugA 50.00 90 77-123 LCS (P7D0017-BSI) Prepared & Analyzed: 04/03/17 1,1,1,2-Tetrachloroethane 20.5 0.50 _ ug/L 20,00 102 79-134 1,1,1-Trichloroethane 24.5 0.50 ug/L 20,00 122 75-136 1,1,2,2-Tetrachloroethane 18.2 0.50 ug/L 20.00 91 62-127 1,1,2-Trichloroethane 22.2 0.50 ug!L 20.00 ill 70-140 1,1-Dichloroethane 22.8 0.50 ug/L 20.00 114 78-130 1,1-Dichloroethylene 25.2 0.50 ug/L 20.00 126 70-154 1, 1 -Dichloropropylene 22.6 0.50 ug/L 20.00 113 71-136 1,2,3-Trichlorobenzene 17.7 2.0 ug/L 20.00 88 58-144 1,2,3-Trichloropropane 19-6 1.0 ug/L 20.00 98 71-127 1,2,4-Trichlorobenzene 17.8 1.0 ug/L 20.00 89 66-139 1. 2,4-Tri methylbenzene 18.6 0.50 ug/L 20.00 93 75-133 1,2-Dibromo-3-chloropropane 18.5 2.0 ug/L 20.00 92 63-134 1,2-Dibromoethane 20.2 0.50 ug/L 20.00 101 77-135 1,2-Dichlorobenzene 19.6 0.50 ug/L 20.00 98 78-128 1,2-Dichloroethane 24.0 0.50 ug/L 20.00 120 68-131 1,2-Dichloropropane 22.3 0.50 ug/L 20.00 ill 77-130 1,3,5-Trimethylbenzene 19.9 0.50 ug/L 20.00 100 75-131 1,3-Dichlorobenzene 19.4 0.50 ug/L 20.00 97 77-125 1,3-Dichloropropane 21.0 0.50 ug/L 20.00 105 76-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. 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Solutions Level II QC Report 4/4/17 Anchor IDEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7D0017 - 6030B Reporting Result Limit Units Prism Work Order: 7030490 Time Submitted: 3/31/2017 3:20:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7D0017-BSI) _ _ _ Prepared & Analyzed: 04/03/17 Trichioroethylene 22.5 0.50 ug/L 20.00 113 77-133 Trichlorofluoromethane 26.2 0.50 ug/L 20.00 131 62-148 Vinyl acetate 24.1 2.0 ug/L 20.00 120 34-167 Vinyl chloride 25.2 0.50 ug/L 20.00 126 57-141 Surrogate:4-Bromofluorobenzene 49.6 ug& 50.00 99 80-124 Surrogate: Dibromotluoromethane 54.7 ug/L 50.00 109 75-129 Sudogate: Toluene-d8 46.7 u92 50.00 93 77-123 LCS Dup (P7D0017-SSD1) Prepared &Analyzed: 04/03/17 11,12-Tetrachloroethane 19.7 0.50 ug/L 20.00 99 79-134 4 20 1,1,1-Trichbroethane 21.6 0,50 ug/L 20.00 108 75-136 12 20 1,1,2,2-Tetrachloroethane 18.9 0.50 ug/L 20.00 94 62-127 3 20 1,1,2-Trichbroethane 21.2 0.50 ug/L 20.00 106 70-140 5 20 1, 1 -Dichloroethane 20.8 0.50 ug/L 20.00 104 78-130 9 20 1,1-Dichloroethylene 22.8 0.50 ug/L 20.00 114 70-154 10 20 1, 1 -Dichloropropylene 20.0 0.50 ug/L 20.00 100 71-136 12 20 1,2,3-Trichlorobenzene 17.6 2.0 ug/L 20.00 88 58-144 0.3 20 1,2,3-Trichloropropane 19.6 1.0 ug/L 20.00 98 71-127 0.1 20 1,24-Trichlorobenzene 17.2 1.0 ug/L 20.00 86 W139 4 20 1,2,4-Trimethylbenzene 17.8 0.50 ug/L 20.00 89 75-133 5 20 1,2-Dibromo-3-chtoropropane 18.3 2.0 ug/L 20.00 92 63-134 0.7 20 1,2-Dibromoethane 20.2 0.50 ug/L 20.00 101 77-135 0.2 20 1,2-Dichlorobenzene 19.4 0.50 ug/L 20.00 97 78-128 1 20 1,2-Dichloroethane 22.4 0.50 ug/L 20.00 112 68-131 7 20 1,2-Dichloropropane 21.0 0.50 ug/L 20.00 105 77-130 6 20 1,3,5-Trimethylbenzene 19.2 0.50 ug/L 20.00 96 75-131 4 20 1,3-Dichlorobenzene 18.7 0.50 ug/L 20.00 94 77-125 4 20 1,3-Dichloropropane 20,6 0.50 ug/L 20.00 103 76-132 2 20 1,4-Dichlorobenzene 18.9 0.50 ug/L 20.00 94 75-126 0.2 20 2,2-Dichloropropane 21.5 2.0 ug1L 20.00 108 29-149 14 20 2-Chlorotoluene 18.3 0.50 ug/L 20.00 91 74-126 3 20 4-Chlorotoluene 18.9 0.50 ug/L 20.00 94 78-129 6 20 4-Isopropyltoluene 17,6 0.50 ug/L 20.00 88 69-132 5 20 Acetone 39.1 5.0 ug/L 40.00 98 40-166 13 20 Acrolein 47.1 20 ug/L 40.00 118 70-130 0.3 20 Acrylonitrile 44.9 20 ug/L 40.00 112 81-127 5 20 Benzene 21.1 0.50 ug/L 20.00 105 77-128 11 20 Bromobenzene 18.1 0.50 ug/L 20.00 90 78-129 5 20 Bromochloromethane 21.3 0.50 ug/L 20.00 106 78-135 8 20 Bromodichloromethane 21.6 0.50 ug/L 20.00 108 76-138 5 20 Bromoform 19.2 1.0 ug/L 20.00 96 71-135 4 20 Bromomethane 23.6 1.0 ug/L 20.00 118 41-168 4 20 Carbon disulfide 23.1 5.0 ug/L 20.00 116 59-135 7 20 Carbon Tetrachloride 20.4 0.50 ug/L 20.00 102 72-142 14 20 Chlorobenzitne 19.6 0.50 ug/L 20.00 98 78-119 3 20 Chloroethane 22.8 0.50 ug/L 20,00 114 57-142 8 20 Chloroform 20.1 0.50 ug/L 20.00 101 77-130 12 20 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364 -Toll Free Number: 1-600/629.6364 - Fax: 70M626-0409 Page 15 of 23 PRISM Full -Service Analytical 8 E nvironmonSolutions tal Solutions Level it QC Report 4/4/17 Anchor QEA of North Carolina, PLLC Project Charlotte Metro Prism Work Order: 7030490 Attn: Mike Falknor Time Submitted. 3/31/2017 3:20.00PM 231 Haywood Street Asheville, NC 28801 volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0017 - 5030B LCS Dup (P7D0017-BSD1) Prepared &Analyzed: 04/03/17 Chloromethane 21.6 0.50 ug/L 20.00 108 47-145 6 20 cis- 1,2-Dichloroethylene 21.3 0.50 ug/L 20.00 107 76-141 12 20 cis- 1,3-Dichloropropylene 22.0 0.50 ug/L 20.00 110 65-140 5 20 Dibromochloromethane 20.8 0.50 ug/L 20.00 104 75-134 2 20 Dibromomethane 21.6 0.50 ug/L 20.00 108 76-135 3 20 Dichlorodifluoromethane 24.1 1.0 ug/L 20.00 121 28-163 6 20 Ethylbenzene 19.7 0.50 ug/L 20.00 98 80-127 4 20 Hexachlorobutadiene 18.8 2.0 ug/L 20.00 94 61-134 6 20 Isopropyl Ether 20.6 0.50 ug/L 20.00 103 60-154 7 20 Isopropylbenzene (Cumene) 19.3 0.50 ug/L 20.00 96 70-130 4 20 m,p-Xylenes 41.3 1.0 ug/L 40.00 103 77-133 4 20 Methyl Butyl Ketone (2-Hexanone) 18.6 5.0 ug/L 20.00 93 64-137 4 20 Methyl Ethyl Ketone (2-Butanone) 20.9 5.0 ug/L 20.00 105 71-134 6 20 Methyl Isobutyl Ketone 22.4 5.0 ug/L 20.00 112 69-134 10 20 Methylene Chloride 20.7 1.0 ug/L 20.00 103 73-131 6 20 Methyl-tert-Butyl Ether 22.5 0.50 ug/L 20.00 112 68-135 5 20 Naphthalene 16.9 1.0 ug/L 20.00 84 64-136 1 20 n-Butylbenzene 17.8 1.0 ug/L 20.00 89 68-134 5 20 n-Propylbenzene 18.8 0.50 ug/L 20.00 94 72-132 3 20 o-Xylene 19.9 0.50 ug/L 20.00 100 78-128 2 20 sec-Butylbenzene 17.3 0,50 ug/L 20.00 87 71-131 5 20 Styrene 18.6 0.50 ug/L 20.00 93 78-129 3 20 tert-Butylbenzene 18.9 0.50 ug/L 20.00 94 70-132 3 20 Tetrachloroethylene 20.1 0.50 ug/L 20.00 100 60-129 4 20 Toluene 21.0 0.50 ug/L 20.00 105 76-131 3 20 trans-1,2-Dichloroethylene 23.1 0,50 ug/L 2000. 115 76-135 0.6 20 trans-1,3-Dichloropropylene 22.6 0.50 ug/L 20.00 113 67-140 2 20 Trichloroelhylene 21.6 0.50 ug/L 20.00 108 77-133 4 20 Trichlorofluoromethane 23.8 0.50 ug/L 20.00 119 62-148 9 20 Vinyl acetate 22.5 2.0 ug/L 20.00 112 34-167 7 20 Vinyl chloride 22.5 0.50 ug/L 20.00 112 57-141 11 20 Surrogate. 4-Bromotluorobenzene 48.6 ug/L 50.00 97 80-124 SurrogateDibromofluoromethane 48.2 ug/L 50.00 96 75-129 Surrogate. Toluene -dB 46.2 ug/L 50.00 92 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-0409 Page 16 of 23 PRISMI Full -Service Analytical Environmental Solutions -e'.e^- - - unonnronrcR�u;. Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GCJMS - Quality Control Analyte Batch P7D0004 - 3510C MS Reporting Result Limit Units Level II QC Report 414/17 Prism Work Order: 7030490 Time Submitted: 3/31/2017 3:20:OOPM Spike Source °/REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7D0004-BLK1) Prepared &Analyzed: 04/03/17 1,2.4-Trichlorobenzene BRL 10 ug/L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL to ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methylnaphthalene BRL 10 ug/L 2,4,5-Trichlorophenol BRL 10 ug/L 2,4,6-Trichlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methylnaphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 3/4-Methylphenol BRL 10 ug/L 3-Nitroaniline BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug/L Aniline BRL 10 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Senzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropypether BRL 10 ug/L Bis(2-Ethylhexy1)phthalate BRL 10 ug.IL Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/6296364 - Toll Free Number: 1.800/529.6364 - Fax: 7041626-0409 Page 17 of 23 P R f S M l Environmental Analytical 8 Environmental Solutions Level 11 QC Report 4/4/17 Anchor IDEA of North Carolina, PLLC Project: Charlotte Metro Attm Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Result Batch P7D0004 - 3510C M5 Blank (P7D0004-BLK1) Dibenzo(a,h)anthracens BRL Dibenzofuran BRL Diethyl phthalate BRL Dimethyl phthalate BRL Di-n-butyl phthalate BRL Di-n-octyl phthalate BRL Fluoranthene BRL Fluorene BRL Hexachlorobenzene BRL Hexachlorobutadiene BRL Hexachlorocyclopentadiene BRL Hexachloroethane BRL Indeno(1,2,3-cd)pyre ne BRL Isophorone BRL Naphthalene BRL Nitrobenzene BRL N-Nitroso-di-n-propylamine BRL N-Nitrosodiphenylamine BRL Pentachlorophenol BRL Phenanthrene BRL Phenol BRL Pyrene BRL Surrogate. 2, 4, 6-Tribromophenol 85.3 Surrogate: 2-Fluorobiphenyl 35.2 Surrogate, 2-Fluorophenol 49.0 Surrogate: Nitrobenzene-d5 35.2 Surrogate. Phenol-d5 31.7 Surrogate. Terphenyl-04 53.1 Prism Work Order: 7030490 Time Submitted: 3/31/2017 3i20:OOPM Reporting Spike Source %REC Limit Units Level Result %REC Limits RPD Prepared & Analyzed: 04/03/17 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug1L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug/L 10 ug1L ug/L 100.0 85 43-140 ug/L 50.00 70 44-119 ug/L 100.0 49 19-119 ug/L 50.00 70 44-120 ug/L 100.0 32 11-52 ug/L 50.00 106 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041625-0409 RPD Limit Notes r Page 18 of 23 Full - 'PRISM I Environmental Analytical 3 Environmental Solutions ..c`� � '�� l RenrtAT(fR1E5 INf Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC/MS - Quality Control Level it QC Report 4/4/17 Prism Work Order: 7030490 Time Submitted: 3/31/2017 3:20:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0004 - 3510C MS LCS (P7D0004-BS1) Prepared &Analyzed: 04/03/17 _ 1,2,4-Trichlorobenzene 26.7 10 ug/L 50.00 53 29-126 1,2-Dichlorobenzene 26.7 10 ug/L 50.00 53 32-111 1,3-Dichlorobenzene 24.4 10 ug/L 50.00 49 28-110 1,4-Dichlorobenzene 25.0 10 ug/L 50.00 50 29-112 1-Methylnaphthalene 35.1 10 ug/L 50.00 70 41-119 2,4,5-Trichiorophenol 42,2 10 ug/L 50.00 84 53-123 2,4,6-Trichlorophenol 43.1 10 ug/L 50.00 86 50-125 2,4-Dichlorophenol 35.1 10 ug/L 50.00 72 47-121 2,4-Dimethylphenol 44.3 10 ug/L 50.00 89 31-124 2,4-Dinitrophenol 56.7 10 ug/L 50.00 113 23-143 2,4-Dinitrotoluene 45.6 10 u9/1- 50.00 91 57-128 2,6-Dinitrotoluene 46A 10 ug/L 50,00 93 57-124 2-Chloronaphihalene 37.4 10 ug/L 50.00 75 40-116 2-Chlorophenol 36.7 10 ug/L 50.00 73 38-117 2-Methylnaphthalene 33.0 10 ug/L 50.00 66 40-121 2-Methylphenol 36.9 10 ug/L 50.00 74 30-117 2-Nitroaniline 39.4 10 ug/L 50,00 79 55-127 2-Nitrophenol 36.1 10 ug/L 50.00 72 47-123 3,3'-Dichlorobenzidine 48.8 10 ug/L 50.00 96 27-129 3/4-Methylphenol 30.8 10 ug/L 50.00 62 29-110 3-Nitroaniline 40.2 10 ug/L 50.00 80 41-128 4,6-Dinitro-2-methylphenol 48.8 10 ug/L 50.00 98 44-137 4-Bromophenyl phenyl ether 42.2 10 ug/L 50.00 84 55-124 4-Chloro-3- methyl phenol 39.4 10 ug/L 50.00 79 52-119 4-Chloroaniline 34.3 10 ug/L 50.00 69 33-117 4-Chlorophenyl phenyl ether 39.4 10 ug/L 50.00 79 53-121 4-Nitroaniline 38.7 10 ug/L 50.00 77 45-135 4-Nitrophenol 20.2 10 ug/L 50.00 40 10-77 Acenaphthene 42.9 10 ug/L 50.00 86 47-122 Acenaphthylene 39.9 10 ug/L 50,00 80 41-130 Aniline 44.8 10 ug/L 50.00 90 12-197 Anthracene 45.7 10 ug/L 50.00 91 57-123 Azobenzene 45.8 10 ug/L 50.00 92 61-116 Benzo(a)anthracene 48.1 10 ug/L 50.00 96 58-125 Benzo(a)pyrene 45.2 10 ug/L 50.00 90 54-128 Senzo(b)fluoranthene 47.1 10 ug/L 50,00 94 53-131 Benzo(g,h,i)perylene 41.5 10 ug/L 50.00 83 50-134 Benzo(k)fluoranthene 43.8 10 ug/L 50.00 88 57-129 Benzoic Acid 15.1 100 ug/L 50.00 30 10-125 J Benzyl alcohol 34.6 10 ug/L 50.00 69 31-112 bis(2-Chloroethoxy)methane 35.6 10 ug/L 50.00 71 48-120 8is(2-Chloroethy1)ether 33.3 10 ug/L 50.00 67 43-118 Bis(2-chloroisopropy1)ether 34.7 10 ug/L 50.00 69 37-130 Bis(2-Ethylhexyl)phthalate 48.5 10 ug/L 50.00 97 55-135 Butyl benzyl phthalate 47.8 10 ug/L 50.00 96 53-134 Chrysene 46.8 10 ug/L 50.00 98 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/62M364 - Toll Free Number: 1-8001629-6364 - Fax: 704/625-0409 Page 19 of 23 Fice AnelytdPRISM 1 Environmentet Solutions Level II QC Report 4/4117 Anchor QEA of North Carolina, PLLC Project. Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Prism Work Order: 7030490 Time Submitted: 3/31/2017 3:20:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7D0004 - 3510C MS LCS {P7D0004-113SI) Prepared & Analyzed: 04/03/17 Dibenzo(a,h)anthracene 44.9 10 ug/L 50.00 90 51-134 Dibenzofuran 41.6 10 ug/L 50.00 83 53-118 Diethyl phthalate 42.6 10 ug,'L 50.00 85 56-125 Dimethyl phthalate 42.7 10 ug,'L 50.00 85 45-127 Di-n-butyl phthalate 43.1 10 ug/L 50.00 86 59-127 Di-n-octyl phthalate 46.2 10 ug/L 50.00 92 51-140 Fluorenthene 44.6 10 ug/L 50.00 89 57-128 Fluorene 42.6 10 ug/L 50.00 85 52-124 Hexachlorobenzene 43,5 10 ug/L 50.00 87 53-125 Hexachlorobutadiene 24.6 10 ug/L 50.00 49 22-124 Hexachlorocyclopentadiene 9.72 10 ug/L 50.00 19 32-117 L, J Hexachtoroethane 23.3 10 ug/L 50.00 47 21-115 Indeno(1,2,3-cd)pyrene 44.4 10 ug/L 50.00 89 52-134 Isophorone 37.8 10 ug/L 50.00 76 42-124 Naphthalene 31,4 10 ug/L 50.00 63 40-121 Nitrobenzene 33.4 10 ug/L 50.00 67 45-121 N-Nitroso-di-n-propylamine 37.6 10 ug/L 50.00 75 49-119 N-Nitrosodiphenylamine 54.0 10 ug/L 50.00 108 51-123 Pentachlorophenol 59.1 10 ug/L 50.00 118 35-138 Phenanthrene 45.6 10 ug/L 50.00 91 59-120 Phenol 18.6 10 ug/L 50.00 37 12-58 Pyrene 47.2 10 ug/L 60.00 94 57-126 Surrogate: 2,4,6-Tribromophenol 86.4 uglL 100.0 86 43-140 Surrogate 2-Fluorobiphenyl 38.0 uglL 50.00 76 44-119 Surrogate:2-Fluorophenol 46.1 uglL 100.0 46 19-119 Surrogate: Nitrobenzene-d5 32.8 uglL 50.00 66 44-120 Surrogate: Phenol-d5 32.0 uglL 100.0 32 11-52 Surrogate. Terphenyl-d14 52.5 uglL 50.00 105 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041626-0409 rPage27777 0 of 23-1 Pull-Sewice Analytical 8 Environmental Solutions Level II QC Report 4/4/17 Anchor OEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville. NC 28801 Project Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7D0004 - 3510C MS Reporting Result Limit Units Prism Work Order: 7030490 Time Submitted: 3/31/2017 3.20:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 1-CS Dup (P7D0004-BSD1) Prepared & Analyzed. 04/03/17 1,2,4-Trichlorobenzene 23.7 10 ug/L 50.00 47 29-126 12 20 1,2-Dichlorobenzene 24.6 10 ug/L 50,00 49 32-111 9 20 1,3-Dichlorobenzene 22.7 10 ug/L 50.00 45 28-110 7 20 1,4-Dichlorobenzene 23.2 10 ug/L 50.00 46 29-112 8 20 1-Methylnaphthalene 31,0 10 ug/L 50.00 62 41-119 12 20 2,4,5-Trichlorophenol 38.2 10 ug/L 50.00 76 53-123 10 20 2,4,6-Trichlorophenol 39.5 10 ug/L 50.00 79 50-125 9 20 2,4-Dichlorophenol 31.9 10 ug/L 50.00 64 47-121 12 20 2,4-Dimethylphenol 39.5 10 ug/L 50.00 79 31-124 11 20 2,4-Dinitrophenol 50.0 10 ug/L 50.00 100 23-143 12 20 2,4-Dinitrotoluene 42.0 10 ug/L 50.00 84 57-128 8 20 2,6-Dinitrotoluene 42.1 10 ug/L 50.00 84 57-124 10 20 2-Chloronaphthalene 33.7 10 ug/L 50.00 67 40-116 10 20 2-Chlorophenol 32.9 10 ug/L 50.00 66 38-117 11 20 2-Methylnaphthalene 29.3 10 ug/L 50.00 59 40-121 12 20 2-Methylphenol 32.4 10 ug/L 50.00 65 30-117 13 20 2-Nitroaniline 35.9 10 ug/L 50.00 72 55-127 9 20 2-Nitrophenol 31.3 10 ug/L 50.00 63 47-123 14 20 3,3'-Dichlorobenzidine 44.5 10 ug/L 50.00 89 27-129 9 20 3/4-Methylphenol 26.7 10 ug/L 50.00 53 29-110 14 20 3-Nitroaniline 36.8 10 ug/L 50.00 74 41-128 9 20 4,6-Dinitro-2-methylphenol 43.6 10 ug/L 50.00 87 44-137 11 20 4-Bromophenyl phenyl ether 38.2 10 ug/L 50.00 76 55-124 10 20 4-Chloro-3-methylphenol 36.1 10 ug/L 50.00 72 52-119 9 20 4-Chloroaniline 29.8 10 ug/L 50.00 60 33-117 14 20 4-Chlorophenyl phenyl ether 37.0 10 ug/L 50.00 74 53-121 6 20 4-Nitroaniline 36.6 10 ug/L 50.00 73 45-135 6 20 4-Nitrophenol 18.2 10 ug/L 50.00 36 10-77 10 20 Acenaphthene 38.5 10 ug/L 50.00 77 47-122 11 20 Acenaphthylene 36.2 10 ug/L 50.00 72 41-130 10 20 Aniline 38.1 10 ug/L 50.00 76 12-197 16 20 Anthracene 42.0 10 ug/L 50.00 84 57-123 8 20 Azobenzene 40,7 10 ug/L 50.00 81 61-116 12 20 Benzo(a)anthracene 43.9 10 ug/L 50.00 88 58-125 9 20 Benzo(a)pyrene 41.2 10 ug/L 50.00 82 54-128 9 20 Benzo(b)fluoranthene 41.4 10 ug/L 50.00 83 53-131 13 20 Benzo(g,h,i)perylene 37.5 10 ug/L 50.00 75 50-134 10 20 Benzo(k)fluoranthene 41.6 10 ug/L 50.00 83 57-129 5 20 Benzoic Acid 8.92 100 ug/L 50.00 1 B 10-125 51 20 D. J Benzyl alcohol 30.8 10 ug/L 50.00 62 31-112 12 20 bis(2-Chloroethoxy)methane 31.6 10 ug/L 50.00 63 48-120 12 20 Bis(2-Chloroethyl)ether 30.5 10 ug/L 50.00 61 43-118 9 20 Bis(2-chloroisopropyl)ether 31.1 10 ug/L 50.00 62 37-130 11 20 Bis(2-Ethylhexyl)phthaIate 44.0 10 ug/L 50.00 88 55-135 10 20 Butyl benzyl phthalate 44.7 10 ug/L 50,00 89 53-134 7 20 Chrysene 45.6 10 ug/L 50.00 91 59-123 7 20 This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 21 of 23 �ice Analytical 8RISM Environments) SolutionsP Level II QC Report 4/4/17 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Prism Work Order: 7030490 Attn: Mike Falknor Time Submitted: 3/31/2017 3:20:OOPM 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7D0004 - 3510C MS LCS Dup (P7D0004-8SD1) Prepared &Analyzed: 04/03/17 Dibenzo(a,h)anthracene 40.6 10 ug1L 50.00 81 51-134 10 20 Dibenzofuran 38.5 10 ug/L 50.00 77 53.118 8 20 Diethyl phthalate 39.5 10 ug/L 50.00 79 56-125 7 20 Dimethyl phthalate 38.6 10 ug/L 50.00 77 45-127 10 20 Di-n-butyl phthalate 39.4 10 ug/L 50.00 79 59-127 9 20 Di-n-octyl phthalate 42.3 10 ug/L 50.00 85 51-140 9 20 Fluoranthene 40.6 10 ug/L 50.00 81 57-128 9 20 Fluorene 39.1 10 ug/L 60.00 78 52-124 8 20 Hexachlorobenzene 40.9 10 ug/L 50.00 82 53-125 6 20 Hexachlorobutadiene 22.5 10 ug/L 50.00 45 22-124 9 20 Hexachlorocyclopentadiene 8.64 10 ug/L 50.00 18 32-117 9 20 L,J Hexachloroethane 21.6 10 ug/L 50.00 43 21-115 8 20 Indeno(1,2,3-cd)pyrene 41.5 10 ug/L 50.00 83 52-134 7 20 Isophorone 33.6 10 ug/L 50.00 67 42-124 12 20 Naphthalene 27.9 10 ug/L 50.00 56 40-121 12 20 Nitrobenzene 30.1 10 ug/L 50,00 60 45-121 10 20 N-Nitroso-di-n-propylamine 34.0 10 ug/L 50.00 68 49-119 10 20 N-Nitrosodiphenylamine 46.2 10 ug/L 50.00 96 51-123 11 20 Pentachlorophenol 53.2 10 ug/L 50.00 106 35-138 11 20 Phenanthrene 41.8 10 ug/L 50.00 84 59-120 9 20 Phenol 16.1 10 ug/L 50.00 32 12-58 14 20 Pyrene 43.5 10 ug/L 50.00 87 57-126 8 20 Surrogate: 2,4,6-Tribromophenol 77.1 ug/L 100.0 77 43-140 Surrogate:2-Fluorobiphenyl 34.0 ug/L 50.00 68 44-119 Surrogate:2-Fluorophenol 40.6 ug/L 100.0 41 19-119 Surrogate: Nitrobenzene-d5 29.4 ug/L 50.00 59 44-120 Surrogate: Phenol-d5 27.4 ug/L 100.0 27 11-52 Surrogate. Terphenyf-d14 48.1 ug/L 50,00 96 50-134 Sample Extraction Data Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 7030490-01 P7D0004 880 mL 1 mL 04/03/17 10,20 7030490-02 P7D0004 960 mL 1 mL 04/03/17 10:20 Prep Method:5030B Lab Number Batch Initial Final DatelTme 7030490-01 P7D0017 10 mL 10 mL 04/03/17 9:58 7030490-02 P7D0017 10 mL 10 mL 04/03/17 9:58 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 -Toll Free Number: 1.8001529-6364 - Fax: 7D41526-0409 1 Page 22 of 23 =uii5erv�r:�� Ang;Y`•�r:ai R7 PRISM ;7;i ;aonmental Solutin•is PAGE I 011 1 _ QUOTE C TO MOUR1 PROPER BILLING, OWE .tag Sprtnabrook Road •Charlotte. NC 28217 Project Name: P tone 704623-636a • F• x 7041525-4409 Short Hold Analysis: es)' (No) UST Project: (Yes) (NO) Client Company Name: t ^� (1,C 'Please ATTACH any piliblIlEt specific reporting (QC LEVEL I n ill IV) provisions and/or QC Requirements Report To/Contact Name: invoice To: Reporting Address: I 1;- ck i .Ct i` - . � Address: YES NO NIA Samples INTACT upon arrival? Received ON WET ICE? PROPER PRESERVATIVES indicated? Received WITHIN HOLDING TIMES? CUSTODY SEALS INTACT? VOLATILES w.d WIOU7 HEADSPACE7 PROPER CONTAINERS used? TEMP: Therm ID:,f�',T�! Observed.S. 'C 1 Corr: - Phone: ax (Yes)(No):k/t' ::;K� �� purchase Order No1Blliing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONN L Email Address: 4ti o{r^r(Lv"N 6!�w L "' (--v--hequestwl Due Date 5P Day 0 2 Days 0 3 Days ❑ 4 Deys ❑ 5 Days Certification: NELAC DoD FL NC EDD Type: PDF 12! xcel f'Other *Working Days" 0 6-9 Days ❑ Standard 10 days WorkMustBe OTHER_,_ NIA Site Location Name: _ 'r' -k-i -z. Site be o ea next tw mp sales received after 14 0o will be -1'=' Site Location Physical Address: Tumaround time is based on business days, excluding weekends and hdidays. Water Chlorinated: YES_ NO ` (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) S8m,.1a iC@d Upon Collection: YES PO ` NO CLIENT DATE TIME COLLECTED MATRD( (SOIL, SAMPLE CONTAINER PRESERVA• �/ ANALYSIS REQUESTED � REMARKS PRISM LAB TYPE NO.SIZEW SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR T►4ES 2ID YK�cl " NO. HOURS 3LUDGE) SEE BELOW v tikLN a ".� 1 1 i Sampler's Signature Sampled By (Print Name) l- Affiliation� Upon relinquishing, t Chain of Custody is yout,4horintlon for Prism to proceed with the analyses as sted above. Any changes must be li e submitted In writing to the Prism Project Manager. There wili be ch for any changes after analyses have been InlWal zed. Relinquistied By:(Signature) eceNed By: rena Additional Comments: SiteAfrwa#tfiime �. _ !� he : (Signature) eoeroed ignetureDate I Site Departure Tlme: l TO foe: RermWlahed y, ( nature- Received m By: Date F,FIek1 -Q o SH OLD BE TAPED SH E DI SAMPLES ARE NOT A AND VERIFIED AGAINST UNTIL RECEIVED AT THE LABORATORY. (� (D Ex 0 LIPS O Hw d�de Kww Field Service D Other L) tSEE N ES: II UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL II OTHER: RIFVERSEFOR TERMS & CONDITIONS NCOSCI ONC OSC LlNC ❑SC UNC NC ❑SC ONC ❑SC+ OSC I OONC OSC 0NC0SCI O ONC OSC O O O hero O i)ltlCzli�^,- GP TAINE``R TYPE CODES: A = Amber C = Clear _.... _..._...._._.. _ _.._.....�._.._ G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Z Head Space) _........_..........._.......... ..,.............,,.....:,<..,.,...< ,�..,.,...,, .< ,, r,a.•......,,..,...�., .�.,, � , �.,:.,,,...,., .a M..,.�.., _ Case Narrative PRISM LABORATORI[S. INC Full -Service Analytical & Environmental Solutions Anchor QEA of North Carolina, PLLC Mike Falknor 231 Haywood Street Asheville, NC 28801 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: Charlotte Metro Lab Submittal Rate: 03/29/2017 Prism Work Order: 7030450 03/31 /2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: Reviewed By Angela D. Overcash For Robbi A. Jones VP Laboratory Services CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704l529.6364 . Toll Free Number: 1-8001529.6364 - Fax: 7041626.0409 Page 1 of 19 A113 I S I Y I Full -Service analytical 8 Environmental Solutions � UiOA�TOn�ES r+C Sample Receipt Summary 03/31 /2017 Prism Work Order: 7030450 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received M W-4 7030450-01 Water 03/29/17 03/29/17 Samples were received in good condition at 4.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041526-0409 Page 2 of 19 PRISM I Environmental Full-ServicemeAnalytical s Environmental Solutions Summary of Detections 03/3112017 Prism Work Order: 7030450 Prism ID Client ID Parameter Method Result Units 7030450-01 MW-4 Bis(2-Ethylhexy1)phthalate 8270D 3.2 1 ug/L 7030450-01 MW-4 Bromodichloromethane 8260B 1.7 ug,'L 7030450-01 MW-4 Chloroform 8260B 6.5 uglL 7030450-01 MW-4 Dibromochloromethane 8260E 1.0 ug/L 7030450-01 MW-4 m,p-Xylenes 8260E 0.62 1 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 • Fax: 704/625-0409 Page 3 of 19 RI S n �� Full -Service Analytical 8 `FeO'wTLktc_ Nc Environmental Solutions Laboratory Report 03/31 /2017 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-4 Attn: Mike Falknor Prism Sample ID. 7030450-01 231 Haywood Street Prism Work Order 7030450 Asheville, NC 28801 Sample Matrix: Water Time Collected 03/29/17 00:00 Time Submitted: 03/29/17 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 11 1.9 1 8270D 3/30/17 11:32 JMV P7C0471 1,2-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 3/30/17 11:32 JMV P7C0471 1,3-Dichlorobenzene BRL ug/L 11 2.0 1 8270D 3130117 11:32 JMV P7C0471 1,4-Dichlorobenzene BRL ug/L 11 1.7 1 8270D 3/30/17 11.32 JMV P7C0471 1-Methylnaphthalene BRL ug/L 11 2.8 1 8270D 3/30/17 11:32 JMV PX0471 2,4,5-Trichlorophenol BRL ug/L 11 1.7 1 8270D 3/30/17 11:32 JMV P7C0471 2,4,6-Trichlorophenol BRL ug/L 11 2.0 1 8270D 3/30/17 11,32 JMV PX0471 2,4-Dichlorophenol BRL ug/L 11 2.7 1 8270D 3/30/17 11:32 JMV P7C0471 2,4-Dimethylphenol BRL ug/L 11 3.7 1 8270D 3/30/17 1132 JMV P7C0471 2,4-Dinitrophenol BRL CCV ug/L 11 2.9 1 8270D 3/30/17 11:32 JMV P7C0471 2,4-Dinitrotoluene BRL CCV ug/L 11 1.5 1 8270D 3130/17 11:32 JMV P7C0471 2,6-Dinitrotoluene BRL ug/L 11 1.2 1 8270D 3130/17 11:32 JMV P7C0471 2-Chloronaphthalene BRL ug/L 11 2.9 1 8270D 3/30/17 11:32 JMV P7C0471 2-Chlorophenol BRL ug/L 11 2.0 1 8270D 3/30/17 11:32 JMV P7C0471 2-Methylnaphthalene BRL ug/L 11 2.6 1 8270D 3/30/17 11:32 JMV P7C0471 2-Methylphenol BRL ug/L 11 1.9 1 8270D 3/30/17 11:32 JMV PX0471 2-Nitroaniline BRL ug/L 11 1.5 1 8270D 3/30/17 11:32 JMV PX0471 2-Nitrophenol BRL ug/L 11 2.5 1 8270D 3/30/17 11:32 JMV P7Co471 3,3'-Dlchlorobenzidine BRL ug/L 11 1.5 1 8270D 3/30/17 11:32 JMV P7CD471 3/4-Methylphenol BRL ug/L 11 1.6 1 8270D 3130/17 1132 JMV P7C0471 3-Nitroaniline BRL ug/L 11 1.5 1 8270D 3130/17 11:32 JMV PX0471 4,6-Dinitro-2-methylphenol BRL CCV ug/L 11 1.5 1 8270D 3130117 11:32 JMV P7C0471 4-Bromophenyl phenyl ether BRL ug/L 11 1.4 1 8270D 3/30/17 11:32 JMV P7C0471 4-Chloro-3-methylphenol BRL ug/L 11 2.5 1 8270D 3/30/17 11:32 JMV PX0471 4-Chloroaniline BRL ug/L 11 2.6 1 8270D 3/30/17 11:32 JMV P7Co471 4-Chlorophenyl phenyl ether BRL ug/L 11 1,4 1 8270D 3/30117 11:32 JMV P7C0471 4-Nitroaniline BRL ug/L 11 0.99 1 8270D 3/30/17 11.32 JMV P7C0471 4-Nitrophenol BRL ug/L 11 0.64 1 8270D 3130/17 11:32 JMV P7C0471 Acenaphthene BRL ug/L 11 1.9 1 8270D 3/30/17 11:32 JMV P7C0471 Acenaphthylene BRL ug/L 11 22 1 8270D 3/30/17 11:32 JMV PX0471 Aniline BRL ug/L 11 2.6 1 8270D 3130/17 11:32 JMV P7C0471 Anthracene BRL ug/L 11 1.5 1 8270D 3130/17 11.32 JMV P7C0471 Azobenzene BRL ug/L 11 1.9 1 8270D 3130/17 11:32 JMV P7C0471 Benzo(a)anthracene BRL ug/L 11 1.5 1 8270D 3/30/17 11:32 JMV PX0471 Benzo(a)pyrene BRL ug/L 11 1_5 1 8270D 3/30/17 11:32 JMV P7C0471 Benzo(b)fluoranthene BRL ug/L 11 1.2 1 8270D 3130/17 11:32 JMV P7C0471 Benzo(g,h,i)perylene BRL ug/L 11 1.6 1 8270D 3/30/17 1132 JMV P7CD471 Benzo(k)fluoranthene BRL ug/L 11 1.5 1 8270D 3130117 11.32 JMV P7C0471 Benzoic Acid BRL ug/L 110 5.0 1 8270D 3130117 11:32 JMV P7C0471 Benzyl alcohol BRL ug/L 11 2.3 1 8270D 3130/17 11.32 JMV FX0471 bis(2-Chloroethoxy)methane BRL ug/L 11 2.7 1 8270D 3/30117 11.32 JMV P7C0471 Bis(2-Chloroethyl)ether BRL ug/L 11 2.5 1 8270D 3/30/17 11:32 JMV P7C0471 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/62"409 Page 4 of 19 Laboratory Report Analytical x Environmental Solutions P i S M Environmental �:'1LMORnTO%K4 HG 03/31l2017 Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW4 Attn: Mike Falknor Prism Sample ID: 7030450-01 231 Haywood Street Prism Work Order. 7030450 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/29/17 00:00 Time Submitted: 03/29/17 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bis(2-chbroisopropyl)ether BRL ug/L 11 2.1 1 8270D 3/30/17 11:32 JMV P7C0471 Bla(2-Ethylhexyl)phthalate 3.2 J ug/L 11 1.4 1 8270D 3130/17 11:32 JMV 127C0471 Butyl benzyl phthalate BRL ug/L 11 1.4 1 8270D 3/30/17 11:32 JMV P7C0471 Chrysene BRL ug/L 11 1.5 1 8270D 3/30/17 11:32 JMV P7C0471 Dibenzo(a,h)anthracene BRL ug/L 11 1.3 1 8270D 3130117 11:32 JMV P7C0471 Dibenzofuran BRL ug/L 11 1.9 1 8270D 3/30/17 11:32 JMV P7C0471 Diethyl phthatate BRL ug/L 11 3.5 1 8270D 3130117 11:32 JMV P7C0471 Dimethyl phthalate BRL ug/L 11 1.5 1 8270D 3130117 11:32 JMV P7C0471 Di n-butyl phthalate BRL ug/L 11 1.8 1 8270D 3130117 11:32 JMV P7C0471 Dt n-octyl phthalate BRL uglL 11 1A 1 8270D 3/30/17 11:32 JMV P7C0471 Fluoranthene BRL ug/L 11 1.8 1 8270D 3130117 11:32 JMV P7C0471 Fluorene BRL ug/L 11 1.8 1 8270D 3/30/17 11.32 JMV P7C0471 Hexachlorobenzene BRL ug/L 11 1.4 1 8270D 3130/17 11:32 JMV P7C0471 Hexachtorobutadiene BRL ug/L 11 2.3 1 8270D 3130/17 11:32 JMV P7C0471 Hexachlorocydopentadiene BRL ug/L 11 1,8 1 8270D 3/30/17 11:32 JMV P7C0471 Hexachloroethane BRL ug/L 11 1.9 1 82700 3130117 11:32 JMV P7C0471 Indeno(1,2,3-cd)pyrene BRL uglL 11 4.1 1 8270D 3/30117 11.32 JMV P7C0471 Isophorone BRL ug/L 11 2.7 1 8270D 3/30/17 11:32 JMV P7C0471 Naphthalene BRL ug/L 11 2.7 1 8270D 3/30117 11:32 JMV P7C0471 Nitrobenzene BRL ug/L 11 2.7 1 8270D 3/30117 11:32 JMV P7C0471 N-Nitroso-di-n-propylamine BRL ug/L 11 2.3 1 8270D 3/30/17 11:32 JMV P7C0471 N-Nitrosodiphenylamine BRL ug/L 11 1.4 1 8270D 3130/17 11:32 JMV P7C0471 Pentachlorophenol BRL ug/L 11 1.3 1 8270D 3/30/17 11:32 JMV P7C0471 Phenanthrene BRL ug/L 11 1.6 1 0270D 3130/17 11:32 JMV P7C0471 Phenol BRL ug/L 11 1.0 1 8270D 3/30/17 11:32 JMV P7C0471 Pyrene BRL ug/L 11 1.5 1 8270D 3130/17 11:32 JMV P7C0471 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 114 % 43-140 2-Fluorobiphenyl 87 % 44-119 2-Fluorophenol 58 % 19-119 Nitrobenzene-d5 86 % 44-120 Phenol-d5 36 % 11-52 Terphenyt-d14 117 % 50-134 Volatile Organic Compounds by GCIMS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 3/30/17 14:43 KDM P7C0502 1,11-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 3/30/17 14:43 KDM P7C0502 1,1,2,2-Tetrachbroethane BRL ug/L 0.50 0.036 1 8260B 3/30/17 14:43 KDM P7C0502 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 3130/17 14A3 KDM P7C0502 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 3130/17 14:43 KDM P7C0502 1,1-Dichloroethylens BRL ug/L 0.50 0.083 1 8260B 3/30/17 14:43 KDM P7C0502 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 3/30/17 14:43 KDM P7C0502 1,2,3-Trichlorobenzene BRL ug/L 2.0 0,40 1 8260B 3/30/17 14:43 KDM P7C0502 1,2,3-Trichloropropene BRL ug/L 1.0 0.14 1 8260B 3/30/17 14:43 KDM P7C0502 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, NC 28224-0543 Phone: 7041629-0364 - Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 r Page-5 of 19 f Laboratory Report LPRISM I FullAnalytical 03/3112017 EnviService ronmental Solutionss �� } �<. L�80�ATOR2fa iNC Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Client Sample ID: MW-4 Attn: Mike Falknor Prism Sample ID: 7030450-01 231 Haywood Street Prism Work Order: 7030450 Asheville, NC 28801 Sample Matrix: Water Time Collected: 03/29/17 00:00 Time Submitted: 03/29/17 14.55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date(Time ID 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 3130/17 14:43 KDM P7C0502 1,2,4-Trimeth ylbenzene BRL ug/L 0.50 0.054 1 8260E 3/30/17 14A3 KDM P7C0502 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 3130/17 14A3 KDM P7C0502 1,2-Dibromoeihane BRL ug/L 0.50 0,051 1 8260B 3/30/17 1443 KDM P7C0502 1,2-Dichlorobenzene BRL ug/L 0.50 0,076 1 8260B 3/30117 14:43 KDM P7C0502 1,2-Dichloroethane BRL ug/L 0.50 0,066 1 8260B 3/30/17 14:43 KDM PX0502 1.2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 3/30/17 14:43 KDM PX0502 1,3,5-Trimethylbenzene BRL ug/L 0.50 0,076 1 8260B 3130/17 14:43 KDM PX0502 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 3130/17 14:43 KDM P7C0502 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 3/30/17 14:43 KDM P7C0502 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 3/30/17 14:43 KDM P7C0502 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 3/30/17 14:43 KDM PX0502 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 3/30/17 14:43 KDM P7C0502 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 3/30117 14:43 KDM P7C0502 4-1sopropyltoluene BRL ug/L 0.50 0.089 1 8260B 3/30/17 14:43 KDM PX0502 Acetone BRL ug/L 5.0 0,31 1 8260B 3/30/17 14:43 KDM PX0502 Acrolein BRL ug/L 20 0.20 1 8260B 3/30/17 14:43 KDM P7C0502 Acrylonitrile BRL ug/L 20 0.20 1 8260B 3/30/17 14:43 KDM P7C0502 Benzene BRL ug/L 0.50 0.048 1 8260B 3130117 14:43 KDM P7C0502 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 3/30/17 14.43 KDM P7C0502 Bromochloromethane BRL ug/L 0.50 0.14 1 8260E 3/30/17 14:43 KDM P7C0502 Bromodichloromethane 1.7 ug/L 0.60 0.062 1 02608 3/30/17 14:43 KDM P7C0502 Bromoform BRL ug/L 1.0 0.040 1 8260B 3/30/17 14:43 KDM P7C0502 Bromomethane BRL ug/L 1.0 0.18 1 8260B 3/30/17 14.43 KDM P7C0502 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 3/30/17 14:43 KDM P7C0502 Carbon Tetrachloride BRL ug/L 0,50 0.11 1 8260B 3/30/17 14:43 KDM P7C0502 Chlorobenzene BRL ug/L 0.50 0,062 1 8260B 3/30/17 14:43 KDM P7Co502 Chloroethane BRL ug/L 0.50 0.22 1 8260B 3/30M7 14:43 KDM P7C0502 Chloroform 6.6 ug/L 0.50 0.076 1 8260B 3130/17 14:43 KDM P7C0502 Chloromethane BRL ug/L 0.50 0.079 1 8260B 3/30/17 14:43 KDM P7C0502 cis-1,2-Dichloroethylene BRL ug/L 0.50 0,056 1 8260B 3/30/17 14A3 KDM P7C0502 cis-1,3-Dichloropropylene BRL ug/L 0.50 0,079 1 8260E 3/30/17 14,43 KDM P7C0502 Dibromochloromethane 1.0 ug/L 0.50 0.081 1 8260B 3/30/17 14:43 KDM P7C0502 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 3130/17 14:43 KDM P7C0502 Dichlorod ifluoromethane BRL ug/L 1.0 0.11 1 8260B 3/30117 14:43 KDM PX0502 Ethylbenzene BRL ug/L 0.50 0,061 1 8260E 3130/17 14:43 KDM P7C0502 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 3/30/17 14:43 KDM PX0502 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 3/30/17 1443 KDM P7C0502 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260E 3/30/17 14:43 KDM P7C0502 m,p-Xylenes 0.62 J ug/L 1.0 0.12 1 8260B 3/30/17 14:43 KOM P7C0502 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 3130/17 14:43 KDM PX0502 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 82608 3/30117 14:43 KDM P7C0502 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 3/30/17 1443 KDM P7C0502 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road • P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001629.6364 • Fax: 7041625-0409 r Page 6 of 19 PRISM EW e Analytical 3 Envivonmelivnmental Solutions ...`-ueonntorta4 Inc Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Sample Matrix: Water Laboratory Report 03/31/2017 Client Sample ID: MW-4 Prism Sample ID: 7030450-01 Prism Work Order: 7030450 Time Collected: 03/29/17 00:00 Time Submitted: 03/29/17 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Methylene Chloride BRL ug/L Methyl-tert-Butyl Ether BRL ug/L Naphthalene BRL ug/L n-Butylbenzene BRL ug/L n-Propylbenzene BRL ug/L o-Xylene BRL ug/L sec-Butylbenzene BRL ug/L Styrene BRL ug/L tart-Butylbenzene BRL ug/L Tetrachloroethylene BRL ug/L Toluene BRL ug/L trans- 1,2-Dichloroethyiene BRL ug/L trans- 1. 3-Dichloropropylene BRL ug/L Trichloroethylene BRL ug/L Trichtorofluoromethane BRL ug/L Vinyl acetate BRL ug/L Vinyl chloride BRL ug/L 1.0 0.083 1 8260B 3/30/17 14:43 KOM P7C0502 0.50 0.042 1 8260B 3/30117 14:43 KDM P7C0502 1.0 0.19 1 8260B 3/30117 14:43 KDM PX0502 1.0 0.076 1 8260B 3130/17 14:43 KDM P7C0502 0.60 0.087 1 02608 3/30/17 14:43 KDM P7C0502 0.50 0.044 1 8260E 3/30/17 14:43 KDM P7C0502 0.50 0.076 1 8260B 3130/17 14:43 KDM P7C0502 0.50 0.047 1 8260B 3130/17 14:43 KDM PX0502 0.50 0,088 1 8260B 3/30117 14A3 KDM PX0502 0.50 0.098 1 8260B 3/30/17 14:43 KDM PX0502 0.60 0.044 1 8260B 3130/17 14:43 KDM P7C0502 0.50 0.094 1 8260B 3/30/17 14:43 KDM PX0502 0.50 0.070 1 8260B 3/30117 14:43 KDM PX0502 0.50 0,078 1 8260B 3/30117 14:43 KDM PX0502 0.50 0.062 1 8260B 3/30/17 14:43 KDM P7C0502 2.0 0.060 1 8260B 3/30/17 14:43 KDM P7C0502 0.50 0.097 1 8260B 3/30/17 14:43 KDM P7C0502 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 80-124 Dibromofluoromethane 110 % 75-129 Toluene-d8 95 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spring brook Road • P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number. 1-8001629-6364 • Fax: 7041626-0409 Page 7 of 1971 t n Q (h N Nd (;3 a IL Z U a � o o _ � CN cV � J J O in M N a Q of r _N p N Q `U cr E _0 >O N W M M a d N N cc 0 Q 06 a d Y 7 a a ca a d OI O) O co m OI III Ql O, a cm OI OI m O1 OI cm Ol m O) QI co pi W pl O) m W O m OI 0I O) m m Ol O] O] m 01 01 CD OI OI O � 17 3 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 C G C E 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 N N] h Nl K1 V1 N N '- '- h N b b U] N b N N LL] N N W) N N N N N N N 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 '- b Y'1 tp b N b � Iq In N b N O O J 0 O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O — L � U U Oy 0 0 J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J J cr a m Lt x x J J J J J J J J J J J J J J J cr w x m x¢ w x w m ir a m x a_ a U a)m m m m m m m m m m m m m in m m m m m cm m m m m m m m m m m m m m m m m m m m m m m m m m m qy N C _ c� 0 lQ ao a Q � N � N rc J � C J n o tO a �w O N t6 C V ' c t nON1 C 0 CZ00U a EaO_ Ch cCooV_7a _ 0 c C a C a O Cp7g � C w O 6 =a L a N Y E E VLa EO u o L nO pO m 7 c aL a yLa_ oa u a a a O�OhryO W a O O O O O O O O O p EO L EE 0 E ot °Q N 0o E zd Nc . a 14 ' La LNa .' sLU �aa O -0 OO E E 0yL Yry OmC NC H N L 0 p 'M fl 0 C OO LaC O O O O L co m L Lc 1]L N Q ¢ Q Q Q m m m m m m U U U U U U -u .v o 0 o W 2 P R I S M Fuller o men al Sol Icon & Environmanlal Solutions s��•e s.. inAonn*oe Fs we Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7CO502 - 5030B Blank (P7CO602-BLK1) Isopropyl Ether Isopropylbenzene (Cumene) m, p-Xyle ne s Methyl Butyl Ketone (2-Hexanone) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methylene Chloride Methyl-tert-Butyl Ether Naphthalene n-Butylbenzene n-Propylbenzene o-Xylene sec-Butyibenzene Styrene tert-Butylbenzene Tetrachloroethylene Toluene Vans-1,2-Dichloroethylene trans-l ,3-Dichloropropylene Trichloroethylene Trichlorofluoromethane Vinyl acetate Vinyl chloride Surrogate: 4-Bromolluorobenzene Surrogate: Dibromofluoromethane Surrogate. To/uene-dB LCS (P7C0502-BS1) 1,1,1,2-Tetra chio roethane 1,1,1-Trichloroethane 1, 1, 2, 2-Tetrachloroetha ne 1,1,2-Trichloroethane 1,1-Dichloroethane 1, 1 -Dichloroethy lene 1,1-Dichloropropylene 1,2,3-Trichlorobenzene 1, 2, 3-Trish loropropa ne 1, 2,4-Trichlorobenzene 1, 2, 4-Tri meth y I be nz en e 1, 2-D ibro mo-3-chloropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,3, 5-TrimethyIbenzene 1,3-Dichlorobenzene 1,3-Dichloropropane Reporting Result Limit Units Level II QC Report 3/31 / 17 Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Prepared & Analyzed: 03/30/17 BRL 0.50 ug/L BRL 0.50 ug/L BRL 1.0 ug/L BRL 5.0 ug/L BRL 5.0 ug/L BRL 5.0 ug/L BRL 1.0 ug/L BRL 0.50 ug/L BRL 1.0 ug/L BRL 1.0 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 0.50 ug/L BRL 2.0 ug/L BRL 0.50 ug/L 48.1 ug/L 50.00 96 80-124 52.8 ug/L 50.00 106 75-129 46.9 ug/L 50.00 94 77-123 Prepared & Analyzed: 03/30/17 _ 20.3 0.5D ug/L 20.00 101 79-134 21.2 0.50 ug/L 20.00 106 75-136 19.5 0.50 ug/L 20.00 97 62-127 21.8 0.50 uglL 20.00 109 70-140 20.2 0.50 ug/L 20.00 101 78-130 21.1 0.50 ug/L 20.00 106 70-154 20.0 0.50 ug/L 20.00 100 71-136 18.5 2.0 ug/L 20.00 92 58-144 20.2 1.0 ug/L 20.00 101 71-127 18.2 1.0 u91L 20.00 91 66-139 19.2 0.50 ug/L 20.00 96 75-133 18.4 2.0 ug/L 20.00 92 63-134 20.8 0.50 ug/L 2000. 104 77-135 20.2 0.50 ug/L 20.00 101 78-128 21.6 0.50 ug/L 20,00 108 68-131 20.2 0.50 ug/L 20.00 101 77-130 20.4 0.50 ug/L 20.00 102 75-131 20.0 0,50 ug/L 20.00 10D 77-125 20.7 0.50 ug/L 20.00 103 76-132 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 9 of 19 PRISM I Full - Service Analytical E nvironrnental Solutions Level it QC Report 3/31/17 Anchor OEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7CO502 - 5030B Reporting Result Limit Units Prism Work Order 7030450 Time Submitted 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7CO502-BSI) v Prepared & Analyzed_ 03/30/17 1,4-Dichlorobenzene 19.5 0.50 ug/L 20.00 98 75-126 2,2-Dichloropropane 21.6 2.0 ug/L 20,00 108 29-149 2-Chlorotoluene 19.5 0.50 ug/L 20,00 97 74-126 4-Chlorotoluene 20,7 0.50 ug/L 20.00 104 78-129 4-Isopropyltoluene 18.9 0.50 ug/L 20.00 95 69-132 Acetone 36.0 5.0 ug/L 40.00 90 40-166 Acrolein 40.7 20 ug/L 40.00 102 70-130 Acrylonitrile 40.9 20 ug/L 40.00 102 81-127 Benzene 20.8 0.50 ug/L 20.00 104 77-128 Bromobenzene 19.1 0.50 ug/L 20.00 95 78-129 Bromochloromethane 21.1 0.50 ug/L 20.00 106 78-135 Bromodichloromethane 21,5 0,50 ug/L 20.00 107 76-138 Bromoform 19.2 1.0 ug/L 20.00 96 71-135 Bromomethane 20.2 1.0 ug/L 20.00 101 41-168 Carbon disuiride 21.8 5.0 ug/L 20.00 109 59-135 Carbon Tetrachloride 20.4 0.50 ug/L 20.00 102 72-142 Chlorobenzene 20.3 0.50 ug/L 20.00 101 78-119 Chloroethane 20.6 0.50 ug/L 20.00 103 57-142 Chloroform 19.6 0.50 ug/L 20.00 98 77-130 Chloromethane 19.7 0.50 ug/L 20.00 98 47-145 cis-1,2-Dichloroethylene 20.6 0.50 ug/L 20.00 103 76-141 cis- 1,3-D ichloropropylene 22.3 0,50 ug/L 20.00 112 65-140 Dibromochloromethane 21.0 0.50 ug/L 20.00 105 75-134 Dibromomethane 20.3 0.50 ug/L 20,00 102 76-138 Dichlorodifluoromethane 21.3 1.0 ug/L 20.00 106 28-163 Ethylbenzene 20.6 0.50 ug/L 20.00 103 80-127 Hexachlorobutadiene 19.6 2.0 ug/L 20.00 98 61-134 Isopropyl Ether 19.1 0.50 ug/L 20.00 96 60-154 Isopropylbenzene (Cumene) 20.4 0.50 ug/L 20.00 102 70-130 m,p-Xylenes 42.4 1.0 ug/L 40.00 106 77-133 Methyl Butyl Ketone (2-1-lexanone) 17.5 5.0 ug/L 2000, 88 64-137 Methyl Ethyl Ketone (2-Butanone) 19.7 5.0 ug/L 20.00 98 71-134 Methyl Isobutyl Ketone 20.6 5.0 ug/L 20.00 103 69-134 Methylene Chloride 19.4 1.0 ug/L 20.00 97 73-131 Methyl-tert-Butyl Ether 20.6 0.50 ug/L 20.00 103 68-135 Naphthalene 17.7 1.0 ug/L 20.00 88 64-136 n-Butylbenzene 19.2 1.0 ug/L 20.00 96 68-134 n-Propylbenzene 20.3 0,50 ug/L 20.00 102 72-132 o-Xylene 20.3 0.50 ug/L 20,00 102 78-128 sec-Butylbenzene 18.6 0.50 ug/L 20.00 93 71-131 Styrene 19.3 0.50 ug/L 20.00 97 78-129 tert-Butylbenzene 20.3 0.50 ug/L 20,00 102 70-132 Tetrachloroethylene 20.6 0.50 ug/L 20.00 103 80-129 Toluene 21.1 0.50 ug/L 20.00 105 76-131 trans- 1,2-Dichloroethylene 20.8 0.50 ug/L 20.00 104 76-135 trans-1,3-Dichloropropylene 21.6 0.50 ug/L 20.00 108 67-140 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: l-8001629-6364- Fax: 7041525-0409 Page 10Of 19, P E E I S M I Full -Service Analytical s Environmental Solutions .. Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GC1MS - Quality Control Analyte Batch P7CO502 - 5030B Reporting Result Limit Units Level 11 QC Report 3/31/17 Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7CO602-BSI) Prepared & Analyzed. 03/30/17 Trichloroethylene 21.8 0.50 ugtL 20.00 109 77-133 Trichlorofluoromethane 22.1 0.50 ug1L 20.00 ill 62-148 Vinyl acetate 21.0 2.0 ug/L 20.00 105 34-167 Vinyl chloride 21.2 0.50 uglL 20.00 106 57-141 Surrogate:4-Bromofluorobenzene 49.3 ug/L 50.00 99 80-124 Surrogate. Dibromofluoromethane 48.4 ug/L 50.00 97 75-129 Surrogate Toluene -dB 47.3 ug/L 50,00 95 77-123 LCS Dup (P7C0502-BSD1) Prepared & Analyzed: 03/30/17 1,1,1,2-Tetrachloroethane 19.4 0.50 ug/L 20.00 97 79-134 5 20 1,1,1-Trichloroethane 19.8 0.50 ug/L 20.00 99 75-136 7 20 1,1,2,2-Tetrachloroethane 18.8 0.50 ug/L 20.00 94 62-127 4 20 1,1,2-Trichloroethane 20.7 0.50 ug/L 20.00 104 70-140 5 20 1,1-Dichloroethane 18.8 0.50 ug/L 20.00 94 78-130 7 20 1,1-Dichloroethylene 20.0 0.50 ug1L 20.00 100 70-154 5 20 1,1-Dichloropropylene 19A 0.50 ug/L 20.00 97 71-136 3 20 1,2,3-Trichlorobenzene 18.6 2.0 ug/L 20.00 93 58-144 0.5 20 1,2,3-Trich] oropropane 19.5 1.0 ug/L 20.00 97 71-127 4 20 1,24-Trichlorobenzene 17.8 1.0 ug/L 20.00 89 66-139 2 20 1,2,4-Trimethylbenzene 18.5 0.50 ug/L 20.00 92 75-133 4 20 1,2-Dibromo-3-chloropropane 18.6 2.0 ug/L 20.00 93 63-134 1 20 1,2-Dibromoethane 20.3 0.50 ug/L 20.00 101 77-135 3 20 1,2-Dichlorobenzene 19.6 0.50 ug/L 20.00 98 78-128 3 20 1,2-Dichloroethane 20.9 0.50 ug/L 20.00 104 68-131 3 20 1,2-Dichloropropane 19.4 0.50 ug/L 2000 97 77-130 4 20 1,3,5-Trimethylbenzene 19.5 0.50 ug/L 20,00 98 75-131 4 20 1,3-Dichlorobenzene 18.9 0.50 ug/L 20,00 95 77-125 5 20 1,3-Dichloropropane 20.2 0.50 ug/L 20.00 101 76-132 2 20 1,4-Dichlorobenzene 18.8 0.50 ug/L 20.00 94 75-126 4 20 2,2-Dichloropropane 20.2 2.0 ug/L 20.00 101 29.149 7 20 2-Chlorotoluene 18.4 0.50 ug/L 20.00 92 74-126 6 20 4-Chlorotoluene 20-1 0.50 ug/L 20.00 101 78-129 3 20 4-Isopropyltoluene 18.2 0.50 ug/L 20.00 91 69-132 4 20 Acetone 35.6 5.0 ug/L 40.00 89 40-166 1 20 Acrolein 39.1 20 ug/L 40.00 98 70-130 4 20 Acrylonitrile 41.4 20 ug/L 40.00 103 81-127 1 20 Benzene 19.8 0.50 ug/L 20.00 99 77-128 5 20 Bromobenzene 18.3 0.50 ug/L 20.00 91 78-129 4 20 Bromochloromethane 20.3 0.50 ug/L 20.00 102 78-135 4 20 Bromodichloromethane 21.2 0.50 ug/L 20.00 106 76-138 2 20 Bromoform 19.7 1.0 ug/L 20.00 99 71-135 3 20 Bromomethane 19.8 1.0 ug/L 20.00 99 41-168 2 20 Carbon disulfide 21.2 5.0 ug/L 20.00 106 59-135 3 20 Carbon Tetrachloride 19.2 0.50 ug/L 20.00 96 72-142 6 20 Chlorobenzene 19.4 0.50 ug/L 20.00 97 78-119 4 20 Chloroethane 19.8 0.50 ug/L 20.00 99 57-142 4 20 Chloroform 18.9 0,50 ug/L 20.00 94 77-130 4 20 This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc, 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1.8001529-6364 - Fax: 7041626-0409 ! Page 11 Of 19 1= P R I S M I Full -Service Analytical Environmental Solutionss ��,^•�_. ..__' unonuonies. me Anchor QEA of North Carolina, PLLC Attm Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Volatile Organic Compounds by GC1MS - Quality Control Analyte Batch P7C0502 - 5030B Reporting Result Limit Units Level II QC Report 3/31 /17 Prism Work Order. 7030450 Time Submitted: 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P7C0602-BSD1) J Prepared & Analyzed: 03/30/17 Chloromethane 18.7 0.50 ug/L 20.00 93 47-145 5 20 cis- 1,2-Dichloroethylene 20.0 0.50 ug/L 20.00 100 76-141 3 20 cis- 1,3-Dichloropropylene 21.3 0.50 ug/L 20.00 106 65-140 5 20 Dibromochloromethane 20.2 0.50 ug/L 20.00 101 75-134 4 20 Dibromomethane 21.5 0.50 ug/L 20.00 107 76-138 5 20 Dichlorodifluoromethane 19.5 1.0 ug/L 20.00 97 28-163 9 20 Ethylbenzene 19.4 0.50 ug/L 20.00 97 80-127 6 20 Hexachlorobutadiene 18.7 2.0 ug/L 20.00 94 61-134 4 20 Isopropyl Ether 18.6 0.50 ug/L 20.00 93 60-154 3 20 Isopropylbenzene (Cumene) 19.6 0.50 ug/L 20.00 98 70-130 4 20 m,p-Xylenes 40.4 1.0 ug/L 40.00 101 77-133 5 20 Methyl Butyl Ketone (2-Hexanone) 18.1 5.0 ug/L 20,00 91 64-137 3 20 Methyl Ethyl Ketone (2-Butanone) 20.0 5.0 ug/L 20.00 100 71-134 2 20 Methyl Isobutyl Ketone 20.0 5.0 ug/L 20.00 100 69-134 3 20 Methylene Chloride 18.6 1.0 ug/L 20.00 93 73-131 4 20 Methyl-tert-Butyl Ether 20.5 0.50 ug/L 20.00 103 68-135 0.4 20 Naphthalene 17.4 1.0 ug/L 20,00 87 64-136 1 20 n-Butylbenzene 18.2 1.0 ug/L 20.00 91 68-134 6 20 n-Propylbenzene 19.2 0.50 ug/L 20.00 96 72-132 6 20 o-Xylene 19.3 0.50 ug/L 20.00 96 78-128 5 20 sec-Butylbenzene 17.6 0.50 ug/L 20.00 88 71-131 6 20 Styrene 18.6 0.50 ug/L 20.00 93 78-129 4 20 tert-Butyl benzene 19.0 0.50 ug/L 20.00 95 70-132 6 20 Tetrachloroethylene 19.7 0.50 ug/L 20.00 99 80-129 4 20 Toluene 20.0 0.50 ug/L 20.00 100 76-131 5 20 trans- 1,2-Dichloroethylene 20.0 0.50 ug/L 20.00 100 76-135 4 20 trans-1,3-Dichloropropylene 21.1 0.60 ug/L 20,00 105 67-140 3 20 Trichloroethylene 20.4 0.50 ug/L 20.00 102 77-133 7 20 Trichlorofluoromelhane 20.6 0.50 ug/L 20.00 103 62-148 7 20 Vinyl acetate 21.0 2.0 ug/L 20.00 105 34-167 0.1 20 Vinyl chloride 20.4 0.50 ug/L 20.00 102 57-141 4 20 Surrogate:4-Bromotluorobenzene 48.7 ug/L 50,00 97 80-124 Surrogate. Dibromofluoromethane 48.4 ug/L 50.00 97 75-129 Surrogate. Toluene-d8 47.2 ug/L 50.00 94 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041625-0409 Page 12 of 19 P Analytical 8 Environmental Solutions R I S M I Pull -Service Level II QC Report 3/31/17 Anchor QEA of North Carolina, PLLC Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Project. Charlotte Metro Semivoiatile Organic Compounds by GCIMS - Quality Control Analyte Batch PX0471 - 3610C MS Blank (P7C0471-BLK1) _ 1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1-Melhylnaphthalene 2, 4, 5-Trich loroph enol 2,4, 6-Trichtoroph enol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-C hloroph en of 2-Methy[naphthalene 2-Methylphenol 2-Nitroaniline 2-Nitrophenol 3,3'-Dichlorobenzidine 3/4-Methylphenol 3-Nitroaniline 4, 6-D in itro-2-methylph enol 4-Bromophenyl phenyl ether 4-C hloro-3-methy (phenol 4-Chloroaniline 4-Chlorophenyl phenyl ether 4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline Anthracene Azobenzene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane B i s (2-C hloroethyl)eth er Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phlhalate Butyl benzyl phthalate Chrysene Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Reporting Spike Source Result Limit Units Level Result %REC %REC RPD Limits RPD Limit Notes Nreparea is Anaiyzeo: W/29/1 t BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL BRL 10 10 ug/L ug/L RECEIVED/NCflEQ/DWR BRL 10 ug/L BRL 10 ug/L JUL 0 g 2019 BRL 10 ug/L BRL 10 ug/L Water Quality BRL 10 ug/L Permitting Section BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 100 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/629-6364 -Fax: 7041526-0409 Page 13 Of 19 P R I S M I Full -Service Analytical R Environmental Solutions - ,F....,o. �,- Anchor QEA of North Carolina, PLLC Project. Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC1MS - Quality Control Level II QC Report 3/31 / 17 Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:00PM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7C0471 - 3510C MS Blank (P7C0471-BLK1) Prepared & Analyzed: 03/29/17 Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocyclopentadiene BRL 10 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate:2,4,6-Tribromophenot 96.5 ug/L 100.0 96 43-140 Surrogate:2-Fluorobiphenyl 34.6 ug/L 50,00 69 44-119 Surrogate:2-Fluorophenol 58.7 u91L 100.0 59 19-119 Surrogate: Nitrobenzene-d5 37.6 ug/L 50.00 75 44-120 Surrogate: Phenol-d5 36.4 ug/L 100.0 36 11-52 Surrogate: Terphenyl-d14 58.7 ug/L 50.00 117 50-134 This report should not be reproduced, except in its entirety without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240S43 - Charlotte, NC 28224-0543 77777-1 Phone: 704/629.6364- Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 14 of 19 FUll- Service 8I S VEnvironmental Solutitn5 :" �i" IAR/N1AtOgiF.R lkf. Anchor QEA of North Carolina, PLLC Attm Mike Falknor 231 Haywood Street Asheville, NC 28801 Project: Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7C0471 - 3510C MS Reporting Result Limit Units Level II QC Report 3/31 /17 Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:00PM Spike Source °/REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7C0471-BS1) Prepared: 03/29/17 Analyzed: 03/30/17 1,2,4-Trichlorobenzene 27.5 10 uglL 50.00 55 29-126 1,2-Dichlorobenzene 29.2 10 ug/L 50.00 58 32-111 1,3-Dichlorobenzene 28.3 10 ug/L 50.00 57 28-110 1,4-Dichlorobenzene 28.2 10 ug/L 50.00 56 29-112 1-Methylnaphthalene 33.6 10 ug/L 50.00 67 41-119 2,4,5-Trichlorophenol 41.0 10 ug/L 50.00 82 53-123 2,4,6-Trichloropheno[ 40.4 10 ug/L 50.00 81 50-125 2,4-Dichlorophenol 34.3 10 ug/L 50.00 69 47-121 2,4-Dimethylphenol 40.7 10 ug/L 50.00 81 31-124 2,4-Dinitrophenol 73.4 10 ug/L 50.00 147 23-143 L1 2,4-Dinitrotoluene 58.0 10 ug/L 50.00 116 57-128 2,6-Dinitrotoluene 54.4 10 ug/L 50.00 109 57-124 2-Chloronaphthalene 37.1 10 ug/L 50.00 74 40-116 2-Chlorophenol 36.9 10 ug/L 50.00 74 38-117 2-Methylnaphthalene 32.1 10 ug/L 50.00 64 40-121 2-Methylphenol 35.2 10 ug/L 50.00 70 30-117 2-Nitroanifine 42.8 10 ug/L 50.00 86 55-127 2-Nitrophenol 38.8 10 ug/L 50.00 78 47-123 3,3'-Dichlorobenzidine 51.1 10 ug/L 50.00 102 27-129 3/4-Methylphenol 28.1 10 ug/L 50.00 56 29-110 3-Nitroaniline 43.6 10 ug/L 50,00 87 41-128 4,6- Din itro-2-methylphenol 63.8 10 ug/L 50.00 128 44-137 4-Bromophenyl phenyl ether 39.7 10 ug/L 50.00 79 55-124 4-Chloro-3-methylphenol 36.6 10 ug/L 50.00 73 52-119 4-Chloroaniline 31.3 10 ug/L 50.00 63 33-117 4-Chlorophenyl phenyl ether 37.7 10 ug/L 50.00 75 53-121 4-Nitroaniline 37.9 10 ug/L 50.00 76 45-135 4-NitrophenDl 20.0 10 ug/L 50,00 40 10-77 Acenaphthene 41.0 10 ug/L 50,00 82 47-122 Acenaphthylene 39.8 10 ug/L 50.00 80 41-130 Aniline 44.0 10 ug/L 50.00 88 12-197 Anthracene 45.7 10 ug/L 50.00 91 57-123 Azobenzene 43.4 10 ug/L 50.00 87 61-116 Benzo(a)anthracene 45,9 10 ug/L 50.00 92 58-125 Benzo(a)pyrene 43.5 10 ug/L 50.00 87 54-125 Benzo(b)fluoranthene 43.8 10 ug/L 50.00 88 53-131 Benzo(g,h,i)perylene 40.2 10 ug/L 50,00 80 50-134 Benzo(k)fluoranthene 43.4 10 ug/L 50.00 87 57-129 Benzoic Acid 9.04 100 ug/L 50.00 18 10-125 J Benzyl alcohol 32.6 10 ug/L 50.00 65 31-112 bis(2-Chloroethoxy)methane 31.6 10 ug/L 50.00 63 48-120 Bis(2-Chloroethyl)ether 35.2 10 ug/L 50.00 70 43-116 Sis(2-chloroisopropyl)ether 31.6 10 ug/L 50.00 63 37-130 6is(2-Ethylhexyl)phthalate 48.2 10 ug/L 50.00 96 55-135 Butyl benzyl phthalate 45.1 10 ug/L 50.00 90 53-134 Chrysene 47.0 10 ug/L 50.00 94 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364 - Toll Free Number: 1-8001529-6364 -Fax: 7041626-0409 Page 15 of 1971 - Fun -Service Analytical Envromnal SStubionr Level II QC Report 3/31 /17 Anchor QEA of North Carolina, PLLC Project. Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7C0471 - 3510C MS Reporting Result Limit Units Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7C0471-BSI) Prepared. 03/29/17 Analyzed: 03/30/17 Di ben zo(a,h)anth racene 43.3 10 ug/L 50,00 87 51-134 Dibenzoturan 41.9 10 ug/L 50.00 84 53-118 Diethyl phthalate 42.2 10 ug/L 50.00 84 56-125 Dimethyl phthalate 42.3 10 ug/L 50.00 85 45-127 Di-n-butyl phthalate 43.2 10 ug/L 50.00 86 59-127 Dr-n-octyl phthalate 47.0 10 ug/L 50.00 94 51-140 Fluoranihene 44.5 10 ug/L 50,00 89 57-128 Fluorene 42.1 10 ug/L 50.00 84 52-124 Hexachlorobenzene 42.0 10 ug/L 50.00 84 53-125 Hexachlorobutadiene 25.9 10 ug/L 50.00 52 22-124 Hexachlorocyclopentadiene 11.0 10 ug/L 50.00 22 32-117 L Hexachloroethane 25.4 10 ug/L 50.00 51 21-115 Indeno(1,2,3-cd)pyrene 43.7 10 ug/L 50.00 87 52-134 Isophorone 33.9 10 ug/L 50.00 68 42-124 Naphthalene 33,1 10 ug/L 50.00 66 40-121 Nitrobenzene 34.2 10 ug/L 50.00 68 45-121 N-Nitroso-di-n-propylamine 32.5 10 ug/L 50.00 65 49-119 N-Nitrosodiphenylamine 52.4 10 ug/L 50.00 105 51-123 Pentachlorophenol 63.2 10 ug/L 50.00 126 35-138 Phenanlhrene 44.9 10 ug/L 50.00 90 59-120 Phenol 16.3 10 ug/L 50.00 33 12-58 Pyrene 45.8 10 ug/L 50.00 92 57-126 Surrogate:2,4,6-Tribromophenol 103 ug/L 100.0 103 43-140 Surrogate:2-Fluorobiphenyl 37.6 ug/L 50.00 75 44-119 Surrogate. 2-Fluorophenol 50.6 ug/L 100.0 51 19-119 Surrogate: Nitrobenzene-dS 35.2 ug/L 50.00 70 44-120 Surrogate Phenol-d5 30.8 ug/L 100.0 31 11-52 Surrogate Terphenyl-d14 51.1 ug/L 50.00 102 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041625-0409 Page 16 of 19 Full al 'PRISM , ■ I `- M ( Environmental Service al Solutions ,1 �- -�.'!1 Environmental Solutions Level II QC Report 3/31 /17 Anchor QEA of North Carolina, PLLC Attn. Mike Falknor 231 Haywood Street Asheville, NC 28801 Project Charlotte Metro Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7C0471 - 3510C MS Reporting Result Limit Units Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P7C0471-BSD1) Prepared &Analyzed: 03/29/17 1,2,4-Trichlorobenzene 27.0 10 ug/L 50.00 54 29-126 2 20 1,2-Dichlorobenzene 29.1 10 ug/L 50.00 58 32-111 0.3 20 1,3-Dichlorobenzene 27.7 10 ug/L 50.00 55 28-110 2 20 1,4-Dichlorobenzene 27.6 10 ug/L 50.00 55 29-112 2 20 1-Methylnaphthalene 35.3 10 ug/L 50.00 71 41-119 5 20 2,4,5-Trichlorophenol 44.0 10 ug/L 50.00 88 53-123 7 20 2,4,6-Trichlorophenol 45.9 10 ug1L 50.00 92 50-125 13 20 2,4-Dichlorophenol 36.9 10 ug/L 50.00 74 47-121 7 20 2,4-Dimethylphenol 45.7 10 ug/L 50,00 91 31-124 12 20 2,4-Di nitro phenol 71.3 10 ug/L 50.00 143 23-143 3 20 2,4-Dinitrotoluene 63.8 10 ug/L 50.00 128 57-128 9 20 2,6-Dinitrotoluene 58.6 10 ug/L 50.00 117 57-124 8 20 2-Chloronaphthalene 39.8 10 ug/L 50.00 80 40-116 7 20 2-Chlorophenol 39.8 10 ug/L 50.00 80 38-117 7 20 2-Methylnaphthalene 33.1 10 ug/L 50.00 66 40-121 3 20 2-Methylphenol 39.8 10 ug/L 50.00 80 30-117 12 20 2-Nitroaniline 46.1 10 ug/L 50.00 92 55-127 8 20 2-Nitrophenol 40.9 10 ug/L 50.00 82 47-123 5 20 3,T-Dichlorobenzidine 56.4 10 ug1L 50.00 113 27-129 10 20 3/4-Methylphenol 32.2 10 ug/L 50.00 64 29-110 13 20 3-Nitroaniline 47.6 10 ug/L 50.00 95 41-128 9 20 4,6-Dinitro-2-methylphenol 64.6 10 ug/L 50.00 129 44-137 1 20 4-Bromophenyl phenyl ether 43.8 10 ug/L 50.00 88 55-124 10 20 4-Chloro-3-melhylphenol 40.0 10 ug/L 50.00 80 52-119 9 20 4-Chloroaniline 35.1 10 ug/L 50.00 70 33-117 11 20 4-Chlorophenyl phenyl ether 41.7 10 ug/L 50.00 83 53-121 10 20 4-Nitroaniline 43.2 10 ug/L 50.00 86 45-135 13 20 4-Nitrophenol 20.5 10 ug/L 50.00 41 10-77 2 20 Acenaphthene 45.1 10 ug/L 50.00 9D 47-122 10 20 Acenaphthylene 44.3 10 ug/L 50.00 89 41-130 11 20 Aniline 51.2 10 ug/L 50.00 102 12-197 15 20 Anthracene 49.2 10 ug/L 50.00 98 57-123 8 20 Azobenzene 48.2 10 ug/L 50.00 96 61-116 10 20 Benzo(a)anthracene 50.6 10 ug/L 50.00 101 58-125 10 20 Benzo(a)pyrene 48.5 10 ug/L 50.00 97 54-128 11 20 Benzo(b)fluoranthene 47.5 10 ug/L 50.00 95 53-131 8 20 Benzo(g,hJ)perylene 45.1 10 ug/L 50,00 90 50-134 12 20 Benzo(k)fluoranthene 48.8 10 ug/L 50.00 98 57-129 12 20 Benzoic Acid 8.95 100 ug/L 50.00 18 10-125 1 20 J Benzyl alcohol 36.7 10 ug/L 50.00 73 31-112 12 20 bis(2-Chloroethoxy)methane 35.8 10 ug/L 50.00 72 48-120 12 20 Bis(2-Chloroethyt)ether 38.8 10 ug/L 50.00 78 43-118 10 20 Bis(2-chloroisopropyl)ether 35.8 10 ug/L 50.00 72 37-130 12 20 Bis(2-Ethylhexyl)phihalate 55.0 10 ug/L 50.00 110 55-135 13 20 Butyl benzyl phthalate 51.9 10 ug/L 50.00 104 53-134 14 20 Chrysene 52.2 10 ug/L 50.00 104 59-123 10 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/62"409 Page 17 of 1 ✓ 1 P R I S M I Environmental Full -Service al Solution 8 z� Fa2' Environmental Solutions '�Fc ""usonnron�ct u+:. Anchor QEA of North Carolina, PLLC Project: Charlotte Metro Attn: Mike Falknor 231 Haywood Street Asheville, NC 28801 Semivolatile Organic Compounds by GC/MS - Quality Control Level 11 QC Report 3131 /17 Prism Work Order: 7030450 Time Submitted: 3/29/2017 2:55:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7CO471 - 3610C MS LCS Dup (P7C0471-BSD1) Prepared & Analyzed: 03/29/17 Dibenzo(a,h)anthracene 48.7 10 ug/L 50.00 97 51-134 12 20 Dibenzoturan 45,9 10 ug/L 50.00 92 53-116 9 20 Diethyl phthatate 46.6 10 ug/L 50.00 93 56-125 10 20 Dimethyl phthalate 46.4 10 ug/L 50.00 93 45-127 9 20 Di-n-butyl phthalate 48.3 10 ug/L 50.00 97 59-127 11 20 Di-n-octyl phthalate 53.3 10 ug/L 50.00 107 51-140 13 20 Fluoranthene 48.8 10 ug/L 50.00 98 57-128 9 20 Fluorene 46.4 10 ug/L 50.00 93 52-124 10 20 Hexachlorobenzene 45.5 10 ug/L 50.00 91 53-125 8 20 Hexachlorobutadiene 25.3 10 ug/L 50.00 51 22-124 3 20 Hexachlorocyclopentadiene 11.4 10 ugtL 50.00 23 32-117 3 20 L Hexachloroethane 25.1 10 ug/L 50.00 50 21-115 D.8 20 Indeno(1,2,3-cd)pyrene 49.7 10 uglL 50.00 99 52-134 13 20 Isophorone 38.5 10 ug/L 50.00 77 42-124 13 20 Naphthalene 34.2 10 ug/L 50.00 68 40-121 3 20 Nitrobenzene 36.5 10 ug/L 50.00 73 45-121 7 20 N-Ndroso-di-n-propylamine 38.7 10 ug/L 50.00 77 49-119 17 20 N-Nitrosodiphenylamine 58.5 10 ug/L 50.00 117 51-123 11 20 Pentachlorophenot 66.3 10 ug/L 50.00 133 35-138 5 20 Phenanthrene 48.4 10 ug/L 50.00 97 59-120 8 20 Phenol 17.9 10 ug/L 50.00 36 12-58 9 20 Pyrene 50.7 10 ug/L 50.00 101 57-126 10 20 Surrogate:2,4,6-Tdbromopheno1 110 u9/L 100.0 110 43.140 Surrogate:2-Fluorobiphenyl 41.4 ug/L 50.00 83 44-119 Surrogate:2-Fluorophenol 51.4 u91L 100.0 51 19-119 Surrogate: Nitrobenzene-d5 37.8 u91L 50.00 76 44-120 Surrogate: Phenol-ri5 33.8 ug/L 100.0 34 11-52 Surrogate: Terpheny4-d14 56.4 ug/L 50.00 113 50-134 Sample Extraction Data Prep Method: 3610C MS Lab Number Batch Initial Final Date/Time 7030450-01 P700471 940 mL 1 mL 03/30/17 7:50 Prep Method: 6030E Lab Number Batch Initial Final Datelrime 7030450-01 P7CD502 10 mL 10 mL 03/30/17 10:21 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/625-0409 Page 18 of 19 .-/ x•rf•+• •r: » ::•.v: •r: -._-::YL.f. ._..��.lfb,• v,,V` [ i�,:if r :i?'rr;.:'5 i;::::;rr::.�-.:;.:.::. �.r.•r: r•r.:.:.r.• !•rix::. ...-.,_.:isC+1.Ir!•!.f'SY..:_/.SL-•ll.:.:.•..:.. ,Ylf. CHAIN OF CUSTODY RECORD LAB USE ONLY ua�' ISfl A v'l Full -Service Analytical &Environmental Solutions PAGE OFpUOTE #TO ENSURE PROPER BILLING: Samples INTACT u rival? O LAuonATOn1ES INC Project Name: Y , 0 ROD *,ON W 777 449 S rin brook Road • Charlotte. NC 25217 Phone 7529 63t"a4 •Fax: 7041525 oaos Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) "Please PROPER PRE9�RNA7lVESkkddY .11 ATTACH any project speciflc reporting (OC LEVEL I If III IV) Rgc�oltiWWITNINNOLPtNG:-.TW3't- Client Company Name: �V1d1h.U-v— provisions and/or QC Requirements '' t1 Report To/Contact Name: Invoice To: VOiATILEScfl WLQIJT.HEApSRAGE?-':': -- Reporting Address: Address: PROPEKPONTAI S,t 7 TEMP. Therm:10: Observed: •C.I.Corr: . 'oC Phone: Fax (Yes) (No): Email Address: Purchase Order NoJBllling Reference Requested Due Date 01 Day �2 Days Q 3 Days Q 4 Days ❑ 5 Days TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL Cerdfication• NELAC DOD FL NC EDD Type: PDF,EXCeI`Other Site Location Name: Site Location Physical Address: "Working Days" ❑ 6-9 Days O Standard 10 days p Rush Work Must Be Pre -Approved Samples received after 14:00 will be processed next business day. Turnaround time is based on business days, excluding weekends and holidays. (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) SC OTHER NIA Water Chlorinated: YES+,,, NO_ Sample Iced Upon Collection: YES_ NO CLIENT SAMPLE DESCRIPTION DATE COLLECTED TIME COLLECTED MILITARY HOURS MATRIX (SOIL, WATER OR SLUDGE) SAMPLE CONTAINER PRTIVES - TIVES 'J ANALYSIS REQUESTED �V REMARKS F 1/ PRISM LAB ID NO. *TYPE NO. SIZE W l Z`t /SEESELOW ! , • • Sampler's Signature �• Sampled By (Print Name) U I ration Upon relinquish in this C aln of C d is your authorization for Prism to proceed with the analyses as requested above. Any changes must be 1 submitted in w t It Pris Pr jec anager. There will be charges for any changes after analyses have been initialized. •' PRISM USE NLY e lnq y. not Received By. (Signature to IlitarylHours Additional Comments: , Site.�lIThraf.Tilrls: Relinquished By. (Signature) Received By: (Signature) Date Site OepettYte'Time: Relinquished By: (Signature) Rece' d For Prom Lnhoratones y: Dow //�- ���-�---' 3' 9-I�% Mdethoor SNpment NOTE ALL SAMPLECOOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. ' f`CSC 70,16 Flotd'TecKFee: Mileage'. ' SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. D Fed Ex 0 UPS U Hand -delivered 0 Prism Field Service 0 Other (V 0 Y50 NPDES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER: ' ❑ NC El SC ❑ NC ❑ SC O NC ❑ SC ❑ I NC ❑ SC ❑ NC ❑ SC ❑ NC 0 SC'I O NC O SC ❑ NC 0 SC ❑ NC ❑ SC TERMS & CONDITIONS n n n I n n ❑ ❑ ❑ ❑ *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -tined Cap VOA = Volatile Organics Analysis (Zero Head Space) Case Narrative P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. NOVA Engineering & Environmental Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: CLT Metro Lab Submittal Date: 05/30/2019 Prism Work Order: 9050492 6/6/19 10:14 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a,j Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference Reviewed By Angela D. Overcash VP Laboratory Services 1 Samples for volatiles analysis received with headspace A Recovery is less than the lower limit due to lack of HCI to stabilize the Sb spike. (Samples are not digested.) All samples results are less than the MDL. No action taken. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken. LH High LCS recovery. Analyte not detected in the sample(s). No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Receipt Summary Full -Service Analytical & PRISMSample Environmental Solutions 06/06/2019 Prism Work Order: 9050492 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received MW#1 9050492-01 Water 05/30/19 11:20 05/30/19 14:55 MW#4 9050492-02 Water 05/30/19 13:30 05/30/19 14:55 MW#3 9050492-03 Water 05/30/19 14:35 05/30/19 14:55 Samples were received in good condition at 2.3 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 4P��R I S M Full -Service Analytical & �}": Environmental Solutions Summary of Detections O6/06/2019 Prism Work Order: 9050492 Prism ID Client ID Parameter Method Result Units 9050492-01 MW#1 Total Hardness *200.7 360 mg/L 9050492-01 MW#1 Calcium *200.7 97 mg/L 9050492-01 MW#1 Chromium '6010D 0.029 mg/L 9050492-01 MW#1 Magnesium *200.7 30 mg/L 9050492-01 MW#1 Nickel '6010D 0.014 mg/L 9050492-01 MW#1 cis- 1,2-Dichloroethylene 8260E 0.38 J ug/L 9050492-01 MW#1 Tetrachloroethylene 8260B 0.72 ug/L 9050492-02 MW#4 Nickel '6010D 0.013 mg/L 9050492-02 MW#4 Total Hardness *200.7 230 mg/L 9050492-02 MW#4 Calcium •200.7 53 mg/L 9050492-02 MW#4 Chromium '6010D 0.020 mg/L 9050492-02 MW#4 Copper *6010D 0.017 mg/L 9050492-02 MW#4 Magnesium *200.7 24 mg/L 9050492-02 MW#4 Nickel •6010D 0.020 mg/L 9050492-03 MW#3 Total Hardness •200.7 210 mg/L 9050492-03 MW#3 Calcium *200.7 44 mg/L 9050492-03 MW#3 Chromium *6010D 0.024 mg/L 9050492-03 MW#3 Copper *6010D 0.013 mg/L 9050492-03 MW#3 Lead *601OD 0.011 mg/L 9050492-03 MW#3 Magnesium *200.7 23 mg/L 9050492-03 MW#3 Zinc *601OD 0.045 mg/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/526-0409 PRISMFun -Service Analytical Environmental Solutions IARORATCRIES INC. Laboratory Report 06/06/2019 NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW##1 Attn: Alex Kuczero Prism Sample ID: 9050492-01 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 11:20 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Dissolved Metals Mercury BRL mg/L 0.00050 0.00016 1 *7470A 5/31/19 11:27 MMR P9E0529 Antimony BRL mg/L 0.020 0.014 1 *6010D 5/31/19 15:45 JAB P9E0531 Arsenic BRL mg/L 0.020 0.0060 1 *6010D 5/31/19 15:45 JAB P9E0531 Beryllium BRL mg/L 0.0020 0.0010 1 *6010D 5/31/19 15:45 JAB P9E0531 Cadmium BRL mg/L 0.0020 0.00040 1 *6010D 5/31/19 15:45 JAB P9E0531 Chromium BRL mg/L 0.010 0.0030 1 *6010D 5/31/19 15:45 JAB P9E0531 Copper BRL mg/L 0.010 0.0050 1 *6010D 5/31/19 15:45 JAB P9E0531 Lead BRL mg/L 0.0050 0.0039 1 *6010D 5/31/19 15:45 JAB P9E0531 Nickel BRL mg/L 0.010 0.00036 1 *6010D 5/31/19 15:45 JAB P9E0531 Selenium BRL mg/L 0.020 0.013 1 *6010D 5/31/19 15:45 JAB P9E0531 Silver BRL mg/L 0.0050 0.00090 1 *6010D 5/31/19 15:45 JAB P9E0531 Thallium BRL mg/L 0.020 0.0050 1 *6010D 5/31/19 15:45 JAB P9E0531 Zinc BRL mg/L 0.040 0.020 1 *6010D 5/31/19 15:45 JAB P9E0531 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.10 0.027 1 8081B 6/5/19 16:55 ZRC P9E0544 4,4'-DDE BRL ug/L 0.10 0.022 1 8081B 6/5/19 16:55 ZRC P9E0544 4,4'-DDT BRL ug/L 0.10 0.018 1 8081B 6/5/19 16:55 ZRC P9E0544 Aldrin BRL ug/L 0.052 0.016 1 8081B 6/5/19 16:55 ZRC P9E0544 alpha-BHC BRL ug/L 0.052 0.0065 1 8081B 5/5/19 16:55 ZRC P9E0544 cis -Chlordane BRL ug/L 0.10 0.019 1 8081B 5/5/19 16:55 ZRC P9E0544 beta-BHC BRL ug/L 0.052 0.011 1 8081B 6/5/19 16:55 ZRC P9E0544 Chlordane BRL ug/L 0.52 0.19 1 8081B 6/5/19 16:55 ZRC P9E0544 delta-BHC BRL ug/L 0.052 0.0085 1 8081B 6/5/19 16:55 ZRC P9E0544 Dieldrin BRL ug/L 0.052 0.014 1 8081B 615/19 16:55 ZRC P9E0544 Endosulfan I BRL ug/L 0.052 0.016 1 8081B 6/5/19 16:55 ZRC P9E0544 Endosulfan II BRL ug/L 0.052 0.012 1 8081B 6/5/19 16:55 ZRC P9E0544 Endosulfan Sulfate BRL ug/L 0.052 0.017 1 8081B 6/5/19 16:55 ZRC P9E0544 Endrin BRL ug/L 0.052 0.014 1 8081B 6/5/19 16:55 ZRC P9E0544 Endrin Aldehyde BRL ug/L 0.052 0.016 1 8081B 6/5/19 16:55 ZRC P9E0544 Endrin Ketone BRL ug/L 0.10 0.019 1 8081B 6/5/19 16:55 ZRC P9E0544 gamma-BHC BRL ug/L 0.052 0.0063 1 8081B 6/5/19 16:55 ZRC P9E0544 trans -Chlordane BRL ug/L 0.10 0.024 1 8081B 5/5/19 16:55 ZRC P9E0544 Heptachlor BRL ug/L 0.052 0.013 1 8081B 6/5/19 16:55 ZRC P9E0544 Heptachlor Epoxide BRL ug/L 0.10 0.023 1 8081B 6/5/19 16:55 ZRC P9E0544 Methoxychlor BRL ug/L 0.10 0.018 1 8081B 6/5/19 16:55 ZRC P9E0544 Toxaphene BRL ug/L 1.0 0.36 1 8081B 6/5/19 16:55 ZRC P9E0544 Surrogate Recovery Control Limits Decachlorobiphenyl 68 % 13-186 Tetrachloro-m-xylene 85 % 40-134 Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 11 3.1 1 8270D 5/31/19 16:27 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 /�.. Laboratory Report /PAR ISM Full -Service Analytical 8 Environmental Solutions 06/06/2019 -RATORIES INC. NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#1 Attn: Alex Kuczero Prism Sample ID: 9050492-01 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 11:20 Time Submitted: 05/30/19 14:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,2-Dichlorobenzene BRL ug/L 11 2.6 1 8270D 5/31/19 16:27 JMV P9E0534 1,3-Dichlorobenzene BRL ug/L 11 4.1 1 8270D 5/31/19 16:27 JMV P9E0534 1,4-Dichlorobenzene BRL ug/L 11 4.3 1 8270D 5/31/19 16:27 JMV P9E0534 1-Methylnaphthalene BRL ug/L 11 3.8 1 8270D 5/31/19 16:27 JMV P9E0534 2,4,5-Trichlorophenol BRL ug/L 21 3.8 1 8270D 5/31/19 16:27 JMV P9E0534 2,4,6-Trichlorophenol BRL ug/L 21 4.8 1 8270D 5/31/19 16:27 JMV P9E0534 2,4-Dichlorophenol BRL ug/L 11 2.8 1 8270D 5/31/19 16:27 JMV P9E0534 2,4-Dimethylphenol BRL ug/L 11 5.1 1 8270D 5/31/19 16:27 JMV P9E0534 2,4-Dinitrophenol BRL ug/L 53 12 1 8270D 5/31/19 16:27 JMV P9E0534 2,4-Dinitrotoluene BRL ug/L 11 4.4 1 8270D 5/31/19 16:27 JMV P9E0534 2,6-Dinitrotoluene BRL ug/L 21 4.1 1 8270D 5/31/19 16:27 JMV P9E0534 2-Chloronaphthalene BRL ug/L 21 4.9 1 8270D 5/31/19 16:27 JMV P9E0534 2-Chlorophenol BRL ug/L 11 2.9 1 8270D 5/31/19 16:27 JMV P9E0534 2-Methylnaphthalene BRL ug/L 11 4.4 1 8270D 5/31/19 16:27 JMV P9E0534 2-Methylphenol BRL ug/L 11 2.6 1 8270D 5/31/19 16:27 JMV P9E0534 2-Nitroaniline BRL ug/L 11 4.3 1 8270D 5/31/19 16:27 JMV P9E0534 2-Nitrophenol BRL ug/L 11 2.7 1 8270D 5131/19 16:27 JMV P9E0534 3,3'-Dichlorobenzidine BRL ug/L 11 4.1 1 8270D 5/31119 16:27 JMV P9E0534 3/4-Methylphenol BRL ug/L 11 2.6 1 8270D 5/31/19 16:27 JMV P9E0534 3-Nitroaniline BRL ug/L 11 4.0 1 8270D 5/31/19 16:27 JMV P9E0534 4,6-Dinitro-2-methylphenol BRL ug/L 53 12 1 8270D 5/31/19 16:27 JMV P9E0534 4-Bromophenyl phenyl ether BRL ug/L 21 4.6 1 8270D 5/31/19 16:27 JMV P9E0534 4-Chloro-3-methylphenol BRL ug/L 11 3.1 1 8270D 5131/19 16:27 JMV P9E0534 4-Chloroaniline BRL ug/L 11 3.7 1 8270D 5/31/19 16:27 JMV P9E0534 4-Chlorophenyl phenyl ether BRL ug/L 21 4.9 1 8270D 5/31/19 16:27 JMV P9E0534 4-Nitroaniline BRL ug/L 11 4.4 1 8270D 5/31/19 16:27 JMV P9E0534 4-Nitrophenol BRL ug/L 11 2.7 1 8270D 5/31/19 16:27 JMV P9E0534 Acenaphthene BRL ug/L 11 4.5 1 8270D 5/31/19 16:27 JMV P9E0534 Acenaphthylene BRL ug/L 21 4.6 1 8270D 5/31119 16:27 JMV P9E0534 Aniline BRL ug/L 53 12 1 8270D 5/31/19 16:27 JMV P9E0534 Anthracene BRL ug/L 11 4.8 1 8270D 5/31/19 16:27 JMV P9E0534 Azobenzene BRL ug/L 11 3.4 1 8270D 5/31/19 16:27 JMV P9E0534 Benzo(a)anthracene BRL ug/L 11 3.4 1 8270D 5/31/19 16:27 JMV P9E0534 Benzo(a)pyrene BRL ug/L 11 3.7 1 8270D 5/31/19 16:27 JMV P9E0534 Benzo(b)fluoranthene BRL ug/L 11 3.6 1 8270D 5/31/19 16:27 JMV P9E0534 Benzo(g,hJ)perylene BRL ug/L 11 3.8 1 8270D 5/31/19 16:27 JMV P9E0534 Benzo(k)fluoranthene BRL ug/L 11 2.8 1 8270D 5/31/19 16:27 JMV P9E0534 Benzoic Acid BRL ug/L 110 20 1 8270D 5/31/19 16:27 JMV P9E0534 Benzyl alcohol BRL ug/L 11 2.6 1 8270D 5/31/19 16:27 JMV P9E0534 bis(2-Chloroethoxy)methane BRL ug/L 11 4.0 1 8270D 5/31/19 16:27 JMV P9E0534 Bis(2-Chloroethyl)ether BRL ug/L 11 2.7 1 8270D 5/31119 16:27 JMV P9E0534 Bis(2-chloroisopropyl)ether BRL ug/L 11 2.9 1 8270D 5/31/19 16:27 JMV P9E0534 Bis(2-Ethylhexyl)phthalate BRL ug/L 11 3.9 1 8270D 5/31/19 16:27 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 P R I S M Laboratory Report Full -Service Analytical & Environmental Solutions 06/06/2019 LA-CIRIES INC. NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#1 Attn: Alex Kuczero Prism Sample ID: 9050492-01 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 11:20 Time Submitted: 05/30/19 14:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bromochloroacetonitrile BRL ug/L 11 1 8270D 5/31/19 16:27 JMV P9E0534 Butyl benzyl phthalate BRL ug/L 11 3.1 1 8270D 5/31/19 16:27 JMV P9E0534 Chrysene BRL ug/L 11 3.5 1 8270D 5/31/19 16:27 JMV P9E0534 Dibenzo(a,h)anthracene BRL ug/L 21 6.0 1 8270D 5/31/19 16:27 JMV P9E0534 Dibenzofuran BRL ug/L 21 4.4 1 8270D 5/31/19 16:27 JMV P9E0534 Diethyl phthalate BRL ug/L 21 4.4 1 8270D 5/31/19 16:27 JMV P9E0534 Dimethyl phthalate BRL ug/L 11 4.3 1 8270D 5/31/19 16:27 JMV P9E0534 Di-n-butyl phthalate BRL ug/L 11 4.5 1 8270D 5/31/19 16:27 JMV P9E0534 Di-n-octyl phthalate BRL ug/L 11 4.7 1 8270D 5/31/19 16:27 JMV P9E0534 Fluoranthene BRL ug/L 11 4.3 1 8270D 5/31/19 16:27 JMV P9E0534 Fluorene BRL ug/L 11 5.3 1 8270D 5/31/19 16:27 JMV P9E0534 Hexachlorobenzene BRL ug/L 21 4.1 1 8270D 5/31/19 16:27 JMV P9E0534 Hexachlorobutadiene BRL ug/L 21 4.7 1 8270D 5/31/19 16:27 JMV P9E0534 Hexachlorocyclopentadiene BRL ug/L 21 7.6 1 8270D 5/31/19 16:27 JMV P9E0534 Hexachloroethane BRL ug/L 11 3.9 1 8270D 5/31/19 16:27 JMV P9E0534 Indeno(1,2,3-cd)pyrene BRL ug/L 11 2.8 1 8270D 5/31/19 16:27 JMV P9E0534 Isophorone BRL ug/L 11 4.3 1 8270D 5/31/19 16:27 JMV P9E0534 Naphthalene BRL ug/L 11 4.3 1 8270D 5/31119 16:27 JMV P9E0534 Nitrobenzene BRL ug/L 11 4.1 1 8270D 5/31/19 16:27 JMV P9E0534 N-Nitroso-di-n-propylamine BRL ug/L 21 3.4 1 8270D 5/31/19 16:27 JMV P9E0534 N-Nitrosodiphenylamine BRL ug/L 21 4.7 1 8270D 5/31/19 16:27 JMV P9E0534 Pentachlorophenol BRL ug/L 53 11 1 8270D 5/31/19 16:27 JMV P9E0534 Phenanthrene BRL ug/L 11 4.1 1 8270D 5/31/19 16:27 JMV P9E0534 Phenol BRL ug/L 11 1.5 1 8270D 5/31/19 16:27 JMV P9E0534 Pyrene BRL ug/L 11 3.7 1 8270D 5/31/19 16:27 JMV P9E0534 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 105 % 43-140 2-Fluorobiphenyl 111 % 44-119 2-Fluorophenol 62 % 19-119 Nitrobenzene-d5 101 % 44-120 Phenol-d5 42 % 11-52 Terphenyl-d14 113 % 50-134 Total Metals Mercury BRL mg/L 0.00050 0.00016 1 '7470A 5/31/19 12:13 MMR P9E0530 Total Hardness 360 mg/L 1.3 0.38 1 *200.7 5131/19 14:53 JAB (CALC] Antimony BRL mg/L 0.020 0.014 1 '6010D 5/31/19 16:52 JAB P9E0532 Arsenic BRL mg/L 0.020 0.0060 1 '6010D 5/31/19 16:52 JAB P9E0532 Beryllium BRL mg/L 0.0020 0.0010 1 '6010D 5/31/19 16:52 JAB P9E0532 Cadmium BRL mg/L 0.0020 0.00040 1 '6010D 5/31/19 16:52 JAB P9E0532 Calcium 97 mg/L 0.20 0.072 1 *200.7 5131119 14:53 JAB P9E0533 Chromium 0.029 mg/L 0.010 0.0030 1 '6010D 5/31/19 16:52 JAB P9E0532 Copper BRL mg/L 0.010 0.0050 1 '6010D 5/31/19 16:52 JAB P9E0532 Lead BRL mg/L 0.0050 0.0039 1 '6010D 5/31/19 16:52 JAB P9E0532 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report �. Full -Service Analytical 8 P R I S M Environmental Solutions 06/06/2019 IARORATORIE$ INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#1 Attn: Alex Kuczero Prism Sample ID: 9050492-01 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 11:20 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Magnesium 30 mg/L 0.20 0.049 1 •200.7 5/31/19 14:53 JAB P9E0533 Nickel 0.014 mg/L 0.010 0.00036 1 '6010D 6/31/19 16:52 JAB P9E0532 Selenium BRL mg/L 0.030 0.013 1 '6010D 5/31/19 16:52 JAB P9E0532 Silver BRL mg/L 0.0050 0.00090 1 '6010D 5/31/19 16:52 JAB P9E0532 Thallium BRL mg/L 0.020 0.0050 1 '6010D 5/31/19 16:52 JAB P9E0532 Zinc BRL mg/L 0.040 0.020 1 '6010D 5/31/19 16:52 JAB P9E0532 Volatile Organic Compounds by GC/MS 1 1. 1, 1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:23 KDM P9E0549 1,1,1-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 5/31/19 17:23 KDM P9E0549 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 5/31/19 17:23 KDM P9E0549 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:23 KDM P9E0549 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 5/31/19 17:23 KDM P9E0549 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 5/31/19 17:23 KDM P9E0549 1, 1 -Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 5/31/19 17:23 KDM P9E0549 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 5/31/19 17:23 KDM P9E0549 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 5/31/19 17:23 KDM P9E0549 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 5/31/19 17:23 KDM P9E0549 1,2,4-Tdmethylbenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:23 KDM P9E0549 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 5/31/19 17:23 KDM P9E0549 1,2-Dibromoethane BRL ug/L 0.50 0,051 1 8260E 5/31119 17:23 KDM P9E0549 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:23 KDM P9E0549 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:23 KDM P9E0549 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:23 KDM P9E0549 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:23 KDM P9E0549 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:23 KDM P9E0549 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 5/31/19 17:23 KDM P9E0549 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:23 KDM P9E0549 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 5/31/19 17:23 KDM P9E0549 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:23 KDM P9E0549 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:23 KDM P9E0549 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 5/31/19 17:23 KDM P9E0549 Acetone BRL ug/L 5.0 0.31 1 8260B 5/31/19 17:23 KDM P9E0549 Acrolein BRL ug/L 20 0.20 1 8260B 5/31/19 17:23 KDM P9E0549 Acrylonitrile BRL ug/L 20 0.20 1 8260B 5/31/19 17:23 KDM P9E0549 Benzene BRL ug/L 0.50 0.048 1 8260B 5/31/19 17:23 KDM P9E0549 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 5/31/19 17:23 KDM P9E0549 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 5/31/19 17:23 KDM P9E0549 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:23 KDM P9E0549 Bromoform BRL ug/L 1.0 0.040 1 8260B 5/31/19 17:23 KDM P9E0549 Bromomethane BRL ug/L 1.0 0.18 1 8260B 5/31/19 17:23 KDM P9E0549 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 5/31/19 17:23 KDM P9E0549 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:23 KDM P9E0549 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:23 KDM P9E0549 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report Full -Service Analytical 8 'C" Environmental Solutions R ISM UBOF RIES INC. 06/06/2019 NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#1 Attn: Alex Kuczero Prism Sample ID: 9050492-01 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 11:20 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chloroethane BRL ug/L 0.50 0.22 1 8260B 5131/19 17:23 KDM P9E0549 Chloroform BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:23 KDM P9E0549 Chloromethane BRL ug/L 0.50 0.079 1 8260B 5/31119 17:23 KDM P9E0549 cis-1,2-Dichloroethylene 0.38 J ug/L 0.60 0.056 1 8260B 5/31/19 17:23 KDM P9E0549 cis- 1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 5/31119 17:23 KDM P9E0549 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 5/31/19 17:23 KDM P9E0549 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 5/31/19 17:23 KDM P9E0549 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260B 5/31/19 17:23 KDM P9E0549 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 5/31119 17:23 KDM P9E0549 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 5/31/19 17:23 KDM P9E0549 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:23 KDM P9E0549 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:23 KDM P9E0549 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 5/31/19 17:23 KDM P9E0549 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 5/31/19 17:23 KDM P9E0549 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 5/31/19 17:23 KDM P9E0549 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 5/31119 17:23 KDM P9E0549 Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 5/31/19 17:23 KDM P9E0549 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 5/31/19 17:23 KDM P9E0549 Naphthalene BRL ug/L 1.0 0.19 1 8260B 5/31/19 17:23 KDM P9E0549 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 5/31119 17:23 KDM P9E0549 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 5/31/19 17:23 KDM P9E0549 o-Xylene BRL ug/L 0.50 0.044 1 8260B 5/31/19 17:23 KDM P9E0549 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:23 KDM P9E0549 Styrene BRL ug/L 0.50 0.047 1 8260B 5/31119 17:23 KDM P9E0549 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 5/31/19 17:23 KDM P9E0549 Tetrachloroethylene 0.72 ug/L 0.50 0.098 1 8260B 5/31/19 17:23 KDM P9E0549 Toluene BRL ug/L 0.50 0.044 1 8260B 5/31/19 17:23 KDM P9E0549 trans- 1, 2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 5/31/19 17:23 KDM P9E0549 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 5/31/19 17:23 KDM P9E0549 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 5/31/19 17:23 KDM P9E0549 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:23 KDM P9E0549 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 5/31/19 17:23 KDM P9E0549 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 5/31/19 17:23 KDM P9E0549 Xylenes, total BRL ug/L 1.5 0.15 1 8260B 5/31/19 17:23 KDM P9E0549 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 80-124 Dibromofluoromethane 97 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 P R I S M Laboratory Report Full -Service Analytical 8 Environmental Solutions 06/06/2019 -RATORIES INC. NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW/#4 Attn: Alex Kuczero Prism Sample ID: 9050492-02 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 13:30 Time Submitted: 05/30/19 14:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Dissolved Metals Mercury BRL mg/L 0.00050 0.00016 1 '7470A 5/31/19 11:38 MMR P9E0529 Antimony BRL mg/L 0.020 0.014 1 `6010D 5/31/19 16:08 JAB P9E0531 Arsenic BRL mg/L 0.020 0.0060 1 '6010D 5/31/19 16:08 JAB P9E0531 Beryllium BRL mg/L 0.0020 0.0010 1 '6010D 5/31/19 16:08 JAB P9E0531 Cadmium BRL mg/L 0.0020 0.00040 1 '6010D 5/31/19 16:08 JAB P9E0531 Chromium BRL mg/L 0.010 0.0030 1 '6010D 5/31/19 16:08 JAB P9E0531 Copper BRL mg/L 0.010 0.0050 1 '6010D 5/31/19 16:08 JAB P9E0531 Lead BRL mg/L 0.0050 0.0039 1 '6010D 5/31/19 16:08 JAB P9E0531 Nickel 0.013 mg/L 0.010 0.00036 1 •6010D 5131/19 16:08 JAB P9E0531 Selenium BRL mg/L 0.020 0.013 1 '6010D 5/31119 16:08 JAB P9E0531 Silver BRL mg/L 0.0050 0.00090 1 '6010D 5/31/19 16:08 JAB P9E0531 Thallium BRL mg/L 0.020 0.0050 1 '6010D 5/31/19 16:08 JAB P9E0531 Zinc BRL mg/L 0.040 0.020 1 '6010D 5/31/19 16:08 JAB P9E0531 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.11 0.028 1 8081 B 5/5/19 17:37 ZRC P9E0544 4,4'-DDE BRL ug/L 0.11 0.023 1 8081B 6/5/19 17:37 ZRC P9E0544 4,4'-DDT BRL ug/L 0.11 0.019 1 8081B 6/5/19 17:37 ZRC P9E0544 Aldrin BRL ug/L 0.053 0.016 1 8081B 6/5/19 17:37 ZRC P9E0544 alpha-BHC BRL ug/L 0.053 0.0066 1 8081B 6/5/19 17:37 ZRC P9E0544 cis -Chlordane BRL ug/L 0.11 0.020 1 8081B 6/5/19 17:37 ZRC P9E0544 beta-BHC BRL ug/L 0.053 0.012 1 8081B 6/5/19 17:37 ZRC P9E0544 Chlordane BRL ug/L 0.53 0.19 1 8081B 6/5/19 17:37 ZRC P9E0544 delta-BHC BRL ug/L 0.053 0.0086 1 8081B 6/5/19 17:37 ZRC P9E0544 Dieldrin BRL ug/L 0.053 0.014 1 8081B 6/5/19 17:37 ZRC P9E0544 Endosulfan I BRL ug/L 0.053 0.017 1 8081B 6/5/19 17:37 ZRC P9E0544 Endosulfan II BRL ug/L 0.053 0.013 1 8081B 6/5/19 17:37 ZRC P9E0544 Endosulfan Sulfate BRL ug/L 0.053 0.017 1 8081B 6/5/19 17:37 ZRC P9E0544 Endrin BRL ug/L 0.053 0.014 1 8081B 6/5/19 17:37 ZRC P9E0544 Endrin Aldehyde BRL ug/L 0.053 0.017 1 8081B 5/5/19 17:37 ZRC P9E0544 Endrin Ketone BRL ug/L 0.11 0.019 1 8081B 6/5/19 17:37 ZRC P9E0544 gamma-BHC BRL ug/L 0.053 0.0064 1 8081B 6/5/19 17:37 ZRC P9E0544 trans -Chlordane BRL ug/L 0.11 0.024 1 8081B 6/5119 17:37 ZRC P9E0544 Heptachlor BRL ug/L 0.053 0.014 1 8081B 6/5/19 17:37 ZRC P9E0544 Heptachlor Epoxide BRL ug/L 0.11 0.024 1 8081B 6/5/19 17:37 ZRC P9E0544 Methoxychlor BRL ug/L 0.11 0.019 1 8081B 6/5/19 17:37 ZRC P9E0544 Toxaphene BRL ug/L 1.1 0.37 1 8081B 6/5/19 17:37 ZRC P9E0544 Surrogate Recovery Control Limits Decachlorobiphenyl 63 % 13-186 Tetrachloro-m-xylene 100 % 40-134 Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL ug/L 10 3.0 1 8270D 5/31/19 16:50 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704152"409 P R I S M Laboratory Report Full -Service Analytical 6 Environmental Solutions 06/06/2019 -HATONIES, INC. NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW##4 Attn: Alex Kuczero Prism Sample ID: 9050492-02 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 13:30 Time Submitted: 05/30/19 14:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270D 5/31/19 16:50 JMV P9E0534 1,3-Dichlorobenzene BRL ug/L 10 4.0 1 8270D 5/31/19 16:50 JMV P9E0534 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270D 5/31/19 16:50 JMV P9E0534 1-Methylnaphthalene BRL ug/L 10 3.7 1 8270D 5/31/19 16:50 JMV P9E0534 2,4,5-Tdchlorophenol BRL ug/L 20 3.7 1 8270D 5/31/19 16:50 JMV P9E0534 2,4,6-Trichlorophenol BRL ug/L 20 4.6 1 8270D 5/31/19 16:50 JMV P9E0534 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270D 5/31/19 16:50 JMV P9E0534 2,4-Dimethylphenol BRL ug/L 10 5.0 1 8270D 5/31/19 16:50 JMV P9E0534 2,4-Dinitrophenol BRL ug/L 51 12 1 8270D 5/31119 16:50 JMV P9E0534 2,4-Dinitrotoluene BRL ug/L 10 4.3 1 8270D 5/31/19 16:50 JMV P9E0534 2,6-Dinitrotoluene BRL ug/L 20 4.0 1 8270D 5/31/19 16:50 JMV P9E0534 2-Chloronaphthalene BRL ug/L 20 4.8 1 8270D 5/31/19 16:50 JMV P9E0534 2-Chlorophenol BRL ug/L 10 2.8 1 8270D 5/31/19 16:50 JMV P9E0534 2-Methylnaphthalene BRL ug/L 10 4.3 1 8270D 5/31/19 16:50 JMV P9E0534 2-Methylphenol BRL ug/L 10 2.5 1 8270D 5/31/19 16:50 JMV P9E0534 2-Nitroaniline BRL ug/L 10 4.2 1 8270D 5/31/19 16:50 JMV P9E0534 2-Nitrophenol BRL ug/L 10 2.6 1 8270D 5/31/19 16:50 JMV P9E0534 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270D 5/31/19 16:50 JMV P9E0534 3/4-Methylphenol BRL ug/L 10 2.5 1 8270D 5/31/19 16:50 JMV P9E0534 3-Nitroaniline BRL ug/L 10 3.8 1 8270D 5/31/19 16:50 JMV P9E0534 4,6-Dinitro-2-methylphenol BRL ug/L 51 12 1 8270D 5/31/19 16:50 JMV P9E0534 4-Bromophenyl phenyl ether BRL ug/L 20 4.5 1 8270D 5/31/19 16:50 JMV P9E0534 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270D 5/31/19 16:50 JMV P9E0534 4-Chloroaniline BRL ug/L 10 3.6 1 8270D 5/31/19 16:50 JMV P9E0534 4-Chlorophenyl phenyl ether BRL ug/L 20 4.8 1 8270D 5/31119 16:50 JMV P9E0534 4-Nitroaniline BRL ug/L 10 4.2 1 8270D 5/31/19 16:50 JMV P9E0534 4-Nitrophenol BRL ug/L 10 2.7 1 8270D 5/31/19 16:50 JMV P9E0534 Acenaphthene BRL ug/L 10 4.3 1 8270D 5/31/19 16:50 JMV P9E0534 Acenaphthylene BRL ug/L 20 4.5 1 8270D 5131/19 16:50 JMV P9E0534 Aniline BRL ug/L 51 12 1 8270D 5/31/19 16:50 JMV P9E0534 Anthracene BRL ug/L 10 4.7 1 8270D 5/31/19 16:50 JMV P9E0534 Azobenzene BRL ug/L 10 3.3 1 8270D 5/31/19 16:50 JMV P9E0534 Benzo(a)anthracene BRL ug/L 10 3.3 1 8270D 5/31/19 16:50 JMV P9E0534 Benzo(a)pyrene BRL ug/L 10 3.5 1 8270D 5/31/19 16:50 JMV P9E0534 Benzo(b)fluoranthene BRL ug/L 10 3.5 1 8270D 5/31119 16:50 JMV P9E0534 Benzo(g,hJ)perylene BRL ug/L 10 3.7 1 8270D 5/31/19 16:50 JMV P9E0534 Benzo(k)fluoranthene BRL ug/L 10 2.7 1 8270D 5/31/19 16:50 JMV P9E0534 Benzoic Acid BRL ug/L 100 20 1 8270D 5/31/19 16:50 JMV P9E0534 Benzyl alcohol BRL ug/L 10 2.5 1 8270D 5/31/19 16:50 JMV P9E0534 bis(2-Chloroethoxy)methane BRL ug/L 10 3.9 1 8270D 5/31/19 16:50 JMV P9E0534 Bis(2-Chloroethyl)ether BRL ug/L 10 2.7 1 8270D 5/31/19 16:50 JMV P9E0534 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270D 5/31/19 16:50 JMV P9E0534 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 3.8 1 8270D 5/31/19 16:50 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 P R I S M Laboratory Report Full -Service Analytical 8 Environmental Solutions 06/06/2019 IARO ORIE$ INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW##4 Attn: Alex Kuczero Prism Sample ID: 9050492-02 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 13:30 Time Submitted: 05/30/19 14:55 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Bromochloroacetonitrile BRL ug/L 10 1 8270D 5/31/19 16:50 JMV P9E0534 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270D 5/31/19 16:50 JMV P9E0534 Chrysene BRL ug/L 10 3.3 1 8270D 5/31/19 16:50 JMV P9E0534 Dibenzo(a,h)anthracene BRL ug/L 20 5.8 1 8270D 5/31/19 16:50 JMV P9E0534 Dibenzofuran BRL ug/L 20 4.3 1 8270D 5/31/19 16:50 JMV P9E0534 Diethyl phthalate BRL ug/L 20 4.3 1 8270D 5/31/19 16:50 JMV P9E0534 Dimethyl phthalate BRL ug/L 10 4.1 1 8270D 5/31/19 16:50 JMV P9E0534 Di-n-butyl phthalate BRL ug/L 10 4.4 1 8270D 5131/19 16:50 JMV P9E0534 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270D 5/31/19 16:50 JMV P9E0534 Fluoranthene BRL ug/L 10 4.1 1 8270D 5/31/19 16:50 JMV P9E0534 Fluorene BRL ug/L 10 5.1 1 8270D 5/31/19 16:50 JMV P9E0534 Hexachlorobenzene BRL ug/L 20 4.0 1 8270D 5/31/19 16:50 JMV P9E0534 Hexachlorobutadiene BRL ug/L 20 4.6 1 8270D 5/31/19 16:50 JMV P9E0534 Hexachlorocyclopentadiene BRL ug/L 20 7.4 1 8270D 5/31/19 16:50 JMV P9E0534 Hexachloroethane BRL ug/L 10 3.8 1 8270D 5/31/19 16:50 JMV P9E0534 Indeno(1,2,3-cd)pyrene BRL ug/L 10 2.7 1 8270D 5/31/19 16:50 JMV P9E0534 Isophorone BRL ug/L 10 4.2 1 8270D 5/31/19 16:50 JMV P9E0534 Naphthalene BRL ug/L 10 4.2 1 8270D 5/31/19 16:50 JMV P9E0534 Nitrobenzene BRL ug/L 10 3.9 1 8270D 5/31/19 16:50 JMV P9E0534 N-Nitroso-di-n-propylamine BRL ug/L 20 3.3 1 8270D 5/31/19 16:50 JMV P9E0534 N-Nitrosodiphenylamine BRL ug/L 20 4.5 1 8270D 5/31/19 16:50 JMV P9E0534 Pentachlorophenol BRL ug/L 51 11 1 8270D 5/31/19 16:50 JMV P9E0534 Phenanthrene BRL ug/L 10 4.0 1 8270D 5/31/19 16:50 JMV P9E0534 Phenol BRL ug/L 10 1.4 1 8270D 5/31/19 16:50 JMV P9E0534 Pyrene BRL ug/L 10 3.6 1 8270D 5/31/19 16:50 JMV P9E0534 Surrogate Recovery Control Limits 2,4,6-Tdbromophenol 104 % 43-140 2-Fluorobiphenyl 111 % 44-119 2-Fluorophenol 60 % 19-119 Nitrobenzene-d5 101 % 44-120 Phenol-d5 42 % 11-52 Terphenyl-d14 111 % 50-134 Total Metals Mercury BRL mg/L 0.00050 0.00016 1 *7470A 5/31/19 12:16 MMR P9E0530 Total Hardness 230 mg/L 1.3 0.38 1 *200.7 5/31/19 15:01 JAB [CALC] Antimony BRL mg/L 0.020 0.014 1 *6010D 5/31/19 17:16 JAB P9E0532 Arsenic BRL mg/L 0.020 0.0060 1 *6010D 5/31/19 17:16 JAB P9E0532 Beryllium BRL mg/L 0.0020 0.0010 1 *6010D 5/31/19 17:16 JAB P9E0532 Cadmium BRL mg/L 0.0020 0.00040 1 *6010D 5/31/19 17:16 JAB P9E0532 Calcium 53 mg/L 0.20 0.072 1 *200.7 5/31/19 15:01 JAB P9E0533 Chromium 0.020 mg/L 0.010 0.0030 1 *6010D 5/31119 17:16 JAB P9E0532 Copper 0.017 mg/L 0.010 0.0050 1 *6010D 5/31/19 17:16 JAB P9E0532 Lead BRL mg/L 0.0050 0.0039 1 *6010D 5/31/19 17:16 JAB P9E0532 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Laboratory Report �P R ISM Full -Service Analytical 8 Environmental Solutions 06/06/2019 LABORATORIES ING NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#4 Attn: Alex Kuczero Prism Sample ID: 9050492-02 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 13:30 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Magnesium 24 mg/L 0.20 0.049 1 •200.7 5/31/19 15:01 JAB P9E0533 Nickel 0.020 mg/L 0.010 0.00036 1 `6010D 5131/19 17:16 JAB P9E0532 Selenium BRL mg/L 0.030 0.013 1 `6010D 5/31/19 17:16 JAB P9E0532 Silver BRL mg/L 0.0050 0.00090 1 '6010D 5/31/19 17:16 JAB P9E0532 Thallium BRL mg/L 0.020 0.0050 1 '6010D 5/31/19 17:16 JAB P9E0532 Zinc BRL mg/L 0.040 0.020 1 '6010D 5/31/19 17:16 JAB P9E0532 Volatile Organic Compounds by GC/MS 1 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:49 KDM P9E0549 1, 1, 1 -Trichloroethane BRL ug/L 0.50 0.061 1 8260B 5/31/19 17:49 KDM P9E0549 1, 1, 2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 5/31/19 17:49 KDM P9E0549 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:49 KDM P9E0549 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 5/31/19 17:49 KDM P9E0549 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 5/31119 17:49 KDM P9E0549 1, 1 -Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 5/31/19 17:49 KDM P9E0549 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 5/31/19 17:49 KDM P9E0549 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 5/31/19 17:49 KDM P9E0549 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 8260B 5/31119 17:49 KDM P9E0549 1,2,4-Tdmethylbenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:49 KDM P9E0549 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 5/31/19 17:49 KDM P9E0549 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 5/31/19 17:49 KDM P9E0549 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:49 KDM P9E0549 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:49 KDM P9E0549 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:49 KDM P9E0549 1,3,5-Tdmethylbenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:49 KDM P9E0549 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:49 KDM P9E0549 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 5/31/19 17:49 KDM P9E0549 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:49 KDM P9E0549 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 5/31/19 17:49 KDM P9E0549 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 5/31/19 17:49 KDM P9E0549 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:49 KDM P9E0549 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 5/31/19 17:49 KDM P9E0549 Acetone BRL ug/L 5.0 0.31 1 8260B 5/31/19 17:49 KDM P9E0549 Acrolein BRL ug/L 20 0.20 1 8260B 5/31/19 17:49 KDM P9E0549 Acrylonitrile BRL ug/L 20 0.20 1 8260B 5/31/19 17:49 KDM P9E0549 Benzene BRL ug/L 0.50 0.048 1 8260B 5/31/19 17:49 KDM P9E0549 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 5/31/19 17:49 KDM P9E0549 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 5/31/19 17:49 KDM P9E0549 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:49 KDM P9E0549 Bromoform BRL ug/L 1.0 0.040 1 8260B 5/31/19 17:49 KDM P9E0549 Bromomethane BRL ug/L 1.0 0.18 1 8260B 5/31/19 17:49 KDM P9E0549 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 5/31/19 17:49 KDM P9E0549 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 5/31/19 17:49 KDM P9E0549 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:49 KDM P9E0549 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 fiP R I S M FullService Analytical 8 Laboratory Report Environmental Solutions 06/06/2019 VARORMTORIE$ INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#4 Attn: Alex Kuczero Prism Sample ID: 9050492-02 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 13:30 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chloroethane BRL ug/L 0.50 0.22 1 8260B 5131/19 17:49 KDM P9E0549 Chloroform BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:49 KDM P9E0549 Chloromethane BRL ug/L 0.50 0.079 1 8260B 5131/19 17:49 KDM P9E0549 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 5131119 17:49 KDM P9E0549 cis- 1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 5/31/19 17:49 KDM P9E0549 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 5/31/19 17:49 KDM P9E0549 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 5/31/19 17:49 KDM P9E0549 Dichlorodifluoromethane BRL ug/L 5.0 0.11 1 8260B 5/31/19 17:49 KDM P9E0549 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 5/31/19 17:49 KDM P9E0549 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 5/31/19 17:49 KDM P9E0549 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 5/31/19 17:49 KDM P9E0549 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 5/31/19 17:49 KDM P9E0549 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 5/31/19 17:49 KDM P9E0549 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 5/31/19 17:49 KDM P9E0549 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 5/31/19 17:49 KDM PgE0549 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 5/31/19 17:49 KDM P9E0549 Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 5/31/19 17:49 KDM P9E0549 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 5/31/19 17:49 KDM P9E0549 Naphthalene BRL ug/L 1.0 0.19 1 8260B 5/31/19 17:49 KDM P9E0549 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 5131/19 17:49 KDM P9E0549 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 5/31/19 17:49 KDM P9E0549 o-Xylene BRL ug/L 0.50 0.044 1 8260B 5/31/19 17:49 KDM P9E0549 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 17:49 KDM P9E0549 Styrene BRL ug/L 0.50 0.047 1 8260B 5/31/19 17:49 KDM P9E0549 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 5/31/19 17:49 KDM P9E0549 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 5131/19 17:49 KDM P9E0549 Toluene BRL ug/L 0.50 0.044 1 8260B 5/31/19 17:49 KDM P9E0549 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 5/31119 17:49 KDM P9E0549 trans- 1, 3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 5/31/19 17:49 KDM P9E0549 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 5/31/19 17:49 KDM P9E0549 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 5/31/19 17:49 KDM P9E0549 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 5/31/19 17:49 KDM P9E0549 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 5/31119 17:49 KDM P9E0549 Xylenes, total BRL ug/L 1.5 0.15 1 8260B 5/31/19 17:49 KDM P9E0549 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 80-124 Dibromofluoromethane 96 % 75-129 Toluene-d8 98 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 ,A%IP. R ISM Fun -Service u8 Laboratory Report Environmentalal SolSolutiotio ns 06/06/2019 I.A90RATCRIES. INC. NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#3 Attn: Alex Kuczero Prism Sample ID: 9050492-03 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 14:35 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Dissolved Metals Mercury BRL mg/L 0.00050 0.00016 1 *7470A 5/31/19 11:42 MMR P9E0529 Antimony BRL mg/L 0.020 0.014 1 *6010D 5/31/19 16:16 JAB P9E0531 Arsenic BRL mg/L 0.020 0.0060 1 *6010D 5/31/19 16:16 JAB P9E0531 Beryllium BRL mg/L 0.0020 0.0010 1 *6010D 5/31/19 16:16 JAB P9E0531 Cadmium BRL mg/L 0.0020 0.00040 1 *6010D 5/31/19 16:16 JAB P9E0531 Chromium BRL mg/L 0.010 0.0030 1 *6010D 5131/19 16:16 JAB P9E0531 Copper BRL mg/L 0.010 0.0050 1 *6010D 5/31/19 16:16 JAB P9E0531 Lead BRL mg/L 0.0050 0.0039 1 *6010D 5/31/19 16:16 JAB P9E0531 Nickel BRL mg/L 0.010 0.00036 1 *6010D 5/31/19 16:16 JAB P9E0531 Selenium BRL mg/L 0.020 0.013 1 *6010D 5/31/19 16:16 JAB P9E0531 Silver BRL mg/L 0.0050 0.00090 1 *6010D 5/31/19 16:16 JAB P9E0531 Thallium BRL mg/L 0.020 0.0050 1 *6010D 5/31/19 16:16 JAB P9E0531 Zinc BRL mg/L 0.040 0.020 1 *6010D 5/31/19 16:16 JAB P9E0531 Organochlorine Pesticides by GC/ECD 4,4'-DDD BRL ug/L 0.10 0.027 1 8081B 6/5/19 18:20 ZRC P9E0544 4,4'-DDE BRL ug/L 0.10 0.022 1 8081B 6/5/19 18:20 ZRC P9E0544 4,4'-DDT BRL ug/L 0.10 0.018 1 8081B 6/5/19 18:20 ZRC P9E0544 Aldrin BRL ug/L 0.051 0.016 1 8081B 6/5/19 18:20 ZRC P9E0544 alpha-BHC BRL ug/L 0.051 0.0064 1 8081B 6/5/19 18:20 ZRC P9E0544 cis -Chlordane BRL ug/L 0.10 0.019 1 8081B 6/5/19 18:20 ZRC P9E0544 beta-BHC BRL ug/L 0.051 0.011 1 8081B 6/5/19 18:20 ZRC P9E0544 Chlordane BRL ug/L 0.51 0.18 1 8081B 6/5/19 18:20 ZRC P9E0544 delta-BHC BRL ug/L 0.051 0.0084 1 8081B 6/5/19 18:20 ZRC P9E0544 Dieldrin BRL ug/L 0.051 0.014 1 8081B 6/5/19 18:20 ZRC P9E0544 Endosulfan I BRL ug/L 0.051 0.016 1 8081B 6/5/19 18:20 ZRC P9E0544 Endosulfan II BRL ug/L 0.051 0.012 1 8081B 6/5/19 18:20 ZRC P9E0544 Endosulfan Sulfate BRL ug/L 0.051 0.017 1 8081B 6/5/19 18:20 ZRC P9E0544 Endrin BRL ug/L 0.051 0.014 1 8081B 6/5/19 18:20 ZRC P9E0544 Endrin Aldehyde BRL ug/L 0.051 0.016 1 8081B 6/5/19 18:20 ZRC P9E0544 Endrin Ketone BRL ug/L 0.10 0.018 1 8081B 6/5/19 18:20 ZRC P9E0544 gamma-BHC BRL ug/L 0.051 0.0062 1 8081B 6/5/19 18:20 ZRC P9E0544 trans -Chlordane BRL ug/L 0.10 0.024 1 8081B 6/5/19 18:20 ZRC P9E0544 Heptachlor BRL ug/L 0.051 0.013 1 8081B 6/5/19 18:20 ZRC P9E0544 Heptachlor Epoxide BRL ug/L 0.10 0.023 1 8081B 6/5/19 18:20 ZRC P9E0544 Methoxychlor BRL ug/L 0.10 0.018 1 8081B 6/5/19 18:20 ZRC P9E0544 Toxaphene BRL ug/L 1.0 0.36 1 8081B 6/5/19 18:20 ZRC P9E0544 Surrogate Recovery Control Limits Decachlorobiphenyl 58 % 13-186 Tetrachloro-m-xylene 93 % 40-134 Semivolatile Organic Compounds by GC/MS 1,2,4-Tdchlorobenzene BRL ug/L 10 3.0 1 8270D 5/31/19 17:13 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Analytical & Environmental Solutions /RR I S M I Environmental LARD TONIES INC NOVA Engineering & Environmental Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Project: CLT Metro Sample Matrix: Water Laboratory Report 06/06/2019 Client Sample ID: MW#3 Prism Sample ID: 9050492-03 Prism Work Order: 9050492 Time Collected: 05/30/19 14:35 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,2-Dichlorobenzene BRL ug/L 10 2.5 1 8270D 5/31/19 17:13 JMV P9E0534 1,3-Dichlorobenzene BRL ug/L 10 3.9 1 8270D 5/31/19 17:13 JMV P9E0534 1,4-Dichlorobenzene BRL ug/L 10 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 1-Methylnaphthalene BRL ug/L 10 3.6 1 8270D 5/31/19 17:13 JMV P9E0534 2,4,5-Trichlorophenol BRL ug/L 20 3.7 1 8270D 5/31/19 17:13 JMV P9E0534 2,4,6-Trichlorophenol BRL ug/L 20 4.6 1 8270D 5/31/19 17:13 JMV P9E0534 2,4-Dichlorophenol BRL ug/L 10 2.7 1 8270D 5/31/19 17:13 JMV P9E0534 2,4-Dimethylphenol BRL ug/L 10 4.9 1 8270D 5/31/19 17:13 JMV P9E0534 2,4-Dinitrophenol BRL ug/L 51 12 1 8270D 5/31/19 17:13 JMV P9E0534 2,4-Dinitrotoluene BRL ug/L 10 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 2,6-Dinitrotoluene BRL ug/L 20 4.0 1 8270D 5/31/19 17:13 JMV P9E0534 2-Chloronaphthalene BRL ug/L 20 4.7 1 8270D 5/31/19 17:13 JMV P9E0534 2-Chlorophenol BRL ug/L 10 2.7 1 8270D 5/31/19 17:13 JMV P9E0534 2-Methylnaphthalene BRL ug/L 10 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 2-Methylphenol BRL ug/L 10 2.5 1 8270D 5/31/19 17:13 JMV P9E0534 2-Nitroaniline BRL ug/L 10 4.1 1 8270D 5/31/19 17:13 JMV P9E0534 2-Nitrophenol BRL ug/L 10 2.6 1 8270D 5/31/19 17:13 JMV P9E0534 3,3'-Dichlorobenzidine BRL ug/L 10 4.0 1 8270D 5/31/19 17:13 JMV P9E0534 3/4-Methylphenol BRL ug/L 10 2.5 1 8270D 5/31/19 17:13 JMV P9E0534 3-Nitroaniline BRL ug/L 10 3.8 1 8270D 5/31/19 17:13 JMV P9E0534 4,6-Dinitro-2-methylphenol BRL ug/L 51 11 1 8270D 5/31/19 17:13 JMV P9E0534 4-Bromophenyl phenyl ether BRL ug/L 20 4.4 1 8270D 5/31/19 17:13 JMV P9E0534 4-Chloro-3-methylphenol BRL ug/L 10 3.0 1 8270D 5/31/19 17:13 JMV P9E0534 4-Chloroaniline BRL ug/L 10 3.5 1 8270D 5/31/19 17:13 JMV P9E0534 4-Chlorophenyl phenyl ether BRL ug/L 20 4.7 1 8270D 5/31/19 17:13 JMV P9E0534 4-Nitroaniline BRL ug/L 10 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 4-Nitrophenol BRL ug/L 10 2.6 1 8270D 5/31/19 17:13 JMV P9E0534 Acenaphthene BRL ug/L 10 4.3 1 8270D 5/31119 17:13 JMV P9E0534 Acenaphthylene BRL ug/L 20 4.4 1 8270D 5/31/19 17:13 JMV P9E0534 Aniline BRL ug/L 51 12 1 8270D 5/31/19 17:13 JMV P9E0534 Anthracene BRL ug/L 10 4.6 1 8270D 5/31/19 17:13 JMV P9E0534 Azobenzene BRL ug/L 10 3.2 1 8270D 5/31/19 17:13 JMV P9E0534 Benzo(a)anthracene BRL ug/L 10 3.2 1 8270D 5/31/19 17:13 JMV P9E0534 Benzo(a)pyrene BRL ug/L 10 3.5 1 8270D 5/31/19 17:13 JMV P9E0534 Benzo(b)fluoranthene BRL ug/L 10 3.5 1 8270D 5/31/19 17:13 JMV P9E0534 Benzo(g,hJ)perylene BRL ug/L 10 3.6 1 8270D 5/31/19 17:13 JMV P9E0534 Benzo(k)fluoranthene BRL ug/L 10 2.7 1 8270D 5/31/19 17:13 JMV P9E0534 Benzoic Acid BRL ug/L 100 19 1 8270D 5/31/19 17:13 JMV P9E0534 Benzyl alcohol BRL ug/L 10 2.5 1 8270D 5/31/19 17:13 JMV P9E0534 bis(2-Chloroethoxy)methane BRL ug/L 10 3.8 1 8270D 5/31/19 17:13 JMV P9E0534 Bis(2-Chloroethyl)ether BRL ug/L 10 2.6 1 8270D 5/31/19 17:13 JMV P9E0534 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.8 1 8270D 5/31/19 17:13 JMV P9E0534 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 3.8 1 8270D 5/31/19 17:13 JMV P9E0534 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 �P R I S M Full -Service Analytical & Laboratory Report Environmental Solutions 06/06/2019 IARORATORIE$ INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#3 Attn: Alex Kuczero Prism Sample ID: 9050492-03 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 14:35 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Bromochloroacetonitrile BRL ug/L 10 1 8270D 5/31/19 17:13 JMV P9E0534 Butyl benzyl phthalate BRL ug/L 10 3.0 1 8270D 5/31/19 17:13 JMV P9E0534 Chrysene BRL ug/L 10 3.3 1 8270D 5/31119 17:13 JMV P9E0534 Dibenzo(a,h)anthracene BRL ug/L 20 5.7 1 8270D 5/31/19 17:13 JMV P9E0534 Dibenzofuran BRL ug/L 20 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 Diethyl phthalate BRL ug/L 20 4.2 1 8270D 5/31/19 17:13 JMV P9E0534 Dimethyl phthalate BRL ug/L 10 4.1 1 8270D 5/31/19 17:13 JMV P9E0534 Di-n-butyl phthalate BRL ug/L 10 4.4 1 8270D 5/31119 17:13 JMV P9E0534 Di-n-octyl phthalate BRL ug/L 10 4.6 1 8270D 5131/19 17:13 JMV P9E0534 Fluoranthene BRL ug/L 10 4.1 1 8270D 5/31/19 17:13 JMV P9E0534 Fluorene BRL ug/L 10 5.0 1 8270D 5/31/19 17:13 JMV P9E0534 Hexachlorobenzene BRL ug/L 20 3.9 1 8270D 5/31/19 17:13 JMV P9E0534 Hexachlorobutadiene BRL ug/L 20 4.5 1 8270D 5/31/19 17:13 JMV P9E0534 Hexachlorocyclopentadiene BRL ug/L 20 7.3 1 8270D 5/31/19 17:13 JMV P9E0534 Hexachlorcethane BRL ug/L 10 3.8 1 8270D 5/31/19 17:13 JMV P9E0534 Indeno(1,2,3-cd)pyrene BRL ug/L 10 2.6 1 8270D 5/31/19 17:13 JMV P9E0534 Isophorone BRL ug/L 10 4.1 1 8270D 5/31/19 17:13 JMV P9E0534 Naphthalene BRL ug/L 10 4.1 1 8270D 5/31/19 17:13 JMV P9E0534 Nitrobenzene BRL ug/L 10 3.9 1 8270D 5/31/19 17:13 JMV P9E0534 N-Nitroso-cli-n-propylamine BRL ug/L 20 3.3 1 8270D 5/31/19 17:13 JMV P9E0534 N-Nitrosodiphenylamine BRL ug/L 20 4.5 1 8270D 5/31/19 17:13 JMV P9E0534 Pentachlorophenol BRL ug/L 51 11 1 8270D 5/31/19 17:13 JMV P9E0534 Phenanthrene BRL ug/L 10 4.0 1 8270D 5/31/19 17:13 JMV P9E0534 Phenol BRL ug/L 10 1.4 1 8270D 5/31/19 17:13 JMV P9E0534 Pyrene BRL ug/L 10 3.5 1 8270D 5/31/19 17:13 JMV P9E0534 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 89 % 43-140 2-Fluorobiphenyl 100 % 44-119 2-Fluorophenol 54 % 19-119 Nitrobenzene-d5 90 % 44-120 Phenol-d5 36 % 11-52 Terphenyl-d14 104 % 50-134 Total Metals Mercury BRL mg/L 0.00050 0.00016 1 '7470A 5/31/19 12:20 MMR P9E0530 Total Hardness 210 mg/L 1.3 0.38 1 *200.7 5/31/19 15:09 JAB [CALC] Antimony BRL mg/L 0.020 0.014 1 '6010D 5/31/19 17:24 JAB P9E0532 Arsenic BRL mg/L 0.020 0.0060 1 '6010D 5/31/19 17:24 JAB P9E0532 Beryllium BRL mg/L 0.0020 0.0010 1 '6010D 5/31/19 17:24 JAB P9E0532 Cadmium BRL mg/L 0.0020 0.00040 1 '6010D 5/31/19 17:24 JAB P9E0532 Calcium 44 mg/L 0.20 0.072 1 *200.7 5/31/19 15:09 JAB P9E0533 Chromium 0.024 mg/L 0.010 0.0030 1 '6010D 5/31/19 17:24 JAB P9E0532 Copper 0.013 mg/L 0.010 0.0050 1 '6010D 5/31/19 17:24 JAB P9E0532 Lead 0.011 mg/L 0.0050 0.0039 1 '6010D 5/31/19 17:24 JAB P9E0532 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Laboratory Report Full -Service Analytical & P R I S M Environmental Solutions 06/06/2019 L SOAATORIES INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW##3 Attn: Alex Kuczero Prism Sample ID: 9050492-03 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 14:35 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Magnesium 23 mg/L 0.20 0.049 1 *200.7 6/31/19 15:09 JAB P9E0533 Nickel BRL mg/L 0.010 0.00036 1 '6010D 5/31/19 17:24 JAB P9E0532 Selenium BRL mg/L 0.030 0.013 1 '6010D 5/31/19 17:24 JAB P9E0532 Silver BRL mg/L 0.0050 0.00090 1 '6010D 5/31/19 17:24 JAB P9E0532 Thallium BRL mg/L 0.020 0.0050 1 '6010D 5/31/19 17:24 JAB P9E0532 Zinc 0.045 mg/L 0.040 0.020 1 '6010D 5131/19 17:24 JAB 139E0532 Volatile Organic Compounds by GC/MS 1, 1, 1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 5/31/19 18:15 KDM P9E0549 1,1,1-Tdchloroethane BRL ug/L 0.50 0.061 1 8260B 5/31/19 18:15 KDM P9E0549 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 5/31/19 18:15 KDM P9E0549 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 18:15 KDM P9E0549 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 5/31/19 18:15 KDM P9E0549 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 5/31/19 18:15 KDM P9E0549 1. 1 -Dichloropropylene BRL ug/L 0.50 0.051 1 8260B 5/31/19 18:15 KDM P9E0549 1,2,3-Tdchlorobenzene BRL ug/L 2.0 0.40 1 8260B 5/31/19 18:15 KDM P9E0549 1,2,3-Tdchloropropane BRL ug/L 1.0 0.14 1 8260B 5/31/19 18:15 KDM P9E0549 1,2,4-Tdchiorobenzene BRL ug/L 1.0 0.13 1 8260B 5/31/19 18:15 KDM P9E0549 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 18:15 KDM P9E0549 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 5/31/19 18:15 KDM P9E0549 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 5131/19 18:15 KDM P9E0549 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 5131/19 18:15 KDM P9E0549 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 5/31/19 18:15 KDM P9E0549 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 5131/19 18:15 KDM P9E0549 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 5/31/19 18:15 KDM P9E0549 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 5/31/19 18:15 KDM P9E0549 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 5/31/19 18:15 KDM P9E0549 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 5/31/19 18:15 KDM P9E0549 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 5/31/19 18:15 KDM P9E0549 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 5/31/19 18:15 KDM P9E0549 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 5/31/19 18:15 KDM P9E0549 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 5/31/19 18:15 KDM P9E0549 Acetone BRL ug/L 5.0 0.31 1 8260B 5/31119 18:15 KDM P9E0549 Acrolein BRL ug/L 20 0.20 1 8260B 5/31/19 18:15 KDM P9E0549 Acrylonitrile BRL ug/L 20 0.20 1 8260B 5/31/19 18:15 KDM P9E0549 Benzene BRL ug/L 0.50 0.048 1 8260B 5/31/19 18:15 KDM P9E0549 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 5/31/19 18:15 KDM P9E0549 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 5/31/19 18:15 KDM P9E0549 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 5/31/19 18:15 KDM P9E0549 Bromoform BRL ug/L 1.0 0.040 1 8260B 5/31/19 18:15 KDM P9E0549 Bromomethane BRL ug/L 1.0 0.18 1 8260B 5/31/19 18:15 KDM P9E0549 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 5/31/19 18:15 KDM P9E0549 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 5/31/19 18:15 KDM P9E0549 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 5/31/19 18:15 KDM P9E0549 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 P R I S M Laboratory Report &GI Fun -Service Analytical 8 Environmental Solutions 06/06/2019 -RRTORIE$ INC NOVA Engineering & Environmental Project: CLT Metro Client Sample ID: MW#3 Attn: Alex Kuczero Prism Sample ID: 9050492-03 5104 Reagan Drive Suite 8 Prism Work Order: 9050492 Charlotte, NC 28206 Sample Matrix: Water Time Collected: 05/30/19 14:35 Time Submitted: 05/30/19 14:55 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chloroethane BRL ug/L Chloroform BRL ug/L Chloromethane BRL ug/L cis-1,2-Dichloroethylene BRL ug/L cis- 1, 3-Dichloropropylene BRL ug/L Dibromochloromethane BRL ug/L Dibromomethane BRL ug/L Dichlorodifluoromethane BRL ug/L Ethylbenzene BRL ug/L Hexachlorobutadiene BRL ug/L Isopropyl Ether BRL ug/L Isopropylbenzene (Cumene) BRL ug/L m,p-Xylenes BRL ug/L Methyl Butyl Ketone (2-Hexanone) BRL ug/L Methyl Ethyl Ketone (2-Butanone) BRL ug/L Methyl Isobutyl Ketone BRL ug/L Methylene Chloride BRL ug/L Methyl-tert-Butyl Ether BRL ug/L Naphthalene BRL ug/L n-Butylbenzene BRL ug/L n-Propylbenzene BRL ug/L o-Xylene BRL ug/L sec-Butylbenzene BRL ug/L Styrene BRL ug/L tert-Butylbenzene BRL ug/L Tetrachloroethylene BRL ug/L Toluene BRL ug/L trans- 1,2-Dichloroethylene BRL ug/L trans- 1, 3-Dichloropropylene BRL ug/L Tiichloroethylene BRL ug/L Trichlorofluoromethane BRL ug/L Vinyl acetate BRL ug/L Vinyl chloride BRL ug/L Xylenes, total BRL ug/L 0.50 0.22 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.076 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.079 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.056 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.079 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.081 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.065 1 8260B 5/31/19 18:15 KDM P9E0549 5.0 0.11 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.061 1 8260B 5/31/19 18:15 KDM P9E0549 2.0 0.16 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.050 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.054 1 8260B 5/31/19 18:15 KDM P9E0549 1.0 0.12 1 8260B 5/31/19 18:15 KDM P9E0549 5.0 0.065 1 8260B 5/31/19 18:15 KDM P9E0549 5.0 0.24 1 8260B 5/31/19 18:15 KDM P9E0549 5.0 0.078 1 8260B 5/31/19 18:15 KDM P9E0549 1.0 0.083 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.042 1 8260B 5/31119 18:15 KDM P9E0549 1.0 0.19 1 8260B 5/31/19 18:15 KDM P9E0549 1.0 0.076 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.087 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.044 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.076 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.047 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.088 1 8260B 5/31119 18:15 KDM P9E0549 0.50 0.098 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.044 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.094 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.070 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.078 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.062 1 8260B 5/31/19 18:15 KDM P9E0549 2.0 0.060 1 8260B 5/31/19 18:15 KDM P9E0549 0.50 0.097 1 8260B 5/31/19 18:15 KDM P9E0549 1.5 0.15 1 8260B 5/31/19 18:15 KDM P9E0549 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 80-124 Dibromofluoromethane 97 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 S M Environmental Analytical & Envronmental Solutions LABORATORIES INC. Level II QC Report 6/6119 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO549 - 5030B Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes Blank (P9E0549-BLK1) Prepared & Analyzed: 05/31 /19 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrachloroethane BRL 0.50 ug/L 1,1,2-Trichloroethane BRL 0.50 ug/L 1,1-Dichloroethane BRL 0.50 ug/L 1,1-Dichloroethylene BRL 0.50 ug/L 1, 1 -Dichloropropylene BRL 0.50 ug/L 1,2,3-Tdchlorobenzene BRL 2.0 ug/L 1,2,3-Tdchloropropane BRL 1.0 ug/L 1,2,4-Tdchlorobenzene BRL 1.0 ug/L 1,2,4-Trimethylbenzene BRL 0.50 ug/L 1,2-Dibromo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromoethane BRL 0.50 ug/L 1,2-Dichlorobenzene BRL 0.50 ug/L 1,2-Dichloroethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3,5-Trimethylbenzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlorotoluene BRL 0.50 ug/L 4-Isopropyltoluene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonitrile BRL 20 ug/L Benzene BRL 0.50 ug/L Bromobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disulfide BRL 5.0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 5.0 ug/L Ethylbenzene BRL 0.50 ug/L Hexachlorobutadiene BRL 2.0 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 &RRISM Full -Service Analytical Environmental Solutions LABORATORIES INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO549 - 5030B Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %BREC RPD Level Result %REC Limits RPD Limit Notes Blank (P9E0549-BLK1) Prepared & Analyzed: 05/31/19 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hexanone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.50 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tert-Butylbenzene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans- 1,2-Dichloroethylene BRL 0.50 ug/L trans- 1,3-Dichloropropylene BRL 0.50 ug/L Trichloroethylene BRL 0.50 ug/L Trichlorofluoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Xylenes, total BRL 1.5 ug/L Surrogate:4-Bromofluorobenzene 49.9 ug/L 50.00 100 80-124 Surrogate: Dibromofluoromethane 46.7 ug/L 50.00 93 75-129 Surrogate: Toluene-d8 48.9 ug/L 50.00 98 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Full- IR R ISM Environmental Service al Solution s Environmental Solutions 'gG LABOR OHIEB. INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9E0549 - 5030B LCS (P9E0549-13S1) Prepared & Analyzed: 05/31/19 1,1,1,2-Tetrachloroethane 19.9 0.50 ug/L 20.00 99 79-134 1,1,1-Trichloroethane 19.6 0.50 ug/L 20.00 98 75-136 1,1,2,2-Tetrachloroethane 21.6 0.50 ug/L 20.00 108 62-127 1,1,2-Trichloroethane 21.0 0.50 ug/L 20.00 105 70-140 1,1-Dichloroethane 20.7 0.50 ug/L 20.00 103 78-130 1,1-Dichloroethylene 20.0 0.50 ug/L 20.00 100 70-154 1, 1 -Dichloropropylene 20.7 0.50 ug/L 20.00 104 71-136 1,2,3-Tdchlorobenzene 21.6 2.0 ug/L 20.00 108 58-144 1,2,3-Tdchloropropane 21.3 1.0 ug/L 20.00 107 71-127 1,2,4-Trichlorobenzene 21.4 1.0 ug/L 20.00 107 66-139 1,2,4-Trimethylbenzene 20.4 0.50 ug/L 20.00 102 75-133 1,2-Dibromo-3-chloropropane 22.1 2.0 ug/L 20.00 111 63-134 1,2-Dibromoethane 20.5 0.50 ug/L 20.00 103 77-135 1,2-Dichlorobenzene 21.0 0.50 ug/L 20.00 105 78-128 1,2-Dichloroethane 18.4 0.50 ug/L 20.00 92 68-131 1,2-Dichloropropane 20.8 0.50 ug/L 20.00 104 77-130 1,3,5-Trimethylbenzene 20.6 0.50 ug/L 20.00 103 75-131 1,3-Dichlorobenzene 20.9 0.50 ug/L 20.00 105 77-125 1,3-Dichloropropane 20.3 0.50 ug/L 20.00 101 76-132 1,4-Dichlorobenzene 20.4 0.50 ug/L 20.00 102 75-126 2,2-Dichloropropane 19.2 2.0 ug/L 20.00 96 29-149 2-Chlorotoluene 20.1 0.50 ug/L 20.00 100 74-126 4-Chlorotoluene 20.1 0.50 ug/L 20.00 100 78-129 4-Isopropyltoluene 23.1 0.50 ug/L 20.00 115 69-132 Acetone 38.1 5.0 ug/L 40.00 95 40-166 Acrolein 47.4 20 ug/L 40.00 118 70-130 Acrylonitrile 49.4 20 ug/L 40.00 124 81-127 Benzene 20.6 0.50 ug/L 20.00 103 77-128 Bromobenzene 19.9 0.50 ug/L 20.00 99 78-129 Bromochloromethane 22.3 0.50 ug/L 20.00 112 78-135 Bromodichloromethane 19.9 0.50 ug/L 20.00 99 76-138 Bromoform 18.6 1.0 ug/L 20.00 93 71-135 Bromomethane 13.0 1.0 ug/L 20.00 65 41-168 Carbon disulfide 20.4 5.0 ug/L 20.00 102 59-135 Carbon Tetrachloride 18.4 0.50 ug/L 20.00 92 72-142 Chlorobenzene 19.8 0.50 ug/L 20.00 99 78-119 Chloroethane 17.8 0.50 ug/L 20.00 89 57-142 Chloroform 19.6 0.50 ug/L 20.00 98 77-130 Chloromethane 19.4 0.50 ug/L 20.00 97 47-145 cis-1,2-Dichloroethylene 20.0 0.50 ug/L 20.00 100 76-141 cis-1,3-Dichloropropylene 19.2 0.50 ug/L 20.00 96 65-140 Dibromochloromethane 18.7 0.50 ug/L 20.00 94 75-134 Dibromomethane 20.7 0.50 ug/L 20.00 103 76-138 Dichlorodifluoromethane 15.4 5.0 ug/L 20.00 77 28-163 Ethylbenzene 19.4 0.50 ug/L 20.00 97 80-127 Hexachlorobutadiene 21.0 2.0 ug/L 20.00 105 61-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 /9m'adR I S M Full -Service Analytical & Environmental Solutions LABORATORIES INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO549 - 5030B Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P9E0549-BS1) Prepared & Analyzed: 05/31/19 Isopropyl Ether 22.6 0.50 ug/L 20.00 113 60-154 Isopropylbenzene (Cumene) 20.9 0.50 ug/L 20.00 105 70-130 m,p-Xylenes 39.8 1.0 ug/L 40.00 99 77-133 Methyl Butyl Ketone (2-Hexanone) 21.7 5.0 ug/L 20.00 109 64-137 Methyl Ethyl Ketone (2-Butanone) 20.1 5.0 ug/L 20.00 100 71-134 Methyl Isobutyl Ketone 22.6 5.0 ug/L 20.00 113 69-134 Methylene Chloride 20.4 1.0 ug/L 20.00 102 73-131 Methyl-tert-Butyl Ether 20.9 0.50 ug/L 20.00 104 68-135 Naphthalene 22.5 1.0 ug/L 20.00 112 64-136 n-Butylbenzene 20.2 1.0 ug/L 20.00 101 68-134 n-Propylbenzene 20.3 0.50 ug/L 20.00 102 72-132 o-Xylene 19.7 0.50 ug/L 20.00 98 78-128 sec-Butylbenzene 19.1 0.50 ug/L 20.00 96 71-131 Styrene 22.8 0.50 ug/L 20.00 114 78-129 tert-Butylbenzene 20.9 0.50 ug/L 20.00 105 70-132 Tetrachloroethylene 20.3 0.50 ug/L 20.00 102 80-129 Toluene 20.5 0.50 ug/L 20.00 102 76-131 trans-1,2-Dichloroethylene 20.2 0.50 ug/L 20.00 101 76-135 trans- 1, 3-Dich loropropylene 18.7 0.50 ug/L 20.00 93 67-140 Trichloroethylene 20.9 0.50 ug/L 20.00 105 77-133 Trichlorofluoromethane 16.3 0.50 ug/L 20.00 81 62-148 Vinyl acetate 22.8 2.0 ug/L 20.00 114 34-167 Vinyl chloride 17.5 0.50 ug/L 20.00 87 57-141 Xylenes, total 59.4 1.5 ug/L 60.00 99 77-133 Surrogate:4-Bromofluorobenzene 49.9 ug/L 50.00 100 80-124 Surrogate: Dibromofluoromethane 47.8 ug/L 50.00 96 75-129 Surrogate: Toluene-d8 48.0 ug/L 50.00 96 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 AGP R I S M Full -Service Analytical 8 Environmental Solutions LABORATORIES INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO549 - 5030B Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS Dup (P9E0549-BSD1) Prepared & Analyzed: 05/31/19 1,1,1,2-Tetrachloroethane 19.3 0.50 ug/L 20.00 96 79-134 3 20 1. 1, 1 -Trichloroethane 19.1 0.50 ug/L 20.00 96 75-136 3 20 1. 1, 2,2-Tetrachloroethane 19.7 0.50 ug/L 20.00 98 62-127 9 20 1,1,2-Trichloroethane 20.3 0.50 ug/L 20.00 101 70-140 4 20 1,1-Dichloroethane 19.6 0.50 ug/L 20.00 98 78-130 5 20 1,1-Dichloroethylene 19.3 0.50 ug/L 20.00 96 70-154 4 20 1, 1 -Dichloropropylene 19.5 0.50 ug/L 20.00 97 71-136 6 20 1,2,3-Trichlorobenzene 19.7 2.0 ug/L 20.00 98 58-144 9 20 1,2,3-Tdchloropropane 19.1 1.0 ug/L 20.00 95 71-127 11 20 1,2,4-Trichlorobenzene 20.3 1.0 ug/L 20.00 101 66-139 6 20 1,2,4-Trimethylbenzene 19.2 0.50 ug/L 20.00 96 75-133 6 20 1,2-Dibromo-3-chloropropane 20.4 2.0 ug/L 20.00 102 63-134 8 20 1,2-Dibromoethane 19.9 0.50 ug/L 20.00 100 77-135 3 20 1,2-Dichlorobenzene 19.6 0.50 ug/L 20.00 98 78-128 7 20 1,2-Dichloroethane 17.9 0.50 ug/L 20.00 90 68-131 3 20 1,2-Dichloropropane 20.1 0.50 ug/L 20.00 100 77-130 3 20 1,3,5-Trimethylbenzene 19.3 0.50 ug/L 20.00 97 75-131 6 20 1,3-Dichlorobenzene 19.5 0.50 ug/L 20.00 98 77-125 7 20 1,3-Dichloropropane 19.9 0.50 ug/L 20.00 100 76-132 2 20 1,4-Dichlorobenzene 19.1 0.50 ug/L 20.00 96 75-126 7 20 2,2-Dichloropropane 18.6 2.0 ug/L 20.00 93 29-149 3 20 2-Chlorotoluene 18.8 0.50 ug/L 20.00 94 74-126 6 20 4-Chlorotoluene 18.8 0.50 ug/L 20.00 94 78-129 6 20 4-Isopropyltoluene 21.5 0.50 ug/L 20.00 108 69-132 7 20 Acetone 36.5 5.0 ug/L 40.00 91 40-166 4 20 Acrolein 45.1 20 ug/L 40.00 113 70-130 5 20 Acrylonitrile 44.7 20 ug/L 40.00 112 81-127 10 20 Benzene 20.1 0.50 ug/L 20.00 100 77-128 3 20 Bromobenzene 18.8 0.50 ug/L 20.00 94 78-129 6 20 Bromochloromethane 21.8 0.50 ug/L 20.00 109 78-135 2 20 Bromodichloromethane 19.2 0.50 ug/L 20.00 96 76-138 3 20 Bromoform 17.5 1.0 ug/L 20.00 88 71-135 6 20 Bromomethane 14.4 1.0 ug/L 20.00 72 41-168 10 20 Carbon disulfide 19.6 5.0 ug/L 20.00 98 59-135 4 20 Carbon Tetrachloride 17.4 0.50 ug/L 20.00 87 72-142 6 20 Chlorobenzene 19.5 0.50 ug/L 20.00 97 78-119 2 20 Chloroethane 16.8 0.50 ug/L 20.00 84 57-142 6 20 Chloroform 19.1 0.50 ug/L 20.00 95 77-130 3 20 Chloromethane 18.5 0.50 ug/L 20.00 92 47-145 5 20 cis-1,2-Dichloroethylene 19.4 0.50 ug/L 20.00 97 76-141 3 20 cis-1,3-Dichloropropylene 18.4 0.50 ug/L 20.00 92 65-140 4 20 Dibromochloromethane 17.9 0.50 ug/L 20.00 90 75-134 4 20 Dibromomethane 19.6 0.50 ug/L 20.00 98 76-138 5 20 Dichlorodifluoromethane 14.3 5.0 ug/L 20.00 72 28-163 7 20 Ethylbenzene 19.1 0.50 ug/L 20.00 96 80-127 2 20 Hexachlorobutadiene 19.6 2.0 ug/L 20.00 98 61-134 7 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 �P R I S M Full -Service Analytical s Environmental Solutions LARORATORIE$ INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO549 - 5030B Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P9E0549-BSD1) Prepared & Analyzed: 05/31/19 Isopropyl Ether 22.0 0.50 ug/L 20.00 110 60-154 3 20 Isopropylbenzene (Cumene) 19.6 0.50 ug/L 20.00 98 70-130 6 20 m,p-Xylenes 39.0 1.0 ug/L 40.00 98 77-133 2 20 Methyl Butyl Ketone (2-Hexanone) 20.3 5.0 ug/L 20.00 101 64-137 7 20 Methyl Ethyl Ketone (2-Butanone) 19.1 5.0 ug/L 20.00 96 71-134 5 20 Methyl Isobutyl Ketone 21.1 5.0 ug/L 20.00 105 69-134 7 20 Methylene Chloride 19.6 1.0 ug/L 20.00 98 73-131 4 20 Methyl-tert-Butyl Ether 20.1 0.50 ug/L 20.00 100 68-135 4 20 Naphthalene 20.2 1.0 ug/L 20.00 101 64-136 10 20 n-Butylbenzene 18.7 1.0 ug/L 20.00 94 68-134 8 20 n-Propylbenzene 19.3 0.50 ug/L 20.00 96 72-132 5 20 o-Xylene 19.2 0.50 ug/L 20.00 96 78-128 3 20 sec-Butylbenzene 17.8 0.50 ug/L 20.00 89 71-131 7 20 Styrene 22.0 0.50 ug/L 20.00 110 78-129 4 20 tert-Butylbenzene 19.8 0.50 ug/L 20.00 99 70-132 5 20 Tetrachloroethylene 20.1 0.50 ug/L 20.00 100 80-129 1 20 Toluene 19.8 0.50 ug/L 20.00 99 76-131 3 20 trans-1,2-Dichloroethylene 19.7 0.50 ug/L 20.00 98 76-135 2 20 trans- 1,3-Dichloropropylene 18.1 0.50 ug/L 20.00 90 67-140 3 20 Trichloroethylene 20.5 0.50 ug/L 20.00 102 77-133 2 20 Trichlorofluoromethane 15.7 0.50 ug/L 20.00 78 62-148 4 20 Vinyl acetate 22.0 2.0 ug/L 20.00 110 34-167 4 20 Vinyl chloride 17.1 0.50 ug/L 20.00 85 57-141 2 20 Xylenes, total 58.2 1.5 ug/L 60.00 97 77-133 2 20 Surrogate:4-Bromofluorobenzene 48.2 ug/L 50.00 96 80-124 Surrogate: Dibromofluoromethane 47.8 ug/L 50.00 96 75-129 Surrogate: Toluene-d8 48.1 ug/L 50.00 96 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 P R I S M Full -Service Analytical s Environmental Solutions I. ARORATORIES. INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P9EO534 - 3510C MS Blank (P9E0534-BLK1) Prepared & Analyzed: 05/31/19 1 2,4-Trichlorobenzene BRL 10 u /L 1,2-Dichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methylnaphthalene BRL 10 ug/L 2,4,5-Trichlorophenol BRL 20 ug/L 2,4,6-Trichlorophenol BRL 20 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethyl phenol BRL 10 ug/L 2,4-Dinitrophenol BRL 50 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 20 ug/L 2-Chloronaphthalene BRL 20 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methylnaphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlorobenzidine BRL 10 ug/L 3/4-Methylphenol BRL 10 ug/L 3-Nitroaniline BRL 10 ug/L 4,6-Dinitro-2-methylphenol BRL 50 ug/L 4-Bromophenyl phenyl ether BRL 20 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 20 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 20 ug/L Aniline BRL 50 ug/L Anthracene BRL 10 ug/L Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Benzo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chloroethoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 �IR R ISM Full -Service Analytical Environmental Solutions LABORATORIES, INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9EO534 - 3510C MS Blank (P9E0534-BLK1) Prepared & Analyzed: 05/31/19 Dibenzo(a,h)anthracene BRL 20 ug/L Dibenzofuran BRL 20 ug/L Diethyl phthalate BRL 20 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlorobenzene BRL 20 ug/L Hexachlorobutadiene BRL 20 ug/L Hexachlorocyclopentadiene BRL 20 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 20 ug/L N-Nitrosodiphenylamine BRL 20 ug/L Pentachlorophenol BRL 50 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate:2,4,6-Tribromophenol 114 ug/L 100.0 114 43-140 Surrogate:2-Fluorobiphenyl 57.8 ug/L 50.00 116 44-119 Surrogate:2-Fluorophenol 72.5 ug/L 100.0 73 19-119 Surrogate: Nitrobenzene-d5 54.2 ug/L 50.00 108 44-120 Surrogate: Phenol-d5 46.7 ug/L 100.0 47 11-52 Surrogate: Terphenyl-04 59.4 ug/L 50.00 119 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 QRR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO534 - 3510C MS Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS (P9E0534-BS1) Prepared & Analyzed: 05/31/19 1,2,4-Tdchlorobenzene 42.1 10 ug/L 50.00 84 29-126 1,2-Dichlorobenzene 43.8 10 ug/L 50.00 88 32-111 1,3-Dichlorobenzene 42.1 10 ug/L 50.00 84 28-110 1,4-Dichlorobenzene 43.0 10 ug/L 50.00 86 29-112 1-Methylnaphthalene 47.6 10 ug/L 50.00 95 41-119 2,4,5-Trichlorophenol 51.5 20 ug/L 50.00 103 53-123 2,4,6-Trichlorophenol 50.8 20 ug/L 50.00 102 50-125 2,4-Dichlorophenol 44.3 10 ug/L 50.00 89 47-121 2,4-Dimethylphenol 57.6 10 ug/L 50.00 115 31-124 2,4-Dinitrophenol 26.7 50 ug/L 50.00 53 23-143 J 2,4-Dinitrotoluene 55.5 10 ug/L 50.00 111 57-128 2,6-Dinitrotoluene 57.1 20 ug/L 50.00 114 57-124 2-Chloronaphthalene 55.5 20 ug/L 50.00 111 40-116 2-Chlorophenol 48.2 10 ug/L 50.00 96 38-117 2-Methylnaphthalene 45.9 10 ug/L 50.00 92 40-121 2-Methylphenol 48.1 10 ug/L 50.00 96 30-117 2-Nitroaniline 54.5 10 ug/L 50.00 109 55-127 2-Nitrophenol 42.9 10 ug/L 50.00 86 47-123 3,3'-Dichlorobenzidine 62.8 10 ug/L 50.00 126 27-129 3/4-Methylphenol 39.9 10 ug/L 50.00 80 29-110 3-Nitroaniline 53.8 10 ug/L 50.00 108 41-128 4,6-Dinitro-2-methylphenol 40.7 50 ug/L 50.00 81 44-137 J 4-Bromophenyl phenyl ether 56.2 20 ug/L 50.00 112 55-124 4-Chloro-3-methylphenol 46.8 10 ug/L 50.00 94 52-119 4-Chloroaniline 49.0 10 ug/L 50.00 98 33-117 4-Chlorophenyl phenyl ether 56.4 20 ug/L 50.00 113 53-121 4-Nitroaniline 55.4 10 ug/L 50.00 111 45-135 4-Nitrophenol 27.0 10 ug/L 50.00 54 10-77 Acenaphthene 57.6 10 ug/L 50.00 115 47-122 Acenaphthylene 53.6 20 ug/L 50.00 107 41-130 Aniline 63.1 50 ug/L 50.00 126 12-197 Anthracene 60.1 10 ug/L 50.00 120 57-123 Azobenzene 58.9 10 ug/L 50.00 118 61-116 L1 Benzo(a)anthracene 59.0 10 ug/L 50.00 118 58-125 Benzo(a)pyrene 59.1 10 ug/L 50.00 118 54-128 Benzo(b)fluoranthene 59.7 10 ug/L 50.00 119 53-131 Benzo(g,hJ)perylene 56.8 10 ug/L 50.00 114 50-134 Benzo(b)fluoranthene 60.2 10 ug/L 50.00 120 57-129 Benzoic Acid BRL 100 ug/L 50.00 10-125 L Benzyl alcohol 48.3 10 ug/L 50.00 97 31-112 bis(2-Chloroethoxy)methane 49.6 10 ug/L 50.00 99 48-120 Bis(2-Chloroethyl)ether 47.1 10 ug/L 50.00 94 43-118 Bis(2-chloroisopropyl)ether 52.7 10 ug/L 50.00 105 37-130 Bis(2-Ethylhexyl)phthalate 61.2 10 ug/L 50.00 122 55-135 Butyl benzyl phthalate 59.6 10 ug/L 50.00 119 53-134 Chrysene 59.5 10 ug/L 50.00 119 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041526-0409 Level II QC Report &W R I S M I Full -Service Analytical 6/6/19 Environmental Solutions IABOPF-ES.NC. NOVA Engineering & Environmental Project: CLT Metro Prism Work Order: 9050492 Attn: Alex Kuczero Time Submitted: 5/30/2019 2:55:OOPM 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9EO534 - 3510C MS LCS (P9E0534-BS1) Prepared & Analyzed: 05/31/19 Dibenzo(a,h)anthracene 57.4 20 ug/L 50.00 115 51-134 Dibenzofuran 57.4 20 ug/L 50.00 115 53-118 Diethyl phthalate 58.6 20 ug/L 50.00 117 56-125 Dimethyl phthalate 57.3 10 ug/L 50.00 115 45-127 Di-n-butyl phthalate 59.4 10 ug/L 50.00 119 59-127 Di-n-octyl phthalate 60.8 10 ug/L 50.00 122 51-140 Fluoranthene 57.4 10 ug/L 50.00 115 57-128 Fluorene 58.4 10 ug/L 50.00 117 52-124 Hexachlorobenzene 53.9 20 ug/L 50.00 108 53-125 Hexachlorobutadiene 41.7 20 ug/L 50.00 83 22-124 Hexachlorocyclopentadiene 41.4 20 ug/L 50.00 83 32-117 Hexachloroethane 39.8 10 ug/L 50.00 80 21-115 Indeno(1,2,3-cd)pyrene 67.1 10 ug/L 50.00 134 52-134 L1 Isophorone 48.2 10 ug/L 50.00 96 42-124 Naphthalene 44.1 10 ug/L 50.00 88 40-121 Nitrobenzene 47.2 10 ug/L 50.00 94 45-121 N-Nitroso-di-n-propylamine 52.2 20 ug/L 50.00 104 49-119 N-Nitrosodiphenylamine 67.0 20 ug/L 50.00 134 51-123 LH Pentachlorophenol 48.7 50 ug/L 50.00 97 35-138 J Phenanthrene 58.7 10 ug/L 50.00 117 59-120 Phenol 26.3 10 ug/L 50.00 53 12-58 Pyrene 59.6 10 ug/L 50.00 119 57-126 Surrogate: 2,4,6-Tribromophenol 101 ug/L 100.0 101 43-140 Surrogate:2-Fluorobipheny/ 55.8 ug/L 50.00 112 44-119 Surrogate:2-Fluoropheno/ 59.4 ug/L 100.0 59 19-119 Surrogate: Nitrobenzene-0 46.8 ug/L 50.00 94 44-120 Surrogate: Phenol-d5 41.0 ug/L 100.0 41 11-52 Surrogate: Terphenyl-04 57.9 ug/L 50.00 116 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 AFun-Service Analytical 8 PR ISM Environmental Solutions LABORATORIES INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9E0534 - 3510C MS LCS Dup (P9E0534-BSD1) Prepared & Analyzed: 05/31/19 1,2,4-Tdchlorobenzene 41.7 10 ug/L 50.00 83 29-126 0.8 20 1,2-Dichlorobenzene 43.9 10 ug/L 50.00 88 32-111 0.05 20 1,3-Dichlorobenzene 42.1 10 ug/L 50.00 84 28-110 0.02 20 1,4-Dichlorobenzene 42.7 10 ug/L 50.00 85 29-112 0.7 20 1-Methylnaphthalene 47.1 10 ug/L 50.00 94 41-119 1 20 2,4,5-Trichlorophenol 56.6 20 ug/L 50.00 113 53-123 10 20 2,4,6-Trichlorophenol 58.4 20 ug/L 50.00 117 50-125 14 20 2,4-Dichlorophenol 47.3 10 ug/L 50.00 95 47-121 7 20 2,4-Dimethylphenol 55.5 10 ug/L 50.00 111 31-124 4 20 2,4-Dinitrophenol 37.1 50 ug/L 50.00 74 23-143 33 20 D, J 2,4-Dinitrotoluene 56.9 10 ug/L 50.00 114 57-128 2 20 2,6-Dinitrotoluene 58.2 20 ug/L 50.00 116 57-124 2 20 2-Chloronaphthalene 56.5 20 ug/L 50.00 113 40-116 2 20 2-Chlorophenol 52.3 10 ug/L 50.00 105 38-117 8 20 2-Methylnaphthalene 45.3 10 ug/L 50.00 91 40-121 1 20 2-Methylphenol 48.5 10 ug/L 50.00 97 30-117 0.7 20 2-Nitroaniline 55.7 10 ug/L 50.00 111 55-127 2 20 2-Nitrophenol 46.4 10 ug/L 50.00 93 47-123 8 20 3,3'-Dichlorobenzidine 62.9 10 ug/L 50.00 126 27-129 0.05 20 3/4-Methylphenol 40.6 10 ug/L 50.00 81 29-110 2 20 3-Nitroaniline 54.8 10 ug/L 50.00 110 41-128 2 20 4,6-Dinitro-2-methylphenol 51.5 50 ug/L 50.00 103 44-137 23 20 D 4-Bromophenyl phenyl ether 55.1 20 ug/L 50.00 110 55-124 2 20 4-Chloro-3-methylphenol 48.4 10 ug/L 50.00 97 52-119 3 20 4-Chloroaniline 48.2 10 ug/L 50.00 96 33-117 2 20 4-Chlorophenyl phenyl ether 57.9 20 ug/L 50.00 116 53-121 3 20 4-Nitroaniline 54.9 10 ug/L 50.00 110 45-135 0.9 20 4-Nitrophenol 32.4 10 ug/L 50.00 65 10-77 18 20 Acenaphthene 58.5 10 ug/L 50.00 117 47-122 2 20 Acenaphthylene 53.8 20 ug/L 50.00 108 41-130 0.4 20 Aniline 60.0 50 ug/L 50.00 120 12-197 5 20 Anthracene 58.9 10 ug/L 50.00 118 57-123 2 20 Azobenzene 57.4 10 ug/L 50.00 115 61-116 2 20 Benzo(a)anthracene 57.4 10 ug/L 50.00 115 58-125 3 20 Benzo(a)pyrene 57.3 10 ug/L 50.00 115 54-128 3 20 Benzo(b)fluoranthene 55.5 10 ug/L 50.00 111 53-131 7 20 Benzo(g,h,i)perylene 55.8 10 ug/L 50.00 112 50-134 2 20 Benzo(k)fluoranthene 62.1 10 ug/L 50.00 124 57-129 3 20 Benzoic Acid BRL 100 ug/L 50.00 10-125 20 L Benzyl alcohol 48.2 10 ug/L 50.00 96 31-112 0.06 20 bis(2-Chloroethoxy)methane 48.5 10 ug/L 50.00 97 48-120 2 20 Bis(2-Chloroethyl)ether 47.2 10 ug/L 50.00 94 43-118 0.2 20 Bis(2-chloroisopropyl)ether 51.7 10 ug/L 50.00 103 37-130 2 20 Bis(2-Ethylhexyl)phthalate 58.0 10 ug/L 50.00 116 55-135 5 20 Butyl benzyl phthalate 58.0 10 ug/L 50.00 116 53-134 3 20 Chrysene 58.2 10 ug/L 50.00 116 59-123 2 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 PRISM Fun -Service Analytical Environmental Solutions �. LABO-ORIEs INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9EO534 - 3510C MS Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P9E0534-BSD1) Prepared & Analyzed: 05/31/19 Dibenzo(a,h)anthracene 56.6 20 ug/L 50.00 113 51-134 1 20 Dibenzofuran 57.2 20 ug/L 50.00 114 53-118 0.5 20 Diethyl phthalate 58.5 20 ug/L 50.00 117 56-125 0.2 20 Dimethyl phthalate 57.8 10 ug/L 50.00 116 45-127 1 20 Di-n-butyl phthalate 58.0 10 ug/L 50.00 116 59-127 2 20 Di-n-octyl phthalate 58.4 10 ug/L 50.00 117 51-140 4 20 Fluoranthene 56.4 10 ug/L 50.00 113 57-128 2 20 Fluorene 59.3 10 ug/L 50.00 119 52-124 2 20 Hexachlorobenzene 52.5 20 ug/L 50.00 105 53-125 3 20 Hexachlorobutadiene 41.4 20 ug/L 50.00 83 22-124 0.8 20 Hexachlorocyclopentadiene 41.4 20 ug/L 50.00 83 32-117 0.2 20 Hexachloroethane 38.7 10 ug/L 50.00 77 21-115 3 20 Indeno(1,2,3-cd)pyrene 66.3 10 ug/L 50.00 133 52-134 1 20 Isophorone 47.0 10 ug/L 50.00 94 42-124 3 20 Naphthalene 43.8 10 ug/L 50.00 88 40-121 0.5 20 Nitrobenzene 45.9 10 ug/L 50.00 92 45-121 3 20 N-Nitroso-di-n-propylamine 50.1 20 ug/L 50.00 100 49-119 4 20 N-Nitrosodiphenylamine 65.6 20 ug/L 50.00 131 51-123 2 20 LH Pentachlorophenol 58.0 50 ug/L 50.00 116 35-138 17 20 Phenanthrene 57.4 10 ug/L 50.00 115 59-120 2 20 Phenol 27.6 10 ug/L 50.00 55 12-58 5 20 Pyrene 58.1 10 ug/L 50.00 116 57-126 2 20 Surrogate:2,4,6-Tribromophenol 113 ug/L 100.0 113 43-140 Surrogate:2-Fluorobipheny/ 55.4 ug/L 50.00 111 44-119 Surrogate:2-Fluorophenol 67.7 ug/L 100.0 68 19-119 Surrogate: Nitrobenzene-d5 45.5 ug/L 50.00 91 44-120 Surrogate: Phenol-d5 43.8 ug/L 100.0 44 11-52 Surrogate: Terphenyl-d14 57.3 ug/L 50.00 115 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 /A1QR I S M Full -Service Analytical Environmental Solutions -ONATONIE& INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Organochlorine Pesticides by GC/ECD - Quality Control Analyte Batch P9E0544 - 3510C GC Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes Blank (P9E0544-BLK1) Prepared: 05/31/19 Analyzed: 06/05/19 4,4'-DDD BRL 0.10 ug/L 4,4'-DDE BRL 0.10 ug/L 4,4'-DDT BRL 0.10 ug/L Aldrin BRL 0.050 ug/L alpha-BHC BRL 0.050 ug/L cis -Chlordane BRL 0.10 ug/L beta-BHC BRL 0.050 ug/L Chlordane BRL 0.50 ug/L delta-BHC BRL 0.050 ug/L Dieldrin BRL 0.050 ug/L Endosulfan I BRL 0.050 ug/L Endosulfan II BRL 0.050 ug/L Endosulfan Sulfate BRL 0.050 ug/L Endrin BRL 0.050 ug/L Endrin Aldehyde BRL 0.050 ug/L Endrin Ketone BRL 0.10 ug/L gamma-BHC BRL 0.050 ug/L trans -Chlordane BRL 0.10 ug/L Heptachlor BRL 0.050 ug/L Heptachlor Epoxide BRL 0.10 ug/L Methoxychlor BRL 0.10 ug/L Toxaphene BRL 1.0 ug/L Surrogate: Decachlorobipheny/ 0.490 ug/L 1.000 49 13-186 Surrogate: Tetrachloro-m-xylene 0.830 ug/L 1.000 83 40-134 LCS (P9E0544-BSI) Prepared: 05/31/19 Analyzed: 06/05/19 4,4'-DDD 0.920 0.10 ug/L 1.000 92 56-143 4,4'-DDE 1.02 0.10 ug/L 1.000 102 57-135 4,4'-DDT 0.980 0.10 ug/L 1.000 98 51-143 Aldrin 1.01 0.050 ug/L 1.000 101 45-134 alpha-BHC 0.800 0.050 ug/L 1.000 80 54-138 cis -Chlordane 1.03 0.10 ug/L 1.000 103 60-129 beta-BHC 0.970 0.050 ug/L 1.000 97 56-136 delta-BHC 0.470 0.050 ug/L 1.000 47 52-142 L Dieldrin 1.04 0.050 ug/L 1.000 104 60-136 Endosulfan 1 1.03 0.050 ug/L 1.000 103 62-126 Endosulfan II 1.10 0.050 ug/L 1.000 110 52-135 Endosulfan Sulfate 0.880 0.050 ug/L 1.000 88 62-133 Endrin 1.05 0.050 ug/L 1.000 105 60-138 Endrin Aldehyde 0.970 0.050 ug/L 1.000 97 51-132 Endrin Ketone 1.07 0.10 ug/L 1.000 107 58-134 gamma-BHC 0.880 0.050 ug/L 1.000 88 59-134 trans -Chlordane 1.02 0.10 ug/L 1.000 102 56-136 Heptachlor 1.11 0.050 ug/L 1.000 ill 54-130 Heptachlor Epoxide 1.02 0.10 ug/L 1.000 102 61-133 Methoxychlor 0.980 0.10 ug/L 1.000 98 54-145 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 P R I S M Full -Service Analytical Environmental Solutions Z�' LABORATORIES INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Organochlorine Pesticides by GC/ECD - Quality Control Analyte Batch P9EO544 - 3510C GC Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P9E0544-BS1) Prepared: 05/31/19 Analyzed: 06/05/19 Surrogate: Decachlorobiphenyl 0.740 ug/L 1.000 74 13-186 Surrogate: Tetrachloro-m-xylene 0.980 ug/L 1.000 98 40-134 LCS (P9E0544-BS2) Prepared: 05/31/19 Analyzed: 06/05/19 Chlordane 9.41 0.50 ug/L 10.00 94 62-140 Surrogate: Decachlorobiphenyl 0.670 ug/L 1.000 67 13-186 Surrogate: Tetrachloro-m-xylene 0.860 ug/L 1.000 86 40-134 LCS (P9E0544-BS3) Prepared: 05/31/19 Analyzed: 06/05/19 Toxaphene 10.4 1.0 ug/L 10.00 104 33-134 Surrogate: Decachlorobiphenyl 0.380 ug/L 1.000 38 13-166 Surrogate: Tetrachloro-m-xylene 0.780 ug/L 1.000 78 40-134 LCS Dup (P9E0544-BSD1) Prepared: 05/31/19 Analyzed: 06/05/19 4,4'-DDD 0.860 0.10 ug/L 1.000 86 56-143 7 30 4,4'-DDE 0.990 0.10 ug/L 1.000 99 57-135 3 30 4,4'-DDT 0.900 0.10 ug/L 1.000 90 51-143 9 30 Aldrin 0.990 0.050 ug/L 1.000 99 45-134 2 30 alpha-BHC 0.830 0.050 ug/L 1.000 83 54-138 4 30 cis -Chlordane 1.04 0.10 ug/L 1.000 104 60-129 1 30 beta-BHC 0.970 0.050 ug/L 1.000 97 56-136 0 30 delta-BHC 0.460 0.050 ug/L 1.000 46 52-142 2 30 L Dieldrin 1.03 0.050 ug/L 1.000 103 60-136 1 30 Endosulfan 1 1.04 0.050 ug/L 1.000 104 62-126 1 30 Endosulfan II 1.06 0.050 ug/L 1.000 106 52-135 4 30 Endosulfan Sulfate 0.810 0,050 ug/L 1.000 81 62-133 8 30 Endrin 1.02 0.050 ug/L 1.000 102 60-138 3 30 Endrin Aldehyde 0.960 0.050 ug/L 1.000 96 51-132 1 30 Endrin Ketone 0.990 0.10 ug/L 1.000 99 58-134 8 30 gamma-BHC 0.900 0.050 ug/L 1.000 90 59-134 2 30 trans -Chlordane 1.02 0.10 ug/L 1.000 102 56-136 0 30 Heptachlor 1.11 0.050 ug/L 1.000 ill 54-130 0 30 Heptachlor Epoxide 1.04 0.10 ug/L 1.000 104 61-133 2 30 Methoxychlor 0.880 0.10 ug/L 1.000 88 54-145 11 30 Toxaphene BRL 1.0 ug/L 33-134 30 Surrogate: Decachlorobiphenyl 0.860 ug/L 2.000 43 13-186 Surrogate: Tetrach/oro-m-xylene 1.96 ug/L 2.000 98 40-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 &P R ISM Full -Service en al Sryrioa� s Environmental Solutions LABORATORIES INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Total Metals - Quality Control Analyte Batch P9EO530 - 7470A Project: CLT Metro Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P9E0530-BLK1) Prepared & Analyzed: 05/31/19 Mercury BRL 0.00050 mg/L LCS (P9E0530-BSI) Prepared & Analyzed: 05/31/19 Mercury 0.00937 0.00050 mg/L 0.009375 100 80-120 Batch P9EO532 - 301 OA Blank (P9E0532-BLK1) Prepared & Analyzed: 05/31/19 Antimony BRL 0.020 mg/L Arsenic BRL 0.020 mg/L Beryllium BRL 0.0020 mg/L Cadmium BRL 0.0020 mg/L Chromium BRL 0.010 mg/L Copper BRL 0.010 mg/L Lead BRL 0.0050 mg/L Nickel BRL 0.010 mg/L Selenium BRL 0.030 mg/L Silver BRL 0.0050 mg/L Thallium BRL 0.020 mg/L Zinc BRL 0.040 mg/L LCS (P9E0532-BS1) Prepared & Analyzed: 05/31/19 Antimony 0.507 0.020 mg/L 0.5000 101 80-120 Arsenic 0.503 0.020 mg/L 0.5001 101 80-120 Beryllium 0.510 0.0020 mg/L 0.4998 102 80-120 Cadmium 0.510 0.0020 mg/L 0.5000 102 80-120 Chromium 0.523 0.010 mg/L 0.5001 105 80-120 Copper 0.512 0.010 mg/L 0.5001 102 80-120 Lead 0.506 0.0050 mg/L 0.5001 101 80-120 Nickel 0.512 0.010 mg/L 0.5001 102 80-120 Selenium 0.492 0.030 mg/L 0.4999 98 80-120 Silver 0.202 0.0050 mg/L 0.2000 101 80-120 Thallium 0.496 0.020 mg/L 0.4999 99 80-120 Zinc 0.497 0.040 mg/L 0.5001 99 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/526-0409 ,AGIPA R ISM Fun -Service Analytical Environmental Solutions LABORATORIES, INC Level II QC Report 6/6/19 NOVA Engineering & Environmental Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Total Metals - Quality Control Analyte Batch P9EO532 - 3010A Project: CLT Metro Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes Matrix Spike (P9E0532-MS1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Antimony 0.512 0.020 mg/L 0.5000 BRL 102 75-125 Arsenic 0.513 0.020 mg/L 0.5001 BRL 103 75-125 Beryllium 0.506 0.0020 mg/L 0.4998 BRL 101 75-125 Cadmium 0.495 0.0020 mg/L 0.5000 BRL 99 75-125 Chromium 0.550 0.010 mg/L 0.5001 0.0286 104 75-125 Copper 0.517 0.010 mg/L 0.5001 0.00691 102 75-125 Lead 0.494 0.0050 mg/L 0.5001 BRL 99 75-125 Nickel 0.513 0.010 mg/L 0.5001 0.0141 100 75-125 Selenium 0.489 0.030 mg/L 0.4999 BRL 98 75-125 Silver 0.202 0.0050 mg/L 0.2000 BRL 101 75-125 Thallium 0.477 0.020 mg/L 0.4999 BRL 95 75-125 Zinc 0.508 0.040 mg/L 0.5001 BRL 102 75-125 Matrix Spike Dup (P9E0532-MSD1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Antimony 0.515 0.020 mg/L 0.5000 BRL 103 75-125 0.6 20 Arsenic 0.523 0.020 mg/L 0.5001 BRL 105 75-125 2 20 Beryllium 0.511 0.0020 mg/L 0.4998 BRL 102 75-125 0.9 20 Cadmium 0.499 0.0020 mg/L 0.5000 BRL 100 75-125 0.8 20 Chromium 0.556 0.010 mg/L 0.5001 0.0286 106 75-125 1 20 Copper 0.522 0.010 mg/L 0.5001 0.00691 103 75-125 1 20 Lead 0.499 0.0050 mg/L 0.5001 BRL 100 75-125 0.9 20 Nickel 0.519 0.010 mg/L 0.5001 0.0141 101 75-125 1 20 Selenium 0.485 0.030 mg/L 0.4999 BRL 97 75-125 0.8 20 Silver 0.203 0.0050 mg/L 0.2000 BRL 102 75-125 0.7 20 Thallium 0.481 0.020 mg/L 0.4999 BRL 96 75-125 0.9 20 Zinc 0.514 0.040 mg/L 0.5001 BRL 103 75-125 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 AMR_I S M Fun -Service Analytical sEnvironmental SolutlonaN�TO. INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Project: CLT Metro Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Total Metals - Quality Control Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9EO533 - 200.7 Blank (P9E0533-BLK1) Prepared & Analyzed: 05/31/19 Calcium BRL 0.20 mg/L Magnesium BRL 0.20 mg/L LCS (P9E0533-BS1) Prepared & Analyzed: 05/31/19 Calcium 52.8 0.20 mg/L 50.00 106 85-115 Magnesium 52.2 0.20 mg/L 50.00 104 85-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 ,Aw 2R ISM Full -Service Analytical Environmental Solutions LABORATORIES INC. Level II QC Report 6/6/19 NOVA Engineering & Environmental Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Dissolved Metals - Quality Control Analyte Batch P9EO529 - 7470A Project: CLT Metro Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Blank (P9E0529-BLK1) Prepared & Analyzed: 05/31/19 Mercury BRL 0.00050 mg/L LCS (P9E0529-BSI) Prepared & Analyzed: 05/31/19 Mercury 0.00899 0.00050 mg/L 0.009375 96 80-120 Matrix Spike (P9E0529-MS1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Mercury 0.00922 0.00050 mg/L 0.009375 BRL 98 80-120 Matrix Spike Dup (P9E0529-MSD1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Mercury 0.00918 0.00050 mg/L 0.009375 BRL 98 80-120 0.4 20 Batch P9EO531 - 3010A Blank (P9E0531-BLK1) Prepared & Analyzed: 05/31/19 Antimony BRL 0.020 mg/L Arsenic BRL 0.020 mg/L Beryllium BRL 0.0020 mg/L Cadmium BRL 0.0020 mg/L Chromium BRL 0.010 mg/L Copper BRL 0.010 mg/L Lead BRL 0.0050 mg/L Nickel BRL 0.010 mg/L Selenium BRL 0.020 mg/L Silver BRL 0.0050 mg/L Thallium BRL 0.020 mg/L Zinc BRL 0.040 mg/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 �P R I S M Environmental Analytical Environmental Solutions �-OAATO-i INC Level If QC Report 6/6/19 NOVA Engineering & Environmental Attn: Alex Kuczero 5104 Reagan Drive Suite 8 Charlotte, NC 28206 Dissolved Metals - Quality Control Analyte Batch P9EO531 - 3010A Project: CLT Metro Reporting Result Limit Units Prism Work Order: 9050492 Time Submitted: 5/30/2019 2:55:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P9E0531-BSI) Prepared & Analyzed: 05/31/19 Antimony 0.379 0.020 mg/L 0.5000 76 80-120 A Arsenic 0.492 0.020 mg/L 0.5001 98 80-120 Beryllium 0.483 0.0020 mg/L 0.4998 97 80-120 Cadmium 0.500 0.0020 mg/L 0.5000 100 80-120 Chromium 0.503 0.010 mg/L 0.5001 101 80-120 Copper 0.482 0.010 mg/L 0.5001 96 80-120 Lead 0.489 0.0050 mg/L 0.5001 98 80-120 Nickel 0.496 0.010 mg/L 0.5001 99 80-120 Selenium 0.499 0.020 mg/L 0.4999 100 80-120 Silver 0.197 0.0050 mg/L 0.2000 98 80-120 Thallium 0.516 0.020 mg/L 0.4999 103 80-120 Zinc 0.491 0.040 mg/L 0.5001 98 80-120 Matrix Spike (P9E0531-MS1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Antimony 0.393 0.020 mg/L 0.5000 BRL 79 75-125 Arsenic 0.503 0.020 mg/L 0.5001 BRL 101 75-125 Beryllium 0.483 0.0020 mg/L 0.4998 BRL 97 75-125 Cadmium 0.487 0.0020 mg/L 0.5000 BRL 97 75-125 Chromium 0.492 0.010 mg/L 0.5001 BRL 98 75-125 Copper 0.478 0.010 mg/L 0.5001 BRL 95 75-125 Lead 0.478 0.0050 mg/L 0.5001 BRL 96 75-125 Nickel 0.483 0.010 mg/L 0.5001 0.000366 97 75-125 Selenium 0.536 0.020 mg/L 0.4999 BRL 107 75-125 Silver 0.177 0.0050 mg/L 0.2000 BRL 88 75-125 Thallium 0.497 0.020 mg/L 0.4999 BRL 99 75-125 Zinc 0.486 0.040 mg/L 0.5001 BRL 97 75-125 Matrix Spike Dup (P9E0531-MSD1) Source: 9050492-01 Prepared & Analyzed: 05/31/19 Antimony 0.403 0.020 mg/L 0.5000 BRL 81 75-125 3 20 Arsenic 0.502 0.020 mg/L 0.5001 BRL 100 75-125 0.4 20 Beryllium 0.480 0.0020 mg/L 0.4998 BRL 96 75-125 0.7 20 Cadmium 0.485 0.0020 mg/L 0.5000 BRL 97 75-125 0.5 20 Chromium 0.488 0.010 mg/L 0.5001 BRL 98 75-125 0.9 20 Copper 0.475 0.010 mg/L 0.5001 BRL 95 75-125 0.6 20 Lead 0.476 0.0050 mg/L 0.5001 BRL 95 75-125 0.5 20 Nickel 0.481 0.010 mg/L 0.5001 0.000366 96 75-125 0.5 20 Selenium 0.530 0.020 mg/L 0.4999 BRL 106 75-125 1 20 Silver 0.176 0.0050 mg/L 0.2000 BRL 88 75-125 0.1 20 Thallium 0.495 0.020 mg/L 0.4999 BRL 99 75-125 0.4 20 Zinc 0.484 0.040 mg/L 0.5001 BRL 97 75-125 0.4 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Sample Extraction Data Prep Method: 3010A Lab Number Batch Initial Final DatelTime 9050492-01 P9E0531 50 mL 50 mL 05/31/19 8:15 9050492-02 P9E0531 50 mL 50 mL 05/31/19 8:15 9050492-03 P9E0531 50 mL 50 mL 05/31/19 8:15 Prep Method: 7470A Lab Number Batch Initial Final DatelTime 9050492-01 P9E0529 20 mL 30 mL 05/31/19 8:10 9050492-02 P9E0529 20 mL 30 mL O5/31/19 8:10 9050492-03 P9E0529 20 mL 30 mL 05/31/19 8:10 Prep Method: 3510C GC Lab Number Batch Initial Final Date/Time 9050492-01 P9E0544 970 mL 10 mL 05/31/19 11:21 9050492-02 P9E0544 950 mL 10 mL 05/31/19 11:21 9050492-03 P9E0544 980 mL 10 mL 05/31/19 11:21 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 9050492-01 P9E0534 950 mL 1 mL 05/31/19 8:26 9050492-02 P9E0534 980 mL 1 mL 05/31/19 8:26 9050492-03 P9E0534 990 mL 1 mL 05/31/19 8:26 Prep Method: 200.7 Lab Number Batch Initial Final Date/Time 9050492-01 P9E0533 50 mL 50 mL 05/31/19 7:15 9050492-02 P9E0533 50 mL 50 mL 05/31/19 7:15 9050492-03 P9E0533 50 mL 50 mL 05/31/19 7:15 Prep Method: 3010A Lab Number Batch Initial Final Date/Time 9050492-01 P9E0532 50 mL 50 mL 05/31/19 7:10 9050492-02 P9E0532 50 mL 50 mL 05/31/19 7:10 9050492-03 P9E0532 50 mL 50 mL 05/31/19 7:10 Prep Method: 7470A Lab Number Batch Initial Final Date/Time 9050492-01 P9E0530 20 mL 30 mL 05/31/19 8:10 9050492-02 P9E0530 20 mL 30 mL 05/31/19 8:10 9050492-03 P9E0530 20 mL 30 mL 05/31/19 8:10 Prep Method: 5030B Lab Number Batch Initial Final Date/Time 9050492-01 P9E0549 10 mL 10 mL 05/31/19 8:57 9050492-02 P9E0549 10 mL 10 mL 05/31/19 8:57 9050492-03 P9E0549 10 mL 10 mL 05/31/19 8:57 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/526-0409 , .�.. _ ....,...w a � _ _ ..�......� Full -Service Analytical 8 PRISM Environmental Solutions PAGE__ OF - QUOTE # TO ENSURE PROPER BILLING: YES NO N/A _ Samples INTACT upon arrival? 449 Road •Charlotte, NC 28217 Project Name:i wy �� (c.�� Received ON WET ICE? - oneSpr7041529 Phone 704/528-ti364 Fax: 704/525-0409 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) PROPER PRESERVATIVES indicated? - Client Company Name: 'Q* �JC—t--i t `Please ATTACH any project specific reporting (QC LEVEL I II III IV) Received WITHIN HOLDING TIMES? provisions and/or QC Requirements CUSTODY SEALS INTACT? Report To/Contact Name: L 'rlvoice To: VOLATILES reed W/OUT HEADSPAC _ Reporting Address: Address: Sj_ �� (�i-�V�. �-- PROPER CONT E used? _ 2� TEMP: Therm I Observe -C / Corry . °C Phone: 10fax(Yes) ): Purchase Order NodPilling Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL Email Addres : A 1 •:a�r��� (�C. L cv A nt::, r a 1`11% Ka Requested Requested Dete KDay ❑ 2 Days ❑ 3 Days ❑ 4 Days 0 5 Days Certification: NELAC DoD FL NC EDD Type: PDF E;cel Other "Working Days" ❑ 6-9 Days 7 Standard 10 days U Rush Work Must Be Site Location Name: (u r`� T-� Pre -Approved Samples received after 14 00 will be processed next business day. Sc OTHER N/A Site Location Physical Address: 51Q b Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO� '(.-- 2-- (SEE REVERSE FOR TERMS 8 CONDITIONS REGARDING SERVICES RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sample Iced Upon Collection: YES NO TIME MATRIX SAMPLE CONTAINER I ANALYSIS REQUESTED, CLIENT SAMPLE DESCRIPTION DATE COLLECTED COLLECTED MILITARY (SOIL, _ PRESERVA-/$� � REMARKS PRISM LAB HOURS WATER OR *TYPE SLUDGE) SEE BELOW/ NO. SIZE TIVES �0 ID NO. MQW, \ = k �d 1 M 13 M + 03 Sampler's Signature Y lc- .. Sampled By (Print Name) &�t!C. CwL-�,� Affiliation , . Upon relinquishing, th Chain f ustody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be submitted i writing t the Pris Project Manager. There ill any changes after analyses have been initialized. PRISM USE ONLY Relinquished natur RIZFeive atuto) _ at Mil ryi rs Additional Comments: Site Arrival Time - Rein o 1 na , rvod By- (Si 7 Det Site Departure Time: Relinquished By (Signature) Field Tech Fee: Recgived F r , s L ratones By: Date Mileage 'Nb Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT W H CUSTft S L FOR NSPORTATION TO THE LABORATORY. Group SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST CDC UNTIL RE I D AT THE LABORATORY. �^t 77 � S �I ❑ Fed Ex ❑ UPS ❑ Hand -delivered ❑ Prism Field Service ❑ Other V `' 19r'1lJCJ: Ua t: I bKUUtVUYYAI CK: UKIMINIF410 YVAI CK: SULIU WAb I t: i KtrKA: GtKGLA LANDrILL ! OTHER: ❑NC❑SC ❑NC ❑SC I ❑NC ❑SC ❑NC ❑SC El NC ❑SCI ❑NC❑SC' ❑NC ❑SC ❑NC ❑SC' ❑NC ❑SC El ❑ _ ❑ _. ❑ ❑ ❑ ' ❑ ❑. I ❑ *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ENGINEERING ALTERNATIVES ANALYSIS N OVA July 8, 2019 NCDENR - DwION OF WATER RESOURCES - NPDES COMPLEX PERMrMNG UNrr 1617 Mail Service Center Raleigh, North Carolina 27699 Subject: Engineering Alternative Analysis (EAA) CHARLOTTE METRO OFFICE TOWER CONSTRUCTION Charlotte, North Carolina NOVA Project Number 2019008 NOVA Engineering and Environmental, Inc. (NOVA), on behalf of Childress Klein, is requesting a NPDES permit be issued for water generated from dewatering operations during the construction of a new high-rise office building. Once construction below the groundwater table is completed, the collection and discharge of on -site water will be terminated. BACKGROUND INFORMATION The Subject Property consists of six (6) land parcels referenced by Mecklenburg Tax Assessor's office as Property Identification Numbers (PINs) 12505302, 12505303, 1250304, 1250306, 1250307, and 125308 with corresponding addresses 522 South College Street, 518 South College Street, 510 South College Street, 509 South Tryon Street, 521 South Tryon Street, and 525 South Tryon Street, respectively. The Subject Property encompasses a total of approximately 2.09-acres of active construction. A previous Phase II Environmental Site Assessment performed by Anchor QEA dated April 2017 identified soil and groundwater impacts resulting from the historical use of the subject Property as a garment cleaning facility, an automotive sales and repair facility, and an automotive painting facility. Petroleum impacts to soils were reported in four (4) of the nine (9) soil borings. Chlorinated solvents above NC DEQ 2L regulations were reported in the groundwater samples in two (2) of the five (5) groundwater monitoring wells installed. NOVA collected groundwater samples from three (3) of the on -site monitoring wells on May 30, 2019. The remaining two (2) monitoring wells were dry at the time of NOVA's May 2019 sample collection. The collected samples were analyzed for Volatile Organic Compounds (VOCs) by United States Environmental Protection Agency (US EPA) Solid Waste (SW)-846 Method 8260D, Semi -Volatile Organic Compounds (SVOCs) by USEPA SW-846 Method 8270E, Chlorinated Pesticides by USEPA SW-846 Method 8081, and Total and Dissolved Metals by USEPA SW-846 Method 6010D and 7470A. Tetrachloroethylene (0.72-pg/L) and total Chromium (0.029-pg/L, 0.020-pg/L, and 0.024-pg/L) were identified above NC DEQ 2L regulatory standards. Dissolved Chromium was not detected above laboratory detection limits. PROFESSIONAL I PRACTICAL I PROVEN 5401 Reagan Drive, Suite 8, Charlotte, North Carolina 28202 t. 980.321.4100 / f. 980.321.4099 / usanova.com Engineering Alternative Analysis July 8, 2019 South College Street and South Tryon Street NOVA Project Number 2019008 PROJECT DESCRIPTION The project consists of the construction of a new high-rise office building located on six (6) land parcels encompassing approximately 2.09-acres. Foundation construction will extend below the groundwater table which will require dewatering for an estimated period of four (4) months. Currently, dewatering pumps will be placed in the areas of excavation with the water being routed through a pretreatment system prior to discharge into the municipal storm water system located along South Tryon Street and South College Street. The storm drains discharge to an unnamed tributary of Little Sugar Creek, part of the Sugar Creek watershed. Applicant Information Childress Klein 301 South College Street, Suite 2800 Charlotte, North Carolina 28202 (704) 343-4396 Attention: Mike Haney E-mail: mike.haney@childressklein.com Facility Charlotte Metro Office Tower Construction South Tryon Street and South College Street Charlotte, North Carolina EEA Preparer NOVA Engineering and Environmental, Inc. 5401 Reagan Drive, Suite 8 Charlotte, North Carolina 28202 (980) 321-4100 Attention: Keith Rice, Senior Geologist E-mail: krice@usanova.com ENGINEERING ALTERNATIVE ANALYSIS Evaluation of potential restrictions to a wastewater discharge to surface waters Based on review of Low -Flow Characteristics of Streams in North Carolina, published by the USGS and issued in 1993 and the Low -Flow Characteristics and Flow -Duration Statistics for Continuous -Record Stream Gaging Stations in North Carolina through 2012, published by the USGS in 2015; Little Sugar Creek is a Class C (fishable/swimmable) water located within the Catawba River Basin. The USGS reports provide the following information: N OVA Page 2 Engineering Alternative Analysis July 8, 2019 South College Street and South Tryon Street NOVA Project Number 2019008 • Drainage Area - 40.80 square miles • Summer/Winter 7Q10 - 34 cubic feet per second (cfs) • 30Q2 Flow Statistics - 87 cfs • W7Q10 Low -Flow Yield - 55 cfs • Qavg Unit Flow Yield - 12 cfs/square mile Little Sugar Creek is listed on the 303(d) as an impaired waterway. The total maximum daily limits (TMDLs) include fecal coliform (9.41012 cfu/100mL), dissolved oxygen (no less than 5.Omg/I for the daily average and no less than 4.Omg/I for a minimum instantaneous value during 7Q10 conditions), and turbidity. NON -MUNICIPAL FLOW PROJECTIONS Based on similar construction projects from the Charlotte downtown area, it is estimated that the dewatering pumps will produce a flow rate of approximately 50 gallons per minute (72,000 gallons per day). EVALUATION OF FEASIBLE ALTERNATIVES Alternative A: Connection to Existing Wastewater Treatment System Ms. Sarah Daley, Environmental Compliance Supervisor with Charlotte Water sent a response letter to NOVA on May 28, 2019 stating that they do not accept groundwater discharges as referenced in the City of Charlotte Sewer Use Ordinance Section 23-79 (b)(14). Alternative 8: Land Application Based on the location of the project within the downtown area of Charlotte, this alternative is not feasible due to the limitations of land area available. Alternative C: Infiltration Galleries Based on the location of the project within the downtown area of Charlotte, this alternative is not feasible due to the limitations of land area available. Alternative D: In -Situ Remediation Wells Based on the proposed new construction utilizing dewatering pumps, this alternative is not feasible due to excess water entering the system and the limitation of land area available. Alternative E: Closed Loop Remediation Wells Based on the proposed new construction utilizing dewatering pumps, this alternative is not feasible due to excess water entering the system and the limitation of land area available. N OVA Page 3 Engineering Alternative Analysis July 8, 2019 South College Street and South Tryon Street NOVA Project Number 2019008 Alternative G: Discharge to Surface Waters Discharging removed groundwater into the municipal stormwater system located along South Tryon Street and South College Street is feasible for this project. Charlotte Water has approved the use of the storm drain system as it is not anticipated to create hazardous conditions. Neither Mecklenburg County nor City of Charlotte have returned a completed Local Government Review Form. Consequently, the certified mail receipts and delivery tracking information is attached as proof of delivery. If you have any questions, or if we may be of further assistance, please do not hesitate to contact US. Sincerely, NOVA Engineering and Environmental, LLC Jason K. Harris Keith Rice Staff Geologist Senior Geologist Attachments: Certified Mail Receipts Delivery Tracking Information N OVA Page 4 -0 Ln Domestic S For CHFjft Q1 PC� eOj FU Certified Mal) Fee ED $3. 0 I_II I%Il $ 5iI Extra Services & Fees (check box, add f" epp opdale) O ❑ Return Receipt (hardwpy) $ I- . - C3 []Return Receipt (electronic) $ IA - 11-1 Postmark ❑ Certified Mail Restricted Delivery $ $1�0 ti,-„ Here ❑ Adult Signature Required $ ❑ Adult Signature Restricted Delivery $ Postage cc 0 $C1. 5 0 Total Postage and Fees 16/1 °/?i 119 $ ESent To -------------------- Si eei rindApt Ni.; or Ft0 tz No. City State IP+4+ Cl ,ter loa' L Or 2'Q20 Z Postal CERTIFIED MAIL' RECEIPT co 02 Fu Certified Mail FeOt170 o �3 . `� 50 Ir $ Extra Services & Fees (check box, adid fee di m'w!la) ❑ Return Recelpt (hardcopy) $1 I II 1 Postmark ❑ Return Receipt (electronic) $ � Here C3 ❑ Certified Mail Restricted Delivery $ $1 � ❑Adult Signature Required $ dry ❑ Adult Signature Restricted Delivery S Postage $j I � j5 _n 06/18/2019 ri $ Total Postage and F s. 05 Sent To pFFrLFJ Qt t01A �( IN ANACVF� - ----------------------- - $Beef rind Apt.lV — of FtCJ �oz No. I 'V- ,S'Etarf 17�(PDei tA5( .4' ....... �irySfafe,ZIP+4e_l�C�