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HomeMy WebLinkAboutWQ0001105_Monitoring (Report)_20190627L - L trien- Feeding the Future - June 27, 2019 NCDEQ DIVISION OF WATER RESOURCES GROUNDWATER SECTION — PERMITS AND COMPLIANCE UNIT 1636 MAIL SERVICE CENTER RALEIGH, N. C. 27699-1636 Re: Semiannual Groundwater Monitoring Data Permit No. WQ0001105 Cooling Ponds Facility Wastewater Recycle System PCS Phosphate Inc. - Beaufort County Per Condition No. 20 of the above referenced permit, please find attached the semiannual groundwater monitor well sampling report for samples taken in May 2019. Also attached are a GW -59A Compliance Report Form and a Spreadsheet addressing line item 5 in the GW -59A Form. Please do not hesitate to call me at 252-322-8283 should you have any questions concerning this. Sincerely, kO,IDOAlt� 11v D. Daniel Winstead III Senior Environmental Engine, PCS Phosphate PC: David May — DWR, WaRO (w/attachments) 12-02-003-02 (w/attachments) Irm 1530 NC Hwy 306 South, Aurora, NC USA 27806_ -- nutrien.com / GW -59A COMPLIANCE REPORT FORM Permit # WQ 0008570 ' (Submit one each monitoring period with GW -59 forms) Enter date monitoring results were due. (6-30-2019) Will this monitoring report (GW -59 and GW -59A) be YES NO submitted after the established due date? X 2 Was any required information missing on the GW -59 report forms? YES NO X IF the answer to question 1 or Z is "YES" list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. No access to wells MW2-3A and MW2-3B. 3 re any of the monitor wells in need of repair or maintenance(damaged casing, unlocked or missing cap, YES NO missing identification plate, area overgrown, etc.)? if the answer is "Yes" contact the Regional Office for X guidance. 4 YES NO Are any monitored constituents equal to or above the established standards? X the answer to question 4 is "NO" skip to section 8. K the answer to question 4 is "YES", list the affected wells individually with constituent(s) and concentrations(s) exceeding standards in the space provided below: See attached spreadsheet for details. 5 For the constituents identified in question 4 above, have standards been exceeded previous for the same YES NO constituent(s) in the same well(s) X if the answer to question 5 is 'NO", skip to section 8. K the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). See attached spreadsheet. g YES NO Are the monitoring wells listed in section 5 located at or beyond the review boundary? X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Contacted the WaRO on 6/27/2019 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? X if the answer to question 7 is "YES", describe those actions in the space provided below. K the answer to question 7 is "NO", contact the Regional Office within 90 days,• an evaluation may be required to determine the impact the waste dis o�ystem is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation. fines. and/or end . The Cooling Pond Remedial Action System Design Report was submitted to NCDENR on September 27, 1990 and approved by NCDENR January 7, 1991. The system was installed by PCS Phosphate between July 8, 1991 and April 9,1992. In 2008 the cut-off wall was extended on the south perimeter of CP -1. This action was taken due to the location of the active mine pit. 8 The person completing this portion (GW -59A) of the monitoring report should sign below and submit this form with GW -59 forms for required wells to be address provided at the top of the current GW -59 form. ..................................................................................................................... I:Etereby:aslciiowfectgethat:theabove:irifoiriiatiop...... eval...... arid.....ir ..........................brie .0..... . ..................................................................................................................... (Ciiinpliance:Repo :GW 9A1... true nd.... te.......... .9 (oZ�2vq Signaturl of Permittee (or Authorized Agent) Date r -Ra: taamptes Tor metals were collected unfiltered U Yes No . .:... .........................................:....................:.:...............:.:.:. •. . : . :. nwr. J `:[i ........, :................................. RTM EN :........:........ :...... .......:....:...... i F EtV1Yf<iCSI�EMEN ;:;:::;:.I'.;.;.;.;.;.;.;.;.:4:,:,:.:.:..,,...;....,... � 8�3VA�l�AL'•R�Sb1aR�f��; :::::::::::::::::::: ::. . ................... .......................................:.:.............:....................:.:.................:...... PRSP.................................................:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:::::.:.:.:::.:.:.:.:. ..r1E�#ER:12E$flEIf�CES�INFQf#�IFA: N:PROC Coliform:" MF Fecal N/A mg/L /100mL L 1 N . . x'1626- .. � ... .. .948.80........ .. FACILITY INFORMATION PERMIT.#: ' W00008570 DATE 01/31/23 Facilty•Name: PCS PHOSPHATE'CO., INC.-Aurora'Division ,.'-.EXPIRATION Non -Discharge X UIC X Permit Name (if different): NPOES Facility.Addresss: 1530 NC Hwy 306 South TYPE OF PERMITTED OPERATION, BEING -MONITORED Aurora, NC 27806 County: `Beaufort' -.1 1 Contact Person: Danny'Winstead Telephone: (252)322=8283. Lagoon ' Remediation: Infiltration Gallery lt Locations/Site:Name: #1 Cooling Pond No. of Wells to'be Sampled 1.2 Spray.Field , X Remediation:. Rotary Distributor ' Land Application of Sludge ..�. . 1 Identification Number (from Permit): MW1-3A For Groundwater Treatment rWel Depth: 21.35 ft. Well Diamter:. 2 inch X Other water Source Heat Pump . systems check one: N/A eened;lnterval: 18.85 ft. to 20.85 ft.Influent (98) Note: Values should reflect dissolved and If,WELL WAS Depth to Water Level: 5:19 ft. below measuring point. Effluent (99) ' ' colloidal concentrations DRY tat time: Measuring Point is 2.85 . ft above land surface. Date sample collected: 5%23/2019 of sampling, MILILITERS of water, pumped/bailed before, sampling: -2100Date •. sample analyied; 5/2372019- to 6/26/2019 check Field Analysis: ,pH - 5.4 , Specific.. Conductance 2222 uMhos Laboratory Name: PCS PHOSPHATE = here:; Temp. 22:0 oC,•Odor NONE- Appearance:: CLEAR - Certification NO(s) ; 330 10 r -Ra: taamptes Tor metals were collected unfiltered U Yes No and field-acidifieduYes [No i Coliform:" MF Fecal N/A mg/L /100mL Nitrite (NO2 as N) Nitrate {NOs as N) N/A mg/L ` mg/L Ni -Nickel ..1. /A . • ' ug/L '. a N/A : N/A Coliform: MF'Total N/A /•100ml- Phosphorus: Total as P 102.00 m /L Pb -Lead Zn'—Zinc N/A ug/L. l (Note Use MPN•method f.or-highly turbid samples) orthophosphate P N/A mg/L -Ammonia`N&ogen mg/L. DH Splved.SOhds: TOtal' p (when analyzed) 1780 5.6 • m /L _ g Al um -Ba Barium N/A mg/L Other (Specify Compounds and Concentration Units) .. s '. , TOC - N/A units mg/L - Ca -Calcium N/A ug/L mg/L Fluoride MIBK 4'10 mg/L N/A Chloride 39.0 mg/L Cd- `Cadmium, N/A, • ug/L ; :,N/A- Ag -.Silver ug/L.. N/A Arsenic 730 ug/L Chromium: Total N/A ug/LSe= Selenium N/A _ Grease and Oils N/A mg/L Cu -Copper N/A m /L' g Sodium 332' m g/I i ...Phenol, N/A mg/L Fe - Iron N/A ug/L Organics:(GC, GC/MS, HPLC) Sulfate772:0 mg/L Hg - Mercury. N/A ug/L (Specify test method #. Attach lab report.) # Specific Conductance` Total N/A uMhos K- Potassium= N/A mg/L Report attached? Yes (1) No X (2) Ammonia' N/A mg/L Mg - Magnesium N/A mg/L VOC method#;. TKN, as, N' N/A mg/L Mn - Manganese 1517 - ug/L method# method#: WIN IL NOTE: Mark D. Johnson, General Manager ' Permittee (oliALforized Agent) Name and Title -.Please type or print i GW=59 Rev.4198 - - _ Signature of ermittee.(or Authorized Agent) (D e) - MENi :..: ........ ..........:.................. .................. EfitiN &3A Q. ..... V$0NQFWI�RRESbEICESaNF TOPR .: GROW - AIG .ARE.. .. ..:. r. 8� : t NG-. 1.Gfl 626- •' '�' � ': ; :::: :.:: `. ;?':` FACILITY INFORMATION Facilty Name: PCS PHOSPHATE .CO. INC. - Aurora Division Permit Name (if different): Facility.Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact'Person: Danny Winstead Telephoner (252)322-8283 'WeKtocations/Site Name: #1 Cooling Pond No. of Wells to be,Sampled. 12 Well- Identification Number (from Permit): MW1-3B For Groundwater Treatment Well,Dspth '33.00 -ft. Well Diamter: '2 inch sygc.mg cheek on.:- . Screened Interval': 30.10 ft. to 32.10. -ft. Influent (98)' Depth to Water Level:. 6.30 %.below measuring.point.� Effluent (99) . Measuring Point is 290 ft -above land surface. MILILITERS of water pumped/bailed ,before sampling: -2100' Field Analysis: -pH 6.3 , ,Specific Conductance 3443. uMhos Temp. 20.9 oC, Odor NONE Appearance: CLEAR PERMIT #: -. W00008570' EXPIRATION DATE: 01/31/23' and field acidified UYes uNo ) Non -Discharge X UIC X. NPDES. mg/L Nitrite (NO2 as N) TYPE OF PERMITTED' OPERATION.BEING.MONITORED mg/L'Ni -Nickel Lagoon Remediation: Infiltration Gallery ' ug/L Spiray'Field , X Remediation N/A /100mL - Rotary Distributor Land Application of Sludge N/A mg/L' X Other' Water Source Heat Pump . N/A' 6g/L' -` Note: Values should reflect dissolved and If WELL WAS, /100mL Colloidal concentrations DRY.at time mg/L Date sample collected: 5/23/2019 of sampling,,` _ Date sample analyzed: _ 5/23/2019 to. ,6/26/2019 check ' Orthophosphate Laboratory Name: PCS PHOSPHATE . here: Ammonia Nitrogen Certification No(s) 330 10 Dissolved. Solids. Total 2920 mg/L , r••s!►rw1V1t1 r_Kb.-{samples Tor metals were collected unfiltered U Yes U No and field acidified UYes uNo ) N/A mg/L Nitrite (NO2 as N) N/A mg/L'Ni -Nickel N/A ug/L Coliform'. MF. Fecal 'MF N/A /100mL - Nitrate (NO3 as N) N/A mg/L' Pb - Lead. - . N/A' 6g/L' -` Coliform` Total , N/A /100mL Phosphorus: Total as P55.000 mg/L Zn -Zinc N/A ug/C; (Note Use MPN method forhighly,.furbid samples) Orthophosphate N/A _ mg/L. Ammonia Nitrogen mg/L' Dissolved. Solids. Total 2920 mg/L , Al - Aluminum. ' N/A mg/L .' Other (SpeciN Compounds and Concentration Units) -pH.(when analyzed) 6.6 units Ba - Barium . N/A ug/L Fluoride 0:71 mg/L' TOC N/A mg/L Ca = Calcium N/A mg/L MIBK N/A' . - ug/L- -Chloride' ` 55.0 mg/L Cd- Cadmium N/A ug/L Ag-- Silver N/A ug/L Arsenic < 5,0 ug/L., Chromium: Total N/A Ug/L Se -.Selenium. N/A. ug/L Grease•and Oils N/A' mg/L Cu - Copper N/A mg/L Sodium 315 - mg'l Phenol:' N/A mg/L Fe --'Iron N/A ug/L .- Organics: (GC, GC/MS, HPLC): Sulfate 'Specific 1420.0' . mg/L Hg:- Mercury r N/A ug/L (Specify test method #. Attach lab report.) Conductance N/A,..- uMhos K- Potassium N/A mg/L Report attached? Yes. (1) . No X (2) Total Ammonia . N/A mg/L Mg - Magnesium N/A mg/L VOC method#'" TKN as'N. N/A mg/L Mn -,Manganese 7.86 ug/L method# 7 method# rcertify;that, to the best of my:kn6wiedg'e and belief. the . analysis by a bW[R-certihed lab'o-ratory. I am aware that information submitted there -are significant in th; is report is true, accurate, and, complete, penalties for submitting false information, and including the that the laboratory possibility analytical data was produced using approved methods of of fines and imprisonment for knowing violations. NOTE: Mark D: Johnson General Mana er Permittee (o A thorized"Agent) Name and Title - Please,type or print GYN-59,Rev 4/98,' Signature of ermittee (or Authorized Agent) (Date) PARAMETERS::: (Samples for metals were collected unfiltered U Yes U No and field acidified Yes, No) COD N/A. mg/L Nitrite (NO2 as"N) N/A mg(L Ni - Nickel,;N/A , ug/,L. ' Coliform;, MF _Fecal Coliform:.- N/A /100mL . Nitrate,(NO3,as.N)- N/A' mg/L• - 'Pb'- Lead.,-, N/A ug/L_ MF Total ' N/A LTOOmL Phosphorus: Total as P 1.560, mg/L Zn -Zinc : N/A ' ug/L . ` .. (Note: use MPN method tor, nignly turbid samples) ' Orthophosphate N/A mg'/L :. Ammonia Nitrogen mg/L Dissolved Solids: Total 4080 mg/L Al - Aluminum N/A mg/L other (Specify compounds"and'conceritration units), pH (when''analyzed) 6.9 ' � units. Ba - Barium N/A ug/L .'Fluoride 1.94 mg/L TOC N/A mg/L Ca =Calcium N/A mg/L, MIBK N/A' ug/L, Chloride 42.0 mg/L . Cd-* Cadmium N/A •ug/L Ag - Silver N/A ug/L:' ' Arsenic < 5:0 ug/L' Chromium: Total N/A ug/L:, Se- Selenium - N/A ug/L'. _ a Grease and Oils Phenol N/A . mg/L " Cu'- Copper N/A mg/L Sodium 436 m /I 9 N/A mg/L Fe --Iron .... N/A ug/L •Organics: (GC, GC/MS, HPLC) Sulfate 2070.0 mg/LHg - Mercury N/A ug/L (Specify test method #: Attach 1'6. report) . Specific Conductance N/A uMhos K- Potassium N/A mg/L Report attached? Yes(1 ) No. 'X : (2)- Total`Ammonia N/A mg/L' Mg - Magnesium N/A mg/L VOC method# , TKN as:N N/A mg/L Mn - Manganese -543 ug/L method#' method# I certify, that, to the best of ey knowledge analysis by a DWR-cer�ifiedlaboratory. and belief, the�information i am aware thatthere are; significant suibmitted'in this report is true accurate, and complete, penalties for submitting false information, and including the that the laboratory possibility of analytical data was produced' using approved methods of fines and imprisonment for knowing violations. NOTE: Mark D. Johnson General -Maria er Permittee (of horized Agent) Name and Title.- Please type orprint GW, -,59 Rev 4/98' Signature of rmittee (or Authorized Agent) - . (Da ) vVeli'Mentification Number (from Permit): MW1-46ForGroundwater Treatment X Other Water Source Heat Pump Well Depth:. 43.25 ft. Well Diamter: 2 inch Systems check one:. Screened Interval: 40.23 ft. to 42.23 ft. Influent (98) Note: Values should reflect dissolved and If :WELL WAS' Depth to Water. Level:.. 6.17 ft. below measuring point. Effluent (99) coiloidal'con'centrations DRY at time . Measuring, Point is 3.15, ft above land surface. Date sample collected: 5/29/2.019 of sampling, ' MILLITERS of water pumped/bailed before sampling: 3600 Date sample analyzed: 5/29/2019 to • 6/2612019 check Field Analysis::pH 6.3 , , Specific Conductance 4507 uMhos Laboratory Name: PCS PHOSPHATE here: Temp... 23.0. oC, Odor NONE' Appearance:. CLEAR Certification No(s)` 330 10; PARAMETERS:, (Samples for metals .were collected unfiltered Exl -Yes -No and field acidified . []Yes D No ) -COD,N/A 'MF mg/L, Nitrite-(NO2 as N) N/A mg/L Ni - Nickel 'N/A ug/L Coliform: Fecal N/A /100mL Nitrate (NOs as N) N/A mg/L Pb - Lead N/A ug/L Coliform: MF Total N/A /1,00mL. Phosphorus: Total as P 18.400 mg/L Zn - Zinc. N/A , ug/L . (Note: Use MPN method for highly turbid samples) Orthophosphate N/A mg/L• - Ammonia Nitrogen mg[L Dissolved Solids: Total 4010- mg/L Al - Aluminum N/A mg/L Other (Specify Compounds and Concentration Units) _ pH (when.analyzed) .6.6 units Ba - Barium N/A ug/L Fluoride 3,39 mg/L,: . TOC N/A_. mg/L Ca-- Calcium -N/A m9 /L MIBK N/A: ug/L Chloride. 47.0. - mg/L Cd- Cadmium N/A ug/L Ag —Silver N/A ug/L, Arsenic . ' 10 ug/L Chromium: Total N/A ug/L Se- Selenium,N/A , .ug/L Grease'and .Oils N/A mg/L . ' Cu'- Copper N/A mg/L Sodium 379— mg/I Phenol ` N/A mg/.L _ Fe-- Iron N/A . ug/L - Organics: (GC, GUMS, HPLC) Sulfate2040.0 mg/L Hg - Mercury,- N/A - ug/L (Specify test method #: Attach lab -report:). , Specific Conductance N/A uMhos K-. Potassium N/A mg/L Report attached?Yes- (1) No X (2) 0c Total Ammonia N/A. mg/L. Mg - Magnesium L N/A mg/L VOC method# - TKN as. N . N/A mg/L Mn - Manganese 731 ug/L method# ' method# 1 certify that� to the be§tRf:my knowledge and analysis by a bVVIR-c;rti6ed�6boi-atory. I am belief, the� information submitted aware that there are significant in this report is tr6e, accurate. and: complete, penalties for submitting false information including and that the the laboratory analytical data was prodUced using approved methods of possibility of fines and imprisonment for knowing violations. 2. NOTE' . Mark D. Johnson, General Manager Permittee IfIt ohzed Agent) Name and Title - Please type or print GW -59 Rev,4/98 Signature of miittee (or Authorized Agent) (Date) and field acidified FIYes nNo.l COD N/A. - mg/L Nitrite (NO2 as N) N/A, mg/L Ni -"Nickel 'N/A. ug/L Coliform: MF Fecal N/A /100mL Nitrate (NO3.as N) N/A mg/L Pb.- Lead N/A Lig/L %.,C�oliform: MF Total N/A, /100mL .'Phosphorus: 'Total as -P 0.520 mg/L Zn - Zinc WA ugjL (Note:: Use MPN method f6r highly turbid samples) Orthophosphate' N/A mg/L Ammonia Nitrogen mg/L' Ditsbilvcid'Sollds: Total PH (when,analyzed) 3240 7.1 Al - Aluminum' -Bariumug/L, N/A mg/L Other (Specify Compounds and Concentration units) units Ba- N/A Fidorid e. 4.58 m g/L TOC N/A mg/L • Ca -.Calcium N/A mg/L MIBK N/A ug/L Chloride 23.0 mg/L Qd- Cadmium N/A -ug/L Ag - Silver N/A ug/L,,.,. Arsenic, , < 5.0 ug/L Chromium: Total N/A 6g/L Se- , S61enium uj/L Grease and 0 lls 'Phenol N/A/A mg/L CuCU 7 Copper N/A mg/L So'diumi 231 mg/1 . N/A mg/L Fe - Iron N/A ug/L Organics: (GC, GC/MS,.HPLC) Sulfate 1950.0 mg/L. Hg - Mercury. N/A ug/L (Specify test,method'#., Attach lab reporL ) -:Specific Conductance N/AuMhos K- Potassium N/A_ mg/L Report attached? Yes (1) No. Total Amr4onia N/A mg/L Mg -. Magnesium N/A mg/L VOCI_ method#., .(2) TKN'as.N N/A mg/L' Mn - Manganese 103''ug/LI method# meth' od# ----------- -- :I certify that� to the:best of m y'knowledge I analysis by a D VVIR -certified laboratory. and belief, the I am, aware that information there: are significant submitted I _fn tHs report is truej accurate, and penalties for SUbmitting false information, complete, and including that the laboratory analytical data was prodUced Using approved methods of the possibiky of fines and imprisonment for knowing violations. NOTE: Mark'D. Johnson: General Manager Permittee jofjAuthorized Agent) Name and Title.- Please type or print GW -.59 Rew4/98 lq Signature Vf Permittee (or Authorized Agent) (Dato IPI IAMPM-0 -AI:ILI I Y INFORMATION =acilty Name: PCS PHOSPHATE CO.; INC. -'Aurora Division 'ekmitName.(If different): -acilityAddeesss:•' 1530.NCHwy 306.South Aurora, NC' 27806 County:.geaufort' ontact Person: Danny Winstead Telephone: (252)322-8283 WelI Locations/Site Name: #1 Cooling Pond No. of Wells to be Sampled. W-vvAtil rP%mm ir- i crw tU es o and field acidified UYes . - NO D: N/A .. mg/L Nitrite (NOz as N) N/A mg/L Ni - Nicker N/Aug/L • : " '• Coliform. MF Fecal "MF'-TOtaI, N/A 4100mL Nitrate•(NO3 as N). N/A mg/L Pb'- Lead N/A u ' L Coliform' N/A /100mL Phosphorus: Total'as, P 2.700 mg/L Zn -,Zinc - 'N/A ;ug/L,: (Note use:nnPN method for highly turbid samples) Orthophosphate. N/A mg/L Ammonia Nitrogen mg/L Dissolved Solids:: Total 5200 _ mg/L AI'- Aluminum N/A mg/L Other (specify Compounds and Concentration Units) - ..pH (When'analyzed) 6.9, units Ba = Barium N/A ug/L .. Fluoride 13.70- mg/L: TOC WA - mg/L' Ca -'-,Calcium- N/A m /L MIRK. - 'N/A u g Chloride 91.0 mg/L'' Cd -'Cadmium N/A ug/L Ag -,Silver N/A lug Arsenic < 5.0 ug/L Chromium:,. Total - N/A. 'ug/L Se- Selenium N/A Grease and Oils, Phenol N/A mg/L Cu - Copper.. N/A _mg/L Sodium :454' .. . mg/I N/A': mg/L Fe -Iron , N/A ,..ug/L ;, Organics: (GCGUMS, HPLC) . Sulfate 2900 0.- mg/L_. Hg, -Mercury N/A ug/L {Specify test. method,#. Attach lab report.) Specific Conductance _ N/A -uMhos' K-Potassium N/A mg/L P- Report attached? Yes (1) No Total:Ammonia N%A mg/L Mg -Magnesium N/A mg/L VOG method# TKN,as N N/A mg/L Mn -Manganese 167 ug/L method#' method# NOTE Mark D. Johnson General Mana er ' ermi P tte ( thorized Agent Name and a Peas ) a Title - Please type or print GW -59 Rev 4/98 Signature o Permittee (or.Authorized Agent) (Date) ..Ri .NOWWAT..ER:QUA►�ITY::Mt�11TE1#2�M C .:... l.IA1G;REP4T:F�3tM i=AGILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC. Aurora Division Permit Name •(if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort �.ontact•P'erson: Danny Winstead Telephone: , (252)322=8283 Well Locations/Site Name: #1 Cooling Pond No. of Wells to be Sampled: 12 [i£ R7'MENI;QF.;EtVlt�CSNMENi:&iVAiI�AL:R�st`1LIR�ES . - Well uientification Number (from Permit): Well Depth: 33.00 ft. Well Diamter:. MW1-6AR 2 inches For Groundwater Treatment X Other Water, Source.NeatPump_ -.. systems Check one: ;r •_ :; Screened dnterval: 30,00 ft. to 32.00 ft. ,. I EDepth Influenf,(98) ' Note: Values should reflect dissolved, and if WELL WAS'' to WaterLevel:', 6.80 'ft. below. measuring point. Effluent (99) colloidal concentrations i' bRY at'ttme' Measuring Point is .3.05 MILLILITER; of'water ft above land surface. Date sample collected: 5122/2019' of sampling, pumped/bailed before sampling: 2100 Date sample analyzed: 5/22/2019 to 6/2672019 check Field.Analysis: pH 6.2 ,:Specific Conductance 1578 uMhos LaboratoryName: PCS PHOSPHATE here: Temp. 18.8• oC, Odor' NONE Appearance: CLEAR Certification No(s), 330 10 PARAMETERS: (Samples formetals were collected:unfiltered 'IX Yes a ' No and field acidified ❑Yes . DNo ) COD, N/A mg/L Nitrite (NO2 as N) _ N/A mg/L• Ni - Nickel N/A Coliform: MF. Fecal Coliform' N/A /100mL Nitrate (NO3 as. N) ' . . N/A' mg/L Pb - Lead. "N/A ug/L... ' MF Total N/A /100mL, Phosphofus: Total as P -. - 6.650 mg/L - Zn -Zinc : N/A ug: (Note: use•MPN method for highly;turbid samples) Orthophosphate N/A mg/ Ammonia Nitrogen . mg/L Qi§solved ;Solids:.Total 944 mg/L: AI - Aluminum: N/A -L mg/L Other (Spe6fyCompounds andConcentration units) pH (whe'n.a'nalyzed) TOC 6.1 units Ba - Barium N/A u /L Fluoride 9 `0'.72 mg/L , ° .. `:Chloride N/A mg/.L Ca - Calcium N7A mg/L % MIBK. N/A ug/L ' . Arsenic'. 52.0 mg/L' 11 Cd- Cadmium N/A ug/L- Ag - Silver N/A ; ug/L Grease and Oils. ug/L N/A mg/L. Chromium:• Total Cu N/A u /L 'Se -.Selenium mg/L Sodium N/A Phenol N/A mg/L --Copper Fe - Iron • N/A ug/L , -. Organics: (GC, GUMS, HPLC)_ 74 mg/I Sulfate: 527.0. mg/L• Hg'- Mercury , N/A, ug/L. (Specify. test method#. Attach lab report:) .'Specific Conductance Potassium N/A. mg/L Report -attached? Yes (1) -No. X Total Ammonia N/A mg/L- Mg--. Magnesium : UA mg/L VOC.. method#- ` .(2) TKN as'N' N/A mg/L. Mn - Manganese 703 ug/L method#.. method#. NATE: Mark D. Johnson General Manager d Agent) Name and Title - Please type orpri t Permitte (oVermittee GW -59 Rev 4/98 Signature of(or Authorized Agent) (ate) COD N/A mg/L Nitrite (NO2 as N) N/A.. , mg/L Ni :. Nickel N/A,.'. - I Coliform: MF Fecal' N/A /100mL Nitrate (NO3'as,N)/A mg/L PbPb-Lead N/A .ug/L• Ug/L Coliform. - MF Total N/A /100mL, Phosphorus', Total. as •P'- 0.885 mg/L • Zn - Zinc N/A ug/L (Note: use, MPN'me'thod,f6r highlyturbid samples) Orthophosphate N/A'. mg1L 'Ammonia Nitrogen. mglL,: _4 Dissolved Solids:-. Total 2370 mg/L_ Al - Aluminum'. N/A mgjL Other.(Specify Compounds and: Conoentration Units) pH-(wh60.analyzed - Y 6.7 units *'Ba -Barium N/A ug/L Fluoride 0.58 mg/L.:.,• TOC -N/A mg/L. Ca - Calcium N/A mg/L MIBK N/A Chloride - -63.0 _mg/L­Cd- Cadmium N/A ug/L Ag.- Silver N/A,, ug./L ug/L Chromium: Total 'N/A- ug/L Se Selenium N/A Grease -and Oils N/A mg/L CU-- Copper N/A mg/L Sodium 236 mgA --fhenol'; N/A mgjL Fe' - Iron -N/A ug/L'... Organics: -(GQ, GC/MS, HPLC). -Sulfate 1070:0 mg/L Hg - Mercury N/A ug/L (Specify -test method #. Attach lab report.),., Specific Conductance N/A UMhos. K- Potassium N/A mg/L' Report attached? Yes (1) No X (2)_. j Total Ammonia.. N/A mg/L Mg -. Magnesium N/A mg/L VOC method#' ..-,TKN,as N N/A mg/L, Mn -,Manganese 699 ug/L method#::t me thod# MINOR -NOTE: Mark D. Johnson'. General Manager Pe jfAfthorized Agefit) Name and Title- Please type or nnt GW:159,kev 4/98 Signature P6rmiffee (or Auth.orized,Ageht) -1 (Dat &) 77-7 k D. Johnson; General Manaaer fR.� .......... A�ITYi: . U ' G)ftOlMMTMNG .MEN P?a....,._..... �.Q�.E�iW�iQI�MEN�;&3JY1�1��.:RAS£111RCES.:.:.:....•.:.:.:.:.:.:. - C0 M� , . Iiia► F °::�:':�° ::::::':�: ° :'::��:� ;�::::::::::::::::::::::::::::: - • • - •:.:D�VISTbN.OF: .•.RE• • „ RCESaN�(.:�R�IIAT10fiI:PROCEB&ENl�. ::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::.:::.:.:.:::::.:.:::.:.:.:.:.:..:.........: .......... .ERT �.::.::::::::::�: :16fy'NIA�; S�#F�tICL:CEi�'�f�:.:.:.........................•........................................ . ........... ...................................... ... . ............................................ ...1.6 I . 2x626.....:. ;::.:.:.:.:.:.......�......................,.,t.•...:.1?I±orte.::1914):BG��s3tis . FACILITY INFORMATION Facilty.Name: PCS PHOSPHATE CO., INC.- Aurora-Division PERMIT #: W00008570 EXPIRATION DATE: 01/31/23 Permit Name (if different): Non-Discharge X UIC X Facility.Addresss: 1530 NC'Hwy 306 South - NPDES TYPE OF, PERMITTED OPERATION BEING MONITORED •. ; ' Aurora,. NC 27806 County: Beaufort; Contact Person: Danny.Winstead' Telephone: (252)322-8283 Lagoon Remediation: Infiltration Gallery WeII Locations/Site;Name: #1 Cooling Pond No. of Wells to-be Sampled 12 Spray Field X Remediation ., Rotary Distributor Land Application•of Sludge, 1 .. Well Identification Number (from Permit): MW1-7A, X Other Wel15:00 ft. Well Diamter: 2 inch For Groundwater Treatment Water Source Heat Pump.'. _ systems check one: Screened. Interval: 11.80 ft. to 13:80 ft. Influent (98) NOW: Values should reflect dissolved•and If WELL WAS• . •: Depth to_Water Level: 6.02 .ft. below measuring point. Effluent. (99)', colloidal concentrations ` -DRY at'time Measuring Poirit is. 3.04 ft,above land surface. MILILITERS of water pumped/bailed before sam lin sampling: 21.00 Date sample collected: 5/22/2019 of sampling, P 9� Date sample analyzed:' 5/22/2019' to ' 6/26/2019 check ' Field•Analysis: ,pH .: •5.1 ', Specific Conductance 2859 uMhos Laboratory Name: PCS PHOSPHATE here:: Temp. 17.9 oC, Odor NONE', Appearance: CLEAR Certification No(s) . 330 10 PARAMETERS: (Samples for metals were collected unfiltered - . ❑X Yes 0 , . No -and field acidified- . Yes No -COD. N/A m /L-` g Coliform: MFfecal N/A /100mL.. Nitrite (NO2-as N) Nitrate (NO3 as N) N/A , , mg/L Ni.- Nickel - N/Aug/L N/A ` Coliform: MF Total N/X _/100mL Phosphorus. Total•as P 38.000 mg/L. Pb -Lead mg/L N/A ug/L, (Note: use'.MPN method roc n�9niy tumid samples) issolvedSolids: D'Total Orthophosphate N/A - .Zn,-Zinc' -,mg/LaAmmonia Nitrogn N/A ug/L g/L mmg/L y -. 241.0 mg/L pH (When analyzed) 4.8 units AI - Aluminum' Ba - Barium N/A other (Specify compounds and Goneentration units] TO.0 N/A m' . Ca - Calcium N/A VA ug/L 'Fluoride 3'56 mg/L mg/L MIBK Chloride: 34:0'. mg/L Cd- Cadmium N/A ug%L Ag -Silver ' N/A ug/L VA': ug .Arsenic' S ug/L • Grease and Oils, N/A mg/L Chromium: Total Cu -. Copper N/A ug/L. Se-.Selenium N/A" ug/L N/A , P - henol ' N/A' mg/L Fe -Iron- N/A mg/L Sodium ug/L Organics: (GC, GC/MS,.HPLC), 230- Sulfate 1480 0 mg/L. Specific,Conductance N/A uMhos Hg -Mercury K- N/A ug/L = (Specify test method #. Attach lab report.) Total Ammonia N/A mg/L Potassium Mg.- Magnesium N/A mg/L- - . Report attached? -Yes (1);,-No X -.(2) N/A TKN as N. N/A mg/L Mn - Manganese 2365 mg/L' _ VOC method# ug/L' ' :. method.# method# - i knowledge..report s true; accurate, and comoete, and that the laboratory analytical data was produced using approved methods of '. k D. Johnson; General Manaaer VAKAmt i t=Kb: (samptes for metals were collected unfilteredU Yes L No.. and field acidified "Yes uNo ) COD N/A. , mg/L Nitrite (NO2 as.N) N/A mg/L- Ni -.NickelN/A ug/L - ! Coliform MF-Fecal N/A /100mL Nitrate (NO3 as N). N/A mg/L Pb -Lead ' N/A ug[L:. Coliform: MF-Total - use N/A /100mL - Phosphorus: "Total-as P 0.785 mg/L Zn-Zinc N/A 'ug/L. . ,(Note; MPiV method for highly Turbid samples)' . Orthophosphate N/A mg/L . Ammonia Nitrogen mg/L - Dissolved Solids: Total- 2110 mg/L Al -Aluminum N/A.' mg/L Other,(Specity compounds and concentratiori unitsj. H. (when analyzed) ' 6.8 units Ba - Barium N/A ug/L Fluoride < 0.3 mg/L TOG N/A mg/L Ca - Calcium N/A mg/L . MIBK N/A ' ug/L Chloride 134.0 mg/L Cd- Cadmium N/A ug/L Ag - Silver N/A ug/L, Arsenic < 5.0 ug/L Chromium: Total N/A , ug/L Se- Selenium N/A ug/L Grease and Oils N/A . mg/L Cu - Copper N/A mg/l_ Sodium 198 `mg/I Phenol N/A mg/L Fe-Iron° N/A •ug/L Organics:(GC,.GC/MS,-HPLC) Sulfate,,751.0 mg/L Hg - Mercury N/A ug/l_ (Specify test method #. Attach lab report.)- Specific Conductance N/A uMhos K- Potassium N/A mg/LReport attached? Yes . - (1)' No X . (2) - Total Ammonia. N/A. mg/L Mg —Magnesium N/A mg/L VOC'method# TKN'as N N/A mg/L Mn --Manganese 244 ug/L method# method# 1 gqll NOTE: -' Mark D. Joh son General Manager ' Perrni(o thorized Agent) Name and Title:--Please type or p nt GW-59 Rev 4/98 Signature o Permittee (or Authorized Agent) (Date) F-MMAIVIC r arca: tbamptes Tor metals were collected unfiltered X YesU No and field acidified uYes u.No ) COD . ' Coliform: MF.Fecal. N/A mg/L /100mL Nitrite (NOz as N)_,- � Nitrate (NO3 as N) N/A mg/L mg/L- Ni - Nickel Pb --Lead = N/A' N/A N/A Coliform: MF Total N/A " /100mL Phosphorus: .Total as P 100.00 mg/L Zn -Zinc N/A N/A _ ug/L ug/L,, (Note: use MPN metnod,for nigny Turbid samples) Orthophosphate N/A mg/L Ammonia Nitrogen ' mg/L' Dissolved Solids: Total 2330 mg/L Al -Aluminum N/A mg/L other (Specify Compounds and Concentration units) pH (when analyzed) - 4.5 units Ba - BariumN/A ug/L Fluoride. 30 80 TOC. Chloride N/A mg/L Ca - Calcium. N/A mg/L MIBK N/A .mg/L ug/L Arsenic 31.0 mg/L Cd-, Cadmium. N/A ug/L Ag - Silver N/A ug/L Grease and Oils- 179 N/A ug/L mg/L Ctiromium..Total Cu --Copper N/A ug/L Se- Selenium N/A •' ug/L 4-' N/A Phenol N/A mg/L Fe.- Iron N/A mg/L' ug/L Sodium Organics: (GC, GC/MS,,HP.LC) . 211 mgjl ; Sulfate;1160.0 Specific mg/L Hg - Mercury N/A ug/L (Specify test method #. Attach lab report.),, Conductance N/A uMhos K-. Potassium- N/A mg/L Report attached? Yes (1). No X :.(2)' Total -Ammonia N/A.' mg/L Mg - Magnesium N/A mg/L VOC method# TKN'as N N/A mg/L Mn - Manganese 3269 ug/•L . method# " method# NOTE` Mark D. Johnson, General Manager - of t_ rized Agent) Nameand Title - Please type or print. .. --- -_Permittee n 61.%-" 1 9n14 aPa svlat�ran FxLIiA�1iGREPi is FACILITY INFORMATION. Facilty Name: PCS PHOSPHATE CO., INC. -.Aurora Division Permit Name (if different): Facility Addresss: 1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort i Contact Person: Danny Winstead • Telephone: (252)322-8283 WelhLocations/Site Name: ' #1 Cooling Pond - No. of Wells -to be Sampled 12 " Well menTITICaTIon Number (from Permit): MW -11 -8B For Groundwater Treatment Well Depth:, '36.50 ft. Well Diamter: 2 inch systema Check one: S ;MIT #:. W00008570 EXPIRATION DATE: 01/31%23 -Discharge X' UIC X. )ES E OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X. Remediation Rotary Distributor Land Application -of Sludge X Other .Water Source Heat Pump'. creeped Interval. 33.00 ft. to 35.00 ft.Influent (98) Note: Values should reflect dissolved and If WELL WAS ' Depth to Water. Level: 2.78 ft. below measuring point: Effluent (99) colloidal-concentrationsDRY of time + - Measuring Point Js 3.04 ft above land surface:: : Pate samplecollected:. 5/22/2019: of sampling; MILILITERS of•water,pumped/bailed before sampling: 2100" Date.:sample analyzed:- `5/22/2019 to 6126/201.9 check ` ' Field Analysis: pH, 6.2 , Specific Conductance 6500' uMhos. Laboratory Name: PCS PHOSPHATE . here::` Temp. 17.7 oC,.Odor NONE Appearance: ' . LT. CLDY. _- Certification No(s) 330 10 PARAMETERS: (Samples for metals were collected unfiltered' a Yes No and field acidified Yes • X❑No) COD-,. Coliform: N/A mg/L Nitrite (NO2 as N) N/A mg/L Ni -Nickel N/A :ug/L MF Fecal N/A /100mL Nitrate (NO3 as N) N/A mg/L. Pb'- Lead N/A ug/L Coliform: MF'Total. N%A 1100mL Phosphorus: Total as P 1.600' mg/L :Zn -Zinc. N/A " ug/L (Note; Use MPN method for highly'turbid —Dissolved samples) ' OrthophOSphate N/A mg/L Ammonia Nitrogen ;mg, Solids: Total - -5470,- mg/L Al -Aluminum. N/A mg/LOther (Specify Compounds and Concentration' units) -' pH (when analyzed) 6.6 units Ba - Barium N/A ug/L Fluoride <'0.3 mg/L ' TOC ' N/A mg/L Ca - Calcium . N/A mg/L MIBK N/A ug/L Chlonde . ". - 93.0 mg/L , Cd-, Cadmium N/A ug/L _ Ag -Silver N/A ug/L :J Arsenic` < 5.0 ug/L "Cu Chromium: Total N/A- ug/L Se-'SeleniumN/A 'L Grease,pnd Oils N/A mg/L - Copper N/A mg/L Sodium 954 mg/I -Phenol • N/A mglL Fe: Iron. N/A ug/L_ Organics: (GC, GC/MS, HPLC) i Sulfate .3280.0 `' mg/L Hg - Mercury N/A ug/L (Specify test method#: Attach lab.report.) Specific Conductance N/A uMhos .. K -Potassium N/A mg/L Report attached? Yes ("1j No: `X _ (2) Total:Ammonia N/A mg/L. Mg.- Magnesium N/A mg/L VOC method# . TKN as N, N/A mglL Mn = Manganese 474 ug/L method# i method# NOTE Mark. D. Johnson, General Manager " Penn a of uthorized Agent) Name and Title -Please type or pri t Rev 4/98 Signature f Permittee (or Authorized Agent) ate) RTMEN i .....l,1F.,1�11T�2..,NMENI�B. GROWS M '` .................................ENG..............................:.;.:.:.:.:.:.:.:.:.;.:.:.;.;.:.:.:. _ • • ::[)}1lIS1bN;¢FlAf11#ER i2ES I#CES4: FQ:.:.:!A: P P � .1.1 Lr EP AIE $ 1t A! `i' . Gti . .626✓ . ::::::.::::::::::::::::::::::::::::::::::::::::::::::.:.:.:::.:.:.:.:.:::.:.:.:::.:::.:.:.::::.....................................:................................ I-ACILIT'Y INFORMATION ' Facilty Name: PCS PHOSPHATE CO., INC.. - Aurora Division Permit Name (if.different): Facility:Addiresss: 1530 NC Hwy 306 South Aurora, NC 27806 County:- Beaufort ' Contact Person: ''Danny Winstead Telephone: (252)322-8283 Wei LLocations/Site Name: 42•Cooling Pond. No. of Wells to be Sampled 9 RMIT #: • W00008570 EXPIRATION DATE: 01/31/23- n -Discharge X - UIC X DES, PE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field X Remediation:., Rotary Distributor 'Land Application of Sludge X Otheri Water, Source: Heat Pump, P AMAmt i arcs: (samples for metals were collected unfiltered U Yes U No and field acidified U,Yes �'No ). CODN/A ' ".Coliform: MF Fecal mg/'L /100mL Nitrite (NO2 as N ) Nitrate (NO3,as N) N/A m g /L mg/L Ni - Nicker Pb N/A` �sug/L N/A N/A '' Coliform: 'MF Total. N/A . /100mL Phosphorus: - Total as P 30.750 -mg/L -Lead Zn -. Zinc N/A ug/L ug/L N/A (Note::Use MPN methodforhighly turbid samples) Orthophosphate N/A • mg/L Ammonia Nitrogen mg/L'• Dissolved Solids: Total 1030 mg/L -Ali- Aluminum N/A mg/L Other (Specify Compounds and Concentration Units) pH (when analyzed) 5.0 units _ Ba- Barium, N/A ug/L . Fluoride 415- '1 mg%L TOC N/A mg/L Ca -Calcium N/A mg/L MIBK N/A ,.•. Chloride ' 'Arsenic, 53.0 ' mg/L " Cd= Cadmium. 'N/A ug/L Ag -Silver . N/A ,,ug/L, ug/L Grease and Oils 8 ug/L Chromium: Total N/A ug/L Se- Selenium. N/A ug Ph N/A . m9/L. Cu -Copper mL g/ ium 93 - enol N/A m/L Fe - Iron N/A UgL u OrganN/A ics: (G.0 9 , GC/MS, HPLC) Sulfate 537.0 mg/!_ Hg -. Mercury N/A ug/L (Specify test method#. Attach lab report) Spe'cificConductance Total N/A uMhos K -Potassium N/A mg/L 'Report attached?,- Yes- (1)'No . X (2) -Ammonia .. N/A mg/L Mg - Magnesium N/A mg(L VOC: ' method# TKN. as, N N/A mg/L Mn - Manganese . 671 ug/L method# method# NOTE: Mark D. Johnson General Manager ' Permitt (of A_ thorized Agent) Name and Title -Please type•or.prin4 GW=59 Rev 4/98' Signature of ermittee, (or Authorized Agent) Date) GROUNDWATER.............:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.:.::.:.:.:.:.:.:.:.:.::::::::::::::::: .MEN ..:......... - • • - •..:c�vlsrbN..F. A ,¢..lAf. TER;RESbkII�CESaN6 • R�IFA: . N:PROC ' ANGEE�Ep. .. :. �� .. .27s,?s-1�617;;,:.:.Ph,.:1914).84.7¢::::::::::::::::::•:.:.;.:•:::::::::: ;': FACILITY INFORMATION { PERMIT #: W00008570' EXPIRATION DATE: :01/31/23 Facilty Nam'e:. PCS PHOSPHATE CO., INC. -.Aurora Division ' Non -Discharge' X UIC X Permit Name (if different): + NPDES FacilityAddresss: 1530 NC Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora, NC' 27806 County: Beaufort, Contact Person:. Danny Winstead ! Telephone: (252)322=8283 Lagoon Remediation:. Infiltration.Gail lery '- Well, Locations/Site Name: #2 Cooling Pond No. of Wells to be Sampled 9 . Spray Field -. X Remediation: Rotary Distributor Land Application of Sludge ' X Other Water Source Heat'Pum p Well'Identification Number.(from Permit): MW2-1BR For GroundwaterTreatment Well Depth:._ 43.00 ft., Well Diamter:. 2 inch Systems cnecic one Screened, Interval: 39.90 - ft. to 42.40 ft. Influent (98) Note: Values:should reflect dissolved and If WELL'. WAS Depth to: Water Level: 17.80 ft. below measuring point. Effluent (99) colloidal concentration_ s DRY at'time " Measuring Point is 2.70 ft above land -surface. MILILITERS of water pumped/bailed before sampling: 2100' Date sample:collected:. ` - " "5/15/2019 of'sampiirI Date sample analyzed: 5/15/2019 to -6/26/2019 check -0,: Field -Analysis: pH 6:0 , Specific Conductance .4540 uMhos Laboratory Name: PCS PHOSPHATE': here: Temp., 21,.3 QC,, Odor NONE Appearance: CLEAR Certification No(s) 330 10 F1 , PARAMETERS:. (Samples for.metals.were collected unfiltered ❑X Yes, No and field acidified: Yes �No ) COD N/A i mg/L "Nitrite I as N) N/A , mg/L Ni - Nickel N/A U /L Coliform: MF Fecal N/A: /100mL Nitrate (NOs as N) N/A mg/L Pb -Lead N/A ug/L' .Coliform; .MF.Total N/A j /100mL Phosphorus: Total as P 8.850. mg/L Zn = Zinc N/A ug/L (Note: Use MPN method for highly turbid'samples), Orthophosphate Solids: N/A mg/L Ammonia Nitrogen :, mg/L Dissolved Total 3680; mg/L AI - Aluminum N/A mg/L Other (Specify Compounds and Concentration Units) pH (when.analyzed) 6:6 i units Ba-- Barium N/A ug/L Fluoride - < 0.3 TOC N/A ° mg/L Ca - Calcium N/A m 7L MIBK 9_ N/A ug. g. Chloride 110.0' mg/L. - Cd- Cadmium 110 N/A ug/L ` Ag -Silver N/A Arsenic <-5. 0� ug/L Chromium: Total . 'Cu N/A ug/L; • Se- Selenium N/A u /L Grease and Oils N/A I mg/L. -.Copper N/A mg/L ,Sodium = 350 g Phenol N/A mg/L_ Fe -.Iron - N/A ug/L' Organics: (.GC, GC/MS, HPLC). Sulfate 1820.0 -mg/L- Hg- Mercury N/A , ug/L- (Specify test method #. Attach lab,report ) Specific Conductance ° N/A uMhos • K- Potassium N/A mg/L Report attached? Yes - _ (1) `No X (2) Total Ammonia N/A mg/L Mg - Magnesium N/A mg/L VPC method#_ "TK[V.as N N/A ; mg/L Mn - Manganese - 1099 ug/L method# method# ' NOTE: f Mark D. Johnson General Manager . - } Perrnitt e_(i . thorized,Agent) Name and Title -Please type or pri t GW- Rev -4/98 .. ( Zo'1 Signature Permittee (or Authorized Agent) ..lf11�RTR:: PAL IT Y: :.:.:.:...:.:.:.:.:.:........:::.:.:.:.:.:.:.:.:.:.:.:.:::.:.:.:. CAtIAICEREPS RT F3IM..........:.:.:.:.....:.:.:.:..::...............::.:.:.:.:.:.:.:::.:.:.: .................... FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO:, INC. -Aurora Division Permit Name (if different):• . - Facility,Addresss:• .1530 NC Hwy 306 South Aurora, NC 27806 County: Beaufort Contact Person: Danny Winstead Telephone: (252)322-8283 • Well Locations/Site_ Name: #2 Cooling Pond No. of Wells to be Sampled 9 Well•Identification Number (from Permit): MW2-3A For.crouadwatorTreatrnooe X Other Water source Heat Pump Well Depth:. 22.00 ft: Well Diamter: 2 inch Systems check One: Screened Interval:` 18.96 ft. to 20:96 ft.. Influent98 Note: Values should reflect dissolved•and , ( ) If.WELL WAS s Depth to Water Leel: N/A ft.'below measuring point. Effluent (99) colloidal concenfrations -: DRY at,time Measuring Point is 3.18 ft above land surface. Date sample collected: 5/15/2019' of.samphng, ' MILILITERS of water pumped/bailed before sampling: N/A Date sample analyzed:-' 5/15/2019 _ to 5/15/2019 check . Field Analysis: pH ' N/A Specific Conductance N/A uMhos Laboratory Name: PCS PHOSPHATE . here: Temp., N/A - OC, Odor N/A Appearance:. N/A Certification No(s) 330 10 PARi4METERS:. (Samples for metals were collected unfiltered a Yes n/a No , and field�acidified Yes, [n1a] No ) COD N/A mg/L Nitrite (NO2 as N) -N/A mg/L = Ni -Nickel N/A ug/L Coliform-, MF.Fecal `N/A _1100 mL Nitrate_(NO3 as N) N/A mg/L Pb - Lead VA 'ug/L Coliform: MF, Total N/A ./100mL Phosphorus: Total as P N/A mg/L Zn - Zinc N/A ug/L (Note:. Use MPN method for°highly turbid. samples) Orthophosphate N/A mg/L Ammonia -Nitrogen mg/L _Dissolved Solids: Total N/A mg/L I minwL. eciyCornpounds and Concentration Units) pH (when analyzed). N/A units. - 07'a g'luoride N/A mgTOC N/A mg/L .. m'"K N/A ug/L ,Chloride N/A #Rmg1L A :Silver N/A. ug/L g.Arsenic N/A ug/L Chrgmi" _ `'/A u �. '. "'` g " e_ Selenium N/A ug/L Grease and Oils N/A mg/L - Cu - Copper, N/A mg/L Sodium N/A` ug/L Phenol N/A mg/L Fe - Iron N/A ug/L Organics: (GC,�GC/MS, HPLC) Sulfate N/A mg/L . Hg -Mercury N/A ug/L'.' .. (Specify test method #. Attach lab report.).,* Specific Conductance N/A uMhos K -'Potassium N/A mg/L Report attached? Yes (.1) No X (2) Total Ammonia N/A mg/L - Mg - Magnesium N/A' -mg/L VOC method# TKN' as N . N/A mg/L' . - Mn - Manganese N/A Ug/L. method# method# NOTE. Mark' D: Johnson General Mana er NO ACCESS TO WELL. Perm' e f uthorized Agent) Name and Title - Please type or p ' t GW -59, Rev -4/98 Signature f Permittee (or Authorized Agent) Date) CE FACILITY INFORMATION Facilty Name: PCS PHOSPHATE CO., INC: -Aurora Division Permit Name (if different): FacilityAddresss:. 1530 NC Hwy'306 South `Aurora, NC 27806- County: Beaufort Contact.P.erson: Danny Winstead Telephone: (252)322-8283 Well Locations/Site Name: #2 Cooling -Pond No. of Wells to be Sampled r mivrcr meso: toam pies ror metals were collected unfiltered L Yes I n/a I No and field acidified UYesn/a- No) COD Coliform: MF Fecal' N/A mg/L /100mL. Nitrite (NO2 as N) Nitrate (NO3-as N) N/A mg/L mg/L Ni - Nickel Pb Lead N/A ug/L .: . N/A N/A. Coliform: MF Total use N/A • /100mL Phosphorus: Total as P N/A mg/L - Zn - Zinc N/A= ug/L_ N/A (Note: MRN method for highly turbid samples) Solids: Total ho hate `' monia:Nitrogen mg/L Dissolved OH (when.analyzed) N/A N/A mg/L units ; _ min. ' /A fnQ/L ' O er (SpecifyCompounds and'Concentration Units) TO.0 N/A mg/Li ariu - Ici _ -, , m /L S Fluoride MIBKN/AChloride- N/A mg/L . N/A. mg/L - - lum L `^ _ . ° �- ._�' Ag -Silver ug/L . . N/A Arsenic N/A ug/L . Chromium: Total ' N/A . ug/L Se- Selenium N/A- Grease and ,Oils Phenol N/A mg/L Cu --Copper N/A mg/L Sodium N/A ..:ug/L, Sulfate N/A -.mg/L- Fe - Iron N/A : ug/L'," Organics: GC, GC/MS; HPLC N/A mg/L" Hg - Mercury N/A ug/L- " (Specify test method #. Attach lab' report) ' Specific Conductance N/A uMhos . -K- Potassium N/A; mg/L Report attached? .Yes (1) X. (2)+ Total Ammonia. N/A . mg/L Mg - Magnesium N/A mg/L .No VOC method# TKN as N . N/A mg/L Mn - Manganese _ N/A ug/L method# ,'. _ • - met hod# ' - - IF NOTE - - Mark D. Johnson, General Manager NO ACCESS TO WELL' . Permittee (of orized Agent) Name:and Title - Please type or print GW.-59•.Rev 4/98 - Signature of ermittee (or Authorized Agent) - ate) rAruamt l,trc5: (5amples for metals were' collected unfiltered U Yes U ' f, ....................... i�it�fiotte::::1919)BC�:•s3s ;� , IIT #: WO0008670 EXPIRATION DATE: -01131/23 )ischarge X "Llic X mg/L S N/A OF PERMITTED OPERATION BEING MONITORED ,• Ni --Nickel . Lagoon - Remediation: Infiltration Gallery" Spray Field X Remediation Coliform: MF Fecal Rotary Distributor Land Application of Sludge Other Water Source Heat Pump,.,,.-. Nitrate (NO3 as N). Values should :reflect dissolved and : If WELL WAS colloidal concentrations DRY at time: . J .ample collected: 5/15./2019 of sampling; ' , .ample analyzed: 5/15/2019 to ' 6/26/2019 check-. at6q Name: PCS PHOSPHATE here: F-1 cation No(s) • 330 10 -',N/A ; ug/L rAruamt l,trc5: (5amples for metals were' collected unfiltered U Yes U ' No and field acidified uYes u No ) COD N/A mg/L Nitrite (NO2 as N) N/A -mg/L Ni --Nickel . N/A ug/L'_ Coliform: MF Fecal N/A /100mL Nitrate (NO3 as N). N/A mg/L Pb - Lead: N/A' Ug/L' Coliform: MF Total N/A /1.00mL Phosphorus:. Total.as. PO. 114 mg/L' Zn - Zinc -',N/A ; ug/L (Note:- use MPN method rorhighly turbid samples) Orthophosphate N/A mg/L Ammonia Nitrogen Mg,/L Dissolved Solids: Total401 mg/L,- . Al -Aluminum N/A _mg/L Other�(Speciy compounds and concentration units) pH. (when analyzed) . ' 4.1 units •.Ba� Barium. N/A ug/L Fluoride < 0 3 mg/L.' TC N/A ,' „ mg/L Ca., Calcium N/A m /L 9 MIBK N/A ug/L Chloride 7.0 ".6 mg/L , , . ' Cd- Cadmium N/A ug/L- Ag - SilverN/A ug/L Arsenic' ug/L ' Chromium: Total . N/A ug/L Se- Selenium N/A; „7 ug/L Grease and Oils N/A mg/L Cu - Copper N/A mg/L Sodium 25 mg/I +' Phenol N/A mg/L Fe -, Iron N/A ug/L Organics: (GG, GC/MS,'HPLC) ' Sulfate 304.0 mg/L Hg - Mercury.. N/A ug/L (Specify test method. #. Attach- lab report) Specific Conductance N/A uMhos K- Potassium N/A mg/L' Report attached? Yes •(1.) No ` X Total Ammonia N/A mg/L Mg - Magnesium N/A mg/L VOC method# =' TKN;,as N' N/A mg/L Mn - Manganese 315 ug%L _ method# method# I certify that, to:the best of mykn6wiedg e, a n d bellef� the information su brnitted in th is report is, true, accu rate, a nd complete, and that the la boratory a na lytica I data wa s, prod uced using a pproved methods of analysis by a DWR-certified'laboratory� 1:am aware: that: there are significant penalties for -submitting falseinformatiion, including the possibility of fines and imprisonment for knowing violations. ,i NOTE: ' M ark D. Johnson, General Manager Permiflee of ut horized Agent) Name and Title Please type or print I ; GW.'59.Rev.4/98 Signature f.Permittee (or Authorized Agent) (Date) • �ti i . ;...PA. .:...... RTMEN 'iNAI{EN ' ' ' '' '' ' ' '' ' ' '::::::: F NVIR # &iJA .l•ZA $fl R� ;. . •� I�JW A I::.:;:M. �T N:.:.:.:.:.:.:.:.:.:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::•::•:: U....•.•.Y.:.......•.E..��..................•.................•.,...........................................•...:.:.:.:.:.: • • ::Qt1J 81bN UF1Afk#ER RESL)kIIiCESafV FtBIW: N:PIQCE$i�(NIGLEN,LT.....:: ........ P.:.' .........:..... :.:.: :: :::::::: ....I.IAIG.RPE�FtT.ORM.:...:...............:.:...:.:.:.:.:.:.:.:.:.:.:::.:.:.:.:.:.:.:.:.:.:.:.:.:::.:.:.:.:::.:.:::.:.:::.:.:.:.:.... ::::: :::: :: : ........ .....1............................................................4.•...,.•TLP...•..... _ .. :isy I s�vccl i ::::::: ........... L ..:9. •6306 .. �.�27s2sr1�11.;.;::....lto�sei...1.;'(9):80...:.:..............:.:.:.:.:.:.:.:.:.:.:.:.:.:.: .. FACILITY INFORMATION PERMIT #:, W00008570 EXPIRATION DATE:' '01/31/23,*,,:-' FaciltyName: PCS PHOSPHATE CO., INC. - Aurora Division Non -Discharge X- 'UIC', X Permit Na.'mef (if different): NPDES Facility Addresss: 1530 NC Hwy 306 -South TYPE OF PERMITTED OPERATION BEING MONITORED. Aurora, NC. 27806 County:, Beaufort Lagoon Remediation: Infiltration Gallery Contact Person: Danny Winstead Telephone: - : (252)322-8283 Spray Field X Remediation Well Locations/Site Name: #2 Cooling Pond No. of Wells to be Sampled 9 Rotary Distributor Land Application.of Sludge Well;ldentification Number (from Permit): - MW2-4B ForcroonaWaterrreatm X Other Water Source Heat Pump Well Depth: •26.00 ft. Well Diamter: 2• inch . systems check one: Screened Interval: 21.80 - ft. to '23.80 ft. Influent (98) Note: Values should reflect dissolved and ' If WELL WAS _. Depth'to Water Level , 5.10 ft.:'below measuring point Effluent (99) colloidal concentrations DRY'at time. Measuring Point is 3.33 ft above land surface: Date sample collected: 5/15/2019 of sampiing, MILILITERS of water pumped/bailed before sampling: 2100 Date• sample analyzed: 5/15/201.9. to 6/26/2019 check. Field Analysis: pH 4.5 , Specific Conductance: 1047 uMhos Laboratory Name: t PCS PHOSPHATE here: ' ' Temp:_ . 21'.0-'.- oC,, Odor NONE. -Appearance: CLEAR Certification-No(s) 330 10 PARAMETERS;, (Samples for -metals were collected unfiltered �X Yes. No and field acidified Yes X❑ NO) - COD. N/A mg/L Nitrite (NO2 as N) N/A mg/L Ni - Nickel N/A' ug/L ' ..Coliform:: MF Fecal N/A /100M Nitrate (NO3 as N) N/A mg/L Pb -'Lead N/A.-.- ug/L Coliform: MF Total" N/A /100mL Phosphorus: Total, as.P_ 0.185' mg/L Zn - Zinc. ' N/A ug(L (Note: Use MPN method_for highly turbid samples) Orthophosphate N/A :mg/L 'Ammonia Nitrogen :mg/L Dissolved SOIIdS" Total ' .823, mg/L Al - Aluminum' .. N/A mg/L- Other (Specify Compounds and Concentration Units) pH (when.analyzed), 3:4 units Ba - Barium N/A ug/L Fluoride <.0.3 TOC N /A , 'mg/L' •- Ca -Calcium N/A mg/L MIBK rN/A ug/L'' Chloride -23:0. mg/L Cd-. Cadmium N/A ug/L Ag - Silver 'N/A - . Ug/L. Arsenic < 5.0 ug/L Chromium: 'Total N/A -ug/L Se- Selenium -N/A" ug/L Grease and Oils* N/A mg/L Cu - Copper • N/A mg/L ... -Sodium. ' 35 mg/l,'; 'Phenol N/A mg/L F6 -Iron. N/A ug/L Organics:.(GC,.GC/MS, HPLC) Sulfate 532.0 mg/L Hg - Mercury N/A ug/L• (Specify test method #. Attach lab report.), Specific -Conductance VA., :.uMhos K- Potassium N/A ' mg/L Report attached? Yes (,1) No X _(2) Total -Ammonia N/A mg/L Mg - Magnesium N/A. mg/L VOC method# . T.KN.as,N , N/A mg/L Mn - Manganese 12-77 ug/L method#- .. method#' -certify. - best. . -dg . .- -information. analysis by a; - •laboratory.possibility -. -.. .complete,.laboratory.. produced .approvedmethods. ,. - NOTE: Mark D. Johnson, General Manager. Perini a (f uthorized.Agent) Name and Title -Please type or print - GW=59 Rev 4198 signature Permittee (or Authorized. Agent) (Dar ) ...... ........ ..... [P... ART.M Ely ...:.:...::.:.:.: ...:.......:.....:..:.. .:: . ....:.. :. . _::.. T F. Eti�tl�NMENT •. GROU.MM ER'. /AL'ITY: M IST. .... �I�.................................ENG..............:::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::::: • _...... 0 ATI' ...........................:.:.......:.::::: ::l#�TISIbN:OF1KrR#ER:RE$flt1FCESaNl01#9RA N:FI�OCE8&EN6VN . P `. to ..I.I .� R�P�kR .. :. ' A[�C ' TF • • • .•.•ffify.fNll�$E3#ttIC�:C� Nitrite (NO2 as N) - N/A N . l i,... ..27626-iei.........$ho>fe.:. 899 :Bob s3os .. .............:....:: -Ni - Nickel. FACILITY INFORMATION PERMIT'#: W00008570 EXPIRATION DATE: 01/31/23 "Coliform: MF Fecal: Facilty.Name: PCS PHOSPHATE CO., INC. - AuroraDivision _ Non -Discharge X. ,:. UIC' X Nitrate (NO3 as N) Permit Name (if different): NPDE$ Pb - Lead Facility 1530 NC Hwy 306.South TYPE OF PERMITTED OPERATION BEING MONITORED Coliform: MF Total, Aurora,' NC 27806 County: Beaufort Lagoon Remediation: Infiltration Gallery Phosphorus; Total'as P Contact Person: Danny Winstead Telephone: (252)322=8283 Spray Field x Remediation Zn -Zinc Well Locations/Site Name: #2 Cooling Pond. 'No. of Wells to be Sampled 9. Rotary Distributor Land Application of Sludge',' (Note: Use'MPN method.for hidhiy.turbid samples) Well Identification Number (from. Permit): MW24C ..: Forcroanaweterrrestment X Other Water Source Heat Pump mg/L Well'D`epth: 42:00 ft. Well Diamter: 2 inch systems Check one: Dissolved- Solids: Total Screened Interval: 38.95 ft. to 40.95 ft. mg/L Al - Aluminum Influent -(98). Note: Values should reflect dissolved and. If WELL WAS Depth to Water, Level: - 5.30 ft. below measuring point. ' pH (when.analyzed) 6.9 - Effluent (99), colloidal concentrations DRY,.at•tlme a ug/L Measuring Point'is 2.92: ft above land surface. Date sample collected: 5/1.5/2019 of IsamplIng, . MILILITERS of Water pumped/bailed before.sampling: 2100 Date sample analyzed: 5/15/2019 to 6/26/2019 . check N/A Field Analysis: � pH "6.6- , Specific.Conductarice 1524 uMhos -Laboratory Name: PCS PHOSPHATE here: uglL .Chloride, - " Temp:. ..23.1. `o.C, Odor_ NONE Appearance: CLEAR r1 n Certification No(s) 330 10 -Cd- CadmiumN/A uglL Ag - Silver N/A VAKAMtt.tK5:. (samples, for metals were collected unfilteredU Yes U No and field acidified UYes UNo ) COD, N/A mg/L Nitrite (NO2 as N) - N/A mg/L -Ni - Nickel. N/A ug/L "Coliform: MF Fecal: N/A /100mL Nitrate (NO3 as N) N/A mg/L Pb - Lead N/A ug/.L'..- Coliform: MF Total, N/A /100mL. Phosphorus; Total'as P 0.350 mg/L Zn -Zinc NIA - ug/.L (Note: Use'MPN method.for hidhiy.turbid samples) ' Orthophosphate N/A mg/L Ammonia Nitrogen Dissolved- Solids: Total 1140 mg/L Al - Aluminum N/Al. mg/L other.(Specify Compounds and Concen(ration Units) ,. ' pH (when.analyzed) 6.9 - units Ba - Barium N/A ug/L Fluoride < 03 mg/L. TOC N/A mg/L..' Ca - Calcium N/A mg/L MIBK N/A' uglL .Chloride, - 19.0_ . mg/L -Cd- CadmiumN/A uglL Ag - Silver N/A „ ug/L Arsenic . < 5.0 ug/L Chromium: Total - N/A ug/L Se- Selenium N/A :: ug,/L',.:-- Grease and Oils ' . N/A mg/L' Cu - Copper N/A mglL Sodium 56 mg/L Phenol N/A mg/L Fe - Iron N/A . ug/L Organics: (GC,•.GC/MS, HPLC): = Sulfate 454.0 mg/L Hg -Mercury. N/A . ug/L '(Specify test method #. Attach lab report.) Specific. Conductance, N/A uMhos ' K- Potassium- N/A mg/L Report attached? Yes (1) NoX. (2). Total Ammonia. N/A . m /L 9 M - Ma nesium 9 9. N/A mg/L VOC method#` r ;. ! TKN as N N/A mg/L Mn - Manganese 414 ug/L method* method#. . I certif that, to the best of my knowledge Y analysis by a QWR-c6rtified labo'ratory� and belief I am aware that the Information there are significant submitted -tru in this report I s e, accurate, and completej penalties for submitting false information, and including thatthe laboratory the possibilityof analytical data was produced using approved methods of fines and imprisonment for knowing viorations. -NOTE- Mark D. Johnson General Manager Perm1 ( lhorized Agent) Name and Title - Plea'se type or rint , • . ,• q Z1 20 - G1N-59 Rev 4/98 Signature o Permittee (or Authorized Agent) (Da ) 6 rFacilityAddresss: Tr'JR'y Name: PCS PHOSPHATE CO., INC. - Aurora Division it Name (ifdifferent): 1530 NC Hwy. 306 South Aurora, NC 27806 County: Beaufort Contact Person:.. Danny Winstead Telephone: (252)322-8283 -Well,Locations/Site Name: #2 Cooling Pond , No. of Wells to be Sampled 9 (from Permit): MW2-56 For Groundwater Treatment X Other _. Water Source Heat Pump JWelh.Identification.Number Well Depth: 43.80 ft. Well Diamter: 2 inch systems check one: ; Screened, lntervah 39.50 ft. to 41.50 ft. Influent (98); [Note: Values should reflect dissolved and ; If. WELL WAS. . Depth to Water Level: 17.71 ft. below measuring point.. Effluent (99). colloidal concentrations DRY.at.bme Measuring- Point is 2.50, -ft above land surface.. Date sample collected: . 5/16/2019 of sampling, MILILITERS of water pumped/bailed before!sampling:. • -2100_ Date sample analyzed:5/16/2019 to .6/2612019 'check.. Field Analysis:, pH 6.6 , Specific Conductance 2460 uMhos Laboratory Name:. PCS PHOSPHATE. here:. Temp. 23.1 oC, Odor NONE Appearance: CLEAR- Certification No(s) '330 10' PARAMETERS:: (Samples for metals were collected'unfiltered ,- ' �X Yes �; No. and field acidified -Yes X�No) COD `N/A mg/L; Nitrite (NO2 as'•N):• N/A mg/L Ni - Nickel N/A ug/L Coliform. MF Fecal = . N/A /100mL Nitrate' (NO3-as N) . N/A mg/LPb - Lead N/A ug/L. 'Coliform:',MF Total ' .. N/A /100mL Phosphorus:, Total as P 0.655 mg/L Zn - ZincN/A ug/L (Note: use MPN method for highly turbid samples) -,Total Orthophosphate N/A mg/L Ammonia Nitrogen mg/C .• Dissolved, Solids: 1520 mg/L Al -Aluminum N/A mg/L Other (Specify Compounds and Concentration, Units) - pH (when analyzed) 6.8 units Ba = Barium N/A ug/L. ,Fluoride < 0.3 mg/L .;_ TOC N/A mg/L Ca - Calcium N/A mg/L MIBKN/A . , ug/L Chlorideo 266:0 mg/L Cd- Cadmium' _ N/A ug/L Ag - Silver N/A Lig/L'-,. Arsenic < 5.0 Ub/L Chromium: Total N/A ug/L Se- Selenium N/A ug/L Grease and Oils, " N/A mg/L Cu - Copper N/A mg/L Sodium 152 "' mg/l., ' Phenol' • N/A mg/L Fe - Iron N/A, ug/L Organics: (GC; GC/MS, HPLC) Sulfate ' 479.0 mg/L Hg - Mercury N/A ug/L:, (Specify test method #. Attach lab report.)` Specific Conductance N/A uMhos K- Potassium N/A mg/L ' Report attached? Yes (1)No X (2) Total Ammonia. - N/A , mg/L , Mg -.Magnesium N/A •mg/L VOC method# " Y TKN'••as N . N/A mg/L Mn =. Manganese 831 ug/L method# method# 'I certify thati totthe best of my knowledge and belief, the Information submitted i- analysis by a DWR-certified laboratory. liam aware that there are significant in this report:is true, accurate, and complete, penalties for submitting false information; including and that the laboratory analytical data was produced using;approved methods of the possibility of fines and imprisonment for knowing violations. -NOTE:,._Mark D. Johnson General Mana er Pe e f uthonzed Agent) Name and'Title -Please typq or print - GW*59 Rev: 4/98 •- Signaturef Permittee (or Authorized Agent) (Date) f. IgL7U C: E;:1:A:1N7;1; �✓3lI lY�'7 PART F#I IVI' FACILITY INFORMATION PERMIT #: VV00008570 EXPIRATION DATE: 01/31/23 Facilty Name: PCS PHOSPHATE CO., INC: -.Aurora Division Non -Discharge X • UIC - X. Permit Name (if.different): NPDES Facility Addresss: 1530.NC Hwy 306 South TYPE OF PERMITTED. OPERATION BEING -MONITORED Aurora, NC 27806 County: Beaufort Lagoon Remediation: InfiltrationGallery Contact Person: Danny Winstead Telephone: (252)322-8283 Spray Field' X Remediation Well Locations/Site Name: ' #2 Cooling Pond No. of Wells to be Sampled 9 Rotary Distributor. Land Application of Sludge '' Well -identification Number (from Permit):' MW2-5CR For Groundwater Treatment X Other Water Source Heat Pump ' Well Depth: 29:00 ft. Well Diantter: 2 inch - systema check one: Screened Interval: 26.93 ft. to 27.93 ft. Influent (98) Note: Values should reflect dissolved and If WELL WAS n ' Depth to Water Level: 18.20 ft. below measuring point. Effluent (99)' colloidal concentrations DRY`at time Measuring Point is 3.08 ft above land -surface. Date sample collected: 5/1612019 of Sam pling, =.. ;... MILILITERS: of water pumped/bailed before sampling:. 3600 Date sample analyzed: 5/16/2019 to • 6/26/2019- • check' ` Field'Analysis: pH 6.3' •, Specific Conductance 1520 uMhos Laboratory Name: PCS PHOSPHATE here: -Temp. 21.4- oC, Odor NONE Appearance: CLEAR Certification No(s) 330 10 'PARAMETERS:. (Samples -for metals were collected unfiltered 0 Yes 0 No and field acidified []Yes FX- ]No) Q0 D, ' N/A -- mg/L ' Nitrite (NO2 as N)' N/A mg/L Ni - Nickel N!A ug/L ` .Coliform; -MF Fecal N/A /1OOmL Nitrate (NO3 as N) N/A mg/L Pb - Lead N/A. , ug/L, -Coliform: MF Total NIA •. /100mL: Phosphorus: Total as:P 1.475 mg/L Zn -.Zinc N/A ug/L' : . (Note: use MPN method for highly turbid samples) Orthophosphate- N/A mg/L Ammonia Nitrogen mglL DissolVed:Solids: Total 812 mg/L Al - Aluminum N/A mg/L Other (Specify Compounds and Concentration units)' pH (when analyzed) 6:8 -units. Ba - Barium N/A ug/L Fluoride 1.62- - •mg!L . TOC N/A mg/L Ca - CalciumN/A mg/L MIBK N/A ug/!_ Chloride 111.0. mg/L .. -Cd-.. Cadmium N/A. ug/L Ag,- Silver N/A, ", ug/L.'­--- g/L "-- <5 0 •: ug/L .' <5.0 Chromium: Total . N/A ug/L " Se- Selehium N/A ug/L t Grease -and Oils N/A ..mg/L: Cu - Copper N/A mg/L Sodium 76 mg/L. Phenol N/A mg/L Fe - Iron N/A ug/L Organics: (GC', GUMS, HPLC). Sulfate 288.0 mg1L • : Hg - Mercury N/A ug/L (Specify test method #. Attach lab report.) ' Specific Conductance N/A uMhos K= Potassium N/A mg/L Report attached? Yes (1) No X (2) Total,Ammonia. N/A mg/L . Mg - Magnesium' N/A mg/L VOC method# TKN-as. N.- N/A mg/L. • Mn - Manganese 675 ug/L method# method# . :.•'.. I certify that� to tke best of my knowledge and beliefj the information submitted'in analysis 'by a bwR-certified laboratory. I am aware that there;are significant this report is true, accuratej and complete, penalties for submitting false information, inClUding and that the laboratory analytical data was produced using approved methods of the possibility of fines and imprisonment for knowing violations. NOTE: Mark D: Johnson' GenerafMana er Perm' ee f uthorized Agent) Name and Title - Please type=or print'- ' GW -59 Rev 4198 Signature f Permittee (orAuthorized Agent) Date); Cooling Pond Number One Wells MW1-3A Date Dissolved Solids pH Sulfate Fluoride Arsenic Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (10) (50) (Feet from CP) 16 -May -17 2200 5.2 1220.0 4.3 15 -Nov -17 1800 5.4 1280.0 4.5 40 15 -May -18 1840 5.3 838.0 4.4 27 -Nov -18 1880 5.5 983.0 4.5 23 -May -19 1780 5.4 772.0 4.1 730.0 1517.0 MW1-3B Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 16 -May -17 3180 6.4 1750.0 15 -Nov -17 2826 6.4 1670.0 40 15 -May -18 2890 6.3 1500.0 27 -Nov -18 3150 6.3 1420.0 23 -May -19 2920 6.3 1420.0 786.0 MW1-4A Date Dissolved Solids pH Sulfate Fluoride Nickel Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (100) (50) (Feet from CP) 16 -May -17 No Access No Access No Access No Access 40 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 28 -Nov -18 3930.0 2640.0 2.1 23 -May -19 4080.0 2070.0 543.0 MW1-5A Date Dissolved Solids pH Cooling Pond Number One Wells Fluoride Cadmium Manganese MW1-4B Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (2.0) (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 16 -May -17 No Access No Access No Access No Access 40 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 28 -Nov -18 Suspended solids level to high for representative sampling to occur. 29 -May -19 4010.0 6.3 2040.0 3.4 731 MW1-5A Date Dissolved Solids pH Sulfate Fluoride Cadmium Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (2.0) (50) (Feet from CP) 16 -May -17 No Access No Access No Access No Access 50 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 28 -Nov -18 3280.0 1660.0 6.2 23 -May -19 3240.0 1950.0 4.6 103 MW1-5B Date Dissolved Solids pH Sulfate Fluoride Cadmium Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (2.0) (50) (Feet from CP) 16 -May -17 No Access No Access No Access No Access 50 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 28 -Nov -18 5950.0 3380.0 13.1 23 -May -19 5200.0 2900.0 13.7 167.0 Cooling Pond Number One Wells MW1-6AR Date Dissolved Solids pH Sulfate Fluoride Arsenic Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (10) (50) (Feet from CP) 2120 17 -May -17 1460 6.1 674.0 14 -Nov -17 1390 6.1 813.0 14 -May -18 1060 6.0 612.0 29 -Nov -18 1180 6.1 523.0 22 -May -19 944 6.2 527.0 13 703 MW1-6BR Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 2120 15 -May -17 3040 1460.0 14 -Nov -17 2480 1490.0 14 -May -18 2710 1180.0 29 -Nov -18 2490 1290.0 22 -May -19 2370 1070.0 699 Cooling Pond Number One Wells MW1-7A Date Dissolved Solids pH Sulfate Fluoride Arsenic Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (10) (50) (Feet from CP) 16 -May -17 1200 5.1 627.0 9.4 250 14 -Nov -17 1340 5.3 882.0 7.3 14 -May -18 1780 1030.0 4.9 26 -Nov -18 2150 5.3 1100.0 4.3 22 -May -19 2410 5.1 1480.0 3.6 2635 MW1-7B Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 14 -Nov -17 1740 638.0 250 14 -May -18 2020 616.0 26 -Nov -18 1870 559.0 26 -Nov -18 1870 559.0 22 -May -19 2110 751.0 244 MW1-8A Date Dissolved Solids pH Sulfate Fluoride Arsenic Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (10) (50) (Feet from Cl?) 16 -May -17 2120 4.4 1360.0 24.4 250 15 -Nov -17 2130 4.4 1510.0 27.7 14 -May -18 2160 6.4 1140.0 24.0 27 -Nov -18 2290 4.3 1120.0 31.6 22 -May -19 2330 4.4 1160.0 30.8 179.0 3269 Cooling Pond Number One Wells MW1-8B - Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 16 -May -17 6320.0 6.0 3010.0 250 15 -Nov -17 5530.0 6.2 3130.0 15 -May -18 5380.0 5.9 2740.0 27 -Nov -18 5900.0 6.3 2580.0 22 -May -19 5470.0 6.2 3280.0 474 Cooling Pond Number Two Wells MW2-1AR Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 17 -May -17 525 4.7 399.0 3.4 30 16 -Nov -17 806 5.0 435.0 3.8 17 -May -18 894 4.6 379.0 3.7 16 -Nov -18 1030 4.8 526.0 4.0 15 -May -19 1030 4.5 537.0 4.2 671.0 Well Location (Feet from Cl?) 30 Well Location (Feet from CP) 40 Well Location (Feet from CP) 40 Cooling Pond Number Two Wells MW2-1 BR Date Dissolved Solids pH Sulfate Fluoride Cadmium Manganese (500.0) (6.5-8.5) (250.0) (2.0) (2.0) (50) 16 -Nov -17 3720 6.1 1800.0 17 -May -18 3880 5.7 1660.0 14 -Nov -18 3890 6.2 1860.0 14 -Nov -18 3890 6.2 1860.0 15 -May -19 3680 6.0 1820.0 1099.0 MW2-3A Date Dissolved Solids pH Sulfate Fluoride (500.0) (6.5-8.5) (250.0) (2.0) 17 -May -17 No Access No Access No Access No Access 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 16 -Nov -18 No Access No Access No Access No Access 15 -May -19 No Access No Access No Access No Access MW2-3B Date Dissolved Solids pH Sulfate Fluoride (500.0) (6.5-8.5) (250.0) (2.0) 17 -May -17 No Access No Access No Access No Access 15 -Nov -17 No Access No Access No Access No Access 15 -May -18 No Access No Access No Access No Access 16 -Nov -18 No Access No Access No Access No Access 15 -May -19 No Access No Access No Access No Access Well Location (Feet from Cl?) 30 Well Location (Feet from CP) 40 Well Location (Feet from CP) 40 Cooling Pond Number Two Wells M W2 -4A Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 17 -May -17 574 4.5 369.0 70 16 -Nov -17 526 4.5 380.0 16 -May -18 585 4.5 323.0 14 -Nov -18 509 4.4 299.0 15 -May -19 4.4 304.0 315.0 MW2-4B Date Dissolved Solids pH Sulfate Fluoride Cadmium Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (2.0) (50) (Feet from CP) 17 -May -17 616 4.2 371.0 70 16 -Nov -17 622 4.7 436.0 16 -May -18 720 4.5 419.0 20 -Nov -18 706 4.6 458.0 15 -May -19 823 4.5 532.0 1277.0 MW2-4C Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 17 -May -17 1150 6.4 471.0 70 16 -Nov -17 1210 546.0 16 -May -18 1190 456.0 20 -Nov -18 1140 417.0 15 -May -19 1140 454.0 414.0 Cooling Pond Number Two Wells MW2-5B Date Dissolved Solids pH Sulfate Fluoride Chloride Manganese Well Location (500.0) (500.0) (6.5-8.5) (250.0) (2.0) (250.0) (50) (Feet from CP) 18 -May -17 1750 6.4 496.0 284.0 560 16 -Nov -17 1670 1110 536.0 296.0 17 -May -18 1850 6.2 407.0 278.0 20 -Nov -18 1550 288.0 675.0 419.0 278.0 16 -May -19 1520 479.0 266.0 831.0 MW2-5C Date Dissolved Solids pH Sulfate Fluoride Manganese Well Location (500.0) (6.5-8.5) (250.0) (2.0) (50) (Feet from CP) 18 -May -17 1270 6.3 414.0 560 16 -Nov -17 1180 6.3 448.0 17 -May -18 1110 6.0 296.0 20 -Nov -18 1030 6.3 297.0 16 -May -19 812 _ 6.3 288.0 675.0 PCS PHOSPHATE CO 17leo I 3,L-3 913-0 22.49 11,6-9 :5-,09 Aurora Division &,,0117 ................................ .................................. ................................ .................................. MW1-1A PHOSPHATE OPERATIONS mW1-1B 18.26 /A WELL MEASUREMENTS 15.84 MW1-2B ............. TOC TOC 6'. 99 ............. PZ2 -8A ezo.me ............... .. ...... TOC TOC Elevation Stc Wtr Wtr Lvl MW2-2A Elevation Stc Wtr Wtr Lvl Well ID MSL Level Rel to MSL .......... 77= . Well ID MSL Level Rel to MSL .............................. ............. ............. ............. :::::, ... ... . C. 0 n . .... . . .... .......... ....... .............. .......... ....... ....... ............. ... PZ1 - 1A 22.51 40 -17 1-4-V iiiiiiiiji PZ2 - 1A 22.57 1 B 22.75 1 B 22.46 0 B. 40Y is 22.58 .. is .... . .... 22.43 ........ ...... ............ .. ................... ............ . /S,:3-0 PZ2 - 2A 21.11 PZ1 - 2A 21.89 2B 21.85 2B 21.12 6 q 2S 21.92 G O 16,- 02- 2S 21.09 6 : 0 PZ1-9A-0 22.52 17leo I 3,L-3 913-0 22.49 11,6-9 :5-,09 ................................. .................................. ................................. .................................. 21.95 &,,0117 ................................ .................................. ................................ .................................. MW1-1A 18.26 mW1-1B 18.26 /A MW1-2A 15.84 MW1-2B ............. 15.98 17, tW 6'. 99 ............. PZ2 -8A ezo.me ............... .. ...... 19+50 PZA 50.361 PZB 33.24 1 27+50 PZA PZB 52.15 34.19 40+00 PZA 1 53.30 PZB 35.89 dAforms\piezometer Measurements.xis PZ2 - 3A 21.70 3B 21.72 3S 21.81 PZ2-4A 22.05 11bV '10, RS - 4B 21.95 11,6-9 P. %Yle 4S 21.95 &,,0117 PZ2 -7A 21.82 ............... ....... ......... PZ2 -8A 21.92 MW2-2A 21.89 109, MW2-2B 22.06 .......... 77= . .............. .....77777 CID #1 CP#2 Piezometers could not be located. Tech: e- e -- Date: