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HomeMy WebLinkAboutWQ0011431_Renewal Application_20190701INITIAL REVIEW Reviewer Thornburg, Nathaniel Project Number* WQ0011431 SUBMITTAL DATED: 6/28/2019 Project Contact Information Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Rob Willcox Email Address* rob@Wllco)Tnabesoil.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number WQ0011431 currently has project Applicant\Permittee * Town of Cleveland Facility Name * Town of Cleveland WWTP Phone Number* 336-339-9128 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) 15-03 Town of Cleveland Residuals Land Application Program - Permit Renewal June-2019- 39.44MB signed.pdf upload only 1 R7F docurrent. IVUltiple documents rust be corrbined into one R7F file. For new and modification permit applications, a paper copy may be required. If YGL' have any questions about what is required, please contactthe reviewer or Tessa Monday. If a aaoe- a1,o1:cation is required, be advised, applications accepted far pre -review until both the paper and eIect-c-i_ col. es -,ave been received. The paper copy shall include the following: o Application Form o All relevant attachments (cales, soils report, specs, etc.) o One full-size engineering plan set o One 11x27" engineering plan set o One extra set of specifications o Fee (if required) Mailing address: - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - By U.S. Postal Service - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - By Courier/Special Delivery: �---------------------------------------------------------------------------- --------------------------- ❑ivision of Water Resources i Division of Water Resources -------------- - ---- ----- ----------------------------------- Non -Discharge Branch 1--------- Non -Discharge Branch 1617 Mail Service Center i Aft: Nathaniel Thornburg, 90 Floor, O f`uce #942W Raleigh. NC 27699-1617 512 N. Salisbury St. Far questions or problems contact Tessa Monday attessa.monday@ncdenr.Qov or 919.707.3560. * I;W By checking this box I acknowledge that I understand the application will not be accepted for pre -review until the paper copy (if required) and fee (if required) have been received by the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Signature Submission Date 6/28/2019 APPLICATION FOR RESIDUALS LAND APPLICATION PROGRAM PERMIT RENEWAL TOWN OF CLEVELAND WWTP PERMIT NO. W00011431 WMSS Project No. 15-03 Prepared for: Town of Cleveland Post Office Box 429 Cleveland, North Carolina 27013 Prepared by: Willcox & Mabe Soil Solutions, PLLC 7231 B Summerfield Road Summerfield, North Carolina 27358 willcox&mabe 5 0 1 L S❑ L U T 10 N S June 2019 willcoX&'l abe SOIL SOLUTIONS June 28, 2019 NCDEQ/DWR Water Quality Permitting Section Non -Discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attention: Non -Discharge Permitting Unit Reference: Application for Residuals Land Application Program Permit Renewal Town of Cleveland WWTP Permit No. WQ0011431 Willcox & Mabe Soil Solutions, PLLC Project No. 15-03 Non -Discharge Permitting Unit: Willcox & Mabe Soil Solutions, PLLC (WMSS) is submitting the enclosed Residuals Land Application Program Permit Renewal application for the Town of Cleveland WWTP (Cleveland) on behalf of Cleveland and BioGreen Services, Inc. (BioGreen). The permit renewal package includes information for: Renewal of one field (10.0 net acres), Town of Cleveland (Site 1, Field 1). Current annual volume of 82.0 dry tons to remain the same. If there is any further information required or questions regarding this application please do not hesitate to contact Cleveland, Ms. Cathy Payne at (704) 278-4777, or WMSS at (336) 339-9128 for further assistance. Sincerely, Willcox & Mabe Soil Solutions, PLLC Martin Mabe Agronomist cc: Town of Cleveland Rob Willcox, L.S.S. Soil Scientist Shared\WMSS Projects\2015\15-03 Bio-Green Services\Phase 03A - Cleveland Permit Renewal\15-03 Town of Cleveland Residuals Land Application Program - Permit Renewal June-2019.doc Willcox & Mabe Soil Solutions, PLLC / 7231 B Summerfield Road / Summerfield, INC 27358 / Rob 336.339.9128 or Martin 336.312.1396 / www.willcoxmabesoil.com TABLE OF CONTENTS APPENDIX TITLE Page 1 RESIDUALS LAND APPLICATION PROGRAM APPLICATION FORM (FORM: RLAP 06-16) OPERATION AND MAINTENANCE PLAN (Updated) COPY OF EXISTING PERMIT (PERMIT NO. WQ0011431) II RESIDUALS SOURCE CERTIFICATION • TOWN OF CLEVELAND (FORM: RSC 06-16) III LAND APPLICATION SITE CERTIFICATION (FORM: LASC 06-16) Renewal Site IV TOWN OF CLEVELAND (SITE 1, FIELD 1) LANDOWNER AGREEMENT (FORM: LOA 06-16) UPDATED SITE MAPS UPDATED CUMULATIVE POLLUTANT LOADING RATES APPENDIX I RESIDUALS LAND APPLICATION PROGRAM APPLICATION FORM (FORM: RLAP 06-16) OPERATION AND MAINTENANCE PLAN (Updated) COPY OF EXISTING PERMIT (PERMIT NO. WQ0011431) RESIDUALS LAND APPLICATION PROGRAM APPLICATION FORM (FORM: RLAP 06-16) State of North Carolina Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages): ® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ® If this project is for a modification of an existing permit, submit one copy of the existing permit. ® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) 10 Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). (Renewal Only — no requested changes) Facility Classification New Permit Major Modification 1 Major (land are permitted for > 300 acres) $1,310 $395 Minor (land are permitted for < 300 acres) $810 $245 ' - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional land application areas not previously approved for that particular program [including transferring of field(s) from one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor modifications to a permit. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. D. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300) (N/A) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3 E. Operation and Maintenance Plan (New and Renewal Application Packages) (UPDATED — APPENDIX I) ❑ For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ❑ Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ❑ Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ❑ Maintenance schedules; may include equipment calibration, maintenance of signs, etc. ❑ Safety measures; may include safety training program, manuals, signs, etc. ❑ Spill response plan; including control, containment, remediation, emergency contact information, etc. ❑ Inspection plan including the following information; ❑ Names and titles of personnel responsible for conducting the inspections. ❑ Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ❑ Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ❑ Sampling and monitoring plan including the following information; ❑ Names and titles of personnel responsible for conducting the sampling and monitoring. ❑ Detailed description of monitoring procedures including parameters to be monitored. ❑ Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY. (N/A) F. Program Determination ❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T .110202). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable: ❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies greater than agronomic rates. ❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal, and agricultural crop production is of secondary importance. ❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system. rl Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program falls under the dedicated program definitions. G. Program Information ❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system. ❑ Provide an explanation of the dedicated system and its operation. H. Detailed Site Maps (All New or Modification Application Packages) ❑ Submit three (3) sets of standard size plans and two (2) sets of I I" by 17" plans (electronic format is acceptable - Adobe PDF only). For Modifications, submit plans specific to the modification(s) only. ❑ Plans must include the following minimum items: ❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site relief and showing all facility related structures and fences within the land application area. ❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s). ❑ Delineation of the review and compliance boundaries ❑ Setbacks as required by 15A NCAC 02T .1108 ❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s). ❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray irrigation zones as they will be operated. ❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3 I. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites) ❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops and their ability to accept the proposed application rates. J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity) ❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy available at: http://www.ncwater.ory/Rules Policies and -Regulations/. The document shall be signed, sealed and dated by a qualified professional. K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation facilities fed through fixed supply system) ❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or Professional Land Surveyor in accordance with 15A NCAC 02T .1104(d)(2). For Modifications, submit an updated site map specific to the modification(s) only. The design documents must include the following minimum items: ❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new units or are critical to the understanding of the complete process; ❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the finished product including leaking testing; and ❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head curve analysis for each pump, and irrigation design. ❑ Soil mapping units shown on all disposal sites. L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or irrigation facilities fed through fixed supply systems) ❑ Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy available at: http://www.ncwater.or /g Rules_ Policies_ and Regulations/. M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment or irrigation components) ❑ Property ownership documentation shall consist of one of the following: ❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or ❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or ❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of 15A NCAC 02L .0107(fl, or ❑ A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or survey map. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Deliverv: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Town of Cleveland Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ® Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Danny Gabriel Title: Mayor Applicant's mailing address: Post Office Box 429 City: Cleveland State: N.C. Zip: 27013 Telephone number: (704) 278-4777 Email Address: clevelandclerk@clevelandnc.org 2. Consultant's name: Rob Willcox, L.S.S. License Number (for P.E.): N/A Affiliation: ❑ On Staff ® Retained (Firm: Willcox & Mahe Soil Solutions, PLLC) Consultant's mailing address: 7231B Summerfield Road City: Summerfield State: N.C. Zip: 27358 Telephone number: (336) 339-9128 Email Address: rob(a)willcoxmabesoil.com 3. Agronomist's name: Martin Mahe License Number: N/A Affiliation: ❑ N/A ❑ On Staff 0 Retained (Firm: Willcox & Mahe Soil Solutions, PLLC) Agronomist's mailing address: 7231B Summerfield Road City: Summerfield State: N.C. Zip: 27358 Telephone number: (336) 312-1396 Email Address: martinna,willcoxmabesoil.com 4. Soil Scientist's name: Rob Willcox, L.S.S. License Number: 1098 Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: Willcox & Mabe Soil Solutions, PLLC) Soil Scientist's mailing address: 7231B Summerfield Road City: Summerfield State: N.C. Zip: 27358 Telephone number: (336) 339-9128 Email Address: rob(a)willcoxmabesoil.com 5. Fee submitted: $0.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00011431 Date of most -recently issued permit: January 1, 2015 Date of most -recently certified Attachment A (if different than the permit): July 24, 2017 Date of most -recently certified Attachment B (if different than the permit): _ FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: Third Creek Church Road City: Cleveland State: N.C. Zip: 27013 Coordinates: Latitude: 35' 44' 37.7" Longitude: 80' 40' 59.8" Datum: NAD83 Level of accuracy: one tenth of a second Method of measurement: MAP 2. County where residuals land application program is headquartered: Rowan 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Sherrill Ray Gambill Bio-Green Services, Inc. 985951 Back -Up ORC Denise Gambill Harrison Bio-Green Services, Inc. 989912 Additional Back -Up ORCs (if applicable) _ If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 82.0 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 34.33 34.60 2,815 2,837 Five -Year Maximum Adjusted 51.32 51.59 4,208 4,230 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops Hay 10.0 Pasture hm- Total: 10.0 Methods Surface 10.0 Incorporation or Injection Total: 10.0 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 40.6 40.9 62.1 62.4 100 20.3 20.4 31.1 31.2 150 13.5 13.6 20.7 20.8 200 10.1 10.2 15.5 15.6 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. I R_ Residuals Source Certification APPENDIX II V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. IR Land Application Siite Certification.doc APPENDIX III FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system on1X. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM (N/A) 1. The irrigation system is: 0 Spray 0 Drip 2. Disposal system is: ❑ existing a proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ❑ Yes or L] No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate in/hr Recommended Loading Rate in/ r 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met: t- 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field /Zone Design Area (ft2) Number of Nozzles Maximum Application Rate ( allons/hr) Design Annual Loading Rate ( allons/ r ■ Total Spray Irrigation Design Element Plan Sheet Number Specification Pa a Number Wetted diameter of nozzles ft _ Wetted area of nozzles ft2 Nozzle capacity gpm - Nozzle manufacturer / model Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. 0 Yes E] No, Explain; I, Danny Gabriel Mayor (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Renewal to the Town of Cleveland Non-Discharize Permit No. W 0011431 (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. t Signature: Date: r FORM: RLAP 06-16 Page 5 of 5 CLEVELAND WWTP LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: April 15,2019 Cleveland WWTP Mineralization Rate 0.3 2.28 %Solids 5.65 pH Permit No. WQ0011431 Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg x 0.002) Nitrogen (TKN) 4.382 43,817.500 87.635 Phosphorus 0.033 330.000 0.660 Potassium 0.251 29510.000 5.020 PAN (injected)* 1.730 17,299.283 34.599 PAN (surface)* 1.716 17, 164.195 34.328 Ammonia Nitrogen 0.027 270.175 0.540 Calcium 3.230 329300.000 64.600 Calcium Carbonate Eq. --- --- --- Magnesium --- 29330.000 4.660 Sodium --- 99474.000 18.948 Sulfur --- --- --- Nitrate N / Nitrite N --- 39964.910 7.930 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 4%000.00 98.000 Arsenic --- 0.402 --- Cadmium --- 1.570 0.003 Chromium --- --- --- Copper --- 591.00 1.182 Lead --- 0.430 0.001 Mercury --- 0.658 --- Molybdenum --- 14.500 --- Nickel --- 16.10 0.032 Selenium --- 0.440 --- Zinc --- 19399.00 J 2.798 1 1 I Statesville Analytical 190415-17-01 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. SAR 2.07 Ceiling Co (MO/Kq 75 85 49300 840 57 75 420 100 79500 Willcox & Mabe Soil Solutions, PLLC RESIDUAL PAN CALCULATION Town of Cleveland TKN= 43,818 mg/kg NH3= 270 mg/kg NO3-NO2-N= 3,964.9 mg/kg Min Rate= 0.30 PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO21 0.30 431547 135 3964.91 PAN= 17164.20 mg/kg Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine the amount of PAN/DT remaining. 2ND YEAR RESIDUAL PAN PAN= [min.rate (1st year org. - N 2nd year min. - NJ 0.15 43,547 139064 PAN= 4572.47 mg/kg remaining from I st year application 3RD YEAR RESIDUAL PAN PAN= [min.rate (2nd year org. - N 3rd year min. - NJ 0.08 305483 4)572 PAN= 2072.85 mg/kg remaining from I st year application 4TH YEAR RESIDUAL PAN PAN= [min.rate (3rd year org. - N 4th year min. - NJ 0.05 251911 21073 PAN= 1191.89 mg/kg remaining from I st year application 5TH. YEAR RESIDUAL PAN PAN= [min.rate (4th year org. - N 5th year min. - NJ 0.03 235838 11192 PAN= 658.31 mg/kg remaining from I st year application Residual PAN from years 2 thru 5 after the initial application = 8495.52 mg/kg Application Five Year Maximum Method First Year PAN Adjusted PAN (mg/kg) (mg/kg) Surface 17,164 251660 Incorporation 179299 259795 Application Five Year Maximum Method First Year PAN Adjusted PAN (lbs/DT) (lbs/DT) Surface 34.33 51.32 Incorporation 34.60 51.59 SAR Calculation ! Na mg/I Ca mg/I Mg mg/I 216.0072 736.44 53.124 Na Ca Mg SAR i 9.392 1 36.822 i 4.427 2.068 Na mil eq Ca mil eq Mg mil eq 9.392 36.822 4.427 nter Enter . o T 2.28 _1 Data Na mg/kg 9474 i Ca mg/kg32300 Mg mg/kg 2330 : Job Name: I Town of Cleveland j i Page 1 Cleveland WWTP Permit # WQ0011431 RESIDUALS APPLICATION DATA 82 Dry Tons of residuals to be certified PLANT AVAILABLE NITROGEN SUMMARY PAN Pounds of PAN per DT (Weighted Average) Pounds of PAN per Year Surface Incorp. Or Inject. Surface Incorp. Or Inject. First -Year 34.33 34.60 2,815 2!)837 Five -Year Maximum Adjusted 51.32 51.59 4,208 4,230 Assumed Application Rate (lbs PAN/ac-yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Surface Incorp. Or Inject. Surface Incorp. Or Inject. 50 56.3 56.7 84.2 84.6 100 28.2 28.4 42.1 42.3 150 18.8 18.9 28.1 28.2 200 14.1 14.2 21.0 21.2 OPERATION AND MAINTENANCE PLAN (Updated) OPERATION AND MAINTENANCE PLAN Town of Cleveland Non -Discharge Permit No. WQ0011431 LAND APPLICATION OF CLASS B BIOSOLIDS Town of Cleveland Wastewater Treatment Plant (WWTP) Class B Biosolids Description and Overview The purpose of the Town of Cleveland Operation and Maintenance Plan is to put into place a plan that implements the requirements of North Carolina Department of Environmental Quality (NCDEQ) — Division of Water Resources (DWR) Class B Land Application Permit (WQ0011431). 1. Operational Functions The operational functions of this program involve hauling biosolids from the respective WWTP to the land application sites permitted under NCDEQ-DWR and land applying the biosolids in accordance with regulatory requirements. Biosolids will be land applied at or below agronomic rates that are determined using the Realistic Yield Expectations (RYE) as outlined in the permit. The current land application contractor will also account for any nutrient sources the landowner/lessee has applied. Some source(s) may be land applied as either a liquid or cake material utilizing either pumper trucks, vacuum trucks, tractor trailer, tractor and cake spreader and/or tractor and pull tank. In some instances, biosolids may have to be injected or surface applied with incorporation depending upon the pathogen and vector attraction reduction methods employed by the respective WWTP. Whichever method is utilized to land apply the biosolids, the current land application contractor will spread evenly and at consistent rates. Biosolids will be land applied on fields that are used for hay production, grazing, or row crop production harvested for animal feed. In the case where biosolids are land applied on fields utilized for grazing, applications rates will be reduced by 25% in accordance with USDA-NRCS 590 Nutrient Management Standards. Grazed fields will be determined by the current land application contractors Manager on site. 11. Maintenance Schedules The Town of Cleveland staff is responsible for maintenance of the facilities and equipment at the respective WWTP's. The current land application contractor is responsible for maintenance of the equipment associated with the land application program. Operation and Maintenance Plan Town of Cleveland - Class B Biosolids Permit No. W00011431 Safety plans and training are the responsibility of the personnel associated with the land application program. All employees involved with the land application program will be required to comply with safety plans and training as applicable to the Class B Biosolids Permit. Land application program employees shall be trained, as appropriate, in general awareness for the protection of water and pollution prevention general practices. This training will be provided as part of a new employee orientation program or as part of ongoing environmental awareness training. General refresher training for those employees involved will be provided in accordance with applicable regulatory or permit requirements. III. Spill Response Plan Includes the following: • Spill Control Plan (Attached), • Spill Prevention Plan (Attached), • Spill Control, Containment and Cleanup Plan (Attached). IV. Inspection Plan The land application Operator in Responsible Charge (ORC) or personnel under direct supervision of the ORC has responsibilities to include daily inspections of WWTP and land application sites (when land application activities are scheduled). The ORC will maintain daily record keeping logs of land application activities, inspections of field applications equipment and maintenance, loading operation, roads, crops, crop maintenance and harvesting practices. All daily record keeping logs will be coordinated with the ORC at the end of each day. In the event that a noncompliance event is observed during any inspection, the ORC of the WWTP will be immediately notified. The ORC will determine the course of action to be taken in order to rectify the noncompliance issue. NCDEQ will be notified as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence. At a minimum, these inspections will consist of the following: • Verify that a biosolids analysis has been collected prior to land application activities being performed and that it meets the criteria for land application. • Verify that pathogen and vector attraction reduction data has been collected for the source to be land applied and that it meets the criteria for land application. • Verify the crop that is planted or is to be planted on the respective field(s). • Confirm that the correct amount of biosolids are being land applied. Operation and Maintenance Plan Town of Cleveland - Class B Biosolids Permit No. W00011431 • Confirm that manned equipment has a copy of the permit and the operations and maintenance plan. • Check that the field has been properly flagged and that buffers are adhered to. • Check that proper signage is posted. • Confirm that records are turned in at the end of each business day. Inspections will also be conducted by the respective employees of the biosolids generating facilities (at the source generating facility). The land application contractor will not be responsible for inspections at the source generating facilities. These inspections should be conducted by the respective ORC of each facility and should fall under their own Operations and Maintenance Plans. V. Sampling and Monitoring Plan The respective WWTP's Class B Biosolids will be monitored to confirm compliance with conditions in Non -Discharge Permit No. WQ0011431 to include: • Toxicity Characteristics Leaching Procedure (TCLP), • Reactivity, Ignitability and Corrosivity, • 15A NCAC 02T .1105 Pollutant Limits and nutrient analysis, • Pathogen and Vector Attraction Reduction requirements, • Annual Representative Soil Analysis of each field which receives land application during each respective year. • Any other applicable Permit conditions. All sampling and monitoring shall be performed in accordance with the current Permit. Pollutant concentrations in the Town of Cleveland WWTP Class B Biosolids shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 Operation and Maintenance Plan Town of Cleveland - Class B Biosolids Permit No. WO0011431 The Town of Cleveland WWTP Class B Biosolids shall be analyzed to demonstrate it is non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed annually. TCLP shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1 1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride Endrin (0.02) Silver (5.0) (0.5) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachlor -1,3-butadiene Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) An analysis shall be conducted on the Town of Cleveland WWTP Class B Biosolids based on conditions (monitoring frequencies) set forth in Permit No. WQ0011431. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) Operation and Maintenance Plan Town of Cleveland - Class B Biosolids Permit No. W00011431 The Town of Cleveland WWTP Class B Biosolids shall be analyzed to demonstrate compliance with Pathogen Reduction and Vector Attraction Reduction requirements based on conditions (monitoring frequencies) set forth in Permit No. WQ0011431. The current Pathogen Reduction Alternatives and Vector Attraction Reduction Options utilized are as follows: Pathogen Reduction: Per 15A NCAC 02T.1106 For Land Application of Class B: Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration or ® Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP) Specify one: aerobic digestion, air drying, 0 anaerobic digestion, I composting, or I lime stabilization. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107 For Land Application of Class B: ® Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). or Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion) or ® Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization Attachments: Spill Control Plan Spill Prevention Plan Spill Control, Containment and Cleanup Plan Shared\WMSS Projects\2015\15-03 Bio-Green Services\Phase 03A - Cleveland Permit Renewal\DEQ Forms\O&M Plan - Town of Cleveland - June 2019.doc k, TOWN OF CLEVELAND SPILL CONTROL PLAN NON -DISCHARGE PERMIT NO. WQ0011431 THE FOLLOWING ACTIONS MUST BE TAKEN IN THE EVENT OF A SPILL: 1. Halt the source of the spill: Ruptured line, valve, or container / damaged tank or transport unit. 2. Contain spill: Use straw bales to form a barrier. Straw or hay bales can be obtained from several sources for this purpose. Soil near the site can also be used to form a barrier for containment. 3. Clean up: Use land application equipment to recover as much of the material as possible. After the application equipment has recovered as much of the material as possible, it will be land applied as per the management plan. A temporary sump pit may be dug in the containment area to enhance recovery, if necessary. 4. Notification: As soon as possible after a spill occurs notify: • NC Department of Environmental Quality Division of Water Resources Regional Office Mooresville Regional Office (704) 663-1699 • Fire Department if assistance is required for wash down 5. Management of clean up efforts: The responsible party for land application shall take immediate charge of the clean up activities. Additional labor will be requested as needed. 6. Reporting: Within 24 hours of a spill the responsible party for land application shall present a written report detailing the cause of the spill and all action taken in response to the spill. The Mooresville Regional Office shall be notified in no case more than 24 hours or on the next working day following the occurrence. SPILL PREVENTION PLAN The spill prevention plan requires that all equipment used to transport biosolids be subject to periodic safety inspections. Tires, brakes, lights, and turn signals will be inspected for proper working order. Each truck will be equipped with safety flares and appropriate signs to be used in the event of a breakdown. Any deficiencies observed during the safety inspections will result in the vehicle being removed from service and the responsible party for land application will be notified so that these deficiencies can be corrected and documented. Routes leading from the storage point to the land application sites will be inspected for road hazards. The road hazards will be documented and the drivers will be informed of the hazards. Alternate routes will be investigated and routes which minimize road hazards will be selected. Hazardous situations resulting from rush-hour traffic will be avoided during hauling. Drivers and management personnel associated with the hauling of biosolids will be instructed in the spill prevention plan and will be required to attend training sessions. Drivers will be trained in defensive driving techniques in order to minimize road hazards. A driver who observes a road hazard will be required to report the hazard to the field superintendent who, in turn, will warn other drivers. As part of the spill prevention plan, drivers will be required to inspect the safety equipment of their vehicles on a daily basis. Any deficiency in safety equipment will be noted for corrective action. Drivers will be trained in the procedures to be taken in the event of a spill that occurs during the hauling of biosolids. These procedures are discussed in the spill control, containment, and cleanup plan. SPILL CONTROL, CONTAINMENT, AND CLEANUP PLAN Spills that occur during loading or unloading biosolids will occur at the generation point and the land application sites, respectively. These spills will not involve an environmental hazard or an over the road hazard and, therefore, will be handled using the equipment that will be available at either site. Spills that occur over -the -road will be subject to the contingencies contained in the spill control, containment, and cleanup plan. The equipment used in the spill control, containment, and cleanup consists of the following: 1. Vacuum pump, pump truck or tanker truck. A vacuum truck, vacuum pump or tanker truck will be used to assist with clean-up of biosolids spills. 2. Outside equipment if required The following personnel will be involved in the spill control, containment, and cleanup. 1. The responsible party for land application will respond to the spill site and make an assessment of the spill and determine the containment procedures to be initiated and the equipment to be used to clean up the spill. 2. The responsible party for land application will be responsible for the direction of the cleanup team. In the event of a spill, the driver of the truck or application vehicle, if he has not sustained a debilitating injury, will call the responsible party for land application and report the spill. The responsible party for land application will notify the appropriate authorities and will also notify the DWR Regional Office. The driver will set up safety flares and signs to warn motorists of the hazard. The responsible party for land application will mobilize the necessary equipment and personnel to the site, and will initiate the containment procedures. When the cleanup team arrives at the site, the site will be cleaned up according to the contingency plan. Biosolids cleaned up from the site will be transported to the land application sites where it will be applied in accordance with the permit. In the event that the driver is incapacitated due to personal injury, the responsible party for land application will mobilize the cleanup team as soon as the authority's notification of an incident. COPY OF EXISTING PERMIT (PERMIT NO. WQ0011431) WaterResources ENVIR011IM-eNTAL. QUALiTY iff,,y 24, 201.7 THE HONORABLE DANNY GABRIEL Tw& NL OF CLEVE LAND POSTOFFICE Box 429 CLEVELAND,, NORTH CAROLINA 2,7013 Dear Mayor Gabriel-, ROY COOPER Govei-�m,),r MICI-LAEL S. REGAN & JAY ZIMMERNIAN Subject.- Attachment B Certification Permit No. W'QOO 11431 Town of Cleveland RLAP Rowan County In accordance witb your pemiit modificat-ion request received July 3, 2017, and subsequent additional information received July 1-0, 2017, we are fonvarding herewith a 1-nodified Attachment B certified July 24, 2017, to the Town of Cleveland for the subject residuals progrwi. This certification is being lssucdtoniodifp Attaclinicnt.B by: Change of ownership of field NC- RA-01-0L This niodified Attachment B shall be effective, from the date of certiflication until December 3 11 2019 (i.e., expiration date of the currentperm-it), shall void Attachment B of PermitNo. W'Q001 1431 issued I October 24, 201.4 that was previouslY certified on April 27, 2017, arid shall be subject to the conditions and lim itations as specified therein, as well as those specified in -the above -referenced permit. Please replace the Attachment B of Pen -nit No. WQ001 1.431 that was certified on April 27., 201-7 with this modified ,.AAtachment B. Please note that the maps issued previously are still, applicable to this permit. It is the Permitte e's responsibility to ensure that a complete permit is created by inserting only this arriended Attachment B into the previously issued pemilt, Ira . parts, requirements, and/or limitations contained in this certifileation or modified Affachment B are unacceptable, you have the right to request an adjudicatory hearing, upon written request within 30 4:7 da S following rje.celiptof the certification, This request shall be in the formtng of a written petition, conforming y to Chapter 150B of the North Carolina G(Meral Statutes and filed with the Office of Administrative Hearingos 't � at 6714 Mail Service Center, Raleigh, North Carolina 27699-6714, Unless such demands are made, this permit shall be final and binding. ny ennutreun", 1617 Mad Sorvlice Center 1,R,,:t'Leigh,, North. Cuo'lina 27699­1617 919.-807-6332 In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended., and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO rW-1 -t-own. of Cleveland Rowan County FOR THE continued operation of a residuals management program for the Town of Cleveland and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received July 8, 2014, and in conformity with other supporting data subsequently filed and approved by the Department of Environment and, Natural Resources and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from January 1, 2015 until December 31, 2019, shall void Permit No. WQ001 1431 issued January 25, 2006 and shall be subject to the following specified conditions and limitations: Im SCHF-DES I e No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule I SA NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. 2. The permittee shall be in full compliance with the regional of5ce notification requirements established in Condition 111-3. by February 1, 2015. 3. The permittee shall be in full compliance with the signage requirements established in Condition 111. 13. by June 1, 2015. -a---, a . ^ T 't r - 1 1% P& Qhol I Afr-rzinn ]AMM Page I of 12 L V 1_1149" I The subject residuals management program shall be effectively maintained and aperated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals to the site, contact the Mooresville regional office supervisor, and take any immediate corrective actions. 2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. 3. Only residuals generated by the facilities listed in Attachment A are approved for land application iri accordance with this permit. 4. Only the sites listed in Attachment B are approved for residuals land application. 5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant LoadinLy Rates XPLRs): Parameter Ceiling Ceiling Concentration (milligrams per kilogram)— CPLR (pounds per acre) Arsenic 75 36 Cadmium SS 34 Copper 41300 u 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 77500 2,498 The Permittee shall determine compliance with the CPLRs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application have not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. 6- Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC 02T.1 l06 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. 7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing 0 wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1 107(a)- Exceptions to. this requirement shall be specified in Attachment A. 8. Setbacks for Class B land application sites shall be as follows: WQOO 114331 Version 3.0 'Rh�11 Ver6cm 1 AAI')A Setback by application type (feet) Setback Description Vehicular Irrigation Surface Surface Injection Application Application Incorporation Habitable residence or place of public assembly under separate ownership or not to be maintained as 400 400 200 part of the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the 0 200 0 lessee/operator of the land to be maintained as pan of the pEo ject site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, 100 100 50 perennial waterbodies, and wetlands) Surface water diversions (ephemeral streams, 25 100 25 wateryvays, ditches) Groundwater lowering ditches (where the bottom of 25 100 25 the ditch intersects the SHWT) Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 100 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or 15 15 15 more in vertical height Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 9. Land application areas shall be clearly marked on each site prior to and during any residuals application event. M Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in Nitrogen exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected Z-7 nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculatinc, CI the mean of the best three yields of the last five consecutive crop harvests for each. field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (Litt ://iiLit.rierits.soil.nesu.edu/viela's/index.PLIP). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: 1 Office, the North i Crop management plan as outlined by the local Cooperative Extension Of Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. .11 ^ JAAT7A Paiie 3 of 12 ii• Waste Utilizatiou Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter I '.,P-ovLSWC/tecii/doeLimeats/ 9tiI Quidance Doc 100 109.,pLij). iiio Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS)- These plans must meet the USDA-NRCS 590 Nutrient Management Standards (t :tp-.//ftR- c.sc.e gy u�sda.�ov/�N-1-1­�l/`,)r�actic�c-�,,t�and�aa L.,,/§ _t�jn4ard )Qpd d. If the RYE. and appropriate nutrient, application rates cannot be determined, the 'Perrnittee shall contact the Division to determine necessary action. 11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. '11 If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the surnmer and rye grass in the winter with both crops to receive residuals), then the second crop can receive all application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may be alloured as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. 13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist-, or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Pen-nittee t:7 9 � shall maintain written records of these recommendations and details of their implementation. 14. The compliance boundary for fesidual land application sites shall be specified in accordance with ISA NCAC 02L .0107(b). These sites were individually permitted on or after December 30, 1983; therefore-, the compliance boundary is established at either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to rernediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved relocation Of the COMPLIANCE BOUNDARY will be noted in Attachment B. 15. In accordance with 15A NCAC 02L.0 108, the review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L .01064 t. The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. 2. The Mooresville Regional Office, telephone number (704) 663-1699, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least, 48 hours prior to -the initial residuals land application to any new land application site. Notification to the regional supervisor rvisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday', regional State Holidays. WQOO 11431 Version 3.0 She]] Version 140324 Dutvj� A -%P 11 3. The Mooresville Regional Office shall be notified via einail or telephone, (704) 663-1699, at least 24 hours prior to conducting any land application activity, Such notification shall indicate at a t:) 3 minimum, the anticipated application times, field U)s, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) pursuant to 15A NCAC 02T 1110. Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan- The O&M Plan, at the rninimurn, shall include -- a) Operational functions; b) Maintenance schedules, c Safety measures; d) Spill response plan.; e) Inspection plan including the following information.- i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f) Sampling and monitoring plan including the following information: 0 i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; p 7 i L Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling -frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). 5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with I SA NCAC 08G .0201.. The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 080. 0204, or as specified in the most recently approved O&M plan (Le., see Condition HL 4.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Technical Assistance & Certification Unit at (919) 733-0026. 6. 'then the Permitted land applies bulk residuals, a copy of this permit and a copy of O&M Plan. shall be maintained at the land application sites during land application activities. 7. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. 8. Residuals shall not be stored at any land application site, unless written approval has been requested and received from the Division. 1% 1 It A ^ 1 49 r fl In Qliall Vareinn ldnl?A Paia_e 5 of 12 9. When the Pemiittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters, 10- When the Perrnittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto -which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative ]Extension office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division, It. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. ,If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation., unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; 9. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h- If the soil PH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0 0, or if an agronomist provides information indicatina that the PH of the soil, residuals and lime mixture is suitable for the specified crop, Any pproved variations to the acceptable soil pH (6.0) will be noted in this pen -nit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period 'following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.&, golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application evellt. 13. Public access controls shall include the posting Of signs with a minimum area of 3 square feet (e.g -n shall indicate the activities conducted at each site, permit number, and name and 1.5' x 2'). Each sign contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under J11. 12 apply. 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: WQOO 1143 1 Version 3 -0 Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for.- 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with hairvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 38 months surface shall not be harvested for: I 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (NRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. C; I Any Division required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established., and an acceptable sample reporting schedule shall be followed. 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)l shall be performed at the frequency specified in Attachment A. and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. .­_­ — �F ^ ^ Q"11 Xlxnrjz;nn IAWZ)A Page 7 of 12 The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses). - Arsenic (5.0) 1)4-D ich foro, benzene (7.5) Nitrobenzene (2.0) Barium. (100-0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1:? 1 -Dich loroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2.4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0,03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) Lead (5.0) 2,426-Trichlorophenol (2-0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200,0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 274-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, I the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters -- Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized,, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2), and one vector attraction reduction requirement in 15A NCAC 02T .1107 (a) shall be met. Any uccptions from the requirements in this condition shall be specified in Attachment A. WQOO 1143 1 Version -3. 0 et- -il I An2�A - -1 ­ 5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted OD each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services, website (http://www.neagr.goviagronomi/pLibs.htm). The Permittee shall maintain these results and a description of the sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity—___ Exchan eable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Calcium Potassium P�aCse Exell" S �t Manganese Sodium Cation EY ,,change Capacity Percent Humic Matter, Zinc Copper pH 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 02B �0505. 7. The Permirtee shall maintain records tracking all residual land application events. At a minimum,, these records shall include the following: a- Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number as listed in Attachment B); d. Approximate areas applied to (acres); e. Method of land application; f. Weather conditions (e.g., sunny, cloudy, raining, etc.); g. Predominant Soil Mapping Unit (e-g., CbB2); h. Soil conditions (e.g., dry, wet, frozen, etc.); j. Type of crop or crops to be grown on field; j. Nitrogen Application Rate based on RYEs (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years); k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet ton per acre; 1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or wet tons per acre; m. - Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per acre or wet tons per acre, and m Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other sources of nutrients (e.g,, if applicable), annual and cumulative pounds per acre of each heavy metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury,, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of Phosphorus applied to each field. Qh.:.J1 Pa2e 9 of 12 9. Three copies of an annual report shall be submitted on or before March I". The annual report shall meet the requirements described in the Instructions for Residuals AP_ R Forms. �Kg �Ortinlg Instructions for reporting and annual report forms are available at or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address Division of Water Resources In -formation Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 9. Noncompliance Notification The Permittee shall report by telephone to the Mooresville Regional Office, telephone number (704) 0 663-1699, as soon, as possible, but in no case more than 24 hours or on the next working da following the occurrence or first knowledge of the occurrence of any of the following: y a. Any occurrence with the land application program resulting in the land application I of significant amounts of wastes that are abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to surface waters. Z:1 c. Any time self -monitoring indicates the facility has gone out of compliance with its pen -nit I im itations, d. Any process unit failure, due to known or unknown reasons, rendering the facility p incaable of adequate residual treatment, e- Any spill or discharge from a vehicle or Piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters imminent failure of a storage structure etc. outside normal business hours shall be reported to the, Division's Emergent Response personnel at telephone number (800) 662-y 7956, (800) 858-0368, or (919) 733-3300.PersonF reporting such occurrences by telephone shall also file a written report in letter form within five das following first knowledge of the occurrence. This report shall outline the actions taken or y proposed to be taken to ensure that the problem does not recur, V. ESPECTIOINS The Permit -tee shall provide adequate inspection and maintenance to ensure proppanon of the er oer sub . ect facilities and shall be in accordance with the approved O&M Plan. 9 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals storage, transport and application facilities to prevent malfunctions. facility deterioration and operator errors resulting in discharges, which may cause the release of wastes to the environment, a threat to human health or a public nuisance. The Permittee ha maintain an inspection log that includes, at a minimum tt shall , the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee for a periodshall maintain this inspection. log Division upon request., Of five years from the date of inspection, and this log shall be made available to the Any duly authorized Division representative may, upon Presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or fa i ties permitted at any e cl 0 'ere determining Compliance with this permit; may inspect or reasonable time for the purpose of dete herein cOpy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. WQOO 114 31 Version 3.0 Shp-11 Vptrzin-n I Anl')A V 1 GENERAL,CONDITION'S 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143- 215.6A to 143-215,6C., 1 This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting doCLImentation. 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules,, regulations, or ordinances,, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO 10000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 0214.0500; and documentation of compliance with.Article 21 Part 6 of Chapter 143 of the General Statutes. 5. In the event the residuals program chancres ownership hip or the Permittee changes their name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms,, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. 6. This permit is subject to revocation or unilateral modification upon 60 days notice from the Division Director, in whole or part for the requirements listed in 15.A NCAC 02T.0 I I Oo 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Peri-nittee exemplifies any of the criteria in 15A NCAC 02T .0 1 20(b). 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit pursuant to 15A NCAC 02T.0 I 05(e)(3). Permit issued this the 24hday of October 2014 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION Thomas AAeeder, Director -___ ^__ DJVIS144 Water Resources By Authority of the Environmental Management Commission Permit Number WQ0011431 1 *9 ;rw-,. e% f% I I Alb A F __- —.._ I A Qh.-11 X/Prc;nn I AA I ?,d Pate 11 of 12 C14 10 CC# all cli ca cc —C cs lc� 2 10 U 10 -C CJ co cc C'5 4— ca Cd > mo 0 crs 0 to ce) u cz cli cry 4 vi Coli C6 ca ry ci cz cn U ci ;- Cc op Gn Qn > PC : -- cr OJ 6 R cCt I�T pig ca M=9) Strearn x — x - Fence Ed OnSiteHouse Drain L - PropertyLine Outbuilding -.- . I Pond ApplicationArea UnsuitablIce UtZ01 I inch = 660 feet (all locations approximate) The compliance boundary is established - either 250 feet from the residuals applicat area or 5-0 feet within the property bouriclar-y---- whichever is closest to the application area. The review boundary is established r-nid-ay between the compliance boundary and the perimeter of the residuals applicati-co area. F e, re t 0 160320 640 960 1, 2 86' Legend Stream Drain S-3urf2ceWater x — x - Fence R-4 Propertyl-ine "'N, OnSiteWell AppllcationAre2 M Unsuitable OnSiteHouse Outbuilding A R A2 d a Am ftr IM I inch = 660 feet (6/1 locations approximate) The compliance boundary is established at either 25G feet from the residuals application area or 50 feet within the property boundar� whichever is closest to the application area,._,, The review boundary is established midway between the compliance boundary and the perimeter of the residuals application area - Feet 0 160320 640 960 1.28C APPENDIX II RESIDUALS SOURCE CERTIFICATION • TOWN OF CLEVELAND (FORM: RSC 06-16) RESIDUALS SOURCE CERTIFICATION • TOWN OF CLEVELAND (FORM: RSC 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Town of Cleveland Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current b Proposed Town of Cleveland Cleveland WWTP Rowan NCO049867 82.0 82.0 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 L 1 0 &61J It Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Town of Cleveland 2. Facility permit holder is: ❑ Federal, N State, 0 Local Government, or 0 Private. Facility permit issued by: FlI Div. of Water Resources, Div. of Environmental Health, or Q' Other (explain: M. 3. Facility contact person and title: Paul Land, WWTP Operator Complete mailing address: PO Box 429 City: Cleveland State: N.C. Zip: 27013 Telephone number: (704) 278-4669 E-mail address: 4. Facility physical address: 625 Third Creek Church Road City: Cleveland State: N_C Zip: 27013 Coordinates: Latitude: 35' 44' 38" Longitude: 80' 40' 59.8" Datum: NAD83 Level of accuracy: nearest tenth of second Method of measurement: MAP 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ® treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: 60 % industrial and 40 % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ® Yes ❑ No 7. Facility permitted/design flow: 0.27 MGD and facility average daily flow: 0.15 MGD 8. Average amount of residuals being generated at this facility 11 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 2-oxidation ditches totaling 270,000 gallons, 1-80,000 gallon di eg ster Type and volume of residuals storage (i.e., outside of residuals treatment units): above II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: Biological 0 Non -Biological Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). FORM: RSC 06-16 Page 1 of 5 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: 0 yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 5/28/19 Passed corrosivity test: yes no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: yes no. Flashpoint: >200 OF (> 140°F) Passed reactivity test: Eyes Ono. HCN: <39.1 mg/kg (<250) & H2S: <391 mg/kg (<500) TCLP Parameter Limit (mg/l) Result (Mg/7) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 <0.05 Hexachlorobenzene 0.13 <0.05 Barium 100.0 <0.25 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.10 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <0.005 Lead 5.0 <0.025 Carbon Tetrachloride 0.5 <0.10 Lindane 0.4 <0.0005 Chlordane 0.03 <0.003 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.10 Methoxychlor 10.0 <1.0 Chloroform 6.0 <0.10 Methyl Ethyl Ketone 200.0 <0.20 Chromium 5.0 <0.05 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.05 Pentachlorophenol 100.0 <0.10 o-Cresol 200.0 <0.05 Pyridine 5.0 <0.05 p-Cresol 200.0 <0.05 Selenium 1.0 <0.10 Cresol 200.0 <0.05 Silver 5.0 <0.025 2,4-D 10.0 <0.002 Tetrachloroethylene 0.7 <0.10 1,4-Dichlorobenzene 7.5 <0.05 Toxaphene 0.5 <0.003 1,2-Dichloroethane 0.5 <0.10 Trichloroethylene 0.5 <0.10 1, 1 -Dichloroethylene 0.7 <0.10 2,4,5-Trichlorophenol 400.0 <0.05 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.05 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.002 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.10 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Statesville Analytical and Date of analysis: May 30, 2019 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg1kg) Monthly Average Concentration Limits (Class A Only) (mg1kg) Result (mglkg) Arsenic 75 41 0.402 Cadmium 85 39 1.57 Copper 4,300 1,500 591 Lead 840 300 18.9 Mercury 57 17 0.658 Molybdenum 75 n/a 14.5 Nickel 420 420 16.1 Selenium 100 100 <0.44 Zinc 7,500 2,800 1,399 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 2.28 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Statesville Analytical and Date of analysis: May 30, 2019 Parameter Result (mg/kg) Aluminum 49,000 Ammonia -Nitrogen 270.175 Calcium 32,300 Magnesium 2,330 Nitrate -Nitrite Nitrogen 3,964.91 pH (Standard Unit) 5.65 Phosphorus 330 Potassium 2,509 Sodium 9,473.68 Total Kjeldahl Nitrogen 43,817.5 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 2.06 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): 0 default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: _ e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (11h Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg/kg) Surface 17,164 25,660 Injection/Incorporation 17,299 25,795 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: _ FORM: RSC 06-16 Page 4 of 5 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: composting, 0 heat drying, rq heat treatment, thermophilic aerobic digestion, ❑ beta ray irradiation, gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, air drying, Q anaerobic digestion, composting, i I lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. El Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: 11 Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). [J Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.1107(b)(2)]. id Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of 5 TOWN OF CLEVELAND (FORM: RSC 06-16) (ATTACHMENTS) • VICINITY MAP • PROCESS FLOW DIAGRAM AND/OR NARRATIVE • QUANTITATIVE JUSTIFICATION • SAMPLING PLAN • ANALYTICAL L Vy !7 0 Ji Ltoj As JuaWa/a, CO i7) ;s Awape, a 0 L Oz4" > loo9c, N Of les,cif C�- to Mr co 3rd-Creek Church Rd S6hool Doe R > 0 o 40, Z rNr CION � /. �0�, 460A o Ei� Wastewater Treatment Plant (WWTP) Non -Discharge Permit No. WQ0011431 Requested Dry Tons for Renewal — 82.0 ® Previously Permitted Dry Tons ® 82.0 e Requested Dry Tons for Renewal ® 82.0 V. Sampling and Monitoring Plan Sampling for this project consists of sampling the soils of the permitted fields in order to document that the fields are suitable for land application. Residuals samples are to be collected at the residuals processing facility by the Land Application ORC or his designee. This may include nutrient and metal, pathogen, vector attraction, reduction,, and TCLP samples. Samples should be obtained by the Town of Cleveland or their designated representative prior to any land application activities being performed in order to verify that samples meet regulatory requirements set forth in the permit. Samples should be collected at the frequency specified in the referenced permit. If necessary, the Town of Cleveland or their representative will perform alkaline stabilization of residuals at the wastewater treatment facility. The Land Application ORC or his designee will provide documentation of times, temperatures, and pH of the residuals for the lime stabilization events. The Town of Cleveland or their representative will provide the alkaline stabilization materials and personnel to perform this operation and will designate a responsible party for the documentation that the residuals have passed the alkaline stabilization process. C: Wse rskRob\OneD rive for Business\SharedMMSS Projects\201 5kl 5-03 Bio-Green Services\Phase 03A - Cleveland Permit RenewalXDEQ FormsXTown of Cleveland O&M Plan -Sampling & Monitoring Section - June 2019.doc 6/28/2019 Analytical Results Bio Green Services 383 Potts Road Advance, NC 27006 Receive Date: 04/15/2019 Reported: 06/26/2019 For: Cleveland Digestor Comments: Sample Number Parameter Sample ID Result 190415-17-01 30 Day Benchscale Cleveland 190415-17-01 Aluminum Cleveland 190415-17-01 Ammonia Nitrogen Cleveland 190415-17-01 Arsenic - Solid Cleveland 190415-17-01 Cadmium ICP Cleveland 190415-17-01 Calcium Cleveland 190415-17-01 Copper Cleveland 190415-17-01 Lead Cleveland 190415-17-01 Magnesium Cleveland 190415-17-01 Mercury Solid Cleveland 190415-17-01 Molybdenum Cleveland 190415-17-01 Nickel Cleveland 190415-17-01 Nitrate/Nitrite - Cleveland Solids 190415-17-01 PAN Cleveland 190415-17-01 pH Cleveland 190415-17-01 Potassium - Solid Cleveland 190415-17-01 SAR Cleveland 190415-17-01 Selenium Cleveland 190415-17-01 T. Phosphorous Cleveland 190415-17-01 TCLP Cleveland 190415-17-01 TKN Cleveland 190415-17-01 Zinc Cleveland Unit Method Analyzed Analyst 13.3 % EPA625-R-92/0 04/15/2019 WC 49000 mg/kg EPA 200.7 rev4.4 1994 04/29/2019 MD 270.175 mg/kg SM4500NH3BE-1997 04/16/2019 CL 0.402 mg/kg SM3113 B-2004 04/30/2019 MD 1.57 mg/kg EPA 200.7 04/24/2019 M D 32300 mg/kg EPA 200.7 04/24/2019 MD 591 mg/kg EPA 200.7 04/29/2019 M D 0.43 mg/L SM3113B-2004 04/17/2019 MD 2330 mg/kg EPA 200.7 04/24/2019 M D 0.658 mg/kg SM311213-2011 04/26/2019 MD 14.5 mg/kg EPA 200.7 04/29/2019 MD 16.1 mg/kg EPA 200.7 04/29/2019 M D 3964.91 mg/kg SM450OF/A 05/01 /2019 CL 210.7 mg/L Calculation 05/02/2019 CL 5.65 Std. Units SM4500HB-2011 04/16/2019 MD 2510 mg/kg EPA200.7 04/22/2019 Meritech 2.06 % Calculation 05/02/2019 CL <0.44 mg/kg EPA 200.7 04/30/2019 MD 330 mg/L SM450OPE-2011 04/25/2019 CL See Attached as Noted 04/16/2019 PACE 43817.5 mg/kg SM4500Norg B-2011 04/17/2019 CL 1399 mg/kg EPA 200.7 04/29/2019 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 45 Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst wwwuwn� 190415-17-01 Percent Solids Cleveland 2.28 % SM254OB-2011 190415-17-01 Sodium - Solid Cleveland 9473.68 mg/kg SM 3111 B Respectfully submitted, (" Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 04/16/2019 IVID 04/18/2019 IVID PO Box 228 • Statesville, NC 28687 * 704/872/4697 Page 2 of 45 Condition m� �*��~��~,. Receipt ~u_~Sample Number 190415-17-01 Temp on Arrival: 3.2 Parameter Schedule: Nitric Acid Received onIce Chemicals in containers, lab Received onIce Chemicals in containers, lab Received onIce Chemicals in containers, lab Parameter Schedule: Arsenic -SoUd Nitric Acid Parameter Schedule: Nitric Acid Parameter Schedule: Nitric Acid Parameter Schedule: Nitric Acid Parameter Schedule: Received onIce Chemicals incontainers, lab Copper Received onIce Chemicals in containers, lab Lead Received onIce Chemicals in containers, lab Selenium Received onIce Chemicals in containers, lab Nitric Acid Received onIce Chemicals in containers, lab Parameter Schedule: Sodium Nitric Acid Chemicals incontainers, |ob Received onIce Parameter Schedule: Sodium - Solid Nitric Acid Received onIce Chemicals in containers, lab Parameter Schedule: Nitric Acid Received onIce Chemicals in containers, lab Parameter Schedule: Received onIce Chemicals in containers, lab PDBox 22O°Statesville, NC28G07°7O4/072/4G97 Parameter Schedule: Parameter Schedule: Received on Ice Chemicals in containers, lab Received on Ice Chemicals in containers, lab Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: pH Received on Ice Chemicals in containers, lab Parameter Schedule: Received on Ice Parameter Schedule: TCLP Received on Ice Parameter Schedule: TKN Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Parameter Schedule: Received on Ice Received on Ice Parameter Schedule: Potassium Received on Ice Chemicals in containers, lab PO Box 228 ® Statesville, NC 28687 • 704/872/4697 Page 4 of 45 Parameter Schedule: Potassium ® Solid Chemicals in containers, lab Received on Ice Parameter Schedule: Nitrate/Nitrite Received on Ice Chemicals in containers, lab Parameter Schedule: Nitrate/Nitrite ® Solids Chemicals in containers, lab Received on Ice P® Box 228 9 Statesville, NC 28687 ® 704/872/4697 Page 5 of 45 gt, jo 9 abeci /-69-V/Z/-8/i7O/- e 1-898Z:)Nf@ll!AS31elS ® SZZ X®8 ®d d z Ul t z w 0 a E C) CL C:cz 0 0 a �G CD E E r- 0 0 0 L419 Cj) ca V2 r) E E E C. CL E E E L.L 00 cyj cv� E E E E 0 2i ti cn c 0 a- a- d: 0 (U.0 E 0 z cz ca E per, E E E E CL CL CIL E E E E co co Ck 75 >I Zn w 0 (D > cr CD E E C)l a) a) Q Q ol E E E 0 o 0 U cr- EL cEr-cr- 9-V 10 L abed 1-69t,/Z1-8/i701- * 1-898Z DN "@jj!ASajejS ® 8ZZ X09 Od The TCLF1 analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4-Dichlorobenzene (7.:)') Nitrobenzene (2.0) Pentachlorophenol (100.0) Barium (100.0) 1,2-Dichloroethafie (0.5) Benzene (0.5) 1, 1 -D ich loroethylene (0.7) Pyridine (5.0) Cadmium (i .0) 1,4-Dinitrotoluene (0. 13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02.) Silver (5�0) w. Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0,7) Chlorobenzene (100,0) Heptachlor (and its hydroxide) Toxaphene (0,115) Chloroform (6.0) il 14exacliloro-t.3-1)utadiene(0,5)t-- Trichloroethylene(0.55) Chromium (5.0) Hexach]OTOCIhane (3.0) 2.4,5-Trichlorophenol (4WO) rn-Cresol (200.0') Lead (5.0) 1),4,6-Trichlorophenot o-Cresol (200.0) Lindane (0,4) 2,4,S-T1 (Silvex) (1.0) p-Cresol (200.0) Mercury (0,121) Vinyl chloride (0,2) Cresol (200.0) Mlethoxvchlor (1100) .1,-1-D (10,0) Meths vh\i ketone (200.0) Once the residuals have been monitored for Mlo years at the frequency specified in Attachment A. the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement, In no case shall the monitoring frequency be less than onu per permit cycile. as An analysis shall be conducted on residuals from each sou"%-e generating facilit-y at the frequency specified in Attachment A, and the Perminee shall maintain he results for a minimurn of five years. The analysis shall include, the fbllo�� ink; Aluminum mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic N Icke I SodIUM Sodium Adsorption Ratio Cadmium Mt -.ate -Nitrite Nitrogen (SAR) Calcium PercentTo-tal Solids TKN Copper PH Zinc Lead Phosphorus Plant Available Nitrogen i Magnesium (by calculation) 4e Residual's shall be monitored for compliance %,ith pathogen and vector attraction reduction requirements at the frequency specified in Attachment A. and at the time indicated in the sampling and monitoring sections of the approved O&M plena. The required data sha-11 be specific to the stabilization process utilized, and sufficient to demonstrate compliance with thr. Class 'R pathonen reduction requirements in 15A NCAC 02T .1 106- (,ti) and (b){.2}, and one vector attraction reduCtion requirement in 15A NCAC 021' .1107 (a) shall be met. Any exce-Intions fTorn the requirements in this condition shall be spccificd in Attachnicnt A. WQ001 1431 Version 3.0 1c,"n'.01 lAn'I'lil Meriftech, Inc. Environmental Laboratory Laboratory Certification No. 165 Contact: C. Little Report Date: 5/1/2019 Client: Statesville Analytical 122 Court St Statesville, NC 28677 Date Sample Rcvd: 4/18/2019 Meritech Work Order # 04181972 Sample: 190415.17.01 Grab 4/15/2019 Parameter Results Analvsis Date Reuortine Linflt Potassium, total ST2 nig/L 4/22/201.9 1.00 mg/L EPA 200,7 I hereby certify that I have reviewed and approve the.ve data. Lab ra-61--Y Re' prese n ta t! ve 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 P® Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 8 of 45 V) cj (D 0 =3 CL CDL c 3 A, 0 rD CL rD V (D X 0 0 ;V M m a c CL CD 0 (D 0) < z 0 3 < (D m ii p :3 Z c) m r+ V) 0 0 CL 0 0 m Ln ro z .4 M 0 0 Ln tD w M -n > CL 0 0 0 J 0 > + r cr 3 in cu 3 3 mum (D 20 m NJ M -3 CL 00 CL —4 M (D (A ro (D (D D IAJ 1� 1� z 0 0 0 3 CA > e*+ it > CL (D CL r 0 rD r+ Vw 0 m ni (D =r cz a- CL EL cr :3 r+ m 3 7V a— 0 - M� (D M r+ (D 0 4 0 -a CL) 0 X (D 44 tit% b a (D < C: .-Q K m Ej C CL OQ m rD Ln > V, 0, rb < LJ N�4 (D jy M 0 -jN PO Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 9 of 45 ceAnalytical www.pacelabs.com Crystal Little Statesville Analytical, Inc. 122 Court Street PO Box 228 Statesville, NC 28687 RE: Project: 190415.17.01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Crystal Little: Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Tyriek Hooks tyriek.hooks@pacelabs.com (704)875-9092 Project Manager Enclosures : hkoo, 4A', REPORT OF LABORATORY ANALYSIS k 121 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 36 PO Box 228 * Statesville, NC 28687 * 704/872/4697 Page 10 of 45 Analytical wwwpa"41abs, com Project: 190415.17.01 Pace Project No,: 92425692 Pennsylvania Certification lDs 1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601 Missouri Certification 235 ANAB DOD-ELAP Rad Accreditation #: L2417 Montana Certification Cert0082 Alabama Certification #: 41590 Nebraska Certification #*, NE-OS-29-14 Arizona Certification M AZ0734 Nevada Certification #: PA01457201 &-1 Arkansas Certification New Hampshire/TNI Certification #- 2976,17 California Certification #: 04222CA New Jersey/TNI Certification #' PA051 Colorado Certification #. PA01 547 New Mexico Certification #: PA01457 Connecticut Certification 4: PH-0694 New York/TNI Codification #: 10888 Delaware Certification North Carolina Certification #: 42706 EPA Region 4 DW Rad North Dakota Certification #: R-190 Flodda/TNI Certification #-, E87683 Ohio EPA Rad Approval: #41249 Georgia Certification #: C040 Oregon/TNI Certification #. PA200002-010 Guam Certification Pennsylvania/TNI Certification #: 65-00282 Florida; Cod E871149 SEKS WET Puerto Rico Certification #-, PA01457 Hawaii Certification Rhode Island Certification #'. 65-00282 Idaho Certification South Dakota Certification Illinois Certification Tennessee Certification #. 02867 Indiana Certification Texas/TNI Certification #: T104704188-17-3 Iowa Certification #-, 391 Utah/TNI Certification #: PA014572017-9 Kansas/TNI Certification 4: E-10358 USDA Soil Permit #: P330-17-00091 Kentucky Certification #'. KY90133 Vermont Dept, of Health: ID# VT-0282 KY WW Permit #. KY0098221 Virgin Island/PADEP Certification KY WW Permit #: KY0000221 Virginia/VELAP Certification #: 9526 Louisiana DHH/TNI Certification #-. LA180012 Washington Certification #: C868 Louisiana DEQ/TNI Certification #. 4086 West Virginia DEP Certification #: 143 Maine Certification #: 2017020 West Virginia DHHR Certification #. 9964C Maryland Certification #. 308 Wisconsin Approve List for Rad Massachusetts Certification #. M-PA1457 Wyoming Certification #: 8TMS-L Michigan/PADEP Certification #: 9991 Charlotte Certification lDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #. 99006001 LOLlisiana/NELAP Certification # LAI 70028 Florida/NELAP Certification #-. E87627 North Carolina Drinking Water Certification #: 37706 Kentucky LIST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #-1 460221 North Carolina Wastewater Certification 9: 12 Asheville Certification lDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification E87648 South Carolina Certification 99030001 Massachusetts Certification M-NC030 Virginia/VELAP Certification 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 36 PO Box 228 * Statesville, NC 28687 ® 704/872/4697 Page 11 of 45 .-OWN ",-,..,6ceAna1yfica1 wwwpac;elabs,com Project: 190415.1T01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 HUntersville, NC 28078 (704)875-9092 Anarlytes Lab ID Sample ID Method Analysts Reported Laboratory 92425692001 190415.17.01 EPA 8081 B SEM 9 PASI-C EPA 8082A SEM 8 PASI-C EPA 8082A SEM 8 PASI-C EPA 601 OD SH1 7 PASI-A EPA 7470A JMW1 I PASI-A EPA 8270E BPJ 18 PASI-C EPA 8260D CLAW 14 PASI-C ASTM D2974-87 KDF I PASI-C EPA 101 OA SMK 1 PASI-A EPA 9045D SMK 1 PASI-A EPA 9095B MD W 1 PASI-A EPA 9014 PAS 1 PASI-PA SM 450OS2F-00 PAS 1 PAS1--PA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC- Page 3 of 36 PO Box 228,* Statesville, NC 28687 * 704/872/4697 Page 12 of 45 cemalyticab 9. wvvwpacelabs'com ANALYTICAL RESULTS Project: 190415.17.01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HUntersville, NC 28078 (704)875-9092 Sample. 190415.17.01 Labll): 92425692001 Collected: 04/15/19 10:00 Received: 04/16/19 13:55 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 TCLP Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 351 OC Leachate Method/Date: EPA 1311; 04/23/19 12.30 Initial pH.- 4.68; Final pH: 5 gamma-BHC (Lindane) ND ug/L 0.50 1 04/24/19 12:09 04/25/19 20:53 58-89-9 Chlordane (Technical) ND ug/L 3.0 1 04/24/19 12:09 04/25/19 20:53 57-74-9 Endrin ND ug/L 0.50 1 04/24/19 12:09 04/25119 20:53 72-20-8 Heptachlor ND ug/L 0.50 1 04/24119 12:09 04/25/19 20:53 76-44-8 Heptachlor epoxide, ND ug/L 0.50 1 04/24/19 12:09 04/25119 20:53 1024-57-3 Methoxychlor ND ug/L 1000 1 04/24/19 12:09 04/25119 20:53 72-43-5 Toxaphene ND uq1L 3.0 1 04/24/19 12-,09 04/25/19 20:53 8001-35-2 Surrogates Decachlorobiphenyl (S) 96 % 10-138 1 04/24/19 '12:09 04/25/19 20-53 2051-24-3 Tetrachloro-m-xylene (S) 84 % 10-110 1 04/24/19 12.09 04/25119 20:53 877-09-8 8082 GCS PCB Analytical Method: EPA 8082A Preparation Method. EPA 3546 PCB-1016 (Aroclor 1016) ND ug/kg 1300 1 04/18/19 16,18 04/24/19 05:03 12674-11-2 PCB-1221 (Aroclor 1221) ND uglkg 1300 1 04/18/19 16:18 04/24/19 05:03 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/kg 1300 1 04/18119 16:18 04/24/19 05:03 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/kg 1300 1 04/18119 16:18 04/24/19 05,03 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/kg 1300 1 04/18/19 16:18 04/24119 05:03 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/kg 1300 1 04/181119 16:18 04/24/19 05,03 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/kg 1300 1 04/18/19 16:18 04124/19 05,03 11096-82-5 Surrogates Decachlorobiphenyl (S) 79 % 10:-130 1 04/18/19 16.18 04/24/19 05:03 2051-24-3 8082 TCLP PCBs RVE Analytical Method: EPA 8082A Preparation Method: EPA 351 OC Leachate Method/Date, EPA 1311; 04/23/19 12,30 Initial pH- 4.68,- Final pH, 5 PCB-1016 (Aroclor 1016) ND ug/L 1000 1 04/24/19 12:09 04/25/19 23:39 12674-11-2 PCB-1221 (Aroclor 1221) ND ug/L 1000 1 04/24/19 12:09 04/25/19 23:39 11104-28-2 PCB-1232 (Aroclor 1232) ND ug/L 1000 1 04/24119 12:09 04/25119 23.39 11141-16-5 PCB-1242 (Aroclor 1242) ND ug/L 1000 1 04/24/19 12:09 04/25119 23,39 53469-21-9 PCB-1248 (Aroclor 1248) ND ug/L 1000, 1 04/24/19 12:09 04/25/19 23:39 12672-29-6 PCB-1254 (Aroclor 1254) ND ug/L 1000 1 04/24/19 12:09 04/25/19 23:39 11097-69-1 PCB-1260 (Aroclor 1260) ND ug/L 1000 .1 04/24/19 12:09 04125119 23:39 11096-82-5 Surrogates Decachlorobiphenyl (S) 92 % 10-132 1 04/24/19 12:09 04/25/19 2339 2051-24-3 6010 MET ICP, TCLP Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA Leachate Method/Date. EPA 1311; 05/01/19 18:34 Initial pH: 6.7; Final pH: 4,5 Arsenic ND mg/L 0,050 1 05/03/19 1239 05/04/19 16:08 7440-38-2 Ig Barium ND mg/L 0,25 1 05/03/19 12:39 05/04119 16:08 7440-39-3 1g Cadmium ND mg/L 0.0050 1 05103119 12:39 05/04119 16,08 7440-43-9 Ig Chromium ND mg/L- 0.050 1 05103119 12:39 05/04/19 16:08 7440-47-3 19 Lead ND mg/L 0.025 1 05/03119 12:39 05/04/19 16:08 7439-92-1 1g Selenium ND mg/L 0.10 1 05/03/19 1239 05/04/19 16:08 778249-2 lg Silver ND mg/L 0.025 1 05/03119 12:39 05/04/19 16:08 7440-22-4 1g REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC, Page 4 of 36 P® Box 228 e Statesville, NC 28687 9 704/872/4697 Page 13 of 45 ucue A 1"Unlytical wwwpacelabs.com ANALYTICAL RESULTS Project- 190415,17.01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 190415.17.01 Lab ID: 92425692001 Collected. 04/15/19 10.00 Received: 04/16/19 13.55 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. (dual 7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A Leachate Method/Date: EPA 1311; 05/01/19 18:34 Initial pH. 6.7; Final pH: 4.5 Mercury 8270E MSSV TCLP Sep Funnel 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3--butadiene Hexachlorobenzene Hexachloroethane 2-Methylptienol(o-Cresol) 3&4- M ethyl phenol (m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4.,5-Trichlorophenof 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 12-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Date: 05/28/2019 05:00 PM ND mg/L 0,,00020 1 05102/19 16:48 05/03119 14:11 7439-97-6 Ig Analytical Method, EPA 8270E Preparation Method: EPA 351 OC ND ug/L 50,0 1 04/24/19 22:40 04125119 18,36 106-46-7 ND ug/L 50,0 1 04/24/19 22:40 04/25119 18:36 121-14-2 ND ug/L 50.0 1 04/24/19 22.40 04/25/19 18:36 87-68-3 ND ug/L 50.0 1 04/24/19 22:40 04/25/19 18:36 118-74-1 ND ug/L 50.0 1 04/24/19 22:40 04/25/19 1&36 67-72-1 ND ug/L 50.0 1 04/24/19 22:40 04/25/19 18,36 95-48-7 ND ug/L 50.0 1 04/24/19 22:40 04125/19 18:36 15831-10-4 ND ug/L 50.0 1 04124/19 22,40 04/25/19 18,36 98-95-3 ND ug/L 100 1 04/24119 22A0 04/25/19 18:36 87-86-5 ND ugIL 50,0 1 04/24/19 22;40 04/25/19 18:36 110-86-1 ND ug/L 50.0 1 04/24/19 22:40 04/25/19 18.36 95-95-4 ND ug/L 50.0 1 04/24/19 22:40 04/25/19 18:36 88-06-2 50 % 12-102 1 04/24119 22:40 04/25/19 18:36 4165-60-0 71 % 13-107 1 04/24/19 22;40 04/25/19 18,36 321-60-8 113 % 21-132 1 04/24/19 22:40 04/25/19 18:36 1718-51-0 7 % 10-110 1 04/24/19 22:40 04/25/19 18:36 '13127-88--3 S2 5 % 10-110 1 04/24/19 22,40 04/25/19 1836 367-12-4 S2 17 % 27-108 1 04/24/19 22.40 04/25/19 18:36 118-79-6 S2 Analytical Method, EPA 8260D ND ug/L 100 20 04/26/19 03:11 71-43-2 ND ug/L 200 20 04126/19 03-11 78-93-3 ND ug/L 100 20 04/26119 03.11 56-23-5 ND ug/L 100 20 04/26/19 03:11 108-90-7 ND ug/L 100 20 04/26/19 03:11 67-66-3 ND ug/L 100 20 04/26/19 03:11 106-46-7 ND ug/L 100 20 04/26/19 03:11 107-06-2 ND ug/L 100 20 04/26/19 03:11 75-35-4 ND ug/L 100 20 04/26/19 0111 127-18-4 ND ug/L 100 20 04/26/19 03:11 79-01-6 ND ug/L 100 20 04/26/19 03:11 75-01 A 103 % 70-130 20 04/26/19 03:11 17060-07-0 108 % 67-135 20 04/26/19 03:11 2037-26-5 103 % 70-130 20 04/26/19 03:11 460-00-4 Analytical Method: ASTM D2974-87 97.5 % 0.10 1 04/16/19 17:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC, Page 5 of 36 P® Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 14 of 45 ceAnalytical w1mpacelabs,corn FIIINXTIMWA061149N�� Project: 190415,17.01 Pace Project No., 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 190415.17.01 LablD: 92425692001 Collected: 04/15/19 10:00 Received: 04/16/19 13:55 Matrix: Solid Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 1010 Flashpoint,Closed Cup Analytical Method: EPA 101 OA Flashpoint >200 deg F 70.0 1 04/28119 14A4 9045 pH Soil Analytical Method: EPA 9045D pH at 25 Degrees C 6.7 Std. Units 0,10 1 04/29/19 11:23 H3 9095 Paint Filter Liquid Test Analytical Method. EPA 9095B Free Liquids Fail 1.0 1 04/18/19 17,55 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method- SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 39,1 1 04122/19 17:39 04/22/19 18:54 734E Reactive Sulfide Analytical. Method: SM 4504S2F-00 Preparation Method, SW-846 73.4.2 Sulfide, Reactive ND mg/kg 391 1 04/22/19 17:39 04/22/19 17,48 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC, Qual Page 6 of 36 P® Box 228 o Statesville, NC 28687 o 704/872/4697 Page 15 of 45 ;e u^ n Ar-t -n a 'n, a ly Aca wwwpacelabscurry Project: 190415.17.01 Pace Project No.: 92425692 QC Batch: 472928 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP Associated Lab Samples- 92425692001 METHOD BLANK- 2563088 Associated Lab Samples, 92425692001 Parameter Units Mercury mq/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.00020 05/03/19 13,55 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2565344 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/L 0,0025 O.0024 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2565345 2565346 MS MSD 92425680001 Spike Spike IVIS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury nig/L ND 0.0025 0.0025 0.0026 0,0026 104 103 75-125 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date- 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 36 PO Box 228 e Statesville, NC 28687 e 704/872/4697 Page 16 of 45 -1? 41of" 11 A `�v. ",flakeAnalyfical wwwpacelabs.com Project, 190415.17,01 Pace Project No.: 92425692 QC Batch: 472926 Analysis Method: EPA 601 OD QC Batch Method: EPA 301 OA Analysis Description: 6010 MET TCLP Associated Lab Samples, 92425692001 METHOD BLANK: 2563088 Associated Lab Samples, 92425692001 Parameter Arsenic Barium Cadmium Chromium Lead Selenium Silver Matrix: Water Blank Reporting Units Result Limit Analyzed Qualifiers rng/L ND 0.050 05/04/19 15;38 mg/L ND 0.25 05/04/19 15:38 mg/L ND 0.0050 05/04/19 15:38 mg/L ND 0,050 05/04/19 15:38 mg/L ND 0.025 05/04/19 15.38 mg/L ND 0.10 05/04/19 15:38 mg/L ND 0.025 05/04119 15:38 LABORATORY CONTROL SAMPLE: 2565337 Parameter Units Arsenic mg/L Barium mg/L Cadmium mg1L Chromium mg/L Lead mg/L Selenium mg/L Silver mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2,3 92 80-120 2.5 2.3 93 80-120 2.5 2A 94 80-120 2.5 2A 94 80-120 2.5 2.3 91 80-120 2.5 24 97 80-120 1.2 1.2 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2565338 2565339 MS MSD 92422459001 Spike Spike MS MSD MS MSD % I-Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Arsenic mg/L ND 2.5 2.5 2.3 2-3 94 92 75-125 2 Barium mg/L 0.74 2.5 2.5 3.2 3.1 97 95 75-125 1 Cadmium mg/L. ND 2.5 2.5 2.4 23 95 94 75-125 2 Chromium mg/L. ND 2.5 2.5 2A 2.3 96 94 75-125 2 Lead mg/L ND 2.5 2.5 2,3 2.3 92 91 75-125 2 Selenium mg/L ND 2.5 2.5 2.4 2.4 97 96 75-125 1 Silver mg/L ND 12 1.2 1.2 1,2 96 95 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date., 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LIC. Page 8 of 36 PO Box 228 e Statesville, NC 28687 ® 704/872/4697 Page 17 of 45 ceAnalytical wwwpacelabs.com Project: 190415,17.01 Pace Project No.: 92425692 QC Batch: 471650 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV TCLP Associated Lab Samples: 92425692001 METHOD BLANK: 2559314 Associated Lab Samples: 92425692001 Parameter Units Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers M-Dichloroethene ug/L ND 5.0 04/26/19 01-29 1,2-Dichloroethane ug/L ND 5.0 04/26119 01,29 1,4.-Dichlorobenzene ug/L ND 5.0 04/26/19 01:29 2-Butanone (MEK) ug/L ND 10.0 04/26/19 01:29 Benzene ug/L ND 5.0 04/26/19 01:29 Carbon tetrachloride ug/L ND 5,0 04/26/19 01:29 Chlorobenzene ug/L ND 5.0 04/26/19 01:29 Chloroform ug/L ND 5.0 04/26/19 01-29 Tetra ch loroethene ug/L ND 5,0 04/26119 01.29 Trichloroethene ug/L ND 5.0 04/26/19 01:29 Vinyl chloride ug/L ND 5,0 04/26119 01:29 1,2-Dichlor,oethane-d4 (S) % 104 70-130 04/26/19 01 :29 4-Bromofluorobenzene (S) % 102 70-130 04/26/19 01-29 Toluene-d8 (S) % 112 67-135 04/26/19 01:29 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 HUntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2559313 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1-Dichloroethene ug/L 50 46.6 93 70-130 1,2-Dichloroethane Ug/L 50 45A 91 70-130 1,4-Dichlorobenzene ug/L 50 49.3 99 70-130 2-Butanone (MEK) ug/L. 100 123 123 64-135 Benzene ug/L 50 48-5 97 70-130 Carbon tetrachloride ug/L 50 47.3 95 70-130 Chlorobenzene ug/L 50 48.9 98 70-130 Chloroform ug/L 50 417 87 70-130 Tetra ch loroethen e Ug/L 50 51A 103 69-130 Trichloroethene ug/L 50 51.6 103 70-130 Vinyl chloride ug/L 50 42.0 84 70-131 1,2-Dichloroetl1ane-d4 (S) % 92 70-130 4-Bromofluorobenzene (S) % 93 70-130 Toluene-d8 (S) % 93 67-135 MATRIX SPIKE& MATRIX SPIKE DUPLICATE- 2559315 2559316 MS MSD 92425692001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc., Result Result % Rec % Rec Limits RPD Qual 1,1-Dichloroethene ug/L ND 400 400 381 410 95 103 70-154 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LIC, Page 9 of 36 PO Box 228 ® Statesville, NC 28687 9 704/872/4697 Page 18 of 45 jceAna1y6crW' wwwpacelabs. Coln MMM Project: 190415.17.01 Pace Project No.: 92425692 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2559315 MS 92425692001 Spike Parameter Units Result Conc. 1,2-Dichloroethane ug/L ND ~ 400 1,4-Dichlorobenzene ug/L ND 400 2-Butanone (MEK) ug/L ND 800 Benzene ug/L ND 400 Carbon tetrachloride ug/L ND 400 Chlorobenzene ug/L ND 400 Chloroform ug/L ND 400 Tetra ch loroethen e ug/L ND 400 Trichloroethene ug/L ND 400 Vinyl chloride ug/L. ND 400 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HUntersville, NC 28078 (704)875-9092 2559316 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 400 381 384 95 96 70-137 1 400 411 433 103 108 70-133 5 800 852 830 107 104 60-139 3 400 421 437 105 109 70-151 4 400 427 469 107 117 70-143 9 400 412 424 103 106 70-138 3 400 352 386 86 94 70-139 9 400 415 424 104 106 59-143 2 400 459 450 115 112 70-147 2 400 434 436 108 109 70156 1 91 89 70-130 96 96 70-130 96 95 67-135 Results presented on this page are in the units indicated by the "Units" column except when an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date, 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 36 PO Box 228,* Statesville, NC 28687 ® 704/872/4697 Page 19 of 45 AI www.pacefabs.com Project: 190415.17,01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875--9092 QC Batch: 471215 Analysis Method: EPA 8081 B QC Batch Method: EPA 351 OC Analysis Description- 8081 TCLP Pesticides RV Associated Lab Samples: 92425692001 METHOD BLANK: 2555379 Matrix- Water Associated Lab Samples, 92425692001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chlordane (Technical) ug/L ND 3.0 04/25/19 20:40 Endrin ug/L ND 0.50 04/25/19 20.40 gamma-BHC (Lindane) ug/L ND 0,50 04125/19 20--40 Heptachlor ug/L ND 0,50 04/25/19 20:40 Heptachlor epoxide ug/L ND 0.50 04/25/19 20-40 Methoxychlor ug/L ND 1000 04/25/19 20:40 Toxaphene ug/L ND 3.0 04/25/19 20,40 Decachlorobiphenyl (S) % 93 10-138 04/25/19 20:40 Tetrachloro-m-xylene (S) % 64 10-110 04/25/19 20:40 LABORATORY CONTROL SAMPLE: 2557097 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Endrin ug/L 1.2 1.1 89 20-134 gamma-BHC (Lindane) ug/L 12 11 87 20-118 Heptachlor ug/L 1.2 I'D 81 20-142 Heptachlor epoxide ug/L 1,2 I'll 91 22-133 Methoxychlor ug/L 3.8 37J 97 44-150 Decachlorobiphenyl (S) % 93 10-138 Tetra ch loro-m-xylene (S) % 82 10-110 MATRIX SPIKE SAMPLE: 2557098 92425245001 Spike MS IVIS % Rer, Parameter Units Result Conc. Result % Rec Limits Qualifiers Endrin ug/L ND 1.2 1A 86 21-133 gamma-BHC (Lindane) ug/L ND 11 1.0 83 24-119 Heptachlor ug/L ND 1.2 0.95 76 16-128 Heptachlor epoxide ug/L ND 1.2 1,0 81 50-150 Methoxychlor ug/L ND 3.8 3.5J 94. 50-1150 Decachlorobiphenyl (S) % 82 10-138 Tetrachloro-m-xylene (3) % 77 10-110 SAMPLE DUPLICATE'- 2557099 92425245002 Dup Parameter Units Result Result RPD Qualifiers Chlordane (Technical) ug/L ND ND Endrin ug/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05128/2019 05:00 PM ,vithout the written consent of Pace Analytical Services, LLC. Page 11 of 36 PO Box 228 e Statesville, NC 28687o 704/872/4697 Page 20 of 45 aceAnalytical wwwpacefabsecom Project: 190415.17,01 Pace Project No.., 92425692 SAMPLE DUPLICATE: 2557099 Parameter gamma-BHC (Lindane) Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Units ug/L ug/L ug/L ug/L ug/L 92425245002 Dup Result Result ND ND ND ND ND 93 93 RPD Qualifiers Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville-,, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT ®F LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05-00 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 36 PO Box 228 9 Statesville., NC 28687 e 704/872/4697 Page 21 of 45 -1 '00-0 7 vewwpacelabs, corn Project: 190415.17.01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 HUntersville, NC 28078 (704)875-9092 QC Batch: 470280 Analysis Method: EPA 8082A QC Batch Method-, EPA 3546 Analysis Description. 8082 GCS PCB Associated Lab Samples: 92425692001 METHOD BLANK: 2553290 Matrix: Solid Associated Lab Samples: 92425692001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers PCB-1016 (Aroclor 1016) ug/kg ND 33.6 04/24/19 07:08 PCB-1221 (Aroclor 1221) ug/kg ND 33,6 04/24/19 07:08 PCB-1232 (Aroclor 1232) ug/kg ND 33.6 04/24/19 07:08 PCB-1242 (Aroclor 1242) ug/kg ND 316 04/24/19 07:08 PCB-1248 (Aroclor 1248) ug/kg ND 33,6 041124/19 07-08 PCB-1254 (Aroclor 1254) uglkg ND 33.6 04/24/19 07:08 PCB-1260 (Aroclor 1260) ug/kg ND 33.6 04/24/19 07:08 Decachlorobiphp.nyl (S) % 86 10-130 04/24/19 07-08 LABORATORY CONTROL SAMPLE: 2553291 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) uglkg 169 164 97 35-130 PCB-1260 (Aroclor 1260) ug/kg 169 129 76 46-130 Decachlorobiphenyl (S) % 91 10-130 MATRIX SPIKE SAMPLE: 2553292 92425960001 Spike IVIS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) uglkg ND 206 ....... 174 ...... 85 10-130 PCB-1260 (Aroclor 1260) ijg/kg ND 206 125 61 10-130 Decachlorobiplienyl (S) % 71 10-130 Results presented on this page are in the units indicated by the "Units" COILIMn except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC., Page 13 of 36 PO Box 228 ® Statesville, NC 28687 * 704/872/4697 Page 22 of 45 A c e /4 na lXica wwpacelabs.com Project: 190415.17,01 Pace Project No.: 92425692 QC Batch: 471354 Analysis Method: EPA 8082A QC Batch Method: EPA 351 OC Analysis Description., 8082 TCLP PCB RV Associated Lab Samples, 92425692001 METHOD BLANK: 2555379 Associated Lab Samples: 92425692001 Parameter Units PCB-1016 (Aroclor 1016) ug/L PCB-1221 (Aroclor 1221) ug/L PCB-1232 (Aroclor 1232) ug/L PCB-1242 (Aroclor 1242) ug/L PCB-1248 (Aroclor 1248) ug/L PCB-1254 (Aroclor 1254) ug/L PCB-1260 (Aroclor 1260) Ug/L Decachlorobiphenyl (S) % Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1000 04/26/19 00.04 ND 1000 04126/19 00.04 ND 1000 04/26/19 00:04 ND 1000 04/26/19 00:04 ND 1000 04/26119 00-04 ND 1000 04/26/19 00:04 ND 1000 04/26/19 00:04 89 10-132 04/26/19 00:04 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE. 2557804 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L. 25 ND 90 38-113 PCB-1260 (Aroclor 1260) ug/L 25 ND 76 35-120 Decachlorobiphenyl (S) % 98 10-132 MATRIX SPIKE SAMPLE: 2557805 92425245001 Spike IVIS IVIS % Rec Parameter Units Result Cork, Result % Rec Limits Qualifiers PCB-1016 (Aroclor 1016) ug/L ND 25 ND 82 19-142 PCB-1260 (Aroclor 1260) ug/L ND 25 ND 64 19-142 Decachlorobiphenyl (S) % 77 10-132 SAMPLE DUPLICATE. 2557806 92425245002 Dup Parameter Units Result Result RPD Qualifiers PCB-1016 (Aroclor 1016) ug/L ND ND PCB-1221 (Aroclor 1221) ug/L ND ND PCB-1232 (Aroclor 1232) ug/L ND ND PCB-1242 (Aroclor 1242) ug/L ND ND PCB-1248 (Aroclor 1248) ug/L ND ND PCB-1254 (Aroclor 1254) ug/L ND ND PCB-1260 (Aroclor 1260) ug/L ND ND Decachlorobiphenyl (S) % 91 76 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 36 1 PO Box 228 e Statesville, NC 28687 * 704/872/4697 Page 23 of 45 ceAnalyfical wwwpacelab&com Project: 190415,17,01 Pace Project No.: 92425692 QC , Batch: 471352 Analysis Method: EPA 8270E QC Batch Method: EPA 351 OC Analysis Description: 8270E TCLP MSSV Associated Lab Samples: 92425692001 METHOD BLANK: 2555379 Associated Lab Samples'. 92425692001 Parameter Units 2,4,6-Tribromophenol (S) % 2-Fluorobiphenyl (S) % 2-Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6(S) % Terphenyl-d14 (S) % Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HUntersville, NC 28078 (704)875-9092 Matrix. Water Blank Reporting Result Limit Analyzed Qualifiers 90 27-108 04/25/19 10-33 67 13-107 04/25/19 10:33 18 10-110 04/25/19 10:33 68 12-102 04/25/19 10:33 10 10-110 04/25/19 10:33 85 21-132 04/25/19 10:33 LABORATORY CONTROL SAMPLE, 2557796 Spike LCS LCS Parameter Units Conc. Result % Rec 1,4-Dichlorobenzene ug/1- 500 317 63 2,4,5-Trichlorophenol ug/L 500 393 79 2A6-Trichlorophenol ug/L 500 412 82 2A-Dinitrotoluene Ug/L 500 430 86 2-Methylphenol(o-Cresol) ug/L 500 302 60 3&4-Methylphenol(m&p Cresol) ug/L. 500 265 53 Hexachloro- 1,3--butadiene ug/L 500 260 52 Hexachlorobenzene ug/L 500 424 85 Hexachloroethane ug/L 500 232 46 Nitrobenzene ug/L 500 362 72 Pentachlorophenol ug/L 1000 737 74 Pyridine uq1L 500 179 36 2,4,6-1-ribromophenof (S) % 92 2-1Wluorobiphenyl (S) % 77 2-Fluorophenol (S) % 40 Nitrobenzene-d5 (S) % 76 Phenol-d6(S) % 24 Terphenyl-d14 (S) % 88 % Rec Limits Qualifiers 10-110 39-108 40-104 42-109 31-110 30-110 10-110 39-121 10-110 32-101 18-108 10-110 27-108 13-107 10-110 12-102 10-110 21-132 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical SenAces, LLC, Page 15 of 36 PO Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 24 of 45 aCuMInlanlyfical www�p,,ICelabs.com Project: 190415.17.01 Pace Project No.: 92425692 QC Batch: 469764 Analysis Method: ASTM D2974-87 QC Batch Method, ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92425692001 ----------- SAMPLE DUPLICATE: 2550987 92425391001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 20.5 2000 2 SAMPLE DUPLICATE: 2550989 Parameter Percent Moisture 92425692001 Dup Units Result Result RPD Qualifiers % 975 97A 0 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 36 1 PO Box 228 ® Statesville, NC 28687 e 704/872/4697 Page 25 of 45 ",,"Pace Analytical wwwpacelaces. coat Project: 190415.17.01 Pace Project No.: 92425692 QC Batch: 471992 Analysis Method: EPA 1010A QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Point, Closed Cup Associated L.ab Samples: 92425692001 SAMPLE DUPLICATE: 2561048 92426441001 Dup Parameter Units Result Result RPD Qualifiers Flashpoint deg F >200 >200 Pace Analytical Services, LLG 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result, REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date- 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC, Page. 17 of 36 P® Box 228 * Statesville, NC 28687* 704/872/4697 Page 26 of 45 A 200, -ac'eAnalytical wwwpacelbbs,rcom Project- 190415.17.01 Pace Project No.: 92425692 QC Batch: 471999 Analysis Method: EPA9045D QC Batch Method, EPA 9045D Analysis Description: 9045 pH Associated Lab Samples., 92425692001 SAMPLE DUPLICATE: 2561062 Parameter pH at 25 Degrees C SAMPLE DUPLICATE,,- 2561063 Parameter pH at 25 Degrees C 92425490001 Dup Units Result Result RPD Qualifiers Std. Units 5A 5.5 2 H3 92426076004 Dup Units Result Result RPD Qualifiers Std. Units 7.4 7A 0 H3 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 36 PO Box 228 ® Statesville, NC 28687 9 704/872/4697 Page 27 of 45 C Ie e a Analytical wwwpacelabs,com Project: 190415.17,01 Pace Project No.: 92425692 OC Batch: 470323 Analysis Method: EPA 9095B QC Batch Method; EPA 9095E Analysis Description: 9095 PAINT FILTER LIQUID TEST Associated Lab Samples: 92425692001 SAMPLE DUPLICATE.- 2553508 92425692001 Dup Parameter Units Result Result RPD Qualifiers Free Liquids Fail Fail Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 36 PO Box 228 o Statesville, NC 28687 o 704/872/4697 Page 28 of 45 11 11-,-.,-,AaceAna1ytica1 wwwpace tabs. corn A&I Project: 190415.17,01 Pace Project No,: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 HUntersville, NC 28078 (704)875-9092 QC Batch: 339303 Analysis Method: EPA 9014 QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide Associated Lab Samples- 92425692001 METHOD BLANK- 1651467 Matrix: Solid Associated Lab Samples: 92425692001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide, Reactive mg/kg ND 1.0 04/22/19 18:38 LABORATORY CONTROL SAMPLE: 1651468 Spike LCS L.CS % Rec Parameter Units Conc. Result % Rec Lit -nits Qualifiers Cyanide, Reactive mg/kg 99,4 ND 0 0-8 SAMPLE DUPLICATE: 1651469 30289318001 Dup Parameter Units Result Result RPD Qualifiers Cyanide, Reactive mg/kg ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LLC.. Page 20 of 36 PO Box 228 * Statesville, NC 28687 ® 704/872/4697 Page 29 of 45 0a j/ Analytical wwwpacelabscam Project- 190415.17.01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 339302 Analysis Method: SM 4500S2F-00 QC Batch Method: SW-846 73.4.2 Analysis Description: 734E Reactive Sulfide Associated Lab Samples: 9242,9692001 METHOD BLANK: 1651463 Matrix: Solid Associated Lab Samples: 92425692001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide, Reactive rn.g/kg ND 10 04/22/19 17:48 LABORATORY CONTROL. SAMPLE: 1651464 Spike LCS L.Cs % Rec Parameter- Units Conc. Result % Rec Urnits Qualifiers Sulfide, Reactive mg/kg 199 35,8 18 0-52 SAMPLE DUPLICATE: 1651465 30289318001 Dup Parameter Units Result Result RPD Qualifiers Sulfide, Reactive mq/kg ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05-00 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 36 P® Box 228 9 Statesville, NC 28687 e 704/872/4697 Page 30 of 45 acceAnalytical wvilwpacelabscom Project: 190415,17,01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor-, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit, TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit, MDL­ Adjusted Method Detection Limit. PQL - Practical Quantitation Limit, RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration, Consistent with EPA guidelines, unrouncled data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not. detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-NitrosodiphenylarTiine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute, LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte PASI-PA Pace Analytical Services - Greensburg ANALYTE QUALIFIERS 1g The temperature in the TCLP/ZHE extraction area was outside the method required range of 21-25 degrees C, H3 Sample was received or analysis requested beyond the recognized method holding time. S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05.00 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 36 PO Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 31 of 45 11 )!2a A Cc; nalytkal wwwpacelabs,com Project, 190415,1 7,01 Pace Project No.: 92425692 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92425692001 190415.17.01 EPA 351 OC 471215 EPA 8081 B 92425692001 190415.17.01 EPA 3546 470280 EPA 8082A 92425692001 190415.17.01 EPA 351 OC 471354 EPA 8082A 92425692001 190415.1T01 EPA 301 OA 472926 EPA 601 OD 92425692001 190415.17.01 EPA 7470A 472928 EPA 7470A 92425692001 190415.17,01 EPA 351 OC 471352 EPA 8270E 92425692001 190415.17.01 EPA 8260D 471650 92425692001 190415.17.01 ASTM D2974-87 469764 92425692001 190415.17.01 EPA 1010A 471992 92425692001 190415.17.01 EPA 9045D 471999 92425692001 190415AT01 EPA 9095B 470323 92425692001 190415.17.01 SW-846 T3.3.2 339303 EPA 9014 92425692001 190415.17.01 SW-846 7.3.4.2 339302 SM 4500S2F-00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/28/2019 05:00 PM without the written consent of Pace Analytical Services, LIC, Analytical Batch 471416 470695 471417 473223 472965 471456 339409 339407 Page 23 of 36 P® Box 228 e Statesville, NC 28687 e 704/872/4697 Page 32 of 45 Document Name: Sample Condition Upon Receipt(SCURI Docurnent Revised: February 7, 2018 Pa I of 2 Document No.: F-CAR-CS-033-Rev.06 - Issuing Authority* Pace Carolinas Quality Office Laboratory receiving samples: Asheville Eden [J Greenwood HuntersvilleEl RaleitzhF1 LAI -.0 W0# zwzlz : 4ft24Z Clien Name: Project Courier: OUPS OFed Ex ( 1i5P5 M []Client Commercial [3Pace Dither:- 9242SS92 Custody Seal Present? Des 0No Seals Intact? [3Yes ONo Date/Initials Person Examining Contents. Packing Material.- ElBubble Wrap 08ubble Bags []None Other Biological Tissue Frozen? Therrhometer: 'OIRGun lot 92TO48 Type of Ice. []Wet Divue E]Yes []No n.N/A []None Cooler Ternp (*Q: Correction Factor, Add/Subtract ("Q 0.0 Cooler Temp Corrected (.*C): Temp should be above freezing to 6"C [DSamples out of temp criteria. Samples on ice, cooling process USDA Regulated Soil (O'N/A, water sample) has begun Did samples originate in a quarantine zone within the United States- CA, NY, or SC (check maps)? f"_1VaC Did samples originate from a foreign source (internationaliv, Comm ents/Discrepa n cy., Chain of Custody Present? r7l 1"T No EIN/A 1. -Samples Arrived within Hold Time? ayes ONo []NIA 2. -Short Hold Time Analysis (<72 hr.)? Flyes QNo._ _ON/A 3. -Rush Turn Around Time Requested?. YesQNo ON/A 4. Sufficient Volume? (]No QN/A S,__,__ Correct Containers Used? OYes' ONo []t4/A 6, -Pace Containers Used? OYes ONO Containers Intact? _QNIA Yes No ON/A 7, Dissolved analysis:. Samples Field Filtered? 0yes Na E] NIA C] R. Sample Labels Match COC? ZYes ONO []N/A 9i -includes Date/Time/Its/Analysis Matrix: 10'. Headspace in VOA Vials (>5-6mm)? Elye5 No t4/A Trip Blank Present? [,Yes ONO [3iqlA 11. Trip Blank Custody Seals Present? r-11 At mrto dN/A COMMENTS/SAMPLE DISCREPANCY . . . . .......... CLIENT NOTIFICATION/RESOLUTION Lot ID of split containers: Person contacted: Date/Time: Project Manager SCURF Review-, Date: Project Manager SRF Review: Date: Field Data Required? FlYes [:]No Page 24 of 36 PO 8®x 228 e Statesville, NC 28687 9 704/872/4697 Page 33 of 45 / Document Name: Document Revised., February 7, 2018 Pr A?Ce, AMIOMI Sample Condition Upon Receip_t(SCUR) Page I of 2 Document No.: Issuing Authority: -- F-CAR-05-033-Rev,06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or clechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle 7'rojec"Wo# so 92,425692 pM; TIH Due Date: 04/30/19 C�JCMT: 92—States"' Cn -A. z 0 < z z z z z CL z z z V ad A z ::) rq V irl > -0 < 1-1 > 10 M 4-1 CIL V z z z z z �A 0 Ck QL QL C C 0 M U Q. Ck ex 0 8 N W .0 ;�'� 0 '4 z v Ln rM 0 CL U > "I CL D C rq X z Z 0 U1 eq kA a 0 0. T > z D 0 C z: 4- W -J E M y. L. -J -Jix E E < E E < E < 0 > 0 > < 0 5 Q > CL E E 0 rV E E 0 0 Ln 0 4-- E LA E 0 Ln E Ln E Ln -0 QJ - 4� fi- (U E W E 0 �te 0 M < M E E E -J E .2 > > E E E 8 -J E E V 04 rN LA 04 rid — r-J z W X to 1-1 tn PA m tv 0. CL ri 4. a am 101r. 12 rl Q us 0. en V4 M U Qii m M M In 0. 4 ch co co (a ca to M M 0 > 4'A '%'n EL co \J\N I 3 4 6 7 -------- 10 11 N - I 2 A Sample ID Type of Preservative PH upon receipt Date preservation adjusted Time presentation adjusted Amount of Preservative added t - 0 in Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wlll 6e sent to the North Carolina DFHNR Certification Office (i,e. Out of hold, incorrect preservative, out of ternp, incorrect containers, Page 25 of 36 PO Box 228 e Statesville, NC 28687 ® 704/872/4697 Page 34 of 45 ua 0 < C7- Q. Z Cy z (t� 2 �Nqy� tom} i4 � YS ,4ri qry ii co' Gti v Cik.s i. fy w ul ' Z s.. ,. e, (p (} (NIA) C? ut dlt101 44 IL I ,rI ff tv >Fts !±�� rtt ��i{('`" ��qg te F' asal w ISAjewv uj ..........,.............._,..._.....,.....,...._.........,.... H V V ,`.. paA.ta3wdun .•11> H3NIVlNOO wad} # LU - z W Z V) V} �:� Z Ca U1 LU V t.d.i t✓ }_ cC ` z ci: W a i_ tWY .za}{ G'i i2 uj 4�1 3000 X[8i W �.�� i€ Fri h m Rt X- 1 r ry i d _ i1;s ?a .. ». u Q i6 {�M {{' CL Wage 26 of 36 ��gy�� j hP W PO Box 228 ® Statesville, NC 28687,9 704/872/4697 Page 35 of 45 , A NALYTICAL REPORT 'PakeAnal ytical April 25, 2019 Pace Analytical - Huntersville, NC Sample Delivery Group: L1090481 Samples Received: 04/18/2019 Project Number: 92425692 Description: 190415.17,C)l Site'. 001 Report To: -ryriek Hooks 9800 Kincey Avenue, Suite 100 1-11-Intersville, NC 28078 4 Ditire Report Reviewed By.- N a n cy M c La i n c Project Manager Results re ate onY, to the iterls iesteCf Or cal!bf aled and a, e-P1 % ' -c-u, ded vaes. "'is test !?Post shalloo. Di' repfoduc-od, OXC(Mt i;l fL,11, V'Afh here, app�icabllo' sarmolnng Conduc.ted Dy pa(�o out wriflen app�tcmfl of trK, IfIll")"DI'W'01Y VVI I is perfixm(-"(! pc.?r guidancr,-.. provided 1 i laboratoty 0'andard oc)(nating prl'xrAures 060302, 060303, and 06101304. ACCOUNT: PROJECTSDG- DATE/TIME. PAGE. I Paf-e Analytical - Huntetsvdk,, INC 92425692 L1090481 04/25'1011 121-31 1 of 10 PO Box 228 e Statesville, NC 28687 ® 704/872/4697 Page 36 of 45 TABLE OF CONTENTS te S 2 w Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 190415.17.01 L1090481-01 5 ]n QC: QW-flity (-.ont[rol Surnrnaty 6 ChIr,'winat(,:-�d, Acid F-Ierbi--id�',-;s IGC) by IN ethod 811- IA 6 GI: Glossary of Terms 7 F Sc.,- Sample Chain Of CLIstody 9 LEI F7S 7, 1 ACCOUNT - Pace Aj ialyfl,,'-)! - H � svoke, NC Page 28 of 36 PROJECT- SM DATEMME: PAGE. 92425692 1-109048", 04/2519 35 2 10 PO Box 228 ® Statesville, NC 28687 9 704/872/4697 Page 37 of 45 SAMPLE SUMMARY C't Hrwjnci 190415,17.01 1-10904-81-01 Waste 0 1 i 9 E0 08 mc,th"od Batch Diluflon Preparation Analysis Analyst Locat.or datc,/tinic, date/timp Pieparation by Method 1311 WG1270126 1 04/22/19 20:03 04/22/19 20;03 CGD Mt, Juliet, TN Chlorinated Acid Herbidd(n (GC) by Mcthod 8151A WG1270887 1 04/24/19 OT35 04,1124/19 22,.28 KLM Mt. Jullot, TN ACCOUNT, Pi;ice Analfyflcai - Hurittfsvdk-,,, NC Page 29 of 36 PROJECT: SDG- DATE/TIME., PAGE' 3 of 10 92425692 L109,048' 0 4 19, 3'-1 i PO Box 228 e Statesville, NC 28687 * 704/872/4697 Page 38 of 45 '01 CASE NAtP2-,,a,T1VE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis, All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance forryi or properly qualified within the sample results. By my digital signatUre below, I affirm to the best of nay knowledge, all problerns/ariornalies observed by the laboratory as having the potential to affect the quality of the data have Been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data, [7— El Nancy McLain Project M,--i n a g'e r Page 30 of 36 ACCOUNT: PROJECT: SDG,, DATE/TIME. PAGE' Pace Anoily Uccil - NC 92425692 L10901181 04/251") 1112:34 of 10 PO Box 228 * Statesville, NC 28687 ® 704/872/4697 Page 39 of 45 190415.17.01 SAMPLE RESULTS - 01 Coflectpd date/time: 04/15/19 10,00 L1090481 j1....' P I 4e!_1 c)! I I-) Y M I o c! --� Result Qualifier Prep Batch Analyte date / hme TCLP Extraction 4/22/2019 3,03-07 PM WG1270126 Fluid 1 4/22/2019 8,03:07 PM WG1270126 Initial pH 6.37 4/22/2019 8:031-07 PM WG1270126 Final pH 4,86 4/22/2019 &03:07 PM WG1270126 Chdon!"'fated Add by iod 815"A Analyte Result Qualifier mg/l RDL Limit rng/l ing/l Dilution Analysis Mate; tirne Batch 2,4,5-TP (Sil-vex) ND 0.00200 1 1 04/24/2019 22,28 WG 1, 27083-7 2,4-D ND 0,00200 10 1 04124/2019 22:28 WG12 7088-7 Acid 72, 14.0-1,58 041'2412019 22,28 W G 12 7 083'3 7 c 21-1 1 c ACCOUNT; P ac c,, Analyflic-al - Hlumeisvffle. NC Page 31 of 36 PROJECT: SDG-, DATE/TIME: PAGE: 92/1-25-692 L1090.481 04/251119 12:'35 0 of 10 PO Box 228 ® Statesville, NC 28687 e 704/872/4697 Page 40 of 45 4 'A i WG1270887 QUALITY CONTROL SUMMARY iN L Chlorinated Acid Herhicides (GCj by Method 8151A L,0904 31.01 --------- --- . . ....... . . . .. . .............. . ......... . . ...... (MD) R-3140171,082-1 04/24/19 14A33 MD Result W Oualifier MB MDL MD RDL Analyte fria/1 2,4-D U 0.00()66)7 000200 2,4,5-TP (Silvexl U 0,000616 7 0 00200 (S) 2, 4-Dioiluj (wheii34A ell,", 66 6 Aleid 14 6 158 (LCS)R3405082,2 04/241191457 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/1 11-1,cd 2,4--D 0,0500 0.0417 81-1 500-120 2,4,:'-Tp 0, 0 5 01 0 0 0406 81 50, 0 125 ophe;;J4 Ac eric 85") illy, 6 158 Aoc! (OS) L109036,101 04/24,19 15,26 - (NrIS) R04050182-3 04/24119 15' 9 - (MSD) R34015-082 4 04/24/19 15,53 SpikeAmount Original Result MS Result MSD Result MS Rec, MSD RecDilution Rec, Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/! l"'ic"I rng I i-110 q 06 2,4-D 0,V)00 N D 0,05010 O.0448 100 89,6 1 5 01, 0 Al 2 0 11.0 20 2,4,5-,TP (&Ivex) 00500 ND 0,03-'95 0,0350 79,0 700 1 50 0-125 121 20 61' 2,4 Ac;d 80,6 72 2 ACCOUNT: Pic -& An a I � ! f c ,-Al 11 ue-sv i I I (�. NC En Page 32 of 36 PnOJECT. SDG: DATE/TIME PAGE. 9 2,12 156 9 2 1-1090491 ('W25/19 K")�35 eoflc PO Box 228 is Statesville, NC 28687 e 704/872/4697 Page 41 of 45 GLOSSARY OF TERMS -Z' r Gui(jje to Reachrily �_.irid Undel-Std1_11dilIg YOLA L�ibor-�',iLory Repc')( T"he information below is designed to better* xi.,.lain the various 1EIMIS used in you.r report s eof analytical resull�s from the Laboratory. phis is not intended as a cornf--yrehensive explanation, and if YOU have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Revorted Detection Limit. Rec. Recovery. PPD Reiative Percent Difference. En SDG S,.-in-iple Delivery (..,roup. (S) SUH-0gate (Surrogate Standard) - Aiwflytes added to every blank, sample, Laboratory Control Sarnple/Duplicate and Matrix Spike/Duplicate, used to evalUale analytical efficiency by rneasuring recovery. Surrogates are not expecLed 11-0 be defected in all e-nvironincantal media, U Not detected at the Reporting Limit (or MDL where applicable). Analyte, The n�_-jmc. of the particular compound or analysis per, - ormed, Some Analyses and Methods will have multiple analytes reported. if the sample matrix contains an interfering material, the sample preparation volunne or we. ighit varies differ from the standard, or if concentrations of analytes in the sample are higher than the highest limit of concentrati on that the DilUti0f) Laboratory can aMlral report, reort, the sarnple n-jay be diluted for analysis. If'a value different than 1 is used in this field, the ' result reported has already been corrected' for this fac"tot. rm Thc.-se are the target O'C') recoveiy ranges or '7,, diff.& ence value that the. laboratory has historically determined as normial Limits for the rnethod and analvte being reported, Successful CC Sample analysis will target all analytes recoverecl of- clul.-)IIcatexd within t1hese ranges. _ Original Sample The non -spiked sample in the Dreg !'.-J-aich used to determine the Relative Percent Difference (RIDDI from a qU6111ty central fir, s'arnplo The Onciinal Snmplo may not be included v.,ithin the reported SDG. This column provides a letter and/01 number designation that corresponds to additional information concerning the result QUalifier reported. If a Qualifier is present, a definition p,er Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications Of the Qualifier in the Case Narrative- if applicable, I The actual analytical final result (corrected for any sample specific characte rlstics) reported for Your sarnpic, If there was no measurable result returned for a specific ana!yte, the reSUIt in this COIUrnn may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column shot.fld always be accompanied by either an MDL (tvlothod Detection Limit) or RDL (Reporting Detection Urnit) that defines the lowest value that the laboratory could detect or report for tillis analyte. Uncertait-ity (Radiochemistry) Confidence, level rat sigma. A brief discUssion about. the included sample results, including a dt5cussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during th-e- analytical process. If present, there be a section in the Case Narrative to diSCUS'S the meaning of any data qualifiers U'Sed in the report. Quiality Control 1-his sectioln of the report includes the results of the laboratory quality control analyses required by procedure or C SUrnnIal'y (0) analytical methods to assist in evaluating the validity of the results reported for your sarnj.-)Ies. These ;analyses are not being performed on your samples typically, but on laboratory generat:=:d material. This is the docurnent created ini the field when your SFAITIPIeS Were initially collected, This is used to verifythe time and Sample Chain of date of coilection, the person collecting the samples, and the anal�,se5 that, the laboratory iS requested to perform. Ti'lls ci-Istody (Sc) chain of custody also documents all persons (excluding con-irnercial shippers) that helve I lad control or possession of the sm-riples fium the time of collection until deliveiy to the I'--fl_)o1aL0[y for reanalysis, This section of your rcpoit will provide the. results of . all testing performed on your sariplus. These results are provided P Sarnple Results (Sr) by sample ID iand are- separated by the analyses perforry)6d on each sample. The head et line of each anaiysis section for each sample will provide the name and method number f)t the analysis reported, c Sample Surnmary (Ss) This section of the. Analytical Report deffines tine specific- analyses performed for each sample ID, including the dates and times of preparation and./or analysis. G 1- lc- I I 'I I C-t I' D(::�scro+iol The rernainder of this page intentionally left blank, there are no qUalifiers applied to this SDG. ACCOUNT- Ana�ytic',0 - NC Page 33 of 36 PROJECT: SDG: DATE/TIME., PAGE: 92425692 L1090481 04,12"519 12 31� 7ol 10 P® Box 228 e Statesville, NC 28687 ® 704/872/4697 Page 42 of 45 I I ACCREDITATIONS & LOCATIONS LAU, Pace National is the only environmental lahioratoiy accredited/certified to support your work nationwide from onr� location. One phone ull), one point of contact, one laboratory- No other lib is as accessible or pr epared to handle your needs throughout the Country. Our Capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. model is conducive to accelerated productivity, decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity, Our focus on prerniurn quality and prompt >ervis e allows us to be YOUR LAO OF CHOICE. Not, all certifications held by the laboratory are applicabip to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National, ... Alabama ..... ... 40660 Nebraska NE-OS-15-05 Alaska 17-026 Nevada TN-,03-2002-34 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey-NELAR TNO02 California 2932 New Mexico' rit Colorado TNO0003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 41 Georgia 923 North Dakota R-140 Idaho TNO0003 Ohio--VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 63-02979 Kansas E-10277 Rhode Island LA000356 Kentucky" 90010 South Carolina 84004 Kentucky 16 South Dakota nia Louisiana A130792 Tennessee 2006 Louisiana LA180010 Texas T104704245-18-15 Maine TNO002 Texas' LAB0ISS2 Maryland 324 Utah TNO0003 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 460132 Minnesota 047-999-395 Washington C847 Mississippi TNO0003 West Virginia 233 Missouri 340 Wisconsin 9980939910 Montana CERT0086 Wyorning A2LA A2LA - ISO 17025 146101 AIHA-LAP,LLC EMLAP 100789 A2LA - ISO 17025'3 1461,02 DOD 1461,01 Canada 1461,01 USDA P330-15.,00234 EPA-Cr ypto 1'NO0003 'DiinkingWater 2, Underground Storage'Tanks 1Aquatic Toxicity 'CIIO.M.icalf'Microbiologi,,-,31 51VIold "Wastewater n/a Accreditation not ap Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If YOU Would like assistance from one of our support offices, please contact out, main office, Pace National performs all testing at our central laboratory. 4P ­'4 'Al N 4f ACCOUNT: Poce, Aridk/tic�al - 1'­1tfate!,vflk,.', NC PROJECT: SDG,. DATE/TIME: 92425692 1-1,119048i 04,12',>(19 12:35i Page 34 of 36 PAGE: 8 0i I() PO Box 228 ® Statesville, NC 28687 e 704/872/4697 Page 43 of 45 Chain of Custody Workorder, 924f2'5692 Workorder Nimrzn, 1 -7 n -i ;acIeAna1yVcaI' 2 t 09 Pago 35 of 36 PO Box 228 ® Statesville, NC 28687 ® 704/872/4697 Page 44 of 45 Page 36 of 36 PO Box 228 • Statesville, NC 28687 ® 704/872/4697 Page 45 of 45 APPENDIX III LAND APPLICATION SITE CERTIFICATION (FORM: LASC 06-16) LAND APPLICATION SITE CERTIFICATION (FORM: LASC 06-16) State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources LAND APPLICATION SITE CERTIFICATION INSTRUCTIONS FOR FORM: LASC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 06-16 or FORM: SDR 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documcntation listed below. A. Land Application Site Certification (FORM: LASC 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit the requested information for all land application sites. ❑ For modified permits, submit the requested information for only those sites that are new, transferred or affected by the proposed modification. B. Land Application Site Information: ® The status of the land application site with respect to this residuals land application program must be provided in table I. The status categories and their corresponding codes are as follows: ♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T) ♦ Deleted (D) ® Attach the following in accordance with each status code: Status Code Required Item N R T M ✓ County Board Notification.doc +' I . Land Owner Agreement (If applicable) I A I' V V/ V/ V/ Setback Waiver Agreement An updated vicinity/setback map in accordance with the "Map Guidance for Residuals Land Application Permits" ✓ ✓ ✓ A soils and agronomic evaluation in accordance with the "Soil Scientist Evaluation Policy" ✓ INSTRUCTIONS FOR FORM: LASC 06-16 Page 1 of 3 An updated accounting of the land application site's cumulative pollutant loading rates (CPLRs) Required Item Status Code N7 R T M For previously permitted sites without a soil series name indicated in the Attachment B, submit County Soil Survey Map (or equivalent) clearly ✓ indicate the location of the land application site and in accordance with the soil map requirements in the "Soil Scientist Evaluation Policy" Acknowledgement of field transfer from Land Owner (Fields may not be permitted to multiple Permittees over the same time period) * This item may be required for land application site with a status code "M", please contact the Division if you need assistant in determining attachment requirements. ❑ Crop Type should include the most likely crop types for the life of the permit (five years). ❑ Predominant Soils Series Name must be either the name of the soil indicated in Attachment `B" of the existing permit, or name of the soil series as provided by the licensed soil scientist. ❑ Predominant Soil Mapping Unit or Representative Slope: Either the Soil Mapping Unit or the representative slope of each site must be provided. The predominant soil -mapping unit must be consistent with the predominant soil series name. Please note that the soil mapping units are variable between Counties, so care should be taken in properly identifying the correct mapping unit. If a representative slope is provided, it must be determined accordingly: ❑ For sites previously permitted for use, but do not have an established soil mapping unit (the mapping unit provides information on both the soil series name and the slope of the soil), the Applicant may determine the representative slope by using the average slope provided in the County Soil Survey (or equivalent). A soil type with a slope range of 4 - 8% would have a representative slope of 6%. ❑ New Sites to be permitted must have slopes determined as part of the soils report prepared by a licensed soil scientist. ❑ Acceptable methods for determining location coordinates (i.e., latitude and longitude) and their corresponding codes are as follows: • Address Matching (ADD) • Aerial Photography with Ground Control (AER) • Cadastral Survey (SUR) • Conversion from Coordinate Plane (CP) • Conversion from Township -Section -Range (TSR) • Conversion from Universal Trans Merc (UTM) • Map Interpretation by Digital or Manual Extraction (MAP) • Digital or Raw Photo Extraction (EXT) • Geodetic Quality GPS Survey (GEO) • LORAN-C Navigation Device (LOR) • Navigation Quality GPS (GPS) • Remote Sensing (RS) • Zip Code Centroid (ZIP) C. Waterbody and Classifications Information: (new sites only) ❑ Use an 8.5 by 11-inch copy of the portion of a 7.5-minute USGS Topographic Map to identify the location where the residuals program activities are planned to occur as well as the closest downslope surface waters as clearly as possible. Each map portion must be labeled with the map name and number, the identified location, and be of clear and reproducible quality. ❑ Surface water body classifications information may be found at: hLtp:Hdeq.nc.gov/about/divisions/water- resources/planning/classification-standards/classifications ❑ Any questions concerning the waterbody and its classification, please contact the Division's regional offices. ❑ A list of the Division's regional offices, their county coverage, and their contact information may be downloaded at: http://deq.nc.gov/contact/regional-offices ❑ General Instructions: There are 17 river basins in North Carolina. Each basin has associated waterbodies with assigned subbasins, location descriptions, stream index numbers and established classifications. 1. Identify the project area on a 7.5 minute USGS topographical map (an 8.5 x 11-inch sheet showing the project area should be submitted with the permit application regardless of whether a Stream classification was completed). 2. Determine the names of all the closest down slope surface waters from the project site. For unnamed tributaries, see Table 1: Unnamed Tributaries Entering Other States or for Specific Basin Areas. Label any unnamed tributaries as "UT to stream name" as the waterbody name. 3. Open the link http:Hdeg.nc.gov/about/divisions/water-resources/planning/classification-standards/classifications. ❑ Stream Classification Process: One of the options below may be used depending on the known initial project information. ❑ KNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select proper basin from the List all Waterbodies in Basin sorted report. Sort hydrologically as this will provide the proper location descriptions if multiple runs. INSTRUCTIONS FOR FORM: LASC 06-16 Page 2 of 3 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ KNOWN COUNTY WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Select the proper county from the List all Waterbodies in county, hydrologically report. 2. Locate the name of the identified waterbody (from General Directions) on the list. 3. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 4. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ UNKNOWN BASIN WHERE CLOSEST DOWN SLOPE SURFACE WATER IS LOCATED 1. Use the Clickable basin map to hydrologically sorted list report. 2. Click on the approximate project location to bring up the hydrologically sorted list. 3. Locate the name of the identified waterbody (from General Directions) on the list. 4. For multiple listings of the same waterbody name in the report, select and verify the location description. The term "source" in the description means the beginning of the waterbody segment (most upstream point). 5. Record all Basins, Stream Index Numbers and Classifications applicable to the project. ❑ Notes on index number and unnamed streams: Unnamed Streams 15ANCAC 02B .0301(i). ❑ Any stream which is not named in the schedule of stream classifications carries the same classification as that assigned to the stream segment to which it is tributary (at the point of entry) except: (A) unnamed streams specifically described in the schedule of classifications; (B) unnamed freshwaters tributary to tidal saltwaters will be classified "C"; or (C) after November 1, 1986, any newly created areas of tidal saltwater which are connected to Class SA waters by approved dredging projects will be classified "SC" unless case -by -case reclassification proceedings are conducted. ❑ The following river basins have different policies for unnamed streams entering other states or for specific areas of the basin: Unnamed Tributaries Entering Other States or for Specific Basin Areas Hiwassee River Basin Streams entering Georgia or Tennessee shall be classified "C Tr." Little Tennesse River Basin And Savannah River Drainage Area Streams entering Georgia or Tennessee shall be classified "C Tr." Such streams in the Savannah River drainage area entering South Carolina shall be classified "B Tr." French Broad River Basin Streams entering Tennessee will be classified "B." Watauga River Basin Streams entering the State of Tennessee are classified "C." Broad River Basin Streams entering South Carolina are classified "C." New River Basin Streams entering the State of Tennessee are classified "C." Catawba River Basin Streams entering South Carolina are classified "C." Yadkin -Pee Dee River Basin Streams entering Virginia are classified "C," and such streams entering South Carolina are classified "C." Lumber River Basin Streams entering South Carolina are classified "C Sw." Roanoke River Basin Streams entering Virginia are classified "C." Except that all backwaters of John H. Kerr Reservoir and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "B," and all backwaters of Lake Gaston and the North Carolina portion of streams tributary thereto not otherwise named or described shall carry the classification "C and B." Chowan River Basin Streams entering Virginia are classified "C." Tar -Pamlico River Basin All drainage canals not noted in the schedule are classified "C Sw." except the main drainage canals to Pamlico Sound and its bays which shall be classified "Sc." Pasquotank River Basin All drainage canals not noted in the schedule are classified "C." INSTRUCTIONS FOR FORM: LASC 06-16 Page 3 of 3 LAND APPLICATION SITE CERTIFICATION Applicant's name: Town of Cleveland Land application sites currently certified: 44.3 net acres and Total to be certified: 10.0 net acres. I. LAND APPLICATION SITE INFORMATION (See Instruction B): Status Codes Site/Field ID Landowners O Lessees or Operator(s) O Net Acres County ty s Crop(s) pO Predominant Soil Series Nameb Mapping Unit or Rep. Slope R NC-RA-01-01 Guy Byrd 10.0 Rowan Fescue Enon EnB D NC-RA-56-o1A Hodge, Ira Franklin 10.3 Rowan Fescue Lloyd LdB2 D NC-RA-56-01B Hodge, Ira Franklin 11.8 Rowan Fescue Enon EnB N N N EL I N N a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted) n Soil Series Name (i.e. Appling, Cecil, etc.) Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2) II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C): Site/Field ID Latitude Longitude Location Datum Location Method Code Location Accuracy Waterbody Subbasin and Stream Index No. Current and Proposed p Class 01/01 350 44' 17.8" 800 39' 59.3" NAD 83 MAP Nearest tenth of second UT to Third Creek (12-108-20-4) C C .°.. .°.. NAD 83 ADD Nearest Second _ NAD 83 ADD Nearest Second _ a° M F " a M M' NAD 83 ADD Nearest Second M [" .°.." NAD 83 ADD Nearest Second W W " it M' NAD 83 ADD Nearest Second _ _ ° ' M' NAD 83 ADD Nearest Second _ _0 = F = F' �°.. NAD 83 ADD Nearest Second _ Note: Please keep the site information (I.) and waterbody information (I1.) of the same field on the same page. FORM: LASC 06-16 Page 1 APPENDIX IV Renewal Site TOWN OF CLEVELAND (SITE 1, FIELD 1) LANDOWNER AGREEMENT (FORM: LOA 06-16) SITE MAPS (Vicinity Map) (Buffer/Setback Map) UPDATED CUMULATIVE POLLUTANT LOADING RATES TOWN OF CLEVELAND (SITE 1, FIELD 1) LANDOWNER AGREEMENT (FORM: LOA 06-16) D-1 WR Division of Water Resources State of North Carolina Department of Environment and Natural Resources Division of Water Resources LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting_ Unit General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): Submit the completed and appropriately executed Residuals Source Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Town of Cleveland hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-RA-01-01 No Fescue (Hay) Animal Feed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1636 Mail Service Center, Raleigh, NC 27699-1636. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil PH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil PH of at least 6.0, unless an agronomist provides information indicating that the PH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. 11. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods a.4 ,.'(-.r such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14- month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. HL ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105Uh allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; F-1 A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. of the compliance boundary and attach a map showing the newly proposed IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) El The land application field(s) ID: , is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced Iand application sitc(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the Iand application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: pp "T 1 O W �Y jl� R�`t L. I E\i ('A ajl a Address: 4h bo x- ,)� 9 city: (I Le-- [ a== n 6- State: N Phone: Signatu NORTH CAROLINA, f� 1) W ai1 COUNTY zip: _ 2 7- I I, the undersigned Notary Public do hereby certify that r Dn r} tl C�Ckb rid personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the C-2 6 _�± day of , 20 Signature and seal: ��� �� _tv MOM. SEAL My commission expires: CAP _t C C) LATHY GRAHAM PAYNE swan un My Comm. UP Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official Signature: Date: t? 27 r / FORM: LOA 06-16 Page 3 of 3 TOWN OF CLEVELAND (SITE 1, FIELD 1) UPDATED SITE MAPS (Vicinity Map) (Buffer/Setback Map) SITE/FIELD TOTAL ACRES BUFFERED ACRES NET ACRES 1-1 10.9 0.9 10 REFERENCE: GIS DATA LAYERS WERE OBTAINED FROM ESRI, INC. PLEASE NOTE THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN, LEGAL, OR ANY OTHER USES. THERE ARE NO GUARANTEES ABOUT ITS ACCURACY. WMSS, PLLC ASSUMES NO RESPONSIBILITY FOR ANY DECISION MADE OR ANY ACTIONS TAKEN BY THE USER BASED UPON THIS INFORMATION. SCALE: 1 " = 500 DATE: p6-24-19[~�_}(�{jy_]} DRAWN BY: MEM * *'I1`-"Ji ry`'^* ' "� SOLU7IDNS Ph: REVIEW BOUNDARY shall be established around each land application site midway between the Compliance Boundary and the perimeter of the residuals land application area. COMPLIANCE BOUNDARY: The Compliance Boundary for each land application site is established at either 250 feet from the residuals land application area or 50 feet within the property boundary, whichever is closest to the residual land application area. L� FieldL1-1 � fW llt cc=;J ski, Dl�gitalGlobe, GeoEye, Ea , USGS, A R4ID, IGN, and BUFFER MAP TOWN OF CLEVELAND, NC NC-RA-1-1 LAND APPLICATION PROGRAM I Access Road ♦ Structure ■ Dwelling Stream Pond ® Buffer Field Boundary Property Boundary FIGURE NO. TOWN OF CLEVELAND (SITE 1, FIELD 1) UPDATED CUMULATIVE POLLUTANT LOADING RATES ®I o I I v � O r } MM � V W W ® O C •p U U Cn LL ao 0 0 0 0 0 H o con A N A�z � W o � A W I...I O ,—, 00 00 W � O M •� Q' -Ono 0 pug s� _ a� • PRO V " a O W � w CTS W � cH O � GO Cu N a3 N O U U � � � 0 O U N O O O O O O O O O O U CO CO CO CO O O O O O CO Ammonia 2 Oo O d. O cc Nitrogen E 00 N N Mineralizatio M M n Rate*** o co Volatilization Rate* * ® o Application Method* .Q" N a) � U � O O ,C � v O 0 O M � 00 00 M M kr) � 0�0 P-+ O pp A, O o a 00 ® o 0 I� C 00 v o co co O o�ooa� h N rn O O O IN 0 � Lj o 0 00 0 `� o co 0 It 00 d- °° 00 e� U O kn "o •� M O N � � O O O N kn N 0 0 0 0 U O 0 0 0 0 0 0 co o ® co co co co co co ° N N p O O CT CU O � � > � U gTUOW JO Olva vs O 00 M r—, ►4 C O U IC a� a� C13WHOM a O N U) LL O LL w w ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Cleveland Total Dry Tons Applied (Annual): WQ0011431 Cation Exchange Capacity (non 503 only): Bio-Green Services, Inc. Owner: G Byrd Predominant Soil Series: SO Acres Permitted: 1.0 Site #: NC-RA-01 Field #: 117.81 Enon 1 Residual Analvsis Data (Heavv Metals and Total PhosDhorus use miALY. % Solids use Raw Percent #): Sample or Com- posite Date 1 5/23/18 2 3 4 5 6 7 PT 9 10 11 12 Solids 2.04 Arsenic 5.88 Cadmium 0.98 Copper 630 Chromium 0.05 Lead 1.274 Mercury 0.706 Molyb- denum 7.35 Nickel 25.2 Selenium 2.45 Zinc 1323.5 Total Phos- horus 22902 Annual Heaw Metal Field Loadings (Calculated in lbs/acre): Total TF 31 6 7 8 qj 101 111 12 DT/Ac./ _jj o App. Event 11.78 Arsenic 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 Cadmium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:023 Copper 14.844 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 14.844 Chromium 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.001 Lead 0.030 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.030 Mercury 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Molyb- 0.173 0.000 0.000 0.000 0.000 0.000 0.000 0. 000 0.000 0.000 0.000 0.000 0.173 denum Nickel 0.594 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.594 Selenium 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.058 Zinc 31.185 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 31.185 Total Phos- 539.617 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Chorus 1. cerilIy, unuer penalty of iaw, tnat tnis aocument was prepares unaer my airection or supervision in accoruance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DEAR FORM MFLSF (12/2006)