WQ0003504_2014 Residual Annual Report_20150302

CITY OF DURHAM, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0003504
2014 ANNUAL REPORT

City of Durham, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00003504 County Durham Year 2014
Facility Name (as shown on permit) North Durham WRF, South Durham WRF, Brown WTP, & Williams WTP
NPDES No. NC0023841, NC0047597, 03-32-010(A). 03-32-010(B)
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summa
Total number of application fields in the permit: 158
Total number of fields utilized for land application during the year: 42
Total amount of dry tons applied during the year for all application sites: 4849.50
Total number of acres utilized f6r-land application during the year: 1223.3
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Don Greeley. Director of Water Management
Permittee Name and Title (type or print)
Signature of Preparer* Date
(if different from Permittee)
i itt ��� t -I 2015
Si ature of Land A plier Date
(if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
DURHAM,NC
DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2014
1,728.00
Y
220.93
D
200.38
April 2014
8,224.00
Y
1051.43
D
953.66
May 2014
1,696.00
Y
217.69
D
197.44
September 2014
1,257.00
Y
159.32
D
144.50
October 2014
5,552.00
Y
703.74
D
638.29
December 2014
550.00
Y
77.08
D
69.92
YEARLY TOTAL
19,007.00
Y
2,430.19
D
2,204.19
DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
MONTH/YEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
May 2014
4,832.00
Y
693.89
D
629.36
June 2014
2,752.00
Y
395.18
D
358.44
July 2014
3,905.00
Y
552.53
D
501.17
August 2014
525.00
Y
74.29
D
67.38
September 2014
1,484.00
Y
204.23
D
185.26
YEARLY TOTAL
13,498.00
Y
1,920.12
D
1,741.61
DURHAM, NC BROWN WTP CAKE
DRY METRIC
MONTH/YEAR
AMOUNT
UNIT
DRY TONS
UNIT
TONS
March 2014
129.35
W
25.21
D
22.87
April 2014
450.87
W
93.87
D
85.15
May 2014
128.44
W
26.74
D
24.25
June 2014
203.09
W
42.29
D
38.35
July 2014
68.03
W
14.67
D
13.31
July 2014
525.00
Y
95.36
D
86.51
August 2014
243.64
W
52.56
D
47.67
September 2014
274.73
W
59.27
D
53.73
October 2014
417.84
W
84.32
D
76.50
December 2014
24.26
W
4.90
D
4.44
YEARLY TOTAL
1,940.25
W
403.83
D
366.27
YEARLY TOTAL
525.00
Y
95.36
D
86.51
1 /30/2015

DURHAM,NC
DURHAM, NC N. DURHAM VIMTP CONTAM MATE® SOILS
MONTHNEAR
February 2014
March 2014
YEARLY TOTAL
AMOUNT UNIT
642.88 W
710.48 W
1,353.36 W
2/3/2015

2014 ANNUAL REPORT
PROJECT:
FACILITY:
NORTH DURHAM WWTP NPDES:
SOUTH DURHAM WWTP NPDES:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APLICATION ANNUAL REPORT:
City of Durham
Durham, NC
North Durham WRF
1900 E Club Blvd
Durham, NC 27704
[phone]
South Durham WRF
6605 Farrington Rd.
Chapel Hill, NC 27517
[phone]
NCO023 841
NC 0047597
Don Greeley,Director of Water Management
101 City Hall Plaza
Durham, NC 27701
[phone]
John Dodson, Superintendent (North)
1900 E Club Blvd
Durham, NC 27704
[phone]
Charles Cocker, Superintendent (South)
6605 Farrington Rd.
Chapel Hill, NC 27517
[phone]
Synagro Central, LLC
Contact: Marshall Puryear
[phone]

2014 ANNUAL REPORT
PROJECT:
FACILITY:
PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
City of Durham
Durham, NC
Williams WTP
1405 Hillandale Rd
Durham, NC 27705
[phone]
WQ0000691
Don Greeley, Director,
101 City Hall Plaza
Durham, NC 27701
[phone]
Water Management
FACILITY OPERATOR: Bobby Whisnant, Assistant Superintendent
101 City Hall Plaza
Durham, NC 27701
[phone]

2014 ANNUAL REPORT
PROJECT:
FACILITY:
PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
City of Durham
Durham, NC
Brown WTP
1615 Infinity Rd
Durham, NC 27712
[phone]
WQ0000691
Don Greeley, Director, Water Management
101 City Hall Plaza
Durham, NC 27701
[phone]
Tom Lucas, Assistant Superintendent
101 City Hall Plaza
Durham, NC 27701
[phone]

" } Biosolids Handling in Calendar Year 2014
City Of Durham, North Carolina — Permit WQ0003504
Biosolids from the City of Durham Williams WTP (NPDES 03-32-010(B)) were
transferred to City of Durham Brown WTP as a liquid where they were then dewatered
and land applied or taken to a compost facility .

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504 Laboratory
Facility Name: DURHAM, NC A&L Eastern Laboratories Inc.
NPDES# : NCO023841
or WQ# (residual only)
WWTP Name: NORTH DURHAM WWTP
Residuals Analysis Data
Product Type
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
Date Sampled (grab) or
01/06/14
03/10/14
04/23/14
06/24/14
08/26/14
10/22/14
Date Composited
Percent Solids
16.35
15.18
15.24
15.24
15. 05
16.64
PARAMETERS (mg/kg
dry weight)
Arsenic
5
5
6
5
6
5
Cadmium
2
2
2
2
2
2
Mercury
1.4
0.6
0.8
0.7
1.2
0.4
Chromium
43
82
35
44
47
34
Copper
318
305
263
286
292
302
Lead
34
37
33
.31
28
29
Molybdenum
8
8
7
8
8
5
Nickel
23
36
22
27
27
24
Selenium
<5
<5
5
<5
<5
<5
Zinc
3260
3340
3030
2940
3100
3080
Total Phosphorus
38000
38800
30700
34700
33000
31300
TKN
54300
58000•
61500
59400
60100
60100
Ammonia -Nitrogen
15300
15300
12500
14100
14900
14800
Nitrate and Nitrite
5.5
15.2
5.25
13.8
611
1080
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 15
F PREPARER)
DENR FORM RSSF (5/2003) Printed: Friday - January 30, 2015 at 08:28:22 for: 2012 01

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504
Laboratory
Facility Name: DURHAM, NC
A&L Eastern
Laboratories Inc.
NPDES# : NCO023841
or WQ# (residual only)
WWTP Name: NORTH DURHAM WWTP
Residuals Analysis Data
Product Type ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
Date Sampled (grab) or 01/06/14
03/10/14
04/23/14
06/24/14 08/26/14
10/22/14
Date Composited
Percent Solids 16.35
15.18
15.24
15.24
15.05
16.64
PARAMETERS (mg/kg dry weight)
Aluminum 14100
11000
13500
16400
17300
16400
Calcium 17800
17500
15200
15400
16100
18400
Magnesium 9230
10200
7220
8080
7990
8140
pH 8.40
8.60
8.53
8.45
8.78
8.14
Potassium 4260
4260
3910
3710
4130
3760
Sodium 786
798
626
719
885
790
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
signific.aq penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X \
(SIG
NR-
F PREPAR
Not Reported or Data Not Required
Date i
DENR FORM RSSF-B (7/2002) Printed: Friday - January 30 2015 at 08:29:24 for: 2012 01

Page: 1 of 2
Report Number: 14-010-0202
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab'Number : 97421
Sample Id: NORTH DURHAM WRF
990 A&L Eastern Laboratories, Inc:_
7621 Whitepine Road Richmond, Virginii 23237 [phone] Fax [phone],446
wwwaleastem.com
Project: DURHAM NORTH WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled- 1/6/201411:20:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Solids *
16.35
163500
100.0
JM
01/10/2014 14:19
SM-2540G
Moisture"
83.65
100.0
JM
01/10/201414:19
SM-2540G
Total Kjeldahl Nitrogen
5.43
54300
10.0
JM
01/13/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
3.80
38000
100
KM
01/13/2014 11:35
SW 6010C
Total Potassium
0.43
4260
100
KM
01/13/2014 11:35
SW 6010C
Total Sulfur
1.49
14900
100
KM
01/13/2014 11:35
SW 6010C
Total Calcium
1.78
17800
100
KM
01/13/2014 11:35
SW 6010C
Total Magnesium
0.92
9230
100
KM
01/13/2014 11:35
SW 6010C
Total Sodium
0.08
786
100
KM
01/13/2014 11:35
SW 6010C
Total Iron
43400
100
KM
01/13/2014 11:35
SW 6010C
Total Aluminum
14100
100
KM
01/13/2014 11:35
SW 6010C
Total Manganese
1070
5
KM
01/13/2014 11:35
SW 6010C
Total Copper
318
5
KM
01/13/2014 11:35
SW 6010C
Total Zinc
3260
5
KM
01/13/2014 11:35
SW 6010C
Ammonia Nitrogen
1.53
15300
10.0
JM
01/13/2014 08:30
SM-4500-NI3C
Organic N
3.90
39000
10.0
01/13/2014 08:30
CALCULATION
Nitrate+Nitrite-N
5.50
2.00
JM
01/13/2014 08:30
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
01/13/2014 11:35
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , (`
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-010-0202
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97421
Sample Id: NORTH DURHAM WRF
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (904) 743-9.401 Fax (604) 271-W6
wwwaleastern.com
Project: DURHAM NORTH WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/6/2014 11:20:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Chromium
43
5
KM
01/13/2014 11:35
Total Nickel
23
5
KM
.01/13/2014 11:35
Total Lead
34
5
KM
01/13/2014 11:35
Total Arsenic
5.0
3.0
KM
01/13/2014 11:35
Total Mercury
1.4
0.4
KM
01/13/2014 09:00
Total Selenium
<5.0
5.0
KM
01/13/2014 11:35
pH (Standard Units) *
8.40
2.00
JM
01/13/2014 08:30
Total Volatile Solids
63.87 638700
100.0
JM
01/10/2014 14:19
Total Molybdenum
8
5
KM
01/13/2014 11:35
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S"
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW-7471 B
SW 6010C
SW-9045D
SM-2540G
SW 6010C
ALL OTHER QC

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 1/6/2014 1/1/2014-2/28/2014 0.4798
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (786 x 16.3500) = 100 = 128.511
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (17800 x 16.3500) _ 100 = 2910.3
Mg mg/I = (mg mg/kg x % Solids) = 100 = (9230 x 16.3500) _ 100 = 1509.11
Na meq = Na mg/I = Molec.Wgt.Na = 128.511 + 23 = 5.58743
Ca meq = Ca mg/I _ Molec.Wgt:Ca = 2910.3 = 20 = 145.515
Mg meq = Mg mg/I = Molec.Wgt.Mg = 1509.11 = 12 = 125.759
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.58743 = SgrRoot[0.5(145.51.5+125.759)] = 0.479750
Printed: 1/30/2015
Page 1
10:46

Page: 1 of 2
Report Number: 14-073-0208
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98391
Sample Id: NORTH DURHAM WRF
p� A&L Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
ww%aleastern.com
Project: NORTH DURHAM WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/10/2014 09:20:00
Date Received: 03/14/2014 00:00
Date Reported: 03/21/2014
Total Solids "
15.18
151800
100.0
BW
03/14/2014 15:00
SM-2540G
Moisture *
84.82
100.0
BW
03/14/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.80
58000
10.0
JM
03/17/2014 09:15
SM-4500-NH3C-TKN
Total Phosphorus
3.88
38800
100
KM
03/17/2014 12:04
SW 6010C
Total Potassium
0.43
4260
100
KM
03/17/2014 12:04
SW 6010C
Total Sulfur
1.40
14000
100
KM
03/17/2014 12:04
SW 6010C
Total Calcium
1.75
17500
100
KM
03/17/2014 12:04
SW 6010C
Total Magnesium
1.02
10200
100
KM
03/17/2014 12:04
SW 6010C
Total Sodium
0.08
798
100
KM
03/17/2014 12:04
SW 6010C
Total Iron
44700
100
KM
03/17/2014 12:04
SW 6010C
Total Aluminum
11000
100
KM
03/17/2014 12:04
SW 6010C
Total Manganese
982
5
KM
03/17/2014 12:04
SW 6010C
Total Copper
305
5
KM
03/17/2014 12:04
SW 6010C
Total Zinc
3340
5
KM
03/17/2014 12:04
SW 6010C
Ammonia Nitrogen
1.53
15300
10.0
JM
03/17/2014 08:44
SM-4500-NH3C
Organic N
4.27
42700
10.0
03/17/2014 08:44
CALCULATION
Nitrate+Nitrite-N
15.2
2.00
JM
03/17/2014 08:45
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
03/17/2014 12:04
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-073-0208
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: ,SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98391
Sample Id : NORTH DURHAM WRF
@Do
A&L EasternLaboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237(804) 743.9.401 Fax [phone]
Wwwaleastern.GOm
Project: NORTH DURHAM WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/10/2014 09:20:00
Date Received: 03/14/2014 00:00
Date Reported: 03/21/2014
Total Chromium
82
5
KM
03/17/2014 12:04
SW 6010C
Total Nickel
36
5-1
KM
03/17/2014 12:04
SW 6010C
Total Lead
37
5
KM
03/17/2014 12:04
SW 6010C
Total Arsenic
5.0
3.0
KM
03/17/2014 12:04
SW 6010C
Total Mercury
0.6
0.4
KM
03/17/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
03/17/2014 12:04
SW 6010C
pH (Standard Units) "
8.60
2.00
JM
03/17/2014 08:44
SW-9045D
Total Molybdenum
8
5
KM
03/17/2014 12:04
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Mn". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)'
Product Code Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 3/10/2014 3/1/2014-4/3012014 0.4603
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (798 x 15.1800) -= 100 = 121.136
Ca mg/1= (Ca mg/kg x % Solids) _ 100 = (17500 x 15.1800) = 100 = 2656.5
Mg mg/1 = (mg mg/kg x % Solids) = 100 = (10200 x 15.1800) = 100 = 1548.36
Na meq = Na mg/I = Molec.Wgt.Na = 121.136 = 23 = 5.2668
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2656.5 = 20 = 132.825
Mg meq = Mg mg/1 + Molec.Wgt.Mg = 1548.36 = 12 = 129.03
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.2668 + SgrRoot[0.5(132.825+129.03)] = 0.46029
Printed: 1 /30/2015
Page 1 10:51

Page: 1 of 2
Report Number: 14-119-0204
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55063
Sample Id: N DURHAM
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271=U46
wwwaleastern.cotn
Project: NORTH DURHAM WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2014 08:30:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014
Total Solids *
15.24
152400
100.0
JM
04/29/2014 15:00
SM-2540G
Moisture
84.76
100.0
JM
04/29/201415:00
SM-2540G
Total Kjeldahl Nitrogen
6.15
61500
10.0
JM
04/30/2014 08:35
SM-4500-NH3C-TKN
Total Phosphorus
3.07
30700
100
KM
05/01/2014 08:58
SW 6010C
Total Potassium
0.39
3910
100
KM
05/01/2014 08:58
SW 6010C
Total Sulfur
1.24
12400
100
KM
05/01/2014 08:58
SW 6010C
Total Calcium
1.52
15200
100
KM
05/01/2014 08:58
SW 6010C
Total Magnesium
0.72
7220
100
KM
05/01/2014 08:58
SW 6010C
Total Sodium
0.06
626
100
KM
05/01/2014 08:58
SW 6010C
Total Iron
40800
100
KM
05/01/2014 08:58
SW 6010C
Total Aluminum
13500
100
KM
05/01/2014 08:58
SW 6010C
Total Manganese
657
5
KM
05/01/2014 08:58
SW 6010C
Total Copper
263
5
KM
05/01/2014 08:58
SW 6010C
Total Zinc
3030
5
KM
051/01/2014 08:58
SW 6010C
Ammonia Nitrogen
1.25
12500
10.0
JM
04/30/2014 08:35
SM-4500-NI3C
Organic N
4.90
49000
10.0
04/30/2014 08:35
CALCULATION
Nitrate+Nitrite-N
5.25
2.00
JM
04/30/2014 08:35
SM-4500NO3F
Total Cadmium
2.0
2.0
KM
05/01/2014 08:58
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. (�+
4L
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , �+1�
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-119-0204
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55063
Sample Id : N DURHAM
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Arbinia23137 [phone] Fax [phone]
wwwaleastern.com
Project: NORTH DURHAM WWTP
NC CERT#257
REPORT OFANALYS/S Date Sampled: 4/23/2014 08:30:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014
Total Chromium
35
5
KM
05/01/2014 08:58
SW 6010C
Total Nickel
22
5
KM
05/01/2014 08:58
SW 6010C
Total Lead
33
5
KM
05/01/2014 08:58
SW 6010C
Total Arsenic
6.0
3.0
KM
05/01/2014 08:58
SW 6010C
Total Mercury
0.8
0.4
KM
04/30/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
05/01/2014 08:58
SW 6010C
pH (Standard Units)
8.53
2.00
JM
04/30/2014 08:35
SW-9045D
Total Molybdenum
7
5
KM
05/01/2014 08:58
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N", "Al", "K", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
�- 7Ti23inR

Sodium Absorption Ratio Calculation (SAR)
Product Code - Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 4/23/2014 5/112014-6/30/2014 0.4072
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (626 x 15.2400) _ 100 = 95.4024
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (15200 x 15.2400) = 100 = 2316.48
Mg mg/I = (mg mg/kg x % Solids) = 100 = (7220 x 15.2400) + 100 = 1100.33
Na meq = Na mg/I _ Molec.Wgt.Na = 95.4024 = 23 = 4.14793
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2316.48 20 = 115.824
Mg meq = Mg mg/I = Molec.Wgt.Mg = 1100.33 _ 12 = 91.694
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.14793 = SgrRoot[0.5(115.824+91.694)] = 0.40721
Printed: 1 /30/2015
Page 1 10:51

Page: 1 of 2
Report Number: 14-177-0209
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56138
Sample Id: DURHAM NORTH PLANT
A&L Eastern Laboratories, Inc._
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: DURHAM NORTH PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 14:00:00
Date Received: 06/26/2014 00:00
Date Reported: 06/30/2014
Total Solids *
15.24
152400
100.0
JM
06/26/2014 14:30
SM-2540G
Moisture *
84.76
100.0
JM
06/26/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
5.94
59400
10.0
JM
06/27/2014 08:15
SM-4500-NH3C-TKN
Total Phosphorus
3.47
34700
100
KM
06/27/2014 12:53
SW 6010C
Total Potassium
0.37
3710
100
KM
06/27/2014 12:53
SW 6010C
Total Sulfur
1.27
12700
100
KM
06/27/2014 12:53
SW 6010C
Total Calcium
1.54
15400
100
KM
06/27/2014 12:53
SW 6010C
Total Magnesium
0.81
8080
100
KM
06/27/2014 12:53
SW 6010C
Total Sodium
0.07
719
100
KM
06/27/2014 12:53
SW 6010C
Total Iron
43900
100
KM
06/27/2014 12:53 .
SW 6010C
Total Aluminum
16400
100
KM
06/27/2014 12:53
SW 6010C
Total Manganese
639
5
KM
06/27/2014 12:53
SW 6010C
Total Copper
286
5
KM
06/27/2014 12:53
SW 6010C
Total Zinc
2940
5
KM
06/27/2014 12:53
SW 6010C
Ammonia Nitrogen
1.41
14100
10.0
JM
06/27/2014 08:15
SM-4500-NI3C
Organic N
4.53
45300
10.0
06/27/2014 08:15
CALCULATION
Nitrate+Nitrite-N
13.8
2.00
JM
06/27/2014 08:15
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
06/27/2014 12:53
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-177-0209
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56138
Sample Id: DURHAM NORTH PLANT
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Project: DURHAM NORTH PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 14:00:00
Date Received: 06/26/2014 00:00
Date Reported: 06/30/2014
Total Chromium
44
5
KM
06/27/2014 12:53
SW 6010C
Total Nickel
27
5
KM
06/27/2014 12:53
SW 6010C
Total Lead
31
5
KM
06/27/2014 12:53
SW 6010C
Total Arsenic
5.0
3.0
KM
06/27/2014 12:53
SW 6010C
Total Mercury
0.7
0.4
KM
06/27/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/27/2014 12:53
SW 6010C
pH (Standard Units) *
8.45
2.00
JM
06/27/2014 08:15
SW-9045D
Total Molybdenum
8
5
KM
06/27/2014 12:53
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 6/24/2014 7/112014-8131/2014 0.4543
DIGESTED CAKE
Na mg/1= (Na mg/kg x % Solids) = 100 = (719 x 15.2400) _ 100 = 109.576
Ca mg/1= (Ca mg/kg x % Solids) + 100 = (15400 x 15.2400) = 100 = 2346.96
Mg mg/1 = (mg mg/kg x % Solids) = 100 = (8080, x 15.2400) _ 100 = 1231.30
Na meq = Na mg/l _ Molec.Wgt.Na = 109.576 = 23 = 4.76416
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 2346.96 = 20 = 117.348
Mg meq = Mg mg/l _ Molec.Wgt.Mg = 1231.39 = 12 = 102,616
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.76416 = SgrRoot[0.5(117.348+102.616)] = 0.454282
Printed: 1/30/2015
Page 1 10:53

Page: 1 of 2
Report Number: 14-240-0203
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57266
Sample Id: NORTH DURHAM PLANT
@A&L� Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia 23237 ,[phone] Fax [phone]
P. --
wwwaleastern.com
Project: NORTH DURHAM PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/26/2014 11:30:00
Date Received: 08/28/2014 00:00
Date Reported: 09/03/2014
Total Solids "
15.05
150500
100.0
JM
08/28/2014 14:30
SM-2540G
Moisture *
84.95
100.0
JM
08/28/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
6.01
60100
10.0
JM
08/29/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
3.30
33000
100
KM
08/29/2014 11:49
SW 6010C
Total Potassium
0.41
4130
100
KM
08/29/2014 11:49
SW 6010C
Total Sulfur
1.37
13700
100
KM
08/29/2014 11:49
SW 6010C
Total Calcium
1.61
16100
100
KM
08/29/2014 11:49
SW 6010C
Total Magnesium
0.80
7990
100
KM
08/29/2014 11:49
SW 6010C
Total Sodium
0.09
885
100
KM
08/29/2014 11:49
SW 6010C
Total Iron
41600
100
KM
08/29/2014 11:49
SW 6010C
Total Aluminum
17300
100
KM
08/29/2014 11:49
SW 6010C
Total Manganese
669
5
KM
08/29/2014 11:49
SW 6010C
Total Copper
292
5
KM
08/29/2014 11:49
SW 6010C
Total Zinc
3100
5
KM
08/29/2014 11:49
SW 6010C
Ammonia Nitrogen
1.49
14900
10.0
JM
08/29/2014 08:19
SM-4500-NH3C
Organic N
4.52
45200
10.0
08/29/2014 08:19
CALCULATION
Nitrate+Nitrite-N
611
2.00
JM
09/02/2014 08:15
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
08/29/2014 11:49
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-240-0203
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To. SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57266
Sample Id: NORTH DURHAM PLANT
A&L Eastern Laboratories, Inc.
99.
7,621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: NORTH DURHAM PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/26/2014 11:30:00
Date Received: 08/28/2014 00:00
Date Reported: 09/03/2014
Total Chromium
47
5
KM
08/29/2014 11:49
SW 6010C
Total Nickel
27
5
KM
08/29/2014 11:49
SW 6010C
Total Lead
28
5
KM
08/29/2014 11:49
SW 6010C
Total Arsenic
6.0
3.0
KM
08/29/2014 11:49
SW 6010C
Total Mercury
1.2
0.4
KM
08/29/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/29/2014 11:49
SW 6010C
pH (Standard Units) *
8.78
2.00
JM
08/29/2014 09:00
SW-9045D
Total Molybdenum
8
5
KM
08/29/2014 11:49
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Ca", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 8/26/2014 9/1/2014-10/31/2014 0.5504
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) _ 100 = (885 x 15.0500) =100 = 133.193
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (16100 x 15.0500) = 100 = 2423.05
Mg mg/I = (mg mg/kg x % Solids) = 100 = (7990 x 15.0500) = 100 = 1202.49
Na meq = Na mg/I = Molec.Wgt.Na = 133.193 = 23 = 5.79098
Ca meq = Ca mg/I = Molec.Wgt.Ca = 2423.05 = 20 = 121.153
Mg meq = Mg mg/I = Molec.Wgt.Mg = 1202.49 = 12 = 100.208
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.79098 _ SgrRoot[0.5(121.153+100.208)] = 0.550449
Printed: 1 /30/2015
Page 1 10:53

Page: 1 of 2
Report Number: 14-296-0211
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58320
Sample Id: NORTH DURHAM
99.
A&L EasternLaboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: NORTH DURAHM
NC CERT#257
REPORT OFANALYSIS Date Sampled: 10/22/2014 10:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Solids *
16.64
166400
100.0
JM
10/23/2014 14:44
SM-2540G
Moisture `'
83.36
100.0
JM
10/23/2014 14:44
SM-2540G
Total Kjeldahl Nitrogen
6.01
60100
10.0
JM
10/24/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
3.13
31300
100
KM
10/24/2014 13:19
SW 6010C
Total Potassium
0.38
3760
100
KM
10/24/2014 13:19
SW 6010C
Total Sulfur
1.16
11600
100
KM
10/24/2014 13:19
SW 6010C
Total Calcium
1.84
18400
100
KM
10/24/2014 13:19
SW 6010C
Total Magnesium
0.81
8140
100
KM
10/24/2014 13:19
SW 6010C
Total Sodium
0.08
790
100
KM
10/24/2014 13:19
SW 6010C
Total Iron
35000
100
KM
10/24/2014 13:19
SW 6010C
Total Aluminum
16400
100
KM
10/24/2014 13:19
SW 6010C
Total Manganese
797
5
KM
10/24/2014 13:19
SW 6010C
Total Copper
302
5
KM
10/24/2014 13:19
SW 6010C
Total Zinc
3080
5
KM
10/24/2014 13:19
SW 6010C
Ammonia Nitrogen
1.48
14800
10.0
JM
10/24/2014 09:00
SM-4500-NH3C
Organic N
4.53
45300
10.0
10/24/2014 09:00
CALCULATION
Nitrate+Nitrite-N
1080
2.00
JM
10/27/2014 08:30
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
10/24/2014 13:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-296-0211
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58320
Sample Id : NORTH DURHAM
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271-W6
www.aleastern.co_m
Project: NORTH DURAHM
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/22/2014 10:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Chromium
34
5
KM
10/24/2014 13:19
SW 6010C
Total Nickel
24
5
KM
10/24/2014 13:19
SW 6010C
Total Lead
29
5
KM
10/24/2014 13:19
SW 6010C
Total Arsenic
5.0
3.0
KM
10/24/2014 13:19
SW 6010C
Total Mercury
0.4
0.4
KM
10/24/2014 11:15
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/24/2014 13:19
SW 6010C
pH (Standard Units)
8.14
2.00
JM
10/24/2014 09:00
SW-9045D
Total Molybdenum
5
5
KM
10/24/2014 13:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

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Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-01-ANDCAK-NC DURHAM, NC N. DURHAM WWTP ANAEROB. 10/22/2014 1111/2014-12/31/2014 0.4956
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (790 x 16.6400) _ 100 = 131.456
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (18400 x 16.6400) _ 100 = 3061.76
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (8140 x 16.6400) = 100 = 1354.5
Na meq = Na mg/I _ Molec.Wgt.Na = 131.456 + 23 = 5.71548
Ca meq = Ca mg/I = Molec.Wgt.Ca = 3061.76 _ 20 = 153.088
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 1354.5 + 12 = 112.875
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.71548 = SgrRoot[0.5(153.088+112.875)] = 0.49563
Printed: 1 /30/2015
Page 1 10:53

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504
Laboratory
Facility Name: DURHAM, NC
A&L Eastern Laboratories Inc.
NPDES# : NCO047597
or WQ# (residual only)
WWTP Name: SOUTH DURHAM WWTP
Residuals Analysis Data
Product Type ANDCAK ANDCAK
ANDCAK ANDCAK ANDCAK ANDCAK
Date Sampled (grab) or 01/06/14 03/10/14
04/23/14 06/24/14 08/26/14 10/22/14
Date Composited
Percent Solids 18.18 17.71
17.05 16.80 16.34 17.80
PARAMETERS (mg/kg dry weight)
Arsenic
4
4
6
4
4
5
Cadmium
<2
<2
2
2
2
2
Mercury
0.6
0.6
0.8
0.6
1.3
0.4
Chromium
41
80
46
47
58
34
Copper
343
341
333
371
413
386
Lead
17
20
19
19
24
20
Molybdenum
10
11
10
8
10
9
Nickel
2.1
35
27
26
32
29
Selenium
<5
5
7
<5
<5
5
Zinc
3230
3340
3370
3550
3360
3070
Total Phosphorus
39200
36100
38300
37200
37000
36600
TKN
59400
55400
55400
58100
56900
52100
Ammonia -Nitrogen
16600
16800
14 600
16300
14 900
12 600
Nitrate and Nitrite
6.6
<2
25.2
47
857
1080
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X L
(SIGNATURE
Date _-Z - '5;?-Is"
DENR FORM RSSF (5/2003) Printed: Friday - January 30, 2015 at 08:28:32 for: 2012 02

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
WQ0003504
Laboratory
Facility Name:
DURHAM, NC
A&L Eastern
Laboratories Inc.
NPDES# :
NCO047597
or WQ# (residual only)
WWTP Name:
SOUTH DURHAM WWTP
Residuals Analysis Data
Product Type
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
ANDCAK
Date Sampled (grab) or
01/06/14 03/10/14
04/23/14
06/24/14 08/26/14
10/22/14
Date Composited
Percent Solids
18.18
17.71
17.05
16.80
16.34
17.80
PARAMETERS (mg/kg
dry weight)
Aluminum
25000
24300
28000
28000
29900
30400
Calcium
19100
19400
20600
19700
19400
19200
Magnesium
7220
6090
5890
6000
73A0
5900
pH
8.53
8.81
8.22
8.26
8.54
7.42
Potassium
3920
3570
4080
4030
3910
3590
Sodium
908
952
953
914
1100
990
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X
(SIGNATURE OF PREPARER)
NR - Data Not Reported or Data Not Required
Date :Z - % -/-4,
DENR FORM RSSF-B (7/2002) Printed: Friday - January 30, 2015 at 08:29:39 for: 2012 02

Page: 1 of 2
Report Number: 14-010-0203
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97422
Sample Id: DURHAM SOUTH WRF
A� A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastem.com
Project: DURHAM SOUTH WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/6/2014 12:10:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Solids *
18.18
181800
100.0
JM
01/10/2014 14:19
SM-2540G
Moisture *
81.82
100.0
JM
01/10/2014 14:19
SM-2540G
Total Kjeldahl Nitrogen
5.94
59400
10.0
JM
01/13/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
3.92
39200
100
KM
01/13/2014 11:35
SW 6010C
Total Potassium
0.39
3920
100
KM
01/13/2014 11:35
SW 6010C
Total Sulfur
1.28
12800
100
KM
01/13/2014 11:35
SW 6010C
Total Calcium
1.91
19100'
100
KM
01/13/2014 11:35
SW 6010C
Total Magnesium
0.72
7220
100
KM
01/13/2014 11:35
SW 6010C
Total Sodium
0.09
908
100
KM
01/13/2014 11:35
SW 6010C
Total Iron
18300
100
KM
01/13/2014 11:35
SW 6010C
Total Aluminum
25000
100
KM
01/13/2014 11:35
SW 6010C
Total Manganese
845
5
KM
01/13/2014 11:35
SW 6010C
Total Copper
343
5
KM
01/13/2014 11:35
SW 6010C
Total Zinc
3230
5
KM
01/13/2014 11:35
SW 6010C
Ammonia Nitrogen
1.66
16600
10.0
JM
01/13/2014 08:30
SM-4500-NH3C
Organic N
4.28
42800
10.0
01/13/2014 08:30
CALCULATION
Nitrate+Nitrite-N
6.60
2.00
JM
01/13/2014 08:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
01/13/2014 11:35
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , 6�
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-010-0203
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97422
Sample Id: DURHAM SOUTH WRF
TT'
JL
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Wwwaleastern,com
Project: DURHAM SOUTH WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/6/2014 12:10:00
Date Received: 01/10/2014 00:00
Date Reported: 01/15/2014
Total Chromium
41
5
KM
01/13/2014 11:35
SW 6010C
Total Nickel
21
5
KM
01/13/2014 11:35
SW 6010C
Total Lead
17
5
KM
01/13/2014 11:35
SW 6010C
Total Arsenic
4.0
3.0
KM
01/13/2014 11:35
SW 6010C
Total Mercury
0.6
0.4
KM
01/13/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
01/13/2014 11:35
SW 6010C
pH (Standard Units) *
8.53
2.00
JM
01/13/2014 08:30
SW-9045D
Total Volatile Solids
65.85 658500
100.0
JM
01/10/2014 14:19
SM-2540G
Total Molybdenum
10
5
KM
01/13/2014 11:35
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Se". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As" AND "S".
ALL OTHER QC
DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 1/6/2014 1/1/2014-2/28/2014 0.6034
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) _ 100 = (908 x 18.1800) _ 100 = 165.074
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (19100 x 18.1800) + 100 = 3472.38
Mg mg/I = (mg mg/kg x % Solids) + 100 = (7220 x 18.1800) _ 100 = 1312.6
Na meq = Na mg/1 _ Molec.Wgt.Na = 165.074 = 23 = 7.17715
Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 3472.38 + 20 = 173.619
Mg meq = Mg mg/I — Molec.Wgt.Mg = 1312.6 + 12 = 109.383
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.17715 = SgrRoot[0.5(173.619+109.383)] = 0.603354
Printed: 1 /30/2015
Page 1 10:55

Page: 1 of 2
Report Number: 14-073-0209
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98392
Sample Id: SOUTH DURHAM
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 7434401 Fax [phone]
Wmaleastern,cllm
Project: SOUTH DURHAM WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/10/201412:10:00
Date Received: 03/14/2014 00:00
Date Reported: 03/21/2014
Total Solids *
17.71
177100
100.0
BW
03/14/2014 15:00
SM-2540G
Moisture *
82.29
100.0
BW
03/14/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.54
55400
10.0
JM
03/17/2014 09:15
SM-4500-NH3C-TKN
Total Phosphorus
3.61
36100
100
KM
03/17/2014 12:04
SW 6010C
Total Potassium
0.36
3570
100
KM
03/17/2014 12:04
SW 6010C
Total Sulfur
1.22
12200
100
KM
03/17/2014 12:04
SW 6010C
Total Calcium
1.94
19400
100
KM
03/17/2014 12:04
SW 6010C
Total Magnesium
0.61
6090
100
KM
03/17/2014 12:04
SW 6010C
Total Sodium
0.10
952
100
KM
03/17/2014 12:04
SW 6010C
Total Iron
19900
100
KM
03/17/2014 12:04
SW 6010C
Total Aluminum
24300
100
KM
03/17/2014 12:04
SW 6010C
Total Manganese
908
5
KM
03/17/2014 12:04
SW 6010C
Total Copper
341
5
KM
03/17/2014 12:04
SW 6010C
Total Zinc
3340
5
KM
03/17/2014 12:04
SW 6010C
Ammonia Nitrogen
1.68
16800
10.0
JM
03/17/2014 08:44
SM-4500-NI3C
Organic N
3.86
38600
10.0
03/17/2014 08:44
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
03/17/2014 08:45
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
03/17/2014 12:04
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-073-0209
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98392
Sample Id: SOUTH DURHAM
A� A&L Eastern Laboratories, Inc._
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastemxom
Project: SOUTH DURHAM WRF
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 3/10/2014 12:10:00
Date Received: 03/14/2014 00:00
Date Reported: 03/21/2014
Total Chromium
80
5
KM
03/17/2014 12:04
SW 6010C
Total Nickel
35
5
KM
03/17/2014 12:04
SW 6010C
Total Lead
20
5
KM
03/17/2014 12:04
SW 6010C
Total Arsenic
4.0
3.0
KM
03/17/2014 12:04
SW 6010C
Total Mercury
0.6
0.4
KM
03/17/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
03/17/2014 12:04
SW 6010C
pH (Standard Units) *
8.81
2.00
JM
03/17/2014 08:44
SW-9045D
Total Molybdenum
11
5
KM
03/17/2014 12:04
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Mn". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 3/10/2014 3/112014-4130/2014 0.6409
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) + 100 = (952 x 17.7100) _ 100 = 168.599
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (19400 x 17.7100) _ 100 = 3435.74
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (6090 x 17.7100) _ 100 = 1078.54
Na meq = Na mg/I = Molec.Wgt.Na = 168.599 _ 23 = 7.3304
Ca meq = Ca mg/I -= Molec.Wgt.Ca = 3435.74 = 20 = 171.787
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 1078.54 _ 12 = 89.8782
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.3304 + SgrRoot[0.5(171.787+89.8782)] = 0.64087
Printed: 1 /30/2015
Page 1
10:55

Page: i of 2
Report Number: 14-119-0205
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55064
Sample Id : S DURHAM
p� A&L Eastern Laboratories, Inc.,
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www aleastern.co- n
Project: SOUTH DURHAM WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2014 09:30:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014
Total Solids "
17.05
170500
100.0
JM
04/29/2014 15:00
SM-2540G
Moisture *
82.95
100.0
JM
04/29/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
5.54
55400
10.0
JM
04/30/2014 08:35
SM-4500-NH3C-TKN
Total Phosphorus
3.83
38300
100
KM
05/01/2014 08:58
SW 6010C
Total Potassium
0.41
4080
100
KM
05/01/2014 08:58
SW 6010C
Total Sulfur
1.27
12700
100
KM
05/01/2014 08:58
SW 6010C
Total Calcium
2.06
20600
100
KM
05/01/2014 08:58
SW 6010C
Total Magnesium
0.59
5890
100
KM
05/01/2014 08:58
SW 6010C
Total Sodium
0.10
953
100
KM
05/01/2014 08:58
SW 6010C
Total Iron
21000
100
KM
05/01/2014 08:58
SW 6010C
Total Aluminum
28000
100
KM
05/01/2014 08:58
SW 6010C
Total Manganese
899
5
KM
05/01/2014 08:58
SW 6010C
Total Copper
333
5
KM
05/01/2014 08:58
SW 6010C
Total Zinc
3370
5
KM
05/01/2014 08:58
SW 6010C
Ammonia Nitrogen
1.46
14600
10.0
JM
04/30/2014 08:35
SM-4500-NH3C
Organic N
4.08
40800
10.0
04/30/2014 08:35
CALCULATION
Nitrate+Nitrite-N
25.2
2.00
JM
04/30/2014 08:35
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
05/01/2014 08:58
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 6W9
9Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-119-0205
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55064
Sample Id: S DURHAM
@P, A&L Eastern Laboratories, Inc._
7621 Whitepine Road Richmond,- Virginia 23237 '[phone], Fax [phone]
wwWaleastemACHM
Project: SOUTH DURHAM WWTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2014 09:30:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014
Total Chromium
46
5
KM
05/01/2014 08:58
SW 6010C
Total Nickel
27
5
KM
05/01/2014 08:58
SW 6010C
Total Lead
19
5
KM
05/01/2014 08:58
SW 6010C
Total Arsenic
6.0
3.0
KM
05/01/2014 08:58
SW 6010C
Total Mercury
0.8
0.4
KM
04/30/2014 09:00
SW-7471 B
Total Selenium
7.0
5.0
KM
05/01/2014 08:58
SW 6010C
pH (Standard Units) '
8.22
2.00
JM
04/30/2014 08:35
SW-9045D
Total Molybdenum
10
5
KM
05/01/2014 08:58
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N", "A[", "K", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 4/23/2014 511/2014-6/30/2014 0.6204
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) _ 100 = (953 x 17.0500) = 100 = 162.487
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (20600 x 17.0500) _ 100 = 3512.3
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (5890 x 17.0500) _ 100 = 1004.25
Na meq = Na mg/I _ Molec.Wgt.Na = 162.487 _ 23 = 7.06463
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 3512.3 _ 20 = 175.615
Mg meq = Mg mg/I = Molec.Wgt.Mg = 1004.25 = 12 = 83.6871
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.06463 = SgrRoot[0.5(175.615+83.6871)] = 0.620442
Printed: 1/30/2015
Page 1 10:55

Page: 1 of 2
Report Number: 14-177-0208
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56137
Sample Id: DURHAM SOUTH PLANT
A&L Eastern Laboratories, Inc:.
7.611 Whitepine Road Richmond, Virginia 23237 (804)'743-9401 F.ax (804) 271-W. G
-wwwaleastern.com
Project: DURHAM SOUTH PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 13:00:00
Date Received: 06/26/2014 00:00
Date Reported: 06/30/2014
Total Solids *
16.80
168000
100.0
JM
06/26/2014 14:30
SM-2540G
Moisture *
83.20
100.0
JM
06/26/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
5.81
58100
10.0
JM
06/27/2014 08:15
SM-4500-NH3C-TKN
Total Phosphorus
3.72
37200
100
KM
06/27/2014 12:53
SW 6010C
Total Potassium
0.40
4030
100
KM
06/27/2014 12:53
SW 6010C
Total Sulfur
1.26
12600
100
KM
06/27/2014 12:53
SW 6010C
Total Calcium
1.97
19700
100
KM
06/27/2014 12:53
SW 6010C
Total Magnesium
0.60
6000
100
KM
06/27/2014 12:53
SW 6010C
Total Sodium
0.09
914
100
KM
06/27/2014 12:53
SW 6010C
Total Iron
26300
100
KM
06/27/2014 12:53
SW 6010C
Total Aluminum
28000
100
KM
06/27/2014 12:53
SW 6010C
Total Manganese
883
5
KM
06/27/2014 12:53
SW 6010C
Total Copper
371
5
KM
06/27/2014 12:53
SW 6010C
Total Zinc
3550
5
KM
06/27/2014 12:53
SW 6010C
Ammonia Nitrogen
1.63
16300
10.0
JM
06/27/2014 08:15
SM-4500-NH3C
Organic N
4.18
41800
10.0
06/27/2014 08:15
CALCULATION
Nitrate+Nitrite-N
47.0
2.00
JM
06/27/2014 08:15
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
06/27/2014.12:53
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-177-0208
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56137
Sample Id: DURHAM SOUTH PLANT
A� A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: DURHAM SOUTH PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 13:00:00
Date Received: 06/26/2014 00:00
Date Reported: 06/30/2014
Total Chromium
47
5
KM
06/27/2014 12:53
SW 6010C
Total Nickel
26
5
KM
06/27/2014 12:53
SW 6010C
Total Lead
19
5
KM
06/27/2014 12:53
SW 6010C
Total Arsenic
4.0
3.0
KM
06/27/2014 12:53
SW 6010C
Total Mercury
0.6
0.4
KM
06/27/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/27/2014 12:53
SW 6010C
pH (Standard Units) `
8.26
2.00
JM
06/27/2014 08:15
SW-9045D
Total Molybdenum
8
5
KM
06/27/2014 12:53
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 9
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made -- �%
�K�C..
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 6/24/2014 711/2014-8/3112014 0.5978
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) + 100 = (914-x 16.8000) _ 100 = 153.552
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (19700 x 16.8000) = 100 = 3309.6
Mg mg/I = (mg mg/kg x % Solids) = 100 = (6000 x 16.8000) =100 = 1008
Na meq = Na mg/I = Molec.Wgt.Na = 153.552 _ 23 = 6.67617
Ca meq = Ca mg/I + Molec.Wgt.Ca = 3309.6 _ 20 = 165.48
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 1008 = 12 = 84
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 6.67617 = SgrRoot[0.5(165.48+84)] = 0.597757
Printed: 1 /30/2015
Page 1 10:55

Page: 1 of 2
Report Number: 14-240-0204
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57267
Sample Id: SOUTH DURHAM PLANT
�L A&L Eastern Laboratories, Inc._
7621 Whitepine Road Richmond, Vlrglnia 23237' '(8m) 743-9401 Fax [phone]
wwwaleastem,com
Project: SOUTH DURHAM PLANT
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 8/'26/2014 10:45:00
Date Received: 08/28/2014 00:00
Date Reported: 09/03/2014
Total Solids
16.34
163400
100.0
JM
08/28/2014 14:30
SM-2540G
Moisture "
'83.66
100.0
JM
08/28/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
5.69
56900
10.0
JM
08/29/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
3.70
37000
100
KM
08/29/2014 11:49
SW 6010C
Total Potassium
0.39
3910
100
KM
08/29/2014 11:49
SW 6010C
Total Sulfur
1.22
12200
100
KM
08/29/2014 11:49
SW 6010C
Total Calcium
1.94
19400
100
KM
08/29/2014 11:49
SW 6010C
Total Magnesium
0.73
7340
100
KM
08/29/2014 11:49
SW 6010C
Total Sodium
0.11
1100
100
KM
08/29/2014 11:49
SW 6010C
Total Iron
21000
100
KM
08/29/2014 11:49
SW 6010C
Total Aluminum
29900
100
KM
08/29/2014 11:49
SW 6010C
Total Manganese
907
5
KM
08/29/2014 11:49
SW 6010C
Total Copper
413
5
KM
08/29/2014 11:49
SW 6010C
Total Zinc
3360
5
KM
08/29/2014 11:49
SW 6010C
Ammonia Nitrogen
1.49
14900
10.0
JM
08/29/2014 08:19
SM-4500-NH3C
Organic N
4.20
42000
10.0
08/29/2014 08:19
CALCULATION
Nitrate+Nitrite-N
857
2.00
JM
09/02/2014 08:15
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
08/29/2014 11:49
SW 6010C
-All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may hot be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-240-0204
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 57267
Sample Id: SOUTH DURHAM PLANT
A&L Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia 23237 '[phone] Fax [phone]
uvwweleastern.com
Project SOUTH DURHAM PLANT
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 8/26/2014 10:45:00
Date Received: 08/28/2014 00:00
Date Reported: 09/03/2014
Total Chromium
58
5
KM
08/29/2014 11:49
SW 6010C
Total Nickel
32
5
KM
08/29/2014 11:49
SW 6010C
Total Lead
24
5
KM
08/29/2014 11:49
SW 6010C
Total Arsenic
4.0
3.0
KM
08/29/2014 11:49
SW 6010C
Total Mercury
1.3
0.4
KM
08/29/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
08/29/2014 11:49
SW 6010C
pH (Standard Units) *
8.54
2.00
JM
08/29/2014 09:00
SW-9045D
Total Molybdenum
10
5
KM
08/29/2014 11:49
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Ca", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
1on- Z07-3 11-10

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 8/26/2014 911/2014-10/31/2014 0.6875
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) + 100 = (1100 x 16.3400) =100 = 179.74
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (19400 x 16.3400) = 100 = 3169.96
Mg mg/I = (mg mg/kg x % Solids) + 100 = (7340 x 16.3400) = 100 = 1199.36
Na meq = Na mg/I + Molec.Wgt.Na = 179.74 = 23 = 7.81478
Ca meq = Ca mg/I = Molec.Wgt.Ca = 3169.96 _ 20 = 158.498
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1199.36 : 12 = 99.9463
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.81478 + SgrRoot[0.5(158.498+99.9463)] = 0.687462
Printed: 1 /30/2015
Page 1 10:55

Page: 1 of 2
Report Number: 14-296-0212
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58321
Sample Id: SOUTH DURHAM
A&L Eastem Laboratories, Inc.
7621 Whitepine, Road Richmond, Virginia 23237 [phone] Fax (8(4),271.6446
wwwaleastern.com
Project: SOUTH DURHAM
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/22/2014 09:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Solids *
17.80
178000
100.0
JM
10/23/2014 14:44
SM-2540G
Moisture *
82.20
100.0
JM
10/23/2014 14:44
SM-2540G
Total Kjeldahl Nitrogen
5.21
52100
10.0
JM
10/24/2014 09:00
SM-4500-NH3C-TKN
Total Phosphorus
3.66
36600
100
KM
10/24/2014 13:19
SW 6010C
Total Potassium
0.36
3590
100
KM
10/24/2014 13:19
SW 6010C
Total Sulfur
1.26
12600
100
KM
10/24/2014 13:19
SW 6010C
Total Calcium
1.92
19200
100
KM
10/24/2014 13:19
SW 6010C
Total Magnesium
0.59
5900
100
KM
10/24/2014 13:19
SW 6010C
Total Sodium
0.10
990
100
KM
10/24/2014 13:19
SW 6010C
Total Iron
20300
100
KM
10/24/2014 13:19
SW 6010C
Total Aluminum
30400
100
KM
10/24/2014 13:19
SW 6010C
Total Manganese
902
5
KM
10/24/2014 13:19
SW 6010C
Total Copper
386
5
KM
10/24/2014 13:19
SW 6010C
Total Zinc
3070
5
KM
10/24/2014 13:19
SW 6010C
Ammonia Nitrogen
1.26
12600
10.0
JM
10/24/2014 09:00
SM-4500-NH3C
Organic N
3.95
39500
10.0
10/24/2014 09:00
CALCULATION
Nitrate+Nitrite-N
1080
2.00
JM
10/27/2014 08:30
SM-4500NO3F.
Total Cadmium
2.0
2.0
KM
10/24/2014 13:19
SW 6010C
All values are on a dry weight
basis except as noted by asterisk. Detection limit on all N series
is on a wet
basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any
reference, be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-296-0212
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58321
Sample Id: SOUTH DURHAM
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] :Fax (804) 27-1.W6
www.aleastem.com
Project: SOUTH DURHAM
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/22/2014 09:30:00
Date Received: 10/23/2014 00:00
Date Reported: 10/29/2014
Total Chromium
34
Total Nickel
29
Total Lead
20
Total Arsenic
5.0
Total Mercury
0.4
Total Selenium
5.0
pH (Standard Units) *
7.42
Total Molybdenum
9
Comments:
SULFUR AND ORGANIC NITROGEN NOT
FOR COMPLIANCE PURPOSES.
5
KM
10/24/2014 13:19
SW 6010C
5
KM
10/24/2014 13:19
SW 6010C
5
KM
10/24/2014 13:19
SW 6010C
3.0
KM
10/24/2014 13:19
SW 6010C
0.4
KM
10/24/2014 11:15
SW-7471 B
5.0
KM
10/24/2014 13:19
SW 6010C
2.00
JM
10/24/2014 09:00
SW-9045D
5
KM
10/24/2014 13:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

-"8AMPI.:I.Ni3, LOG W A -A
1QC1 Wbit.eplr
-4-
PRQj,�0TIMANAGtR:
-9,
YrN)
14-2§&02-12 N-� Epy
4
2y"�'dR.O.C6NyFiAL'L[.t/IDURIIAM 1 t2R'BOO 2014
-�;CkUTHDUkHANf4d CERX0 . 57 *310:29•
A&L cus-TOM6R SAMPLING SAMOLE ffO'F PAMPLING NETHOD' MF-THIOP
T�ME PAESERVED SHiPPEO
LAB i� 9AMAL81117D. WQ-ATIOM WOE CONTAINERS PARE-
Re11n46ished by,54npler:
RelinquisHo'j' Y,.*:
Relinquished: by:
SPECIAL INSTRUCTIONS-
;:nr M-0-nitorina. ourDoses.
Date Time
Recieved'by.-
F'O#;
,�N'ALYSI$ VE"QUEST
1�1 --
SAMPLE
$U
SL2
Cd
Cr,
--
Pb
As
Hq
SO
CAC01"
vblktlfe
Solids
C1
OeR
pc
.6 DvAlop
--- Alttt
-aW-Solids(Moisture), Total'Kjelctahl !Nitrogpn, Phospboru5j, and Potassium
:SL-2*:'� Basic Tesi 80 plu's:8ultir, Calcium, Magnesium,'Sodium, Iron, Alum MUM, Mangpnpse., Copper and Zinc

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-02-ANDCAK-NC DURHAM, NC S. DURHAM WWTP ANAEROB. 10/22/2014 11/1/2014-12/31/2014 0.6741
DIGESTED CAKE
Na mg/I = (Na mg/kg x % Solids) = 100 = (990 x 17.8000) _ 100 = 176.22
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (19200 x 17.8000) _ 100 = 3417.6
Mg mg/1 = (mg mg/kg x % Solids) _ 100 = (5900 x 17.8000) : 100 = 1050.2
Na meq = Na mg/I _ Molec.Wgt.Na = 176.22 _ 23 = 7.66174
Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 3417.6 _ 20 = 170.88
Mg meq = Mg mg/1 = Molec.Wgt.Mg = 1050.2 = 12 = 87.5167
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.66174 = SgrRoot[0.5(170.88+87.5167)] = 0.674061
Printed: 1 /30/2015
Page 1 10:55

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504
Facility Name: DURHAM, NC
NPDES#:
or WQ# (residual only)
WWTP Name: BROWN WTP
Residuals Analysis Data
Laboratory
A&L Eastern Laboratories Inc.
Product Type
WPC
WPC
WPC
WPC
Date Sampled (grab) or 02/20/14
04/23/14
06/24/14
10/07/14
Date Composited
Percent Solids
19.49
20.82
21.57
20.18
PARAMETERS (mg/kg dry -weight)
Arsenic
9
7
8
10
Cadmium
<2
2
<2
8
Mercury
<0.4
<0.4
<0.4
<0.4
Chromium
21
27
23
21
Copper
176
58
112
419
Lead
29
38
26
30
Molybdenum
<5
<5
<5
<5
Nickel
22
24
28
32
Selenium
<5
<5
<5
<5
Zinc
104
85
102
112
Total Phosphorus
1070
981
851
867
TKN
8210
7780
7740
6890
Ammonia -Nitrogen
975
961
881
4410
Nitrate and Nitrite
6.67
3.36
16.2
30.2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant pegplties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date �l '-
(SIGNATURE OF PREP,
DENR FORM RSSF (5/2003) Printed: Friday - January 30, 2015 at 08:28:57 for: 2012 04

ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0003504
Laboratory
Facility Name: DURHAM, NC
'A&L Eastern Laboratories Inc.
NPDES#:
or WQ# (residual only)
WWTP Name: BROWN WTP
Residuals Analysis Data
Product Type WPC
WPC
WPC
WPC
Date Sampled (grab) or 02/20/14
04/23/14
06/24/14
10/07/14
Date Composited
Percent Solids 19.49
20.82
21.57
20.18
PARAMETERS (mg/kg dry weight)
Aluminum 8400
18200
11400
490'0
Calcium 1120
719
752
1200
Magnesium 347
497
317
214
pH 5.81
5.03
5.16
5.47
Potassium 266
460
317
164
Sodium 229
175
262
256
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Date 1- (- (
(—SIGNAThRE OF PREPARER)
NR - Data Not Reported or Data Not Required
DENR FORM RSSF-B (7/2002) Printed: Friday - January 30, 2015 at 08:29:47 for: 2012 04

Page: 1 of 2
Report Number: 14-057-0204
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL L.LC/DURHAM
Mary Brewer.
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98066
Sample Id: DURHAM BROWN WTP
A&L Eastern Laboratories,, Inc._
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9.401 Fax [phone]
www aleastern.com
Project: DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 2/20/2014 10:35:00
Date Received: 02/26/2014 00:00
Date Reported: 03/03/2014
Total Solids
19.49
194900
100.0
JM
02/26/2014 15:09
SM-2540G
Moisture "
80.51
100.0
JM •
02/26/2014 15:09
SM-2540G
Total Kjeldahl Nitrogen
0.82
8210
10.0
JM
02/27/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
0.11
1070
100
KM
02/27/2014 11:11
SW 6010C
Total Potassium
0.03
266
100
KM
02/27/2014 11:11
SW 6010C
Total Sulfur
0.29
2850
100
KM
02/27/2014 11:11
SW 6010C
Total Calcium
0.11
1120
100
KM
02/27/2014 11:11
SW 6010C
Total Magnesium
0.03
347
100
KM
02/27/2014 11:11
SW 6010C
Total Sodium
0.02
229
100
KM
02/27/2014 11:11
SW 6010C
Total Iron
336000
100
KM
02/27/2014 11:11
SW 6010C
Total Aluminum
8400
100
KM
02/27/2014 11:11
SW 6010C
Total Manganese
2900
5
KM
02/27/2014 11:11
SW 6010C
Total Copper
176
5
KM
02/27/2014 11:11
SW 6010C
Total Zinc
104
100
KM
02/27/2014 11:11
SW 6010C
Ammonia Nitrogen
0.10
975
10.0
JM
02/27/2014 08:30
SM-4500-NH3C
Organic N
0.72
7235
10.0
02/27/2014 08:30
CALCULATION
Nitrate+Nitrite-N
6.67
2.00
JM
02/27/2014 08:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
02/27/2014 11:11
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.-�
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-057-0204
Account Number: 46451
Submitted By: JAMES BLACKWELL
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 98066
Sample Id: DURHAM BROWN WTP
p� A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www,aleastern.com
Project: DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 2/20/2014 10:35:00
Date Received: 02/26/2014 00:00
Date Reported: 03/03/2014
Total Chromium
21
5
KM
02/27/2014 11:11
SW 6010C
Total Nickel
22
5
KM
02/27/2014 11:11
SW 6010C
Total Lead
29
5
KM
02/27/2014 11:11
SW 6010C
Total Arsenic
9.0
3.0
KM
02/27/2014 11:11
SW 6010C
Total Mercury
<0.4
0.4
KM
02/27/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
02/27/2014 11:11
SW 6010C
pH (Standard Units) *
5.81
2.00
JM
02/27/2014 08:30
SW-9045D
Total Volatile Solids
32.53 325300
100.0
JM
02/26/2014 15:09
SM-2540G
Total Molybdenum
<5
5
KM
02/27/2014 11:11
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

ti
J
SAMPLNG LOG
YNAGRG S-OU1
76
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Illlllllllll�llilllllllll�llllll�6flll�ll�llll�lilllllelllllll 46451,
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sampling,, prad6dbi.Lps
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AWPLE
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-Y Tree R:e:6ieyed'by:-
SPEd,IAL NSTRUCTION&
Q*010 ;For,---- f —monitoringip urposes,.
MTAT,11
Rog:" <aooea
LISS"
8AMPLE
ANAWS S- EQUEST
Di
.dwv6j�
SLR'
-pll
cd
Cr'r, i
W,
Pb l,
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Se
PH
'c
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-IN02-N :
841 IV.
0
2 4 -7,
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i0o
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J010011
-1
F
Tota
l Total K-jp1d;�hl'Nitrogjan, Phogipbdrus �'a
2 �n Potassium
`_SL2. BasicTesf.SLi plus Sulfur, Calcium, Lim, Manganese Copper and Zino
qgqesiom m�, .6n,,Alumin
-An� r -,j - AGERCOPY
white —Ail C
17
m

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio.
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 2/20/2014 1/1/2014-3/31/2014 0.6746
Na mg/I = (Na mg/kg x % Solids) = 100 = (229 x 19.4900) = 100 = 44.6321
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (1120 x 19.4900) + 100 = 218.288
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (347 x 19.4900) + 100 = 67.6308
Na meq = Na mg/I + Molec.Wgt.Na = 44.6321 - 23 = 1.94053
Ca meq = Ca mg/I + Molec.Wgt.Ca = 218.288 + 20 = 10.9144
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 67.6303 = 12 = 5.63586
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.94053 + SgrRoot[0.5(10.9144+5.63586)] = 0.674578
Printed: 1 /30/2015
Page 1 10:56

Page: 1 of 2
Report Number: 14-119-0203
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55062
Sample Id: DURHAM WTP
99.A&L EasternLaboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 '[phone] Fax [phone]
wwmaleastern.com
Project: DURHAM WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2014 18:00:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014 '
Total Solids *
20.82
208200
100.0
JM
04/29/2014 15:00
SM-254OG
Moisture *
79.18
100.0
JM
04/29/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
0.78
7780
10.0
JM
04/30/2014 08:35
SM-4500-NH3C-TKN
Total Phosphorus
0.10
981
100
KM
05/01/2014 08:58
SW 6010C
Total Potassium
0.05
460
100
KM
05/01/2014 08:58
SW 6010C
Total Sulfur
0.34
3390
100
KM
05/01/2014 08:58
SW 6010C
Total Calcium
0.07
719
100
KM
05/01/2014 08:58
SW 6010C
Total Magnesium
0.05
497
100
KM
05/01/2014 08:58
SW 6010C
Total Sodium
0.02
175
100
KM
05/01/2014 08:58
SW 6010C
Total Iron
289000
100
KM
05/01/2014 08:58
SW 6010C
Total Aluminum
18200
100
KM
05/01/2014 08:58
SW 6010C
Total Manganese
1470
5
KM
05/01/2014 08:58
SW 6010C
Total Copper
58
5
KM
05/01/2014 08:58
SW 6010C
Total Zinc
85
5
KM
05/01/2014 08:58
SW 6010C
Ammonia Nitrogen
0.10
961
10.0
JM
04/30/2014 08:35
SM-4500-NH3C
Organic N
0.68
6819
10.0
04/30/2014 08:35
CALCULATION
Nitrate+Nitrite-N
3.36
2.00
JM
04/30/2014 08:35
SM-450ON08F
Total Cadmium
2.0
2.0
KM
05/01/2014 08:58
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-119-0203
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028,
Lab Number: 55062
Sample Id : DURHAM WTP
AwL A&L Eastern Laboratories, Inc.,
7621.Whitepine Road Richmond, Virginia 23237 [phone] Fax (804) 271.W6
wwwaleastern.com
Project: DURHAM WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/23/2014 18:00:00
Date Received: 04/29/2014 00:00
Date Reported: 05/02/2014
Total Chromium
27
5
KM
05/01/2014 08:58
SW 6010C
Total Nickel
24
5
KM
05/01/2014 08:58
SW 6010C
Total Lead
38
5
KM
05/01/2014 08:58
SW 6010C
Total Arsenic
7.0
3.0
KM
05/01/2014 08:58
SW 6010C
Total Mercury
<0.4
0.4
KM
04/30/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
05/01/2014 08:58
SW 6010C
pH (Standard Units) *
5.03
2.00
JM
04/30/2014 08:35
SW-9045D
Total Molybdenum
<5
5
KM
05/01/2014 08:58
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N","AI", "K", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
9-1-iT-3.1RH

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 4/23/2014 41112014-6/30/2014 0.5582
Na mg/I = (Na mg/kg x % Solids) = 100 = (175 x 20.8200) =100 = 36.435
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (719 x 20.8200) =100 = 149.696
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (497 x 20.8200) + 100 = 103.475
Na meq = Na mg/I + Molec.Wgt.Na = 36.435 _ 23 = 1.58413
Ca meq = Ca mg/I = Molec.Wgt.Ca = 149.696 + 20 = 7.48479
Mg meq = Mg mg/I = Molec.Wgt.Mg = 103.475 _ 12 = 8.62295
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.58413 = SgrRoot[0.5(7.48479+8.62295)] = 0.558198
Printed: 1 /30/2015
Page 1 10:56

Page: 1 of 2
Report Number: 14-177-0207
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56136
Sample Id: DURHAM BROWN WTP
Q L A&L Eastern Laboratories, 'Inc.-
-7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.co n
Project:: DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 15:00:00
Date Received- 06/26/2014 00:00
Date Reported: 06/30/2014
Total Solids *
21.57
215700
100.0
JM
06/26/2014 14:30
SM-2540G
Moisture *
78.43
100.0
JM
06/26/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
0.77
7740
10.0
JM
06/27/2014 08:15
SM-4500-NH3C-TKN
Total Phosphorus
0.09
851
100
KM
06/27/2014 12:53
SW 6010C
Total Potassium
0.03
317
100
KM
06/27/2014 12:53
SW 6010C
Total Sulfur
0.29
2930
100
KM
06/27/2014 12:53
SW 6010C
Total Calcium
0.08
752
100
KM
06/27/2014 12:53
SW 6010C
Total Magnesium
0.03
317
100
KM
06/27/2014 12:53
SW 6010C
Total Sodium
0.03
262
100
KM
06/27/2014 12:53
SW 6010C
Total Iron
365000
100
KM
06/27/2014 12:53
SW 6010C
Total Aluminum
11400
100
KM
06/27/2014 12:53
SW 6010C
Total Manganese
2320
5
KM
06/27/2014 12:53
SW 6010C
Total Copper
112
5
KM
06/27/2014 12:53
SW 6010C
Total Zinc
102
5
KM
06/27/2014 12:53
SW 6010C
Ammonia Nitrogen
0.09 -
881
10.0
JM
06/27/2014 08:15
SM-4500-NH3C
Organic N
0.68
6859
10.0
06/27/2014 08:15
CALCULATION
Nitrate+Nitrite-N
16.2
2.00
JM
06/27/2014 08:15
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
06/27/2014 12:53
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-177-0207
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56136
Sample Id : DURHAM BROWN WTP
@P. A&L Eastern Laboratories, Inc._
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.aleastern.com
Project: DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/24/2014 15:00:00
Date Received: 06/26/2014 00:00
Date Reported: 06/30/2014
Total Chromium
23
5
KM
06/27/2014 12:53
SW 6010C
Total Nickel
28
5
KM
06/27/2014 12:53
SW 6010C
Total Lead
26
5
KM
06/27/2014 12:53
SW 6010C
Total Arsenic
8.0
3.0
KM
06/27/2014 12:53
SW 6010C
Total Mercury
<0.4
0.4
KM
06/27/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/27/2014 12:53
SW 6010C
pH (Standard Units) *
5.16
2.00
JM
06/27/2014 08:15
SW-9045D
Total Molybdenum
<5
5
KM
06/27/2014 12:53
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 6/24/2014 7/1/2014-9/30/2014 0.9351
Na mg/I = (Na mg/kg x % Solids) _ 100 = (262 x 21.5700) _ 100 = 56.5134
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (752 x 21.5700) = 100 = 162.206
Mg mg/I = (mg mg/kg x % Solids) = 100 = (317 x 21.5700) =100 = 68.3769
Na meq = Na mg/I _ Molec.Wgt.Na = 56.5134 = 23 = 2.4571
Ca meq = Ca mg/I = Molec.Wgt.Ca = 162.206 _ 20 = 8.11032
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 68.3769 = 12 = 5.69808
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.4571 _ SgrRoot[0.5(8.11032+5.69808)] = 0.935119
Printed: 1/30/2015
Page 1 10:56

Page: 1 of 2
-Report Number: 14-283-0211
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028.
Lab Number: 58055
Sample Id: DURHAM BROWN WTP
AFL A&L Eastern Laboratories, Inca
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
0
wwwaleastem4om
Project : DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/7/2014 16:00:00
Date Received: 10/10/2014 00:00
Date Reported: 10/21/2014
Total Solids '
20.18
201800
100.0
MW
10/13/2014 07:39
SM-2540G
Moisture *
79.82
100.0
MW
10/13/2014 07:39
SM-2540G
Total Kjeldahl Nitrogen
0.69
6890
10.0
JM
10/14/2014 08:19
SM-4500-NH3C-TKN
Total Phosphorus
0.09
867
100
KM
10/17/2014 11:35
SW 6010C
Total Potassium
0.02
164
100
KM
10/17/2014 11:35
SW 6010C
Total Sulfur
0.30
2990
100
KM
10/17/2014 11:35
SW 6010C
Total Calcium
0.12
1200
100
KM
10/17/2014 11:35
SW 6010C
Total Magnesium
0.02
214
100
KM
10/17/2014 11:35
SW 6010C
Total Sodium
0.03
256
100
KM
10/17/2014 11:35
SW 6010C
Total Iron
369000
100
KM
10/17/2014 11:35
SW 6010C
Total Aluminum
4900
100
KM
10/17/2014 11:35
SW 6010C
Total Manganese
5810
5
KM
10/17/2014 11:35
SW 6010C
Total Copper
419
5
KM
10/17/2014 11:35
SW 6010C
Total Zinc
112
5
KM
10/17/2014 11:35
SW 6010C
Ammonia Nitrogen
0.44
4410
10.0
JM
10/13/2014 07:54
SM-4500-NH3C
Organic N
0.25
2480
10.0
10/13/2014 07:54
CALCULATION
Nitrate+Nitrite-N
30.2
2.00
JM
10/13/2014 07:55
SM-450ONO3F
Total Cadmium
8.0
2.0
KM
10/17/2014 11:35
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-283-0211
Account Number: 46451
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58055
Sample Id: DURHAM BROWN WTP
_A&L Eastern Laboratories, Inc.,
AFL .7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
wwwaleastern.com
Project: DURHAM BROWN WTP
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/7/2014 16:00:00
Date Received: 10/10/2014 00:00
Date Reported: 10/21/2014
Total Chromium
21
5
KM
10/17/2014 11:35
SW 6010C
Total Nickel
32
5
KM
10/17/2014 11:35
SW 6010C
Total Lead
30
5
KM
10/17/2014 11:35
SW 6010C
Total Arsenic
10.0
3.0
KM
10/17/2014 11:35
SW 6010C
Total Mercury
<0.4
0.4
KM
10/13/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/17/2014 11:35
SW 6010C
pH (Standard Units) *
5.47
2.00
JM
10/13/2014 07:54
SW-9045D
Total Molybdenum
<5
5
KM
10/17/2014 11:35
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Cr", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
i9a$":na

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2012-04-WPC-NC DURHAM, NC BROWN WTP CAKE 10/7/2014 1011/2014-12/31/2014 0.8015
Na mg/I = (Na mg/kg x % Solids) = 100 = (256 x 20.1800) _ 100 = 51.6608
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (1200 x 20.1800) + 100 = 242.16
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (214 x 20.1800) + 100 = 43.1852
Na meq = Na mg/I _ Molec.Wgt.Na = 51.6608 _ 23 = 2.24612
Ca meq = Ca mg/I _ Molec.Wgt.Ca = 242.16 = 20 = 12.108
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 43.1852 = 12 = 3.59877
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.24612 _ SgrRoot[0.5(12.108+3.59877)] = 0.801503
Printed: 1 /30/2015
Page 1 10:56

FACILITY NAME: DURHAM, NC
OWNER: CLAUDE LYNCH, JR
SITE #: NC AM 00022 FIELD# : AM 00022 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 232.13
OPERATOR: CLAUDE LYNCH, JR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 58.90 ACRES PERMITTED: 58.90
Page : 1
Lime Applied "*
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
8/28/14
122.61 (W)
2.082
21.57
0.449
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
F 1829
I FESCUE
8/29/14
25.43 (W)
0.432
21.57
0.093
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
Aug-14
148.04 (W)
2.514
8/28/14
200.00 (CY)
3.396
16.80
0.480
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
IFESCUE
8/29/14
300.00 (CY)
5.093
16.80
0.721
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100. p
16,300.00 p
47.00 p
16557
FESCUE
Aug-14
500.00 (CY)
8.489
9/3/14
46.33 (W)
0.787
121.57
0.170
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
Sep-14
46.33 (W)
0.787
9/2/14
308.00 (CY)
5.229
16.34
0.720
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
I FESCUE
9/3/14
476.00 (CY)
8.081
16.34
1.112
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
I FESCUE
9/4/14
84.00 (CY)
1.426
16.34
0.196
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
FESCUE
Sep-14
868.00 (CY)
14.736

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: APPLING
OWNER: CLAUDE LYNCH JR PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 232.13
SITE #: NCAM00022 3��LD#:AM000220001 OPERATOR: CLAUDE LYNCH, JR CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 58.90 ACRES PERMITTED: 58.90
Page: 2
Lime Applied ***
Date Lbs/Ac
3allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 3.30
Total Cubic Yds/Ac: 23.23
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
110
Annual lbs/acre
0.037
0.016
0.381
2.726
0.180
0.007
0.067
0.232
0.039
22.302
240.66
Cumulative lbs/acre
0.147
0.048
1.527
10.429
0.631
0.027
0.251
0.633
0.138
97.081
77777771­�
1
''e
-v Iff
Z�
158
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1
1339.0
267.9
15.0 375.0
89.0
2500.0
7
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X 144 al 2-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A= Not Applicable NR =Not Reported or Not Required % = percent p = ppm or mg/lcg Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0
Application Method: SUR-Surface, INJ -Injection, SURIN -Incorporation See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: CLAUDE LYNCH, JR
SITE #: NC AM 00022 FIELD# : AM 00022 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 59.96
OPERATOR: CLAUDE LYNCH, JR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.00 ACRES PERMITTED: 18.00
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) orCubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
9/4/14.
22.56 (W)
1.253
21.57
0.270
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
9/5/14
23.17 (W)
1.287
21.57
0.278
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
Sep-14
45.73 (W)
2.540
9/4/14
252.00 (CY)
14.000
16.34
1.927
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
I FESCUE
9/5/14
112.00 (CY)
6.222
16.34
0.856
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
FESCUE
Sep-14
364.00 (CY)
20.222
Total Wet Tons/Ac: 2.54
Total Cubic Yds/Ac: 20.22
-
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
95
Annual lbs/acre
0.031
0.013
0.348
2.422
0.162
0.008
0.061
0.209
0.033
18.814 206.87
Cumulative lbs/acre
0.121
0.128
93.450 E=
0.042
1.532
9.254
0.625
0.033
0.246
0.625
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
ss
"1• t4
•
•n
Wk
.a •
169
,
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: CLAUDE LYNCH, JR
SITE #: NC AM 00022 FIELD# : AM 00022 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 34.68
OPERATOR: CLAUDE LYNCH, JR CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 23.70 ACRES PERMITTED: 23.70
Page : I
Lune Applied ***
Date J LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
9/2/14
196.00 (CY)
8.270
16.34
1.138
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
I FESCUE
9/4/14
56.00 (CY)
2.363
16.34
0.325
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
56,900. p
14,900.00 p
857.00 p
16707
1 FESCUE
Sep-14
1 252.00 (CY)
10.633
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 10.63
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
49
Annuallbs/acre
0.012
0.006
0.170
1.209
0.070
0.004
0.029
0.094
0.015
9.833
108.28
Cumulative Ibs/acre
0.051
0.014
0,520
3.510
0.218
0.012
0.080
0.222
0.044
32.953
....:.:......
.r.��
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
?
w= ._
r.,
s.
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0:a`,£. '
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
XW/'ow,C> 2//0 lfl/ f
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the infornation submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: REBECCA JEFFERIES
SITE #: NC AM 00025 FIELD# : AM 00025 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: DURHAM
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 176.97
OPERATOR: ROGER TATE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 55.70 ACRES PERMITTED: 55.70
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(PP-)
Crop
MONTH
Total
Per Acre
Solids
7/15/14
100.00 (CY)
1.795
16.80
0.254
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
F 16557
I FESCUE
7/17/14
560.00 (CY)
10.054
16.80
1.423
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
I FESCUE
7/18/14
420.00 (CY)
7.540
16.80
1.067
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16117
FESCUE
Jul-14
1,080.00 (CY)
19.389
8/5/14
95.60 (W)
1.716
21.57
0.370
DBWPC
MOIST
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
Aug-14
95.60 (W)
1.716
8/5/14
25.00 (CY)
0.449
116.80
0.064
DSDANDC
MOIST
0-<1/2"
SUR
0.5
0.20
58,100. p
16,300.00 p
7.00 p
16557
FESCUE
Aug-14
25.00 (CY)
0.449
Total Wet Tons/Ac: 1.72
Total Cubic Yds/Ac: 19.84
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS: ,
94
Annuallbs/acre
0.028
0.013
0.281
2.166
0.126
0.004
0.049
0.167
0.032
20.005
209.47
Cumulative lbs/acre
0.050
0.023
0.544
3.970
0.217
0.010
0.097
0.274
0.059
36.594
$a
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
194
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
Lt_:
1339.0
267.9
15.0 375.0
89.0
2500.0i'L
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
DBWPC = DURHAM, NC BROWN WTP CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
s Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 207.57
SITE #: NC GR 00005 FIELD# : GR 00005 0001 OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5 1. 10 ACRES PERMITTED: 51.10
Page: 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/21/14
76.86 (W)
1.504
20.18
0.304
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
10/22/14
51.77 (W)
1.013
20.18
0.204
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
10/29/14
23.23 (W)
0.455
20.18
0.092
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
10/31/14
47.58 (W)
0.931
20.18
0.188
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.Op
4,410.00 p
30.20 p
2731
FESCUE
Oct-14
199.44 (W)
3.903
10/21/14
445.00 (CY)
8.708
15.05
1.104
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
I FESCUE
10/22/14
358.00 (CY)
7.006
15.05
0.888
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
I FESCUE
10/23/14
109.00 (CY)
2.133
15.05
0.270
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
I FESCUE
10/28/14
190.00 (CY)
3.718
15.05
0.471
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
I FESCUE
10/29/14
218.00 . (CY)
4.2661
15.05
0.541
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
1,320.00 (CY)l
25.831

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 207.57
SITE #: NC GR 00005 FIELD# : GR 00005 0001 OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 5 1. 10 ACRES PERMITTED: 51.10
Page : 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 3.90
Total Cubic Yds/Ac: 25.83
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
116
Amoral lbs/acre
0.055
0.026
0.341
2.572
0.231
0.008
0.060
0.227
0.041
20.477
217.47
Cumulative lbs/acre
0.110
0.060
1.418
8.370
1.039
0.021
0.344
0.621
0.290
45.492
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
°.,
; ,
.. , ` ;,
�.. ,
145
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
i
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for luiowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 170.77
SITE #: NC GR 00005 FIELD# : GR 00005 0002 OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 39.00 ACRES PERMITTED: 39.00
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
"�o
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppin)
Crop
MONTH
Total
Per Acre
Solids
6/26/14
22.98 (W)
0.589
20.82
0.123
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
I FESCUE
6/27/14
46.81 (W)
1.200
20.82
0.250
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
FESCUE
Jun-14
1 69.79 (W)
1.789
6/25/14
128.00 (CY)
3.282
17.05
0.471
DSDANDC
DRY
0-<I/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I FESCUE
6/26/14
512.00 (CY)
13.128
17.05
1.885
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I FESCUE
6/27/14
448.00 (CY)
11.487
17.05
1.650
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
11411
FESCUE
Jun-14
1,088.00 (CY)
27.897
Total Wet Tons/Ac: 1.79
1 oUlll1101C xQSHG: L79U
As
Cd
Cr
Cu
Ph
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual Ibs/acre
0.053
0.018
0.389
2.711
0.181
0.007
0.084
0.234
0.060
27.064
307.60
125
Cumulative lbs/acre
0.128
0.071
2.104
10.325
1.459
0.023
0.509
0.970
0.364
55.209
Z �
vl
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
-
*
145
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X s
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: HENRY THORPE
SITE #: NC GR 00005 FIELD# : GR 00005 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: VANCE
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 365.85
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 94.30 ACRES PERMITTED: 94.30
Page
Lime Applied ***
Date
LWAc
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
6/30/14
45.85 (W)
0.486
20.82
0.101
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
1848
FESCUE
Jun-14
45.85 (W)
0.486
6/30/14
416.00 (CY)
4.411
17.05
0.633
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
FESCUE
Jun-14
416.00 (CY)
4.411
7/1/14
21.81 (W)
0.231
21.57
0.050
DBWPC
DRY
0-<1/2"
SUR
0.5.
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
7/1/14
50.00 (CY)
0.530
21.57
0.096
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
7/2/14
50.00 (CY)
0.530
21.57
0.096
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
Jul-14
121.81 (CY)
1.291
7/1/14
350.00 (CY)
3.712
16.80
0.525
DSDANDC
DRY
0-<1/2"
SUR
6.5
0.20
58,100. p
16,300.00 p
47.00 p
16557
FESCUE
7/2/14
275.00 (CY)
2.916
16.80
0.413
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100. p
16,300.00 p
47.00 p
16557
FESCUE
Jul-14
625.00 (CY)
6.628
10/24/14
23.59 (W)
0.250
20.18
0.050
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
Oct-14
23.59 (W)
0.250
10/23/14
162.00 (CY)
1.718
15.05
0.218
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
10/24/14
467.00 (CY)
4.952
15.05
0.628
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
10/27/14
477.00 (CY)
5.058
15.05
0.641
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
10/28/14
318.00 (CY)
3.372
15.05
0.427
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
1,424.00 (CY)
15.100

FACILITY NAME: DURHAM, NC
OWNER: HENRY THORPE
SITE #: NC GR 00005 FIELD#: GR 00005 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: VANCE
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 365.85
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 94.30 ACRES PERMITTED: 94.30
Page: 2
Lane Applied ***
Date Lbs/Ac
3allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond. -
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 0.97
i otai t_uoic Y us/Ac: :47.ZU
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.044
0.016
0.345
2.344
0.190
0.007
0.062
0.208
0.041
22.874
245.33
118
Cumulative lbs/acre
0.078
0.029
0.679
4.383
1 0.337
1 0.014
0.109
1 0.389
0.075
42.931
-hu-4
1
1
145
Permit PAN Limit (lbs/acre) I st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DB)ATC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
X d) -Z
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % = percent p = pp- or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR-Surface, INJ-hijection,SURIN-hicorporation See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: HENRY THORPE
SITE #: NC GR 00005 FIELD#': GR 00005 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: ENON
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 168.32
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 44.90 ACRES PERMITTED: 44.90
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppni)
Crop
MONTH
Total
Per Acre
Solids
6/23/14
512.00 (CY)
11.403
17.05
1.637
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I FESCUE
6/25/14
480.00 (CY)
10.690
17.05
1.535
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
FESCUE
Jun-14
992.00 (CY)
22.093
10/23/14
24.56 (W)
0.547
20.18
0.110
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
Oct-14
24.56 (W)
0.547
10/23/14
165.00 (CY)
3.6751
15.05
0.466
DNDAND(
DRY
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
165.00 (CY)
3.675
Total Wet Tons/Ac: 0.55
i Uwi %-'U", 1 uyr"c: W.
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
115
0.046
0.016
0.340
2.478
0.153
0.006
0.072
0.204
0.050
24.296
273.96
Cumulative hbs/acre
0.085
0.032
0.732
4.869
0.326
0.015
0.127
0.415
0.089
47.820
M
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
zw
145
Y
r
a
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
'
1339.0
2679
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
X J& odozf�l_;-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: HENRY THORPE
SITE #: NC GR 00005 FIELD# : GR 00005 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 165.57
OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 28.60 ACRES PERMITTED: 28.60
Page
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/28/14
22.77 (W)
0.796
20.82
0.166
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
FESCUE
May-14
1 22.77 (W)
0.796
5/28/14
608.00 (CY)
21.259
17.05
3.053
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I FESCUE
5/29/14
512.00 (CY)
17.902
17.05
2.571
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
11411
FESCUE
May-14
1,120.00 (CY)
39.161
Total Wet Tons/Ac: 0.80
1 otffi %,uuie r us/Hc: 39.10
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.070
0.023
0.526
3.764
0.226
0.009
0.114
0.312
0.080
37.931
431.09
175
Cumulativelbs/acre
0.107
0.038
0.898
6.035
0.390
0.017
0.166
0.513
0.118
60.261
211
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop,
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
s3
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: HENRY THORPE PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 54.97
SITE #: NC GR 00005 FIELD# : GR 00005 0006 OPERATOR: HENRY THORPE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 11.90 ACRES PERMITTED: 11.90
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons
Cond.
Precip.
cation
till-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
6/2/14
87.45 (W)'
7.349
20.82
1.530
DBWPC
DRY
0- 1/2"
SUR
0.5
0.26
7,780.0 p
961.00 p
3.36 p
1848
FESCUE
Jun-14
87.45 (W)
7.349
6/2/14
256.00 (CY)
21.5131
17.05
3.089
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
FESCUE
Jun-14
256.00 (CY)
21.513
JDSDANDC
I
1
-
1
1
1
Total Wet Tons/Ac: 7.35
!ULM I.UUIU IUyjw: LL,1
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.058
0.018
0.367
2.235
0.234
0.006
0.077
0.240
0.059
21.081
239.64
101
Cumulative lbs/acre
0.086
0.029
0.642
3.914
0.355
0.012
.0.116
0.389
0.086
37.595
Fan,
,
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
,
€
194
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.01
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to -assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including thepossibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -,Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: MILTON LATTA & SONS DAIRY
SITE #: NC OR 00001 FIELD# : OR 00001 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 73.39
OPERATOR: BILLY LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.00 ACRES PERMITTED: 15.00
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/14/14
21.43 (W)
1.429
20.82
0.297
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
1848
SORGHUM
May-14
21.43 (W)
1.429
5/12/14
224.00 (CY)
14.933
17.05
2.144
DSDANDC
DRY
0-<I/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I SORGHUM
5/13/14
224.00 (CY)
14.933
17.05
2.144
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485 I
SORGHUM
5/14/14
32.00 (CY)
2.133
17.05
0.306
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
SORGHUM
May-14
480.00 (CY)
31.999
Total Wet Tons/Ac: 1.43
1 Oral LuDic Y as/AC: SL.UU
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.059
0.020
0.439
3.095
0.197
0.008
0.095
0.262
0.067
31.022 352.58
143
Cumulative lbs/acre
0.086
0.030
0.683
5.203
0.441
0.023
0.166
0.375
0.097
36.093
1
1
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
"'
t"
? r
223
`v
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 :. 375.0
89.0
2500 0 ) N.
-,Y :'
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
K Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: MILTON LATTA & SONS DAIRY
SITE #: NC OR 00001 FIELD# : OR 00001 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 63.34
OPERATOR: BILLY LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 8.10 ACRES PERMITTED: 8.10
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/12/14
39.37 (W)
4.860
20.82
1,012
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.Op
961.00 p
3.36 p
F 1848
SORGHUM
May-14
39.37 (W)
4.860
5/12/14
384.00 (CY)
47.4071
17.05
6.808
DSDANDC
DRY
i
0-<I/2"
SUR
i
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
SORGHUM
May-14
384.00 (CY)
47.407
Total Wet Tons/Ac: 4.86
m orai t umc Y Us/Hc: 47.41
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.096
0.031
0.681
4.651
0.336
0.012
0.146
0.416
0.105
46.056
523.46
215
r
Cumulative lbs/acre
0.137
0.045
1 1.008
7.525
1 0.640
0.030
0.238
1 0.577
0.153
52.791
"
Permit PAN Limit (lbs/acre) 1st Crop/2nd CropF
mt223
,4n
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L,
1339.0
267.9
15.0 375.0
89.0
2500.0 =t
_
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are, significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: MILTON LATTA & SONS DAIRY
SITE #: NC OR 00001 FIELD# : OR 00001 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 41.36
OPERATOR: BILLY LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.10 ACRES PERMITTED: 6.10
Page : 1
Lane Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pptn)
Crop
MONTH
Total
Per Acre
Solids
5/13/14
288.00 (CY)
47.213
17.05
6.780
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
F 15485
SORGHUM
May-14
1 288.00 (CY)
47.213
1
1
Total Wet Tons/Ac:
1 Uiai I.UUIU iUWPIU. 4/.L1
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
210
0.081
0.027
0.624
4.515
0.258
0.011
0.136
0.366
0.095
45.696
519.33
Cumulative lbs/acre
0.094
1 0.032
1 0.724
1 5.411
1 0.354
1 0.016
0.172
1 0.417
0.105
47.969
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
A..
...
-
223
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
(
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, [NJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: MILTON LATTA & SONS DAIRY
SITE #: NC OR 00001 FIELD# : OR 00001 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 124.07
OPERATOR: BILLY LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 18.10 ACRES PERMITTED: 18.10
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/13/14
256.00 (CY)
14.144
17.05
2.031
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
I SORGHUM
5/14/14
608.00 (CY)
33.591
17.05
4.824
DSDANDC
DRY
0-<I/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
SORGHUM
May-14
864.00 (CY)
47.735
Total Wet Tons/Ac:
1 oral uuoic Y a&Ac: 47.73
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.082
0.027
0.631
4.565
0.260
0.011
0.137
0.370
0.096
46.201
525.07
212
Cumulative lbs/acre
0.103
0.036
0.843
6.238
0.461
0.023
0.199
0.466
0.124
50.350
�:',
k� ;� ' ,., . '• "
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
223
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 i 375.0
89.0
2500.0
,"
DSDANDC = DURHAM, NC S. DURHAM W WTP ANAEROB. DIGESTED CAKE
x A &,a 0210 #/ !,�-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: LIGNUM
OWNER: DAVID WALKER PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 10.61
SITE #: NC OR 00005 FIELD# : OR 00005 0001 OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 2.70 ACRES PERMITTED: 2.70
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Prebip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/7/14
75.00 (CY)
27.778
16.80
3.930
DSDANDC
DRY
0- 1/2"
SUR
0.5
0.20T�]
16,300.00 p
1 47.00 p
16557
SOYBEANS
Jul-14
75.00 (CY)
27.778
Total Wet Tons/Ac:
fouti t_uoic Y as/Ac: L7.75
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.031
0.016
0.369
2.916
0.149
0.005
0.063
0.204
0.039
27.906
292.42
130
Cumulative lbs/acre
0.049
1 0.026
1 0.651
1 4.295
1 0.303
0.008
0.122
1 0.352
0.059
29.971
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
135
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X�4&d2�eP 4//.f'_
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: DAVID WALKER
SITE #: NC OR 00005 FIELD# : OR 00005 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 17.69
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 6.40 ACRES PERMITTED: 6.40
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppnt)
Crop
MONTH
Total
Per Acre
Solids
7/7/14
75.00 (CY)
11.719
16.80
1.658
DSDANDC
DRY
0-<1/2"
SUR
0.5
.0.20
58,100.p
16,300.00 p
47.00 p
16557
ORCHARDGRASS
7/8/14
50.00 (CY)
7.813
16.80
1.105
DSDANDC
DRY
0-<I/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
ORCHARDGRASS
Jul-14
1 125.00 (CY)
19.532
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 19.53
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
92
Annual Ibs/acre
0.022
0.011
0.260
2.051
0.105
0.003
0.044
0.144
0.028
19.621
205.61
Cumulative lbs/acre
0.031
0.013
0.315
2.446
0.161
0.005
0.069
0.173
0.034
19.631
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
169
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X a24
(SIGNATURE OF LAND APPLIER) DATE
"I certify, tinder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 '
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: DAVID WALKER
SITE #: NC OR 00005 FIELD# : OR 00005 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 24.76
OPERATOR: DAVID WALKER CATION EXCHANGE CAPAC]TY (NON-503):
ACRES UTILIZED: 8.00 ACRES PERMITTED: 8.00
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/7/14
125.00 (CY)
15.625
16.80
2.211
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
I SOYBEANS
7/8/14
50.00 (CY)
6.250
16.80
0.884
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
SOYBEANS
Jul-14
1 175.00 (CY)
21.875
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 21.88
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
102
Annuallbs/acre
0.025
0.012
0.291
2.297
0.118
0.004
0.050
0.161
0.031
21.976
230.28
Cumulativelbs/acre
0.040
0.020
0.499
3.355
0.240
0.006
0.098
0.270
0.046
23.373
1st Crop/2nd Crop"
'}
169
Permit PAN Limit (lbs/acre)
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
x All /,600/t_ e)�d '-//j
(SIGNATURE OF LAND APPLIER) DATE
"I certify, tinder penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: DAVID WALKER
SITE #: NC OR 00005 FIELD# : OR 00005 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 31.84
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 9.80 ACRES PERMITTED: 9.80
Page : 1
Lime Applied ***
Date::T Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Total
Per Acre
Solids
7/8/14
225.00 (CY)
22.959
16.80
3.249
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100. p
16,300.00 p
47.00 p
16557
SOYBEANS
Jul-14
225.00 (CY)
22.959
Total Wet Tons/Ac:
dotal cubic Yos/Ac: 22.96
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.026
0.013
0.305
2.410
0.123
0.004
0.052
0.169
0.032
23.065
_F
241.70
108
Cumulative lbs/acre
0.041
1 0.021
0.523
1 3.510
1 0.250
0.006
0.101
0.283
0.048
24.547
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
159
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X Z JID 4/ (A 0Z1,r),y1,.r
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: DAVID WALKER
SITE #: NC OR 00005 FIELD# : OR 00005 0007
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 21.22
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 5.50 ACRES PERMITTED: 5.50
Page: 1
Lime Applied ***
Date Lbs/Ae
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pptn)
Crop
MONTH
Total
Per Acre
Solids
7/8/14
50.00 (CY)
9.091
16.80
1286
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
F 16557
I FESCUE
7/9/14
100.00 (CY)
18.182
16.80
2.573
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
1 FESCUE
Ju1-14
1 150.00 (CY)
27.273
Total Wet Tons/Ac:
roratt—unic zas/Ac: 27.27
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.031
0.015
0.363
2.863
0.147
0.005
0.062
0.201
0.039
27.399
287.11
128
Cumulative lbs/acre
0.058
0.028
1 0.666
1 5.166
0.486
0.014
0.164
1 0.359
0.090
32.501
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
158
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
XAvh/,Oi�o 210
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
*** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: RONALD WALKER
SITE #: NC OR 00006 FIELD# : OR 00006 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 318.73
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 62.40 ACRES PERMITTED: 62.40
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Mine
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili=
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
7/10/14
25.53 (W)
0.409
21.57
0.088
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
I FESCUE
7/11/14
200.00 (CY)
3.205
21.57
0.582
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20'
7,740.0 p
881.00 p
16.20 p
1829
I FESCUE
7/14/14
20.69 (W)
0.332
21.57
0.072
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0 p
881.00 p
16.20 p
1829
FESCUE
Jul-14
246.22 (W)
3.946
7/10/14
375.00 (CY)
6.010
16.80
0.850
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
(FESCUE
7/11/14
325.00 (CY)
5.208
16.80
0.737
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
I FESCUE
7/14/14
425:00 (CY)
6.811
16.80
0.964
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
FESCUE
7/15/14
150.00 (CY)
2.404
16.80
0.340
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100:p
16,300,00 p
47.00 p
16557
FESCUE
Jul-14
1,275.00 (CY)
20.433
10/8/14
399.00 (CY)
6.394
15.05
0.811
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
10/9/14
327.00 (CY)
5.240
15.05
0.664
DNDANDC
DRY
0-<1/2"
SUR
•0.5
0.20
60,100. p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
726.00 (CY)
11.634

FACILITY NAME: DURHAM, NC
OWNER: RONALD WALKER
SITE #: NC OR 00006 FIELD# : OR 00006 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: W00003504
OPERATOR: DAVID WALKER
ANNUAL DRY TONS APPLIED: 318.73
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 62.40 ACRES PERMITTED: 62.40
Page : 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-
. or Wet Tons (WTEn
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Solids
Total Wet Tons/Ac: 0.74
t Wal Cum; x us/tic. 35.27
--
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
149
0.053
0.020
0.445
3.173
0.231
0.008
0.077
0.272
0.051
29.822
313.70
Cumulative lbs/acre
0.129
0.114
1.097
7.476
0.542
0.018
0.234
0.559
0.148 •
40.492
.
-
__f
Permit PAN Limit (lbs/acre) 1st Cro /2nd Croppzv
i�
`
"°.'
)
" '"
�. t?€'L'„^ai`G" q ✓ . ".».y ,yF
t."i" ""
;go-, $ .";.a ; ky„ 'i'A ."' Xy....i
`
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
"
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM W WTP ANAEROB. DIGESTED CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
x 4xlt�Gy D2�61/�S
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface0.5, hijection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: RONALD WALKER
SITE #: NC OR 00006 FIELD# : OR 00006 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 65.64
OPERATOR: DAVID WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 10.20 ACRES PERMITTED: 10.20
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
Win)
Crop
MONTH
Total
Per Acre
Solids
7/9/14
175.00 (CY)
17.157
21.57
3.117
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
r 1829
I FESCUE
7/10/14
50.00 (CY)
4.902
21.57
0.891
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
Jul-14
1 225.00 (CY)
22.059
7/9/14
125.00 (CY)
12.255
16.80
1.734
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100.p
16,300.00 p
47.00 p
16557
(FESCUE
7/10/14
50.00 (CY)
4.902
16.80
0.694
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,100. p
16,300.00 p
47.00 p
16557
FESCUE
Jul-14
175.00 (CY)
17.157
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 39.22
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
95
Annual lbs/acre
0.084
0.026
0.413
2.699
0.301
0.000
0.079
0.351
0.064
18.054
187.43
Cumulative lbs/acre
0.225
0.074
1.251
1 8.921
1 0.896
0.033
0.256
0.861
0.207
1 31.439
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
158
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
x aw &�: .,Oz�aw/
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
k Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: FAIRCREST LAND & CATTLE
SITE #: NC OR 00070 FIELD# : OR 00070 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: APPLING
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 125.36
OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 30.00 ACRES PERMITTED: 30.00
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Total
Per Acre
Solids
9/22/14
138.69 (W)
4.623
21.57
0.997
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
Sep-14
138.69 (W)
4.623
9/16/14
168.00 (CY)
5.600
15.05
0.710
DNDANDC
MOIST
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
(FESCUE
9/22/14
504.00 (CY)
16.800
15.05
2.129
DNDANDC
DRY
0-<I/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
IFESCUE
9/23/14
81.00 (CY)
2.700
15.05
0.342
DNDAND(
DRY
0-<I/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Sep-14
753.00 (CY)
25.100
1
Total Wet Tons/Ac: 4.62
lorai uuntc Yas/Ac: 25.0
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.054
0.017
0.345
2.081
0.230
0.008
0.061
0.228
0.042
19.929
211.68
112
Cumulative lbs/acre
0.707
0.295
12.454
44.303
6.547
0.234
3.109
4.801
0.656
364.948
1
°"
177
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hnjection/hncorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: FAIRCREST LAND & CATTLE
SITE #: NC OR 00070 FIELD# : OR 00070 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HELENA
PERMIT #: , W00003504 ANNUAL DRY TONS APPLIED: 75.60
OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 28.40 ACRES PERMITTED: 28.40
Page : I
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppnl)
Crop
MONTH
Total
Per Acre
Solids
10/6/14
22.89 (W)
0.806
1 20.18
0.163
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0p
4,410.00 p
30.20 p
7731
FESCUE
Oct-14
22.89 (W)
0.806
10/6/14
560.00 (CY)
19.718
15.05
2.499
DRY
1 0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
1 17101
1 FESCUE
Oct-14
560.00 (CY)
19.718
IDNDAND(
Total Wet Tons/Ac: 0.81
Total Cubic Yds/Ac: 19.72
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
86
Annuallbs/acre
0.033
0.013
0.242
1.596
0.150
0.006
0.042
0.145
0.027
15.533
165.24
Cumulative lbs/acre
0.643
0.358
10.065
37.442
6.223
0.174
2.128
4.272
0.509
272.624
163
Permit PAN Limit (lbs/acre) I st Crop/2nd Crop
a
FD Cumulative Pollutant Loading Rate Limit lbs/acre2500.0
g ( )
36.6
34.8
1339.0
267.9
15.0 ." 375.0
89.0
,
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM W WTP ANAEROB. DIGESTED CAKE
XIME.W�L
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable' NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: VANCE
OWNER: FAIRCREST LAND & CATTLE PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 108.27
SITE #: NC OR 00070 FIELD# : OR 00'070 0003 OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 33.50 ACRES PERMITTED: 33.50
Page,: 1
Lime Applied ***
Date Lbs/Ac.,
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/6/14
49.76 (W)
1.485
20.18
0.300
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
F 2 331
I FESCUE
10/7/14
72.22 (W)
2.156
20.18
0.435
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
Oct-14
121.98 (W)
3.641
10/7/14
660.00 (CY)
19.7011
15.05
2.497
DNDANDC
DRY
1 0-<1/2"
SUR
0.5
0.20
60,100. p
14,900.00 p
611.00 p
1 17101
FESCUE
Oct-14
660.00 (CY)
19.701
Total Wet Tons/Ac: 3.64
total Cubic Yds/AC: 19.7U
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.045
0.022
0.266
2.074
0.184
0.007
0.047
0.182
0.032
15.648
166.09
89
Cumulative lbs/acre
0.539
0.389
11.408
37.051
4.982
0.346
1.948
5.152
0.585
268.310
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop_
a.
188
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: FAIRCREST LAND & CATTLE
SITE #: NC OR 00070 FIELD# : OR 00070 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HERNDON
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 73.37
OPERATOR: WOLFGANG LOTZ CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 27.00 ACRES PERMITTED: 27.00
Page
Line Applied
***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
9/23/14
43.98 (W)
1.629
21.57
0.351
DBWPC
DRY
0-<I/2"
SUR
0.5
0.20
7,740.0p
881.00 p
16.20 p
1829
FESCUE
Sep-14
43.98 (W)
1.629
9/23/14
504.00 (CY)
18.6671
15.05
2.366
DRY
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Sep-14
504.00 (CY)l
18.667
IDNDAND(
I
1
1
1
1
Total Wet Tons/Ac: 1.63
i uL uvi� 1 uyAu. 1a.0 /
,
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
82
.
0:034
0.011
0.239
1.461
0.151
0.006
0.041
0.147
0.027
14.742
156.76
Cumulative lbs/acre
0.623
0.339
11.623
40.678
4.454
0.310
1.831
5.368
0.613
353.860
00
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop"
t £
r
N'
N=r
)7
""
122
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
t
1339.0
267.9
15.0 « ; 375.0
89.0
2500 0 `
MI L
_7
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
x
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: , Surface 0.5, hijection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: WILLIAM BREEZE, SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0009
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 45.95
OPERATOR: WILLIAM LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.80 ACRES PERMITTED: 15.10
Page: 1
Lime Applied ***
Date Lbs Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/19/14
320.00 (CY)
41.026
17.05
5.891
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
1 25.20 p
11415
1 SORGHUM
May-14
320.00 (CY)
41.026
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 41.03
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.071
0.024
0.542
3.924
0.224
0.009
0.118
0.318
0.082
39.707
451.27
182
Cumulative lbs/acre
0.388
0.128
6.512
1 20.668
3.254
0.054
0.906
1 2.287
0.347
151.371
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate.Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: WILLIAM BREEZE, SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0010
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 137.86
OPERATOR: WILLIAM LATTA CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 22.40 ACRES PERMITTED: 22.40
Page: 1
Litne Applied ***
Date:�:T Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/15/14
32.00 (CY)
1.429
17.05
0.205
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
F 15485
I SORGHUM
5/19/14
352.00 (CY)
15.714
17.05
2.257
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400.p
14,600.00 p
25.20 p
15485
I SORGHUM
5/20/14
576.00 (CY)
25.714
17.05
3.693
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
11415
SORGHUM
May-14
960.00 (CY)l
42.857
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 42.86
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.074
0.025
0.566
4.099
0.234
0.010
0.123
0.332
0.086
41.480
471.42
191
Cumulative Ibs/acre
0.437
0.137
8.012
1 23.241
1 3.180
0.067
1.011
2.525
0.389
173.078
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
223
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
f
I
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X Ok=--
o2 Li��_�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: WILLIAM BREEZE, SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0012
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 41.36
OPERATOR: PERCY HESTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 12.20 ACRES PERMITTED: 12.20
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/15/14
192.00 (CY)
15.738
17.05
2.260
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
CORN
5/19/14
96.00 (CY)
7.869
17.05
1.130
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
CORN
May-14
1 288.00 (CY)
23.607
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 23.61
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.041
0.014
0.312
2.258
0.129
0.005
0.068
0.183
0.047
22.848
259.67
105
Cumulative lbs/acre
0.502
1 0.177
1 9.940
1 30.905
1 4.014
1 0.090
1.076
1 2.777
0.318
173.291
Permit PAN Limit (lbs/acre) Ist Crop/2nd Crop
132
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X4iz
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I our aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: WILLIAM BREEZE, SR.
SITE #: NC OR 00076 FIELD# : OR 00076 0014
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 18.38
OPERATOR: PERCY HESTER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.90 ACRES PERMITTED: 15.20
Page: I
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TICN
Nitrogen
and
(ppnm)
Crop
MONTH
Total
Per Acre
Solids
5/15/14
128.00 (CY)
26.122
17.05
3.751
DSDANDC
DRY
0-<1/2"
SUR
0.5
0.20
55,400. p
14,600.00 p
25.20 p
15485
CORN
May-14
128.00 (CY)
26.122
Total Wet Tons/Ac:
lbtal Cubic Yds/Ac: 26.12
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annuallbs/acre
0.045
0.015
0.345
2.498
0.143
0.006
0.075
0.203
0.053
25.283
287.34
116
Cumulative Ibs/acre
0.561
0.185
11.065
31.694
4.054
0.083
1.278
1 3.431
0.463
219.728
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
132
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0, 375.0
89.0
2500.0
DSDANDC = DURHAM, NC S. DURHAM WWTP ANAEROB. DIGESTED CAKE
X G� oziD�f�1.5"�
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: LARRY & DEBORAH WALKER
SITE #: NC OR 00091 FIELD# : OR 00091 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: HIWASSEE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 36.68
OPERATOR: LARRY & DEBORAH WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 7.90 ACRES PERMITTED: 7.90
Page : 1
Lane Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/9/14
25.38 (W)
3.213
20.18
0.648
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
Oct-14
25.38 (W)
3.213
10/9/14
249.00 (CY)
31.519
15.05
3.995
DNDAND(
DRY
i
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
249.00 (CY)
31.519
I
Total Wet Tons/Ac: 3.21
r otat uuoic Y as/Ac: 3L�L
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.061
0.026
0.403
2.877
0.263
0.010
0.070
0.257
0.046
24.916
264.81
140
Cumulative Ibs/acre
0.306
1 0.102
1 4.196
1 13.429
1 1.653
0.065
0.623
1 1.497
0.242
117.282
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
t
*w.
?
198
-�f
FD Cumulative Pollutant LoadingRate Limit lbs/acre.»
( )
36.6
34.8
ry"
`' �
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM W WTP ANAEROB. DIGESTED CAKE
Xoe4z
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: LARRY & DEBORAH WALKER
SITE #: NC OR 00091 FIELD# : OR 00091 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 3.55
OPERATOR: LARRY & DEBORAH WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 1.60 ACRES PERMITTED: 1.60
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/9/14
28.00 (CY)
17.500
15.05
2.218
DNDAND(
DRY
0-<1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
28.00 (CY)
17.500
Total Wet Tons/Ac:
Total Cubic Yos/Ac: 17.5U
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.027
0.009
0.209
1.295
0.124
0.005
0.035
0.120
0.022
13.753
146.40
76
Cumulative lbs/acre
0.091
0.037
1.738
3.939
0.756
0.025
0.235
0.702
0.081
27.486
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
211,
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
I
1339.0
267.9
15.0
375.0
89.0
2500.0
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: LARRY & DEBORAH WALKER
SITE #: NC OR 00091 FIELD# : OR 00091 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 10.65
OPERATOR: LARRY & DEBORAH WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 4.10 ACRES PERMITTED: 4.10
Page : 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
. TKN
Nitrogen
and
(ppni)
Crop
MONTH
Total
Per Acre
Solids
10/10/1.4
84.00 (CY)
20.488
15.05
2.597
DNDANDC
DRY
0 <1/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
84.00 (CY)
20.488
Total Wet Tons/Ac:
I Vial 1.U01G I MVIAU. LU.4Y
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.031
0.010
0.244
1.517
0.145
0.006
0.042
0.140
0.026
16.101
171.40
89
Cumulative Ibs/acre
0.238
0.084
3.518
13.682
1.680
0.065
0.631
1.586
0.245
119.718
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
^
2 11
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
"'c 's. • ` F `
1339.0
267.9
15.0 375.0
89.0
2500.0 +
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
X 26
(SIGNATURE OF LAND APPLIER) DATE lr
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: LARRY & DEBORAH WALKER
SITE #: NC OR 00091 FIELD# : OR 00091 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: GEORGEVILLE
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 42.59
OPERATOR: LARRY & DEBORAH WALKER CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 11.00 ACRES PERMITTED: 11.00
Page: 1
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
"�"
Tons
Cond.
Precip.
cation
till-
all-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
10/10/14
336.00 (CY)
30.545
15.05
3.872
DNDANDC
DRY
0-<I/2"
SUR
0.5
0.20
60,100.p
14,900.00 p
611.00 p
17101
FESCUE
Oct-14
336.00 (CY)
30.545
1
Total Wet Tons/Ac:
i vial
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
P
PAN
TOTALS:
Annual lbs/acre
E24.005
132
0.046
0.015
0.364
2.261
0.217
0.009
0.062
0.209
0.039
255.54
Cumulative lbs/acre
0.184
0.057
2.176
11.692
1.179
0.050
0.466
1.158
0.194
106.192`�;;�•
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
,.
.>w
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DNDANDC = DURHAM, NC N. DURHAM W WTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page : 1
Lune Applied ***
FACILITY
NAME: DURHAM, NC
ANNUAL DRY TONS APPLIED:
401.60
Date LbsAc
OWNER:
SIDNEY THOMPSON
PERMIT #:
W00034195
SITE #:
NC PS 00001 FIELD#
: PS 00001
0001
OPERATOR:
SIDNEY THOMPSON
CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL
SOURCE(S):* See list at bottom of report
OLD FIELD #:
ACRES UTILIZED: 100.20
ACRES PERMITTED:
100.20
allons (G) or Cubic Yards (CY)
Dr, Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (VM (specify)
Tons Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per Residual Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total Per Acre
Solids
3/27/14
87.08 (W)
0.869
19.49
,0.169 DBWPC DRY
0-<1/2"
SUR
0.5
0.20
8,210.0 p
975.00 p
6.67
p
1941
I FESCUE HAY
3/28/14
23.51 (W)
0.235
19.49
0.046 DBWPC DRY
0-<1/2"
SUR
0.5
0.20
8,210.0 p
975.00 p
6.67
p
1941
FESCUE HAY
3/31/14
18.76 (W)
0.187
19.49
0.036 DBWPC DRY
0-<1/2"
SUR
0.5
0.20
8,210.0 p
975.00 p
6.67
p
1941
FESCUE HAY
Mar-14
129.35 (W)
1.291
3/27/14
256.00 (CY)
2.555
15.18
0.327 DNDANDC DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20
p
16205
I FESCUE HAY
3/28/14
480.00 (CY)
4.790
15.18
0.612 DNDAND( DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20
p
16205
I FESCUE HAY
3/31/14
992.00 (CY)
9.900
15.18
1.266 DNDANDC DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20
p
16205
FESCUE HAY
Mar-14
1,728.00 (CY)
17.245
•4/1/14
128.00 (CY)
1.277
15.18
0.163 DNDANDC DRY
0-<1/2"
SUR
0.5
0.20
5$,000: p
15,300.00 p
15.20
p
16205
FESCUE HAY
4/14/14
704.00 (CY)
7.026
15.18
j
0.898 DNDANDC DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20
p
16205
I FESCUE HAY
4/17/14
384.00 (CY)
3.832
15.18
0.490 DNDANDC DRY
0-<1/2"
SUR
0.5
0.20
58;000. p
15,300.00 p
15.20
p
16205
FESCUE HAY
Apr-14
1,216.00 (CY)
12.135

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 401.60
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 100.20 ACRES PERMITTED: 100.20
Page : 2
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pp-)
Crop
MONTH
Total
FP.r Acre
Solids
Total Wet Tons/Ac: 1.29
Total Cubic Yds/Ac: 29.38
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
123
Annual lbs/acre
0.042
0.016
0.627
2.380
0.293
0.005
0.063
0.282
0.040
25.145
292.04
Cumulative Ibs/acre
0.141
0.054
1.860
8.531
1.007
0.022
0.266
1 0.915
0.095
43.656
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
194
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DB WPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: TOAST
PERMIT #: WQ0003504 ANNUAL DRY TONS APPLIED: 260.71
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 57.60 ACRES PERMITTED: 57.60
Page : 1
Lune Applied ***
Date:::T Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/18/14
65.64 (W)
1.140
20.82
0.237
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
I FESCUE
4/22/14
96.97 (W)
1.684
20.82
0.351
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
I FESCUE
4/25/14
67.76 (W)
1.176
20.82
0.245
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
FESCUE
Apr-14
230.37 (W)
4.000
4/18/14
320.00 (CY)
5.556
15.18
0.710
DNDANDC
MOIST
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/22/14
640.00 (CY)
11.111
15.18
1.421
DNDANDC
DRY
0-<I/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/23/14
480.00 (CY)
8.333
15.18
1.065
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/25/14
224.00 (CY)
3.889
15.18
0.497
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
FESCUE
Apr-14
1,664.00 (CY)
28.889
1

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 000010002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: TOAST
PERMIT 4: WQ0003504 ANNUAL DRY TONS APPLIED: 260.71
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 57.60 ACRES PERMITTED: 57.60
Page : 2
Lime Applied ***
Date
Lbs/Ac
3allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
. TKN
Nitrogen
and
(ppni)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 4.00
I Mal k-UDIC I US AC-.
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.049
0.018
0.651
2.350
0.337
0.005
0.067
0.306
0.045
24.814
288.2.5
123
Cumulative lbs/acre
0,049
0.018
0.651
2.350
0.337
0.005
0.067
0.306
0.045
24.814
A
129
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
7
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
Wx
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
X t //1
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A =Not Applicable NR =Not Reported or Not Required % = percent p = pp- or mg/kg Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR-Surface, 1NJ -Injection, SURIN -Incorporation See Site pH &Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0005
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 127.86
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 24.20 ACRES PERMITTED: 24.20
Page: 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/1/14
20.42 (W)
0.844
20.82
0.176
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
7 1848
I FESCUE HAY
4/12/14
43.49 (W)
1.797
20.82
0.374
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
1848
FESCUE HAY
Apr-14
63.91 (W)
2.641
4/1/14
672.00 (CY)
27.769
15.18
3.550
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE HAY
4/12/14
224.00 (CY)
9.256
15.18
1.183
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
FESCUE HAY
Apr-14
896.00 (CY)
37.025
Total Wet Tons/Ac: 2.64
i ULM �,uuic iUV, Vo J/.UL
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
155
0.055
0.021
0.806
2.951
0.392
0.006
0.081
0.367
0.053
31.714 368.41
Cumulative lbs/acre
0.134
0.044
1.499
7.639
0.942
0.023
0.216
0.857
0.070
48.742
1
1
1
1
1
s-
'
194
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
," ;„g
,.
$f
n
a . ,
. k%X .ara,
4 .kv"", mr.�., ae ,*
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0 ,w
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: DURHAM, NC PREDOMINANT SOIL SERIES: TOAST
OWNER: SIDNEY THOMPSON PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 324.50
SITE #: NC PS 00001 FIELD# : PS 00001 0006 OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 93.10 ACRES PERMITTED: 93.10
Page : 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/4/14
44.10 (W)
0.474
20.82
0.099
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
1848
I FESCUE
4/12/14
21.04 (W)
0.226
20.82
0.047
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0 p
961.00 p
3.36 p
1848
FESCUE
Apr-14
65.14 (W)
0.700
4/3/14
896.00 (CY)
9.624
15.18
1.230
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/4/14
416.00 (CY)
4.468
15.18
0.571
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/5/14
384.00 (CY)
4.125
15.18
0.527
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000, p
15,300.00 p
15.20 p
16205
I FESCUE
4/I1/14
640.00 (CY)
6.874
15.18
0.879
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/12/14
96.00 (CY)
1.031
15.18
0.132
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
FESCUE
Apr-14
1 2,432.00 (CY)l
26.122

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0006
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: TOAST
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 324.50
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 93.10 ACRES PERMITTED: 93.10
Page : 2
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
oho
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 0.70
Total Cubic Yds/Ac: 26.12
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.035
0.014
0.556
2.054
0.258
0.004
0.055
0.247
0.035
22.334
259.45
109
Cumulativelbs/acre
0.212
0.039
1 1.833
7.196
1 1.123
0.069
0.168
1 1.242
0.099
37.596
° °
129
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
"?
°'
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
XS-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0
e Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0007
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: FAIRVIEW
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 106.79
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 30.20 ACRES PERMITTED: 30.20
Page : 1
Lime Applied ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/7/14
192.00 (CY)
6.358
15.24
0.816
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
61,500. p
12,500.00 p
5.25 p
16055
FESCUE
5/8/14
512.00 (CY)
16.954
15.24
2.176
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
61,500. p
12,500.00 p
5.25 p
16055
FESCUE
5/9/14
128.00 (CY)
4.238
15.24
0.544
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
61,500. p
12,500.00 p
5.25 p
16055
FESCUE
May-14
832.00 (CY)l
27.550
Total Wet Tons/Ac:
rotas Cubic YasiAc: 27.55
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
.
Annual Ibs/acre
0.042
0.014
0.248
1.860
0.233
0.006
0.050
0.156
0.035
21.429
217.12
114
Cumulative lbs/acre
0.108
0.030
1 0.777
5.580
1 0.697
0.019
0.131
1 0.554
0.044
35.674
Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop
146
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
Xyz(o, %e _�;_
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface .0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN -incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0010
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 226.61
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 75.40 ACRES PERMITTED: 75.40
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/24/14
480.00 (CY)
6.366
15.1.8
0.814
DNDANDC
- DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/25/14
128.00 (CY)
1.698
15.18
0.217
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
FESCUE
4/28/14
224.00 (CY)
2.971
15.18
0.380
DNDANDC
DRY
0-<I/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
FESCUE
Apr-14
832.00 (CY)
11.035
5/6/14
44.87 (W)
0.595
20.82
0.124
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.Op
961.00 p
3.36 p
1848
FESCUE
May-14
44.87 (W)
0.595
5/6/14
544.00 (CY)
7.215
15.24
0.926
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
61,500. p
12,500.00 p
5.25 p
16055
FESCUE
5/7/14
320.00 (CY)
4.244
15.24
0.545
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
61,500. p
12,500.00 p
5.25 p
16055
FESCUE
May-14
864.00 (CY)
11.459

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0010
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 226.61
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 75.40 ACRES PERMITTED: 75.40
Page : 2
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
"�o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
A
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
Total Wet Tons/Ac: 0.60
Total Cubic YOSIAc: 22.49
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.033
0.012
0.341
1.649
0.211
0.004
0.044
0.172
0.030
18.358
200.03
93
Cumulative lbs/acre
0.095
0.028
0.913
1 4.696
0.767
0.048
0.101
0.668
0.051
26.258
Perniit PAN Limit (lbs/acre) 1st Crop/2nd Crop
„;-
162
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L
1339.0
267.9
15.0 375.0
89.0
2500.0
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
DB WPC = DURHAM, NC BROWN WTP CAKE
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SIDNEY THOMPSON
SITE #: NC PS 00001 FIELD# : PS 00001 0012
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: CLIFFORD
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 170.42
OPERATOR: SIDNEY THOMPSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 30.60 ACRES PERMITTED: 30.60
Page: I
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner-'
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/2/14
42.24 (W)
1.380
20.82
0.287
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
FESCUE
4/12/14
49.21 (W)
1.608
20.82
0.335
DBWPC
DRY
0-<1/2"
SUR
0.5
0.20
7,780.0p
961.00 p
3.36 p
1848
FESCUE
Apr-14
1 91.45 (W)
2.988
4/2/14
1,024.00 (CY)
33.464
15.18
4.278
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16205
I FESCUE
4/12/14
160.00 (CY)
5.229
15.18
0.668
DNDANDC
DRY
0-<1/2"
SUR
0.5
0.20
58,000. p
15,300.00 p
15.20 p
16201
FESCUE
Apr-14
1,184.00 (CY)
38.693
Total Wet Tons/Ac: 2.99
rotas uuotc rastAc: 3iS.6�
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
TOTALS:
Annual lbs/acre
0.058
0.022
0.845
3.090
0.413
0.006
0.085
0.386
0.056
33.151 385.10
163
Cumulative Ibs/acre
0.194
0.069
2.273
11.561
1.789
0.041
0.258
1.376
0.074
59.831
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
216
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
I
1339.0
267.9
15.0
375.0
89.0
2500.0
DBWPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
x Jr/ �//, t - ,
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SUSAN SATTERFIELD
SITE #: NC PS 00029 FIELD# : PS 00029 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WEDOWEE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 42.04
OPERATOR: CRAIG MORROW CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 15.10 ACRES PERMITTED: 15.10
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
12/18/14
275.00 (CY)
18.212
16.64
2.552
DNDANDC
MOIST
0-<1/2"
SUR
0.5
0.20
60,100.p
14,800.00 p
1,080.00 p
17540
FESCUE
12/19/14
25.00 (CY)
1.656
16.64
0.232
DNDANDC
MOIST
0-<1/2"
SUR
0.5
0.20
60,100.p
14,800.00 p
1 1,080.00p
17140
1 FESCUE
Dec-14
300.00 (CY)
19.868
Total Wet Tons/Ac:
Total Cubic Yds/Ac: 19.87
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
98
Annuallbs/acre
0.028
0.011
0.189
1.682
0.162
0.002
0.028
0.134
0.028
17.152
174.30
Cumulative Ibs/acre
0.322
0.119
5.197
16.490
2.512
0.079
0.783
2.629
0.269
126.680
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
126
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
� -
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

FACILITY NAME: DURHAM, NC
OWNER: SUSAN SATTERFIELD
SITE #: NC PS 00029 FIELD# : PS 00029 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: WEDOWEE
PERMIT #: W00003504 ANNUAL DRY TONS APPLIED: 39.93
OPERATOR: CRAIG MORROW CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 27.70 ACRES PERMITTED: 27.70
Page: 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry'
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
12/19/14
24.26 (W)
0.876
20.18
0.177
DBWPC
MOIST
0-<1/2"
SUR
0.5
0.20
6,890.0 p
4,410.00 p
30.20 p
2731
FESCUE
Dec-14
24.26 (W)
0.876
12/19/14
250.00 (CY)
9.025
16.64
1.265
DNDANDC
MOIST
i
0-<1/2"
SUR
0.5
0.20
60,100. p
14,800.00 p
1,080.00 p
17540
FESCUE
I
Dec-14
250.00 (CY)
9.025
Total Wet Tons/Ac: 0.88
Total Cubic Yds/Ac: 9.03
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
45
Annual lbs/acre
0.016
0.008
0.093
0.912
0.084
0.001
0.014
0.072
0.014
7.831
79.49
Cumulative lbs/acre
0.450
1 0.160
7.070
20.634
1 2.316
0.077
1.051
1 2.942
0.252
143.357
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
96
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
DB WPC = DURHAM, NC BROWN WTP CAKE
DNDANDC = DURHAM, NC N. DURHAM WWTP ANAEROB. DIGESTED CAKE
x Gil e)2/����
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015

Summit Environmental Technologies, Inc.
Sa
3310 Win St.
FtCuyahoga Falls, Ohio44223
t�rtadyrical t' i� rsaf� l TEL: [phone] FAX..• [phone]
Website: ha.-Ilivivw.settek.com
January 16, 2014
James Blackwell
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Durham
Dear James Blackwell:
Order No.: 14010513
Summit Environmental Technologies, Inc. received 2 sample(s) on 1/10/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Geo o a
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-011-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 9

Summit Environmental Technologies, Inc. Workorder
3310 Win St.
iWAVlf1t?UIAWrALINC, Cuyahoga Falls, Ohio 44223 Sample Summary
t re �i rlff:ai 1 15Crt'r 3r?d'�t'S TEL: [phone] FAX. [phone] WO#: 14010513
Website: httn://www.settek.conz 17-Jan-14
CLIENT: Synagro
Project: Durham
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
14010513-001 North Durham WRF 1/6/2014 11:20:00 AM 1/10/2014 9:52:00 AM Sludge
14010513-002 South Durham WRF 1/6/2014 12:10:00 PM 1/10/2014 9:52:00 AM Sludge
Page 2 of 9

Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
GP5VIr�C�P1h9Ej1%�L tiG3$iC1L1'.i�9p'9f�C?. Cuyahoga Falls, Ohio 44223 WO#: 14010513
r$n;cri} Ls`ora? 5r1� TEL: [phone] FAX.- [phone]
Website: hay.-Ilwww.settek.com Date: 1/16/2014
CLIENT: Synagro
Project: Durham
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Revision v1
Page 3 of 9

Summit Environmental Technologies, Inc.
WO#:
14010513
�_1
PCb1rIRCi�1P�1f='AI;P�L.,7`��}i�.it�l,Q�i8$;.9t��
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
P
1/16/2014
4 4'rraF�,tf,: t Riaraidrle
TEL: [phone] FAX. • [phone]
Company:
Synagro
Website: htto:/hvimsettek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 1/10/2014
Project#: Durham
TCLP Metals
Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
,Method
DF
RegLvl
Run
Analyst
North Durham WRF
001
1/6/2014
TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/14/2014
WK
North Durham WRF
001
1/6/2014
TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
TCLP Mercury Analysis
(1311/7470)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham WRF
001
1/6/2014
TCLP Mercury
0.0020
ND mg/L
Sludge
EPA 7470 A
1
0.20
1/14/2014
ALJ
SVOC
SW-846: 8081-TCLP
Pesticides
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham WRF
001
1/6/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/15/2014
JBN
North Durham WRF
001
1/6/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
1/15/2014
JBN
North Durham WRF
001
1/6/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/15/2014
JBN
North Durham WRF
001
1/6/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/15/2014
JBN
North Durham WRF
001
1/6/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
North Durham WRF
001
1/6/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
North Durham WRF
001
1/6/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/15/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham WRF
001
1/6/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
North Durham WRF
001
1/6/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
North Durham WRF
001
1/6/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
North Durham WRF
001
1/6/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
North Durham WRF
001
1/6/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
1/15/2014
MES
North Durham WRF
001
1/6/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/15/2014
MES
North Durham WRF
001
1/6/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
North Durham WRF
001
1/6/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
North Durham WRF
001
1/6/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/15/2014
MES
North Durham WRF
001
1/6/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/15/2014
MES
Page 4 of 9

Summit Enviromnental Technologies, Inc. WO#: 14010513
3310 Win St.
3i`�E-:Cuyahoga Falls, Ohio 44223 Date Reported: 1/16/2014
trf�SVIfiOhIPatE#�;ri.�L'B''�C�-4BdC�l.,�4",,1t;�;
L- `' _ /lnafl�t;:at'i akaargP TEL: [phone] FAX. • [phone] Company: Synagro
Website: httn:/Avww.settek.com Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/10/2014
Project#: Durham
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham WRF
001
1/6/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C.
1
7.5
1/14/2014
AKE
North Durham WRF
001
1/6/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/14/2014
AKE
North Durham WRF
001
1/6/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/14/2014
AKE
North Durham WRF
001
1/6/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
' 200
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/14/2014
AKE
butadiene
North Durham WRF
001
1/6/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
1/14/2014
AKE
North Durham WRF
001
1/6/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/14/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
` DF
RegLvl
Run
Analyst
North Durham WRF 001 1/6/2014 2,4-D
5.0 ND mg/L
Sludge
EPA 8321 A
1
10
1/14/2014
AMZ
North Durham WRF 001 1/6/2014 2,4,5-TP
0.50 ND mg/L
Sludge
EPA 8321 A
1
1.0
1/14/2014
AMZ
TCLP Metals Analysis (6010)
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
South Durham WRF
002
1/6/2014
TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/14/2014
WK
South Durham WRF
002
1/6/2014
TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/14/2014
WK
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst
South Durham WRF 002 1/6/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 1/14/2014 ALJ
Page 5 of 9

Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14010513
FFfiVIRCfhlpa7E?J`pt�L 9E stPdt]l{1'G1BS�Ir C
Cuyahoga Falls, Ohio 44223
Date Reported:
1/16/2014
arc Fl.tie�?t Ltiliaialvri s
TEL: [phone] FAX: [phone]
Company:
Synagro
Website: http://wwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received: 1/10/2014
Project#: Durham
SVOC SW-846: 8081-TCLP Pesticides
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
South Durham WRF
002
1/6/2014
Chlordane,'total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/15/2014
JBN
South Durham WRF
002
1/6/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
1/15/2014
JBN
South Durham WRF
002
1/6/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/15/2014
JBN
South Durham WRF
002
1/6/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/15/2014
JBN
South Durham WRF
002
1/6/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
South Durham WRF
002
1/6/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/15/2014
JBN
South Durham WRF
002
1/6/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/15/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
South Durham WRF
002
1/6/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
-outh Durham WRF
002
1/6/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
-outh Durham WRF
002
1/6/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
South Durham WRF
002
1/6/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
South Durham WRF
002
1/6/2014
Chlorobenzene
0.10
ND mg/L-
Sludge
EPA 8260 B
1
100
1/15/2014
MES
South Durham WRF
002
1/6/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/15/2014
MES
South Durham WRF
002
1/6/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/15/2014
MES
South Durham WRF
002
1/6/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/15/2014
MES
South Durham WRF
002
1/6/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/15/2014
MES
South Durham WRF
002
1/6/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/15/2014
MES
SVOC 8270 TCLP BNA List
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
South Durham WRF
002
1/6/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
1/14/2014
AKE
South Durham WRF
002
1/6/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/14/2014
AKE
South Durham WRF
002
1/6/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/14/2014
AKE
South Durham WRF
002
1/6/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/14/2014
AKE
butadiene
South Durham WRF
002
1/6/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
1/14/2014
AKE
South Durham WRF
002
1/6/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/14/2014
AKE
Page 6 of 9

_
�• � �
S
Summit Environmental Technologies, Inc.
WO#:
14010513
"M
#14,
3310 Win St.
FNVI!'i47
Cuyahoga Falls, Ohio 44223
Date Reported:
1/16/2014
AFFAq t ral f iora'rpde�
TEL: [phone] FAX. • [phone]
Company:
Synagro
Website: htto://www.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Durham
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
South Durham WRF 002
South Durham WRF 002
1/6/2014 2,4-D
1/6/2014 2,4,5-TP
5.0 ND mg/L
0.50 ND mg/L
Sludge
Sludge
EPA 8321 A
EPA 8321 A
1
1
10
1.0
1/14/2014
1/14/2014
AMZ
AMZ
Page 7 of 9

-M!'-somwart
Summit Environmental Technologies, Inc.
WO#:
14010513
3310 Win Si.
EfdVIRDtJ1e1�R!'P1�L'T£CHd @13'G:es SPtC
Cuyahoga Falls, Ohio 44223
Date Reported:
1/16/2014
ArrafyUral L*horzjor/e=
TEL: [phone] FAX.- [phone]
Company:
Synagro
Website: htto://wiviv.settekeom
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Durham
Client ID#
Lab ID# Collected Analyte
Result Units
Matrix
Method
DF
RL
Run
Analyst
North Durham WRF
001
1/6/2014
Flashpoint (140T)
>140 T
Sludge
EPA 1010
1
1/13/2014
TAH
North Durham WRF
001
1/6/2014
Cyanide, Reactive .
ND ppm
Sludge
EPA 9014
1
0.50
1/13/2014
TIR
North Durham WRF
001
1/6/2014
pH
8.0 s.u.
Sludge
EPA 9045 D
1
1/13/2014
AYS
North Durham WRF
001
1/6/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1
25
1/13/2014
TIR
Client ID#
Lab ID#
Collected Analyte
Result Units
Matrix
Method
DF
RL
Run
Analyst
South Durham WRF
002
1/6/2014
Flashpoint (140T)
>140 T
Sludge
EPA 1010
1
1/13/2014
TAH
South Durham WRF
002 •
1/6/2014
Cyanide, Reactive
ND ppm
Sludge
EPA 9014
1
0.50
1/13/2014
TIR
outh Durham WRF
002
1/6/2014
pH
7.8 s.u.
Sludge
EPA 9045 D
1
1/13/2014
AYS
South Durham WRF
002
1/6/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 9034
1
25
1/13/2014
TIR
Page 8 of 9

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CD
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Summit Environmental Te.chnologies-" Inc. Aoalysia' 'c�,q4est/Chahi of Custody
R
33TOWifiStreet
For Stiiiiiiiit-[:i)vii-oiiiiietitaI 1echpologies.b1c. use Only
C.'Lly,ihoga Falls, Ohio 441221 T&1: 330,253.82'1,1 RLx: 330-253;4489 - Rage-6f—.- SET Ni,.
C.Q111pally Nanie- 0110.m& paint)
Project Nanie-
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Addrqq.S
Client Phone;.No.
R port to
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Quote No!
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Rush Requt.-Sled By' by Must bc-'Upp.roved
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6��d4'IRt3f#f�tE`'CiiL'f��"li;�dOLO�Ic`S, i�F�
January 30, 2014
James Blackwell
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: North Durham
Dear James Blackwell:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. [phone]
Website: hun.-Ilivww.settek.com
Order No.: 14011068
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/17/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
W ��
Dr. Mo Osman
Proj ect Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A21-A 0724.01, Alabama 41600, Arkansas 88-0735, Califomia 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.S, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 8

F „ Sunni:it Environmental Technologies, Inc.
Workorder
P3VfR
a
31iPa1i h1fi1L �fC: W 0 LO d] B,5
3310 Win St.
t IN 0, Cuyahoga Falls, Ohio 44223
Sample Summary
t rr
%rrivcaf LaPa4t�kjrie5
TEL: [phone] FAX: [phone]
WO#: 14011068
Website: httn://iviviv.settek.com
31-Jan-14
CLIENT:
Synagro
Project:
North Durham
Lab SampleID
Client Sample ID
Tag No Date Collected
Date Received Matrix
14011068-001
North Durham Drying Beds
1/15/2014 11:35:00 AM
1/17/2014 9:50:00 AM Sludge
Page 2 of 8

Summit Environmental Technologies, Inc. Case Narrative
In'suh s� NOUT 3310 Win St.
:uS'Jl.RomaEWALTjEC1JUQk.4`(!Msjplr, Cuyahoga Falls, Ohio44223 WO#: 14011068
/k`a"z1'ytvc°sl LTEL: [phone] FAX.- [phone]
Website: htto:/hviviv.settek.com Date: 1/30/2014
CLIENT: Synagro
Project: North Durham
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 8

Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14011068
��StrIR4i11�tEi!'PI<L T'i ��$5 �51 �G3,`e��9 �C.
Cuyahoga Falls, Ohio 44223
Date Reported:
1/30/2014
rrt+'#, al L:taaxa3r
TEL: [phone] FAX. • [phone]
Company:
Synagro
Website: huy.-11www.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/17/2014
Project#:
North Durham
TCLP Metals Analysis (6010)
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham Drying 001
1/15/2014 TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/23/2014
WK
Beds
North Durham Drying 001
1/15/2014 TCLP Badum(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
1/23/2014
WK
Beds
North Durham Drying 001
1/16/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/23/2014
WK
Beds
North Durham Drying 001
1/15/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/23/2014
WK
Beds
North Durham Drying 001
1/15/2014 TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/23/2014
WK
Beds
North Durham Drying 001
1/15/2014 TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/23/2014
WK
Beds
North Durham Drying 001
1/15/2014 TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/23/2014
WK
Beds
j
TCLP Mercury Analysis (1311/7470)
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham Drying 001
1/15/2014 TCLP Mercury
0.0020
ND mg/L
Sludge
EPA 7470 A
1
0.20
1/22/2014
ALJ
Beds
SVOC
SW-846: 8081-TCLP
Pesticides
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham Drying 001
1/15/2014 Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/23/2014
JBN
Beds
North Durham Drying 001
1/15/2014 Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/23/2014
JBN
Beds
Page 4 of 8

��.� _
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14011068
y
r wiRommEt4iiiL YEC�kCdClt �Gi-c�a�-I"qc;
Cuyahoga Falls, Ohio 44223
Date Reported:
1/30/2014
fdieaP3;fir 1 L; Ii'are7�a�/e
TEL: [phone] FAX.. [phone]
Company:
Synagro
Website: htto:/Avivw.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/17/2014
Project#:
North Durham
VOC by GC/MS (8260)-TCLP
Client ID# Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham Drying 001
1/15/2014 1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/23/2014
MES
Beds
North Durham Drying 001
1/15/2014 Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/23/2014
MES
-eds
orth Durham Drying 001
.1/15/2014 Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/23/2014
MES
weds
North Durham Drying 001
1/15/2014 MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/23/2014
MES
Beds
SVOC 8270 TCLP BNA List
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
North Durham Drying 001
1/15/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/23/2014
AKE
Beds
butadiene
North Durham Drying 001
1/15/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
1/23/2014
AKE
Beds
North Durham Drying 001
1/15/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/23/2014
AKE
eds
Page 5 of 8

Summit Emviromnental Technologies, b,c.
WO#:
14011068
3310 Win St.
f.t51EIFitIPuiErl'f 4L SEiEc`dtiL'i�3E5 3tAu
Cuyahoga Falls, Ohio 44223
Date Reported:
1/30/2014
Artat�trcal i': 3lae�aat�i�le� TEL:
[phone] FAX: [phone]
Company:
. Synagro
Website: htto:/hvwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/17/2014
Project#:
North Durham
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method DF RegLvl Run Analyst
North Durham Drying 001 1/15/2014 2,4-D
5.0 ND mg/L
Sludge EPA 8321 A 1 10 1/29/2014 AMZ
Beds
North Durham Drying 001 1/15/2014 2,4,5-TP
0.50 ND mg/L
Sludge EPA 8321 A 1 1.0 1/29/2014 AMZ
Beds
Page 6 of 8

-m'suyt
Summit Environmental Technologies, Lzc•
m,, 11
3310 Win St.
WO#: 14011068
ENVIF10t4li01'I'ALTECHaNO1-1-I ip$, tc
Cuyahoga Falls, Olio 44223
Date Reported: 1/30/2014
%AiT3sysiti2.1 L;3['taral�7t'ie5 TEL: [phone] FAX.- [phone]
Company: Synagro
Website: hup.-Iliviviv.settek.com
Address: 284 Boger Rd.
Mocksville NC 27028
Received: 1/17/2014
Project#: North Durham
Client ID# Lab ID# Collected Analyte
Result Units
Matrix Method DF RL
Run Analyst
North Durham Drying 001 1/15/2014 Flashpoint (140°F)
>140 °F
Sludge EPA 1010 1
1/20/2014 TAH
Beds
North Durham Drying 001 1/15/2014 Cyanide, Reactive
ND ppm
Sludge EPA 9014 1 0.50
1/20/2014 TIR
Beds
North Durham Drying 001 1/15/2014 Free Liquid
PASS Free
Sludge EPA 9095 1
1/21/2014 AYS
Beds
Liquid
North Durham Drying 001 1/15/2014 pH 5.1 s.u. Sludge EPA 9045 D 1 1/17/2014 AYS
Beds
North Durham Drying 001 1/15/2014 Sulfide, Reactive ND ppm Sludge EPA 9034 1 25 1/20/2014 TIR
Beds
Page 7 of 8

Su unit inc. i -of
el -An4lysis Re -� 'CUSt � d'
33 1 0:AM h --istre e, I/Chala y
-�,81 t F�x-: Tor use only
�myahOki',Fzilk,'. Wi-6,44,221 T&1:--�'3-X`253 1 33'0.�53.449q-
I—r
Compaq Nnmc: (Please Piinp
Anafyticaf,,Plfirameters anid Nlethods,i
Xc�f o,
J10i
P`111
N!L
0 Unit iZ ail 1 ET: ( Ple.-IseT "Jil R40trits
t
, Civet. cy 114sorf.
-$pmpled I)Y.r
Check.if Ohio VAPjsa!Ini lcfi,v
-,zzl
I
1�5,2�
Coltccted
C.
z
CD
00
0
h
00

POW IM)Nh1ENTALTECH NOLt-s-I1r1r,
�$n�lpiicaP. E.3�afxf�dlt?S
March 07, 2014
James Blackwell
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Durham Brown WTP
Dear James Blackwell:
Summit Envir•omnental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX. • [phone]
Website: http://lvivw.settek.cont
Order No.: 14021945
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/26/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
N�
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH00923201 1 -1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
Page 1 of 1

i Summit Environmental Technologies, Inc.
� 3310 Win St.
FYSJIRO#alelEtv'id4LTg1"u!3@L3�+p3N Cuyahoga Falls, Ohio44223
l r .�Fla'teirai !pia®raial'! + TEL: [phone] FAX: [phone]
Website: http://www.settekcom
CLIENT: Synagro
Project: Durham Brown WTP
Workorder
Sample Summary
WO#: 14021945
07-Mar-14
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
14021945-001 Durham Brown WTP 2/20/2014 10:35:00 AM 2/26/2014 11:10:00 AM Sludge
Page 1 of 1

Summit Environmental Technologies, Inc. Case Narrative
ffll; _ 3310 Win St.
FPS,rIlitiHIAENTALTECt-�NOLOG 145',•_NO, Cuyahoga Falls, Ohio44223 WO#: 14021945
#a?7e�iIpCA11•jb or'gWie;s TEL: [phone] FAX. • [phone]
Website: huy.- vwiv.settek.com Date: 3/7/2014
CLIENT: Synagro
Project: Durham Brown WTP
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover -Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 1 of 1

SununitEnvironmental Technologies, Inc.
W0 14021945
3310 Win St.Date
(»vmhvxosx�omof*zzs Reported: 3�D�0l4
TEL: [phone]//FAu�[phone]
Company: Qyuugrn
wem��
�
AdJ,uxm: 284Boger
Rd.
MoukovdloNC 27028
Received: 2/26/2014
nrojeut#: Durham Brown
TCLPMetals Analysis (68lO)
Climd0m# LubID# Collected Anulyto
Rep Lint Result 0oim
Matrix
Method
DF
RogLvl
Ron
Analyst
Durham Brown vvTP 001 2/20/2014ToLpxmoniu(Am)
0.50 wo mgx'
Sludge
EPA no1oC
1
oo
3/3s014
vvn
Durham Brown vvTP 001 2o0/2014TcLpsanum(sa)
*.o wo mg/L
Sludge
EPA oo1oo
1
100
3m/2014
vvn
Durham Brown vvTP 001 2120/2014TcLpoaummm(ou)
0.10 mo mg/L
o|uuga
EPA no1oo
1
1.0
3mm014
vvn
Durham Brown vvTP 001 2s0o014TcLpc»mm|um(nr)
0.20 wo mg/L
a|uuga
EPA oo1on
1
5.0
3m12014
vvn
Durham Brown vvTP 001 2120m014ToLpL*no(PW
0.50 wo mox'
Sludge
EPA nn1oo
1
oo
3m12014
vvn
Durham Brown vvTp 001 2m012014ToLPae|en|um(ao)
u.*u wo mgu'
Sludge
EPA no1oo
1
1.0
3m/2014
vvo
Durham Brown vvTp 001 2o0/2014ToLPai*ar(A)
0.50 wo mg/L
G|uouo
EPA oo1no
1
oo
3m12014
vvm
TCLPMercory Auu}yuiu(l3ll/747O)
Client00# Lu6DD# "ColleotedAnuhto
RepLou Result Units
Matrix
Method
]NF
RogLpl
Roo
Analyst
Durham Brown vvTP 001 mzmzo14TCLpMercury
0.0020 wo mu/L
a|uuga
EPA 747ox
1
0.20
3m/2014
au
' 0VOCSW-846: 0001'TCLP Pesticides
CbeotD0# LubID# Collected Aoulytm
Rep Lmt Result Units
Matrix
Method
DF
RwQLv}
Ron
Analyst
Durham Brown vvTP 001 2/20/2014 Chlordane, total
0.010 wo mg/L
8|uooe
EpA0001 s
1
0.030
3wo014
xBw
Durham Brown vvTP 001 2m012014 Tuxap»ane
0.10 wo mg/L
Smuuv
ePA0001 o
1
0.50
314o014
Jew
Durham Brown vvTp 001 2/20/2014snonn
0.0020 womu/L
Sludge
EPA 00010
1
0.020
314m014
Jaw
Durham Brown vvTP 001 2/20/20148amma'oxC
0.0020 womu/L
Sludge
EPA ooa1s
1
0.40
3*412014
xaw
Durham Brown vvTP 001 2/20/2014 Heptachlor
00000 wo mg/L
Sludge
epAuoo1 s
1
0.0080
3wo014
xow
Durham Brown vvTp 001 2o0/2014 Heptachlor epoxide
uonuu wo mo/L
Sludge
EPA oou1a
1
0.0080
3w/2014
Jsw
Durham Brown vvTp 001 2/20/2014 me*xnxyomnr
0.0020 wo mg/L
e|uuuo
EPA uoo1s
1
10
3w/201*
Jsw
VOCDyGCIM9(8%6O)-TCLP
ClloutD0# Lmb8D# Collected Auulytw
Rep Lou Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Durham Brown vvTp 001 2o0/2014 1.1'momomc«hnne
0.10 wo mo/L
Sludge
EPA oxooa
1
0.70
3mo014
mEa
Durham Brown vvrP 001 2s0/20141.2'ommvme«hano
0.10 wo mg/L
Sludge
EPA au000
1
noo
3mo014
Mes
Durham Brown vvrP 001 2/20/201* Benzene
0.10 wo mg/L
S|uuua
EPA a000a
1
0.50
313o014
MEs
Durham Brown vvTP 001 usmuo14Carbon tetrachloride
0.10 wo mu/L
Sludge
EPA aznos
1
oao
3mo014
mEe
Durham Brown vvTp 001 2m0/201* omomuonzone
0.10 wo mg/L
6|uugo
EPA ousoo
1
100
313/2014
MeG
Durham Brown vvrP 001 2120/2014omu,mbnn
0.10 wo mg/L
Sludge
EPA ecooa
1
so
3mo014
mea
Durham Brown vvrp 001 2o01201*ngmxmumetxano
0.10 wo mg/L
Sludge
EPA aenoo
1
0.70
3mo014
mEa
Durham Brown vvTp 001 2/20/2014Tnomvmethono
0.10 mo mg/L
8|uuuo
EPA ocnoe
1
oan
3mo014
mEa
Durham Brown vvTp 001 2m0/2014 Vinyl chloride
0.20 wo mo/L
a|uuoe
EPA uunos
1
0.20
313o014
mea
Durham Brown vvTp 001 2o0/201* men
2.0 wo mo/L
Sludge
EPA a2nos
1
200
3/3o014
Mes
Page 1 of 2

�
' g
Summit Environmental Technologies, Inc.
-
3310 Win St.
WO#:
14021945
�
t tSVIrRt}tdh1E1J'f�1LifCaCt�LO'G1s SPEC
Cuyahoga Falls, Ohio 44223
Date Reported:
3/7/2014
itrsa;yitcsi t:3t5'ersPdrl�
TEL: [phone] FAX [phone]
Company:
Synagro
Website: _htty.Ilivwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
2/26/2014
Project#:
Durham Brown
SVOC 8270 TCLP BNA List
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Durham Brown WTP
001
2/20/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
3/4/2014
AKE
butadiene
Durham Brown WTP
001
2/20/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
3/4/2014
AKE
Durham Brown WTP
001
2/20/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
3/4/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client ID# Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Durham Brown WTP
001
2/20/2014 2,4-D
5.0
ND mg/L
Sludge
EPA 8321 A
1
10
3/7/2014
AMZ
Durham Brown WTP
001
2/20/2014 2,4,5-TP
0.50
ND mg/L
Sludge
EPA 8321 A
1
1.0
3/7/2014
AMZ
Page 2 of 2

•� • - •� ; ., �
it Eg
Summit tl Technologies, ies, Inc.
3310 Win St.
WO#:
14021945
HNIROIN&IENTd4LTPCHt'dt3Li' 1sS�9dC,
Cuyahoga Falls, Ohio44223
Date Reported:
3/7/2014
l�rt�f�rtif.s!'It�arel�t'i
TEL: [phone] FAX. • [phone]
Company:
Synagro
Website: http://wwiv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
2/26/2014
Project#:
Durham Brown
Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst
Durham Brown WTP
001
Durham Brown WTP
001
Durham Brown WTP
001
Durham Brown WTP
001
2/20/2014
Flashpoint (140T)
>140 T
2/20/2014
Cyanide, Reactive
ND ppm
2/20/2014
pH
6.0 s.u.
2/20/2014
Sulfide, Reactive
ND ppm
Sludge
EPA 1010
1
2/27/2014
TJR
Sludge
EPA 9014
1
0.50 2/27/2014
TIR
Sludge
EPA 9045 D
1
2/26/2014
AYS
Sludge
EPA 9034
1
25 2/27/2014
TIR
Page 1 of 1

Spnimit PnvironmpntaFTOIUfOI` gies,, 1111c...
3. fscrst
23- 448(
.153 At _j301S34_,_
'Alfal J." Ri'' u -,-ie.st--/,C-hai-ii,�6f-.-'Custody
W� I --eq
forStrnttriit 11IC-joSe oil
SFT N..
ameters rametersand'- Nil eiltods
Par
Compan)­ Addy,
C.
$&vavr to
(�,Ii IWEak of��k. 1-111cask; P �ax Resm
po#�
j
Q�
Gficiii:, mail PL
4 'j;
Y�NXI�
;S414
Checkirobio VAP,sarlipies;.t
7�
Date
Ide tifibdon.
Samplen
Collected -
-Coilectcd
U
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IN
co
CD
0
h
N)

Dater D7/2 7 /1
Cooler Reteip', V.Onlrb
Initials Of person inSpe.-ting.w6ler and sa-rnplbs:: SL
but: A V VI
q6oleqs) opened andsa'rnples inspected: 241
I 1IA
iiippen rED �, 'Lll' -OHL Airborne USI.Pa'slal'
Walk-in 'Pickup 9th6r;
Pa .9 in�'�
ck 9 .; Pea6uts E bbleVqr
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Custody ss'alsintact :
(9
C-10-din pfaitir
Pb
fyJA
Ice Blueiee
pr t I mhlted Nit�
tainp;'16mpeiature It? Gun #f(50 4456 CF
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191A
#35_1 27
a I'L
ldff
(see P�-P' F�r �-Can results)
saMirls I-s'l4pt saik" 6�flccr must ba
fiIled oui properly`
S fV
-NIA
Z§rpPlii 'jin sep
y
Sample, containers Anla&'
"lf no, list brbken sample(s):
S#mpld label(g).cdmfp[ewd:(ID; date, etc:.)
U-y 4
ITA
Labe!ls)_`aqree'j"[th C-0-C,
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bwfect cb nIaiftefs used,
14
141A
5Vi`64qnispwe 're6dj' &
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Elubbrle.s-absleiit from 40 mL
y
A*,SaMpj I sS UVjfh bubbles <6mm are acceptable:
i6didtite bubblesiZeIC>ainrij�,
V94 cljenfco6lacled``about samples
y
6tidnVidnid niv,f samples
y
pl!E�pt
Date./T - hie:
Logged in by:
RE'MD'6cument . Contral-..Templates= Tiackin letrecel form,RdvA2-07-2713.d 1 06 R\P�qo _ 0� Page I.-o(2
Page-2 of 2

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number
WWTP Name: North Durham WRF NPDES Number: _
lionitoring Period: From 01/01/14 To 02/28/14
WQ0003504
NCO023841
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlienhle to alternative nerfnrmPd (Clncs A nr (Tics Rl emmnlPtr the. fnllnwina mnnitnrina dnfa-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 6 th
MPN
1,333
7,601
66,667
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent —North Durham VW
�Ireparer Name and Title (print or type)
iQV6�
t5
i nature of Preparer* at
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. /g. is
7,601
4,965
_ 5,634
2/20/2014
16,667
66,667
5,926
5,970
1,333
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411'
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
57
Sample Set #2
MPN
f. coliform/g total solids
125
Sample Set #3
MPN
f. coliform/g total solids
37
Sample Set #4
MPN
f. coliform/g total solids
152
Sample Set #5
MPN
f. coliform/g total solids
417
Sample Set #6
MPN
f, coliform/g total solids
123
Sample Set #7
MPN
f. coliform/g total solids
84
Geometric Mean
fcol. / g. is
108
2/20/2014
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

North Durham Water Reclamation Facility
Sludge Report
Jan'14
in 75 %
out 63 %
PRIMARY SLUDGE TO DIGESTER - A
WASTING TOTAL
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
1
58,835
5.93
29,073
75
21,754
1
910,336
1.2
91,106
73.7
2
56,453
5.88
27,684
80.1
22,164
2
988,770
1.7
140,188
72.7
3
64,804
5.25
28,374
81.1
23,019
3
1,312,420
1.2
131,347
73.2
4
93,555
4.51
35,209
80.7
28,413
4
1,599,334
1.2
160,061
72.9
TOTAL
273,647
5.39
120,340
79.2
95,350
TOTAL
4,810,860
1.33
522,703
73.1
TO GBT
TWAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
lbs. D.S.
lbs. V.M.
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
951,394
95,216
70,174
1
222,545
7.6
141,058
73.95
104,312
2
1,144,200
162,225
117,937
2
248,312
7.1
147,035
74.6
109,688
3
1,606,286
160,757
117,674
3
339,967
6.55
185,714
74.75
138821
4
1,483,431
148,462
108,229
4
350,114
5.85
170,817'
74.55
127:344
TOTAL
5,185,311
566,659
414,014
TOTAL
1,160,938
6.78
644,624
74.5
4801166
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
WEEK
Yds
% Solids
1
300,347
3.6
90,176
63
56,811
1
288
14.83
2
358,129
3.3
98,564
63.1
62,194
2
384
15.95
3
382,274
2.8
89,269
63.3
56,507
3
312
15.33
4
560,884
3.1
145,011
62.8
91,067
4
480
14.14
TOTAL
1,601,634
3.2
423,020
63.1
266,579
TOTAL
1464
15.06
Summary
Total Gallons to Anaerobic Dig.
1,434,585
Total Pounds of Dry'Solids to Anaerobic Dig.
764,965
Total Pounds of Vol. Solids to Anaerobic Dig.
575,516
Total Gallons from Anaerobic Dig.
1,601,634
Total lbs. of Dry Solids from Anaerobic Dig.
423,020
Total lbs. of Vol. Solids from Anaerobic Dig.
266,579
Detention Time - Days
79
Gas Production
8,666,442
Ft3 of Gas Produced/lb of VM Added
15
% Reduction
44 (VK) 54 % (AMB)
lbs VM
67,145
101,917
96,146
116,685
381,893

North Durham Water Reclamation Facility
in 76%
Sludge Report
out
64%
Feb'14
PRIMARY SLUDGE TO DIGESTER -
A
WASTING TOTAL
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1 82,671 4.22 29,096
81
23,591
1
871,197
1.1
79,924
72.8
58,184
2 74,004 4.24 26,169
81.6
21,364
2
843,150
1.2
84,382
73.6
62,063
3 61,644 3.56 18,302
77.4
14,170
3
922,834
1.2
92,357
74.3
68,621
4 73,633 5.14 31,565
79.7
25,157
4
932,187
0.5
38,872
72.9
28,338
TOTAL 291,952 4.29 105,132
80
84,282
TOTAL
3,569,368
1
295,535
73.4
217,207
TO GBT
TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons lbs. D.S. lbs. V.M.
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1 941,,175 86,343 62,858
1
216,990
6
108,582
74.25
80,622
2 868,210 86,890 63,908
2
206,301
6.3
108,395
74.95
81,242
3 994,283 99,508 73,934
3
233,748
6.65
129,639
75.4
97,748
4 1,069,256 44,588 32,505
4
220,824
6.9
127,075
75.1
95,434
TOTAL 3,872,924 317,330 233,205
TOTAL
877,863
6.46
473,691
74.9
355,045
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF
PRESS
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Yds
% Solids
1 302,784 3.5 88,383
64.1
56,653
1
15.83
2 293,534 2.5 61,202
63.3
38,741
2
240
15.13
3 245,621 3.4 69,648
65.3
45,480
3
264
15.57
4 423,468 2.5 88,293
64.1
56,596
4
288
14.25
TOTAL 1,265,407 2.98 307,526
64.2
197,470
TOTAL
792
15.2
ANAEROBIC SLUDGE
TO BEDS
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
1
2
3
4 6.2
85.1
TOTAL 6.2
85.1
Summary
Total Gallons to Anaerobic Dig.
1,169,815
Total Pounds of Dry Solids to Anaerobic Dig.
578,823
Total Pounds of Vol. Solids to Anaerobic Dig.
439,327
Total Gallons from Anaerobic Dig.
1,265,407
Total lbs. of Dry Solids from Anaerobic Dig.
307,526
Total lbs. of Vol. Solids from Anaerobic Dig.
197,470
Detention Time - Days
97
Gas Production
7,917,825
Ft3 of Gas Produced/lb of VM Added
18
% Reduction
44
(VK)
55
% (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number:
WWTP Name: North Durham WRF NPDES Number:
✓Ionitoring Period: From 03/01/14 To 04/31/14
W00003504
NCO023841
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
U nnnlienhle to nitrrnntive nrrfnrmed W..lace A nr C lncc Rl ram nlnfe fhe fnllnwina mnniinrina datn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10to the 61
MPN
1,948
8,728
100,629
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. l
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent —North Durham WRF
Ireparer Name and Title (print or type)
i nature of Preparer* D atel
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f. COL /g. is
y
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21 /2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. /g. is
2/20/2014
57
125
37
152
417
123
84
108
4/16/2014
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

.North Durham Water Reclamation Facility
in 76
%
Sludge Report
out 64
%
Mar'14
PRIMARY SLUDGE TO DIGESTER - A
TO GBT
WEEK
Gallons
Solids
Lbs Dry
% Vol
lbs VM
WEEK Gallons
lbs. D.S.
Ibs. V.M.
1
74,208
4.62
28,593
82
23,343
1 662,165
66,269
48,443
2
71,085
5.68
33,674
76.6
25,787
2 912,473
98,930
72,219
3
78,982
5.56
36,624
77.4
28,362
3 920,747
92,148
67,729
4
106,862
5.35
47,681
80
38,160
4 1,203,425
120,439
88,522
TOTAL
( 331,137
5.3
146,572
78.9
115,653
TOTAL 3,698,810
377,787
276,914
WASTING TOTAL
WEEK Gallons Solids Lbs Dry % Vol lbsVM
1
902,436
1.2
90,316
73.1
66,021
2
789,924
1.3
85,644
73
62,520
3
939,238
1.2
93,999
73.5
69,089
4
1,114,817
1.2
111,571
73.5
82,005
TOTAL
3,746,415
1.23
381,529
73.3
279,634
ANAEROBIC
SLUDGE
TO PRESS
WEEK
Gallons
Solids
Lbs Dry
% Vol
lbs; VM
1
255,752
3.7
78,920
63.5
50,114
2
127,967
3.9
41,623
64.3
26,763
3
189,846
3
47,499
64.8
30,780 _
4.
326,697
3
81,740
64.6
52,804
TOTAL
900,262
3.4
249,782
64.3
160,461
Summary
Total Gallons to Anaerobic Dig.
1,013,090
Total Pounds of Dry Solids to Anaerobic Dig.
519,932
Total Pounds of Vol. Solids to Anaerobic Dig.
393,848
Total Gallons from Anaerobic Dig.
900,262.
Total lbs. of Dry Solids from Anaerobic Dig.
249,782
Total lbs. of Vol. Solids from Anaerobic Dig.
160,461
Detention Time - Days
112
Gas Production
9,063,218
Ft3 of Gas Produced/lb of VM Added
23
} % Reduction
43
TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons '% Solids Lbs Dry % Vol lbsVM
1
140,922
6.25
73,456
73.1
53,696
2
175,666
6.3
92,298
75
69,178
3
158,700
6.7
88,678
74.3
65,888
4
206,665
6.9
118,927
75.2
89,433
TOTAL
681,953
6.54
373,360
74.4
278,195
SOLIDS OFF PRESS
WEEK
Yds
% Solids
1
192
14.89
2
72
14.85
3
96
15.13
4
264
14.74
TOTAL
624
14.9
(VK) 59 % (AMB)

North Durham Water Reclamation Facility
in 75
%
Sludge Report
out
66
%
Apr'14
PRIMARY SLUDGE TO DIGESTER
- A
TO GBT
WEEK
Gallons
%
Lbs Dry
% Vol
lbs VM
WEEK
Gallons
lbs. D.S.
lbs. V.M.
1
123,360
4.38
45,062
76
34,365
1
1,101,475
119,422
88,850
2
54,555
5.08
23,113
71.6
16,558
2
1,382,701
126,849
93,234
3
118,317
3.98
39,224
75.3
29,516
3
1,103,202
110,408
80,598
4
143,945
4.07
48,820
76.6
37,396
4
1,020,433
110,635
82,091
TOTAL
440,177
4.38
156,220
74.9
117,835
TOTAL
4,607,811
467,315
344,774
WASTING TOTAL
TWAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
%
Lbs Dry
% Vol
lbs; VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
1
1,227,025
1.3
133,034
74.4
98,977
1
180,129
7.2
108,164
75.2 81,339
2
1,199,241
1.1
110,018
73.5
80,,864
2
227,324
7.3
138,399
74.6 103,246
3
1,192,809
1.2
119,376
73
87,145
3
204,524
8.2
139,870
74.25 103,853
4
1,394,235
1.3
151,163
74.2
112,163
4
171,063
6.73
95,943
74.5 71,478
TOTAL
5,013,310
1.23
513,592
73.8
379,148
TOTAL
783,040
7.36
482,376
74.6 359,916
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK
Gallons
%
Lbs Dry
% Vol
lbs VM
WEEK
Yds
%Solids
1
432,582
3
108,232
65.2
70,567
1
192
28.55
2
256,743
2.7
57,813
66.1
38,215
2
216
16.24
3
372,041
2.7
83,776
65.9
55,209
3
120
15.23
4
488,160
2.75
111,959
67.7
75,741
4
408
14.66
TOTAL
1,549,526
2.79
361,781
66.2
239,731
TOTAL
936
18.67
Summary
Total Gallons to Anaerobic Dig.
1,223,217
Total Pounds of Dry Solids to Anaerobic Dig.
638,596
Total Pounds of Vol. Solids to Anaerobic Dig.
477,752
Total Gallons from Anaerobic Dig.
1,549,526
Total lbs. of Dry Solids from Anaerobic Dig.
361,781
Total lbs. of Vol. Solids from Anaerobic Dig.
239,731
Detention Time - Days
92
Gas Production
8,609,370
Ft3 of Gas Produced/lb of VM Added
18
% Reduction
34 (VK) 50 % (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
WWTP Name: North Durham WRF NPDES Number: NCO023841
Monitoring Period: From 05/01/14 To 6/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 'Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Unnnlirnhle to alternative nerformed (Gins.- A or Chm R) rmmnlete the fn1inwinv mnnitnrinv dntn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic(
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61
MPN
3,125
11,135
30,864
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN pergram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying— Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent —North Durham WRF
reparer Name and Title (print or type) Land Applier Name and Title (if applicable) (type or print)
Z �5
S' ature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
fcol. / g. is
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/20141
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21 /2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN .
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. / g. is
2/20/2014
57
IWAA,<
125
<... �
37
152
417�
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

North Durham Water Reclamation Facility
Sludge Report
May '14
PRIMARY SLUDGE TO DIGESTER - A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
1
149,717
4.12
51,444
76
2
104,456
4.12
35,892
79
3
77,961
6.6
42,913
65.6
4
91,199
5.32
40,439
66.5
TOTAL
423,333
5.04
170,687
71.8
WASTING TOTAL
WEEK
Gallons
% Solids
Lbs Dry
% Vol
1
1,407,421
1.3
152,593
71.4
2
1,388,029
1.4
162,066
74.2
3
1,116, 525
1.3
121,054
72.6
4
1,684,832
1.2
168,618
71
TOTAL
5,596,807
1.3
604,330
72.3
ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
% Solids
Lbs Dry
% Vol
1
289,578
2.4
57,962
65.4
2
436,864
2.6
94,730
67.1
3
300,406
2.7
67,645
67.1
4
410,130
3.6
123,137
63.2
TOTAL
1,436,978
2.83
343,474
65.7
in
72 %
out
66
%
TO GBT
lbs VM
WEEK
Gallons
lbs. D.S.
lbs. V.M.
39,200
1
939,815
101,895
72,753
28,362
2
1,569,814
183,291
136,002
28,142
3
1,139,462
123,540
89,690
26,905
4
1,662,834
166,416
118,156
122,609
TOTAL
5,311,925
575,143
416,601
TWAS FROM GRAVITY
BELT THICKENER
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
108,951
1
158,391
7.7
101,716
71.9
73,133
120,253
2
255,912
6.85
146,200
74
108,188
87,885
3
181,061
6.15
92,868
73.2
67,979
119,719
4
323,672
5.4
145,769
67.6
98,540
436,808
TOTAL
919,036
6.53
486,552
71.7
347,841
SOLIDS OFF PRESS
lbs VM
WEEK
Yds
% Solids
37,907
1
264
15.28
63,564
2
396
14.78
45,390
3
84
15.44
77,823
4
96
15.58
224,684
TOTAL
840
15.27
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons % Solids Lbs Dry % Vol
lbs VM
1
2 1.97 68.8
3
4
TOTAL 1.97 68.8
Summary
Total Gallons to Anaerobic Dig.
1,342,369
Total Pounds of Dry Solids to Anaerobic Dig.
657,240
Total Pounds of Vol. Solids to Anaerobic Dig.
470,450
Total Gallons from Anaerobic Dig.
1,436,978
Total lbs. of Dry Solids from Anaerobic Dig.
343,474
Total lbs. of Vol. Solids from Anaerobic Dig.
224,684
Detention Time - Days
84
Gas Production
9,349,436
Ft3 of Gas Produced/lb of VM Added
20
% Reduction
24
(VK) 52 % (AMB)

North Durham Water Reclamation Facility
in
72 %
Sludge Report
out
64
%
Jun '14
PRIMARY SLUDGE TO DIGESTER
- A
TO
GBT
WEEK Gallons % Solids Lbs Dry % Vol
lbs VM
WEEK
Gallons
lbs. D.S.
lbs. V.M.
1 80,217 3.78 25,289 71
17,965
1
1,227,949
122,893
87,500
2 79,418 4.56 30,203 '68.3
20,635
2
1,459,726
146,089
104,454
3 87,267 4.6 33,479 74.1
24,801
3
1,247,076
114,407
82,258
4 55,703 5.05 23,460 82
19,234
4
1,780,707
178,213
128,670
TOTAL 302,605 4.5 112,431 73.9
82,635
TOTAL
51-715,458
561,602
402,882
WASTING TOTAL
TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry % Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
1 1,247,669 1.2 124,867 71.2
88,905
1
182,007
7.2
109,292
71.5 78,143
2 1,185,144 1.2 118,609 71.5
84,806
2
208,139
7
121,512
71.7 87,124
3 1,316,054 1.1 120,735 71.9
86,808
3
174,534
7.6
110,627
72 79,651
4 1,597,302 1.2 159,858 72.2
115,417
4
237,915
8.05
159,729
72.3 115,484
TOTAL 5,346,169 1.18 524,069 71.7
375,936
TOTAL
802,595
7.46
501,159
71.9 360,402
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK Gallons % Solids Lbs Dry % Vol
lbs VM
WEEK
Yds
% Solids
1 328,607 3.3 90,439 64.5
58,333
1
348
15.52
2 257,619 3.3 70,902 64.7
45,874
2
324
15.96
3 223,413 3.7 68,941 64
44,122
3
312
15.73
4 312,192 3.9 101,544 63.7
64,683
4
480
15.92
TOTAL 1,121,831 3.55 331,825 64.2
213,012
TOTAL
1464
15.78
ANAEROBIC SLUDGE TO BEDS
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
1
2.6
64.4
2
3
4
3.2
61.5
TOTAL
2.9
62.95
Summary
Total Gallons to Anaerobic Dig.
1',105,200
Total Pounds. of Dry Solids to Anaerobic Dig.
613,590
Total Pounds of Vol. Solids to Anaerobic Dig.
443,037
Total Gallons from Anaerobic Dig.
1,121,831
Total lbs. of Dry Solids from Anaerobic Dig.
331,825
Total lbs. of Vol. Solids from Anaerobic Dig.
213,012
Detention Time - Days
102
Gas Production
5,487,517
F1:3 of Gas Produced/lb of VM Added
12
% Reduction
32
(VK)
52
% (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
WVWTP Name: North Durham WRF NPDES Number: NCO023841
Aonitoring Period: From 07/01/14 To 08/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to alternative nerfnrmed lrinss A nr Class itl rmmnlete the fnllawina mnnitnrina datn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
MPN
1,463
4,449
14,545
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3
Option/Alt.4
(VS reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent —North Durham VW
'-Ireparer Name and Title (print or type) 21*5
jgn,ture of Preparer* ate
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliforMg total solids
Sample Set #2
MPN
f. coliforMg total solids
Sample Set #3
MPN
f. coliformg total solids
Sample Set #4
MPN
f. coliforMg total solids
Sample Set #5
MPN
f. coliformg total solids
Sample Set #6
MPN
f. coliformg total solids
Sample Set #7
MPN
f. colfform/g total solids
Geometric Mean
f.Col. /g, is
,., uxaw:.. ,r.m
.. w...... ... w.ry .?t'A.. a
s, .. .. ..,r " r. .. .^me[ ,....
,,..k....c:•a v^ > ... . r
m. ."+&a..
.k .
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliformg total solids
Sample Set #2
MPN
f. coliforMg total solids
Sample Set #3
MPN
f. coliforMg total solids
Sample Set #4
MPN
f. coliforMg total solids
Sample Set #5
MPN
f. coliforMg total solids
Sample Set #6
MPN
f. coliformg total solids
Sample Set #7
MPN
f. coliformg total solids
Geometric Mean
fcol. /g. is
2/20/2014
57
125
37
152
417
123
84
108
4/16/2014
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
11408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

North Durham Water Reclamation Facility
Sludge Report
Jul '14
PRIMARY SLUDGE TO DIGESTER - A
WEEK
Gallons
Solids
Lbs Dry
-%Vol
1
44,406
4.83
17,869
82
2
56,703
4
18,916
77.4
3
80,027
5.2
34,706
68
4
70,779
5.38
31,728
73.2
TOTAL
251,915
4.85
103,220
75
WASTING TOTAL
WEEK
Gallons
Solids
Lbs Dry
% Vol
1
1,298,901
1.1
119,161
71.6
2
1,358,142
2.05
232,202
72
3
1,629,198
1
135,875
71.3
4
1,988,020
1
165,801
71.3
TOTAL
6,274,261
1.29
653,039
71.6
in 73 %
out 64 %
TO GBT
lbs VM WEEK Gallons lbs. D.S. lbs. V.M.
14,586
1
1,344,312
123,327
88,302
14,634
2
1,370,438
234,304
168,699
23,586
3
1,741,617
145,251
103,564
23,221
4
2,342,533
195,367
139,297
76,027
TOTAL
6,798,900
698,240
499,862
TWAS FROM GRAVITY BELT THICKENER
lbs VM WEEK Gallons % Solids Lbs Dry % Vol lbs VM
85,319
1
174,969
7.65
111,632
71.45
79,761
167,185
2
168,539
7.5
105,421
71.83
75,719
96,879
3
223,143
7.2
133,993
73.4,
98,351
118,216
4
287,009
7.05
168,753
71.88
121,291
467,599
TOTAL
853,660
7.35
519,799
72.1
375,122
ANAEROBIC SLUDGE TO PRESS SOLIDS OFF PRESS
WEEK
Gallons
Solids
Lbs Dry
% Vol
lbs VM
WEEK
Yds
1
194,092
&9
63,130
65.4
41,287
1
348
2
-283,345
3.45
81,527
64.4
52,463
2
168
3'
247,500
4
82,566
64.1
52,925
3
372
4
511,895
4
170,768
63.9
109,121
4
240
TOTAL
1,236,832
3.84
397,991
64.4
255,795
TOTAL
1128
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons Solids Lbs Dry % Vol lbs VM
1
2
3
4 3.1 63.2
TOTAL 3.1 63.2
Summary
Total Gallons to Anaerobic Dig.
1,105,575
Total Pounds of Dry Solids to Anaerobic Dig.
623,019
Total Pounds of Vol. Solids to Anaerobic Dig.
451,148
Total Gallons from Anaerobic Dig.
1,236,832
Total lbs. of Dry Solids from Anaerobic Dig.
397,991
Total lbs. of Vol. Solids from Anaerobic Dig.
255,795
Detention Time - Days
102
Gas Production
7,758,145
Ft3 of Gas Produced/lb of VM Added
17
% Reduction
32
(VK)
% Solids
16.2
15.68
16.97
16.47
16.33
48 % (AMB)

North Durham Water Reclamation Facility
in 71
%
Sludge Report
out
62
%
Aug '14
PRIMARY SLUDGE TO DIGESTER -A
TO GBT
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Gallons
lbs. D.S.
Ibs. V.M.
1 42,867 5.86 20,950
78
16,417
1
1,443,591
132,435
93,499
2 40,441 6.9 23,272
65.9
15,332
2
1,223,254
102,019
72,230
3 47,341 6.36 25,111
62.4
15,679
3
1,528,589
140,233
99,004
4 77,511 6.75 43,635
77.7
33,897
4
1,683,607
140,413
96,042
TOTAL 208,160 6.47 112,968
71.1
81,324
TOTAL
5,879,041
515,100
360,776
WASTING TOTAL
TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
1 1,412,804 1.1 129,611
70.6
91,505
1
179,939
7.3
109,550
72.4 79,315
2 1,200,931 1 100,158
70.8
70,912
2'
153,161
7.25
92,609
70.45 65,243
3 1,415,458 1.1 129,854
70.6
91,677
3
189,652
8.05
127,327
70.7 90,020
4 1,879,005 1 156,709
68.4
107,189
4
213,639
7.6
135,413
70.25 95,128
TOTAL 5,908,198 1.05 516,331
70.1
361,283
TOTAL
736,391
7.55
464,899
71 329,705
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Yds
% Solids
1 321,124 3.3 88,380
61.4
54,265
1
15.59
2 329,736 3.3 90,750
63.6
57,717
2
312
16.25
3 258,902 3.5 75,573
62.3
47,082
3
264
16.3
4 418,590 3.5 122,186
62
75,756
4
384
16.25
TOTAL 1,328,352 3.4 376,890
62.3
234,820
TOTAL
960
16.1
Summary
Total Gallons to Anaerobic Dig.
944,551
Total Pounds of Dry Solids to Anaerobic Dig.
577,867
Total Pounds of Vol. Solids to Anaerobic Dig.
411,029
Total Gallons from Anaerobic Dig. -.
1,328,352
Total lbs. of Dry Solids from Anaerobic Dig.
376,890
Total lbs. of Vol. Solids from Anaerobic Dig.
234,820
Detention Time - Days
120
Gas Production
8,429,698
Ft3 of Gas Produced/lb of VM Added
21
% Reduction
32
(VK)
43
% (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
WWTP Name: North Durham WRF NPDES Number: NCO023841
;RonitoringPeriod: From 09/01/14 To 10/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followine monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
MPN
922
2,148
8,280
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
(VS reduction) X
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent — North Durham WRF
?rep re am nd Title (print or type)
ature of Preparer* a
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.Col. /g. is
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.Col. / g. is
2/20/2014
57
125
37
152
417
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

North Durham Water Reclamation Facility
Sludge Report
Sep'14
PRIMARY SLUDGE TO DIGESTER -A
WEEK
Gallons
Solids
Lbs Dry
% Vol
1
54,972
5.2
23,840
82
2
56,129
4.72
22,095
83.7
3
44,280
4.76
17,578
85.7
4
76,681
5.44
34,808
80.2
TOTAL
232,062
5.03
98,322
82.9
WASTING TOTAL
WEEK
Gallons
Solids
Lbs .Dry
%Vol
1
1,122,945
1
93,654
' 68.6
2
1,112,825
3
1,542,885
0.9
115,809
69.9
4
1,268,444
0.9
95,209
70.2
TOTAL
5,047,099
0.93
304,672
69.6
ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
Solids
Lbs Dry
% Vol
1
215,209
. 3.8
68,204
62.9
2
184,551
3.5
53,870
63.2
3
243,231
3.4
68,971
62.7
4
549,380
3.7
169,528
63.7
TOTAL
1,192,371
3.6
360,573
63.1
in 74 %
out 63 %
TO GBT
lbs VM WEEK Gallons lbs. D.S. lbs. V.M.
19,507
1
1,199,126
100,007
68,605
18,502
2
1,397,568
15,068
3
1,906,349
143,091
100,020
27,906
4 _
1,145,550
85,985
60,361
80,984
TOTAL
5,648,593
329,083
228,987
TWAS FROM GRAVITY BELT THICKENER
lbs VM WEEK Gallons % Solids Lbs Dry % Vol lbs VM
64,246
1
168,535
7.15
100,499
69.4
69,696
2
68,589
7.55
43,188
69.4
29,973
80,950
3
177,688
7.55
111,885
70.4
78,767
66,837
4
25,591
6.8
14,513
70.6
10,250
212,034
TOTAL
440,403
7.26
270,086
69.9
188,686
SOLIDS OFF
PRESS
lbs VM
WEEK
Yds
% Solids
42,900
' 1
264
16.63
34,046
2
216
16.33
43,245
3
360
16.02
107,989
4
408
15.97
228,180
TOTAL
1248
16.24
Summary
Total Gallons to Anaerobic Dig.
672,465
Total Pounds of Dry Solids to Anaerobic Dig.
368,407
Total Pounds of Vol. Solids to Anaerobic Dig.
269,670
Total Gallons from Anaerobic Dig.
1,192,371
Total lbs. of Dry Solids from Anaerobic Dig.
360,573
Total lbs. of Vol. Solids from Anaerobic Dig.
228,180
Detention Time - Days
168
Gas Production
4,120,650
Ft3 of Gas Produced/lb of VM Added
15
% Reduction
41
(VK)
15 % (AMB)

North Durham Water Reclamation Facility
in 75
%
Sludge Report
out
64
%
Oct '14
PRIMARY SLUDGE TO DIGESTER -
A
TO GBT
WEEK . Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Gallons
lbs. D.S.
lbs. V.M.
1 52,804 5.16 22,724
86
19,570
1
1,775,325
133,256
92,746
2 51,591 5.42 23,321
82.7
19,277
2
1,354,382
101,660
73,297
3 48,569 6.34 25,681
75.6
19,425
3
1,365,053
102,461
73,464
4 84,660 5.24 36,980
81
29,959
4
1,631,249
503,371
326,184
TOTAL 237,624 5.54 108,706
81.4
88,230
TOTAL
6,126,009
840,748
565,692
WASTING TOTAL
TWAS FROM GRAVITY BELT THICKENER
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
1 1,540,821 0.9 115,654
69.6
80,495
1
145,225
7.15
86,599
71 61,485
2 1,310,186 0.9 98,343
72.1
70,905
2
45,621
7.1
27,014
72.9 19,693
3 1,165,595 0.9 87,490
71.7
62,730
3
101,531
7.05
59,697
72.6 43,340
4 1,533,170 3.7 473,106
64.8
306,572
4
190,175
7.6
120,541
73.1 88,115
TOTAL 5,549,7721.6 774,592
69.6
520,703
TOTAL
482,552
7.23
293,851
72.4 212,634
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK Gallons % Solids Lbs Dry
% Vol
lbs VM
WEEK
Yds
% Solids
1 363,638 3.5 106,146
65.2
69,207
1
336
16.13
2 288,915 3.7 89,153
64.1
57,147
2
312
16.23
3 429,354 3.6 128,909
63.6
81,986
3
360
15.66
4 500,245 3.7 154,366
64.8
100,029
4
360
15.7
TOTAL 1,582,152 3.63 478,574
64.4
308,370
TOTAL
1368
15.93
Summary
Total Gallons to Anaerobic Dig.
720,176
Total Pounds of Dry Solids to Anaerobic Dig.
402,557
Total Pounds of Vol. Solids to Anaerobic Dig.
300,864
Total Gallons from Anaerobic Dig:
1,682,152
Total lbs. of Dry Solids from Anaerobic Dig.
478,574
Total lbs. of Vol. Solids from Anaerobic Dig.
308,370
Detention Time - Days
157
Gas Production
Ft3 of Gas Produced/lb of VM Added
% Reduction
41
(VK)
-2
% (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
WWTP Name: North Durham WRF NPDES Number: NCO023841
Monitoring Period: From 11/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2xl0to the 6 1h
MPN
3,472
8,610
20,134
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
(VS reduction) X
(40-day bench)
Option/Alt. 5
Option/Alt. 6
(14-Day Aerobic)
(Alk Stabilization)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
Option/Alt. 3 Option/Alt. 4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
No vector attraction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.11,06 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
John Dodson, Superintendent — North Durham WRF
Preparer Name and Title (print or type)
2
S ature of Preparer* i7a�e
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.Col. / g. is
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/20141
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205.
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f col. / g. is
�. <..,.........
- ... .x _
�, �rw. . ..a., ._.
2/20/2014
57
125
37
152
417
123
84
108
4/16/2014
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391,
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

North Durham Water Reclamation Facility
in 77
%
Sludge -Report
out 65
%
Nov'14
PRIMARY SLUDGE TO DIGESTER
- A
TO GBT
WEEK
Gallons
Lbs Dry
% Vol
lbs VM
WEEK
Gallons
lbs. D.S.
lbs. V.M.
Solids
1
49,791
6
24,915
85
21,093
1
966,454
72,542
50,925
2
48,962
5
22,377
80
17,978
2
984,023
73,861
53,697
3
69,854
5
31,459
85
26,819
3
939,108
70,489
51,175
4
24,273
7
14,373
78
11,264
4
62,571
4,697
3,386
TOTAL
192,880
6
93,125
82
77,154
TOTAL
2,952,156
221,589
159,183
WASTING
TOTAL
TWAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
Lbs Dry
% Vol
lbs VM
WEEK
Gallons
% Solids
Lbs Dry
% Vol lbs VM
Solids
1
940,120
1
70,565
70
49,537
1
110,628
6.35
58,587
73.6 43,120
2
923,486
1
69,317
73
50,393
2
115,158
7.05
67,709
74.2 50,240
3
933,079
1
70,037
73
50,847
3
131,664
6.65
73,022
74.7 54,548
4
317,510
1
23,832
72
17,183
4
0
6.7
0
73.5 0
TOTAL
3,114,195
1
233,751
72
167,960
TOTAL
357,450
6.69
199,319
74 147,908
ANAEROBIC SLUDGE TO PRESS
SOLIDS OFF PRESS
WEEK
Gallons
Lbs Dry
% Vol
lbs VM
WEEK
Yds
% Solids
Solids
1
301,116
4
87,896
64
56,253
_ 1
240
14.63
2
287,550
4
83,936
65
54,642
2
300
15.93
3
302,309
4
88,244
65
57,623
3
264
15.82
4
1,825
3.4
517
65
336
4
372
15.6
TOTAL
892,800
3
260,593
65
168,855
TOTAL
1176
15.49
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons % Solid: Lbs Dry % Vol lbs VM
1
2 3.5 76.4
3
.4
TOTAL 3.5 76.35
Summary
Total Gallons to Anaerobic Dig.
550,330
Total Pounds of Dry Solids to Anaerobic Dig.
292,444
Total Pounds of Vol. Solids to Anaerobic Dig.
225,062
Total Gallons from Anaerobic Dig.
892,800
Total lbs. of Dry Solids from Anaerobic Dig.
260,593
Total lbs. of Vol. Solids from Anaerobic Dig.
168,855
Detention Time - Days
206
% Reduction
44
(VK) 25 % (AMB)

North Durham Water Reclamation Facility
Sludge Report
Dec ' 14
PRIMARY SLUDGE TO DIGESTER - A
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
99,181
5.96
49,299
76
37,290
2
99,843
5.76
47,963
83.1
39,867
3
60,264
6.54 .
32,870
81.3
26,723
4
61,333
6.28
32,123
77.4
24,857
TOTAL
320,621
6.14
162,256
79.4
. 128,737
WASTING TOTAL
WEEK Gallons % Solids Lbs Dry % Vol
1
1,060,450
1.1
97,286
74.3
2
652,399
1
54,410
74.6
3
709,420
1.1
65,082
74.6
4
1,016,559
1.15
97,498
74.7
TOTAL
3,438,828
1.09
314,276
74.5
ANAEROBIC
SLUDGE TO PRESS
WEEK
Gallons
% Solids
Lbs Dry
`% Vol
1
301,146
3.5
87,905
65.4
2
238,948
3.6
71,742
65.3
3
338,538
3.4
95,996
65.7
4
530,801
3.55
157,154
65
TOTAL
1,409,433
3.51
412,796
65.4
Summary
Total Gallons to Anaerobic Dig.
Total Pounds of Dry Solids to Anaerobic Dig.
Total Pounds of Vol. Solids to Anaerobic Dig.
Total Gallons from Anaerobic Dig.
Total Ibs. of Dry Solids from Anaerobic Dig.
Total Ibs. of Vol. Solids from Anaerobic Dig.
Detention Time - Days
% Reduction
Ibs VM
72,283
40,590
48,551
72,782
234,207
in
77
%
out
65
%
TO GBT
WEEK
Gallons
Ibs. D.S.
lbs. V.M.
1
798,773
73,279
54,447
2
735,221
61,317
45,743
3
818,272
75,068
56,001
4
1,303,620
125,030
93,335
TOTAL
3,655,886
334,695
249,525
TWAS FROM GRAVITY BELT THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
108,959
6.9
62,702
75.4
47,277
2
96,484
-7.2
57,937
75.3
43,626
3
114,281
6.5
61,952
75.85
46,990
4
186,598
6.2
96,486
74.73
72,099
TOTAL
506,322
6.7
279,076
75.3
209,993
SOLIDS OFF PRESS
Ibs VM
WEEK
Yds
% Solids
57,490
1
312
15.08
46,847
2
240
14.54
63A9
3
204
14.23
102,150
4
360
14.66
269,556
TOTAL
1116
14.63
826,943
441,332
338,730
1,409,433
412,796
269,556
137
43 (VK) 20
% (AMB)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham
WQ Permit Number: WQ0003504
WWTP Name: South Durham WRF NPDES Number: NCO047597
✓Ionitoring Period: From 01/01/14 To 02/28/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annliCahle to alternative performed (Class A or Class R) rmmnlefe the fnllnwina mnnifnrina dafa-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6 1h
MPN
37
108
417
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent — South Durham VW
-reparer Nam and Title (print or e)
��� ��
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.Col. /g. is
2/20/2014
�.,.�. 16,667�
66,667
5,926
5,970
1,333
�� 4,965
,
��� 5,634-
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/20141
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. Ig. is
t,�
s �. , -R .
�... x
.... .
�.
2/20/2014
57
125
37
152
417
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

South Durham Water Reclamation Facility
Sludge Report
inuary'2014
SD PRIMARY SLUDGE TO DIGESTER `GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK Gallons
% Solids
Lbs Dry
% Vol
lbs VM :: Gallons % Solids Lbs Dry % Vol lbs VM
1 199,810
4.2
69,989
78.5
54,942
2 224,599
3.3
61,814
86.3
53,346
3 191,060
3.0
47,803
84.6
40,442
4 304,108
3.2
79,892
88.9
70,984
TOTAL 919,677
3.4
259,499
84.6
219,713
WASTING TO GRAVITY THICKENER ,4WAS GBT TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Gallons
% Solids
Lbs Dry
% Vol
lbsVM
9
1,159,575
1.14
110,414
,99.7
110,082
j 165,099
6.4
88,123
75.3
66,357
2
1,161,010
1.11
107,161
77.9
83,479
? 198,928
6.8
112,816
75.2
84,838
3
1,155,266
1.12
107,567
88.3
94,982
:! 184,442
6.3
96,910
75.0
72,682
4
1,651,295
1.06
146,367
83.8
122,655
280,419
6.8
159.031
76.0
120,864
TOTAL
5,127,146
1.11
471,508
87.4
411,198
° 828,888
6.6
456,880
75.4
344,740
SD ANAEROBIC SLUDGE TO PRESS
! SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
i Yds
% Solids
% Vol
Gallons % Solids Lbs Dry % Vol lbs VM
-64:7--
401847'
219-.
-17:0.----
66:5-
- 300;873 -
3.4
- 85,316
2
335,155
2.8
78,265
64.7
50,638 ;;
275
16.9
66.4
367,778
3.2
98,153
74.7
73,320
14
331,601
2.7
74,670
64.7
48,311
275
16.7
67.1
377,107
3.1
97,497
74.1
72,245
i
380,122
2.8
88,766
65.3
57,920
325
15.8
66.7
481,683
3.3
132,569
74.8
99,095
TOTAL
1,317,234
2.8
304,835
64.8
197,716 ?
1,095
16.6
66.7
1,527,441
3.3
413,534
74.5
308,221
ANAEROBIC SLUDGE TO BEDS
':SOLIDS OFF DRYING BEDS
Beds Yards
WEEK
Gallons
% Solids
Lbs Dry
%, Vol
lbsVM :? Cleaned % Solids Removed
1
.
2
3
123,700
2.7
27,855
65.4
18,217
4
116,700
2.7
26,279
65.3
17,160
TOTAL
240,400
2.7
54,133
65.4
35,377
Summary
Total Gallons to Anaerobic Dig.
1,748,465
Total Pounds of Dry Solids to Anaerobic Dig.
716,379
Total Pounds of Vol. Solids to Anaerobic Dig.
564,453
Total Gallons from Anaerobic Dig.
1,657,634
.
Total lbs, of Dry Solids from Anaerobic Dig.
358,968
Total lbs. of Vol. Solids from Anaerobic Dig.
233,093
Detention Time - Days
71
Gas Production Ft3
4,743,443
Ft3 of Gas Produced/lb of VM added
8.4
' "eduction
54
% (VK)
lbs Polymer
$fib
rounds of Polymer Used - GBT
1,824
$1.75
Pounds of Polymer Used - BFP
2,360
$1.75
59 % (LBS)
Poly Cost $!DT
3,192
4,130 27.10

South Durham Water Reclamation Facility
Sludge Report
�abruary '2014
SD PRIMARY SLUDGE TO DIGESTER
GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
191,090
3.6
57,373
88.8
50,947
2
199,637
3.2
53,279
87.3
40,513
3
147,612
3.1
38,164
85.8
32,744
4
181,855
3.1
47,017
86.9
40,858
TOTAL
720,194
3.3
195,832
87.2
171,062 .•
WASTING TO GRAVITY THICKENER
JWAS GBT TO ANAEROBIC DIGESTER
WEEK
Gallons.
% Solids
Lbs Dry
% Vol
Ibs VM
: Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
1,155,195
1.13
109,006
89.0
97,015
192,963
6.3
101,387
77.0
78,068
2
1,165,124
1.05
100,975
81.5
82,295
196,226
6.8
111,284
77.4
86,134
3
1,154,867
1.00
96,082
69.6
66,873 ..170,995
6.3
92,997
74.8
09,562
4
1.232,980
1.10
113,319
90.9
103,007
181,113
6.8
102,713
77.0
79,089
TOTAL
4,698,166
1,07
419,382
82.8
349,190
747,297
6.6
408,380
76.6
312,852
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Yds
% Solids
% Vol
Gallons
% Solids Lbs Dry % Vol lbs VM
....... ..... _
1
.._...-...--.......
334,140
_.........-_.._.
2.7
-_._.
75,242
_.-........
64,9
48..._.,832__.--.-.._...
-._._...__._...._
275
... ................__...._..........--.........._.......-
16.6
66.8
343,466
_....__.............. _........ __......._............................ .--- ..... ..... .... ......... .... _.
3.3 94,529 76.1 71,936
2
260,524
2.7
58,665
64.8
38,015
219
16.4
66.4
346,769
3.4 98,330 76.3 75,026
73
337,965
2.7
76,103
64.8
49,315
275
16.7
66.0
350,109
2.8 81,757 76.0 62,136
4
336,787
2.6
73,029.
64.6
47,177
275
16.5
64.8
361,090
3.0 90,345 75.5 68,210
TOTAL
1,269,416
2.7
283,038
64.8
183,338
1,045
16.6
66.0
1,401,434
3.1 364.961 76.0 277,308
ANAEROBIC SLUDGE TO BEDS
:SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Cleaned
% Solids
Removed
1
2
3
4
TOTAL
Summary
Total Gallons to Anaerobic Dig.
1,467,491
Total Pounds of Dry Solids to Anaerobic Dig.
604,212
Total Pounds of Vol. Solids to Anaerobic Dig.
483,913
Total Gallons from Anaerobic Dig.
1,269,416
Total lbs. of Dry Solids from Anaerobic Dig.
283,038
Total lbs. of Vol. Solids from Anaerobic Dig.
183,338
Detention Time - Days
77
Gas Production Ft3
4,003,405
Ft3 of Gas Produced/lb of VM added
8.3
-educ#ion
59
% (VK)
lbs Polymer
$Ab
Pounds of Polymer Used - GBT
1,404
$1.75
Pounds of Polymer Used - BFP
2,311
$1.76
62 % (LBS)
Poly Cost $/DT
2,457
4,044 28.58

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
`. WTP Name: South Durham WRF NPDES Number: NCO047597
,Monitoring Period: From 03/01/14 To 04/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlienhlr to niternntivr nerfnrmrd W.1ncc A nr Clnee Rl rmmnlrtr thn fnllnwina man itnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2xl0to the 6 1h
MPN
26
444
11,194
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Mt. 3 Option/Mt.4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent— South Durham WRF
' Ireparer Name and Title (Print or t p
Signature of Preparer*
Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. colfform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. /g. is
�
2/20/2014
16,667
66,6675,926
5,970
1,333
4,965
5,634
7,601
4/16/20141
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286.
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20, 1341
5,6341
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f, coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. / g. is
2/20/2014
57
125
37
152
417
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
.7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

South Durham Water Reclamation Facility
Sludge Report
arch `2014
SD PRIMARY SLUDGE TO DIGESTER
'GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
195,180
3.4
55,345
87.6
48,482
2
162,970
3.9
53,008
79.4
42,088
3
265,922
3.5
77,623
82.3
63,883
4
393,214
2.7
88,644
83.1
73,580 .
TOTAL
1,017,286
3.4
274,519
63.1
228,034
WASTING TO GRAVITY THICKENER
.TWAS GBT TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
1,290,814
1.08
115,974
83.3
96,606
: 101,766
7.0
94,439
77.0
72,718
2
1,330,773
1.07
118,851
86.2
102,449
232,950
6.0
116,568
75.8
88,359
3
1,334,917
1.06
118,012
79.4
93,702 ::
80,124
6.2
41,431
75.4
31,239
4
1,906,983
1.10
174,485
85.7
149,634
274,849
6.3
144,411
75.8
109,464
TOTAL
5,863,487
1.08
527,322
83.7
442,291 -.:
749,689
6.4
398,849
76.0
301,779
SD ANAEROBIC SLUDGE TO PRESS
!
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Yds
% Solids
% Vol
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
..4.......
269,574
. 2:7
6T,703
65.2_
.._............_. _._....._..._.
39,57.8
__.
219
...-..... .._..............
16.8
........... _._..
66.9
..... ......... _...._........_..._.._...
290,317
...........
3.3
................... .........
79,901
.._...
76.7
- -. _ ._.._ ..._.. .
60,485
2
346,811
2.6
75,202
64.5
48,506
275
16.7
66.7
403,674
3.4
114,460
74.0
84,705
69,315
2.6
15,030
64.8
9,740
56
16.6
66.7
133,646
3.6
40,126
74.3
29,814
d
403,955
2.7
90,963
64.9
59,036
325
16.2
66.4
467,656
3.5
136.509
74.9
102,245
TOTAL
1,089,655
2.7
241,898
64.9
156,858 .:
876
16.6
66.7
1;295,293
3.5
371,002
74.7
277,248
ANAEROBIC SLUDGE TO BEDS .;SOLIDS OFF DRYING BEDS
Beds Yards
WEEK Gallons % Solids Lbs Dry % Vol lbs VM Cleaned % Solids Removed
a
2
3 363,745 2.6 79,886 64.6 51,606
4
TOTAL 363,746 2.6 79,886 64.6 51,606
Summalry
Total Gallons to Anaerobic Dig.
1,766,975
Total Pounds of Dry Solids to Anaerobic Dig.
671,368
Total Pounds of Vol. Solids to Anaerobic Dig.
529,813
Total Gallons from Anaerobic Dig.
1,453,400
Total lbs. of Dry Solids from Anaerobic Dig.
321,784
Total lbs. of Vol. Solids from Anaerobic Dig.
208,464
Detention Time - Days
71
Gas Production Ft3
4,178,449
Ft3 of Gas Produced/lb of VM added
7.9
:eduction
54
% (VK)
lbs Polymer
$Ab
r-oiinds of Polymer Used - GBT
1,464
$1.75
Pounds of Polymer Used - BFP
1,884
$1.75
. 61 % (LBS)
Poly Cost $IDT
2,562
3,297 27.26

South Durham Water Reclamation Facility
Sludge Report
;pril '2Q14
SD PRIMARY SLUDGE TO DIGESTER
GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
200,201
3.2
53,430
86.4
46,163
2
234,474
3.2
62,576
82.6
51,688
3
145,945
2.8
34,081
83.8
28,560
4
322,336
4.4
116,284
85.2
100,778
.
TOTAL
902,956
3.4
268,372
84.5
227,190
WASTING TO GRAVITY THICKENER
•TWAS GBT TO ANAEROBIC DIGESTER
WEEK ,
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
1,404,287
1.05
122,923
78.9
96,986
283,155
6.4
151,137
75.8
114,562
2
1,310,431
0.96
104,669
62.6
65,623
166,463
6.4
83,514
75.2
62,802
3
1,330,377
1.02
112,618
71.2
80,184
161,035
6.5
87,297
75.4
65,822
4
1,650,357
0.99
135,713
73.6
99,817
327,217
7.0
191,029
75.3
143,845
TOTAL
5,695,452
1.00
475,922
71.6
342,510
927,870
6.6
512,977
75.4
387,031
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Yds
% Solids % Vol
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
47%22T
21
107,686...-64:8-...fi9;780._.._.......3g4._..
_..-15.8......._...67.0-
526,538
.. 3.3..._....144,914.......MT
..168,251---
2
333,135
2.9
80,572
64.9
52,291
275
16A 66.9
301,759
2.8
70,467
74.3
52,357
113
201.768
2.8
47,117
64.4
30,343
103
16.1 66.4
294,955
3.3
B1,178
74.0
60,071
4
454,286
3.0
113,662
66.2
75,244
382
16.6 65.9
585,133
3.3
161,040
75.1
120,941
TOTAL
1,467,410
2.9
349,037
65A
227,659
1,213
16.1 66.5
1,708.386
3.2
457,598
74.5
341,620
ANAEROBIC SLUDGE TO BEDS
SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
Cleaned
% Solids Removed
1 118,890 2.7 26,772 65.0
17,402
2 95,445 2.9 23,084 65.1
15,028
2
3 233,120 3.0 58,327 64.7
37,737
4
TOTAL 447,455 2.9 108,183 64.9
70,167
2
Summary
Total Gallons to Anaerobic Dig.
1,830,826
Total Pounds of Dry Solids to Anaerobic Dig.
781,348
Total Pounds of Vol. Solids to Anaerobic Dig.
614,221
Total Gallons from Anaerobic Dig.
1,914,865
Total Ibs. of Dry Solids from Anaerobic Dig.
457,220
Total lbs. of Vol. Solids from Anaerobic Dig.
297,826
Detention Time - Days
54
Gas Production Ft3
4,253,881
Ft3 of Gas Produced/lb of VM added
6.9
eduction
53
% (VK) 52 % (LBS)
Ibs Polymer
$Ab Poly Cost $/DT
Pounds of Polymer Used - GBT
11806
$1.75 3,161
Pounds of Polymer Used - BFP
2,721
$1.75 4,762 27.29

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
"VWTP Name: South Durham WRF NPDES Number: NCO047597
Qonitoring Period: From 05/01/14 To 06/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annlirahle to alternative nerfnrmed Wlace A nr Chm- Rl rmmnletP the fnllnwina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 61h
MPN
7,328
12,661
22,843
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent— South Durham WRF
'reparer� Title (print or e)
2- Y /s
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. /g. is
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. / g. is
2/20/2014
57
125
37
152
417
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

South Durham Water Reclamation Facility
Sludge Report
SD PRIMARY SLUDGE TO DIGESTER
GRAVITY THICKENER TO ANAEROBIC DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM Gallons % Solids Lbs Dry % Vol lbs VM
1
185,205
3.3
50,972
86.7
44,193
2
197,337
3.9
64,186
88.3
56,676
3
209,335
3A
59,359
87.6
51,999
4
334.937
2.6
72,628
83.6
60,680
TOTAL
926,814
3.3
247,145
86.5
213,548
WASTING TO GRAVITY THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
1,280,181
1.00
100,767
74.1
79,114
2
1,331,578
0.94
104,025
68.8
71,570
3
1,335,814
0.97
108,510
63.4
68,796
4
1,877,591
0.93
146,178
70.9
103,640
TOTAL
5,825,164
0.96
465,481
69.3
323,120
TWAS GBT TO ANAEROBIC DIGESTER
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
191,816
6.2
99,184
74.6
73,991
192,952
6A
102,990
74.5
76,728
166,441
7.1
98,556
74.7
73,622
236,076
6.8
132,899
72.5
96,285
787,285
6.6
433,630
74.1
320.626
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS
OFF PRESS,
GRAVITY THICKENER TO GBT
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Yds
% Solids % Vol
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
'_-"
323,-820---...
31-­-
-83,18U
64.8-
53,734 ­-
_
275
.__..._...._...._...-_..._-.._..-_..._-..._..
16.4 65.9
....... _....._-....
353,355
.....
2.9
......... _........ _......
85,462
_. _....._.
73.6
_....._.._ _................. ...
62;900
z
326,176
. 3.1
84,330
65.4
55,185
272
17.1 66.4
366,260
3.1
94,690
74.3
70,355
309,246
3.1
79,437
65.2
51,809
256
16.8 66.3
348,297
3.1
90,049
73.7
66,366
4
398,609
3.1
101,394
65.2
66.058
332
16.0 65.1
473,641
3.2
124,430
71.3
88,719
TOTAL
1,357,851
3.1
348,341
65.1
226,787
1,135
16.8 65.9
1,541,543
3.1
394,632
73.2
288,340
ANAEROBIC SLUDGE TO BEDS
SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Cleaned
% Solids Removed
1 120,190 3.0 30,072 64.7 19,456
2
3
4
TOTAL 120,190 3.0 30,072 64.7 19,456
Summary
Total Gallons to Anaerobic Dig.
1,714.099
Total Pounds of Dry Solids to Anaerobic Dig.
680,774
Total Pounds of Vol. Solids to Anaerobic Dig.
534,174
Total Gallons from Anaerobic Dig.
1,478,041
Total lbs. of Dry Solids from Anaerobic Dig.
378,412
Total lbs. of Vol. Solids from Anaerobic Dig.
246,243
Detention Time - Days
59
Gas Production Ft3
3,663,153
Ft3 of Gas Produced/lb of VM added
6.9
-,:eduction
56
% (VK)
lbs Polymer
$/lb
Pounds of Polymer Used - GBT
1,706
$1.75
Pounds of Polymer Used - BFP
2,635
$1.75
54 % (LBS)
Poly Cost $/DT
2.986
4,611 26.48

South Durham Water Reclamation Facility
Sludge Report
line '2014
SD PRIMARY SLUDGE TO DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
216,083
3.1
55,608
85.0
47,266
2
169,914
3.5
49,598
81.6
40,472
3
188,803
3.1
48,813
84.3
41,149
4
232,261
3.8
73,608
85.2
62,714
TOTAL
806,061
3.4
227,627
84.0
191,602
GRAVITY THICKENER TO ANAEROBIC DIGESTER
Gallons % Solids Lbs Dry % Vol lbs VM
WASTING TO GRAVITY THICKENER
TWAS GBT TO ANAEROBIC DIGESTER
WEEK
Gallons
%v Solids
Lbs Dry
% Vol
lbs VM
Gallons
%, Solids
Lbs Dry
% Vol'
lbs VM
1
1,272,071
0.91
96,194
69.7
67,047
172,808
6.5
93,679
72.5
67,917
2
1,235,574
0.91
93,993
70.7
66,463
169,272
7.0
98,821
72.9
72,041
3
1,206,829
0.94
95,099
71.5
67,996
,.1.68,480
6.9
96,954
72.8
70,582
4
1,469,519
0.94
114,673
72.2
82,794
144,667
6.5
78,424
72.7
51,014
TOTAL
5,183,993
0.92
399,960
71.0
284,291
655,227
6.7
367,878
72.7
267,554
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
Yds
% Solids % Vol
1............
._..323;455......._........3:0
_ ..80;92£3
_ 64.6
._.. ._..
52,280
..-.._...__..-..
275
._-.._...._. -. __.
16.0 65.6
2
201,351
3.1
52,057
65.0
33,837
175
15.1 65.6
)3
238,195
3.0
59,596
63.7
37,963
205
14.6 65.4
4
269,877
2.9
62,854
63.5
39,912
219
16.4 65.1
TOTAL
1,022,878
3.0
255,436
64.2
163,992
874
15.5 65.4
ANAEROBIC SLUDGE TO BEDS
'SOLIDS
OFF DRYING BEDS
Beds
Yards
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbsVM
Cleaned
% Solids Removed
1
2 113,120 3.1 29,246 63.5 18,571
3
4
TOTAL 113,120 3.1 29,246 63.6 18,671
Summary
Total Gallons to Anaerobic Dig.
Total Pounds of Dry Solids to Anaerobic Dig
Total Pounds of Vol. Solids to Anaerobic Dig.
Total Gallons from Anaerobic Dig.
Total lbs. of Dry Solids from Anaerobic Dig.
Total lbs. of Vol. Solids from Anaerobic Dig.
Detention Time - Days
Gas Production Ft3
Ft3 of Gas Produced/lb of VM added
_" -,:duction
Pounds of Polymer Used - GBT
Pounds of Polymer Used - BFP
1,461,288
595,504
459,156
11135,998
284,682
182,563
67
3,363,269
7.3
-62 % (W)
lbs Polymer $/Ib
1,460 $1.75
1,919 $1.75
60 % (LB5)
Poly Cost
2,555
3,358
GRAVITY THICKENER TO GBT
Gallons
% Solids Lbs Dry
% Vol
357,524
2.9
86,471
71.5
333,953
3.2
89,126
72.3
341,206
3.0
85,370
72.1
289,543
3.2
77,273
71.7
1,322,226
3.1
338,239
71.9
$/DT
26.29
lbs VM
01,827
64,438
61,552
55,405
243,221

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
",VWTP Name: South Durham VW NPDES Number: NCO047597
✓Ionitoring Period: From 07/01/14 To 08/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlirnhle to alternative nerfnrmed !mica A nr ('laca I;l rmmnlete the fnllnwinu mnnitnrino data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 6th
MPN
12,448
54,299
82,902
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent — South Durham WRF
'rep��Title (print or type �... Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.COL /g. is
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliforMg total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.COL /g. is
2/20/2014
57
125
37
152
417
123
.84
108
4/16/2014
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

South Durham Water Reclamation Facility
Sludge Report
Juiy'2014
SD PRIMARYMUDGETO DIGESTER
l
WEEK
Gallons
%Solids Lbs Dry
% Vol
Ibs VM
1
147,118
$.8
46,625
84.9
39,684
2
228,724
3.6
88,072
86.1
59,127
3
132,383
4.6
50,787
75.2
38.192
4
186,680
3.7
57,577
82.1
47,270
TOTAL
694,811
3.9
228,681
82.4
184,174
WASTING TO GRAVITY THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM '
1
11069,880
0.97
86,500
79.4
68,681
2
1,050,670
0.93
81.771
65.6
63,641
3
944,720
1.00
79,071
60.8
48,075 j
4
1,365,960
1.19
135,042
81.9
110,532
TOTAL
4,431,430
1.02
382,384
71.9
280,930
8D ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
% solids
Lbs Dry
% Vol
lbs•VM
........
1
.... _..................................
227,727
3.0 ��
66,977
63.2
3S,()1Q
2
282,772
3
309,694
3.1
80,068
64.7
61,804
4
467,108
2.9
112,974
63.3
71,513
TOTAL
1.287,209
3.0
250,020
63.7
159,327
ANAEROBIC SLUDGE TO BEDS
Gallons % Solids Lbs Dry % Vol Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
j iA828
0.3
72,943
73.2
53,394
1200,253
127,943
0.4
68,291
72.1
49,238
296.286
6.6
160,617
69.9
1112,271
763,310
0.4
301,851
71.7
214,903
Yds
% Solids
% Vol
1. .........
_16:5......
64:6........
256
16.4
62.1
275
16.7
65.4
388
17.6
64.9
1,107
10.8
64.3
Beds Yards
WEEK Gallons %Solids Lbs Dry %Vol
IbsVM
Cleaned %Solids Removed
1
2 212,100 3.6 63,681 80.1
54,829
•
3
'
4
TOTAL 212,100 3.0 e$,681 $6.1
54,829
Sui'ilit'1Si'V
Total Gallons to Anaerobic Dig.
1.458,121
Total Pounds of Dry Solids to Anaerobic Dig.
525,511
Total Pounds of Vol. Solids to Anaerobic Dig.
399,077
Total Gallons from Anaerobic Dig.
1,499,399
Total Ibs. of Dry Solids from Anaerobic DIg.
313,701
Total Ibs. of Vol. Solids from Anaerobic Dig.
214,156
Detention Time - Days
70
Gas Production Ft3
3,124.915
Ft3 of Gas Pfoducedllb of VM added
7.8
% Reduction
38
% (V19 46 % (CBS)
ibs Polymer
$lib Poly Cost
?oonds of Polymer Used - GBT
1,900
$1.75 3,325
_ iym
rounds of Polymer used - BFP
2,366
$1.75 4,141
GRAVITY THICKENER TO-OITT
Gallons % Solids Lbs Dry % Vol Ibs VM
257,609 3.2-_ 68,751 71.9 49,432 -
331,811
246,005 3.1 63,602 72.2 45,921
590,527 2.9 142,825 68.9 98,406
1,425,952 3.1 275,178 71.0 193,769
$IDT
K-MM

South Durham Water Reclamation Facility
�3Iudge Report
August'2014
SD PRIMARY
SLUDGE TO DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
143,849
4.0 •
47,988
81.7
39,206
2
135,402
3.0
33,900
77.2
26,171
3
115,330
3.8
38,560
81.0
20,606
4
310,694
3.3
84,214
83.9
70,613
TOTAL
705,365
3.6
202.652
80.9
165,5981
WASTING TO GRAVITY THICKENER
I'
WEEK
Gallons
% Solids Lbs Dry
% Vol
lbs VM
1
1,017.069
1.23 104,698
97.6
102,080
2
1,016,039
1.23 104,494
79.2
82,759
a
1.015.272
1.20 .101,598
89.0
90,421
4
1,430,78B
1.14 138,308
85.0
115,862
TOTAL
4.479,708
1.20 447,090
87.7
391,122
8D ANAEROBIC
SLUDGE TO PRESS
WEEK
Gallons
% Solids Lbs Dry
% Vol
lbs VM
1
324,162
3.1 . 83,809
64.1-.
- 53.721
2
319,684
. 3.1 • 82,651
53,1
62,153
3
310,098
3.1 80,173
62.8
50,348
4
363.262
3.2 96,947
MA
59,720
TOTAL
1,317,206
3.1 343,580
62.0
215,042
ANAEROBIC SLUDGE TO BEDS
WEEK Gallons % Solids Lbs Dry % Vol lbsVM
z.
3
4
TOTAL
Gallons % Solids Lbs Dry % Vol lbsVM
Gallons
%solids
Lbs Dry
% Vol
lbs VM
171,253
0.7
95,693
69.5
66.500
190,383
6.6
104.794
68.9
72,203
196,524
6.6
108,175
69A
75,073
221,018
6.6
119,814
69.8
83,630
779,178
6.6
428,476
69.4
297,413
SD SOLIDS OFF
PRESS
GRAVITY THICKENER TO GBT
Yds
% Solids
% Vol
Gallons
% Solids Lbs Dry
% Vol
lbs VM
li 275
-17.6
03.7 --
-
345.598.
..... 2.8. -..
80,704
-69.2-
65,847
275
17.6
63.1
357,813
3,5
104,446
68A
71,441
275
17.8
63.0
349,677
2.9
84.573
69.3
59,609
332
17.6
62.6
388,736
3.0
95,641
69.4
66,327
1,157
17.6
03.0
1,441,824
3.0
365,363
69.1
262,224
Beds Yards
Cleaned %Solids Removed
SUM=
Total Gallons to Anaerobic Dig.
1,484,543
Total Pounds of Dry Solids to Anaerobic Dig.
631,128 {
Total pounds of Vol. Solids to Anaerobic Dig.
463.009
Tota[ Gallons from Anaerobic Dig.
1,317,206.
Total lbs. of Dry Solids from Anaerobic Dig.
343,580
Total lbs. of Vol. Solids from Anaerobic Dig.
215,942
Detention Time - Days
68
Gas Production Ft3
3,316.163
Ft3 of Gas Produced/lb of VM added
7.2
% Reduction
43 % (VK) 53 % (LBS)
lbs Polymer $Ab Poly Cost $/DT
?ounds of Polymer Used- GBT
1,323 $1.75 2,315
I3ounds of Polymer Used - BFP
2,342 $1.75 4,099 23.86

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
`VWTP Name: South Durham WRF NPDES Number: NCO047597
I
vlonitoring Period: From 09/01/14 To 10/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahip fn alternative nerfnrmed Wlace A nr ('lnce R) emmnlete the fnllnwina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,-
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 1h
MPN
ill
3,132
77,669
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU/g
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(V S reduction) X
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent — South Durham WRF
repare Title (print or pe) Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

South Durham Water Reclamation Facility
Sludge Report
September r2014
SD PRIMARY SLUDGE TO DIGESTER
WEEK
Gallons
% Solids Lbs Dry
% Vol
Ibs VM
1
270,510
3.0
81,218
82.6
67,086
2
163,327
2.8
38,140
$4.5
32,228
3
171,346
3.1
44,300
85.4
37,832
4
193,131
3.0
48,321
80.2
38,764
TOTAL
798,314
3.1
211,979
83.2
175,900 E
WASTING TO GRAVITY
THICKENER
WEEK
Gallons
% Solids Lbs Dry
% Vol
Ibs VM
4
1,015,644
1.16 98,284
84.6
83,148
2
1.021,616
1.07 91,569
80.3
73,630
3
1,001,600
1.05 87,472
77.0
67,353
4
1-1257,035
1.09 114,249
82.0
93,684
TOTAL
4,295,800
1.09 391,573
81.0
317,715
SD ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
% Solids Lbs Dry
%Vol
lbs VM e
1.
298,864"""
-3.2, ... 79,761 '
60.6
_48,335 -
2
270,774
3.2 72,264
60.6
43,792
3
304.420
3.2 81,245
60.9
49,478
4
508,439
3.2 135,692
61.3
83,179
TOTAL
1,382,503
3.2 308,962
60.9
224,785
ANAEROBIC SLUDGE TO BEDS
I Gallon % Solids Lbs Dry % Vol Ibs VM
Gallons
%Solids
Lbs Dry
% Vol
Ibs VM
201,202
5.6
93,009
' 70.4
66,154
182,927
6.9
90,011
71.1
63,998
197,660
6.9
97,281
72.0
70,028
262,385
6.3
137,862
72.5
99,950
844,174.
6.0
419,103
71.6
$00,130
SD SOLIDS OFF PRESS
GRAVITY
THICKENER TO GBT
Yds
% Solids
% Vol
Gallons
% Solids Lbs Dry
% Vol
Ibs VM
275 . _..
...17.3
01.5
335,979
.._.3.0_"
84,062
70:0
269
17.0 '
61.9
303,054
3.1
78,352
69.8
54,689
275
18.1
62.4
344.294
2.9
83,271
71.2
59,289
1 444
18.2
63.2
469,357'
3.1
118,762
71.0
85,034
1,263
17-6
62.4
1,442,684
3.0
364,447
70.7
257,855
Beds Yards
WEEK Gallons %Solids Lbs Dry % Vol Ibs VM
Gleaned %Solids Removed
1
.2 3.3
60
3
4
TOTAL 3.3
60
Summary
Total Gallons to Anaerobic Dig.
13642,488
Total Pounds of Dry Solids to Anaerobic Dig.
031,083
Total Pounds of Vol. Sollds to Anaerobic Dig.
470,030
Total Gallonsfrom Anaerobic Dig.
1,382,603
Total Ibs. of Dry Solids from Anaerobic Dig.
388,962
Total Ibs- of Vol. Solids from Anaerobic Dig,
224.78.5
Detention Time - Days
60
Gas Production Ft3
3,350,620
Ft3 of Gas Producedflb of VM added
7.0
Reduction
54
% (VX) 53 % (LBS)
ibsPolymer
$!lb Poly Cost $IDT
ounds of Polymer Used - GBT
1,269
$1.75 2,221
ounds of Polymer Used - BFP
2,490
$1.75 4,358 23.62

South Durham Water Reclamation Facility
Sludge Report
ctober'2014
SD PRIMARY SLUDGE TO DIGESTER.
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
160,956
3.8
51,010
85.1
43,410
2
166,263
4.3
59,625
86.6
51,635
3
147,906
3.4
41,940
82.3
34,517
4
172,819
3.6
51,167
86.5
44,259
TOTAL
647,944
3.8
203,742
85.1
173,821
WASTING TO GRAVITY THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
977,343
1.17
95,379 -V 77.3
73,728
2
1,014,486
1.19
100,732
81.9
82,449
3
1,074,664
1.03
92,568
70.5
65,260
4
1,551,472
0.96
124,217
79.6
98;877 .
TOTAL 4,617,965 1.09 412,896 77.3 320,314
SD ANAEROBIC SLUDGE TO PRESS
WEEK
Gallons
% Solids
Lbs Dry
% Vol
lbs VM
1
351,256
3.1
90,814
61.2
55,578
2
304,662
3.2
81,308
62.4
50,736
3
285,526
3.0
71,439
61.5
43,935
4
399,840
3.0
100,040
61.8
61,825
TOTAL
1,341,284
3.1
343,600
61.7
212,074.
ANAEROBIC SLUDGE TO BEDS
Gallons % Solids Lbs Dry % Vol lbs VM
Gallons
% Solids
Lbs Dry
% Vol
184,489
5.9
90,780
72.6
174,314
6.1
88,681
73.1
155,481
6.2
80,396
73.2
263,447
6.6
145,012
74.0
777,731
6.2
404,868
73.2
Yds % Solids % Vol
300
16.7
62.7
288
17.0
63.6
263
16.8
63.4
375
16.9
62.9
1,225
16.9
63.1
Beds Yards
WEEK Gallons % Solids Lbs Dry % Vol lbsVM Cleaned % Solids Removed
1
2
3
4
TOTAL
Summalii/
Total Gallons to Anaerobic Dig.
1,425,676
Total Pounds of Dry Solids to Anaerobic Dig.
608,610
Total Pounds of Vol. Solids to Anaerobic Dig.
470,639
Total Gallons from Anaerobic Dig.
1,341,284
Total lbs. of Dry Solids from Anaerobic Dig.
343,600
Total lbs. of Vol. Solids from Anaerobic Dig.
212,074
Detention Time - Days
71
Gas Production Ft3
3,446,288
Ft3 of Gas Produced/lb of VM added
7.3
.
Reduction
56
% (VK)
lbs Polymer
. $/Ib
Pounds of Polymer Used - GBT
1,188
$1.75
Pounds of Polymer Used - BFP
2,175
$1.75
lbs VM
65,906
64,825
68,850
107,236
296,818
GRAVITY THICKENER TO GBT
Gallons
% Solids Lbs Dry
% Vol
lbs VM
329,453
3.1
85,177
71.6
60,987
314,899
3.2
84,040
66.1
. 65,551
264,922
3.4
75,121
72.3
54,313
434,181
3.4
123,116
71.9
86,521
1,343,455
3.3
367,455
70.5
259,371
* Week 1 %VM for the Wasting to Gravity Thickener' is the average of the four other
data points in the month of October. No Lab result was reported.1126/15 CWC
55 % (L85)
Poly Cost $/DT
2,079
3,806 22.16

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. / g. is
2/20/2014
16,667
66,667
5.926
5.970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliform/g total solids
Sample Set #2
MPN
f. coliform/g total solids
Sample Set #3
MPN
f. coliform/g total solids
Sample Set #4
MPN
f. coliform/g total solids
Sample Set #5
MPN
f. coliform/g total solids
Sample Set #6
MPN
f. coliform/g total solids
Sample Set #7
MPN
f. coliform/g total solids
Geometric Mean
f.col. / g. is
N
2/20/2014
57
125
37
152
417
123
84
108
4/16/20141
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/2015
9,202
1,389
165
394
2,347
412
199
770

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number:
WWTP Name: South Durham WRF NPDES Number:
4onitoring Period: From 11/01/14 To 12/31/14
W00003504
NCO047597
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Unnnlienble. to alternative nerfarmed Winac A nr rlacc Rl rmmnlete the fnllawina mnnitnrina data
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x10 to the 6`
MPN
165
770
9,202
MPN/g
0
Bi-monthly
Grab
9221 E
Coliform
power per gram of
total solids
CFU
CFU/g
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt.4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Charles Cocker, Superintendent — South Durham WRF
--�reparerC�Title (print or e)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

North & South Durham Sludge Fecal Coliform Analysis
2014 Summary
North Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliformg total solids
Sample Set #2
MPN
f. coliformg total solids
Sample Set #3
MPN
f. coliformg total solids
Sample Set #4
MPN
f..coliform/g total solids
Sample Set #5
MPN
f. coliforMg total solids
Sample Set #6
MPN
f. coliforMg total solids
Sample Set #7
MPN
f. coliformg total solids
Geometric Mean
f.col. / g. is
,..
....:
4 ....., .. ... ........
2/20/2014
16,667
66,667
5,926
5,970
1,333
4,965
5,634
7,601
4/16/2014
8,966
3,937
15,484
100,629
5,195
1,948
6,934
8,728
6/19/2014
14,286
17,777
30,864
3,125
14,907
4,487
12,953
11,135
8/21/2014
14,545
4,268
3,378
1,463
7,514
3,049
4,908
4,449
10/30/2014
922
3,205
3,876
1,513
8,280
1,043
1,411
2,148
12/19/2014
20,134
5,634
9,848
12,057
5,229
3,472
14,342
8,610
South Durham WRF
Sample
Date
Sample Set #1
MPN
f. coliforMg total solids
Sample Set #2
MPN
f. coliforMg total solids
Sample Set #3
MPN
f. coliforMg total solids
Sample Set #4
MPN
f. coliformg total solids
Sample Set #5
MPN
f. coliformg total solids
Sample Set #6
MPN
f. coliforMg total solids
Sample Set #7
MPN
f. coliforMg total solids
Geometric Mean
f.COL / g. is
.„ n -E..
URT
.-...'. Y.
Jrra'.. .a:"m o-d".MMUM
.e.r .uW ., '.1^ +:„v.
awkFaf
a .'
2/20/2014
57
125
37
152
417
123
84
108
4/16/2014
11,194
6,996
209
1,805
37
120
26
444
6/19/2014
7,391
14,006
22,843
10,417
19,011
15,198
7,328
12,661
8/21/2014
43,689
69,648
81,633
78,049
82,902
12,448
69,565
54,299
10/30/2014
9,770
4,444
1,408
1,122
77,669
5,000
111
3,132
12/19/20151
9,202
1,389
165
394
2,347
412
199
770

South Durham Water Reclamation Facility
Sludge Report
lovember'2014
SD PRIMARY SLUDGE TO DIGESTER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
163,875
3.6
49,202
85.4,
42,018
2
202,206
3.5
59,024
83.9
49,521
3
264,049
3.1
68,267
87.2
59,529
4
208,212
2.7/
46,886
80.9
37,930
TOTAL
838,342
3.2
223,378
84.4
188,999
WASTING.TO GRAVITY THICKENER
WEEK
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
1,085,900
0.97
88,093
'78.4
69,065 I
2
1,020,704
0.93
78,967
60.2
47,538
3
1,021,079
1.06
90,104
54.7
49,287
4
1,309,018
1.06
116,1471964A
74,799
TOTAL
4,437,601
_ 1.01
373,311
64.4
240,688
SD ANAEROBIC SLUDGE TO PRESS
WEEK
- Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1
315,903
3.0
79,039
62.2
49,162
2
325,568
3.1
84,172
64.1
53,954 {
3
330,398
3.1
85,421
63.9
54,584
4
191,604
3.0
47,939
63.8
30,585
TOTAL
1,163,473
3.1
296,572
63.5
188,286
ANAEROBIC SLUDGE TO BEDS
j
WEEK
1
2
3
4
TOTAL
Gallons % Solids Lbs Dry % Vol Ibs VM 11
109,585 3.0 27,418 62.8 17,219
102,515 3.0
212,100 3.0
Summary
25,649 63.8 16,364
53,067 63.3 33,583
Gallons % Solids Lbs Dry % Vol Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
198,119
6.4
105,748
75.0
79,311
169,237
6.2
87,509
76.0
66,507
171,762
6.3
90,247
76.3
68,859
133,050
6.9
76,565
76.3
58,419
672,168
6.5
360,069
75.9
273,096
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
Yds
% Solids
% Vol
Gallons
% Solids Lbs Dry
% Vol
Ibs VM
288
16.2
61.8
342,705
3.1
88,603
73.6
65,212
300
17.3
64.5
317,247
2.8
74,064
75.8
56,155
300
17.2
65.0
305,910
3.0
76,539
75.7
57,940
175
17.2
65.5
228,171
3.4
64,700
75.6
48,913
1,063
17.0
64.2
1,194,033
3.1
303,925
75.2
228,220
! Beds Yards
!Cleaned % Solids Removed
Total Gallons to Anaerobic Dig.
1,510,510
Total Pounds of Dry Solids to Anaerobic Dig.
583,447
Total Pounds of Vol. Solids to Anaerobic Dig.
462,094
Total Gallons from Anaerobic Dig.
1,375,573
Total Ibs.-of Dry Solids from Anaerobic Dig.
349,639
Total Ibs' � Vol. Solids from Anaerobic Dig.
221,869
Detentio,�Time - Days
65
* Week 4 %VM for the 'Wasting to Gravity Thickener' is the average of the three
Gas Production Ft3
3,423,643
other data points in the month of November. No Lab result was reported.
Ft3 of Gas P oduced/lb of VM added
7.4
1/26/2015 CWC
',Reduction
58
% (VK)
52 % (LBS)
Ibs Polymer
$Ilb
Poly Cost $IDT
Pounds of Polymer Used = GBT
1,116
$1.75
1,953
Pounds of Polymer Used - BFP-
1,905
$1.75
3,334 22.48

South Durham Water Reclamation Facility
Sludge Report
_jecember'2014
SD PRIMARY SLUDGE TO DIGESTER
,iGRAVITY
THICKENER TO ANAEROBIC DIGESTER
WEEK Gallons % Solids Lbs Dry
% Vol
:1
Ibs VM
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1 213,933 4.0. 71,368
85.5
61,020
2 211,352 3.2 56,406
85.2
48,058
3 193,622 2.7 43,600
86.6
37,757
4 271,298 2.2 49,778
83.4
41,515
TOTAL 890,205 3.0 221,151
85.2
188,349
WASTING TO GRAVITY THICKENER
TWAS GBT TO ANAEROBIC DIGESTER
WEEK Gallons % Solids Lbs Dry
% Vol
Ibs VM
s
Gallons
% Solids
Lbs Dry
% Vol
Ibs VM
1 1,017,217 1.08 91,405
80.9
73,946
217,915
6.3
114,497
76.1
87,132
2 1,016,634 1.09 92,300
78.0
71,994
212,007
6.0
106,088
76.3
80,945
3 1,017,443 1.17 99,122
97.7
96,843
195,460
6.2
101,068
76.6
77,418
4 1,464,348 1.21 146,546
88.9
130,206 -
249,234
6.6
136,149
76.8
104,562
TOTAL 4,506,642 1.14 429,373
86.4
372,989
t
674,616
6.3
457,803
76.5
350,058
SD ANAEROBIC SLUDGE TO PRESS
SD SOLIDS OFF PRESS
GRAVITY THICKENER TO GBT
WEEK Gallons % Solids Lbs Dry
% Vol
Ibs VM F
Yds
% Solids
% Vol
Gallons
% Solids Lbs Dry % Vol Ibs VM
1 338,564 2.9 81,885
64.5
52,816 ::
300
17.0
66.0
349,929
3.6 106,063 75.6 79,427
2 340,626 2.9 82,384
64.9
53,467 N
300
17.1
66.5
350,068
3.2 - 93,426 75.6 70,630
3 273,614 2.8 63,894
64.8
41,404
238
17.2
66.5
316,354
3.4 89,422 76.0 67,961
- 4 130,332 2.8 30,435
65.8
20,026
113
17.6
67.2
405,300
3.6 119,997 76.0 91,198
TOTAL 1,083,136 2.9 258,598
65.0
167,713
950
17.2
66.5
1,420,651
3.4 407,908 75.8 309,216
ANAEROBIC SLUDGE TO BEDS
SOLIDS OFF DRYING BEDS
Beds
Yards
WEEK Gallons % Solids Lbs Dry
% Vol
Ibs VM
Cleaned
% Solids
Removed
1
2
3 95,445 2.8 22,288
64.9
14,465
4
TOTAL 95,445 2.8 22,288
64.9
14,465 '.
Summary
Total Gallons to Anaerobic Dig.
1,764,821
Total Pounds of Dry Solids to Anaerobic Dig.
678,954
Total. Pounds of Vol. Solids to Anaerobic Dig.
538,408
Total Gallons from Anaerobic Dig.
1,178,581
Total lbs. of Dry Solids from Anaerobic Dig.
280,887
Total lbs. of Vol. Solids from Anaerobic Dig.
182,178
Detention Time - Days
57
Gas Production Ft3
3,554,869
Ft3 of Gas Produced/lb of VM added
6.6
Reduction
56
% (VK)
66
% (LBS)
-1bsPolymer
$Ib
Poly Cast
$/DT
Pounds of Polymer Used - GBT
1,443
$1.75
2,525
Pounds of Polymer Used - BFP
1,755
$1.75
3,071
23.75

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
-VWTP Name: Brown WTP NPDES Number: 03-32-010(A)
Monitoring Period: From 03/01/14 To 4/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlien hip. to altrrnntivP nerfnrmed tClacc A nr Clacc III emmnlntP the fnllnwina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
MPN
MPN/g
Coliform
power per gram of
total solids
CFU
46
48
56
CFU/g
0
4/Yr
Grab
9222D
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization)
(Drying— Stable)
(Drying —Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Tom Lucas, Assistant Superintendent Brown WTP
reparer Name and Title (print or e� Land Applier Name and Title (if applicable) (type or print)
, - -2-9
Si ature o reparer* Date Signature of Land Applier (if applicable)
Date
* parer is defined in 40 CFR Part 503.9 r and 15A NCAC 2T.1102 26

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Pagel
Contact: Marshall Puryear Report Date 4/29/2014
Client: Synagro Project: Durham WTP (Brown)
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 4/24/2014
Meritech Work Order # 04241402 Sample: Durham WTP 1 Grab 4/23/14
Parameters Results Analysis Date Reporting Limit etho
% Total Solids 19.2 % 4/25/14 0-100 % SM 2540B
Fecal Coliform (Sludge) 47 col/g dry wt 4/24/14 130 col/g dry wt SM 9222D
Meritech Work Order # 04241403 Sample: Durham WTP 2 Grab 4/23/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.8 % 4/25114 0-100 % SM 2540B
Fecal Coliform (Sludge) 46 col/g dry wt 4/24/14 130 col/g dry wt SM 9222D
i
Meritech Work Order # 04241404 Sample: Durham WTP 3 Grab 4/23/14
Parameters
% Total Solids
Fecal Coliform (Sludge)
Results
18.9 %
< 48 col/g dry wt
Analysis Date
4/25/14
4/24/14
Reporting Limit
0-100 %
130 col/g dry wt
Method
SM 2540E
SM 9222D
Meritech Work Order##
04241405 Sample: Durham WTP 4 Grab
4/23/14
Parameters
Results
Analysis Date
ReportingUrnit
Method
% Total Solids
18.9 %
4/25/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
48 col/g dry wt
4/24/14
130 col/g dry wt
SM 9222D
Meritech Work Order #
04241406 Sample: Durham WTP 5 Grab
4/23/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
19.3 %
4/25/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 47 col/g dry wt
4/24/14
130 cal/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Marshall Puryear Report Date 4/29/2014
Client: Synagro Project: Durham WTP (Brown)
284 Boger Road
Mocksvilie, NC 27028 Date Sample Rcvd: 4/24/2014
Meritech Work Order # 04241407 Sample: Durham WTP 6 Grab 4/23/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 19.3 % 4/25/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 47 col/g dry wt 4/24/14 130 col/g dry wt SM 9222D
Meritech Work Order # 04241408 Sample; Durham WTP 7 Grab 4/23/14
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
16.2 %
4/2$./14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
i
56 col/g dry wt
4/24/14.
130 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. �2�L
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
teI.[phone] fax.[phone]

3-20.2013 Chain of Custody Record (COC)
NPDES#:
Client: , Phone: tr3IW-73$--040 �-
Address: 19eq t-4 i¢-L-- Fax:
L9 f1r.�lj eAl 6 s�7�2� Email• i a1�-
Project: U J P
P.O.#:
Attention: Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
apply {preferred ax, Mail St d 10da s) 3-5 DaXs 24-48Hrs
Circle all that a 1 Email Ir�{t
®
ENVIRONMENTAL LABORATORIES
T642 Tamco.Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
A �� A'� A Qp^ } �r� �p h�+ �+
VV VV VV . e 01 ec 9—Iabs.com
Sample Location and/or ID #
.Sampling Dates & Tames
Person Taking Sample (Sign/Print):
Lab Use Only.
Start
End
comp?
Grab?
#of
Cont.
�� S�
S R d r� d
on.lce?:`
Yes •/ No �
PH`.O.K3'
;.Cl OK?
Date
Time
Date
Time
.0Ut1i
d fl`�Lk
Temperature; Upon : ;
•Receipt:.,'
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TO
samples must be done in the field prior to preservation. ***
Comments:
Compositor:
Jug#
UPS
Fed Ex
Are the a results for regulatory purposes? Yes .. No
Report results in: mg/La mg/kg ug/L
gHand Delivery
Reiff y Date: s e:
Ej 2 %
Received by: Date: Time:
C Other
Reli q d y: Dat . Time:
Received by: Date: Time:
Relinquished by: Date: Time:
R ived by L_ L date: `,►ef
21

Lab result
47
46
48
48
47
47
56
Average
FECAL DATA SHEET
Log
1.67
Min
1.66
Max
1.68
Geometric Mean
1.68
1.67
1.67
1.75
1.68
46
56
48

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
WWTP Name: Brown WTP NPDES Number: 03-32-010(A)
✓Ionitoring Period: From 5/01/14 To 7/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf annhenhle to alternative nerformed ((lace Aar (lace R1 emmnlete the fnllnwinv mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytic,
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6th
MPN
MPN/g
Coliform
power per gram of
total solids
38
41
45
CFU/g
0
4/Yr
Grab
9222D
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. I
Option/Alt. 2
Option/Mt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Tom Lucas, Assistant Superintendent Brown WTP
,—reparer Name and
/Title (print or type)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Rum
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Revised Date; 812912014
Contact: Marshall Puryear Report Date 7/14/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 7/7/2014
Meritech Work Order If 07071414 Sample: Brown WTP 1 Grab 7/7/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
22.1 %
7/8/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 45 col/g dry wt
7/7/14
45 col/g dry wt
SM 9222D
Meritech Work Order It 07071415 Sample: Brown WTP 2 Grab
7/7/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 25.2 % 7/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 40 col/g dry wt 7/7/14 40 col/g dry wt SM 9222D
Meritech Work Order # . 07071416. Sample: Brown WTP 3 Grab 7/7/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids . 23.6 % 7/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 42 col/g dry wt 7/7/14 42 col/g dry wt SM 9222D
Meritech Work Order If 07071417 Sample: Brown WTP 4 Grab 7/7/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 22.9 % 7/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 44 col/g dry wt 7/7/14 44 col/g dry wt SM 9222D
Meritech Work Order It 07071418 Sample: Brown WTP 5 Grab 7/7/14
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 26.0 % 7/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 38 col/g dry wt 7/7/14 38 col/g dry wt SM 9222D
0
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
-- Environmental Laboratory
Laboratory Certification No.165
Page 2
Revised Date: 812912014
Contact: Marshall Puryear Report Date 7/14/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 7/7/2014
Meritech Work Order # 07071419 Sample: Brown WTP 6 Grab 7/7/14
Parantetets Results Analysis Date Reporting Limit Method
Total Solids 24.6 % 7/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 41 col/g dry wt 7/7/14 41 col/g dry wt SM 9222D
Meritech Work Order # 07071420 Sample: Brown WTP 7 Grab 717114
Parameters Results Analysis Date Reporting Lirnit Method
Total Solids
25.5 %
718114
0-100 .%
SM 2540B
Fecal Coliform (Sludge)
< 39 col/g dry wt
717114
39 col/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. -
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3,20.2013 Chain of Custody Record (COC)
NPDES#: _
Client: �7 Ty In4 Phone:
2-24
°
Address: RQ,. Fax:
(ENVIRONMENTAL LABORATORIES
'�19 . A)C 970';�LSS Email:
642 TamcoAd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Turn Around Time*
How would you like our report sent? *RUSH work needs prior approval.
/®� �e r�
0!!! V@® �1� ereriech`labSnc®! !I 9
Circle all that apply Em�d(pr.fered),aX, Mail Std lOda 3�-5 Da j5 24-48Hrs
Person Taking5 fe ign/Pr' ): ��� �5�. ®���
Sampling DatesTimes
Sample Location and/or ID #
Start
End
comp?
#of
Tests)
Req u i red
on Ice?
Yes / No
pH OK?
Date
Time
Date
Time
Grab?
Cont.
::.Cf.OK?
awo. �� i
i�P
��=ate
-771
/1r� .,._
b
o
I f Z/
----
7 /
1; .�
c{
/1. ,
6E4
f
Few 1
1
y : p3-,
1'(
I!: ls*Z�
(&,r�
t
cw
ea 7;-,
-77) K
74.
�' �
'I
-�CA t
`
Temperature Upon
ilvr)
Receipt:
Method o�
**� Dechlorination i<0.5 ppm) of Ammonia, Cyanide, Phenol and samples must be done in the field prior to preservation. **
Comments:
..
Compositor #
Shipment:
UPS•
Jug#
Q" Fed Ex
Area s results for regulatory purposes? Yes Q? No Q
Report results in: mg/L [ mg/kg Q ug/L Q:
%Hand
Relinquished by Dare: Time:
Received by: Date: Time:
Delivery
cs � f
��kk
i-..i Other
Relinquished y: Date: Time:
Received by: Date: Time:
-_
Relinquished by: Date: Time:
Received by La
Date: , Time:
Q9

Lab result
45
40
42
44
38
41
39
Average
FECAL DATA SHEET
Log
1.65
Min
1.60
Max
1.62
Geometric Mean
1.64
1.58
1.61
1.59
1.62
38
45
41

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: W00003504
WWTP Name: Brown WTP NPDES Number: 03-32-010(A)
:Qonitoring Period: From 8/01/14 To 10/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilie
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlirnhle to niternntivP nrrfnrmed Wins A nr (lnsc Yh rmmnlete fhr fnunwina mnnitnrina dntn-
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
AnalyticE
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
WO to the 6 th
MPN
MPN/g
Coliform
power per gram of
total solids
CFU
48
49
51
CFU/g
0
4/Yr
Grab
9222D
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt.3
Option/Alt.4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable) _
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Tom Lucas, Assistant Superintendent Brown WTP
arer Name and Title (print or type)
rr
Im
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inca
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Marshall Puryear Report Date 10/13/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 10/7/2014
Meritech 10
Work Order # 10071411 Sample: Durham WWTP 1 Grab /614
Parameters Results Analysis Date ReportingUrnit Method
%Total Solids 20.6 % 10/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 49 col/g dry wt 10/7/14 49 col/g dry wt SM 9222D
Merited Work Order # 10071412 Sample: Durham WWTP 1 Grab 10/6/14
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
20.4 % 10/8/14 0-100 %
< 49 col/g dry wt 10/7/14 49 cot/g dry wt
SM 2540B
SM 9222D
Fecal Coliform (Sludge)
10071413 Sample: Durham WWTP 1 Grab
10/6/14
Meritech Work Order #
Parameters
Results Analysis Date Reporting Limit
Method
Total Solids
.
0 10/8/14 0-100 %
19.5 /o /g y
'col dry 51 col dr wt
SM 2540B
_ SM 9222D . -.. .
Fecal Coliform (Sludgy}
< 51 /g Y wt-10/7/14
Meritech WorkOrder #
.10071414 ..........Sample: Durham WW'I'P 1 Grab
I.0�.14 /
... .
Parameters
Results Analysis Date Reporting Limit
Method
Total Solids
21.0 % 10/8/14 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 48 cal/g dry wt 10/7/14 48 col/g dry wt
SM 9222D
Meritech Work Order #
10071415 Sample: Durham WWTP 1 Grab
10/6/14
Parameters
Results Analysis Date Reporting Limit
Method
%Total Solids
0 10/8/14 0-100 %
21.0 /o
SM 2540B
Fecal Coliform (Sludge)
< 48 col/g dry wt 10/7/14 48 col/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
_ Environmental Laboratory
- Laboratory Certification No.16S
Page 2
Contact: Marshall Puryear Report Date 10/13/2014
Client: Synagro
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 10/7/2014
Meritech Work Order # 10071416 Sample: Durham WWTP 1 Grab 10/6/14
Parameters Results Analysis Date ReportingLimit imit Method
% Total Solids 20.7 % 10/8/14 0-100 % SM 2540B
Fecal Coliform (Sludge) < 48 col/g dry wt 10/7/14 48 col/g dry wt SM 9222D
Meritech Work Order # 10071417 Sample: Durham WWTP 1 Grab 10/6/14
Parameters Results Analysis Date ReportingLimit imit Method
% Total Solids
20.6 %
10/8/14
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 49 col/g dry wt
10/7/14
49 col/g dry wt
SM 9222D
I hereby certify that have reviewed and approve these data. tf.It -4ea �-
Laboratory Representative
642 Tarnco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-=0,=013 Chain of Custody Record (C®C)
NPDES:
Client: Phone:
ERITE"M� I ' CO
Address: Fax -
F `^~ LABORATORIES
ENVIRONMENTAL
Email:
642 Tamco.Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax:[phone]
P,O,#:
Email: [e-mail]
Attention: Turn Around Time*
How. would you like your report sent? *RUSH work needs prior approval.
® �y�
�r� errfl teC�—'lasso
01�����t
Stcl 10da 3-5 Da 24-48Hrs
. Y U
Circle all that apply:; Email (preferred) , Fax, Mail s) S
Sampling. . Dates & Times
Person Taking Sample {Sign/Paint}:
Lab Usk Only
Sample Location? and/or 0 #
Start
End
,
Comp.
., of
"
Test(s) Required
,
On Ice?
Date
Time
Date
Time
Grab?
Cont.
Yes / No
?
CHOK.
f Vim.
a
Temperature Upon
Receipt::
Method o **` Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Compositor # :
•
rComments:
Shipmer�-�:
[] UPS
lug #
Q Fed Ex Are these results for regulatory purposes? Yes No
Report results in: mg/L mg/kg s ug/L
Relinquished b Date- Time:
Q;: ; Y-
. -•Hand Delivery�'
Received b y. Date: Time:
..Other lRelinquished by: Date: Time:
1
Received b •
Y• Date: Time:
Relinquished by: Date: Time:
r
e by Date: a
�

Lab result
49
49
51
48
48
48
49
Average
FECAL DATA SHEET
Log
1.69
Min
1.69
Max
1.71
Geometric Mean
1.68
1.68
1.68
1.69
1.69
48
51
49

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Durham WQ Permit Number: WQ0003504
WWTP Name: Brown WTP NPDES Number: 03-32-010(A)
✓Ionitoring Period: From 11/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlirahla fn alternative nnrfarmrrl Wince A nr 9-lace R) rmmnlrtP thr fnllnwina mnnitnrina dntar
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytick
Excee-
of
Type
Techniqu
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 1h
MPN
MPN/g
Coliform
power per gram of
total solids
461
476
490
CFU/g
0
VYr
Grab
9222D
CFU
1000 MPN per gram of total
MPN/g
solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed X
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel
properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am
aware that there are significant penalties for false certification including fine and imprisonment."
Tom Lucas, Assistant Superintendent Brown WTP
n eparer Name and Title (print or type)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
*` Laboratory Certification No.165
Page 1
Contact: Nate Roth
Report Date
1/26/2015
Client: Synagro
Project:
2014 Material
284 Boger Road
Mocksville, NC 27028
Date Sample Rcvd:
1/16/2015
Meritech Work Order # 01161552 Sample: Durham Brown WTP 1 Grab
1/16/15
Parameters
Results Analysis Date Reporting Limit
Method
% Total Solids
21.5 % 1/19/15 0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 465 col/g dry wt 1/16/15 465 col/g dry wt
SM 9222D
Meritech Work Order #
01161553 Sample: Durham Brown WTP 2 Grab
1/16/15
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
21.0 %
1/19/15
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 476 col/g dry wt
1/16/15
476 col/g dry wt
SM 9222D
Meritech Work Order #
01161554 Sample: Durham Brown WTP 3 Grab
1/16/15
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
20.8 % -
1/19/15
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 481 col/g dry wt
1/16/15
481 col/g dry wt
SM 9222D
Meritech Work Order #
01161555 Sample: Durham Brown WTP 4 Grab
1/16/15
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
20.8 %
1/19/15
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 481 col/g dry wt
1/16/15
481 col/g dry wt
SM 9222D
Meritech Work Order # 01161556 Sample: Durham Brown WTP 5 Grab 1/16/15
Parameters Results Analysis Date Reporting Limit Metho
% Total Solids 21.7 % 1/19/15 0-100 % SM 2540B
Fecal Coliform (Sludge) < 461 col/g dry wt 1/16/15 461 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Qz 01-14-1
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Contact: Nate Roth Report Date 1/26/2015
Client: Synagro Project: 2014 Material
284 Boger Road
Mocksville, NC 27028 Date Sample Rcvd: 1/16/2015
Meritech Work Order # 01161557 Sample: Durham Brown WTP 6 Grab 1/16/15
Parameters
Results
Analysis Date
Reporting Lirnit
Method
% Total Solids
20.9 %
1/19/15
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 478 col/g dry wt
1/16/15
478 col/g dry wt
SM 9222D
Meritech Work Order # 01161558 Sample: Durharn Brown WTP 7 Grab 1/16/15
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
20.4 %
1/19/15
0-100 %
SM 2540B
Fecal Coliform (Sludge)
< 49 0 col/gdry wt
1/16/15
490 col/gdry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. (�
Laborator y Represen to tive
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] €ax.[phone]

Chain of Custody Record (COC)
NPDES#:
Client: �yn 4 1-0 Phone:
Address: Fax:
Email: iN{ro h®:: QYA, �
a'
Project:
P.O.#:
Attention: AIAL e-- Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: nt0' (preferred), Fax, Mail Stcl 10days) 3-5 Des 24-48Hrs
MER �� INC.
ENVIRONMENTAL LABORATORIES
�. 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
e �� A (may .-�
uv VV VV .meritech-11. bs.com
Sample Location and/or I©#
.Sampling Dates & Times
Person Taking Sa pie (Si n/Print):
„ �
. Lab Use.Only
Start
End
Comp?
Grab?
# of
Cont.
r
��5�`S� Req ���
`. On Ice? '.
e / No
: pH O.Q.
0.00--
Date
Time
Date
Time
ZO/� i tfT0.J Z
�
.. �
.. .. •.
. Temperature.Upon : m .
Re ei t b•
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field priorto preservation.
Comments:
Compositor.# :: • , .
Jug#' .: .
Q' UPS
Fed Ex
Are these results for regulatory purposes? YesNo
Report results in: mg/L [ mg/kg i ug/L:
QHand Delivery
Relinquishe �� D�t% /-5 7ime:2<Q z
Received by: Date: Time:
Other
Relinquished by: D te: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Re ed by la G �tTipae:l
12

Lab result
465
476
481
481
461
478
490
Average
Log
2.67
2.68
2.68
2.68
2.66
2.68
2.69
2.68
FECAL DATA SHEET
Min
Max
Geometric Mean
461
490
476

Agricultural Lime Application Log _
Year: 2014
Project:. DURHAM
Field
(state -county -site -field code) I
Soil pH
Lime Requirement
I (from soil analysis)
Tons/Acre
Applied
ING-AM-22-01 Claude ync
c.
NC-AM-22-02 Claude Lynch
5.6
0.8T/Ac.
NC-AM-22-03 Claude Lynch
5.6
1.OT/Ac.
NC-AM-25-01 Rebecca Jefferies
5.4
0.9T/Ac.
NC-GR-05-01 Henry Thorpe
5.9
O.OT/Ac.
NC-GR-05-02 Henry Thorpe
6.2
O.OT/Ac.
NC-GR-05-03 Henry Thorpe
5.9
O.OT/Ac.
NC-GR-05-04 Henry Thorpe
5.9
O.OT/Ac.
NC-GR-05-05 Henry Thorpe
5.8
0AT/Ac.
NC-GR-05-06 Henry Thorpe
5.9
O.OT/Ac.
NC-OR-01-01 Won Latta & Sons Dairy
5.7
0.5T/Ac.
NC-OR-01-02 Won Latta & Sons Dairy
5.9
O.OT/Ac.
NC-OR-01-03 Won Latta & Sons Dairy
5.8
0.3T/Ac.
NC-OR-01-04 Won Latta & Sons Dairy
5.9
0.OT/Ac.
NC-OR-05-01 David Walker
5.3
1.3T/Ac.
NC-OR-05-02 David Walker
4.4
2.5T/Ac.
NC-OR-05-03 David Walker
5.0
1.8T/Ac.
NC-OR-05-04 David Walker
5.2
1.3T/Ac.
NC-OR-05-07 David Walker
6.5
O.OT/Ac.
NC-OR-06-01 Ronald Walker
6.5
O.OT/Ac.
NC-OR-06-02 Ronald Walker
6.6
O.OT/Ac.
NC-OR-70-01 Faircrest Land & Cattle
5.7
1.3T/Ac.
NC-OR-70-02 Faircrest Land & Cattle
5.5
1.8T/Ac.
NC-OR-70-03 Faircrest Land & Cattle
6.2
O.OT/Ac.
NC-OR-70-04 Faircrest Land & Cattle
5.6
1.5T/Ac.
NC-OR-76-09 William Breeze
6.0
O.OT/Ac.
NC-OR-76-10 William Breeze
5.9
O.OT/Ac.
NC-OR-76-12 William Breeze
5.0
1.9T/Ac.
NC-OR-76-14 William Breeze
5.3
1.5T/Ac.
NC-OR-91-01 Larry & Deborah Walker
6.1
O.OT/Ac.
NC-OR-91-02 Larry & Deborah Walker
5.7
0.5T/Ac.
NC-OR-91-03 Larry & Deborah Walker
5.6
0.7T/Ac.
NC-OR-91-04 Larry & Deborah Walker
5.9
O.OT/Ac.
NC-PS-01-01 Sidney Thompson
6.1
O.OT/Ac.
NC-PS-01-02 Sidney Thompson
5.7
0AT/Ac.
NC-PS-01-05 Sidney Thompson
6.0
O.OT/Ac.
NC-PS-01-06 Sidney Thompson
5.8
0AT/Ac.
NC-PS-01-07 Sidney Thompson
5.8
0AT/Ac.
NC-PS-01-10 Sidney Thompson -
5.8
0AT/Ac.
NC-PS-01-12 Sidney Thompson
7.1
O.OT/Ac.
NC-PS-29-01 Susan Satterfield
5.6
1.OT/Ac.
NC-PS-29-02 Susan Satterfield
5.7
1.5T/Ac.

NCDA&CS Agf nomic Division Phone: [phone] Website: www.r �Qyi:gov/agronomi/` Report No. FY:),-__901833
4� Client: Claude Lynch Advisor: Creighton Brown
Predictive9129 Harmony Church Rd Synagro Central
s r °a' Mebane, NC 27302 284 Boger Rd
.
i.x Mocksville, NC 27028
:. S o i I Re „„o rt Mehlich-3 Extraction
�`s , . N Sampled County: Alamance
^ >a ^4�:. _
~•k-YlVJi15�5t�
Sampled: 07/01/2014 Received: 07/30/2014 completed: 08/08/2014 Farm: Durham Links to Helpful Information
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or 7" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to
crop production. The C and Z symbols are printed on your report for soil test index levels of 2000 or more; for peanuts with zinc, the level is 300. This note is designed to be a "trigger"
that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu &amp; Zn has
been set at 3000 index; for peanuts with zinc, the level is 500. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped.
The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops grown on afield.
Sample ID: AM221
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.8 120-200 0 50 0 0 0 0 0 0
Note: 12
2 - $pH
Test Results [units - WN in glcnf; CEC and Na in meq/100'cd; NO3-N in mg/drrt3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1. K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N
0.36 1.17 8.5 79 1.8 ' 5.5 306 43 54 22 52 553 349 1666 1666 222 0.1 1
Sample ID: AM222
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.8 120-200 0 40 0 0 0 Z 0 0
Note: 12 Note:
2 - $pH
Test Results [units - WN in glcd; CEC and Na in meq/100 cO; NO3-N in mg/dd]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N
0.32 1.09 11.1 82 2.0 5.6 486 48 61 19 42 188 130 2739 2739 259 0.1 1
,-North Carolina:
'Tol±awo.3rus& Fuad 611111[kssaoft
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS.,u,v.iomic Division Phone: [phone]
Website: www.i.;,;.yt:gov/agronomi/
Report No. FY',',_,—)01833
Claude Lynch
Page 2 of 3
Sample ID: AM223
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O Mg
S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 1.0
120-200 0
0 0
0
0 Z
0 0
Note: 12 Note:
2 -
$pH
Test Results [units - W/V in glcd; CEC and Na in meq/100 cm3; NO3-N in mg/dr&]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-1 Mn-All
Mn-AI2
Zn-1 Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 0.93 13.3 81 2.6 5.6 703 101
57 20 63
196 135
4633 4633
420 0.1 1

I,CDA&CS',' _^ iomic Division Phone: [phone] Website: www.i z,,-__& ,gov/agronomi/
Report No. FY'�L 4D01833
Claude Lynch
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or,other large areas are listed separately for each nutrient to be added (in units of -
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N ,(and sometimes for B) are based on research/field studies
K20
potash .
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-AI1
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should a special attention to micronutrient levels. If $, pH$, $pH, C or Z
p pay p
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the -report, visit www.ncapr.pov/apronomi/oboart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS-1, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncapr.gov/agronomi/uvrst.htm
for more information.

NCDA&CS ���: ;4aomic Division Phone: [phone] Website: www.rtiC wd_ gov/agronomi/ Report No. FY1,L, � ,_001834
Client: Roger Tate Advisor: Creighton Brown
Predictive 8615 Harmony Ch Rd Synagro Central
' a Efland, NC 27243 284 Boger Rd
Soil Report Mehlich-3 Extraction Mocksville, NC 27028
N Sampled County: Alamance
Sampled: 07/01/2014 Received: 07/30/2014 Completed: 08/07/2014 Farm: Durham Links to Helpful Information
Sample ID: AM251 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Fescue/OGrass/Tim, 1 0.9 120-200 0 30 0 0 0 0 0 0 Note: 12
2 - $pH
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 crrr3; NO3-N in mgldm3]: Soil Class: Mineral
HM% WN CEC BS% At pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.46 1.19 9.3 81 1.8 5.4 321 55 62 16 42 138 100 1140 1140 145 0.1 1
-North•=Carolina
'Ta'L�c�o irusr Euitil:Gt,a�iiati'sstu�r-
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA'&CS �° . iomic Division Phone: (919)'733-2656 Website: www.r _ govlagronomi/
Report No. FY1� )01834
Roger Tate
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index-
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-Ail
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index _
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agrbnomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncaar.pov/apronomi/ob,oart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate -For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-1
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn=1, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncacrr.crov/aaronomi/uvrsthtm
for more information.

NCDA&CS i a_ comic Division Phone: [phone] Website: www.nJ�_,�=gov/agronomi/
Report No. FY1�,,)16370
Client: Henry Thorpe
Advisor:
Nate Roth
��cuuuut;4"
Predictive
5676 Old Roxboro Rd.
Synagro
Oxford, NC 27565
284 Boger Rd
` dl
„
x Soil I Re o rt Mehlich-3 Extraction
Mocksville, NC 27028
N
Sampled County: Granville
r, �istnr:Sr tir''4�
Sampled: Received: 11/14/2014 completed: 12/09/2014
Farm: NC-GR-05
Links to Helpful Information
Sample ID: 05-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0 120-200 0
0 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-1
Zn-AI
Cu-1
Na ESP SS-1 NO3-N
0.41 0.98 10.3. 86 1.4 5.9 153 114 47 34
64 155 110
416
416
67
0.1 1
Sample ID: 05-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0 120-200 0
50 0 0
0
0
0
0
Note: 12
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 carp; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-1
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.13 1.07 8.1 84 1.3 5.9 243 45 50 31
40 133 97
1019
1019
118
0.1 1
Sample ID: 05-06 Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P205
K20 Mg S
Mn
Zn
Cu
B Information
Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0
80 0 0
0
0
0
0 Note: 12
2-
Test Results [units - WN in g/crap; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.27 0.98 8.1 82 1.4 5.9 115 30 50 30
42 239 160
658
658
139
0.1 1
°North ,Ciairolina,
" �
%tracao=%ust Fu+iiJ,Cita�llei6saicra.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS .%°y:_ 1omic Division Phone:.[phone] Website: www
Report No. FY1°, . )_ 370
Henry Thorpe Page 2 of 2 I
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
Ib/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncapr.aov/aaronomi/obnart4.htm#fs to find
information ,that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.pov/apronomi/uvrst.htm
for more. information.
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I.
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen .
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS �:s,_ L6omic Division Phone:[phone]
Website: wwwaL�,_L� ov/agronomi
Report No. FYi, _.—h,')01830
G�«u�r• "
Client: Henry Thorpe
Advisor: Creighton Brown
Predictive
5676 Old Roxboro Rd.
Oxford, NC 27565
Synagro Central
284 Boger Rd
Mehlch-3 Extraction
Report
Mocksville, NC 27028SoiI
Sampled County: Granville
P tY
Sampled: 06/24/2014 Received: 07/30/2014
Completed: 08/07/2014
Farm: Durham
Links to Helpful Information
Sample ID: GRO54
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
40 0 0
0
0
0 0
Note: 12
2 -
$pH
Test Results [units - WIV in glcrrP; CEC and Na in meq/100 crrt3; NO3-N in mg/drrP]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.60 0.93 9.8 90 1.0 5.9 67 54
52 36
82 772 480
491
491
161 0.1 1
Sample ID: GR5-2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
2 -
$pH
Test Results [units - WIV in g/ca; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.51 0.85 14.0 88 1.7 6.2 186 84
50 35
43 367 234
1206
1206
168 0.1 1
North -.Carolina:
rsat�ccer'irusl:Fwsd.Ca�niatls;toa� _
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS ..a�._:iomic Division Phone: [phone] Website: www.r� _, gov/agronomi/
Report No. FYt__1001830
Henry Thorpe
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full -rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-Al2
Mn-availability index for crop 1
Mn-availability index for crop 2
Mn-I
manganese. index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note:.Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncaar.pov/aaronomi/obpart4.htm#fs to find
P-I
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/v
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index.
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, 8-1, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncacir.aov/aaronomi/uvmt.htm
for more information.

NCDA&CS -"U.
Division Phone: [phone] Website: www.
Predictive
p
Soil !Report Mehlich-3 Extraction
y,.gov/agronomi/
Client: Henry Thorpe
5676 Old Roxboro Rd.
Oxford, NC 27565
Sampled County: Granville
Report No. FYI=.__-J37224
Advisor: Creighton Brown
Synagro Central
284 Boger Rd
Mocksville, NC 27028
Sampled; Received: 06/05/2014
Completed: 06/13/2014
Farm; Durham
Links to Helpful Information
Sample ID: GR5-5
Recommendations: Lime
Nutrients (Ib/acre )
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.4
120-200 0
90
0
0
0
0
0 0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
90
0
0
0
0
0 0
Note: 12
Test Results [units - W/V in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mgldd]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.13 1.09 8.8 83 1.5 5.8 125 25
56 26
84 141
102
102
480
480
94 0.0
Narih Carolina
Tobacco Trwc Fund Ctunniission
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS ,r;,_,,,,-,iomic Division Phone: [phone] Website: www.ri _;: `gov/agronorni/
ReportNo. FY1 )37224
Henry Thorpe
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
.an
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-Al2
Mn-availability index for crop 1
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagrgov/agronomi/obnari4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-1
zinc availability index
zinc index
remaining 16 [P-1, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwncagr.gov/agronomi/uyrst.htm
for more information.

NCDA&CS ,;_,a iiomic Division Phone: [phone] Website: www.r -gQ 'gov/agronomil
Report No. FY1}.._,_,,-116372
Client: Latta, Bill (William)/M.A.
Advisor:
Nate Roth
Predictive
3315 Edmund Latta Rd
Synagro
284 Boger Rd
} w + y
Soil Report
Mehlich-3 Extraction
Hillsborough, NC 27278
Mocksville, NC 27028
Sampled County: Orange
Sampled: Received;
11/14/2014 Completed: 12/09/2014
Farm: NC-OR-01
Links to Helpful Information
Samplelb. 01-01
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -SG silage/Soybean
0.5 80-100 0
110 0 0
0
0
0
0
Note: 3
2-
Test Results [units - W/V in g1cm3; CEC and Na in meg1100 crr-P; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 1.04 10.3 84 1.6 5.7
108 36 62 21
55 677 416
501
501
131
0.2 2
Sample ID: 01-02
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -SG silage/Soybean
0.0 80-100 0
120 0 0
0
0
0
0
Note: 3
2-
Test Results [units - W/V in g/ca; CEC and Na in meg1100 cm3; NO3-N in mgldrr>3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.46 0.92 10.6 88 1.3 5.9
193 31 69 17
66 907. 554
795
795
202
0.2 2
Sample ID: 01-03
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -SG silage/Soybean
0.3 80-100 0
110 0 0
0
0
0
0
Note: 3
2-
Test Results [units - WN in g/crrr3; CEC and Na in meg1100 crrr3; NO3-N in mgldnt3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.96 9.9 87 1.3 5.8
145 35 60 25
81 905 553
629
629
139
0.2 2
North'Carolina
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture
l

Website: www.rr--,e1gov1agronomi/
Report No. FY1;--_- )16372
NCDA&CS . s6._Aomic Division Phone: [phone]
Page 2 of 3
Sample ID: 01-04
Recommendations: Lime
Nutrients (Ib/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1 -SG silage/Soybean 0.0
80-100 0
120
0
0
0 0
0 0
Note: 3
2-
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-1
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.51 0.94 11.2 88 1.4 5.9 177 33
63 23 78
712
437
698 698
184 0.2 2

NCDA&CS ,:y,.;aomic Division Phone: [phone] Website: www.r-,'--,_�,gov/agronomi/
Report No. FY1� _., .)16372
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/apronomi/oboart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-I, S-I,'SS-I, Na, ESP, SS -I, NO3-N (not
Zn-I
zinc index
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uymt.htm
for more information.

NCDA&CS . _comic Division Phone: [phone] Website: www.r';= .
_,;;gov/agronomi/
Report No. FYI D01828
Predictive
Client:
David Walker
2909 Walker Rd.
Advisor:
Creighton Brown
Synagro Central
wt
Hillsborough, NC 27278
284 Boger Rd
=?�
®
S o i I Report
Soil
Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Orange
Sampled: 07/01/2014 Received:
07/30/2014 Completed: 08/08/2014
Farm: Durham
Links to Helpful Information
Sample ID: 0135-1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
1.3 0 0
40
0 0
0
0
0
0
Note: 3
2 -
$pH
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cd; NO3-N in mgldrrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 0.95 7.8 69 2.4 5.3
76 49 49 17
60
438
273
96
96
86
0.1 1
Sample ID: OR5-2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre) N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
2.5 0 0
80
0 0
0
0
0
0
Note: 3
2 -
$pH
Test Results [units -W/V in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mg1drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.27 0.91 7.9 57 3.4 4.4
66 29 40 15
127
860
526
78
78
83
0.1 1
Sample ID: OR5-3
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Soybean
1.8 0 0
10
0 0
0
0
0
0
Note: 3
2 -
$pH
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mgldd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 1.00 7.9 65 2.8 5.0
90 71 43 17
72
1012
617
107
107
97
0.0
NorLh Carolina
&�ba.ccn Ru>r I'u�od icunroilasluq
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS''.%"y.., iomic Division Phone: [phone]
Website: Wwwx��,k,govlagronomi/
Report No.
FY1L.___,�,)01828
David Walker
Page 2 of 3
Sample ID: OR5-4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean
1.3
0 0
30
0
0
0
0
0 0
Note: 3
2 -
$pH
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.08 6.5
65 2.2 5.2
118 57
45 15
60
1152
701
103
103
87 0.0
Sample ID: OR6-1
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1
0.0
120-200 0
0
0
0
0
0
0 0
Note: 12
2 -
$pH
Test Results [units - WN in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.86 16.1
94 1.0 6.5
214 88
78 13
41
407
254
326
326
215 0.1
1
Sample ID: OR6-2
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1
0.0
120-200 0
80
0
0
pH$
0
0 0
Note: 12 Note:
2 -
$pH
Test Results [units - W/V in
g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.36 0.89 10.8
93 0.8 6.6
68 31
75 16
54
560
344
145
145
135 0.1
1
Sample ID: OR507
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, I*
0.0
120-200 0
0
0
0
0
0
0 0
Note: 12
2 -
$pH
Test Results [units - WN in g/cd; CEC and Na in meq/100 ca; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.82 20.6
94 1.2 6.5
348 88
79 13
67
942
575
384
384
256 0.1
0

NCDA&CS.-yu_iomicDivision Phone: [phone] Website: www.r__,;..gov/agronomi/
Report No. FYI' ,._-)01828
David Walker
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-AI1
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-n- I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/oboart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not
Zn-I
zinc index
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm
for more information.

Page 1 of 2 -
Repoli Number: 15-007-0679
@P.
Account Number: 46451
wwwaleastern.com
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
.284 BOGER RD
MOCKSVILLE NC 27028
n.fn Rcroivnrh n1/07/9r1.F natP OfAnalvcis: n1/nR/2015
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower: Submitted By: NATE ROTH
FAIRCREST LAND & CATTLE Farm ID: OR-70
DURHAM PROJECT
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 01/09/2015
Organic
Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate lbs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm
Rate
P H
Index
meq/100g
meq/100g
70-01
01140
4.3 M 120
1225 VH
83 L
273
H
1221
M
28
VL
5.7
6.70
2.3
11.0
NC=1021
NC=42
70-02
01141
5.4 H 142
998 VH
M
7NC
1265
H
1169
M
126
VL
5.5
6.63
3.0
11.5
NC=832
=68
70-03
VH
M
VH
1198
M
VL
6.2
1
1.3
10.5
01143
3.1 M
97
�455
1144
1332
1
126
NC=379
NC=74
70-04
01144
6.2 H 150
1233 VH
1 131 M
1323
H
1375
M
148
VL
5.6
6.62
3.1
13.2
NC = 1027
NC = 67
Percent
Base
Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble
Salts
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
%
%
%
%
%
PP m Rate
PP m Rate
m Rate
ppm
PP m Rate
PP m
Rate
P.P m Rate
PP m
Rate
ms/cm Rate
PP m Rate
PP m
70-01
34 H
146.5 VH
37 H
425
VH
11.1 VH
0.8
M
0.15
VL
1.9
20.7
55.5
1.1
21.2
NC = 71
NC = 3662.5
NC = 231
1 NC = 555.0
70-02
VH
VH
50 H
VH
VH
H
VL
2.9
19.2
50.8
1.0
25.7
137
NC = 77
1133.4
NC = 3335.0
NC = 313
�396
18.9
NC = 445.0
11.5
10.19
70-03
H
VH
H
VH
2.7 H
M
VL
3.5
26.3
57.0
1.1
12.1
130NC=62
138.4
NC=960.0
135
NC=219
1272
NC=135.0
10.8
10.16
70-04
35 H
181.3 VH
VH
466
VH
12.6 VH
M
VL
2.5
20.4
52.1
1.6
23.3
NC = 73
NC = 4532.5
152
NC = 325
NC = 630.0
10.9
10.2
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: iX"a
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

Page 2 of 2 - -
Report Number: 15-007-0679
Account Number:46451
Send To: SYNAGRO CENTRAL LLC/DURHAM
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/07/2015
Date Of Report: 01/09/2015
@P.
www.aleastem.com
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
FAIRCREST LAND & CATTLE
DURHAM PROJECT
SOIL FERTILITY RECOMMENDATIONS
Submitted By: NATE ROTH
Farm ID: OR-70
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
Tons/A
N
P 2 05
K zO
M 9
S
Zn
Mn
Fe
Cu
B
Field ID
Tons
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
70-01
Fescue Hay
4
1.3
50
0
250
0
0
0
0
0
0
0
70-02
Fescue Hay
4
1.8
50
0
227
0
0
0
0
0
0
0
70-03
Fescue Hay
4
0.0
50
0
198
0
0
0
0
0
0
0
70-04
Fescue Hay
4
1.5
50
0
230
0
0
0
0
0
0
0
Comments:
Sample(s) : 70-02,70-03,70-04 Crop: Fescue Hay
Apply additional 50 pounds of nitrogen after every cutting and harvest of hay.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q �1
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

NCDA&CS iomic Division Phone: [phone] Website: www.rh_�:-:gov/agronomi/ ReportNo. FY1. _ .-:)16371
Client: Latta, Bill (William)/M.A. Advisor: Nate Roth
Predictive
3315 Edmund Latta Rd Synagro
�,• w� �- �
�• w'ai~�
Mehlich-3 Extraction
a: Soil Report
Hillsborough, NC 27278 284 Boger Rd
g 9
Mocksville, NC 27028
Sampled :Oran e
P County: g
Sampled: Received: 11/14/2014 Completed: 12/10/2014 Farm: NC-OR-76 Links to Helpful Information
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have
accumulated in the soil and are approaching a level that could be detrimental to
crop production. The C and Z symbols are printed on your report for soil test index levels of 2000 or more; for peanuts with zinc, the level is 300. This note is designed to be a "trigger"
that allows enough time to either reduce the rate of application or find another field for application
of biosolids and/or waste water. The CTL (critical toxic level) for Cu &amp; Zn has
been set at 3000 index; for peanuts with zinc, the level is 500. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped.
The CTL for copper and zinc was set to prevent levels from accumulating to the goint where the
become toxic to cro s grown on a field.
Sample ID: 76-09
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P2O6
K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -SG silage/Soybean 0.0 80-100 0
110 0 0 0 0 0 0
Note: 3
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mgldd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1
Mn-1 Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS -I NO3-N
0.36 1.01 10.1 86 1.4 6.0 296 37 59 25 53
257 164 1287 1287 264 0.2 2
Sample ID: 76-10
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre) N P2O6
K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -SG silage/Soybean 0.0 80-100 0
90 0 0 0 0 0 0
Note: 3
2-
Test Results [units - WN in g/crrr't; CEC and Na in meq/100 cm3; NO3-N in mgldd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I
Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N
0.32 1.01 9.5 84 1.5 5.9 325 47 58 24 62
304 192 1679 1679 241 0.2 2
_North Carolina
3c�baccc�.Trust I'we�.Comiaik;sian,
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ntayr.gov/agronomi/
ReportNo.
FY1;,=.i_,J16371
Page 2 of 3
Sample ID: 76-12
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, silage 1.9
180-220 0
90
0
0
0
Z
0 0
Note: 3 Note:
2-
Test Results [units - WN in g/crrr?; CEC and Na in meq/100 cd; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 0.78 10.8 72 3.0 5.0 410 53
58 11'
82
641
402
2445
2445
400 0.2
2
Sample ID: 76-14
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, silage 1.5
180-220 0
130
0
0
0
Z
0 0
Note: 3 Note:
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn'-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 0.88 10.7 75 2.7 5.3 398 32
59 14
65
425
272
2662
2662
420 0.2
2

NCDA&CS Division Phone: [phone] Website: www.r:%.i-.,,,,:gov/agronomi/
Report No. FY1°�, 016371
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test, results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs,, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs. htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncaar.aov/agronomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
Page 3 of 3
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
KI
potassium index
K2O
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-0
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil •pH
P-1
phosphorus index
P206
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrst.htm
for more information.
weight per volume
zinc availability index
zinc index

NCDAiCS Ukkiomic Division Phone: [phone]
Website: www.n�;.,-,,.,.'gov/agronomi/
Report No. FY11� a�116357
Mjjq-
Client:
Larry Walker
Advisor:
Nate Roth
e Predictive
5120 St. MaRd
rys
Synagro,
Hillsborough, NC 27278
284 Boger Rd
Mehlich-3 Extraction
Soil Reoft
p
Mocksville, NC 27028
Sampled County: Orange
Sampled: Received: 11/14/2014
Completed: 12/09/2014
Farm: NC-OR-91
Links to Helpful Information
Sample ID: 91-01
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P206
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
50
0 0 0
0
0
0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/1 00 cd; NO3-N in mg/dd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH - P-1 K-1
Ca% . Mg%
S-1
Mn-1
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.32 0.89 13.5 90 1.3 6.1 365 44
60 28
52
723
450 1437
1437
291
0.2 1
Sample ID: 91-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S Mn
Zn
Cu
13
Information
Lime History:
I -Fescue/OGrass/Tim, 1 0.5
120-200 0
80
0 0 0
0
0
0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/1 00 cn-P; NO3-N in mg/dd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.41 0.81 9.1 84 1.5 5.7 164 28
55 27
52
360
233 365
365
103
0.1 1
Sample ID: 91-03
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.7
120-200 0
-
70
0 0 01
0
0
0
Note: 12
2-
Test Results [units - WN in g/crTP; CEC and Na in meq/1 00 cd; NO3-N in mgldd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2 Zn-I
Zn-Al
Cu-1
Na ESP SS-1 NO3-N
0.36 0.82 11.2 85 1.7 5.6 397 36
58 26
59
318
208 1797
1797
330
0.2 2
,Norih-Carolina,
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco -Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
. - Steve Troxler, Commissioner of Agriculture

NCDA&CS y..,.iomic Division Phone: [phone]
Website: www.r:,;-,..gov/agronomil
ReportNo. FY1�J �)16357
Larry Walker
Page 2 of 3
Sample ID: 91-04
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
50
0
0
0 0
0 0
Note: 12
2-
Test Results [units - WN in g/cnn ; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.32 0.83 12.7 88 1.6 5.9 325 44
57 28 53
447
285
1584 1584
310 0.2 2

NCDA&CS may,, _'aomic Division Phone: [phone]
Website: www.r:_-_1. gov/agronomi/ Report No. FY1t, _2g)16357
Larry Walker
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is.not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot
find the exact fertilizer grade recommended on the report, visit www.ncapraov/aaronomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.gov/agronomi/uvrst.htm
for more information.
Page 3 of 3
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-1
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-I
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-Ail
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
W/V
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

NCDA&CS , y.--4iomic Division Phone: [phone]
Predictive
e
Soil Report
a.
Website:
Mehlich-3 Extraction
y.gov/agronomi/
Client: Sidney Thompson
1431 Barker Rd
Milton, NC 27305
Sampled County: Person
Report No. FYI'L— d)32419
Advisor: Synagro/J Blackwell
284 Boger Rd
Mocksville, NC 27028
Sampled: Received: 04/07/2014
completed: 04/16/2014
Farm: Durham
Links to Helpful Information
Sample ID: PSI-1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
2 = Fescue/OGrass/Tim, 0.0
120-200 0
60
0
0
0
0
0 0
Note: 12
Test Results [units - W/V in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.32 1.06 7.3 85 1.1 6.1 113 38
53 30
45 334
216
216
345
345
185 0.1 1
North "Carolina
1"eUa�za.7'tust fwd�:+Cfnrns6sst€��e.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
Steve Troxler, Commissioner of Agriculture

NCDA&CS -;.riomlc Division Phone: [phone] Website: www.r,_-1,.gov/agronomi/
Report No. FY1L,,�•)32419
Sidney Thompson
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange.capacity
full rateis applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-1
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels.. If $, pH$, $pH, C or Z
M-0
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncaar..pov/aaronomi/obpart4.htm#fs to find
P-I
phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.crov/apronomi/uvrst.htm
for more information.

NCDA&CS'-'-v-4.'iomic Division Phone: [phone]
Website: www.r.�,-,,..',gov/agron-omi/
Report No. FY1�1-016373
Client:
Sidney Thompson
Advisor:
Nate Roth
Predictive
1431 Barker Rd
Milton, NC 27305
Synagro
284 Boger Rd
Soil Report Mehlich-3
Extraction
Mocksville, NC 27028
Sampled County: Perquimans
Sampled: Received: 11/14/2014
Completed: 12/09/2014
Farm; NC-PS-1
Links to Helpful Information
Sample ID: 01-02
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
I -Fescue/OGrass/Tim, 1 0.4
120-200 0
10
0 0
0
0
0
0
Note: 12
2-
Test Results [units -WIV in glCd; CEC and Na in meq/1 00 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC IBS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All Mn-Al2
Zn-1
Zn-Al
Cu-1
Na ESP SS-1 NO3-N
0.32 1.14 6.4 80 1.3 5.7 81 74
50 24
39
525
332
384
384
72
0.1 2
Sample ID: 01-06
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.4
120-200 0
30
0 0
0
0
0
0
Note: 12
2-
Test Results [units - WIV in g/crrP; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All MnwAl2
Zn-1
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.36 1.08 8.5 84 1.4 5.8 217 59
54 26
39
160
113
1022
1022
334
0.1 1
Sample ID: 01-07
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
I -Fescue/OGrass/Tim, 1 0.4
120-200 0
20
0 0
0
0
0
0
Note: 12
2-
Test Results [units - WIV in g/crrP; CEC and Na in meq/1 00 cmP; NO3-N in mg/drT?]:
Soil Class:
Mineral
HM% WIV CEC 13S% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-1
-Mn-All Mn-Al2
Zn-1
Zn-Al
Cu-I
Na ESP SS-1 NO3-N
0.41 1.07 8.1 82 1.5 5.8 164 64
49 28
40
205
140
741
741
157
0.1 1
- %--Norih Carolina
'I—
J
Ow
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

'NCDA&CS A �g,�Giomic Division Phone: [phone]
Website: www.r q,i.-.gov/agronomi/
Report No. FY14 - a)16373
Sidney Thompson
Page 2 of 3
Sample ID: 01-10
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O6
K2O Mg
S ,
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.4
120-200 0
0 0
0
0 0
0 0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.46 0.97 9.4 84 1.5 5.8 121 119
49 28 48
307 201
740 740
226 0.1 1

NCDA&CS;-,..J iomic Division Phone: [phone] Website: www.r..­,p!.govlagronorni/ Report No. FY'l ._ A16373
Sidney Thompson Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG'is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-I
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
% CEC occupied by magnesium
MIN
mineral soil class
Mn
Mn-A11
Mn-AI2
Mn-I
M-O
N
Na
NO3-N
ORG
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot pH
find the exact fertilizer grade recommended on the report, visit www.ncaar.gov/aaronomi/obpart4.htm#fs to find P-1
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P206
S-1
Test Results SS-1
W/V
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-1, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncaar.gov/apronomiluvrst.htm
for more information.
manganese
Mn-availability index for crop 1
Mn-availability index for crop 2
manganese index
mineral -organic soil class
nitrogen
sodium
nitrate nitrogen
organic soil class
current soil pH
phosphorus index
phosphate
sulfur index
soluble salt index
weight per volume
zinc availability index
zinc index

NCDA&CS °;�•,, fiomic Division Phone: [phone]
Website: www.rt__,,��govlagronomi/
Report No. FY1, ._-9!)34331
Client:
Sidney Thompson
Advisor:
Creighton Brown
�r `�,•!,, Predictive
1431 Barker Rd
Synagro Central
",
Mehlich-3 Extraction
Milton, NC 27305
284 Boger Rd
Mocksville, NC 27028
A , Soil Report
Sampled County: Person
Sampled: 04/01/2014 Received: 04/28/2014
completed:_ 05/06/2014
Farm: Durham
Links to Helpful Information
Sample ID: PS1-5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
40
0 0
0
0
0
0
Note: 12
2-Fescue/OGrass/Tim, 0.0
120-200 0
40
0 0
0
0
0
0
Note: 12
Test Results [units - WIV in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mgldm3]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH 0-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.92 1.02 11.3 87 1.4 6.0 91 50
64 21
90 461
294 294
689
689
268
0.1 1
Sample ID: PS112
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
70
0 0
pH$
0
0
0
Note: 12 Note:
2-Fescue/OGrass/Tim, 0.0
120-200 0
70
0 0
pH$
0
0
0
Note: 12 Note:
Test Results [units - WIV in glcm3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WIV CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.66 0.83 20.7 99 0.1 7.1 331 32
91 8
63 159
96 96
356
356
272
0.1 0
.-North Carolina,
i .
�'Ftiir�c�a5'rust funrJ�ConvsrSssi�s�.
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS _ _-___iomic Division Phone: [phone] Website: www.i_1�.___jgov/agronomi/
ReportrtNo. FY
Sidney Thompson Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Lime
If testing finds that soil pH is too loW for the crop(s) indicated, a lime recommendation will be given in units of either
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Fertilizer
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
only on reports for greenhouse soil or problem samples.
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
ncagr.gov/agronomi/pubs.htm.
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot
find the exact fertilizer grade.recommended on the report, visit www.ncagr.pov/agronomi/obpart4.htm#fs to find
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer
Test Results
The first seven values'[soil class, HM%, W/V,'CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
remaining 16 [P-I, K-1, Ca%, Mg%, Mn-.I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-1, S-I, SS -I, Na, ESP, SS-1, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrsthtm
for more information.
_ Report Abbreviations
Ac
exchangeable acidity
B
boron
BS%
% CEC occupied by basic cations
Ca%
% CEC occupied by calcium
CEC
cation exchange capacity
Cu-1
copper index
ESP
exchangeable sodium percent
HM%
percent humic matter
K-1
potassium index
K20
potash
Mg%
%o CEC occupied by magnesium
MIN
mineral soil class
Mn
manganese
Mn-All
Mn-availability index for crop 1
Mn-AI2
Mn-availability index for crop 2
Mn-1
manganese index
M-O
mineral -organic soil class
N
nitrogen
Na
sodium
NO3-N
nitrate nitrogen
ORG
organic soil class
pH
current soil pH
P-1
phosphorus index
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
WIV
weight per volume
Zn-AI
zinc availability index
Zn-I
zinc index

Page 1 of 2 ___. ___
Report Number: 15-007-0678 A�
Account Number:46451 �;,i�
Send To: SYNAGRO CENTRAL LLC/DURHAM wwwaleaste- rn.-
com
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 01/07/2015 Date Of Analvsis: 01/08/2015
-A&L_.Eastern Laboratories
7621 Whitepine Road Richmond, Virginia-23237' (804)Y4379401 Fax (804) 271,6446
Grower:
CLINT MORROW Farm ID: PS-29
DURHAM PROJECT
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 01/09/2015
"Organic Matter
Phosphorus
Potassium
Magnesium
Calcium.
Sodium
_
pH
Acidity
C.E.C_� x"
Sample.ID
Lab
ENR-
"
Mehlich 3
Reserve
K
Mg,
Ca
-Na
Soil
BufferH-
Field ID
Number
% Rate IbslA
_
_
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
pH
Index_
meq/100g
meq/100g"
29-01
01138
4.4 M 126
498 VH
83 L
247 VH
778
L
23
VL
5.6
6.74
1.9
8.2
NC=415
NC=42
29-02
01139
7.8 VH 150
906 VH
184 VH
1322 H
1 1328
M
128
VL 1
5.7
6.67
2.6
12.6
NC=755
NC=94
Percent
Base Saturation
Nitrate .
Sulfur
Zinc
Manganese
Iron
Copper, .
'Boron
Soluble
Salts
Chloride
Aluminum
Sample ID
K
Mg "�
Ca
Na
H"
NON,
S
Zn- ..
Min
Fe
Cu
B `
SS
Cl
Al -
Field ID
%"
%
oho
%
%
ppm Rate
,ppm Rate
ppm Rate,ppm
Rate
ppm
Rate,
ppm Rate
;ppm
Rate
ms/cm Rate.,,ppm
Rate
ppm." "
29-01
24 M
48.1 VH
30 H
324
VH
4.6 VH
0.6
M
0.09
VL
2.6
25.1
47.4
1.2
23.2
NC = 50
NC = 1202.5
NC = 188
I
NC = 230.0
1
.
29-02
H
VH
H
416
VH
VH
M
VL
3.7
21.3
52.7
1.0
21.0
131NC = 64
1119.4
NC = 2985.0
128
NC = 175
18.6
NC = 430.0
10.9
10.12
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Fwz. 10 Gewr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

.Kt ,
Page 2 of 2
Report Number: 15-007-0678 Rj
Account Number: 46451
Send To: SYNAGRO CENTRAL LLC/DURHAM .wwwaleasternxom
Mary, Brewer
284 BOGER RD
MOCKSVILLE NC 27028
A&L Eastern .Laboratories
7621 Whitepine Road Richmond, Virginia 23237- (8A4).743-A01 —Fax (804) 271.g06
i
Grower:
CLINT MORROW Farm ID: PS-29
DURHAM PROJECT
I
Date Received: 01/07/2015
Date Of Report: 01/09/2015 SOIL FERTILITY RECOMMENDATIONS
Nitr gen
o
osph
Ph ate
P h
Potash
riesi
Mag um
S ur
ulf
Zinc
Ma gan se
n e
1 ron
C er
opp
B n
oro
Supple ID
Intended Crop
Yield Goal
Lime
-
N
P205
K20
Mg
S
Zn -
Mh
Fe
Cu "
B
Field ID
Tons
TonslA
Ib/A
JbIA
Ib/A
IbIA
Ib/A
-�Ib/A
IbIA
Ib/4
IbIA
Ib/A °
29-01
Fescue Hay
4
1.0
50
0
250
0
0
0
0
0
. 0
0
29-02
Fescue Hay
4
1.5
50
0
102
0
0
0
0
0
0"
0
Comments:
Sample(s) : 29-02 Crop: Fescue Hay
Apply additional 50 pounds of nitrogen after every cutting and harvest of hay.
If this soil is organic sand, no lime is needed for soil with pH 5.2 or above. If the soil pH is lower than 5.2 then apply 1.0 ton per acre.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." �f
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Pori.f"c 1eo"
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary