WQ0002883_2014 Residual Annual Report_20150302

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CITY OF ELIZABETH
CITY
2014 ANNUAL LAND APPLICATION OF
RESIDUAL BIO-SOLIDS REPORT
CLASS B PROGRAM
WQ0002883
Submitted by:
Soil Plus
208 Williams Street
Greenville, North Carolina 27858
February 17, 2015
S AWA"1.
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RECEIVEDIDENRIDWR
MAR m 2.2015
WatwQuality
Penkting Section

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February 17, 2015
J NCDENR-DWQ
Information Processing Unit
J 1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2014 LAND APPLICATION ANNUAL REPORT
Elizabeth City "Class B" Program
y NC Permit No.: WQ002883
Soil Plus Project No. 200704.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the City of Elizabeth City on behalf of
Granville Farms, Inc. Soil Plus compiled this report using data gathered during the
compliance year. This data includes (1) certification form, (2) residual sampling, (3) field
loading calculations, (4) pathogen and vector attraction reduction documentation, (5)
standard soil fertility nutrient analysis.
The City of Elizabeth City conducted application events on permitted fields in Pasquatank
County during 2014. A total of 696.13 Dry Tons or 8,813,000 gallons of permitted residual
bio-solids from the City's WWTP and 2,345,000 gallons or 1,796.10 Dry Tons of Water
Treatment Plant were land applied to permitted fields. A total of 147,000 gallons or 85.82
Dry Tons of Water Treatment Plant residuals were land applied under Granville Farms'
Class A Permit (WQ0033587) in Pasquotank Counties for Agricultural uses. A total of
119,000 gallons or 82.87 Dry Tons of Water Treatment Plant residuals were taken to the
City of Elizabeth City's Surface Disposal Unit (WQ0014808) for further processing. A
total of 11,424,0.00 gallons or 2,660.92 Dry Tons were generated by permitted City of
Elizabeth City Sources in 2014.
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Elizabeth City (252-337-6626) for further assistance.
Respectfully,
0"Z�-L-7
C. Scott Carpenter, L.S.S.
North Carolina Nutrient Management Planner
208 Williams St. Stephen Carver, City of Elizabeth City
Greenville, NC 27858 Bryan Smith, Granville Farms
t [phone]
f [phone]
www.soilplus.net

City of Elizabeth
City. 2014 Annual
Land Application of
Residual Bio-Soilds
Report
WQ0002883
Elizabeth City, NC
(7
ANNUAL
CERTIFICATION FORM
Source Summary
Field Loading Summary
RESIDUAL SAMPLING
SUMMARY FORM
Elizabeth City WWTP
Elizabeth City WI?
FIELD SUMMARY FORM
PATHOGEN & VECTOR
REDUCTION FORM
Elizabeth City WWTP
SOIL SAMPLES

APPENDIX I
CERTIFICATION FORM
SUMMARY FORM

ANNUAL LAND APPLICATION CERTIFICATION FORM
PermitNumber FacilityName Land Application Operator County Phone Number
i)
WQ0002883 City of Elizabeth City Granville Farms Pasquotank [phone]
Year: 2014
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the
Fill
residuals were handled.
~,Part A - Residuals Application Summary:
Total number of application fields in the permit: 48
Total number of fields utilized for land application during the year: 9
i
Total amount of dry tons applied during the year for all application sites: 2316.73
Total number of acres utilizes for land application during the year: 1146.83
i Part B - Annual Compiance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
" Including but not limited to items 1-13 below) issued by the Division of Water Quality ❑� ❑�
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) 'to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
zesults are attached
1. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
zertified laboratory results are attached
6.The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
Facilities).
S. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated
Facilities).
). All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
-received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
nclude appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
t2. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Fart C - Certification:
•'I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
:omplete. I am aware that there are significant penalties for submitting false information, ' luding the ossibility of fines and
mprisonment for knowing violations."
+?aul A. Fredette, Public Utilities Director
Pe i ee d itle (type or print): Signature of Permittee
signature of Preparer* Date
`,if different from Permittee)
- * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
2-17-2015
Signature of Land Applier Date
(if different from Permittee)
Tuesday, February 17, 2015
r-

Source Summary Report _dV
Elizabeth City WTP 2,345,000 1620.61
Elizabeth City WVrl? 8,813,000 696.13
Total 11,158,000 2316.73
Wednesday, March 4,2015 Page 1 of 1

:T Source Summary Report 4r.
✓ WWT VolumeApphed Total Dry Tons
Elizabeth City WTP 2,345,000 1796.10
Elizabeth City WWTP 8,813,000 696.13
Total 11,158,000 2492.22
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fT_Juesday, February 17, 2015 Page 1 of 1
a

FEAR TO DATE FIELD LOADING SUMMARY
CROPS USED AND VOLUME APPLIED PERMITTED CROPS AND LOADING RATES
Acres Volume Crop 1 PAN Crop 2 PAN Total P Crop 1 PAN 1 Crop 2 PAN 2
Field Used Applied Total DT lbs/Ac. lbs/Ac. lbs/Ac. Crop 1 Name PAN Used Crop 2 Name PAN Used
Site# LL
2 153.02 833,000 174.99 2.04 3.96 Wheat, Grain 100 2.0% Soybeans, Manured, 50
Full Season
Site# WB
1 155.84
1,505,000
639.89
4.46
3.24 6.54
Wheat, Grain
100
4.5%
Soybeans, Manured,
50 6.5%,
Full Season
2 153.02
798,000
95.84
6.20
4.74
Wheat, Grain
100
6.2%
Soybeans, Manured,
50
Full Season
3 110.39
2,744,000
705.84
8.97
10.42 6.85
Corn, Grain
160
5.6%
Wheat, Grain
50 20.8%
4 79.19
532,000
65.44
13.46
6.44
Corn, Grain
160
8.4%
Wheat, Grain
50
5 166.49
700,000
14.60
1.96
3.31
Wheat, Grain
100
2.0%
Soybeans, Manured,
50
Full Season
6 144.21
840,000
17.51
2.71
4.58
Wheat, Grain
100
2.7%
Corn, Grain
50
7 166.71
2,233,000
545.41
21.21
13.07
Corn, Grain
160
13.3%
Wheat, Grain
50
8 104.42
973,000
57.21
13.34
7.31
Wheat, Grain
100
13.3%
Soybeans, Manured,
50
Full Season
Total 11,158,000
Tuesday, February 17, 2015 Page 1 of 1

f
APPENDIX II
RESIDUAL SAMPLING SUMMARY FORM
FIELD LOADING CALCULATIONS
ANALYTICAL

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0002883 Facility Name City of Elizabeth City Source Permit No. NCO025011
Laboratory 1
Environment
hnvironment
linvironment
1{nrironment
1, Inc.
I, Inc.
I, Inc.
I, Inc.
Laboratory 2
Sample or CompositcDate
3/24/2014
6/20/2014
9/24/201.1
12/222/2014
Parameter (mg/Kg) Class A Clas B
-- Aluminum -N/A- N/A
6,250
-- 9,304
-- 7,659- -
- 5,301
Ammonia Nitrogen N/A N/A
468
356
383
324
Arsenic 41 75
5.3
6
6
2.9
Cadmium 39 85 -
- 1.3 -- -
1.8
_
L6
Calcium N/A N/A
93,521)
107,479
71,426
154,462
Copper
1,500
4,300
204
.267
318
231
Lead
300
840
22
22
25
22
Magnesium
N/A
N/A
5,092
7,389
6,623
5,751
Mercury
17
57
0.26
0.47
0.53
0.29
Molybdenum
N/A
75
5
5
5
5
Nickel
420
420
9
8
9
7
Nitrate -Nitrite Nitrogen
N/A
N/A
44
68
29
108
Percent Solids
N/A
N/A
2.88
2.95
1.41
0.50
- pH (no units)
-N/A
-12.03 --
-N/A
-- 12.07
12.07
11.69 --
-----Phosphorus
- 6,669--
- 18,867
N/A
N/A
3,781 -
3,899 --
- -- Potassium
- N/A
N/A
-- 6,357 -
- 4,889 -
- 5,030 --
- 5,097 --
- PAN (Inj./Inc.)
-N/A
N/A
-- 5,185 -
8,319 -
-- 12,170
- 11,324
PAN (Surface)
11,162
N/A
N/A
4,951,
8,141
11,979
- Selenium
100
100
5
5
5
5
Sodium
N/A
N/A
3,787
4,347
5,150
51591
SAR
N/A
N/A
0.55
0.59
0.59
0.27
TKN
N/A
N/A
16,042
26,672
39,578
36,631
Zinc
2,800
7,500
659
740
849
612
Source Name Llizabeth City WWI?
" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
iignamreVof Preparer *
*Pmnnrer is defined in 40 CFR Part 503.9(rl anti 15A NCAC 2T .1102 (26)
Date

FIELD LOADING ESTIMATES
( Facility Elizabeth City WWTP
Sampling Date 3/24/2014
�.
% Solids 2.88
'
Mineralization Rate 0.3
�.
Gallons per DT 8,326.67
pH 12.31
'
Sodium Absorpotion 0.55 <5.0 Safe 5.0
- 10.0 Careful Management >15.0 Do Not Land Apply
.r
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 16,042
lbs./1,000 gal 3.85
Potassium lbs./1,000 gal
1.53
t.
C.
Ammonia Nitrogen (mg/Kg) 468.00
lbs./1,000 gal 0.11
Phosphorus lbs./1,000 gal
0.91
Nitrate -Nitrite (mg/Kg) 44.39
lbs./1,000 gal 0.01
Calcium lbs./1,000 gal
22.46
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
1.22
PAN (mg/Kg) 4,951
lbs./1,000 gal 1.19
Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 5185
lbs./1 000 gal 1.25
Molybdenum lbs./1,000 gal
0.00
1 Volatization Rate= 0.5 Surface Application
1.0Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Limits (mg/Kg)
41
Class B Ceiling
Limits (mg/Kg)
75
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
5.30
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
. 1.30
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
204.00
Copper lbs./1,000 gal
0.05
` Lead (mg/Kg)
22.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.26
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
9.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
659.00
Zinc lbs./1,000 gal
0.16
' RESIDUAL NITROGEN CALCULATION
' 1st Year
)2nd Year
i '3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TEN
PAN PAN
Nitrogen
TEN
PAN PAN
Nitrogen
(mg/kg) (lbs/DT)
(mg/Kg)
(mg/kg) (lbs/DT)
(mg/Kg)
16,042
4,951 9.90
11,091
16,042
5,185 10.37
10,857
11,091
1,664 3.33
9,428
10,857
1,629 3.26
9,229
9,428
707 1.41
8,721
9,229
692 1.38
8,537'
8,721
327 0.65
81394
8,537
320 0.64
8,217
8,394
157 0.31
8,236
8,217
154 0.31
8,062
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 7,806 15.61
Total 7,980 15.96

11.0. 30X 7085. 114i OAKMONT DRIVE
GREEN'VILLE_ N.C. 27835-7085
CITY OF ELIZABETH CITY
MR. ALPHONSO BROWN
ATTN: WWTP, —
P.O. BOX 347
ELIZABETH CITY ,NC 27907-0404
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, % '
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Chloride (dry wt. basis), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
6250
04/02/14 LFJ
EPA200.7
5.3
04/15/14 MEL
3113B-04
93520
04/02/14 LFJ
EPA200.7
1.3
04/14/14 MEL
3113B-04
204
04/02/14 LFJ
3111B-99
18
04/02/14 LFJ
EPA200.7
22
04/30/14 MEL
3113B-04
5092
04/02/14 LFJ
EPA200.7
0.26
03/28/14 MTM
245.1 R3-94
9
04/02/14 LFJ
EPA200.7
6357
04/02/14 LFJ
EPA200.7
<5.0
04/21/14 MEL
3113B-04
3787
04/16/14 MTM
3111B-99
659
04/02/14 MTM
3111B-99
2.88
03/27/14 LW
254OG-97
16042.
03/31/14 ANO
351.2 R2-93
468
03/27/14 ANO
350.1 R2-93
3781
03/31/14 ALB
365.4 -74
12850
03/31/14 MDD
4500CLB-97
44.39
03/28/14 ANO
353.2 R2-93
<5.0
04/02/14 LFJ
EPA200.7
Drinking'Water ID: 37715
Wastewater ID: 10
PHONE "252) 756-6208
FAX ;252? 756-0633
ID#: 1054
DATE COLLECTED: 03/24/14
DATE REPORTED : 05/01/14
REVIEWED BY:

f
r_.
i
C
Y l 14-
Lam, J��g
Facility Elizabeth City WWTP
Sampling Date 6/20/2014
% Solids 2.95
Mineralization Rate 0.3
FIELD LOADING ESTIMATES
Gallons per DT 8,129.09
pH 12.04
Sodium Absorpotion 0.59 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 26,672 lbs./1,000 gal. 6.56 Potassium lbs./1,000 gal 1.20
Ammonia Nitrogen (mg/Kg) 356.00 lbs./1,000 gal 0.09 Phosphorus lbs./1,000 gal 0.96
Nitrate-Nitrite,(mg/Kg) 67.80 lbs./1,000 gal 0.02 Calcium lbs./1,000 gal 26.44
PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./1,000 gal .1.82
PAN (mg/Kg) 8,141 - lbs./1,000 gal 2.00
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 8,319 lbs./1,000 gal 2.05
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Limits (mg/Kg)
41
1st Year
2nd Year
3rd Year
4th Year
5th Year
39
1,500
300
17
420
100
2,800
Class B Ceiling
Limits
75
85
4,300
840
57
420
100
7,500
HEAVY METAL CONCENTRATION
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL LOADING
Arsenic (mg/Kg)
6.00
Cadmium (mg/Kg)
1.80
Copper (mg/Kg)
267.00
Lead (mg/Kg)
22.00
Mercury (mg/Kg)
0.47
Nickel (mg/Kg)
8.00
Selenium (mg/Kg)
5.00
Zinc (mg/Kg)
740.00
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
(mg/Rg)
TIEN
(mg/kg) (lbs/DT)
(mg/Kg)
26,672
8,141 16.28
18,531
26,672
8,319 16.64
18,353
18,531
2,780 5.56
15,752
18,353
2,753 5.51
15,600
15,752
1,181 2.36
14,570
15,600
1,170 2.34
14,430
14,570
546 1.09
14,024
14,430
541 1.08
13,889
14,024
263 0.53
13,761
13,889
260 0.52
13,629
Arsenic lbs./1,000 gal
0.00
Cadmium lbs./1,000 gal
0.00
Copper lbs./1,000 gal
0.07
Lead lbs./1,000 gal
0.01
Mercury lbs./1,000 gal
0.00
Nickel lbs./1,000 gal
0.00
Selenium lbs./1,000 gal 0.00
Zinc lbs./1,000 gal ' 0.18
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x N113)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 12,911 25.82
Total 13,043 26.09

Dec. 1 /. 2014 11: 15AM
ERWOTOME(M % hog
hd
P.O. BOX 7085,114 OAKMONT DRIVE
GREE=NVILLE, .N.C. 27836.7085
CITY OF ELIZABETH CITY
MR, ALPHON80 BROWN
ATTN.- WWTP
P.O. BOX 347
SLIZABSTH CITY ,NC 27907-0404
Sludge
Analysis
Method
PAILUV ETERS
Sample
Date Analyst
Code
Aluminum, (dry wt. basis), rng/1cg
9304
07/01/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
6
07/1.0/.14 ME,I;
3113B-04
Calcium (dry wt, bask), tng%kg
1.07479
07/01/14 LFJ
EPA200.7
Cadmium (dry wt, basis), mg/kg
1.8
07/08/.14 h1EL
3113?3-04
Copper Wry wt. basis), mg/kg
267
07/01/14 US
MIA200.7
Chromium, 11'.(dry wt. basts),n►g/kg
23
07/01/14 LFJ
EPA200.7
Lead (dry weight basis), mg/lcg
22
07/.11/14 N..IF,I,
3113B-04
Nlagnesiuut (Jry wi. basis), mgtkg
7389
07/01/14 LFJ'
EPA200.7
Mercury (dry wt, basis), mglkg
0.47
06/26/14 NITIM
245.1 R3-94
Nickel (dry wt. basis), ntg/kg
8
07/01/14 1 .I J
EVA200.7
Potassium (dry wt. basis), mg/kg
4889
07/01/14 LFJ
EPA200.7
SCIcuhun (dry wt. basls), rug/kg
<5.0
07/15114 WIEL
3113B-04
Sodium (dry wt. hasis), mg/kg
4347
07/22/14 MTM
311.11i-99
Zinc (dry wt. basis), mg/kg
740
07/22/14 lvl'1'1V1
3111E-99
Total Solids, TO
2.95
06/23/14 LW
2540C-97
'1'RN (dry wt.), mg/1%
26672
06/26/14 ANO
351.2 R2-93
Ammunia Nitrogen (dry vvQ,mg/kg
356
06/24/14 ALB
350.1 R2-93
Phosphorus, 'P. (dry wt,), mglkg
3899
06/26/14 ALB
365.4 -74
Chloride (dry wt. basi9), nrg/lcg
2590
06/24/1.4 LW
4500CLB-97
Nitrate -Nitrite. (dry wt.), mg/kg
67.80
06/25/14 ANO
353.2 R2-93
iV,tolyb(lcnmu (dry wt. basis), mg/kg
<5.0
07/01/14 Ll!J
MIA200.7
No.33Z1 r. Z
.PHONE (252) 756=6208 .: .
• FAX [phone]
IM 1054
DATE COLLECTIED; 06/20/14
DATE REPORTED : 07/24/14
REVIEWED BYt
<<< LABORATORY COPY >>>

- AGMAN
FIELD LOADING ESTIMATES
(
Facility Elizabeth City WWTP
-;
Sampling Date 9/24/2014
_-'
% Solids 1.41
Mineralization Rate 0.3
�A
Gallons per DT 17,007.67
PH 12.17
�."
Sodium Absorpotion 0.59 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 39,578 lbs./1,000 gal 4.65
Potassium lbs./1,000 gal
0.59
,
Ammonia Nitrogen m / 383.00 lbs. 1 000 al 0.05
g ( gam) / g _
Phosphorus lbs. 1 000 al
p / g
0.78
Nitrate -Nitrite (mg/Kg) 28.79 lbs./1,000 gal 0.00
Calcium lbs./1,000 gal
8.40
_.
-
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
0.78
PAN (mg/Kg) 11,979 lbs./1,000 gal 1.41
Manganese lbs./1,000 gal
Man g
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 12,170 lbs./1,000 gal 1.43
Molybdenum lbs./1,000 gal
0.00
{
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling Class B Ce
Limits (mg/Kg) Limits (mg
41 75
t
39 85
1,500 4,300
300 840
17 57
420 420
100 100
2,800 7,500
i
r=.
r 1st Year
{ 2nd Year
'3rd Year
4th Year
5th Year
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
6.00
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
318.00
Copper lbs./1,000 gal
0.04
Lead (mg/Kg)
25.00
Lead lbs./1,000 gal
0.00
Mercury (mg/I4
0.53
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
9.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
849.00
Zinc lbs./1,000 gal
0.10
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
39,578
11,979
23.96
27,599
39,578
12,170 24.34
27,408
27,599
4,140
8.28
23,459
27,408
4,111 8.22
23,297
23,459
1,759
3.52
21,700
23,297
1,747 3.49
21,549
21,700
814
1.63
20,886
21,549
808 1.62
20,741
20,886
392
0.78
20,495
20,741
389 0.78
20,352
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/K& 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN.(mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 19,083 38.17 Total .19,226 38.45

/ E3
ElmdQo[MHGP1' �Q MopoQ �ci
P.C. R�X 7085114, GAKWONT DRIVFE
N.C. 27835-7085
CITY OF ELIZABETH CITY
MR. ALPHONSO BROWN
ATTN: WWTP
P.O. BOX 347
ELIZABETH CITY ,NC 27907-0404
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry 'wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids, % .
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Chloride (dry wt. basis), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Molybdenum (dry wt. basis), mg/kg
Sludge Analysis Method
Sample Date Analyst Code
7659
09/30/14
LFJ
EPA200.7
6
10/06/14
MEL
3113B-04
71426
09/30/14
LFJ
EPA200.7
2
10/16/14
MEL
3113B-04
318
09/30/14
LFJ
EPA200.7
24
09/30/14
LFJ
EPA200.7
25
10/21/14
N EL
3113B-04
6623
09/30/14
LFJ
EPA200.7
0.53
10/09/14
MTM
245.1 R3-94
9
09/30/14
LFJ
EPA200.7
5030
09/30/14
LFJ
EPA200.7
<5.0
10/23/14
MEL
3113B-04
5150
10/02/14
MTM
311113-99
849
10/07/14
MTM
3111B-99
1.41
09/25/14
LW
254OG-97
39578
10/02/14
ANO
351.2 R2-93
383
09/30/14
AKS
350.1 R2-93
6669
10/02/14
AKS
365.4-74
9060
10/06/14
CMC
4500CLB-97
28.79
10/01/14
ANO
353.2 R2-93
<5.0
09/30/14
LFJ
EPA200.7
Drinking Water ZD: 37715
Wastewater ZD: 10
PHONE-
f7X (2S2) 756-063'3
ID#: 1054
DATE COLLECTED: 09/24/14
DATE REPORTED : 10/28/14
REVIEWED BY:

1
r
AG:M[AN
o,-
Facility Elizabeth City' V VTP
Sampling Date 12/22/2014
% Solids 0.5
Mineralization Rate 0.3
Gallons per DT 47,961.63
pH 11.93
FIELD LOADING ESTIMATES
Sodium Absorpotion 0.27 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 36,631 lbs./1,000 gal 1.53 Potassium lbs./1,000 gal 0.21
Ammonia Nitrogen (mg/Kg) 324.00 lbs./1,000 gal 0.01 Phosphorus lbs./1,000 gal 0.79
Nitrate -Nitrite (mg/Kg) 108.00 lbs./1,000 gal 0.00 Calcium lbs./1,000 gal 6.44
PLANT AVAILABLE NITROGEN SURFACE APPLIED Magnesium lbs./1,000 gal 0.24
PAN (mg/Kg) 11,162 lbs./1,000 gal 0.47 Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED Sulfur lbs./1,000 gal
PAN (mg/Kg) 11,324 lbs./1,000 gal 0.47 Molybdenum lbs./1,000 gal 0.00
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Class A Ceiling
Limits (mg/Kg)
41
1st Year
2nd Year
3rd Year
'4th Year
1 5th Year
Class B Ceiling
Limits mg Kg)
75
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
2.90
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.60
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
231.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
22.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
- 0.29
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
7.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
612.00
Zinc lbs./1,000 gal
0.03
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (Ibs/DT)
(mg/Kg)
TKN
(mg/kg) (Ibs/DT)
(mg/Kg)
36,631
11,162
22.32
25,469
36,631
11,324 22.65
25,307
25,469
3,820
7.64
21,649
25,307
3,796 7.59
21,511
21,649
1,624
3.25
20,025
21,511
1,613 3.23
19,898
20,025
751
1.50
19,274
19,898
746 1.49
19,151
19,274
361
0.72
18,913
19,151
359 0.72
18,792
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (1Mit/16)
Total 17,718 35.44
Total 17,839 35.68

Jan• 16. 2M 4:30PM
4> III;i lt !�ijii �?'��I� •�j:^:ii �•s; ts' i• t;ji{: i�fq ,r =-she
i.:1E1Ll i�E!i}r�l:, ': L'E1'�::;i�_?• v � ��rs ;''f %�L� ��`.L!�� ,-�t7 �:.7t:J..:
No.3�36 P. 2/3
?5 -'?
-: -r.'B9X CJ85.•.it4 0AI MM)NIFVP,1VE ::.'` :::•:::::.::: :.•:: •:'.::::::.::•.... 'PHONE .E � ��)•7zb �_tr8:: •:::::
L�FEE(v�1EE.F,'.f.'. 27�;`r 7C�Ei.:.:...:.:.:......•.::.::.::•::•..:.::•:
CITY OF ELIZABETH CITY
MR. ALPHONSO BROWN
ATTN: WWTP
P.O. BOX 347
BLZZAS>3TH CITY ,NC 27907-0404
PARAMETERS
Alundmun, (dvy wt. hnsiq), mg/kg
Arsenic (dry ►►'t. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wl. hmis), mg/kg
Copper (dry wt. hnsiv), •mg/kg
Chromium, T.(dry ►r(. basis),1119/kg
Lead (dry ►ralght basis), mg/kg
1%ingne.dum (dry wt. basis), mg/kg
Mercury (dry ►rl, basis), mg/Icg
Nickcl (dry wt, hub), mg/kg
Potassium (dry ►►•t. basis), :ng/kg
ScUmium (dry wt. haaic), mgfkg
Sodium (dry wt. basis), mg/kg
Zuic (dry ►vt. basis), mg/kg
TOIRl Solids, %
TKN (dry wt.), mgfkg
Anuuania Nitrogen Wry w(.),mg/lcg
1'hosptiorls, T, (dry'wt.), mgfkg
Chloride (dry ►vl. basis), mgJkg
Nitrate-Nllrite Wry wt.), mg/kg
Mnlyhdenum (dry wt. basis), mg/kg
Sludge
Analysls
.
Method
Sample
]late Analyst
C:odc
5301
01/08115
LFJ
EPA200.7
2.9
01/08/15
lY TM
3113H-04
154462
01/08/15
1,10
EPA200.7
1.6
01/12/15
MTM
311311-04
231
01/08115
LFJ
lelIA200.7
16
01/08/15
LF-1
EPA200.7
ZZ
0111411S
NMI
311311.04
5751
01/08/15
13.1
EPA200.7
0.29
01/08/15
ATTNI
245.1 113.94
7
01/08/15
LIQ
LPA200.7
5097
01/08115
LFJ
EPA200.7
<S,U
01/15/15
A•fTM
3113H.04
5591
01 / 1211,5
1Y.1
311I B -99
612
01108/15
14ITM
3111 B.99
0,50
12/23/14
1AV
2540G-97
36631
0//05115
AKS
351.2 1.2 93
324
12/30/14
AK5
150.1 112-93
19967
01/05/15
KDR
365.4-74
968
12/29/14
Ii:KF
45000LH-97
108
12/31/14
I PII
353,2 R2-93
<5.0
01/08115
LFJ
EPA200.7
ID#: 1054
DATE COLLECTED: 12/22/14
DATE REPORTED : 01/16/15
RN:VX13WED •BY: z//,'_

Jan. 7. 2015 9:OOAM
No.3425 P. 2
S77nmth Em-irmimeniul Technulugirs. Llc.
;;: 'fit,' I•`'1�CJ rf=lfG L� 3310 will Si.
Fri: ., r; -• � ,.
�5r rNVIO1•11,1FIAht. 1.eCHUr.1LOVIEH, INC, CtgYrhugarnrrs. olno44223
_,•_.A,,:_:_ lm4y (h-.al tshar.3ivrf'm M: [phone] PAX [phone]
Websile: lmp:/As�sv .renekcam
January 06, 2015
T7ccdcc Woolard
Environment 1,1nc.
114 Oakmont Dr
11.0, Box 708.5
Greenville, NC 27858
TEL: [phone]
FAX; [phone]
RE: 1054 C
Dear Ueedee Woolard: Order No.: 14122544
There were no problems with (lie analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or nletllod specified acceptance limits except
where noted.
if you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabana •1160Q Atlmna A[0788, Arksalsai 88.0735, Callilatds 07256CA, Colorado, Comwelleut Pit•0105, Miawaro, F'lorMa MAC
E27688, t9ootglS L•'87688 and 913, ItW4l O1100923, OlinVix 400061 aml Reg.5, Indiana U•UI p13, Kru u H-103.17, Keauucky (lhdwglOwnl Stotago'1'w1k)
3, Kenlueky 901.16, l thtlximu 01061 and 1.A11001, Afaine 2D12015, Altuyland 339, D1aicaclanccll<AI•UI`I1923, AtinneANa•10971 i, Atoulyre CElf1'0099,
New 1 F.anp.hire29%, New Jmoy O1 iD06, New York 11777, North Cmolini 39705 and 631, Ohio Thinking Water 4170, Ohio VAP CIM52, Oklahoma
9940, Oregon OH2O0001, PennsyM+nis 68.01335, Rhode lsiond LA000317, South Carolina 92016001, Tennessee TN04018, Toms TI Ol70JA66.11.5,
Regian 8 MIS-1, USMVAPHIS P330-11-MZ44. Utah OHOW232011-I, Vermont VT•87688, Virginio W440 told MI. WnshinSton C991, West
Viq,inia 248 and 9957C and H7688, Whoonsin 39901301D a
Page 1 of 6

Jan. 1. 2015 9, OOAM No. 3425 P. 3
L ,r
Sumatillittvirmmtettfnllklutalogies.lte.
3310 ll'in fit.
Workorder
Sample Summary
ru�uu»nerrty'nriPt;i�rtnttltsu!;t,i;ir
L'u)•olingoPalls, Ohio 44223
llnslytic.il L.4hv-iMr?4.;
TEL: [phone] RA1: [phone]
WOII: 14122544
li'ebaite: ktm:/hrhn►settek.can
OG-Jnu-15
CLIENT:
Environment 1,1nc.
Project:
1054 C
Ub SnmpleIl) Client Sample l l) Tag No Dale Collected Dntc Recelved hlntrix
14122544-001 Sludge Sample 12/2212014 8:53:00 AM 12t2412014 10:25:00 AM Solid
Page 2 of 6

Jan. 7. 2015 9:OOAM
No. JQZ V. 4
S}iamdf k'nriranmentai �cdinalagles, Inc.
Case Narrative
1` f—
;uvk�i,raNr,tn�-,�cKr;o�oc�es,��c.
Cuyahoga ralls. Ohio 44221 w0ll:, 14122544
Analyllrnl kah"'r-l-11ic!
TEL: [phone] RX-(130)253-d489
Date: 1/6120I5
—
Website: him. A wir.setrek.com
CLIENM
Environment 1, Inc.
- Project:
1054 C
This report in its entirety consists ofthe documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Anulytical Results, Applicable Quality,
Control Summary Reports, and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit. of Quantitation
(I ,OQ) but greater than the established Method Detection Limit (MDL).
Method numbers, unless specified as SM (Standard Methods) or ASTM, are HPA methods,
listimated uncertainty values are available upon request.
All solid results arc reported on awe( weight basis unless indicated as dry weight using tlic mg/Kg-dry
designation.
Summit Filvironmental holds the accredit itions/certifications listed below that may or may not pertain
to this report.
Any comments or problems with the analytical events associated with this report are noted below,
Original
Page 3 of

Jan. 7. 2015 9:OOAM
No.3425 P. 5
U t+ /'y % =.
1 MU
S'rnerrrU enr/ronmental TWinologles, Inc.
' WO#:
14122544
RI N` (P
r n�ntar,r:(wr,ra�-', ECxlloLocies, r,:C
Cig-ahogaYalls. 0/rin 4,1223
T)elC Rc purled:
1/612015
j
nnafylleal
TEL: (330) 2JJ-82111,A.l': [phone]
Company:
N.nvironnlent ], lnc.
if'ebsile: hrnr.//�nr�v.serlek.cnm
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
12/24/2014
Projecthl:
1054 C
TCLP Metals Annlysis (6010)
Client IDN T.nb TT)# Collected Analyle Rej) Ln1t Result Units Matrix Method T)F RegLvl Run Annlyst
Sludge Sample
001
12/22/2014 TCLP Arsenlo(As)
0.50
NO mg1L
Solid
EPA 6010 C
1
6.0
12/2912014
WK
Sludge Sample
001
12/22/2014 TCLP Barlum(Ba)
5.0
NO mg/L
Solid
EPA 6010 C
1
100
12/2912014
WK
Sludge Sample
001
12/22/2014 TCLP Cadmlum(Cd)
0.10
No mg1l.
Solid
EPA 0010 C
1
1,0
12/2912014
WK
Sludge Sample
001
12/2212014 TCLP Chromlum(Cr)
0.20
NO m0/L
Solid
EPA 6010 C
1
6.0
12/29/2014
WK
Sludge Sample
001
12/2212014 TCLP Load(Pb)
0.50
NO mg/l.
Solid
EPA 6010 C
1
5.0
12129/2014
WK
Sludge Sample
001
12/22/2014 TCLP Solanlum(So)
0.50
NO rngll.
Solid
EPA 6010 C
1
1.0
12/29/2014
WK
Sludge Sample
001
12/22/2014 TCLP Sliver(Ag)
0.50
NO mg/L
Solid
FPA 0010 C
1
5.0
12129/2014
WK
Client 11)9
Lab 0/1 Collected Annlytc
TCLP Mcrculy Annlysls (131117470)
Rep but Result Units Ma(U'Ix Method D RegLvl Run Analyst
Sludge Semple 001 12/22/2014 TCLP Meroury 0.0020 NO mg1L Solid EPA 7470 A 1 0.20 12/29/2014 AU
SVOC SW-846; 808I- TCLP Pcslieldes
Client TD# Lnb IV# Collected Anulyte Rep Lint Wsult Units Matrix Method DT -RegLvl Run Analys(
Slu(Ige Sample
001
12/22/2014 Chlordene, total
0.010
ND mg(L
Solid
EPA 0001 B
1
0.030
1213112014
JBN
Sludge Sample
001
12/22/2014 Toxaphene
0.10
NO mg1L
Solid
EPA 8081 B
1
0.60
1213112014
JBN
Sludge Sample
001
12/22/2014 Endrin
0.0020
NO mg/L
Solid
EPA 6081 B
1
0.020
12/3112014
JBN
Sludge Sample
001
12/22/2014 gamine-61-1C
0,0020
NO mg1L
Solid
EPA 80813
1
0.40
12131/2014
JBN
Sludge Sample
001
12/22/2014 Heptachlor
0.D020
NO mglL
Solid
EPA 808113
1
0.0080
12/31/2014
JBN
Sludge Sample
0011
12/22/2014 Heptachlor epoxide
0,0020
NO mg/L
Solid
EPA 8081 B
1
0.0000
12/31/2014
JBN
Sludge Sample
OD1
12/22/2014 Melhoxychlor
0.0.020
NO mg/L
Solid
EPA 8061 B
1
10
12/3112014
JBN
SVOC SW-846: 8151 'Herbicides-TCLP
Client I Lab IDN Collected Annlytc lief) Lmt Result Units- Matrix Method DF RegT,vl Run Annlyst
Sludge Sample 001 12122/2014 2,4-D 0.10 NO mg/L Solid EPA 8151 A 1 10 12/3112014 JBN
SI(rdge Sample 001 12/2212014 2,4,5-TP 0.10 ND mg/L Solid CPA 61$1 A 1 1.0 12/31/2014 JON
Page 4 of

Jan. 7. 2015 9:01AM
No.3425 P. 6
�w
f::-.:�• f : l _
Simurrlt h'nvn nnrenral %ecGir I rep, h1c.
1 ?� = r r u o�
3310 Win St.
W04: 14122544
Date Reported: 1 /6R015
r.MVIR(�Ilt,1>
1�'iAL'IEtHtil�LttiGIEG, �;:C
Ci uhugaralls, 01du 44223
., ,..•. .• �,,arpuc,lr.ni>oraru�lc;: TEL: [phone]
F.U. (330) 2JJ-4489
Company: Environment 1, Inc.
wab,ire: ltrrp:7/�rtvu.sctrek.eunc
Address: 114 Oakmont
Or
t
Greenville NC: 27858
Received: 12/24/2014
Nrojecm: 1054 C
r
VOC by C UMS (8260)-'l'CLl'
...... ...... ..... _.. ...... ........ ....
_• Client TD#
Nib ID# e:ollcctcd Aunlyte,
Rep Linn, Rcsult Dilts
Mntrlx Method DF
RegLvl
Run
Analyst
_ Sludge Sample
001 12122120141,1•Dlchloroelhene
0.10 NO mg/L
Solid EPA 8260 B 1
0.70
12/2912014
MFS
Sludge Sample
001 12/22120141,2•0ichloroethane
0.10 ND mg/L
Solid EPA 8260 B 1
0.60
12129/2014
MES
Sludge Sample
001 M2212014 Benzene
0.10 NO mg/L
Solid EPA 8200 B 1
0.50 '
12120/2014
MES
,. Sludge Sample
001 12/22/2014 Carbon tetrachloride 0.10 ND mg/L
Solid EPA 8260 B 1
0.50
12/29/2014
MES
Skxlge Sample
D01 12/22/2014 Chlorobenzene
0.10 NO mg/L
Solid EPA 8200 B 1
100
12120/2014
MES
Sludge Sample
001 12/22/2014 Chloroform
oA0 NO mglL
Solid EPA 8260 B 1
6.0
12/29/2014
MES
Sludge Sample
D01 12/22/2014 Teirachloroethene
0A0 NO mg/L
Solid EPA 8260 B 1
0.70
12/292014
MF.S
Sludge Sample
D01 12/22/2014 Trichloroethene
0.10 NO mg/L
Solid EPA 8200 8 1
0.50
121202014
MES
Sludge Sample
001 12/22/2014 Vinyl chloride
0.20 NO mg/L
Solid EPA 8200 B 1
0.20
121292014
MES
Sludge Semple
001 12/2212014 MEK
210 NO mg/L
Solid EPA 6200 B 1
200
12/29/2014
MES
SVOC: 8270 TCLP RNA List
Client IDO Lab IDN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run AnAlysl
Sludge Sample
001
12/22/2014 1,4-01chlDrobonzono
0.10
NO mg1L
Solid
EPA 0270 C
1 7.5
12/302014
MO
Sludge Sample
001
12/22/2014 2,4,5-Trlchlorophenol
0.25
NO mg/L
Solid
EPA 8270 C
1 40D
12/30/2014
MO
Sludge Sample
001
12/22/2014 2,4,6-Tdchlorophenol
0.25
NO mg/L
Solid
EPA 8270 C
1 2.0
121302014
MO
Sludge Sample
001
12/22/2014 2,401nitrololuene
0.10
NO mg/L
Solid
EPA 8270 C
1 0.13
IV3012014
MO
Sludge Sample
001
12/22/2014 Cresols, Total
5.0
ND mg/L
Solid
EPA 8270 C
1 20D
12t30/2014)
MO
Sludge Sample
001
12/22/2014 Hexachloro•1,3•
0.10
NO mg1L
Solid
EPA 8270 C
1 0.60
12/30/2014
MO
buladiene
Sludge Semple
001
12/22/2014 Hexachiorobenzene
0.10
NO mg/L
Solid
EPA 8270 C
1 0.13
IN3012014
MO
Sludge Sample
001
12f22/2D14 Hexachloroethane
0.10
NO mg/L
Solid
EPA 0270 C
1 3.0
12/3012014
MO
Sludge Sample
001
12122/2014 Nitrobenzene
0.10
NO mg/L
Solid
EPA 8270 C
1 2.0
12/30/2014
MO
Sludge Sample
001
12/2212014 Pentachlorophenol
0.25
NO mg1L
Solid
EPA 8270 C
1 100
12I3012014
MO
Sludge Sample
001
12/22/2014 Pyridine
0.25
NO mg/L
Solid
EPA 8270 C
1 5.0
12130J2014
MO
Page 5 of 6

Jan. 7. 2015 9:01AM
No.3425 P. 7
J•'•- c-A•s � �', y f4 . ffinn7iff H r%ronotemal Telllltalugies, /RC.
3310 ►i rrt St.
NON: 14122544
Date
r•vani4NtdEr�7tlt_7r".t:f�rt�f nrii�r;, �;;r,
C.'u�nhagoFolls, 41,iu•ld223
Reported: 1/6/2015
An.tlyttr:all.sUoratn;lr,R MI.: (330) 2S3821/ r,LY. [phone]
Company:Environment 1, Inc.
Webjlle: Wit:/hrt�u.aul/ekGuttt
Address: 114 Oaknnont Dr
Greenville NC 27858
Received: 12/24/2014
Projectfi: 1054 C
Client 1D# Lab M# Collected Analyte
Resell Units
Matrix Method DF RL
Run Analpt
Sludge Sample 001 12122/2014 Flashpolttt (140°F)
>200 IF
Solid EPA 1010 1
12/20/2014 TAH
Sludge Sample 001 12/22/2014 Cyanide, Reactive
ND ppm
Solid EPA 9014 1 0.60
1/5/2015 TIR
SltKlge Sample 001 12/22/2014 pH
12.6 s.u.
Solid EPA 9045 0 1
1/2/2016 DHC
Sludge Sample 001 12/22/2014 Sulfide, Reacllve
ND ppm
Solid EPA 9034 1 26
115/2016 TIR
Page 6 of 6

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ANNUAL RESIDUAL SAMPLING SUMMARY FORM
WQ Permit No. WQ0002883 Facility Name City of Elizabeth City Source Permit No. 04-70.010
Laboratory 1
Laboratory 2
Sample or CompositcDate
Parameter (mg/Kg) Class A ` Clas B
Environment
1, Inc.
Environment
1, Inc.
Environment
1, Inc.
Environment
I, Inc.
2/11/2014
4/22/2014
8/25/2014
10/27/2014
Aluminum
N/A
N/A
7,994
8,111
7,479
7,395
Ammonia Nitrogen
N/A
N/A
19
198
47
9
Arsenic
41
75
2.5
2.5
2.5
2.5
Cadmium
39
85
0.5
0.5
0.5
0.5
Calcium
N/A
N/A
322,784
308,562
322,005
321,524
Copper
1,500
4,300
5
5
5
5
Lead
300
840
2.5
2.5
2.5
2.5
Magnesium
N/A
N/A
12,296
12,098
13,067
14,944
Mercury
17
57
0.02
0.02
0.02
0.008
Molybdenum
N/A
75
5
5
5
5
Nickel
420
420
5
5
5
5
Nitrate -Nitrite Nitrogen
N/A
N/A
4
5
4
4
Percent Solids
N/A
N/A
16.70
14.84
19.27
14.00
PH (no units)
N/A
N/A
10.20
10.58
9.70
10.40
Phosphorus
N/A
N/A
496
830
419
524
Potassium
N/A
N/A
145
250
250
127
PAN (Inj./Inc.)
N/A
N/A
152
327
1,15
174
PAN (Surface)
N/A
N/A
143.
233
122
169
Selenium
100
100
5
5
5
5
Sodium
N/A
N/A
1.250
1.250
1,250
1,250
SAR
N/A
N/A
0.24
0.79
0.26
0.22
THIN
N/A
N/A
343
524
284
411
Zinc
2,800
1 7,50
224
8
5
5
Source Name Elizabeth City WTP
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Pre rer * Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1102 (26)

t
_�
A`
-°� AGMAN
Facility Elizabeth City WTP
Sampling Date 2/11/2014
% Solids 16.7
1 Mineralization Rate 0.4
-- Gallons per DT 1,435.98
pH 10.2
FIELD LOADING ESTIMATES
Sodium Absorpotion 0.24 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION NUTRIENT APPLICATION
TKN (mg/Kg) 343 lbs./1,000 gal 0.48
Ammonia Nitrogen (mg/Kg) .18.61 lbs./1,000 gal 0.03
Nitrate -Nitrite (mg/Kg) 3.92 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 143 lbs./1,000 gal 0.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 152 lbs./1,000 gal 0.21
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
Potassium lbs./1,000 gal 0.20
Phosphorus lbs./1,000 gal 0.69
Calcium lbs./1,000 gal 449.57
Magnesium lbs./1,000 gal 17.13
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
%
Class A Ceiling,
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
1,500
4,30,0
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.01
r-
300
840
Lead (mg/Kg)
2.50
Lead lbs./1,000 gal
0.00
17
57
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.01
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.01
2,800
7,500
Zinc (mg/Kg)
24.00
Zinc lbs./1,000 gal
0.03
RESIDUAL NITROGEN CALCULATION
1st Year
2nd Year
'3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
TKN
PAN PAN
Nitrogen
TIEN
PAN PAN
Nitrogen
(mg/kg) (lbs/D1)
(mg/Kg)
(mg/kg) (lbs/DT)
(mg/Kg)
343
143 0.29
200
343
152 0.30
191
200
40 0.08
160
191
38 0.08
153
160
16 0.03
144
153
15 0.03
137
144
7 0.01
137
137
7 0.01
130
137
3 0.01
133
130
3 0.01
127
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
'Total 210 0.42
Total 216 ' 0.43

_ - - Waitevia-ter ID. 10-
`P.O. BOX 7085, 114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27835-7085 FAX [phone] -
ID#: 165
r ELIZABETH CITY (WATER PLANT)
MS. AVA GOODWIN
ATTN: WATER TREATMENT PLANT DATE COLLECTED: 02/11/14
P.O. BOX 347 DATE REPORTED 03/28/14
A
ELIZABETH CITY ,NC 27907-0404
J
- REVIEWED BY:
Water Plant Analysis Method
PARAMETERS Sludge Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
r
' Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Total Solids,
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Chloride (dry wt. basis), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
( Sulfate (dry weight), mg/kg
Molybdenum (dry wt. basis), mg/kg
7994
03/05/14 LFJ
EPA200.7
<2.5
03/24/14 MEL
3113B-04
322784
03/05/14 LFJ
EPA200.7
<0.5
03/19/14 MEL
311313-04
<5.0
03/05/14. LFJ
EPA200.7
<2.5
03/05/14 LFJ
EPA200.7
< 2.5
03/21/14 MEL
3113B-04
12298
03/05/14 LFJ
EPA200.7
<0.02
02/26/14 ADD
245.1 113-94
<5.0
03/07/14 LFJ
EPA200.7
145
03/05/14 LFJ
EPA200.7
<5:0
03/25/14 MEL
311313-04
< 1250
03/07/14 ADD
311113-99
24
02/21/14 ADD
3111B-99
16.7
02/17/14 MDD
2540G-97
343
02/20/14 ANO
351.2 112-93
18.61
02/18/14 ALB
350.1 R2-93
496
02/20/14 ALB
365.4 -74
199
02/17/14 CMC
4500CLB-97
<3.92
02/19/14 ANO
353.2 R2-93
5621
02/14/14 TRB '
4500S02E97
<5.0
03/05/14 LFJ
EPA200.7

Environment 1, Inc.
P.O. Box 70&5 114 Oakmont Dr.
Greenville, NC27858
CHAIN OF CUSTODY RECORD
Pagc I o1' I
Phonc [phone] • Fax [phone]
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
pH CHECK (LAB)
CLIENT: 165 Week: C
Uv
ELIZABETII CITY (WATER PLANT)
CONTAINER TYPE,
MS. AVA GOODWIN
NONE_
j
P
P
P
P
P
P
P_
P,
*1 {{L
ATTN: WATER 'TREATMENT PLANT
P.O. BOX 347
I
A
A
A
A
A
A
A
A
CHEMICALPRESERVATION
ELIZABETII CITY NC 27907
E oF-
A-NONE D-NAOH
(252) 335-21'I6
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Cr
CrL
B- HNO, E- HCL
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COLLECTION
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a
SAMPLELOCATION
DATE
TIME
r Plan Sludge,
Water Plant c
s
e
CLASSIFICATION:
WASTEWATER (NPDES)
'DRINKING WATER
DWQ/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING
r
/SH,I�MENT/DELIVERY
�J N
SAMPLES COLLECTED BY:
(Please Print)
C • Law
SAMPLES RECEIVED IN LAB AT (9 °C
RELINQUIS E BY SIG.) (SAMPLER)
DATEMME
RECE VED BY ICE.)
DATEMME
COMMENTS:
'ell
V111,q 11. A
RELINQUISHED BY (SIG.)
DATEMME
REC D BY
DATEMME
N
Z
q
RELINQUISHED BY (SIG.)
DATEMME
RECEIVED B (Sl
A EUIME
PLEASE READ Instructions for completing this farm on the reverse side. Sampler must place a " C" for composite sample or a "G" for No- 267693
- ....r f_`. t, nn... nln ... 31... 1.I,...1.....1....... [....

}
_ R
goAGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 4/22/2014
% Solids 14.84
Mineralization Rate 0.4
_- Gallons per DT 1,615.96
PH 10.58
Sodium Absorpotion 0.79 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
NUTRIENT APPLICATION
TKN (mg/Kg) 524 lbs./1,000 gal 0.65
Potassium lbs./1,000 gal
0.31
- Ammonia Nitrogen (mg/Kg) 188.00 lbs./1,000 gal 0.23
Phosphorus lbs./1,000 gal
1.03
Nitrate -Nitrite (mg/Kg) 4.79 lbs./1,000 gal 0.01
Calcium lbs./1,000 gal
381.89
PLANT AVAILABLE NITROGEN SURFACE APPLIED
Magnesium lbs./1,000 gal
14.97
PAN (mg/Kg) 233 lbs./1,000 gal 0.29
Manganese lbs./1,000 gal
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
Sulfur lbs./1,000 gal
PAN (mg/Kg) 327 lbs./1,000 gal 0.40
x
Molybdenum lbs./1,000 gal
0.01
Volatization Rate= 0.5 Surface Application
1.0 Inj ection/Incorporation
EPA METAL LIMITS
HEAVY METAL CONCENTRATION- HEAVY METAL LOADING
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
2.50
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.60
Selenium lbs./1;000 gal
0.01
Zinc (mg/Kg)
8.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
1st Year
2nd Year
3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
. Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
(mg/Kg)
TEN
(mg/kg) (lbs/DT)
(mg/Kg)
524
233 0A7
291
524
327 0.65
197
291
58 0.12
233
197
39. 0.08
157
233
23 0.05
209
157
16 0.03
142
209
10 0.02
199
142
7 0.01
135
199
5 0.01
194
135
3 0.01
131
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN(mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 330 0.66 Total 393 0.79

I'I z F,t `�-5% "I, (I...at�('rll •I {II' _I I+
` IMF I i-I '-� I.J u •ti�f'�i :� 1 ! I.' I. i }u1 I i 4 '.. LJ UP4T [..✓J J
c�
ID#: 165
EsLIZABETH CITY (WATER PLANT)
EMAIL RESULTS AND COC ONLXIII
DATE COLLECTED: 04/22/14
DATE REPORTED : 05/19/14
REVIEWED BX:
SVater Plant
Analysis
Dlethod
PARAA4ETERS
Sludge
Date Analyst
Code
Aluminum, (dry wt. basis), nrg/kg
8111
05/06/14 LFJ
EPA200.7
Arsenic (dry wt. basis), ling/kg
<2.5
05/07/14 i\'IEL
3113B-04
Calcium (dry wt. basis), rug/kg
308562
05/06/14 LFJ
EPA200.7
r Cadmium (dry wt. basis), mg/kg
<0.5
05/15/14 ME1,
3113B-04
_.. Copper (dry wt. basis), nrg/kg
<5.0
05/06/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
<2.5
05/06/14 LFJ
EPA200.7
Lead (dry weight basis), nrg/kg
<2.5
05/06/14 MEL
3113B-04
Maguesimn (dry wt. basis), mg/kg
12098
05/06/14 LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
<0.02
05/08/14 AITM
245.1 R3-94
Nickel (dry wt. basis), nrg/kg
<5.0
05/06/14 LFJ
EPA200.7
Potassium (dry wt. basis), rug/kg
<250
05/06/14 LFJ
EPA200.7
Selenium (dry wt. basis), mgAkg
<5.0
05/14/14 \•IEL
3113B-04
Sodium {ciry wt. basis), mg/kg
4250
05/06/14 INITiAI
3111B-99
Zure (dry wt. basis), mg/kg
8
05/07/14 IITII
3111B-99
Total Solids, %
14.84
04/25/14 CMC
2540G-97
TI NI (dry wt.), nrg/kg
524
04/28/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry )vt.),nng/kg
188
04/29/14 ALB
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
830
04/28/14 ALB
365.4 -74
- Chloride (dry wt. basis), nrg/kg
398
04/28/14 LTV
4500CLB-97
Nitrate -Nitrite (dry wt.), mg/kg
4.79
04/25/14 ANO
353.2 R2-93
Sulfate (dry weight), rng/kg
5747
04/29/14 TRB
4500SO2E97
=. Alolybdenum (dry wt. basis), mg/kg
y_
<5.0
05/06/14 LFJ
EPA200.7
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ELIZABETH CITY (WATER PLANT)
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P.O. BOX 347 A A A A [A A
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Water Plant Sludge
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FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 8/25/2014
%Solids 19.27
Mineralization Rate 0.4
Gallons per DT 1,244.46
pH 9.7
Sodium Absorpotion 0.26 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 284 lbs./1,000 gal 0.46
Ammonia Nitrogen (mg/Kg) 46.75 lbs./1,000 gal 0.08
Nitrate -Nitrite (mg/Kg) 3.82 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 122 lbs./1,000 gal 0.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 145 lbs./1,000 gal 0.23
Volatization Rate= 0.5 Surface Application
1.0 Injection / Incorporation
EPA METAL LIMITS
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.40
Phosphorus lbs./1,000 gal 0.67
Calcium lbs./1,000 gal 517.50
'Magnesium lbs./1,000 gal 21.00
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.01
Lead (mg/Kg)
2.50
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN.
(mg/kg) (lbs/DT)
(mg/Kg)
TEN
(lbs/DT)
(mg/Kg)
284
122 0.24
162
284
145 0.29
139
162
32 0.06
130
139
28 0.06
ill
130
13 0.03
117
ill
11 0.02
100
117
6 0.01
ill
100
5 0.01
95
ill
3 0.01
108
95
2 0.00
92
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8).
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 176 0.35
Total 192 0.38

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ID##: 165
ELIZABETH CITY (WATER PLANT)
EMAIL RESULTS AND COC ONLY111 -
DATE COLLECTED: 08/25/14
DATE REPORTED : 10/03/14
REVIEWED BY:
Water Plant Analysis Method
PARANIETERS
Sludge
Date Analyst
Code
Aluminum, (dry wt. basis), uig/kg
7479
09/02/14
LFJ
EPA200.7
Arsenic (dry art. basis), mg/kg
<2.5
09/03/14
MEL
3113E-04
' Calcium (dry wt. basis), ing/kg
322005
09/02/14
LFJ
EPA200.7
`-, Cadmium (dry wt. basis), ncg/kg
<0.5
09/09/14
MEL
3113B-04
Copper (city wt, basis), ing/kg
<5.0
09/02114
LFJ
EPA200.7
Chromium, T.(dry wt, basis),mg/kg
<5.0
09/02/14
LFJ
EPA200.7
Lead (dry weight basis), mg/kg
-<2.5
09/11/14
MEL
3113E-04
Magnesium (dry wt, basis), mg/kg
13067
09/02/14
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
<0,02
09/10/14
NITM
245.1 113-94
Nickel (dry wt. basis), mg/kg
<5.0
09/02/14
LFJ
EPA200.7
Potassium (dry wt, basis), mg/kg
<250
09/02/14
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
09/05/14
NIEL
311313-04
Sodium (dry wt. basis), mg/kg
<1250
09/04/14
MT\y
311113-99'
Zuic (dry wt. basis), mg/kg
<5.0
09/11/14
MTM
311113-99
Total Solids, %
19.27
08/26/14
CMC
2540G-97
TKN (dry wt.), mg/kg
284
09/04/14
ANO
351.2 R2-93
' Ammonia Nitrogen (dry wt.),mg/kg
46.75
09/04/14
ANO
350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg
419
09/03/14
ALB
365.4-74
Chloride (dry wt. basis), mg/kg
301
09/02/14
LW
4500CLB-97
Nitrate -Nitrite (dry wt.), mg/kg
<3.82
09/03/14
ANO
353.2 R2-93
Sulfate (dry weight), mg/kg
5629
09/09/14
TRB
4500902E97
Molybdenum (dry- wt. basis), mg/kg
<5.0
09/02/14
LFJ
EPA200.7

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165 Week: 31 D
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ELIZABETH CITY (WATER PLANT) NC*i-N' p P 11 P P p P p
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EMAIL RESULTS AND COC ONLYM
[phone]
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Water Plant Sludge
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AV MAN
Facility Elizabeth City WTP
Sampling Date 10/27/2014
% Solids 14
Mineralization Rate 0.4
Gallons per DT 1,712.02
pH 10.4
FIELD LOADING ESTIMATES
Sodium Absorpotion 0.22 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 411 lbs./1,000 gal 0.48
Ammonia Nitrogen (mg/Kg) •8.93 lbs./1,000 gal 0.01
Nitrate -Nitrite (mg/Kg) 3.97 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 169 lbs./1,000 gal 0.20
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 174 lbs./1,000 gal 0.20
Volatization Rate= 0.5 Surface Application
1.0 Injection/Incorporation
EPA METAL LIMITS
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.15
Phosphorus lbs./1,000 gal 0.61
Calcium lbs./1,000 gal 375.41
Magnesium lbs./1,000 gal 17.45
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
HEAVY METAL CONCENTRATION
HEAVY METAL LOADING
41
75
Arsenic (mg/Kg)
2.50
Arsenic lbs./1,000 gal
0.00
39
85
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
1,500
4,300
Copper (mg/Kg)
5.00
Copper lbs./1,000 gal
0.01
300
840
Lead (mg/Kg)
2.50
Lead lbs./1,000 gal
0.00
17
57
Mercury (mg/Kg)
0.01
Mercury lbs./1,000 gal
0.00
420
420
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.01
100
100
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.01
2,800
7,500
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
1st Year
2nd Year
3rd Year
4th Year
5th Year
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TEN
(mg/kg) (lbs/DT)
(mg/Kg)
T
(mg/kg) (lbs/DT)
(mg/Kg)
411
169 0.34
242
411
174 0.35
237
242
48 0.10
193
237
47 0.09
190
193
19 0.04
174
190
19 0.04
171
174
9 0.02
165
171
9 0.02
162
165
4 0.01
161
162
4 0.01
158
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Total 250 0.50
Total 253 0.51

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r - I 35�r'}�7
ELIZABETH CITY (WATER PLANT)
EMAIL RESULTS AND COC ONLY111
PARAMETERS
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt, basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt, basis), mg/kg
Selenium (dry wt. basis), ingtkg
Sodium (dry wt. basis), mg/kg
Zhic (dry wt. basis), ing/kg
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (cry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Chloride (dry wt. basis), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Sulfate (dry weight), mg/kg
Molybdenum (dry wt. basis), mg/kg
Water Plant
Analysis
Method
Sludge
Date Analyst
Code
7395
11/04/14
LFJ
EPA200.7
<2.5
11/21/14
MTM
3113E-04
321524
11/04/14
LFJ
EPA200.7
< 0.5
11/22/14
MTM
3113B-04
<5.0
11/04/14
LFJ
EPA200.7
<2.5
11/04/14
LFJ
EPA200.7
<2.5
11/25/14
AITM
3113B-04
14944
11/04/14
LFJ
EPA200.7
<0.008
10/30/14
AITAI
245.1 113-94
<5.0
11/04/14
LFJ
EPA200.7
127
11/04/14
LFJ
EPA200.7
<5.0
11/17/14
LFJ
311313-04
<1250
11/04/14
LFJ
EPA200.7
<5.0
11/04/14
LFJ
EPA200.7
14,0
10/28/14
KKF
2540G-97
411
11/03/14
AIDS
351.2 R2-93
8.93
10/30/14
ANO
350.1 R2-93
524
11/03/14
ALB
365.4-74
521
11/03/14
LW
4500CLB-97
<3.97
10/31/14
AKS
353.2 R2-93
4917
11/03/14
TRB
4500S02E97
<5.0
11/04/14
LFJ
EPA200.7
ZD#: 165
DATE COLLECTED: 10/27/14
DATE REPORTED : 11/26/14
REVIEWED BY:

1., li%l._
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1
Summit Environmental Technologies, Inc.
Case -Narrative
I_r-I',,"��;�;t
3310ii'imSt.
Cuyahoga Falls, Ohio 44223
WO#: 14042322
:.
TEL: [phone] FAX: [phone]
_.
611'ebsile: hup.-Mminv.settek.can
Date: 4/3012014
CLIENT:
Environment 1, Inc.
Project:
Water Plant Sludge
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 8

I
1, r r r - -, , • r,
I f 'r',
Summit Envirorvnental Technologies, Inc.
WOn:
14042322
/;t
'' I
3310 TYin St.
- -'
.::40i;i: -.. �,•_ _s __n:_� _ _.,, , :
CuyahogaFal/s, Ohio 99223
Date Reported:
4/30/2014
TEL: [phone] FAX: [phone]
Company:
Environment 1, Inc.
N'ebsire: hitp://xninv.settek.coni
Address:
114 Oakmont Dr
'
Greenville NC 27858
Received:
4/24/2014
Project#:
Water Plant Slud
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Water Plant Sludge
001
4/22/2014 TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Barium(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Selenium(Se)
0.50
ND mg1L
Sludge
EPA 6010 C
1
1.0
4/29/2014
WK
Water Plant Sludge
001
4/22/2014 TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
4/29/2014
WK
TCLP Mercury Analysis
(1311/7470)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Water Plant Sludge
001
4/22/2014 TCLP Mercury
0.0020
ND mg/L
Sludge
EPA 7470 A
1
0.20
4/29/2014
ALJ
SVOC
SW-846: 8081-TCLP
Pesticides
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Water Plant Sludge
001
4/22/2014 Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
4/29/2014
JBN
Water Plant Sludge
001
4/22/2014 Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
4/29/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Water Plant Sludge
001
4/22/2014 1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
4/29/2014
' MES
Water Plant Sludge
001
4/22/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
4/2912014
MES
Water Plant Sludge
001
4/22/2014 Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 Tetrachloroethene
0.10
ND mg%L
Sludge
EPA 8260 B
1
0.70
4/29/2014
MES
Water Plant Sludge.
001
4/22/2014 Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
4/29/2014
MES
Water Plant Sludge
001
4/22/2014 MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
4/29/2014
MES
Page 4 of 8

Sununif Environnienfal Technologies, Inc.
WO#: 14042322
I
3310 ff"in St.
,J
Cityahoga Falls, Ohio 44223
Date Reported: 4/30/2014
TEL: [phone] FAX.- [phone]
Company: Environment 1, Inc.
Mehsile: h11P.1Avmv.set1ek.00?2?
Address: H 4 Oakmont Dr
Greenville NC 27858
Received: 4/24/2014
Project#: Water Plant Slud
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Ltnt Result Units
Matrix Method DF RegLvl
Run
Analyst
Water Plant Sludge
001
4/22/2014 1,4-Dichlorobenzene
0.10 ND mg/L
Sludge EPA 8270 C 1 7.5
4/2912014
AKE
Water Plant Sludge
001
4/2212014 2,4,5-Trichlorophenol
0.25 ND mg1L
Sludge EPA 8270 C 1 400
4/29/2014
AKE
Water Plant Sludge
001
4/22/2014 2,4,6-TriGhlorophenol
0.25 ND mg/L
Sludge EPA 8270 C 1 2.0
4/29/2014
AKE
Water Plant Sludge
001
4/22/2014 2,4-Dinitr6toluene
0.10 ND mg/L
Sludge EPA 8270 C 1 0.13
4/29/2014
AKE
Water Plant Sludge
001
4/22/2014 Hexachloro-1,3-
0.10 ND mg1L
Sludge EPA 8270 C 1 0.50
4/29/2014
AKE
butadiene
Water Plant Sludge
001
4/22/2014 Hexachlorobenzene
0.10 ND rng/L
Sludge EPA 8270 C 1 0.13
4/29/2014
AKE
Water Plant Sludge
001
4/22/2014 Hexachloroethane
0.10 ND mg1L
Sludge EPA 8270 C 1 3.0
4129/2014
AKE
Water Plant Sludge
001
4/22/2014 Nitrobenzene
0.10 ND mg/L
Sludge EPA 8270 C 1 2.0
4/29/2014
AKE
Water Plant Sludge
001
4/22/2014 Pentachlorophenol
0.25 ND mg/L
Sludge EPA 8270 C 1 100
4129/2014
AKE
Water Plant Sludge
001
4/22/2014 Pyridine
0.25 ND mg/L
Sludge EPA 8270 C 1 5.0
4/29/2014
AKE
SVOC SW-846: 8321 Herbicides-TCLP
Client 1D#
Lab ID#
Collected Analytd
Rep Lrnt Result Units
Matrix
Method
DF
RegLvI
Run
Analyst
Water Plant Sludge
Water Plant Sludge
001
001
4122/2014 2,4-D
4/22/2014 2,4,5-TP
5.0 ND mg/L
0.50 ND mg/L
Sludge
Sludge
EPA 8321 A
EPA 8321 A
1
1
10
1.0
4/29/2014
4/29/2014
AMZ
AMZ
Page 5 of 8

r
Summit Environmental Technologies. hic.
WO#:
14042322
v 1:4 c
33 10 Win St.
Cuyahoga Falls, 01do 44223
Date Reported:
4/30/2014
TEL: [phone] FAX.- [phone]
Company:
Environment 1, Inc.
Websile: h11P.-1Avww.se1tekC0M
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
4/24/2014
Project#:
Water Plant Slud
Client ID#
Lab ID#
Collected Analyte
Result Units
Matrix
Method
DF
RL Run
Analyst
Water Plant Sludge
001
4/22/2014
Flashpoint (140T)
>200 T
Sludge
EPA 1010
1
4/25/2014
TAH
Water Plant Sludge
001
4/22/2014
Cyanide, Reactive
ND pprn
Sludge
EPA 9014
1
0.50 4/25/2014
TIR
Water Plant Sludge
001
4/22/2014
pH
9.8 s.u.
Sludge
EPA 9045 D
1
4/25/2014
AYS
Water Plant Sludge
001
4/22/2014
Sulfide, Reactive
ND pprn
Sludge
EPA 9034
1
25 4/25/2014
TIR
Page 6 of 8

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Page 8 of 8

Environment 1, Inc.
P.O. Box 7085, 114 Oakmont Dr.
Grecnvilfc; NC 27858
CHAIN OF CUSTODY RECORD
Page I of 1
Phone [phone] • Fax [phone]
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
JCFILORINE
2 GO � \DYti
CLIENT: 165 A Wcek: 18
JU V
pH CHECK (LAB) 1®. 58
P
P
P
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CONTAINERTYPE, P/G
ELIZABETH CITY (WATER PLANT)
NONE
MS. AVA GOODWIN
CHEMICAL PRESERVATION
ATTN: WATER TREATMENT PLANT
P.O. BOX 347
A
A
A
A
A
A
A
ELIZABETH CITY NC 27907
ma_
A -NONE D-NAOH
[phone]
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SAMPLE LOCATION
DATE
TIME
WaterPlant ant Sludge4
1
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CLASSIFICATION:
WASTEWATER (NPDES)
FA DRINKING WATER
DWQ/GW
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING SHIPMENT/DELIVERY
Y N
SAMPLES COLLECTED BY:
(Please Print)
Aga Cc�W�w
SAMPLES RECEIVED IN LAB AT °C
RELINQUISHED BY (SIG.) (SAMPLER)
DATElf[ME
RECEIVED BY (SIG.)
DATEMME
COMMENTS:
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RELINQUISHED BY (SIG.)
DATBTIME
RECEIV BY (SIG.)
r / DATErRME
RELYSHED IG.)
iJ D TE/TIME
RECEIVED BY (S NJ
DATEMME
7 Z' r �'e�
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a "G" for 2 7 5 9 '52
r,roh eamnlo in tho hlne Le ❑hnun fnr nnrh noramotor rommetorl

APPENDIX III
FIELD LOADING SUMMARY FORM
cr_

PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner Lawrence Larabee
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# LL County Pasquotank Crop 1 Wheat, Grain
Field Name 2 SoilSeries Crop 1 Pan 100
Acres Permited 66.56 Soil Abbrevation: Crop 2 Soybeans, Manured, Full Season
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement
Applied % Solids Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization
Mineralization
THIN Ammonia Nitrite
PAN
PAN Crop
10/09/2014 Gallons
203,000 0.50
153.02
0.03 4.23
Elizabeth City WWTP
Dry
0 Surface
1.04
0.50
0.3
36,631
324.00 108.00
0.62
Crop 1
10/10/2014 Gallons
175,000 0.50
153.02
0.02 3.65
Elizabeth City WWTP
Dry
0 Surface
0.90
0.50
0.3
36,631
324.00 108.00
0.53
Crop 1
10/21/2014 Gallons
175,000 0.50
153.02
0.02 3.65
Elizabeth City WW'IP
Dry
0 Surface
0.90
0.50
0.3
36,631
324.00 108.00
0.53
Crop 1
11/04/2014 Gallons.
140,000 14.00
153.02
0.53 81.73
Elizabeth City WTP
Moist
0 Surface
0.56
0.50
0.4
411
8.93 3.97
0.18
Crop 1
11/05/2014 Gallons
140,000 14.00
153.02
0.53 81.73
Elizabeth City WTP
Moist
0 Surface
0.56
0.50
0.4
411
8.93 3.97
0.18 -
Crop 1
Total Volume Applied
833,000 .
Total DryTons 174.99
Sum Total P
3.96
Total
2.04
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN-
PAN
Current Year
0.006 0.001
0.045
0.008
0.009 0.000
0.011
0.012
0.011
0.103
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.055 0.029
2.045
0.037
0.308 0.001
0.102
0.109
0.089
4.412
Cumulative Total
0.061 0.031
2.090
0.045
0.317 0.001
0.114
0.121
0.101
4.515
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/� *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
Qom, aerobically digested -0.3, raw sludge -0.4
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
****C.P.L.R.: Cumulative Pollutant Loading Rate
2-17-2015
Signature of Land Applier Date

1
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0002883 Site# WB County Pasquotank Crop 1 Wheat, Grain
Facility Name City of Elizabeth City Field Name 1 SoilSeries Crop 1 Pan 100
LandOwner W.B. Bateman Acres Permited 155.84 Soil Abbrevation: Crop 2 Soybeans, Manured, Full Season
Operator Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids Used DT/Ac. Tons
Source
'Condition Precip
Method
P
Volatilization
Mineralization
TKN Ammonia Nitrite
PAN
PAN Crop
01/14/2014 Gallons
224,000 16.70
155.84
1.00 155.99
Elizabeth City WTP
Moist
0 Surface
0.99
0.50
0.4
343
18.61
3.92
0.29
Crop 1
01/21/2014 Gallons
231,000 2.88
155.84
0.18 27.74
Elizabeth City WWTP
Moist
0 Surface
1.35
0.50
0.3
16,042
468.00
4439
1.76
Crop 1
01/27/2014 Gallons
203,000 2.88
155.84
0.16 24.38
Elizabeth City WWTP
Moist
0 Surface
1.18
0.50
0.3
16,042
468.00
44.39
1.55
Crop 1
02/25/2014 Gallons
28,000 16.70
155.84
0.13 19.50
Elizabeth City WTP
Moist
0 Surface
0.12
0.50
0.4
343
18.61
3.92
0.04
Crop 1
02/26/2014 Gallons
259,000 16.70
155.84
1.16 180.37
Elizabeth City WTP
Moist
0 Surface
1.15
0.50
0.4
343
18.61
3.92
0.33
Crop 1
02/27/2014 Gallons
133,000 16.70
155.84
0.59 92.62
Elizabeth City WTP
Moist
0 Surface
0.59
0.50
0.4
343
18.61
3.92
0.17
Crop 1
04/24/2014 Gallons
175,000 14.84
155.84
0.69 108.29
Elizabeth City WTP
Moist
0 Surface
1.15
0.50
0.4
524
188.00
4.79
0.32
Crop 1
06/01/2014 Gallons
252,000 2.95
155.84
0.20 31.60
Elizabeth City WWTP
Dry
0 Surface
1.55
0.50.
0.3
26,672
356.00
67.80
3.24 Crop 2.
Total Volume Applied
1,505,000
Total Dry Tons 639.89
Sum Total P
8.09
Total
4.46
3.24 Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.029 0.006
0.290
0.045
0.047 0.001
0.052
0.056
0.052
0.939
Lime (T/Ac.) Date
(lbs./Ac.)
(lbs./Ac.)
Prior Year
0.235 0.109
15.472
0.263
1.416 0.004
0.442
2.109
0.205
17.815
Cumulative Total
0.264 0.115
15.761
0.308
1.463 0.005
0.494
2.165
0.257
18.754
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/y *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner W.B. Bateman
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# WB County Pasquotank Crop 1 Wheat, Grain
Field Name 2 SoilSeries Crop 1 Pan 100
Acres Permited 153.02 Soil Abbrevation: Crop 2 Soybeans, Manured, Full Season
Crop 2 Pan 50 -
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement
Applied
% Solids
Used DT/Ac. Tons
Source
Condition
Precip
Method
P
Volatilization Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
02/20/2014
Gallons
112,000
2.88
153.02
0.09
13.45
Elizabeth City WWTP
Moist
0
Surface
0.66
0.50
0.3
16,042
468.00
44.39
0.87
Crop 1
02/21/2014
Gallons
245,000
2.88
153.02
0.19
29.42
Elizabeth City WWTP
Moist
0
Surface
1.45
0.50
0.3
16,042
468.00
44.39
1.90
Crop 1
02/24/2014
Gallons
161,000
2.88
153.02
0.13
19.34
Elizabeth City WWTP
Moist
0
Surface
0.96
0.50
0.3
16,042
468.00
44.39
1.25
Crop 1
02/27/2014
Gallons
280,000
2.88
153.02
0.22
33.63
Elizabeth City WWTP
Moist
0
Surface
1.66
0.50
0.3
16,042
468.00
44.39
2.18
Crop 1
Total Volume Applied
798,000
Total Dry Tons 95.84
Sum Total P 4.74
Total 6.20
Total
Reported in Gallons
Arsenic Cadmium
Copper Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.007
0.002
0.256 0.023
0.028
0.000
0.006
0.011
0.006
0.825
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.082
0.037
3.776 0.236
0.491
0.002
0.078
0.184
0.137
9.364
Cumulative Total
0.089
0.039
4.032 0.259
0.518
0.003
0.085
0.195
0.143
10.190
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1; anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Appher Date

PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner W.B. Bateman
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
, Site# WB County Pasquotank Crop 1 Corn, Grain
Field Name 3 SoilSeries Crop 1 Pan 160
Acres Permited 110.39 Soil Abbrevation: Crop 2 Wheat, Grain
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate-
Crop 1
Crop 2
Date Measurement Applied
% Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method
P
Volatilization Mineralization
TIiN
Ammonia Nitrite
PAN
PAN
Crop
03/01/2014
Gallons
245,000
2.88
110.39
0.27
29.42
Elizabeth City WWTP
Moist
0
Surface
2.02
0.50
0.3
16,042
468.00
44.39
2.64
Crop 1
03/02/2014
Gallons
119,000
2.88
110.39
0.13
14.29
Elizabeth City WWTP
Moist
0
Surface
0.98
0.50
0.3
16,042
468.00
44.39
1.28
Crop 1
03/11/2014
Gallons
126,000
2.88
110.39
0.14
15.13
Elizabeth City WWTP
Moist
0
Surface
1.04
0.50
0.3
16,042
468.00
44.39
1.36
Crop 1
03/12/2014
Gallons
119,000
2.88
110.39
0.13
14.29
Elizabeth City WWTP
Moist
0
Surface
0.98
0.50
0.3
16,042
468.00
44.39
1.28
Crop 1
03/24/2014
Gallons
112,000
2.88
110.39
0.12
13.45
Elizabeth City WWTP
Moist
0
Surface
0.92
0.50
0.3
16,042
468.00
44.39
1.21
Crop 1
03/25/2014
Gallons
112,000
2.88
110.39
0.12
13.45
Elizabeth City WWTP
Moist
0
Surface
0.92
0.50
0.3
16,042
468.00
44.39
1.21
Crop 1
08/20/2014
Gallons
175,000
19.27
110.39
1.27
140.62
Elizabeth City WTI?
Dry
0
Surface
1.07
0.50
0.4
284
46.75
3.82
0.31
Crop 2
08/21/2014
Gallons
175,000
19.27
110.39
1.27
140.62
Elizabeth City WTP
Dry
0
Surface
1.07
0.50
0.4
284
46.75
3.82
0.31
Crop 2
08/25/2014
Gallons
175,000
19.27
110.39
1.27
140.62
Elizabeth City WTI?
Dry
0
Surface
1.07
0.50
0.4
284
46.75
3.82
0.31
Crop 2
08/26/2014
Gallons
175,000
19.27
110.39
1.27
140.62
Elizabeth City WTP
Dry
0
Surface
1.07
0.50
0.4
284
46.75
3.82
0.31
Crop 2
09/11/2014
Gallons
175,000
1.41
110.39
0.09
10.29
Elizabeth City WWTP
Dry
0
Surface
1.24
0.50
0.3
39,578
383.00
28.79
2.23
Crop 2
09/12/2014
Gallons
112,000
1.41
110.39
0.06
6.59
Elizabeth City WWTP
Dry
0
Surface
0.80
0.50
0.3
39,578
383.00
28.79
1.43
Crop 2
09/19/2014
Gallons
147,000
1.41
110.39
0.08
8.64
Elizabeth City WWTP
Dry
0
Surface
1.04
0.50
0.3
39,578
383.00
29.79
1.88
Crop 2
09/23/2014
Gallons
42,000
1.41
110.39
0.02
2.47
Elizabeth City WWTP
Dry
0
Surface
0.30
0.50
0.3
39,578
383.00
28.79
0.54
Crop 2
10/07/2014
Gallons
245,000
0.50
110.39
0.05
5.11
Elizabeth City WWTP
Dry
0
Surface
1.75
0.50
0.3
36,631
324.00
108.00
1.03
Crop 2
10/25/2014
Gallons
210,000'
0.50
110.39
0.04
4.38
Elizabeth City WWTP
Dry
0
Surface
1.50
0.50
0.3
36,631
324.00
108.00
0.89
Crop 2
10/26/2014
Gallons
140,000
0.50
110.39
0.03
2.92
Elizabeth City WWTP
Dry
0
Surface
1.00
0.50
0.3
36,631
324.00
108.00
0.59
Crop 2
10/27/2014
Gallons
140,000
0.50
110.39
0.03
2.92
Elizabeth City WWTP
Dry
0
Surface
1.00
0.50
0.3
36,631
324.00
108.00
0.59
Crop 2
Total Volume Applied
2,744,000
Total Dry Tons 705.84
Sum Total P 19.74
Total 8.97
10.42 Total
Reported in Gallons
Arsenic
- Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2 ,
Current Year
0.039
0.009
0.646
0.100
0.084
0.001
0.064
0.074
0.064
1.846
PAN
(lbs./Ac.)
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
2.112
0.088
6.485
0.314
1.007
0.023
0.328
0.273
0.208
14.446
Cumulative Total
2,151
0.097
7.131
0.414
1.091
0.024
0.392
0.347
0.272
16.292
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/f *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0. 1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.- Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0002883 Site# WB County Pasquotank Crop 1 Corn, Grain
Facility Name City of Elizabeth City Field Name 4 SoilSeries Crop 1 Pan 160
LandOwner W.B. Bateman Acres Permited 79.19 Soil Abbrevation: Crop 2 Wheat, Grain
Operator Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date Measurement
Applied
% Solids Used DT/Ac. Tons
Source
Condition Precip
Method
P Volatilization Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
04/01/2014 Gallons
126,000
2.95 79.19 0.20
15.50
Elizabeth City WWTP
Moist 0
Surface
1.53 0.50 0.3
26,672
356.00 67.80
3.19
Crop 1
04/04/2014 Gallons
175,000
2.95 79.19 0.27
21.53
Elizabeth City WWTP
Moist 0
Surface
2.12 0.50 0.3
26,672
356.00 67.80
4.43
Crop 1
04/23/2014 Gallons
231,000
2.95 79.19 0.36
28.42
Elizabeth City WWTP
Moist 0
Surface
2.80 , 0.50 0.3
26,672
356.00 67.80
5.84
Crop 1
Total Volume Applied
R
532,000
Total Dry Tons
65.44
Sum Total P
6.44
Total
13.46
Total
eporte to a ons
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Crop 1
Crop 2
Current Year
0.010
0.003
0.441
0.038
0.036
0.001
0.008
0.013
0.008
1.223
'PAN
(lbs./Ac.)
PAN
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.116
0.084
6.260
0.311
0.870
0.013
0.235
0.251
0.179
13.845
Cumulative Total
0.125
0.087
6.701
0.349
0.906
0.014
0.243
0.264
0.187
15.068
Permitted CPLR
36
34
1338
267
15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface_, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
2-17-2015
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner W.B. Bateman
Operator
Site# WB County Pasquotank Crop 1 Wheat, Grain
Field Name 5 SoilSeries Crop 1 Pan 100
Acres Permited 166.49 Soil Abbrevation: Crop 2 Soybeans, Manured, Full Season
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application
Total
Nitrate- Crop 1
Crop 2
Date
Measurement Applied
% Solids
Used
DT/Ac.
Tons
Source
Condition
Precip
Method
P
Volatilization Mineralization
TKN
Ammonia
Nitrite
PAN
PAN Crop
12/15/2014
Gallons
140,000
0.50
166.49
0.02
2.92
Elizabeth City WWTP
Moist
0
Surface
0.66
0.50
0.3
36,631
324.00
108.00
0.39
Crop 1
12/16/2014
Gallons
140,000
0.50
166.49
0.02
2.92
Elizabeth City WWTP
Moist
0
Surface
0.66
0.50
0.3
36,631
324.00
108.00
0.39
Crop 1
12/17/2014
Gallons
140,000
0.50
166.49
0.02
2.92
Elizabeth City WWTP
Moist
0
Surface
0.66
0.50
0.3
36,631
324.00
108.00
0.39
Crop 1
12/18/2014
Gallons
140,000
0.50
166.49
0.02
2.92
Elizabeth City WWTP
Moist
0
Surface
0.66
0.50
0.3
36,631
324.00
108.00
0.39
Crop 1
12/19/2014
Gallons
140,000
0.50
166.49
0.02
2.92
Elizabeth City WWTP
Moist'
0
Surface
0.66
0.50
0.3
36,631
324.00
108.00
0.39
Crop 1.
Total Volume Applied
700,000
Reported in Gallons
Arsenic Cadmium
Current Year
0.001
0.000
Prior Year
0.122
0.048
Cumulative Total ,
0.122
0.048
Permitted CPLR
36
34
Total Dry Tons 14.60
Copper
Chromium
Lead
0.041
0.003
0.004
4.524
0.299
0.646
4.565
0.302
0.650
1338
267
Mercury Molybdenum
0.000 0.001
0.012 0.256
0.012 0.257
15
Sum Total P 3.31
Nickel
Selenium
Zinc
0.001
0.001
0.107
1.024
0.207
10.821
1.025
0.207
10.928
374
89
2498
Total 1.96 Total
Crop 1 Crop 2
PAN PAN
(Ibs./Ac.) (Ibs./Ac.)
Lime (T/Ac.) Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
1CM **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 R ****C.P.L.• Cumulative Pollutant Loading Rate
Signature of Land Applier Date

PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner W.B. Bateman
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM -
Site# WB County Pasquotank Crop 1 Wheat, Grain
Field Name 6 SoilSeries Crop 1 Pan 100
Acres Permited 144.21 Soil Abbrevation: Crop 2 Corn, Grain
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied % Solids
Used
DT/Ac. Tons
Source
Condition Precip Method
P
Volatilization
Mineralization TIiN Ammonia Nitrite
PAN
PAN Crop
11/03/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WWTT
Moist
0 Surface
0.76
0.50
0.3 36,631
324.00
108.00
0.45
Crop 1
11/06/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WWTP
Moist .
0 Surface
0.76
0.50
0.3 36,631
324.00
108.00
0.45
Crop 1
11/10/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WWTP
Moist
0 Surface
0.76
0.50
0.3 36,631
324.00
108.00
0.45
Crop 1
11/11/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WWTP
Moist
0 Surface
0.76
0.50
0.3 36,631
324.00
108.00
0.45
Crop 1
11/13/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WWTP
Moist
0 Surface
0.76
0.50
0.3 36,631
324.00
108.00
0.45
Crop 1
11/20/2014 Gallons
140,000 0.50
144.21
0.02 2.92
Elizabeth City WW7 P
Moist
0 Surface
0.76
0.50,
0.3 36,631
324.00
108.00
0.45
Crop 1
Total Volume Applied
840,000
Total Dry Tons 17.51
Sum Total P
4.58
Total
2.71
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.001 0.000
0.056
0.004
0.005 0.000
0.001
0.002
0.001
0.149
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.105 0.057
4.022
0.196
0.727 0.013
0.190
0.200
0.161
9.151
Cumulative Total
0.105 0.057
4.078
0.200
0.732 0.013
0.191
0.202
0.162
9.300
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation. *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.K: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

PermitNumber WQ0002883
Facility Name City of Elizabeth City
LandOwner W.B. Bateman
Operator
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Site# WB County Pasquotank Crop 1 Com, Grain
Field Name 7 SoilSeries Crop 1 Pan 160
Acres Permited 166.71 Soil Abbrevation: Crop 2 Wheat, Grain
Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied
% Solids Used
DT/Ac.
Tons
Source
Condition Precip Method
P
Volatilization
Mineralization
TKN Ammonia Nitrite
PAN
PAN Crop
05/11/2014 Gallons
161,000
2.95
166.71
0.12
19.81
Elizabeth City WWI?
Dry
0 Surface
0.93
0.50
0.3
26,672
356.00
67.80
1.93
Crop 1
05/12/2014 Gallons
231,000
2.95
166.71
0.17
28.42
Elizabeth City WWTP
Dry
0 Surface
1.33
0.50
0.3
26,672
356.00
67.80
2.78
Crop 1
05/13/2014 Gallons
217,000
2.95
166.71
0.16
26.69
Elizabeth City WWTP
Dry
0 Surface
1.25
0.50
0.3
26,672
356.00
67.80
2.61
Crop 1
05/14/2014 Gallons
217,000
2.95
166.71
0.16
26.69
Elizabeth City WWTP
Dry
0 Surface
1.25
0.50
0.3
26,672
356.00
67.80
2.61
Crop 1
05/15/2014 Gallons
224,000
2.95
166.71
0.17
27.56
Elizabeth City WWTP
Dry
0 Surface
1.29
0.50
0.3
26,672
356.00
67.80
2.69
Crop 1
05/18/2014 Gallons
210,000
2.95
166.71
0.15
25.83
Elizabeth City WWTP
Dry
0 Surface
1.21
0.50
0.3
26,672
356.00
67.80
2.52
Crop 1
05/19/2014 Gallons
147,000
2.95
166.71
0.11
18.08
Elizabeth City WWTP
Dry
0 Surface
0.85
0.50
0.3
26,672
356.00
67.80
1.77
Crop 1
05/20/2014 Gallons
196,000
2.95
166.71
0.14
24.11
Elizabeth City WWTP
Dry
0 Surface
1.13
0.50
0.3
26,672
356.00
67.80
2.35
Crop 1
05/27/2014 Gallons
140,000
14.84
166.71
0.52
86.64 -
Elizabeth City WTP
Dry
0 Surface
0.86
0.50
0.4
524
188.00
4.79
0.24
Crop 1
05/28/2014 Gallons
140,000
14.84
166.71
0.52
86.64
Elizabeth City WTP
Dry
0 Surface
0.86
0.50
0.4
524
188.00
4.79
0.24
Crop 1
05/29/2014 Gallons
154,000
14.84
166.71
0.57
95.30
Elizabeth City WTP
Dry
0 Surface
0.95
0.50
0.4
524
188.00
4.79
0.27
Crop 1
05/30/2014 Gallons
112,000
14.84
166.71
0.42
69.31
Elizabeth City WTP
Dry
0 Surface
0.69
0.50
0.4
524
188.00
4.79
0.19
Crop 1
05/31/2014 Gallons
84,000
2.95
166.71
0.06
10.33
Elizabeth City WWTP
Dry
0 Surface
0.48
0.50
0.3
26,672
356.00
67.80
1.01
Crop 1 .
Total Volume Applied
2,233,000
Total Dry Tons
545.41
Sum Total P
13.07
Total
21.21
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
PAN
PAN
Current Year
0.025 0.007
0.685
0.067
0.065 0.001
0.033
0.040
0.033
1.875
(lbs./Ac.)
(lbs./Ac.)
Lime (T/Ac.) Date
Prior Year
0.093 0.036
3.427
0.233
0.460 0.013
0.182
0.204
0.165
8.107
Cumulative Total
0.118 0.043
4.112
0.300
0.524 0.015
0.215
0.244
0.197
9.982
Permitted CPLR
36 34
1338
267 15
374
89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
/f *Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R.: Cumulative Pollutant Loading Rate
Signature of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PermitNumber WQ0002883 Site# WB County Pasquotank Crop 1 Wheat, Grain
Facility Name City of Elizabeth City Field Name 8 SoilSeries Crop 1 Pan 100
LandOwner W.B. Bateman Acres Permited 104.42 Soil Abbrevation: Crop 2 Soybeans, Manured, Full Season
Operator Crop 2 Pan 50
Volume
Acres
Dry
Soil
Application Total
Nitrate- Crop 1
Crop 2
Date Measurement Applied "/, Solids
Used
DT/Ac. Tons
Source
Condition Precip
Method P
Volatilization Mineralization
TKN
Ammonia Nitrite
PAN
PAN Crop
07/15/2014 Gallons
161,000 1.41
104.42
0.09 9.47
Elizabeth City WWTP
Dry
0 ction/Incorpora 1.21
1.00
0.3
39,578
383.00
28.79
2.21
Crop 1
07/28/2014 Gallons
98,000 1.41
104.42
0.06 5.76
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.74
1.00
0.3
39,578
383.00
28.79
1.34
Crop 1
07/29/2014 Gallons
126,000 1.41
104.42
0.07 7.41
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.95
1.00
0.3
39,578
383.00
28.79
1.73
Crop 1
07/30/2014 Gallons
112,000 1.41
104.42
0.06 6.59
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.84
1.00
0.3
39,578
383.00
28.79
1.54
Crop 1
08/11/2014 Gallons
126,000 1.41
104.42
0.07 7.41
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.95
1.00
0.3
39,578
383.00
28.79
1.73
Crop 1
08/12/2014 Gallons
112,000 1.41
104.42
0.06 6.59
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.84
1.00
0.3
39,578
383.00
28.79
1.54
Crop 1
08/13/2014 Gallons
119,000 1.41
104.42
0.07 7.00
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.89
1.00
0.3
39,578
383.00
28.79
1.63
Crop 1
08/14/2014 Gallons
119,000 1.41
104.42
0.07 7.00
Elizabeth City WWTP
Dry
0 ction/Incorpora 0.89
1.00
0.3
39,578
383.00
28.79
1.63
Crop 1
Total Volume Applied
973,000
Total Dry Tons 57.21
Sum Total P 7.31
Total
13.34
Total
Reported in Gallons Arsenic Cadmium
Copper
Chromium
Lead Mercury
Molybdenum
Nickel Selenium
Zinc
Crop 1
Crop 2
Current Year
0.007 0.002
0.348
0.026
0.027 0.001
0.005
0.010 0.005
0.930
(]bs./Ac.)
PAN
PAN
(lbs./Ac.)
Lime (T/Ac.)
Date
Prior Year
0.044 0.013
2.319
0.099
0.299 0.011
0.088
0.095 0.059
4.998
Cumulative Total
0.050 0.015
2.668
0.125
0.327 0.011
0.093
0.105 0.065
5.928
Permitted CPLR
36 34
1338
267 15
374 89
2498
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 aerobically digested -0.3, raw sludge -0.4
2-17-2015 ****C.P.L.R-: Cumulative Pollutant Loading Rate
Signature of Land Appher Date

APPENDIX IV
PATHOGEN AND VECTOR VERIFICATION

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWfP NPDES Number: NCO025011
Monitoring Period: 01 /01 /2014 to 03/31 /2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stabllzation
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
IAnalytical Technique
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 6 (Alk. Stabilization)
❑"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
�4 ale C,,,, . U nr ri rl� AAA
Prepartr Name and Title (type or print)
Signature of Preparer* Date
J. Bryan Smith, Operator
Land Applier Name and Title (if applicable)(type or print)
IA,r—�Z-m
2-17-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
'_Monday, February 2, 2015

Entered By: T.Tucker
Alternative 2 PSRP
Class B Biosolids
Dates: 1/1/2014 thru 1/31/2014
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial
pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Befor
a Corr
Temp
Temp
Corr
pH
After
Corr
Time
pH
Befor
a Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
1/8
1
15.1
12.73
-0.30
12.431744
12.76
15.0
-0.30
12.461944
12.54
15.6
-0.27
12.241945
20000
1/8
2
15.0
12.51
-0.30
12.211744
12.55
15.0
-0.30
12.251945
12.44
15.3
-0.30
12.141945
20000
1/9
1
15.4
12.64
-0.30
12.34
0745
12.48
15.0
-0.30
12.18
0945
12.43
15.2
-0.30
12.13
0945
20000
1/9
2
15.4
12.49
-0.30
12.19
0745
12.42
15.0
-0.30
12.12
0945
12.41
15.1
-0.30
12.11
0945
20000
1/101
1
15.2
12.66
-0.30
12.36
0500
12.62
16.4
-0.27
12.35
0700
1 12.51
16.1
-0.27
12.24
0700
20000
1/10
2
16.0
12.55
-0.27
12.28
0500
12.51
16.2
-0.27
12.24
0700
12.50
16.0
-0.27
12.23
0700
20000
1/11
1
18.2
12.40
-0.18
12.19
0200
12.36
18.3
-0.21
12.15
0400
12.34
18.0
-0.21
12.13
0400
20000
1/11
2
19.1
12.45
-0.15
12.27
0200
12.50
19.0
-0.18
12.32
0400
12.46
19.1
-0.18
12.28
0405
20000
1/11
1
19.9
12.60
-0.15
12.45
1800
12.55
19.3
-0.181
12.37
2000
12.50
19.0
-0.18
12.32
2004
20000
1/11
2
20.1
12.54
-0.15
12.39
1800
12.58
18.8
-0.18
12.40
2000
12.53
18.9
-0.18
12.35
2000
20000
1/12
1
18.4
12.42
-0.21
12.211100
12.41
20.4
-0.15
12.261300
12.37
21.0
-0.15
12.221322
20000
1/12
2
18.9
12.46
-0.18
12.281100
12.38
19.7
-0.15
12.231300
12.261
19.8
-0.15
12.111310
20000
1/13
1
19.2
12.23
-0.18
12.051200
12.17
20.2
-0.15
12.021400
12.32
19.9
-0.15
12.171400
20000
1/13
2
19.4
12.25
-0.18
12.071200
12.19
20.1
-0.15
12.041400
12.18
20.2
-0.15
12.031400
20000
1/14
1
18.3
12.43
-0.21
12.22
0100
12.40
18.0
-0.21
12.19
0300
12.18
20.1
-0.15
12.03
0310
20000
1/14
2
18.51
12.45
-0.18
12.27
0100
12.44
18.0
-0.21
12.23
0300 1
12.36
19.0
-0.18
12.18
0300
20000
1/16
1
15.3
12.46
-0.30
12.16
0330
12.50
15.2
-0.30
12.20
1530 1
12.38
19.0
-0.18
12.20
1530
20000
1/16
2
15.6
12.51
-0.27
12.24
0332
12.541
15.0
-0.30
12.24
1532
12.44
15.5
-0.27
12.17
1530
20000
1/17
1
15.9
12.48
-0.27
12.211304
12.56
15.3
-0.30
12.261504
12.50
15.7
-0.27
12.231500
20000
1/17
2
16.9
12.44
-0.24
12.201305
12.49
15.1
-0.30
12.191505
12.46
15.6
-0.27
12.191500
20000
1/19
1
16.41
12.66
-0.27
12.391530
12.62
15.4
-0.30
12.321730
12.52
15.7
-0.27
12.251730
20000
1/19
2
16.4
12.57
-0.27
12.301530
12.51
15.4
-0.30
12.211730
12.45
15.4
-0.30
12.151730
20000
1/21
1
17.7
12.26
-0.21
12.051400
12.301
16.2
-0.27
12.031600
1
12.26
16.0
-0.27
11.991600
20000
1/211
2
17.9
12.27
-0.21
12.061400
1
12.281
16.0
-0.27
12.011600
12.24
16.0
-0.27
11.971600
20000

1/23
1
-13.91
12.48
-0.33
12.15
0900
112.361
13.8
-0.33
12.03
1100
1 12J71
14.0
-0.33
12.04
1100
20000
1/231
21
14.41
12.61
-0.331
12.28
0900
112.541
14.0
-0.33
12.21
1100
112.431
14.1
-0.331
12.10
1100
20000
Sheet Total
520000
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 1/1/2014 thru 1/31/2014
NPDES Permit # NC0025011
Residuals Permit # WO0002883
Initial
pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Befor
a Corr
Temp
Temp
Corr
pH
After
Corr
Time
pH
Befor
a Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
1/24
1
15.41
12.41
-0.30
12.11
1900
12.47
15.0
-0.30
12.17
2100
12.44
15.1
-0.30
12.14
2100
20000
1/24
2
15.2
12.33
-0.30
12.03
1901
12.42
15.0
-0.30
12.12
2101
12.36
15.2
-0.30
12.06
2100
20000
1/26
1
13.9
12.51
-0.33
12.18
0830
12.501
15.1
-0.301
12.20
1030
12.48
14.8
-0.30
12.18
1030
20000
1/26
2
14.2
12.62
-0.33
12.29
0830
12.61
15.3
-0.30
12.31
1030
12.51
15.0
0.30
12.21
1030
20000
1/28
1
14.4
12.46
-0.33
12.13
1950
12.49
14.0
-0.33
12.16
2150
12.47
14.0
-0.33
12.14
2200
20000
1/28
2
14.31
12.40
-0.33
12.071951
12.43
14.0
-0.33
12.101251
12.37
13.7
-0.33
12.04
2200
20000
1/31
1
15.31
12.42
-0.30
12.121647
12.46
15.0
-0.30
12.161847
12.41
15.1
-0.30
12.11
1900
20000
1/31
2
15.1
12.34
-0.30
12.041648
12.39
15.0
-0.30
12.191848
12.33
15.2
-0.30
12.03
1900
20000

f
Sheet Total 680000

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 2/1/2014 thru 2/28/2014
NPDES Permit N NC0025011
Residuals Permit # WO0002883
Initial PH
pH After 2 Hours
PH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
Stabilization Amount
2/1
1
17.3
12.48
-0.21
12.27
1400
12.39
17.1
-0.21
12.18
1400
12.58
15.2
-0.30
12.28
0400
20000
2/1
2
17.1
12.51
-0.21
12.30
1400
12.44
17.1
-0.21
12.23
1400
12.65
16.1
-0.27
12.40
0400
20000
2/4
1
12.3
12.55
-0.39
12.16
2300
12.50
12.0
-0.39
12.11
0100
12.35
17.1
-0.24
_ 12.11
0100
20000
2/4
2
13.01
12.47
-0.36
12.11
2300
12.45
13.1
-0.36
12.09
O100
12.31
17.0
-0.24
12.07
O100
20000
2/6
1
15.81
12.32
-0.27
12.051330
12.20
16.5
-0.24
12.041530
12.18
16.8
-0.24
11.9415BO
20000
2/6
2
16.1
12.38
-0.27
12.111330
12.321
16.8
-0.24
12.081530
12.28
16.7
-0.24
12.0415BO
20000
2/9
1
15.3
12.44
-0.30
12.14
1801
12.48
15.0
-0.30
12.18
2001
12.40
14.7
-0.30
12.10
2000
20000
2/9
2
15.1
12.34
-0.30
12.04
2802
12.41
15.0
-0.30
12.11
2002
12.40
15.0
-0.30
12.10
2000
20000
2/11
1
18.1
12.60
-0.24
12.39
0100
12.57
17.3
-0.24
12.33
0300
12.55
15.1
-0.30
12.25
0300
20000
2/11
2
17.2
12.58
-0.24
12.34
0100
12.55
17.0
-0.24
12.31
0300
12.52
15.3
-0.30
12.22
0300
20000
2/14
1
14.81
12.61
-0.30
12.31
0745
12.53
16.2
-0.27
12.26
0945
12.49
16.0
-0.27
12.22
9945
20000
2/14
2
15.1
12.45
-0.30
12.15
0745
12.47
16.2
-0.27
12.20
0945
12.43
16.1
-0.27
12.16
0945
20000
2/18
1
15.3
12.56
-0.30
12.28
0230
12.60
15.1
-0.30
12.30
0430
12.52
15.0
-0.30
12.22
0430
20000
2/18
2
15.4
12.40
-0.13
12.10
0230
12.30
151
-0.301
12.05
0430
12.24
15.1
-0.30
11.94
0430
20000
2/19
1
17.7
12.30
-0.21
12.09
2015
12.331
17.6
-0.21
12.12
2215
12.27
17.7
-0.21
12.06
2230
20000
2/19
2
18.1
12.24
-0.21
12.03
2015
12.221
17.7
-0.21
12.01
2215
12.20
17.5
-0.21
11.99
2230
20000
2/21
1
19.3
12.66
-0.18
12.48
0100
12.621
19.0
-0.18
12.44
0300
12.54
19.0
-0.18
12.34
0300
20000
2/21
2
19.21
12.54
-0.18
12.44
O100
12.501
19.1
-0.18
12.32
0300
12.47
19.1
-0.18
12.29
0300
20000
2/21
1
20.11
12.22
-0.15
12.071445
12.271
19.4
-0.18
12.091645
12.25
19.2
-0.18
12.071700
20000
2/21
2
19.81
12.31
-0.15
12.161445
12.381
19.0
-0.18
12.201645
12.35
19.0
-0.18
12.171700
20000
2/22
1
17.4
12.64
-0.24
12.40
0430
12.58
17.2
-0.241
12.34
0630
12.51
17.1
-0.24
12.27
0630
20000
2/22
2
17.3
12.59
-0.24
12.35
0430
12.55
17.0
-0.24
12.31
0630
12.51
17.0
-0.24
12.27
0630
20000
2/22
1
16.0
12.39
-0.27
12.121730
12.42
16.0
-0.27
12.151930
12.36
16.1
-0.27
12.091930
20000
2/22
2
16.1
12.30
-0.27
12.031730
12.32
16.0
-0.27
12.051931
12.28
16.0
-0.27
12.011930
20000
2/241
1
18.3
12.27
0.21
12.061100
12.31
18.1
-0.21
12.101300
12.25
18.0
-0.21
12.041300
20000
2/24
2
18.3
12.35
0.21
12.141100
12.36
18.1
-0.21
12.151300
12.30
18.0
-0.21
12.091300
20000
Sheet Total
520000
u
Alternative 2 PSRP
Class B Biosollds
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit N NC0025011
Residuals Permit 4 WO0002883

Dates: 2/1/2014 thru 2/28/2014
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
Stabilization Amount
2/26
1
20.1
12.40
-0.15
12.251300
12.43
20.2
-0.15
12.281500
12.40
20.0
-0.15
12.251500
20000
2/26
2
20.2
12.38
-0.15
12.231300
12.41
20.1
-0.15
12.261500
12.40
20.1
-0.15
12.251500
20000
2/26
1
17.31
12.52
-0.27
12.25
0200
12.50
17.0
-0.27
12.23
0400
12.48
17.0
-0.27
12.21
0400
20000
2/26
2
17.21
12.51
-0.27
12.24
0200
12.501
17.3
-0.27
12.23
0400
12.471
17.1
-0.27
12.20
0400
20000
2/27
1
19.41
12.32
-0.18
12.14
0000
12.28
19.3
-0.18
12.10
0200
12.46
19.3
-0.18
12.28
0200
20000
2/27
2
19.31
12.29
-0.18
12.11
0000
12.25
19.0
-0.18
12.07
0200
12.24
19.0
-0.18
12.06
0200
20000
2/27
1
14.71
12.42
-0.30
12.12
2245
12.41
15.0
-0.30
12.11
0045
12.40
14.2
-0.33
12.07
0045
20000
2/27
2
14.61
12.39
-0.30
12.09
2245
12.38
15.1
-0.30
12.08
0045
12.37
14.1
-0.33
12.04
0045
20000
Sheet Total
680000

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 3/1/2014 thru 3/31/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial
pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before Corr
Temp
Corr
pH After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH After
Corr
Time
Stabilization
Amount
3/1
1
15.4
12.60
-0.30
12.30
0100
12.59
15.2
-0.30
12.29
0300
12.58
17.3
-0.24
12.34
0300
20000
3/11
2
15.31
12.64
-0.30
12.34
0100
12.61
15.3
-0.30
12.31
0300
12.52
17.0
-0.24
12.28
0300
20000
3/41
1
14.3
12.44
-0.33
12.11
1800
12.49
14.0
-0.33
12.16
2000
1 12.47
14.1
-0.33
12.14
2000
20000
3/4
2
14.1
12.37
-0.33
12.04
1801
12.41
14.0
-0.33
12.08
2001
12.38
14.1
-0.33
12.05
2000
20000
3/7
1
17.3
12.39
-0.24
12.15
2100
12.38
17.4
-0.24
12.14
2300
12.39
16.2
-0.27
12.12
2300
20000
3/7
2
17.3
12.35
-0.24
12.11
2100
12.32
17.1
-0.24
12.08
2300
12.32
16.0
-0.27
12.05
2300
20000
3/14
1
17.2
12.38
-0.24
12.14
0230
12.36
17.0
-0.24
12.12
0430
12.32
17.0
-0.24
12.08
0430
20000
3/14
2
17.31
12.28
-0.24
12.04
0230
12.26
17.1
-0.24
12.02
0430
12.221
17.0
-0.24
11.98
0430
20000
3/14
1
17.4
12.36
-0.24
12.12
1705
12.41
17.0
-0.24
12.17
1905
12.27
17.0
-0.24
12.03
1900
20000
3/14
2
17.1
12.26
-0.24
12.02
1706
12.29
17.0
-0.24
12.05
1906
12.25
17.0
-0.24
12.01
1900
20000
3/15
1
19.8
12.18
-0.15
12.03
1615
12.33
20.1
-0.15
12.18
1815
12.25
20.0
-0.15
12.10
1830
20000
3/15
2
20.5
12.16
-0.12
12.04
1615
12.32
20.1
-0.15
12.17
1815
12.27
20.1
-0.15
12.12
1830
20000
3/18
1
16.3
12.57
-0.27
12.30
0400
12.55
16.1
-0.27
12.28
0600
12.52
17.3
-0.24
12.28
0600
20000
3/181
2
16.21
12.50
-0.27
12.23
0400
12.48
16.0
-0.27
12.21
0600
12.46
17.0
-0.24
12.22
0600
20000
3/20
1
16.61
12.30
-0.24
12.06
0300
12.28
16.7
-0.24
12.04
0500
12.26
16.7
-0.24
12.02
0500
20000
3/20
2
16.11
12.31
-0.27
12.04
0300
12.30
16.9
-0.24
12.06
0500
12.34
17.1
-0.24
12.10
0500
20000
3/22
1
17.31
12.36
-0.24
12.12
1810
12.39
17.0
-0.24
12.15
2010
12.37
17.2
-0.24
12.13
2010
20000
3/22
2
17.11
12.33
-0.24
12.09
1811
12.31
17.0
-0.24
12.07
2011
12.40
17.4
-0.24
12.16
2011
20000
3/24
1
15.51
12.31
-0.27
12.04
1900
12.34
15.6
-0.27
- 12.07
2100
12.251
16.0
-0.271
11.98
2100
20000
3/241
2
15.8
12.30
-0.27
12.03
1900
12.32
15.8
-0.27
12.05
2100
12.32
16.0
-0.27
12.05
2100
20000
3/26
1
16.3
12.27
-0.27
12.00
0400
12.29
16.0
-0.27
12.02
0600
12.30
16.6
-0.27
12.03
0600
20000
3/26
2
16.4
12.28
-0.27
12.01
0400
12.27
16.0
-0.27
12.00
0600
12.27
16.1
-0.27
12.00
0600
20000
3/28
1
19.2
12.44
-0.18
12.26
2300
12.56
18.9
-0.18
12.38
0100
12.49
19.0
-0.18
12.31
0100
20000
3/28
2
19.4
12.42
-0.18
12.24
2300
12.55
19.2
-0.18
12.37
0100
12.50
19.1
-0.18
12.32
0100
20000
3/311
11
19.0
12.57
-0.18
12.39
2100
12.591
18.4
-0.211
12.38
2300 1
12.381
19.8
-0.151
12.23
2300 1
20000
3/311
21
19.1
12.30
-0.18
12.12
2100
12.341
18.8
-0.181
12.16
2300 1
12.221
20.2
-0.151
12.07
2300 1
20000
Sheet Tntn 11
520000

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWTP NPDES Number: NCO025011
Monitoring Period: 04/01/2014 to 06/30/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry• 0 0 Continuous Grab Samples
Weight)
Technique
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 6 (Alk. Stabilization)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Cak oc y' W VV!I ► &UP2f 1/1t u� aJ' Bryan Smith, Operator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
i � 2-17-2015
Signa re of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 2, 2015

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 4/1/2014 thru 4/30/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
Stabilization Amount
4/12
1
23.1
12.24
-0.06
12.181620
12.29
23.0
-0.06
12.231820
12.27
23.0
-0.06
12.211820
20000
4/12
2
23.0
12.20
-0.06
12.141621
12.26
23.0
-0.06
12.201821
12.26
23.0
-0.06
12.201820
20000
4/15
11
23.1
12.31
-0.06
12:251729
12.34
23.0
-0.06
12.281929
12.28
23.1
-0.061
12.221930
20000
4/15
21
23.3
12.26
-0.06
12.201730
12.29
23.0
-0.06
12.231930
12.301
23.1
-0.06
12.241930
20000
4/17
11
17.1
12.28
-0.24
12.04
0500
12.27
17.0
-0.24
12.03
0700
12.23
17.1
-0.24
11.99
0700
20000
4/17
21
17.3
12.31
-0.241
12.07
0500
12.25
17.1
-0.24
12.01
0700
12.22
17.1
-0.24
11.98
0700
20000
4/18
11
17.3
12.36
-0.24
12.12
1840
12.41
17.0
-0.24
12.17
2040
12.38
17.0
-0.24
12.14
2040
20000
4/18
21
17.2
12.29
-0.24
12.05
1841
12.31
17.0
-0.24
12.07
2041
12.30
17.0
-0.24
12.06
2040
1 20000
4/20
11
19.4
12.35
-0.18
12.17
0300
12.33
19.1
-0.181
12.15
0500
12.31
19.0
-0.18
12.13
0500
20000
4/20
21
19.3
12.32
-0.18
12.14
0300
12.30
19.0
-0.18
12.12
0500
12.30
19.0
-0.18
12.22
0500
20000
4/21
11
19.4
12.26
-0.18
12.08
1810
12.31
19.2
-0.18
12.13
2010
12.27
19.2
-0.18
12.09
2010
20000
4/21
21
19.1
12.20
-0.181
12.02
1811
12.24
19.1
-0.18
12.06
2011
12.20
19.2
-0.18
12.02
2010
20000
4/23
11
19.3
12.27
-0.18
12.091200
12.25
19.3
-0.18
12.071400
12.24
19.2
-0.18
12.061400
20000
4/23
21
19.1
12.31
-0.18
12.131200
12.29
19.3
-0.18
12.111400
12.27
19.2
-0.18
12.09140b
20000
4/23
11
20.2
12.24
-0.15
12.09
1817
12.27
20.0
-0.151
12.12
2017
12.251
20.0
-0.15
12.10
2018
20000
4/23
21
20.0
12.20
-0.15
12.05
1818
12.21
20.0
-0.15
12.06
2018
12.19
20.0
-0.15
12.04
2018
20000
4/24
11
19.4
12.39
-0.18
12.211200
12.37
20.3
-0.15
12.221400
12.35
20.0
-0.15
12.201400
20000
4/24
21
20.1
12.23
-0.151
12.081200
12.20
20.7
-0.12
12.081400
12.20
20.5
-0.12
12.081400
20000
4/26
11
20.3
12.27
-0.15
12.27
2330
12.25
20.2
-0.15
12.10
0130
12.20
20.4
-0.15
12.05
0130
20000
4/26
21
20.1
12.24
-0.15
12.14
2330
12.30
20.1
-0.15
12.15
0130
12.28
20.3
-0.15
12.13
0130
20000
4/27
11
21.2
12.23
-0.12
12.091539
12.28
21.0
-0.121
12.161739
12.281
21.0
-0.12
12.161740
20000
4/27
21
21.0
12.16
-0.12
12.041540
12.20
21.0
-0.12
12.081740
12.171
21.0
-0.12
12.051740
20000
4/28
1
17.3
12.50
-0.24
12.26
0100
12.52
17.2
-0.24
12.28
0300
12.50
17.1
-0.24
12.26
0300
20000
4/28
2
17.4
12.61
-0.24
12.37
0100
12.60
17.1
-0.24
12.36
0300
12.57
17.1
-0.24
12.33
0300
20000
4/28
1
18.3
12.46
-0.21
12.25
1922
12.53
18.0
-0.21
12.32
2122
12.48
18.0
-0.21
121.01
2130
1 20000
4/28
2
18.1
12.33
-0.21
12.12
1923
1 12.38
18.0
-0.21
12.17
2123
12.36
18.0
-0.21
12.02
2130
20000
Sheet Total
520000
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization

e � •
Alternative 2 PSRP
Class B Biosolids
Dates: 4/1/2014 thru 4/30/2014
NPDES Permit # NC0025011
Residuals Permit # WO0002883
--
-----------------
---
-------------
-
--------------
-----------------
-----------------
-----------------
.rrrr

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 5/1/2014 thru 5/31/2014
NPDES Permit # NC0025011
Residuals Permit # WO0002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp-
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
5/1
11
21.4
12.38
-0.12
12.26
1830
12.42
21.1
-0.12
12.30
2030
12.40
22.1
-0.12
12.28
2030
2001
5/1
2
21.2
12.31
-0.12
12.19
1831
12.30
21.0
-0.12
12.18
2031
12.28
21.1
-0.12
12.16
2030
2061
5/3
1
20.4
12.22
-0.15
12.07
0200
12.20
20.3
-0.15
12.05
0400
12.17
20.0
-0.15
12.02
0400
2001
5/3
2
20.1
12.23
-0.15
12.08
0200
12.17
20.1
-0.15
12.02
0400
12.15
20.0
-0.15
12.00
0400
2001
5/3
1
23.0
12.35
-0.06
12.291645
12.37
23.2
-0.06
12.311845
12.35
23.1
-0.06
12.291830
2001
5/3
2
23.11
12.36
-0.06
12.30
1645
12.39
' 23.0
-0.06
12.33
1845
12.35
23.1
-0.06
12.29
1830
2001
5/4
1
23.1
12.47
-0.06
12.411700
12.49
23.1
=0.06
12.431900
12.47
23.1
-0.06
12.411900
2001
5/4
2
23.2
12.39
-0.06
12.331701
12.44
23.0
-0.06
12.381901
12.42
23.1
-0.06
12.361900
2001
5/6
1
21.3
12.51
-0.12
12.39
0100
12.50
21.1
-0.12
12.38
0300
12.48
21.0
-0.12
12.36
0300
2001
5/6
21
21.2
12.54
-0.12
12.42
0100
12.56
21.0
-0.12
12.44
0300
12.53
21.0
-0.12
12.41
0300
2001
5/7
1
20.7
12.41
-0.12
12.29
0615
12.40
21.0
-0.12
12.28
0815
12.39
21.1
-0.12
12.27
0830
2001
5/7
2
20.6
12.38
-0.12
12.26
0615
12.32
21.0
-0.12
12.20
0815
12.26
21.1
-0.12
12.14
0830
2001
5/9
1
24.3
12.22
-0.03
12.19
1630
12.27
24.0
-0.03
12.24
1830
1 12.27
24.1
-0.03
12.24
0830
1 2001
5/9
2
24.1
12.17
-0.03
12.14
1631
12.19
24.0
-0.03
12.16
1831
12.16
24.0
-0.03
12.13
0830
2001
5/11
11
24.9
12.18
0.00
12.181730
12.21
23.8
-0.03
12.181930
12.19
24.0
-0.03
12.161930
2001
5/11
2
25.2
12.25
0.00
12.251730
12.26
24.3
-0.03
12.231930
12.24
24.0
-0.03
12.211930
200(
5/12
1
25.4
12.39
0.00
12.39
1900
12.42
25.2
0.00
12.42
2100
12.39
25.1
0.00
12.39
2100
2001
5/12
2
25.3
12.28
0.00
12.28
1901
12.31
25.1
0.00
12.31
2100
12.28
25.1
0.00
12.28
2100
2001
5/13
2
24.1
12.23
-0.03
12.20
2300
12.20
24.0
-0.03
12.17
0100
12.18
24.2
-0.03
12.15
0100
2001
5/13
11
25.3
12.36
0.00
12.36
1813
12.39
25.0
0.00
12.39
2013
12.39
25.2
0.00
12.39
2013
200(
5/14
1
24.3
12.26
-0.03
12.23
0400
12.29
24.2
-0.03
12.26
0400
12.28
24.2
-0.03
12.25
0400
200(
5/15
1
24.3
12.09
-0.03
12.06
0215
12.07
23.8
-0.03
12.04
0415
1 12.06
24.0
-0.03
12.03
0430
200(
5/15
2
24.4
12.19
-0.03
12.16
0215
12.14
24.0
-0.03
12.11
0415
12.14
24.0
-0.031
12.11
0430
200(
5/16
1
23.8
12.10
-0.03
12.07
0630
12.07
24.1
-0.03
12.04
0630
12.04
24.0
-0.03
12.01
0630
200(
5/16
2
23.8
12.14
-0.03
12.11
0630
12.121
23.8
-0.03
12.09
0630
12.09
24.1
-0.031
12.06
0630
200(

5/171 11 23.71 12.11 -0.031 12.08 0800 1 12.071 24.0 -0.031 12.04 0800 1 12.031 24.1 -0.031 12.00 0800
Sheet Total
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 5/1/2014 thru 5/31/2014
200(
5200(
NPDES Permit # NCO025011
Residuals Permit # WO0002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tanis
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
5/17
1
24.3
12.21
-0.03
12.18
1820
12.26
24.0
-0.03
12.23
2020
12.22
24.0
-0.03
12.19
2030
200(
5/17
2
24.1
12.17
-0.03
12.14
1821
12.19
24.0
-0.03
12.16
2021
1 12.13
23.8
-0.03
12.10
2030
200(
5/20
1
21.3
12.18
-0.12
12.06
0845
12.12
22.0
-0.09
12.03
1045
12.08
22.1
-0.09.
11.99
1100
200(
5/20
2
22.5
12.10
-0.06
12.04
0930
12.03
22.3
-0.09
11.94
1130
12.01
22.1
-0.09
11.92
1130
200(
5/20
1
23.6
12.40
-0.03
12.371005
12.32
22.8
-0.06
12.261200
12.28
23.0
-0.06
12.221200
200(
5/21
1
22.1
12.24
-0.09
12.15
0800
12.17
23.2
-0.06
12.11
1000
12.10
23.0
-0.06
12.04
1000
200(
5/21
2
22.5
12.23
-0.06
12.17
0800
12.26
24.2
-0.03
12.23
1000
12.26
24.1
-0.03
12.23
1000
200(
5/22
1
25.4
12.26
0.00
12.261615
12.30
25.1
0.00
12.301815
12.26
24.7
0.00
12.261900
200(
5/22
2
25.3
12.17
0.00
12.171616
12.19
25.0
0.00
12.191816
12.15
24.9
0.00
12.151900
200(
5/25
1
25,3
12.45
0.00
12.45
0000
12.44
25.1
0.00
12.44
0200
12.35
24.1
-0.03
12.32
0200
200(
5/25
2
25.1
12.42
.0.00
12.42
0000
12.40
25.0
0.00
12.40
0200
12.40
24.0
-0.03
12.37
0200
200(
5/27
1
27.1
12.04
0.06
12.101615
12.13
26.11
0.03
12.161815
12.01
25.6
0.03
12.041815
200(
5/27
2
26.7
12.06
0.06
12.121615
12.14
26.31
0.03
12.171815
12.03
26.1
0.03
12.061815
200(
5/30
1
25.1
12.21
0.00
12.211000
12.23
25.1
0.00
12.231200
12.20
25.0
0.00
12.201200
200(
5/30
2
25.0
12.17
0.00
12.121000
12.19
25.1
0.00
12.191200
12.16
25.11
0.00
12.161200
200C

Sheet Total 8200(

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 6/1/2014 thru 6/30/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial
pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
6/2
11
24.3
12.22
-0.03
12.19
1940
12.26
, 24.0
-0.03
12.23
2141
12.17
24.0
-0.03
12.14
2140
200(
6/2
21
24.1
12.16
-0.03
12.13
1941
12.20
24.0
-0.03
12.17
2141
12.10
25.41
0.00
12.10
2141
200(
6/6
11
24.2
12.18
-0.03
12.15
1803
12.24
24.1
-0.03
12.21
2030
11.96
24.0
-0.03
11.93
2030
200(
6/6
2
24.1
12.12
-0.03
12.09
1804
12.13
24.0
-0.03
12.10
2031
11.90
24.0
-0.03
11.87
2031
200C
6/8
1
27.0
11.97
0.06
12.031100
11.95
27.1
0.06
12.011300
11.94
27.01
0.06
12.001300
200(
6/8
2
26.8
12.11
0.06
12.171100
12.201
27.0
0.06
12.261300
12.16
27.11
0.06
12.221300
200(
6/11
1
27.1
12.02
0.06
12.08
0430
12.011
27.0
0.06
12.07
0630
12.01
25.1
0.00
12.01
0630
200(
6/11
2
27.31
12.04
0.06
12.10
0430
12.02
27.1
0.06
12.08
0630
12.06
25.0
0.00
12.06
0630
200(
6/14
1
25.4
12.07
0.00
12.07
0430
12.05
25.2
0.00
12.05
0630
12.02
-25.3
0.00
12.02
0630
200(
6/14
2
25.2
12.03
0.00
12.03
0430
12.00
25.1
0.00
12.00
0630
12.01
25.1
0.00
12.01
0630
200(
6/16
1
26.1
12.11
0.03
12.14
1800
12.16
26.01
0.03
12.19
2000
11.83
25.4
0.00
11.83
2000
200(
6/16
2
26.0
12.06
0.03
12.09
1801
12.08
26.01
0.03
12.11
2001
1 11.74
25.3
0.00
11.74
2001
200(
6/19
1
25.81
12.05
0.03
12.08
2115
12.10
25.3
0.00
12.10
2315
12.06
26.3
0.03
12.09
2315
200(
6/19
2
25.7
12.04
0.03
12.07
2115
12.06
25.0
0.00
12.06
2315
12.02
26.1
0.03
12.05
2315
200(
6/24
1
25.7
12.09
0.03
12.12
0650
12.11
26.0
0.03
12.14
0900
12.04
26.21
0.03
12.07
1730
200(
6/24
2
26.0
12.13
0.03
12.16
0650
12.18
26.0
0.03
12.21
0900
11.97
26.0
0.03
12.00
1731
200(
6/28
1
25.4
12.32
0.00
12.32
0100
12.28
25.11
0.00
12.28
0300
12.25
23.1
-0.06
12.19
0300
200(
6/28
2
25.2
12.25
0.00
12.25
0100
12.23
25.0
0.00
12.23
0300
12.23
23.4
-0.06
12.17
0300
200(

Sheet Total 3600(

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth Citv IXA= NPDES Number: NCO025011
Monitoring Period: 07/01/2014 to 09/30/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stabilization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Technique
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 6 (Allk. Stabilization)
"fV
I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
S 4- f\ Z>1 �c ✓ �1 eY �WHD
Preparer Name and Title (type or print)
Signature of Preparer* Date
J. Bryan Smith, Operator
Land Applier Name and Title (if applicable)(type or print)
-¢
2-17-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 2, 2015
I&

City of Elizabeth City WVVfP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates:. 7/1/2014 thru 7/31/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial
pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
-
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
7/1
1
27.3
12.18
0.06
12.241730
12.22
27.0
0.06
12.281930
12.19
26.7
0.06
12.251930
20000
7/1
2
27.1
12.13
0.06
12.191731
12.14
27.0
0.06
12.201931
12.09
26.9
0.06
12.151930
20000
7/3
1
25.4
12.26
0.00
12.26
0400
12.28
25.1
0.00
12.28
0600
12.26
25.0
0.00
12.26
0600
20000
7/3
2
25.2
12.33
0.00
12.33
0400
12.30
25.3
0.00
12.30
0600
12.26
25.0
0.00
12.26
0600
20000
7/7
1
27.2
12.34
0.06
12.40
0400
12.40
27.1
0.06
12.46
0600
12.38
27.0
0.06
12.44
0600
20000
7/7
2
27.4
12.35
0.06
12.41
0400
12.40
27.0
0.06
12.46
0600
12.40
27.0
0.06
12.46
0600
20000
7/9
2
28.2
12.15
0.09
12.24
1952
12.21
28.2
0.09
12.30
2200
12.17
28.0
0.09
12.26
2200
20000
7/101
1
27.0
12.06
0.06
12.12
0430
12.05
26.8
0.06
12.11
0630
12.05
27.0
0.06
12.11
0630
20000
7/10
2
27.4
12.16
0.06
12.22
0430
12.10
27.5
0.09
12.19
0630
12.10
27.5
0.09
12.19
0630
20000
7/13
1
26.1
12.51
0.03
12.54
0100
12.50
26.2
0.05
12.53
0300
12.51
25.5
0.03
12.54
0300
20000
7/16
1
27.3
12.20
0.06
12.26
0430
12.18
26.1
0.03
12.21
0630
12.22
26.0
0.03
12.25
0630
20000
7/16
2
26.1
12.03
0.03
12.06
0430
12.02
25.0
0.00
12.02
0630
12.02
25.0
0.00
12.02
0630
20000
7/22
1
27.2
12.08
0.06
12.14
1800
12.10
26.6
0.06
12.16
2000
12.15
26.0
0.03
12.18
20.00
20000
7/22
2
26.7
12.02
0.06
12.08
1800
12.03
25.9
0.03
12.06
2000
12.00
26.0
0.03
12.03
2000
20000
7/23
1
26.5
12.04
0.06
12.101400
12.10
26.0
0.03
12.131600
12.07
26.0
0.03
12.101600
20000
7/23
2
26.5
12.06
0.06
12.12
1400
12.08
26.0
_ 0.03
12.11
1600
12.04
26.0
0.03
12.07
1600
20000
7/26
1
24.0
12.17
-0.03
12.14
0645
12.01
25.9
0.03
12.04
0845
12.00
26.0
0.03
12.03
0845
20000
7/26
2
24.0
12.15
-0.03
12.12
0645
11.98
26.4
0.03
12.01
0845
12.00
26.2
0.03
12.03
0845
20000
7/281
2
28.0
12.04
0.09
12.131550
12.13
26.0
0.03
12.161550
12.09
26.1
0.03
12.121600
20000
7/30
1
25.3
12.27
0.00
12.27
0100
12.25
25.1
0.00
12.25
0300
12.28
25.0
0.00
12.28
0300
20000
7/30
2
25.4
12.20
0.00
12.20
0100
12.15
25.0
0.00
12.15
0300
12.25
25.0
0.00
12.25
0300
20000
7/31
1
25.1
12.36
0.00
12.36
0500
12.34
25.0,
0.00
12.34
0700
12.20
25.0
0.00
12.20
0700
20090
7/31
2
25.3
12.30
0.00
12.30
0500
12.32
25.2
0.00
12.32
0700
12.32
25.0
0.00
12.32
0700
20060
Sheet Total
460000

Alternative 2 PSRP
Class B Biosolids
Dates: 8/1/2014
thru 8/31/2014
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
8/1
11
24.3
12.22
-0.03
12.191701
12.29
24.0
-0.03
12.261901
12.27
24.1
-0.03
12.231900
200(
8/1
2
24.1
12.15
-0.031
12.121702
12.19
24.0
-0.03
12.161902
12.14
24.1
-0.03
12.111900
200(
8/2
1
25.0
12.26
0.00
12.261630
12.32
25.0
0.00
12.321830
12.27
25.0
0.00
12.271830
200(
8/2
2
25.0
12.18
0.00
12.181631
12.21
25.0
0.00
12.211831
12.16
25.0
0.00
12.161830
200(
8/4
1
24.5
12.12
0.00
12.12
0530
12.08
24.2
-0.03
12.05
1614
12.03
24.1
-0.03
12.00
1615
200(
8/4
2
24.61
12.24
0.00
12.24
0530
12.06
24.1
-0.03
12.03
1615
12.29
24.0
-0.03
12.06
1615
200(
V 8/7
1
24.7
12.04
0.00
12.04
0500
12.07
24.6
0.00
12.07
0700
12.10
25.01
0.00
12.10
0700
200(
8/7
2
24.8
12.10
0.00
12.10
0500
12.13
24.5
0.00
12.13
0700
12.05
24.8
0.00
12.05
0700
200(
8/9
2
24.5
12.03
-0.03
12.00
1430
11.95
25.4
0.00
11.95
0730
11.92
25.3
0.00
11.92
0730
200(
8/9
11
25.1
12.13
0.00
12.13
1814
12.18
25.0
0.00
12.18
2014
12.15
25.0
0.00
12.15
2014
200(
8/11
1
25.0
12.16
0.00
12.161713
12.19
25.01
0.00
12.191913
12.09
25.1
0.00
12.091915
200(
8/11
2
26.0
12.06
0.03
12.091714
12.08
25.0
0.00
12.081914
12.03
25.1
0.00
12.031915
200(
8/16
1
26.4
12.03
0.03
12.06
0300
12.03
26.1
0.03
12.06
0500
1 12.03
26.11
0.03
12.06
0500
200(
8/16
2
26.2
12.10
0.03
12.13
0300
12.07
26.0
0.03
12.10
0500
12.01
26.0
0.03
12.04
0500
200(
8/21
1
27.41
12.22
0.06
12.281730
12.27
27.0
0.06
12.331930
12.19
26.8
0.06
12.251930
200(
8/21
2
27.1
12.14
0.06
12.201731
12.17
27.01
0.06
12.231931
12.14
26.8
0.06
12.201930
200(
8/22
1
24.5
12.03
0.00
12.031701
12.08
24.5
-0.03
12.031901
12.04
25.0
0.00
12.041900
200(
8/22
2
26.5
11.99
0.03
12.021702
12.02
24.3
0.03
12.051902
12.00
24.0
-0.03
11.971900
200(
8/23
1
24.0
12.30
0.00
12.301730
12.29
24.0
-0.03
12.261930
12.18
24.0
-0.03
12.151930
200(
8/23
2
23.6
12.24
0.00.
12.241730
12.21
24.0
0.00
12.211930
12.17
24.0
-0.03
12.141930
200C
8/24
1
24.0
12.05
0.03
12.081700
12.12
25.0
0.03
12.151900
12.09
25.1
0.00
12.091900
200C
8/24
2
23.5
12.01
0.03
12.041700
12.08
24.5
0.03
12.111900
12.05
24.8
0.00
12.05
1900
200C
8/25
1
26.1
12.13
0.03
12.161630
12.15
26.0
0.03
12.181830
12.11
26.1
0.03
12.141830
200C
8/25
2
26.01
12.04
0.031
12.071631
12.06
26.0
0.03
12.091831
12.02
26.1
0.03
12.051830
200C
8/26
11
2S.81
12.04
0.031
12.071700
12.061
25.11
0.00
12.061900
12.05
25.0
0.00
12.051900
200C

8/261 21 26.2
12.001 0.031 12.03 1700 1 12.071 25.5 0.031 12.10 1900 1 12.051 25.01 0.061 12.05 1900
Sheet Total
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B.Biosolids
Dates: 8/1/2014 thru 8/31/2014
200C
5200C
NPDES Permit # NC0025011
Residuals Permit # WO0002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Date
Tank
Temp
pH Before
Corr
Temp
Corr
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr -
pH
After
Corr
Time
pH
Before
Corr
Temp
Temp
Corr
pH
After
Corr
Time
Stabilization
Amount
8/29
1
25.3
12.25
0.00
12.25
0000
12.27
25.2
0.00
12.27
0200
12.24
25.1
0.00
12.24
0200
200(
8/29
2
26.1
12.281
0.03
12.31
0000
12.26
25.41
0.00
12.26
0200
12.24
25.0
0.00
12.24
0200
200(
8/29
1
25.4
12.10
0.00
12.10
1804
12.13
25.0
0.00
12.13
2004
12.09
25.0
0.00
12.09
2000
1 200(
8/29
2
26.1
12.01
0.03
12.04
1805
12.03
26.1
0.03
12.06
2005
12.01
26.0
0.03
12.04
2000
200(
8/30
1
24.2
12.20
0.00
12.201700
12.06
25.5
0.03
12.091900
12.01
26.0
0.03
12.041900
200(
8/30
2
25.01
12.12
0.03
12.15
1700
12.01
26.1
0.03
, 12.04
1900
11.97
26.0
0.03
12.00
1900
200(
8/31
1
23.8
12.201
0.00
12.201700
12.12
26.11
0.03
12.151900
12.07
26.0
0.03
12.101900
200(
8/31
2
25.1
12.32
0.00
12.321700
12.25
26.2
0.03
12.281900
12.21
26.0
0.03
12.241900
1 200(

Sheet Total 68001

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Mternative 2 PSRP
:lass B Biosolids
)ates: 9/1/2014 thru 9/30/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial pH
pH After 2 Hours
pH After 24 Hours
hate
Tank
Temp
pH Before
Corr
Temp Carr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
Stabilization Amount
9/1
1
27.3
12.16
0.06
12.22
1918
12.21
27.0
0.06
12.27
2018
22.17
27.0
0.06
12.11
2020
20000
9/1
2
27.1
12.08
0.06
12.14
1919
12.11
27.0
0.06
12.17
2019
12.06
26.8
0.06
12.00
2020
20000
9/3
1
25.5
12.10
0.06
12.16
0800
12.02
25.2
0.00
12.02
1000
12.08
25.1
0.00
12.08
1000
20000
9/3
2
26.4
12.16
0.06
12.22
0800
12.06
24.8
0.00
12.06
1000
12.06
25.0
0.00
12.06
1000
20000
9/5
1
26.3
12.05
0.03
12:08
0400
12.05
26.1
0.03
12.08
0600
12.01
26.1
0.031
12.D4
1600
20000
9/5
2
26.2
12.07
0.03
12.10
0400
12.06
26.0
0.03
12.09
0600
12.04
26.0
0.031
12.07
1600
20000
9/7
1
25.3
12.24
0.00
12.24
0000
12.22
25.1
0.00
12.22
0200
12.19
25.1
0.00
12.19
0200
20000
9/7
2
25.4
12.27
0.00
12.27
0000
12.25
25.2
0.00
12.25
0200
12.25
25.1
0.00
12.25
0200
20000
9/9
1
25.3
12.19
0.00
12.19
1910
12.22
25.0
0.00
12.22
2100
12.22
25.0
0.00
12.22
2100
20000
9/9
2
25.1
12.10
0.00
12.10
1911
12.11
25.0
0.00
12.11
2111
12.17
25.0
0.00
12.17
2100
20000
' 9/11
1
26.4
12.27
0.03
12.30
1800
12.33
26.1
0.03
12.36
2000
12.30
26.0
0.03
12.33
2000
20000
9/11
2
27.0
12.19
0.06
12.25
1801
12.24
27.0
0.06
12.30
2001
12.21
27.0
0.06
12.27
2000
20000
9/13
1
27.3
12.22
0.06
12.28
2040
12.27
27.0
0.06
1233
2240
12.24
26.8
0.06
12.30
2240
20000
9/13
2
27.4
12.17
0.06
12.23
2041
12.21
27.0
0.06
12.27
2241
12.17
26.8
0.06
12.23
2240
20000
9/15
1
25.3
12.20
O.GOI
12.20
1820
12.27
25.0
0.00
12.27
2020
12.23
25.0
0.00
12.23
2020
20000
9/15
2
25.1
12.10
0.00
12.10
1821
12.13
25.0
0.00
12.13
2021
12.09
25.0
0.00
12.09
2020
200DO
9/17
1
25.0
12.16
0.00
12.16
1900
12.19
25.0
0.00
12.19
2100
12.15
25.0
0.00
12.15
2100
20000
9/17
2
25.0
12.07
0.00
12.07
1901
12.14
25.0
0.00
12.14
2101
12.14
25.0
0.00
12.14
2100
20000
9/19
1
24.4
12.24
-0.03
12.21
1510
12.28
24.1
-0.031
12.25
1710
12.24
24.0
-0.03
12.21
1715
20000
9/19
2
24.1
12.18
-0.03
12.15
1511
12.20
24.0
-0.03
12.17
1711
12.20
24.0
-0.03
22.17
1715
20000
9/21
1
26.2
12.30
0.03
12.33
1720
12.34
26.0
0.03
12.37
1920
12.28
25.8
0.03
12.31
1925
20000
9121
2
26.0
12.22
0.03
12.25
1721
12.27
26.0
0.03
12.30
1921
12.22
25.9
0.03
12.25
1925
20000
9/22
1
25.4
12.1711
0.00
12.17
1730
12.21
25.1
0.00
12.21
1930
12.17
25.0
0.00
12.17
1930
20000
' 9/22
2
25.2
12.06
0.00
12.06
1731
12.08
25.0
0.00
12.08
1931
12.04
25.0
0.00
12.04
1930
20000
9/23
1
21.0
12.07
0.06
12.13
1730
12.10
27.0
0.06
12.16
1930
12.03
27.0
0.06
12.09
1930
20000
9/231
21
20.9
12.011
0.061
12.07
1730
12.05
27.2
0.06
12.11
1930
12.01
27.0
0.06
12.07
1930
20000
Sheet Total
520000
City of Elizabeth City W WTP
Monitoring Sheet for Lime Stabilization
llternative 2 PSRP
:lass B Biosolids
)ates: 9/1/2014 thru 9/30/2014
NPDES Permit # NCDO25011
Residuals Permit # W00002883
Initial pH
pH After 2 Hours
pH After 24 Hours
Oate
Tank
Temp
pH Before
Corr
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
Stabilization Amount
9/24
1
25.1
12.17
0.00
12.17
1600
12.24
25.0
0.00
12.24
1800
12.20
25.0
0.00
12.20
18M
'20000
9/24
2
25.0
12.09
0.00
12.09
1601
12.14
25.0
0.00
12.14
1801
12.11
25.0
0.00
12.11
1800
200DO
9/27
1
24.3
12.12
-0.03
22.08
1930
12.15
24.0
-0.03
12.12.
2130
12.13
24.1
-0.03
12.10
2130
200DO
9/27
2
24.1
12.05
-0.03
12.02
1931
12.07
24.0
-0.03
12.04
2131
12.07
24.1
-0.03
12.04
2130
200DO
9/28
1
24.01
12.11
-0.03
12.08
1934
1 12.14
24.0
-0.03
12.11
2134
12.111
24.1
-0.03
12.08
2130
20000
9/28
2
24.0
12.07
-0.03
12.04
1935
12.10
24.0
-0.03
12.07
2135
12.101
24.0
-0.03
12.07
2130
20000
9/29
1
23.5
12.14
-0.03
12.11
121S
12.11
23.8
-0.03
12.08
1415
12.07
24.0
-0.03
12.04
1420
20000
9/29
2
23.8
12.17
-0.03
12.14
1216
12.13
24.2
-0.03
12.10
1416
12.09
24.1
-0.03
12.06
1420
20000
' 9/30
1
23.2
12.08
-0.06
12.02
0735
12.10
23.7
-0.03
12.07
0935
12.05
24.0
-0.03
12.02
0935
20000
9/30
2
23.1
12.10
-0.06
12.04
0736
12.08
24.4
-0.03
12.05
0936
12.05
24.8
0.00
12.05
0936
200M
'
Sheet Total
7200DO

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City %VWI P NPDES Number. NCO025011
Monitoring Period: 10/01/2014 to 12/31/2014
Pathogen Reduction (40 CFR 503.32) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
(Analytical Technique
Vector Attraction Reduction Performed (40 CFR 503.33): Alt. 6 (Alk. Stabilization)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
" I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have
not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imtprisonment."r
CAI-ye.►� � J Bryan Smith, Operator
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date
P,�
2-17-2015
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Monday, February 2, 2015

City of Elizabeth City W WTP
Monitoring Sheet for Ume Stabilization
Alternative 2 PSRP
Gass B Biosolids
Dates: 10/1/2014 thru 10/31/2014
NPDES Permit N NCO025011
Residuals Permit N W00002883
Temp
24.1
24.0
21.5
21.9
24.0
24.2
Initial
pH Before
Corr
12.27
12.20
12.19
12.19
12.22
12.19
12.22
12.16
12.19
12.07
12.11
12.09
12.07
12.24
12.23
12.14
12.15
12.19
12.15
12.17
12.06
12.21
12.14
12.23
12.17
Temp
Corr
-0.03
-n ni
-0.09 I12.10
-0.09
-0.03
-0.03
-0.06
-0.06
0.00
-0.03
-0.03
-0.06
0.06
-0.09
.0.09
-0.12
-0.09
0.03
0.03
0.D0
0.D0
-0.03
-0.03
-0.12
-0.12
pH
After
Corr
12.24
12.17
12.10
12.19
12.16
12.16
12.10
12.191600
12.04
12.08
12.03
12.010911
12.15
12.14
12.021245
12.061246
12.22
12.18
12.17
12.06
12.181740
12.111741
12.09
12.05
Time
1910
1911
0735
0736
0430
0430
0200
0200
1940
1941
0910
0200
0200
08D0
0800
1805
1806
2011
2012
pH
Before
Corr
12.31
12.22
Ali
12.20
12.15
12.14
12.16
12.16
12.06
12.08
12.20
12.17
12.13
12.12
12.15
12.11
12.22
12.10
12.26
12.18
12.26
12.18
PH After
Temp
24.0
24.0
22.2
23.1
23.0
23.1
23.1
25.0
24.0
23.4
23.0
23.1
22.0
22.0
22.3
22.4
22.1
22.1
25.0
25.0
24.0
24.0
21.1
21.0
2 Hours
Temp
Corr
-0.03
-0.03
-0.09
-0.06
-0.06
-0.06
0.06
0.00
-0.03
-0.06
-0.06
-0.06
-0.09
-0.09
-0.09
-0.09
0.03
0.03
0.00
0.00
-0.03
-0.03
-0.12
-0.12
pH
After
Corr
12.20
12.19
12.08093610/8
12.14
12.11
12.14
12.09
12.141800
12.16
12.10
12.00
12.021111
12.11
12.08
12.041445
12.031446
12.18
12.14
12.22
12.102
12.231940
12.151941
12.14
12.06
Time
2130
2111
063010/8
0630
0400
0400
2140
2141
1130
0400
0400
1000
1000
2005
2211
2212
pH
Before
Corr
12.30
12.19
12.16
12.18
12.15
12.10
12.07
12.18
12.10
12.05
12.17
12.14
12.15
12.12
12.09
12.07
12.18
12.03
12.19
12.18
12.24
12.15
pH After
Temp
22.7
22.6
22.1
25.0
25.1
25.0
25.1
25.0
24.0
24.1
24.1
24.3
23.7
23.6
23.5
23.5
24.9
24.7
25.1
25.1
25.0
25.1
24 Hours
Temp
Corr
-0.06
-0.06
-0.06
0.00
0.00.
0.00
O.QO
0.00
-0.03
-0.03
-0.03
-0.03
-0.03
-0.03
-0.03
-0.03
0.00
0.00
0.00
0.00
0.00
0.00
pH
After
Corr
12.24
12.13
12.10
12.18
12.15
12.101800
12.07
12.18
12.07
12.021100
12.14
12.11
12.121445
12.091445
12.06
12.04
12.18
12.03
12.191940
12.181940.
12.24
12.15
Time
2110
2110
0630
0400
0400
2140
2140
1100
0400
0400
1000
1000
2000
2000
2211
2211
Stabilization
Amount
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
200�
Date
Tank
10/4
1
10/4
2
10/6
1
10/6
2
1
2
10/10
1
23.0
23.2
10/10
21
10/11
2
25.3
10/15
1
24.0
24.0
22.6
10/15
2
10/17
1
10/17
2
22.9
10/18
1
22.4
22.1
21.1
21.8
24.2
24.0
25.3
25.0
24.4
24.0
21.3
21.1
10/18
2
10/18
1
10/18
2
1
10/20
10/20
2
1
10/28
10/28
2
10/29
1
10/29
2
10/31
1
2
10/31
Sheet Total
520000

City of Elizabeth City W WTP ,
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
Dates: 11/1/2014 thru 11/30/2014
NPDES Permit # NCO025011
Residuals Permit # W00002883
Initial pH
Temp pH Before Temp Corr pH After Time
pH After 2 Hours
pH Before Temp Temp Corr pH After Time
pH After 24 Hours
pH Before Temp Temp Corr pH After Time
Stabilization Amount
Date
Tank
Corr Corr
Corr Corr
Corr Corr
11/1
1
20.3
12.25
-0.15
12.10
1255
12.32
20.0
-0.15
12.17
1455
12.26
20.0
-0.15
12.11
1455
20000
11/11
2
20.3
12.28
-0.15
12.131256
12.37
20.0
-0.15
12.221456
12.29
20.0
-0.15
12.141455
20000
11/2
1
21.2
.12.24
-0.12
12.12
0500
12.22
21.0
-0.12
12.10
0700
12.18
21.1
-0.12
12.16
0700
20000
11/2
2
21.3
12.25
-0.12
12.13
0500
12.23
21.1
-0.12
12.11
0700
12.27
21.1
-0.12
12.15
0700
20000
11/3
1
19.2
12.24
-0.18
12.06
0300
12.22
19.1
-0.18
12.04
0500
12.20
19.4
-0.18
12.02
0500
20000
11/3
2
19.21
12.27
-0.181
12.09
0300
12.251
19.0
-0.18
12.07
0500
12.221
19.1
-0.181
12.04
050D
20000
11/4
1
19.4
12.29
-0.18
12.11
0100
12.27
19.1
-0.18
12.09
0300
12.25
19.1
-0.18
12.07
0300
20000
11/4
2
19.3
12.27
-0.18
12.09
0100
12.23
19.0
-0.18
12.05
0300
12.21
19.0
-0.18
12.03
0300
20000
11/5
1
20.4
12.22
-0.15
12.07
0000
12.18
20.1
-0.15
12.03
0200
12.14
20.0
-0.15
11.99
0200
20000
11/5
2
20.4
12.20
-0.15
12.05
0000
12.17
20.0
-0.15
12.02
0200
12.09
20.0
-0.15
11.94
0200
20000
11/8
1
19.4
12.27
-0.18
12.09
1943
12.31
19.0
-0.18
12.13
2143
12.27
19.0
-0.18
12.09
1245
20000
11/8
2
19.11
12.22
-0.18
12.04
1944
12.24
19.0
-0.18
12.06
2144
12.24
18.9
-0.18
12.06
1245
20000
11/91
1
20.91
12.15
-0.12
12.031215
12.18
21.3
-0.12
12.061415
12.15
21.1
-0.12
12.031415
20000
11/9
2
21.11
12.14
-0.12
1 12.021216
12.10
21.5
-0.09
12.011416
11.89
22.3
-0.09
11.801416
20000
11/11
1
21.31
12.17
-0.12
12.05
0430
12.16
21.0
-0.12
12.04
0630
12.17
22.4
-0.09
12.08
0630
20000
11/11
2
21.2
12.15
-0.12
12.03
0430
12.13
21.0
-0.12
12.01
0630
12.14
22.1
-0.09
12.05
0630
20000
11/13
1
23.2
12.21
-0.06
12.15
2300
12.19
23.0
-0.06
12.13
0100
12.16
23.0
-0.06
12.10
0100
20000
11/13
2
23.1
12.17
-0.06
12.11
2300
12.15
23.0
-0.06
12.09
0100
12.11
23.0
-0.06
12.05
0100
20000
11/14
1
19.2
11.89
-0.18
11.711230
11.93
18.7
-0.18
11.751430
11.90
18.6
-0.18
11.721115
20000
11/14
2
19.5
11.90
-0.15
11.751230
11.96
19.1
-0.18
11.781430
11.84
18.6
-0.18
11.661119
20000
11/16
1
18.01
11.93
-0.21
11.72
0850
11.95
18.2
-0.21
11.74
1050
11.89
18.1
-0.21
11.68
1050
20000
11/16
2
18.2
11.88
-0.21
11.67
0850
1 11.97
18.6
-0.18
11.79
1050
11.95
18.6
-0.18
11.75
1050
20000
11/17
1
19.9
11.96
-0.15
11.811240
11.92
19.9
-0.15
11.771440
12.03
15.3
-0.30
11.731440
20000
11/17
2
20.5
11.98
0.12
11.861240
11.96
20.6
0.12
11.841440
12.05
16.1
0.27
11.781440
20000
11/18
1
18.8
11.91
-0.18
11.731350
12.01
17.1
-0.12
11.891550
12.17
16.5
-0.24
11.931550
20000
11/18
2
19.0
11.94
-0.18
11.76
1350
12.08
18.
--0.12
11.91
1550
12.14
' 16.8
0.33
11.81
1550
20000
Sheet Total
520000
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
0
NPDES Permit # N00025011
Residuals Permit # W00002883

Dates: 11/1/2014 thru 11/30/2014
Initial pH
pH After 2 Hours
pH After 24 Hours
Stabilization Amount
Date
Tank
Temp
pH Before
Corr
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
pH Before
Corr
Temp
Temp Corr
pH After
Corr
Time
17.7
18.21
11.98
11.87
12.17
12.11
12.24
12.20
11.96
12.07
12.29
12.20
12.22
12.16
-0.21
-0.21
-0.18
-0.18
-0.18
-0.18
-0.21
-0.24
-0.12
-0.12
-0.12
-0.12
11.771150.
11.661150
11.99
11.93
12.06
12.02
11.751045
11.831045
12.17
12.081737
12.10
12.04
1815
1816
0100
0100
1736
0500
0500
12.06
11.91
12.26
12.20
12.20
12.18
12.12
12.16
12.33
12.21
12.19
12.14
17.5
17.9
19.0
19.0
19.0
19.0
17.4
17.2
21.0
21.0
21.2
21.0
-0.21
-0.21
-0.18
-0.18
-0.18
-0.18
-0.24
-0.24
-0.12
-0.12
-0.12
-0.12
11.851350
11.701350
12.08
12.02
12.02
12.00
11.881245
11.921245
12.21
12.091937
12.07
12.02
2015
2016
0300
0300
1936
0700
0700
12.03
11.90
12.24
12.17
12.17
12.14
11.88
11.93
12.28
12.20
12.15
12.08
17.5
17.7
19.0
19.0
19.0
19.0
18.3
18.1
21.0
21.0
21.1
21.0
-0.21
-0.21
-0.18
-0.18
-0.181
-0.18
-0.21
-0.21
-0.12
-0.12
-0.12
-0.12
11.821350
11.791350
12.06
11.99
11.99
11.86
11.671245
11.721245
12.16
12.081935
12.03
11.96
2015
2015
0300
0300
1935
0700
0700
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
20000
11/19
1
11/19
2
11/20
1
19.41
19.11
19.31
.19.11
17.81
17.41
21.41
21.21
21.41
21.31
11/20
2
11/22
1
11/22
2
11/23
11/23
1
2
11/24
11/24
1
2
11/25
1
11/25
2
Sheet Total
760000

City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
Alternative 2 PSRP
Class B Biosolids
n.-- 111,/1.- 1h., 17/31/2014
NPDES Permit p NCO025011
Residuals Permit 4 WOON2883
Initial H
pH
After 2 Hours
pH After 24 Hours
-
Stabilization Amount
Date
Tank
Temp
pH Before
Temp
pH After
Time
pH Before
Temp
Temp
pH After
Time
pH Before
Temp
Temp
PH After
Time
Corr
Corr
Corr
Corr
Corr
Corr
Corr
Corr
Corr
12/1
1
18.0
11.86
-0.21
11.65
0745
12.00
18.4
-0.21
11.79
0945
12.01
13.4
-0.36
11.65
0945
2000D
12/1
2
18.5
11.88
0.18
11.70
0745
11.98
19.0
-0.18
11.90
0945
1206
13,7
-0.33
11.73
0945
200DO
12/2
1
18.1
11.87
-0.21
11.66
1200
12.02
18.1
-0.21
11.81
1400
12.11
17.0
-0.24
11.87
1400
20000
20000
12/2
2
18.5
11.96
-0.18J11.7800
12.05
18.4
-0.21
11.941400
12.18
16.7
-0.24
11.941400
12/3
1
18.5
11.99
-0.184
112.01
18.9
-0.1811.831345
11.94
36.4
-0.27
11.671345
20000
12/3
2
18.9
11.96
-0.1845
12.03
19.2
-0.18
1L851345
11.99
15.8
-0.27
11.721345
20000
20000
12/8
1
17.4
12.20
-0.24820
12.26
17.1
-0.2412.02
2020
11.90
17.0
-0.24
11.66
2020
20000
12/8
2
1
12.16
-0.24821
12.19
17.2
-0.24
11.95
2021
11.82
17.0
-0.24
11.58
2021
20000
1219
1
17.0
12.30
-0.24011
12.37
17.0
-0.24
12.13
2211
12.15
17.1
-0.24
11.86
2211
1219
2
17.1
12.26
-0.24012
12.29
17.0
-0.24
1205
7212
12.17
17.0
-0.33
11.93
2211
20000
1
17.5
11.79
-0.21145
12.06
17.4
-0.24
11.82
1345
12.05
13.7
-0.33
11.72
1345
1345200DO12/11
20W
12/11
2
17.9
11.87
-0.21
11.661145
11.91
17.9
-0.21
11.701345
1209
13.6
-0.33
11.731345
12/12
1
17.4
12.15
-0.30
11.851700
1212
173
-0.21
11.911900
1210
17.4
-0.24
11.861900
12/12
2
17.2
1219
-0.18
1201
1700
12.22
17.9
-0.21
12.01
1900
1219
17.0
4
12.00
20000
22/14
1
16.4
12.30
-0.27
12.03
0600
12.27
16.1
-0.27
1200
0900
1224
17.1
-UO.
-0.24
1200
0900
0800
0000
Z
2
16.3
12.29
-0.27
12.02
MO
12.31
16.0
-0.27
1204
0800
12.27
17.1
-0.24
1203
0800
1
173
11.94
-0.24
11.70
12.24
16.8
-0.24
1200
1800
11.94
16.4
-0.27
11.67
1800
20000
2
17.5
11.98
-0.21
11.77
12.29
16.7
-0.24
12.05
S1
18.8
11.81
-0.18
11.63
�00
11.89
17.8
-0.21
11.681
...2
190
11.83
-0.18
11.65
11.93
18.1
-0.21
11.721655
1207
16.2
-0.27
11.801655
20000
1
17.7
11.88
-0.21
11.67
1130
12.OR
17.2
-0.21
11.87
1344
1208
16.8
-0.24
11.84
1344
20000
2
V12V/2112
17.8
11.52
-0.21
11.641130
12.03
17.7
-0.21
11.B21344
1211
16.4
-0.27
11.841344
20000
1
18.4
12.26
-0.21
1205
0230
12.22
18.0
-0.21
12.01
0430
1225
_ 17.1
-0.24
1201
0430
20000
2
18.3
12.23
-0.21
12.02
0230
12.21
18.1
-0.21
1200
0430
1222
18.2
-0.21
12.01
0430
Z0000
1
17.4
11.89
-0.24
11.65
0400
11.90
17.2
-0.24
11.60
D600
12.28
18.1
-0.21
12.07
0600
2000O
2
17.2
11.93
-0.24
11.69
0400
11.92
17.0
-0.24
11.68
0600
12.21
18.0
-0.21
1200
0600
20000
Sheet"rtall
520000
City of Elizabeth City WWTP
Monitoring Sheet for Lime Stabilization
NPDES Permit$1 NCO025011
Alternative 2 PSRP
Residuals Permit q W00002883
Class B Blosolids
nat- 12/1/2014 thru 12/31/2014
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slum
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------------------
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i
r-
APPENDIX V
SOIL SAMPLES

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY14-SL013189
Predictive
Client:
Granville Farms Inc.
3717 Edwards Mill Rd
Advisor: Scott Carpenter
Soil Plus LLC
252-903-0390
208 Williams St.
'I Mehlich-3 Extraction
Soil Report
Raleigh, NC 27612
Greenville, NC 27858
Sampled: 10/13/2013 Received: 10/28/2013 completed: 11/08/2013
Farm: Bateman
Sampled County: Pasquotank
Links to Helpful Information
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B'
Information
Lime History:
1- Soybean 0.0 0 0
0
0 0
$pH
0
0 0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain 0.0 120 - 160 0
0
0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
2.92 0.99 27.4 99 0.3 7.2 218 123 78 18
52
36
14 21
64
64
83 0.1 0
Sample ID: 2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1-Soybean 0.0 0 0
0
0 0
$pH
0
0 0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain .0.0 120 - 160 0
0
0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-1
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.47 0.95 27.2 99 0.3 7.2 204 110 80 17
43
32
12 19
63
63
82 0.1 0
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Soybean 0.0 0 0
0
0 0
$pH
0
0 0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain 0.0 120 - 160 0
0
0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral -Organic
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.57 0.97 27.2 99 0.3 7.2 223 128 79 18
42
32
11 18
62
78
80 0.1 0
North Carolina
1 t5 4 J
Tobarco Trust I"urkd i�,iusliswlc±i5
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&GS Agronomic Division phone, (9i9) 733-2655
Website: www.ncagr.gov/agronomi/
Report No.
FY14-SL013189
Page 2 of 4
Sample ID: 4
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
$pH
0
0
0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 - Corn, grain
0.0
120 - 160 0
0
0
0
$pH
0
0
0
Note: 3 Note:
Test Results [units - W/V in
g/cm3; CEC and Na in meq/100 cO; NO3-N in mg/d0]:
Soil Class:
Mineral -Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
3.67 0.92 28.5
98 0.4 7.2
264 147
79 17
34
36
13
20
69
86
81
0.1
0
Sample ID: 5
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
$pH
0
0
0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain
0.0
120 - 160 0
0
0
0
$pH
0
0
0
Note: 3 Note:
Test Results [units - W/V in
g/cO; CEC and Na in meq/100 cnr3; NO3-N in mg/do]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% - Mg%
S-1
Mn-1
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N
3.37 0.92 27.599
0.2 7.3
221 133
80 17
41
33
10
17
64
64
85
0.1
0
Sample ID: 6
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
$pH
0
0
0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain
0.0
120 - 160 0
0
0
0
$pH
0
0
0
Note: 3 Note:
Test Results [units - W/V in
g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral -Organic
HM% WN CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-1
Na ESP
SS-1 NO3-N
3.57 0.92 28.6
99 0.4 7.2
247 149
79 17
40
34
12
19
78
98
80
0.1
0
Sample ID: 7
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Soybean
0.0
0 0
0
0
0
$pH
0
0
0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 -Corn, grain
0.0
120 - 160 0
0
0
0
$pH
0
0
0
Note: 3 Note:
Test Results [units - W/V in
g/crr>3; CEC and Na in meq/100 cO; NO3-N in mg/dO]:
Soil Class:
Mineral
-Organic
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP
SS-1 NO3-N .
3.57 0.93 27.4
99 0.4 7.1
222 126
79 17
48
31
11
18
67
84
81
0.1
0

1 }( ,
INCDA&C5 Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY14-SL013189
Page 3 of 4
Sample ID: 8 Recommendations: Lime Nutrients (lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1- Soybean 0.0 0 0 0 0 0 $pH 0 0 0 Note: 3 Note:
1.00 tons/acre; 3/2012 2 -Corn, grain 0.0 120 - 160 0 0 0 0 $pH 0 0 0 Note: 3 Note:
Test Results [units - WN in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
3.19 0.94 27.0 99 0.4 7.2 229 124 79 17 41 32 12 19 61 61 80 0.1 0

NCDA&cS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY14-SL013190
Predictive
Client:
Granville Farms Inc.
3717 Edwards Mill Rd
Advisor: Scott Carpenter
Soil Plus LLC
252-903-0390
208 Williams St.
Soil Report Mehlich-3
Extraction
Raleigh, NC 27612
Greenville, NC 27858
h� 1115
Sampled County: Pasquotank
Sampled: 10/13/2013 Received: 10/28/2013
Completed: 11/08/2013
Farm: L Larabee
Links to Helpful Information
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.0
120-200 0
0
0 0
$
0
0 0
Note: 12 Note:
1.00 tons/acre; 3/2012
2 - Fescue/OGrass/Tim, 0.0
120-200 0
0
0 0
$
0
0 0
Note: 12 Note:
Test Results [units - WN in g/crap; CEC and Na in meq/100 crr73; NO3-N in mg/drrr ]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.47 0.95 26.4 98 0.5 7.0 187 102
.78 18
57
35
23 23
68
68
83 0.1 0
Sample ID: 2
Recommendations: Lime
Nutrients (Ib/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
0
0 0
$pH
0
0 0
Note: 3 Note:
1.00 tons/acre; 3/2012
2- Soybean 0.0
0 0
0
0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 carp; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.37 0.91 28.2 99 0.2 7.3 244 141
79 17
55
38
21 14
65
65
83 0.1 0
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn-
Zn
Cu B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
0
0 0
pH$
0
0 0
Note: 3 Note:
1.00 tons/acre; 3/2012
2- Soybean 0.0
0 0
0
0 0
$pH
0
0 0
Note: 3 Note:
Test Results [units - W/V in g/cO; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
3.37 0.96 25.9 99 0.4 7.1 199 104
79 18
61
44
26 19
69
69
86 0.1 0
North Carolina
li�baccu 1nisC F�ncl (:t�miribtislcm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&U5 Agronomic division phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY14-SL013190
Page 2 of 3
Sample ID: 4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1 -Corn, grain 0.0
120 - 160 0
0
0
0
$pH
0
0
0
Note: 3 Note:
1.00 tons/acre; 3/2012
2- Soybean 0.0
0 0
0
0
0
$pH
0
0
0
Note: 3 Note:
Test Results [units - WIV in
g/cd; CEC and Na in meq/100 crrrl; NO3-N in mg/drrr3]:
Soil Class:
Mineral
HM%._ WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I
Na
ESP SS-1 NO3-N
3.47 0.95 28.4
100 0.1 7.3 230 122
81 17 56
36
19
12
64
64
85
0.1
0
Sample ID: 5
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu
B
Information
Lime History:.
1 -Corn, grain 0.0
120 - 160 0 .
0
0
0
$pH
0
0
.0
Note: 3 Note:
1.00 tons/acre; 3/2012
2 - Soybean 0.0
0 - 0
0
0
0
$pH
0
0-
0
Note: 3 Note:
Test Results [units - WN in
g/crrrii; CEC and Na in meq/1-00 crrr3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I
Zn-AI
Cu-I
Na
ESP SS -I' NO3-N
3.19 0.97 27.0 100 0.1 7.3 214 115
80 18 47
33
17
10
70
70
84
0.1
0