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WQ0002672_Residual Annual Report 2014_20150213
ANNUAL LAND APPLICATION REPORT 2014 a SUMMARY OF THE LAND APPLICATION PROGRAM FOR THE TOWN OF MAYODAN prepared by United Water Clemmons, North Carolina (336) 766-0270 ANN UAL LAND APPLICATION (;ERFI1 ICA ION FORM Permit#: WQ0002672 County: Rockingham Year: - 2014 Facility Name (as shown on permit): Town of Mayodan Land Application Operator: Jamie Whitten Phone: 336-427-5733 Land application of residual solids as allowed by the permit occurred during the past calendar year? r p Yes, ® No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Part B: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Resources.0 Yes ® No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH.was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5_, All other monitoring was performed in accordance with the permit and reported during the year as required ,md three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." fte_lnel Bre noV �wh Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) Signature of Permittee Date � I I- P- 15 S' nature of Land Applier (if different from Permittee and Preparer) Date DENR FORM ACF (5/2003) ANNUAL RESIDUAL SAl . ING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002672 Laboratory., 1) Environment 1 Facility Name: Town of Mayodan 2) NPDES # or NCO021873 3) WQ#: 4) WWTP Name: Mayodan WWTP 5) Residual Analysis Data Sample or Composite Date "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer a ;s Date DENR FORM RSSF (5/2003) ANNUAL RESIDUAL Si, LING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ000267.2 Facility Name: Town of Mayodan NPDES # or NCO021873 WQ#c ,WWTP Name: Mayodan WWTP Residual Analysis Data Laboratory: 1) Environment 1 2) 3) 4) 5) Sample- or "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer ///S Date DENR FORM RSSF-B (5/2003) rnw,unf]Haw alp hcwpombel a te�ater ID' L0 ffOx 7b_ , i4 'A'K_MONT DRIVE - - PHONE (252)"7566208 : N.C. 2783s-70s F� 2� ass �_. ti. _. t_5 )_ UNITED WATER (MAYODAN WWTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 PARAMETERS PH, Units Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), mg/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg �romium, T.(dry wt. basis),mg/kg -�:id (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Plant Available Nitrogen, mg/kg Molybdenum (dry wt. basis), mg/kg Sludge Analysis Method Sample Date Analyst Code 5.4 12/01/14 TRB 4500H13-00 11120 12/18/14 LFJ EPA200.7 <2.5 12/11/14 MTM[ 311313-04 12301 12/18/14 LFJ EPA200.7 2 12/12/14 MTM 311313-04 582 12/18/14 LFJ EPA200.7 22 12/18/14 LFJ EPA200.7 50 12/10/14 MTM 311313-04 3094 12/18/14 LFJ EPA200.7 1.6 12/19/14 MTM 245.1 R3-94 14 12/18/14 LFJ EPA200.7 3574 12/18/14 LFJ EPA200.7 < 5.0 12/08/14 MTM 311313-04 4941 12/10/14 MTM 3111B-99 931 12/11/14 MTM 3111B-99 0.33 12/22/14 LFJ 2.45 12/01/14 KKF 254OG-97 37714 12/04/14 AKS 351.2 R2-93 2692 12/02/14 KDB 350.1 R2-93 16047 12/04/14 KDB 365.4-74 484 12/03/14 BJC 353.2 R2-93 12337 12/04/14 SEJ 7 12/18/14 LFJ EPA200.7 ID#: 990 DATE COLLECTED: 11/25/14 DATE REPORTED : 12/22/14 REVIEWED BY: f�p United Water 3364275733 p.1 CHAIN OF CUSTODY Sample Location: 40� eS%E?e^0 , l Sample Collection Date: I-.25-14 Sample Collection Time: �� 001.44<< , Person Collecting Sample Na Temperature Samples Sent to Laboratory for additional analyses? YfS NO e-.,.Y,. --+,- yraer Attach copy of commercial laboratory Chain of Custody to this form aceAnalytical www..pacelabs.com Laboratory Report Jamie Whitten United Water PO Box 1279 Clemmons, NC 27012 Project: WWTesting 12/22/2014 Pace Project No.: 92230631 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Page 1 of 1 Report Date: 12/31/2014 Date Received: 12/22/2014 Sample: Effluent Lab ID: 92230631001 Collected: 12/22/14 08:00 Matrix: Water Parameters Results Units Report Limit Analyzed Qualifiers Fecal Coliforms 1.0 MPN/100mL 1.0 12/22/14 15:50 D6 Sample: Sludge sample Lab ID: 92230631002 Collected: 12/22/14 08:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit Analyzed Qualifiers Total Solids 1.4 % 0.000010 12/24/14 12:26 Percent Moisture 98.6 % 0.10 12/24/14 17:14 ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Reviewed by: \—Aa �a Terri Page terri.page@pacelabs.com Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Eden Certification IDS 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 Florida/NELAP Certification'#: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 Page 1 of 3 r. Summit Environmental Technologies, Inc. �. 3310 Win St. ENVIRONMENTAL %EC'kiN rLQt,11=1S, l+atx Cuyahoga Falls, Ohio 44223 a�nlyteal Ln'"s3f�rdw TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hgp.-1Avww.set1ek.com December 12, 2014 Deedee Woolard Environment 1, Inc. 114 Oakmont Dr P.O. Box 7085 Greenville, NC 27858 TEL: (252) 756-6208 FAX: (252) 756-0633 RE: United Water Dear Deedee Woolard: Order No.: 14120087 Summit Environmental Technologies, Inc. received 1 sample(s) on 12/2/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A21LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-I I-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 6 Page 1 of 8 SuMMOT Summit Environmental Technologies, Inc. 3310 Win St. ENVl$$O #d?ARNTAL TAA,-PrjoLonjES, fNC Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX: (330) 253-4489 Wehsite: httn✓/www.settek.com Workorder Sample Summary WO#: 14120087 12 Dec-14 CLIENT: Environment 1, Inc. Project: United Water Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14120087-001 Sludge Sample 11/25/2014 8:00:00 AM 12/2/2014 9:45:00 AM Solid Page 2 of 6 Page 2 of 8 w Summit Environmental Technologies, Inc. 3310 Win St. Case Narrative UNV1R0tdPelCr TAL 5`ECH N0L0Cir$, ttvr,:. Cuyahoga Falls, Ohio 44223 WO#: 14120087 AnzltyUcal TEL: (330) 253-8211 FAX- (330) 253-4489 Website: hap✓hvivw.settek.com Date: 12/12/2014 CLIENT: Environment 1, Inc. Project: United Water This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 6 Page 3 of 8 r' 5 Summit Environmental Technologies, Inc. 3310 WO#: 14120087 Win St . �etvt�tsrt#ai�7wy',tt1.3'c��AitiLO�iESt i{��o Cuyahoga Falls, Ohio 49223 Date Reported: p 12/12/2014 - AmgtyUral t .5or #a,,e TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Environment 1, Inc. Website: hgp:/Avww.settek.com Address: 114 Oakmont Dr Greenville NC 27858 Received: 12/2/2014 Project#: United Water TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst Sludge Sample 001 11/25/2014 TCLP Arsenic(As) 0.50 ND mg/L Solid EPA 6010 C_ 1 5.0 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Barium(Ba) 5.0 ND mg/L Solid EPA 6010 C 1 100 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Solid EPA 6010 C 1 1.0 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Chromium(Cr) 0.20 ND mg/L Solid EPA 6010 C 1 5.0 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Lead(Pb) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Selenium(Se) 0.50 ND mg/L Solid EPA 6010 C 1 1.0 12/4/2014 WK Sludge Sample 001 11/25/2014 TCLP Silver(Ag) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 12/4/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge Sample 001 11/25/2014 TCLP Mercury 0.0020 ND mg/L Solid EPA 7470 A 1 0.20 12/4/2014 AU SVOC SW-846: 8081-TCLP Pesticides Oient ID# Lab ID# Collected Analyte Rep Lint Result Units Matrix Method DF RegLvl Run Analyst Sludge Sample 001 11/25/2014 Chlordane, total 0.010 ND mg/L Solid EPA 8081 B 1 0.030 12/9/2014 JBN Sludge Sample 001 11/25/2014 Toxaphene 0.10 ND mg/L Solid EPA 8081 B 1 0.50 12/9/2014 JBN Sludge Sample 001 11/25/2014 Endrin 0.0020 ND mg/L Solid EPA 8081 B 1 0.020 12/9/2014 JBN Sludge Sample 001 11/25/2014 gamma-BHC 0.0020 ND mg/L Solid EPA 8081 B 1 0.40 12/9/2014 JBN Sludge Sample 001 11/25/2014 Heptachlor 0.0020 ND mg/L Solid EPA 8081 B 1 0.0080 12/9/2014 JBN Sludge Sample 001 11/25/2014 Heptachlor epoxide 0.0020 ND mg/L Solid EPA 8081 B 1 0.0080 12/9/2014 JBN Sludge Sample 001 11/25/2014 Methoxychlor 0.0020 ND mg/L Solid EPA 8081 B 1 10 12/9/2014 JBN SVOC SW-846: 8151 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge Sample 001 11/25/2014 2,4-D 0.10 ND mg/L Solid EPA 8151 A 1 10 12/11/2014 JBN Sludge Sample 001 11/25/2014 2,4,5-TP 0.10 ND mg/L Solid EPA 8151 A 1 1.0 12/11/2014 JBN I Summit Environmental Technologies, Inc. », �` � � �r: `y - WO#: 14120087 °- 3310 Win St. ENVI3#C>NMENTAL TFC1 NOLOa1,Ef ts�� Cuyahoga Falls, Ohio 44223 Date Reported: 12/12/2014 - imlyllt al Lar;cratorle , TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Environment 1, Inc. Website: hUp://www.settek.com Address: 114 Oalanont Dr Greenville NC 27858 Received: 12/2/2014 Project#: United Water VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Sludge Sample 001 11/25/2014 1,1-Dichloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.70 12/4/2014 MES Sludge Sample 001 11/25/20141,2-Dichloroethane 0.10 ND mg/L Solid EPA 8260 B 1 0.50 12/4/2014 MES Sludge Sample 001 11/25/2014 Benzene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 12/4/2014 MES Sludge Sample 001 11/25/2014 Carbon tetrachloride 0.10 ND mg/L Solid EPA 8260 B 1 0.50 12/4/2014 MES Sludge Sample 001 11/25/2014 Chlorobenzene 0.10 ND mg/L Solid EPA 8260 B 1 100 12/4/2014 MES Sludge Sample 001 11/25/2014 Chloroform 0.10 ND mg/L Solid EPA 8260 B 1 6.0 12/4/2014 MES Sludge Sample 001 11/25/2014 Tetrachloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.70 12/4/2014 MES Sludge Sample 001 11/25/2014 Trichloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 12/4/2014 MES Sludge Sample 001 11/25/2014 Vinyl chloride 0.20 ND mg/L Solid EPA 8260 B 1 0.20 12/4/2014 MES Sludge Sample 001 11/25/2014 MEK 2.0 ND mg/L Solid EPA 8260 B 1 200 12/4/2014 MES SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst lge Sample 001 11/25/20141,4-Dichlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 7.5 12/5/2014 AKE �Sju ge Sample 001 11/25/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Solid EPA 8270,C 1 400 12/5/2014 AKE Sludge Sample 001 11/25/2614 2,4,6-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 2.0 12/5/2014 AKE Sludge Sample 001 11/25/2014 2,4-Dinitrotoluene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 12/5/2014 AKE Sludge Sample 001 11/25/2014 Cresols, Total 5.0 ND mg/L Solid EPA 8270 C 1 200 12/5/2014 AKE Sludge Sample 001 11/25/2014 Hexachloro-1,3- 0.10 ND mg/L Solid EPA 8270 C 1 0.50 12/5/2014 AKE butadiene Sludge Sample 001 11/25/2014 Hexachlorobenzene 0.10 ND mg/L Solid EPA'8270 C 1 0.13 12/5/2014 AKE Sludge Sample 001 ' 11/25/2014 Hexachloroethane 0.10 ND mg/L Solid EPA 8270 C 1 3.0 12/5/2014 AKE Sludge Sample 001 11/25/2014 Nitrobenzene 0.10 ND mg/L Solid EPA 8270 C 1 2.0 12/5/2014 AKE Sludge Sample 001 11/25/2014 Pentachlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 100 12/5/2014 AKE Sludge Sample 001 11/25/2014 Pyridine 0.25 ND mg/L Solid EPA 8270 C 1 5.0 12/5/2014 AKE P6ee5 d(B 'AllSummit ' Environmental Technologies, Inc. WO#: 14120087 3310 Win St. d:(tAltaiE#Tx1Lt'¢LC?;=, t, Cuyahoga Falls, Ohio 44223 Date Reported: 12/12/2014 Araly°Pfeil L�trrairles TEL: (330) 253-8211 FAX.• (330) 253-4489 Company: Environment 1, Inc. Websile: hgp://wivw.settek.com Address: 114 Oakmont Dr Greenville NC 27858 Received: 12/2/2014 Project#: United Water Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Sludge Sample 001 11/25/2014 Flashpoint (140°F) >200 °F Solid EPA 1010 1 12/3/2014 TAH Sludge Sample 001 11/25/2014 Cyanide, Reactive ND ppm Solid EPA 9014 1 0.50 12/3/2014 TIR Sludge Sample 001 11/25/2014 pH 5.3 s.u. Solid EPA 9045 D 1 12/3/2014 DHC Sludge Sample 001 11/25/2014 Sulfide, Reactive ND ppm Solid EPA 9034 1 25 12/3/2014 TIR ' �'t • - i O'i is ANNUAL RESIDUAL S, iivfAING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ00002672 Facility Name: Mayodan WTP Residual Source WQ # or NPDES #: WQ00002672 WWTP Name: - Mayodan WTP Residual Analysis Data Laboratory: 1) 2) 3) 4) 5) A&L Eastern Labs Parameter . I= = GO -nC. Sample or Composite Date ®---.---® --- Molybdenum Total Phosphorus IIINitrate and Nitrite a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 7/23/2014 Reported: 7/29/2014 For: Mayodan WTP Sample ID Parameter Cust ID Result Unit: 140723-27.1 % Solids 1 140723-27.1 Fecal Coliform MTF 1 !3-27.1 Geometric Mean 1 140723-27.2 % Solids 2 140723-27.2 Fecal Coliform MTF 2 140723-27.3 % Solids 3 140723-27.3 Fecal Coliform MTF 3 140723-27.4 % Solids 4 140723-27.4 Fecal Coliform MTF 4 140723-27.5 % Solids 5 140723-27.5 Fecal Coliform MTF 5 140723-27.6 % Solids 6 140723-27.6 Fecal Coliform MTF 6 140723-27.7 % Solids 7 140723-27.7 Fecal Coliform MTF 7 62.2 <3 <4 57.4 <3 60.5 <3 38A <5 53.7 <4 58.5 <3 56.3 <4 MP MP MP MP Date Method Analyzed Analyst SM2540B-1997 SM9221 CE-2006 dry wt. basis SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM254OB-1997 SM9221 CE-2006 SM254013-1997 SM9221 CE-2006 :3M2540B-1997 SM9221 CE-2006 113M2540B-1997 �SM9221 CE-2006 07/24/14 HM 07/24/14 HM 7/29/14 CL 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM 07/24/14 HM P.O. Box 228 Statesville, North Carolina 28687. 704/872/4697 Southern Soil Builders $58 Hoots Road Roaring River NC 28669 Entered 7/23/2014 >orted: 7/29/2014 For: Sample ID Parameter Cust ID Result Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 it Date Un Method Anal, I I P.O. Box 228 •I Statesville, North Carolina 28687 • 704/8 Analyst - .... aceAnalXical www.pacelabs.com t ANALYTICAL RESULTS Project: MAYODAN TCLP Pace Project No.: 92208323 sample: A2 LAGOON Lab ID: 9220832300 -Collected: 07/07/1 Results reported on a "dry -weight" basis Parameters Results Units Report Limit 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Meti- Leachate Method/Date: EPA 1311; 07/10/14 14 gamma-BHC (Lindane) ND ug/L 0.50 Chlordane (Technical) ND ug/L 3.0 Endrin Heptachlor epoxide NO ug/L NO ug/L 0.50 Methoxychlor NO ug/L 0.50 1000 Toxaphene NO ug/L 3.0 Surrogates Decachlorobiphenyl (S) 96 % 10-138 Tetrachloro-m-xylene (S) 72 % 10-110 6010 MET ICP, TCLP Analytical Methods EPA 6 Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury 8270 MSSV TCLP Sep Funnel 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-04 (S) Phenol-d6 (S) 2-Fluorophenol(S) 2,4,6-Tribromophenol (S) 010 Preparation Mett Leachate Method/Date: EPA 1311; 07/10/14 17 ND mg/L 0.050 0.40 rng/L 0.25 NO mg/L 0,0050 ND mg/L 0.025 NO mg/L 0.025 NO mg/L 0.10 ND mg/L 0.025 Analytical Method: EPA 7470 Preparation Meth Leachate Method/Date: EPA 1311; 07/10/14 17: ND ug/L 0.20 Analytical Method: EPA 8270 Preparation Meth Leachate Method/Date: EPA 1311; 07/10/14 14: NO ug/L 50.0 NO ug/L 50.0 ND ug/L 50.0 NO ug/L 50.0 NO ug/L 50.0 NO ug/L 50.0 ND ug/L 50.0 NO ug/L 50.0 NO ug/L 100 NO ug/L 50.0 ND ug/L 50.0 NO ug/L 50.0 Pace Analytical S rvlces, Inc, 205 East Meadow R ad • Suile A Ede , NC 27288 (3 6)623.8921 15:30 Received: 07/08/14 14:55 Matrix: Solid DF Prepared EPA 3510 Analyzed CAS No, Qual _i 1 07/16/14 08:26 07/16/14 17:21 58-89-9 1 07/16/14 08:26 07/16/14 17:21 57-74-9 1 07/16/14 08:26 07/16/14 17:21 72-20-8 1 07/16/14 08:26 07/16/14 17:21 1024-57-3 1 07/16/14 08:26 07/16/14 17:21 72-43-5 1 07/16/14 08:26 07/16/14 17:21 8001-35-2 1 07/16/14 08:26 07/16/14 17:21 2051-24-3 1 07/16/14 08:26 07/16/14 17:21 877-09-8 d: EPA 30-10 1 07/1111414:30 07/14/1414:05 7440-38-2 1 07111/1414:30 07/14/1414:05 7440-39-3 1 07/11/1414:30 07/14/1414:05 7440-43-9 1 07/11/1414:30 07/15/1413:18 7440-47-3 1 07/'11/1414:30 07/14/1414:05 7439-92-1 1 07/11/1414:30 07/14/1414:05 7782-49-2 1 07/11/1414:30 07/14/1414:05 7440-22-4 : EPA 7470 1 07/11/1415:10 07/14/1414:06 7439-97-6 : EPA 3510 1 07/11/14 08:49 07/11/14 16:04 106-46-7 1 07/11/14 08:49 07/11/14 16:04 121-14-2 1 07/11/14 08:49 07/11/14 16:04 87-68-3 1 07/1'1/14 08:49 07/11/14 16:04 118-74-1 1 07/1'1/14 08:49 07/11/14 16:04 67-72-1 1 07/11/14 08:49 07/11/14 16:04 95-48-7 1 07/11/14 08:49 07/11/14 16:04 1 07/11/14 08:49 07/11/14 16:04 98-95-3 1 07/11/14 08:49 07/11/14 16:04 87-86-5 1 07/11/14 08:49 07/11/14 16:04 110-86-1 1 07/11/14 08:49 07/11/14 16:04 95-95-4 1 07/11/14 08:49 07/11/14 16:04 88-06-2 67 % 12-102 n 07/11/14 08:49 07/11/14 16:04 4165-60-0 61 % 13-107 1 07/11/14 08:49 07/11/14 16:04 321-60-8 70 % 21-132 07/11/14 08:49 07/11/14 16:04 1718-51-0 21 % 10-110 07/11/14 08:49 07/11/14 16:04 13127-88-3 31 % 10-110 07/11/14 08:49 07/11/14 16:04 367-12-4 61 % 27-108 07/11/14 08:49 07/11/14 16:04 118-79-6 / REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/17/2014 05:16 PM without the written consent of Pace Analytical Services, Inc.. Pagel Iof16 /�Palce Analytical I www.pacelabs.com ANALYTICAL RESOLTS Project: MAYODAN TCLP Pace Project No.: 92208323 i Pace Analytical Services, Inc. 205 East Meadow fjoad - Suite A Eden, NC 27288 (1..36)623-8921 j sample: ;;Z LAGOON Lab ID: 92208323001 Collected: 07/07/ 4 15:30 Received: 07/08/14 14:55 Matrix: Solid Results reported on a "dryweight" basis Parameters Results Units Report Limit DF _ Prepared Analyzed CAS No. Qual 8260 MSV TCLP Analytical Method: EPA 8260 Leachate MethoJ/Date: EPA 1311; 07/10/14 10:22 Benzene 2-Butanone (MEK) ND ug/L ND u /L 9 192 38.5 07/11/14 05:09 71-43-2 Carbon tetrachloride ND ug/L 385 38.5 07/11/14 05:09 78-93-3 Chlorobenzene ND ug/L 192 38.5 07/11/14 05:09 56-23 5 Chloroform ND ug/L 192 38.5 07/11/14 05:09 108-90-7 1,4-Dichlorobenzene ND ug/L 192 38.5 07/11/14 05:09 67-66-3 1,2-Dichloroethane ND ug/L 192 38.5 07/11/14 05:09 106-46-7 1,1-Dichloroethene ND uglL 192 192! 38.5 07/11/14 05:09 107-06-2 Tetrachloroethene ND ug/L 38.5 07/11/14 06:09 75-35-4 Trichloroethene ND ug/L 192 38.5 07/11/14 05:09 127-18-4 Vinyl chloride ND u /L g 192 38.5 07/11/14 05:09 79-01-6 Surrogates 192 38.5 07/11/14 05:09 75-01-4 .1,2-Dichloroethane-d4 (S) 90 % 70-130 38.5 Toluene-d8 (S) u 99 �0 67-135 38.5 07/11/14 05:09 17060-07-0 1g 4-Bromofluorobenzene (S) 93 % 07/11/14 05:09 2037-26-5 70-130 38.5 07/11/14 05:09 460-00-4 Date: 07/17/2014 05:16 PM REPORT OF LABORATORY)A This report shall not be reproduced, exc without the written consent of Pace Analytical VALYSIS pt in full, 'ervices, Inc.. Page-5 of 16 Page: 1 of 2 Report Number: 14-205-0200 Account Number: 46381 Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 Lab Number: 56663 Sample Id : MAYODAN WTP Total Solids Moisture * Total Kjeldahl Nitrogen Total Phosphorus Total Potassium Total Sulfur -.. Total -Calcium--- ---- Total Magnesium Total Sodium Total Iron Total Aluminum Total Manganese Total Copper Total Zinc Ammonia Nitrogen Organic N Nitrate+Nitrite-N Total Cadmium �L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 www.aleastem.com aleastem.com Project: MAYODAN WTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/22/2014 11:00:00 Date Received: 07/24/2014 00:00 Date Reported: 07/31/2014 65.52 655200 100.0 JM 07124/201415:00 SM-2540G 34.48 100.0 JM 07/24/201415:00 SM-2540G 0.29 2900 10.0 JM 07/25/2014 09:24 SM-4500-NH3C-TKN 0.12 1190 100 KM. 07/25/2014 13:22 SW 601 OC 0.21 2090 100 KM 07/25/2014 13:22 SW 601 OC 0.20 2020 100 KM 07/25/2014 13:22 SW 601 OC —0 6 --- 604 —-00- KlFll-- 07-)25/201-4-13:22— SW-60-1-OC - 0.30 2980 100 KM 07/25/2014 13:22 SW 601 OC <0.01 <100 100 KM . 07/25/2014 13:22 SW 601 OC 48800 100 KM 07/25/2014 13:22 SW 601 OC 117000 100 KM 07/25/2014 13:22 SW 601 OC 602 5 KM 07/25/2014 13:22 ' SW 6010C 37 5 KM 07/25/2014 13:22 SW 601 OC 97 5, KM 07/25/2014 13:22 SW 601 OC 0.01 137 10.0 JM 07/25/2014 09:24 SM-4500-NH3C 0.28 2763 10.0 07/25/2014 09:24 CALCULATION 35.0 2.00 JM 07/25/2014 09:25 SM-450ONO3F <2.0 2.0 KM 07/25/2014 13:22 SW 601 OC All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our rpoorts a,7d terrors are for the exclusive and conriden ?ai :;sc of our clients. !'d may not be reproduced in whole or parr, nor i??ay any , ere; e.^ce �,e rude to ehe wc, k' z'he resU/t S. Of the co,v?pary m any aJvertisa news &;ease, or other public a: u?ou;?ccmen<z: ,nthot+? obtar.?ing OUr Or?Or' v.ritreP au`hoazar.Or'. Debbie Holt Page: 2 of 2 Report Number: 14-205-0200 Account Number: 46381 Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 AILA&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271 6446 WWIN.aleastern.com Project: MAYODAN WTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/22/2014 11:00:00 Lab Number: 56663 Date Received: 07/24/2014 00:00 Sample Id: MAYODAN WTP Date Reported: 07/31/2014 i otai chromium 66 5 KM 07/25/2014 13:22 SW 6010C Total Nickel 24 5 KM 07/25/2014 13:22 SW 6010C Total Lead 18 5 KM 07/25/2014 13:22 SW 6010C Total Arsenic 5.0 3.0 KM 07/25/2014 13:22 SW 6010C Total Mercury <0.4 0.4 KM 67/25/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 07/25/2014 13:22 SW 6010C __._pH CStandard Units) _ 5 97 - -- -- — -.... - - - - — 200 - - ... - - J M---- -.... ---07/25/2014-09:24 SW--9045-D - - Total Molybdenum <5 5 KM 07/25/2014 13:22 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Mo", AND "Se". THE MSD WAS OUT OF LIMITS FOR "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and let<er s are for the exclusive and confidential use of cur c?ienrs, and may no; be reproduced in vinole or pana , nor n-, any reference be n7ade to -'he work. the results. or The company in any advertising, naves release. er vi er pubii anrouncernen;'s without obtaining eur prior rriiten author izabon. Debbie Holt ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: ^---rator: Used: Town of Mayodan - Total Dry Tons Applied (Annual): WQ0002672 Cation Exchange Capacity (non 503 only): Jamie Whitten Owner: ' H Dumaine 24 Acres Permitted: 24 Site #: 158.6976 Field #: 32 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): posite Date Total Phos- phorus •�. •� �� al Heavy Metal Field Loadings (Calculated in Ibs/acre): 1 2 L±j5 6 7 8 9 10 ftlj 12 __3j ' y r4 o 0.6364 5.976 Arsenic 0.0032 0.0598 0 0 0 0 0 0 0 0 0 0 0.0629 Cadmium 0.0025 .0.0239 0 0 0 0 0 0 0 0 0 0 0.0264 Chromium 0.028 0.4422 0 0 0 0 0 0 0 0 0 0 0.4702 Copper 0.7408 0.7888 0 0 0 0 0 0 0 0 0 0 1.5296 Lead 0.0636 0.2151 0 0 0 0 0 0 0 0 0 0 0.2788 Mercury 0.002 0.0048 0 0 0 0 0 0 0 0 0 0 0.0068 Molyb- 0.0089 0.0598 0 0 0 0 0 0 0 0 0 0 0.0687 denum Nickel 0.0178 0.2868 0 0 0 0 0 0 0 0 0 0 0.3047 Selenium 0.0064 0.0598 0 0 0 0 0 0 0 0 0 0 0.0661 Zinc 1.185 1.1593 0 0 0 0 0 0 0 0 0 0 2.3443 Total Phos- 20.425 14.223 0 0 0 0 0 0 0 0 0 0 34.648 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, in' `.ng the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date x See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATIOl'i jy1ELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Mayodan Owner: H Dumaine Site #: 008 Field #: Permit #: WQ0002672 Operator: Jammie Whitten 32 Acres Utilized: 24 Annual Dry Tons Applied: 158.7133275 Cation Exchange Capacity (non 503): Acres Permitted: 24 o � 0 � o A Specify Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 * * G�• Cu.Yd. TReport Totals in Gal. Crop 1 Crop 2 4-2014 149500 6229.2 2.45 0.636402813 WWTP dry 0 s 0.5 0.3 37714 2692 484 15.7021 ####### Corn 1 11-20141 52500 2187.5 65.52 5.9766525 WTP dry 0 s 0.5 0.3 2900 137 35 11.1453 ######4. Corn 2 0 0 1 0 0• .. 3 0 0 0 0. 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 84171:<.':' As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.062942 0.02645 0.470231 1.5296 0.27878 0.00682 0.06867 0.30467 0.06612 2.34432 34.6475 26.8474 0 Date lbs/ac .:..: Current Cumulative lbs/ac 0.133740938 10.16805 0.47023 4.20088 0.42038 0.01212 10.23839 10.44627 0.09444 5.89431 ;• ;>: `"'. °'-. .`.,: - : ; ° 0.070798938 0.1416 0 2.67128 0.1416 0.0053 10.169721 0.1416 0.02832 3.54999� 36 34 NA 1338 267 15 NA 374 89 2498 " " ^:.'. 200 lra0iti 0000 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit lst/2nd Cro p "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC -Incorporation **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR.FORM FSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: e-- ator: Used: Town of Mayodan Total Dry Tons Applied (Annual): WQ0002672 . Cation Exchange Capacity (non 503 only): Jamie Whitten Owner: H Dumame 15 Acres Permitted: 15 Site #: 110.235 Field #: 33 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total Phos- phorus A; - 4 Vd Heavy Metal Field Loadings (Calculated in lbs/acre): 71 2 3 4 5 6 7 8 9 10 11 12 �y� o o H o 0.974 6.375 Arsenic 0.0049 0.0638 0 0 0 0 0 0 0 0 0 0 0.0686 Cadmium 0.0039 0.0255 0 0 0 0 0 0 0 0 0 0 0.0294 Chromiurr. 0.0429 0.4718 0 0 0 0 0 0 0 0 0 0 0.5146 Copper 1.1337 0.8415 0 0 0 0. 0 0 0 0 0 0 1.9752 Lead 0.0974 0.2295 0 0 0 0 0 0 0 0 0 0 0.3269 Mercury 0.0031 0.0051 0 0 0 0 0 0 0 0 0 0 0.0082 Molyb- 0.0136 0.0638 0 0 0 0 0 0 0 0 0 0 0.0774 denum Nickel 0.0273 0.306 0 0 0 0 0 0 0 0 0 0 0.3333 Selenium 0.0097 0.0638 0 0 0 0 0 0 0 0 0 0 0.0735 Zinc 1.8136 1.2368 0 0, 0 0 0 0 0 0 0 0 3.0503 Total Phos- 31.26 15.173 0 0 0 0 0 '0 0 0 0 0 46.432 horus "I ,certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, inr' `ig the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATIOk � ; GELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Mayodan Owner: H Dumaine Site #: 008 Field #: Annual Dry Tons Applied: 110.236035 Operator: Jammie Whitten Cation Exchange Capacity (non 503): 33 Acres Utilized: 15 Permit #: WQ0002672 Acres Permitted: 15 o o A Specify Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Molqt. Inches Precip. Past 24 Hrs. A li pp cation Meth- od* Vola- tili- nation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 Gal. Cu.Yd. Report 4 Totals in Gal. Crop 1 Crop 2 4-2014 143000 9533.3 2.45 0.973973 WWTP dry 0 s 0.5 0.3 37714 2692 484 24.031 ####### Corn 1 11-2014 35000 2333.3 65.52 6.375096 WTP dry 0 s 0.5 0.3 2900 137 35 11.8883 ####### Corn 2 0 0 0 0 3 0 0 0 0- 4 0 0 1 0 0 5 0 0 1 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 .. 0 12 TOTALS: 11867 `,::;:. ` As - Cd Cr Cu Pb Hg Mo -Ni Se Zri P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.06862 0.0294 0.51461 1.97524 0.3269 10.00822 0.07739 0.33327 0.07349 3.05034 46.4321 35.9193 0 Date lbs/ac Current Cumulative lbs/ac 0.156130552 0.107 0.51461 4.77409 0.51291 0.01397 0.30922 0.50829 0.14097 8.3693 0.087510552 0.0776 0. 2.79885 0.18601 0.00575 0.23183 0.17502 0.06748 5:34896�;��°;:..;�� 36 34 NA 1338 267 15 NA 374 89 2498 7--77777 r. .s . 200 Prior Years -Cumulative lbs/ac Permitted C. P. L. R. t Perms PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,E 17Y4 Sigffature of Land Applier i -a"-Is Date *Application Method: S - Surface,IN - Injection, INC - Incorporation **Volatilization Rate:.Surface - 0.5. Iniection/Ificorporation - 1.0 * * * C.P.L.R.: Cumulative Pollutant Loadins Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Town of Mayodan Total Dry Tons Applied (Annual): Permit #: WQ0002672 Cation Exchange Capacity (non 503 only): ,7perator: Jamie Whitten Owner: Acres Used: 46 Acres Permitted: 46 Site #: 001 Field #: H. Dumaine 21.9143925 30 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Phos- phorusTotal .�� annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 4 5 6 7 8 9 10 11 12 CD 0.4764 0 0 0 1 0 0 -Arsenic' 0.0024 0 0 0 0 0 0 0 0 0 0 0 0.0024 Cadmium 0.0019 0 0 0 0 0 0 0 0 0 0 0 0.0019 Chromiunj 0.021 0 0 0 0 0 0 0 0 0 0 0 0.021 Copper 0.5545 0 0 0 0 0 0 0 0 0 0 0 0.5545 Lead 0.0476 0 0 0 0 0 0 0 0 0 0 0 0.0476 Mercury 0.0015 0 0 0 0 0 0 0 0 0 0 0 0.0015 Molyb- denum 0.0067 0 0 0 0 0 0 0 0 0 0 0 0.0067 Nickel 0.0133 0 0 0 0 0 0 0 0 0 0 0 0.0133 Selenium 0.0048 0 0 0 0 0 0 0 0 0 0 0 0.0048 Zinc 0.8871 0 0 0 0 0 0 0 1 0 0 0 0 0.8871 Total Phos- 15.29 0 0 0 0 0 0 0 0 0 0 0 15.29 horus, J. cerury, unaer penalty of iaw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Iuding the possibility of fines and imprisonment for knowing violations" Signature of Lan Appher Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION,, -tLD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Mayodan Owner: Dumaine Trust Operator: Site #: 001 Permit #: WQ0002672 Annual Dry Tons Applied: 21.9143925 Jamie Whitten Cation Exchange Capacity (non 503): Field #: 30 Acres Utilized: 46 Acres Permitted: 46 c N s� � o A s eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Inches Precip. Past 24 Hrs. A li pp cation Meth- od* Voli- tila- zation Rate* * Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- Irate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 G� Cu.Yd. TReport Totals Gal Crop 1 Crop 2 4/20141 214500 4663 2.45 0.476399837 Mayodan WWTP Dry 0 S 0.5 0.3 37714 2692 484 11.7543 ####### Corn 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 1 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 4663 :,. °._ As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.002381999 0.00191 0.02096 0.55453 0.04764 0.00152 0.00667 0.01334 0.00476 0.88706 15.2896 11.7543 0 Date lbs/ac Current Cumulative lbs/ac 0.129894535 10.07141 0.02096 7.59263 2.4768 10.0041910.52939 0.44536 0.11884 11.7772 0.127512535 0.06951 0 7.0381 2.429 160.00267 0.52272 0.43203 0.11408 10.8902 =, _ 36 34 1338 267 15 ----1 374 89 1 2498 200 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Limit 2n o Permit PAN L t 1st/ d Cr "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." / 7� ��- Signatur of Land Applier 1- a-7- ►v Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: 7perator: Acres Used: Town of Mayodan Total Dry Tons Applied (Annual): 13.28145 WQ0002672 Cation Exchange Capacity (non 503 only): Jamie Whitten Owner: 29 Acres Permitted: 29 Site #: 001 H. Dumaine Field #: 29 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): © [�. Em 113 ,,nnual Heavy Metal Field Loadings (Calculated in lbs/acre): ' K o 1 2 3 4 5 6 7 8 9 10 11 2 H o 0.458 0 0 0 0 0 Arsenic 0.0023 0 0 0 0 0 0 0 0 0 0 0 0.0023 Cadmium 0.0018 0 0 0 0 0 0 0 0 0 0 0 0.0018 Chromiurr 0.0202 0 0 0 0 0 0 0 0 0 0 0 0.0202 Copper 0.5331 0 1 0 0 0 0 0 0 —0 0 0 0 0.5331 Lead 0.0458 0 0 0 0 0 0 0 0 0 0 0 0.0458 Mercury 0.0015 0 0 0 0 0 0 0 0 0 0 0 0.0015 Molyb- 0.0064 0 0 0 0 0 0 0 0 0 0 0 0.0064 denum Nickel 0.0128 0 0 0 0 0 0 0 0 0 0 0 0.0128 Selenium 0.0046 0 0 0 0 0 0 0 0 0 0 0 0.0046 Zinc 0.8528 0 0 0 0 0 0 0 0 0 0 0 0.8528 Total Phos- 14.698, 0 0 0 0 0 0 0 0 0 0 0 14.698 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, "Juding the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATIa'4, ELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: Owner: Site #: 001 H. Dumaine PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Mayodan Field #: Permit #: WQ0002672 Operator: Jamie Whitten 29 Acres Utilized: 29 Annual Dry Tons Applied: 13.28145 Cation Exchange Capacity (non 503): Acres Permitted: 29 o oEReportPer A Specify Totals Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. A li pp cation Meth- od* Voli- tila- zation- Rate** Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop P p 2 Gal. CuNd. Crop 1 Crop 2 4/2 130000 4482.8 2.45 0.457981034 Mayodan WWTP Dry 0 S 0.5 0.3 37714 2692 484 11.2999 ####### Corn 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 1 0 0 1 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 4483 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied r' k Annuallbs/acre 0.002289905 0.00183 0.02015 0.53309 0.0458 0.00147 0.00641 0.01282 0.00458 0.85276 14.6984 11.2999 0 Date lbs/ac ,< V Current Cumulative lbs/ac 0.137452626 0.12452 1.20915 8.88801 1.40146 0.0117 0.42657 0.56445 0.16224 16.0683 0.135162721 0.12269� 1.189 8.35492 1.35567 0.01024 0.42016 0.55163 0.15766 15.2155 36 34 1338 267 15 ---- 374 89 2498t 200 ll-aviq auob " -; Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i�A Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5, Iniection/Incorvoration -1.0 ***.C.P.L.R.: Cumulative Pollutant Loadina Rate * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: r,)perator: Acres Used: Town of Mayodan Total Dry Tons Applied (Annual): 9.9610875 WQ0002672 Cation Exchange Capacity (non 503 only): Jamie Whitten Owner: H. Dumaine 16 Acres Permitted: 16 Site #: 001 Field #: 31 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 10 b M a G M in in . Phos- orus •Anual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 4 5 6 7' 81 9 10 11 12 tri cs C is y 4 o 0.6226 0 0 0 1 0 0 Arsenic 0.0031 0 0 0 0 0 R 0 0 0 0 0 0.0031 Cadmium 0.0025 0 0 0 0 0 0 0 0 0 0 0 0.0025 Chromiurr 0.0274 0 0 0 0 0 0 0 0 0 0 0 0.0274 Copper 0.7247 0 0 0 0 0 0 0 0 0 0 0 0.7247 Lead 0.0623 0 0 0 0 0 0 0, 0 0 0 0 0.0623 Mercury 0.002 0 0 0 0 0 0 0 0 0 0 0 0.002 Molyb- 0.0087 0 0 0 0 0 0 0 0 0 0 0 0.0087 denum Nickel 0.0174 0 0 0 0 0 0 0 0 0 1 0 0 0.0174 Selenium 0.0062 0 0 0 0 0 0 0 0 0 0 0 0.0062 Zinc 1.1592 0 0 0 0 0 0 0 0 0 0 0 1.1592 Lhs 19.981 0 0 0 0 0 0 0 0 0 0 0 19.981 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, ?huding the possibility of fines and imprisonment for knowing violations" ���". ��/ V 7- t � Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATI6.,_,tELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: Owner: Site #: 001 H. Dumaine PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Mayodan Field #: Operator: 31 Permit #: WQ0002672 Jamie Whitten Acres Utilized: 16 Annual Dry Tons Applied: 9.9610875 Cation Exchange Capacity (non 503): Acres Permitted: - 16 �. o o o A S eci Totals Per Acre % Solid s Dry Tons Per Acre I Residual Sources (Summarize) ' 1 e Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Voli- tila- zation Rate** Miner- ala- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 * � Gal. Cu.Yd. :,: Report Totals in Gal. Crop 1 Crop 2 4/2014 97500 6093.8 2.45 0.622567969 Mayodan WWTP Dry 0 S 0.5 0.3 37714 2692 484 15.3607 ####### Corn 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 6094 As Cd Cr Cu Pb Hg I Mo Ni Se I Zn P I PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.00311284 0.00249 0.02739 0.72467 0.06226 0.00199 0.00872 0.01743 0.00623 1.15922 19.98071 15.3607 0 Date lbs/ac Current Cumulative lbs/ac 0.018059919 0.0057 0.04639 1.72673 0.36152 0.00215 0.03996 0.06183 0.02087 3.22363 0.014947079 0.00321 0.019 1.00206 0.29926 0.00016 0.03125 0.04439 0.01465 2.06441 36 34 1338 267 15 ---- 374 89 2498 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Prmi 2Crop e t PAN Limit 1st/ nd "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 5&< r // Signature of Land Applier I-J-1-(y- Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5. Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Town of Mayodan Permit Number: WQ0002672 VVWTP Name: Town of Mayodan WWTP NPDES Number: NCO021873 Monitoring Period: From 1/1/2014 To 12/31/2014 "'athogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1® Alternative 2 ® Alternative 3 ®, Alternative 40 Alterative 5 ® Alternative 6 0 -� If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 131 Heat Drying ® Heat Treatment ® Thermophilic E] `ter Beta e Ra Y ® G Ray aroma ast 'z P eun ation Class B: Alternative 121 Alterative 2 ® Alterative 3 ®_'_''� If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ® CompostingCoMposting ® jAerobic Digestion 21 Anaerobic eo bic Di estion If applicable to alternative performed (Class A or Class B) complete the follow, monitoring data: Pathogen Density Number o Frequency Sample Analytical Parameter Level in Excee- of Tech- Geo. Mean Maximuir Units dcrices Type niaue 2 x 10 to the 6th power NTN per 6725 9763 22333 #/gram 0 7 G 9221 E gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per gram, of 1000 mpn per gram of total solid (dry weight) salmonella bacteria 3 NTN per 4 (in lieu of fecal grams total solid coliform) (dry Weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: (Option 1 C3 Option 2 ® Option 3 ® Option 4 R1 Option 5 Option 6 ® Option 7 ® Option 8 ® Option 9 ® Option 10 13 No vector attraction reduction options were performed ® CERTIFICATION STATEMENT (please check the appropriate statement) R1 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ® "1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." :;parer Name and Title (type or print) v Land Applier Wdme and Title (if applicable)(type or print) Signature of Preparer Date Signature of rand Applier (if applicable) Date DENR FORM RF (5/2003) "=ACILITY NAME: QUARTER SAMPLING ANNUAL SAMPLING Town of Mayodan YES WORKSHEET FOR SLUDGE SAMPLING Total Gallons Hauled 734500 Total Dry Tons 75.03 68.0522 Total Acres Applied 130 SAMPLE DATE VS in VS out i ------------- ------------ ------------- ------------- ------------- ------------- ------------- ------------- ------------- M Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Town of Ma odan Biosolids Permit Number: WO0002672 Date: 12/31/2014 Digester Temperature: 20 Sampling Date/Time: 12/31/14 / 1:45 Sampled By: Jamie Whitten Analysis Date/Time: 12/31/14 / 1:57 Analyzed By: Jamie Whitten Sample Volume: milliliters Total Solids: 1.4 % Dry Solids Beginning Temperature: 20 degrees Celsius End Temperature: 20 degrees Celsius Dissolved Oxygen Level E:11�'; 8.43 39YA 8.24 -]K M M W r&sL! rM W-1v FAI-11 7.8 Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 8.8 0.8 5.15 mg Oxygen/L/Hr 0.368 mg Oxygen/hr/g 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Rate:1 0.370 mg Oxygen/hr/g Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 12 10 FA Oxygen Uptake Rate Chart Y; -0a085 x + 8.92 3x . e4 •R a + sx ' 7�a 1 2 3 4 5 6 7 8 9 10 11 12 13 Time (minutes) 14 15 16 Sample Location: Mayodan Digester Sample Date: 12/31/14 Sample Time: 1:45 PM Analysis Date: 12/31/14 Analysis Time: 1:57 PM ElMommiN Flo lumpombd Wa8£ema ter I. BOX 7085, 114 OAKMONT DRIVE - _ - - - - PHONE (252) 756-6208 _-- _EENVILLE, N.C., 27835-7085 FAX 252 756-0633 ID#: 990 B UNITED WATER (MAYODAN WWTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 DATE COLLECTED: 12/10/14 CLEMMONS ,NC 27012 DATE REPORTED : 12/15/14 PARAMETERS Total Residue, mg/l Fecal Coliform (MPN), /gram Solids REVIEWED BY: Sample Sample Sample Sample Sample Analysis Method #1 #2 #3 #4 #5 Date Analyst Code 24180 25280 25040 25080 20040 12/11/14 LW 2540B-97 22333 6725 13978 9569 6487 12/11/14 LW 9221E-06 4;6 ®.r Emwokamu(PIW % kwup umbd t+ia§tawat'erSD 10` BOX 7085, 114 OAKMONT DRIVE 4' - _- - PHONE (252) 75676208. ,,...EENVILLE,- N.C. 27835-7085 FAX 252 756-0633 UNITED WATER (MAYODAN WWTP-SLUDGE) NADINE BLACKWELL P.O. BOX 1279 CLEMMONS ,NC 27012 ID#: 990 B DATE COLLECTED: 12/10/14 DATE REPORTED : 12/15/14 REVIEWED BY: Sample Sample Analysis Method PARAMETERS #6 #7 Date Analyst Code Total Residue, mg/l 21160 23440 12/11/14 LW 2540B-97 Fecal Coliform (MPN), /gram Solids 6616 9806 12/11/14 LW 9221E-06 .10 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Mayodan WQ Permit Number: WWTP Name: Mayodan WTP NPDES Number: WQ0002672 Monitoring Period: From 1/1/2014 To 12/31/2014 -pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ® 7Alt B (Alk Treatment) ® Alt. C (Prior Testing) A1t.D (No Prior Test) ® Process to Further Reduce Pathogengs If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ® Heat Drying ® Heat Treatment ® Thermophilic Beta Ray ® Gamma Ray ® Pasteurization Class B: Alt. (1) Fecal Density M1 Alt. (2) Process to Significantly Reduce Pathogens El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization . ® Air Drying ® 1 Composting EJ Aerobic Digestion Anaerobic bic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number or Excee- dences Frequency of Analysis , Sample Type a y ica Tech - ni ue Minimum Geo. Mean Maximum, Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN cFu 1000 mpn per gram of total solid (dry weight) 3 4 5 MPN/g 0 7 grab sm9221 c Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry�, wei t :'xtor Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed: Alt.l (VS reduction) ® Alt. 2 (40-day bench) ® Alt. 3 (30-daybench) ® Alt. 4 (Spec. 02 uptake) 13 Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk. Stabilization ® Alt 7 (Drying - Stable) ® I Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ® Alt. 10 (Incorporation) ®. No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) 211" "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with, the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Preparer Name and Title (type or print) Land Applier Aame and Title (if applicable)(type or print) ( nature of Preparer* Date Signature of L d Applier (if applicable) Date *Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) r NCDA&I ;ronomic Division Phone: (919) 733-2656 Website: w agr.gov/agronomi/ Report No. i-SL014691 Client: Southern Soil Builders, Inc. 958 Hoots Rd Advisor: Predictive Roaring River, NC 28669 Soil Report � Mehlich-3 Extraction Sampled County :Rockingham �N1FilU- f Sampled: Received: 11/07/2014 Completed: 11/26/2014 Farm: Links to Helpful Information Sample ID: 00129 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P20S K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, silage 1.0 180-220 0 60 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN In g/cO; CEC and Na In meg1100 cO; NO3-N in mgldrr�]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 1.11 7.8 76 1.8 5.3 83 68 48 24 44 191 132 69 69 125 0.1 1 Sample ID: 00130 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, silage 0.0 180-220 40 70 0 0 0 0 0 0 Note: 3 2- Test Results [units - W/V In glcO; CEC and Na In meq/100 cm3; NO3-N in mgldrrr ]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.22 1.08 9.7 88 1.1 6.3 52 66 56 29 35 247 161 77 77 200 0.1 1 Sample ID: 00131 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, silage 0.9 180-220 20 60 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN In glcmr ; CEC and Na In meq/100 cmP; NO3-N in mgidd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.27 1.14 6.6 74 1.7 5.3 63 70 45 24 34 569 358 112 112 102 0.1 2 North Carohna f�/ f 2 Al. 1f'4';1 ' hum ft-wdC Lq Et:5iw.". Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDAB s •ironomic Division Phone: (919) 733.2655 Website: w :agr.goviagronomil Report No. i a-SL014691 Page 2 of 3 Sample ID: 00832 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Corn, silage 0.7 180-220 0 50 0 0 0 0 0 0 Note: 3 2- Test Results [units - WN In g/cm3; CEC and Na in meq/100 cnr3; NO3-N In mg/dm3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 1.09 8.2 82 1.5 5.5 112 79 52 24 32 495 314 117 117 590 0.1 1 Sample ID: 00833 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1- Corn, silage 0.0 '180-220 0 80 0 0 0 0 0 0 Note: 3 2- Test Results [units - W/V in g/cm3; CEC and Na In meq/100 cmP; NO3-N In mg/dm31: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 1.08 8.4 86 1.2 6.2 178 56 58 25 31 277 181 147 147 752 0.1 1