WQ0002645_Residual Annual Report 2014_20150318

RECEIVED
MAR 18 2015
Town of
Columbus
Town of Columbus
2014 Annual Report
Land Application Report
NC Permit no. WQ0002645

U
WQ Permit#: WQ0002645 _ County:
Facility Name (as shown on permit):
Land Application Operator: So
Land application of residuals as allowed by the pe
W' Yes ® No - If No, skip Part A, and Part
generated but not land applied, please attach an e
A - Residuals Annlievitian Cnmmarv-
Total number
Total number of fields utilized f(
Total amount of dry tons applied durir
Total number of acres utilizes f(
Part: B - Annual Comnian(:e Statement:
Facility was compliant during calendar year
(including but not limited -to items 1-1:3 below) issue
If no please, provide a written description why the
taken.
Polk Year: 2014
Town of ColumbL s
tern Soil Builders, Inc. P one: 336-957-8909
]it occ rred during the past calendar ear?
and proceed to Part C. Also, If residuals were
lanation on how the residuals were handled.
f application fields in thepermit: 9
land application during the year: 2
the year for all application sites: 18.2145
land application during the year: 25.6
2014 with all conditions of the #and application permit
by the Division of Water Resources. ® Yes N"'No
.ility was not compliant, the dates, at d explain corrective action
1) Only residuals approved for this permit were applied to th
2) Soil pH was adjusted as specified in the permit and lime N
the limit specified in the: permit.
3) Annual soils analysis were performed on each site receivi
of laboratory results are attached.
4) Annual TCL13 analysis (if required) was performe and th
5) All other monitoring was performed in accordance with tl
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Co centra
Loading Rates in 15A NCAC 02T .1105(b) (applicable to
7) All general requirements in as specified in the Land Appt
503 regulated facilities).
8) All monitoring and reporting requirements in 15A CA(
503 regulated facilities).
9) All operations and maintenance requirements in th pern
authorization was received from the Division of W Etter R
10) No contravention of Ground Water Quality Standards oc
attached to include appropriate actions and remedi tions,
11) 'Vegetative cover was maintained and proper crop nianag
specified in the permit.
12) No runoff of residuals fi-om the application sites onto adj
13) All buffer requirements as specified on the permit Were r
Part C - Certification:
"I certify, under penalty of law, that the above info
and complete. I am aware that there acre significant
possibility of fines and imprisonment for knowing.,v
Permittee Name and Title (type or print)
Signature of Preparer*
(if different from Permittee)
* Preparer is defined in 40 CFR Part 503.9 (r) and 1
permitted sites.
s applied (if needed) to achieve ;a soil pH of at least 6.0 or
residuals during the past calendar year and'three (3) copies
e (3) copies of certified laboratory results are attached.
permit and reported during the l ear as required and three (3)
i Limits in 15A NCAC 02T .1 105(a) or the Pollutant
CFR Part 503 regulated facilities).
ion Permit were complied with, (applicable to 40 CFR Part
1111 were complied with (
were complied with or, in the
at a monitoring well or
was performed on each site
to 40 CFR Part
of a deviation, prior
of violations are
residuals, as
property or nearby surface w ters has occurred.
ined during each application of residuals.
oration is, to the best of my knowledg
)enalti s for submitting false informa
Elation i."
Signature of dt ee
)ate Signature of Land Applier
(if different from Permittee,
9CAC i 2T .1102 (26) DEN
and belief, true, accurate,
on, including the
to
3 o-'
Date
3--
Date
id Preparer)
FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional pare meters ti, be analyzed. The parameters can be reported in FORM RSSF - B
`J`dQ Permit Number: WQ0002645
Facility Name•
T fC
Laboratory: 1)
• own o olumbus 2)
Residual Source WQ # or
NPDES #: W00002645 3)
4)
WWTP Name: Town of Columbus
Jf
Residual Analysis Data
r
Conc n ,
ETS
Parameter Limit 10-1-
lmgiKg) (m a l 2014
Percent Solids (%) NA 3.2
sample or Lomposite Date
Arsenic 75
Cadmium 85
copper 4,300
Chromium NA
Lead 640
Mercury 57
Molybdenum 75
Nickel 420
Selenium 100
limits listp—.d in this fnrn,
Zinc 7,500
Total Phosphorus NA
TKN NA
Ammonia -Nitrogen NA
Nitrate and Nitrite NA
-
,a
For surface disposal facilities the ceiling concentration
„vt UFF 1;aule. 1Clerence me individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for sub 'tt' alse information, including the possibility of fines and imprisonment for knowing violations."
gnature of Preparer * 3 t
ate
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

v _ I'1 V1CI1Ik1 1 "A%IVl
Attach this form to the corresponding Field'Loading, Summary Form to be submi
Facility Name: Town of Columbus Total Dry Tons Applie
Permit #: WQ0002645 __ Cation Exchange Capacity (non 503 o
Operator: Frank Smith _ Owner: rank Smith Predomina
Acres Used: 15.8 Acres Permitted: 15.8 Site #: C1-3
Residual Analysis Data (Eleavy Metals and Total Phosphorus use mg/kg, % Solids
Ire -if 4
Com-
posite
Date 1 10/1/14
% Solids . 3.2
Arsenic
Cadmium
Lead
Nickel_
Selenium_
Zinc _
Total
Phos-
Annual Heavy Metal Field Loa Calculat in
lbs/
cre):
Total Lij 141 5 11 6j
7 81
DT/Ac./
App.
Event
Arsenic
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0.000
0.000
0.006
0. 000
.000
0.060
0.000
Copper
0.000
0.000
0.0 00
0.000
0.000
0.000
0.000
0.000
Chromium
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
.000
0.000
.0.000
Mercury
0.000
0.000
0.1000
0.000
0.000
.000
0.00,0
0.000
Molyb-
denum
0.000
0.000
0.000
0.000
0.000
0.000
0.00'0
0.000
Nickel
0.000 1
0.000
0.000
0.000
0.000
0.000
0.000
-0.000
Selenium
0.000
0.000
0.000
0.000
0.000
0
000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
0.000
0.000
0.000
0.000
0
000
0.006
0.000
"I certify, under penalty of law, that this document i
with a system designed to assure that qualified perso
I am aware that there are significant penalties for su
imprisonment for knowing violations".
Sign ure'of Land A Tier
PP
ed in Annual Report
(Annual): 0.00
ly):
t Soil Series: Pacolet
Field #: C1-3
se Raw Percent #l:
I�
' 1 111
1 11!
1 111
1 111
1 111
' 1 111
1 111
1 111
1 1!1
1 111
' 1 111
' 1 111
1 111
1 11'
1 111
1 111
1 111
1 111
1 111
1 111
I 1111
1 111
1 111
1 11!
1 111
I 1111
till
1 111
1 111
1 111
I1111
1 110
1 111
1 111
1 111
I 1111
1 110
! 111
1 111
1 111
I ! 111
1 110'
1 111
! 111
1 111
I 1111
1 1!0
1 111
1 111
1 111
1 111
1 111
! 111
! 111
1 111
under t ion or sup 'ervis of n in accordance
gathered and evaluated the information submitted.
information, including the possibility of fines and
3-1_rs,
Date
DENR F RM MFLSF (12/2006)

Attach this form to -the corresponding Field Loading Summary Form to be subint
Facility Name: Town of Columbus Total Dry Tons Applie
Permit #: WQ0002645 Cation Exchange Capacity (non 503 o
Operator: Frank Smith Owner: Frank Smith Predomina
Aches Used: 9.8 Acres Permitted: 9.8 Site #: C1-4
Residual Analvsis Dntn (FrPaw Ma+. jo .-A qrm-_ D1...
ed in Annual Report
(Annual): 0.00
y):
t Soil Series: Pacolet
Field #: C14
Sample or
Com-
posite;
Date
10/1/14
2
3
1 4
_5
6
7
all., 11g,
8
/„ „U,lum
9
10
se
tcaw rercent
ifs:
11
12
% Solids
3.2
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molyb-
denum
Nickel.
Selenium
Zinc
Total
Phos-
horus
Annual
Nenw Metal
TlArl
T
T
DT/Ac./
App.
Event
LIJ
L.2_F_3
I
5
Arsenic
0.000
0.000
0.000
0.000
0.000
Cadmium
0.000
0,000
0.000
0.000
0.000
Copper
0.000
0.000
0.000
0.000
0.000
:Iromium
0.000
0.000
0.000
0.000
0.000
Lead
0.000
0.000
0.000
0.000
0.000
Mercury
Molyb
denumenum
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Nickel
0.000
0.000
0.000
0.000
0.000
Selenium
.0.000
0.000
0.000
0.000
0.000
Zinc
0.000
0.000
0.000
0.000
0.000
Total
Phos-
0.000
0.000
0.000
0.000
0.000
"I certify, under penalty of law, that this document i
with a system designed to assure that qualified perso
I am aware that there are significant penalties for su
imprisonment for knowing violations".
Signature of Land pplier
Elm
1 111
1 111
1 111
1 111�
1 111
1 111
1 1!1
1 111
1 111
1 111
1 111
111
f 1 111
1 111
1 111
! 111
1 111
111
1 1/1
1 111
1 !11
1 111
1 111
111
1 1/1
1 ! 11
1 111
1 111
1 111
1 111
1 11!
1 111
1 111
1 111
1 111
1 111
1 111
Cal
l l/1
1 111
1 111
1 111
1 111
MI
1 111
1 111
1 111
1 !11
1 111
MIMM
1 1i1
1 111
1 111
111
1 111
fit
1 11!
1 111
! 111
1 111
1 1!1
1 111
1 111
1 111
1 111
111
EKIM
1 111
1 111
1 111
111
_ 1 111
IMI1
1 111
111 ,! 111 1 1 11 1 111 1 1 1' 1 11 1 1 111 of
gyred under my direction or sul ervision in accordance
ierly gathered and evaluated t ie information submitted.
false information, including tt e possibility of fines and
Date
DENR FPRM MFLSF (12/2006)

PLEASE MAID ANNUAL �, ; X.;; ,.r_ _
A COPY OF THIS BL er;u � "PL1CATION FIELD SUMMARY FORM
FORM 1 O BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
Facility Name: Town of Colurribus PLACE A "N/A" IN A BLANK OR BOX
r , . WHEN NOT A pPIrIs hA iD r
�q„a Owner: Frank Smith WQ Permit #: W
00002645 Field #: C1-3 Acres Utilized: 15.8
Operator: Frank Smith Annual Dry Tons Applied: 6.0715
11-2014
Predominant Soil. Series: Site #: C1-3
Pacolet Acres Permitted: 15.8
Crop 1 Name: Fescue Cation Exchange Capacity non 503 .
Vol Crop 1 Max. PAN: 119 g p ( )' ume applied Crop 2 Name:
(enter one) Solids/ o Volume Q. 'd Soil Crop 2 Max. PAN:
Liquid i
Solids
Cu. Yds Gallons
4S,S00 3 2
Applied „e..
Per
Acre
(ory Tons/Ac
0.384
0.000
0.000
0.000
0.000
0.000
esi ual Sources
(1VP17Es #, W #
Q '
Fert., An
Waste, etc)Wet,
WQ0002645
Cond.
(Dry,
Moist)
Precip.
Past 24
Hrs.o
inches
0
'>
b
a �'.
o
�
s
C
c
:v
#
�"
O.S
�
%� �
?�
*
o
0.3
q
TKN o
°u
w•
mg/kg mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of CropType
yp
ReceivingResidual
Application
Crop 1
0.000
Crop 2
Crop 1
Crop 2
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
-0�00-
0.000
0.000
0.000
0.000
0.000
0.000
0 000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0 45500 Residuals Applications totals on FIRM FSF supp ( attach FORM FSF supp to this form):
Prior Years Cumulative lbs/ac 0.000 0.00CrCr0 0.000 0.000 Pb H -
0.000 0.000 0 0 0.000 0 000 0.000 0. 00 0.000 0.000 Lime A lies
Current Cumulative lbs/ac - _
Permitted C. p. L. R **** 0.000 0.000 0.000 Date lbs/ai
AN Limit 1 st/2nd
Permit P 36 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cro 34 1338 NA
P 267
"I certify, under 15 NA 374 89 2498
qualified Ae Penalty of law, that this document
w Prepare un er my direction or supervision in accordance with a system designed to assure that
informationr�onne�F�r y gathered and evaluated the information submitted. I a
including the possibilitym aware that there are significant penalties for submitting false
of fines and imprisonment for knowing violations."
y f _ *Application Method: S - Surface, 1N - Injection, INC - Incorporation
Signature ofLand Applier **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoudinLRate

ANNUAL LAND APPLICATION FIELD SUMMARv Fnuxl
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPf IED O �,
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE
Facility Name: Town of Columbus
WO Permit #: Wnnnn2cec
Field #..
Land Owner: Frank Smith
.Zu"VTR
Annual Dry Tons Applied: 12.1430
C14
Acres Utilized: 9.8
Operator: Frank Smith
Site #: C14
Acres Permitted: 9.8
Predominant Soil Series: Pacolet
Cation Exchange Capacity g p ty (non 503):
Crop 1 Name:
Fescue
Crop 1 Max. PAN: 119
Crop2
Name:
Crop 2 Max. PAN:
Y
Volume applied
Volume
Residual Sources
Soil
Precip.
o
Z
a) t~
(enter one) Solids/ o
/o
Applied per
DES # W
Q''
Cond.
p� 4
C
Nitrate pnu QrYed
Name of CropT e
� `�
Q
Liquid
4 SolidsL(Dry
Acre
Fert., Animal
�rY,
Hrs.
a o
o w
°'
�'
C
11(v
aoc o
and
(lbs/acre)
Receivin g Residual
Cu. Yds GallonsWaste,
Tons/Ac)
etc )
Wet,
o
�*.
o
Nitrite
Application
11-2014
910
Moist )
inches
0
mg/kg
mg/kg
mg/kg Crop 1 Crop 2
Crop 1
crop 2
� 1 1 1 111
1 111
1 111 1 111
1 111 1 111
I oil
_-
�__-
__
r0TALS:1 0 91
Annual lbs/acre
-riur x ears Uumulative lbs/ac
�urrent Cumulative lbs/ac
3ermitted C. P. L. R.****
'ermit PAN Limit 1st/2nd Cj
0.000
0.000
As
0000
E�E�
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
Cd I Cu Cr Pb I Hg Mo I Ni Se I Zn P
0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000
0.000
0.0OA00
00 ,
o.000
0.000
0.000
0.000
0.00o
Lime
0.000
Date
0.000 0.000 0.000
0.000
0.000
0.000
0.000 0.000
NA 374
0.000
89
0.000
2498
36 34 1338 1
NA
267
15
- .. - . . 119
`I certify, under penalty of law, that this document was prepared under my direction or cunervicinn
T--_—-in-accordanc ed-to ure tea
lualiited7ersonnel properly gat ered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility, of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC -Incorporation
i Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0.
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

1 Environmental Testing Solutions, Inc.
Project name: Columbus WWTP
Collection date:
Date received:
1-Oct-14
1-Oct-14
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: (828) 350=9364
Fax: (828) ;;50-9368
Project number: 141001.504
Sample identification: Sludge - Composite _
Sample number:
120683
Parameter
Method
Result
RL
Units
Date
Time
Analyst
Footnotes
Analyzed
Analyzed
Arsenic - TCLP
6010
<0.25
0.25
mg/L
13-Oct.14
MEC
1
]
Barium - TCLP
6010 C
<2.50
2.50
mg/L
13-Oct-14
MEC
1
1
Cadmium -TCLP
6010 C
<0.05
0.05
mg/L
13-O.t.14
MEC
1
1
Chromium - TCLP
6010 C
<0.10
0.10
mg/L
13-Oct-14
MEC
1
1
Lead - TCLP
6010 C
<0.25
0.25
mg/L
13-Oct-14
MEC
1
1
Selenium - TCLP
6010 C
<0.25
0.25
mg/L
13-Oct-14
MEC
1
1
Silver - TCLP
6010 C
<0.10
0.10
mg/L
13-0ct.14
MEC
1
1
Mercury - TCLP
7470A,
<0.0020
0.0020
mg/L
16-Oct-14
DER
1
1
Full Scan TCLP Organics
Seel attached
sheets
1
1,2
Total Solids
SM 2540 G
32000
1000
mg/L
3-0ct-14
1500
LCB
1
Total Volatile Solids.
SM 2540 G
20800
1000
mg/L
3-Oct-14
o:oo
LCB
1
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyed by Rogers & Calcott Environmental.
2. Sample analzyed by Enviro Chemists, Inc.
Date reviewed: 10 - Z2.. 1 —1
Data reviewed by: Kelley�E.. Keenan
Iv Signature:
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

ENVIRONMENTAL
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Dear Client:
Laboratory Report
Project:
Work Order:
Received:
Columbus WWTP
4100140
10/01 /2014 12:40
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of
custody for samples that were received on October 01, 2014. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted, all
analyses performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence
interval for each test method unless otherwise qualified. Estimated uncertainty is available upon request.
Privileged / Confidential information may be contained in this report and is intended only for the use of the addressee. if you are not the addressee, or
the person responsible for delivering to the person addressed, you'lmay not copy or deliver this message to anyone else. If you receive this message by
mistake, please notify Rogers and Callcott immediately.
We strive to provide excellent service to our clients. Please contact Amy Ashley, your Project Manager, at [e-mail] or
(864)-335-4962 if you have any questions about this report.
Report Approved By:
Amy Ashley
Project Manager
This report may not he reproduced, except in fill, without written permission from Rogers 4- Callcott, Inc.
PO Box 5655 1 Greenville, SC 29606 1 426 Faiiforest Way I Greenville, SC 29607 I main 664.232.1556 1 fax [phone] rogersandcallcott.eom
_------ _...— —. an employee -owned company
C Page'' 'of 28

Rogers&Cakott.
ENVIRONMENTAL
Certificate of Analysis
Client Environmental Testing Solutions
Kelley E. Keenan
351 Depot St.
Asheville, NC 28801-4310
Sample Number Sample Description
4100140-01 . Columbus WWTP Sludge
gf�
South Carolina Greenville Laboratory Identification 23105
South Carolina Columbia Laboratory Identification 40572
North Carolina Laboratory Certification Number 27
North Carolina Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
Project: Columbus WWTP
Work Order: 4100140
Received: 10/01/2014 12:40
Matrix Sampled Type
Sludge 10/01/14 09:00 Grab
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforest Way -1 Greenville, 5C 29607 1 main 864.232.1556 1 fax [phone]I40 rogersandcallcott.eom
... ...... ..w.a..,......... ....... an employee -awned company
10121/2014 1 a:29 This report nury not be reproduced, except r'n,fidl, H•ithmrt written pertnissinn.ft•ou, Rogers c& C'allcotl, Inc.
C Page,2'of 26

sr,ENV[RONIIENTAL
ti- --l-f�.�t,
Enviromnental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
Oise Narrative
Total solids and total Volatile solids results are reported in mg/I Fier client request.
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 864.232.1556 i fax [phone] rogersandcallcott.com
..a...__...�,.__._........._._......,�....__._._..___._,,......_�..._�_.__,..._._......_�.;...._.w..._.__....._-wd_.....,._.._.,._......._.,�.,...._.,_.___..._...__.s�.�.......,_...._.._..._..���.e an employee -owned company
10,12112014 14:29 This, report nary not he reproduced, except i.v,jdl, ii•ithaaa written pei•tni.vsinn,fi•oin Rogers & C'allcon, Inc. '
CF?age 3 of 28"

=i ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
Sample Data
Sample Number 4100140-01
Sample Description Columbus WWTP Sludge collected on 10/01/14 09:00
Reporting
Parameter Result Limit Units
Dp'
Analyzed
Method
Flag
Analy;tt
Batch
General Chemistry Parameters
Total Solids
32000
1000
mg/L
1.00
10/03/14 15:00
SM 254OG
LCB
BU0209
Total Volatile Solids
65.0
0.1
%
1.00
10/03/14 15:00
SM 2540G
Z
LCB
B4JO238
TCLP Metals
Mercury
ND
0.0020
mg/L
10.0
10/16/14 11:29
EPA7470A
DER.
B4JO568
Arsenic
ND
0.25
mg/L
5.00
10/13/14 12:14
EPA 6010C
MEC
BU0419
Barium
ND
2.50
mg/L
5.00
10/13/14 12:14
EPA 6010C
MEC
B4JO419
Cadmium
ND
0.05
mg/L
5.00
10/13/14 12:14
EPA 601OC
MEC
1BU0419
Chromium
ND
0.10
mg/L
5.00
10/13/14 12:14
EPA 6010C
MEC
BU0419
Lead
ND
0.25
mg/L
5.00
10/13/14 12:14
EPA 6010C
MEC:
BU0419
Selenium
ND
0.25
mg/L
5.00
10/13/14 12:14
EPA 6010C
MEC:
BU0419
Silver
ND
0.10
mg/L
5.00
10/13/14 12:14
EPA 601OC
MEC
BU0419
TCLP Volatile Organics
Benzene
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBIA'
B4JO528
2-Butanone (MEK)
ND
0.200
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
BU0528
Carbon tetrachloride
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260E
S 1
LBW
B4JO528
Chlorobenzene
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
B4J0528
Chlorofornn
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
BU0528
1,2-Dichloroethane
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
B4JO528
1,4-Dichlorobenzene
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
B4JO528
1,1-Dichloroethene
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBIA'
B430528
Tetrachloroethene
ND
0,100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW'
B4JO528
Trichloroethene
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260B
LBW
BU0528
Vinyl chloride
ND
0.100
mg/L
50.0
10/14/14 18:01
EPA 8260E
LBW
BU0528
Surrogates
%REC
%REC Limits
Flag
1,2-Dichloroethane-D4
109
70-130
Toluene-D8
88
70-130
4-Bromo/Ivorobencene
89
70-130
TCLP Semi -Volatile Organics
2-Methylphenol (o-Cresol)
ND 0.100 mg/L 10.0 10/14/14 21:54 EPA 8270D
RJM B4J0483
3/4-Methylphenol (m,p-Cresol)
ND 0.100 mg/L 10.0 10/14/14 21:54 EPA 8270D
RJM B4J0483
total Cresol
ND 0.200 mg/L 10.0 10/14/14 21:54 EPA 8270D
RJM B4J0483
2,4-Dinitrotoluene
ND 0.100 mg/L 10.0 10/14/14 21:54 EPA 8270D
RJM B4JO483
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 864.232.1556 I fay. 864.232.6140
rogersandcallcott,.com
_..-._m.... - ._--...W_
- an employee -owned company
1012112014 14:29
This report may not be reprodirced, except in.fidl, without written pernvission fiirom Rogers R- C'allcon, Inc.
C , 9 4 01 28

1
ig>. �1i
Rogers& Cakott-
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801.-4310 Reported: 10/21/14 14:29
Sample Number 4100140-01
Sample Description Columbus WWTP Sludge collected on 10/01/14 09:00
Reporting
Parameter Result Limit Units DF Analyzed
TCLP Semi -Volatile Organics
Method Flag Analyst Batch
Hexachlorobenzene
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
Hexachlorobutadiene
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
Hexachloroethane
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
Nitrobenzene
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 9270D
RJM
B4J0483
Pentachlorophenol
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
Pyridine
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
2,4,5-Trichlorophenol
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
2,4,6-Trichlorophenol
ND
0.100
mg/L
10.0
10/14/14 21:54
EPA 8270D
RJM
B4J0483
Surrogates
'UREC
%REC Limits
Flag
Nilrahenzene-D5
77
35-114
2-Fluornhiphenyl
78
43-116
2-Fl:mrophenol
50
21-110
Phenol-D5
34
10-110
2, a, 6-Trihromophenol
101
10-123
Telphenyl-1)14
94
33-141
TCLP Pesticides
Gamma-BHC (Lindane)
ND
0.00050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
B4J0492
Chlordane
ND
0.0050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
B4J0492
Endrin
ND
0.00050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
B4J0492
Heptachlor
ND
0.00050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
134J0492
Heptachlor epoxide
ND
0.00050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RK11
B4J0492
Toxaphene
ND
0.0050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
B4J0492
Methoxychlor
ND
0.00050
mg/L
10.0
10/19/14 04:28
EPA 8081B
RKH
B4J0492
Surrogates
%REC
%REC Limits
Flag
2,4,5,6-Ten•acldoro-m-xylene
80
60-130
Decachlorohiphenyl
77
30-150
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 864,232.1556 1 fax [phone] rogersandcallaatt.com
_ _ W __..._._..._..w _ __._.____, ..__._..._.. ....._ ._.._._.., .._...._._ _...___.._._...._..-_ ........ .__ ......_.. _ _...... ..a . _,.-...._._. n... an employee-owr.ed company
1012112014 1 a:29 This report may not be reproduced, except in,f dl, u•ithmtl written perrnicsion from Rogers & C'allcall, Inc. �_; ,
E.f age 5of 28

Ropes & Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
General Chemistry Parameters
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit _ Units Level Result %REC Limits RPD Limit _ Flag
Batch B4J0209 - General Prep - Solids
Duplicate (B4J0209-DUP1) Source: 4091134-02
Total Solids 12000 1000 mg/L 12000 0 15
Duplicate (B4J0209-DUP2) Source: 4091146-09
Total Solids 720000 1000 mg/L 730000 1 15
Batch B4J0238 - General Prep - Solids
Duplicate (B4J0238-DiJPl) Source: 4091134-02
Total Volatile Solids 33.0 0.1 % 34.0 3 15
PO Box 5655 1 Greenville, SC 29606 1 426 Fairiorest Way,l Greenville, SC 29607 1 inain 864.232.1556 1 fax [phone] rogersandcalle,ott.com
___ �_.. _..._ _...�.......___.m _. _._ ....w .. �.. _ ,_.._..-__�... _.._.W_........._..----- _ _.._ an employee -owned company
1012112014 14:29 This repor7 may not he reproquced, except !n,frdl, without written permission ,from Rogers R Collcott, Inc.
C�Page 6.of 28

Rogers &Cakott
ENV IRONIIENTAIL
Enviromllental Testing Solutions Project: Columbus WWTP
351 Depot St, Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result ' Limit Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0419 - EPA 3005A
Blank (B4J0419-BLK1)
Arsenic
ND
0.05
mg/L
Barium
ND
0.50
mg/L
Cadmium
ND
0.01
mg/L
Chromium
ND
0.02
mg/L
Lead
ND
0.05
mg/L
Selenium
ND
0.05
mg/L
Silver
ND
0.02
mg/L
Blank (B4J0419-BLK2)
Arsenic
ND
0.25
mg/L
Barium
ND
2.50
mg/L
Cadmium
ND
0.05
mg/L
Clironuum
ND
0.10
mg/L
Lead
ND
0.25
mg/L
Selenium
ND
0.25
mg/L
Silver
ND
0.10
mg/L
LCS (B4J0419-BS1)
Arsenic
0.52
0.05
mg/L
0.500
103
80-120
Barium
0.52
0.50
mg/L
0.500
104
80-120
Cadmium
0.52
0.01
mg/L
0.500
104
80-120
Chromium
0.51
0.02
mg/L
0.500
102
80-120
Lead
0.52
0.05
mg/L
0.500
104
80-120
Selenium
0.50
0.05
mg/L
0.500
99
80-120
Silver
0.51
0.02
mg/L
0.500
102
80-120
Matrix Spike (B4J0419-MSl)
Source: 4090965-03
Arsenic
2.67
0.25
mg/L
2.50
ND
105
75-125
Barium
3.62
2.50
mg/L
2.50
ND
99
75-125
Cadmium
2.58
0.05
mg/L
2.50
ND
103
75-125
Chromium
2.47
0.10
mg/L
2.50
ND
98
75.125
Lead
2.51
0.25
mg/L
2.50
ND
101
75-125
Selenium
2.52
0.25
mg/L
2.50
ND
97
75-125
Silver
2.58
0.10
mg/L
2.50
ND
103
75-125
PO Box 5655 I Greenville, SC 29606 1 426 Fairforesc Way 1 Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
.............__.._.._- L_...._........_..._._.. _..__._. __ .-_ .__.._ an emp'Ioyee-owned company
1012112014 14:29 This report mary not he reproduced, except in,idl, without written pertnission,f •ntu Rogers & C'allcnn, Inc.
C�f'age 7 of 28

Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TiCLP Metals
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit _ Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0419 - EPA 3005A
Matrix Spike (B4J0419-MS2)
Source: 4090965-04
Arsenic
2.63
0.25
mg/L
2.50
ND
104
75-125
Barium
2.91
2.50
mg/L
2.50
ND
101
75-125
Cadmium
2.60
0.05
mg/L
2.50
ND
104
75-125
Chromium
2.51
0.10
mg/L
2.50
ND
99
75-125
Lead
2.53
0.25
mg/L
2.50
ND
101
75-125
Selenium
2.53
0.25
mg/L
2.50
ND
99
75-125
Silver
2.63
0.10
mg/L
2.50
ND
105
75-125
Matrix Spike (B4J0419-MS3)
Source: 4090965-05
Arsenic
2.64
0.25
mg/L
2.50
ND
104
75-125
Barium
2.99
2.50
mg/L
2.50
ND
102
75-125
Cadmium
2.58
0.05
mg/L
2.50
ND
103
75-125
Chromium
2.52
0.10
mg/L
2.50
ND
100
75-125
Lead
2.56
0.25
mg/L
2.50
ND
102
75-125
Selenium
2.54
0.25
mg/L
2.50
ND
99
75-125
Silver
2.56
0.10
mg/L
2.50
ND
102
75-125
Matrix Spike (B4J0419-MS4)
Source: 4090965-06
Arsenic
2.74
0.25
mg/L
2.50
ND
109
75-125
Barium
4.74
2.50
mg/L
2.50
ND
105
75-125
Cadmium
2.68
0.05
mg/L
2.50
ND
106
75-125
Chromium
2.57
0.10
mg/L
2.50
ND
103
75-125
Lead
2.62
0.25
mg/L
2,50
ND
104
75-125
Selenium
2.60
0.25
mg/L
2.50
ND
101
75-125
Silver
2.70
0.10
mg/L
2.50
ND
108
75-125
Matrix Spike (B4J0419-MS5)
Source: 4100140-01
Arsenic
2.74
0.25
mg/L
2.50
ND
108
75-125
Barium
3.25
2.50
mg/L
2.50
ND
107
75-125
Cadmium
2.67
0.05
mg/L
2.50
ND
107
75-125
Chromium
2.61
0.10
mg/L
2.50
ND
104
75-125
Lead
2.64
0.25
mg/L
2.50
ND
106
75-125
Selenium
2.60
0.25
mg/L
2.50
ND
101
75-125
Silver
2.66
0.10
mg/L
2.50
ND
107
75-125
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way,1 Greenville, SC 29607 1 main 664.232.1556 1 fax [phone] rogersandcallcott.com
an employee -owned company
1012112014 1.1:29 This report may not he reproduced, except in fill, without written perinission firon: Rogers 8• Callcoll, Inc.
CeF4g"e.8 of 28

Rogers &Calkcott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 _ Reported: 10/21/14 14:29
T(TP Metals
Quality Control Summary _
Reporting Spike Source %REC RPD
Parameter Result ;Limit Units Level Result %REC Limits RPD Limit _Flags
Batch B4J0419 - EPA 3005A
Matrix Spike Dup (B4J0419-MSD1) Source: 4090965-03
Arsenic
2.73
0.25
mg/L
2.50
ND
107
75-125
2
20
Barium
3.69
2.50
mg/L
2.50
ND
102
75-125
2
20
Cadmium
2.65
0.05
mg/L
2.50
ND
106
75-125
3
20
Chromium
2.53
0.10
mg/L
2.50
ND
101
75-125
2
20
Lead
2.58
0.25
mg/L
2.50
ND
103
75-125
2
20
Selenium
2.63
0.25
mg/L
2.50
ND
102
75-125
4
20
Silver
2.66
0.10
mg/L
2.50
ND
106
75-125
3
20
Post Spike (B4J0419-PSI)
Source:4090965-03
Arsenic
2.71
0.25
mg/L
2.50
ND
106
80-120
Barium
3.68
2.50
mg/L
2.50
ND
102
80-120
Cadmium
2.62
0.05
mg/L
2.50
ND
104
80-120
Chromium
2.51
0.10
mg/L
2.50
ND
100
80-120
Lead
2.55
0.25
mg/L
2.50
ND
102
80-120
Selenium
2.60
0.25
mg/L
2.50
ND
101
80-120
Silver
2.63
0.10
mg/L
2.50
ND
105
80-120
Batch B4J0568 - EPA 7470A
Blank (B4J0568-BLKI)
Mercury
ND
0.0002
mg/L
Blank (B4J0568-BLK2)
Mercury
ND
0.0020
mg/L
LCS (B4J0568-BS1)
Mercury
0.0048
0.0002
mg/L
0.00500
95
85-115
LCS (B4J0568-BS2)
Mercury 0.0499 0.0020 mg/L 0.0500 100 85-115
Matrix Spike (B4J0568-MS1) Source: 4090965-03
Mercury 0.0510 0.0020 mg/L 0.0500 ND 102 75-125
PO Box 5655 I Greenville, SC 29606 1 426 Pairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.com
Y�...-a.._.__...._.._..... _..... ....... -.--,...d.---........_...-_--_..an employee -owned company
1012112014 14:29 This report nary not he reproduced, except in,(dl, without written permiscian,fi»n+ Rogers R• Callcon, Inc. Pe p 9 of 28
C��

�.a.* .Rogers.Rogers& Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCL,P Metals
Quality (Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0568 - EPA 7470A
Matrix Spike (B4J0568-MS2) Source: 4090965-04
Mercury
0,0509
0.0020
mg/L
0.0500
ND
102
75-125
Matrix Spike (B4J0568-MS3)
Source: 4090965-05
Mercury
0,0540
0.0020
mg/L
0.0500
ND
108
75-125
Matrix Spike (B4J0568-MS4)
Source: 4090965-06
Mercury
0.0529
0.0020
mg/L
0.0500
ND
106
75-125
Matrix Spike (B4J0568-MS5)
Source: 4100140-01
Mercury
0.0523
0.0020
mg/L
0.0500
ND
105
75-125
Matrix Spike (B4J0568-MS6)
Source: 4100472-01
Mercury
0.0527
0.0020
mg/L
0.0500
ND
105
75-125
Matrix Spike (B4J0568-MS7)
Source: 4100472-02
Mercury
0.0422
0.0020
mg/L
0.0500
ND
84
75-125
Matrix Spike (B4J0568-MS8)
Source: 4100538-01
Mercury
0.0528
0.0020
mg/L
0.0500
ND
106
75-125
Matrix Spike Dup (134J0568-MSDI)
Source: 4090965-03
Mercury
0.0500
0.0020
mg/L
0.0500
ND
100
75-125 2 20
Post Spike (B4J0568-PSI)
Source: 4090965-03
Mercury 3.88 ug/L 4.00 ND 97 80-120
PO Box 5655 I Greenville, SC 29606 1426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 I fax [phone] rogersandcallc:ott,com
�.__....--..-.......W.._....... _. ..-_ _._......_...... ..... ........m..._ ............_ ...,._.... _-... an employee-owned'company
1012112014 14:29 This report inay not he reproduced, except in,f dl, u ithoie written pertnissian.finnt Rogery X C'allcott, Inc.
C 1 age 10 of 28

" ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29 _
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0528 - EPA 5030
Blank (B4J0528-BLK1)
Benzene
ND
0.00200
mg/L
2-Butanone (MEK)
ND
0,00400
mg/L
Carbon tetrachloride
ND
0.00200
mg/L
Chlorobenzene
ND
0,00200
mg/L
Chloroform
ND
0.00200
mg/L
1,2-Dichloroethane
ND
0.00200
mg/L
1,4-Dichlorobenzene
ND
0.00200
mg/L
],I-Dichloroethene
ND
0.00200
mg/L
Tetrachloroethene
ND
0.00200
mg/L
Trichloroethene
ND
0.00200
mg/L
Vinyl chloride
ND
0.00200
mg/L
Surrogate: 1,2-Divhloroethane-D4
102 70-130
Surrogate: Tohtene-D8
87 70-130
Arrogate:4-BrontgJfuo•nhenzene
89 70-130
Blank (B4J0528-BLK2)
Benzene
ND
0,100
mg/L
2-Butanone (MEK)
ND
0.200
mg/L
Carbon tetrachloride
ND
0.100
mg/L
Chlorobenzene
ND
0.100
mg/L
Chloroform
ND
0.100
mg/L
1,2-Dichloroethane
ND
0.100
mg/L
1,4-Dichlorobenzene
ND
0.100
mg/L
1,1-Dichloroethene
ND
0.100
mg/L
Tetrachloroethene
ND
0.100
mg/L
Trichloroethene
ND
0.100
mg/L
Vinyl chloride
ND
0.100
mg/L
Surrogate: 1,2-Dichloroethane-D4
106 70-130
Surrogate: Toluene-D8
89 70-130
Surrogate:4-Brnnm/Irrnrnhenzene
89 70-130
LCS (B4J0528-BSI)
Benzene 0.0214 0.00200 mg/L 0.0200 107 70-130
2-Butanone(MEK) 0.0151 0.00400 mg/L 0.0200 76 60-140
Carbon tetrachloride 0.0252 0.00200 mg/L 0.0200 126 70-130
Chlorobenzene 0.0200 0.00200 mg/L 0.0200 100 70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcallcott.eom
_.._._........._. an employee -owned company
10/21i2011 J /:29 This report nary not he reproduced, except in,it ll, without writren permission,iront Rogers R Callcort, Inc.
C-1'age 1l of 28

Rogers &Cakott
ENVIRONMENTAL
Enviromnental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit - Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0528 - EPA 5030
LCS (B4J0528-BS1)
Chloroform
0.0197
0.00200
mg/L
0.0200
98
70-130
1,2-Dichloroethene
0.0222
0.00200
mg/L
0.0200
ill
70-130
1,4-Dichlorobenzene
0.0189
0.00200
mg/L
0.0200
95
70.130
M-Dichloroethene
0.0211
0.00200
mg/L
0.0200
105
70-130
Tetrachloroethene
0.0232
0,00200
mg/L
0.0200
116
70-130
Trichloroethene
0.0215
0.00200
mg/L
0.0200
107
70-130
Vinyl chloride
0.0233
0.00200
mg/L
0.0200
117
60-140
Surrogate: 1,2-Dichloroethene-D4
119
70-130
Surrogate: Toluene-D8
103
70-130
Surrogate: 4-Branmfluor•obenzene
83
70-130
Matrix Spike (B4J0528-MS1)
Source: 4100472-01
Benzene
1.05 '
0.100
mg/L
1.00
ND
105
70-130
2-Butanone (MEK)
0.758
0.200
mg/L
1.00
ND
76
60-140
Carbon tetrachloride
1.35
0,100
mg/L
1.00
ND
135
70-130 S1
Chlorobenzene
1.00
0.100
mg/L
1.00
ND
100
70-130
Chloroform
1.05
0.100
mg/L
1.00
ND
105
70-130
1,2-Dichloroethane
1.15
0.100
mg/L
1.00
ND
115
70-130
1,4-Dichlorobenzene
0.922
0.100
mg/L
1.00
ND
92
70-130
1,1-Dichloroethene
1.12
0,100
mg/L
1.00
ND
112
70-130
Tetrachloroethene
1.18
0.100
mg/L
1.00
ND
Il8
70-130
Trichloroethene
1.06
0.100
mg/L
1.00
ND
106
70-130
Vinyl chloride
1.23
0.100
mg/L
1.00
ND
123
60-140
Sur•rogate:l,2-Dic•hloraethane-D4
124
70-130
Surrogate: Toluene-D8
104
70-130
Surrogate: 4-Bromq luorobenzene
85
70-130
Matrix Spike (B4J0528-MS2)
Source: 4100472-02
Benzene
1.06
0.100
mg/L
1.00
ND
106
70-130
2-Butanone (MEK)
0.627
0,200
mg/L
1.00
ND
63
60-140
Carbon tetracliloride
1.38
0.100
mg/L
1.00
ND
138
70-130 S 1
Chlorobenzene
1.01
0.100
mg/L
1.00
ND
101
70-130
Chloroform
1.03
0.100
mg/L
1.00
ND
103
70-130
1,2-Dichloroethene
1.11
0.100
mg/L
1.00
ND
Ill
70-130
1,4-Dichlorobenzene
0.909
0.100
mg/L
1.00
ND
91
70-130
M-Dichloroethene
1.13
0.100
mg/L
1.00
ND
113
70-130
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way I Greenville, SC 29607 1 main 864.232.1556 1 fax 864,232.6140 rogersandcallcott.com
o.__.....-....... an employee -owned company
1012112014 14:29 This report may not be reproduced, except nr,f:dl, i+•ithouJ written permission,fr•arn Rogers & Callcolt, Inc.
C Page 12 of 28

.ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP `Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0528 - EPA 5030
Matrix Spike (B4J0528-MS2) Source: 4100472-02
Tetrachloroethene
1.21
0.100
mg/L
1.00
ND
121
70-130
Trichloroethene
1.07
0.100
mg/L
1.00
ND
107
70-130
Vinyl chloride
1.24
0.100
mg/L
1.00
ND
124
60-140
Surrogate:l,l-Dichloroethane-D4
122
70-130
Surrogate: Tohiene-DR
104
70-130
Surrogate: -l-Broninfluorohenzene
86
70-130
Matrix Spike (B4J0528-MS3)
Source: 4090965-03
Benzene
1.11
0.100
mg/L
1.00
ND
111
70-130
2-Butanone (MEK)
0.720
0.200
mg/L
1.00
ND
72
60-140
Carbon tetrachloride
1.37
0.100
mg/L
1.00
ND
137
70-130 51
Chlorobenzene
0.995
0.100
mg/L
1.00
1\110
100
70-130
Chloroform
1.08
0.100
mg/L
1.00
ND
108
70-130
1,2-Dichloroethane
1.19
0.100
mg/L
1.00
ND
119
70-130
IA-Dichlorobenzene
0.895
0.100
mg/L
1.00
ND
90
70-130
1,1-Dichloroethene
1.14
0.100
mg/L
1.00
ND
114
70-130
Tetrachloroethene
1.18
0.100
mg/L
1.00
ND
118
70-130
Trichloroethene
1.09
0.100
mg/L
1.00
ND
109
70-130
Vinyl chloride
1.28
0.100
mg/L
1.00
ND
128
60-140
Surrogate: 1,2-Dichloroethane-N
126
70-130
Surrogate: Toluene-D8
106
70-130
Surrogate: 4-Bromofluorohenzene
82
70-130
Matrix Spike (B4J0528-MS4)
Source: 4090965-04
Benzene
1.03
0.100
mg/L
1.00
ND
103
70-130
2-Butanone (MEK)
0.745
0.200
mg/L
1.00
ND
74
60-140
Carbon tetrachloride
1.33
0.100
mg/L
1.00
ND
133
70-130
S1
Chlorobenzene
0.958
0,100
mg/L
1.00
ND
96
70-130
Chloroform
1.01
0.100
mg/L
1.00
ND
101
70-130
1,2-Dichloroethane
1.10
0.100
mg/L
1.00
ND
110
70-130
1,4-Dichlorobenzene
0.913
0.100
mg/L
1.00
ND
91
70-130
1,1-Dichloroethene
1.09
0.100
nrg/L
1.00
ND
109
70-130
Tetrachloroethene
1,15
0.100
mg/L
1.00
ND
115
70-130
Trichloroethene
1.02
0.100
mg/L
1.00
ND
102
70-130
Vinyl chloride
1.24
0.100
mg/L
1.00
ND
124
60-140
Surrogate: 1,2-Dichloroethane-D4
120
70-130
PO Box 5655 1 Greenville,
SC 29606 1 426 Fait -forest Way
I Greenville,
SC 29607 I
main 864.232.1556
1 fax [phone]
rogersandcal Icott.com
an employee -owned company
1012112014 14:29
This repart may not he reproduced,
except ln,hdl, without written permission front
Rogers & Callcott, Inc.
Page"13 of 28

{g ` Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29 _
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _Flags
Batch B4J0528 - EPA 5030
Matrix Spike (B4J0528-MS4) Source: 4090965-04
Surrogate: Tohmne-D8 100 70-130
Surrogate:4-Bromofluor•ohenzene 82 70-130
Matrix Spike (B4J0528-MS5) Source: 4090965-05
Benzene
1.08
0.100
mg/L
1.00
ND
108
70-130
2-Butanone (MEK)
0.725
0.200
mg/L
1.00
ND
72
60-140
Carbon tetrachloride
1.31
0.100
mg/L
1.00
ND
131
70-130 Si
Chlorobenzene
0.962
0.100
mg/L
1.00
ND
96
70-130
Chloroform
1.06
0.100
mg/L
1.00
ND
106
70-130
1,2-Dichloroethane
1.19
0.100
mg/L
1.00
ND
119
70-130
1,4-Dichlorobenzene
0.872
0.100
mg/L
1.00
ND
87
70-130
1,1-Dichloroethene
1.10
0.100
mg/L
1.00
ND
110
70-130
Tetrachloroethene
1.15
0.100
mg/L
1.00
ND
115
70-130
Trichloroethene
1.04
0.100
mg/L
1.00
ND
104
70-130
Vinyl chloride
1.41
0.100
mg/L
1.00
ND
141
60-140 _ Si
Surrogate: 1,2-Dichloroethane-D4
126
70-130
Surrogate: Toluene-D8
103
70-130
Surrogate:4-BronuJluor•ohenzene
83
70-130
Matrix Spike (B4J0528-MS6)
Source: 4090965-06
Benzene
1.08
0,100
mg/L
1.00
ND
108
70-130
2-Butanone (MEK)
0.705
0,200
mg/L
1.00
ND
70
60-140
Carbon tetrachloride
1.34
0.100
mg/L
1.00
ND
134
70-130 Si
Chlorobenzene
0.982
0.100
mg/L
1.00
ND
98
70-130
Chloroform
1.06
0.100
mg/L
1.00
ND
106
70-130
1,2-Dichloroethane
1.16
0.100
mg/L
1,00
ND
116
70-13D
1,4-Dichlorobenzene
0.902
0.100
mg/L
1.00
ND
90
70-130
1,1-Dichloroethene
1.11
0.100
mg/L
1.00
ND
ill
70-130
Tetrachloroethene
1.20
0.100
mg/L
1.00
ND
120
70-130
Trichloroethene
1.03
0.100
mg/L
1.00
ND
103
70-130
Vinyl chloride
1.32
0.100
mg/L
1.00
ND
132
60-140
Surrogate:l,2-Diehloroelhane-Da
125
70-130
Surrogcae: Toluene-1)8
107
70-130
Surrogate: 4-BromoJluornhenzene
85
70-130
PO Box 5655 I Greenville, SC 29606 1 426 Fairforest Way i Greenville, SC 29607 1 main 864.232.1556 1 fax 864.232,6140 rogersandcallcott.eom
._`....... _-.......... _.e .._ .m. r ... M. an employee-otwned company
10121.2014 14:29 This report/ may not be reproduced, except in,lidl, s+•ithorAwritten permission,j•om Rogenc R• C erllcort, Inc•.
C�Paigi3 14 of 28

Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Volatile Organics
Quality Control Summary
Reporting Spike Source °/REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0528 - EPA 5030
Matrix Spike (B4J0528-MS7) Source: 4100140-01
Benzene
1.07
0.100
mg/L
1.00
ND
107
70-130
2-Butanone (MEK)
0.728
0.200
mg/L
1.00
ND
73
60-140
Carbon tetrachloride
1.36
0.100
mg/L
1.00
ND
136
70-130
Sl
Chlorobenzene
0.998
0.100
mg/L
1.00
ND
100
70-130
Chloroform
1.04
0.100
mg/L
1.00
ND
104
70-130
1,2-Dichloroethane
1.15
0.100
mg/L
1.00
ND
115
70-130
1,4-Dichlorobenzene
0.882
0.100
mg/L
1.00
ND
88
70-130
1,1-Dichloroethene
1.12
0.100
nrg/L
1.00
ND
112
70-130
Tetrachloroethene
1.19
0.100
mg/L
1.00
ND
119
70-130
Trichlor•oethene
1.03
0.100
mg/L
1.00
ND
103
70-130
Vinyl chloride
1.30
0.100
mg/L
1.00
ND
130
60-140
Surrogate: 1,2-Dichlor•oethane-D4
722
70-130
Surrogate: Toluene-D8
105
70-130
Surrogcae: 4-Bronrofluorobenzenc
84
70-130
Matrix Spike Dup (B4J0528-MSDI) Source: 4100472-01
Benzene
0.993
0.100
mg/L
1.00
ND
99
70-130
5
20
2-Butanone (h4EK)
0.775
0.200
mg/L
1.00
ND
78
60-140
2
20
Carbon tetrachloride
1.24
0.100
mg/L
1.00
ND
124
70-130
8
20
Chlorobenzene
0.928
0.100
mg/L
1.00
ND
93
70-130
8
20
Chloroform
0.982
0.100
mg/L
1.00
ND
98
70-130
7
20
1,2-Dichloroethane
1.11
0.100
mg/L
1.00
ND
111
70.130
3
20
1,4-Dichlorobenzene
0.876
0.100
mg/L
1.00
ND
88
70-130
5
20
l,l-Dichloroethene
1.03
0.100
mg/L
1.00
ND
103
70-130
8
20
Tehachloroethene
1.07
0.100
mg/L
1.00
ND
107
70-130
10
20
Trichloroethene
0.964
0.100
mg/L
1.00
ND
96
70-130
9
20
Vinyl chloride
1.12
0.100
mg/L
1.00
ND
112
60-140
10
20
Surrogate: 1, 2-Dichloroethane-L)d
Surrogate: Toluene-D8
Surrogate: 4-Br•oma Jl uor•ob enzen e
119 70-130
96 70-130
79 70-130
PO Box 5655 : Greenville, SC 29606 1 426 FalrforesC Way I Greenville, SC 29607 1 rnain 864.232.1556 1 fax 864.232,6140 rogersandcallcott.com
............... _.... ......_.u... _. -_..� an employee -owned company
10:21/2014 14:29 This report )nrry not he reproduced, except uv,Jid1, u•ithonr written petinissi(,n,T•onr kagenc & C'er lcott, Inc.
C -Page 15 7 28

III Rogers &Cakott
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RFD
Parameter Result Limit — Units Level Result %REC Limits RPD Limit — Flags
Batch B4J0483 - EPA 3510C - GCMS
Blank (B4J0483-BLKI)
2-Methylphenol (o-Cresol)
ND
0.0100
mg/L
3/4-Methylphenol (ni,p-Cresol)
ND
0.0100
mg/L
total Cresol
ND
0.0200
mg/L
2,4-Dinitrotoluene
ND
0.0100
mg/L
Hexachlorobenzene
ND
0.0100
mg/L_
Hexachlorobutadiene
ND
0.0100
mg/L
Hexachloroethane
ND
0.0100
mg/L
Nitrobenzene
ND
0.0100
mg/L
Pentachlorophenol
ND
0.0100
mg/L
Pyridine
ND
0.0100
mg/L
2,4,5-Trichlorophenol
ND
0.0100
mg/L
2,4,6-Trichlorophenol
ND
0.0100
mg/L
Surrogate: Nilrohar_ena-D5
61
35-114
Surrogate: 2-Fluorohiphenyl
64
43-116
Surrogate: 2-Fluorophenol
39
21-110
Surrogate: Phenol-D5
29
10-1/0
Surrogate: 2, 4, 6-Tribronmphenol
84
10-123
Surrogate: Terphenyl-D14
47
33-141
Blank (B4J0483-BLK2)
2-Methylphenol (o-Cresol)
ND
0.100
mg/L
3/4-Methylphenol (m,p-Cresol)
ND
0.100
mg/L
total Cresol
ND
0.200
mg/L
2,4-Dinitrotoluene
ND
0.100
mg/L
Hexachlorobenzene
ND
0.100
mg/L
Hexachlorobutadiene
ND
0.100
mg/L
Hexachloroethane
ND
0.100
mg/L
Nitrobenzene
ND
0.100
mg/L
Pentachlorophenol
ND
0.100
mg/L
Pyridine
ND
0.100
mg/L
2,4,5-Trichlorophenol
ND
0.100
mg/L
2,4,6-Trichlorophenol
ND
0.100
mg/L
Surrogate: Nitrobenzene-D5
62
35-114
Surogate: 2-Fluo robiphenyl
69
43-116
Surrogate: 2-Fluorophenal
46
21-110
Surrogate: Phenol-I)5
31
10-170
PO Box 5655 1 Greenville, 5C 29606 1 426 Fairforesc Way I Greenville, 5C 29607 1 main 664.232.1556 1 fax [phone] rogersandcallcott.com
..._m_,.......___..._........ ..,.....__........_......_.._.....-__._...._ an employee -owned company
1012112014 14:29 This report may nat be reproduced, eccept igjdl, without written permission,jrom Rogers K C'allcort, Inc.
Page 16 of 28

i
Rogers &Cakott
t.x:.
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Semi -Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit _ Flags]
Batch B4J0483 - EPA 3510C - GCMS
Blank (B4J0483-BLK2)
Surrogate: 2, 4, 6-Tribromophenol 93 10-123
Surrogate: Tet77heny1-D14 74 33-141
LCS (B4J0483-BS])
2-Methylphenol (o-Cresol)
0.509
0,100
mg/L
0.800
64
50-90
3/4-Methylphenol (m,p-Cresol)
1.04
0.100
rig/L
1.60
65
42-92
2,4-Dinitrotoluene
0.614
0.100
mg/L
0.800
77
65-104
Hexachlorobenzene
0,713
0.100
mg/L
0.800
89
72-116
Hexachlorobutadiene
0.399
0.100
mg/L
0.800
50
39-100
Hexachloroethane
0.386
0.100
mg/L
0.800
48
36-99
Nitrobenzene
0.427
0.100
mg/L
0.800
53
51-108
Pentachlorophenol
0.695
0.100
mg/L
0.800
87
49-111
Pyridine
0.329
0.100
mg/L
0.800
41
23-67
2,4,5-Trichlorophenol
0.595
0.100
mg/L
0.800
74
56-112
2,4,6-Trichlorophenol
0.540
0.100
mg/L
0.800
67
55-113
Surrogate: Nitrobanzene-D5
59
35-114
Surrogate: 2-Fluorobiphenyl
63
43-116
Surrogate: 2-Flunrophenol
42
21-110
Surrogate: Phenol-D5
31
10-170
Surrogate: 2, 4, 6-Tribrotnophenol
92
10-123
Surrogate: Teuphenyl-D14
95
33-141
LCS (B4J0483-BS2)
2-Methylphenol (o-Cresol)
0.599
0.100
mg/L
0.800
75
50-90
3/4-Methylphenol (m,p-Cresol)
1.18
0.100
mg/L
1,60
74
42-92
2,4-Dinitrotoluene
0.690
0.100
mg/L
0.800
86
65-104
Hexachlorobenzene
0.761
0.100
mg/L
0.800
95
72-116
Hexachlorobutadiene
0.573
0.100,
mg/L
0.800
72
39-100
Hexachloroethane
0.580
0.100
mg/L
0.800
72
36-99
Nitrobenzene
0.583
0,100
mg/L
0.800
73
51-108
Pentachlorophenol
0.777
0.100
mg/L
0.800
97
49-111
Pyridine
0.286
0.100
mg/L
0.800
36
23-67
2,4,5-Trichlorophenol
0.716
0.100
mg/L
0.800
90
56-112
2,4,6-Trichlorophenol
0.654
0.100
mg/L
0.800
82
55-113
Surrogate: Nitrobenzene-D5
Surrogate: 2-Atorobiphenyl
82 35-114
82 43-116
PO Box 5655 1 Greenville, SC 29606 1 426 Faiiforest Way I Greenville, SC 29607 1 main 864,232.1556 1 fax [phone] rogersandcallcott.com
.._...___-..._._._v_....... ...... _-....._.._.,__ ._ __ ._ ._.- an employee -owned company
1012112014 14:29 This repon may not be reproduced, except in.f dl, without wrinen peruuission,fi nun Rogers & C'allcoll, Inc.
[Page 17 of 28

,Ij Rogers akott,
ENV IRONf IENTAI_
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 j Reported: 10/21/14 14:29
i
TCLP Senli-Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit units Level Result %REC Limits RPD Limit _ Flag:�
i
Batch B4J0483 - EPA 3510C - GCMS
LCS (B4J0483-BS2)
Surrogate: 2.Flumrophenol
49
21-110
Surrogate: Phenol-D5
34
10-110
Surrogate: 2, 4, 6-Trihrornophenol
102
10-123
Surrogate: Terphenyl-1)14
80
33-141
Matrix Spike (B4J0483-MSI)
Source: 4090965-03
2-Methylphe.nol(o-Cresol)
0,570
0.100
mg/L
0.800
ND
71
35-100
3/4-Methylphenol (m,p-Cresol)
1.12
0.100
mg/L
1.60
ND
70
30-97
2,4-Dinitrotoluene
0.714
0.100
mg/L
0.800
ND
89
60-109
Hexachlorobenzene
0.766
0.100
mg/L
0.800
ND
96
68-114
Hexachlorobutadiene
0.608
0.100
mg/L
0.800
ND
76
35-101
Hexachloroethane
0.613
0.100
mg/L
0.800
ND
77
37-93
Nitrobenzene
0.602
0.100
mg/L
0.800
ND
75
40-112
Pentachlorophenol
0.806
0.100
mg/L
0.800
ND
101
44-120
Pyridine
0.259
0.100
mg/L
0.800
ND
32
14-68
2,4,5-Trichlorophenol
0.709
0.100
mg/L
0.800
ND
89
30-132
2,4,6-Trichlorophenol
0.662
0.100
mg/L
0.800
ND
83
40-123
Surrogate: Nitrohen-ene-D5
82
35-114
Svrrogate:2-Fluorobiphenyl
85
43-116
Surrogate: 2-Fluorophenol
49
21-110
Surrogate: Phenol-D5
34
10-110
Surrogate: 2,4, 6-Trihhlmophenol
102
10-123
Surrogate: Terphenyl-D14
77
33-141
Matrix Spike (B4J0483-MS2)
Source: 4090965-04
2-Methylphenol (o-Cresol)
0.547
0.100
mg/L
0.800
ND
68
35-100
3/4-Methylphenol (m,p-Cresol)
1.05
0.100
mg/L
1.60
ND
66
30-97
2,4-Dinitrotoluene
0.658
0.100
mg/L
0.800
ND
82
60-109
Hexachlorobenzene
0.733
0.100
mg/L
0.800
ND
92
68-114
Hexachlorobutadiene
0.543
0.100
mg/L
0.800
ND
68
35-101
Hexachloroethane
0.516
0.100
mg/L
0.800
ND
65
37-93
Nitrobenzene
0.557
0.100
mg/L
0.800
ND
70
40-112
Pentachlorophenol
0.738
0,100
mg/L
0.800
ND
92
44.120
Pyridine
0.321
0.100
mg/L
0.800
ND
40
14-68
2,4,5-Trichlorophenol
0.675
0.100
mg/L
0,800
ND
84
30-132
2,4,6-Trichlorophenol
0.626
0.100
mg/L
0.800
ND
78
40-123
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforesc Way 11 Greenville, SC 29607 1 main 864.232,1556 [fax [phone] rogersandcallcott.com
.r�.......,._...._........_.__...,-__,_�.._.,-..............__......._....._.._.___.___._..._..._...�..._�......._..._..__.._.._.._,__._...,.._..__....._..�_._......._...._.m_,��__.._.......,.._.e......__._. an employee-rnvned company
1012112014 M: 29 This repor7 may not he reproduced, except m fill, without written permission, f rant Rogers &- C.'allcou, Inc.
C�Fage 8 of 28

Rogers & Cakotl
ENVIKONMENTA
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Serni-Volatile Organics
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B4J0483 - EPA 3510C - GCMS
Matrix Spike (B4J0483-MS2) Source: 4090965-04
Matrix Spike (B4J0483-MS3)
Surrogate: Nitrobenzene-D5
Surrogate:2-Fhrorohiphenyl
Surrogate: 2-Fhrorophenol
Surrogate: Phenol-D5
Surrogate: 2,4, 6-Tribromophenol
Surrogate: Terphenvl-D14
Source: 4090965-05
77
80
45
31
96
70
35-114
43-116
21-110
10-110
10-123
33-141
2-Methylphenol(o-Cresol)
0.626
0.100
mg/L
0.800
ND
78
35.100
3/4-Methylphenol (m,p-Cresol)
1.18
0.100
mg/L
1.60
ND
73
30-97
2,4-Dinitrotoluene
0.702
0.100
mg/L
0.800
ND
88
60-109
Hexachlorobenzene
0.769
0.10D
mg/L
0.800
ND
96
68-114
Hexachlorobutadiene
0.676
0.100
mg/L
0.800
ND
84
35.101
Hexachloroethane
0.689
0.100
mg/L
0.800
ND
86
37-93
Nitrobenzene
0.646
0.100
mg/L
0.800
ND
81
40-112
Pentachlorophenol
0.798
0.100
mg/L
0.800
ND
100
44-120
Pyridine
0.252
0.100
mg/L
0.800
ND
32
14-68
2,4,5-Triehlorophenol
0.718
0.100
mg/L
0.800
ND
90
30-132
2,4,6-Trichlorophenol
0.676
0.100
mg/L
0.800
ND
85
40-123
Surrogate: Nitrobenzene-D5
90
35-114
Surrogate:2-Fltmrobiphenyl
86
43-116
Surrogate:2-Fhmrophenol
56
21-110
Surrogate: Phenol-1)5
37
10-110
Surrogate: 2,4,6-Tribromophenol
103
10-123
Surrogate: Terphenvl-D14
94
33-14I
Matrix Spike (B4J0483-MS4)
Source: 4090965-06
2-Methylphenol (o-Cresol)
0.451
3/4-Methylphenol (m,p-Cresol)
0.882
2,4-Dinitrotoluene
0.525
Hexachlorobenzene
0.576
Hexachlorobutadiene
0.496
Hexachloroethane
0.511
Nitrobenzene
0.532
Pentachlorophenol
0.608
Pyridine
0.214
2,4,5-Trichlorophenol
0.553
ter. -.. rcrr i ( ___.,m ce- )acna I d1L G , r ant.,.,
0.100
mg/L
0.800
ND
56
35-100
0.100
mg/L
1.60
ND
55
30-97
0.100
mg/L
0.800
ND
66
60-109
0.100
mg/L
0.800
ND
72
68-114
0.100
mg/L
0.800
ND
62
35-101
0,100
mg/L
0.800
ND
64
37-93
0.100
mg/L
0.800
ND
66
40-112
0.100
mg/L
0.800
ND
76
44-120
0.100
mg/L
0.800
ND
27
14-68
0.100
mg/L,
0.800
ND
69
30-132
1 Greenville,
SC 29607
1 main 864.232.1556
1 fax
864.232.6140'
rogersandcallcott.com
an employee -owned company
1012112014 14:29 This report may not be
!need, except in fill, without written permission,irnm Rogers & Callcott, Inc.
C Page '19 of 28

Rogers &Cakott 1:.
t> ENV IRONMENTAI
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TF-LP Semi -Volatile Organics
Quality 1"ontrol Summary
22eporting - Spike Source %REC RPD -
Parameter Result I Limit Units Level Result %REC Limits RPD Limit Flag!
Batch B4J0483 - EPA 3510C - GCMS
Matrix Spike (B4J0483-MS4) Source: 4090965-06
2,4,6-Trichlorophenol
0.521
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fl uorob tph enyl
Surrogate: 2-Fl uoraphen of
Surrogate: Phenol-D5
Surrogate: 2,4, 6-Tribrrrnrophenol
Surrogate: Twphenrl-D14
Matrix Spike (B4J0483-MS5)
Source: 4100140-01
2-Methylphenol (o-Cresol)
0.620
3/4-Methylphenol (m,p-Cresol)
1.23
2,4-Dinitrotohuene
0.708
Hexachlorobenzene
0.763
Hexachlorobutadiene
0.657
Hexachloroethane,
0.672
Nitrobenzene
0.638
Pentachlorophenol
0,828
Pyridine
0.173
2,4,5-Trichlorophenol
0.743
2,4,6-Trichlorophenol
0.697
Surrogate: Nitrobenzene-D5
Surrogate: 2-Fluorobiphenyl
Surrogate: 2-Fhroroph onol
Surrogate: Phenol-D5
Surrogate: 2,4, 6-Tribronrophenol
Surrogate: Twphenl4-D14
Matrix Spike Dup (B4J0483-MSDI) Source: 4090965-03
2-Methylphenol (o-Cresol)
0.556
3/4-Methylphenol (m,p-Cresol)
1.10
2,4-Dinitrotoluene
0.665
Hexachlorobenzene
0.763
Hexachlorobutadiene
0.526
Hexachloroethane
0.509
Nitrobenzene
0.544
Pentachlorophenol
0.760
Pyridine
0.300
PO Box 5655 1 Greenville, SC 29606 1 426 Fah forest Way
1012112014 14:29 This report may not he reprou
0.100
mg/L
0.800
ND
65
40.123
89
35-114
84
43-116
50
21-110
35
10-110
97
10-123
79
33-141
0.100
mg/L
0.800
ND
77
35-100
0.100
mg/L
1.60
ND
77
30-97
0.100
mg/L
0.800
ND
89
60-109
0.100
mg/L
0.800
ND
95
68-114
0.100
mg/L
0.800
ND
82
35-101
0.100
mg/L
0.800
ND
84
37-93
0.100
mg/L
0.800
ND
80
40-112
0.100
mg/L
0.800
ND
103
44-120
0.100
mg/L
0.800
ND
22
14-68
0.100
mg/L
0.800
ND
93
30-132
0,100
mg/L
0.800
ND
87
40-123
88
35-114
84
43-116
55
21-110
38
10-110
102
10-123
103
33-141
0.100
mg/L
0.800
ND
70
35-100
2
30
0.100
mg/L
1.60
ND
68
30-97
2
30
0.100
mg/L
0.800
ND
83
60-109
7
30
0,100
mg/L
0.800
ND
95
68-114
0.4
30
0.100
mg/L
0.800
ND
66
35-101
14
45
0.100
mg/L
0.800
ND
64
37-93
19
45
0.100
mg/L
0.800
ND
68
40.112
10
30
0.100
mg/L
0.800
ND
95
44-120
6
30
0.100
mg/L
0.800
ND
37
14-68
15
30
I Greenville,
SC 29607
1 main 864.232.1556
I fax [phone]
rogersandcaiicott.com
an employee -owned company
'need, eroept in
fill, ll, without
wi-iffen pernrtscirar,j-onr Rogers & Callcou, Inc.
C Page 20 of 28

'A .. Rogers &Cakott
di'.Ttr_i -1't; ENV[ R0NMENTA
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Semi -Volatile Organics
Quality (Control Summary
Ieporting
Spike
Source
%REC
RPD
Parameter Result
Limit Units
Level
Result
%REC
Limits RPD
Limit
_ Flags
Batch B4J0483 - EPA 3510C - GCMS
Matrix Spike Dup (B4J0483-MSD1) Source: 4090965-03
2,4,5-Trichlorophenol 0.673
0.100 mg/L
0.800
ND
84
30-132 5
30
2,416-Trichlorophenol 0.632
0.100 mg/L
0.800
ND
79
40-123 5
30
Surrogate: Nin•obenz-ene-D5
74
35-114
Surrogate:2-Fluorobiphenyl
78
43-116
S'urrogate:2-Fluorophcnol
46
21-110
Surrogate: Phenol-D5
34
1U-110
Surrogate: 2,4.6-Tribromophenol
99
1 U-123
Swwogate: Terphenvl-DI4
91
33-141
PO Box 5655 i Greenville, SC 29606 1 426 Fairforesc Way I Greenville, SC 29607 1 main 864.232.1556 ! fax [phone] rogersandcallcotticom
........... an _. ... _.,.._... .. _. _.. _..._..._.._ _._._ an employee -owned company
1012112014 14:29 This report may not be reprod+ cent, except in•fdl, ithont written pern».esinn,fr on+ Rogers• d C'aJlcott, Inc.
�P.�g621 of 28

Rogers & Cakot
Ifi`-r1--rtf r=� INVIKONMENTAL
Environmental Testing Solutions
Project:
Columbus WWTP
351 Depot St.
Work Order:
4100140
Asheville, NC 28801-4310
Reported:
10/21/14 14:29
TCLP Pesticides
Quality Control Summary
Reporting
Spike Source
%REC RPD
Parameter Result
Limit -
Units
Level Result
%REC
Limits RPD Limit
_ 'Flags
Batch BV0492 - EPA 3510C - GC
Blank (B4J0492-BLK1)
Gamma-BHC (Lindane) ND
0.000050
mg/L
Chlordane ND
0.00050
mg/L
Endrin ND
0.000050
mg/L
Heptachlor ND
0.000050
mg/L
Heptachlor epoxide ND
0.000050
mg/L
Toxaphene ND
0.00050
mg/L
Methoxychlor ND
0.000050
mg/L
Surrogate:2,4,S,GTenachlan-m:rrle
e
78
60-130
Surrogate: Decachlorobiphem4
55
30-150
Blank (B4J0492-BLK2)
Gamma-BHC (Lindane) ND
0.00050
mg/L
Chlordane ND
0.0050
mg/L
Endrin ND
0.00050
mg/L
Heptachlor ND
0.00050
mg/L
Heptachlor epoxide ND
0.00050
mg/L
Toxaphene ND
0.0050
mg/L
Methoxychlor ND
0.00050
mg/L
Surrogate: 2,4,5,6-Tetrachla•o-nt-xrlet
e
82
60-130
Surrogate: Decachlorobiphetryl
96
30-150
LCS (B4J0492-BSI)
Gamma-BHC (Lindane) 0.0034
0.00050
mg/L
0.00400
84
70-130
Endrin 0.0040
0.00050
mg/L
0.00400
100
70-130
Heptachlor 0,0034
0.00050
mg/L
0.00400
86
70-130
Heptachlorepoxide 0.0035
0.00050
mg/L
0.00400
87
70-130
Methoxychlor 0.0040
).00050
mg/L
0.00400
99
70-130
Surrogate:2,a,5,6-7'etiachlot•o-nr:rrlene
80
60-130
Surrogate: Decachlorobiphen),I
91
30-150
Matrix Spike (B4J0492-MSl) Source: 4100140-01
Gamma-BHC (Lindane) 0.0035
.00050
mg/L
0.00400 ND
88
60.140
Endrin 0.0043
.00050
mg/L
0.00400 ND
109
60-140
Heptachlor 0.0036
00050
mg/L
0.00400 ND
90
60-140
Heptachlor epoxide 0.0036
.00050
mg/L
0.00400 ND
90
60-140
Methoxychlor 0.0042
.00050
mg/L
0.00400 ND
106
60-140
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way II Greenville, SC 29607 1 main 864.232.1556 1 fax [phone] rogersandcailcott.com
_�............-._.._........ _. ._ . _ _. ._ _- _.- .�.. _.,..-._ � _ ._ -_... .._._.._,__. an employee -owned cgmpany
1012112014 14:29 This report nary not he reprodiced, except in,jdl, N•ithout written pernvission,l•om Rogers & Callcon, Inc. '
CPage 22 of 28

Rogers akot�
ENVIRONMENTAL
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 2880 1 -43 10 Reported: 10/21/14 14:29
TCLP Pesticides
Quality Control Summary
Reporting
Spike
Source
%REC
RPD
Parameter Result
Limit
Units
Level
Result
%REC
Limits
RPD
Limit
Flags
Batch B4J0492 - EPA 3510C - GC
Matrix Spike (B4J0492-MSI) Source: 4100140-01
Surrogate: 2,4,5,6-Ten•achloro-m x'vic
a
86
60-130
Surrogate: Decochlorobiphenyl
81
30-150
Matrix Spike Dup (B4J0492-MSD1) Source: 4100140-01
Gamma-BHC (Lindane) 0.0035
0.00050
mg/L
0.00400
ND
88
60-140
0.6
20
Endrin 0.0043
0.00050
mg/L
0.00400
ND
108
60-140
0.8
20
Heptachlor 0.0036
0.00050
mg/L
0.00400
ND
91
60-140
0.4
20
Heptachlor epoxide 0.0036
0,00050
mg/L
0.00400
ND
91
60-140
0.7
20
Methoxychlor 0.0042
0.00050
mg/L
0.00400
ND
105
60-140
0.9
20
Surrogate; 2, 1,5,6-Termchlarn-nr-.rrler
e
87
60-130
Surrogate: Decachlorobiphenvl
82
30-150
PO Box 5655 1 Greenville, SC 29606 1 426 Fairforest Way�I Greenville, SC 296D7 I main 864.232,1556 I fax 864.232,6140 rogersandcalleott.eom
...... —� _......_..._.�a- _..�. _.._ _.. _ ..�...-.-. > �.. _...., ompany
1012112014 14:29 This• report may not he repro aced, except in fill, u•ithotrr written permis•.cion,fi•ou Rogers & Callcon, Inc.
C Page 23'of 28

ENV IRONMENTA
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
TCLP Bottle Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result Limit _ Units Level Result %REC Limits RPD Limit _ Flags
Batch B4J0384 - EPA 1311
Blank (B4J0384-BLKl)
TCLP Bottle Extraction Complete
Blank (B4J0384-BLK2)
TCLP Bottle Extraction Complete
PO Box 5655 I Greenville, SC 29606 1426 Faiiforesc Way Greenville, SC 29607 1 main 864.232.1556 I fax 864.232,6140 rogersandcallcott.com
_ __ __._._...-_.._ .�.....,._.._ .... __m... ..._ _.. __....� .. _.. .__........ _.. .... .. an employee -owned cbmpany
10121,12014 I4:29 This report may not he reprod iced, except ruff ill, withma written permiscion,Ji•am Rogers R C'allcan, Inc.
C Pale 24 of 28

iiu;' iFra. Rogers & Cako�
yr *411
l ENVIRONMEN'1
Enviromnental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28 801-43 10 Reported: 10/21/14 14:29
TCI..P ZHE Extraction
Quality Control Summary
Reporting Spike Source %REC RPD
Parameter Result I Limit Units Level Result v/ REC Limits RPD Limit Flags
Batch B4J0151 - EPA 1311 - ZHE
Blank (B4J0151-BLKI)
TCLP ZHE Extraction
Complete
Sample Preparation Data
Parameter
Batch
Sample 1D Prepared
Analyst
EPA 300.5A ICP Digestion
EPA 3005A
B4J0419
4100140-01 10/10/2014 09:51
MEC
EPA 3510 Extraction
EPA 3510C - GC
B4J0492
4100140-01 10/13/2014 14:00
DBB
EPA 3510 Extraction
EPA 3510C - GCMS
B4J0483
4100140-01 10/13/2014 08:15
DBB
EPA 7470A Mercury Digestion
EPA 7470A
B4J0568
4100140-01 10/15/2014 11:58
DER
TCLP Extraction Data
Extraction Initial Final
Parameter
Batch S
mple ID_ Started Finished
Fluid # pH pH
EPA 1311 - TCLP Extraction
EPA 1311
EPA 1311- TCLP ZHE
EPA 1311 - ZHE
134.10384 4100140-01 10/6/14 at 1635 10/7/14 at 1210
B4J0151 41Q0140-01 10/2/14 at 1500 10/3/14 at 0935
PO Box 5655 1 Greenville, SC 29606 1 426 FairforescWay
1012112014 14:29 This report nny not he
1 7.13 5.04
I N/A N/A
Greenville, SC 29607 1 main 864.232,1556 1 fax [phone] rogersandcallcotb.com
an employee -owned company
iced, except in,jdl, H,ithonhvi itten permission,f•ani Rogem & C'allcon, Inc.
CPage 25 of 28

Rogers &Cakot
ENVIRONMENTA
Environmental Testing Solutions Project: Columbus WWTP
351 Depot St. Work Order: 4100140
Asheville, NC 28801-4310 Reported: 10/21/14 14:29
Qualifiers and Definitions
ND Analyte NOT DETECTED at or above the reporting limit
NR Not reported
RPD Relative Percent Difference
S 1 The matrix spike and / or the matrix spike duplicate ample recovery was not within control limits due to matrix interference. The
Laboratory Control Sample (LCS) was within contro limits.
Z The total volatile solids result is 20800 mg/l based o calculation
PO Box 5655 1 Greenville, 5C 29606 1426 Fairforesc Way I Greenville, SC 29607 1 main 864,232.1556 1 fax [phone] rogersandcallcott.00171
.__ _....._..__.._... .__._.._ �._. ....._..._........ ..._._......_.__._. ._ ._. ..__......__._.......__..__ -_ an employee -owned company
M21/2011 14:29 This report nary not he reproduced, except in,8dl, withmn written permi.esinn,j orn Rngerc C'allcott, Inc.
C'�26 of 28

r' U A 1 1 Y1 r— r=-rri i-%% i rCOKU r� .-.
�-nmiyr t.U'� i vUr RtWORK ORDER
E Ili V i R© Ill M E N TA L
I
I
I
I
I
Filtered (Yes)
Cooled es _o)
MailingPO Box Shipping
Aping 426 Fairforest Way 2156 Stoneridge Drive
Container Type Llastic/ SS)
Address: Greenville, SC 29606 Address: Greenville, SC 29607 Columbia, 5C 29210
Phone [phone] Fax [phone] Phone [phone]
-
Container Volume L) J �lA.ilq
Client Name
Sample Type ab/ mposite)
Address
Sample Source (WW, GW, DW, 5W S, Other)
d
C
ReportTo:
o
Preservation Code(s)
Email Address �1
0
4
A —None E—HCI I—ZnAcetate
B—HNO3 F—Na2.5z03 J—H3PO4
Telephone#
j
C—HZSO4 G—Boric Acid K-MCAA
PO # Project #
z
>_
D—NaOH H—Ascorbic Acid L-
R&C
YR_
WORK ORDER
DATE
TIME
SAMPLE DESCRIPTION
COMMENTS
'
(0a jq
00x
�c
00 161thfap
SAM�— RELINQUISHED BY:
DATE/TIME:
RECEIVED BY:
DATE/TIME:
1 S
Z• ��
�O,D1 1�
Composite Start. Date: .
Composite Start Time:
RELINQUISHED BY:
DATE/TIME:
RE
I v A E IME:
3.
10.01•Ify
4.
6 17��
I/ 41
Time or Flow (Circle one) Initials:
RELINQUISHED BY:
DATE/TIME:
RECEIVED
D TE/TIME:
5
6. A)
Temperature of blank or representative sample
At time of collection10 °C
RELINQUISHED BY:
DATE/TIME:
RECEIVED BY:
DATE/TIME:
7.
8•
At time of lab receipt V °C
Possible Hazards associated with samples: Non -Hazard Flammable ❑Skin Irritant 0 Poison Unknown [Dxher Form Revised July, 2014 Page of

1 ` Rogers & Callc�tt
ENVIRONMENT TAL
Client: I ,
Carrier Name: lie FedEx
Tracking Number:
Sample Receipt Verification
Date � Work �, n
Received: I , ` Order: I -�
UPS US Mail Courier Field Services Other:
Receipt Criteria
y
e
s
o
A
Comments
Shipping container / cooler intact?
Damaged Leaking Other:
Custody seals intact?
COC included with samples?
COC signed when relinquished and received?
Sample bottles intact?
Damaged Leaking Other:
Sample ID on COC agree with label on bottle(s),?
Date / time on COC agree with label on bottle(s�?
Number of bottles on COC agrees with number
of bottles received?
Samples received within holding time?
Sample volume sufficient for analysis?
VOA vials free of headspace (<6mm bubble)?
Samples Cooled? Temp at receipt recorded on CCC
Temp measured with IR thermometer
- SN: 97050067
ce Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH
Note: Samples for metals analysis may be preserved upori
receipt in the lab.
Samples dechlorinated for parameters requiring
the time of sample collection?
hlorine removal at
If in-house preservation used — record Lot #
HCL H,PO4
H,SO4 NaOH
HNO, Other
Comments:
Were non-conformance issues noted at srle receipt? Yes or {� o
Non -Conformance issue other than noted above:
Revised July 2014
Completed by:
r�,
Cagei28,of 28

,�enviroehem"'
SM
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Testing Solutions, Inc.
Post Office Box 7565
Asheville . NC 28802
Attention: Kelley Keenan (ETS)
Environmental Chemists, Inc,,
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Date of Report: Oct 21, 2014
Customer PO #:
Customer ID: 08100055
Report #: 2014-12230
Project ID: Columbus WWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by T
14-30016 Site: Sludge 10/1/2014 9.-00 AM Solid/Sludge Client
Test Method Results Date Analyzec
2,4, 5-TP SW846 Method 8151A <0.003 mg/L 10/16/2014
2,4-D SW846 Method 8151A <0.003 mg/L 10/15/2014
Comment:
Reviewed by:
Report #:: 2014-12230
Page 1 of

Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
CHAIN-OF-CU,gTODV / Analytical
Client Name: -
Address:
Report to:
Phone:
PO Number:
Fax:
Requested Anaivses
pHCheckedUpon Receipt
CI, < 02 mgn Upon Receipt
a
Preservatives
0
0
E
Q Sample Identification o
y
m
R _ y
N
o
0
rnI
w
W
A"
o zOz
F" x
0 v3
Z
\
Meld
x
lcmp. (°C) Comments
L•ty
Z
ZiN
I
-
I
r
Temperature (°C}
Received on Ice:
Y / N
Sealed Cooler:
Samples Intact:
A nel'Coin nts:me-and
Sampler Na Signature
,
Printed
of S - pler.
ate
__�
Signature of Sampler.

N a
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name:
Project Number:
CHAIN -OF -CUSTODY / Analytical Request
Client Name: P �;a !-fp1-'L 9tid�y�c r�s�
Address: 15 �iI-1fz G" F
Report to:
Phone: L'ar Pax:
PO Number:
Requested Anal ses
pH Checked Upon Receipt
- l - C1, < O.2 mg/1 i lnnn Rereint
Preservatives
Sample Identification
`'
E
3 a
a
z
�
�e
U���
+(
>
A
it�
(z
x
p
v�
1�\ Field
ti w
H
x
x
z
z
Temp. (°C) Comments
-
r}
D
-
Temperature (C)
M.(�
• I a
��1 �3
[9
��,
/0-01 /'8
Received on Ice:
/ N
Sealed Cooler:
YY IJN
Samples Intact:
/Y 1 N
Additional Comments:
a/ 0,. 1 ` : o a 1W1,112MM® ,
Printed Name of Sampler:
Signature of Sampler:

Facility Name: Town of Columbus
WWTP Name: Town of Columbus
"ruviknz.i nuies)
WQ Permit Number: WQ0002645
NPnFC Numho.•.
ivionitoritng Fertod: From _ 1/l/2014�
Pathogen Reduction (15A NCAC 02T .1106) -Plea
Class A: Alt. A (time/temp) Al B
AID (No Prior Test) 0
If applicable to alternative performed. (Class A onl ) in
Compost: CAI Heat Drying 0 )t
Beta Ray 13 Gamma Ray 0
_Class Alt. (1) Fecal Density ® Alt. (2;
If applicable to alternative performed (Class B onl3) in,
Lime Stabilization K IAir Dlvill0 Cl
Anaerobic Digestion
If applicable to alternative performed (Class A or
Parameter Allowable Level _ Pat of
in Sludge Minimuix Geo. E
2 x 10 to the MPN
6th power
per gram of Fecal Coliform total solids CFU
1000 mpn per gram
of total solid (dry
weight) _
Salmonella bacteria 3 MPN per 4 grams
(in lieu of fecal I total solid (dry
_Vector Attraction Reduction (15A NCAC 02T . 107) -
_Alt 1 (VS reduction) ® Alt. 2 (40-day bench)
_Alt. 5 (14-Day Aerobic) [] Alt. 6 (Alk. Stabilizatio 9T
Alt. 9 (Injection) ® Alt. 10 (Incorporation) (� r
CERTIFIiCATION STATEMENT (please chec the al
"I certify, under penalty of law, that the pat[
vector attraction reduction requireme t in 1!
--i cerruy, under penalty of law, that t e p
vector attraction reduction requirement in
if you check this statement: attach an a Wa
"This determination has been made under my
designed to ensure that qualified personnel pry
that the pathogen and vector attraction reducl
significant penalties for false certification inch
epa.rer Name and Title (type or print)
Signature of Preparer* D
*Preparer is defined in 40 CFR Part 503.9(r) and 15A
To 12/31/2014
idicate level achieved and a ternative performed:
Treatment) ® Alt. C rior Testing) El
Process to Further Reduce Pathogengs 0
to "Process to Further Reduc Pathogens":
Treatment 0 1 Tl ertnophilic
'ss to Significantly Reduce athogens
"Process to Significantly Re luce Pathogens
Composting ® 12 erobic Digestion Cl
B) complete the following monitoring data:
{3, um er o yt
lst Emcee- Frequency Sample a "
Kim E
off Analysis Type Tech-
dences
lease indicate alternative
3 (30-day bench) R
7 (Drying - Stable)
vector attraction reduction al
ropriate statement)
;en requirements in 15A ;
NCAC 02T .1107 have b
gen requirements in 15A
NCAC 02T .1107 have n
in why you have not met
'ormed:
4 (Spec. 02 uptake) El
8 (Drying - Unstable) [j
hives were performed
W 02T .1106 and the
met."
_AC 02T .1106 and the
been met." (Please note
e or both of the
and supervision in accordance with the system
her and evaluate the infor ation used to determine
,ements have been met. I am aware that there are
and imprisonment."
Dennis Key Southern Soil Builders, Inc.
►d Applier Name and Title (i applicable)(type or print)
nature of Land Applier (if ap licable) Date
1102 (26)
DENR FORM PVRF 02T (12/2006)

Report Number: 14-342-0606
Account Number: 46381
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER NC 28669
I
SOIL ANALYSIS REPORT Analytical Methodis):
Date Of Analysis: 12/09/2014 Date Of Report: 12/09/2014 Mehlich 3
Organic Matter Phosphorus Potassium Magnesium Calclum Sodium pH ;id C.E.0
% Rate ENR Mehlich'3 Reserve K Mg Ca Na Soil Buffer
Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate m RatePp ppm Rate pH Index meq/100g
4.5 M 128 146 VH 108 M 236 H 860 M 19 VLNC = 122 NC = 55 5.8 6.77 8.2
07032 4.0 M 118 148 VH 99 M 252 VH 846 M 21 VL
NC=123 NC=51 5.9 6.79 1.4 8.1
Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Sotuble_S
Alt im
° ° °a °a ° NO3N S Zn Mn Fe Cu B SS Cl AI
�° �0 �O �° �° ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm
Date Received: 12/08/2014
Sample ID Lab
Field ID Number
C1-3
07031
C1-4
Sample ID
l9eld ID
C1-3
C1-4
3.1 1 25.9 1 52.2 1 1.1 1 17.1
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
(fix A A&L E_astern Laboratories
� L
7621 Whitepme Road Richmond, Virginia 23237 [phone] Fax (804) 271.WS r
wwwaleastem.com
Grower: Submitted By: ZACH KEY
SOUTHERN SOIL BUILDERS Farm ID:
NC = 37 I NC = 137.5 1 NC = 156
--]
18 M 5.3 H 25 H 204
NC = 37 NC = 132.5 1 NC = 156
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g
(milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble
Salts ms/cm x 640 = ppm.
NC = 240.0
VH 4.7 VH 10.4 L
NC = 235.0
This report applies to sample(s) tested. Samples are retained a
maximum of thirty days after testing.
Analysis prepared by: A&L Eastern Laboratories, Inc.
by: fpy/ie me 100.-r
Pauric McGroary