HomeMy WebLinkAboutWQ0002431_Residual Annual Report 2014_201502192014 ANNUAL REPORT
HUFFMAN FINISHING COMPANY
LAND APPLICATION PROGRAM
. PERMIT #WQ0002431
Prepared For:
Huffinan Finishing Company
P.O. Box 170
Granite Falls North Carolina 28630
Prepared By:
Branch Residuals & Soils, LLC
8646 W. Market Street — Suite.111
Greensboro, North Carolina 27409
February 2015
RECEIVE®
FEB 19 2015
1N,NAM ® NP 1 "ROCESSING
UNIT
BRANCH RESIDUALS & SOILS, LLC .
8646 W. Market St. — Suite 111 • Greensboro, NC 27409
PHONE (336) 510-0340 a Fax (336) 510-0341
February 15, 2015
North Carolina Department of Environment and Natural Resources
Division of Water Resources - Land Application Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2014 LAND APPLICATION ANNUAL REPORT
Huffinan Finishing Company
Permit No. WQ0002431
Branch Residuals & Soils Project No. 2014-115
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in
the referenced permit on behalf of the Huffman Finishing Company. This report includes: 1)
Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field
Loading Summary Form, 4) Annual Land Application Field Summary Form, 5) Residual
Analysis Lab Sheet, 6) TCLP Lab Sheets, 7) Annual Pathogen & Vector Attraction Form, 8)
Annual Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2014
Application Summary Table, and 11) 2014 Application Condition Summary.
Applications 77,000 gallons (16.54 dry tons) were made to one field (6.6 acres) in 2014. This
has been the first application in several years. Current permit does not require vector attraction
to be performed only pathogen reduction.
If any further information is required regarding this land application program, please do not
hesitate to contact meat (336) 510-0340.
Sincerely,
Robert T. Branch, L.S.S.
Land-Application/Residuals Operator
#15676
RTB
Enclosures
TABLE OF CONTENTS
SECTION NO. TITLE
I
Certification Form
II
Annual Residual Sampling Summary Form
III
Annual Metals Field Loading Summary Form
IV
Annual Land Application Field Summary Form
V
Residual Analysis Lab Sheets
VI
Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII
Annual Pathogen and Vector Attraction Reduction
Form
VIII
Annual Pathogen and Vector Attraction Reduction
Documentation
IX
Soil Analysis Report
X
2014 Application Summary Table
XI
2014 Application Condition Summary
CERTIFICATION FORM
11
ANNUAL LAND APPLICATION CERTIFICAT ON FORM
WQ Permit##: WQ0002431 County: Caldwell Year: 2014
Facility Name (as shown on permit): Huffman Finishing Company
Land Application Operator: Southern Solutions Environmental Phone: 336-753-1256
Land application of residuals as allowed by the permit occurred during the past calendar year's
® Yes ® No - If No, skip Part A, and Part E and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Miplication Summary:
Total number of a lication fields in the ermit: 4
Total number of fields utilized for land application during the year: 1
Total amount of dry tons applied during the year for all application sites: 16.54
Total number of acres utilizes for land application during the year: 6.6
Part 13 - Annual Comnniauce Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes L3 No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective
action taken.
1) Only residuals approved for this permit were applied to the permitted sites.
_ 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three
(3) copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
�— 7) All general requirements in as specified in the Land Application Permit were complied with (applicable -to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
( authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as.
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
n certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
j j 2-ti-Zo1S
i Mr. Lee T. Huffman, Huffman Finishing Treasurer
Signature of PerNttee Date
Mb 2/3/15
Signature of Preparer* (if
Signature o Land Appli
Date
+, (if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26)
DENR FORM ACF (12/2006)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0002431 Laboratory: 1) A & L Eastern Ag Labs
Facility Name: Huffman Finishing Company 2)
Residual Source WQ # or NCO025135 3)
NPDES #: 4)
WWTP Name: HuffinanTinishing WWTP 5)
---------- ------ --- —
Parameter
(mg/kg)
-----
Ceiling
Cone.
Limit
Sample -or Composite Date
10/t/2014
Percent Solids (%)
NA
5.15
Arsenic
75
7.00
Cadmium
85
<2.00
Copper
4,300
640.00
Chromium
NA
0.00
Lead
840
18.00
Mercury
57
1.20
Molybdenum
75
<5.00
Nickel
420
40.00
Selenium
100
<5.00
Zinc
7,500
745.00
Total Phosphorus
NA
5,870
TKN
NA
81,700
Ammonia -Nitrogen
NA
5,050
Nitrate and Nitrite
NA
<2.00
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the mdividual pernut for metals emirs.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties
for sr Tb*ttin=,ding the possibility of fines and imprisonment for knowing violations."
1,doi5
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
r DENR FORM RSSF (12/2006)
ANNUAL METALS FIELD LOADING SUMMARY FORM
ANNUAL METALS FIELD LOADING SUMMARY FORM
I
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Huffman Finishing Company Total Dry Tons applied (Annual): 16.54
Permit #: WQ0002431 Cation Exchange Capacity (non 503 only): n/a
Operator: Lee Huffman Owner: Lee Huffman Predominant Soil Series FaB2
Acres Used: 6.6 Acres Permitted: 6.6 Site #: Huffman Field #: 2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
XW1Y-L/0-VLVL
Sample
or Com-
10/1/14
posite
Date
% Solids
5.15
Arsenic
7.00
Cadmium
2.00
Chromium
0.00
Copper
640.00
Lead
18.00
Mercury
1.20
Molyb-
5.00
denum
Nickel
40.00
Selenium
5.00
Zinc
745.00
Total
Phos-
5,870
honus
A -- .-1 11-- Mn+.mil INAJA T .na.linac WRIV1112ted in lbs/acrel:
� O
0
a
2.51
a
Arsenic
0.04
0.04
Cadmium
0.01
0.01
Chromium
0.00
0.00
Copper
3.21
3.21
Lead
0.09
0.09
Mercury
0.01
0.01
Molyb-
0.03
0.03
denum
0.20
Nickel
0.20
Selenium
0.03
-0.03
Zinc
3.73
3.73
Total
Phos-
29.41
29.41
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of flues and imprisonment for knowing violations"
wwpt* 2/3/15
Signature of Land Applier Date
Author Daryl D. Merritt DENR FORM MFLSF (7/2002)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DT/ACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As —
Arsenic
Cd —
Cadmium
Cr —
Chromium
Cu —
Copper
Pb —
Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn —
Zinc
Nutrients (lbs/ac)
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.
ANNUAL LAND APPLICATION FIELD SUNEWARY FORM
PLEASE MADE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTEDTFOR EACH APPLICATION FIELD.
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
FacWty Name: Huffman Finishing Company WQ Permit#: WQ0002431 Field #• Huffman Acres Utilized: 6.60
Owner: Lae Huflinan Annual Dry Tom Applied: 16.54 Site #: 2 Acres Permitted: 6.60
Operator: Lee Huffman Predominat Soil Series FaB2 Cation Exchange Capacity (non 503): NA
Crop 1 Namc Fescue Crop 1 Mat PAN: 194.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A
129A
Today
PerApe
% Solids
Volume
A Mod
ADeciftwcre
/A
Re &dual Sourom
(NPDES #, WQdt,
FerL,AnftW Wrote,
etc.)
Site
��
Wet,
moist)
Pracip
Past 24
Hra.
$
g
�+° �s
� �
TKN
� dt
9
�
N.it W
and
Nitrite
PAN Applied
(lbs/acre)
MU3t Se1Cd
Crop I or Crop 2
Gai.
t_1
C .Yd.
Repot
Totals
in Gal.
Crop I.
Crop 2
Crop I
Crop 2
Nov-14
77,000
11,667
5.15
151
HuftmMIM WWTP
S
0.50
0.30
81,700
5,050
2
127.89
X
T®PALS: 11,667
Annual lbs/acxe.
Current Cumulative lWacre
Prior'Years Cumulative lbs/acro
Perm:tte&C. P. L R.**es
As Cd Cr Cu Pb H MO Ni 3e 7�t P PAN 1 PAN 2
0.04 0.01 0.00 321 0.09 0.01 1 0.03 0.20 0.03 3.73 29.41 127.89 0.00
0.10 0.06 NA 10.55 035 0.02 1 NA 1 0.62 1 0.09 1 30.86
0.06 0.05 NA 7.34 0.26 1 0.01 LNL4 0.42 0.06 27.12
36 34 NA 1,338 267 15 NA 374 89 2,498
] 94.00
dun 'th oleos
Lime A Lied
Date lbs,'ac
Permit PAN Lmut 1 s02nd Crop
"I cerft, gaoler penalty of law, that this -document was prepared under my direcwo or supery"ioa.ia actor ce wa a ay
wed to acme that qualified -personnel properly pthered and evaluated the information submitted. I am &ware that there fire
front peaaidea for im bmitting false information, indudiug the possibliity of Bees and imprisonment for lmowing violOolm"
Signature of Laud Applier
*Application Method: S - Surface, IN - Injeetioai, INC - Incorporation
**VolitiliztttWn Rate: Suffice - OA Igieetlon/Incorporation -1.0
***Mineralization Rates: Compost - 0.1, Aanaerobically Digested - 0.2,
Date Aerobically Digested - 0J, Raw Sludge - 0.4
****C.P.LJL-. Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)
RESIDUAL ANALYSIS LAB SHEETS
Page: 1 of 2
Report Number: 14-276-0202
Account Number: 46368
Submitted By: BOB BRANCH
Send To: BRANCH RESIDUALS & SOILS LLC
BOB BRANCH
8646 West Market Street
Suite 111
GREENSBORO , NC 27409
Lab Number: 57925
Sample Id: HUFFMAN MILLS
NRL, A&L Easters Laboratories, Inca
7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-6446
wiwwjleastern.com
Project: HUFFMAN MILLS
NC CERT#257
REPORT OF ANALYSIS
Date Sampled:
Date Received: 10/03/2014 00:00
Date Reported: 10/08/2014
Total Solids *
5.15
51500
100.0
JM
10/03/2014 14:30
SM-2540G
Moisture'
94.85
100.0
JM
10/03/201414:30
SM-254OG
Total Kieldahl Nitrogen
8.17
81700
10.0
JM
10/06/2014 08:30
SM-4500-NH3C-TKN
Total Phosphorus
0.59
5870
100
KM
10/06/2014 11:30
SW 6010C
Total Potassium
0.08
813
100
KM
10/06/2014 11:30
SW 6010C
Total Calcium
0.41
4050
100
KM
10/06/2014 11:30
SW 6010C
Total Magnesium
0.19
1,940
100
KM
10/06/2014 11:30
SW 6010C
Total Sodium
0.57
5680
100
KM
10/06/2014 11:30
SW 6010C
Total Iron
13300
100
KM
10/06/2014 11:30
SW 6010C
Total Aluminum
3300
100
KM
10/06/2014 11:30
SW 6010C
Total Copper
640
5
KM
10/06/2014 11:30
SW 6010C
Total Zinc
745
5
KM
10/06/2014 11:30
SW 6010C
Ammonia Nitrogen
0.51
5050
10.0
JM
10/06/2014 08:30
SM-4500-NH3C
Organic N
7.66
76650
10.0
10/06/2014 08:30
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
10/06/2014 08:30
SM-450ONO3F
Total Cadmium
<2.0
2.0
KM
10/06/2014 11:30
SW 6010C
Total Nickel
40
5
KM
10/06/2014 11:30
SW 6010C
Total Lead
18
5
KM
10/06/2014 11:30
SW 6010C
All values are on a dry weight basis.except as noted by asterisk. Detection limit on all N series
is on a wet basis.
9�/w
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced
in whole or part may
any reference be made
(N9nor
to the work, the results, or the company in any advertising, news release, or other
public announcements without obtaining our prior written authorization.
Debbie Holt
! — J
Page: 2 of 2
Report Number: 14-276-0202
Account Number: 46368
Submitted By: BOB BRANCH
Send To: BRANCH RESIDUALS & SOILS LLC
BOB BRANCH
8646 West Market Street
Suite 111
GREENSBORO , NC 27409
Lab Number: 57925
Sample Id: HUFFMAN MILLS
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23231 (604) 743-Mi Fax (604) 271.6446
wn
Project: HUFFMAN MILLS
NC CERT#257
REPORT OF ANALYSIS
Date Sampled:
Date Received: 10/03/2014 00:00
Date Reported: 10/08/2014
Total Arsenic
7.0
3.0
KM
10/06/2014 11:30
SW 6010C
Total Mercury
1.2
0.4
KM
10/07/2014 14:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
10/06/2014 11:30
SW 6010C
pH (Standard Units) " 6.56
2.00
JM
10/06/2014 08:30
SW-9045D
Total Volatile Solids 84.02
840200
100.0
JM
10/03/2014 14:30
SM-2540G
Total Molybdenum
<5
5
KM
10/06/2014 11:30
SW 6010C
Comments:
ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "NO3/NO2-N".
THE MATRIX SPIKE
WAS OUT OF LIMITS FOR
"Se". THE MSD WAS OUT OF LIMITS
FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
l�NINIa�INlll��llIl�4
=2014
BRANCHRESWAL-SA 5O1L5'LLC Id:W*--28
HU,FRAN MILLS
Regular Nutrient and Metal Residuals Analysis
Arsenic
IAead-
Nickel-
Aluminum
% Total Solids -
Potassium
Calcium! --
iron -
Bob Brancb
Bmeh Residuals kSoils
336 51 M340
Bill Brawl) Residuals & Soils
Cadmium
mercuq -
Selenium -.
Ammonia -Nitrogen
pH
Magnesium -
pr6ject: Huffolgil Mills
Pfoj.cut No- 2014-115
ups jayqvLI'/,oSqqS�4"5n
C,ppper,-
Molybdeftum, -
Zinc -
Nitrate -Nitrite NitrogeP -
IPIIOphorus -
volatile Solids -
Sodium -
c
Facility:
Huffman Finishing Company WWTP
Source:
Huffman Mills WWTP
Location:
Granite Falls, North Carolina
Contractor:
Southern Solutions Environmental
Type of Analysis:
Testile Industrial
Report No:
HF14-276-0202
Date Sampled:
10/1/2014
Date Reported:
10/8/2014
Reporting Period:
Annual 2014
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
S' 15:
Nitrogen (TKN)
8.170
81,700.000
Phosphorus
; `.a5$7 ,`_
5,870.000
Potassium
:0.0$1'
813.000
Sulfur
=
0.000
Calcium
0.41O `
4,100.000
Magnesium
: '"0:.1'90
1,900.000
Sodium
5,700.000
Iron
---
1.3,300000:,
Aluminum
---
330,0.000
Manganese
---
"
Copper
---
64a00E0 :
1,500
Zinc
---
745000
2,800
Ammonia Nitrogen
."0.505
5,050.000
Nitrate N / Nitrite N
---
. 2:00Q .
Cadmium
---
,^ =ZOOfJ
, � �'».._�.
39.
Chromium
---
1,200
Nickel
---
=%�fJmOQO
420
Lead
---
111,$000
300
Arsenic
---
7000
41
Mercury
---
l':200.
17
Selenium -
---
�,,,�-.."":.. =-:;�. S.nOOU
100
pH
G560
Calcium Carbonate Eq.
Organic Nitrogen
7.665
Molybdenum
---
6:000,
75
Chloride
---
Boron
Available P205
Specific Gravity
8.340
Testile Industrial
Huffman Mills WWTP
Granite Falls, North Carolina
Southern Solutions Environmental
Annual 2014
Date Reported: 10/8/2014 Report No: HF14-276-0202
Note All Units in Pounds Per Dry Ton
Macro Nutrients
PAN Surf.
51.044
PAN Inj.
56.094
P
11.740
K
1.626
Lime
0.000
Secondary Nutrients
Calcium
8.200
Magnesium
3.800
Sodium
11.400
SAR
4.173
Chloride
0.000
Iron
26.600
Alumium
6.600
Manganese
0.000
Boron
0.000
Sulfur
0.000
Residual Nitrogen Calculation
Year Min Rate PAN #/Acre
Physical Characteristics
% Solids 5.15
pH 6.560
Min Rate 0.300
Metals
Arsenic
0.014
Cadmium
0.004
Chromium
0.000
Copper
1.280
Lead
0.036
Mercury
0.002
Molybdenum
0.010
Nickel
0.080
Seleniun
0.010
Zinc
1.490
2010
2011
2012
2013
2014
0.30
45.99
2015
0.15
16.10
2016
0.08
6.84
2017
0.04
3.16
2018
2019
2020
TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT
- RESEARC[t & Ar4ALyTICAL
c � LAbORATORiES, 'NC.
Analytical/Process Consultations
Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Granite Falls
l,k Branch Residuals & Solls Protect. collected 01 October 2014) _
GF WWTP GF WTP
EPA HW Quantitation Results its Results Characteristic
Number Contaminant umit(ard" (MULL (ma/L) Level(mf: LJ EPA Method
L TCLP METALS
I}004
Arsenic
0.010
SOL
SOL
BOL
5.00
6010C
D-005
Barium
0.040
0.067
0.054
0.096
100
6010C
D-006
Cadmium
0.005
`0.010
BQL
BOL
BOL
1.00
6010C
D-077
Chromium
BQL
0.034
0.031
5.00
6010C
' D.002
Lead
0.005
BOL
BQL
0.012
5.00
6010C
D-009
Mercury
0.0020
BQL
SOL
BQL
0.200
7470A
D410
Selenium
0.100
BQL
SQL
BQL
1.00
6010C
D-011
Silver
0.010
BQL
SOL
SOL
5.00
6010C
II. TCLP VOLATILES
D-018
Benzene
0.050
BOL
139L
BQL
0.500
8260E
D-019
Carbon Tetrachloride
0.050
BQL
BQL
BQL
0.500
6260B
D-021
Chlorobeneene
0.030
BQL
BQL
SOL
100
8260E
D-022
ChlorofOrnt.
0.500
BQL
BQL
SOL
6.00
8260E
D-028
1.2-Dichloroethane
0.050
BQL
BQL
SOL
0.500
8260E
D-029
1.1-Dichlomethylene
0.050
BQL
BOL
SOL
0300
8260B
D-035
Methyl Ethyl Ketone
0.500
BQL
SOL
BQL
200
8260B
D-039
Tetrachloroethylene
0.050
BQL
BQL
SOL
0.700
8260B
D-040
Trichloroethylene
0.050
SOL
BQL
BOL
0.500
6260E
D-043
Vinyl Chloride
0.050
BOL
BOL
SOL
0.200
8260E
-� TCLP SEMI-VOLATILES
D.023
0-0e0301
20.0
BQL
SOL
BQL
200
9270D
D-024
M-Creosol
20.0
BQL
SOL
SQL
200
8270D
D-025
104moso1
20.0
BQL
BQL
SOL
200
8270D
D-026
Creoml
20.0
SQL
BOL
BQL
200
8270D
D-027
1,4.Didd robem.
0.750
SOL
SOL
BQL
7.50
8270D
D-030
2,4-Dirutrotoluene
0.050
BQL
BOL
SOL
0.130
8270D
'
D.032
Hexacb1orobenaene
0.050
BOL
ROL
SOL
0.130
8270D
D-033
Hexachlorobutediene
0.050
SOL
SOL
SOL
0.500
8270D
D-034
Hexnchlomedume
0.300
BOL
SOL
BOL
3.00
8270D
D-036
Nitrobenzene
0.200
BQL
SOL
BQL
2.00
8270D
_
D-037
Pentadmomphenol -
10.0
BQL
SOL
BQL
100
8270D
D-039
Pyridine
0.500
BOL
SOL
BOL
5.00
8270D
D-041
44,5-Trichlorophenol
40.0
SOL
SOL
SOL
400
8270D
D-042
2.4.6-Tticidorephmol
0.200
BQL
SOL
BQL
2.00
8270D
V. TCLP PESTICIDF.SIHERBICHIES
D-020
Chlwdme
0.003
SOL
SOL
SOL
0.030
80918
D-016
2Aa
1.000
BQL
SOL
SOL
10.0
8151 A
D-012
Endrin
0.002
BOL
ROL
SOL
0.020
8081 B
D-031
Heptachlor
0.0008
BQL
BQL
BQL
0.008
8081 B
D-013
Lindmte
0.040
BOL
SOL
ROL
0.400
8081 B
D-014
Medwxychlor
1.000
BQL
SOL
SOL
10.0
8081 B
D-015
Toxaphene
0.050
BQL
BQL
SOL
0.500
9081 B
D-017
2.4.5-TP(Silvex)
0.100
BQL
BQL
BQL
1.00
8151 A
REACrIVITV
D-003
Cyanide
2.0
BQL
BQL
BQL
9010
D-003
Sulfide
10.0
SOL
SOL
BOL
9030
VI. CORROSIVITY
D-002
PH
Std. Units
11.1
6.11
5.71
9045
qj. TCLP MISCELLANEOUS
Paint Filter Test
_
FLP
FLP
FLP
_ /mIGNITABIL TY
D-001
lwdtability
> 1401
> 1400
> 140"
1010
Sample Number
796122
796123
796124
Sample Date
10/01/14
10/01/14
10/01/14
Sample Time (hrs)
1200
1330
1430
--'
Sample Matrix
Solid
Solid
Solid
�I SQL - Below Quantitation Limits WNl a Will Not Ignite
mg/L a milligram per Liter - parts per million (ppm) mgft - milligrams per kilogram o pans per million (ppm)
'ElRESEAR8i & ANAlyfiCAI
LkoMTOMES, INC.
Analytical / Process Consultations
Phone 1338) 998-2841
CHAIN OF CUSTODY RECORD
WATER I WASTEWATER I misc.
•
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ONE
11.11
MARKS:
SAMPLE TEMPERATURE AT RECEIPT --J,-1 11C
LINQUISHED BY
RELl
ANNUAL PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORM
PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION FORM
The Huffinan Finishing Company met pathogen reduction through fecal coliform sampling. This
permit is not required to have vector attraction reduction options. The annual certification form is
marked accordingly to reflect the methods of meeting pathogen reduction.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
4I Facility Name: Huffinan Finishing Company WQ Permit Number:
WWTP Name: Huffman Finishing WWTP NPDES Number:
Monitoring Period: From l/l/2014 To 12/31/2014
Fi
i
Pathogen Reduction (15A NCAC 02T .1106
Class A: Alt. A (time/temp) ❑
:::.......................................
A1t.D o Prior Test) ❑
If applicable to alternative performed (Class A
Compost ❑ 1 Heat Drying ❑
Beta Ray ❑ 1 Gamma Ray ❑
WQ0002431
NCO025135
- Please indicate level achieved and alternative perfori
Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑
Process to Further Reduce Pathogengs ❑
only) indicate "Process to Further Reduce Pathogens":
Beat Treatment ❑ Thermophilic ❑
Pasteurization ❑ _ ..
Class B: TAlt. (1) Fecal Density 21 1 Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑
Ana
erobic Digestion
tion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter Allowable Level Pathogen Density Excee Frequency Sample Analytical Tech -
in in Sludge Geo. Mean Maxi Units of Analysis Type
nioue
2 x 10 to the MPN
6th power
per gram of r!lCFU/ SM20
Fecal Coliform total solids CFU 54,369 69,275 120,388 Gram 0 Annually Grab 9222D
1000 mpn per gram
of total solid (dry
Imonella bacteria 3 MPN per 4 grams
(in lieu of fecal I total solid (dry
cT__4 ♦u-...ti.... In-A....4:..— /MCA N!`Ae' 111 r Vln n - Uidinan indid-atop alitpruntivP 11PrfnrR1P.(1_
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate szaxemcnz)
® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
M. Shuford Wise, Huffman Finishing WWTP ORC
Pre arer Name and itle ( e or print) Land Applier Name and Title (if applicable)(type or print)
X . Aa- U" _- Ulu"
Signature of Preparer* Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
nFNR FORM PVRF 02T (12/2006)
ANNUAL PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The Huffman Finishing Company met pathogen reduction through fecal coliform sampling. This
permit is not required to have vector attraction reduction options. The annual certification form is
marked accordingly to reflect the methods of meeting pathogen reduction. Documentation of the
fecal coliform sampling data is attached.
Huffman Finishing Company
Huffman Finishing WWTP
WQ0002431
Annual 2014
Water Tech Labs
Lab # ;
mate A istyze4
Fecal Colzform
CFX3 per gram
MEN
Log
1
9/29/14
64,078
4.807
2
9/30/14
58,252
4.765
3
10/1/14
79,612
4.901
4
10/6/14
120,388
5.081
5
10/7/14
69,903
4.844
6
10/8/14
54,369
4.735
-71
7
10/9/14
1 56,311
4.751
Totall 334804
Average 4:84-1
Colony Forming Units / Gram . !09,27 . Fecal Coliform/gram
Fecal Coliform values have a geometric mean of less than 2,000,000 and meet
the Class B pathogen reduction requirement
Data provided in this summary have been used for the values reported on the
Annual Pathogen and Vector Attraction Deduction Form for this land
application event.
ldfirsi QO cH L885.111C.
POST OFFICE BOX 1056 A #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828) 396A444
SAMPLE: Huffman Finishing-Digestor COLLECTION DATE,
9/29/2014
PERMIT A COLLECTION TIME:
12:45
ADDRESS: RECEIVED DATE,
9/29/2014
RECEIVED TIME:
13:09
REPORTED:
10/23/2014
ANALYSIS.
ANALYSIS RESULTS UNITS DATE. ANALYST
Fecal Coliform 330,000 /100mL 9/29114 lag
LOG ID: 1409-504 REPORTED BY: NC CERTIFIED LAB #I 50
fl�*
Tony Gragg, Lab Supervisor
ldfir lvirxCH LOINS-mc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828) 3964444
SAMPLE.- Huffman Finishing-Digestor COLLECTION DATE: 9/30/2014
PERMITA, COLLECTION TIME, 10:48
ADDRESS., RECEIVED DATE., 9/30/2014
RECEIVED TIME. 11:35
REPORTED. 10/23/2014
ANALYSIS
ANALYSIS RESULTS UNITS DAT8 ANALYST
Fecal Collform 300,000 1100mL 9/30/14 lag
LOG ID, 1409-512 REPORTED BY: NC CERTIFIED LAB # 50
flll�*
Tony Gragg, Lab Supervisor
firEffrrrCH L1195-Inc,
POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828) 396-4444
SAMPLE: Huffman Finishing-Dlgestor COLLECTIONDATE. 10/1/2014
PERMIT #: COLLECTION TIME. 10:35
ADDRESS: RECEIVED DATE., 10/1/2014
RECEIVED TIME: 11:20
REPORTED: 10/23/2014
ALYSIS
ANALYSTS EFFLUENT LINITS HATE ANALYST
Fecal Coliform 410,000 /100mL 10/1/14 lag
LOG ID: 1410-065 REPORTED BY: NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor
POST OFFICE BOX 1056 4 #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NOM CAROLINA 28630
(828) 3W4444
M SAMPLE.' Huffman Finishing-Digestor COLLECTION DATE: 10/6/2014
PERMIT #: COLLECTION TIME: 12:40
ADDRESS: RECEIVED DATE: 10/6/2014
RECEIVED TIME: 13:08
REPORTED: 10/23/2014
ANALYSTS
ANALYSIS EFFLUENT UNITS DA TE ANALYST
Fecal Coliform 620,000 /100mL 1016/14 lag
LOG 1D: 1410-066 REPORTED BY: NC CERTIFIED LAB # 50
fl�
Tony Gragg, Lab Supervisor
a sovar cm mis .i..
POST OFFICE BOX 1056 0 #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
(828) 396-4444
SAMPLE., Huffman Finishing -Digester COLLECTION DATE. 10/7/2014
PERMIT #- COLLECTION TIME: 09:55
ADDRESS: RECEIVED DATE., 10/7/2014
RECEIVED TIME. 12:10
REPORTED: 1013012014
L YSIS
;
ANALYSIS RESULTS UNITS SATE- ANALYST
Fecal Coliform 360,000 mg1L 1017/14 lag
LOG ID: 1410-201 a
REPORTED BY: NC CERTIFIED LAB # 50
follk
Tony Gragg, Lab Supervisor
mf►rciRimcm LRAys.Irt.
s
— POST OFFICE BOX 1066 - #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROUNA 28630
(828)396-4444
SAMPLE., Huffman Finishing-Digestor COLLECTION DATE: 10/8/2014
PERMIT A COLLECTION TIME. 10:40
ADDRESS: RECEIVED DATE: 10/8/2014
RECEIVED TIME.- 11:20
y REPORTED, 10/23/2014
AN Y`S-18
ANALYSIS RESULTS UNITS DATE ANALYST
Fecal Coliform 280,000 /100mL 10/8/14 lag
LOG ID: 1410-201 REPORTED Bi': NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor
L 1dfi 'KA rjFC ' LAi S-c.
POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR.
1 GRANITE FALLS, NORTH CAROLINA 28630
(828)396-4444
I
SAMPLE: Huffman Finishing-Digestor COLLECTION DATE., 10/9/2014
l; PERMIT #: COLLECTION TIME: 10:00
ADDRESS: RECEIVED DATE: 10/9/2014
RECEIVED TIME., 11:35
REPORTED: 10/23/2014
ANALYSIS
ANALYSIS RESULTS UNITS DATE ANALYST
Fecal Coliform 290,000 /100mL 10/9114 lag
LOG ID: 1410-202 REPORTED : NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor
SOIL ANALYSIS REPORT
NCDA&CS Agronomic Division Phone: (919) 733.2655
Website: www.ncagr.gov/agronomi/
Report No. FY15-SL017239
crr,4P•
Client: A.W. Huffman Jr
Advisor: Bob Branch
¢ -
Predictive
PO Box 170
Branch Residuals &
Granite Falls, NC 28630
Soils -Bob
..
Extraction
Soil Report
8646 W Market St Suite
111
Sampled County: Caldwell
Sampled
�a''•YI'iR9
Greensboro, NC 27409
Sampled: Received: 11/17/2014
completed: 12/16/2014
Farm:
Links to Helpful Information
Sample ID: 002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim,1 0.0
120-200 110
110 0 0 0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, 0.0
120-200 110
110 0 0 0
0
0 0
Note: 12
Test Results [units - WN in g/cd; CEC and Na In meq/100 cd; NO3-N in mg/dnf]:
Soil Class: Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn4
Zn AI
Cu-1 Na ESP SS -I ' NO3-N
0.60 1.08
7.4 84 1.2 6.2 14 14
60 23
37 88 67 67 257
257
131 0.2 3
North Carolina
'rni,.ryrco Truo FLffWW Ccrmmwslm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Trox/er, Commissioner of Agriculture
NCDA$CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.gov/agronomi/
Report No. FY15-SLO17239
A.W. Huffman Jr
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium.
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
ESP
copper index
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-I
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class.
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-a
mineral -organic soil class
notations appear on the. soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncayraovlaaronomiloboart4.htm#fs to find
P-1
phosphorus index
'information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
Test Results
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.nca4r.yovlaoronomiluyrst.htm
for more information.
2014 APPLICATION SUMMARY TABLE
HUFFMAN FINISHING COMPANY
LAND APPLICATION PROGRAM
PERMIT NO. WQ0001618
SOUTHERN SOLUTIONS ENVIRONMENTAL
2014 APPLICATION SUMMARY
. ....... .
'Far
. .... ........ Dato
ere ..: -S-
Fi .. Q'I out
cres: ...--A-- D. T
P
Lee Hufinan
Huffman 2 6.6 Nov-14 77,000 2.51 16.54 Huffman Mills WWTP
Fescue 127.89
Number of Fields Applied to:
Huffman Finishing NVVVTP 77,000 16.54 15.03
6.60
Branch Residuals Soils, LLC Confidential 2/1/2015 Page 1
2014 APPLICATION CONDITION SUMMARY
I
Huffman Finishing Company WWTP
Granite Falls, North Carolina
Southern Solutions Environmental
WQ0002431
Annual 2014
Huffman Mills WWTP
Farmer: Lee Hufinan
Acres: 6.6
Site/Tract: Huffinan
Application Method: Surface
Field: 2
Percent Solids: 5.15
Residual Report No.: HF14-276-0202
Crop: Fescue
Date
Field No.
Subfield
Wet Tons
Soil
Conditions
Weather
Conditions
Prev. 24 Hour
Rainfall
11/10/14
2
49,000.0
Dry
Good
0.00
11/11/14
2
28,000.0
Dry
Good
0.00
Tma.:.:....:..............................................................
0.0
,.............