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HomeMy WebLinkAboutWQ0002431_Residual Annual Report 2014_201502192014 ANNUAL REPORT HUFFMAN FINISHING COMPANY LAND APPLICATION PROGRAM . PERMIT #WQ0002431 Prepared For: Huffinan Finishing Company P.O. Box 170 Granite Falls North Carolina 28630 Prepared By: Branch Residuals & Soils, LLC 8646 W. Market Street — Suite.111 Greensboro, North Carolina 27409 February 2015 RECEIVE® FEB 19 2015 1N,NAM ® NP 1 "ROCESSING UNIT BRANCH RESIDUALS & SOILS, LLC . 8646 W. Market St. — Suite 111 • Greensboro, NC 27409 PHONE (336) 510-0340 a Fax (336) 510-0341 February 15, 2015 North Carolina Department of Environment and Natural Resources Division of Water Resources - Land Application Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2014 LAND APPLICATION ANNUAL REPORT Huffinan Finishing Company Permit No. WQ0002431 Branch Residuals & Soils Project No. 2014-115 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Huffman Finishing Company. This report includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Form, 4) Annual Land Application Field Summary Form, 5) Residual Analysis Lab Sheet, 6) TCLP Lab Sheets, 7) Annual Pathogen & Vector Attraction Form, 8) Annual Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data 10) 2014 Application Summary Table, and 11) 2014 Application Condition Summary. Applications 77,000 gallons (16.54 dry tons) were made to one field (6.6 acres) in 2014. This has been the first application in several years. Current permit does not require vector attraction to be performed only pathogen reduction. If any further information is required regarding this land application program, please do not hesitate to contact meat (336) 510-0340. Sincerely, Robert T. Branch, L.S.S. Land-Application/Residuals Operator #15676 RTB Enclosures TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Form IV Annual Land Application Field Summary Form V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Annual Pathogen and Vector Attraction Reduction Form VIII Annual Pathogen and Vector Attraction Reduction Documentation IX Soil Analysis Report X 2014 Application Summary Table XI 2014 Application Condition Summary CERTIFICATION FORM 11 ANNUAL LAND APPLICATION CERTIFICAT ON FORM WQ Permit##: WQ0002431 County: Caldwell Year: 2014 Facility Name (as shown on permit): Huffman Finishing Company Land Application Operator: Southern Solutions Environmental Phone: 336-753-1256 Land application of residuals as allowed by the permit occurred during the past calendar year's ® Yes ® No - If No, skip Part A, and Part E and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Miplication Summary: Total number of a lication fields in the ermit: 4 Total number of fields utilized for land application during the year: 1 Total amount of dry tons applied during the year for all application sites: 16.54 Total number of acres utilizes for land application during the year: 6.6 Part 13 - Annual Comnniauce Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes L3 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. _ 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). �— 7) All general requirements in as specified in the Land Application Permit were complied with (applicable -to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior ( authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as. specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: n certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." j j 2-ti-Zo1S i Mr. Lee T. Huffman, Huffman Finishing Treasurer Signature of PerNttee Date Mb 2/3/15 Signature of Preparer* (if Signature o Land Appli Date +, (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0002431 Laboratory: 1) A & L Eastern Ag Labs Facility Name: Huffman Finishing Company 2) Residual Source WQ # or NCO025135 3) NPDES #: 4) WWTP Name: HuffinanTinishing WWTP 5) ---------- ------ --- — Parameter (mg/kg) ----- Ceiling Cone. Limit Sample -or Composite Date 10/t/2014 Percent Solids (%) NA 5.15 Arsenic 75 7.00 Cadmium 85 <2.00 Copper 4,300 640.00 Chromium NA 0.00 Lead 840 18.00 Mercury 57 1.20 Molybdenum 75 <5.00 Nickel 420 40.00 Selenium 100 <5.00 Zinc 7,500 745.00 Total Phosphorus NA 5,870 TKN NA 81,700 Ammonia -Nitrogen NA 5,050 Nitrate and Nitrite NA <2.00 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the mdividual pernut for metals emirs. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for sr Tb*ttin=,ding the possibility of fines and imprisonment for knowing violations." 1,doi5 Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) r DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM ANNUAL METALS FIELD LOADING SUMMARY FORM I Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Huffman Finishing Company Total Dry Tons applied (Annual): 16.54 Permit #: WQ0002431 Cation Exchange Capacity (non 503 only): n/a Operator: Lee Huffman Owner: Lee Huffman Predominant Soil Series FaB2 Acres Used: 6.6 Acres Permitted: 6.6 Site #: Huffman Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): XW1Y-L/0-VLVL Sample or Com- 10/1/14 posite Date % Solids 5.15 Arsenic 7.00 Cadmium 2.00 Chromium 0.00 Copper 640.00 Lead 18.00 Mercury 1.20 Molyb- 5.00 denum Nickel 40.00 Selenium 5.00 Zinc 745.00 Total Phos- 5,870 honus A -- .-1 11-- Mn+.mil INAJA T .na.linac WRIV1112ted in lbs/acrel: � O 0 a 2.51 a Arsenic 0.04 0.04 Cadmium 0.01 0.01 Chromium 0.00 0.00 Copper 3.21 3.21 Lead 0.09 0.09 Mercury 0.01 0.01 Molyb- 0.03 0.03 denum 0.20 Nickel 0.20 Selenium 0.03 -0.03 Zinc 3.73 3.73 Total Phos- 29.41 29.41 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of flues and imprisonment for knowing violations" wwpt* 2/3/15 Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL LAND APPLICATION FIELD SUMMARY FORM ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. Cumulative Totals — lbs/ac applied during the lifetime of field use. ANNUAL LAND APPLICATION FIELD SUNEWARY FORM PLEASE MADE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTEDTFOR EACH APPLICATION FIELD. PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE. FacWty Name: Huffman Finishing Company WQ Permit#: WQ0002431 Field #• Huffman Acres Utilized: 6.60 Owner: Lae Huflinan Annual Dry Tom Applied: 16.54 Site #: 2 Acres Permitted: 6.60 Operator: Lee Huffman Predominat Soil Series FaB2 Cation Exchange Capacity (non 503): NA Crop 1 Namc Fescue Crop 1 Mat PAN: 194.00 Crop 2 Name: #N/A Crop 2 Max. PAN #N/A 129A Today PerApe % Solids Volume A Mod ADeciftwcre /A Re &dual Sourom (NPDES #, WQdt, FerL,AnftW Wrote, etc.) Site �� Wet, moist) Pracip Past 24 Hra. $ g �+° �s � � TKN � dt 9 � N.it W and Nitrite PAN Applied (lbs/acre) MU3t Se1Cd Crop I or Crop 2 Gai. t_1 C .Yd. Repot Totals in Gal. Crop I. Crop 2 Crop I Crop 2 Nov-14 77,000 11,667 5.15 151 HuftmMIM WWTP S 0.50 0.30 81,700 5,050 2 127.89 X T®PALS: 11,667 Annual lbs/acxe. Current Cumulative lWacre Prior'Years Cumulative lbs/acro Perm:tte&C. P. L R.**es As Cd Cr Cu Pb H MO Ni 3e 7�t P PAN 1 PAN 2 0.04 0.01 0.00 321 0.09 0.01 1 0.03 0.20 0.03 3.73 29.41 127.89 0.00 0.10 0.06 NA 10.55 035 0.02 1 NA 1 0.62 1 0.09 1 30.86 0.06 0.05 NA 7.34 0.26 1 0.01 LNL4 0.42 0.06 27.12 36 34 NA 1,338 267 15 NA 374 89 2,498 ] 94.00 dun 'th oleos Lime A Lied Date lbs,'ac Permit PAN Lmut 1 s02nd Crop "I cerft, gaoler penalty of law, that this -document was prepared under my direcwo or supery"ioa.ia actor ce wa a ay wed to acme that qualified -personnel properly pthered and evaluated the information submitted. I am &ware that there fire front peaaidea for im bmitting false information, indudiug the possibliity of Bees and imprisonment for lmowing violOolm" Signature of Laud Applier *Application Method: S - Surface, IN - Injeetioai, INC - Incorporation **VolitiliztttWn Rate: Suffice - OA Igieetlon/Incorporation -1.0 ***Mineralization Rates: Compost - 0.1, Aanaerobically Digested - 0.2, Date Aerobically Digested - 0J, Raw Sludge - 0.4 ****C.P.LJL-. Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) RESIDUAL ANALYSIS LAB SHEETS Page: 1 of 2 Report Number: 14-276-0202 Account Number: 46368 Submitted By: BOB BRANCH Send To: BRANCH RESIDUALS & SOILS LLC BOB BRANCH 8646 West Market Street Suite 111 GREENSBORO , NC 27409 Lab Number: 57925 Sample Id: HUFFMAN MILLS NRL, A&L Easters Laboratories, Inca 7621 Whitepine Road Richmond, Virginia 23237 (604) 743-9401 Fax (604) 271-6446 wiwwjleastern.com Project: HUFFMAN MILLS NC CERT#257 REPORT OF ANALYSIS Date Sampled: Date Received: 10/03/2014 00:00 Date Reported: 10/08/2014 Total Solids * 5.15 51500 100.0 JM 10/03/2014 14:30 SM-2540G Moisture' 94.85 100.0 JM 10/03/201414:30 SM-254OG Total Kieldahl Nitrogen 8.17 81700 10.0 JM 10/06/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 0.59 5870 100 KM 10/06/2014 11:30 SW 6010C Total Potassium 0.08 813 100 KM 10/06/2014 11:30 SW 6010C Total Calcium 0.41 4050 100 KM 10/06/2014 11:30 SW 6010C Total Magnesium 0.19 1,940 100 KM 10/06/2014 11:30 SW 6010C Total Sodium 0.57 5680 100 KM 10/06/2014 11:30 SW 6010C Total Iron 13300 100 KM 10/06/2014 11:30 SW 6010C Total Aluminum 3300 100 KM 10/06/2014 11:30 SW 6010C Total Copper 640 5 KM 10/06/2014 11:30 SW 6010C Total Zinc 745 5 KM 10/06/2014 11:30 SW 6010C Ammonia Nitrogen 0.51 5050 10.0 JM 10/06/2014 08:30 SM-4500-NH3C Organic N 7.66 76650 10.0 10/06/2014 08:30 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 10/06/2014 08:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 10/06/2014 11:30 SW 6010C Total Nickel 40 5 KM 10/06/2014 11:30 SW 6010C Total Lead 18 5 KM 10/06/2014 11:30 SW 6010C All values are on a dry weight basis.except as noted by asterisk. Detection limit on all N series is on a wet basis. 9�/w Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part may any reference be made (N9nor to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt ! — J Page: 2 of 2 Report Number: 14-276-0202 Account Number: 46368 Submitted By: BOB BRANCH Send To: BRANCH RESIDUALS & SOILS LLC BOB BRANCH 8646 West Market Street Suite 111 GREENSBORO , NC 27409 Lab Number: 57925 Sample Id: HUFFMAN MILLS A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23231 (604) 743-Mi Fax (604) 271.6446 wn Project: HUFFMAN MILLS NC CERT#257 REPORT OF ANALYSIS Date Sampled: Date Received: 10/03/2014 00:00 Date Reported: 10/08/2014 Total Arsenic 7.0 3.0 KM 10/06/2014 11:30 SW 6010C Total Mercury 1.2 0.4 KM 10/07/2014 14:00 SW-7471 B Total Selenium <5.0 5.0 KM 10/06/2014 11:30 SW 6010C pH (Standard Units) " 6.56 2.00 JM 10/06/2014 08:30 SW-9045D Total Volatile Solids 84.02 840200 100.0 JM 10/03/2014 14:30 SM-2540G Total Molybdenum <5 5 KM 10/06/2014 11:30 SW 6010C Comments: ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Se". THE MSD WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt l�NINIa�INlll��llIl�4 =2014 BRANCHRESWAL-SA 5O1L5'LLC Id:W*--28 HU,FRAN MILLS Regular Nutrient and Metal Residuals Analysis Arsenic IAead- Nickel- Aluminum % Total Solids - Potassium Calcium! -- iron - Bob Brancb Bmeh Residuals kSoils 336 51 M340 Bill Brawl) Residuals & Soils Cadmium mercuq - Selenium -. Ammonia -Nitrogen pH Magnesium - pr6ject: Huffolgil Mills Pfoj.cut No- 2014-115 ups jayqvLI'/,oSqqS�4"5n C,ppper,- Molybdeftum, - Zinc - Nitrate -Nitrite NitrogeP - IPIIOphorus - volatile Solids - Sodium - c Facility: Huffman Finishing Company WWTP Source: Huffman Mills WWTP Location: Granite Falls, North Carolina Contractor: Southern Solutions Environmental Type of Analysis: Testile Industrial Report No: HF14-276-0202 Date Sampled: 10/1/2014 Date Reported: 10/8/2014 Reporting Period: Annual 2014 Parameter % PPM Dry Weight EPA Monthly Limits Solids S' 15: Nitrogen (TKN) 8.170 81,700.000 Phosphorus ; `.a5$7 ,`_ 5,870.000 Potassium :0.0$1' 813.000 Sulfur = 0.000 Calcium 0.41O ` 4,100.000 Magnesium : '"0:.1'90 1,900.000 Sodium 5,700.000 Iron --- 1.3,300000:, Aluminum --- 330,0.000 Manganese --- " Copper --- 64a00E0 : 1,500 Zinc --- 745000 2,800 Ammonia Nitrogen ."0.505 5,050.000 Nitrate N / Nitrite N --- . 2:00Q . Cadmium --- ,^ =ZOOfJ , � �'».._�. 39. Chromium --- 1,200 Nickel --- =%�fJmOQO 420 Lead --- 111,$000 300 Arsenic --- 7000 41 Mercury --- l':200. 17 Selenium - --- �,,,�-.."":.. =-:;�. S.nOOU 100 pH G560 Calcium Carbonate Eq. Organic Nitrogen 7.665 Molybdenum --- 6:000, 75 Chloride --- Boron Available P205 Specific Gravity 8.340 Testile Industrial Huffman Mills WWTP Granite Falls, North Carolina Southern Solutions Environmental Annual 2014 Date Reported: 10/8/2014 Report No: HF14-276-0202 Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 51.044 PAN Inj. 56.094 P 11.740 K 1.626 Lime 0.000 Secondary Nutrients Calcium 8.200 Magnesium 3.800 Sodium 11.400 SAR 4.173 Chloride 0.000 Iron 26.600 Alumium 6.600 Manganese 0.000 Boron 0.000 Sulfur 0.000 Residual Nitrogen Calculation Year Min Rate PAN #/Acre Physical Characteristics % Solids 5.15 pH 6.560 Min Rate 0.300 Metals Arsenic 0.014 Cadmium 0.004 Chromium 0.000 Copper 1.280 Lead 0.036 Mercury 0.002 Molybdenum 0.010 Nickel 0.080 Seleniun 0.010 Zinc 1.490 2010 2011 2012 2013 2014 0.30 45.99 2015 0.15 16.10 2016 0.08 6.84 2017 0.04 3.16 2018 2019 2020 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT - RESEARC[t & Ar4ALyTICAL c � LAbORATORiES, 'NC. Analytical/Process Consultations Toxicity Characteristic Leachate Procedure (TCLP) Analysis of Sample Identified as Granite Falls l,k Branch Residuals & Solls Protect. collected 01 October 2014) _ GF WWTP GF WTP EPA HW Quantitation Results its Results Characteristic Number Contaminant umit(ard" (MULL (ma/L) Level(mf: LJ EPA Method L TCLP METALS I}004 Arsenic 0.010 SOL SOL BOL 5.00 6010C D-005 Barium 0.040 0.067 0.054 0.096 100 6010C D-006 Cadmium 0.005 `0.010 BQL BOL BOL 1.00 6010C D-077 Chromium BQL 0.034 0.031 5.00 6010C ' D.002 Lead 0.005 BOL BQL 0.012 5.00 6010C D-009 Mercury 0.0020 BQL SOL BQL 0.200 7470A D410 Selenium 0.100 BQL SQL BQL 1.00 6010C D-011 Silver 0.010 BQL SOL SOL 5.00 6010C II. TCLP VOLATILES D-018 Benzene 0.050 BOL 139L BQL 0.500 8260E D-019 Carbon Tetrachloride 0.050 BQL BQL BQL 0.500 6260B D-021 Chlorobeneene 0.030 BQL BQL SOL 100 8260E D-022 ChlorofOrnt. 0.500 BQL BQL SOL 6.00 8260E D-028 1.2-Dichloroethane 0.050 BQL BQL SOL 0.500 8260E D-029 1.1-Dichlomethylene 0.050 BQL BOL SOL 0300 8260B D-035 Methyl Ethyl Ketone 0.500 BQL SOL BQL 200 8260B D-039 Tetrachloroethylene 0.050 BQL BQL SOL 0.700 8260B D-040 Trichloroethylene 0.050 SOL BQL BOL 0.500 6260E D-043 Vinyl Chloride 0.050 BOL BOL SOL 0.200 8260E -� TCLP SEMI-VOLATILES D.023 0-0e0301 20.0 BQL SOL BQL 200 9270D D-024 M-Creosol 20.0 BQL SOL SQL 200 8270D D-025 104moso1 20.0 BQL BQL SOL 200 8270D D-026 Creoml 20.0 SQL BOL BQL 200 8270D D-027 1,4.Didd robem. 0.750 SOL SOL BQL 7.50 8270D D-030 2,4-Dirutrotoluene 0.050 BQL BOL SOL 0.130 8270D ' D.032 Hexacb1orobenaene 0.050 BOL ROL SOL 0.130 8270D D-033 Hexachlorobutediene 0.050 SOL SOL SOL 0.500 8270D D-034 Hexnchlomedume 0.300 BOL SOL BOL 3.00 8270D D-036 Nitrobenzene 0.200 BQL SOL BQL 2.00 8270D _ D-037 Pentadmomphenol - 10.0 BQL SOL BQL 100 8270D D-039 Pyridine 0.500 BOL SOL BOL 5.00 8270D D-041 44,5-Trichlorophenol 40.0 SOL SOL SOL 400 8270D D-042 2.4.6-Tticidorephmol 0.200 BQL SOL BQL 2.00 8270D V. TCLP PESTICIDF.SIHERBICHIES D-020 Chlwdme 0.003 SOL SOL SOL 0.030 80918 D-016 2Aa 1.000 BQL SOL SOL 10.0 8151 A D-012 Endrin 0.002 BOL ROL SOL 0.020 8081 B D-031 Heptachlor 0.0008 BQL BQL BQL 0.008 8081 B D-013 Lindmte 0.040 BOL SOL ROL 0.400 8081 B D-014 Medwxychlor 1.000 BQL SOL SOL 10.0 8081 B D-015 Toxaphene 0.050 BQL BQL SOL 0.500 9081 B D-017 2.4.5-TP(Silvex) 0.100 BQL BQL BQL 1.00 8151 A REACrIVITV D-003 Cyanide 2.0 BQL BQL BQL 9010 D-003 Sulfide 10.0 SOL SOL BOL 9030 VI. CORROSIVITY D-002 PH Std. Units 11.1 6.11 5.71 9045 qj. TCLP MISCELLANEOUS Paint Filter Test _ FLP FLP FLP _ /mIGNITABIL TY D-001 lwdtability > 1401 > 1400 > 140" 1010 Sample Number 796122 796123 796124 Sample Date 10/01/14 10/01/14 10/01/14 Sample Time (hrs) 1200 1330 1430 --' Sample Matrix Solid Solid Solid �I SQL - Below Quantitation Limits WNl a Will Not Ignite mg/L a milligram per Liter - parts per million (ppm) mgft - milligrams per kilogram o pans per million (ppm) 'ElRESEAR8i & ANAlyfiCAI LkoMTOMES, INC. Analytical / Process Consultations Phone 1338) 998-2841 CHAIN OF CUSTODY RECORD WATER I WASTEWATER I misc. • • ♦ 1, • • ♦ • • -STREETADDRESS• ' ♦ i ! / JJ}}}} ==NONE■■ ■■■■■■■■■■■■ ■■■ ■■■■■■■■■m ■■■■■■■■■■■■ ■■■ ��■■■■■■ ■■■■■■■■■■■■ ■■■ ��■■■■■■ ■■■■■■■■■■■■ ■■■ ==NONE■■ ■■■■■■■■■■■■ ■■■ ��■■■■■■ ■■■■■■■■■■■■ ■■■ �■■■■■■■■ ■■■■■■■■■■■■ ■■■ .�■■■■■■■ ■�■■■■■■■■■■ ONE 11.11 MARKS: SAMPLE TEMPERATURE AT RECEIPT --J,-1 11C LINQUISHED BY RELl ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION FORM The Huffinan Finishing Company met pathogen reduction through fecal coliform sampling. This permit is not required to have vector attraction reduction options. The annual certification form is marked accordingly to reflect the methods of meeting pathogen reduction. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) 4I Facility Name: Huffinan Finishing Company WQ Permit Number: WWTP Name: Huffman Finishing WWTP NPDES Number: Monitoring Period: From l/l/2014 To 12/31/2014 Fi i Pathogen Reduction (15A NCAC 02T .1106 Class A: Alt. A (time/temp) ❑ :::....................................... A1t.D o Prior Test) ❑ If applicable to alternative performed (Class A Compost ❑ 1 Heat Drying ❑ Beta Ray ❑ 1 Gamma Ray ❑ WQ0002431 NCO025135 - Please indicate level achieved and alternative perfori Alt B (Alk Treatment) ❑ 1 Alt. C (Prior Testing) ❑ Process to Further Reduce Pathogengs ❑ only) indicate "Process to Further Reduce Pathogens": Beat Treatment ❑ Thermophilic ❑ Pasteurization ❑ _ .. Class B: TAlt. (1) Fecal Density 21 1 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Ana erobic Digestion tion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Excee Frequency Sample Analytical Tech - in in Sludge Geo. Mean Maxi Units of Analysis Type nioue 2 x 10 to the MPN 6th power per gram of r!lCFU/ SM20 Fecal Coliform total solids CFU 54,369 69,275 120,388 Gram 0 Annually Grab 9222D 1000 mpn per gram of total solid (dry Imonella bacteria 3 MPN per 4 grams (in lieu of fecal I total solid (dry cT__4 ♦u-...ti.... In-A....4:..— /MCA N!`Ae' 111 r Vln n - Uidinan indid-atop alitpruntivP 11PrfnrR1P.(1_ Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate szaxemcnz) ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." M. Shuford Wise, Huffman Finishing WWTP ORC Pre arer Name and itle ( e or print) Land Applier Name and Title (if applicable)(type or print) X . Aa- U" _- Ulu" Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date nFNR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION DOCUMENTATION PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION DOCUMENTATION The Huffman Finishing Company met pathogen reduction through fecal coliform sampling. This permit is not required to have vector attraction reduction options. The annual certification form is marked accordingly to reflect the methods of meeting pathogen reduction. Documentation of the fecal coliform sampling data is attached. Huffman Finishing Company Huffman Finishing WWTP WQ0002431 Annual 2014 Water Tech Labs Lab # ; mate A istyze4 Fecal Colzform CFX3 per gram MEN Log 1 9/29/14 64,078 4.807 2 9/30/14 58,252 4.765 3 10/1/14 79,612 4.901 4 10/6/14 120,388 5.081 5 10/7/14 69,903 4.844 6 10/8/14 54,369 4.735 -71 7 10/9/14 1 56,311 4.751 Totall 334804 Average 4:84-1 Colony Forming Units / Gram . !09,27 . Fecal Coliform/gram Fecal Coliform values have a geometric mean of less than 2,000,000 and meet the Class B pathogen reduction requirement Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Deduction Form for this land application event. ldfirsi QO cH L885.111C. POST OFFICE BOX 1056 A #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396A444 SAMPLE: Huffman Finishing-Digestor COLLECTION DATE, 9/29/2014 PERMIT A COLLECTION TIME: 12:45 ADDRESS: RECEIVED DATE, 9/29/2014 RECEIVED TIME: 13:09 REPORTED: 10/23/2014 ANALYSIS. ANALYSIS RESULTS UNITS DATE. ANALYST Fecal Coliform 330,000 /100mL 9/29114 lag LOG ID: 1409-504 REPORTED BY: NC CERTIFIED LAB #I 50 fl�* Tony Gragg, Lab Supervisor ldfir lvirxCH LOINS-mc. POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE.- Huffman Finishing-Digestor COLLECTION DATE: 9/30/2014 PERMITA, COLLECTION TIME, 10:48 ADDRESS., RECEIVED DATE., 9/30/2014 RECEIVED TIME. 11:35 REPORTED. 10/23/2014 ANALYSIS ANALYSIS RESULTS UNITS DAT8 ANALYST Fecal Collform 300,000 1100mL 9/30/14 lag LOG ID, 1409-512 REPORTED BY: NC CERTIFIED LAB # 50 flll�* Tony Gragg, Lab Supervisor firEffrrrCH L1195-Inc, POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE: Huffman Finishing-Dlgestor COLLECTIONDATE. 10/1/2014 PERMIT #: COLLECTION TIME. 10:35 ADDRESS: RECEIVED DATE., 10/1/2014 RECEIVED TIME: 11:20 REPORTED: 10/23/2014 ALYSIS ANALYSTS EFFLUENT LINITS HATE ANALYST Fecal Coliform 410,000 /100mL 10/1/14 lag LOG ID: 1410-065 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor POST OFFICE BOX 1056 4 #5 PINEWOOD PLAZA DR. GRANITE FALLS, NOM CAROLINA 28630 (828) 3W4444 M SAMPLE.' Huffman Finishing-Digestor COLLECTION DATE: 10/6/2014 PERMIT #: COLLECTION TIME: 12:40 ADDRESS: RECEIVED DATE: 10/6/2014 RECEIVED TIME: 13:08 REPORTED: 10/23/2014 ANALYSTS ANALYSIS EFFLUENT UNITS DA TE ANALYST Fecal Coliform 620,000 /100mL 1016/14 lag LOG 1D: 1410-066 REPORTED BY: NC CERTIFIED LAB # 50 fl� Tony Gragg, Lab Supervisor a sovar cm mis .i.. POST OFFICE BOX 1056 0 #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE., Huffman Finishing -Digester COLLECTION DATE. 10/7/2014 PERMIT #- COLLECTION TIME: 09:55 ADDRESS: RECEIVED DATE., 10/7/2014 RECEIVED TIME. 12:10 REPORTED: 1013012014 L YSIS ; ANALYSIS RESULTS UNITS SATE- ANALYST Fecal Coliform 360,000 mg1L 1017/14 lag LOG ID: 1410-201 a REPORTED BY: NC CERTIFIED LAB # 50 follk Tony Gragg, Lab Supervisor mf►rciRimcm LRAys.Irt. s — POST OFFICE BOX 1066 - #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROUNA 28630 (828)396-4444 SAMPLE., Huffman Finishing-Digestor COLLECTION DATE: 10/8/2014 PERMIT A COLLECTION TIME. 10:40 ADDRESS: RECEIVED DATE: 10/8/2014 RECEIVED TIME.- 11:20 y REPORTED, 10/23/2014 AN Y`S-18 ANALYSIS RESULTS UNITS DATE ANALYST Fecal Coliform 280,000 /100mL 10/8/14 lag LOG ID: 1410-201 REPORTED Bi': NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor L 1dfi 'KA rjFC ' LAi S-c. POST OFFICE BOX 1056 - #5 PINEWOOD PLAZA DR. 1 GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 I SAMPLE: Huffman Finishing-Digestor COLLECTION DATE., 10/9/2014 l; PERMIT #: COLLECTION TIME: 10:00 ADDRESS: RECEIVED DATE: 10/9/2014 RECEIVED TIME., 11:35 REPORTED: 10/23/2014 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST Fecal Coliform 290,000 /100mL 10/9114 lag LOG ID: 1410-202 REPORTED : NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor SOIL ANALYSIS REPORT NCDA&CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL017239 crr,4P• Client: A.W. Huffman Jr Advisor: Bob Branch ¢ - Predictive PO Box 170 Branch Residuals & Granite Falls, NC 28630 Soils -Bob .. Extraction Soil Report 8646 W Market St Suite 111 Sampled County: Caldwell Sampled �a''•YI'iR9 Greensboro, NC 27409 Sampled: Received: 11/17/2014 completed: 12/16/2014 Farm: Links to Helpful Information Sample ID: 002 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim,1 0.0 120-200 110 110 0 0 0 0 0 0 Note: 12 2- Fescue/OGrass/Tim, 0.0 120-200 110 110 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cd; CEC and Na In meq/100 cd; NO3-N in mg/dnf]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn4 Zn AI Cu-1 Na ESP SS -I ' NO3-N 0.60 1.08 7.4 84 1.2 6.2 14 14 60 23 37 88 67 67 257 257 131 0.2 3 North Carolina 'rni,.ryrco Truo FLffWW Ccrmmwslm Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox/er, Commissioner of Agriculture NCDA$CS Agronomic Division Phone: (919) 733.2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SLO17239 A.W. Huffman Jr Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a time recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium. one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I ESP copper index exchangeable sodium percent Fertilizer HM% percent humic matter Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of K-I potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class. an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear Mn Mn-All manganese Mn-availability index for crop 1 only on reports for greenhouse soil or problem samples. Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z M-a mineral -organic soil class notations appear on the. soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit Na sodium ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen ORG organic soil class Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncayraovlaaronomiloboart4.htm#fs to find P-1 phosphorus index 'information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P205 phosphate S-1 sulfur index SS-1 soluble salt index Test Results W/V weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI Zn-I zinc availability index zinc index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.nca4r.yovlaoronomiluyrst.htm for more information. 2014 APPLICATION SUMMARY TABLE HUFFMAN FINISHING COMPANY LAND APPLICATION PROGRAM PERMIT NO. WQ0001618 SOUTHERN SOLUTIONS ENVIRONMENTAL 2014 APPLICATION SUMMARY . ....... . 'Far . .... ........ Dato ere ..: -S- Fi .. Q'I out cres: ...--A-- D. T P Lee Hufinan Huffman 2 6.6 Nov-14 77,000 2.51 16.54 Huffman Mills WWTP Fescue 127.89 Number of Fields Applied to: Huffman Finishing NVVVTP 77,000 16.54 15.03 6.60 Branch Residuals Soils, LLC Confidential 2/1/2015 Page 1 2014 APPLICATION CONDITION SUMMARY I Huffman Finishing Company WWTP Granite Falls, North Carolina Southern Solutions Environmental WQ0002431 Annual 2014 Huffman Mills WWTP Farmer: Lee Hufinan Acres: 6.6 Site/Tract: Huffinan Application Method: Surface Field: 2 Percent Solids: 5.15 Residual Report No.: HF14-276-0202 Crop: Fescue Date Field No. Subfield Wet Tons Soil Conditions Weather Conditions Prev. 24 Hour Rainfall 11/10/14 2 49,000.0 Dry Good 0.00 11/11/14 2 28,000.0 Dry Good 0.00 Tma.:.:....:.............................................................. 0.0 ,.............