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WQ0002127_Residual Annual Report 2014_20150302
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''' '.. , _ pine 1- , _ , -1 I'�, -11 I -, - - Y"T , , - 11. _2�11'1.1�',,,',',-� _� - " " � - �,.-_ . wl_�. ., -Z., "-;-- " � - �. 1, , I _.-;.,, _;l �` I,.; ,'-- -, , ', I , - " . � V n, 7,"4, " .... .- , - , ,1_2. �,:."��,:. ,., 7. _ -", � �l 4 � . " Vc��.olw;�6 0 � - - , , ", -,, ".j e, , ��, .., �' , , l, -,.�.7 I . I -;� , , � - . '. � �, . r " . , , . ; - 1. 'l-wAs"w"I - _ g",,���-, , WA-,"�,;._" - - -SL.e--�- ��,�,__,-,,:,T,: WAS', Catawba River Pollution Control Facility Compost Annual Report 2014 M Wa �t • ���1IIIIIII/j��� i o � llEi•. - ti • February 6, 2014 ED HARDEE DENR / DWQ / Water Quality Section Non -Discharge Compliance Unit 1636 Mail Service Center Raleigh, NC 27699-1636 Dear Mr. Hardee, Enclosed is the annual report for the City of ] by permit no#. WQ0002127 for the year 2014. Should you have -any questions about this Sincerely, im W Corpening Wastewater Superintendent Enclosure 's composting operations as required please contact me at (828)-438-5375. February 6, 2014 US EPA, Region 4 Water Programs Enforcement Branch Gulf Enforcement Section 61 Forsyth Street, S.W. Atlanta, GA 30303 Subject: City of Morganton Annual Sludge Report NPDES Permit NCO026573 To Whom It May Concern: This documents Morganton's annual sludge report. Included are facility name address and telephone number, NPDES permit n*ber, information about responsible official, information about facility operator, inorganfic pollutant analysis, description of pathogen reduction option and vector attraction reduction option. Included as well is a signed certification statement. Facility Name: Catawba River Pollution Control Facility Facility Address: 1000 Vine Arde a Road Morganton, NC 28680 Facility Telephone Number: 828-438-5375 Responsible Official: Brad Boris Mailing Address: City of Morgant n P.O. Box 3448 Morganton, NC 28680-3448 Physical Address: City of Morganton 305 E. Union Sty eet Suite A 100 Morganton, NC 28680-3448 Telephone Number: 828-438-5285 Facility Operator: Tim W Corpening Mailing Address: City of Morganton PO Box 3448 Morganton, NC 28680-3448 Physical Address: Catawba River Pollution Control Facility 1000 Vine Arden Rd Morganton, NC 28680-3448 Telephone Number: 828-438-5375 The use and disposal practice for the finished compost is mainly as a soil amendment. The humus -like material can also be used in potting mediums, as mulch for shrubbery and as a source for plant nutrients. The amount of compost that goes to each of the uses or disposal practices can vary depending on the appliers needs. The bulk two thirds of the material are going out to the private homeowner for use in landscaping projects. Each individual who has received this material is listed by name. Each name, address, date received and means of contact is on file at the compost facility. Attached are the results of the analysis performed on the compost material along with the analytical methods used in performing these tests. ' Pathogen reduction has been achieved by the recording of pile temperatures of greater than 55°C having been obtained at several monitoring locations on the pile. Air flow is supplied to the organisms in the piles by forced air to keep aerobic conditions in the piles. These air flows are adjusted as needed to obtain desired temperatures. Vector attraction reduction was met by the records that have been maintained on pile temperatures and they indicate a minimum temperature equal to no greater than 40°C for 14 days with temperature being taken daily as this is a one shift operation. Detention time on composting piles is 21 days under aeration plus another 30 days curing period is allowed before any material is distributed. The volume of compost distributed during 2014 has been determined to be 305 dry metric tons. This was calculated by using the guidance for determining dewatered sludge bulk density and equations for converting sludge volume to dry metric tons found in Appendix C of EPA publication 8 3 1 B-93 -002a. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Catawba River Pollution Control Facility WWTP Name: Catawba River Pollution Control Facility Monitoring Period: From 1/1/2014 To WQ Permit Number: WQ0002127 NPDES Number: NCO026573 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A:+Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑............ 1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs 0 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Bet Beta Ray Y Gamma R a Y eu ' P ast i7zation ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting 0 Aerobic Digestion ❑ Anaerobic Digestion If applicable to alternative performed (Class A or Class B) com lete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o Exn es, Frequency of Analysis Sample Type Analytical Tech- nioue inim Geo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) BRL BRL 20806 MPN/g 0 Quarterly Grab SM92210E Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (1.5A NCAC 02T .1107) - Please indicate alternative performed: Alt.l. (VS ,reduction) ❑ Alt. 5 (14-Day Aerobic) 0 Alt. 2 (40-day bench) ❑ Alt. 6 (Alk. Stabilization ❑ Alt. 3 (30-day bench) Alt 7 (Drying - Stable) ❑ It. 4 (Spec. OZ uptake) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." `T-Zr n (2Or_Rg! LT14l0 Preparer Name and Title (type or print) ignature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Annual Distribution and Marketing/Surface Disposal Certification and Summary Form Facility Name Catawba River Pollution Control Facility Permit # NCO026573 County Burke Operator Tim Corpening Phone (828)438-5375 Facility Type (please check one): _ Surface Disposal (complete Part A ( Source(s) and "Residual IN" Volume only) and Part C) ✓ Distribution and Marketing (complete Parts A, B, and C) WAS THE FACILITY IN OPERATION DURING THE PAST CALENDAR YEAR? ✓ YES _ NO. If NO, skip Parts A, B, and C and certify form below. Month Source(s) (Include NPDES # if applicable) Volume(dry tons) Amendment/ bulking agent IN Residual IN Product OUT January February March April May June July August September October November December NC0026573 236 73 29 NCO026573 333 98 32 NCO026573 .328 109 16 NCO026573 493 164 35 NCO026573 185 62 29 NCO026573 493 164 24 NCO026573 398 136 27 NCO026573 324 96 16 NCO026573 297 99 11 NCO026573 386 129 41 NCO026573 182 57 18 NCO026573 474 176 27 Totals: Annual (dry tons) 4129 1363 305 Part B* Reci ient Information Name(s) Volume (dry tons) Intended use(s) . See attached sheet 49 See attached sheet See attached sheet' 29 See attached sheet See attached sheet 43 See attached sheet See attached sheet 12 See attached sheet See attached sheet 13.0 See attached sheet See attached sheet 21 See attached sheet See attached sheet 0 See attached sheet See attached sheet 33 See attached sheet See attached sheet 12 See attached sheet See attached sheet 4.0 See attached sheet See attached sheet 1 See attached sheet See attached sheet 0 See attached sheet 217 Amendment(s) used: Bulking Agent(s) used: Wood chips I * If more space is required than given, please use the comment space provided below or attach additional sheet(s). _ Check if additional sheet(s) are attached. Comments: Part C Facility was compliant during calendar year 2011.with all conditions of the permit (including but not limited to items 1-3 below) issued by the Division of Water Quality7 YES _NO. If NO, please provide a written description why the facility was not compliant. 1. All monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring -well. "I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNOWLEDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS." SIGNATURE OF PERMITTEE EATE GNATURE OF PREPARER* DATE *Preparer is defined, in 40CFR Part 503.90 DEM FORM DMSD (112002) Compost Distribution Tracking Log 2014 Bed #s 2-12 Total volume:1 Dry Tons Sample collection date: 2/6/14 Compost release date: 1 3/03/14 Invoice Number Name Address Cubic Yards Dry Tons 465 ClydeTaylor 6087 Sugar Loaf Connelly Spring 4 1 466 Ethan Pritchard 2061 Piney Knob Rutherton 7 1 467 A Cut Above Landscape 102 Blvd Burnsville 240.0 47.2 468 Mountain Top Landscape Box 13 Burnsville 132 26 469 Appalician Naturescape Box 857 Morganton 60 12 470 Mountain Top Landscape Box 13 Burnsville 108.0 21 471 Scott Brackett 3490 Gwaltney Morganton 30.0 6 472 L&L Landscaping 141 Little Mt. Rd Morganton 4 1 473 Clark Family Farm Burms Rd Nebo 16 3 474 Clark Family Farm Burms Rd Nebo 16 3 475 Arica Franklin Morganton NC 2 0.4 476 John Webb Connelly Springs NC 2.0 0.4 477 Katrina Avery Morganton NC 16 3 478 Olen Baker 194 Crestwood Ave 8.0 2 479 Brewers Nursery 4782 Nursery Rd 12 2 480 Matt Spencer 2600 Birds Dr. Connelly Springs 1.0 0.2 481 A Kut Above 102 E Blvd Burnsville NC 5.0 1 Unless otherwise noted, all screened compost was purchased for use as a soil amendment. Compost Distribution Tracking Log 2014 Bed #sj 11-4 Total volume: Sample collection date: .-'4/01/1,7 Compost release date: 4/23/14 - k Invoice Number Name Address Cubic Yards Dry Tons 482 Matt Spencer 2900 Sids Dr Connelly Springs 1 0.2 483 Harry Crade 361 Linville NC 4.0 0.9 484 Jason Thomson 1145 Alman Ridge Rd 2.0 0.5 485 Mountain Top Box 13 Burnsville NC 36.0 8.3 486 Donna Livinston Conelly Springs NC 1.0 0.2 487 Matt Spencer 2909 Sids Dr Connelly springs 2.0 0.5 488 Steven Hambs 2810 Hill Top Morganton 8.0 1.8 489 Mike Abernath Morganton NC 3.0 0.7 490 Mike Puett Jonas Ridge NC 8.0 1.8 491 Bobby Smith 106 Kimberly Dr Morganton 8.0 1.8 492 Highland Landscape Boone Nc 36.0 8.3 493 James Smith Linconton NC 6.0 1.4 494 Harry Crade 361 Linville NC 2.0 0.5 495 Logan Higden 5496 Scott Rd Morganton 2.0 0.5 496 Rex Shuping Mill Rd Morganton 1.0 0.2 497 DennyCamp 431 Causb - Rd 2.0 0.5 498 A Kut Above 102 Blvd Burnsville 4.0 0.9 499 Doug Cleming 3770 Bradley Rd 2.0 0.5 500 Ricky Lindsy Connelly Springs NC 1 0.2 501 Highland Landscape Box 2622 Boone NC 36.0 8.3 502 Highland Landscape Box 2622 Boone NC 40.0 9.2 503 Allen Bowman Bowman Rd Morganton 2.0 0.5 504 David Beam 112 Quill Dr Morganton 1.0 0.2 505 Linda Lake 6038 Nebo NC 2.0 0.5 506 Matt Spencer 2900 Sids Dr Connelly Springs 2 0.5 unless otherwise noted, all screened compost was purchased for use as a soil amendment. Compost Distribution Tracking Log 2014 Invoice Number Name Address Cubic Yards Dry Tons 551 Highland Landscape Box 2622 Boone NC 48 13.1 552 Void Void 0.0 0.0 553 David Mcclean 107 Morganton NC 1.0 0.3 554 Highland Landscape Box 2622 Boone NC 48.0 13.1 555 Mt Top Landscape Box 13 Burnsville 12 3.3 556 Appalacian 2395 Henderson Mill Rd 12.0 3.3 557 Jim Hawkins 1645 Old.Rd Morganton 6.0 1.6 558 Jim Hawkins 1645 Old Rd Morganton 6.0 1.6 559 Mt Top Landscape Box 13 Burnsville 6 1.6 560 Darryl Whisnant 919 Summer Rd 2.0 0.5 561 Dennis Poteat Union Mills NC 24 6.5 Unless otherwise noted, all screened compost was purchased for use as a soil amendment. Compost Distribution Tracking Log 2014 Bed #sj 16-12 Total volume: Sample collection date: 10-30-14 Compost release date: 11-20-14.'" Invoice Number Name Address Cubic Yards Dry Tons 562 Darryl Whisnant 919 Summers Rd 2.0 0.6 563 Steve Finnster 5011 Sugarloaf Rd 2.0 0.6 564 Void Void 0.0 0.0 565 Vernon Roberts 2133 J Clark Rd 8.0 2.2 566 Susan Stepp 329 Crawly Rd 3.0 0.8 567 Donna Livingston Connelly Springs NC 1.0 0.3 569 Void Void 0.0 0.0 Unless otherwise noted, all screened compost was purchased for use as a soil amendment. 2014 COMPOST WORKSHEET Month/ Day Amendment/ bulking agent IN Cubic yards Amendment/ bulking agent IN Dry Tons Residual IN Cubic yards Residual IN Dry Tons Product OUT Cubic yards Product OUT Dry Tons Product Dist. Cubic yards Product Dist. Dry Tons 1/1-1/5 0 0 0 0 0 0 1/6-1/10 408 80 136 27 0 0 1/13-1/17 151 30 27 5 43 8 1/20-1/24 240 47 80 16 0 0 1 /27-1 /31 400 79 126 25 105 21 Total 1199 236 369 73 148 29 251 49 2/3-2/7 60 12 20 4 30 6 2/10-2/14 684 134 228 45 85 17 2/17-2/21 948 186 251 49 50 10 2/24-2/28 0 0 0 0 0 0 Total 1692 333 499 98 165 32 147 29 3/3-3/7 708 139 236 46 20 4 3/10-3/14 0 0 0 0 60 12 3/17-3/21 180 35 60 12 0 0 3/24-3/28 780 153 260 51 0 0 3/31-3/31 149 29 0 0 0 0 Total 1817 328 556 109 80 16 220 43 4/1-4/5 516 119 172 40 85 20 4/7-4/11 0 0 0 0 15 3 4/14-4/18 672 155 220 51 40 9 4/21-4/25 372 86 129 30 10 2 4/28-4/30 576 133 192 44 0 0 Total 2136 493 713 164 150 35 54 12 5/1-5/2 84 19 28 6 0 0 5/5-5/9 132 30 44 10 45 10 5112-5/18 180 42 60 14 40 9 5/19-5/23 0 0 0 0 0 0 5/26-5/30 408 94 136 31 40 9 Total 804 185 268 62 125 29 57 13 6/2-6/6 708 163 236 54 0 0 6/9-6/13 900 208 300 69 21 5 6/16-6/20 360 83 120 28 56 13 6/23-6/27 168 39 56 13 28 6 Total 2136 493 712 164 105 24 90 21 7/1-7/4 0 0 0 0 0 0 7/7-7/11 108 29 36 10 19 5 7/14-7/18 292 79 110 30 5 1 7/21-7/25 792 216 264 72 60 16 7/28-7/31 270 73 90 24 15 4 Total 1462 398 500 136 99 27 0 0 8/4-8/8 384 105 128 35 30 8 8/11-8/15 296 81 72 20 0 0 8/18-8/22 48 13 16 4 8 2 8/25-8/29 462 126 138 38 20 5 Total 1190 324 354 96 58 16 121 33 9/1-9/5 0 0 0 0 0 0 9/8-9/12 366 100 122 33 0 0 9/15-9/19 0 0 0 0 30 8 9/22-9/26 726 198 242 66 10 3 9/29-9/30 0 0 0 0 0 0 Total 1092 297 364 99 40 11 1 44 12 2014 COMPOST WORKSHEET Month/ Day Amendment/ bulking agent IN Cubic yards Amendment/ bulking agent IN Dry Tons Residual IN Cubic yards Residual IN Dry Tons Product OUT Cubic yards Product OUT Dry Tons Product Dist. Cubic yards Product Dist. Dry Tons 9/29-9/30 0 0 0 0 40 11 10/6-10/10 504 141 168 47 0 0 10/13-10/17 0 0 0 0 0 0 10/20-10/24 576 161 192 54 45 13 10/27-10/31 300 84 100 28 60 17 Total 1.380 386 460 129 145 41 15 4 11/3-11/7 120 34 40 11 40 11 11/10-11/14 304 85 88 25 25 7 11 /17-11 /21 228 64 77 22 0 0 11/24-11/28 0 0 0 0 0 0 Total 652 182 205 57 65 18 2 1 12/1-12/5 186 52 96 27 0 0 12/8-12/12 648 181 216 60 55 15 12/15-12/19 456 128 148 41 40 11 12/22-12/26 0 0 0 0 0 0 12/29-12/31 404 113 168 47 0 0 Total 1694 474 628 176 95 27 0 0 ANNUAL -RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: NC0026573 Laboratory: 1) Statesville Analytical Facility Name: Catawba River Pollution Control Facility 2) NPDES # or WQ0002127 3) WQ#: 4) WWTP Name: Catawba River Pollution Control Facility 5) Sample or Composite Date Percent Solids M ® "I certify, under penalty of law, that this document was. prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Si afore of Preparer Date aC4 5 3 City of Morganton I; ) Box 3448 I-organton i tered 2/6/2014 Reported: 2/14/2014 F -r: Compost Analytical Results NC 28680 Date mple ID Parameter Cust ID Result Units Method Analyzed Analyst 140206-10 % Solids Compost 76.9 % SM2540B-1997 2/7/14 CL 3206-10 Fecal Coliform MTF Compost 20,806 MPN/g SM92210E-2006 2/7/14 CL espectfully submitted, tjg ena Myers NC Cert #440, 'CDW Cert #37755, ?A NCO0909 P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697 Analytical Results City of Morganton 'O Box 3448 ._Iorganton NC 28680 :ntered 4/1/2014 Reported: 4/4/2014 I or: Compost Date "ample ID, Parameter Cust ID Result Units Method Analyzed Analyst 140401-11 % Solids Compost 74.1 % SM2540B-1997 4/1/14 CL 40401-11 Fecal Coliform MTF Compost 54 MPN/g SM92210E-2006 4/1/14 CL 'respectfully submitted, )ena Myers NQ,Cert #440, -UCDW Cert #37755, EPA NCO0909 P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697 Analytical Results I u'ity of Morganton Box 3448 organton. NC 28680 itered 7/10/2014 keported: 7/29/2014 F; _ 'r: Compost Testing mple ID Parameter Cust ID Result Units Method Date Analyzed Analyst 140710-6 % Solids Compost 73.7 % SM2540B-1997 7/10/14 CL 0710-6 Aluminum- Compost 14,677 mg/kg SM 3111 D 7/24/14 MD 140710-6 Arsenic- Compost 0.0068 mg/kg SM3113 B 7/29/14 MD 0710-6 Cadmium- Compost 0.75 mg/kg SM3113B 7/22/14 MD 3710-6 Calcium-Flame/solid Compost 9,202 mg/kg SM 3111 D 7/29/14 MD lA0710-6 Copper-Flame/solid Compost 0.175 mg/kg SM3111B 7/23/14 MD D710-6 Fecal Coliform MTF Compost 27 MPN/g SM92210E-2006 7/10/14 CL 140710-6 Lead-furnace/solid Compost 4.5 mg/kg SM3113B 7/22/14 MD D710-6 Magnesium- Compost 18,838 mg/kg SM 3111, D 7/29/14 MD 140710-6 Mercury -solid Compost 0.73 mg/kg 245.1 7/28/14 MD .3710-6 Molybdenum - Compost 10.7 mg/kg EPA200.7 7/17/14 ENCO �r_f3710-6 NH3N-solid Compost 4635 mg/kg SM4500NH3BE 7/11/14 MD j "0710-6 Nickel-Flame/solid Compost 0.26 mg/kg SM3111B 7124/14 MD 3710-6 NO3NO2-solid Compost 368 mg/kg SM450OF/A 7/15/14 CL 140710-6 pH Compost 7.52 STD units SM4500HB-2000 7/10/14 CL 3710-6 Potassium-ICP/solid Compost 4060 mg/kg EPA200.7 7/17/14 ENCO 140710-6 Selenium -solid Compost 136 mg/kg SM 3113 B 7/25/14 MD b710-6 Sodium -solid Compost 555 mg/kg SM 3111 B 7/24/14 MD 140710-6 T.Phosphorous-solid Compost 3460 mg/kg SM450OPE 7/17/14 CL 3710-6 TKN-solid Compost 2267 mg/kg SM4500NHME 7/14/14 CL 3710-6 Total Solids Compost 736,685 mg/L SM2540B-1997 7/10/14 CL P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697 Aug 13 14 08:27a Statesville Analytical 7048782787 p,1 Analytical Results 'City of Morganton PO Box 3448 Morganton NC 28680 Entered 7/1012014 Reported. 8/12/2014 For: Compost Testing Sample !® parameter Cust ID gate Result Units Method Analyzed Analyst: 140710-6 % Solids Compost 73.7 % SM25408-1997 7t10114 CL _ 140710-6 Aluminum- Compost 14,677 mg/kg SM 3111 D 7124/14 MO 140710-6 Arsenic- Compost 0.0068 mg/kg SM3113 B 7/;29/14 MC 140710-6 Gadmium- Compost 0.75 mg/kg SM31138 7/W14 MD 140710-6 Calcium-Flame/solid Compost 9,202 mg/kg SM 3111 0 7/29/14 MD 140710-6 Copper-Flame/solid Compost 0.175 mg/kg SL-131118 7/23114 iVID 140710-6 P7ecal Cofiform MTF Compost 27 MFtN/g SM9221 CE-2006 7/10114 CL 140710•6 1 Lead-furnac"olid Compost 4-5 m '� 9• •9 SM3113..R r 7,22/14 NiD ^ 14C7106 P/agnes+um- Compost 18,8:38 mg/kg SM31110 712S114 MD 140710-6 hle+cury-solid Compost 0.73 mg/kg 245.1 7;28114 MD 140710-6 Molybdenum - Compost '10.7 mglkg EPA200.7 7i17/14 ENCO 140710-6 NH3N-solid 'Compost 4636 mglkg SM450014H38E 7/11il4 IV,D - 140710-6 N:ckel-Flamelsolid Compost 0.26 mg/kg SIMI116 7/24/14 MD 140710-6 Nv3Ti02-solid Compost 368 mg/kg SM4500Fr14 7/15/14 CL 140710-B pH Compost 7.52 STD units SM4500HB-2000 7.'1Oil 4 CL 140710-6 Potass;urn-ICI'/solid Coat ost p 4060 mg/kg EPA200.7 7117114 ENCO 140710-6 Selenium -solid Compost 0.2 mgfkg sM 3113 B 7/25/14 MD ' 140710-6 140710-6 Sodum-solid T. Phosphorous Compost. —,I 555 mglkg SM 3111 6 7/24/14 MD -solid Co post 3460 mg.'kg SM4500PE 7117114 CL 140710-6 TKN-solid Compost 2267 mglkg SM4500NH3BE 7i14;14 CL 140710-6 i Total Solids Compost 736,685 mglL SM25406-1997 7/10/14 CL P.O. Box 228 9 Statesville, Norrh Carolina 28687 0 '704/87W459 7 i Analytical Results City of Morganton PO Box 3448 Morganton, NC 28680 i Receive Date: 10/30/2014 Reported: 10/31/2014 For: Comments: i Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 141030-08-01 Fecal Coliforms Compost <27 MPN/g SM92210E-2006 10/30/2014 WL 141030-08-01 Percent Solids Compost 74.7 % SM2540B-1997 10/30/2014 WL Respectfully submitted, 61�14 Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0002127 1) Blue Ridge Labs Facility Name: Catawba River Pollution Control Facility 2) Statesville Labs NPDES # or NCO026573 3) WQ#: 4) WWTP Name: Catawba River Pollution Control Facility 5) Sample or Composite Date ^Conc. Limit (mg/kg)a 2/6/14 4/1/14 7/10/14 10/3014 Conc. Limit (mg/kg)a 2/6/14 4/1/14 7/10/14 10/30/14 Percent Solids (%) NA 71.0 74.0 70.9 72.5 Aluminum NA 31923 <0.24 17240 16995 Arsenic 75 <1.3 65 1.2534 <2.5 pH NA 7.7 7.2 7.9 1 7.6 Cadmium 85 1.18 1.08 0.4019 30.8 Sodium NA 6195 865 2420 2096 Copper 4,300 331 164 119 397 Calcium 'NA 33384 11814 13943.5 14826 Lead 840 <1.3 <2.4 3.6 36 Potassium NA 4161 1693, 3666 2942 Mercury 57 0.2089 0.1806 0.3857 0.0275 Magnesium NA 5382 1781 11306.5 3264 Molybdenum 75 4.56 <0.24 5.4845 <0.25 Nickel 420 72 1 7.17 14.33 12.1 Selenium 100 <1.3 1 <2.4 1.45 51 Zinc 7,500 646 421 652 843, Phosphorus NA 36307 10524 14343 25486 TKN NA 25556 21303 6051.5 15963 Ammonia -Nitrogen NA 13113 8890 9430 12297 EEJ Nitrate and Nitrite NA 120 1 17.5 192.3 53.8 "I certify, under penalty -of law, that this document was prepared' under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the -information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing,violations." ignature of Preparer BlIte- Ridge, -tabs PO Box 2940 q Lenoir, NC 28645 .828-728-0149 blue'ridgelabsiep lallslenoil@gmail.com p Client City of'Mor�gallton P. 0.. Box 3448 Morganton, NC 28655 Attention; Ms. C. Benton Dafe,'Rec6ived: I I -Feb-I 4 Report Date,,. 7-F&-14 Sample Date: 067Fpb-14 BRL 9: BRL-20.*14-0073 Lab- Sample ID: L-S I D-20 14 -- 0*04 05 Client Sample IM. Compost .... ... ... . . ..... ...... . ... .... . . . ..... .......... . .. Analysis V*sjs Analysis Parapieter; . .... .. ... Total Phosphorus Al by ICP-AE-S As by ICP-AES. Ca byJCP-AES -Cd by ICP-AES. Cu by fCP7AES- K by ICP-,AES Mg by, (CP-AES Mo by,[CP-AES Na by ICP-AES Ni by ICP-AES Pb by ICP-AES Se by ICP-AES Zn by ICP-AES Mg by Cold Vapor AAS Result Unit Method. Time; ... . Date ...... ............... Analyst . . ... ...... 3007 n8. dry Tng/�g EPA 20.0.7 1.2.-.5. 1 2/20120.1.4 KCJ, 3, .J 923 81.9 d dry mg1kg 46-6 SW-9 010 ]�:51' 2/2Q/2014 KCJ GD 13 dry ffimg/kgSW-846-601,U 12:44, 2/20"20 14 KCJ 33384 400 dry mg/kg SW-846-.60M 12:51 2/20/2044 KCJ iA 0256 dry. djglk g S.W-.846�,6910 12:44, 2/20/20,14 KCJ- 331 16 -4 dq-:Rig/kg -SW-846-,60 10 -5 j2� 1 2/20/2014 KCJ 4116-11 $1.9, dry hid/kg -SW-846-6010 12.:51 2/20/2014 KCJ 5382 81.y. m& dry 9 SW-846-6010 1151 2120/201,4 KCJ 4,56 0.13. g/k -dry'rri g SW-846--�60:1 0 12.44 2/20�/'-Q'14 KCJ 6195 409 447-Y nlg/J g SW-946-60 10 12:51 V2b/2bJ4 KCJ 72 0.1.3 dry'rng/kg SW-846-60-10 12:44 2/20/22044 KCJ 1.3 dry rng/kg SW-846-0,10 12.51. 2,120/20,14 KCJ 1.3 dryrng/k g SW-846-60.10 12:51 2/20/2014 KCJ 64.6 0.13 dry mg/kg. SW-846-6010 12--.51 2/20/2014 KCJ 0.20819 0,0276 dry, mg/kg SW-846-7471 1*5:19' 2/27/2014 KCJ Reported. By: 0 00, r wkqenotcd. NCLAboralory. Certiffew �q-o. 175 P4ge I of 4. Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-oi49 Client Attention: Date Received City, of Morganton P. 0'. *Box 3448 Morganton, NC 28655 M s. C, Benton I I -1--eb- 14 Report Date: 03-Mar-I 4 Sample Date- 06-Feb- 1.4 13RI, 4: BR.L,2014-0073 Lab.Saruplle ID:- USID-20-1 4-00405 Client Sample .10. Compost - .blueridgelab.sienoir@.�gmail.,Com Reissued to due to a typographical error .. ...... . . . .. ... Analysis Analysis Parameter Result MQL UnIt Method Time Date Analyst Total phosphorus .. ....... .328- . dry mglkg EPA.200,7 12:51 2/20i2014 KCJ AI by ICP-AES 31 W-3 81.9 d-ry mg/kg- SW-846-601 0 12:51 21120,12014 KCJ As by ICP-AES 1..3 dry'mSikg SW-846-601 0 12:44 . 2/20/2014 KCJ Ca by ICI?-AES 33384 .409 ilry Mg/kg. SW-846-6010 12,-5:1 2120,12014 KCJ Cd by ICPABS 1.19 0:025-6 dry mg/kg S-W-846-60t0 12'.-44, 2/20/2014 KCJ Cu by ICP-AES :331 16.4 dry i -n alk-g: SW-846-601 0. 12:51 2/20/2014 KCJ K by ICI'-AES 4161 81'.9 dry mg/kgSW-846-601.0 12:5.1- 2120/2014 KCJ N19 by ICP-AES 5382 9119 dry me/kg W-846-601 0, 12:5): 2/20/2014 KCJ Mo by !CP-At-S 4,56 0.13 dry, mg/kg SW-846-6010 12:44 2120;20.1-4 KCJ Na by IC?-A.ES 6195 409 dry rri g/kg SW-846-6-010 12:51: IV?- 01220 14 KCJ 'Ni by ICP-AES 72 6.13 dry mg/kg SW -846-6010 12:44 2/2V-20 14 KCJ Pb by fC?-AT-'S 1.3 dry ngkg SW,7846-6010- 12.-51 2/2012014 KCJ Se by ICP-AES 1.3 dry mglkg SW-*846-601 0 1151 2/.20/2014 KCJ Zn,by ICP-AES 646 0.13 dry mwk SW -846-�601 0. 12:5.1 2120/2014 KCJ H g by Cold. VapOr AAS 0N89 0276 dry mg/kg SW 9.4.6-7471 15,,19. 2/2712014 KCJ P,&p By: S. j -'nso4, D.R. Wessinger -Concentrations are, below Minimum Quantification Limit -except where noted, NC Laboratory Ce r 01,004 te -Stla 275 Page I of 4 - � t Blue Ridge Labs PO Box. 2940 Lemoir,, NC 28645 828-728=0'149 blueridgela.bslenoir@gmaii.com. Client: City. of Morganton P. O. Box 3448 ZvMrganton, NC 28655 Attention; Ms. C. Benton Date Received- 11.-Feb-14 Report D:te: 27=Feb-14 Sample Date: 06-Feb-14 B12L #: B.R:L-2014-0073 Lab Sample ID: LSID-2014-00406 Client Sample. ID: Compost Analysis Analysis Parameter Result MQL CTnit. Method Time, Date. Analyst Ammonia Nitrogen 13.113 118 drymg/kg Ammonia 0:10 2i2112014 KCJ Reported By: '00oo< Johnson,, D.P. Wessinger * Concentrations are Minimum Quandfic tio.n Limit:except where noted. NC Laltoratory Certificate No. 275 " Page 2 of 4 Blue Ridge Labs PO Rox 2940 Lenoir, NC 28645 -828-7280149 blueridgplabsienoir@gmaii.com Client: City of Morganton R 0. Box 3448 Morganton, NC 28655 Attention: , Ms. C. Benton Date Received: 11 -Feb- 14 Report Date: 27-Feb- 14 Sample Date: 06-Feb-] 4 BRL #: BRL-:2014-00.73 Lab Sample TD- LSJD-2014-004,09 Client Sample- M: Compost .. ........ - ......... .. . .. . .... Parameter R6$ult MQL .... .. ... . Analysis Unit Method Timei ! . ........... . . ..... Analysis Date ate Aikalyst Nitrate + Nitrite Nitrogen (M+ 120 10.2 dry-mg/kg SM19450-N j6:46 1/20'2014 KCJ Total Kjeldahl Nitrogen: ("INN) 255-56 234 dry-mg&g 5919 4500-N* 1.5:12 21/27/201A KCJ Reported By, . ... .. ...... i0mob, D.R. WOsihaer Concentrations are w Minimum Quarititcatioir Limit. except �yher:c noted. C Laboratory Certificate No. 275 Page 4 of 4 I Blue Ridge Labs, -PO Box. 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoirOgmail.conj Client: City of Morganton P. O. Box 3448 Morganton, NC 28655 Attention- Ms. C. Benton Date Received: I I-Feb-14 Report Date: 27-Feb- 14 Sample Date: 06-Feb- 14 BRL il: .BRL-2014-0073,* Lab Sample ID: 1910-20.14-00401 Client Sample ID- . . ...... .... .. . .... Compost. ............. . . Parameter . .... . .. .. ... ..... — ...... . Resu . .... ........ ....... . . . .. . .. Result MQL .............. ....... . . ..... .. Unit Method ....... . . . Analysis Time; e: Analysis Date Analyst % Solids 71.0 O.J. % % Solids .... . ..... 10:33 ..... 2/11V20,14 ........................ . KCJ Pit Available Nitrogen '13223 1.28 dry mg/kg Plant Av4ilabl: 10.: 15 2,121 /2 G 14 KCJ pH 7.7 0.1 S.0 SW-846-9040 10:54 2/12/2014 KCJ Reported By:: . ........ . . .......... .. Johnson, Wessinger iger —sh Coficeptratioro are aw Minimum Q444tific.ation Lim it except -here noted, w ...0 Laboratory Certificate N6,..275 Page 3 of 4 w Blue Ridge Labs PO Box 2 ' 940 Lenoir, NC 286,45 828-728-0149 blueridgelabstenoirftmail.cm Client: City of Morganton P. 0... Box 3448 Morganton, NC 28655 Attention; Ms. C. Benton Date.Received: 07-Apr- 14 Report Date: 23-Apr- 14 Sample Date: 0.1 -Apr- 14 BRCS #: BRL-20.1-4-0182 Lab Sample ID: LSID-2014-00942 Client Sample ID; Coml.�Qst Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 10524, 4.8 dry m&.9 EPA 200.7 15:.34 4/22/2014 KCJ Al by fCP-AES .0, 24 dry mg/kg %SW-846-6010 15:34 4/22/2014 KCJ As by 65 2A dry mg/kg SW-846-60 10 15.34 4/22,L?O 14 KCJ Ca by ICP-AES 11814 6.1 dry Aig,/kg SW-846-,6010 15:34 4,,222/2014 KCJ Cd by ICP-A8S 1.08 0.0484 dry mg/kg SW-846-6010 15.34 4/22/2014 KCJ Cu by ICP-AES 1.64 0.24 dfy mg/kg SW-84&60.1 0 1534 4/22/2014 KCJ K by I.CP-AES 1693. 1.2 dry mg/1(1g SW-846-%601.'O 15:34 3A 4/22/2014 KCJ Mg by IQ - P-AES 1781 1.2 dry, ;in Ik . 9 . g SW-846-,60 10 15:34' 4122/2014 KCJ Mo by ICP-AES 0.24. -dry mg/kg SW-846-601 0 15.,34 4122/20 14 KCJ Na by I CP-AES 865 6.1 dry. mg/kg SW4466010 15:34 4/22/2014 KCJ Ni by ICP-AES 7.17 0.24 dry, mg/kg ,SW-846-6o i o 15:34 4!22/2014 KCJ Pb by ICP-AES 2,4 'dry mg/kg, SW-846-60-10 15:34 4/22/2014 KCJ Se by ICP-AES 2A dry mg/kg SW-846-601 0 1534 4,122/2014 KCJ Zn by ICP-AES 421 0.24 dry, mg/kg SW-846-60.1.0 15:34 4/22/201:4 KCJ Fig by Cold Vapor AAS 0,1806 .0.0237 dry rng/kg. $W-846-7471 16.15 4,11,6/2014 KCJ Reported ,By: J. Johnson:, D.R. Wessinger J.; Us" C onmntrations are oW Minimum Quantification Limit except I where noted. NC Laboratory'Certificate No. Page I of 5 Flue Ridge Labs PO Box 2940 Lenoir, NC -28645 828-728-0149 blueridgelabslenoir@gmaii.com Client: City of Morganton P. U. Box.3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 07-Apr-14 Report -Date: 23-Apr- 14 Sample Date: 0 1 -Apr-] 4 BRL 9: BRI.,-2014-0182 Lab Sample ID:- LSID-2014-00943 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Tine Date Analyst Animonia Nitrogen 8890 131 dry:mglkg. Ammonia 15�09 4/18,12014 KCJ Reported By. .... ... ... n s I Johnson, D.R. Wessinger low M low Minimum Quantification. Limit except Where noted. *.Concentrations are inimum Quantification NC Laboratory Certificate. No. 275 Page 2 of 5 Blue Ridge Labs PO Box 2940 Lenoir, AIC 28645. 828-728-0149 Client: City of Morganton P. 0. Box 3448 Morganton, 'NC 28655 Attention: Ms. C- Benton Date Received: 07-Apr-14 Report Date: 23-Apr-14 Sample Date: 01-Apr-14 BRL #: BRL=2014-0182° Lab Sample ID: I-SID-2014-00944 Client Sample Ill: Compost, Parameter Nitrate + Nitrite Nitrogen (N2+- Total Kjeldahl Nitrogen (TKN) Result MQL 17.5 20 2*1303 128. blueridgelabslenoir@gmail.com Analysis Analysis Unit. Method Time Date Analyst dry mg/kg SM1,9 4500-N 16:43 4/16/2014 KC.J ,dry mb g. SM19 4500-N 9:40 41)18/2014 KCJ Reported By: eJ.son, D.R. Wessinger Concentrations arem Quantification Limit except. where noted. NC Laboratory Certificate No. 275 Page 3 of 5 I Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 bluetidgelabsienoir@gmaii.com Client: City of Morganton P. 0. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 07-Apr- 14. Report Date: 2' ) -.A.p r- 14 Sample Date: 0 1 -Apr- 14 BR L #: BRL-2014-0182 Lab Sample ID: LSID-2014-00945* Client Sample ID. Compost Analysis Analysis Parameter Result MQL Unit -Method Time . . Date, Analyst . . ....... .. .. ...... % Solids ....... .... - 74.0 0.1 % % Solids 11:45 4/10/2014 KCj PH 7.2 0.1 su SW-846-9040 12:10 4/1012014 KCJ Reported By: ... . ...... J. Johnsoin, D.R. Wessinger Mini Concentrations are OwIV Minimumfn Quantification Li*it except Where noted. NC Laboratory Certificate No, 275 Page 4 of 5 Blue Ridge Labs PO Box 2940 Lenoir. NC- 2,8645 828-728-0.149 b,lueridgelabsienoir.@gmail.com Client City of Morganton P. 0. Box 3448, Morganton, NC .286.55 Attention: Ms. C. Benton Date Received: 07-Apr-14 Report Date: 23-Apr-14 Sample Date: 02-Apr-14 BRL #., BRL-2014=0182 Lab SampleID: I-SID-2014-00946 Client Sample W.: Compost 2 Parameter Result MQL Unit Method As by ICP-AES 66.3 0.24 drymg/kg SW-846.6010 I .Analysis Analysis Time Date Analyst 15:36 4/221-12014 KCJ Reported By: 1J. J�obngon, D.R. Wessinger �V n1m Concentrations'ar low Minjinum.Quantiffikati.on Limit except where noted. NC Uaboratory, Certificate No.. 175 Page 5 of 5 Blue Blue Ridge Labs PO Box 2940 Lenoir, N-C 28645 828 -72&0149 Client City of Morganton P.O. Box 3448 Morganton, NC 28655 Attention: Ms. C—Benton Date Received: I O-J'u 1- 14. Report Date: 29-Jul-14 Sample Date: I O-Ju 1- 14. EIRL 9: BRL=2014-0450' Lab Sample JD- LSfD-201:4--02036 Client Sample 11): Compost .. ... ......... Parameter 'I'otal Phosphorus A.1 by fCP-AES As by ICP-AES Ca by I.CP-AES Cd by IC-P-AES Cu by ICP-AES K by'ICP-AES Mg by ICP-AES Mo by ICP-AES -Na by ICP-AES Ni by fCP-AES Pb by ICP-AES S'ebylCP-AES Zn by ICP-AES . Uig by Cold Vapor AAS Result 24626 19803 18685 283 3272 37-75 4285 29A 652 0.0414 bluerid.gelabslenoir@gmaii.com . . . . ................ I ................ . .. I ........... Analysis MQL ... ... .. . ........ Unit . . .. . ... .... __... ... .. Method .. ......... .... Time . . . .............. ........ 86 dry mg/kg EPA 200;7 11:29 21.5 dry mg/kg SW-846-6010 11:29 2.7 dry mg/kg W-846-6010 11:29 .108 dry mg/kg SW-.8.46-'6010' I1,:29 0.0538 dry m.g/kg SW-846-6010 1129 4.3 dry mg/kg SW-846-6010 11:29. 21.5 dry mg/kg SW-846=6010 11:29 2.1.5 dry mg/kg S.W-846-601 0 11:29. 0.269 dry mg/kg SW-846-6010 11:29� 21.5 dry in:g/k.g SW-846'-6010 11:29 0:269 dry mg/kg SW-846-6010 .11:29 2,.7 Oryrng/kg SW-8.4 6-601 0 1, 1 2.7 dry mg/kg SW-846-601 0 11:29. 4.3 dry.rng/kg SW-946-60 I b 10:29 0.0 141 dry-mg/kg SW-846-7471 15:14 Analysis Date ............. ...__.____._.. Analyst ....... . .......... 7/29/2014 KC] 7/29/2014 KCJ 7/29/2014 KCJ 7/29/2014 KC] 7/29/2014 KCJ 7/29/2014 KCJ 7/29/2014 KCJ 7/29/2014 :KCJ 7/2-9/2014 KCJ 7/29/2014 KCJ 7/29/2014 KC] 7/29/2014 KC.1 7/29/20.14 KCJ 7.129/20.14 KCJ 7/21/2.014 KCJ O'tS�, s o n Reported BY: .. . . . ...... .... . ................ ..... .... .... . --------- J. ..hnson,,D..R, Wessinger -Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificat.e;Noi.275: Page I of -4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 82&728-0.149 blueridgeiabslenoir@gmail.com Client ; City of Morganton P. 0. Box 3448 Morganton, NC 2W5 Attention: Ms. C. Benton Date Received; 10-Jul-M . Report Date:. .29-Ju1- 1`4 Sample Date: 1.0-Ju.1-14 BRL.4. BRL720:1.4-0450 Lab Sample ID: LSID-20.14-02037 Client Sample. ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst ..,.... ... ......,......,....................... .. Ammonia Nitrogen ..._..................._.... ___..._..... ... ......... .................. ,.....,........._....,...... .... .... 14225 125 dry rpAg Ammonia 13:06 7/22/2014 KCJ I, I stf 'Reported By: _ _ _.... r...... ... ...... ........_._............ ... .... ..... .__............ .... _. S. ohnson, D.R. Wessinger * Concentrations are below Minimum Quantification.Limit except where noted. a NC Laboratory Certificate No. 275 Page 2 of 4 Blue lue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-01-49 Client City of Morganton P. O. Box 3448, Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 1.0-Jul-14 Report Date: 294ul-14 Sample Date: I O-Jul-14 BRL BRL-20,14-104-50 Lab Sample ID: I-SID-201 4-02038 Client Sample ID: Compost .. . ........ . . . .. . .. .... ................ Parameter Result MQL ...... ...... . ........ - . ... . ............. ........... ... .. . ...... .. ...... .. — Nitrate + Nitrite Nitrogen (N2+ 16.6 41.3 Tota],Kjeldah,l Nitrogen (TKN) 9836 144 blueridgelabslenoirftmail-com . .. . ........ .. Analysis I ... ..... . .... Analysis unit Method ....... ........... .. Time ........................ Pate Analyst . . ... ....... .. . - ... ...... ...... I . . .... .. drymgikg SM194500-N 16:14. 7/22/2014 KCJ dry rnglkg SM.194500-N 10:31 7/23/2014 KCJ Reported By: .. .......... .. ... ........ . . ...... nsWessinger on, D.R. Wessinger Concentr9tions are beloW.TO.jnimt;w Qpantification,Limit except where noted. NC ;Laboratory Certificate:. o. 275 Fage 3 of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0-149 Client: City of Morganton P. 0. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: I O-Jul- 14 Report Date.: 29-Jul- 14 Sample Date: .1 O-Ju 1- 14 BRI, 4: 8RL-2014-04-50 Lab Sample ID: LSID-2014-02039 Client. Sample ID: . .. ...... ...... . .. ... Compost .... .. ... . ...... ..... Parameter Result % Solids 68.1 pH T9 Reported By: blueridgelabsienoir@gmail.com . ... . .... . ....... .... -- . ............ .................... ........ ... . .......... .... ..... . Analysis ......... . .. . I ...... Analysis MQL Unit Method Time - -- ... ... ..... ...... ... ..... ........... .. ..... . . ..... . - ..... ...... Date Analyst .............. ... ... 0.1 % % Solids 12-16 7/16/2014 KCJ 0.1. SU SW-846-9040 12:25 7/16/2014 KCJ 5.. . 4ohnson, D,R.. Wessinger Concentrations are below,Minim um Quantification. Limit. except where noted. NC Laboratory CertiticateNo. -275 Page 4 of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: City of Morganton P. O. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 30-Oct-14 Report Date: 20-Nov-14 Sample Date: 30-Oct-14 BRL #: BRL-2014-0768 Lab Sample ID: LSID-2014-03412 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Total Phosphorus 25486 80.3 dry mg/kg EPA 200.7 14:46 11/13/2014 Al by ICP-AES 16995 40 dry mg/kg SW-846-6010 14:46 11/13/2014 As by ICP-AES * 2.5 dry mg/kg SW-846-6010 14:46 11/13/2014 Ca by ICP-AES 14826 100 dry mg/kg SW-846-6010 14:46 11/13/2014 Cd by ICP-AES 30.8 0.8032 dry mg/kg SW-846-6010 14:46 11/13/2014 Cu by ICP-AES 397 4 dry mg/kg SW-846-6010 14:46 11/13/2014 K by ICP-AES 2942 1.3 dry mg/kg SW-846-6010 14:46 11/13/2014 Mg by ICP-AES 3264 1.3 dry mg/kg SW-846-6010 14:46 11/13/2014 Mo by ICP-AES * 0.25 dry mg/kg SW-846-6010 14:46 11/13/2014 Na by ICP-AES 2096 100 dry mg/kg SW-846-6010 14:46 11/13/2014 Ni by ICP-AES 12.1 0.25 dry mg/kg SW-846-6010 14:46 11/13/2014 Pb by ICP-AES 36 2.5 dry mg/kg SW-846-6010 14:46 11/13/2014 Se by ICP-AES 51 2.5 dry mg/kg SW-846-6010 14:46 11/13/2014 Zn by ICP-AES 843 0.25 dry mg/kg SW-846-6010 14:46 11/13/2014 Hg by Cold Vapor AAS 0.0275 0.0124 dry mg/kg SW-846-7471 16:48 11/13/2014 Reported By: S. I * Concentrations are below son, D.R. Wessinger imum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 4 Analyst KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ KCJ Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : City of Morganton P. 0. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 30-Oct-14 Report Date: 20-Nov- 14 Sample Date: 30-Oct-14 BRL #: BRL-2014-0768 Lab Sample ID: LSID-2014-03413 Client Sample ID: Compost Parameter Result MQL Ammonia Nitrogen 12297 134 blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time Date Analyst dry mg/kg Ammonia 9:41 1 1/20/2014 KC.1 Reported By: S. J. .nson, D.R. Wessinger * Concentrations are below inimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : City of Morganton P. O. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 30-Oct-14 Report Date: 20-Nov-14 Sample Date: 30-Oct-14 BRL #: BRL-2014-0768 Lab Sample ID: LSID-2014-03414 Client Sample ID: Compost Parameter Result MQL Nitrate +Nitrite Nitrogen (N2+ 53.8 8.6 Total Kjeldahl Nitrogen (TKN) 15963 132 blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time Date Analyst drymg/kg SM 19 4500-N 16:50 10/30/2014 KCJ dry mg/kg SM19 4500-N 15:09 11/11/2014 KCJ Reported By: S. J. J n, D.R. Wessinger Concentrations are below Mi um Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : City of Morganton P. O. Box 3448 Morganton, NC 28655 Attention: Ms. C. Benton Date Received: 30-Oct-14 Report Date: 20-Nov-14 Sample Date: 30-Oct-14 BRL #: BRL-2014-0768 Lab Sample ID: LSID-2014-03415 Client Sample ID: Compost Parameter Result MQL % Solids 72.5 0.1 Plt Available Nitrogen 12351 142 pH 7.6 0.1 blueridgelabslenoir@gmail.com Unit Method % Solids dry mg/kg Plant Availabl SU SW-846-9040 Analysis Analysis Time Date Analyst 16:03 10/30/2014 KCJ 10:06 11/20/2014 KCJ 16:12 10/30/2014 KCJ Reported By: IMs.j. n, D.R. WessingerConcentrations are bel' um Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 4 2014 Plant Available Nitrogen Calculations Sample Date Mineralization Rate Application Rate surface TKN NH3-N (NO3 - NO2 - N) P'.A.N. 1st Quarter 2/6/2014 0.10 0.50 25,556 13,113 120.0 7,921 2nd Quarter 4/1/2014 0.10 0.50 21,303 8,890 1 17.5 5,704 3rd Quarter 7/10/2014 0.10 0.50 6,052 9,430 192.3 4,569 4th Quarter 1 10/30/2014 0.10 0.50 15,963 12,297 53.8 2,051 Calculation: [(MR) X (TKN — NH3)] + [(AR) X (NH3)] + (NO3 — NO2 — N) = P.A.N. Mineralization Rate (MR) Composted Sludge = 0.1 Anaerobically Digested Sludge = 0.2 Aerobically Digested Sludge = 0.3 Unstabilized Primary and Waste Activated Sludge = 0.4 Application Rate (AR) Surface applications lose Y2 of their NH3 available to plants due to evaporation (0.5). Subsurface applications do not lose NH3 0.0). 2014 Sodium Absorption Rate Calculations SAMPLE DATE Percent Solids Sodium (mg/Kg) Sodium (ME) Calcium (mg/Kg) Calcium (ME) Magnesium (mg/Kg) Magnesium (ME) SAR RATIO 1st Quarter 2/6/2014 71.0 6,195 191.24 33,384 1,185.13 5,382 318.44 6.975' 2nd Quarter 4/1/2014 74.0 865 27.83 11,814 437.12 1,781 109.83 1.683 3rd Quarter 7/10/2014 70.9 2,420 74.60 13,944 404.30 11,307 668.03 3.094 4th Quarter 10/30/2014 72.5 2,096 66.07 14,826 537.44 3,264 197.20 3.447 Calculation: SAR = [Na+] / {([Ca2+] + [Mg2+]) / 21" Na: Sodium (mg/Kg) Equivalent weight: 23 Ca: Calcium (mg/Kg) Equivalent weight: 20 Mg: Magnesium (mg/Kg) Equivalent weight: 12 m COMPOST BED SHEETS 2014 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio:_ to ! mix Depth of blanket material: S Blowers in use: p i"ec-_ Point 1 Point 2 Bed # 6 Point 3 1= Extended Aeration Compost Bed Data Sheet Bed # E Bulking agent to sludge ratio _,3_ : �_ Daily Monitoring Blanket material used: c. Day Bed Temp. °C Point 1 Point 2 Point 3 Date Blower Cycle ON/OFF Initials Blowers in use: 0 A.)C Comments: 1 V ,-I Sz 2 C, l 2 3 0 - _ / u 4 63, - i AD 5 bt 3 61, o b3, 6 le) 141 7 2��- �. r 8 9 G L 44 10 1- G , 2 - /,Y - ro 11 7. 6. 7_3 2- /5---� ��PLO 12 6-3 167. 7 /6,/ 2 C 13 / -/ 14 47, ti 15 - 9-� 16 `7 - O - / .. 17 2-fit �� 2�,� �►, J 18 Date pile taken down Date screened Date collected for analysis: Date available for release: 19 2 -.2 20 , 21 Pile to have one foot of cover material Bed temp. points 2 1 Lnaquu AEA anion k,vmpost Elea Da a Sheet —` Bed # Bulking agent to sludge ratio: to mix _ Daily Monitorin Depth of blanket material: — Bed Tem °C Blower \�- � �r his Da Point 1 Point 2 Point 3 Date C cle Initials Blowers in use: 1 �,� 2 SS S S S�- S'7. Ss 31 S�, 4 6. - 5 Ste• 2 �7 - r 7- o 61 A/ � gS � S' O 10 s` (o - -I 2 11 12 13 `l. 12 8 /0 i6 14 - �•- r 15 16- 17 18 20 21 6 �, �2 Z 1 9 Point 2 Point 1 - Point 3 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio 3 to mix Depth of blanket material Blowers in use: a(\ Point 1 Bed # 1-7 ® clid Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio to r mix Depth of blanket material: Blowers in use: (' /Jr Point 1 Bed #_'77 Daily Monitoring Bed Tern°C Blower Date C cle Initials Day Point 1 Point 2 Point 3 1 -2, Y L,3 ` - / Z 16 s� 2 3 ,b `? &, S- 7, 9 51 6 6 7 6 8 9 10 6 h .9 6(" i 59.9 .ir4! pw 11 (02,, 66_9 57 'S 12 o -t__ _ ./7•/v d 13 2 A G Y �- 14 2 to /. - / 15 6 - 6g, 6 3 � 2,o 17 1� 18 19 // Q b r 1 61 1 l �5 r _2-/y r0 21 G 2. 4. 21, 57 G. Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bed # Bulking agent to sludge ratio_ : Daily Monitoring Blanket material used: Day Bed Temp. °C Point 1 Point 2 Point 3 Date Blower Cycle ON/OFF Initials Blowers in use: Comments: 1 ! - -�, 7 — / f o A2 i0 2 ,z Gr, /. -�zV—! J,b .-X1 31 - i a 4�'3 (0 2, - l �J,o d 8 t? a 9 I 6 5,� 10 , il 11 6 -.2 13 6 J�, 3 6 /, g - Y- /� /►� 15 ��, g L/O 16 6 9 d y 3 17 y �4, i / w Date pile taken down Date screened Date collected for analysis: Date available for release: 19 < << -21 — Lzy/ 20 cf ��, -- - 21 2 7a, �� / ✓J Pile to have one foot of cover material 9 Bed temp. points 2 1 I Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio 3 to / mix Depth of blanket material: 12 2 6e-- h Blowers in use: 0, Point 1 ='• • A Daily Monitorin LDaZ_ Point 1 Bed Tem Point 2 °C Point 3 Date Blower C cle 1 1 2 3 3 60� s� z. 6�, ( �� z s s?' 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Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bed # Bulking agent to sludge ratio �_ :1 Daily Monitoring Blanket material used: 2 Day Bed Temp. °C Point 1 Point 2 Point 3 Date Blower Cycle ON/OFF Initials Blowers in use: (fie- Comments: 1 S1, 6 S s� 6 - -� '-' �J 2 6 I, L/ Sal, I —_�-:—I 4 6 9 `'— S_ Z 5 (6.3 2-7 —I LK z�)Q Dui. 6 .2 3 L-1l t c.? 8 y G, s rJ y� J 10 ,l 6 65"? _I Li 11 6 %,6 �. , ) S - - y/ 12 -7r 7 1, 0 /� 61-, - 3 - ) 13 ,/ flo•L ��PY 15 16 17 t 18 S - Date pile taken down Date screened Date collected for analysis: Date available for release: 19 20 7 3, el77, 69, 21 '; 61 ? 0, ('� Pile to have, one foot of cover material Bed temp. points 2 1 L Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio: _ to I mix Depth of blanket material: /I< Blowers in use: 0 A) c— Point 1 Bed # (3 Daily Monitorin Bed Tern °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 1 s_$.. 6 b/ s�, 9 -3Q-i --I, 2 S g 6 ,1 5- ,j 4 1, S-7, 9 6 (0 6� s�, o 71 16 3.Z,4 Zs 9 2-1 A I 10 111,6.t LV 13 2c, !Z-! 15 18 0 21 �v r 57, z- �5,� l ^ 2v Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio _ to _I mix Depth of blanket material: �� eU c Blowers in use: (,,> e- Point 1 Bed # I QL Daily Monitorin Bed Tern °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 1 r , 1. -/ ,v 2 6 -4,/ 2 3 LG� . L . 'l -S-_/ <o 4 !� 6 s� 6 •G-/ �� 6 6 - 6 `� - 6- 71 G/, / g � 3 6 S, � - ?-/ Q- 9 s ?C), 10 6-�-$ �i, g 6 11 12 6 6 . .7 - Are - 13 62,6 -/J-./ 1V 14 G.f`•/ 15 17 19 7 z.0 7,3, 2 70,. (0 .2/-/ `,)-- Q, � Point 2 Point 3 L Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio 3 to I mix Depth of blanket material: (a; , n C — Blowers in use: 0 tO L Point 1 Bed # l Daily Monitorin Bed Tem °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 1 0 �� 4", u - - / p 3162 . Z -1, 4 6 3 1 4 71 s. 6 1 a -5 3. 1G • 2 � / �,� 8 5) 1 9- 6 3. 9 j 6 q,s- 1 913 6j, 10 le D 12 13 15 d G'2,0 2/ a 16 I 2. / ^/ -21- / / J 18 19 io, -2 20 21 LI, 3 �, 9 �2��/� ii Point 2 Point 3 I�D Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio_ to I mix Depth of blanket material:��� C Blowers in use: (� Point 1 Daily Monitorin Bed Temp °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 1 b 3 4 G Z, 61 b Y , 1 S/` ; G G s; -21- / �� 7 ♦1(- �r C,,, G (� Z 0 / -Z? / yto J 81 5- 9 ? 61-, GZ ,� o p 10 7 14-25r--� z o 11 12 6S, 13 14 15 6e- -s 4y •y 6a G-30-/ 2 /o 16 17 19 2- 20 21 7, 1 70-1 66 3 Point 2 Point 3 I�D Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio _ 3 to I mix Depth of blanket material: _� ` i �1,1 Blowers in use: 0 A) c- Point 1 Bed #_ Q Daily Monitoring Bed Tern °C Date Blower C cle Initials .Day Point 1 Point 2 Point 3 2 3 O.S16 t. 1 4 5 6 10 0 % :2 . l ..• -moo 12 , 13 14 G . 3 d d . 7 - 30 -/c, 15 16 17 18 66.7 7S_7 r) b� _ G-- 3 -2- `/ Y 2 ID,w Y1- 0,L" 19 % 4 . 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S_i,3 - tv 4 I.(o G�.3 &0.2— 6 7 s y -- 11 (, - 1 Ito ,B✓ 12 /1 4 13 5.3 9 3 62.y -�-- 21j. _ 14 1 - �3— -;) /;a 15- 17 rJ_ tI ') 6— J 2 y� 1s �- 1 , Date pile taken down Date screened Date collected for analysis: Date available for release: 19 Itj 1 21 2- Z G —� o Pile to have one foot of cover material Bed temp. points 2 L Extended Aeration Compost Bed Data Sheet ---1 Bulking agent to sludge ratio: 3 to mix Depth of blanket material: Blowers in use: G rJG Point 1 Bed # Daily Monitoring Bed Tem °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 2 2 t G ^i 3 (, 61 61,j I 7 6Z, �, 6i, 4-Z-< 8 2,2 G*2 9-s-�Y /�� v 9 6 a. 101 k 7, 12 13 14 G 15 166y, 17 18 19 6- 3 ro6. 1 Z l -� ?1-`� �1. i 6Y. •! -< -< Z 21 e,—I)— -/� -< /�- r, Point 2 Point 3 I Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio 3 to ( mix Depth of blanket material: Blowers in use: C, ,,,c Point 1 Bed # Daily Monitoring Bed Temp °C Date Blower C cle Initials Day Point 1 Point 2 Point 3 1 fir, b o, r /� 3 jp 41 6 -2S3/4 6 L l •2-� o 71 -1 16 6 , - 2 8 4 3,3 4 L1,F iQ. 9 -9�.2 9 4 3 S 9 93. 3-, zi �- 10 11 S, (3, �:� 1a-2 12 13 62,1 ��-�- ti -•n C� 14 15 16 5 (v GCe. --- /o -? - 17 $, 4t 18 6 6, 1 0 - G 19 4 6 ,1 io . i _. -:�-), a 20 21 b6. 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"2- .(o e-:3-1 b 19 20 Jul-P'lti 10 D 21 6 4s Point 2 Point 3 1_9 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio: 3_ to I mix Depth of blanket material: 13, Blowers in use:(p h),_ Point 1 Bed # -3 Daily Monitoring Bed Temp °C Date Blower Cycle Initials Day Point 1 Point 2 Point 3 21 fj S .4 -! 3 5f, //-I 5 SR. i, s _ y 60, b 6 o' 8 9 11 (,V to a • I / - l S = .z iv /3,,d -rvr o 13 9-c.t,51 kd 14 q 2/ - / -/ /a 0 15 16 6 $, 4. 9/• a� iy �� �►� 17 4 �,3 :::r- 18 66.9 -722 -!e'- 0 Lj 20 Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio: to I mix Depth of blanket material: )a i 1) C Blowers in use: (,) r�,) e Point 1 Bed # c. Daily Monitoring Bed Tern °C Date Blower Cycle Initials Day Point 1 Point 2 Point 3 2 9 IDD. 6 /. Z / •/�-/ ro ro 3 4 5 &.3 6 If 41. ` / 6 . S" 3_ 2. b 1, --1 7 .'1 6 I . -/v (fit s b 1/-2 -/y 2 11 0,7 6b. 11 0_ 12 oQ 67. I Y-/ a� D MO 13 6�,A 7- Z 9- /•� `//icy ,8•v -rn o 16 %, 3 6 , L7 /Z-2--ldy 17 ,3 70, 6 1 2',?-/ ' + 18 6.ssa 70, /2-(4 e 20 ,72,& (o 9A C Z_ 6 Q411 Y 21 (b3,b 166,0 163. 61 ) 2.1-/ Point 2 Point 3 Extended Aeration Compost Bed Data Sheet Bulking agent to sludge ratio:_ to mix Depth of blanket material: Blowers in use: jnNc_ Point 1 Bed # -1 Daily Monitorin Bed Temp 0 C : • IM Vol W©� /�� Point 2 Point 3