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WQ0001990_2014 Residual Annual Report_20150223
T 0_) WN 0 F VA L D ES E - �, LAKE RHODHISS WWTP 2100 Lake Rhodhiss P.O. Sox 339 Valdese, N.C. 28690 (828) 879 - 2131 February 18, 2015 To whom it may concern, Enclosed is our 2014 composted sludge report, which includes the analytical data, recipients, temperatures and process description. In the interest of conservation, information is contained on both sides of each sheet of paper (where applicable) . If you require additional information concerning the report, please contact us at the above number. Regards, Greg A. Padgett Superintendent/ ORC State Non -Discharge Permit for Composted Sludge WQ0001990 State NPDES NCO041696 REcemiDENFJOWR FEB 2 3 %n15 Water QU p®ewedfig So c Oft CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #:lolwncs- 1990 FACILITY NAME: Lake Rhodhiss Wastewater Treatment Facility PHONE: 828-879-2131 COUNTY: Burke OPERATOR: Town of Valdese FACILITY TYPE (please check one): LA Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ' Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar ear? Yesk No ILL --► If No skip parts A, B, C and certifv form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) (dry tons i Reci ient Information Amendment/Volume Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January NCO041696 0 0 0 February 5.81 1.3 7.11 March of9.04 2.02 11.06 April of7.32 1.63 8.95 May 3.23 0.72 3.95 SEE ATTACHED SHEET June to1.94 0.43 2.37 July of4.3 0.96 5.27 August 3.87 0.86 4.74 September 0 0 0 October 0.22 0.05 0.26 November 58.97 13.16 72.13 December NCO041696 3.01 0.67 3.69 Total from FORM DMSDF (sup), Totals: Annual (d tons): 97.71 21.8 119.53 1 0 Amendment(s) used: I Leaves, Mulch. Woodchi s 1 Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: / Facility was compliant during the past calendar year with all conditions of the land application permit JC Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature o ermittee Dat **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer** (if different from Permittee) Date N DENR FORM DMSDF (12/2006) COMPOST CUSTOMERS • Name Address Usage # of Scoops Barus, Dennis 3311 Barus St. Mulch 1 Benfield 530 Laurel St Mulch 5.5 Brady, John 107 Faet St Mulch 0.5 Brookshire, Danny Caldwell Mulch 111 Caldwell, Ed 105 Davis Dr. SE Mulch 7.5 Camp, Denny431 C2usby Rd. Mulch 3 Chester, Randy Valdese Mulch 1.5 Clark, Scott Hildebran Mulch 2.5 G, Chad Laurel St., Valdese -Mulch 3 Henry Lowman, Mulch 1 Humphries, Niki 828 Cline Ave Mulch 0.5 Lowman, Scott Valdese Mulch 5.5 Mathis Valdese Mulch 1 Morris Granite Falls Mulch 1 Presswood, Wayne Hudson Mulch 1 Robbins, David Valdese Mulch . 1 Roper Rutherford College Mulch 1 Sigmon's Mulch Hickory Mulch 32 Stanbury Rhodhiss Mulch 1.5 Stoughton, B. Granite Faffs Mulch 4 Terrel Jim 1354 Malcolm Mulch 34.5 Vance, Mike Chesterrield Mulch g Wood, Eddie Holly Hills Mulch 1 Zimmerman Burke County Mulch 0.5 TOTAL 227 1 2014 COMPOST DISTRIBUTED IN DRY TONS Month # of Scoops Loaded Amendment (DT) Residuals (DT) (DT) Distributed January 0 0.00 0.00 0.00 February 13.5 5.81 1.30 7.11 Mar 21 9.04 2.02 11.06 April 17 7.32 1.63 8.95 May 7.5 3.23 0.72 3.95 June 4.5 1.94 0.43 2.37 July 10 4.30 0.96 5.27 Aug 9 3.87 0.86 4.74 Sept 0 0.00 0.00 0.00 Oct 0.5 0.22 0.05 0.26 Nov 137 58.97 13.16 72.13 Dec 7 3.01 0.67 3.69 TOTAL 227 97.70 21.81 119.52 Dry Weight of 1 % Solids Scoop % Cake 35.1 1053 18.25 % Solids = average percent solids of compost from lab test Dry weight of 1 scoop = 3000 Ibs wet weight times % solids average % Cake = average % solids from operator centrifuge solids testing sheet COMPOST CUSTOMERS Name Address Usage # of Scoops Date 2� 2-T - �A W Iq Ity L. Lf 5 A /V, Cow rwprA <3 4. N Ao 6 5 COMPOST CUSTOMERS x Name Address Usage # of Scoops Date ..a, 77- 2 �) -�a. ,, �'� Cs� n H �� -711 /yr cCr c� 'AL;<z SIC .-� blL r (.r..,�;��-.i"t •� t.i-.? � u f. 3 �=- �� t.-`nv ;-i� ''� �---� ljr.�' f � i r =-` /-j�' �It � !_.�://_(h'✓'`- < r7.,.n,�:G>:`-� 1 )i� iC{• �>� !t ,tom _�l;/i., Iq lei i G 0, COMPOST CUSTOMERS Name Address Usage # of Scoops Date b ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQO-001990 Laboratory: 1) Blue Ridge Labs (NC Lab # 275 ) Facility Name: Lake Rhodhiss WWTP 2) NPDES # or 3 WQ#:) NC0041696 4) WWTP Name: Lake Rhodhiss WWTP - 5) Residual Analysis Data Sample or Composite Date 3-4-14 5-14-14 8-7-14 10-16-14 12-4-14 Percent Solids 44.3 46.1 37.2 26.6 37.5 Arsenic 41 37.2 10.3 Cadmium 2.69 2.87 6.5 * 3.01 Chromium * Samples are below Minimum Quantification Limit 241 Copper 321 293 270 "276 Lead 19.7 39.5 Mercury 0.2865 0.0507 0.0669 0.1135 0.0603 Molybdenum y Nickel 6.31 8.36 7.4 17.9 13.5 Selenium 12.1 59.3 * 28.5 Zinc 384 482 404 288 349 Total Phosphorus 13605 16921 12987 9614 13204 TKN 18380 13894 4747 1 4669 U10114 Ammonia -Nitrogen 1869 1475 1882 819 1786 Nitrate and Nitrite 55.5 806 199 221 - 398 LEI "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are s=ificant lties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preder Date v DENR FORM RSSF-(5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001990 . Laboratory: 1) Blue Ridge Labs (NC Lab # 275 ) Facility Name: , Lake Rhodhiss WWTP 2) NPDES # or - 3) WQ#: NC0041696 - " 4) WWTP Name: Lake Rhodhiss WWTP 5) Residual Analvsis Data Sample or Corn osite Date 3-4-14 5-14-14 8-7-14 10-16-14 12-4-14- Aluminum 38182 34510 * * 13204 Calcium 13381 8323 14607 11315 15246 Magnesium 3682 2479 3282 2463 3318 Potassium 3400 2484 3091 2723 3256 ,d Sodium 7150 3882 3219 4900 6318 PAN 1924 2281 2081 1040 2184 pH(S.U.) 4.5 4.5 5.6 4.8 5.6 SAR 1.2 1..8 2.3 y * Sample is below MQL "I certify, under penalty of law, that this document was' prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the, information submitted. I am aware that there are si 'scant"penalties four submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of P rer Date 1w DENR FORM RSSF-B (5/2003) Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Mar-14 Report Date: 29-Mar-14 Sample Date: 04-Mar-14 BRL #: BRL-2014-0114 Lab Sample ID: LSID-2014-00623 Client Sample ID: Compost Parameter Result MQL Unit Method Total Phosphorus 13605 509 dry mg/kg EPA 200.7 Al by ICP-AES 38182 127 dry mg/kg SW-846-6010 As by ICP=AES 41 2 dry mg/kg SW-846-6010 Ca by ICP-AES 133'81 637 dry mg/kg SW-846-6010 Cd by ICP-AES 2.69 0.04 dry mg/kg SW-846-6010 Cu by ICP-AES 321 0.2 dry mg/kg. SW-846-6010 K by ICP-AES 3400 127 dry mg/kg SW-846-6010 Mg by ICP-AES 3682 127 dry mg/kg SW-846-6010 Mo by,ICP-AES * 0.2 dry mg/kg SW-846-6010 iJa by ICP=.;ES 7150 637 dry frig/kg SW-846-6010 Ni by ICP-AES 6.31 0.2 drymg/kg SW-846-6010 Pb by ICP-AES 19.7 2 dry mg%kg SW-846-6010 Se by ICP-AES 12.1 2- dry mg/kg SW-846-6010 Zn by ICP-AES 384 0.2 dry mg/kg SW-846-6010 Hg by Cold'Vapor AAS 0.2865 0.041 dry mg/kg SW-846-7471 Analysis ' Analysis Time Date Analyst 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/ 13/2-014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 14:25 3/13/2014 KCJ 15:04 3/17/2014 ' KCJ Reported By: J. Johnson, D.R. Wessinger * Concentrations are elow Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 4 t y. Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 - 828-728-0149 blueridgelabsienoir@gmaii.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Mar-14 Report Date: 29-Mar-14 Sample Date: 04-Mar-14 BRL #: BRL-2014-0114 Lab Sample ID: LSID-2014-00624 Client Sample ID: Compost Analysis Analysis Parameter, Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 1869 197 dry mg/kg Ammonia 11:59 3/21/2014 . KCJ Reported By: J. Johnson, D.R. Wessinger * Concentrations are b ow Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of. 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick blueridgelabslenoir@gmail.com Date Received: 04-Mar-14 Report Date: 29-Mar-14 .Sample Date: 04-Mar-14 BRL #: BRL-2014-0114 Lab Sample ID: LSID-2014-00625 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst % Solids 44.3 0.1 % % Solids 15:31 3/12/2014 KCJ Plt Available Nitrogen 1924 214 dry mg/kg Plant Availabl 12:15 3/21/2014 KCJ pH 4.5 0.1 SU SW-846-9040 14:10 3/12/2014 KCJ Reported By: Johnson, D.R. Wessinger * Concentrations are b Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Attention: Date Received: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick 04-Mar-14 Report Date: 29-Mar-14 Sample Date: 04-Mar-14 BRL #: BRL-2014-0114 Lab Sample ID: LSID-2014-00626 Client Sample ID: Compost Parameter Result Nitrate + Nitrite Nitrogen (N2+ 55.5 Total Kjeldahl Nitrogen (TKN) 18380 MQL Unit 17.2 dry mg/kg 293 dry mg/kg blueridgelabslenoir@gmail.com Analysis Method Time SM19 4500-N 17:47 SM 19 4500-N 19:53 Analysis Date Analyst 3/20/2014 KCJ 3/20/2014 KCJ Reported By: Johnson, D.R. Wessinger * Concentrations are b w Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 4 NPDS Reporting >e Groundwater ort To: �rR..T/VZ CK Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone (828) 728-0149 Fax (828) 728-0131 Chain of Custody Sanitary Landfill Hazardous Waste UST/Trust Fund Reporting Bill To: r I� 1U wN 4 r' • A"�C 1p; lM Industrial or QC Non State Reporting Project Name: PvST PO Number: Ice Present: Y N Sample ID Sample Type Date Time Time & Temp HR:MM °C Field Sulfide Check Y N Field Sulfide Present / Removed Y N Resid Chlor Field Check Y N Field Dechlorination Y N pH Resid Chlor PorA uU Temp °C ,..l Sampler Initials Analysis Requested �SU C rwPa,5 i As, cd,SCu,,lmk: .14'., So, Z., , Al, m a, k t '�� N "3 r ?N i n1z�'� 3• �a S,1.d3 r pA4t �, f Knl *nmshed 13v: Date: "Time: I, , I `1(1 Pam• Pate; _ Time: Upon submission of samples, client agrees that invoices are due at the time work is completed. Open accounts arc due 20 d ,1i)/llowing invoice date. A finance charge of f .5% per month will be imposed on all pasiue accounts. When relinquishing samples to Blue Ridge Labs (BRL), buyer authorises HRL to perform only the analysis indicated above and also agrees to pay collection and attorney feef the account becomes delinquent. Blue Ridge Labs reserves the right to deny documentation for any work where payment has not been made. in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work submitted, therefore it is the client's responsibility to request on this firm appropriate tests. NC UENR Certified Lab #275 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town ofValdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 16-May-14 Report Date: 04-Jun-14 Sample Date: 14-May-14 BRL #: BRL-2014-0313 Lab Sample ID: LSID-2014-01558 Client Sample ID: Compost Parameter Result MQL Total Phosphorus 16921 65 Al by ICP-AES 34510 16.3 As by ICP-AES 42 2 Ca by ICP-AES 8323 81 Cd by ICP-AES 2.87 0.0406 Cu by ICP-AES 293 0.203 K by ICP-AES 2484 16.2 Mg by ICP-AES 2479 16.2 Mo by ICP-AES * 0.203 Na by ICP-AES 3882 81 ,Ni by.ICP-AES 8.36 0.203 Pb by ICP-AES 39.5 2 Se by ICP-AES 59.3 2 Zn by ICP-AES 482 0.203 Hg by Cold Vapor AAS 0.0507 0.0215 f' r blueridgelabsienoir@gmaii.com Analysis' Analysis Unit Method Time Date Analyst dry mg/kg EPA 200.7 17:06 6/2'/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 • 17:06 6/2/2014 -KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846=6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-6010 17:06 6/2/2014 KCJ dry mg/kg SW-846-7471 15:54 5/28/20.14 KCJ Reported By: J. Johnson, D.R.'Wessinger * Concentrations are b ow Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page I of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC'28645 828-728-0149 blueridgelabsienoir@gmaii.com Client Town of Valdese P. 0. gox339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 16-May-1r4 Report Date: 07-Aug- 14 Sample Date: 14-May- 14 BRL #: BRL-2014-0535 Lab Sample ID: LSIO-2014-02424 Client Sample ID: Compost (Redigested from previous Sample 1558) Analysis Parameter Result MQL Unit Method Time As by ICP-AES 32.4 2 dry mg/kg SW-846-6010 16:15 Reported By: S. J. Johnson, D.R. Wessinger *Concentrations Oelow Minimum Quantification Limit except where noted. .T' . _u T.T'rI Laboratory a ora ory e, ca e No. 275 Page 1 of 1 - Analysis Date Analyst 7/29/2014 KSM. Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 16-May- 14 Report Date: 04-Jun-14 Sample Date: 14-May- 14 BRL #: BRL-2014-0313 Lab Sample ID: LSID-2014-01559 Client Sample ID: Compost Parameter Result MQL Ammonia Nitrogen, 1475 351 blueridAelabslenoir@gmail'..com Unit Method dry mg/kg Ammonia Analysis Analysis Time Date Analyst 17:02 5/30/2014 KCJ Reported By: 01 #J�oh�nson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2, of 4 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 16-May-14 Report Date: 04-Jun-14 Sample Date: 14-May-14 BRL #: BRL-2014-0313 Lab Sample ID: LSID-2014-01560 Client Sample ID: Compost blueridgelabslenoir@gmail.com Parameter Result MQL Unit Method % Solids 46.1 0.1 % % Solids Plt Available Nitrogen 2281 467 dry mg/kg Plant Availabl PH 4.5 0.1 SU SW-846-9040 Analysis Analysis Time Date Analyst 14:15 5/17/2014 KCJ 12:14 6/3/2014 KCJ 14:30 5/17/2014 KCJ Reported By: . J. Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 4 P Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 16-May-14 Report Date: 04-Jun-14 Sample Date: 14-May-14 BRL #: BRL-2014-03 0' Lab Sample ID: LSID-2014-01561 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate + Nitrite Nitrogen (N2+ 806 116 dry mg/kg SM19 4500-N 11:50 6/3/2014 ' KCJ Total Kjeldahl Nitrogen' (TKN) 13894 213 . dry mg/kg SM19 4500-N 16:10 5/29/2014 KCJ Reported By: Johnson, D.R. Wessinger * Concentrations are be w Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 4 l f Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Attention: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick blueridgelabsienoir@gmail.com Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRi, #: BRL-2014-0538 Lab Sample ID: LSID-2014-02442 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Total Phosphorus 12987 165 dry mg/kg EPA 200.7 20:27 8/26/2014 KCJ Al by ICP-AES 0.52 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ As by ICP-AES 10.3 5.2 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Ca by ICP-AES 14607 207 dry mg/Icg SW-846-6010 20:27 8/26/2014 KCJ Cd by ICP-AES 6.5 0.1034 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Cu by ICP-AES 270 8.2 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ K. by ICP-AES 3091 41.4 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Mg by ICP-AES 3282 41.4 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Mo by ICP-AES * 0.52 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Na by ICP-AES 3219 207 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Ni by ICP-AES 7.4 0.52 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Pb by ICP-AES * 5.2 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Se by ICP-AES * 5.2 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Zn by ICP-AES 404 0.52 dry mg/kg SW-846-6010 20:27 8/26/2014 KCJ Hg by Cold Vapor AAS 0.0669 0.0263 dry mg/kg SW-846-7471 16:02 8/21/2014 KCJ Reported By: -S.t r'F hnson, D.R7Wessinger- Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page I of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRL th BRL-2014-0538 Lab Sample ID: LSID-2014-02443 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 1882 269 dry mg/kg Ammonia 13:00 8/20/2101 KCJ Reported By: r eS.J.nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 bl,ueridgelabsienoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSID-2014-02444 Client Sample ID: Compost Analysis Analysis Parameter Result MQL - -- - - . Unit Method Time Date Analyst ---- Nitrate + Nitrite Nitrogen (N2+ 199 21 dry mg/kg SM19 4500-N 16:16 .8/20/2014 KCJ Total Kjeldahl Nitrogen (TKN)' 4747 261 dry mg/kg SM19 4500-N 16:30 8/21/2014 KCJ Reported By: S. I uson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample,Date: 07-Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSID-2014-02445 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst % Solids 37.2 0.1 % % Solids 15:45 8/8/2014 KCJ Pit Available Nitrogen 2081 290 dry mg/kg Plant Availabl 16:45 8/20/2014 KCJ pH 5.6' 0.1 SU SW-846-9040 15:50 8/8/2014 KCJ Reported By: % S. J. nson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick blueridgelabsienoir@gmail.com Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSID-2014-02446 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ignitability Not Ignitable 70 Deg. F. 1030 SW-846 14:10 8/8/2014 KCJ Reported By: S. J. nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 5 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSID-2014-02447 Client Sample ID: Compost Parameter Result MQL Reactivity as CN * 1 Reactivity as Sulfide * 5 Reported By: blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time Date Analyst mg/kg SW-846-7.3.3 16:15 8/12/2014 KCJ mg/kg SW-846-7.3.3 12:15 8/12/2014 KCJ S. J nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 6 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07=Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSI.D-2014-02448 Client Sample ID: Compost Parameter Result MQL TCLP Extraction Metals extracted Ag * 0.5 As * 0.5 Ba• * 5 Cd * 0.1 Cr * 0.2 Pb * 0.5 Se Hg by Cold Vapor AAS * 0.002. blueridgelabslenoir@gmaii.com Unit Method S W-846-1311 mg/l SW-846-6010 mg/1 SW-846-6010 mg/l SW-846-6010 mg/l SW-846-6010 mg/l SW-846-6010 mg/I SW-846-6010 mg/I SW-846-6010 mg/l SW-846-7471 Analysis Time Analysis Date Analyst Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit 8/15/2014 Summit Reported B : P Y 4S. nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 7 of 9 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRL #: BRL-2014-0538 Lab Sample ID: LSID-2014-02449 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP ZHE Volatiles Extraction extracted SW-846-1311 Summit Benzene * 0.1 mg/I SW846-8260 8/15/2014 Summit Carbon Tetrachloride * 0.1 mg/I SW846-8260 8/15/2014 Summit Chlorobenzene * 0.1 mg/I SW846-8260 8/15/2014 Summit Chloroform * 0.1 mg/l SW846-8260 8/15/2014 Summit Dichloroethane, 1,2- * 0.1 mg/I SW846-8260 8/15/2014 Summit Dichloroethene, 1,1- * 0.1 mg/l SW846-8260 8/15/2014 Summit MEK * 2 mg/l SW846-8260 8/15/2014 Summit Tetrachloroethene * 0.1 mg/l SW846-8260 8/15/2014 Summit Trichloroethene * 0.1 mg/I SW846-8260 8/15/2014 Summit Vinyl Chloride * 0.2 mg/l SW846-8260 8/15/2014 Summit Reported By: S. J. nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 8 of 9 Blue'Ridge Labs PO Box.2940 Lenoir, NC 28845 828-728-0149 Client : Town of Valdese P. O, Box 339 Valdese, N. C. 28690 Attention: Mr. C. 'Bortnick Date Received: 07-Aug-14 Report Date: 27-Aug-14 Sample Date: 07-Aug-14 BRI. #: BRL-2014-0538 Lab Sample ID: LSID-2014-02450 Client Sample ID: Compost Parameter TCLP Semi-VOC Extraction Cresols (Total) Dichlorobenzene, 1,4 Dinitrotoluene, 2,4- .Hexachloro-1,3-Butadiene Hexachlorobenzene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine Trichlorophenol, 2,4,5- Trich'lorophenol, 2,4,6- Reported By: blueridgelabslenoir@gmaii.com Analysis Result MQL Unit Method Time extracted S W-846-1311 * 0.1 mg/1 SW-846-8270 * 0.1 mg/I SW-846-8270 * 0.1 mg/l SW-846-8270 * 0.1 mg/I SW=846-8270 * 0.1 mg/1 SW-846-8270 * 0.1 mg/I SW-846-8270 * 0.25 mg/l SW-846-8270 * 0.25 mg/I SW-846-8270 * 1 mg/I SW-846-8270 * 0.25 mg/1 SW-846-8270 * 0.25 mg/l SW-846-8270 S. J. hnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 9 of 9 Analysis Date Analyst Summit 8/22/2014 Summit 8/22/2014 Summit 8/22/20-14 Summit 8/22/2014 Summit 8/22/2014 Summit 8/22/2014 Summit ,8/22/2014 Summit 8/22/2014 Summit 8/22/2014 Summit 8/22/2014 Summit 8/22/2014 Summit � .: rt+,?VIBONP E'41`faL'?i4ii; ;z Summit Environmental Technologies, Inc. WO#: 14081332 ' 3310 Win St. Cuyahoga Falls, Ohio 44223 Date Reported 8/22/2014 TEL: (330) 253-8111 FAX (330) 2534489 Company: Blue Ridge Labs, Inc. Website: h4271 www.settek.com Address: P 0 Box 2940 Lenoir NC 28645 Received: 8/13/2014 Project#: TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst .2448,2449,2450 001 8/7/2014 TCLP Arsenic(As) 0.50 ' ND mg/L Solid EPA 6010 C 1 5.0 8/15/2014 WK 2448,2449,2450 001 8/7/2014 TCLP Barium(Ba) 5.0' ND mg/L Solid EPA 6010 C 1 100 8/15/2014 WK 2448,2449,2450 001 81`7/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Solid EPA 6010 C 1 1.0 8/15/2014 WK 2448,2449,2460 001 8/7/2014 TCLP Chromium(Cr) 0.20 ND mg/L Solid EPA 6010 C 1 5.0 8/16/2014 WK 2448,2449,2460 001 8/7/2014 TCLP Lead(Pb) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 8/15/2014 WK 2448,2449,2450 001 8/7/2014 TCLP Selenium(Se) 0.50 ND mg/L Solid EPA 6010 C 1 1.0 8/15/2014 WK 2448,2449,2450 001 8/7/2014 ,TCLP Silver(Ag) 0.50 ND mg/L Sdid EPA 6010 C 1 5.0 8/15/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyse Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 2448,2449,2450 001 8/7/2014 TCLP Mercury 0.0020 ' ND mg/L Solid EPA 7470 A 1 0.20 8/15/2014 ALJ VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 2448,2449,2450 001 8/7/2014 1,1-Dichloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.70 8/16/2014 MES 2448,2449,2450 001 8/7/2014 1,2-Dichloroethane 0.10 ND mg/L Sdid EPA 8260 B 1 0.50 8/15/2014 MES 2448,2449,2450 001 8/7/2014 Benzene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 8/15/2014 MES 2448,2449,2450 001 8/7/2014 Carbon tetrachloride 0.10 ND mg/L Solid' EPA 8260 B 1 0.50 8/15/2014 MES 2448,2449,2460 001 8/7/2014 Chlorobenzene. 0.10 , ND mg/L Solid EPA 8260 B 1 100 8/15/2014 MES 2448,2449,2450 001 8/7/2014 Chloroform 0.10 ND mg/L Solid EPA 8260 B 1 -6.0 8/15/2014 MES 2448,2449,2450 001 8/7/2014 Tetrachloroethene 0.10 ND mg/L Sdid EPA 8260 B 1 0.70 8/15/2014 MES 2448,2449,2450 001 8!7/2014 Trichloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 8/15/2014 MES 2448,2449,2450 001 8/7/2014 Vinyl chloride 0.20 ND mg/L Solid EPA 8260 B 1 0.20 8/15/2014 MES 2448,2449,2450 001 8/7/2014 MEK 2.0 ND mg/L Solid EPA 8260 B 1 200, 8/15/2014 MES . Page 4 of 5 #'kr"'?. W j MViROidMFNTAL i'c. cdt3Lcui_S, "NC '�._ ..,^:� i^fir+:'a:.3i LR-ai`:s77•,)z �.tAY; Summit Environmental Technologies, Inc. WO#: 14081332 3310 grin St Cuyahoga Falls, Ohio 44223 Date Reported 8/22/2014 TEL: (330) 253-8211 FAX- (330) 253-4489 Company: Blue Ridge Labs, Inc. Website: h_pt .1Avww.settek.com Address: P 0 Box 2940 Lenoir NC 28645 Received: 8/13/2014 Project#: SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 2448,2449,2450 001 8/7/2014 1,4-Dichlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 7.5 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 400 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 2.0 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 2,4-Dinitrotoluene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 Cresols, Total 0.10 ND mg/L Solid EPA 8270 C 1 200 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 Hexachloro-1,3- 0.10 ND mg/L Solid EPA 8270 C 1 0.50 8/22/2014 AKE butadiene 2448,2449,2450 001 8/7/2014 Hexachlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 Hexachloroethane 0.10 ND mg/L Solid EPA 8270 C 1 3.0 8/22/2014 AKE 2448,2449,2450 001 817/2014 Nitrobenzene 0.25 ND mg/L Solid EPA 8270 C 1 2.0 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 Pentachlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 100 8/22/2014 AKE 2448,2449,2450 001 8/7/2014 Pyridine 1.0 ND mg/L Solid EPA 8270 C 1 5.0 8/22/2014 AKE Page 5 of 5 NPDS Reporting Groundwater ort To: MR_T/VSCX Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone.(828) 728-0149 Fax (828) 728-0131 Chain of Custody = _ Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting — UST/Trust Fund Reporting- -Bill To: ^� .._�A,%.oa E Project Name: PViT _ PO Number: Ice Present: Y N Sample 1D Sample Type Date Time Time & Temp HR:MM °C Field Sulfide Check Y N - Field Sulfide Present/ Removed Y N — Resid Chlor Field heck Y N Field echlorination- Y N n pH CSGrvattves Resid Chlor PorA L.aD Temp °C UneCK Sampler Initials Analysis Requested rr+Pas i d'`t A5,ca,�aCr..,tlt ►' MAO A1, Ott 544•s , PAN t P 1 Kn/ 111Ut11J11Gu av: t - Date: l Ime: Receiv-i&d.$y: Dater _ Time: v Upon submission of samples, client agrees that invoices are due at the time work is completed. Open a When relinquishing samples to Blue Ridge Laps (BRL), buyer authorizes HRI: to perform only thccounts arc due 20 days Billowing invoice date.'A finance charge of I,5%per month will be imposed on all paslue accounts. e analysis indicated above and also agrees to pay collection and attorney feefthe account becomes delinquent. Blue Ridge Labs reserves the right to deny documentation for any work where payment has not been made. in effect rendering that data unsupported for regulatory purposes. BR.L cannot guarantee that any regulatory authority will accept any work submitted, therefore it is the client's responsibility to request on this firm appropriate tests. NC DENR Certified Lab 4275 13 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14 Sample Date: 16-Oct-14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014-03281 Client Sample ID: Compost Parameter Total Phosphorus Al by ICP-AES As by ICP-AES Ca by ICP-AES Cd by ICP-AES Cu by ICP-AES K by ICP-AES Mg by ICP-AES Mo by ICP-AES Na by ICP-AES Ni by ICP-AES Pb by ICP-AES Se by ICP-AES Zn by ICP-AES Hg by Cold Vapor AAS Result 9614 11315 276 2723 2463 4900 17.9 28.5 288 0.1135 blueridgelabslenoir@gmaii.com Analysis Analysis MQL Unit Method Time Date Analyst 12.6 dry mg/kg EPA 200.7 15:21 10/28/2014 KCJ 0.63 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 1.6 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 15.8 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.126 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.63 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 3.2 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 3.2 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.63 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 15.8 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.63 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 1.6 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 1.6 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.63 dry mg/kg SW-846-6010 15:21 10/28/2014 KCJ 0.0351 dry mg/kg SW-846-7471 14:20 10/31/2014 KCJ Reported By: S. Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmaii.com Client Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct- 14 Report Date: 06-Nov- 14 Sample Date: 16-Oct- 14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014-03282 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Ammonia Nitrogen 819 244 dry mg/kg Ammonia 13:30 10/30/2014 KCJ Reported By: S. ohnson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 11 Ib a Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14 Sample Date: 16-Oct-14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014-03283 Client Sample ID: Compost blueridgelabslenoir@gmaii.com Parameter Result MQL Unit Method % Solids 26.6 0.1 % % Solids Plt Available Nitrogen 1040 267 dry mg/kg Plant Availabl PH 4.8 0.1 SU SW-846-9040 Analysis Analysis Time Date Analyst 14:05 10/22/2014 KCJ 17:02 10/30/2014 KCJ 14:32 10/22/2014 KCJ Reported By: S. '9ohnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoir@gmaii.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14. Sample Date: 16-Oct-14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014=03284 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate + Nitrite Nitrogen (N2+ 221 22.7 diy mg/kg SM 19 4500-N 16:48 10/30/2014 KCJ Reported By: S. . Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. B6rtnick Date Received: 17-Oct- 14 Report Date: 06-Nov-14 Sample Date: 16-Oct- 14 BRL #: BRL-2014-073 8 Lab Sample ID: LSID-2014-03285 Client Sample ID: Compost Parameter Result MQL Total Kjeldahl Nitrogen (TKN) 4669 303 blueridgelabslenoir@gmaii.com Analysis Analysis Unit Method Time Date Analyst drymg/kg SM194500-N 10:20 10/31/2014 Kci Reported By: - ----- ---- S. ohnson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 5 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 8287728-0149 blueridgelabsienoir@gmaii.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14 Sample Date: 16-0ct-14 BRL #: .BRL-2014-073 8 Lab,, Sample ID: LSID72014-03286 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP Extraction Metals extracted SW-846-1311 Summit Ag * 0.5 mg/l SW-846-6010 10/29/2014 Summit As * 0.5 mg/l SW-846-6010 10/29/2014 Summit Ba * 5 mg/l SW-846-6010 10/29/2014 Summit Cd * 0.1 mg/l SW-846-6010 10/29/2014 Summit Cr * 0.2 mg/l SW-846-6010 10/29/2014 Summit Pb * 0.5 mg/l SW-846-6010 10/29/2014 Summit Se * 0.5 mg/1 SW-846-6010 10/29/2014 "Summit Hg by Cold Vapor AAS * 0.002 mg/l SW-846-7471. 10/29/2014 Summit Reported'By: S. J1Toinson, D.R. Wessinger * 'Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 6 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14 Sample Date: 16-Oct-14 BRL #: BRL-2014-073 8 Lab Sample ID: LSID-2014-03287 Client Sample ID: Compost Parameter TCLP Semi-VOC Extraction Cresols (Total) Dichlorobenzene,l,4 Dinitrotoluene, 2,4- Hexach Toro-1,3-Butadiene Hexachlorobenzene Hexachloroethane Nitrobenzene Pentachlorophenol Pyridine Trichlorophenol, 2,4,5- Trichlorophenol, 2,4,6- blueridgelabsienoir@gmail.com Result MQL Unit Method extracted S W-846-1311 * 5 mg/1 SW-846-8270 * 0.1 mg/I SW-846-8270 * 0.1 mg/1 SW-846-8270 * 0.1 mg/I SW-846-8270 * 0.1 mg/1 SW-846-8270 * 0.1 mg/I SW-846-8270 * 0.1 mg/1 SW-846-8270 * 0.25 mg/1 SW-846-8270 * 0.25 mg/l SW-846-8270 * 0.25 mg/1 SW-846-8270 * 0.25 mg/1 SW-846-8270 Analysis Analysis Time Date Analyst Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit I1/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit 11/5/2014 Summit Reported By: R - S. Jnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 7 of 11 BRidge �° Labs ������� �������� PO Box2B40 Lenoir, NC 28645 828-728-0149 b|Vehdg8labsieOO|r@gnm@i|.cOOn Client Town ofValdese 9.0.Box 339 Valdese, N.C2Q690 Attention: Mr. [Bortukck Date Received: 17-[}ut 14 Report Date: 06'Nov-14 Sample Date: 16-[ct-}4 BRL #: BRL-2014-0738 Lab Sample ID: I.8lIJ-2014-03208 Client Sample ID: CoouPoa1 Aouh/mis Analysis _Paramnetor___________ Result _ MQL Unit Method _Tboe_ _ Date Analyst TCLPZBEVo|ud|oaExtraction extracted 8W-846'1311 Summit Benzene * 0.1 nog8 SW846'8260 10/29/2014 Summit Carbon Tetrachloride * 0.1 oo8/l S\f846'8260 10/29/2014 Summit Ch|orohouzeue * 0.1 mQ/l SW846'8260 10/29/2014 Summit Cb|unofoon * 0.1 mg/l SW846-8260 10/29/2014 Summit Diobloroethune.l.2' * O. 1 nug/) SW846'8260 10/29/2014 Summit Dicblnroedhoue,l'l' * 0.1 m8/| SVV846'8260 10/20/2014 Summit MEK *' 2 nog/l SVV846'8260 10/29/2014 Summit Totrucbloroudheoe * 0.1 m8/| SW846'8260 10/29/2014 Summit Trio6|oroetb000 * 0.1 m&// SW846-8260 10/20/2014 Summit Vinyl Chloride * 02 nug/) SW846'8260 10/29/2014 Summit � Reported By: ���bmmo,D.R. Wessinger *Concentrations are below Minimum Quantification Limit except- where noted. NC Laboratory Certificate No. %75 poge8of ll Blue -Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct-14 Report Date: 06-Nov-14 Sample Date: 16-Oct-14 BRL #: 8RL-2014-0738 Lab Sample ID: LSID-2014-03289 Client Sample ID: Compost Parameter Result TCLP Semi-VOC Extraction extracted 2,4,5-TP (S'ilvex) 2,4-D Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor oToxaphene MQL 0.5 0.5 0.01 0.002 0.002 0.002 0.002 0.002 0.1 blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time Date Analyst S W-846-1311 Summit mg/I SW-846-8080 10/31/2014 Summit mg/I SW-846-8080 10/31/2014 Summit mg/1 SW-846-8080 10/30/2014 Summit. mg/1 SW-846-8080 10/30/2014 Summit mg/1 SW446-8080 10/30/2014 Summit mg/I SW-846-8080 10/30/2014 Summit mg/I SW-846-8080 10/30/2014 Summit mg/I SW-846-8080 10/30/2014 Summit mg/I SW-846-8080 10/30/2014 Summit Reported By: S. J. hnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 9 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149. Client Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 17-Oct- 14 Report Date: 06-Nov- 14 Sample Date: 16-Oct- 14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014-03290 Client Sample ID: Compost Parameter Ignitability Corrosivity as pH Result MQL Not Ignitable 70 4.8 0.1 blueridgelabslenoir@gmail.com Unit Method Deg. F. 1030 SW-846 su 9045C SW-8 Analysis Analysis Time Date Analyst 15:20 10/22/2014 KCJ 14:32 10/22/2014 KCJ Reported By: S. J. 40"'so�n, D.R. Wessinger C�'/" Concentrations are below Minimum Quantification Limit except where,noted. NC Laboratory Certificate No. 275' Page 10 of 11 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Attention: Date Received: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick 17-Oct- 14 Report Date: 06-Nov-14 Sample Date: 16-Oct- 14 BRL #: BRL-2014-0738 Lab Sample ID: LSID-2014-03291 Client Sample ID: Compost Parameter Reactivity as CN Reactivity as Sulfide Result MQL 5 blueridgelabslenoir@gmail.com Analysis Analysis Unit Method Time -Date Analyst mg/kg SW-846-7.3.3 16:21 '10/23/2014 KCJ mg/kg SW-846-7.3.3 15:42 10/23/2014 KCJ , Reported By: S. S 7=n74son, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 11 of 11 c ,» r .�.T3/$ 4:'..`'€ `v.. t',s. Summit Environmental Technologies, Inc. �j�#: 14102493 3310 Win St. a;f gA �,,; ,,.4 j. j r. nn_r ..� .Ii;>��lt,.I tL a'_-'SL.,d= Date Reported: Cuyahoga Falls, Ohio 11/5/2014 � - •'•r l ^n' T+�,.-r .=; TEL: 330 253-8211 FAX. 330 253-4489 ( ) ( ) Company: Blue Ridge Labs, Inc. Website: httn://Www.settek.com Address: P O Box 2940 Lenoir NC 28645 Received: 10/22/2014 Project#: 3286-89 TCLP Metals Analysis (6010) Client ID# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3286,3287,3288,3289 001 10116/2014 TCLP Arsenic(As) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 10/29/2014 WK 3286,3287,3288,3289 001 1 Oil6/2014 TCLP Barium(Ba) 5.0 ND mg/L Solid EPA 6010 C -1 100 10/29/2014 WK 3286,3287,3288,3289 001 10/16/2014 TCLP'Cadmium(Cd) 0.10 ND mg/L Solid EPA 6010 C 1 1.0 10/29/2014 WK 3286,3287,3288,3289 001 10/16/2014 TCLP Chromium(Cr) 0.20 ND mg/L Solid EPA 6010 C 1 5.0 10/29/2014 WK 3286,3287,3288,3289 001 10/16/2014 TCLP Lead(Pb) 0.50 , ND mg/L Solid EPA 6010 C 1 5.0 10/29/2014 WK 3286,3287,3288,3289 001 10/16/2014 TCLP Selenium(Se) 0.50 ND mg/L Solid EPA 6010 C 1 1.0 10/29/2014 WK 3286,3287,3288,3289 001 10/16/2014 TCLP Silver(Ag) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 10/29/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3286,3287,3288,3289 001 10/16/2014 TCLP Mercury 0.0020 ND mg/L Solid EPA 7470 A 1 0.20 10/29/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run -Analyst 3286,3287,3288,3289 001 10/16/2014 Chlordane, total 0.010 ND mg/L Solid EPA 8081 B 1 0.030 10/30/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Toxaphene 0.10 ND mg/L Solid EPA 8081 B 1 0.50 10/30/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Endrin 0.0020 ND mg/L Solid EPA 8081 B 1 0.020 10/30/2014 AKE 3286,3287,3288,3289 001 10/16/2014 gamma-BHC 0.0020 ND mg/L Solid EPA 8081 B 1 0.'40 10/3012014 AKE 3286,3287,3288,3289 001 10/16/2014'Heptachlor 0.0020 ND mg/L Solid EPA 8081 B 1 0.0080 10/30/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Heptachlor epoxide 0.0020 ND mg/L Solid EPA 8081 B 1 0:0080 10/30/2014 AKE 3286,3287;3288,3289 001 10/16/2014 Methoxychlor 0.0020 ND mg/L Solid EPA 8081 B 1 10 10/30/2014 AKE VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3286,3287,3288,3289 001 10/16/2014 1,1-Dichloroethene 0.10 ND mg/L Solid ' EPA 8260 B 1 0.70 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 1,2-Dichloroethane 0.10 ND mg/L Solid EPA 8260 B 1 0.50 10/29/2014 MES 3286,3287,3288,3289. 001 10/16/2014 Benzene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 Carbon tetrachloride 0.10 ND mg/L Solid EPA 8260 B 1 0.50 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 Chlorobenzene 0.10 ND mg/L Solid EPA 8260 B 1 100 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 Chloroform 0.10 ND mg/L Solid EPA 8260. B 1 6.0 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 Tetrachloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.70 10/29/2014 MES' 3286,3287,3288,3289 001 10/16/2014 Trichloroethene 0.10 ND mg/L Solid EPA 8260 B 1 0.50 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 Vinyl chloride 0.20 ND mg/L Solid EPA 8260 B 1 0.20 10/29/2014 MES 3286,3287,3288,3289 001 10/16/2014 MEK 2.0 ND mg/L Solid EPA 8260 B 1 200 10/29/2014 MES Nfgee4 d57 e i k z� �d1� [ Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14102493 M$� z L1',"i:s�r:. #1's" Cuyahoga Falls, Ohio 44223 Date Reported: 11/5/2014 C ?a __ :ru, _ d:Fi:7 �'�a•;f•±i49 -l..F_. d;.MI'??°,: r..i'1 > •a r -• TEL: (330) 253-8211 FAX (330) 253 4489 Company: Blue Ridge Labs, Inc. Website: httn://www.settek.com Address: P O Box 2940 Lenoir NC 28645 Received: 10/22/2014 Project#: 3286-89 SVOC 8270 TCLP BNA List Client ID# Lab ID# 'Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl ,Run Analyst 3286,3287,3288,3289 001 10/16/20141,4-Dichlorobenzene 0.10 ND mg/L Solid EPA 8270 C, 1 7.5 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 400 1115/2014 AKE 3286,3287,3288,3289 001 10/16/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 2.0 11/5/2014 AKE 3286,3287,3288,3289 001 .10/16/2014 2,4-Dinitrotoluene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Cresols, Total 5.0 ND mg/L Solid EPA 8270 C 1 200 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Hexachloro-1,3- 0.10 ND mg/L Solid EPA 8270 C 1 0.50 11/5/2014 AKE butadiene 3286,3287,3288,3289 001 10/16/2014 Hexachlorobenzene 0.10 ND mg/L Solid EPA 8270 C • 1 0.13 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Hexachloroethane 0.10 ND 'mg/L Solid EPA 8270 C 1 3.0 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Nitrobenzene 0.10 ND mg/L Solid EPA 8270 C 1 2.0 11/5/2014 AKE 3286,3287,3288,3289 001 10/16/2014 Pentachlorophenol 0.25 ND mg/L. Solid EPA 8270 C 1 100 11/5/2014 AKE 3286,3287,,3288,3289 001 10/16/2014 Pyridine 0.25 ND mg/L Solid EPA 8270 C 1 5.0 11/5/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3286,3287,3288,3289 001 10/16/2014 2,4-D 5.0 ND mg/L Solid EPA 8321 A 1 10 10/31/2014 AMZ 3286,3287,3288,3289 001 10/16/2014 2,4,5-TP 0.50 ND mg/L Solid EPA 8321 A 1 1.0 10/31/2014 AMZ P 5 d57 NPDS Reporting KGroundwater Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC-28645 Telephone (828) 728-0149 Fax (828) 728-01131 Chain of Custody Sanitary Landfill Hazardous Waste Industrial or QC Non State Reporting UST/Trust Fund Reporting R(qort To: Bill To: i -i�TiCK W^iv Project Name; Q�ST PO Number: Ice Present: Y N Field Preservatives I.ah Check Sample ID Sample Type Date Time Time & Temp HR:MM- °C Field Sulfide Check Y N Field Sulfide Present / Removed Y_ N Resid Chlor Field Check Y N Field Dechlorination Y N pH Resid Chlor P or A Temp °C Sampler Initials Analysis Requested C 1,1 4o,►b'i �j'1, 66, As,cd,lam CW,Pp li5,a ,4%, Se z., , Ai, m ktNc,iNN3iPNl^li'^13, PA41 ?I tj inq uish By :. , Date: Time: i Time: _ A (�T3VS ry Upon submission ofsamples, client agrees that invoices are due at the time work is completed. Open accounts are due 20 days following invoice date. A Imance charge of 1.5% per month will be imposed on all pastue accounts: When relinquishing samples to Blue Ridge Labs (BRL), buyer authorizes BRI. to perform only the analysis indicated above and also agrees to pay collection and attorney feef the account becomes delinquent. Blue Ridge Labs reserves the right to deny documentation for any work where payment has not been made. in effect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work submitted, therefore it is the client's responsibility to request on this form appropriate tests. NC DENR Certified Lab #275 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date:, 04-Dec-14 BRL #: BRL-2614-0844 Lab Sample ID: LSID-2014-03736 Client Sample ID: Compost Parameter Result Total Phosphorus 13204 Al by ICP-AES. 20919 As by ICP-AES Ca by ICP-AES 15246 Cd by ICP-AES 3.01 Cu by ICP-AES 241 K by ICP-AES 3256 Mg by ICP-AES 3318 Mo by ICP-AES Na by ICP-AES 6318 Ni by ICP-AES 13.5 Pb by ICP-AES . Se by 'ICP-AES Zn by ICP-AES 340 Hg by Cold Vapor AAS 0.0603 blueridgelabslenoir@gmail.com Analysis Analysis MQL Unit Method Time Date Analyst. 144 dry mg/kg EPA 200.7 15:06 12/19/2014 KCJ 36 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 4.5 dry mg/kg SW-846-6010 15:06 12/19/2014 . KCJ 180 dry. mg/kg SW-846-6010 15:06 12/19/2014 KCJ 0.0902 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 7.2 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 36 dry mg/kg SW=846-6010 15:06 12/1'9/2014 KCJ 36 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 0.45 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 180 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ . 0.45 dry mg/kg SW446-6010 15:06 12/19/2014 KCJ 4.5 dry mg/kg SW-846-6.010 15:06, 12/19/2014 KCJ 4.5 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 0.45 dry mg/kg SW-846-6010 15:06 12/19/2014 KCJ 0.0248 dry mg/kg SW-846-7471 16:07 12/15/2014 KCJ �� des•..—' Reported By: —f- —------- S. I Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 1 of 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client: Attention: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03737 Client Sample ID: Compost Parameter Ammonia Nitrogen Result MQL 1786 228 blueridgelabslenoir@gmail.com Unit Method dry mg/kg Ammonia Analysis Analysis Time Date Analyst 12:59 12/22/2014 KCJ A2" Reported By: S. J: Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 2 of 10 c Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Attention: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03738 Client Sample ID: Compost blueridgelabslenoir@gmail.com Analysis Analysis Parameter Result MQL Unit Method Time Date % Solids 37.5 0.1 % % Solids 12:00 12/10/2014 Pit Available Nitrogen 2184 268 dry mg/kg Plant Availabl 13:02 12/22/2014 SAR 65.6 0 SAR 13:27 12/22/2014 pH 5.6 0.1 SU SW-846-9040 10:20 12/5/2014 Nl*�� ,. Icy - Reported By: S. . Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 3 of 10 Analyst KCJ KCJ KCJ KCJ Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: - 22-D'ec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03739 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Nitrate + Nitrite Nitrogen (N2+ 398 39.8 dry mg/kg SM19 4500-N 16:46 , 12/10/2014 KCJ Total Kjeldahl Nitrogen (TKN) 10114 215 drymg/kg SM19 4500-N 10:12 12/11/2014 KCJ Reported By: S. Whnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 4 of 10 41 Q Blue Ridge Labs PO Pox 2940 Lenoir, NC 28645 828-728-0149 Client : Attention: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 12-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03740 Client Sample ID: Compost blueridgelabslenoir@gmaii.com Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst Reactivity as CN * 1 mg/kg SW-846-7.3.3 16:45 12/10/2014 KCJ Reactivity as Sulfide * 5 mg/kg SW-846-7.3.3 15:10 12/10/2014 KCJ Reported By: - S. Xedohnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 5 of 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149' 'Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dee- 14 Report Date: 22-Dec- 14 Sample Date: 04-Dec- 14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03741 Client Sample ID: Compost Parameter Ignitability Corrosivity as pH Result Not Ignitable 5.6 Reported By: blueridgelabsienoir@gmail.com Analysis Analysis MQL Unit Method Time Date 70 Deg. F. 1030 SW-846 11:15 12/12/2014 0.1 su 9045C SW-8 10:20 12/5/2014 .10 S. JfXohnson, D.R. Wessinger Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 6 of 10 Analyst KCJ KCJ A. Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabsienoir@gmail.com Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03742 Client Sample ID: Compost Parameter Result MQL Unit Method Analysis Analysis Time Date Analyst TCLP Extraction Metals extracted SW-8464311 Summit Ag * 0.5 mg/l SW-846-6010 12/12/2014 Summit As * 0.5 mg/l SW-846-6010 12/12/2014 Summit Ba * 5 mg/l SW-846-6010 12/,12/2014 Summit Cd * 0.1 mg/l SW-846-6010 12/12/2014 Summit Cr * 0.2 mg/l SW-846-6010 12/12/2014 Summit Pb * 0.5 mg/l SW-846-6010 12/12/2014 Summit Se * 0.5 mg/l SW-846-6010 12/12/2014 Summit Hg by Cold Vapor AAS * 0.002 mg/l SW-846-7471 12/12/2014 Summit Reported By: S. J.'Johnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 7 of 10 Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 blueridgelabslenoir@gmail.com Client: Town of Valdese P.O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03743 Client Sample ID: Compost Analysis Analysis Parameter Result MQL Unit Method Time Date Analyst TCLP Semi-VOC Extraction extracted SW-846-1311 Summit Cresols (Total) * 5 mg/l SW-846-8270 12/13/2014 Summit Dichlorobenzene, 1,4 * 0.1 mg/1 SW-846-8270 12/13/2014 Summit Dinitrotoluene, 2,4- * 0.1 mg/l SW-846-8270 12/13/2014 Summit Hexachloro-1,3-Butadiene * 0.1 mg/l SW-846-8270 12/13/2014 Summit Hexachlorobenzene * 0.1 mg/1 SW-846-8270 12/13/2014 Summit Hexachloroethane * 0.1 mg/1 SW-846-8270 12/13/2014 Summit Nitrobenzene * 0.1 mg/l SW-846-8270 12/13/2014 Summit Pentachlorophenol * 0.25 mg/l SW-846-8270 12/13/2014 Summit Pyridine * 0.25 mg/l SW-846-8270 12/13/2014 Summit Trichlorophenol, 2,4,5- * 0.25 mg/1 SW-846-8270 12/13/2014 Summit Trichlorophenol, 2,4,6- * 0.25 mg/1 SW-846-8270 12/13/2014 Summit 0 10 Reported By: S. J.4ohnson, D.R. Wessinger * Concentrations are below -Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 8 of 10 Blue Ridge Labs PO Box 2940 Lenoir, NC. 28645 828-728-0149 Client: Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03744 Client Sample,ID: Compost Parameter TCLP ZHE Volatiles Extraction Benzene Carbon Tetrachloride Chlorobenzene Chloroform Dichloroethane, 1,2- Dichlor6ethene, 1,1- MEK Tetrachloroethene Trichloroethene Vinyl Chloride blueridgelabslenoir@gmaii.com Analysis Analysis ' Result MQL Unit Method Time 'Date Analyst extracted S W-846-1311 * 0.1 mg/1 SW846-8260 12/12/2014 Summit * 0.1 mg/l SW846-8260 12/12/2014 Summit * 0.1 mg/l SW846-8260 12/121/2014 Summit * 0.1 mg/1 SW846-8260 12/12/2014 Summit * 0.1 mg/1 SW846-8260 12/12/2014 Summit * 0.1 mg/l SW846-8260 12/12/2014 Summit * 2 mg/l SW846-8260 12/12/2014 Summit * 0.1 mg/l SW846-8260 12/12/2014 Summit * 0.1 mg/l SW846-8260 12/12/2014 , Summit * 0.2 mg/l SW846-8260 12/12/2014 Summit Reported By: S. nson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 9 of 10 k Blue Ridge Labs PO Box 2940 Lenoir, NC 28645 828-728-0149 Client : Town of Valdese P. O. Box 339 Valdese, N. C. 28690 Attention: Mr. C. Bortnick Date Received: 04-Dec-14 Report Date: 22-Dec-14 Sample Date: 04-Dec-14 BRL #: BRL-2014-0844 Lab Sample ID: LSID-2014-03745 Client Sample ID: Compost Parameter TCLP Semi-VOC Extraction 2,4,5-TP (Silvex) 2,4-D Chlordane Endrin Heptachlor Heptachlor Epoxide Lindane Methoxychlor Toxaphene Reported By: blueridgelabslenoir@gmaii.com Analysis Analysis Result MQL Unit Method Time Date Analyst extracted S W-846-1311 Summit * 0.5 mg/1 SW-846-8080 12/12/2014 Summit * 5 mg/l SW-846-8080 12/12/2014 Summit * 0.01 mg/l SW-846-8080 12/13/2014 Summit * 0.002 mg/l SW-846-8080 12/13/2014 Summit * 0.002 mg/l SW-846-8080 12/13/2014 Summit * 0.002 mg/l SW-846-8080 12/13/2014 Summit * 0.002 mg/l SW-846-8080 12/13/2014 Summit * 0.002 mg/1 SW-846-8080 12/13/2014 Summt * 0.1 mg/l SW-846-8080 12/13/2014 Summit S. hnson, D.R. Wessinger * Concentrations are below Minimum Quantification Limit except where noted. NC Laboratory Certificate No. 275 Page 10 of 10 a " - '' Summit. Environmental Technologies, Inc. 3310 Win St. WO#: 14120830 xl ` t dtliar�hl�alEy'I; Cuyahoga Falls, Ohio 44223 Date Reported: p 12/15/2014 zr . An^s" 'rzlj E iao+:=ru>a TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Blue Ridge Labs, Inc. Website:,httP.1Awww.se1tekcom Address: P O Box 2940 Lenoir NC 28645 Received: 12/9/2014 Project#: TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3742,3743,3744,3745 001 12/4/2014 TCLP Arsenic(As) 0.50 NO mg/L Solid EPA 6010 C 1 5.0 12/12/2014 WK 3742,3743,3744,3745 001 12/4/2014 TCLP Barium(Ba) 5.0 NO mg/L Solid EPA 6010 C 1 100 12/12/2014 WK 3742,3743,3744,3745 001 12/4/2014 TCLP Cadmium(Cd) 0.10 NO mg/L Solid EPA 6010 C 1 1.0 12/12/2014 WK 3742,3743,3744,3745 001 12/4/2014 TCLP Chromium(Cr) 0.20 NO mg/L Solid EPA 6010 C 1 5.0 12/12/2014 WK 3742,3743,3744,3745 .001 12/4/2014 TCLP Lead(Pb) 0.50 NO mg/L Solid EPA 6010 C 1 5.0 12/12/2014 WK 3742,3743,3744,3745 001 12/4/2014 TCLP Selenium(Se) 0.50 NO mg/L Solid EPA 6010 C 1 1.0 12/12/2014 WK 3742,3743,3744,3745 001 12/4/2014 TCLP Silver(Ag) 0.50 ND mg/L Solid EPA 6010 C 1 5.0 12/12/2014 WK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3742,3743,3744,3745 001 12/4/2014 TCLP Mercury 0.0020 NO mg/L Solid EPA 7470 A 1 0.20 12/12/2014 AU SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3742,3743,3744,3745 001' 121412014 Chlordane, total 0.010 NO mg/L Solid EPA 8081 B 1 0.030 12/13/2014 MO 3742,3743,3744,3745 001 12/4/2014 Toxaphene 0.10 NO mg/L Solid EPA 8081 B 1 0.50 12/13/2014 MO 3742,3743,3744,3745 001 12/4/2014 Endrin 0.0020 NO mg/L Solid EPA 8081 B 1 0.020 12/13/2014 MO 3742,3743,3744,3745 001 12/4/2014 gamma-BHC 0.0020 NO mg/L Solid EPA 8081 B 1 0.40 12/13/2014 MO 3742,3743,3744,3746 001 12/4/2014 Heptachlor 0.0020 NO mg/L Solid, EPA 8081 B 1 0.0080 12/13/2014 MO 3742,3743,3744,3745 001 12/4/2014 Heptachlor epoxide. 0.0020 NO mg/L Solid EPA 8081,B 1 0.0080 12/13/2014 MO 3742,3743,3744,3745 001 12/4/2014 Methoxychlor 0.0020 NO mg/L Solid EPA 8081 B 1 10 12/13/2014 MO VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl' Run Analyst 3742,3743,3744,3745 001 12/4/2014 1,1-Dichloroethene 0.10 NO mg/L Solid EPA 8260 B 1 0.70 12/12/2014 MES 3742,3743,3744,3745 001 .1214/2014 1,2-Dichloroethane 0.10 NO mg/L Solid EPA 8260 B 1 0.50 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Benzene 0.10 NO mg/L Solid EPA 8260 B 1 0.50 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Carbon tetrachloride 0.10 NO mg/L Solid EPA 8260 B 1 0.50 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Chlorobenzene 0.10 NO mg/L Solid EPA 8260 B 1 100 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Chloroform 0.10 NO mg/L Solid EPA 8260 B 1 6.0 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Tetrachloroethene 0.10 NO mg/L Solid EPA 8260 B 1 0.70 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 Trichloroethene 0.10 NO mg/L Solid EPA 8260 B 1 0.50 12/12/2014 MES 3742,3743,3744,3745 001 12/4/2014 . Vinyl chloride 0.20 NO mg/L Solid EPA 8260 B 1 0.20 12/12/2014 MES 3742,3743,3744,3746 001 12/4/2014 MEK 2.0 NO mg/L Solid EPA 8260 B 1 200 12/12/2014 MES P09W4 &57 �'. Su� Summit Environmental TechnologiesInc 3310 Win St. WO#: 14120830 Date ,t:%IrnM►.9E�°I'�I_ t,iriLu•5. INC Cuyahoga Falls, Ohio 44223 Reported: 12/15/2014 ..tary TEL: (330) 253-8211 FAX.- (330) 2534489 Company: Blue Ridge Labs, Inc. Website: htto✓hvww.settekcom Address: P O Box 2940 Lenoir NC 28645 Received: 12/9/2014 Proj ect#: SVOC 8270 TCLP BNA List Client ID# Lab EN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst 3742,3743,3744,3745 001 12/4/2014 1,4-Dichlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 7.5 12/13/2014 AKE 3742,3743,3744,3745 001 12/4/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 400 12/13/2014 AKE 3742,3743,3744,3745 001 12/4/2014 2,4,8-Trichlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 2.0 12/13/2014 'AKE 3742,3743,3744,3745 001 12/4/2014 2,4-Dinitrotoluene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 12/13/2014 AKE ' 3742,3743,3744,3745 001 12/4/2014 Cresols, Total 5.0 ND mg/L Solid EPA 8270 C 1 200 12/13/2014 AKE 3742,3743,3744,3745.001 12/4/2014 Hexachloro-1,3- 0.10 ND mg/L Solid EPA 8270 C' 1 0.50 12/13/2014 AKE butadiene 3742,3743,3744,3745 001 12/4/2014 Hexachlorobenzene 0.10 ND mg/L Solid EPA 8270 C 1 0.13 12/13/2014 AKE 3742;3743,3744,3745 001 12/4/2014 Hexachloroethane 0.10 ND mg/L Solid EPA 8270 C 1 3.0 12/13/2014 AKE 3742,3743,3744,3745 001 12/4/2014 Nitrobenzene 0.10 ND 'mg/L Solid EPA 8270 C 1 2.0 12/13/2014 AKE 3742,3743,3744,3745 001 12/4/2014 Pentachlorophenol 0.25 ND mg/L Solid EPA 8270 C 1 100 12/13/2014 AKE 3742,3743,3744,3745 001 12/4/2014 Pyridine 0.25 ND mg/L Solid EPA 8270 C 1 5.0 12/13/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lint Result Units - Matrix Method DF RegLvl Run Analyst 3742,3743,3744,3745. 001 12/4/2014 2+13 5.0 ND mg/L Solid EPA 8321 A 1 10 12/12/2014 AMZ 3742,3743,3744,3745 001 12/4/2014 2,4,5-TP 0.50 ND mg/L Solid EPA 8321 A 1 1.0 12/12/2014 AMZ PM W5 d57 NPDS Reporting . Groundwater orttRTo: #%ALTArMC Blue Ridge Labs, Inc. P.O. Box 2940 Lenoir, NC 28645 Telephone.(828) 728-0149 Fax (828) 728-0131 Chain of Custody Sanitary Landfill Hazardous Waste Industrial or QC UST/Trust Fund Reporting Bill To* Non State Reporting ILAn a Project Name: ST Field, Time & Field Resid Temp Field Sulfide Chlor Field Sample 1D Sample Date Time Sulfide Present/ Field Dechlorinatio Type HR:MM- Check ' Removed heck °C Y N Y N- Y N Y N yr '1•`�oM PO Number: Ice Present: Y N Preservatives Lab Check Analysis Requested As, c-d , %6 Cam,, tb, W5 . /Vk. . A1, m y, k, rac, NNj t PHIML-43, `/a Stl,ds PAN t �, TKnJ �lETrf`s Sim 1 w� iI_T?-% inouis d BV: Date: Time: Received BIy- Dater Time: - fa Y 4C1P� Upon submission of samples, client agrees that invoices are due at the time work is completed. Open accounts are due 20 days following invoice date..A finance charge of 1.5%per month When relinquishing samples to Blue Ridge Labs (BRL), buyer authorises Bwill be imposed on all paslue accounts. RI. to perform only the analysis indicated above and also agrees to pay collection and attorney feef the account becomes delinquent. Blue Ridge Labs reserves the right to deny documentation for any work where payment has not been made. in affect rendering that data unsupported for regulatory purposes. BRL cannot guarantee that any regulatory authority will accept any work submitted, therefore it is the client's responsibility to request on this room appropriate tests. NCDENR Certified Lab #275 pH lResid ITeMPISamplei Chlor °C Initials P or A - d-tp I C"t 41 1 )Qw4t, ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) ` Facility Name: Lake Rhodhiss WWTP WQ Permit Number: WQ0001990 WWTP Name: Lake Rhodhiss WWTP NPDES Number: NCO041696 Monitoring Period: From 1/1/2010 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ElAlt B (Alk Treatment) El Alt. C (Prior Testing) AltD No Prior Test Process to Further Reduce Pat o en s If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Diving ® Heat Treatment 0 Thermophilic El G Y Beta Ray Gamma Ray ElPasteurization Class B: Alt. (1) Fecal Density ElAlt. (2) Process to Significantly Reduce Pathogens ........... . If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 13 Air Drying 13 Composting 13 Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density um er 01 Frequency Sample a ica Parameter Sludge Excee- of Anal sis Tech- g Minim Geo. Mean Maximum Units Y Type ninue 2 x 10 to the MPN 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry < 1 3.6 822 MPN/g 0 Monthly Grab dulti.Tubc weight) Salmonella bacteria 3 N1PN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) LI Alt. 2 (40-day bench) El I Alt. 3 (30-day bench) El Alt. 4 (Spec. 02 uptake) Alt. 5 (14-Day Aerobic) X Alt. 6 (Alk. Stabilization DI Alt 7 (Drying - Stable) 13 Alt. 8 (Drying - Unstable) 0 Alt. 9 (Injection) E3 Alt. 10 (Incorporation) E] jNo vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) YJ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant Cpenalties ti�(foor false certification including fine and imprisonment." w r.dPN� v - - Ll40 bTAf-c %d& P arer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature Preparer* �a�eSignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) COMPOST PAD TEMPERATURES WINDROW PAD # : —A L- Ir k 13 DATE BUILT: icy - I .-I - 1.3 DATE FINISHED TEMPING: H ` .3 - 13 ` I q?'Y-�n i- t1.t`I TEMPS COMPLETE (Y/N): VLF_ FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS 1, COMPOST PAD TEMPERATURES WINDROW PAD # : % - o.< 3 DATE BUILT: fe - I- i - ! 3 DATE FINISHED TEMPING: r c r TEMPS COMPLETE (YIN): 1"C, FECAL MPN (PASS/FAIL): 1 q 1..4y�-. 1_�� Iy " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD, TEMPERATURES FAL Lm E 2 f3 - - WINDROW PAD # : ` DATE BUILT: Uk- &2 DATE FINISHED TEMPING: 20 TEMPS COMPLETE (YIN): � FECAL MPN (PASS/FAIL): ** IF PILE DOES NOT MEET THE TIME / TEMP_ STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : FA, ,, DATE BUILT: /�?- ';�-13 DATE FINISHED TEMPING: low -AM Nunn. l _ TEMPS COMPLETE (Y/N): if; FECAL MPN (PASS/FAIL): ** IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD TEMPERATURES WINDROW PAD # : wi n_ I ca 13 I Lq DATE BUILT: - (j - I L) DATE FINISHED TEMPING: 3- ,-? - tq MOTA r 1411 I^I TEMPS COMPLETE (YIN): FECAL MPN (PASS/FAIL): P��` C�1 1. L " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD WINDROWPAD#:� DATE BUILT: DATE FINISHED TEMPING: 3 - d - I q TEMPERATURES will=IWOW r FM�Rm /Y 8AYS TEMPS COMPLETE (Y/N): —� FECAL MPN (PASS/FAIL): P/ASS q� cis " IF PILE DOES NOT MEET THE TIME 1 TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS VO, COMPOST PAD TEMPERATURES R4 WINDROW PAD #: W-Z DATE BUILT: J-,?-7-1 DATE FINISHED TEMPING:, )3- (4 C- f �( 1� a v� TEMPS COMPLETE (Y/N): FECAL MPN (PASS/FAIL): cs) ** IF PILE DOES NOT MEET THE TIME I TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD TEMPERATURES m WINDROW PAD # : �� �� n�v- OkQ I'--1 DATE BUILT: 3 - DATE FINISHED TEMPING: l 3 - l 4 ® J R TEMPS COMPLETE (Y/N): FECAL MPN (PASS/FAIL): A jq iJa YS `• IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS 14 COMPOST PAD WINDROW PAD # : Pf v c l L( DATE BUILT: L4 DATE FINISHED TEMPING: L4 --ay I `i TEMPERATURES • . 1 =gel y �a Now, Lqmw 3 DAYS 64c, al �� TEMPS COMPLETE (Y/N): %_ FECAL MPN.(PASS/FAIL): �a55 I Cti " IF PILE DOES NOT MEET THE TIME ! TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS COMPOST PAD TEMPERATURES I WINDROW PAD # : ��^-=.�;� 3 - 2c-% DATE BUILT: 9 - -1,3 - 1 y DATE FINISHED TEMPING:-�- `�i MEMO TEMPS COMPLETE (Y/N): FECAL MPN (PASS/FAIL): 1 U-� ** IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS A COMPOST PAD TEMPERATURES J iS WINDROW PAD # : pp r.- q — DATE BUILT: a - 9 - [ DATE FINISHED TEMPING: — — iLI TEMPS COMPLETE (YIN): FECAL MPN (PASS/FAIL): Ns. cL 6( " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS 5.� u COMPOST PAD TEMPERATURES WINDROW PAD # : sp- 5- -. DATE BUILT: Cis - ,,3 - 1. i-I _ ,DATE FINISHED TEMPING. �� -• .� =' HE rl M !mil 1 Ll 64'yj l-3� IH TEMPS COMPLETE (Y/N):_ FECAL MPN (PASS/FAIL): �A 6, " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS • COMPOST PAD TEMPERATURES a WINDROW PAD # : DATE BUILT: ( - DATE FINISHED TEMPING: •� -• �� :�F MUM rMIM u TEMPS COMPLETE (Y/N): . FECAL MPN (PASS/FAIL): . I�%�� , -eavi � ��� IytAY5 " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS v �vm . COMPOST PAD TEMPERATURES WINDROW PAD # : DATE BUILT: `1 - DATE FINISHED TEMPING: y V 1' 1� 1: c 1R 1E 1i 1f 1� 2C 21 22 23 24 25 26 27 28 -IIIIIIIIIIIjil I Bill . �f TEMPS COMPLETE (YIN): JL FECAL MPN (PASS/FAIL): Ay IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS 0 COMPOST PAD TEMPERATURES WINDROW PAD DATE BUILT: S)- DATE FINISHED TEMPING: 11 1' 1: 1: .1� 1: 1E 1i 1f 1� 2C 21 22 23 24 25 26 27 28 t t �■ TEMPS COMPLETE (YlN): 7_ C' FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS f. COMPOST PAD TEMPERATURES WINDROW PAD # : �,A �.l_ [ - J<' ILL C�,�-�r � DATE BUILT: DATE FINISHED TEMPING: 3a-2 3-%A 32A 33 A 3y .e 3t a 3i'� A 319 3y X 31"ll lio.-12 12 1� 1e 17 1E 1£ 2C 21 22 23 24 2r, V 2E 27 2E II W�V WAWA O�7-,_ TEMPS COMPLETE (YIN): FECAL MPN (PASS/FAIL): " IF PILE DOES NOT MEET THE TIME / TEMP. STANDARDS, CONTINUE ON SEPARATE TEMP. SHEET UNTIL REQUIREMENTS ARE MET ALL TEMPERATURES ARE TAKEN WITH A CALIBRATED THERMOMETER, READ IN CELSIUS � i,-.�•'iy-:�.�`•. �-+.. >"'� "� •,�`S'a'I �`r rid :'t;tl�.. "I mpte" ID -- Ample Date: Sample Time_ Sampler: Test Date: Test Analyst Tkm in ►-i.�ti � � �� � .f. t�.t� T�ns-13at t-ice-iy - D v kwabat" water earth 9-� q.ti ia'q1P Tub=*" D le Cora iorr Totaln--] Di# ion limos' i 2 { _ Double + _ #z WA} + _ 5 i a — - t p f 4 a `J 4 1© 12 't 3 � Double 14 f 1 18 87mg% _ - i 20 steal _ core 1- Sinow - S tl - - : ._o_. Double- Stnength �c:j- Single - Strength Buff" WMW cD Double - S#eFMm Buffer water: C Incubation T4rrtew. . Dry incubator_ 3 holii -tinter Bain: 21 ♦1- 2 tes. MPN Index: a - Q - v IIKkK 10 x MPN kidex a 100mi Largea Vobmm x % Cky Sots f'K � r c PERCENT SOLIDS FOR COMPOST MPN DATE:.I ! - ! E E ANALYST: DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: !L2 9 , GRAMS DISH WEIGH' & DRY SOLIDS: ,�U;,$ ' GRAMS COMPVTATICN 34. , DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS T CALCULATIONS % SOLIDS s WEIGHT OF DRY SOLIDS X 100 % WEIGHT OF WET SOLIDS X 100 % 16 soups �• `� s = 1 WHO i W33d Md r �noy s=2o�eq�,u1 IC+fl :$am L unulegnoul luj= I Ndul x 01. 6 :* impul �) -P - e =�PUf NdPV =MBAR 3eWn9 "S - algno® M mUng 4ouail S - spulS LUOua4S - algno© + ii�1 0I loz 6L j Q - 4- � lA'�i i 7 Z { ©� $ f i _ v AW _ _sod an7)n uvtI� uS ;II {alo.L � agns LAWS1 e� : wd A EI -41d ! k : l° I I .---v l H Noun -- 'ill i -1 =ISRISW 3so1. =GBQ 1991 :.talduses :awr L ®{dwL,S _also seldW, -01 eldw t PERCENT SOLIDS FOR COMPO-ST MPN DAM, ..._ I ANAL' YST: 1:�.I, , / '� DISH WEIGHT: a , GRAMS DISH WEIGHT & .WET SOLIDS: a+ -7 • GRAMS DISH WEIGHT & DRY SOLIDS: sl' 9 GRAMS COMPUTATI6143r x Y DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS -- DISH WEIGHT * WEIGHT OF DRY SOLIDS CALCULATIONS. � % SOWDS WEIGHT OF bFty SOLIDS iC 100 WEIGHT OF WET SOLIDS ple - A L f_ "7- e t E Anple Date: �.� f - t i LI m► for water Berth Sample Time_ sampler: , Teat Dakw Test Analyst � Broth Saw* � TotalTube Str�a►� tit =.on dos' "ve 2 + + _ DoUb + - s + - {,. A + - 1© 55 + - 1 k 1 8 + + _ t u 14 + - 174 8 + _ 19 tb frJt Md; + 20 - - . Wc:Vfx Control. MPN Index.- Sin�te - sfteputh : —7. a. Double - Strength`- Single - Strength Bulgy Wat : _% IfKbx Double - Sterigth Buffw Water. < 44 X AfiPN bukoc I 100ml " ha wa Vokum x % OSY Satiate i' Incubation Thytew. . Diy lncubator_ 3 h9um ---fatar Bath: 21 +I- 2 iin-s. MPH FECAL COLIFORN i GRAN PERCENT SOLIDS FOR COMPOST MPN DATE:. Ia t_ / 1 �- ANALYST: DISH WEIGHT., DISH . WEIGHT & WET SOLIDS:., C,�,�„�GRAMS DISH WEIGHT & DRY SOLIDS: � � �� GRAMS 1 COMPUTAT08-1 A , DISH WEIGHT & WET SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: � % SOLIDS WRIGHT OF DRY SOLIDS X ton % WEIGHT OF WET SOLIDS 1 X 10o % SOWS FEMAL COL620M - MILTME TU13E F 8 /A' SM G & Ef : mpl [D: 13 .maple Done: a _ t e - (I y icy for water Beth Sample Time: 9 : -19 AM 7hm in I �: A� I : ", Sampler:- nr.� r;✓. ,rims t)ert Pm l�3r Test Date: Test Analyst: Tube # Broth swfvha Confimiadon Total Stranoth I Dikiffion Positive + _ 2 AL + - c `? aDouble 4 - L T - 1 1^2il+U.7 7 R 1. � a - 9 (D_'t all) + - K a 10 + 1 Y t + j 2 1I3 pow f - 14 [Qt} + - 15 IF - 16 _ y+ T _ 117 19 difv Ganftnt Single - 5ar : c� Double - StrengM Broth: _ Single - Strength Buhr Waj: _ Double - Stwoh Buffer Water-- incubation Timms:. Dry Incubator: 3 Burs -fet6r Het: 21 +1- 2 ftm . M>N Inde1C: 0`- <3- Q -e )-. 10 X MRN kukDc / WOW Larumt Vt x % MY Soles PERCENT SOLIDS FOR COMPOST MPN IFC6' DATE: , _ /I.4, Ti . ANALYST. DISH WEIGHT: ��.r:r GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DRY SOLIDS: �...�.�; GRAMS . . GC�N9PUTmTICNV9. ,I 'A ,I DISH WEIGHT WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS 0 P DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS I f� s + T • _ 1 CALCULATIONS � % SOLIDS WEIGHT OF DRY SOLIDS x 100 % WEIGHT OF WET SOLIDS f x 100 % 16 soups rnple, ll3- .:4tnpte Date: Sample Time: Sampler: Test Date; Test Analyst: o C - I y ® o r Water Bath ® eve FCl Q -- Tube Broth Sample Contartt t Total S I Dii lon Pos' "vie Gqq t R f r R 7 a + - fa:# f - 10 lam 12720w 14 L 17 BLE 1s s 2a - Sterility_Con Single - Strerat h Manx .�. Double - Strength Draft - Single - Strength Sulfr Waive: _ Double - Strength Buffer Watw-- n, OrcML *#.- 3Q�F7 Incubation Times:. Dry inmabator: 3 ids MPN Index: 11XIM 0-7 40 x IN kukocI 100ml Larowt Voku e x % #3ry Sates xa7-3 a? 3 -PM FECAL. CA3LJFOFM 1 G PERCENT SOLIDS FOR COMPOST MPN DATE: • I ._. ,.. t , ANALYST. �,, • DISH WEIGHT: :ORAMS DISH WEIGHT & WET SOLIDS: ~' GRAMS DISH WEIQHl' & DRY SOLIDS: 'GRAMS COMPUTATI 811 , DISH WE16HT S WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS- � % SOLIDS WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS � . 5 x i oa % • �2 3 � 8a�a� � �d i Mpte ID: FA -AIRIFOXW a e. ' - 2 (1 - l y - MY k=Ubat" water Etta Sample Time_ q : ,L(I A ^^ J Wmain Sampler1 Q a�oasc t3ra —� Single - fterath Oe : _ -d Double - Strength arm x- Sa - Single - Strength BL4Tw wa : _ 11it E -7, � Double - SBuffer water 10 % Nt N Index / 1t 0ml A-'1 Broth Lot #: 3 _ l ! g = _ /<1, 7 - 7 a incts�sticyn �trr - � V x % � Son& t Dry Incubator_ 3 hgurs +eter Bath: 21 +1- 2 ftm PH FECAL COUFORFA f GRAM : �� : e •.r3�� 'tame tit Test Date: _ ! Test Analyst r A Tube Ek°th � � 'Total Stren Dil Ion loos- ve + _ 2 A + _ 3 ib� + - - + { A + . s + _ i 0.'1 ad + 13 + 12 8 -I 3 + 14 (aatad) + 15 + 16 + _ I$ s + 20 � � a�s't � i a�oasc t3ra —� Single - fterath Oe : _ -d Double - Strength arm x- Sa - Single - Strength BL4Tw wa : _ 11it E -7, � Double - SBuffer water 10 % Nt N Index / 1t 0ml A-'1 Broth Lot #: 3 _ l ! g = _ /<1, 7 - 7 a incts�sticyn �trr - � V x % � Son& t Dry Incubator_ 3 hgurs +eter Bath: 21 +1- 2 ftm PH FECAL COUFORFA f GRAM ` c3 Pry PERCENT SOLIDS -'----FOR COMPOST MPN DATE:. 1 ! l ANALYST: DISH WEIGHT: eGRAMS DISH WEIGHT & WET SOLIDS: Y 7. GRAMS DISH WEIGHT & DRY SOLIDS: r � < �' GRAMS COMPUTATICift. , DISH WEIGHT & WET S'OLIDS DISH WEIGH' WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS -- DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS; % SOWDS = WEIG-KT OF DRY SOLIDS X 1oo % WEIGHT OF WET SOWDS x 100 % ch souot I mple ID: Anple Date: Sample Time: Sampler: Vest Date; Tast Analyst: �i-f5 iLI (�Art'i Q%I 4L..: - =�0 ---FTube # Bfr th Sarc�� cord�t To#al S&M DI! ion 2 + _ P 3 a + - 4 4�MI)- 5 - T f _ 4 y !0 a } R G 3 @ate14 _ F i 15 iS + _ 97 Is { - ?9 20 .� tl-con1 Sing& O,--OL Double - StrengM Srcox- �-r Single - Strength Bulgy Wad: Double - Strom surer Watw- A-1 B %MLAA#: 3Q-7vaf7 Incubation, Times:. Dry Incubator_ 3 iqufs Bath: 21 +IL 2 tics. 90 X WN index 100mi Laffusa Vokum x % Dry Satids ��3�.� 3� PERCENT SOLIDS FOR COMPOST MPN DATE:._ I / ANALYST: DISH WEIGHT: a - GRAMS DISH WEIGHT & WET SOLIDS:c-) GRAMS DISH WEIGHT & DRY SOLIDS: GRAMS CCiNIPUMICift , DISH WEIGHT WET SOLIDS DISH WEIGHT WEIGH" OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: � % SOL.IDS = WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS ..5 X 100 % I/ -I- rnple ID -- Ample Date: Sample Time: Sampkm Test Dakw Test Analyst: ry 2- �y C 'f�mits Ett D ry humbztnr water 6nth Tube Broth 1e Total F Stern iD} ! POSH eve A g v 04- ` 5 2' �a — A + _ S 10 + _ 12 1. 13 Doulft+ - . a 14 Meted) + _ + qt i6 i - tl Is sis► + _ 19 20 + _ Wtv_ contmi Single - 5 an Aff Double - Stibngm 33TCOE Single - Strength.Bulfr Water: Double - StrengtM Buffer Wa%r_ Al BnAh Lot#: -7 Incubation Times:. Dry Incubator_ 3 h9um 1ate�' 8alh: 21 +1- 2 hM MPN In de IOW 44 x MPN fulec! 1OCknl �Pl�tg - ►.c��3� _ Las l=afewt VGkUM x % DIV Solids r_ •K 3 t; 5 J i - s- triPYRIJ PERCENT SOLIDS FOR COMPOST MPN - DATE: , J I I AN&YST; , DISH WEIGHT:- GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DI RY SOLIDS: ' ' 9. GRAMS Dom. PUTATIONS. , DISH WEIGHT & WET SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS FG' CALCULATIONS, % SOL.IDS WEIGHT OF DRY SOLIDS X 100 % . WEIGHT OF WET SOLIDS X 100 % ,� souve a- Y FMA1L c{3EWORm -- mjLTmE TusE i EwEwmm rw Ste'# G & E) - mpie !D_ Angle Date: Sample Time; Sampler. Vest Date: Test Analyst: w9Z, Zen- T-yf�( s flry humbnkt Wager 6mth Tube # Broth ffna ion Tatar Sin i©n Pos 've a ^ + -. �{ DoMble F + 4 }j-5Ems is - y - G10 E {' 12 13 ti D14 f L to -at iS ♦ _ 1 B + _ I S" { _ 19 Ed) 20 Fi fV-Con s_ Single - Swarms s Double - Si wVM Broth: Single - Strength Buhr Wad: Dauble •- Strength Buffer Water: A-4 Bnoth Lot #:' J ';�4 7 (3 � ,j 7 Incubation Times:. DFy InGubator: 3 +�te� 21♦1- 2 rw. l ;W- C�WQ .10 X MPN Indexl 11001ni Largest VGbAM x % Dry Solids PERCENT SOLIDS FOR' COMPO-ST MPN DATE:, 1 f% I . I ANALYST; , DISH WEIGHT: r GRAMS r DISH WEIGHT & WET SOLIDS:; (o GRAMS DISH WEIGHT & DRY SOLIDS: �;,Gj.,,; GRAMS - 1 COMPUTA716 NGI , DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS lWN CALCULATIONS % SOLIDS WEIGHT OF DRY SOLIDS X 100% WEIGHT OF WET SOLIDS X 100 % D sWoo f "r. J. mple 1D_ ample Date: Sample Time: sampler - Test Draw: Test Analyst W- J�P jam. �' .a� - a Y �-[- dLI -ry #Iry hIcUbFA-" t fiftr fttb of Tube #°� �� � Total S Dil ion Posit've } - 4 � � 1 MI) g § 10 • t ,.ham 13 F q Mat so) 1 } 17 B .� 20 -� Wty conftt Single - Strenwn oft , Double - ftwigih Srvth: _ Single - Strength Buffer Ora-taj: --OL Double - Strenglfi Buffer Water, Incubation -erirmes: . Djy Incubator_ 3 hours fdar Beft 21 +1- 2 ti ,& 10 x MM Index i 100MI Est VGkUM x % My Solds PM FECAL CGUFORM I GRAM � j " t PERCENT SOLIDS FOR COMPOST MPN DATE:.�„!{l ., „``I ,.,.(,•„�„ ANALYST.' DISH WEIGHT:' _ (0 GRAMS DISH WEIGHT & WET SOLIDS: ��, 7 GRAMS DISH WEIGHT & DRY SOLIDS: 9 ' GRAMS COMPUTA71CM. r , DISH WEIGHT & WET SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS s C>? J DISH WEIGHT & DRY SOLIDS _ DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS WEIGHT OF DRY SOLIDS x 100 % WEIGHT OF WET SOLIDS - r - 3 x 100 % sauve 1 �--�. 49 rnpw ID_ ample Date: Ll _ .) `I sample Time: „►; ins In Samples : r> �9,�z� s ck �'�nss tarot Test mate: Test Analyst: LI Tube Ekath Sample ConfinTgOt TOW "ve Shen t Dii ion Pos" 2 A t _ i 3 Doublia + 0 ad) + - 5 7 � A + s Sirn s + P 9 l ILI aid j + 10 + pgy \J 12 8 + _ } i3 + _ P -0 .i 5 + 17 I 2Q + _ Wttf_ coed Single - Strength Oe ,_,�L Double - Strength Bronx- SK Single - Strengih Buffer Wad _. Double - Strength Buffer Water. A l Bnofh tat * incubal;ion Tows:, Dry Incubator_ 3 hgws ----- &Wr Bsfh: 21 +1- 2 hm 1 IndeK W 44 X MM Index / fOUmi _ MPN ! Q tweet Vaknue X - ter SoEd - 1 '43 q • S PERCENT SOLIDS FOR COMPOST MPN DATE:. I. ! / ANALYST; DISH WEIGHT: �- c, GRAMS DISH WEIGHT & WET SOLIDS: ' - GRAMS DISH WEIGH' & DRY SOLIDS S' GRAMS COMPUTATON9: , DISH WEIGHT S WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS -- DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATION % WEIGHT OF bRY SOLIDS X 1pp % WEIGHT OF WET SOLIDS f X 100 %E) sauna ells-� 4t • v mple-!D_ -ample Date: Sample ..Time_ � �n Aw• � 1n Sampler: t ,— $a% Vest Dais: Test Analyst: --,�f' nffw hwM3hPdtftr Weser BMW r -0 -7 P^, Tuk�e Broth Samphl Total StrengthIli# ionCordks Pos' 've 2 3 Loubffs + - 5 + - 7 Singft } P ' 9 1© 12 13 Ekmdftt _ 14 17 is s 19 t 9.0" ,>d ) + - 20 �- aaa- ._ 6�f'd iff1. YFs ofi t i MPN l w ' Single - Btrcth Off: Double - Strangtfi _ - Single - Strength Buffer Water: _ Index It Double - St wgp Buffer Water: A-9 MOM Lot #: �� �7� a� � :Uptl ! g = Incubation Times:. Dry lnaAbator_ 3 hq►ats ---!star 88ft 21+1- 21UE. 7D x WN Index! 100MI Lareea V x % MY Soft s MPH FECAL.. COUMRU 1 GRAM la x f 3q �3�c PERCENT SOLIDS FOR -COMPOST MPN DATE: ! ANALYST: DISH WEIGHT: � GRAMS DISH WEIGHT & WET SOLIDS: 7 GRAMS DISH WEIGHT & DRY SOLIDS: '' �.,,1,...,.,.,,, GRAMS COMPUTA►TION$: , DISH WEIGHTS WET '86LIDS DISH WEIGHT WEIGHT OF WET SOLIDS NNW - DISH WEIGHT & DRY SOLIDS - DISH WEIGHT = WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS = WEIGHT OF DRY SOLIDS x 1Q0 % WEIGHT OF WET SOLIDS x 1OQ % ob OWN It • M1pteID: Anple Date: Sample Time: C�b /� ; N>;cy'` 1� In Sampler: �.�4�_.....�.MMna t7W Test Dew. Test Analyst: � y 1�= R to Tube � Broth • Sample Core I V ed Stern D� l©t� limos' 've + _ 2 t Double (� $lr4b y 10 } 12 I3 pouffe + _ F 74 {a@tBe) + 15 17 L 20 - �L- tv G()D 1 Single - 5� Double - Strength Brah:_ Single - Strength SuF)e+r wad: _ Double - StengM Buffer rater_ 40 x MPN twIeK 11GGrnl LaraestVdknmx % Ory Soil Incubation Twies: . Dry [nmAator_ 3 hgUM ---feWF EIMv 21 +1- 2 tus. E� / PERCENT SOLIDS FOR COMPOST MPN DISH WEIGHT., GRAMS DIAH WEIGHT & WET SOLIDS: GRAMS DISH WEIQHT & DRY SOLIDS: GRAMS DISH WE16HT WET'S'OLIDS DISH WEIGHT WEIGHT OF WET SOLIDS Ll DISH WEIGHT & DRY SOLIDS DISH WEIGHT WE'lGHT OF'DRY SOLIDS WEIGHT OF WET SOLIDS - 3c� J Y p€GA! COED - M.TME TU13E Anple Da#e: 4- _ -) a , i If-/ Ikv humbpte,r Water nth sample Time. Sampler: Test Dates: Test Analyst: wMe In -rMM Out � vZ : � . l•'.�w � � J � OStw. Tune # Broth SaRvi@ Conffanaffon =PTO= Siren I�il}©n e i E + _ 2 A + 4 DOMWO t C), 5 7 � �pu A + - §§ 1© + 12 -13 Double i5 + - 16 + - 1 7 18 19 s { - Single - SwergUi Om (a Double - Strangth _ Single - Strength Buftr Water: _ tifl�tlt w- Double - Strength Buffer Water_ 4D X MPN Max 11001ni Largest Vbbmw x % ihy Soil J x3`). j, 3 Incubation Tirrms: . Dry inm"tor_ 3 hours T --_fdar SOL' 21-+/- 21MI& RgPiot FECA9.. COLtFO I _� PERCENT SOLIDS FOR COMPOST MPN DATE: ,� I .& I ANALYST: JIM DISH WEIGHT: DISH WRIGHT & WET SOLIDS: � GRAMS DISH WEIGH' & DRY SOLIDS: I A - -3 GRAMS COMPUTATIONS., , DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS -- DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS WEIGHT OF bRY SOLIDS X loo % WEIGH' OF WET SOLIDS v r � FECAL CO - ice. TUM (89 $221 C & E) mple Eta_ � P r � rr c,- q- iinple Date: '-7 _ -QY (y MY kdcubEa" water Bttx Sample Time: Sampler: -- i', i'eee:s aert � �. Test rite: Test Analyst: � Broth Tune=Strer Sane Confi on �° ?Ori PoS- Ye 2 § A + .�. c - i 1 . y^5 L: - 12 4 i5 17 I$ s B 4 9 y f O.M Md)- _ 20 R�- Single - SWerwowth, froth: <T` Double - SbmTKj1h Sri Single - Strength Bu#ter I 11XIOX W Double - StrengM Buffer Water_ VIS A-1 Broth t c* #: incubation Times:. Dry lnmfttor_ 3 h9um -fdOr Beft 21 +1 a thus. r. I 14 X MPN indGx 11 ODmi Est WAUM x %My Solids , l '``�'(6- W' MPH FECAL COLIFOr c 1 t i PERCENT SOLIDS TOR COMPOST MPN DATE; .�---� I ��'�.. I ....L.`l..a b AN4L' YST; DISH WEIGHT: _ to GRAMS DISH WEIGHT WET SOLIDS: j 9.�. GRAMs DISH WEIGHT & DRY SOLIDS: GRAMS DISH WEIGHT & WET 'SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS 7 - I7 DISH WEIGHT DRY SOLIDS DISCI WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS � `I6 SOWDS WEIGHT OF DRY SOLIDS X 1(]0 WEIGHT OF WET SOLIDS x 1 oo soups PERCENT SOLIDS TOR COMPOST MPN DATE; .�---� I ��'�.. I ....L.`l..a b AN4L' YST; DISH WEIGHT: _ to GRAMS DISH WEIGHT WET SOLIDS: j 9.�. GRAMs DISH WEIGHT & DRY SOLIDS: GRAMS DISH WEIGHT & WET 'SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS 7 - I7 DISH WEIGHT DRY SOLIDS DISCI WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS � `I6 SOWDS WEIGHT OF DRY SOLIDS X 1(]0 WEIGHT OF WET SOLIDS x 1 oo soups REGAL COL. R:OM - MULTME TUM (M 9221 C & Ei -� mple ID,A- - `mple Date: _ a r r y Dry hawAmter waver Bath SampleTime: ' 1 ®?, , , Sampler: Test Date: Test Analyst: Tube Broth Sinath Total Pos• •ve Same Dii !on Ceti you i 2 t A �- 10 .j. { 12 '1 14 17 s i e ssssgse _ 1 -r M& QW01- 1 P'1U ft�t e : Single - St;anaqg opt: .__C%Z_ Double - Strength Draft- Single - Strength Buftr wag . _ 11XIOJE w �. f Double -.Strength Buffer Waten 10 X AfiPN Index 1OOtnl Incubation TEmes:. Largest 11ukam x %try Solids j z ti •gr ys . �' Dry incubator: 3 hours .---tiler Beth: 21 +1- 2 hm PM FECAL COUFORM I GRM.< 1 a PERCENT SOLIDS FOR COMPOST MPN DATE:.._... I .., AN&YST: DISH WEIGHT: GRAMS ©I,SH WEIGHT & WET SOLIDS: C "i GRAMS DISH WEICHlr & DRY SOLIDS: „ j GRAMS COMPUTAVONS: DISH WEIGHT & WETSOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS — DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS X 100 1 7..: _J 96 o. �1 I � souv� FECAL, COLAF01w - nuurm Tom 1809MC&M mple ID., '14nple Date: Dry kwubm" vmftr Raul sample I Ime-, Sampler. Test Date: � Ail R : L4 o A,^ Test Analyst :Z Tube cordinnaffon Total §M20992 on Posifive, + 2 A + 3 f DoUbOR 5 7 A 9 I . 0 I I I T+ 12 14 UE# froth =1 + i 5 + -0 17 13 I$ 87mgj% 19 P Single - Stsiar*qth Mmg MN Indew Double - ftejVM fir: - Single - Strength IBLger Water : lixfox It '90 Double - SuerkgM BUffqr Wat9r.- cj 7` 10 X AfiPN Indoc I I 00ml A-1 8101h Lc* OIL K %N- #-' Incubation Tifftew, Largea VOWAM X % Ow solift 3Q.3 OFY Incubator. 3 hours 21+1- 2ftm UPM FECAL COLWORM I GRM PERCENT SOLIDS FOR COMPOST MPN DATA, ,,....�.._ � �; � , I,�.., AMYSr: DISH WEIGHT: ;,�,GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGHT & DRY SOLIDS: � j,•„ ; GRAMSAM . Com. PUTATIONB.• d - DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: � % SOLIDS � WEIGHT OF DRY SOLIDS x 100 % WEIGHT OF WET SOLIDS x 10o % soave •5 I f�. J FUGAL COLW - MUL3E 7UM f8ft 9221 C & E} ,dnpte Uai e: Y- S = I y Dry/ for Water Btth Sample Tirne_ JC) . v 3l �4�- _ sin MIM90 MIA Sampler: rMIe-Out Test ©ate: Test Analyst: Tube $path San9ft w on Total strap t i�i# ton Positive + - 2 A + a 3 c I — 5 �} „ 5 *Ing i © .t. . a }4 toot/. + _ v i 1 + r❑x R II i a20 Single - Ste maiMmft- Double - Strength froth: Single - Strength Buf%r Wafer: Double - StrengM Buffer Water-- Index W A-1 Broth Lot 3v i c) a -e _ UpM i g Incubation Tines: . Largest Whane x' Dry Solids i ' 3 i. � 3 r _ 1 Ou Incubator_ 3 hwm -h: later ae21 +1- 2 face. FN FECAL.. COLWORM I CRAM I _— ORMOMM u o Single - Ste maiMmft- Double - Strength froth: Single - Strength Buf%r Wafer: Double - StrengM Buffer Water-- Index W A-1 Broth Lot 3v i c) a -e _ UpM i g Incubation Tines: . Largest Whane x' Dry Solids i ' 3 i. � 3 r _ 1 Ou Incubator_ 3 hwm -h: later ae21 +1- 2 face. FN FECAL.. COLWORM I CRAM I _— ORMOMM u o r: PERCENT SOLIDS FOR COMPOST MPN . DATE:, / ANALYST: DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIGH-" & DRY SOLIDS: I ;�� GRAMS GpI�RUTA►TIONBi ,, 'A . DISH WEIGHT & WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS � % SOLIDS = WEIGHT OF DRY SOLIDS X 1Q1) °% WEIGHT OF WET SOLDS l V X 104 % 96 MUDS -r 1 7 r � AO �D- '►iple Date; Sample rime: Sampler Test Date: Test Analyst: - - Dry h water fttb ice in �,1 i l . ag.A Tmw-Out 1LI Tube # Broth Sample TOW Ste'8t� lB Di# ion P s' rye 2 0 6 _ ` _ a 1© 14 P , ' 15 .�- y 5 117 i Sis►�!e + s - 20 -�- Steaw— controt Single - Stem!. Ie: Double - Strern h Siod Single - Strength Buffer water: Double - Strengm Buffer Vlfater_ _ A -I ,ct#: .3Q-7(j;?'7 Incubation Tiamr. . Dry inMAOtor_ 3 ho= —t®ter SOL 21 +1- 2 teas. to W- 44 X MPN lnftx / 1 OUml _MPM / g = . Lawattaa x % cwI/ Sobals = Jc�< � � 3 3s : y Phi FECAL COUFORM 1 GRAM PERCENT SOLIDS FOR COMPOST MPN DATE: • !-7, 1 zl ANALYST; DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: L[ L( GRAMS DISH WEIGH' & DRY SOLIDS: J.Q�, GRAMSAw COMPUTA►TON9: DISH WEIGHT & WET SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS DISH WEIGHT &, DRY SOLIDS DISH WEIGHT WEIGHT OF. DRY SOLIDS 77, CALCULATIONS: � SOLIDS = WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS Ll X 100 % �? 96 SOUPS C� D,5 r FECAL C3LG:OM- - MULE TUB (80 $221 C & E) mple ID-- hnple Date: Semple Time: Sampler: Test Data: Test analyst: A T-Ms In 'i MM-Out 1kv humbaw water 6atb Tube # " Broth Same ConfimWion Total Stran DR ?on l''os' 've � A 3 i3swb6a 14 [[t i S s $ir�ta A + t s '10 f 12. -13 14 1� - f17 q 1(( _ Ge. Single -Stoarwgth fah: Double - Strenuftl Broth: Single - Strength Buffer Watw. Index Double - Strenoth Buffer Waten ci �-- A-3 Bnath i. ct #: �i `7� i j 7 Incubation Tirnw.. Dry 1nGvj ator_ s hgUM -- ater Eleft 21 -+1- 2 hm 10 X AfiPN lndeu! 100MI Largest 1fOknM x % MY SoEds 3 y . t, P14 FECAL COLWORM I GRAM < I r: PERCENT SOLIDS FOR COMPOST MPN QATE: AMAL' YST: DISH WEIGHT: GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISH WEIQHT & DRY SOLIDS: GRAMS ; GRAMS COMPUTATONS: DISH WEIGHT WET SOLIDS DISH WEIGHT a WEIGHT OF WET SOLIDS C�> 3 . G DISH WEIGHT & DRY SOLIDS _ DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: � % SOWDS = WEIGHT CIF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS - .�" X 100 % soups 4 ►' FECAL Vi.i�� � MULTWLE TUM FERFAWATON (W OM C & 0—) j Ample Date: r cti - d > - ty Dry bumd2at" water >tth Sample Time: 7-Me Sampler. � ' Test Date; f ®- A Test Analyst — c� Tube # Broth San4 a won Total Stun tail ion , P©S� 2_ { - A 3 [3oobf f - 4 c s 4- hp 5 � + 7 single S f 1012 _ + r IA 1 f r 1 3 Double 14 wa 15 16 -r- 17, B '► — d Is $ 20 �- - Stadler contra : Single - ftrana th Omft Double -Strength $ram: Single - Strength Buhr w Double - Strength Buffer Water: MPN Index: - 40 X MPH Index / 100ml Lamea VGbMw x % MY Solids I <. incubation Tines:. Dry lncwmu r_ 3 hguts -later Bar 21 +1- F Errs. PN FECAL. COUFORM I GRAM < � c PERCENT SOLIDS FOR COMPOST MPN DATE; /'� I ANAL' YST:..' DISH WEIGHT: c�- 4 GRAMS DISH WEIGHT & WET SOLIDS: 2L 33 GRAMS DISH 1NIGHT & DRY SOLIDS: c GRAMS COMPUTATIONS: A , DISH WEIGHT WET SOLIDS DISH WEIGHT WEIGHT OF WET SOLIDS 02a "7 DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: % 50I.IDS = WEIGHT OF DRY SOLIDS - X 'IQo WEIGHT OF WET SOLIDS x 100 % % souDs tea. L43•- c $PROS fOO OUWIPAVmbwl. 4 XGPUI _ $PU! NdM . a yt �z Ime :sawij uogegnouj L 9-C 1--4 I>� :# wl qwg a-V QiBtu)49 - aignoQ M s8 t8uas - efGutS �6ue:gs - a�aJno� - + oz L ice"'^ ra ] 1 rt y a g 3n. , svd uoJ gtj t i�9 is i �� eLS 41�$ni ��i�b ZsQI ZO -'emu 1991 iL :sadusaS wd vS H :f tor A 1 .1 OJ :Grad-IngoejdweS s e►uc 1 L - ®� :9180 etduy,, 38ft 31k&L-I - viownco-m3d PERCENT DATE: 1® SOLIDS FOR COMPOST ANALYST: MPN DISH WEIGHT: �; ,tb GRAMS DISH WEIGHT & WET SOLIDS: GRAMS DISK WEIGHT & DRY SOLIDS: L �..,�.�.,,� GRAMS COMPUTEATION$: n , DISH WEIGHT & WET SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS a DISH WEIGHT & DRY SOLIDS DISH WEIGHT WEIGHT OF. DRY SOLIDS c� = � n> CALCULATIONS: % SOLIDS= WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS X 100 % I 96 SOUP$ FECAL COED - MIME TME RNEUMMM tom# C & E) mple !a,_- hmple Date:: 1® - a- $ -1 N _ Dry kn r Water ftth Semple Time: ,:r.�� _� � � � c� c1 �- j�2 � c� • P^� Sampler: C < mac. ors" o ci PN► ! s.Z A., T"t ©ate: Test Analyst Tune Broth Stren �e Di aon confim�ion Total t� �s' 've a 3 5 - S 7- 1 ij iJ a 1 12 1314 - - 75 16- I1 B + _ Is g wvw-con e Singe - 5� Oaf:- Double - Strength Dion_ Single - Strength Buffer Wa%: Double - Strength Buffer dilate. A-1 eroM t.a* *: incubation Times: Dry incubator_ 3 h9am ,+stet Bath: 21 +1- 2 W& I 14 x UPN frmftx I I00MI - Largsst Vd um x% My Solids wv FECAL COLIFORM i GRAMaG � PERCENT : SOLIDS FOR COMPOST MPN DATE:. I .. ;. I _.,._L'�, ANAL' YSM MUM DISH WEIGHT: a- GRAMS ©I�SH WEIGHT � WET SOLIDS: o , q GRAMs _ ���� ' DISH IIVEIGHl' 8� DRY SOLIDS: kb GRAMS COMPUTATION& DISH WEIGHT & War 'SOLIDS DISH WEIGHT = WEIGHT OF WET SOLIDS L �-3,3 y DISH WEIGHT DRY SOLIDS DISH WEIGHT WEIGHT OF DRY SOLIDS CALCULATIONS: % SOLIDS WEIGHT OF DRY SOLIDS X 100 °% WEIGHT OF WET SOLIDS X - 10Q % suave