The URL can be used to link to this page

Home My WebLink AboutWQ0001989_Residual Annual Report 2014_20150216L ROANOKE RAPIDS SANITARY DISTRICT RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0001989 2014 ANNUAL REPORT Roanoke Rapids Sanitary District Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. ' Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAN® APPLICATION CERTIFICATION FORM WQ Permit #: W00001989 County Halifax Year 2014 Facility Name (as shown on permit) RRSD WWTP NPDES No. NCO024201 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and Part Band proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 96 Total number of fields utilized for land application during the year: 10 Total amount of dry tons applied during the year for all application sites: 617.47 Total number of acres utilized for land application during the year: 319.1 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. Tire facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." R. Danielev Brown. Chief Executive Officer Permitt a e and�Ti (type or print) S ign ati i e e FEB 1 An 2015' Signatu of preparer* ate Sign.att0e of Land AppliK Date (if different from Pe ' ee) (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION ROANOKE RAPIDS, NC ROANOKE RAPIDS, NC LIME STABILIZED LIQUID MONTHNEAR April 2014 May 2014 June 2014 September 2014 October 2014 YEARLY TOTAL DRY METRIC AMOUNT UNIT DRY TONS UNIT TONS 731,600.00 G 123.25 D 111.79 204,600.00 G 35.83 D 32.49 923, 800.00 G 161.80 D 146.73 1,091,200.00 G 218.41 D 198.10 390,600.00 G 78.18 D 70.92 3,341,800.00 G 617.47 D 560.03 2/2/2015 2014 ANNUAL REPORT PROJECT: Roanoke Rapids Sanitary District FACILITY: Roanoke Rapids Sanitary District WWTP 135 Aqueduct Road Weldon, NC 27892 252-536-4884 NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: NC0024201 R. Danieley Brown, CEO RRSD 1000 Jackson Street PO Box 308. Roanoke Rapids, NC 27870 252-537-9137 Greg Camp, WWTP ORC 135 Aqueduct Road Weldon, NC 27890 252-536-4884 Timmy Skipper, RRSD 135 Aqueduct Road Weldon, NC 27890 252-536-4884 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001989 Laboratory Facility Name: ROANOKE RAPIDS, NC A&L Eastern Laboratories Inc. NPDES# : NCO024201 or WQ# (residual only) WWTP Name: ROANOKE RAPIDS Residuals Analysis Data Product Type LSLIQ LSLIQ LSLIQ LSLIQ Date Sampled (grab) or 02/07/14 04/11/14 07/09/14 12/02/14 Date Composited Percent Solids 4.04 4.20 4.80 5.28 PARAMETERS (mg/kg dry weight) Arsenic Cadmium Mercury Chromium Copper Lead Molybdenum Nickel Selenium Zinc Total Phosphorus TKN Ammonia -Nitrogen Nitrate and Nitrite 4 5 5 5 <2 <2 <2 <2 0.7 <0.4 0.9 <0.4 23 30 30 18 120 142 220 139 16 15 21 16 <5 <5 <5 5 10 12 16 11 <5 <5 <5* <5 512 515 554 419 11300 15500 18100 12400 23500 41000 31700 27500 2230 3330 7500 2270 104 119 169 930 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing vioptions." IF;Irls X Date � /QI/3 TI DC C DAD \ DENR FORM RSSF (5/2003) Printed: Monday - February 2. 2015 at 11:28:18 for: 2029 01 - ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: W00001989 Laboratory Facility Name: ROANOKE RAPIDS, NC A&L Eastern Laboratories, Inc. NPDES# : NCO024201 or WQ# (residual only) WWTP Name: ROANOKE RAPIDS Residuals Analysis Data Product Type LSLIQ LSLIQ LSLIQ LSLIQ Date Sampled (grab) or 02/07/14 04/11/14 07/09/14 12/02/14 Date Composited Percent Solids 4.04 4.20 4.80 5.28 PARAMETERS (mg/kg dry weight) Aluminum 45100 34100 52400 44100 Calcium 187000 142000 137000 174000 Magnesium 4720 4570 4240 3630 pH 11.88 11.32 10.02 11.77 Potassium 1500 2250 2720 1400 Sodium 1230 1120 1280 856 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X GNATU NR - Data Not Reported or Data Not Required Date j DENR FORM RSSF-B (7/2002) Printed: Monday - February 2, 2015 at 11:28:40 for: 2029 01 Page: i of 2 Report Number: 14-041-0203 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAUROANOKE RAPIDS MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 97850 Sample Id : RRSD @P A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwwaleastern.com Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/7/2014 11:00:00 Date Received: 02/10/2014 00:00 Date Reported: 02/12/2014 Total Solids * 4.04 40400 100.0 JM 02/10/2014 15:15 SM-2540G Moisture * 95.96 100.0 JM 02/10/2014 15:15 SM-2540G Total Kjeldahl Nitrogen 2.35 23500 10.0 JM 02/11/2014 09:00 SM-4500-NH3C-TKN Total Phosphorus 1.13 11300 100 KM 02/11/2014 11:31 SW 6010C Total Potassium 0.15 1500 100 KM 02/11/2014 11:31 SW 6010C Total Sulfur 0.55 5530 100 KM 02/11/2014 11:31 SW 6010C Total Calcium 18.70 187000 100 KM 02/11/2014 11:31 SW 6010C Total Magnesium 0.47 4720 100 KM 02/11/2014 11:31 SW 6010C Total Sodium 0.12 1230 100 KM 02/11/2014 11:31 SW 6010C Total Iron 7840 100 KM 02/11/2014 11:31 SW 6010C Total Aluminum 45100 100 KM 02/11/2014 11:31 SW 6010C Total Manganese 153 5 KM 02/11/2014 11:31 SW 6010C Total Copper 120 5 KM 02/11/2014 11:31 SW 6010C Total Zinc 512 5 KM 02/11/2014 11:31 SW 6010C Ammonia Nitrogen 0.22 2230 10.0 JM 02/11/2014 09:00 SM-4500-NI3C Organic N 2.13 21270 10.0 02/11/2014 09:00 CALCULATION Nitrate+Nitrite-N 104 2.00 JM 02/11/2014 09:00 SM-450ONO3F Total Cadmium <2.0 2.0 KM 02/11/2014 11:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-041-0203 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAUROANOKE RAPIDS MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 97850 Sample Id: RRSD A&L Eastern Laboratories, Inc.. @P, 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date Sampled: 2/7/2014 11:00:00 Date Received: 02/10/2014 00:00 Date Reported: 02/12/2014 Total Chromium 23 5 KM 02/11/2014 11:31 SW 6010C Total Nickel 10 5 KM 02/11/2014 11:31 SW 6010C Total Lead 16 5 KM 02/11/2014 11:31 SW 6010C Total Arsenic 4.0 3.0 KM 02/11/2014 11:31 SW 6010C Total Mercury 0.7 0.4 KM 02/11/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 02/11/2014 11:31 SW 6010C pH (Standard Units) * 11.88 2.00 JM 02/11/2014 09:00 SW-9045D Calcium Carbonate Equivalent 40.40 404000 100 JM 02/11/2014 12:45 AOAC 955.01 Total Molybdenum <5 5 KM 02/11/2014 11:31 SW 6010C Comments: CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB AND MATRIX SPIKE WERE OUT OF LIMITS FOR "NO3/NO2-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", AND "Se".ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt SAMPLING LOG ft 1111111gill 111111111111111 CHAIN OF CUSTODY l 11 Q2fi418020143 RECORD& ANALYSIS CUSTOMER: SYNAGRO SOUTHEAST • ■� SYNAGRO CENTRAL'ROANOKE RAPIDS 12.22.17 RRSD RECORD r ) J PROJECT MANAGER: ' Jper field sampling procedures were used during the collection of these samples. ,n Phone: SAMPLER A & L CUSTOMER SAMPLING SAMPLE # OF SAMPLING METHOD METHOD LAB # SAMPLE I.D. LOCATION TYPE CONTAINERS DATE TIME PRESERVED SHIPPED Relinquished by Sampl : Date Time Recieved by. REMARKS: Relinquished by: s 1 , D to Time Recie ed by: Relinquished by: at Time Recieved by: SPECIAL INSTRUCTIONS: For monitoring purposes. PO#: SAMPLE ANALYSIS REQUEST I.D. SLi SL2 NH4-N NO NIOrgNnic Cd Cr Ni Pb As H 9 Se PH I GaCO3 a uiv. Volatile Solids Mo Cl NOZ N ^ 100 100 koo ko foot 1000 lot k*40' 10 1400 100 POO to 1000 toof RSO..-- ,,,, ` .ter „/' G-'�..-..-- SL1: Total Solids (Moisture), Total Kieldahl Nitrogen, Phosphorus, and Potassium SL2: Basic Test SL1 plus Sulfur, Calcium, Magnesium, Sodium, Iron, Aluminum, Manganese, Copper and Zinc White — A & L Canary — MANAGER COPY Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2029-01-LSLIQ-NC ROANOKE RAPIDS, NC LIME STABILIZED 2/7/2014 1/l/2014-4/30/2014 0.1540 LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (1230 x 4.0400) = 100 = 49.692 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (187000 x 4.0400) _ 100 = 7554.8 Mg mg/I = (mg mg/kg x % Solids) i- 100 = (4720 x 4.0400) = 100 = 190.688 Na meq = Na mg/I _ Molec.Wgt.Na = 49.692 = 23 = 2.16052 Ca meq = Ca mg/1= Molec.Wgt.Ca = 7554.8 _ 20 = 377.74 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 190.688 = 12 = 15.8907 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.16052 _ SgrRoot[0.5(377.74+15.8907)] = 0.154003 Printed: 2/2/2015 Page 1 11:29 Page: i of 2 Report Number: 14-104-0201 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/ROANOKE RAPIDS MARSHALLPURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 98954 Sample Id: RRSD A&L Eastern Laboratories, Inc- 1 A�I 7621 Whitepine Road Richmond, Virginia 23237 (904) 743-9401 Fax (604) 271-6446 wwwaleastem.com Project: RRSD/NC CERT#257 REPORT" OF ANALYSIS Date Sampled: 4/11/2014 11:00:00 Date Received: 04/14/2014 00:00 Date Reported: 04/18/2014 Total Solids * 4.20 42000 100.0 JM 04/14/2014 15:00 SM-2540G. Moisture * 95.80 100.0 JM 04/14/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 4.10 41000 10.0 JM 04/15/2014 08:24 SM-4500-NH3C-TKN Total Phosphorus 1.55 15500 100 KM 04/15/2014 00:00 SW 6010C Total Potassium 0.23 2250 100 KM 04/15/2014 00:00 SW 6010C Total Sulfur 0.54 5390 100 KM 04/15/2014 00:00 SW 6010C Total Calcium 14.20 142000 100 KM 04/15/2014 00:00 SW 6010C Total Magnesium 0.46 4570 100 KM 04/15/2014 00:00 SW 6010C Total Sodium 0.11 1120 100 KM 04/15/2014 00:00 SW 6010C Total Iron 11300 100 KM 04/15/2014 00:00 SW 6010C Total Aluminum 34100 100 KM 04/15/2014 00:00 SW 6010C Total Manganese 176 5 KM 04/15/2014 00:00 SW 6010C Total Copper 142 5 KM 04/15/2014 00:00 'SW 6010C Total Zinc 515 5 KM 04/15/2014 00:00 SW 6010C Ammonia Nitrogen 0.33 3330 10.0 JM 04/15/2014 08:24 SM-4500-NH3C Organic N 3.77 37670 10.0 04/15/2014 08:24 CALCULATION Nitrate+Nitrite-N 119 2.00 JM 04/16/2014 08:40 SM-450ONO3F Total Cadmium <2.0 2.0 KM 04/15/2014 00:00 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-104-0201 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/ROANOKE RAPIDS MARSHALL PURYEAR 284 BOGER RD . STE 204 MOCKSVILLE , NC 27889 Lab Number: 98954 Sample Id : RRSD A&L Eastern Laboratories, u 7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446 W W W.aleastern.com Project: RRSD/NC CERT#257 REPORT OF ANALYSIS Date Sampled: 4/11/2014 11:00:00 Date Received: 04/14/2014 00:00 Date Reported: 04/18/2014 Total Chromium 30 5 KM 04/15/2014 00:00 SW 6010C Total Nickel 12 5 KM 04/15/2014 00:00 SW 6010C Total Lead 15 5 KM 04/15/2014 00:00 SW 6010C Total Arsenic 5.0 3.0 KM 04/15/2014 00:00 SW 6010C Total Mercury <0.4 0.4 KM 04/16/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 04/15/2014 00:00 SW 6010C pH (Standard Units) * 11.32 2.00 JM 04/15/2014 08:10 SW-9045D Calcium Carbonate Equivalent 30.30 303000 100 JM 04/15/2014 13:25 AOAC 955.01 Total Molybdenum <5 5 KM 04/15/2014 00:00 SW 6010C Comments: CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr" AND "NO3/NO2-N". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2029-01-LSLIQ-NC ROANOKE RAPIDS, NC LIME STABILIZED 4/11/2014 51112014-6/30/2014 0.1632 LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (1120 x 4.2000) + 100 = 47.04 Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (142000 x 4.2000) = 100 = 5964 Mg mg/I = (mg mg/kg x % Solids) -= 100 = (4570 x 4.2000) _ 100 = 191.94 Na meq = Na mg/I = Molec.Wgt.Na = 47.04 23 = 2.04522 Ca meq = Ca mg/I = Molec.Wgt.Ca = 5964 = 20 = 298.2 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 191.94 = 12 = 15.995 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.04522 = SgrRoot[0.5(298.2+15.995)] = 0.163175 Printed: 2/2/2015 Page 1 11:29 Page: i of 2 Report Number: * 14-196-0206 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/ROANOKE RAPIDS MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 56472 Sample Id: RRSD A&L Eastern Laboratories, Inc._ 99. 7621 Whitepine Road Richmond, Virginia 23237 .(804) 743-9401 Fax (804) 271-6446 wwW aleastem.com Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date Sampled: 7/9/2014 14:00:00 Date Received: 07/15/2014 00:00 Date Reported: 07/21/2014 Total Solids 4.80 48000 100.0 BW 07/15/2014 15:00 SM-2540G Moisture " 95.20 100.0 BW 07/15/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 3.17 31700 10.0 MW 07/16/2014 07:59 SM-4500-NH3C-TKN Total Phosphorus 1.81 18100 100 BW 07/16/2014 09:30 SW 6010C Total Potassium 0.27 2720 100 BW 07/16/2014 09:30 SW 6010C Total Sulfur 0.60 6040 100 BW 07/16/2014 09:30 SW 6010C Total Calcium 13.70 137000 100 BW 07/16/2014 09:30 SW 6010C Total Magnesium 0.42 4240 100 BW 07/16/2014 09:30 SW 6010C Total Sodium 0.13 1280 100 BW 07/16/2014 09:30 SW 6010C Total Iron 19800 100 BW 07/16/2014 09:30 SW 6010C Total Aluminum 52400 100 BW 07/16/2014 09:30 SW 6010C Total Manganese 385 5 BW 07/16/2014 09:30 SW 6010C Total Copper 220 5 BW 07/16/2014 09:30 SW 6010C Total Zinc 554 5 BW 07/16/2014 09:30 SW 6010C Ammonia Nitrogen 0.75 7500 10.0 MW 07/16/2014 07:59 SM-4500-NH3C Organic N 2.42 24200 10.0 07/16/2014 07:59 CALCULATION Nitrate+Nitrite-N 169 2.00 MW 07/16/2014 08:00 SM-450ONO3F Total Cadmium <2.0 2.0 BW 07/16/2014 09:30 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made. to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-196-0206 ILA Account Number: 46485 Submitted By: WILL VARNER Wwwaleastem.com Send To: SYNAGRO CENTRAL/ROANOKE'RAPIDS MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 A&L Eastem Laboratories,. Inc:_ -7621 Whitepine Road Richmond, Virginia 23237 (604)743-9401 Fax (604) 271-6446 Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date'Sampled: 7/9/2014 14:00:00 Lab Number: 56472 Date Received: 07/15/2014 00:00 Sample Id : RRSD Date Reported: 07/21/2014 Total Chromium 30 5 BW 07/16/2014.09:30 SW 6010C Total Nickel 16 5 BW 07/16/2014 09:30 SW 6010C Total Lead 21 5 BW 07/16/2014 09:30 SW 6010C Total Arsenic 5.0 3.0 BW 07/16/2014 09:30 SW 6010C Total Mercury 0.9 0.4 JM 07/16/2014 08:30 SW-7471 B Total Selenium <5.0 5.0 BW 07/16/2014 09:30 SW 6010C pH (Standard Units) * 10.02 2.00 MW 07/16/2014 09:04 SW-9045D CalciumCarbonate Equivalent 27.70 277000 100 MW 07/16/2014 11:50 AOAC 955.01 Total Volatile Solids 47.47 474700 100.0 BW 07/15/2014 15:00 SM-2540G Total Molybdenum <5 5 BW 07/16/2014 09:30 SW 6010C Comments: CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation' (SAR) Product Code Product Name Sample Date Report Range Ratio 2029-01-LSLIQ-NC ROANOKE RAPIDS, NC LIME STABILIZED 7/9/2014 7/112014-10/31/2014 0.2032 LIQUID Na mg/I = (Na mg/kg x % Solids) = 100 = (1280 x 4.8000) _ 100 = 61.44 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (137000 x 4.8000) = 100 = 6576 Mg mg/I = (mg mg/kg x % Solids) -= 100 = (4240 x 4:8000) _ 100 = 203.52 Na meq = Na mg/I = Molec.Wgt.Na = 61.44 = 23 = 2.6713 Ca meq = Ca mg/I = Molec.Wgt.Ca = 6576 _ 20 = 328.8 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 203.52 = 12 = 16.96 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.6713 + SgrRoot[0.5(328.8+16.96)] = 0.203166 Printed: 2/2/2015 Page 1 11:29 Page: 1 of 2 Report Number: 14-343-0203 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRALIROANOKE RAPIDS MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 59148 Sample Id: RRSD AV� A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (604) 271.6446 www.aleastern.com Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/2/2014 11:00:00 Date Received: 12/09/2014 00:00 Date Reported: 12/16/2014 Total Solids * 5.28 52800 100.0 JM 12/09/2014 15:00 SM-2540G Moisture * 94.72 100.0 JM 12/09/2014 15:00 SM-254OG Total Kjeldahl Nitrogen 2.75 27500 10.0 JM 12/15/2014 09:04 SM-4500-NH3C-TKN Total Phosphorus 1.24 12400 100 KM 12/10/2014 12:07 SW 6010C Total Potassium 0.14 1400 100 KM 12/10/2014 12:07 SW 6010C Total Sulfur 0.53 5270 100 KM 12/10/2014 12:07 SW 6010C Total Calcium 17.40 174000 100 KM 12/10/2014 12:07 SW 6010C Total Magnesium 0.36 3630 100 KM 12/10/2014 12:07 SW 6010C Total Sodium 0.09 856 100 KM 12/10/2014 12:07 SW 6010C Total Iron 11400 100 KM 12/10/2014 12:07 SW 6010C Total Aluminum - 44100 100 KM 12/10/2014 12:07 SW 6010C Total Manganese 456 5 KM 12/10/2014 12:07 SW 6010C Total Copper 139 5 KM 12/10/2014 12:07 SW 6010C Total Zinc 419 5 KM 12/10/2014 12:07 SW 6010C Ammonia Nitrogen 0.23 2270 10.0 JM 12/11/2014 08:39 SM-4500-NH3C Organic N 2.52 25230 10.0 12/11/2014 08:39 CALCULATION Nitrate+Nitrite-N 930 2.00 JM 12/10/2014 08:20 SM-450ONO3F Total Cadmium <2.0 2.0 KM 12/10/2014 12:07 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. 61/ 4&a Our rePorts and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made , to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-343-0203 Account Number: 46485 Submitted By: WILL VARNER Send To: SYNAGRO CENTRAL/ROANOKE RAPIDS MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE , NC 27889 Lab Number: 59148 Sample Id: RRSD Y A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond; Virginia 23237 (804).W-94o1 Fax (804) 271-6446 www aleastem.com Project: RRSD NC CERT#257 REPORT OF ANALYSIS Date Sampled: 12/2/2014 11:00:00 Date Received: 12/09/2014 00:00 Date Reported: 12/16/2014 Total Chromium 18 5 KM 12/10/2014 12:07 SW 6010C Total Nickel 11 5 KM 12/10/2014 12:07 SW 6010C Total Lead 16 5 KM 12/10/2014 12:07 SW 6010C Total Arsenic 5.0 3.0 KM 12/10/2014 12:07 SW 6010C Total Mercury <0.4 0.4 KM 12/11/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 12/10/2014 12:07 SW 6010C pH (Standard Units) * 11.77 2.00 JM 12/10/2014 08:24 SW-9045D Calcium Carbonate Equivalent 39.70 397000 100 JM 12/11/2014 14:39 AOAC 955.01 Total Molybdenum 5 5 KM 12/1.0/2014 12:07 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "TKN". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ca", "Fe", "Mg", AND "P". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2029-01-LSLIQ-NC ROANOKE RAPIDS, NC LIME STABILIZED 12/2/2014 12/1/2014-12/31/2014 0.1275 LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (856 x 5.2800) = 100 = 45.1968 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (174000 x 5.2800) = 100 = 9187.2 Mg mg/I = (mg mg/kg x % Solids) = 100 = (3630 x 5.2800) =100 = 191.664 Na meq = Na mg/I — Molec.Wgt.Na = 45.1968 _ 23 = 1.96508 Ca meq = Ca mg/I = Molec.Wgt.Ca = 9187.2 = 20 = 459.36 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 191.664 _ 12 = 15.972 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.96508 = SgrRoot[0.5(459.36+15.972)] = 0.127467 Printed: 2/2/2015 Page 1 11:29 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: QUENTIN GREGORY, JR. SITE #: NC HX 00013 FIELD# : HX 00013 0012 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: BONNEAU PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 176.22 OPERATOR: QUENTIN GREGORY, JR. CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 27.80 ACRES PERMITTED: 27.80 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppin) Crop MONTH Total Per Acre Solids 9/15/14 111,600.00 (G) 4014.388 4.80 0.804 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p F 8759 I FESCUE 9/16/14 142,600.00 (G) 5129.496 4.80 1.027 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 IFESCUE 9/17/14 179,800.00 (G) 6467.626 4.80 1.295 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 FESCUE 9/18/14 198,400.00 (G) 7136.691 4.80 1.428 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 I FESCUE 9/19/14 192,200.00 (G) 6913.669 4.80 1.384 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 FESCUE 9/20/14 55,800.00 (G) 2007.194 4,80 0.402 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 FESCUE Sep-14 880,400.00 (G) 31,669.064 Total Gallons/Ac: 31,669.06 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 111 Annuallbs/acre' 0.063 0.025 0.380 2.789 0.266 0.011 0.063 0.203 0.063 7.023 229.47 7,777, Cumulative lbs/acre 0.089 0.139 0.967 17.267 3.045 0.021 0.125 0.626 0.076 55.639 mg 196 Permit PAN Limit lbs/acre 1st Cro /2nd Cro '* ..1A FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 t - RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent , p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, hijection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: QUENTIN GREGORY, JR. SITE #: NC HX 00013 FIELD# : HX 00013 0014 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: EMPORIA PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 62.98 OPERATOR: QUENTIN GREGORY, JR. CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 99.70 ACRES PERMITTED: 99.70 Page Lime Applied *** Date Lbs/Ac DATE.or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 6/6/14 161,200.00 (G) 1616.851 4.20 0.283 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I SOYBEANS 6/7/14 148,800.00 (G) 1492.477 4.20 0.261 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I SOYBEANS 6/8/14 49,600.00 (G) 497.492 4.20 0.087 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 SOYBEANS Jun-14 359,600.00 (G) 3,606.820 Total Gallons/Ac: 3,606.82 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 12 Annual lbs/acre 0.006 0.003 0.038 0.179 0.019 <.001 0.006 0.015 0.006 0.651 19.58 Cumulative lbs/acre 0.030 0.017 0.282 1.408 0.235 0.006 0.078 0.159 0.019 4.935 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 ._ .. 1339.0 267.9 15.0 375.0 89.0 2500.0 RRLSL = ROANOICE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ROANOKE RAPIDS, NC PREDOMINANT SOIL SERIES: NORFOLK OWNER: RRSD PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 120.38 SITE #: NC NO 00005 FIELD# : NO 00005 0001 B OPERATOR: HOWARD FERGUSON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 41.80 ACRES PERMITTED: 41.80 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 9/29/14 74,400.00 (G) 1779.904 4.80 0.356 RRLSL MOIST 0-<I/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 I FESCUE 9/30/14 136,400.00 (G) 3263.158 4.80 0.653 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 FESCUE Sep-14 1 210,800.00 (G) 5,043.062 10/1/14 142,600.00 (G) 3411.483 4.80 0.683 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 I FESCUE ' 10/2/14 173,600.00 (G) 4153.110 4.80 0.831 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 I FESCUE 10/3/14 74,400.00 (G) 1779.904 4.80 0.356 RRLSL DRY 0-<1/2" SUR 0.5 0.20 31,700. p 7,500.00 p 169.00 p 8759 FESCUE Oct-14 390,600.00 (G) 9,344.497 Total Gallons/Ac: 14,387.56 As Cd Cr Cu Pb Hg Mo Ni Se Zn . P PAN TOTALS: 50 Annual lbs/acre 0.029 0.012 0.173 1.267 0.121 0.005 0.029 0.092 0.029 3.191 104.25 Cumulative Ibs/acre 0.101 0.034 0.874 3.902 0.566 0.018 0,117 0.271 0.089 14.657 Permit PAN Limit (Ibs/acre) 1st Crop/2nd Crop t . 4tLt i ` %* 156 pp FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 .` 375.0 89.0 2500.0 z° a: RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.l am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/lcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: HOWARD FERGUSON SITE #: NC NO 00012 FIELD# : NO 00012 0001 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GOLDSBORO PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 51.04 OPERATOR: HOWARD FERGUSON CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 64.50 ACRES PERMITTED: 64.50 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pptn) Crop MONTH Total Per Acre Solids 5/28/14 55,800.00 (G) 865.116 4.20 0.152 RRLSL DRY 0-<I/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 79318 I FESCUE 5/29/14 18,600.00 (G) 288.372 4.20 0.051 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 1 FESCUE May-14 1 74,400.00 (G) 1,153.488 6/2/14 93,000.00 (G) 1441.860 4.20 0.253 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/3/14 93,000.00 (G) 1441.860 4.20 0.253 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/4/14 31,000.00 (G) 480.620 4.20 0.084 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 FESCUE Jun-14 217,000.00 (G) 3,364.340 Total Gallons/Ac: 4,517.83 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.008 0.003 0.047 0.225 0.024 <.001 0.008 0.019 0.008 0.815 24.53 15 Cumulative lbs/acre 0.313 0.147 3.073 14.945 4.023 0.073 0.926 1.168 0.202 67.234 1 M: x ' , :. 182 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop ,� FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 y, .r az RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/hicorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: ROANOKE RAPIDS, NC PREDOMINANT SOIL SERIES: GRITNEY OWNER: HOWARD FERGUSON PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 83.61 SITE #: NC NO 00012 FIELD# : NO 00012 0002 OPERATOR: HOWARD FERGUSON CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 26.90 ACRES PERMITTED: 26.90 Page Line Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 5/31/14 130,200.00 (G) 4840.149 4.20 0.848 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 FESCUE May-14 130,200.00 (G) 4,840.149 6/1/14 124,000.00 (G) 4609.665 4.20 0.807 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/2/14 31,000.00 (G) 1152.416 4.20 0.202 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/3/14 6,200.00 (G) 230.483 4.20 0.040 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/4/14 68,200.00 (G) 2535.316 4.20 0.444 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 I FESCUE 6/5/14 117,800.00 (G) 4379.182 4.20 0.767 RRLSL DRY 0-<1/2" SUR 0.5 0.20 41,000. p 3,330.00 p 119.00 p 9318 FESCUE Jun-14 347,200.00 (G) 12,907.062 Total Gallons/Ac: 17,747.21 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 58 Annual lbs/acre 0.031 0.012 0.186 0.883 0.093 0.002 0.031 0.075 0.031 3.202 96.36 Cumulative lbs/acre 0.253 0.105 2.135 10.241 2.803 0.043 0.724 0.729 0.154 52.251 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop V,, 145 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 44 RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID ;_-/& -ice (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: MASON ROD HOWELL, JR. SITE #: NC NO 00021 FIELD# : NO 00021 0020 RESIDUAL SOURCE(S):* See list at bottom of report i ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GRITNEY PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 39.69 OPERATOR: MASON ROD HOWELL, III CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 24.50 ACRES PERMITTED: 24.50 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/11/14 235,600.00 (G) 9616.327 4.04 1.620 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 23,500. p 2,230.00 p T 104.00 p 5473 COTTON Apr-14 235,600.00 (G) 9,616.3271 1 1 1 1 1 1 1 1 Total Gallons/Ac: 9,616.33 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 18 Annual lbs/acre 0.013 0.006_ 0.075 0.389 0.052 0.002 0.016 0.032 0.016 1.659 36.61 Cumulative lbs/acre 0.016 1.659 ' 0.013 0.006 0.075 0.389 0.052 0.002 0.016 0.032 1st Crop/2nd Crop Permit PAN Limit (lbs/acre)VJ 44 FD Cumulative Pollutant LoadingRate Limit lbs/acre" a . 1339.0 267.9 15.0 375.0 89.0 2500.0 4 RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for Imowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: MASON ROD HOWELL, JR. SITE #: NC NO 00021 FIELD# : NO 00021 0021 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GRITNEY PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 32.38 OPERATOR: MASON ROD HOWELL, III CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 9.50 ACRES PERMITTED: 9.50 Page: 1 Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and . (ppin) Crop MONTH Total Per Acre Solids 4/11/14 31,000.00 (G) 3263.158 4.04 0.550 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 23,500. p 2,230.00 p 104.00 p 5473 I COTTON 4/12/14 161,200.00 (G) 16968.421 4.04 2.859 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 23,500. p 2,230.00 p 104.00 p 5473 1 COTTON Apr-14 192,200.00 (G) 20,231.579 Total Gallons/Ac: 20,231.58 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 37 Annual Ibs/acre 0.027 0.014 0.157 0.818 0.109 0.005 0.034 0.068 0.034 3.490 77.03 Cumulativelbs/acre 0.027 0.014 0.157 0.818 0.109 0.005 0.034 0.068 0.034 3.490® Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 `, 1339.0 267.9 15.0 375.0 89.0 2500.0 RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: MASON ROD HOWELL, JR. SITE #: NC NO 00021 FIELD# : NO 00021 0031 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: NORFOLK PERMIT #: W00001989 OPERATOR: MASON ROD HOWELL, III ANNUAL DRY TONS APPLIED: 7.31 CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 4.90 ACRES PERMITTED: 4.90 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry " Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/13/14 43,400.00 (G) 8857.143 4.04 1.492 RRLSL MOIST 0- 1/2" SUR 0.5 0.20 23,500. p 2730.00 p 104.00 p F 5473 1 COTTON Apr-14 43,400.00 (G) 8,857.143 Total Gallons/Ac: 8,857.14 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 16 Annuallbs/acre 0.012 0.006 0.069 0.358 0.048 0.002 0.015 0.030 0.015 1.528 33.72 Cumulative lbs/acre 0.026 0.014 0.402 1.460 0.454 0.008 0.225 0.146 0.025 5.589 "" fp• '" ", Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop *." FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 `." 1339.0 267.9 15.0 375.0 89.0 2500.0 RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: MASON ROD HOWELL, JR. SITE #: NC NO 00021 FIELD# : NO 00021 0035 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: CRAVEN PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 7.31 OPERATOR: MASON ROD HOWELL, III CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 5.40 ACRES PERMITTED: 5.40 Page Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total TPer Acre Solids 4/13/14 43,400.00 (G) 8037.037 4.04 1,354 RRLSL MOIST Q-<1/2" SUR 0.5 0.20r7377�12,230.00 p 104.00 p 5473 1 COTTON Apr-14 43,400.00 (G) 8,037.037 1 Total Gallons/Ac: 8,037.04 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual Ibs/acre 0.011 0.005 0.062 0.325 0.043 0.002 0.014 0.027 0.014 1.386 30.60 15 Cumulativelbs/acre 0.034 0.022 0.321 1.479 0.334 0.010 0.046 0.130 0.024 5.959 Permit PAN Limit (lbs/acre) 1st Crop/2nd CropAp FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 r RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, hrjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: ROANOKE RAPIDS, NC OWNER: MASON ROD HOWELL, JR. SITE #: NC NO 00021 FIELD# : NO 00021 0038 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: GRITNEY PERMIT #: W00001989 ANNUAL DRY TONS APPLIED: 36.56 OPERATOR: MASON ROD HOWELL, III CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 14.10 ACRES PERMITTED: 14.10 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia' Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/12/14 105,400.00 (G) 7475.177 4.04 1.259 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 23,500. p 2,230.00 p 104.00 p 5473 I COTTON 4/13/14 111,600.00 (G) 7914.894 4.04 1.333 RRLSL MOIST 0-<1/2" SUR 0.5 0.20 23,500. p 2,230.00 p 104.00 p 5473 1 COTTON Apr-14 1 217,000.00 (G) 15,390.071 Total Gallons/Ac: 15,390.07 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.021 0.010 0.119 0.622 0.083 0.004 0.026 0.052 0.026 2.655 58.60 28 Cumulative lbs/acre 0.033 0.018 0.424 1.628 0.453 0.009 0.218 0.158 0.035 6.360 1 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop, .., ,..v � v- .. FD Cumulative Pollutant Loading Rate Limit (Ibs/acre) 36.6 34.8 . ` - L 1339.0 267.9 15.0 375.0 89.0 2500.0 RRLSL = ROANOKE RAPIDS, NC LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Lijection/Incorporation 1.0 Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 G4PIRCdtJPdE J't'AL �� aDLbC-I_S; aPdrt January 21, 2014 Edward Stephens Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: RRSD Dear Edward Stephens: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httn://ivww.settek.com Order No.: 14010508 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 5 Page 1 of 6 Summit Environmental Technologies, Inc. Workorder 3310 Win St. Sample Summary P tdVlFtOtdPe7EtJi;AL,tg l Py l�1 izsjriG. Cuyahoga Falls, Ohio 44223 rlre�iti,:i'1,f5prpvr{� TEL: (330) 253-8211 FAX." (330) 253-4489 WO#: 14010508 Website: htln://www.settek.com 21-Jan-14 CLIENT: Synagro Project: RRSD Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14010508-001 RRSD 1/7/2014 2:30:00 PM 1/10/2014 9:52:00 AM Sludge Page 2 of 5 Page 2 of 6 Summit Environmental Technologies, hrc. WO#: 14010508 3310 Win St. r 'rt;i9lI�0Y1h9PN't'�L"�`��9�6~dR]k�C�t�7c�'p�Pd� �aho Ct a Falls, Ohio 44223 0 g Date Reported: 1/21/2014 fina;ytt L:�tiaxalcr/ TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: httn://wwiv.settek.coni Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: RRSD TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD 001 1/7/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 1/16/2014 VVK RRSD 001 1/7/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/16/2014 VVK TCLP Mercury Analysis (1311/7470) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD 001 1/7/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 b.20 1/16/2014 ALJ SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD 001 1/7/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 1/17/2014 JBN RRSD 001 1/7/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 1/17/2014 JBN RRSD 001 1/7/2014 Endrin 0.0020 ND mg/L Sludge EPA 8081 B 1 0.020 1/17/2014 JBN RRSD 001 1/7/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 1/17/2014 JBN RRSD 001 1/7/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/17/2014 JBN RRSD 001 1/7/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/17/2014 JBN RRSD 001 1/7/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 1/17/2014 JBN VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD 001 1/7/2014 1,1-Dichloroethene 0.10 ND mg/L RRSD 001 1/7/2014 1,2-Dichloroethane 0.10 ND mg/L RRSD 001 1/7/2014 Benzene 0.10 ND mg/L RRSD 001 1/7/2014 Carbon tetrachloride 0.10 ND mg/L RRSD 001 1/7/2014 Chlorobenzene 0.10 ND mg/L RRSD 001 1/7/2014 Chloroform 0.10 ND mg/L RRSD 001 1/7/2014 Tetrachloroethene 0.10 ND mg/L RRSD 001 1/7/2014 Trichloroethene 0.10 ND mg/L RRSD 001 1/7/2014 Vinyl chloride 0.20 ND mg/L RRSD 001 1/7/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 Sludge EPA 8260 B 1 0.70 1/16/2014 MES 0.50 1/16/2014 MES 0.50 1/16/2014 MES 0.50 1/16/2014 MES 100 1/16/2014 MES 6.0 1/16/2014 MES 0.70 1/16/2014 MES 0.50 1/16/2014 MES 0.20 1/16/2014 MES 200 1/16/2014 MES P 3 off56 Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14010508 tb4tInOFIFatEN1'�LlE9q$C?ld'GteS5Pt4 Cuyahoga Falls, Ohio44223 Date Reported: 1/21/2014 ' lirr�;it+rsl l 17`�arsld le TEL: (330) 253-8211 FAX. (330) 253-4489 Company: Synagro Website: htto://www.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: RRSD SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD 001 1/7/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 1/17/2014 AKE RRSD 001 1/7/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 1/17/2014 AKE RRSD 001 1/7/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 1/17/2014 AKE RRSD 001 1/7/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/17/2014 AKE RRSD 001 1/7/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 1/17/2014 AKE RRSD 001 1/7/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 1/17/2014 AKE butadiene RRSD 001 1/7/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/17/2014 AKE RRSD 001 1/7/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 1/17/2014 AKE RRSD 001 1/7/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 1/17/2014 AKE RRSD 001 1/7/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 1/17/2014 AKE RRSD 001 1/7/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 1/17/2014 AKE SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst RRSD _ 001 1/7/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 1/20/2014 AMZ RRSD 001 1/7/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 1/20/2014 AMZ Summit Environmental Technologies, Inc. WO#: 14010508 ffi-,"Sump"'IT 3310 Win St. fISVIR©PI PIE P.1L YE��pCd[�1 �G:, 9ptC Cuyahoga Falls, Ohio 44223 Date Reported: 1/21/2014 Anafritical taia`arat�ir%€ TEL: (330) 253-8211 FAX (330) 253-4489 Company: Synagro Website: htto:/Ammsettek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/10/2014 Project#: RRSD Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst RRSD 001 1/7/2014 Flashpoint (140°F) >140 °F Sludge EPA 1010 1 1/13/2014 TAH RRSD 001 1/7/2014 Cyanide, Reactive ND ppm Sludge EPA 9014 1 0.50 1/10/2014 TIR RRSD 001 1/7/2014 pH 12 s.u. Sludge EPA 9045 D 1 1/13/2014 AYS RRSD 001 1/7/2014 Sulfide, Reactive, ND ppm Sludge EPA 9034 1 25 1/10/2014 TIR P5 (056 0 0 Summit Environmental Technologies, Inc. 3310 win Street Cuyahoga Falls. Ohio 44223 Tel: 330.2i3.821 l Fax: 330.253.4189 Analysis Request/Chain of Custody pose Summit Environmental ironmental Technologies. Inc. use onh Page�_of � SI=1' No. Compan> Name Wl asc Print) Project Name Analytical Parameters and Methods e QSo Company Address Project Address v - a ` C a Client Phone No. • , Report to Client Fac No. Please Fax Results ✓ ❑ POtt_ u n G y Client Email Please lamail Results ✓ Quote No. Gam/ 41v^r1c v" / , < x .r o — Contact Persons e Sampled hq r Check if Ohio VA samples ✓ ❑ a o y — v Y E �$ Sample Identification Date lime Collected Collected �. Z i V. _ "<. - ® ®■®®M®■■■■■■■Rush ■■ am WARWEA "I .., ®® Requested By: MU't be appro%ed Date I'N lab 111aw1g,7f i` FG1VIRbtgiENI'ALTfK.'1#1'd4L_t GiES,iNC. A,.rTJI ' ' 9P''C1d`€1iAt'1�5'11 July 23, 2014 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 Dear Will Varner: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX. (330) 253-4489 Website: htty.-Apivw.settek.com Order No.: 14071316 Summit Environmental Technologies, Inc. received 1 sample(s) on 7/15/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A21-A 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-014-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 4 Page 1 of 6 Summit Environmental Technologies, bac. 3310 Win St. ; 66VIRQ$JPe1f 119'ieLTJ C#tC�'K2Li7'GaE-11�li VC. Cuyahoga Falls, Ohio 44223 r�rr�ti,tivaf Lrt�tealoC�eS TEL: (330) 253-8211 FAX.- (330) 253-4489 W Website: http:/Avww.settek.Cont CLIENT: Synagro Project: RRSD Lab SampleID Client Sample ID 14071316-001 RRSD Tag No Date Collected 7/10/2014 2:00:00 PM Workorder Sample Summary WO#: 14071316 23-Jul-14 Date Received 7/15/2014 10:15:00 AM Matrix Sludge Page 2 of 4 Page 2 of 6 aITSummit Environmental Technologies, Inc. Case Narrative 3310 Win St. &P�JIRt]#JP�IERJPtILTf tpC36l�'�18s,-1KC. Cuyahoga Falls, Ohio44223 WO#: 14071316 lreaP�'tiraiC�axt+ri�.=< TEL: (330) 253-8211 FAX. (330) 253-4489 Website: htto:Uwww.settek.com Date: 7/23/2014 CLIENT: Synagro Project: RRSD This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 4 Page 3 of 6 Summit Environmental Technologies, Inc. g WO#: 14071316 t- _ � 3310 Win St. a Falls, Ohio 44223aho Date Reported: 7/23/2014 'E=f•&VIRQNI9Eh1YQ,LY,��tdK�Lt�d37F5,.aC�C Cz ry S t#r,'lytlfl rl TEL: (330) 253-8211 FAX.• (330) 253-4489 Company: Synagro Wehsite: http.,Mvww.settek.con? Address: 284 Boger Rd. Mocksville NC 27028 Received: 7/15/2014 Project#: RRSD Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst RRSD 001 7/10/2014 Total PCBs ND mg/Kg Sludge EPA 8082 1 0.20 7/23/2014 AKE Pe4 afF46 SUM IT ENVIRONMENTAL TECHNOLOGIES, INC 3310W1nStreet F'JR.- Ohio 44223 Analysis Request/ Chain of Custody For Summit Env ironniental 'Technologies, Inc. use onk ±■. I� �, �r III II I ! It 111 --- W-110-0 if0hio VAP Samples M M Rush Requested: D.IN t' Rev 12 Dale D7127til Surninit Envtronm&nw -itch"togies. Inc, Canior RocWrA Form S.CPO, 11-p-or UPS4 V,.q A'Wnl-v.r'2Ltl; ivilk- Pea-ldl F.— rarA al N C.0-4, ream 4.fj NIA C-G-r WA Im. , ak'f C4 f-A IR C-. Njo;!Z2.4;* tp— ims 040 2 f:, bQAr �,At "a I'st WOW nffoltis; Sarya rarAko cww-"r 4D daft WTI ^ I Lat*Xgi AW"lh _O C. N VA C.111r 0144"Ws WSM "4 FAOoww E4.)tft. K—4ro *-n I LL .,a,- 14 mwt- we 0 6-, :JeAl , 11.IrA VK. I vo-il -110-1114-1 M% firrrialk r-wo I Ca4bot cj'mltn. - tx2g" a+ ty Gl+X7*;ncFrtr.V--4~iCoft"lTvriam- Ra-j& I ce � ai CD 0') 0 h CD 'M93m rt � . , 1�PFVIi3�iPPdEN'I',AL a€C�.3�34LC:GJP<S,'gP�c; .�rratlicr`c;37 L�i�41'�i�3d1P5 . December 18, 2014 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 Dear Will Varner: Summit Environmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: httg://www.settek.com Order No.: 14120773 Summit Environmental Technologies, Inc. received 1 sample(s) on 12/9/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arizona AZ0788, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho 01100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH200001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 4 f Summit Environmental Technologies, Inc. 3310 Win St. Workorder Sample Summary .1 PSVIRONP4, h'i1iL Cuyahoga Falls, Ohio 44223 r�n�rllttral 1;�Papr'Ad�JFTe TEL: (330) 253-8211 FAX.- (330) 253-4489 WO#: 14120773 Website: http://lvipiv.settek.com 18-Dec-14 CLIENT: Synagro Project: RRSD Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 14120773-001 RRSD 12/2/2014 11:00:00 AM 12/9/2014 11:45:00 AM Solid Page 2 of 4 t Summit Environmental Technologies, Inc. Case Narrative 3310 Win St. If iBJIr QtIP+9i N1AL T£CtgCdr Lt Gs S 9Pt .' CzryahogaFalls, Ohio 44223 WO#: 14120773 Anai�Ft7c J'La axaY t€P5 TEL: (330) 253-8211 FAX: (330) 253-4489 Website: http://wwiv.settek.com Date: 12/18/2014 CLIENT: Synagro Project: RRSD This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J-Flag in the Qualifier Field are values below the Limit of Quantitation (LOQ) but greater than the established Method Detection Limit (MDL). Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. All solid results are reported on a wet weight basis unless indicated as dry weight using the mg/Kg -dry designation. Summit Environmental holds the accreditations/certifications listed below that may or may not pertain to this report. Any comments or problems with the analytical events associated with this report are noted below. Original Page 3 of 4 Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. FNIFIRC36ltAEAJTAL`I'8C€$ldr L �1 a, WC Cuyahoga Falls, Ohio 44223 ratytiCalL°al?rii�rl,;r TEL: (330)253-8211 FAX.- (330) 253-4489 Wehsite: http://wwlv.settek.com WO#: 14120773 Date Reported: 12/18/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 12/9/2014 Project#: RRSD Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst RRSD 001 12/2/2014 Total PCBs ND mg/Kg Solid EPA 8082 1 0.033 12/18/2014 AKE Page 4 of 4 Summit -Environmental T&hnojbgies,,Inc: M—M-In Anglysis Request/Ch-ain of -Custody aj 3310AVin'Strect ro. SUnIn-fjt,Eqvjronrn . cn(dTcchnolokie-v0Rc.'u-w Only , 'Cuyahoga Falls. Ohio 1,4223.' Tel: 330.253'.8211 Fac 330.253-4484 paw—uf_- SU Na C - ompany Name. (Plaw Print) p(Oj AnoyflealParmnefers'and MetbOds Pvjjeet Address L; Cliry PhOSIL No Rcp.rt tg Fo# 1.2 Tainnl EMA QUOIC Nm r—' .3 a -1. A Za Sam by Checkrif Ohio VAP samples , 4 1 Dole IMa # -Sample Ide6firkation I collected, E 01, (5 M z Rev. 12 Date: 07/27113 Summit Environmental Technologies, Inc. Cooler Receipt Form Initials Of person inspecting tooter and samples: Client: Order Number. Date Re — { cenred:� T4Te RCCEIYEd: L l i, pall CpOIB;Csj opened and Samp'r,.5 i715peCtq:_. Numbers &Coolel-exes: 1 WA ShipperUPS DHL 'Airborne US postal Waik•in Pickup Olhcr Packaging: Peanuts •bble ' Paper Foam None other._ Tape 6 cooler ox: / Y } N WA (� Custody Seals Intad N NIA C-O-C in plastic N WA Ice— 13luo ice present I a4ont f malted NIR Sample Temperature IR Gun *1 0a59 Cp -C _ C N!A Radiplogleal Testing Instnfinent serial #351 Y N (see page 2 far scan resuns) A "Uses, sheet persarnPIN for RattiologlealTftting,lFsampielsH0T,theRadiolagicatSafaty immediately. rcormtr3tbenntiEed C-O-C filled cut properly Y N Samples in separate bags Y NIA N WA Sample cantalaers intact` Y ' N NrA -if no, list broken samwe(s): i Sample 10ha1,$) complete (Ib, data, etc.) N NIA Latwl(s) agree with C-G-C N WA Corroct containers used N SufliClcotsample received WA N NIA Bubbles absent from ap MLvials" Y N —Sampler. WAh bubbles -5mrn are acceptable. fndleate bubbla size if >6mm. Was client contxted about samples Y N Will dent send new samples Y N Client contact - Logged in GIQCSHARED0ocimentCo*olTempiates-TraWdng\CooSerreceipt formRev,12g7-Z743.doc Page laf2 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989 WWTP Name: Roanoke Rapids Sanitary District WWTP NPDES Number: NCO024201 Monitoring Period: From 01/01/14 To 03/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to alternative nerfnrmed (rinsc A nr Claw R) rmmnlete the Winwinu mnnitorinu data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units deuces Analysis Fecal 2x10 to the 6 th MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. I Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met ".(Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Brown, PF, Chief Executive Officer Tame and itl or print) of Prenare Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defi4d in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) DIGESTER VSR & 1 MGT FECAL ANALYSIS TR. PRIM; %VS�%VSf DIG. VS DIG. #2 2 D QTR. PR M� DIG. VSR % DIG. #2 DATE DATE P D F % FEC. CT. DATE P D F ...._.. 6/-.VS - FEC. CT. 1/28114 JP BW JP BW HH JP JP 791 i -43I 60 59.4 1344 412/14 4123114 DM Bw DM DM 79 53 70 36.6 26719 60.1 5000 20000 BW Bw SE 64 6748 53 2598 1648 2128 364 364 596 Bw HH 78 80 67 40 42.7 83.3 5/8114 5120/14 SE BW SE Bw 54.5 33.2 65.5 65.2 64.1. < 2111114 2118114 HH JP 9323 1220 Bw DM 59 72 49 47 JP Bw 751 661 59 56 52.3 34.4 6/27/14 -6/2/14 6/12/14 DM HH DM HH < <' 2/26/14 315114 BW DM BW DM 2706 1875 HH TS 71 65 46 46 DM 72 62167.9 TS TS G.M. j j 2958.79 G.M. j j j 1525.476 MIN. 1 65 40 34.41 344 MIN. 1 j ( 591 46133.21 364 MAX. 1 80 67 83.31 20000 MAX. 1 1 791 531 701 26719 AVER. 1 173.6 63.9 55.7 5781.14 AVER. 1I 68.11 8.9 54.2 4916.714 3RD. QTR. PRIMA DIG. %VS VSR! % i DIG. #2 FEC. CT. 4TH. QTR. PRIM DIG. %VSI%VS VSRi j DIG. #2 FEC. CT. DATE P D F %VS DATE P ID IF % 7/2114 HH JP Bw HH JP HH JP 69 71 52151.31 <j455 - 3125 10/1114 10/9/14 10/15/14 JP JP JP 72 71 78 85 45 46 168,1 65.2 <1481 < < 7/10114 7/17114 46 46 65.2 59.9 < BW TS Bw TS -- Bw TS - 11021 410 BW DM BW DM 68 66 1042 417 45 46 76.9 84.9 7/24/14 7/29/14 -_ DM HH 51 53 ._.........--.. 46.3 46.9 < - - 10/23/14 10/29114 1115/14 11/13/14 - SE JP - SE JP SE JP 432 410 HH Bw DM HH Bw DM 68 70 66 556 642 75 78 47 49 70.4 72.9 8112/14 8/21114 Bw DM 51 51 65.3 46.4 < SE DM SE DM SE DM 520 1819 455 72 52 57.8 G.M. 720.038 G.M. j I 616.2013 MIN. 1 66 46 46.31 417 MIN. 711 45 57.8j 410 MAX. j j 71 53 65.21 3125 MAX. 1 851 52 84.9j 1819 AVER. j 68.3 50 53 956 AVER. 75.9 47.1 70.9 727.5714 % VSR CALCULATION: PRIM. %VS--DIG.%VS X 100 MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100) DIG. #2 FECAL MUST BE BELOW 2,000,000 7 SAMPLES (MINIMUM) REQUIRED PER QUARTER PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQ0001989 Jan 2014 NPDES NO. NC0024201 PSRP PSRP PSRP PSRP PSRP RP PSRP PSRP PSRP PSRP PSRP PSRP (PSRP PSRP l PSRP ; PSRP_PSRO PSRP PSRP IPSRPI PSRP PSRP PSRP I PRE TEMP ADJ. I LBS. 2 TEMP ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 1 24 HR 24 HR t I TIME DATEMN GALS. LIME C PRE N 'LIME HOUR C 2 HR N HOUR C 24HR PH SAMPLE REMOVAL N OF OF DATE PH PH T USED PH PH T PH PH TIME NO. DATE T REM REM1/l/14 13250 6.78 25.1 6.78 BW 1200 12.46 26.5 12.5 BW 12.51 22.6 12.44 3:49PM 277 1 t9:50AM 1/2114 BW 3:50PM 1/2/14 1/2/14 6500 6.82 28.1 16.91 BW 600 12.29 25 12.29 BW 12.32 16.4 12.07 2:29PM ; 280 1/3/14 BW 2:35PM ! 1/3/14 113114 6.86 17.5 6.64 HH NOT ENOUGH TO I MIX 1/4/14 12750 6.86 17.5 6.64 HH 1800 12.35 23 12.29 HH 12.75 19.8 12.6 2:42PM 288 115/14 HH 2:50PM 1/5/14 1 HH 115/14 ' 6.75 24.7 6.74 HH NOT iENOUGH TO MIX 116/14 13500 6.75 24.7 6.74 HH 2400 12.6 23.5 12.55 DM 12.38 1 18.4 12.19 1:18PM 294 DM 1:OOPM 1l7/14 DM 1:20PM 117/14 DM 1l7114 NOT ENOUGH TO MIX 1/8/14 12000 6.57 28.6 6.68 DM 1800 12.43 22.1 12.34 DM 12.14 17.2 11.9 10:43AM 301 DM 10:OOAM 1/9114 DM ' 10:45AM 1/9/14 DM 1/9114 6.57 28.6 6.68"DM NOT ENOUGH TO MIX I 1110113 13000 6.57 286 6.68 12.09 22 12 JP 1 12.4 21.51 12.3 11:59AM 308 JP 11:38AM ' 1/11/14 JP 12:05PM' 1/11/14 JP 1111/14 12000 6.77 28.6 6.87 12.2 , 26.9 ! 12.26 JP 12.36 23.2 12.3 4:45PM 314 JP 2:40PM 1/12/14 JP 4:50PM 1/12/14! JP 1/12/14 6.81 28.6 6.9 NOT ENOUGH TO MIX 1/13/14 6.81 28.6 6.9 , NOT ENOUGH TO MIX 1/14114 6.81 28.6 6.9 JP NOT ENOUGH TO MIX 1115114 12750 6.81 28.6 6.9 JP 2100 12.32 22.2 12.23 SE 12.65 18.8 12.47 1:44PM 329 HH 1:30PM 1/16/14 HH ! 1:58PM 1116/14 HH 1/15114; 13500 6.55 29.9 6.7 HH 1500 12.48 26.4 12.53 HH 12.18 20.5 12.05 3:03PM 330 HH 2:30PM 1/16114 HH 3:08PM 1/16/14 HH 1116114 12000 6.73 27.5 6.81 HH 2100 12.52 22.7 12.45 HH ! 12.6 20.3 1 12.45 1:53PM 1 336 BW 1:45PM 1/17/14 HH 1:55PM 1/17114 BW 1117114 6.77 27.2 6.68 ! BW ' NOT ENOUGH TO MIX i 1118114 12500 6.77 27.2 1 6.68 1 BW 1 2100 12.34 24.3 1 12.33 BW 12.39 20.3 12.26 10AM 342 BW 10AM 1/19/14 BW 10:10AM! 1/19/141 BW 1/19/14 6.8 25.8 6.83 BW NOT ENOUGH TO MIX 1/19/14 11250 6.8 25.8 6.83 BW 1800 12.51 24.6 12.51 BW 12.51 22.2 12.37 1:27PM 348 JP 11:59AM 1/20114 BW 1:30PM 1/20/14 JP 1120/14 6.63 28.6 6.74 JP NOT ENOUGH TO MIX 1121114 12750 6.63 28.6 6.74 ! JP 1500 12.18 24.3 12.17 JP I 12.29 20.8 12.17 1:05PM 355 JP 11:35AM 1/22/14 JP 1:10PM 1/22114 JP 1122114 12000 6.78 25.9 i 6.81 JP 1800 12.4 24.9 12.4 JP I 12.66 19.51 12.5 2:49PM 362 JP 1:15PM 1/23/14 JP 2:55PM 1123/14 JP 1/23114 6.25 1 17.2 6.01 JP NOT JENOUGH ', TO MIX 1 1124114 12000 6.25 17.2 6.01 JP 1500 12.25 20.2 12.1 SE 11.9 1 17.2 11.66 10:51AM' 369 DM 10AM 1/25/14 I TS 10:55AM 1/25/14, DM 1/25/14 11625 1 6.5 27 6.56 1 TS 1800 12.53 23.5 12.49 DM 12.59 20.4 12.46 2:OOPM 373 1 DM 11:45AM 1/26/14 DM 2:05PM 1/26114 DM 1126/141 1 6.58 1 31 6.76 DM NOT IENOUGH TO MIX 1/27114 12500 6.58 31 6.76 DM 1800 12.2 24.9 12.2 BW 12.44 21.7 12.35 1PM 384 BW 11:50AM 1/28/14 BW 1:05PM 1/27/14 BW 1128/14 7250 6.85 29.9 7 BW 900 12.19 19.91 12.04 BW 1 12.14 ' 20.1 11.99 , 11AM 387 BW 10:55AM 1/29/14 BW 11:11AM 1/29/14 BW 1/29114 1 NOT JENOUGH TO I MIX 1130/14 I I I NOT ENOUGH TO MIX 1/31/14 6.74 30.5 6.91 HH NOT ENOUGH TO mix ' I i PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQ0001989 Feb 2014 NPDES NO. NC0024201 PSRP PSRP I PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRPj PSRP PSRPI PSRP PSRP PSRP PSR PSRP PSRP PSRP PSRP PSRP jPSRPj PRE TEMP I ADJ. I LBS. 2 TEMP ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR I TIME DATE I GALS. LIME C PRE N LIME HOUR C 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL I REMOVAL N OF OF N DATE PH PH T USED PH PH T PH PH TIME NO. I T TIME DATE T REM REM T 211/14 12750 6.74 30.5 6.91 HH 1800 12.62 23.9 12.59 HH 12.66 1 20.7 12.53 1:37PM 396 HH 1:30PM 2/2/14 HH 11:48PM 1 212/14 HH 2/2114 10500 6.9 18.4 6.71 HH 1500 12.28 . 25 12.28 HH 12.69 , 21 12.57 4:14PM 406 DM 1120AM 2/3114 HH I 4:20PM 2/3/14 DM 213114 12000 6.71 14.4 1 6.4 TS 1500 12.93 15.8 12.66 JP 12.85 1 15.6 12.57 9:11 PM 1 421 HH 7:50PM 214/14 JP 1 5:55AM 215/14 HH 2/3N4 12000 6.78 32 1 6.99 DM 1500 12.76 21.5 12.66 JP 12.42 18.4 12.23 5:49AM 424 HH 1:50AM 2/5/14 JP 1 5:55AM 2/5114 HH 2/4114 1 12000 7.08 14.1 6.75 JP 1200 12.98 15 12.68 DM 12.58 15.8 12.31 5:26AM 433 HH I 6:OOPM 215/14 DM 15:30AM 2/6/14 HH 215/14 12750 7.18 12.9 6.82 DM 1200 12.59 13.5 12.25 HH 12.93 14 12.6 6:09AM 434 HH 5:45AM 2/6/14 I HH 16:15AM 2/6/14 HH 2/5114 11500 7.15 12.5 6.78 HH 900 12.84 14.4 12.55 DM 12.97 15 12.67 3:56PM 438 DM 2:45PM 2/6/14 DM 4:OOPM 216/14 DM 2/6/14 12750 7.05 14 6.72 DM 1200 12.74 12.9 12.38 HH 12.89 15.1 12.54 5:56AM 441 HH 5:15AM 2!7/14 HH 5:58AM 2/7/14 HH 2/7/14 ; 12250 7.21 1 12.5 6.84 HH 1200 12.75 16.6 12.5 JP 12.79 16.3 12.54 4:22PM 456 1 JP 4:25PM 2/8/14 JP 4:25PM 2/8/14 JP 12500 7.41 21.1 7.02 BW 1200 12.84 15 1 12.54 JP 12.96 14.8 12.66 9:32AM 464 JP 8:25AM 219/14 JP 9:40AM 2/9/14 JP 1218114 2/8/14 12500 6.64 11.7 6.22 JP 1200 13.14 13.4 12.76 BW 13.13 14.4 12.92 7:25PM 468 BW 7:15PM 2/9/14 BW 7:30PM 2J10114 BW 219/14 12250 6.53 13.4 6.22 BW 900 12.98 12A 12.61 JP 12.84 15.1 12.54 1:31PM 480 HH 10:25AM 2/10114 JP 1:35PM 2/10/14 HH 219/14 ! 12250 6.76 12.5 6.39 JP 900 : 12.98 11.7 12.58 BW 13.08 14 12.65 11:31 m 485 BW 11:30PM 2/10114 BW 11:35PM 2110114 BW 2110114 12750 8.35 10.9 7.92 BW 1 1200 12.56 13.5 12.22 HH 12.87 16.2 12.6 4:48PM 494 HH 4:20PM 2/11114 HH 4:55PM 2/11/14, HH 2111/14 11000 6.91 13.9 6.58 HH 900 12.81 16.4 12.56 BW 13.06 15.2 12.76 112:21AM 499 JP 11:30PM 2/11/14 BW 12:30AM 2/12114i JP 2111114 12625 7.92 12.5 7.55 BW 900 12.75 13.9 1 12.42 HH 12.94 16.4 12.66 12:33PM 508 BW 11:45AM 2/12/14 HH 112:40PM 2/12/141 BW 2111/14, 12750 7.32 11.3 6.92 I HH 900 12.9 17.8 ! 12.69 HH 13.35 16.4 13.1 5:17PM 511 BW 1 4:35PM 2112/14 HH 5:20PM 2/12/141 BW 2112114 11750 7.52 11.4 7.12 HH 900 12.89 13.9 12.56 JP 12.77 13.3 12.42 5:37AM 515 JP 5:OOAM 2/13/14 JP 5:40AM 2/13/141 JP 2112114 12500 7.74 10 7.29 JP 1 600 1 12.22 17.3 12 BW 1 11.81 16.6 11.56 1:27PM 521 TS 12:20PM 2/13/14 BW ' 1:37PM 2/13/151 TS 2113114 12000 6.78 1 13.6 6.44 BW 900 12.39 1 12.3 12 JP 11.85 15.2 ! 11.55 5:45AM 526 JP 5:41AM 2114/14 JP 5:45AM 2114/14 JP 2114/14 12250 6.97 12.5 6.6 TS 600 12.6 1 15.1 12.3 JP 11.95 16.1 11.68 12:18AM! 530 DM 12:OOAM 2/15/14 JP 12:20AM' 2/15/14 DM 2/14/14 12000 7.33 11.9 6.94 JP 900 13.04 16 12.77 DM 12.6 13 12.24 9:15PM ' 535 DM 9:OOPM 2115/14 DM 9:20PM 2115/14 DM 2115/14 12250 6.85 15.4 6.57 DM 900 12.86 13 1 12.5 DM 12.89 15.4 12.61 ; 6:50 m 544 BW 4:30PM 2/16/14 DM 6:55PM 2/16114 BW 2/161141 12000 7.54 11 7.12 DM 1 900 12.83 11.5 12.43 DM 13.11 1 12.5 12.74 i 5:38AM 549 DM 5:30AM 2/17/14 DM 5:40AM 2117/14 DM 2/171141 12000 7.17 11.5 6.77 DM ' 900 : 12.96 14 12.63 OM i 12.91 1 14 12.58 9:50PM 557 DM 8:OOPM 2/17/14 DM 9:52PM 2/17114 DM 2117/14' 12500 - - - DM 900 12.93 15 12.63 JP 12.78 1 17.9 12.57 1:57PM 564 JP I 1:30PM 2/18114 JP 2:OOPM 2118114 JP 2118114 13500 7.14 13.5 6.8 JP 900 13.03 14 12.7 DM 12.6 14 12.27 6AM 567 BW I 6:OOAM 2/19/14 DM 6:02AM 2/19/14 BW 2118/14 12500 6.95 14 6.62 DM 900 12.58 15 12.28 BW 12.27 17.31 12.05 9:35PM 579 BW 9:30PM 2/19/14 BW 9:40PM 2/19/14 BW 2119/14 12875 6.61 14.5 6.3 ' JP 900 12.7 14.9 i 12.4 JP 12.46 18.4 12.27 2:48PM 587 JP 2:15PM 2/20/14 JP 2:50PM 2/20/14, JP 2119114 12000 7.56 14.3 7.25 JP 900 12.62 17.4 12A2 BW 12.52 18.5 12.33 10:08PM 593 HH 9:45PM 2120/14 BW 10:10PM 2/20/14 � HH 2120114 12875 7.44 14.5 7.13 BWJ 900 12.82 16.4 12.51 JP 12.71 18.5 12.52 1:07PM , 600 DM 11:20AM 2121/14 JP 6:05PM 2121/14 11 DM 2120114 12000 7.41 13.8 7.08 JP 900 12.83 17.6 12.59 JP 12.68 1 18.5 12.49 6:03PM 605 DM 5:40PM 2121/14 JP ! 6:05PM 2121/14 DM 2121114 11250 7.45 14 7.12 1 JP 600 12.19 17.6 11.97 HH 12.12 1 16.3 11.85 5:49AM 612 HH 2:30AM 1 2/22/14 HH 5:55AM 2/22114 HH 2/21114, 12250 , 7.29 14.8 6.99 HH 600 12.69 17.9 I 12.48 DM 12.24 19 12.06 4:07PM 618 DM 2:20PM 2/22/14 DM 4:10PM 2/22/14 DM 2122114 12500 6.91 16 6.64 DM 600 12.32 16 1 12.05 HH 12.05 16.1 11.78 12:30AM 623 HH 12:10AM 2/23/14 HH 12:35AM 2/23/14 HH 2122/14 11750 6.84 16.7 1 6.59 HH 600 12.71 17 12.47 DM 12.31 16.5 12.06 10:45AM 626 DMI 10:15AM 2/23/14 I DM 10:50AM 2123/14 DM 2122/14 12500 7.07 15.5 1 6.79 DM 600 1 12.55 15.9 12.28 HH 11.91 16.9 11.67 12:22AM 632 HH 10:20PM 2/23/14 I HH 12:28AM 2/24114 HH 2123114 12750 7.17 14.1 6.84 HH 600 1 12.53 17 12.29 DM 12.16 15.4 11.88 J 4:05PM 636 BW 4:OOPM 2/24/14 DM 4:10PM 2124/14 BW 2/24114 13000 6.94 17 6.7 DM 900 1 13.02 1 14.3 12.71 1 8:40AM 641 BW 8:30AM 2/25/14 SE 8:45AM 2/25/141 BW 2/24/14 12500 8.49 14.1 8.16 BW 600 12.41 15.5 1 12.13 HH 12.91 15 112.61 12:07AM 661 DM 10:35PM 2/25/14 HH .12:10AM 2/26l14 DM 2125/14 11750 7.11 13.3 6.77 HH 600 12.93 ! 15 ! 12.63 BW 12.46 17.2 12.22 3:55PM 670 BW 3:55PM 2126/14 BW 4PM 2/26/14 BW 2126114 12750 7.9 13 7.54 BW 600 11.95 14.7 11.65 BW 11.87 19.1 11.69 1:13PM 677 BW I 10:20AM 2/27/14 BW 1:15PM 2/27114 BW 2127/14 12000 6.87 16.6 6.64 1 BW 600 12.76 14 12.43 DM 12.84 13.5 12.5 12:53AM 679 DM 12:OOAM 1 2128114 DM 12:55AM 2128/14 DM 2/28/14 7.25 12.9 6.89 OM NOT ENOUGH TO MIX I I I PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT W00001989 Mar 2014 NPDES NO. NCO024201 PSRP PSRP PSRP PSRP PSRP PSR PSRP PSRP PSRP! PSRP PSRPI PSRP PSRPj PSRP PSRP PSRP PSRP PSRP PSRP PSRP' PSRP ! PSRP PSRP 1 I PRE TEMP ADJ. 1 LBS. 2 TEMP ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR I TIME DATE 1 GALS. LIME C PRE N ' LIME HOUR C 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL REMOVAL' N I OF OF N DATE PH j PH T USED! PH PH T PH PH TIME NO. T TIME DATE T REM REM T 3/1114 7.25 12.9 6.89 DM NOT ENOUGH TO MIX ! ! 312/14 7.25 12.9 6.89 DM NOT ENOUGH TO MIX 3/31141 7.25 12.9 6.89 DM I NOT ENOUGH TO ! MIX 3141141 7.25 12.9 1 6.89 DM NOT ;ENOUGH TO MIX 3/5/141 10000 7.25 12.9 1 6.89 DM 1 900 12.84 17 12.6 DM 12.31 13.4 11.97 3:01PM ! 685 DMI 12:00PM 3/6/14 DM 1:10PM 3/12114 HH 3/6114 ; ! NOT ENOUGH TO MIX 3/7/14 NOT I JENOUGH TO MIX 318/14 13125 1 6.91 22 6.82 JP 1200 12.12 26 12.15 1 JP 12.15 23.3 12.11 4:30PM 700 JP 4:30PM 319114 JP 1:10PM 3/12/14 HH 3/9114 12000 6.68 26.4 6.73 JP 1200 12.13 j 27 12.19 1 JP 11.72 22.7 11.65 1:05PM 708 HH 2:50PM 3/10/14 JP 1:10PM . 3/12/14 HH 3110114 NOT I 'ENOUGH TO MIX 3/11/14! 12750 6.64 28.2 6.73 HH 1500 12.4 25.3 12.42 HH 1 12.49 1 24.1 12.46 1 5705PM 710 HH 3:20PM 3112/14 HH 5:08PM 1 3/12/14 HH 3112/14 I NOT ENOUGH I TO I MIX 3113114 7.11 13 6.75 JP NOT ENOUGH TO MIX ; 3114114 7.11 13 6.75 JP NOT ENOUGH TO MIX 3/15114 13000 7.11 13 6.75 JP 900 12.55 14 12.22 DM 12.73 1 15.5 12.45 5:37AM 726 DM I 4:45AM 3116/14 DM 5:40AM 3/16/14 DM 3/15/141 12000 6.91 24.7 6.91 BW 2400 12.02 1 25.1 12.02 BW 12.04 20.6 11.92 2:38PM 730 BWl 2PM 3116/14 BW 2:40PM 3/16/141 BW 3/16/14 11250 7.85 14 7.52 BW 1200 12.5 1 16.7 12.26 1 BW 12.08 15 11.78 2:28PM I 734 JP j 2:30PM 3117/14 BW 2:40PM 3/17114 JP 3/17114 12250 7.17 13.7 6.86 I JP 900 I 12.7 14 ! 12.37 DM 12.54 1 13.5 12.42 5:21AM 1 744 BW 9:45PM 3/18/14 DM 5:25AM 3/19114 BW 3/18114 6.86 13 6.5 1 DM NOT ENOUGH TO I MIX 3/19/14 12000 6.86 : 13 6.5 DM 900 12.42 18.9 12.24 HH 12.45 1 20.2 12.3 12:18AM 763 HH 5:10PM j 3122114 HH 12:25AM 3/23/14 HH 3/19114 12000 1 6.74 26.2 6.74 JP 11200 12.53 20.6 12.4 HH 11.75 19.4 11.59 12:15AM 761 HH 11:20PM 3/22/14 ! HH 12:25AM 3/23/14 HH 3120/14 12000 6.82 30 6.97 JP 1200 12.59 24.7 12.58 HH 12.41 18 1 12.2 112.17AM 762 HH 9:40PM 3/22/14 HH i 1215AM 3/23/14 HH 3/21/14 NOT ENOUGH ! TO MIX 3122114 6.98 14.4 6.67 HH NOT ENOUGH TO MIX 3123114 12625 6.98 14.4 6.67 HH 900 12.46 16.9 12.22 HH 12.82 16.3 12.57 12:42AM 771 HH 12:20AM 3/24/14 HH 12:50AM13/24/14 HH 3124/14 11250 7.04 15.1 6.74 HH 900 12.43 17 12.18 HH 12.71 15.5 12.43 5:18AM 778 HH 2:45AM 3125/14 HH 5:20AM 3/25114 HH 3/25114 11250 7.16 13.8 6.83 HH :1200 12.99 17 12.75 1 BW : 12.76 17.8 12.55 4:18PM ! 791 BWJ 4PM 3/26/14 BW 4:20PM 3126/141 BW 3/25/14 12000 6.56 24.8 6.56 BW ' 1200 12.45 27.4 12.52 BW 12.58 20.5 12.35 11:36AM' 788 BW 1 11:30AM 3/26/14 BW 11:45AM 3/26/14 ' BW 3/26l141 12750 7.75 14.5 7.41 BW 900 12.68 21.3 12.58 BW 12.29 26.7 12.33 11:39AM 793 BW 11:40AM I 3/27/14 BW HOLD 4/11114 BW 31271141 10500 7.35 27.3 7.42 BW 600 12.76 17.4 12.54 BW 12.05 1 20.9 11.93 ! 11:42AM 809 DM 1:30PM 3/27114 BW HOLD 4/11114 BW 31271141 12750 6.71 23.5 6.67 BW 900 1 11.96 i 19.7 11.87 BW 12.6 1 21.4 12.5 12:26PM 812 DM 11:45AM 3128114 BW I HOLD 4111/14 BW 3128/141 12000 6.53 31.2 6.71 HH 1200 12.54 27.2 12.6 HH 12.32 23.4 12.26 11:36AM 807 DM 1:05PM 3129/14 HH HOLD 4/l1/14 BW 3129114 NOT ENOUGH TO MIX 31301141 NOT I IENOUGH TO MIX 3/31H4 NOT (ENOUGH TO MIX I I ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: W00001989 WWTP Name: Roanoke Rapids Sanitary District WWTP NPDES Number: NCO024201 Monitoring Period: From 04/01/14 To 06/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion Yr - .J:....1.1.. 4.. A n.- Cl... M n nln4n *ha fnllnwina mnni*nrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum' Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6th MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal •• coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0ption/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." R. Danieley Brown,PE Chief Executive Officer Prep e a and Title dpLand Applier Name and Title (if applicable) (type or print) Signatu of Preparer* kate Signature of Land Applier (if applicable) Date *Preparer is defined in 0 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQOOO1989 Apr 2014 NPDES NO. NCO024201 PSRP PSRP PSRP PSRP I PSRP PSRP: PSRPj PSRP PSRP PSRP PSRP( PSRP PSRPj PSRP PSRP PSRP JPSR PSRP PSRP IPSRPI PSRP PSRP PSRP I PRE TEMP ADJ. I LBS. 2 ITEMPI ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR ( I TIME DATE I GALS. LIME C PRE N LIME HOUR I C ' 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL REMOVAL N OF OF N DATE PH PH T USED PH i PH T PH PH TIME NO. T TIME DATE ! T t REM REM T 4/1114 NOT I ENOUGH TO MIX 412114 NOT ENOUGH TO ? MIX 413114 NOT ENOUGH TO MIX 4/4114 NOT (ENOUGH TO MIX 4/5114 NOT :ENOUGH TO MIX 4/6/141 NOT 'ENOUGH TO MIX 4/7/14 NOT ENOUGH TO MIX 4/8/14 NOT ENOUGH TO MIX 419114 NOT ENOUGH TO MIX 4/10/14' NOT ENOUGH TO MIX 4/11/14 NOT ENOUGH TO MIX 4112/14 NOT I ENOUGH TO MIX 4/13114 NOT 'ENOUGH TO MIX 4/14/14 12000 6.49 30.6 6.64 JP 12DOI 11.92 30.5 12.07 JP 12.1 24.7 12.05 2:30 m 832 JP 1PM 4/15/14 JP 2:40PM 4/15114 JP 4/14/14 12750 1 6.92 18.8 6.74 JP 1200' 12.81 20.4 1 12.68 JP 12.58 21.7 12.48 5:21PM 833 JP 5:20PM 4/15/14 JP 5:25PM , 4/15114 JP 4/15/14 12000 7.32 18.6 7.13 JP 600 12.84 20.5 12.71 DM 12.38 19.9 12.23 6:31PM 838 JP 1:OOAM 4/16/14 DM 6:35PM 4/16114 JP 4116/14 12000 6.62 18.5 6.43 DM 900 12.72 19.7 12.57 JP 12.42 19.7 12.27 6:05PM 837 JP 6:15PM 4/16114 I JP 6:15PM 4/16/141 JP 4J16114 NOT ENOUGH TO MIX 4/17/14 6.83 ! 16.5 6.61 JP NOT ENOUGH TO I MIX 4118/141 12750 6.83 16.5 6.61 JP 600 12.62 1 18 12.41 DM 12.43 17.4 12.21 4:23PM 851 DM 4:15PM 4119/14 I DM 14:28PM 4/19/14 DM 4/19114 12500 6.74 16.5 6.49 DM 600 12.4 16 12.13 DM 12.29 16.8 12.05 1153AM 858 DMI 11:10AM 4120114 DM 111:55AM 4/20/14 DM 4/19114 12750 7.00 15.9 6.73 DM 900 12.51 15.7 ! 12.23 HH 12.5 18.5 12.31 7:33PM 863 1 HH 7:20PM 4/20/14 HH 17:35PM 4/20/14 HH 4/20114 12000 7.54 15.4 7.26 HH 900 12.49 18.5 1 12.3 DM 12.17 18.4 11.96 1:36PM 868 TS I 1:00PM 4/21/14 DM 1 1:40PM 4/21/14 BW 4/20/14; 13500 6.95 16.4 6.7 DM 900 12.85 17 ! 12.61 HH 12.28 19.5 12.12 Al PM 874 HH : 7:25PM 4/21/14 HH 7:45PM 4/21/14 HH 4/21114 12750 1 7.71 16.6 7.46 1HH 900 12.42 19.7 12.27 TS 12b5 20 12.4 1:40PM 880 TS 1:30PM 4/22/14 TS 1:46PM 4/22/14 TS 4/22/14 12750 7.04 16.7 6.8 TS 900 12.35 16.8 12.11 HH 12.5 19.3 12.32 3:35AM 884 DM 12:20AM 4/23/14 HH 3:40AM 4/23/14 DM 4/22H4 12750 7.24 17 7 HH 900 12.61 19 12.43 TS 12.35 1 20.3 12.2 2:06 m 887 TS 1 1:45PM 4/23114 TS 2:10PM 4/23114 TS 4/23/14 13000 7.09 20.4 6.96 BW 900 1224 ! 21.8 12.25 BW 12.45 1 21.8 12.36 1 4:11PM 897 BW I 4PM 4/24/14 BW I 4:15PM 4124/141 BW 4124114 12750 6.57 17.4 6.35 DM 900 12.5 19.1 12.32 T TS 1229 19.8 1 12.14 10:09AM 904 TS 10AM 1 4/25/14 TS 10:15AM 4/25114 TS 4124114 13000 6.97 20.4 6.82 TS 900 12.71 18.3 12.5 DM 12.61 20.2 12.46 11:52PM; 909 JP 11:30PM 4/25/14 DM 111:58PM 4/25/141 JP 4125/141 12000 6.81 16.6 6.56 DM 900 12.5 18.9 i 12.32 TS ' 12.57 21.4 1 12.47 1:33PM I 913 HH 9AM 4/26/14 TS 1:40PM 4/26/14 HH 4/25fl4l 10500 6.79 18.5 6.6 TS 900 12.51 19.2 12.33 JP 12.39 21.1 12.28 11:58PM 917 JP 11:55PM 4/26/14 JP 12:OOAM 1 4127/14 , JP 4126M4i 6.55 19.5 6.39 HH NOT ENOUGH TO MIX 4/27114 13125 6.55 19.5 6.39 HH 900 12.4 19.2 12.22 HH 12.17 20 12.02 8:50AM 930 SE 5:10AM 4/28/14 JP 8:55AM 4/28/14 SE 41271141 13000 7.01 1 17.9 6.8 HH 900 12.51 19.5 12.35 HH 12.33 18 12.33 2:40PM 933 - DM : 2:25PM 4/28/14 HH 2:45PM 4/28/14 DM 4/28/141 13125 6.61 21.5 6.51 HH 900 12.62 18.9 12.44 1 JP 12.3 1 18.8 12.12 1 5:43AM 939 JP ! 5:40AM 4129114 JP 5:45AM 4/49/14 JP 4/28/14; 12000 6.79 17 6.55 SE 900 12.62 18.5 1 12.43 1 TS 12.46 18.9 12.28 2:19PM 9" DM 2PM 4/29/14 TS 2:25PM 4/29/14 DM 4/29/141 12750 1 6.67 17.4 6.45 DM 900 12.46 18.1 12.25 1 TS 12.49 21.2 12.37 1:10PM 1 953 TS 12:15PM 4/30/14 TS 1:15PM 4/30114 TS 4/29114 12750 6.85 16.7 6.61 TS 900 12.42 18.8 12.24 HH 1 12.29 19.6 12.13 10:OOPM 956 HH 8:1OPM 4/30/14 HH I10:05PM 4/30/14 HH 4130/14 12750 6.87 17.7 6.65 HH 900 12.56 19.2 12.38 TS 12.23 20.8 12.11 1:30PM 959 TS 10:45AM 5/l/2014 TS I 1:36PM 5/1/14 TS 4130114 13000 6.87 19.2 6.69 SE 900 12.44 20 12.29 DM 12.53 21.1 12.41 6:29PM 961 DM 6:10PM 5/1/14 DM 6:35PM 5/1/14 DM � I -zr- aa3m=maaNmmoo°-smog==o=►N-�o��a==oo ooa a a w v v v v v v •t a v v v a v v v v v v v v a yr v a v v v v v T v v ai Q0 W M`v(n (O�r ��._r-a�`v (r_p (r�p��a`rOO 0��af0h mrn .ram a 0 in in rn to ln��N(n�NNN�N47 5U711�()t�l1�O�O�N N(AN (O m i m Z i i i i i i E CL ~OCO WO OOp Cn � Ow ONO tnN (n O(o OOOONS�ONO(an OHO �Nl70rNN uai(ap o Ln(an0 NNrN. LO(ap O -OMr LO M N N N N O ONO O O O r W O a V a M r m r 6 Ct) CO r V N� .r- N n N � 1� IQ N- r r t.0 r N cd (ri y r (V N M 6 v CL 0 z- aa3ma3=()w3a.aaa3x2xv>x3w xxxxxgo a -,mx 0 --»-)mxo=F-z 0U)a oo� - 0- j w N =OQO)o�C�M0)NCO 4(A1� oONM IL 920 O (A(n(ptp (nN�h(p (n N uO rn N(n (nNNCn��h to to Lf)uu))N V)) W)LOUs (ZO g g g g IL tY Q 0 a H =>w vO� SM�O�OV,S o�a�aaoaaaaaaaa(,aa,a(,o„a�d N(h (`) SONV avOrC'?rv)OMMM aaaaNax_aaa_xa NOr S� MM (O CD -0 a N W F C+)N h a N V V'a)cOeq i.:(p��NpiC�� r6DNMNN ri�iri cri LL ( _z� aa3cngaaw33��a3��xx�xwcn�wv�axx�� irna a m a--- -»mF- ��mmoo-�mooxxoxrnF-o(nF-�xxoo OF-� - -- S w J aO m �t- M nC� m rl. (n t0rnm t` r r(pMN(phNOhNO r'NMM V tp (p (D t`M - m (N NtOQ C) m m m�00rN ao (p m C7 t, NMMv e� M a �Qz mmmmmm rrr _] O a W a g a a a _ g a a N M 2 2 M 2 2 2 2 i E z Z to vat F ;7M�o (�� (.MOM `t�co Cn NM�NN NOstNO VNiNOU rO NQO P Q .zr a N MN dCl� Nn 66 i Or �Nn'-'-t+t`Ns��.-.- W --NW in -It rCOY -t O V = x X CO') tNfi. a V a N V (00 M W M NQ, M M M N •t 7 N N f0 M" f'7 Cep-sN� M Y VN' S N w V) v a N N N N N N N N N N r r N N N N N N N N N N r N N N N N N N r N N z N a N r r r r r r r r r r r r r Oo a - 0r-NCRan --- - clgr�r - a a f W (Oh"t U,t0(hmCRcq(p000CA't00 -- oomv Co Q dr Cn a � Ci N O N N N fA r O N .- N N N V' N ii M N N N N 0 N v N a N to N V N N N N N r N (� N m N (� N 1, N (O N w N m N CD N U1 N N h N �t N N (� N ¢Y F z 1-Z �"' ' - N (A O(q Nao Cp NN(�i,M Cp rnNor i9 0 a � NNmNMap�f`N((�pNM(�m Lq at fD 0000 (OM V; MMM Mst cl V CO MM,a r M (D Qa a' d N OS O a O�(O F- N N CV N N 4 N N N N N T N N N N N N N N N r N N N N N N DMMMZ)N O N N O N = r r r r r r r r r r r r r r r r .- r z r z w w -z� aam�=m=►�-Q))m norm- a >� 3 vai noaa��m=o=0E-1: 0aixxm0 zY w a az > z Q IL a' _ 0 m 'Q OD `d N � M (C) c) CM N N r wm (O "t (p M w0 N O mmr N f` - m T O M� Nmt- M M a f`r r v N M o N Y N mW M ~ Cq a0 m Ve Y O Q QNCV fV NNNNNN(V NNNNNN(V CV NNNNCV NNNNNNNZ�NNN .11011 O� O ° Na wr V W r N CDmm N P.: r O NNCMN (q V' N M M N V'M ry m V'N N er r W O v M W r MM r N v r (n(t)C� (n CO 0 N N pi M rA r r` IL a' N W N N r r N N N N N N CV N Cy N N N N N N N N r N NNM N N N N N N N N NIL a O= ~� �(pMNnCA m m t` NMMNMMNmtl •tMr V; C t`(/'(D �(D a (1') t�N V r- �MMN�(pit N 00UV MN=fl n(p CO(n ZNN�NNNN NNfV N(V NNN(V NNNNNNNNNNNNNN(VN r rr 0 0 0rcc: 0 IL wQ W o o o o o 0 o 0 o o 0 0 o 0 0 0 0 o 0 o 0 0 0 0 0MmmmmmmmNmmmNNNNC()(n oo0000000000 o O o o 0 0S 0 000 0 (1)N to (p tp tp (p Cp CONK N zV� m = =w000aaaa3xmxmn(n(�n3xaNxN 2rh 2orf� xrm=aa CO CO mx0xaF-F-F-m0x-)x000=xx a m I,MVOmOVNpDOr mr mm 00 co co Mr O MmN(oa 'ITW MNp 00oOMNaOM'W= gM aaa o.��d ram oori dO ri(cr �ood ti t.Zc�co(d(6(dmm(o M NO COm(pr(pCpp(p CpNM m o r OOOp rn r(p Cp tO 0 IQ M2mxmm aa N Nm NM VOOOONVM N N N NNN NrN N N r N FjN N NN N N W Vr 1h; N1ONOmm C ( O m rn hmaaO. mNmOmcmrmmW M (onr.-r-t-r-0000ro�r�6 t;r.-t;of�r,:0w d (--r6 �v a (p0Sgg00000o(o0oog0000C) NO Cn Lon08U)WOrl 00(p 00(C)o(n 00 0000 000 0 Q �.. a M0000 N N N N r` t- N N t` N O r� N N N N 0 N M N 00gorInrl N N 0 r.-0O O(A NN r\ N r.OhhO N O(p(p0 N N N Cl) O C) N (Np rp O 0p N r r r rrrr rr r r r r r r r r r r r rr r r r r r r r r r r r r v v v v a v t� v T a T v v r= v v v a v v v v v v v v v v v v a v v i, z� Q r TaM�a_- T T r r ! r T T T r 1 -aC-C--(C (pr�t��mpGraMa(t (�{Ot�00�Cr OmN a O uZ N (C t�f C•-�T� �'� a-tr TNNNNNN�V NN N NNMM (( (C (CSC (p Y) PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT W00001989 Jun 2014 NPDES NO. NCO024201 PSRP, PSRP PSRP PSRP PSRP PSRP PSRPI PSRP PSRP PSRP I PSRP PSRP IPSRPI PSRP PSRP PSRP lPSRP PSRP PSRP PSRPI PSRP PRE TEMP ADJ. 1 LBS. 2 TEMP AIH 1 24 TEMP ADJ. 24HR 1 24HR 1 24 HR 24 HR I I TIME GALS. ! LIME C PRE N LIME HOUR C 2 N HOUR C 24HR PH SAMPLEI N REMOVAL REMOVAL N OF WREMT DATE PH PH T USED PH PH T PH PH TIME NO. T TIME DATE T REM 611114 ! NOT ENOUGH TO I M0( 6/2/141 NOT ENOUGH TO MO( I 6/3114 NOT ENOUGH TO MIX 6/4114 NOT ENOUGH TO MIX 6/5114 NOT ENOUGH TO MIX 6/6/141 NOT ENOUGH TO 6i7114 12750 6.93 23.9 6.87 SE 1500 12.45 23.7 12.42 BW 1 12.33 249:05AM 174 BW 9AM 6/8/14 BW 9:10AM 6/8/14 Bw 6/8/14 12250 6.97 23.2 6.91 BW 1200 12.33 23 12.27 SE 12.27 24.57:09AM 181 DM 7AM 6/9/14 SE 7:10AM 16/9/14 DM 619l14 12000 7.05 22.7 6.98 BW 1200 12.43 24 12.4 DM 1999. 264:56AM g122 187 DM 1:45AM 1 6/10114 DM 12:20PM 6l10/14 JP 6/10114 12000 6.95 22.5 6.88 DM 1200 12.4 I 24 12.37 DM 12.02 26.75:41AM 191 1 BW ! 5:15AM 6l11/14 DM 4:40PM 6/13/14 SE 6111114 12500 6.66 26.1 6.69 I BW 1206 12.21 24.6 122 BW 12.21 26.97:50PM 1 206 BW 7:50PM 6/12114 BW 4:40PM 6l13l14 SE 6/12/14 12750 6.81 23.5 6.77 BW 1200 12.17 25.3 12.18 BW 11.66 26.8 11.77 6:27PM 210 SE 6:15PM 6/13/14 TS 6:30PM 6/13/14 SE 6H3/14 13125 7.39 23.8 7.36 BW 1200 12.18 24.6 12.18 SE 11.79 28.5 11.9 6/14114 12750 6.96 22.3 6.85 HH 1200 12.24 23.9 1221 HH 1221 22.9 i 12.15 223 HH 5:05AM 6/15/14 HH 5:33AM 6/15/14 HH 6115114 12750 6.96 22.3 6.89 HH 1200 12.13 24.1 12.1 HH 12.12 25 12.12 t5:25AM 231 HH 12:20AM 6/16/14 HH 12:35AM 6/16/14 HH 6/15114 12000 7.36 23 7.3 HH 1200 12.46 26.5 12.51 DM 12.21 27.7 12.3 237 BW 5:OOPM 6/16/14 DM 15:05PM 6/16/14 BW 6116114 12250 6.85 24.5 6.84 DM 1200 12.2 26.5 12.25 TS 12.1 28.4 12.19 243 TS 12:45PM 6/17/14 TS 1:20PM 6117/14 TS 6117114 12500 7.07 23.8 7.04 I TS 1200 12.2 1 25.8 12.23 ! TS 12.15 1 28.5 12.26 11:02AM 248 1 TS 9AM 6/18114 TS 11:10AM 6/18/141 BW 6118114 10500 7.33 25.3 7.33 TS 1500 12.46 1 27.4 12.52 TS 12.4 1 27.9 12.49 10:51AM 251 1 TS 9:30AM 6/19/14 1 TS 10:58AM 6/19/14 TS 6119114 6.76 27.1 6.82 DM NOT ENOUGH TO MIX 6120/14' 12500 6.76 27.1 6.82 DM 1200 12.09 26.5 12.14 HH 11.81 1 26.9 11.87 i 6713PM 262 HH 2:10PM 6/21/14 HH 6:15PM 6/21/141 HH 6121114 7.31 25.5 7.33 HH NOT ENOUGH TO MIX 6122114 7.31 i 25.5 7.33 HH I NOT JENOUGH TO I I MIX 6123114 7.31 25.5 7.33 HH NOT JENOUGH TO MIX 6/24/14 7.31 25.5 7.33 HH NOT !ENOUGH TO MIX I 6/25114! 10000 7.31 25.5 7.33 HH 1200 12.14 30 12.29 DM 11.95 1 30 12.1 1:32PM 270 TS 1:00PM 6/26/14 DM 1:35PM 6/26/14 TS 6126/14 7.03 25 7.03 TS NOT ENOUGH TO MIX 6127114 12000 7.03 25 7.03 1 TS 15001 12.14 27 12.2 1 TS 12.09 727.3 12.17 1:23PM 282 JP 1:20PM 6/28/14 TS 1:27PM 6/281141 JP 6128114 7.16 25.1 7.16 1 TS NOT ENOUGH TO MIX 6129114 7.16 25.1 7.16 1 TS NOT ENOUGH TO MIX 16130/141 12000 1 7.16 25.1 1 7.16 1 TS 1500 12.22 26.41 12.27 HH 11.66 1 27.9 11.75 4:21PM I 289 HH 12:30PM I 7/1/14 HH I 9:30PM 7/1114 JP I I I DIGESTER VSR & I MGT FECAL TR. PRIK DIG. /oVS /oVS VSR /o �2 FEC. CT. 2 D QTR. o , /oVS D /oVS Vo R /o DATE P D F DATE D F FEC. CT. 1116114 1123114 1/28/14 HH JP Bw HH JP BW HH JP HH JP 651 79; 43 60 59.4 1344 412/14 4/23/14 rDM DM DM 791 53 70 36.6 26719 2598 1648 2128 364 364 596 60.1 42.7 83.3 120000 11220 5000 9323 BW Bw SE Bw DM HH TS 64 67 53 4854.5 BW HH 781 801 67 40 5/8/14 5120114 SE BW 33.2 65.6 65.2 64.1, < 2/11/14 2118114 HH JP 59 72 49 47 JP Bw DM 751 661 59 56 52.3 34.4 _ 5/27/14 6/2/14 6112114 DM HH DM HH < < 2/26/14 315114 BW DM BW DM 2706 1875 71 65. 46 46 72 52 67.9, ' TS TS G.M. 1 2958.791 G.M. 1 1 1525.476 MIN. 1 651 40 34.41 3441 MIN. 1 1 59 46 33.21 364 MAX. 1 801 67183.31 20000 MAX. 1 79 53 70 26719 AVER. 1 173.6153.9155.7 5781.14 AVER. 68.1 48.9 54.2 56.3 4916.714 3RD. QTR. PRIM DIG. %VS VSR % i f DIG. #2 FEC. CT. 4TH. QTR. PRIM DIG. %VSI %VS VSR' DIG. #2 % 1 FEC. CT. DATE P D F %VS DATE P D IF 7/2/14 HH JP BW HH JP BW DM HH Bw HH JP Bw DM HH BW 691 71 68 66 68 70 52 51.31 <1455 3125 1042 417 10/1114 1019/14 10/15/14 10/23/14 10/29/14 11/5114 11/13/14 JP BW TS JP Bw TS JP Bw Ts SE JP 72 71 78 85 45 46 68.1 65.2 <'481 < < 7110/14 7/17114 46 46 65.2 59.9 < 1021 410 45 46 76.9 84.9 7/24114 7/29/14 DM HH 51 53 46.3 46.9 < SE JP SE JP 432 410 556 642 75 78 72 47 49 70.4 72.9 8112114 8/21114 Bw DM 51 51 55.3 46.4 < SE DM SE DM SE DM 520 1819 DM DM 66 455 52 57.8 i G.M. 1 720.0381 G.M. 616.2013 MIN. 66 46 46.31 1 417 MIN. 71 45 57.81 410 MAX. 71 53 65.21 1 31251 MAX. 85 52 84.91 1819 AVER. 68.3 50 53 956 AVER. 75.9 47.1 70.9 = 727.5714 % VSR CALCULATION: PRIM. %VS--DIG.%VS X 100 MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100) DIG. #2 FECAL MUST BE BELOW 2,000,000 7 SAMPLES (MINIMUM) REQUIRED PER QUARTER ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989 WWTP Name: Roanoke Rapids Sanitary District WWTP NPDES Number: NCO024201 Monitoring Period: From 07/01/14 To 09/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion ire - .J:..-M- +--1+....... +.— —*'—.A Wl— A — !90 c Rl n nla*a tha fnllnwina mnnifnrina data - Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6 1h MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Mt.2. Option/Alt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement In 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." R. DanielevJ3rown, PE Chief Executive Officer Prepar a e and T' rint) Land Applier Name and Title (if applicable) (type or print) V AD SSignatu of Preparer e Signature of Land Applier (if applicable) Date *Preparer is defined/ 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQOOO1989 Jul 2014 NPDES NO. NCO024201 PSRP PSRP PSRP PSRP PSRP PSRPIPSRP PSRP IPSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP i 1 PRE TEMP ADJ. I LBS. 2 TEMPI ADJ. I 24 TEMPI ADJ. 24HR 24HR I 24 HR 24 HR I TIME DATE GALS. LIME C PRE N LIME HOUR I C 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL REMOVAL N OF OF N DATE PH I PH ! T JUSED PH I PH T PH PH TIME I NO. T TIME DATE T REM REM T 711114 7.13 25 7.13 HH I NOT ENOUGH TO M0( 712/14 7.13 25 7.13 HH NOT ENOUGH TO M0( 713114 11500 7.13 25 7.13 I HH 18001 12.21 27.8 12.3 HH 12.15 28.7 12.24 4:18PM 301 JP 12:20PM 7/4/14 HH 1:25PM 7/9/14 TS 7/4114 7.08 24.8 7.08 HH NOT ENOUGHI TO M0( 7/5/14 7.08 24.8 7.08 HH NOT i ENOUGH TO MU( 716114 7.08 24.8 7.08 HH NOT (ENOUGH TO MIX 717/14 7.08 24.8 7.08 HH NOT ENOUGH TO MIX 718/14 12500 7.08 24.8 7.08 HH 1800 12.56 1 26.2 1 12.59 BW 12.21 25.2 12.21 8:03PM 305 BW 1 8PM 1 7/9114 BW 8:05PM 719/14 BW 719114 6.99 23.5 6.95 BW: NOT ENOUGH TO MIX I1 7/10/141 12000 6.99 23.5 6.95 1 BW 1 1800 12.25 27.2 12.31 TS 12.14 27.8 12.23 4:18PM 318 SE 10AM 7/11114 JP 4:20PM 7/11/141 SE 7/111141 11250 7.35 22.5 7.28 BW 1500 12.23 27.3 12.29 SE 11.79 28.5 11.9 4:59PM 322 DM 4:30PM 7/12/14 SE 5:05PM ' 7112114 DM- 71121141 71131141 11250 6.91 25.2 6.91 25.2 6.91 6.91 1 HH HH 1500 NOT ' 12.19 29 ENOUGH 12.32 DM TO 1 12.15 I 28.2 MIX 12.24 5:33PM 329 BW 4:30PM 7/14114 1 DM 5:35PM i 7114114 ! BW 71141141 6.74 25.9 6.77 HH NOT ENOUGH I TO 1 MIX 1 7115114 13000 6.74 1 25.9 6.77 HH 1500 12.2 27 12.26 DM 11.79 27.5 1 11.87 12:32AM 337 DM 9:15PM 1 7/16114 DM 112:35AM 7/17114 DM 7/16/14 6.83 25.6 6.85 DM NOT ENOUGH TO MIX 7/171141 13000 6.83 1 25.6 6.85 DM 1500 12.27 26.6 12.32 1 DM 12.19 28 12.28 4:56AM 345 DM 1:00AM 7/18/14 DM 5:OOAM 7/18114 DM 7/1711141 12250 i 6.98 25.1 1 6.98 DM 2100 12.01 30.6 12.17 BW 11.35 30.7 11.53 1:26PM 350 HH 1:20PM 7/18114 BW 1:30PM 7/18/14 TS 7/18114 13500 7.56 26 ' 7.59 BW 1500 12.29 27 12.35 ! TS 11.63 27.1 11.69 11:45AM 354 HH 10AM 7/19114 TS 111:50AM1 7/19/14 HH 7/19114 12250 6.96 25.2 1 6.96 TS 1500 12.37 26.2 12.4 ; HH 12.06 27 12.12 12.59PM 359 HH 12:40PM 7/20/14 HH 1:05PM ; 7/20114 HH 7/20114 12250 6.62 26 6.65 HH 1500 12.3 1 26.8 12.36 JP 12.21 27 12.27 1:18AM 366 JP 12:14AM 7122/14 JP 1:20AM 7/22114 JP 7121/14 7.91 23.7 7.88 JP NOT ENOUGH TO MIX 7122114 12000 7.91 23.7 7.88 JP 1800 12.5 25.5 1 112.52 DM 12.11 30.5 12.28 1:16PM 382 TS 10:30AM 7/23114 DM 11:13PM 7/23114 DM 7122114 11750 4.74 24 4.71 DM 1800 12.32 26.1 i 12.35 DM 11.71 29.1 11.83 1:19PM 383 TS 1:OOPM 7/23114 DM 1:22PM 7/23/14 DM 7122114 12750 4.72 23.4 4.68 HH 2100 i 12.38 24.4 12.4 HH 11.63 26.1 11.66 10:12PM 385 HH 10:10PM 7/23114 HH 10:15PM1 7/23/14 HH 7/23114 1 6.59 26.2 6.62 TS I NOT ENOUGH TO MIX 7/24/14 6.59 26.2 6.62 TS 15001 12.32 ; 27.9 12.41 DM 12 29.5 12.14 4:47PM 396 JP 4:45PM 7/24/14 DM 4:50PM 7/25/14 JP 7/25114 13000 5.49 27.1 5.55 JP 15001 12.39 1 27.1 12.45 1 BW 12.2 26.3 1 12.24 1 8:03PM 404 1 BW 8PM 7/26/14 BW 8:05PM 7/26/14 BW 7126114 12750 6.3 25.8 6.33 JP 1500 12.18 26.1 12.21 BW 12.17 26.41 12.21 18.35PM 409 BW 8:30PM 7/27/14 BW 8:40PM 7/27/14 BW 7127114 12000 6.6 25.6 6.61 BW 1500 12.39 26.4 12.44 BW 12.18 26.3 12.22 8:17PM 412 BW 8PM 7/28/14 BW 8:20PM 7/28/141 BW 71281141 6.42 24.8 6.42 BW NOT ENOUGH TO MIX 1 71291141 12000 6.42 24.8 6.42 BW 1500 12.34 23.8 12.31 BW 12.42 21.4 12.32 6:06AM 424 1 JP 6:05AM 7/30/14 BW 6:08AM 7130/141 JP 7129114 12750 6.4 33.8 6.67 HH 1800 12.36 30.2 12.51 HH 12.29 30.9 12.47 5:14PM 433 HH 5:1OPM 7/30/14 HH 5:18PM 7/30114 HH 7/30114 12750 6.03 25.7 6.05 1 HH 1200 12.29 27.3 12.35 TS 12.16 28.1 12.25 1:59PM 436 TS 1:20PM 7/31/14 TS 2:08PM 7/31114 S T 7131/14 6.79 25 6.79 HH NOT ENOUGH 'TO MIX PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT NC MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WO0001989 Aug 2014 NPDES NO. NCO024201 PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP !PSRPI PSRP IPSRP PSRP PSRP I PSRP ,PSRP PSRP I PSRP PSRPj PSRP PSRP PSRP PRE TEMP ADJ. I I LBS. 2 ITEMP ADJ. 1 1 24 TEMPi ADJ. 24HR 24HR 1 24 HR 24 HR I TIME DATE I GALS. LIME ' C PRE N LIME HOUR I C 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL EMOVA N OF OF N DATE PH PH T USED PH PH T PH PH TIME NO. T TIME DATE T ; REM REM 1 T 811114 12250 6.79 25 6.79 HH 1500 12.28 26.2 12.31 JP 12.16 26 12.19 5:57AM 443 DM 12:35AM 8/2/14 i JP 16:05AM 8/2114 DM 8/1114 7.30 25.2 7.30 JP NOT ENOUGH TO MIX 8/2114 11250 7.30 25.2 7.30 JP 1500 12.41 25.0 12.41 DM 11.8 27.9 11.89 8:54PM 452 DM 8:45PM 8/3/14 ( DM 19:OOPM 8/3/14 DM 8/3114 7.06 24 7.03 DNI I NOT ENOUGH TO ! MIX 814114 11750 7.06 24 7.03 DM 1500 12.3 27.0 12.36 TS 12.21 28.8 12.33 5:39PM 461 TS 5PM 815114 TS 5:45PM 815/14 TS 815/14 6.86 I 24.9 6.86 DM NOT 1 ENOUGH TO MIX 816114 12750 6.86 24.9 6.86 DM 2100 12.24 28.9 12.36 SE 1 12.01 29.5 12.15 10:17AM 468 I SE ! 7:02AM :' 8/7/14 SE 10:30 i 8/7/14 SE 817/14 7.05 24.6 7.05 SE NOT !ENOUGH TO MIX 818/14 7.05 24.6 7.05 SE NOT ENOUGH TO MIX 819114 12000 7.05 24.6 7.05 SE 1500 12.14 28.0 12.23 DM 12.05 27.0 12.11 11:17AM 477 OM IO:OOAM 8/10/14 DM 1:10PM 8110/14 DM 8/9114 12250 7.20 29.8 7.35 DM 15001 12.06 ! 30.5 12.23 DM 11.89 30.4 12.06 1:03PM 478 DM 12:15PM 8/10114 DM 1:10PM 8/10114 DM 8/10114 12250 6.89 32.0 7.10 DM 1800 11.98 34.81 12.28 DM 12.01 30.7 12.19 1:41 PM 482 SE 11:45AM 8/11114 . DM 1:50PM 8/11/14 ; TS 81111141 6.85 24.4 1 6.84 HH i NOT ENOUGH TO MIX 8112114 6.85 24.4 6.84 HH NOT ENOUGH TO MIX 8/13114 11875 6.85 24.4 6.84 HH 1800 12.36 27.5 12.44 DM 12.06 ! 27.5 12.14 i 5:16AM 491 DM 5:OOAM 8114/14 DM 5:18AM 8/14/14 DM 8/13/14 6.94 24.7 6.94 SE NOT 'ENOUGH TO MIX 8/141141 6.94 24.7 6.94 SE NOT H TO MIX 8115114 6.94 24.7 6.94 SE NOT H TO MIX 8116/14 1 6.94 24.7 6.94 SE 1500 12.16 25.5 12.18 JP $1219 23.8 12.31 6:28AM 501 JP 6:25AM 8/17114 JP 6:29AM 8/17/141 JP 8117/14 12750 7.06 ' 23 7 HH 2400 12.22 25.5 12.24 HH 28.5 12.32 1:45PM 510 SE 9:45AM 8/18/14 HH 1:50PM 8/18/14 ' SE 8/18114, 12000 6.75 23.7 6.71 HH 2100 12.17 28.1 12.26 TS 27.8I 12.28 1:52PM 514 TS 1:30PM 8/19114 TS 2PM 8/19/14 TS 8/191141 6.88 25.9 6.91 DM NOT IENOUGH I I TO MIX 8120114 6.88 25.9 6.91 DM NOT !ENOUGH I TO MIX 8121114 12000 ' 6.88 25.9 6.91 DM 2100 1226 262 12.29 HH 12.06 1 27.6 1 12.14 5:49AM ! 525 HH 5:20AM 8/22/141 HH 5:52AM 8122/14 HH 8122114 6.83 25.9 6.86 DM NOT j ENOUGH TO MIX 8123114 6.83 25.9 6.86 DM NOT ENOUGH TO MIX 8124l14l 12250 6.83 25.4 6.86 DM 1800 12.19 25.4 12.2 BW 12.21 25.2 12.21 6:01AM 529 BW 6AM 8/25114 BW 6:05AM 8125/14 BW 8/25/141 NOT ENOUGH TO I MIX $1261141 12000 6.94 23 6.88 SE . 1800 12.28 26.1 12.31 HH 12.1 27 12.16 14:52PM 543 HH 4:25PM 8/27/14 HH 4:55PM 8/271141 HH 8127114 12000 6.62 30.5 6.79 HH 2100 12.16 31 12.34 HH 1 12.11 29.1 1 12.23 1:41PM 542 SE 1:30PM 8/27/14 HH 1:50PM 8/27/14 SE 8127114 11500 6.77 25 6.77 HH 1500 12.22 26.1 12.25 JP ! 12.2 26.7 12.26 9:33PM 551 JP 9:20PM 8/28/14 JP 9:35PM 8/28/14 JP 8128114 7.13 24.8 j 7.13 JP NOT ENOUGH TO MIX 8129/14 12750 7.27 33.1 7.51 BW 1800 12.11 31.8 12.32 BW 12.11 31.8 12.32 2:13PM 554 BW 2:13PM 8/29114 BW I 2:15PM 8129/14 BW 8/30/141 12000 7.13 24.8 7.13 JP 15001 12.26 26.5 12.31 DM 12.06 T 27.5 12.14 5:33AM 560 DM 5:OOAM 8/31114 DM 5:35AM ' 8/31/14 DM 8/311141 7.37 24.3 7.36 BW NOT ENOUGH TO ( MIX I I I I PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQOOO1989 NPDES NO. Sep 2014 SNCO024201 PSRP PSRP PSRP I PSRP ;PSRP PSRR PSRP PSRP PSRP I PSRP PSRP PSRP PSRP PSRP PSRP I PSRP PSR PSRP PSRP PSRP PSRP I PSRPPSRP i i PRE I TEMP I ADJ. i LBS. 2 TEMP ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR I TIME DATE I GALS. LIME I C PRE N UME HOUR C 2 HR N HOUR C 24HR I PH SAMPLO N REMOVAL REMOVAL N : OF OF N DATE PH I PH T USED PH PH T PH PH TIME NO. T TIME DATE T REM REM T 911114 7.37 24.3 7.36 BW NOT ENOUGH I TO MIX 912114 12750 7.37 24.3 7.36 BW 1 1500 12.17 28 12.25 JP 12.12 1 27.6 122 4:25PM 572 JP 1 4:20PM 9/3/14 JP 4:30PM 9/3114 JP 913114 6.79 26.6 6.85 JP 1 NOT ENOUGH I TO MIX 914114 12000 ! 6.79 26.6 6.85 JP 11500 12.29 26.2 12.29 BW 12.17 1 28 12.26 ! 8:24PM 583 HH, 8:20PM 1 915114 BW 8:30PM 9/5114 HH 9151141 6.78 25.2 6.78 SE NOT ENOUG TO MIX 9161141 9/7/14 1 11675 6.78 6.78 25.2 25.2 6.78 6.78 SE SE 1 1500 12.1 28.1 NOT 12.19 ENOUGH DM 122 1 27.8 TO 12.29 4:37PM MIX 591 SE 4:0013M 918114 ! DM 4:40PM ! 9/8/14 SE 9181141 7.08 25 7.08 DM NOT ENOUGH TO MIX 919114 12750 7.08 25 7.08 DM 1800 12.49 25 12.49 HH 12.17 25.4 12.19 5:16AM 602 DM 4:05AM 9110114 I HH 5:25AM 1 9/10114 DM 919114 12750 6.37 25.6 6.38 BW 2400 12.36 26 12.39 SE 12.22 25.5 12.23 5:26PM 609 BW 5:15PM 9/10/14 SE 5:30PM 1 9110/14 BW 9/10114 12750 6.72 25.4 6.73 BW 2100 12.2 25.4 12.21 BW 12.16 25.9 12.19 1:59PM 618 BW 1:30PM 9/11/14 BW 2.05PM 9/11l14 BW 9110114 10500 6.72 25.4 6.73 BW 2100 12.26 25.1 1226 BW 1226 27.5 12.34 6:34PM 620 DM 6PM 9/11/14 BW 6:35PM 9/11/14 ! DM 9/11/10 11875 5.97 24 5.94 DM 2100 12.3 25 12.3 DM 12.14 27 12.2 5:23AM 623 DM 12:15AM 9/12/14 DM 5:23AM 9/12/141 DM 9/12114 NOT ENOUGH TO MIX 9113114 12500 5.33 23.7 5.29 HH 3300 12.27 24.2 12.24 JP 12.29 ; 23.5 12.25 10:12PMV 635 JP 9:45PM 9/14114 JP ',10:18PM 9/14114 JP 9114114 11500 6.74 22.7 6.68 JP 3000 12.33 24.1 12.3 JP 12.52 25 i 12.52 10:33PM: 644 JP 10:35PM 9/15/14 JP ;10:40PM 9/15/14 JP 9/15/14 12500 - - - DM 2100 12.35 27.5 12.43 DM 11.97 27.6 12.05 9:13AM 648 DM 3:45PM 9/16114 DM ! 9:15AM 9/17114 DM 9116114 6.7 24 6.67 DM NOT ENOUGH TO MIX 9/17114 12000 6.7 24 6.67 DM 1800 12.39 27.6 12.47 DM 12.28 27.5 12.36 4:1OPM 658 DM 1 2:30PM 9/18114 OM 4:15PM 9/18/14 DM 9118114 12000 5.78 23.9 5.75 HH 2400 12.32 25 12.32 DM 12.09 26.2 12.12 11:06AM 665 JP 110:OOAM 9/19114 DM 11:10AM 9119/14 JP 9/18114 12000 6.94 33 7.18 DM 2100 12.3 31.9 12.51 DM 12.29 ! 27.9 1 12.38 5:03PM 668 JP 5:OOPM 9/19/14 DM 5:10PM 9/19/14 JP 9119114 10500 7.04 27.8 7.13 HH 2100 11.72 26 11.75 JP 11.7 25.5 11.72 11:54AM 671 JP ; 11:12AM 9/20/14 JP 12:OOPM 9/20114 JP 9/20/14 NOT ENOUGH TO I MIX 9/21114 NOT ENOUGH TO MIX 9/22/141 NOT ENOUGH TO MIX 9123/14 12000 6.67 31.7 6.88 TS 2400 12.5 26.8 12.56 TS 12.32 27.8 12.41 !10:42AM 681 SE 10:30AM 9/24/14 TS 10:50AM 9/24/14 TS 9124114 13500 5.39 24.2 5.36 TS 2400 12.09 24.6 12.09 SE ! 11.67 24.4 11.66 i 1:14PM 688 SE 10:16AM 9/25/14 TS 1:20PM 9/25/14 SE 9/25114 12375 7.07 21.1 6.95 JP 1500 12.54 23.5 12.5 SE 12.39 24.6 12.39 1:15PM 693 TS 1:06PM 9/26/14 SE 10:20PM 9/26/14 DM 9125/14 240000 7.77 - - MJ 29620 12.16 35.5 12.48 SE 11.38 31.5 11.58 111:09AM LAB SE 10:38AM 9/26/14 SE 9/26114 7.02 22.9 6.96 HH NOT ENOUGH TO MIX I 9126114 7.02 22.9 6.96 HH NOT I ENOUGH TO MIX 9127114 11250 7.02 22.9 6.96 HH 1200 12.23 24.5 12.22 DM 11.85 24.5 11.84 ; 5:52AM 700 DM 5:45AM 9/28114 DM 5:55AM 9/28/14 DM 9128114 12625 7.15 21.6 7.05 BW 1800 12.46 24.5 12.45 DM 12.31 24.1 12.28 14:44AM 710 I DM 9:10PM 9/29/14 DM 4:50AM 9/30l14 DM 9129/14 6.62 22.8 6.56 DM NOT !ENOUGH TO MIX 9129/14 12000 6.62 22.8 6.56 JP 1800 12.01 32.3 1224 JP 11.74 28.4 11.86 3:12PM 714 I JP 3:0OPM 9130/14 JP 3:15PM 9/30/14 JP 9130114 13375 7.32 29.4 7.45 JP 1800 12.22 24 12.19 JP 1 12.02 25.2 12.29 4:50PM 723 JP 4:45PM 1011/14 JP ! 4:55PM 1011/14 JP DIGESTER VSR & 1 MGT FECAL NALYSIS R. PRIMj, %VSI%VS DIG. VSR j DIG. #2 2ND QTR. PRIM) DIG. VSR j % DIG. #2 DATE PMHHHH % FEC. CT. DATE P D F %VS1%VS� FEC. CT. 1/16114 HH JP BW 65' 79 43 60 59.4 1344 4/2/14 4/23/14 DM BW DM DM 791 53 70 36.6 26719 2598 1648 2128 364 364 596 i - 1/23114 1/28114 60.1 120000 5000 Bw BW SE 64 67 53 48 78 80 67 40 42.7 83.3 5/8114 5120/14 SE BW SE BW 54.5 33.2 65.5 65.2 64.1 < 2/11114 2118/14 HH JP 11220 9323 BW DM 59 72 49 47 Bw 75 661 59 56 52.3 34.4 5127114 6/2114 6112114 - DM HH DM HH < 2/26/14 315114 - - Bw DM Bw DM - 12706 ;1875 --- HH 71 65 46 46 DM - 72 521 57.9 TS TS TS <; - - - G.M. ( 2958.79 G.M. j j 1525.476 MIN. 65 40 34.41 344 MIN. j 1 59 46 33.2 364 MAX. 80 67 83.31 20000 MAX. 1 79 53 701 26719 AVER. 73.6 53.9 55.7 : 5781.14 AVER. j 1 1 168.1 48.9 54.2 `_ 4916.714 3RD. QTR. PRIMA DIG. %VS VSR! % i DIG. #2 FEC. CT. 4TH. QTR, PRIMLDIG. %VSI %VS VSR i/6-T I DIG. #2 FEC. CT, DATE P D F %VS DATE P D F 7/2/14 HH JP Bw HH JP HH JP 69 71 52j 51.3 < 465 3125 10/1/14 10/9/14 10/15114 10/23/14 10/29/14 _ 1115114 11/13/14 JP BW TS JP Bw TS JP Bw TS 72 71 78 85 75 78 45168.1 46 66.2 <1481 < < 7110114 7/17/14 46 46 65.2 59.9 < 11021 1410 432 410 Bw DM Bw DM 68 66 1042 417 45 46 47 49 76.9 84.9 70.4 72.9 7124114 7129114 DM HH 51 53 46.3 46.9 < SE JP SE JP SE JP HH Bw HH Bw 68 70 556 642 8/12114 8121/14 Bw DM 51 51 55.3 46.4 <1455 SE DM SE DM SE DM 520 1819 DM DM 66 72 52 57.8 G.M. 1 1 ( j 720.038 G.M. j j 616.2013 MIN. 1 1 1 66 46 46.3 417 MIN. 1 71 45 57.81 410 MAX. 1 71 53165.21 3125 MAX. I I 1 1 851 52184.91 1819 AVER. 1 68.3 501 53 956 AVER. I 1 1 1 76.9 47.1 70.9 727.5714 % VSR CALCULATION: PRIM. %VS--DIG.%VS X 100 MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100) DIG. #2 FECAL MUST BE BELOW 2,000,000 7 SAMPLES (MINIMUM) REQUIRED PER QUARTER ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Roanoke Rapids Sanitary District WQ Permit Number: WQ0001989 WWTP Name: Roanoke Rapids Sanitary District WWTP NPDES Number: NCO024201 Monitoring Period: From 10/01/14 To 12/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion .:...........4.A. - J.+.. Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 0 MPN MPN/g Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. I Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 (Injection) Option/Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware.that there are significant penalties for false certification including fine and imprisonment." R. Danieley Brown PE Chief Executive Officer Prepare e and Tit (typ int) Land Applier Name and Title (if applicable) (type or print) 2Wt Signatur of Preparer* Signature of Land Applier (if applicable) Date *Preparer is defined, in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N< MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WO0001989 Oct 2014 NPDES NO. NC0024201 PSRP PSRP PSRP PSRP PSRP IPSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP ! PSRP PSRP IPSRR PSRP I PSRP PSRP PSRP PSRP PSRP PRE TEMP ADJ. 1 LBS. 2 TEMP ADJ. 1 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR I TIME I DATE I GALS. LIME C PRE N LIME HOUR C 2 HR N HOUR C 24HR PH SAMPLEI N REMOVAL REMOVAL N OF I OF N DATE PH PH T I USED PH PH T PH PH TIME NO. ! T TIME DATE T REM i REM T 1011/14 7.3 22.4 7.24 JP NOT ENOUGH 1 TO MIX i 10/2114 10250 7.3 22.4 7.24 JP 1500 12.65 23.9 12.62 JP 11.8 25.9 11.83 2:17PM 735 SE 110:15AM 10/3114 JP 2:25PM 10/3114 SE 1012/14 12000 7.07 28.6 7.18 i JP 2100 12.09 31.7 12.3 JP 11.41 31.1 11.59 2:19PM 736 SE i 2:05PM 10/3/14 JP 2:25PM ' 10/3/14 SE 1012/14 12000 7.07 28.6 7.18 JP 2100 12.17 31.9 12.38 JP 12.07 29.6 12.21 8:47PM 740 HH 6:10PM 10/3/14 JP . 8:50PM 1 10/3/14 HH 1013114 7.53 23.4 7.49 HH NOT JENOUGH TO M1X 1014/14 1 7.53 23.4 7.49 HH NOT IENOUGH TO MIX 10/5114 12000 ' 7.53 23.4 7.49 HH 1 1500 12.3 1 23.5 12.26 DM 12.29 23.8 12.26 1:16PM 755 TS 9:30AM 10/6/14 DM 1:25PM i 10/6/14 SE 10/5114 12000 6.4 22.9 6.34 DM 124001 12.24 1 24.9 12.24 DM 12.43 23.8 12.4 1:18PM ' 756 TS 12:50PM 10/6/14 DM 1:25PM 10/6/14 BW 1015114 12000 6,93 ! 21.4 6.83 DM 2400 12.3 22.3 12.23 HH 12.39 23.2 12.33 10:31 PM 1 758 HH 8:30PM 10/6/14 HH 110:35PM 10/6/14 HH 1016/14 6.84 ( 19.2 6.66 HH I NOT ENOUGH TO MIX 10M14 12000 6.84 19.2 6.66 HH 11800 12.46 22.7 12.39 DM 12.12 23.6 12.08 4:42AM 767 DM 9:30PM 10/8/14 DM 14:45AM 1 10/9/14 1 DM 1018/14 6.76 22.3 6.69 DM NOT ENOUGH TO MIX 10/9/14 6.76 22.3 6.69 1 DM NOT ENOUGH ! TO MIX 10/9114 11250 t 5.81 22 5.72 1 BW 2700 12.47 25.7 12.5 BW 12.27 25.8 1 12.29 2:35PM 778 HH 10:30AM 10/10/14 BW 2:38PM 10/10/141 HH 1019/14 6.25 22.6 6.18 1 DM NOT ENOUGH ! TO MIX 10/10/14 12000 6.76 22.3 6.69 DM 1800 12.4 24.2 12.37 HH 12.24 24.5 12.23 3:22PM 781 HH 1:51PM 10/11/14 HH 3:28PM 10/11/141 HH 10/10/14 12000 6.25 22.6 1 6.18 1 DM 2100 12.28 23.5 1 12.24 HH 12.25 24.5 12.24 3:24PM 782 HH 2:10PM 10/11/14 HH 3:28PM 10/11/141 HH 10/11/14 6.64 i 22.8 1 6.58 HH NOT ENOUGH TO MIX i 10/12114 1 12750 6.64 22.8 6.58 HH 2100 12.29 22.6 ' 12.22 HH 12.35 24.5 12.34 1:20PM 793 TS 10:10PM 10/13/14 HH 1:25PM 10/13/14 TS 1012/14 13125 5.26 21.4 5.16 HH 2400 12.45 22.5 12.38 JP 12.47 23.5 12.43 11:26PM 795 JP 9:40PM 10/13/14 JP 11:30PM 10/13/14 JP 10/13114 5.4 21.9 5.31 JP NOT !ENOUGH TO MIX 10/14/14 12000 5.4 21.9 5.31 JP 11800 12.3 26 12.33 DM 1 12.18 25 12.18 6:OOPM 804 DM 5:20PM 10/15/14 DM 6:05PM 10/15/14 DM 10/15114 11500 6.68 23.2 6.62 DM 2100 12.16 ! 28 12.25 DM 1 12.11 26.9 12.17 4:09PM 809 DM 2:45PM 10/16/14 DM 4:10PM 10/16/14 DM 10/16/14 6.25 22.5 6.18 DM ' NOT IENOUGH TO MIX 10/17/14 12000 6.25 22.5 6.18 DM 2100 12.45 1 22.3 12.38 JP 12.29 24.2 12.26 3:08PM 818 JP 10:40AM 10/18/14 JP 3:20PM 10/18/14 JP 10/17/14 1 12000 6.86 31.4 7.04 JP 2100 12.3 31.8 12.5 JP I 12.22 27 12.28 3:09PM 819 JP 2:25PM 10/18/14 JP 3:20PM 10/18/14 JP 10/181191 NOT 1 (ENOUGH TO MIX 10/19/14 NOT I 'ENOUGH TO MIX I=0/14 5.42 20.1 5.27 DM NOT (ENOUGH TO MIX 10/21/14 5.42 20.1 5.27 DM 2400 12.42 22.7 12.36 SE 12.19 22.5 12.12 1:09PM 830 SE 9:25AM 1 10/22/141 SE 10:OOAM 10/24/14 SE 10/22/14 12875 4.95 21.8 4.86 JP 2100 12.53 20.9 12.41 JP 12.34 20.1 12.19 12:26AM 838 JP 12:10AM 10124114! JP 10:OOAM 10/24/14 SE 10/23/14 13000 6.68 24.7 6.68 JP 2100 12.46 21.9 12.36 JP 12.36 22.3 12.29 7:37PM 842 DM 12:40AM 10/25/14 JP 7:40PM 10/25/14 DM 10/24/141 6.89 18.9 6.71 JP NOT ENOUGH TO MIX 10/25/14 ' 6.89 18.9 6.71 JP I NOT ENOUGH TO MIX 10/26/14 6.89 18.9 6.71 JP NOT ENOUGH TO MIX 10/27/14 11750 6.89 18.9 71 JP 15001 12.3 20.41 12.17 DM 12.35 20.4 12.22 5:28AM 850 DM ! 5:15AM 10/28/14 DM 5:30AM 110/28/14 DM 10/28/14 11375 6.74 1 18.6 56 TS 1500 12.39 22.8 12.33 JP 12.35 21 12.23 5:08PM 863 JP I 4:40PM 10/30/14 JP 5:10PM 10/30/14 JP 10/29/14 7.31 i 20.9 19 17.19 BW NOT ENOUGH TO I MIX 10130/14 7.31 20.9 19 BW NOT ENOUGH TO MIX 10/31/14 7.31 20.9 BW NOT ENOUGH TO MIX PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WO0001989 Nov 2014 NPDES NO. NC0024201 PSRP PSRP PSRP PSRP PSRP PSR PSRP PSRP PSRPj PSRP IPSRP PSRP PSRP PSRP PSRP PSRP PSR PSRP I PSRP PSRPSRP I PSRP PSRP j I PRE TEMP ADJ. I LBS. 2 TEMPI ADJ. 1 1 24 TEMP ADJ. i 24HR 24HR 1 1 24 HR 24 HR I I TIME ! DATE I GALS. LIME C PRE N LIME HOUR C 1 2 HR N HOUR C 24HR PH SAMPLE N REMOVAL REMOVAO N I OF OF N DATE PH PH T USED PH PH T PH PH TIME NO. T TIME I DATE I T ; REM REM T 11/1/14 1 12000 7.31 20.9 7.19 1 BW 11800, 12.31 120.31 12.18 DM 12.26 18.1 12.05 1 9:09AM 870 DM 9:OOAM 111/2/14 I DM 9:10AM 1 1112/14 DM 111211411 12000 7.16 17.6 6.94 1 DM 30001 12.37 1 21.4 12.27 DM 12.43 18.9 12.25 10:02AM 880 TS 9:OOAM 1 11/3/14 !DM 10:10AMI 11/3/14 TS 11/2114 12750 6.71 19.4 6.55 1 DM 01 12.55 1 20.8 12.43 HH 12.41 18.8 12.23 1 4:33AM 888 HH 9:10PM 11/3/14 HH 4:35AM 1 11/4/14 HH 11/3/14 11000 7.07 18.4 ' 6.88 1 HH 12001 12.52 21.6 12.43 TS 12.41 21.3 12.29 1 4:27PM 892 TS 4:20PM 1113114 ! TS 14:30PM 1 1114/14 TS 1113114 12000 6.81 32.5 7.04 1 TS 15001 12.21 30.2 12.36 TS 12.16 25.6 12.19 4:25PM 891 TS 3:15PM 1 1114/14 ITS1 4:30PM 11/5/14 TS 11/4114 7.14 21.3 7.03 1 HH NOT ENOUGH TO MIX I 11/5114 7.14 21.3 7.03 HH NOT ENOUGH TO MIX 11/6114 1 12500 7.14 21.3 7.03 HH 1800 12.4 21.2 12.28 DM 12.01 19.9 11.86 5:10AM 900 DM 5:OOAM 1 11/7/14 DM 15:12AM 1IM14 DM 11M14 6.61 19.2 5.43 SE I NOT ENOUGH TO I MIX 11/7/14 12750 6.98 29.6 7.12 , HH : 2100 12.03 28.7 12.12 I HH 12.02 1 24 11.99 3:29PM j 907 HH 3:10PM 11/8/14 HH 3:35PM 11/8/14 I HH 1118114 6.61 19.2 6.43 TS ' NOT I !ENOUGH TO MIX 1119114 6.61 19.2 6.43 TS NOT IENOUGH 1 TO I MIX 11/1OM4 12000 6.61 19.2 6.43 TS 1500 12.32 1 20.1 i 12.17 DM 1 12.4 1 20.4 12.27 4:43PM 914 DM 4:35PM 11/11/14 DM 4:45PM 11/11/14 DM 11/11/14 6.91 15.9 6.64 JP NOT !ENOUGH TO I MIX 11/12114 12250 6.83 32.6 1 7.06 DM 2100 1223 31.1 12.41 DM 12.29 24 ' 12.26 2:15PM 1 922 DM I 1:45PM 11/13/14 DM 2:20PM 11/13/14 DM 11/131141 12000 6.91 15.9 . 6.64 JP 1500 12.53 20.4 12.4 DM 12.25 18.6 1 12.05 2:13PM 1 926 JP I 1:15PM 11/14/14 DM 2:20PM 11/14/14 JP 11114/14' 10750 6.78 16.9 6.54 DM 1800 12.49 1 16.4 12.24 JP 12.42 16.1 12.15 1:03PM 1 935 JP 12:35PM 11/16/14 JP 1:05PM 11/16/14 JP 11/16/14 6.77 15.6 6.49 BW NOT ENOUGH TO MIX 11/16/14 6.77 15.6 6.49 BW NOT ENOUGH TO MIX 11/17/14 12000 6.77 15.6 6.49 BW 12001 12.35 18.9 12.17 TS 12 16.9 ! 11.76 5:07PM 948 TS I 1:45PM 11/18/14 TS 5:15PM 11/18/14 1 TS 11/17l14 12000 6.83 31.7 7.04 TS 1500 12.31 29.1 12.43 TS 12.2 22.4 12.11 5:09PM I 949 TS 4:30PM 11/18/14 TS 5:15PM 11/18/14 f TS 11/18/14 6.6 1 19.2 6.42 BW NOT ENOUGH TO 1 MIX 11/19/14 6.6 19.2 6.42 1 BW NOT ENOUGH TO MIX 111201141 1 6.6 19.2 1 6.42 BW NOT ENOUGH TO 1 MIX 11/21/141 6.6 19.2 6.42 1 BW NOT ENOUGH TO MIX 11/21/141 12000 6.86 1 29.4 6.98 1 SE 1500 12.17 28.1 12.26 SE 12.32 17.81 12.21 2:14PM 963 BW 1:59PM 11/22/14 SE 2:15PM 11/22/141 BW 111211141 12250 6.6 19.2 6.42 1 BW 11200 12.52 17 12.28 DM 12.24 20.4 12.11 10:01PW 965 DM 9:40PM 11/22/14 DM 10:05PM 11/22/14 DM 111221141 6.79 16.5 6.54 DM NOT ENOUGH TO MIX 11/22/14 10500 6.72 21 6.53 BW 1200 12 29.1 12.12 BW 12.23 21.6 12.14 1126AM 968 BW 11AM 11/23/14 1 BW 11:30AM 11/23/14 BW 11/23/14 12625 6.79 16.5 6.54 DM 11500 12.48 23.1 12.42 JP 12.31 21.8 12.22 4:49PM 983 JP 1:15PM 11)25/14 JP 4:55PM 11/25/14 JP 11/24114 13250 1 6.5 ! 29.3 6.64 JP 11800 11.99 30 12.14 JP 11.8 25.4 11.82 1 4:47PM 982 JP 4:10PM 11/25/14 JP 4:55PM 11/25/14 JP 11/25/14 13125 6.39 i 19.1 i 6.21 DM 1500 12.56 24.61 12.55 JP 12.22 20.9 12.1 1 4:42PM 987 JP 4:45PM 11/27/14 JP 1:40PM 11/27/14 JP 11/26/14 13125 6.63 29.2&6.7DM 1500! 11.93 29.6 12.07 JP 11.97 22.4 11.77 4:41PM 990 JP 4:45PM 11/27/14 JP 4:30PM 11/27/14 JP 11127114. NOT i ENOUGH I TO MIX 11/28/14; NOT ENOUGH TO MIX 11/29/14 12000 6.59 28.42100 12.23 29 12.35 DM 12.38 24 12.35 3.18PM 4 DM 1:20PM 11/30/14 DM 3:25PM 11/30/14 DM 11/29/14 6.59 28.4 1200 12.24 30.4 1 12.41 1 DM 12.41 23.9 12.43 3:20PM 5 DM 2:05PM 1 11/30/14 DM 3:25PM 11/30/141 DM 11130/141 NOT (ENOUGH TO MIX PATHOGEN AND VECTOR ATTRACTION REDUCTION ROANOKE RAPIDS SANITARY DISTRICT PERMIT N( MONTH YEAR ROANOKE RIVER WASTEWATER TREATMENT PLANT WQ0001989 Dec 2014 NPDES NO. NC0024201 PSRP PSRP PSRP PSRP PSRP PSRP PSRP PSRP I PSRP PSRP I PSRP LBS. 2 TEMP ADJ. 1 PSRP I PSRP PSRP I PSRP PSRP PSRP PSRP PSRP PSRPI PSRP PSRP I PSRP DATE 1 PRE TEMP ADJ. I 24 TEMP ADJ. 24HR 24HR 1 24 HR 24 HR 1 1 TIME GALS. LIME C PRE N LIME HOUR C 2 HR N HOUR C 24HR : PH SAMPLE N REMOVAL REMOVALj N I OF OF N DATE PH PH T USED. PH PH T PH PH TIME NO. T TIME DATE T I REM REM T 1211/14 1 1 NOT ENOUGH TO MIX 1212114 i 12000 6.51 29.7 6.66 BW 1500 12.1 30.3 12.25 BW 12.13 24.3 12.12 1:08PM 12 BW 11AM 12/3/14 BW 1:10PM 12/3/14 BW 1213114 6.5 14.9 6.2 DM NOT JENOUGH TO MIX 1214/14 6.5 14.9 6.2 DM NOT JENOUGH TO MIX 12/5/14 12000 6.5 14.9 6.2 DM 11200 12.22 18.2 12.01 JP 11.99 17.5 11.77 4:54AM 22 JP 12:45AM 1217/14 JP 8:40AM 1ZW14 TS_ 12161141 6.9 19.7 6.74 JP I NOT ENOUGH TO MIX 12l7/14 6.9 19.7 6.74 JP NOT ENOUGH TO MIX 12181141 12000 6.9 19.7 6.74 JP 12001 12.6 16.9 12.36 TS 12.3 14.4 11.97 10:44AM 29 TS 10:20AM 1219/14 TS 10:50AM 12/9/14 TS 1219/14 6.26 15.9 5.99 i TS NOT :ENOUGH TO MIX 12/10/1.4 12250 6.26 15.9 5.99 ! TS 1500 12.57 16.5 12.32 TS 12.27 15.7 12 1:19PM : 36 TS 1PM 12/11/14 TS 1:25PM 12/11/14 TS 12/11/14 6.59 14.7 6.71 SE NOT ENOUGH TO I MIX 12/12/14 12000 6.59 14.7 6.71 SE 1500 12.42 17.4 12.2 BW 12.49 16.6: 12.24 1 8 40 BW 8:05PM 12/13/14 BW 835PM 12/13/14 BW 12/13/14 6.62 14.4 6.31 JP NOT ENOUGH TO MIX 12/14/14: 6.62 14.4 6.31 JP NOT ENOUGH TO MIX 12/15/14 12000 16.62 14.4 6.31 JP 1200 12.44 17 12.2 TS 12 16.6 11.75 1:18PM 51 TS 1 PM 12/16/14 TS 1:22PM 12/16/14 TS 12/16/14 7.06 17.9 6.85 HH NOT ENOUGH TO MIX 12/17/14 7.06 17.9 6.85 HH NOT iENOUGH TO MIX 12/18/14 12000 7.06 17.9 6.85 HH 1500 12.7 16.4 12.43 TS 12.42 16.4 12.17 1:19PM 58 TS 12:35PM 12/19/14 TS 1:22PM 12/19/14 TS 12/19/14 6.45 17.9 6.21 TS NOT i ENOUGH I TO MIX 121201141 6.45 17 6.21 TS NOT ENOUGH TO MOC 12/21/14 12250 6.45 17 6.21 TS 1200 12.52 14.9 12.22 DM 12.36 16 12.09 5:39AM 66 DM 5:15AM 12/22/14 DM 5:45AM 12/22/14 DM 12/22/14 6.8 17.2 6.56 BW NOT ENOUGH TO MIX 12/23/14 11500 6.8 17.2 6.56 BW 1200 12.55 18.1 12.34 BW 12.58 19.1 12.4 8:25PM 70 BW 8PM 12/24/14 BW 8:27PM 12/24/14 BW 12/23/14 12250 6.5 14.8 6.2 JP 1500 12.34 28.1 12.43 JP 12.2 20.9 12.08 1:59PM 75 JP 1:45PM 12/24/14 JP 2:OOPM 12/24/14 JP 12124/14 6.46 17.4 6.2 BW NOT ENOUGH TO MIX 12/25/14 6.46 17.4 6.2 BW NOT ENOUGH TO MIX 12/26114 6.46 17.4 6.2 BW I NOT ENOUGH TO MIX 12/27/14 6.46 17.4 6.2 BW I NOT ENOUGH TO MIX 12/28/14 6.46 17.4 6.2 BW NOT ENOUGH TO MIX 12/29M4 6.46 17.4 6.2 BW NOT ENOUGH TO MIX 12/30/14 6.46 17.4 6.2 BW NOT ENOUGH TO MIX 12/31/14 6.46 17.4 6.2 1 BW NOT ENOUGH TO MIX i DIGESTER VSR & 1 MGT FECAL ANALYSIS 1 ST. QTR. PRIM. %VS! DIG. %VSI VSR % I DIG. #2 FEC. CT. 2ND QTR. PRIM1 DIG. VSR % DATE P D F DATE P D F %VSj%VSI FEC.CT. 1/16/14 HH JP Bw HH JP BW HH JP HH JP 65III 79I 431 60 59.4 1344 4/2114 4/23/14 DM BW DM DM 79 53 70 36.6 26719 1/23/14 1/28114 60.1 42.7 83.3 5000 20000 Bw Bw SE 64 67 53 48 2598 1648 2128 364 364 BW HH 78I 801 67 40 518/14 5/20/14 SE BW SE BW 54.5 33.2 65.5 65.2 54.1 < 2/11114 2118114 HH JP 9323 1220 BW DM 59 72 49 47 JP Bw DM 75 66 59 56 52.3 34.4 6127114 6/2114 6/12114 DM HH DM HH < 2/26114 315114 Bw DM Bw DM 2706 HH TS 71 65 46 461 72 5Z 57.9 .1876 TS TS <;596 I G.M. 2958.79 G.M. ( 1525.476 MIN. 1 1 651 40 34.41 344 MIN. j I 1 591 46 33.2 364 MAX. 80 67 83.31 20000 MAX. j 791 53 701 26719 AVER. 73.6 53.9 55.7 5781.14 AVER. 1 68.1 48.9 54.2 4916.714 3RD. QTR. PRIMI DIG. %VS VSR % DIG. #2 4TH. QTR. PRIM, DIG. %VS %VS VSR DIG. #2 FEC. CT. DATE P D F %VS I FEC. CT. DATE P D F % 712114 HH 1P• Bw HH JP HH JP 691 71 521 51.3 <1455 3125 10/1114 1019/14 10/15/14 10/23/14 10/29/14 11/5/14 111131l4 JP JP JP 72 71 45 46 68.1 66.2 < 481 7/10114 7/17114 46 46 65.2 69.9 <' BW TS Bw TS Bw TS 1021 410 Bw DM Bw DM 68 66 1042 78 85 45 46 76.9 84.9 7/24/14 7129114 DM HH 51 53 46.3 46.9 <1417 SE JP SE JP SE JP < < 432 410 HH BW HH Bw 68 70 1556 642 75 78 47 49 70.4 72.9 8112/14 8121114 Bw DM 51 51 55.3 46.4 < SE DM SE DM SE DM 520 1819 DM DM 66 455 72 52 57.8 G.M. 720.038 G.M. 616.2013 MIN. 1 1 66 46 46.31 417 MIN. I 71 45 57.81 410 MAX. I 71 53 65.2 3125 MAX. j 85 52 84.91 1819 4VER. I 1 68.3 50 53 956 AVER. 1 1 75.9 47.1 70.9 727.5714 % VSR CALCULATION: PRIM. %VS--DIG.%VS X 100 MUST BE AT LEAST 38% PRIM. %VS-- ((PRIM. VS X DIG. VS)/100) DIG. #2 FECAL MUST BE BELOW 2,000,000 j 7 SAMPLES (MINIMUM) REQUIRED PER QUARTER Agricultural Lime Application Log Year: 2014 Project: Roanoke Rapids Field . (state -county -site -field) Soil I pH J1 Lime Requirement (from soil analysis) Tons/Acre Applied Date Applied HX-13-12 5.5 0.8 HX-13-13 5.9 0.0 HX-13-14 5.7 0.4 NO-5-1 B 7.5 0.0 N/A NO-12-1 7.3 0.0 N/A NO-12-2 7.4 0.0 N/A NO-21-20 6.9 0.0 N/A NO-21-21 7.1 0.0 N/A NO-21-31 7.0 0.0 N/A NO-21-35 6.5 0.0 N/A NO-21-38 7.0 0.0 N/A *Lime applied via Bio-Soilds NCDA&CS Hyrv-,+omic Division Phone: (919) 733-2655 Website: www.r.--,i..gov/agronomi/ 1uru�r; Client: Quinten (Jr) Gregory 1521 Grapevine Rd. Predictive p Halifax, NC 27839 Mehlich-3 Extraction -'l Soil Report Sampled County :Halifax ReportNo. FYI _, _ 006382 Advisor: Synagro ATTN: Will Varner 2828 Tryon Rd /284 Boger Rd Raleigh, NC 27603 Sampled: 09/23/2014 Received: 09/23/2014 Completed: 10/02/2014 Farm: HX-13 Links to Helpful Information Sample ID: 12 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.8 120-200 0 70 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/crrt3; CEC and Na in meq/100 crrr3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.32 1.12 4.9 66 1.7 5.5 267 34 51 12 28 138 100 341 341 130 0.0 Sample ID: 13 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/cO; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.00 9.7 84 1.5 5.9 314 86 61 19 40 115 86 544 544 173 0.1 1 Aorth'Carollna ,a TobaccaTLsz fwrl coanwisslora Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS i"y: N1omic Division Phone: (919) 733-2665 Website: www Report No. FY Quinten (Jr) Gregory Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for, the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5'ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncadr.pov/apronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values' [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/aaronomi/uvrst.htm for more information. Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index, for crop 2 Mn-1 manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index W/V weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS _!J.u.iomic Division Phone: (919) 733-2656 Website: www.r�_-&::gov/agronomi/ tceporr NO. r rr 1:1_ f i-5064L �rrur:. Client: Quinten (Jr) Gregory Advisor: Synagro ATTN: Will u 1521 Grapevine Rd. Varner Predictive Halifax, NC 27839 2828 Tryon Rd t x! ,- •. Report /284 Boger RdMehlich-3 Extraction Sampled County: Halifax Raleigh, NC 27603 NVIII., Sampled: Received: 06/25/2014 Completed: 07/03/2014 Farm: HX-13 Links to Helpful Information Sample ID: 14 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu - B Information Lime History: 1-Soybean 0.4 0 0 20 0 0 0 0 0 0 Note: 3 2 - $pH Test Results [units - W/V in g/crrP; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 1.15 6.7 80 1.3 5.7 145 68 57 19 73 74 54 416 416 201 0.0 V.North'CaroIina 'fcit��e:�7"euat Fur6tl:�+riniss(�an. Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS i '...v7omic Division Phone: (919) 733-2655 Website: www.n _ _ _gov/agronomil Report No. FY1_. Quinten (Jr) Gregory Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-1, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-1, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm for more information. Page 2 of 2 Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-A11 Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index W1V weight per volume Zn-AI zinc availability index Zn-I zinc index NCDA&CS _ =nomic Division Phone: (919) 733-2655 �ru�ruxr; Predictive 2t Soil Report k�C.truyi 5� Website: www.l___;,=.gov/agronomi/ Client: Howard Ferguson 1334 Beef Rd Emporia, VA 23847 Mehlich-3 Extraction Sampled County: Northampton Report No. FY`— ._-019571 Advisor: Synagro ATTN: Will Varner 2828 Tryon Rd /284 Boger Rd Raleigh, NC 27603 Sampled: 11/20/2014 Received: 11/21/2014 , Completed: 01/12/2015 Farm: NO-5 Links to Helpful Information Sample ID: 1 B Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 70 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.18 1.13 9.8 100 0.0 7.5 168 33 91 8 38 113 62 234 234 122 0.1 1 North Carolina '%Uacco Taut rwid comillbsion Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS _.comic Division Phone: (919) 733-2655 Website: www.r.__._.gov/agronomi/ Report No. FYI D19571 Howard Ferguson Page 2 of 2 I Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based. on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncaar.aov/agronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results Report Abbreviations Ac B BS% Ca% CEC Cu-1 ESP HM% K-1 K20 Mg% MIN Mn Mn-AI1 Mn-Al2 Mn-1 M-O N Na NO3-N O RG pH P-1 P206 S-1 SS-1 W/V The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI remaining 16 P-I K-I Ca% M % Mn-1Mn-All, Mn-AI2 Zn-I Zn-AI Cu-I, S-I, SS -I, Na ESP, SS -I, NO3-N (not Zn-I routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncapr.ciov/aaronomi/uvrsthtm for more information. exchangeable acidity boron • CEC occupied by basic cations • CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index mineral -organic soil class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index NCDA&CS , comic Division Phone: (919) 733-2655 Website: WWW.r _ gov/agronomi/ Report No. FYI 338344 Predictive Client: Howard Ferguson 1334 Beef Rd Advisor: Synagro ATTN: Will Varner ti Soil Report Mehlich-3 Extraction Emporia, VA 23847 Sampled County :Northampton 2828 Tryon Rd /284 Boger Rd Raleigh, NC 27603 Sampled: Received: 06/25/2014 Completed: 07/03/2014 Farm: NO-12 Links to Helpful Information Sample ID: 1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 0 80 0 0 pH$ 0 0 0 Note: 12 Note: 2 - $pH Test Results [units - WN in gled; CEC and Na in meq/100 crrr3; NO3-N in mgldd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.22 1.04 18.6 99 0.1 7.3 315 29 92 6 54 84 47 574 574 217 0.0 Sample ID: 2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P206 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, 1 0.0 120-200 0 60 0 0 pH$ 0 0 0 Note: 12 Note: 2 - $pH Test Results [units - WN in glcrrP; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.32 1.04 23.1 100 0.0 7.4 299 41 94 5 80 101 56 626 626 214 0.0 v,,-North Carolina Tobacco Trust Fund comIsIhMou Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS ,u.„ iomic Division Phone: (919) 733-2656 Website: www.n_-,..gov/agronomi/ Report No. FY1 . __)38344 Howard Ferguson Page 2 of 2 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You. can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft . If you cannot find the exact fertilizer grade recommended on the report, visit www.ncagrgov/apronomi/6bpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fer Test Results The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P,-I, K-I, Ca%, Mg%, Mn-1, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagrgov/agronomi/uvrsthtm for more information. Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K20 potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Mn-1 manganese index M-0 mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS-1 soluble salt index WIV weight per volume Zn-AI zinc availability index Zn-I zinc index A r� Page 1 of 1 Report Number: 15-029-0594 Account Number:46485 wlNwaleastemxom Send To: SYNAGRO CENTRAL/ROANOKE RAPID MARSHALL PURYEAR 284 BOGER RD STE 204 MOCKSVILLE NC 27889 ..1. AA lnrl/Ol1A G n_Le nF An 1 .;.. n'i nnnn'I ri A_&L Eastern Laboratories 7621_Whitepine Road Rlchmond,Virginia 23237 (804j743-9401 Fax (804) 271.6446 Grower: ROD HOWELL SOIL ANALYSIS REPORT nano of Rannrf, n1/nn/gn15 Submitted By: WILL VARNER Farm ID: NO-21 Analytical Method(s): Mehlich 3 Organic Matter- Phosphorus Potassium 'Magnesium Calcium Sodium pH Acidity C.E.0 ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Sample ID Lab Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index megl100g megl100g, NO-21-20 67 H 71 M 73 M 642 H 13 VL 6.9 0.1 4.1 13217 1.6 L 76 NC=56 NC=36 NO-21-21 61 H 69 M M 591 H 13 VL 7.1 0.0 3.6 13218 1.3 L 71 146 NC=51 NC=35 NO-21-31 VH 82 L 70 M 993 ' VH 14 VL7.0 0.0 5.8 13220 2.0 L 82 1133C' N=111 NC=42 NO-21-35 61 H 90 M L 572 H 112 VL 6.5 0.3 3.8 13221 1.3 L 71 144 NC=51 NC=46 NO-21-38 75 H M M 792 H VL 7.0 0.0 4.9 13222 1.7 L 77 184 178 1 112 NC=62 NC=43 Percent Base Saturation Nitrate Sulfur, Zinc Manganese Iron' Copper Boron Soluble Salts Chloride, Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS CI AI Field ID % % % % % PP m Rate PP rn Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate ms/cm Rate PP m Rate PP m NO-21-20 7 VL 2.3 M 12 M 104 VH 1.7 H 0.4 L 0.06' VL 4.4 14.8 78.3 1.4 1.4 NC=15 NC=57.5 NC=75 NC=85.0 NO-21-21 8 VL 1.6 L 9 L 83 VH 1.4 M 0.2 VL 0.06 VL 4.9 10.6 82.1 1.6 0.0 NC=17 NC=40.0 NC=56 NC=70.0 NO-21-31 12 L M M 241 VH VH 0.5 L VL 3.6 10.1 85.6 1.0 0.0 13.4 NC=25 NC=85.0 115 NC=94 13.5 NC=175.0 10.07 NO-21-35 10 L L 6 L 96 VH 1.7 H L VL 6.1 9.6 75.3 1.4 7.4 12.0 NC=21 NC=50.0 NC=38 NC=85.0 10.4 10.04 NO-21-38 9 VL L 8 L VH H 0.4 L 0.07 VL 4.4 13.3 80.8 1.1 0.0 11.9 NC = 19 NC = 47.5 NC = 50 1121 12.6 NC = 130.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retainea a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: Pwia or 60wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble ,analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary