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HomeMy WebLinkAboutWQ0001953_Residual Annual Report 2014_20150209Town of Spindale Town of Spindale, NC 2014 Annual Report Land Application Program NC Permit No. WQ0001953 F?ECEIVED FEB 0 9 2015 INFO ION PROCESR SECTION NATIOSING UNIT Vr- A' uz, R M 1. t A1r l� U AL ,u�r 1V L AYY.I.,,il;A i ivir Uhx jL iiu iuA ntyiV jv vKlvi WQ Permit#: ' WQ0001953 County: Rutherford Year: 2014 Facility Name (as shown on permit): Town of Spindale Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909 Land application of residuals as allowed by the permit occurred during the past calendar year? ® Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 1 6 Total number of fields utilized for land application during the year: 4 Total amount of dry tons applied during the year for all application sites: 73.39 Total number of acres utilizes for land application during the year: 42.5 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. EJ Yes ® No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to. 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part . 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Name and Title (type or rint) Signature of Permittee Date / OZ a3 .S_ l .-ram: 2n Signature of Preparer* Date Sigildiure of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC; 02T. 1102 (26) nFNR FnRM ArF (19/9nns) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001953 Facility Name: Town of Spindale Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data WQ0001953 Town of Spindale, NC Laboratory: 1) 2) 3) 4) 5) A&L Eastern Labs Parameter (mg/kg) Conc. Limit m /k a Sample or Composite Date 6-19-14 Percent Solids (%) NA 4.23 Arsenic 75 3 Cadmium 85 3 Copper 4,300 1850 C'hrnminm NA J 77 Lead 840 69 Mercury 57 2 Molybdenum 75 10 Nickel 420 279 Selenium 100 38 Zinc 7,500 1780 Total Phosphorus NA 16900 TKN NA 48200 Ammonia -Nitrogen NA 7570 Nitrate and Nitrite NA 1 37.8 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 02 e) s Date f�a *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) tVl\lINVIV•,IVI 19"La r11',LL I..VA JuNki z.'0VIVllVXAKY VVAIV1'- Attach this form to the corresponding Field Loading; Summary Form to be submitted in Annual Report Facility Name: Town of Spindale I Total Dry Tons Applied (Annual): 41.28 Permit #: WQ0001953 Cation Exchange Capacity (non 503 only): Operator: Acres Used: Mark Koone Owner: Mark Koone Predominant Soil Series: PaC2 17.1 Acres Permitted: 17.1 Site #: SP06 Field #: Residual Analysis Data (Heavy Metals and Total Ph,os horus use mg/kg, % Solids use Raw Percent # Com- posite MENEM VAN TotalDate • " .•�� I Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total L1J 21 3 j4 5 6 7 8 9 10 11 12 DT/Ac./ c App. Event 2.41 14 Arsenic 0.014 0.000 0:000 0.000 0.006 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.014 Cadmium 0.014 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 8.932 0.000 0.000 0.000 0.000 0.0001 0.000 0.000 0.000 0.000 0.000 0.000 8.932 Chromium 1.096 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1.096 Lead 0.333 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.333 Mercury 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Molyb- denum 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Nickel 1.347 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 1.347 Selenium 0.183 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.183 Zinc 8.594 0.000 0.000 0.000 0.000 0.000 0.000 , 0.000 0.000 0.000 0.000 0.000 8.594 Total Phos- 81.593 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 81.593 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signa,Pdre of Land Applier ( -I9-o- Date DENR FORM MFLSF (1212006) AlIN 114 U L-]L 1VM I l • ,o V 1L' LiJ L V'AVjLLV lT 3 U 1V1LVIA-K Y r Vl(1Vl " Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility -Name: Town of Spindale Total Dry Tons Applied (Annual): 17.20 Permit #: WQ0001953 Cation ]Exchange Capacity (non 503 only): Operator: Mark Koone Owner: Mark Koone Predominant Soil Series: PaC2 Acres Used: 7.8 Acres Permitted: 7.8 Site #: SP06 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite D. - IM a a MEN 0 won Total Phos- .. .•�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total L_IJ 21 5 6 7 1 91 110111 12 DT/Ac./ _.§_j o App. Event 2.21 14 Arsenic 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 1 0.000 0.000 0.013 Cadmium 0.013 0.000 0.000 6.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 8.159' 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 8.159 Chromium 1.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.001 Lead 0.304 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.304 Mercury 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.044 m denu Nickel 1.230 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.230 Selenium 0.168 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.168 Zinc 7.850 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.850 Total Phos- 74.529 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 74.529 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting; false information, including the possibility of fines and imprisonment for knowing violations". ��lw-rr Sign ture of Laad <pplier Date DENR FORM MFLSF (12/2006) Lill1\ U L-1L lViG 1 lvjuc V lL' LlJ ib"A MILLI V iJ U 1V11V1E1K Y V VnIVl Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Spindale Total Dry Tons Applied (Annual): WQ0001953 Cation Exchange Capacity (non 503 only): Mark Koone 2.4 Owner: Mark Koone Acres Permitted: 2.4 Site #: 2.29 Predominant Soil Series: PaC2 SP06 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite DateKom Total Phos- phorus .'�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total L1J L2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ o App. Event 0.96 14 Arsenic 0.006 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.006 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 3.534 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.534 Chromium 0.434 0.000 0.000 0.00.0 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.434 Lead 0.132 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.132 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.004 Molyb- 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 0.000 0.000 0.019 denum Nickel 0.533 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.533 Selenium 0.073 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.073 Zinc 3.400 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.400 Total Phos- 32.279 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.279 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". f'%,: %/y Signature of Land Applier l-o-iS- Date DENR FORM MFLSF (12/2006) A.N1VUAL 1VMlAJ.,.N V*ILLV LV,WJlr(i lU1V11VJAKY rYICVl''- Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Torun of Spindale Total Dry Tons Applied (Annual): 12.62 Permit #: WQ0001953 Cation Exchange Capacity (non 503 only): Operator: Mark Koone Owner: Mark Koone Acres Used: 15.2 Acres Permitted: 15.2 Site #: Predominant Soil Series: PaD2 SP06 Field #: 5 Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): positeI Wim7mov Com- Date MIE TotalW. Phos- phorus .•�� Annual Heave Metal Field Loadings (Calculated in lbs/acre): Total 1 2j 3 41 5 6 j 7 __§.i 91 LOJ 111 12 H DT/Ac./ c App. y Event 0.83 ?! Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.005 Cadmium 0.005 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Copper 3.071 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.071 Chromium 0.377 0.000 0.000 0.000 0.000 0.000 0.000 6.000 0.000 0.000 0.000 0.000 0.377 Lead 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.115 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 denum Nickel 0.463 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.463 Selenium 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Zinc 2.955 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.955 Total Phos- 28.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 28.054 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting; false information; including the possibility of fines and imprisonment for knowing violations".. Signature of Land pplier I',rl-15- Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Spindale WQ Permit #: WQ0001953 Field #: 1 Acres Utilized: 17.1 Land Owner: Mark Koone Annual Dry Tons Applied: 41.2755 Site #: SP06 Acres Permitted: 17.1 Operator: Mark Koone Predominant Soil Series: PaC2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: ° 0 o Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (N Q PDES #, W # Fert., Animal Waste etc ) Soil Cond. (Drys Wet, Moist) Precip. Past 24 Hrs. inches > b * 6 Z o %`� 5 4 7d cc w * r' TKN mg/kg Z o R 0. mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7-2014 1 234000 4.23 2.414 WQ0001953 dry 0 s 0.5 0.3 48200 7570 37.8 77.298 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 V•UUVv.uuu u.uuu 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 0 234000 _ As Cd Cu Cr Pb Hg Mo Ni Se Zn P 77.298 0.000 Lime Applied Annuallbs/acre 0.014 0.013 0.027 36 0.014 0.013 0.027 34 8.932 9.548 18.480 1338 1.096 1.033 2.129 NA 1 0.333 0.318 0.651 267 1 0.010 0.008 0.018 15 1 0.048 0.048 0.096 NA 1.347 1.487 2.834 374 1 0.183 0.205 0.388 89 8.594 7.543 16.137 3498 81.593 Date lbs/ac Prior Years Cumulative lbs/ac 12-14 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** 1 Permit PAN Limit lst/2nd Crop 158 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Spindale Land Owner: Mark Koone Operator: Mark Koone Crop 1 Name: Fescue WQ Permit #: WQ0001953 Field #: 1 Annual Dry Tons Applied: 41.2755 Site #: SP06 Predominant Soil Series: PaC2 Crop 1 Max. PAN: 158 Crop 2 Name: Acres Utilized: 17.1 Acres Permitted: 17.1 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° y o A Volume a lied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume A lied er PP P Acre D Tons/Ac ry ) _ Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. D (Dry, Wet, Moist) Precip. Past 24 Hrs. inches y 4 b 0 o' o o _. * o o qy �, � �' x ?: o o 91 ;u � � ., = * o' a TKN mg/kg Z t i o ° CD w mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7-1014 234000 4.23 2.414 WQ0001953 dry 0 s 0.5 1 0.3 48200 7570 1 37.8 77.298 NA Fescue 0.000 0.000 0.000 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.606 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp. ( attach FORM FSF supp to this form): '0TALS:1 01 234000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 77.298 0.000 Lime Applied knnual lbs/acre 0.014 0.013 0.027 36 1 0.014 0.013 0.027 34 8.932 9.548 18.480 1 1338 1 1.096 1.033 2.129 NA 0.333 0.318 0.651 267 0.010 0.008 0.018 15 0.048 0.048 0.096 NA 1 1.347 1.487 2.834 374 1 0.183 0.205 0.388 89 1 8.594 7.543 16.137 3498 81.593 Date lbs/ac 'rior Years Cumulative lbs/ac 12-14 1000 :urrent Cumulative lbs/ae 'ermitted C. P. L. R.**** 'ermit PAN Limit 1 st/2nd Crop 158 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly,gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier / %-/ S Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Spindale WQ Permit #: WQ0001953 Field #: 3 Acres Utilized: 7.8 Land Owner: Mark Koone Annual Dry Tons Applied: 17.1981 Site #: SP06 Acres Permitted: 7.8 Operator: Mark Koone Crop 1 Name: Fescue Predominant Soil Series: PaC2 Crop I Max. PAN: 158 Cation Exchange Capacity (non 503): Crop 2 Name: Crop 2 Max. PAN: �, o Q 0 Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. W Moist) Precip. Past 24 Hrs. inches Y c� a a o o w w r. tZ E: 7y � w �, * �3 TKN mg/kg Z o mg/kg Nitrate and Nitrite mg/kg PAN Applied PP Ibs/acre ( ) Name of CropType � Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 7-2014 97500 4.23 2.205 WQ0001953 dry 0 s 0.5 0.3 48200 7570 37.8 70.608 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0o0 0.000 El Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'oTALs: 0 97500 As Cd Cu Cr Pb H Mo Ni Se Zn P 70.608 o.000 Lime AEplied knnuallbs/acre 0.013 0.013 8.159 1.001 0.304 0.009 0.044 1.230 0.168 7.850 74.529 Date lbs/ac 'rior Years Cumulative lbs/ac 0.012 0.025 36 0.012 0.025 34 8.169 16.328 1338 0.892 1.893 NA 0.272 0.576 267 0.006 0.015 15 0.041 0.085 NA 1.286 2.516 374 1 0.168 0.336 89 1 6.437 14.287 3498 12-14 1000 .urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit 1st/2nd Crop _ 158 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations." JJ *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, InjectionAncorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE.COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE Facility Name: Town of Spindale WQ Permit #• WQ0001953 Field #: 4 Acres Utilized: 2.4 Land Owner: Mark Koone Annual Dry Tons Applied: 2.2931 Site #: SP06 Acres Permitted: 2.4 Operator: Mark Koone Predominant Soil Series: PaC2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: o a; o(enter A Volume applied one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per pP � P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Wasteetc) , Soil Cond. (Dry, Wet, Moist) 7-2014 13000 4.23 0.955 WQ0001953 dry 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 170TAL&I 01 1 4 mtual lbs/acre ?rior Years Cumulative Ibs/ac Iurrent Cumulative lbs/ac ?ermitted C. P. L. R.**** 'ermit PAN Limit 1 As Residuals Cd Applic Cu 0.006 0.006 3.534 0.005 0.005. 3.898 0.011 0.011 7.432 36 34 1338 Precip. y o4.0 z Nitrate Past 24 �' '» F " a TKN o and Hrs. 0 * *L� � w• Nitrite inches 0 mg/kg mg/kg mg/kg 0 s 0.5 0.3 48200 7570 T 37.8 tions totals Cr on FORM Pb FSF Hg 0.434 0.132 0.004 0.422 0.13 0.003 0.856 0.262 0.007 NA 1 267 15 PAN Applied ( Ibs/acre) Crop 1 Crop 2 30.597 NA 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.060 0.000 Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Fescue ipp ( attach Mo FORM Ni FSF supp I Se to this Zn form): P 30.597 0.000 32.279 _ Lime Applied Date lbs/ac 0:019 0.533 0.073 3.400 3.306 6.706 3498 0.021 0.666 0.085 12-14 1000 0.040 1.199 0.158 NA 374 89 _ _ _ . `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations.,, *Application Method: S - Surface, IN - Injection, INC - Incorporation J�d 4 is **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature. of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0:2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Town of Spindale WQ Permit #• W 0001953 Field #• 5 15.2 ' Q Acres Utilized: Land Owner: Mark Koone Annual Dry Tons Applied: 12.6120 Site #: SP06 Acres Permitted: 15.2 Operator: Mark Koone Predominant Soil Series: paD2 Cation Exchange Capacity (non 503)• Crop 1 Name: Fescue Crop 1 Max. PAN: 139 Crop 2 Name: Crop 2 Max. PAN: ° ° A 0 7-2014 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons 71500 % Solids 4.23 Volume A lied er PP P Acre (Dry Tons/Ac) 0.830 Residual Sources (NPDES #, WQ#, Fert., Animal Waste etc) WQ0001953 Soil Cond. (Dry, We Moist) dry Precip. Past 24 Hrs. inches 0 y 410 -- o m °' �''. ^� s o w _ 0.5 w :; # w * 0.3 TKN mg/kg 48200 Z o vo 0 w mg/kg Nitrate and Nitrite mg/kg 1 7570 37.8 0.000 0.000 0.000 0.000 0.000 0.000 0.000 v.ovv 0.000 r0.0 00 0.000 roT !S: 0 71500 - Annuallbs/acre 'rior Years Cumulative lbs/ac �urrent Cumulative lbs/ac ?ermitted C. P. L. R.**** 'ermit PAN Limit 1st/2nd Crop As 0.005 0.005 0.010 36 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): Cd I Cu Cr Pb Ha Mo I Ni Se_ Zn P 0.005 3.071 0.377 0.115 0.003 0.017 0.463 0.063 2.955 28.054 0.005 3.127 0.347 0.104 0.002 0.016 0.501 0.06 2.455 0.010 6.198 0.724 0.219 0.005 0.033 .0.964 0.123 5.410 34 1338 1 NA 267 1 15 1 NA 374 89 3498 PAN Applied (lbs/acre) Crop 1 26.571 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 26.571 Crop 2 NA 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Name of Crop Type Receiving.Residual Application Crop 1 Crop 2 Fescue 0.000 1 Lime 1 12-14 1 1000 1 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land APplier Date *** Mineralization Rates: Compost -0.1, anaerobiall digested -0.2 , aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Page: 1 of 2 Report Number: 14-174-0201 Account Number: 46381 Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 Lab Number: 56047 Sample Id : SPINDALE A&L Eastern Laboratories, Inc. 7621 Whitepine*Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastem.com Project: SPINDALE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/19/2014 13:15:00 Date Received: 06/23/2014 00:00 Date Reported: 06/26/2014 Total Solids * 4.23 42300 100.0 JM 06/23/2014 13:30 SM-2540G Moisture' 95.77 100.0 JM 06/23/201413:30 SM-2540G Total Kjeldahl Nitrogen 4.82 48200 10.0 JM 06/24/2014 08:44 SM-4500-NH3C-TKN Total Phosphorus 1.69 16900 100 KM 06/24/2014 15:02 SW 6010C Totai Potassium 0.30 2960 100 KM 06i24i2U14 15:02 SW 6010C Total Sulfur 1.67 16700 100 KM 06/24/2014 15:02 SW 6010C Total Calcium 1.61 16100 100 KM 06/24/2014 15:02 SW 6010C Total Magnesium 0.30 3040 100 KM 06/24/2014 15:02 SW 6010C Total Sodium 0.52 5240 100 KM 06/24/2014 15:02 SW 6010C Total Iron 18700 100 KM 06/24/2014 15:02 SW 6010C Total Aluminum 25000 100 KM 06/24/2014 15:02 SW 6010C Total Manganese 344 5 KM 06/24/2014 15:02 SW 6010C Total Copper 1850 5 KM 06/24/2014 15:02 SW 6010C Total Zinc 1780 5 KM 06/24/2014 15:02 SW 6010C Ammonia Nitrogen 0.76 7570 10.0 JM 06/24/2014 08:44 SM-4500-NI3C Organic N 4.06 40630 10.0 06/24/2014 08:44 CALCULATION Nitrate+Nitrite-N 37.8 2.00 JM 06/24/2014 08:45 SM450ONO3F Total Cadmium 3.0 2.0 KM 06/24/2014 15:02 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced n whole or part, nor may any reference be made to the work. the results. or the company in, any advertising, news release, or other public announcements witrouut obtaining out prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-174-0201 Account Number: 46381 Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 �L A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastem.com Project: SPINDALE NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/19/2014 13:15:00 Lab Number: 56047 Date Received: 06/23/2014 00:00 Sample Id : SPINDALE Date Reported: 06/26/2014 Total Chromium 227 5 KM 06/24/2014 15:02 SW 6010C Total Nickel 279 5 KM 06/24/2014 15:02 SW 6010C Total Lead 69 5 KM 06/24/2014 15:02 SW 6010C Total Arsenic 3.0 3.0 KM 06/24/2014 15.02 SW 6010C Total Mercury 2.0 0.4 KM 06/24/2014 12:00 SW-7471 B Total Selenium 38.0 5.0 KM 06/24/2014 15:02 SW 6010C pH (Standard Units) * 7.42 2.00 JM 06/24/2014 08:44 SW-9045D Total Molybdenum 10 5 KM 06/24/2014 15:02 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and !eaters are for the exclusive and confidential use of our clients. and may not be reproduced in v✓ro,e or part, nor may any reference be, made to the work., the ; esults or the company ir: any advertising, newvs release. or otherpubiic announcements r ithout obtaining our prior wrtten authorization. Debbie Holt SAR Sodium Absorption Ratio PLa(Mq�. Ca(Mg/L) IVIcM /L Na: Sodium (Mg/L) Equivalent weight: 23 E221.652 681.03 128.59 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 N IUIE Ca I'VIE. Mg (ME) 1 9.637043 34.0515 10.7'1583 Milli Equivalent = Mg/L / Equivalent weight The amour amount of c SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power Permitting l SAR = 2.03694 (1=rorn Mg/L entered above) SAR= 2.035618 (From ME entered below) Na (ME) 1 Ca (ME). 1 MgJMEJ 9.63 34.05 10.71 PAN Mineralization as decimal Jj2t�ald tons/dear jAcres Appli don 1 42.5 Rate 0.3 TkN 48200 -NH3 7570 NO3 37.8 NO2 0 % Solids 0.0423 1 73.39 PAN Surface 16011.8 1 mgikg 32.0236 lbs/dry ton 2350.212llbs total PAN 55.299111Ibs PAN/acre PAN Injection 19796.31mg/kg 39.5936 lbs/dry ton 2905.774 1 Ibs total PAN 68.371161lbs PAS!/acre Dry Tons/1000 gal. 0.176391 ist year PAN Surface lbs. F-72-375-0212004 1st year PAN Injected Ibs. 2905.774304 ibs./acre Surface 55.29910598 Ibs./acre Injected 10009 MR(TKN-NH3)+ +.5(NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton 1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal." 2000 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 2.8669 Entered 6/19/2014 Reported: 6/24/2014 For: Spindale Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 140619-19.1 % Solids 1 4.53 % SM2540B-1997 6/20/14 CL 140619-19.1 Fecal Coliform MTF 1 <442 MPN/g SM92210E-2006 6/20/14 CL 140619-19.1 Geometric Mean 1 705 MPN/g dry wt. basis 6/23/14 CL 140619-19.2 % Solids 2 4.53 % SM2540B-1997 6/20114 CL 140619-19.2 Fecal Coliform MTF 2 883 MPN/g SM9221 CE-2006 6/20/14 CL 140619-19.3 % Solids 3 4.35 % SM254OB-1997 6/20/14 CL 140619-19.3 Fecal Coliform MTF 3 1379 MPN/g SM9221 CE-2006 6/20/14 CL 140619-19.4 % Solids 4 4.49 % SM254OB-1997 6/20/14 CL 140619-19.4 Fecal Coliform MTF 4 891 MPN/g SM92210E-2006 6/20/14 CL 140619-19.5 % Solids 5 4.57 % SM2540B-1997 6/20/14 CL 140619-19.5 Fecal Coliform MTF 5 875 MPN/g SM92210E-2006 6/20/14 CL 140619-19.6 % Solids 6 4.47 % SM2540B-1997 6/20/14 CL 140619-19.6 Fecal Coliform MTF 6 <447 MPN/g SM9221 CE-2006 6/20/14 CL 140619-19.7 % Solids 7 4.32 % SM2540B-1997 6/20/14 CL 140619-19.7 Fecal Coliform MTF 7 <463 MPN/g SM9221 CE-2006 6/20/14 CL P.O, Box 228 9 Statesville, North Carolina 28687 • 704/872/4697 Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 6/19/2014 Reported: 6/24/2014 For: Sample ID Parameter Gust ID Result Units Method Respectfully submitted, 'a"-/ - Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 Date Analyzed Analyst P.O. Box 228 9 Statesville, North Carolina 28687 • 704/872/4697 Analytical Results Southern Soil Builders 958 Hoots Rd. Roaring River, NC 28669 Entered: 7/11/2014 Reported:8/12/2014 Sample ID: 140711-11 For: Spindale PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day) Total Solids Volatile Solids % Volatile Solids Week 1 1.47 0.97 0.6599 Week 2 1.47 0.98 0.6667 Week 3 1.46 0.97 0.6635 Week 4 1.47 0.98 0.6659 Week 5 1.32 0.86 0.6532 Volatile Solids Reduction: 0.6599 - 0.6532 X 100 = 2.93 % 0.6599 - (0.65991 X 0.6532) Respectfully submitted, J Dena Myers Statesville Analytical, Inc. NC WW Cert.# 440NC DW Cert. #37755 P.O. Box 228 ® Statesville, North Carolina 28687 ® 704/872/4697 Client: STATESVILLE ANALYTICAL IZZ Court Street - P.O. Box 228 Statesville, NC 28687 (704) 872-4697 �. W-WA 0 Address: L& 4, Aj C Contact Person: Phone # ZY_ct 9-"'_� ?I k - q q 1 FAXO 0 Chain of Custody Record PO # U Requisitioned by: (Time Date) Customer Sample fD# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only) Matrix Parameters requested for analysis Sf.dg.1 W IWW C, Relinquished by: Receivedby: Relinquished by: Received by: Composite Sampling Time begin- Time end Composite Sampling Time begin- Time end X/ ^ AV #1: am, pm Date am, pm Date #2: am, pm Date am, pm Date Time s15 Time '2 Time Time Lab Comments: am, 1(PM_­­,Date U / am, pi rU Date am, pm Date am, pm Date Sampled by: 11 Transported by: 7- Holding times met: Compliance work: Non-compliance work: n Condition of Receipt Sample ID 140711-11 Client Southern Soil Builders Temp on Arrival 2 pH upon Arrival Parameter Schedule El El Bench :10 Day HNO;; ❑ Chemicals in containers, client HCI W Chemicals upon receipt NaOIi FV] Received on Ice H2SCI ❑ Samples chilled upon receipt Na2S O ❑ Chemicals in containers, lab Dechlorinated Page 1 of 1 1, 1 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 6/19/2014 Reported: 8/20/2014 For: Spindale Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 140619-21 Corrosivity Spindale See Attached SW-846 07/07/14 PACE 140619-21 Ignitability Spindale See Attached 1010M 07/07/14 PACE 140619-21 Reactivity Spindale See Attached SW-846 07/07/14 PACE 140619-21 TCLP Spindale See Attached 1311 07/07/14 PACE Respectfully submitted, C"Jn- 011/�� Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 M P.O, Box 228 9 Statesville, North Carolina 28687. 704/872/4697 Client: S6 : sr SB `) /-�v tCir P rf �` -' Address: 1 -1 "`'1 STATESVILLE ANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 28687 (704) 872-4697 Chain of Custody record Contact Person: Phone # 3 J 6 e� s �- '78"7 ( Fes# 3 3� 4J p Y o r PO # j Requisitioned b : (Time Date q v ) Customer Sample ID# Lab -ID # Time Sampled Grab Only) ( y) Date Sampled (Grab Only) a d Matrix ISludgalw I ww �0-4-(C I �C!(Ci�` ?! /, 1 D Tit' (�-�� J�t7 }� 7e LYE �.c a Relinquished by: Received by: Relinquished by: � �- %� ^ Time J = S C am, .�m2Date Time `S am<ym Date / Time am, pm Date / / Sampled by: ate:/ Transported by: Holding times met: Received by: Composite Sampling #1 Time am, pm Date / / Compliance work: Time begin am, pm Date _/ / Non-compliance work: Time end am, pm Date / / Lab Comments: Composite Sampling #2- Time begin am, pm Date Time end am, pm Date / / t 4 a Condition of Receipt Sample ID 140619-21 Client Southern Soil Builders Temp on Arrival 6 pH upon Arrival Parameter Schedule TCLP ❑ HNO3 ❑ HCl ❑ NaOH ❑ H2SO ❑ Na2S2O ❑ Dechlorinated ❑ Chemicals in containers, client ❑ Chemicals upon receipt V Received on Ice ❑ Samples chilled upon receipt ❑ Chemicals in containers, lab Page 1 of 1 aceAnalytical www.pacelabs.corn I ANALYTICAL RESULTS Project: 140619 Pace Project No.: 92206260 Pace Analytical Services, Inc. 9800 KlnceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 140619-21 Lab ID: 92206260001 Collected: 06/20/14 13:10 Received: 06/20/14 14:21 Matrix: Solid Results reported on a "dry -weight" basis Parameters 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury 8270 MSSV TCLP Sep Funnel 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3-butadiene Hexachiorobenzene Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methyl phenoI(m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichiorophenol 2,4,6-Trichlorophenol Date: 07/10/2014 04:48 PM Results Units , Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 06/20/14 21:00 ND ug/ I 1 0.50 1 06/24/14 10:23 06/29/14 14:00 58-89-9 ND ug/ d 3.0 1 06/24/14 10:23 06/29/14 14:00 57-74-9 ND ug/ 0.50 1 06/24/14 10:23 06/29/14 14:00 72-20-8 ND ug/L 1 0.50 1 06/24/14 10:23 06/29/14 14:00 1024-57-3 ND ug/ ND ug/111 1000 1 3.0 06/24/14 10:23 06/29/14 14:00 72-43-5 1 06/24/14 10:23 06/29/14 14:00 8001-35-2 72 % i 10-138 1 06/24/14 10:23 06/29/14 14:00 2051-24-3 41 % 1 10-110 1 06/24/14 10:23 06/29/14 14:00 877-09-8 Analytical Methid: EPA 8151 Preparation Method: EPA 3510 ND mg/L 0.010 1 06/26/14 07:30 06/27/14 09:08 94-75-7 ND mg/L 0.010 1 06/26/14 07:30 06/27/14 09:08 93-72-1 94 % 42-142 1 06/26/14 07:30 06/27/14 09:08 19719-28-9 Analytical ry Leachate M ND ND ND ND ND ND ND Analytical M Leachate M ND Analytical M Leachate M EPA 6010 Preparation Method: EPA 3010 )ate: EPA 1311; 06/23/14 15:45 0.050 1 06/24/14 11:40 06/24/14 22:40 7440-38-2 0.25 1 06/24/14 11:40 06/24/14 22:40 7440-39-3 0.0050 1 06/24/14 11:40 06/24/14 22:40 7440-43-9 0.025 1 06/24/14 11:40 06/24/14 22:40 7440-47-3 0.025 1 06/24/14 11:40 06/24/14 22:40 7439-92-1 0.10 1 06/24/14 11:40 06/24/14 22:40 7782-49-2 0,025 1 06/24/14 11:40 06/24/14 22:40 7440-22-4 EPA 7470 Preparation Method: EPA 7470 )ate: EPA 1311; O6/23/14 15:45 0.20 1 06/24/1412:15 06/24/1417:36 7439-97-6 EPA 8270 Preparation Method: EPA 3510 )ate: EPA 1311; 06/20/14 21:00 ND ug/12, 50.0 1 06/2411410:08 06/25/14 14:13 106-46-7 ND ug/L� ND 50.0 1 06/24/14 10:08 06/25/14 14:13 121-14-2 ug/L1 50.0 1 06/24/14 10:08 06125/1414:13 87-68-3 ND ug/L 50.0 1 06/24/14 10:08 06/25/14 14:13 118-74-1 ND ug/L, 50.0 1 06/24/14 10:08 06/25/14 14:13 67-72-1 ND ug/L1 ND 50.0 1 06/24/14 10:08 06/25/14 14:13 95-48-7 ug/L 50.0 1 06/24/14 10:08 06/25/14 14:13 ND ug/L' 50.0 1 06/24/14 10:08 06/25/14 14:13 98-95-3 ND ug/L 100 1 06/24/14 10:08 06125/1414:13 87-86-5 ND ug/1-1 50.0 1 06/24/14 10:08 06/25/14 14:13 110-86-1 ND ug/L 50.0 1 06/24/14 10:08 06/2511414:13 95-95-4 ND ug/L 50.0 1 06/24/14 10:08 06/25/14 14:13 88-06-2 i REPiORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without1the written consent of Face Analytical Services, Inc.. Page 4 of 21 P 4 i aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project; 140619 Pace Project No.: 92206260 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 140619-21 Lab ID: 92206260001 Collected: 06/20/14 13:10 Received: 06/20/14 14:21 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 0(3/20/14 21:00 Surrogates Nitrobenzene-d5 (S) 32 % 12-102 1 06/24/14 10:08 06/26/14 14:13 4165-60-0 2-Fluorobiphenyl (S) 28 % 13-107 1 06/24/14 10:08 06/25/14 14:13 321-60-8 Terphenyl-04 (S) 65 % 21-132 1 06/24/14 10:08 06/25/14 14:13 1718-51-0 Phenol-d6 (S) 11 % 10-110 1 06/24/14 10:08 06/25/14 14;13 13127-88-3 2-Fluorophenol (S) 16 % 10-110 1 06/24/14 10:08 06/25/14 14:13 367-12-4 2,4,6-Tribromophenol (S) 43 % 27-108 1 06/24/14 10:08 06/25/14 14:13 118-79-6 8260 MSV TCLP Analytical Method: EPA8260 Leachate Method/Date: EPA 1311; 06/24/14 12:58 Benzene ND ug/L 5.0 1 07/03/14 15:55 71-43-2 2-Butanone (MEK) 198 ug/L 10.0 1 07/03/14 15:55 78-93-3 Carbon tetrachloride ND ug/L 5.0 1 07/03/14 15:55 56-23-5 Chlorobenzene ND ug/L 5.0 1 07103/1415:55 108-90-7 Chloroform ND ug/L 5.0 1 07/03/14 15:55 67-66-3 1,4-Dichlorobenzene ND ug/L 5.0 1 07/03/14 15:55 106-46-7 1,2-Dichloroethane ND ug/L 5.0 1 07/03/14 15:55 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1 07103/1415:55 75-35-4 Tetrachloroethene ND ug/L 5.0 1 07/03/14 15:55 127-18-4 Trichloroethene ND ug/L 5.0 1 07/03/14 15:55 79-01-6 Vinyl chloride ND ug/L 5.0 1 07/03/14 15:55 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 07/03/14 15:56 17060-07-0 Toluene-d8 (S) 102 % 67-135 1 07/03/14 15:65 2037-26-5 4-Bromofluorobenzene (S) 96 % 70-130 1 07/03/14 15:55 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 96.1 % 0.10 1 07/07/14 15:53 1010 Flash point,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 07/09/14 10:30 9045 pH Soil Analytical Method: EPA9045 pH at 25 Degrees C 6.8 Sid. Units 0.10 1 06/23/14 17:58 733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 25.8 1 06/30/14 23:22 735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/kg 258 1 06/30/14 19:00 Date: 07/10/2014 04:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Face Analytical Services, Inc.. Page 5 of 21 4, } A1NV VUk' '1'VK A'1l 1'_KACTIVN REDUCTION FORM (02T Rules) Facility Name: Town of Spindale WQ Permit Number: WQ0001953 WWTP Name: Town of Spindale, WWTP NPDES Number: NC0020664 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please_ indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ® 1 Alt B (Alk Treatment) ® I Alt. C (Prior Testing) El A1t.D (No Prior Test) Process to Further Reduce Pathogengs If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 11 Heat Drying Ca Heat Treatment El Therm.ophilic Beta Ray ® Gamma Ray ® Pasteurization ....................................... Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens Il If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ® Composting ® Aerobic Digestion D Anaerobic a robrc Digestion strop C1 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number o Frequency Sample Analytical Parameter in Sludge Excee- of Anal y p Tech- g Minim Geo. Mean axim Units Ce Analysis Type nicue 2 x 10 to the NTN 442 705 1379 MPN/ 0 7 6th power g grab sm9221 c per gram of Fecal Coliform total solids CFU 1000 mpn per gram - ------- _T of total solid (dry Salmonella bacterial 3 NTN per 4 grams (in lieu of fecal total solid (dry Vector Attraction Reduction 05A NCAC 67T _11071 - Plnacn infla..a+o ai+o,..,.,+;.,,, ---.r .....,.a. Alt.l (VS reduction) ® Alt. 2 (40-day bench) ® ;Alt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) Ll Alt. 5 (14-Day Aerobic) ® Alt. 6 (Alk. Stabilization ® Alt 7 (Drying - Stable) ® Alt. 8 (Drying - Unstable) Alt. 9 (Injection) ® !'ITTT TTTT/^I 1 TT rr Alt. 10 (Incorporation) ® No vector attraction reduction alternatives were performed Il 11.'1v�a11V1I 1.71Cf1LlVll,l\ 1 spiv Nv lurzuK tue appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 115A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in' 15A NCAC 02T .1106 and the vector attraction reduction requirement in 115A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification, including fine and imprisonment." Zewle- W/ - Dennis Key Southern Soil Builders, Inc. Preparer Name arfA Title (type or p nt) 'Land Applier Name and Title (if applicable)(type or print) 1- I )-1 S Signature of Preparer* Date Signature of L Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nF=NP FCIPAA P\/PF n7T /1717nna\ NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006829 Client: Southern Soil Builders, Inc. Advisor: 1 Predictive •�Y 5 Sid 958 Hoots Rd .�.. : =. Roaring River, NC 28669 `,,,'k�`•d-~;ail Soil Report Mehlich-3 Extraction ... L;.> Sampled County : Rutherford Sampled: Received: 09/25/2014 completed: 10/06/2014 Farm: Links to Helpful Information Sample ID: SP601 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.4 120-200 90 110 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.36 1.12 6.7 78 1.4 5.8 21 16 56 21 36 326 213 166 166 391 0.2 3 Sample ID: SP603 Recommendations: Lime Nutrients (lb/acre) More Crop (tonslacre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.5 120-200 80 110 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 cd; NO3-N in mg/dnr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 1.12 6.8 78 1.5 5.7 23 15 55 21 40 325 212 197 197 445 0.2 3 Sample ID: SP604 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.8 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/ctn3; CEC and Na in meq/100 cd; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.66 1.08 8.5 77 2.0 5.6 83 65 55 18 49 141 102 262 262 366 0.2 2 North Carolina tt..� L`h.iec+; i:uer ! ur?i Lr.nu;a:x:..n Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006829 Page 2 of 3 Sample ID: SP605 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.8 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WIV in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 1.05 8.6 76 2.1 5:6 82 67 54 18 50 125 92 314 314 397 0.2 2