HomeMy WebLinkAboutWQ0001953_Residual Annual Report 2014_20150209Town of
Spindale
Town of Spindale, NC
2014 Annual Report
Land Application Program
NC Permit No. WQ0001953
F?ECEIVED
FEB 0 9 2015
INFO ION PROCESR SECTION
NATIOSING UNIT
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WQ Permit#: ' WQ0001953 County: Rutherford Year: 2014
Facility Name (as shown on permit): Town of Spindale
Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909
Land application of residuals as allowed by the permit occurred during the past calendar year?
® Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
1 6
Total number of fields utilized for land application during the year:
4
Total amount of dry tons applied during the year for all application sites:
73.39
Total number of acres utilizes for land application during the year:
42.5
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources. EJ Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to. 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
. 503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (type or rint) Signature of Permittee Date
/ OZ a3 .S_ l .-ram: 2n
Signature of Preparer* Date Sigildiure of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC; 02T. 1102 (26) nFNR FnRM ArF (19/9nns)
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0001953
Facility Name: Town of Spindale
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0001953
Town of Spindale, NC
Laboratory:
1)
2)
3)
4)
5)
A&L Eastern Labs
Parameter
(mg/kg)
Conc.
Limit
m /k a
Sample or Composite Date
6-19-14
Percent Solids (%)
NA
4.23
Arsenic
75
3
Cadmium
85
3
Copper
4,300
1850
C'hrnminm
NA
J 77
Lead
840
69
Mercury
57
2
Molybdenum
75
10
Nickel
420
279
Selenium
100
38
Zinc
7,500
1780
Total Phosphorus
NA
16900
TKN
NA
48200
Ammonia -Nitrogen
NA
7570
Nitrate and Nitrite
NA 1
37.8
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
02 e) s
Date
f�a
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)
tVl\lINVIV•,IVI 19"La r11',LL I..VA JuNki z.'0VIVllVXAKY VVAIV1'-
Attach this form to the corresponding Field Loading; Summary Form to be submitted in Annual Report
Facility Name: Town of Spindale I Total Dry Tons Applied (Annual): 41.28
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator:
Acres Used:
Mark Koone Owner: Mark Koone Predominant Soil Series: PaC2
17.1 Acres Permitted: 17.1 Site #:
SP06 Field #:
Residual Analysis Data (Heavy Metals and Total Ph,os horus use mg/kg, % Solids use Raw Percent #
Com-
posite
MENEM
VAN
TotalDate
•
"
.•��
I
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
L1J
21
3 j4
5
6
7
8
9
10
11
12
DT/Ac./
c
App.
Event
2.41
14
Arsenic
0.014
0.000
0:000
0.000
0.006
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.014
Cadmium
0.014
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.014
Copper
8.932
0.000
0.000
0.000
0.000
0.0001
0.000
0.000
0.000
0.000
0.000
0.000
8.932
Chromium
1.096
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
1.096
Lead
0.333
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.333
Mercury
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Molyb-
denum
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
Nickel
1.347
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
1.347
Selenium
0.183
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.183
Zinc
8.594
0.000
0.000
0.000
0.000
0.000
0.000 ,
0.000
0.000
0.000
0.000
0.000
8.594
Total
Phos-
81.593
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
81.593
horus
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signa,Pdre of Land Applier
( -I9-o-
Date
DENR FORM MFLSF (1212006)
AlIN 114 U L-]L 1VM I l • ,o V 1L' LiJ L V'AVjLLV lT 3 U 1V1LVIA-K Y r Vl(1Vl "
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility -Name: Town of Spindale Total Dry Tons Applied (Annual): 17.20
Permit #: WQ0001953 Cation ]Exchange Capacity (non 503 only):
Operator: Mark Koone Owner: Mark Koone Predominant Soil Series: PaC2
Acres Used: 7.8 Acres Permitted: 7.8 Site #: SP06 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
D. -
IM
a
a
MEN
0
won
Total
Phos-
..
.•��
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
L_IJ
21
5
6
7
1 91
110111
12
DT/Ac./
_.§_j
o
App.
Event
2.21
14
Arsenic
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000,
0.000
0.000
1 0.000
0.000
0.013
Cadmium
0.013
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
8.159'
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.159
Chromium
1.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.001
Lead
0.304
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.304
Mercury
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Molyb-
0.044
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.044
m denu
Nickel
1.230
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.230
Selenium
0.168
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.168
Zinc
7.850
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
7.850
Total
Phos-
74.529
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
74.529
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting; false information, including the possibility of fines and
imprisonment for knowing violations".
��lw-rr
Sign ture of Laad <pplier Date
DENR FORM MFLSF (12/2006)
Lill1\ U L-1L lViG 1 lvjuc V lL' LlJ ib"A MILLI V iJ U 1V11V1E1K Y V VnIVl
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spindale Total Dry Tons Applied (Annual):
WQ0001953 Cation Exchange Capacity (non 503 only):
Mark Koone
2.4
Owner: Mark Koone
Acres Permitted: 2.4 Site #:
2.29
Predominant Soil Series: PaC2
SP06 Field #: 4
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
DateKom
Total
Phos-
phorus
.'��
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
L1J
L2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
o
App.
Event
0.96
14
Arsenic
0.006
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.000
0.000
0.006
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
3.534
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.534
Chromium
0.434
0.000
0.000
0.00.0
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.434
Lead
0.132
1 0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.132
Mercury
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.600
0.000
0.000
0.000
0.000
0.004
Molyb-
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000,
0.000
0.000
0.000
0.000
0.019
denum
Nickel
0.533
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.533
Selenium
0.073
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.073
Zinc
3.400
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.400
Total
Phos-
32.279
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
32.279
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
f'%,: %/y
Signature of Land Applier
l-o-iS-
Date
DENR FORM MFLSF (12/2006)
A.N1VUAL 1VMlAJ.,.N V*ILLV LV,WJlr(i lU1V11VJAKY rYICVl''-
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Torun of Spindale Total Dry Tons Applied (Annual): 12.62
Permit #: WQ0001953 Cation Exchange Capacity (non 503 only):
Operator: Mark Koone Owner: Mark Koone
Acres Used: 15.2 Acres Permitted: 15.2 Site #:
Predominant Soil Series: PaD2
SP06 Field #: 5
Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
positeI Wim7mov
Com-
Date
MIE
TotalW.
Phos-
phorus
.•��
Annual Heave Metal Field Loadings (Calculated in lbs/acre):
Total
1
2j
3
41
5
6 j
7
__§.i
91
LOJ
111
12
H
DT/Ac./
c
App.
y
Event
0.83
?!
Arsenic
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.005
Cadmium
0.005
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Copper
3.071
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
3.071
Chromium
0.377
0.000
0.000
0.000
0.000
0.000
0.000
6.000
0.000
0.000
0.000
0.000
0.377
Lead
0.115
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.115
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molyb-
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
denum
Nickel
0.463
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.463
Selenium
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
2.955
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.955
Total
Phos-
28.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
28.054
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting; false information; including the possibility of fines and
imprisonment for knowing violations"..
Signature of Land pplier
I',rl-15-
Date
DENR FORM MFLSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale WQ Permit #: WQ0001953 Field #: 1 Acres Utilized: 17.1
Land Owner: Mark Koone Annual Dry Tons Applied: 41.2755 Site #: SP06 Acres Permitted: 17.1
Operator: Mark Koone Predominant Soil Series: PaC2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN:
°
0 o
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
u
/o
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(N Q
PDES #, W #
Fert., Animal
Waste etc )
Soil
Cond.
(Drys
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
>
b
* 6
Z
o
%`�
5
4
7d cc
w
* r'
TKN
mg/kg
Z
o
R 0.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7-2014
1
234000
4.23
2.414
WQ0001953
dry
0
s
0.5
0.3
48200
7570
37.8
77.298
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
V•UUVv.uuu
u.uuu
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals
on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
0
234000
_
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
77.298
0.000
Lime Applied
Annuallbs/acre
0.014
0.013
0.027
36
0.014
0.013
0.027
34
8.932
9.548
18.480
1338
1.096
1.033
2.129
NA 1
0.333
0.318
0.651
267 1
0.010
0.008
0.018
15 1
0.048
0.048
0.096
NA
1.347
1.487
2.834
374 1
0.183
0.205
0.388
89
8.594
7.543
16.137
3498
81.593
Date
lbs/ac
Prior Years Cumulative lbs/ac
12-14
1000
Current Cumulative lbs/ac
Permitted C. P. L. R.**** 1
Permit PAN Limit lst/2nd Crop
158
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale
Land Owner: Mark Koone
Operator: Mark Koone
Crop 1 Name: Fescue
WQ Permit #: WQ0001953 Field #: 1
Annual Dry Tons Applied: 41.2755 Site #: SP06
Predominant Soil Series: PaC2
Crop 1 Max. PAN: 158 Crop 2 Name:
Acres Utilized: 17.1
Acres Permitted: 17.1
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
° y
o
A
Volume a lied
PP
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
A lied er
PP P
Acre
D Tons/Ac
ry ) _
Residual Sources
(NPDES #, WQ#
Fert., Animal
Waste, etc)
Soil
Cond.
D
(Dry,
Wet,
Moist)
Precip.
Past 24
Hrs.
inches
y
4 b
0
o'
o
o _.
* o
o
qy �,
�
�'
x ?:
o
o
91
;u �
� .,
=
* o'
a
TKN
mg/kg
Z t
i
o
°
CD
w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
pp
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7-1014
234000
4.23
2.414
WQ0001953
dry
0
s
0.5
1 0.3
48200
7570
1 37.8
77.298
NA
Fescue
0.000
0.000
0.000
0.060
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.606
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals
on FORM FSF supp. ( attach
FORM
FSF supp to this form):
'0TALS:1
01
234000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
77.298
0.000
Lime Applied
knnual
lbs/acre
0.014
0.013
0.027
36 1
0.014
0.013
0.027
34
8.932
9.548
18.480
1 1338 1
1.096
1.033
2.129
NA
0.333
0.318
0.651
267
0.010
0.008
0.018
15
0.048
0.048
0.096
NA 1
1.347
1.487
2.834
374 1
0.183
0.205
0.388
89 1
8.594
7.543
16.137
3498
81.593
Date
lbs/ac
'rior Years Cumulative lbs/ac
12-14
1000
:urrent Cumulative lbs/ae
'ermitted C. P. L. R.****
'ermit PAN Limit 1 st/2nd Crop
158
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly,gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
/ %-/ S
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale WQ Permit #: WQ0001953 Field #: 3 Acres Utilized: 7.8
Land Owner: Mark Koone Annual Dry Tons Applied: 17.1981 Site #: SP06 Acres Permitted: 7.8
Operator: Mark Koone
Crop 1 Name: Fescue
Predominant Soil Series: PaC2
Crop I Max. PAN: 158
Cation Exchange Capacity (non 503):
Crop 2 Name: Crop 2 Max. PAN:
�,
o
Q 0
Volume applied
PP
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
W
Moist)
Precip.
Past 24
Hrs.
inches
Y
c�
a a
o
o
w
w r.
tZ
E:
7y �
w �,
*
�3
TKN
mg/kg
Z
o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
PP
Ibs/acre
( )
Name of CropType
�
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7-2014
97500
4.23
2.205
WQ0001953
dry
0
s
0.5
0.3
48200
7570
37.8
70.608
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
0.000
0.000
0:000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.0o0
0.000
El
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
'oTALs:
0
97500
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
70.608
o.000
Lime AEplied
knnuallbs/acre
0.013
0.013
8.159
1.001
0.304
0.009
0.044
1.230
0.168
7.850
74.529
Date
lbs/ac
'rior Years Cumulative lbs/ac
0.012
0.025
36
0.012
0.025
34
8.169
16.328
1338
0.892
1.893
NA
0.272
0.576
267
0.006
0.015
15
0.041
0.085
NA
1.286
2.516
374 1
0.168
0.336
89 1
6.437
14.287
3498
12-14
1000
.urrent Cumulative lbs/ac
'ermitted C. P. L. R.****
'ermit PAN Limit 1st/2nd Crop
_
158
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
JJ *Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, InjectionAncorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE.COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE
Facility Name: Town of Spindale WQ Permit #• WQ0001953 Field #: 4 Acres Utilized: 2.4
Land Owner: Mark Koone Annual Dry Tons Applied: 2.2931 Site #: SP06 Acres Permitted: 2.4
Operator: Mark Koone Predominant Soil Series: PaC2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN:
o
a; o(enter
A
Volume applied
one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
pP � P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Wasteetc)
,
Soil
Cond.
(Dry,
Wet,
Moist)
7-2014
13000
4.23
0.955
WQ0001953
dry
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
170TAL&I 01 1
4 mtual lbs/acre
?rior Years Cumulative Ibs/ac
Iurrent Cumulative lbs/ac
?ermitted C. P. L. R.****
'ermit PAN Limit 1
As
Residuals
Cd
Applic
Cu
0.006
0.006
3.534
0.005
0.005.
3.898
0.011
0.011
7.432
36
34
1338
Precip.
y
o4.0
z
Nitrate
Past 24
�'
'»
F "
a
TKN
o
and
Hrs.
0
*
*L�
� w•
Nitrite
inches
0
mg/kg
mg/kg
mg/kg
0
s
0.5
0.3
48200
7570
T 37.8
tions totals
Cr
on FORM
Pb
FSF
Hg
0.434
0.132
0.004
0.422
0.13
0.003
0.856
0.262
0.007
NA 1
267
15
PAN Applied
( Ibs/acre)
Crop 1 Crop 2
30.597 NA
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.000 0.000
0.060 0.000
Name of Crop Type
Receiving Residual
Application
Crop 1 Crop 2
Fescue
ipp ( attach
Mo
FORM
Ni
FSF supp
I Se
to this
Zn
form):
P 30.597 0.000
32.279 _
Lime Applied
Date lbs/ac
0:019
0.533
0.073
3.400
3.306
6.706
3498
0.021
0.666
0.085
12-14
1000
0.040
1.199
0.158
NA
374
89
_ _ _ .
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations.,,
*Application Method: S - Surface, IN - Injection, INC - Incorporation
J�d 4 is **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature. of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0:2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Spindale WQ Permit #• W 0001953 Field #• 5 15.2
' Q Acres Utilized:
Land Owner: Mark Koone Annual Dry Tons Applied: 12.6120 Site #: SP06 Acres Permitted: 15.2
Operator: Mark Koone Predominant Soil Series: paD2 Cation Exchange Capacity (non 503)•
Crop 1 Name: Fescue Crop 1 Max. PAN: 139 Crop 2 Name: Crop 2 Max. PAN:
°
°
A 0
7-2014
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
71500
%
Solids
4.23
Volume
A lied er
PP P
Acre
(Dry Tons/Ac)
0.830
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste etc)
WQ0001953
Soil
Cond.
(Dry,
We
Moist)
dry
Precip.
Past 24
Hrs.
inches
0
y
410
--
o m
°' �''.
^�
s
o
w _
0.5
w :;
# w
*
0.3
TKN
mg/kg
48200
Z
o
vo 0
w
mg/kg
Nitrate
and
Nitrite
mg/kg
1 7570
37.8
0.000
0.000
0.000
0.000
0.000
0.000
0.000
v.ovv
0.000
r0.0
00
0.000
roT !S: 0 71500 -
Annuallbs/acre
'rior Years Cumulative lbs/ac
�urrent Cumulative lbs/ac
?ermitted C. P. L. R.****
'ermit PAN Limit 1st/2nd Crop
As
0.005
0.005
0.010
36
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
Cd I Cu Cr Pb Ha Mo I Ni Se_ Zn P
0.005 3.071 0.377 0.115 0.003 0.017 0.463 0.063 2.955 28.054
0.005 3.127 0.347 0.104 0.002 0.016 0.501 0.06 2.455
0.010 6.198 0.724 0.219 0.005 0.033 .0.964 0.123 5.410
34 1338 1 NA 267 1 15 1 NA 374 89 3498
PAN Applied
(lbs/acre)
Crop 1
26.571
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
26.571
Crop 2
NA
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Name of Crop Type
Receiving.Residual
Application
Crop 1 Crop 2
Fescue
0.000 1 Lime
1 12-14 1 1000 1
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
nformation, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land APplier Date *** Mineralization Rates: Compost -0.1, anaerobiall digested -0.2 ,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)
Page: 1 of 2
Report Number: 14-174-0201
Account Number: 46381
Submitted By: ZACH KEY
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
Lab Number: 56047
Sample Id : SPINDALE
A&L Eastern Laboratories, Inc.
7621 Whitepine*Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastem.com
Project: SPINDALE
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 6/19/2014 13:15:00
Date Received: 06/23/2014 00:00
Date Reported: 06/26/2014
Total Solids *
4.23
42300
100.0
JM
06/23/2014 13:30
SM-2540G
Moisture'
95.77
100.0
JM
06/23/201413:30
SM-2540G
Total Kjeldahl Nitrogen
4.82
48200
10.0
JM
06/24/2014 08:44
SM-4500-NH3C-TKN
Total Phosphorus
1.69
16900
100
KM
06/24/2014 15:02
SW 6010C
Totai Potassium
0.30
2960
100
KM
06i24i2U14 15:02
SW 6010C
Total Sulfur
1.67
16700
100
KM
06/24/2014 15:02
SW 6010C
Total Calcium
1.61
16100
100
KM
06/24/2014 15:02
SW 6010C
Total Magnesium
0.30
3040
100
KM
06/24/2014 15:02
SW 6010C
Total Sodium
0.52
5240
100
KM
06/24/2014 15:02
SW 6010C
Total Iron
18700
100
KM
06/24/2014 15:02
SW 6010C
Total Aluminum
25000
100
KM
06/24/2014 15:02
SW 6010C
Total Manganese
344
5
KM
06/24/2014 15:02
SW 6010C
Total Copper
1850
5
KM
06/24/2014 15:02
SW 6010C
Total Zinc
1780
5
KM
06/24/2014 15:02
SW 6010C
Ammonia Nitrogen
0.76
7570
10.0
JM
06/24/2014 08:44
SM-4500-NI3C
Organic N
4.06
40630
10.0
06/24/2014 08:44
CALCULATION
Nitrate+Nitrite-N
37.8
2.00
JM
06/24/2014 08:45
SM450ONO3F
Total Cadmium
3.0
2.0
KM
06/24/2014 15:02
SW 6010C
All values are on a dry weight basis except as noted
by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients. and
may not be reproduced
n whole or part, nor may
any reference
be made
to the work. the results. or the company in, any advertising,
news release, or other public announcements witrouut obtaining out prior
written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-174-0201
Account Number: 46381
Submitted By: ZACH KEY
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
�L A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastem.com
Project: SPINDALE
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 6/19/2014 13:15:00
Lab Number: 56047 Date Received: 06/23/2014 00:00
Sample Id : SPINDALE Date Reported: 06/26/2014
Total Chromium
227
5
KM
06/24/2014 15:02
SW 6010C
Total Nickel
279
5
KM
06/24/2014 15:02
SW 6010C
Total Lead
69
5
KM
06/24/2014 15:02
SW 6010C
Total Arsenic
3.0
3.0
KM
06/24/2014 15.02
SW 6010C
Total Mercury
2.0
0.4
KM
06/24/2014 12:00
SW-7471 B
Total Selenium
38.0
5.0
KM
06/24/2014 15:02
SW 6010C
pH (Standard Units) *
7.42
2.00
JM
06/24/2014 08:44
SW-9045D
Total Molybdenum
10
5
KM
06/24/2014 15:02
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and !eaters are for the exclusive and confidential use of our clients. and may not be reproduced in v✓ro,e or part, nor may any reference be, made
to the work., the ; esults or the company ir: any advertising, newvs release. or otherpubiic announcements r ithout obtaining our prior wrtten authorization.
Debbie Holt
SAR
Sodium Absorption Ratio
PLa(Mq�.
Ca(Mg/L) IVIcM /L
Na: Sodium (Mg/L) Equivalent weight: 23
E221.652
681.03 128.59
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
N IUIE
Ca I'VIE. Mg (ME)
1
9.637043
34.0515 10.7'1583
Milli Equivalent = Mg/L / Equivalent weight The amour
amount of c
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
Permitting l
SAR = 2.03694 (1=rorn Mg/L entered above)
SAR= 2.035618 (From ME entered below)
Na (ME)
1
Ca (ME).
1
MgJMEJ
9.63
34.05
10.71
PAN
Mineralization
as decimal
Jj2t�ald
tons/dear
jAcres
Appli don
1 42.5
Rate
0.3
TkN
48200
-NH3
7570
NO3
37.8
NO2
0
% Solids
0.0423
1 73.39
PAN Surface
16011.8 1 mgikg
32.0236 lbs/dry ton
2350.212llbs
total PAN
55.299111Ibs
PAN/acre
PAN Injection
19796.31mg/kg
39.5936 lbs/dry ton
2905.774
1 Ibs total PAN
68.371161lbs
PAS!/acre
Dry Tons/1000 gal.
0.176391
ist year PAN
Surface lbs.
F-72-375-0212004
1st year PAN
Injected Ibs.
2905.774304
ibs./acre
Surface
55.29910598
Ibs./acre
Injected
10009
MR(TKN-NH3)+ +.5(NH3)+NO3+NO2 =mg/kg
mg/kg x.002 =Ibs/dry ton
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x.002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal."
2000
Analytical Results
Southern Soil Builders
958 Hoots Road
Roaring River NC 2.8669
Entered 6/19/2014
Reported: 6/24/2014
For: Spindale
Sample ID
Parameter
Cust ID
Result
Units
Method
Date
Analyzed Analyst
140619-19.1
% Solids
1
4.53
%
SM2540B-1997
6/20/14
CL
140619-19.1
Fecal Coliform MTF
1
<442
MPN/g
SM92210E-2006
6/20/14
CL
140619-19.1
Geometric Mean
1
705
MPN/g
dry wt. basis
6/23/14
CL
140619-19.2
% Solids
2
4.53
%
SM2540B-1997
6/20114
CL
140619-19.2
Fecal Coliform MTF
2
883
MPN/g
SM9221 CE-2006
6/20/14
CL
140619-19.3
% Solids
3
4.35
%
SM254OB-1997
6/20/14
CL
140619-19.3
Fecal Coliform MTF
3
1379
MPN/g
SM9221 CE-2006
6/20/14
CL
140619-19.4
% Solids
4
4.49
%
SM254OB-1997
6/20/14
CL
140619-19.4
Fecal Coliform MTF
4
891
MPN/g
SM92210E-2006
6/20/14
CL
140619-19.5
% Solids
5
4.57
%
SM2540B-1997
6/20/14
CL
140619-19.5
Fecal Coliform MTF
5
875
MPN/g
SM92210E-2006
6/20/14
CL
140619-19.6
% Solids
6
4.47
%
SM2540B-1997
6/20/14
CL
140619-19.6
Fecal Coliform MTF
6
<447
MPN/g
SM9221 CE-2006
6/20/14
CL
140619-19.7
% Solids
7
4.32
%
SM2540B-1997
6/20/14
CL
140619-19.7
Fecal Coliform MTF
7
<463
MPN/g
SM9221 CE-2006
6/20/14
CL
P.O, Box 228 9 Statesville, North Carolina 28687 • 704/872/4697
Southern Soil Builders
958 Hoots Road
Roaring River NC 28669
Entered 6/19/2014
Reported: 6/24/2014
For:
Sample ID Parameter Gust ID Result Units Method
Respectfully submitted,
'a"-/ -
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
Date
Analyzed Analyst
P.O. Box 228 9 Statesville, North Carolina 28687 • 704/872/4697
Analytical Results
Southern Soil Builders
958 Hoots Rd.
Roaring River, NC 28669
Entered: 7/11/2014
Reported:8/12/2014
Sample ID: 140711-11
For: Spindale
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
Week 1 1.47 0.97 0.6599
Week 2 1.47 0.98 0.6667
Week 3 1.46 0.97 0.6635
Week 4 1.47 0.98 0.6659
Week 5 1.32 0.86 0.6532
Volatile Solids Reduction: 0.6599 - 0.6532 X 100 = 2.93 %
0.6599 - (0.65991 X 0.6532)
Respectfully submitted,
J
Dena Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
DW Cert. #37755
P.O. Box 228 ® Statesville, North Carolina 28687 ® 704/872/4697
Client:
STATESVILLE ANALYTICAL
IZZ Court Street - P.O. Box 228
Statesville, NC 28687
(704) 872-4697
�. W-WA
0
Address:
L& 4,
Aj C
Contact Person: Phone #
ZY_ct 9-"'_� ?I k - q q 1
FAXO
0
Chain of
Custody Record
PO # U Requisitioned by: (Time Date)
Customer
Sample fD#
Lab -ID #
Time Sampled
(Grab Only)
Date Sampled
(Grab Only)
Matrix
Parameters requested for analysis
Sf.dg.1
W
IWW
C,
Relinquished by:
Receivedby:
Relinquished by:
Received by:
Composite Sampling
Time begin-
Time end
Composite Sampling
Time begin-
Time end
X/
^
AV
#1:
am, pm Date
am, pm Date
#2:
am, pm Date
am, pm Date
Time s15
Time '2
Time
Time
Lab Comments:
am, 1(PM_,Date
U /
am, pi rU Date
am, pm Date
am, pm Date
Sampled by:
11
Transported by: 7-
Holding times met:
Compliance work:
Non-compliance work:
n
Condition of Receipt
Sample ID 140711-11 Client Southern Soil Builders
Temp on Arrival 2
pH upon Arrival Parameter Schedule
El
El
Bench :10 Day
HNO;;
❑ Chemicals in containers, client
HCI
W Chemicals upon receipt
NaOIi
FV] Received on Ice
H2SCI
❑ Samples chilled upon receipt
Na2S O
❑ Chemicals in containers, lab
Dechlorinated
Page 1 of 1
1, 1
Analytical Results
Southern Soil Builders
958 Hoots Road
Roaring River NC 28669
Entered 6/19/2014
Reported: 8/20/2014
For: Spindale
Sample ID
Parameter
Cust ID
Result Units
Method
Date
Analyzed Analyst
140619-21
Corrosivity
Spindale
See Attached
SW-846
07/07/14 PACE
140619-21
Ignitability
Spindale
See Attached
1010M
07/07/14 PACE
140619-21
Reactivity
Spindale
See Attached
SW-846
07/07/14 PACE
140619-21
TCLP
Spindale
See Attached
1311
07/07/14 PACE
Respectfully submitted,
C"Jn- 011/��
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
M
P.O, Box 228 9 Statesville, North Carolina 28687. 704/872/4697
Client:
S6 : sr SB `) /-�v tCir P rf �` -'
Address: 1
-1 "`'1
STATESVILLE ANALYTICAL
122 Court Street • P.O. Box 228
Statesville, NC 28687
(704) 872-4697
Chain of
Custody record
Contact Person: Phone # 3 J 6 e� s �- '78"7 ( Fes# 3 3� 4J p Y o
r
PO # j Requisitioned b : (Time Date
q v )
Customer
Sample ID#
Lab -ID #
Time Sampled
Grab Only) ( y)
Date Sampled
(Grab Only)
a
d
Matrix
ISludgalw
I ww
�0-4-(C
I �C!(Ci�` ?!
/, 1 D Tit'
(�-�� J�t7
}�
7e LYE
�.c a
Relinquished by:
Received by:
Relinquished by:
� �- %� ^
Time J = S C am, .�m2Date
Time `S am<ym Date /
Time am, pm Date / /
Sampled by: ate:/
Transported by:
Holding times met:
Received by:
Composite Sampling
#1
Time
am, pm Date
/ /
Compliance work:
Time begin
am, pm Date _/ /
Non-compliance work:
Time end
am, pm Date / /
Lab Comments:
Composite Sampling
#2-
Time begin
am, pm Date
Time end
am, pm Date / /
t 4 a
Condition of Receipt
Sample ID 140619-21 Client Southern Soil Builders
Temp on Arrival 6
pH upon Arrival
Parameter Schedule TCLP
❑
HNO3
❑
HCl
❑
NaOH
❑
H2SO
❑
Na2S2O
❑
Dechlorinated
❑ Chemicals in containers, client
❑ Chemicals upon receipt
V Received on Ice
❑ Samples chilled upon receipt
❑ Chemicals in containers, lab
Page 1 of 1
aceAnalytical
www.pacelabs.corn
I
ANALYTICAL RESULTS
Project: 140619
Pace Project No.: 92206260
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: 140619-21 Lab ID: 92206260001 Collected: 06/20/14 13:10 Received: 06/20/14 14:21 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachiorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methyl phenoI(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichiorophenol
2,4,6-Trichlorophenol
Date: 07/10/2014 04:48 PM
Results Units
,
Report Limit DF
Prepared
Analyzed
CAS No. Qual
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 06/20/14 21:00
ND ug/ I
1
0.50 1
06/24/14 10:23
06/29/14 14:00
58-89-9
ND ug/
d
3.0 1
06/24/14 10:23
06/29/14 14:00
57-74-9
ND ug/
0.50 1
06/24/14 10:23
06/29/14 14:00
72-20-8
ND ug/L
1
0.50 1
06/24/14 10:23
06/29/14 14:00
1024-57-3
ND ug/
ND ug/111
1000 1
3.0
06/24/14 10:23
06/29/14 14:00
72-43-5
1
06/24/14 10:23
06/29/14 14:00
8001-35-2
72 %
i
10-138 1
06/24/14 10:23
06/29/14 14:00
2051-24-3
41 % 1
10-110 1
06/24/14 10:23
06/29/14 14:00
877-09-8
Analytical Methid:
EPA 8151
Preparation Method: EPA 3510
ND mg/L
0.010 1
06/26/14 07:30
06/27/14 09:08
94-75-7
ND mg/L
0.010 1
06/26/14 07:30
06/27/14 09:08
93-72-1
94 %
42-142 1
06/26/14 07:30
06/27/14 09:08
19719-28-9
Analytical ry
Leachate M
ND
ND
ND
ND
ND
ND
ND
Analytical M
Leachate M
ND
Analytical M
Leachate M
EPA 6010 Preparation Method: EPA 3010
)ate: EPA 1311; 06/23/14 15:45
0.050
1
06/24/14 11:40
06/24/14 22:40
7440-38-2
0.25
1
06/24/14 11:40
06/24/14 22:40
7440-39-3
0.0050
1
06/24/14 11:40
06/24/14 22:40
7440-43-9
0.025
1
06/24/14 11:40
06/24/14 22:40
7440-47-3
0.025
1
06/24/14 11:40
06/24/14 22:40
7439-92-1
0.10
1
06/24/14 11:40
06/24/14 22:40
7782-49-2
0,025
1
06/24/14 11:40
06/24/14 22:40
7440-22-4
EPA 7470 Preparation Method: EPA 7470
)ate: EPA 1311; O6/23/14 15:45
0.20 1 06/24/1412:15 06/24/1417:36 7439-97-6
EPA 8270 Preparation Method: EPA 3510
)ate: EPA 1311; 06/20/14 21:00
ND ug/12,
50.0
1
06/2411410:08
06/25/14 14:13
106-46-7
ND ug/L�
ND
50.0
1
06/24/14 10:08
06/25/14 14:13
121-14-2
ug/L1
50.0
1
06/24/14 10:08
06125/1414:13
87-68-3
ND ug/L
50.0
1
06/24/14 10:08
06/25/14 14:13
118-74-1
ND ug/L,
50.0
1
06/24/14 10:08
06/25/14 14:13
67-72-1
ND ug/L1
ND
50.0
1
06/24/14 10:08
06/25/14 14:13
95-48-7
ug/L
50.0
1
06/24/14 10:08
06/25/14 14:13
ND ug/L'
50.0
1
06/24/14 10:08
06/25/14 14:13
98-95-3
ND ug/L
100
1
06/24/14 10:08
06125/1414:13
87-86-5
ND ug/1-1
50.0
1
06/24/14 10:08
06/25/14 14:13
110-86-1
ND ug/L
50.0
1
06/24/14 10:08
06/2511414:13
95-95-4
ND ug/L
50.0
1
06/24/14 10:08
06/25/14 14:13
88-06-2
i
REPiORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without1the written consent of Face Analytical Services, Inc..
Page 4 of 21
P 4 i
aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project; 140619
Pace Project No.: 92206260
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: 140619-21 Lab ID: 92206260001 Collected: 06/20/14 13:10 Received: 06/20/14 14:21 Matrix: Solid
Results reported on a "dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 0(3/20/14 21:00
Surrogates
Nitrobenzene-d5 (S)
32 %
12-102
1
06/24/14 10:08
06/26/14 14:13
4165-60-0
2-Fluorobiphenyl (S)
28 %
13-107
1
06/24/14 10:08
06/25/14 14:13
321-60-8
Terphenyl-04 (S)
65 %
21-132
1
06/24/14 10:08
06/25/14 14:13
1718-51-0
Phenol-d6 (S)
11 %
10-110
1
06/24/14 10:08
06/25/14 14;13
13127-88-3
2-Fluorophenol (S)
16 %
10-110
1
06/24/14 10:08
06/25/14 14:13
367-12-4
2,4,6-Tribromophenol (S)
43 %
27-108
1
06/24/14 10:08
06/25/14 14:13
118-79-6
8260 MSV TCLP
Analytical Method: EPA8260 Leachate
Method/Date:
EPA 1311; 06/24/14 12:58
Benzene
ND ug/L
5.0
1
07/03/14 15:55
71-43-2
2-Butanone (MEK)
198 ug/L
10.0
1
07/03/14 15:55
78-93-3
Carbon tetrachloride
ND ug/L
5.0
1
07/03/14 15:55
56-23-5
Chlorobenzene
ND ug/L
5.0
1
07103/1415:55
108-90-7
Chloroform
ND ug/L
5.0
1
07/03/14 15:55
67-66-3
1,4-Dichlorobenzene
ND ug/L
5.0
1
07/03/14 15:55
106-46-7
1,2-Dichloroethane
ND ug/L
5.0
1
07/03/14 15:55
107-06-2
1,1-Dichloroethene
ND ug/L
5.0
1
07103/1415:55
75-35-4
Tetrachloroethene
ND ug/L
5.0
1
07/03/14 15:55
127-18-4
Trichloroethene
ND ug/L
5.0
1
07/03/14 15:55
79-01-6
Vinyl chloride
ND ug/L
5.0
1
07/03/14 15:55
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
109 %
70-130
1
07/03/14 15:56
17060-07-0
Toluene-d8 (S)
102 %
67-135
1
07/03/14 15:65
2037-26-5
4-Bromofluorobenzene (S)
96 %
70-130
1
07/03/14 15:55
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
96.1 %
0.10
1
07/07/14 15:53
1010 Flash point,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
07/09/14 10:30
9045 pH Soil
Analytical Method: EPA9045
pH at 25 Degrees C
6.8 Sid. Units
0.10
1
06/23/14 17:58
733C S Reactive Cyanide
Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
25.8
1
06/30/14 23:22
735S Reactive Sulfide
Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
258
1
06/30/14 19:00
Date: 07/10/2014 04:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Face Analytical Services, Inc..
Page 5 of 21
4, } A1NV VUk' '1'VK A'1l 1'_KACTIVN REDUCTION FORM (02T Rules)
Facility Name: Town of Spindale WQ Permit Number: WQ0001953
WWTP Name: Town of Spindale, WWTP NPDES Number: NC0020664
Monitoring Period: From 1/1/2014 To 12/31/2014
Pathogen Reduction (15A NCAC 02T .1106) - Please_ indicate level achieved and alternative performed:
Class A: Alt. A (time/temp) ® 1 Alt B (Alk Treatment) ® I Alt. C (Prior Testing) El
A1t.D (No Prior Test) Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 11 Heat Drying Ca Heat Treatment El Therm.ophilic
Beta Ray ® Gamma Ray ® Pasteurization
.......................................
Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens Il
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ® Air Drying ® Composting ® Aerobic Digestion D
Anaerobic
a robrc Digestion strop
C1
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density Number o Frequency Sample Analytical
Parameter in Sludge Excee- of Anal y p Tech-
g Minim Geo. Mean axim Units Ce Analysis Type
nicue
2 x 10 to the NTN 442 705 1379 MPN/ 0 7
6th power g grab sm9221 c
per gram of
Fecal Coliform total solids CFU
1000 mpn per gram - ------- _T
of total solid (dry
Salmonella bacterial 3 NTN per 4 grams
(in lieu of fecal total solid (dry
Vector Attraction Reduction 05A NCAC 67T _11071 - Plnacn infla..a+o ai+o,..,.,+;.,,, ---.r .....,.a.
Alt.l (VS reduction) ®
Alt. 2 (40-day bench) ®
;Alt. 3 (30-day bench)
Alt. 4 (Spec. 02 uptake) Ll
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) ®
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) ®
!'ITTT TTTT/^I 1 TT rr
Alt. 10 (Incorporation) ®
No vector attraction reduction alternatives were performed Il
11.'1v�a11V1I 1.71Cf1LlVll,l\ 1 spiv Nv lurzuK tue appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 115A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in' 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 115A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification, including fine and imprisonment."
Zewle- W/ - Dennis Key Southern Soil Builders, Inc.
Preparer Name arfA Title (type or p nt) 'Land Applier Name and Title (if applicable)(type or print)
1- I )-1 S
Signature of Preparer* Date Signature of L Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
nF=NP FCIPAA P\/PF n7T /1717nna\
NCDA&CS Agronomic Division Phone: (919) 733-2655
Website: www.ncagr.gov/agronomi/
Report No.
FY15-SL006829
Client:
Southern Soil Builders, Inc.
Advisor:
1
Predictive
•�Y 5 Sid
958 Hoots Rd
.�.. : =.
Roaring River, NC 28669
`,,,'k�`•d-~;ail Soil Report Mehlich-3 Extraction
... L;.>
Sampled County : Rutherford
Sampled: Received: 09/25/2014
completed: 10/06/2014
Farm:
Links to Helpful Information
Sample ID: SP601
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, 1 0.4
120-200 90
110
0 0 0
0
0 0
Note: 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-1 Na ESP SS-1 NO3-N
0.36 1.12 6.7 78 1.4 5.8 21 16
56 21 36
326
213 166
166
391 0.2
3
Sample ID: SP603
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tonslacre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, 1 0.5
120-200 80
110
0 0 0
0
0 0
Note: 12
2-
Test Results [units - WN in g/cm3; CEC and Na in meq/100 cd; NO3-N in mg/dnr3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 1.12 6.8 78 1.5 5.7 23 15
55 21 40
325
212 197
197
445 0.2
3
Sample ID: SP604
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.8
120-200 0
20
0 0 0
0
0 0
Note: 12
2-
Test Results [units - WN in g/ctn3; CEC and Na in meq/100 cd; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-AI2 Zn-I
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.66 1.08 8.5 77 2.0 5.6 83 65
55 18 49
141
102 262
262
366 0.2
2
North Carolina
tt..�
L`h.iec+; i:uer ! ur?i Lr.nu;a:x:..n
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture
NCDA&CS Agronomic Division Phone: (919) 733-2655
Website: www.ncagr.gov/agronomi/
Report No. FY15-SL006829
Page 2 of 3
Sample ID: SP605
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P205
K20
Mg
S
Mn Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, 1 0.8
120-200 0
20
0
0
0 0
0 0
Note: 12
2-
Test Results [units - WIV in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.66 1.05 8.6 76 2.1 5:6 82 67
54 18 50
125
92
314 314
397 0.2 2