890001_ENFORCEMENT_20171231

NUH I H LAHULINA
Department of Environmental Quaff

ENFORCEMENT
ENFORCEMENT
ENFORCEMENT

A
- VA
CDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor . Director Secretary
June 28, 2010
New Colony Farms, LLC
New Colony Farms
365 N. Phelps Rd
Columbia, North Carolina 27925
RE: Acknowledgment of Receipt of Payment
Case No. PC-2010-0018
Farm # 89-0001
Tyrell County
Dear New Colony Farms, LLC:
This letter is to acknowledge receipt of your check No. 0113538 in the amount of $2641.23
on June 25, 2010. This payment satisfies in full the civil assessment in the amount of $2641.23
levied against New Colony Farms, LLC and the case has been closed. 1f you have any questions,
please call me at [phone]. _
Sincerely,
Miressa D. Garoma
Animal Feeding Operations Unit
cc David -May, Washington-A-PS-Regional-SuperVi—
File # PC-201 0-0018
APS Central Files
AQUIFER PROTECTION SECTION
1636 Mail Service Center, Rale�h, North Carolina 27699-163S
Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604
Phone: [phone] FAX t: 919-715-0588 FAX 2: 919-715-60481 Customer Service: 1-877-623-6748
Internet www.ncwatemuality.org_
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FJYU N 3 0 2010
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North Carolina Department of Environment and Natura
Division of Water Quality
Beverly caves Perdue Coleen K. Sullins
Governor Director
May 27, 2010
Resources
CERTIFIED MAIL - #7006 2150 0003 5467 2220
RETURN RECEIPT REQUESTED
New Colony Farms, LLCe,�\
New Colony Farms 1 t 2d1O
365 N. Phelps Rd
Columbia, North Carolina 27925
SUBJECT: Assessment of Civil Penalties for Violation(s)'of
N.C. General Statute(s) 143-215.1
Farm # 89-0001
Tyrell County
File No. PC-2010-0018
Permit No. AWS890001
Dear, New Colony Farms, LLC:
This letter transmits notice of a civil penalty assessed against New Colony Farms, LLC in the
amount of S2641.23, which includes S641.23 in investigative costs. Attached is a copy of the
assessment document explaining this penalty.
Dee Freeman
Secretary
This action was taken under the authority vested in me by delegation provided by the Secretary of the
Department of Environment and Natural Resources and the Director of the Division of Water Quality. Any
continuing violation(s) may be the subject of a new enforcement action, including an additional penalty.
Within thirty days of receipt of this notice, you must do one of the following three items:
1. Submit payment of the penalty:
Payment should be made to the order of the Department of Environment and Natural Resources.
Payment of the penalty will not foreclose further enforcement action for any continuing or new
violation(s). Do not include the attached waiver form if making payment.
Please send payment to the attention of:
Miressa D Garoma
DWQ
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
AQUIFER PROTECTION SECTION
1635 Mail Service Gentes, Raleiah, North Carolina 27699-1636
Location: 272B Capital Boulevard, Raleigh, North Carolina 27604
Phone: [phone] FAX 1: 919-715-0588 FAX 2: 919.715-60461 Customer Service: 1-877-623.6748
Internet: www.nmaterauality.org
Oise
NorthCarolina
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Page 2 a
New Colony Farms, LLC
May 27, 2010
2. Subunit a written request for remission including a detailed justification for such request:
Please be aware that a request for remission is limited to consideration of the five factors listed below as they
may relate to the reasonableness of the amount of the civil penalty assessed. Requesting remission is not the
proper procedure for contesting whether the violation(s) occurred or the accuracy of any of the factual
statements contained in the civil penalty assessment document. Because a remission request forecloses the
option of an administrative hearing, such a request must be accompanied by a waiver of your right to an
administrative hearing and a stipulation and agreement that no factual or legal issues are in dispute. Please
prepare a detailed statement that establishes why you believe the civil penalty should be remitted, and submit
it to the Division of Water Quality at the address listed below. In determining whether a remission request
will be approved, the following factors shall be considered:
(1) whether -one or more of the civil penalty assessment factors in NCGS 143B-282.1(b) were
wrongfully applied to detriment of the violator;
(2) whether the violator promptly abated continuing environmental damage resulting from the
violation;
(3) whether the violation was inadvertent or a result of an accident;
(4) whether the violator has been assessed civil penalties for any previous violations; or
(5) whether payment of the civil penalty will prevent payment for the remaining necessary remedial
actions.
Please note that all evidence presented in support of your request for remission must be submitted in writing.
The Director of the Division of Water Quality will review your evidence and inform you of his decision in
the matter of your remission request. The response will provide details regarding the case status, directions
for payment, and provision for further appeal of the penalty to the Environmental Management
Commission's Committee on Civil Penalty Remissions (Committee). Please be advised that the Committee
cannot consider information that was not part -of the original remission request considered by the Director.
Therefore, it is very important that you prepare a complete and thorough statement in support of your request
for remission.
In order to request remission, you must complete and submit the enclosed "Request for Remission of Civil
Penalties, Waiver of Right to an Administrative Hearing, and Stipulation of Facts" form within thirty (30)
days of receipt of this notice. The Division of Water Quality also requests that you complete and submit the
enclosed "Justification for Remission Request." Both forms should be submitted to the following address:
Miressa D. Garoma
Division of Water Quality
1636 Mail Service Center
Raleigh, NC 27699-1636
OR
3. File a petition for an administrative hearing with the Office of Administrative Hearings:
If you wish to contest any statement in the attached assessment document you must file a petition for an
administrative hearing. You may obtain the petition form from the Office of Administrative Hearings. You
must file the petition with the Office of Administrative Hearings within thirty (30) days of receipt of this
notice. A petition is considered filed when it is received in the Office of Administrative Hearings during
normal office hours. The Office of Administrative Hearings accepts filings Monday through Friday between
the hours of 8:00 a.m. and 5:00 p.m., except for official state holidays. The petition may be filed by

Page 3
New Colony Farms. LLC
May 27. 2010
facsimile (fax) or electronic mail by an attached file (with restrictions) - provided the signed original, one (1)
copy and a filing fee (if a filing fee is required by NCGS § 150B-23.2) is received in the Office of
Administrative Hearings within seven (7) business days following the faxed or electronic transmission. You
should contact the Office of Administrative Hearings with all questions regarding the filing fee and/or the
details of the filing process. The mailing address and telephone and fax numbers for the Office of
Administrative Hearings are as follows:
Office of Administrative Hearings
6714 Mail Service Center
Raleigh, NC 27699-6714
Tel: [phone]
Fax: [phone]
One (1) copy of the petition must also be served on DENR as follows:
Mary Penny Thompson, General Counsel
DENR
1601 Mail Service Center
Raleigh, NC 27699-1601
Failure to exercise one of the options above within thirty (30) days of receipt of this notice, as evidenced by
an internal date/time received stamp (not a postmark), will result in this matter being referred to the Attorney
General's Office for collection of the penalty through a civil action.
Please be advised that additional penalties may be assessed for violations that occur after the review period
of this assessment. 1f you have any questions, please contact Miressa D. Garoma at (919) 71 5-6937.
Sincerely,
kodore L. Bush Jr. Chief
Aquifer Protection Section
Division of Water Quality
ATTACHMENTS
cc: David May, Washington APS Regional Supervisor w/ attachments
File # PC-2010-0018 w/ attachments
APS Central Files w/ attachments
Susan Massengale w/ attachment

STATE OF NORTH CAROLINA
COUNTY OF TYRELL
IN THE MATTER OF
NEW COLONY FARMS, LLC
FOR VIOLATIONS OF SWINE WASTE
MANAGEMENT SYSTEM
GENERAL PERMIT AWG 100000
PURSUANT TO NORTH CAROLINA
GENERAL STATUE 143-215.1
NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND
NATURAL RESOURCES
File No. PC-2010-001 S
}
FINDINGS AND.DECISIQN
AND -ASSESSMENT, O!F�--,O�
I CIVII;,PENALTMS t
Acting pursuant to delegation provided by the Secretary of the D nt of Environment and
Natural Resources and the Director of the Division of Water Quahty,STheodore L. Busli, Jr., Chief of
the Aquifer Protection Section, of the Division of Water Quality (DWQ) make the following:
I. FINDINGS OF FACT
A. New Colony Farms, LLC owns and operates New Colony Farms, a permitted swine animal
feeding operation in Tyrell County. .
B. New Colony Farms, LLC was issued Certificate of Coverage AW S890001 under General Permit
AWG100000 for New Colony Farms on July 1, 2007, effective upon issuance, with an expiration
date of September 30, 2009. This permit was renewed on March 4, 2010, with an expiration date
of September 30, 2014.
C. Condition No. I. 1, of the General Permit AWG100000 states in part that "Any discharge or
application of waste to a ditch that drains to surface waters or wetlands is prohibited except as
follows: (a) discharges from the ditches are controlled by best management practices (BMPs)
designed in accordance with NRCS standards; (b) the BMPs have been submitted to and
approved by the Division; (c) the BMPs were implemented as designed to prevent a discharge to
surface waters or wetlands; (d) the waste was removed immediately from the ditch upon
discovery; and (e) the event was documented and reported in accordance with Part IH.11. of this
permit. Nothing in this exception shall excuse a discharge to surface waters or wetlands except as
may result because of rainfall from a storm event more severe than the 25-year, 24-hour storm."
D. Condition No. II. 5, of the General Permit AWG100000 states in part that "in no case shall land
application rates result in excessive ponding or any runoff during any given application event."
E. DWQ staff from Washington Regional Office made a site visit on February 23, 2010 due to
complaint call received and discovered a wastewater discharge to a drainage ditch at the New
Colony Farms. During the February 20, 2010 wastewater application event at the New Colony
Farms, wastewater was applied to fields in a manner resulting in ponding of wastewater.
Additionally, a direct discharge to a ditch occurred when a hose supplying wastewater to the
irrigation equipment was disconnected from the equipment and placed next to a ditch, allowing
wastewater to flow directly into the ditch.

F. New Colony Farms, LLC does not have a permit for the above described activities.
G. DWQ responded by issuing the facility a Notice of intent to Enforce.
H. The cost to the State of the enforcement procedures in this matter totaled $641 23
Based upon the above Findings of Facts, I make the following:
II. CONCLUSIONS OF LAW:
A. New Colony Farms is a "person" within the meaning of G. S. 143-215.6A pursuant to G: S. 143-
212(4).
B. A permit for an animal waste management system is required by G.S. 143-215.1.
,
C. The above -cited irrigation activity resulting in wastewater ponding and discharge to a ditch that
drains to surface waters violated Condition No. I. 1. and No. 11.5. of General Permit
AWG 100000.
D. New Colony Farms, LLC may be assessed civil penalties in this matter pursuant to G.S. 143-
215.6A(a)(2), which provides that a civil penalty of not more than twenty-five thousand dollars
($25,000.00) per violation may be assessed against a person who is required but fails to act in
accordance with the terms, conditions, or requirements of a permit required by G.S. 143-215.1.
E. The State's enforcement costs in this matter may be assessed against New Colony Farms, LLC
pursuant to G. S. 143-215.3(a)(9) and G. S. 143B-282.1(b)(8).
F. The Chief of the Aquifer Protection Section, Division of Water Quality, pursuant to delegation
provided by the Secretary of the Department of Environment and Natural Resources and the
Director of the Division of Water Quality, has the authority to assess civil penalties in this matter.
Based upon the above Findings of Facts and Conclusions of Law, I make the following:
III. DECISION:
Accordingly, New Colony Farms LLC owner of New Colony Farms at the time of the noncompliance is
hereby assessed a civil penalty of:
$ p 0 for violating Condition No. I. I. and No. II. 5. of the General
Permit AWG100000 for failure to properly irrigate wastewater,
resulting in excessive ponding, and discharge of wastewater to a
ditch that drains to Waters of the State.
S O Q Ono TOTAL CIVIL PENALTY
S 641.23 Enforcement costs
$ / �. TOTAL AMOUNT DUE

As required by G. S. 143-215.6A(c) in determining the amount of the penalty I have considered
the factors listed in G. S. 143B-282.1(b), which are:
(1) The degree and extent of harm to the natural resources of the State, to the public health, or to private
property resulting from the violation;
(2) The duration and gravity of the violation;
(3) The effect on ground or surface quantity or quality;
(4) The cost of rectifying the damage;
(5) The amount of money save by noncompliance;
(6) Whether the violation was committed willfully or intentional;
(7) The prior record of the violator in complying or failing to comply with programs over which the
Environmental Management Commission has regulatory authority;
(8) The cost to the State of the enforcement procedures.
(Date) eodore L. Bush, Jr. Chief
Aquifer Protection Section
Division of Water Quality

April 1, 2010
To: Keith Larick, Supervisor Animal Feeding Unit
Through: David May, Aquifer Protection Supervisor
Washington Regional Office
From: Marlene Salyer, Environmental Specialist
Washington Regional Office
Subject: Enforcement Package DV
New Colony Farm
Permit Number AWS89001
Tyrell County
Introduction:
Following up on a complaint call, a site visit on February 23, 2010 revealed a discharge
to a ditch of waste water that occurred on February 20, 2010. The discharge was a result
of the supply hose being unconnected from an Aerway system and placed directly by a
ditch allowing the wastewater to drain (flow) directly into the ditch. Runoff may have
also occurred at the time of application due to ponding and the presence of "water
furroughslhoe drains that drain directly to ditches within the application field.
The Finding, Decisions and Assessment Factors are attached for review.
Recommendations:
It is recommended that the appropriate civil penalties be assessed against this subject
facility, Newlands Farm located in Tyrrell County and New Colony Farms LLC.

DIVISION OF WATER QUALITY
ANIMAL OPERATIONS
ENFORCEMENT CASE REPORT
Section 1: General Information
1. Facility Name: New Colony Farm
2. Facility or Permit No.: AWS890001
3. Party named in assessment: New Colony Farms, LLC
4. Address: 365 N. Phelps Road, --Columbia, North Carolina 27925
5, Telephone No.: 252-796-2037
6. Location of Facility: Facility is located off 1105 SR in Tyrrell Coun
7. Type of Operation: 10,000 Farrow to Feeder swine
8. Registered Agent (if applicable): N/A
9. Registered Agent Address (if applicable): NIA
10. Date(s) of noted violations: February 22,2010
11. Receiving Stream and Classification :NA
12. Regional Office: Washington Regional Office
13. Report Prepared By: Marlene Salver
Section II: Findings
Case Narrative:.A complaint was called in to the Washington Regional Office on Monday
February 22 2010 regarding the application of wastewater into the ditches. DWQ staff made a
site visit the following day. The irrigation that occurred on Saturday February 20 was still visible
and staff could confirm that irrigation had been too close to the ditches. This is further evidenced
by wastewater analysis and video documentation showing the disconnecting of drag line, with
application immediately adjacent to ditch and ponding. Permittee and applicator do not contest
events, but do contend that wastewater strength was low. The application was being performed
by a contract operator working under the OIC of New Colony Farm.
2. Farm and/or company compliance History: This facility has two past NOD's for inadequate
freeboard levels and one of those occurred during Hurricane Floyd. However, it has been
operated according to the CAWMP and permit in the recent past and is considered a well
operated site in general.
3. Amount of Waste discharged (if applicable). It is unknown but the drag hose was seen to be
emptying into the ditch for several minutes before it was hooked back up to the tractor.
4. Violator's degree of cooperation (including efforts to prevent or restore) recalcitrance: The staff
of New Colony Farm have always been very cooperative to work with.
5. Damage? YIN: Yes the Fecal analysis would indicate that waste water did enter the ditch which
flows to the canal which flows into the Scuppernong River and out to the Albemarle Sound.

6. Mitigating Circumstances: The application event was performed by a contract company. The
facility OIC was on vacation and the contract company staff needs to attend some training
sessions.
7. Recommendations made to the owner/operator: It was recommended to the Operator in Charge to
closely monitor the contract company staff.
8. Costs to the State for the enforcement procedures (Show Breakdown):
Total Staff Time $ 130.00
Central Office $ 100.00
Travel Cost (142 miles X .43) $ 61.00
Laboratory Cost (see table) $350.23
TOTAL $ 641.23
BOD
$18.11 X 2 = $ 36.22
Fecal MF
17.75 X 3 = $ 53.25
Total K'eldahl N
16.39 X4 = $ 65.56
NH3
14.14 X 4 = $ 56.56
NO2+NO3
18.37 X 4 = $ 73.48
Phosphorus
16.29 X 4 = $ 65.16
9. Recommendations for further DWQ Action: None
10. Other Comments: NA
Section III: Assessment Factors required to be considered by G.S. 14313-282.1(b)
The degree and extent of harm to the natural resources of the State, to the public health, or to private
property resulting from the violation: The fecal analysis is significant enough in two ditches to
believe that the Quality of water was degraded and thus harmful to aquatic organisms living in the
ditches. Animal waste has the potential to deplete dissolved oxygen in the affected water body to a
point which is harmful to aquatic life. Wastewater also contains nutrients, which have the potential to
spawn algal gowth to the point which is harmful to aquatic life. Any impacted groundwater may
eventually find -its way into the surface water system.
2. The duration and gravity of the violation: The irrigation event was for one day however over
application can cause runoff or filtration into the Uoundwater.

3. The effect on ground or surface quantity or quality: Samples were collected and the results are as
follows:
Ditch 1-A
Ditch 1-B
Ditch 2-A
Ditch 3-A
BOD
5.3 mg/L
NE
NE
5.9
Fecal
Coliform
240 CFU/100m1
460
230
15
N113
1.3 mg/L as N
1.3
0.23
0.06
TKN
3.4 mg/L as N
3.0
2.1
1.3
NO2+NO3
2.2 mg/L as N
2.0
2.0
7.6
Total P
0.42 mg/L aP
0.33
0.36
0.17
As seen in the above table, ditch 1 is the ditch that had the hose flowing directly into it, ditch two
was impacted by runoff from the "hoe drains" and ditch 3 did not seem to have much impact from
the application event on this particular date.
4. The cost of rectifying the damage: No known damages required corrections.
5. The amount of money saved by noncompliance: No money was saved by this incorrect application of
wastewater into the ditches. Furthermore events such as this destroy the public trust in the facility
and of the compliance monitoring program. Money is saved when better management skills are
implemented to improve overall management of the facility, environmentally and productively.
6. Whether the violation was committed willfully or intentional: NO, it is the opinion of DWO that this
incident was not intentional. It is attributed to experience of applicator not having been familiar with
wastewater management requirements.
7. The prior record of the violator in complying or failing to comply with programs over which the
Environmental Management Commission has regulatory authority: The New Colony Farm has an
overall good record and the OIC has been excellent to work with in the past six years.
8. The cost to the State of the enforcement procedures:
Total Staff Time $ 130.00
Central Office $ 100.00
Travel Cost (142 miles X .43) $ 61.00
Laboratory Cost $350.23
TOTAL $ 641.23

STATE OF NORTH CAROLINA NORTH CAROLINA
COUNTY OF TYRELL
DEPARTMENT OF ENVIRONMENT AND
NATURAL RESOURCES
File No. PC -
IN THE MATTER OF )
New Colony Farms Inc }
FINDINGS AND DECISION
FOR VIOLATIONS OF SWINE WASTE ) AND ASSESSMENT OF
MANAGEMENT SYSTEM }
GENERAL PERMIT AWG100000 ) CIVIL PENALTIES
PURSUANT TO NORTH CAROLINA )
GENERAL STATUE 143-215.1 )
Acting pursuant to delegation provided by the Secretary of the Department of
Environment and Natural Resources and the Director of the Division of Water Quality, 1,
Theodore L. Bush, Jr., Chief of the Aquifer Protection Section, of the Division of Water Quality
(DWQ) make the following:
1. FINDINGS OF FACT
A. New Colony Farms, LLC owns New Colony Farm, a permitted/certified swine animal feeding
operation in Tyrell County.
B. New Colony Farms, LLC was issued Certificate of Coverage AWS890001 under NC General Permit
AWG100000 for New Colony Farm on July 1, 2007 effective upon issuance, with an expiration date
of September 30, 2009. The latest Certificate of Coverage was issued on March 4, 2010 and shall be
effective until September 30, 2014.
C. Condition No. 11. of the "Performance Standards" of the Swine Waste General Permit states; "any
discharge of waste that reaches surface waters or wetlands is prohibited except as otherwise provided
in this General Permit and associated statutory and regulatory provisions. Waste shall not reach
surface waters or wetlands by runoff, drift, manmade conveyance, direct application, direct discharge
or through ditches, terraces, or grassed waterways not otherwise classified as state waters.
Any discharge or application of waste to a ditch that drains to surface waters or wetlands is prohibited
except as follows: (a) discharges from the ditches are controlled by best management practices
(BMPs) designed in accordance with NRCS standards; (b) the BMPs have been submitted to and
approved by the Division of Water Quality (Division); (c) the BMPs were implemented as designed

to prevent a discharge to surface waters or wetlands (d) the waste was removed immediately from the
ditch upon discovery; and (e) the event was documented and reported in accordance with Part 11I.13.
of this General Permit. Nothing in this exception shall excuse a discharge to surface waters or
wetlands except as may result because of rainfall from a storm event more severe than the 25-year,
24-hour storm.
D. Condition No. II. 5 of the "Operation and Maintenance Requirements" of the Swine Waste General
Permit states; "in no case shall land application rates result in excessive ponding or any runoff during
any given application event."
E. On February 20, 2010 an application of wastewater was applied on the New Colony farm in Tyrrell
County. During the application event, wastewater was applied adjacent to drainage ditches in a
manner resulting in ponding. Additionally, a direct discharge to a ditch occurred when a hose
supplying wastewater to irrigation equipment was disconnected from such equipment and placed next
to a ditch, allowing wastewater to flow directly into the ditch. New Colony Farms LLC does not have
a permit for the above described activities.
F. The cost to the State of the enforcement procedures in this matter totaled $641.23
Based upon the above Findings of Facts, I make the following:
1I. CONCLUSIONS OF LAW:
A. New Colony Farms is a "person" within the meaning of G. S. 143-215.6A pursuant to G. S. 143-
212(4).
B. The affected constitutes waters of the State within the meaning of G.S. 143-215.1 pursuant to G.S.
143-212(6).
C. The above -cited incident violated Conditions No. 1. 1. of the General Permit. Condition No. 1. 1.
states in part "any discharge of waste that reaches surface waters or wetlands is prohibited except as
otherwise provided in this General Permit and associated statutory and regulatory provisions. Waste
shall not reach surface waters or wetlands by runoff, drift, manmade conveyance, direct application,
direct discharge or through ditches, terraces, or grassed waterways not otherwise classified as state
waters. Any discharge or application of waste to a ditch that drains to surface waters or wetlands is
prohitited."
D. New Colony Farm may be assessed civil penalties in this matter pursuant to G. S. 143-215.6A(a)(2),
which provides that a civil penalty of not more that twenty-five thousand dollars ($25,000.00) per
violation may be assessed against a person who is required but fails to act in accordance with terms,
conditions, or requirements of a permit required by G. S. 143-215.1.
E. ' The State's enforcement costs in this matter may be assessed against New Colony Farm pursuant to
G. S. 143-215.3(a)(9) and G. S. 143B-282.I(b)(8).
F. The Chief of the Aquifer Protection Section, Division of Water Quality, pursuant to delegation
provided by the Secretary of the Department of Environment and Natural Resources and the Director
of the Division of Water Quality, has the authority to assess civil penalties in this matter.

Based upon the above Findings of Facts and Conclusions of Law, I make the following:
111. DECISION:
Accordingly, New Colony Farms LLC owner of New Colony Farms at the time of the
noncompliance is hereby assessed a civil penalty of.
R
For violating Condition No. I.1. of the General Permit for
application of wastewater into a ditch and failure to prevent the
discharge of pollutants to surface waters or wetlands as required
by G.S. 143-215.1.
$ TOTAL CIVIL PENALTY
$ Enforcement costs
$ TOTAL AMOUNT DUE
As required by G. S. 143-215.6A(c) in determining the amount of the penalty I have considered
the factors listed in G. S. 143B-282. I (b), which are:
(1) The degree and extent of harm to the natural resources of the State, to the public health, or to private
property resulting from the violation;
(2) The duration and gravity of the violation;
(3) The effect on ground or surface quantity or quality;
(4) The cost of rectifying the damage;
(5) The amount of money save by noncompliance;
(6) Whether the violation was committed willfully or intentional;
(7) The prior record of the violator in complying or failing to comply with programs over which the
Environmental Management Commission has regulatory authority;
(8) The cost to the State of the enforcement procedures.
(Date) Theodore L. Bush, Jr. Chief
Aquifer Protection Section
Division of Water Quality

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:-
Redefinin9 World
March 24, 2010
Mr. David May
Washington Regional Supervisor
North Carolina Division of Water Quality (DWQ) — Aquifer Protection Section (APS)
943 Washington Square Mall
Washington, NC 27889
RE: NOTICE OF VIOLATION/NOTICE OF INTENT
Newlands Farm, Facility 489-01
Permit #: NCAWS890001
Tyrrell County
NOV#: NOV-2010-PC-0229
Dear Mr. May,
This letter is in response to the referenced violation received from North Carolina DWQ-APS on
March 9, 2010 and outlines events that took place surrounding the violation, corrective actions
already taken, and those which will occur during future swine wastewater application events.
Environmental stewardship is of utmost importance at M2P2, LLC. We strive to ensure that
swine nutrients produced at our farms are handled, stored, and utilized properly by applying
swine wastewater to cropland according to agronomic rates. However, on the afternoon of
February 20, 2010 a contracted applicator compromised M2P2 and North Carolina waste
management guidelines by improperly applying swine facility process wastewater from the Cow
Island Lagoon. This resulted in a complaint call to members of the M2P2 staff and DWQ-APS.
The following events took place surrounding the incident:
• February 15--18: Mark McCulley, V.F. of Strategic Relations at M2P2, LLC, was onsite
at the M2132-North Carolina office and spoke with Craig Schoff about proper wastewater
application techniques. Mark observed Mr. Schoff properly applying swine wastewater
on the evening of February 181h.
• February 19-20: Larry Dietz, General Manager for M2P2-North Carolina, observed
Mr. Schoff properly applying swine wastewater on both the l 9`s and 20a'. Mr. Dietz last
observed Mr. Schoff around noon on the 201h, at which time Mr. Schoff was applying
properly and was an adequate distance from any�residential properties, irrigation ditches
and canals.
• February 20: At approximately 3:30pm, Leigh Ann Schreckengost contacted Sandi
Smith, Human Resources and Safety Coordinator at M2P2-North Carolina, and reported
that someone was applying swine wastewater directly behind her residence. Mrs.
Schreckengost noted standing wastewater in the field where application was occurring
and wastewater being emptied directly into an irrigation ditch. Mrs. Schreckengost also
collected video documentation of the violations taking place. Mrs. Smith assured Mrs.
1615 Golden Aspen Drive I Suite 104 1 Ames. IA 50010 1 p 515.598A640 1 f 515.956.3226 1 www.m2p2.com
Colorado I Iowa I Oklahoma I North Carolina

(_R!edeWfinirk9 x�
:Y
Schreckengost that the observed actions were neither acceptable nor tolerable by M2P2
and she would take action immediately to remedy the situation.
o Mrs. Smith immediately notified Larry Dietz and Mark McCulley of the situation.
Mr. Dietz called Craig Schoff, who had wastewater pumping and application
cease immediately. Application equipment was also moved from behind the
Schreckengost residence.
o Mr. Dietz and Mr. McCulley called Mrs. Schreckengost to express their concern
and disappointment with the actions that had occurred.
• February 21: Mr. McCulley followed up with the Schreckengost's and set-up a time for
Mr. Dietz to meet with them.
• Februa 23: Mr. Dietz met with Jim Schreckengost to again express his concern and
answer questions. Mr. Schreckengost expressed his concern that his drinking water may
be contaminated due to the proximity of his-underground-weE4o-the-location-of the -ditch
where the waste spill occurred. Mr. Dietz offered to have the Schreckengost's drinking
water tested for domestic suitability.
• February 25: Mr. McCulley and Mr. Dietz had conversations with Mr. Schoff and once
again explained the importance of following proper wastewater application techniques.
• March 6: DVD was submitted to Mr. Dietz by Mrs. Schreckengost documenting events
that took place on February 20.
• March 8: Mrs. Smith accompanied Tony Armstrong, Maintenance Supervisor for
M2P2-North Carolina, to collect a sample of the Schreckengost's drinking water. This
sample was sent to Midwest Laboratories (Omaha, NE) to be analyzed for domestic
suitability. Results from this analysis are shown in Attachment 1.
• March 12: Mr. Schoff met with Mr. Dietz to review the video taken by Mrs.
Schreckengost on February 20 and Mr. Dietz reiterated the unacceptable nature of his
actions.
Although the events previously outlined are completely unacceptable and in violation of our
Certified Animal Waste Management Plan and Swine Waste System General Permit No.
AWG100000, such an environmental challenge allows us the opportunity to fine tune our
policies and procedures concerning wastewater application and environmental stewardship.
Therefore, the following corrective actions were or will take place in regards to Violation 1 and 2
of NOV# NOV-2010-PC-0229:
Violation 1 Corrective Action:
As previously outlined in the events surrounding the incident, M2P2 staff responded swiftly and
took immediate action in ceasing wastewater application to prevent further ponding and runoff.
Mr. Schoff was strictly reminded of the importance of following proper techniques during swine
wastewater application, and he took full responsibility for his negligence.
M2P2 was very concerned about the integrity of the Schreckengost's drinking water supply and
offered to have a sample analyzed by an independent laboratory. Although there is no excuse for
the improper application techniques which led to a runoff and discharge event, the analysis
1615 Golden Aspen Drive I Suite 104 j Ames, IA 50010 1 p 515.598.4640 1 f 515.956.3226 1 www.m2p2.com
Colorado I Iowa I Oklahoma i North Carolina

Redefining woK1d
shows the Schreckengost water supply is still safe to drink. This statement was verified by
personnel at Midwest Labs who reviewed the analysis.
It should also be noted that the wastewater being applied during the violation was from the Cow
Island Lagoon. Since 2008 this lagoon has only stored swine wastewater from two small staging
facilities and therefore has very low nutrient values (Attachment 2). Because of this, the small
amount of wastewater allowed to discharge into the adjacent ditch appeared to have minimal
impact, according to DWQ samples taken on February 23rd. This statement was verified by Gary
Chapman, M2P2 consulting engineer from Enviro-Ag Engineering, Inc., who reviewed the
DWQ analyses. Again, this is not meant to condone or take away from the seriousness of this
event.
Violation 2 Corrective Action:
When swine wastewater application occurs in the future, applicators will be checked twice daily
and-ohservations-wile-noted-(tee ' a Sri. nt ?1 *^ a- w� ,
M2P_2's Waste -Utilization -Plan (Attachment-4) and North -Carolina -state -law. We- will-- ------
aggressively pursue Mr. Schoff to obtain his applicators license as soon as possible. -In the mean
time, Mr. Schoff will re -read M2P2's Waste Utilization Plan and sign a form verifying he
understands its contents.
Since M2P2 acquired New Colony Farms in 2001, our company has done everything to adhere to
local, state, and federal regulations. This is accomplished by using sound and proven manure
storage technologies, identification of suitable and adequate fields for nutrient application,
identification of environmentally sensitive aspects in fields, strict application standards and
thorough record keeping.
The DWQ analyses and consultations with Mr. Chapman lead us to believe that actions or civil
penalties against M2P2 regarding this matter should be minimized. However, we fully
understand the seriousness of this event and will work diligently to prevent this from happening
in the future. This is the first violation M2P2 has incurred and we hope our clean record helps
support our commitment to positive environmental stewardship.
Respectfully,
M21`2 / New Colony Farms, LLC
Mark A. McCulley
V.P. of Strategic Relations
1615 Golden Aspen Drive j Suite 104 1 Ames, IA 50010 1 p 515.598.4640 1 f 515.956.3226 1 www.m2p2.com
Colorado I Iowa I Oklahoma I North Carolina

I
Domestic Water Report Account 20391h s://www.
Report Number: 10-071-2241 40 % Midwest
!*
Reported to: M2132-NORTH CAROLINAr� bdmmftl��
LARRY DIETZ DOMESTIC WATER ANALYS
365 N PHELPS RD
COLUMBIA NC 27925-8426
DOMESTIC WATER ANALYI
Sample lD SCHRECKENGOST
Lab Number 1687336
comAims__reports/WDN rpt.php?parent=&rep...
Date Reported: Mar 12, 2010
Date Received: Mar 09, 2010
Date Sampled: Mar 08, 2010
Level
E)ceeds
EPA
Pro lems
ik ly
Potential
Problems
No
Apparent :Non-Detec#,
l
L`iimiitts—
JI
LProblemsE
J
'�'- _il
�_
—�I
i• - sl—
Analyte.
SODIUM
Na
CAL-;
CIUM
Ca
NIAG-
NESIUM
Mg
'
PH
NITRATE
NITROGEN
SUL-
FATE:
CONDUC- ;
TIVIT1r
TOTAL
DISSOLVED,
SOILDs
HARD-
NESS
TAL �
COLFORM.
P 7U0
IRON:
Fe
MANGA-
NESE
Mn
CHLO-
COPPER
RIDE
CI Cu
FLUO-
RIDE
F
PPm
PPm...,
..Pp!n. _
.
03
S a;mmhoslcm
-. _ ..
_...
�} PPm
gr/gallon
r
L
PPm :
Vim.
PPm
PPm...
PPm-
0.1Lo
�.-.. _._►
145
__J_
-
0.10,I003
_ .. it
001�.
__�_1
__..
_.
..d
[n.d
...
0
...
. -- ,--.__
...
�n_d
.....
I 6
0.1
Level;
Found
145
0.10 ,
0.01
7.44 `
n.d.
[n.d.
0.553 !
I
I
359
n.d.
F.
I
n d. �
0.031
n.d.
i
�
!
'
Cautions
Level
100
80 '•
30
6.519.0
10
!
400
0.75
500
20
s
0.3 I
�
Q.QS ;
2Q0
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;
Notes:
n rl - Nnt ngtArtarl
r

Bio-Solids Analysis for Account 20391 Page 1 of 1
Report
10-062-2048
Number:
Reported
M2P2-NORTH
to:
CAROLINA
365 N PHELPS
RD
COLUMBIA
NC, 27925-8426
Sample ID:
Cl 2
Project
PO:
G
DWEST Date Reported:Mar 03, 2010
'of 4b�+r r� �r1'ti��f Date Received:Feb 2b, 2010
114 eg
a� rya eh�+d
q
MANURE ANALYSIS Lab Number: 1683828
Bio-Solids Analysis Report
VIEW YOUR SUBMITTAL FORM
na ysis
utrients IlNutrients
Parameters
mmonium Nitrogen cM
as Received
1 153 ppm]l
ibs/acre inch
34.NJ
lbs/1000gais
1.29
Or anic Nitrogen tr„
1 105 ppm11
23.7
0.89
Total Nitroge
1 258 ppm
1 58.2 2.16
Phosphorus (P20$)
156 ppm
35.3 1.3
Potassium tK20j
393 ppmll
88.7]1 3.3
Sulfur (s)
10.5 ppm1
2.411 0.09
Calcium (Ca)
39.8 ppm1
9,911
0.34
Magnesium (Me) J1
21.7 ppm
4.911
El8
Sodium (Na)
Copper(co
10 3. 5 ppm
0.2 ppm
23.311 0.87
0.041 0.01
Iron (Fe)
2.1 ppm
0.4811
0.02
Manganese (w)
0.2 ppm1
0.05
0.01
Zinc(zr,)
2.9 ppm
O.U61 0.02
pH 11
7.2
rConductance ��
2.84 mSlcm
n.d.= Non Detected
Research suggest that when Lagoon Water is applied by irrigation, conductance
values of 6 mS/cm or less should be safe for corn and soybeans at all growth stages;
conductance values up to 12 mS/cm should be safe for soybeans and corn by late July.
https://www.midwestlabs.conVtims_reports/BIO—rpt.php?labnum=1683828 3/23/2010

Bio-Solids Analysis for Account 20391 Page 1 of 1
Report
10-062-2047
Number:
Reported
M2P2-NORTH
to:
CAROLI NA
365 N PHELPS
RD
COLUMBIA
NC, 27925-8426
Sample ID:
Cl 1
Project
PO:
Date Reported:Mar 03, 2010
` f "at,,kr Date Received:Feb 25, 2010
°Ot rer� 8a4e 2 rn3� _ Yam
MANURE ANALYSIS Lab Number: 1683827
Bio-Solids Analysis Report
VIEW YOUR SUBMITTAL FORM
Analysis 11Nutrients
Nutrients
Parameters
Ammonium Nitrogen (N)
as Received
1 183 ppm]l
Ibslacre inch
41.3
Ibs11000ga1s
1.55
Organic Nitrogen (N) 1 83 ppm
18-J71
0.70
Total Nitrogen (N) =1
266 ppm
1 60.0]1
2.25
Phosphorus (p,o3)
172 ppm
38.7
1.5
Potassium (Kzo3
404 ppm
1 91.211
3.4
Sulfur (s)
11.7 ppm
1 2.6
0.10
Calcium tcaa
42.7 ppm1
9.6
0.36
Magnesium (mg)
25.0 ppm
1 5.611
0.21
Sodium (Na) 11
107.0 pp-mll
24.1
0.9Q
Copper (co =1
0.3 ppmL
0.06
0.01
Iron (re) 1
2.8 PPM11
0.63
0.02
Manganese (Mn) 11
0.3 ppm1
0-06]1
0.01
Zinc (zn) 11 3.7 pp-m]l
0.83
Q.03
pH 11
7.1
2.89 mS/cm
Conductance
n.d.= Non Detected
Research suggest that when Lagoon Water is applied by irrigation, conductance
values of 6 mSlcm or less should be safe for corn and soybeans at all growth stages;
conductance values up to 12 mS/cm should be safe for soybeans and corn by late July.
https://www.midwestiabs.com/lims reportsBIO_rpt.php?labnum=1683827
3/23/2010

M2P2, LLC
Twice daily check on nutrient
Date Time Comments I (Initial
observed �

M2P2 QUALITY MANAGEMENT SYSTEM
Issue Date: band Application Total Pages 5
March 2010 New Colon SOP
Issued by: Environmental Approved by: M2P2 Management
48defini" World CA Manager
Core Process: Environment /z//#6�-
GZ"ftic,
Key Process: Compliance with State regulations Z;�'/ 7o—/
Objective: To properly land apply manure within State regulations and agronomic rates.
Flow of Steps:
+ Animal-manure-shall-be-applied-to-mec-t,-but-not-exceed,-the-nitrogen — - -
allocations for crop yields unless there are regulations that restrict the
rate of application for other nutrients.
• The primary nutrient limiting application is the nitrogen from animal
manure only. if nutrients from other sources such as commercial
fertilizers are applied they must be accounted for when determining
application rates and be recorded in the proper documentation
2. Application Rate Determination Based on Nitrogen and Records
Based on the permit, AW1890001, in no case shall land application
rates exceed the PIant Available Nitrogen rate for the receiving crop or
result in runoff during any given application.
The nutrient loading rates, as stated in the permit, shall not exceed the
nitrogen values for these identified crops:
o Corn 150 lbs/ ac
o Wheat --- 125 lbs / ac
o Soybean -. 135 lbs / ac
o Potatoes --140 lbs / ac
3. Application Rate Calculation
Whether applications are made with a tractor drawn applicator, a
gun/reel system, or a vacuum tank truck the calculation used to
determine the amount of waste applied is the same.
Determine application amount per acre using actual manure test results
and maximum nitrogen loading rates. The following calculation to
determine application rate (gal/acre) is as follows:
crop PANrequirement (lb) 1,000
Application Rate (gall acre) T. x
acre lb PANper1,000ga1
Lb: PANper 1, 000 gal. is obtained from the waste analysis report

M21>2 QUALITY MANAGEMENT SYSTEM
Issue Date: I Land Application Total Pages 5
March 2010 New Colony SOP
Issued by: Environmental Approved by: M2P2 Management
Redefining Worldia55 Manager
• Determine the width of application area per pass.
• Use inline gallonage flow meter to determine gallons per minute flowrate.
• Then use the listed equation to determine return speed of reel gun, tractor,
or truck. The equation used to determine the application amount of a
traveling gun, draghose system, or tank truck is:
Applicalian Volume acre — in _ 19.3xGPM
acre LNSP x TSPD
GPM is the flow rate of the "applicator" in gallons per minute
LNSP is the space in feet between the "lanes", "runs" or spreader width
TSPD is the travel speed of the gun cart or tractor in inches per minute.
• If multiple waste applications are necessary to meet the crop nitrogen
loading rates, the following equation can be used to identify how many
application events are necessary:
Number of Waste Applications =
Application Rate (acre — in / acre)
Application Yolume(in.)
Where: Application Rate is converted from gal/acre to acre-in/acre
4. Application Documentation
• Application records, maps of waste application fields, waste sample
analysis, and annual soil analysis for each field receiving waste
applications will be available at the farm.
• Records used to record application events, known as the IRR-1 and IRR-2
or SLUR-1 and SLUR-2, are further detailed as follows:
o IRR-1: Lagoon Liquid Irrigation Filed Record to be used to record
each application event.
o IRR-2: Cumulative Lagoon Liquid Application Field Record is to
record the total annual manure application to one field per crop
cycle. It provides for calculating the total nitrogen application to
the field and comparing it to the recommended nitrogen loading
rate.

M2P2 QUALITY MANAGEMENT SYSTEM
Issue Date: sand Application Total Pages 5
March 2010 New Colon SOP
Issued by: Environmental Approved by: M2P2 Management
19.0 Manager
Redefining WOO
o SLUR-1: Liquid Manure Slurry Field Record is to be used to
record each manure application event if the producer is using
slurry or pump and haul system.
o SLUR-2: Cumulative Liquid Manure Slurry Field Record is to
record the total annual manure application to one field per Crop
cycle with a slurry or pump and haul system. It provides for
calculation the total nitrogcn applia-a-fioun to-th-e- field and rempa . ring
—�-�- it-to_therer, mmende nitmuPn-loading-rate
5. Application Windows
• Manure shall not be apphed more than 30 days prior to planting of the
crop or forages breaking dormancy.
• Manure applications can also be applied to growing crops as long as the
fallowing restriction is upheld:
o Application of animal manure onto land which is used to grow
crops for direct human consumption (e.g, strawberries, melons,
cabbage, apples, etc.) shall not occur following the planting of the
crop or at any time during the growing season, or in the case of
fruit bearing trees, following breaking dormancy.
o Application of animal manure shall not occur within 30 days of the
harvesting of fiber and food crops for direct human consumption
that undergo further processing.
6. Maximum Application Rate (inches/hr)
Liquid manure shall be applied at rates not to exceed the soil infiltration
rate such that runoff does not occur offsite or to surface waters and in a
method that does not cause drift from the site during application. No
ponding should occur in order to control odor or flies.
Maximum application rates per soil types are as follows:
a Hyde, Portsmoth, Arapahoe, and Timothy = 0.40 in/hr
o Organic (muck) and Cape Fear soils = 0.35 in/hr
o Conetoe = 0.75 in/hr

M2P2 QUALITY MANAGEMENT SYSTEM
Issue Date; Land Application Total Pages 5
March 2010 1 New Colonv SOP
Issued by: Environmental Approved by; M2P2 Management
4edefining world 0
5� Manager
7. Manure Application Restrictions
• Manure applied to conventionally tilled bare soil shall be incorporated into
the soil within two days after application on the land. This does not apply
to no -till fields, pasture, or fields where crops are actively growing.
• Land application equipment will be calibrated at least once every three
years.
• Records will be maintained identifying when the equipment is calibrated,
calibration results, and any changes made to the system as a result of
•---Manure hall owe an s or sur ace wa er or s ali Ii not reach
wetlands of surface waters of the state by runoff, drift, manmade
conveyances, direct application, or direct discharge during operation or
land application.
• Manure shall not be applied on saturated soils, during rainfall events, or
when the soil surface is frozen.
• Manure shall not be applied in fall or winter for spring planted crops on
soils with a high potential for leaching. Manure loading rates on these
soils should be held to a minimum and a suitable winter crop planted to
take up released nutrients. Waste shall not be applied more than 30 days
prior to planting of the crop or forages breaking dormancy.
• Manure may be applied to land that is eroding at 5 or more tons but Iess
than 10 tons/acre/yr providing grass filter strips are'installed where runoff
leaves the field.
• There must be documentation in the form of land application agreements
for all land application sites not owned by the producer.
• Manure shall be applied on actively growing crops in such a manner that
the crop is not covered with manure'to a depth that would inhibit growth.
• Animal waste shall not be applied closer than 100 feet to wells.
• Animal waste shall not be applied closer than 200 feet of dwellings other
than those owned by the landowner.
• Waste shall be applied in a manner not to reach other property and public
right-of-ways.
• Manure application equipment should be inspected on a regular basis to
prevent breakdowns, leaks, and spills. A regular maintenance checklist
should be kept on site.
• Manure shall be tested within 60 days of utilization.
• Soil shall be tested at least annually at crop sites where manure is applied.
• Nitrogen shall be the rate -determining element.
• Zinc and copper levels in the soil shall be monitored and alternative crop
sites shall be used when these metals approach excessive levels.

ML
M2P2 QUALITY MANAGEMENT SYSTEM
issue Date:
Land Application
Fota] Pagcs 5
19,
March 2010
New Colon SOP
Issued by: Environmental
Approved by: M21`2 Management
�o
Red��ntnglNorl�
Manager
• pH shall be adjusted for optimum crop production and maintained.
• Soil and manure analysis records shall be kept for five years.
• Manure application records shall be maintained for five (5) years.
• No manure shall be applied in wind conditions that would cause mist to
reach surface water.
trt >, .
r�
Er For delivery Information visit our website at www.usps.coml)
ru ?oste $Er
ce�d Fee. XSd
� i'- '� of
p Realm Recelpl Fea ` 0
p ((Endorsement Required) 0
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C] (EndrGd)
Ln
rU Total Po-"
ru
senr To
NEWLANDS FARM
Ir NEW COLONY FARMS LLC
� � ' 4 365 N "PHELPS ROAD - ---
r` COLUMBIA NC 27925 ----

I have read and understand the Waste Utilization Plan. I agree to follow the standard
operating procedures listed within this document.
Signature of applicator:.
Printed Name of applicator:
General Manager signature:

DM Gaborato ection suits
County:
TYRRELL
-5VC
Sample ID:
AB88239
River Basin
�04 WA7�;9
PO Number#
10GO099
Report To
WAROAP
Q�
Date Received:
02/2412010
} r
Time Received:
08:28
Collector:
Q MAY
O
Labworks LoginlD
$MATHIS
Region:
WARE
Date Reported:
319110
Sample Matrix:
GROUNDWATER
Loc. Type:
WATER SUPPLY
Report Generated;
03/09/2010
Emergency Yes/No
Yes/No
MODCOC
+ f
D.
Loc. Deacr.: JIM S
I "" I
Location 1D:
WAROAPNLC
Collect Date: 0212312010 Collect Time:: 10:26
Sample Depth
Sample Qualifiers and Comments
N
Routine Qualifiers
For a more detailed description of these qualifier Codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
81-Countable membranes with <20 colonies; Estimated
NE -No established PQL
82- Counts from all filters were zero.
P-Elevated PQL due to matrix Interference and/or sample dilution
B3- Countable membranes with more than 80 or 80 colonies; Estimated
01-Holding time exceeded prior to receipt at lab.
84-Flltere have counts of bath >80 Cr 80 and < 20: Estimated
02- Holding time exceeded following receipt by lab
B5-Tao many colonies were present; too numerous to count (TNTC) _
PQL- Practical Quantitalion Limlt-subject to change due to Instrument sensitivity'
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
U- Samples analyzed for this compound but not detected
J3-The sample matrix Interfered with the ability to make any accurate determination; Estimated ,.
Xi- Sample not analyzed for this compound r-----^—^•-^�^""`- � ,f
JB-The lab analysis was from an unpreserved or Improperly chemically preserved sample; Estimated
W-The component has been tentatively identified based on mass spectral library search and has an estimated value
MAR 1 7 2010
LAB .• .; =it
r
Laboratory Section 1523 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 1 of 2"•-• �'

GROUNDWATER FIELD/LAB FORM
Location code
SAMPLE TYPE
County 7ti j-lrwi ❑ Water
Quad No Serial No. ❑ Soil
Lat. Long. ❑ Other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, WaRO, WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, Courier, Hand Del., Other:
Collector(s):_1). MdJ Z — /l7 -5,fZge,� Date 'r 3-/( Tim,
FIELD ANALYSES j
PH 400 Spec. Cond.94 at 250C
Temp.,0 °C Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOO 310 mg1L
COD High 340 mg1L
COD Low 335 mg1L
Coliform. MF Fecal31616 1looml
Coliforw MF ToW 31504 1100mi
TOC 660 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mglL
Carbonate 445 mglL
Bicarbonate 440 mg1L
Carbon dioxide 405 mg1L
Chloride 940 mg1L
Chromium: Hex 1032 ug1L
Color. True 80 CU
Cyanide 720 mg1L
Lab Comments
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
1D(_ 0091 X)
i'`��i Lab Number
El Routine
❑ Emergency
Date Received c�' a 8 Time:
J Rec'd By: From:Bus, oune , Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
_ Purpose:
/d : a6- Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
Owner Siv! (viral, aL,
Location or Site ;T,,, - GrJ& /4 - It
Description of sampling point &n,v
Sampling Method-G,r^/., Sample Interval
Remarks umo. a6 i erc.f—
{Pumping lime, air temp., etc )
Diss: Solids 70300 mg1L
Fluoride 951 mg1L
Hardness: Total goo mglL
Hardness (non-carb) 902 mg1L
Phenols 32730 ugll
Specific Cond. 95 NMhoslcm
Sulfate 945 mg1L
Sulfide 745 mglL
Oil and Grease mg1L
NH3 as N 610 mglL
TKN as N 625 mg1L
NO2 NO3 as N 630 mglL
R Total as P 665 mglL
Nitrate (NO3 as N) 620 mg1L
Nitrite (NO2 as N) 615 mglL
Ag-Silver 46566 u 1L
AI -Aluminum 46557 u 1L
As -Arsenic 46551 u 1L
Ba-Barium 46558 u /L
Ca -Calcium 46552 mg1L
Cd-Cadmium 46559 u IL
Cr-Chromium 46558 u 1L
Cu-Copper 46552 u IL
Fe -Iron 46563 u 1L
Hg-Mercury 71900 u IL
K-Potassium 46555 mg1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u IL
Na-Sodium 46556 mg1L
Ni-Nickel u 1L
Pb-Lead 46564 u IL
Se -Selenium u 1L
Zn-Zinc46567 u IL
GW-54 REV, 7103 For Dissolved Analysis -submit filtered sample and wdte'DIS' in block.
i
Pesticides
Acid Herbicides
Semivolatile
Volatile
LAB USE ONLY '
Temperature on arrival (°C):

Sample ID AB55239
.PVC (D`iNQ Laboratory Section Wsufts
'Location ID: WAROAPNLC Collect date: 02l2312010
Loc. Descr.: JtM S Collect Time:: 10:26
Visit ID
CAS 8. Analyte Name PDL Result Qualifier Units AnslysUData Approved By /Date
Semple temperature at racelpt by lab 1.2 •C DSAUNDERS SMATHIS
Method Reference 2124110 2124110
NUT
NI13 as N In liquid 0.02 OAO mg1L as N MAJAYI CGREEN
Method Reference Lac10.107-06-1-J
2125110
312/10
Total KJeldahl N as N in Oquid
0.2
0.56 mg1L as N
MOVERMAN
CGREEN
Method Reference Lachatl07-05-2-H
2126110
M110
NO2+NO3 as N In liquid
0.02
0.02 U mg1L as N
MAJAYI
CGREEN
Method Reference LacIO-107-04.1-c
2125110
3W10
Phosphonis total as P In liquid
0A2
0.25 mg/L as P
GBELK
CGREEN
Method Reference Lac10-115-01-1EF
3010
3/9110
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699.1623 [phone] Page 2 of 2

ti
County:
Tyrrell
River Basin
Report To
WARQSP
Collector:
MM SALYER
Region:
WAR
Sample Matrix:
SURFACEWATER
Loc. Type:
Emergency Yes/No
COC Yes/No
I Location ID: WAROSPNLC
Visit) D
Loc, Descr.: sftM WEL•CA-HORE'WE L PUMP
Collect Date; 0212312010 Collect Tlme:: r
Sample Oualifiers and Comments
Sample ID:
AB55088
PO Number #
GWID0167
Date Received:
OV2312010
Time Received:
14:10
Labworks LoginlD
LBUCK
Date Reported:
316/10
Report Generated:
0310812010
.
315]ja
Sample Depth
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is c PQL and >MDL
B1-Countable membranes with e20 colonies; Estimated
NE -No established PQL
B2- Counts from all filters.were zero.
'03= Countable,membrones'with more than 60 or 80 colonies; Estimated
84-Filters have counts of both >60 or 80 and < 20; Estimated
B6-Too many colonies were present; too numerous to count (TNTC)
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
N 1-The component has been tentatively identified based on mass spectral library search and has an estimated value
P-Elevated PQL due to matrix interference and/or sample dilution
01-Holding time exceeded prior to receipt at lab.
Q2- Holding time exceeded following receipt by lab
PQL- Practical Quantization Limit -subject to change due to instrument sensitivity
U. Samples analyzed for this compound but not detected
X1- Sample not analyzed for this compound
WARD ',• , , .i I �!
a
Laboratory Section» 1623 Mall Service Center. Raleigh, NC 27699.1523 [phone] Page 1 of 2

11-1
oROUNDWATER FIELDLAB FORM
L�cjtion code
K!nsirm H'), Fed. Trust, Central 00:tvr
N--irt6i Catalinn
Dup'lrwv! c:i-::vjmme;it arit Naturm
Dale
.2'/
Propm !
f.30S. (:.L)LIliQ,. rialbLT., of",,:
S. e'Le Ie Timej 3,C.Ainn Compla.004-Ir, I T,inc�i -U,;"l s1w Study. y, F -4 TfLl,�, C
F!EID ANAYSCx2
Spec -77
e r--. 1-� 'C Cuor puiw tl-
. ..... .. ..
LAUCRATORY ANALYSES
D'ss IMOND 1_
A I Alu'-",num -f'] WA
0q) I i f) ,l rl,,, u Tr. 1,00 A-- Artp2ti.c 4f; 55
1: wA: AT r 'I I C. 16 eWoll-, rik-,ii�n 902 R%fllkm 465�:'F.
•
_,615 5C-4 32 /"a In 4,555" ii
f r, F,% C' rrq�L Sr-A'Az: Crr-d K�S I I
7r. NTU sWa:e 914G
t SQIW%: 74 5 44Sfit
- ----------
fi.:Ifl
mgtL
Ai I(j fli 41 t- mn miarganolpv.rs or r
Ca t r i la I d 4 5 PIML hiN,, as N cliff 1 Na
J Ktt-
440 t3 i TKN as N A�i mwL
'd-1 d f! , Ll NO. Z5 Pi U"D mnll. -rf�C-4
07'av�e 9,10 Fl TrM: as P 60 I'e
Cr1rCm%- "�f" }Clj? Wrale 'NQ,as Nj 620 r -7m': 465C, T
Coc'! r.,UL: 80 Co 1")('15 LAB USE ONLY
olf 7 27J i ET r VmPf:�Iule Of 3ffiva) ("C)
Lab C ow fil C-nt
f'cv 'rRTT'-' c. 0 noved Aria3ysis slLrne Mlerf-
S-minle ;;md wi'A*m�' n. twi

`.f
Sample ID AB55088
NC (D`i�VQ, Ga6oratory Section IResufts
Location ID: WAROSPNLC Collect Gate: 0212312010
Loc, Dew.: JIM WELL A HOME WELL PUMP Collect Time:: 10:25
Visit ID
CAS M Ann" Name PQL Result Qualifier Units AnalysVDats Approved By (Date
Sample temperature at fecelpt by lob 1.0 'C LBUCK SMATHIS
Melhod Reference 2J23110 2125/10
Coliform, MF Fecal In liquid 1 1 B2 CFU1100ml LBUCK ESTAFFORD
Method Reference APHA9222D.20ih 2/23110 3/3110
Laboratory Section 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 7333908 Page 2 of 2

NC DM LaboratoaSection &sults
County: Tyrrell
Sample ID:
AB66086
River Basin
WA7F�
PO Number#
GW100167
�[}f
Q
Report To WA S
d�
Date Received:
OV23/2010
j
Time Received:
14:10
Collector. M SALYER
"4
Labworks LoginlD
LBUCK
Region: WARQ
Date Reported:
3/8110
Sample Matrix: SURFACE11ifATER
Loc. Type:
Report Generated:
0310812010
Emergency Yes/No
VisitlD
COC Yes/No
Lac. Descr.: JIM WELL A HOME WELL PUMPtJ
✓
Location ID: WAROSPNLC
Collect Dates 02l2312010 Collect Time:: 10:25
Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwgiab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is c PQL and ?MDL
B1-Countable membranes with c20 colonies; Estimated NE -No established PQL
132- Counts from all filters.were zero, P-Elevated PQL due to matrix Interference andlor sample dilution
133- Countable membranes with more than 60 or 80 colonies; Estimated
41-Holding time exceeded prior to receipt at lab.
B4-Filters have counts of both >60 or 80 and c 20; Estimated 02- Holding time exceeded following receipt by lab
85-Too many colonies were present; too numerous to count (TNTC)
POL-Practical Quantftation Limit -subject to change due to Instrument sensitivity
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
U. Samples analyzed for this compound but not defected
J3-The sample matrix Interfered with the ability to make any accurate determination; Estimated
J8-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Semple not analyzed for this compound
N1-The component has been tentatively identified based on mass spectral library search and has an estimated value
WARD MAR 1 7 2010 J'
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 2 1

�C,:WROUNDWATER FIELD/LAB FORM Dvw,,im ,�`Luvrrwl:tlerit HIM NAMil Resoufce:z
DIVIS H-) N Oj� CUM, I Ty-GROt)NL)%.1qATF.-R
Lacajon code
APCE'TYPE MORITY
V./ater Roulino
3ef ial No. soil L; DalH Received T In i c-
Long ❑Other R�:C,41 CRY �X,6 1
Chain of(',iiiiwi,
,rf•,- ARO, FRC. MRO, h. Di�;i '-jilry BY:
Kinston f:O. Fed. Trust, Centrai 00 '-"(iit?r
Dxe Time ha"'Olinn, Complaiw. comphrncf-, (Icmirirlo Study, Federal T:LJSt.
FlPt D )CNALYSES
sc f:or'0
25°C Location i Iite L
I f- rn crier
- — ------- Dmuiolin-i r)f,;i-.ro:br1g puirit 11
Sampiing int1wN.'c11
Fjed
-----
LABOR ?'ORY ANALYSES
i tlrl 1 3itl w.j:L 'Aq 5p[ver diS4:C-
wlk 01q;IfI001101me
cor.,,+qr, s io IngI Fiticna. "51 P19,L At-AlurvIT)LIM 46557
0 F L..�w 'j,� A-�-Art;en,C Pe-sIicicts
I I s Tc,
Aoo I
M7 POK.'al 116 16 mr�5 002, Mq'i. fia R,:.f.orr. 4655i;,
I!,fr, f
tfj rrT1
Orr.1 t'a
T,j,palily 7P NTQ Suil te '145
Mf,rJ_150110c 745 j L
O'l aml M91 Hg W-tcury I 1906
pli A 0.1 0.11s 4fi�55
�A i.�Iodj 1(� prH 4 -'-fi m%o, Mg 46954 ... AI 415 fligjL klar,,ganr.�� 4K565
..{ .. ..., -- -- n,
g�L TKN 14 (125
mq& N 610 171,11 Gas -7� -
P!j-_PTEX
CA -bon 1=ArjIp. 4u,� .7 NO, NO�.:m N V-10 rrqt, Pb-Ltiad A61564
cv,�2rlre �40 mgkl I P Tr)1a? as P 50, rngl. St,-Suiumum
He, )Vi, N,traleN0,as %; 620 mall
Cu W5 mg;L LAB USE ONLY
remperalure on arrival rc),
Lab Corlmerljc
f,WA' Rr.-v 1.10 --c, Dsso!ved Analysis submd ftltrqee c.Imp14- Nnclvx,lq 'MZ' -n tvorl

Sample ID AS55088
NC �DWQQ Lador'atory Section �sults
Locatlan ID: WAROSPNLC Collect Date: 0212312010
Loc. Deacr.: JIM WELL A HOME WELL PUMP Collect Time:: 10:25
Visit ID
CAS # Analyte Name } PQL Result • Quallfier Units Analyat[Date Approved By /Date
Semple tempereture at receipt by;b 1.0 'C LBUCK SMATHIS
Method Reference 2rMl0 2125110
ColHorm, MF Fecal In liquid 1 1 B2 CFU1100ml LBUCK ESTAFFORD
Method Reference APHA9222D-20th 2t23110 3010
Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27899-1623 [phone] Page 2 of 2

County:
TYRRELL
Sample ID:
ASS5244
River Basin
WA7hi
�
PO Number p
10G0104
Report To
WAROAP
�(
Q� ¢
Date Received:
0212412010
?_
Time Received:
08:23
Collector:
p MAY
0 '<
Labworks LoginlD
SMATHIS
Region:
WW ROO
Date Reported:
319/10
Sample Matrix:
GROUNDWATER
Loc. Type:
WATER SUPPLY
Report Generated:
0310912010
Emergency Yes/No
COC Yes/No
VizitlD
I v
Loc. Descr.: NJe2 NEW COLONY Q " i`-C
Location 1D:
WAROAPNLC
Collect Date: 0212312010 Co11ed Time;; F14.00
Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www,dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < POL and >MDL
BL-Countable membranes with <20 colonies; Estimated
NE -No established POL
B2- Counts from all filters were zero.
P-Elevated POL duo to matrix interference andlor sample dilution
B3- Countable membranes with more than 60 or 80 colonies; Estimated
01-Molding time exceeded prior to receipt at lab.
B4-Filters have counts of both >60 or 80 and c 20; Estimated
02-Holding time exceeded following receipt by lab
B5-Too many colonies were present; too numerous to count (TNTC)
POL- Practice! Quantization Limit -subject to change due to instrument sensitivity
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
U- Samples analyzed for this compound but not detected
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
X1- Semple not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
NI -The component has been tentatively identified based on maze spectral library search and has an estimated value
LAB
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27099-1823 [phone] Page 1 of 2
' i

North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
'DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code SAMPLE TYPE SAMPLE PRIORITY I D f0a
County �if�Zl ❑ Water ❑ Routine Lab Number ?? f J
Quad No Serial No. ❑ Soil ❑ Emergency Ca. Im Date Received Tim 95-
Lat. Long. ❑ Other Rec'd By: From.Bus,' Courier, and Dei.,
❑ Chain of Custody Other'.
Report To: ARO, FRO, MRO, RRO, aR0 iRO, Data Entry By: Ck:
WSRO, Kinston FO�rust, Central Off., Other: Date Reported:
Shipped by: Bus, rl and Del., Other:' Purpose:
Cohector(s): 'rm Date d Time 0,,-9 *,o Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust
FIELD ANALYSES Owner t`I°° al
pH 400 Spec. Cond.94 at 25°C Location or Site .
Temp.,o °C Odor Description of sampling point
Appearance Sampling Method Sample Interval
Field Analysis By: Remarks_ I Purno. brer. etc.)
LABORATORY ANALYSES
800 310 mglL
COD High 340 mgIL
COD Low 335 mglL
Coliform: MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100ml
TOG 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg/L
pH 403 units
Alkalinity to pH 4.5 410 mg/L
Alkalinity to pH 8-3 415 mg1L
Carbonate 445 mg1L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg1L
Chloride 940 mg1L
Chromium: Hex 1032 ug1L
Color: True 80 Cu
Cyanide 720 mg1L
Lab Comments
Diss. Solids 70300 mg1L
Fluoride 951 mg1L
Hardness: Total goo mglL
Hardness (non-carb) 902 mg1L
Phenols 32730 ugll
Specific Cond, 95 NMhoslcm
Sulfate 945 mg1L
Sulfide 745' mg1L
oil and Grease mg1L
NH3 as N 610 mg1L
TKN as N 625 mglL
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg1L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit fittered sample and write'DIS' in block.
(Pumping lime, air temp„ etc )
Ag-Silver45566 u 1L
AI -Aluminum 46557 u 1L
As -Arsenic 46551 u 1L
Ba-Barium 46558 u IL
Ca -Calcium 46552 m IL
Cd-Cadmium 46559 u IL
Cr-Chromium 46559 u IL
Cu-Copper46562 u 1L
Fe-tron 46563 u IL
Hg-Mercury 71900 u IL
K-Potassium 46555 mg1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u /L
Na-Sodium 46556 m IL
Ni-Nickef u IL
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zr)-Zinc 46567 u IL
Or anochlorine Pesticides
Of an0 has horus Pesticides
Nitrogen Peslicides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics(VOA bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (°C):
Other:
r

NC (DWQQ Ga6oratory Section Results Sample ID AB55244
Location ID: WAROAPNLC Collect Date: 02/2312010
Loc. Descr.: N2P2 NEW COLONY Collect Time:: %00
Visit 10
1ple temperature at receipt by lab
Method Reference
1.2
DSAUNDERS SMATHIS
2124110 2724110
NUT
NH3 as N In liquid
0.02
1:i
mg& as N
MAJAYI
CGREEN
Method Reference Lac10.101-06.1-J
2125110
3010
Total IQeldahl N as N In liquid
0.2
1 4 3- ,.
mgA- as N
MOVERMAN
CGREEN
Method Reference Lachat107-0&2-H
2f26110
312110
NO2+NO3 as N In liquid
T 0.02 ....
^9 2 =
mg& as N
MAJAYI
CGREEN-
Method Reference Lac10.107.04.1-c
2J25110
3010
Phosphorus_twtl as P In liquid
0.02
O:SS`,
rng& as P
GBELK
CGREEN
Method Reference Lac10.115-01-IEF
YV10
319110
N
Laboratory Section 1023 Mail Service Center, Raleigh, NC 27699.1623 [phone] Page 2 of 2

.r
County: JOREL6
River Basin
Report To WAROAP
Collector: D MAY
Region: WAR )t
Sample Matrix: GROUNDWATER
Loc. Type: �P
Emergency Yes/No
COC Yes/No
Location ID: WAROAPNLC
. WATF�
oti� P.
h
O `K
VIsRID
Loc. Dsscr.: !gE2 NEW COLONY
Collect Date: 0212312010 Collect Time:: 14:00
Sample Qualifiers and Comments
Sample ID:
PO Number#
Date Received:
Time Received:
Labworks LoginlD
Date Reported:
Report Generated
Sample Depth
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported Is the average of two or more determinations
N3-Estimated concentration is < PdL and >MDL
81-Countable membranes with <20 colonies; Estimated
82- Counts from all filters were zero,
NE -No established POL
B3- Countable membranes with more than 80 or 80 colonies; Estimated
P-Elevated PQL due to matrix interference and/or sample dilution
o1-Holding time exceeded prior to receipt at lab.
84-Filters have counts of both >60 or 80 and < 20: Estimated
95-Too many colonies were present too numerous 10 count (TNTC)
02- Holding time exceeded following receipt by lab
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
PQL- Practical Quantitation Limit -subject to change due to Instrument sensitivity
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated
U- Samples analyzed for this compound but not detected
-
.16-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
X1- Sample not analyzed for this compound
NII-The component has been tentatively Identified based on mass spectral library search and has an estimated value
LAB
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27699.1623 (919) 7334908
AB86244
IDG0104
02/24/2010
08:25
SMATHIS
3/9110
D310912010
31
MAR 1 7 2010
Page 1 of 2
._ Ur-FICE

North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
,Location code SAMPLE TYPE SAMPLE PRIORITY I D f o q t e ❑ 5> C
County! � ❑ Water Routine Lab Number Quad No Serial No. ❑ Soil ❑ Emergency Dale Received 10 Tim ;t� Lat. Long. ❑ Other Ree'd By: From:Bus, Courier, and Del.,
El Chain of Custody Other: kv
Report To: ARO, FRO, MRO, RRO, aR0 IRO, Data Entry By: Ck:
WSRO, Kinston F�rust, Central Off., Other: Date Reported:
Shipped by: Bus, ri and Del., Other: Purpose:
Collector(s): �Trn _ �S'. _ _ DateR=a;LL Time t),�2 ; oD Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner t`rcle°gal
pH 40o Spec. Cond.94 at 25°C Location or Site c
Temp.t0 °C Odor Description of sampling point
Appearance Sampling Method Sample Interval
Field Analysis By: Remarks (FlUmo, bik'°`�
LABORATORY ANALYSES (Pumping time. air temp., etc.)
BOO 310 mg1L
COD High 340 mg1L
COD Low 335 mg1L
Coliform: MF Fecal 31616 1100ml
Coiiform: MF Total 31504 1100ml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg/L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg1L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg1L
Chloride 940 • mg1L
Chromium: Hex 1032 ug/L
Color: True 80 Cu
Cyanide 720 , mg
Lab Comments
Diss. Solids 70300 mg1L
Fluoride 951 mg1L
Hardness Total900 mglL
Hardness (non-carb) 902 mg1L
Phenols 32730 ug/1
Specific Cond. 95 uMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
NH3 as N 610 mg/L
TKN as N 625 mg1L
NO2 + NO3 as N 630 m91L
P: Total as P 565 mg1L
Nitrate (NO3as N) 620 mg1L
Nitrite (NO? as N) 615 mg
Gw-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "D1S' in block,
Ag-Silver 46566 u !L
Ai -Aluminum 46557 u !L
As -Arsenic 46551 u !L
Ba-Barium 46558 u !L
Ca -Calcium 46552 m !L
Cd-Cadmium 46559 u !L
Cr-Chromium 46559 u !L
Cu-Copper 46562 u !L
Fe4ron 46563 u !L
Hg-Mercury 71900 u !L
K-Potassium 46555 m !L
Mg -Magnesium 46554' m 1L
Mn-Manganese 46565 u IL
Na-Sodium 46556 mg1L
Ni-Nickel u 1L
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zn-Zinc 45567 a 1L
Or anochlorine Pesticides
Or ano hos horns Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivotatile Organics
TPH-Dieset Range
Volatile Or anics(VOA bottle
TPH-Gasoline Range
TPH-13TEX Gasoline Range
LAB USE ONLY !
Temperature on arrival (°C): [

X DWQ La6oratory Section &sufts Sample ID AB55244
Location ID: WAROAPNLC Collect Date: 02/23/2010
Loc. Deser.: N2P2 NEW COLONY Collect Time:: 14:00
Visit 10
CAS k Analyte Name PQL Result Qualifier Units AnalystlDate Approved By /Date
Sample temperature at receipt by lab 1.2 T DSAUNDERS SNdATHIS
Method Reference 2124110 2f24110
NUT
NH3 as N In liquid
0.02
1.1
mglL as N
MAJAYI
CGREEN
Method Reference Lac10-107-M-1-J
2125110
3010
Total K)SIdahl N as N In liquid
0.2
4.3
mgk as N
MOVERMAN
CGREEN
Method Reference LacKa1107.0&2•H
2rA10
3/2110
NO2+NO3 as N In liquid
0.02
9.2
mg1L as N
MAJAYI
CGREEN
Method Reference Lac10.107.04.1-e
2125110
3010
Phosphorus_total as P in Ilquid
0.02
0.55
mg1L as P
GBELK
CGREEN
Method Reference Lacll)-11541AEF
312110
319110
Laboratory Section>> 1623 Mall Service Center, Raleigh, NC 27899-1023 [phone] Pape 2 of 2

County: Nrte11
Semple Ip:
A855069
RlverBasin
ys}�WA7EH
P�
PONumber q
GW100168
Report To AW ROSP
O�
Date Received:
02x2312010
h
r
�
Time Received;
14:10
Collector. M SALYER
`a
Lebworks LoginlD
LBUCK
Region: WARO
Date Reported:
318110
Sample Matrix: SURFACEWATER
Loc. Type:
Emergency Yes/Na
Report Generated:
0"0"10" 0
VIsItID
COC Yes/No
,4eA
Loc. Dow.: NEW COLONY
Location ID: WAROSPNLC
Collect Date: 02f23/2010 Collect Time:: 10:60
Sample Depth •BBT
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www,dwglab.org under Staff Access
A -Value reported is the average of two or more determinations N3-Estimated concentration is a POL and >MDL
131-Countable membranes with <20 colonies; Estimated
NE -No established PQL
132- Counts from all filters were zero.
P-Elevated PQL due to matrix interference and/or sample dilution
B3- Countable membranes with more than 60 or 80 colonies; Estimated
Qt-Holding time exceeded prior to receipt at lab.
134-Filters have counts of both >60 or 80 and < 20; Estimated
02- Holding time exceeded fallowing receipt by lab
B5-Too many colonies were present; too numerous to count (TNTC)
PQL- Practical Quantkation Limit -subject to change due to instrument sensitivity
J2- Reported value failed to most QC criteria for either precision or accuracy; Estimated
U-Samples analyzed for this compound but not detected
4-The sample matrix Interfered with the ability to make any accurate determination; Estimated
X7- Sample net analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
NI -The component has been tentatively identified based on macs spectral library search and has an estimated value
u
WARD
I
MAR 1 7 2010 �
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27620-1623 (910) 7333908 Pape 1 of 2
G,'Fi4E

m
I CROUNDW, TER FIELD/LAB FORM
Location code _
Ouad No__
_ierial NO-
!_Ung —
Report To: ARC) 's:i; 1.11:C}, RRO,�l�C aF�Q ANIRO.
VUSRO, Kinslon t C; F a:c. 'I nisi Central Off ,Other:
Shipped by: fails..;, :nor 's�1.f51 D '. Olher:� --
Collsctor(sl:lJ:rz._-_�_..�:::�':`...::�;.�.._ L7ate�.�
FIELD ANALYSE.;
Norm C.:: cl n:,
/� �1 Crepartmem of Environml of :• '.! rJB!417,1 P,ut'UurLOS
/7 % � r _!___ .._ 01V;! IONI OF WATER QUALITY cG ;:":I,r1CWATER SECTION
..TYMESP,h1 L1 Fr I:_Ir:i.
Lab Num6er�:Cl%r
Date Recelveu Time /�
h'? Gt 1 r i c `
Rec d f3YQJ� l"rom Eitls. C o+anFr, L%e�I.
�i of Custody ! Other: —_--
-- Data Entry fey
-.-.--- Dale Reportr,rl --- ----------_.._ .._
YurposF':
rlinldCe,rLUST:PI: ef Trust, ]ti[f: a
Suer,. cued.," 25
Odor
Appearance
Field Analvs+s Py _�—
Oviner
LoCatio+t of Situp tom..•. I•: ,' _
Description of sampli:k; p0irjl.
Sampling fvtethod C=; �`,_ _
Remarks ---
LABORATORY ANALYSES
130D 3Ur miT:d ! - nl 9 In mg1L A:tS iurr
IL
rnq'L hlr,on7. ysl mg — AI.Alur 1 n
_..__...... _ . - _ .-.. - . ---- --- - --
PIf'
"`...
} :L F�ache,s-Toler Cr rttl ,As.F•xn1 �r,l
+ mg I = ;L
GrvlSsalmrahf :1ri I; :--- } { iHalrirw;5lnr;.ri.[arnit•i:'1 mp'I. I I j14;1.11ar�um �' 4 u?L
r1I (T''Iln �rF lq•;i+!1:f]� ii(}t'1n,1 j ' NhC IGIS 3� r t:�il IE',a. C-id,_t,.:n6l S.7.
of '�
_ ..... _9
'I ()c olo my;t II til!ec= r [ U r c; unAhos^c^ Cr..r;,anm>unr
Tmb.olty ' 1JilJ _I Sultale (,45 1110A I t.r-Ci:r_m�•.m �ija54 L
i Res:cue,Tc•1.1,->.,sr.n F,:..-,J_ n,}rl lSuthrvinb mgR i #r:u.CaGUers,;-.G
i._....-i-t)d MI 1 ,y ---•--�-._ fti�r� ±i,� h+ru;u-v tI�'ylo urrL
pr140' 11rkM I I W K•F'r,!,egysuu, SE5
a A 1 4t , Grn'• ,u : 1 �
.l Alhahnlry W F11 $:: 41;. :rgrh, i _ _ I ! Alr, hL;nr�an?.•;.c 4?5�:5 u ;L
,I ;,; i A45 bc+,_ �1.3r1_ i ;—....S--.y_._.._.« ._....._.__._ .•.••.i
�•r } NIi�s _N 1i111 nygl I NN•4a�!�s:rnlri`,�5 ,_,qil.
Ae irhun,llr; 44,G mgL TKN as to 6275 ma' L - N, NiJ i.el - ua L
r
Carbon ❑,0aic'.e.105 mp.1L JG; • Nc' as t•I Gou mg1L PL1.Le.1t�t-IG:rs+:
_.46!_-- U .._..._._..__._.-__._ Tumt as rnctL $r.,;t•1e:,1u^^ urrL
L hlGKtdZ (•Sr: - � IT7 1L P- ,
IChlomrum He.T 10:2 g„ - -} ---- 9•
c cor. Truf: Frl- -- - - Cu _ Wrap
LVQ, as N VS m L 2 n.Z1n•, at °G,
trltP tNO; a5 NI fits mp;L
-- -- - - ---- _
Cyanir}e 720 nygrL I !— —
L�lh Comments
OW-114 HF: V 1 t+};i 1:of 1)P^.salvM An@I}'Si$-sulamrt 61iwred sAmple and route '�,15' 1^ bkcck —�
Sample interval
�_,
Acla tiE!U1r1Cu1 _... _...._,__._._.—..._
�.» _-• _-'_—_
l
Volaulo firaa niu. IV(lA RC,ri1B)—•,...___.. i
---_— -_ ....T— _....._...
7PN-Gaeahre Ranip
_
TPl I-OTE>< Gasoline Rare _
Tumperaturc, er1 arrival {°C):
a?

NC DWQ La6oratory Section Wsufts Sample I❑ AB55089
Location ID: WAROSPNLC Collect Date: 02123/2010
Loc. Descr.: NEW COLONY DITCH 1-A Collect Time:: 10:50
Visit ID
CAS # Analyte Name PQL Result Quallflar Units Analyst/Date Approved By 1Date
Sample temperature at necelpt try lab 1.0 'C LBUCK SMATHIS
Method Reference 2123110 212W10
SOD, f'rDay In liquid 2 5.3 mgh MSTARR ESTAFFORD
Method Reference APHAS2108 2rM10 316110
ColHmm, MF Feral In liquid 1 240 CFU1100ml LBUCK ESTAFFORD
Method Reference APHA9222D-20th 2l23110 313110
Laboratory Sectlon» 11623 Mail Service Canter, Raleigh, NC 27699-1623 (919) 7334908 - Page 2 of 2

a
County: TYRRELL
River Basin
Report To WAROAP
Collector: D MAY
Region: WARO
Sample Matrix: GROUNDWATER
Loc. Type: WATER-SUPPJ-Y
Emergency Yes/No
COC Yes/No
I Location ID: WAROAPNLC
WA7�C�4
ti
? y
1? Y
VisitlD
Loc. Descr.: NZP2 NEW C
Collect Date: OV2312010 Collect Time:: 10:50
Sample Qualifiers and Comments
Sample ID:
A955240
PO Numberti
10G0100
Date Received:
OV2412010
Time Received:
08:25
Lebworks LoginlD
SMATHIS
Date Reported:
3010
Report Generated:
03109/201 D
116
Sample Depth
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwqiab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-E3timeted concentration is < PQL and >MDL
B1-Countable membranes with <20 colonies; Estimated
NE -No established PpL
82- Counts from all filters were zero.
P-Elevated PQL due to matrix interference andlor sample dilution
B3- Countable membranes with more than 60 or 80 colonies; Estimated
O1-Holding time exceeded prior to receipt at lab.
B4-Filters have counts of both >60 or 80 and � 20; Estimated
Q2_ Holding time exceeded following receipt by lab
B5-Too many colonies were present; too numerous to count (TNTC)
PQL- Practical Ouantitation Limit -subject to change due to instrument sensitivity
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
U- Samples analyzed for this compound but not detected'
J3-The sample matrix interfered with the ability to make any accurate determination: Estimated r
X1-Sampie not analyzed for this compound -
JB-The lab analysis was from an unpreserved or Improperly chemically preserved sample; Estimated
W-The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB
/J i �7
MAR 1 7 2010
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1823 (9191 7333908 Page 1 of 2 ' ' C1MCE

p North Carolina
GRtOUNDWATER FIELD/LAB FORM I
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code AS MPLE TYPE
CountyTiv l f/ ❑ Water
Quad No Serial No. ❑ Soil .
Lat. Long. ❑ Other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, 42aR0 WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus-,qZjr Hand Del., Other: Purp�
CoIIector(s): _j-_ -- _ /!I Z/7 lam✓ Dated -a3 - ZQ Timed
SAMPLE PRIORITY
❑ Routine
❑ Emergency
Ib(_O) 00 A�__lJ �j a({V
Lab Number
Date Received '� I"(G Time: a
Rec'd By: From:Bus, aurier and Dal.,
Other:
Data Entry By, Ck:
Date Reported:
Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner a- � i""'g°"el
PH 400 Spec. Cond.94 at 250C Location or Site eL,,
Temp.,o °C Odor Description of Sampling point 617
_
Appearance Sampling Method G-y-•A.h Sample Interval
Field Analysis By: Remarks umn abTTalt.I '
LABORATORY ANALYSES (Pumping lime• air temp, etc)
BOD 310 mg1L
COD High 340 mglL
COD Low 335 mg1L
Coliform: MF Fecal 31616 1100ml
Coliform� MF Total 31504.. Noomt
TOC 680 mg/L
Turbidity 76 NTU
Residue, Total Suspended 530 m91L
pH 403 units
Alkalinity to pH 4.5 410 mgfL
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 m91L
Bicarbonate 440 mglL
Carbon dioxide 405 mg1L
Chloride 940 mg1L
Chromium: Hex 1032 ug1L
Color: True 80 CU
Cyanide 720 mg/L
Lab Comments
Diss. Solids %300 mg1L
Fluoride 951 mg1L
Hardness: Total 900 mg1L
Hardness (non-carb) 902 mg1L
Phenols 32730 ugll
Specific Cord, 95 NMhoslcm
Sulfate 945 mglL
Sulfide 745 mg1L
Oil and Grease mg1L
NH3 as N 610 mg1L
TKN as N 625 mg1L
NO2 + NO3 as N 630 mg1L
R Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg1L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS" in block.
Ag-Silver 46566 u 1L
AI -Aluminum 46557 u IL
As -Arsenic 46551 u IL
Ba-Barium 46558 u IL
Ca -Calcium 46552 m IL
Cd-Cadmium 46559 u IL
Cr-Chromium 46559 u 1L
Cu-Copper 46562 u IL
Fe -Iron 46563 u IL
Hg-Mercury 71900 u /L
K-Potassium 46555 m 1L
Mg -Magnesium 46554 m 1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m 1L
Ni-Nickel u 1L
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zn-Zinc 46567 u 1L
Organochlorine Pesticides
Or ano hos horns Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolable Organics
TPH-Diesel Range
Volatile Organics(VOA bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY f
Temperature on arrival (°C): I;

Sample ID ABS6240
NC (DWQ, Laboratory Section Wgsufts
Location ID: WAROAPNLC Collect Date: 02l2312010
Lon. Descr.-. N2P2 NEW COLONY Collect Time:: 10:50
Visit ID
CAS # Analyte Name PQL Result Qualiflor Units Analyst/Dole Approved By (Date
Sample temperature at recslpt by lab 1.2 'C DSAUNDERS SMATHIS
Method Reference 2124/10 2124110
HUT
NH3 as N In Ilquld 0.02 1.3
mg1L as N
MAJAYI
CGREEN
Method Reference 000-107-DS-14
2125110
312110
Total IQeldahl N as N In Muld 0.2 3A
mg11. as N
MOVERMAN
CGREEN
Method Reference } achot107.05.2•H
2126110
3010
NO2+NO3 as N in liquid 0,02 2.2
not as N
MAJAYI
CGREEN
Method Reference 000-107-04.1-c
2125110
W211D
Phosphorus —total as P in liquid 0.02 0.42 mg1L as P GBELK CGREEN
Method Reference L8010.115.01•1EF 312r10 31911D
Laboratory Section>> 1623 Mall Service Canter, Raleigh, NC 27609.1623 [phone] Page 2 of 2

r
aboraton Sech
County: Tyrrell
Sample ID:
A11366090
River Basin
PO Numherll
GW100168
Report To WAROSP
O�
y
Date Received:
0212312010
?_
r
Time Received:
14:10
Collector M SALYER
d
y
Lebworks LoginlD
LBUCK
Region: WARD
Date Reported:
313110
Sample Matrix: SURPACIZATER
Loc. Type:
Report Generated:
03/0312010
Emergency Yes/No
Visitl0
COC Yes/No
Loc. Dozer.: NEW DITCH
-COLONY
'3 g (J
Location ID: WAROSPNLC
Collect Date: 02123/2010
Collect Time:: 10:66
Sample Depth 0.1
Sample Qualifiers and Comments
Oc"
t l -11-
CHAR 1 7 2010
c -
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimaled concentration is < PQL and >MDL
81-Countable membranes with <20 colonies; Estimated
NE-Na established PQL
132- Counts from all filters were zero.
P-Elevated PQL due to matrix interference and/or sample dilution
133-Countable membranes with more than 80 or 80 colonies; Estimated
Q1-Holding time exceeded prior to receipt et lab.
B4-Filters have counts of both >60 or 80 and < 20; Estimated
02-Holding time exceeded following receipt by lab
135-Tao many colonies were present; too numerous to count (TNTC)
PQL- Practical Quantitadon Limit -subject to change due to instrument sensitivity
J2-Reported value failed to meat oC criteria for either precision or accuracy; Estimated
Samples analyzed for this compound but not detected
J3-The sample matrix Interfered with the ability to make any accurate determination; EstimatedU-
X1- Sample not analyzed for this compound
JB-The lab analysis was from an unproserved or Improperly chemically preserved sample; Estimated
N1-The component has been tentatively Identified based on mass spectral library search and has an estimated value
WARD
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2

' I GrOUNDWATER FIELD/LAD FORM
Loc.itiosl code _._ . _- SAMPLE TYPE .�,r.1ULC r F:ICi: ITY
(ter^.1.I111Y._.,•rr"..ia=__}" ..� .-_---._..._...._....., ___ u Water F"oulw!a
(a1:1[; Nc; Serial No. i `;orl -1 Gri(!'c,e•1c):
....._....._... } Other
��_ C Chair, of Custody
Rep(.:ir fn Ak'O, FRO, mr-10, RRO'yaI�UDV"11; . — --
.r
JlSki,i, Kip swri FO. Fed. Trust (_..Entral 01f .
!•;Or!!'. (.-rnhnts
Dekall=nvlu u! Cr •;1,�r,r.lenl and Natulsl Resourus
,iON 0F'v 7A i t:(•' :_`UAI lTY-GROUNDWATER SECTION
Lab NJ:;It,r-r r/���G�r�a---
j •-�d Date F'aa:�irpri�hl�/f� Tim
> Frnm;E�lrs, Cnuri� r, ,a d 11iti
Dates i (nici qed'
Sllipllr?r^ hY CiUS, Catmer, t,1nd C)el 011ie[
Purpnro-
Caltecto:;s;. j;; 1,a iJ:?
_ _
�;,r /� a.F_ 4:l,rlr;• ' - f"G Ttrne (Q.� �, 8,:sr.Jme. Crsnlplaint. Cornaiiance. LUST, f'r sticid,�
-
�Illdy, Federal Truss, Other
;r
t SES/
FIELn ANALYSES/
.
�---
OwnerPH
,.,,;
Spec.
Sec. Cond a, 2VC
Location of Sita
T?m
Odor ._.._.._
Description r1} pgnrt4L,.,•r_'J1r�f
�'�� _....._...-._
Kppeaiamce_. _
Sampling Method Crr?�`';'
Sample Int(:rval
_
Field Analysis by
_ ,
Rernarks--
LABORATORY ANALYSES
--- --
r"�r",: " ':ram
I100 1E'
4 COD Ho3GSa,
m
mglL
r1 p v,hY-;i13t�r1
FI rCn4-i1$I
rru�L
MOIL
_
I �Ra-6iir�� :�a�ii6
I �Ar-41L+^.}!r�iln-.i4�^�'
�.ali.� I
Iflr�i ['CJ7g5�hnrus PPS11���i}r�
_... _.
I COD Lc•1. 33S
rnplL
r lfarnr,.tsS Totzl 9L'U
mg'L
t A$-rti.y�.nx_ 46551
[;a!1. 3 i
! rl�l'U Nn ?eslrr7as
iI
V
ICvf0lrrl VF F!. -al3f 616
I{t;�s1",��5{irr.r,,ra-h1's42-..-_..- mg'L
---....---ll0firni
f-al ? n i MT7 '1 r as 31504 r 1 GDm!
f 41,rt I. f r �G ,lgrl
_ .. _...._ -- -- -------- -
1()r,hri7
F--- -----__.-�.
1,ypPCliC OItC 4, Vhlh4grfhl�
__-_rn971-
NTU
Sultate 4,4t mg�
'
3tes!+rrF, Tgl,,t SuspenUed 130 n�.grl.
--' -- --- -
! su45ee 145 rngrL-i
- . _..-.
FiMi 4u; � coot;.-
^ ;
Alh;rlinity !c �-H 4 5 410 ^- ,- Ing"L----
r
A;k'alrnrtg 1u HH 8 3 415 r:a L
Nil; ,,y N ri1M1---'--'-.-_..._ .. __...-., L--
i NN a•. N 525
— NO., , NO, as N 530 -�_— mqlL
P Tnra� as f' nt1,5
-..
�
Elr�artrUnllp 44gµ h mgl1. _
carton wxj ie 4o5 . •...._..— nlglL
t;n1c,�M1� 94n Ing`l,
Cnro mrum He! 103,' ugtt_
N hate MCI I as Ny 5-20 wqr L
- �CpYI
Lab
----
Two80 CU
�N+lrletNil; a N15t5 Ty- ..-r.__ rtiWL-
--
T -
C1'anedr
Cornmenis
rrly For Dissolved Analysis-SUDmll filtered 5amrwb an(] wnle INS' In hi",I,
lil larnusi 4F5:g
r'a (;;ilrn,m 45552
Cd[;adm�um 4ss�r
i:r•Gnlnmiam 4r.M9
I ru-G'copei 413562-
1C.Irpn 4fi5fl —
K pF '155iu1n 4It`s -�
r. ,hl3pnr c_wrr; 46',54
I Ltn.NL'tnganecr sPSF
r 143-547m m 4F556
NI-Nr�l,et
Pb-Lead 4 G %4—�
5e-5alem�um
Zn-Zlnc 40!67
17
--
.,-----_._....__ °4't _; (.._ _ I Tf•N BTEx Gagohm�
LAB USE ONLY C)
Temperature on arrtvaI MY

.,1
PVC D`%VQ Laboratory Section Results Semple ID AB66090
Locatlon ID: WAROSPNLC Collect Date: 02/2312010
Loc. Descr.: NEW COLONY DITCH 1-9 Collect Time:: 10:55
Visit ID
CAS N Anatyte Name PQL Result Qualifier Units Analyst/Date Approved By !Date
Sample temperature at recelpt by lap 1.0 'C LSUCK SMATHIS
Method Reference 023110 U25110
Collform, MF Focal In liquid 1 460 CFU1100ml LBUCK ESTAFFORD
Method Reference APHA9MD-20th 203110 3/3110
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 [phone] Pape 2 of 2

County:
TYRRELL
River Basin
Report To
WAROAP
Collector:
D MAY
Region;
WARD
Sample Matrix;
GROUNDWATER
Loc. Type:
WATER SUPPLY .
Emergency Yes1No
CDC Yes/No
a
Sample ID:
AB56241
ypF WA7��
Q
PO Number#
10GO101
Date Received:
02/2412010
r
A =a
Time Received:
08:25
O Y
Labworks LoginID
SMATHIS
Date Reported:
319110
Report Generated:
03/0912010
VisItID
Loc. Descr.:- N2PZ NEW_COl-ONY
Location ID: WAROAPNLC I Collect Date: 02/23/2010 1 Collect Time:: 10:55 I Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier Codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N9-Estimated concentration is a pQL and >MDL
Bt-Countable membranes with 120 colonies; Estimated
NE -No established PQL
B2- Counts from all filters were zero.
B3- Countable membranes with more than 80 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution
134-Filters have counts of both >60 or 84 and < 20; Estimated Q1-Holding time exceeded prior to receipt at lab.
BS-Too many colonies werepresent; too numerous to count (TNTC) t72- Holding time exceeded following receipt by lab
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated POL- Practical Quentitation Limit -subject to change due to instrument sensitivity
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compound but not detected - • -
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound '
NA -The component has been tentatively Identified based on mass spectral library search and has an estimated value��.,__
LAB
Laboratory Section» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
Page 1 of 2
II Vi
MAR 1 7 2010 ; l
- UFFICE

North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code SAMPLE TYPE SAMPLE PRIORITY )t)O- 010t
County �x C ZI ❑ water ❑ Routine p fc 1� Lab Number
Quad No Serial No. ❑ soil ❑ Emergency Dale Received J Time: a
Lat. Long, ❑Other Rec'd By: From:Bus, ourier, and Del.,
IL❑ Chain of Custody Other:
Report To: ARO, FRO, MRO, RRO, aR0 WiRO, Data Entry By: v Ck:
WSRO, Kinston F0, Fed. Trust, Central Off., Other: Date Reported:
Shipped by: Bus, uri Hand Del., Other: Purpose:
Collector(s): Dated-40 Time Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner s``r`la°net
pH 40o Spec. Cond.94 at 250C Location or Site
Temp.lo eC Odor Description of sampling point 7 -_ A _
Appearance Sampling Method_ C=r&L,
Field Analysis By: Remarks uma. over. etc
LABORATORY ANALYSES (Pumping time. air temp„ etc.
130D 310 m91L
COD High 340 m91L
COD Low 335 mg[L
Coliform: MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100m1
TOC 680 mg/L
Turbidity 76 NTU
Residue, Total Suspended 530 mg/L
pH 403 units
Alkalinity to pH 4.5 410 m91L
Alkalinity to pH 8.3 415 mg/L
Carbonate 445 m91L
Bicarbonate 440 m911L
Carbon dioxide 405 mg/L
Chloride 940 mg/L
Chromium: Hex 1032 ug/L
Color: True 80 CU
Cyanide 720 mg/L
Lab Comments
Diss. Solids 70300 mg1L
Fluoride 951 mg/L
Hardness: Total 900 mg/L
Hardness (non-carb) 902 mg1L
Phenols 32730 ugll
Specific Cond. 95 NMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg&
Oil and Grease mg/L
Hs as N 610 mg/L
TKN as N 625 mg/L
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg/L
Nitrate (NO3 as N) 620 mg/L
Nitrite (NO2 as N) 615 mg/L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write -DIS' in block.
Ag•Silver 46566 u 1L
AI -Aluminum 46557 u 1L
As -Arsenic 46551 a 1L
Ba-Barium 46558 a 1L
Ca -Calcium 46552 m IL
Cd-Cadmium 46559 u 1L
Cr-Chromium 46559 u 1L
Cu-Copper 46562 u IL
Fe -Iron 46563 u IL
Hg-Mercury 71,300 u IL
K-Potassium 46555 m IL
Mg -Magnesium 46554 m 1L
Mn-Manganese 46565 u IL
Na-Sodium 46556 mg/L
Ni-Nickel u IL
Pb-Lead 46564 u 1L
Se -Selenium u IL
Zn-Zinc46567 u IL
Sample Interval
Organochlorine Pesticides
Or ano hos horus Pesticides
Nitrogen Pesticides
Acid Herb+tides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics OA bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAS USE ONLY
Temperature on arrival (°C):

XC {D`fNQQ Ga6oratory Section 2ssufts Sample ID AB55241
Location ID: WAROAPNLC Collect Data: 02123/2010
Loc. Descr.: N2P2 NEW COLONY Collect Time:: 10:65
Visit ID
CAS 0 Anslyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date
Sample temperature at recelpt by lab 1.2 'C DSALINDERS SMATHIS
Method Reference 2124110 2)24110
NUT
NH3 as N In liquid
0.02
1.3
mg1L as N
MAJAYI
CGREEN
Method Reference Lac10-107-0&W
2125110
312110
Total Igeldahl N as N in liquid
0.2
3.0
mg1L as N
MOVERMAN
CGREEN
Method Reference Lachet107.06-2-H
V28110
312/10
NO2+NO3 as N In liquid
0.02
2.0
n1g1L as N
MAJAYI
CGREEN
Method Reference Lac10.107.04.1-c
225110
312110
Phosphorusj al as P In liquid
0.02
0.33
mg1L as P
GBELK
CGREEN
Method Reference Lae10.115-01.1EF
312110
319110
Laboratory Sectlona�,- 1623 Mall Service Canter, Raleigh, NC 27699-1623 1919) 733.3908 Page 2 of 2

County: Tyrrell
River Basin
Report To AW ROSP
Collector: M SALYER
Region: WARD
Sample Matrix: SURFACEWATER
Loc. Type:
Emergency Yes/No
COC Yes/No
11 Location ID: WAROSPNLC
Vlsitl D
Loc. Descr.: NEW COLONY DITCH 2-A
Collect Date: 0212312010 Collect Time:: 11.00
Sample Qualifiers and Comments
Sample ID:
ABBS091
PO Number #
GW100170
Date Received:
0212312010
Time Received:
14:10
Labworks LoginlD
LBUCK
Date Reported:
318110
Report Generated:
03/08/2010
A
Sample Depth
Routine Quallfiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported Is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
51-Countable membranes with <20 colonies; Estimated
NE -No established PQL
B2- Counts from all filters were zero.
P-Elevated PQL due to matrix interference and/or sample dilution
B3-Countable membranes with mom than 60 or 80 colonies; Estimated Q1-Holding time exceeded prior to receipt at lab.
134-Filters have counts of both >60 or 80 and < 20; Estimated
02- Holding time exceeded following receipt by lab
BS-Too many colonies were present; too numerous to count (TNTC)
J2-Reported value failed tomeet QC criteria for either precision or accuracy; Estimated PQL- practical Quantitation Limit -subject to change due to Instrument sensitivity
J3-The sample matrix Interfered Samples analyzed for this compound but not detected
with the ability to make any accurate determination; Estimated �_�..�..-•• ; ` • i '~�
X1- Sample not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
11 I
Ni -The component has been tentatively identified based on mass spectral library search and has an estimated value
MAR 1 7 2010
• I
WARD
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27600.1623 [phone] �Page'1-6f 2

Locition codia _______AhiPLEI
—'
3o62No`_______
Ar(,'
w-n'' R7 Fvm Trust,Cem �� ���mn . __.m| u
/
�
r�D ssrl ved Armly5is-s"lmz fJleied pie and wi- le
PCUS
_MH-STEX Gasoline
LAB USE ONL
Temperalwre an arrival ('C)

NC (DWQ Laboratory Section �Rgsurts Sample ID AB55091
Locatlrn ID: WAROSPNLC Collect Date: 0212312010
Loc. Descr.: NEW COLONY DITCH 2-A Collect Time:: 11,00
Visit ID
CAS # Analyte Name PQL Result Qualifier Units Analyst/Date Approved By /Date
Sample temperature at receipt by lab 1.0 •C LBUCK SMATHIS
Method Reference 2I23110 2125110
ColNorm. MF Fecal In liquid 1 230 CFU1100ml LBUCK ESTAFFORD
Method Reference APHA9222D-2Dth
2123l10 31311{t
Laboratory Section>> 1623 Mail Service Center, Raleigh, NC 27699.1623 (919) 7333903 Page 2 of 2

County: TYRRELL
Sample ID;
ASS6242
River Basin
lOf V�A7�19
�i
PO Number k
1000102
Report To A�II ROAP
O�
Date Received:
0212412010
y r
}
Time Received:
08,25
Collector. i? MAY
,�
p -t
Labworks LoginlD
SMATHIS
Raglan: WARO
Data Reported:
319I10
Sample Matrix: 2ROUNDWATER
Loc. Type; WATE"LUPPLY
Report Generated:
0310912010
Emergency YeslNo
VIsk1D
COC Yes/No
Loc. Descr,;COLONY�.
+JJ
Location ID: WAROAPNLC
Collect Date: 0212312010 Collect Tlme:: 11;00
Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations
N3-Estimated concentration is < PQL and >MDL
131-Countable membranes with <20 colonies; Estimated
NE -No established PQL
62-Counts from all filters were zero.
63- Countable membranes with more than 60 or 90 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution
64-Filters have counts of both >60 or 80 and a 20; Estimated 01-Holding time exceeded prior to receipt at lab.
65-Too many colonies were present; too numerous to count (TNTC) 02- Holding time exceeded following receipt by lab
J2- Reported value failed to meet QC criteria for either precision or accuracy; Estimated PQL- Practical Quentitation Limit -subject to change due to instrument sensitivity
U- Samples analyzed for this compound but not detected
J3-The sample matrix Interfered with the ability to make any accurate determination; Estimated
X1- Sample not analyzed for this compound
J6-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
N1-The component has been tentatively Identified based on mass spectral library search and has an estimated value
LAB
i
MAR 1 7 2010
I
Laboratory $action>> 1023 Mall Service Center, Raleigh, NC 27099-1623 (919) 733,3908 Page 1'of 2' - 1
r.

GROUNDWATER FIELD/LAB FORM
Location code SAMPLE TYPE
County L Yr_ .t- C Ji ❑ Water
Quad No T Serial No. 0 Soil
Lat. Long. ❑ other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO,tLIROWRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, ouri Hand Del., Other:
Collector(s): Date 2 -d,3 Tim(
FIELD ANALYSE
PH 400 Spec. Gonda, at 250C
Temp., aC Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOD 310 M91L
COD High 340 mg1L
COD Low 335 m91L
Coliform: MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100ml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
PH 403 units
Alkalinity to pH 4.5 4111 mg1L
Alkalinity to pH 8,31415 mg1L
Carbonate 445 mg1L
Bicarbonate 440 mg/L
Carbon dioxide 405 mg/L
Chloride 940 mg1L
Chromium: Hex 1032 ug1L
Color: True 80 Cu
Cyanide 720 mg1L
Lab Comments
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
❑ Routine Lab Number
❑ Emergency Date Received
�ft Rec'd By: From:Bus, ourier, and Del.,
Other: _1� _
Data Entry By: Ck:
Date Reported:
Purpose:
/�O D� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
Owner I`ir��aoney
Location or Site o '
Description of sampling point
Sampling Method Sample Interval
Remarks umo. a�
Diss. Solids 70360 mg1L
Fluoride 051 mg1L
Hardness: Total 900 mg1L
Hardness (non-carb) 902 mg/L
Phenols 32730 U9A
Specific Cond. 95 pMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease m91L
Hs as N 610 M91L
TKN as N 625 mg1L
Vj
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NO3asN) 620 mg1L
Nitrite IN02 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS' in block.
(Pumping lime, air lamp., etc,)
Ag-Silver 46566 u 1L
AI -Aluminum 46557 u 1L
As -Arsenic 46551 u 1L
Ba-Barium 46558 u 1L
Ca -Calcium 46552 mg1L
Cd-Cadmium 46559 u 1L
Cr-Chromium 46559 u lL
Cu-Copper 46562 u 1L
Fe-tron 46563 u 1L
Hg-Mercury 71900 u 1L
K-Potassium 45555 mg1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u 1L
Na-Sodium 46555 mg1L
Ni-Nickel u IL
Pb-Lead 46564 u 1L
Se-Se)enium u 1L
Zn-Zinc 46567 u 1L
Or anochlorine Pesticides
Or ano hos horus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics (VOA bot9e
TPH-Gasoline Range
TPH-STEX Gasoline Range
LAB USE ONLY f
Temperature on arrival (°C)-

s Sample ID AB55242
.71trC �DWQ Laboratory Section Irsufts
Location ID: WAROAPNLC Collect Date: 0212312010
Loc. Dow.: N2P2 NEW COLONY Collect Tlme:: 11:00
Visit ID
CAS it Analyte Name PQL Result Qualifier Unita AnalyatlDate Approved By /Date
Sample temperature at receipt by lab 1.2 'C DSAUNDERS SMATHIS
Method Reference. Z24110 2124110
NUT
NH3 as N In liquid 0.02 0.23
mp1L as N
MAJAYI
CGREEN
Method Reference Lac10.107.06.1-J
2126110
3tV10
Total Kjeldahl N as N In liquid 0.2 2.1
mplL as N
MOVERMAN
CGREEN
Method Reference Lachat1074)6.2•H
212&10
312110
NO2+NO3 as N In liquid 0.02 2.0
mg/L as N
MAJAYI
CGREEN
Method Reference Lac10.107.04-1-c
212&10
312110
Phosphorus --total as P In liquid 0.02 0.36 mg1L as P GBELK CGREEN
Method Reference Lac10.115_01.1EF 3W10 319110
Laboratory Sectloma 1623 Mall Service Center, Raleigh, NC 27692-1623 [phone] Page 2 of 2

County:
J
I1MU
River Basin
Report To
WARO_SP
Collector:
M SALYER
Region:
WARD
Sample Matrix:
SURFACEWATER
Loc. Type:
Emergency Yes/No
COG Yes/No
1 Location ID: WAROSPNLC
VisitlD
Loc. Descr.: NEW COLONY RIMH 3-A
Collect Date: 02/23/2010 Collect Time:: 11:15
Sample Qualifiers and Comments
Sample ID:
AB68092
PO Number #
GW100171
Date Received;
0212312010
Time Received:
14:10
Labworks LoginID
LBUCK
Date Reported:
318110
Report Generated:
03/08/2010
4 t'j ID
Sample Depth IV
Routine Qualifiers
For a more detailed description of these qualifier codes refer to WwW.dwglab.o�g under Staff Access
A -Value reported is the average of two or more determinations
N3-E3timated concentration is < PQL and >MDL
B1-Countable membranes with <20 colonies; Estimated
NE -No established PQL
82- Counts from all fitters werezero.
P-Eleveted PQL due to matrix interference and/or sample dilution
B3- Countable membranes with more than 60 or 80 colonies; Estimated
01-Hdding time exceeded prier to receipt at lab.
B4-Fllters have counts of both >60 or 80 and < 20; Estimated
Q2- Holding time exceeded following receipt by lab
B5-Too many colonies were present; too numerous to count (TNTC)
PQL- Practical Ouentitatfon Limit -subject to change due to instrument sensitivity
J2- Reported value failed to meet OC criteria for either precision or accuracy; Estimated
J3-The sample matrix interfered with the ability to make any accurate determination; Estimated V- Samples analyzed for this compound but not detected
J6-The lab analysis was from an unpraserred or improperly chemically preserved sample; Estimated X1- Sample not analyzed for this compound
NI -The component has been tentatively Identined based on mass spectral library search and has an estimated value
i
wARo MAR 1 7 2010 ,
. .
Laboratory Section» 1023 Mall Service Center, Raleigh, NC 27699-1623 [phone] Page 1 of 2 1
Ut=> �E

GROUNDWATER FIELD/LAB FORM A � ;;, 1
Location code
':n.IsntY�—�'—Cyr—.� ! .-,— •-- -- --. --• ---- ••--
North Carolina
:i,aparwwmz ui Envnunnlent and Natural
aJl'•'l r'r1 0' WATER QUALITY -GROUND NA16 t :;L.•: I I:_IId
SAFAPLC ,' •=i'C= - — 'N4tv1PE,F PRIORITY
CJ Y1a: r Q Routine L;th Number
❑ Soil ❑ Emergency fate Received
❑ Cthr; Rec'd $y� Frr„I I?r.:, i":r:a:rwr HHnitDe.
Other:
;?e purl To! ARO, FRO, FARO. f2f.',,. „•' r __,- ...............--
a,�..,':`.IR . , _—..____ __. -. _.._—. .. - -- Data Entry By:
VSRO. Kinston F4, Fed Dols', C.oilli -il CI!I., C"5'.her D,,te Reported:
-hipped by" Bus. CouriEr• 2t'tl rkl �?liter F't,rresSe
dale %3 Tirn< /'_ / :_ Baseline, Complaint, Carslplla;;r: wS'T, Pesticide Study, FederZl I'rusl. !llr.r:' --- _
FIE, Q ANALYSE :l:m�f �: ' _ 1:11� „•,
Soec Coni'I �y .. _S1 25-C LCx:a? wi or SIte 1iJ •� --
Tr.;t1p,.,1 "�: (?+pill'— _� i:•'.�rrlptlon of Shcllpllnry point•-,1'I.'r�s', _ --.-*
Appptir@n-,p __•__-,------ _ sampling Itlethod
Field Analysis By: iRrawa0's_...-
LA ORATORY ANALYSES
eoD 31C for $m
A piss ess i0300 P„lrL
� I � Ag5�lVe! 4ri5Gn r,rrl- � I Gganrx:l5
Icoo Hig+tLse u7r:L - FlunrideU'51 _— mpl. i ,i f..N-Alum mumAb'S:,� ut1'i �anOjh
0
0 LC.' 2.35
._._.. 71, hiaronr Ss: 7a18i 50C .�+L A. Ar;emr 4111S
_ _
'I MVF!,calL1C, Hardness knpn•r35rh% 9?�- a-9anum4H55&
IL
!1CrC lirtrt:!h[ Ti131-'.7j0e :t0pml ' 1'hannls 3273C ur,,, Ca-CaiCurm aG5a2g' PC(t6
L C �d - --_. --iri,l°L I j S_pulCl(ic Corc. 95 �14hC� [m .j I I Cd-( adm,U r 46569 t—
i op rip t tdll1 SutrZle945 q!l. Cr•.:hfmm�iman559
+` I Ij 5vt�ie -rolal JusC�ndeo a3Q sr�il, t {—I- c L � G4-CAnf�9r dfi5F,7
" J4rniQP Td5 a
Fe -Iran ar•,d3 _ _ _ ,L _ - Semi r»6et
LF I pd and Fins_& mg.L -, Hg-Nter cun' 71906
mc
1 t
4 ! pri 4t.2 un,ts I iC•FOlasS,um 4055 -_--
AI ail lty;o FIB a n 1,. m I I rvtn.r,4�nyhnus�'rttgJL
Inlh.ahnr•y+.npHc ale
465C511" I ....,-•---- h1r.Ma nEs,ulna----.----......-__..._..._.... .��-
rY5G5
,,,pr;n;,,L" 4't5 mVL i Nit;.55 N 61G mq•1 Nri-tiUr,mal df%556 nu,l TPLf•GdSt
Sample Infer'
e Rr ernes
BkJ,UB'13SV d-Ir, rngll. _._! TKN ds N &'l1• n=g:1 h`i•r`��:Myi •--- -_ U iL TPH-PTF.k 685,pluru
•� C:aICAIt rJKif1{t�•301,, ..------------ rrlg:L N01-NQ, 3.N ti30 - _. P5!1: L� Ptr Lead 46SEA
ChlBf'oe SAC rog;L � P.-Total as P U5 �--_ »»-^---marl �� j Sr*•Selenium u rL ...._-_._. _.
-f Chremrum He.',022 ug7L NivOe IN0,as Ntf}i9 -- rya. r Zn-2�in: de7�,1:-T
--
j Go[n trUr A,.ry Cu
L
Lab.comments
Name (NO, as N) h?
i:5^! !,A Rf V, 7I0? 1-r,,, Umsolved Analysis-st,L`rm SiHared samFde and w•rte' DIS' in N36
I�ik1 VJt urv�r �
�- Temperature on arrival (4C)

NC DWQ Laboratory Section Wgsufts Sample ID AB55092
Location ID, WAROSPNLC Collect Date: 0212312010
Loc. Doscr.: NEW COLONY DITCH 3-A Collect Time:: 11:15
Visit ID
CAS p Analyte Name
PQL Result Qualifier Units
Analyst/Date
Approved By (Date
Sample temperature at nscelpt by tab
r 1.0 'C
LBUCK
SMATHIS
Mathad Reference
2123110
2R5110
BCD, &Day In liquid
2 5.9 M91L
MSTARR
ESTAFFORD
Method Reference APHA5210B
V25110
315110
Colllorm, MF Fecal In liquid
1 15 CFU1100ml
LBUCK
ESTAFFORD
Method Reference APKA9222D-20th
2W10
3133110-
Laboratory Section>> 1523 Mail Service Center, Raleigh, NC 27t399-1623 [phone] Page 2 of 2

M DM Laboratory Section sults
County: TYRRELL Sample ID: A855243
River Basin �L}F WA7�AP PO Number p 10G0103
Report To WAROAP ��� Q Date Received: 02/2412010
r Time Received: 08:25
Collector. D MAY
Region: WARS Labworks LoginlD SMATHIS
Date Reported: 319110
Sample Matrix: GROUNDWATER
Loa Type: WATER_StlP= Report Generated: 03109/2010
Emergency Yes/No
VIskID
CDC YesfNo I
Loc. Descr.: N2P2 NEW COLONY
. � 1
Location ID: WAROAPNLC Collect Date: 0212312010 Coiled Time:: 11:16 Sample Depth
Sample Qualifiers and Comments
Routine Qualifiers
For a more detailed description of these qualifier codes refer to www.dwglab.org under Staff Access
A -Value reported is the average of two or more determinations N3-Estimated concentration is < PQL and >MOL
B1-Countable membranes with <20 colonies; Estimated
NE -No established PQL
132- Counts from all filters were zero.
83-Countable membranes with more than 80 or 80 colonies; Estimated P-Elevated PQL due to matrix interference and/or sample dilution
64-Filters have counts of bath >60 or 80 and < 20; Estimated 01-Hold ing time exceeded prior to receipt at lab.
85-Too many colonies were present; too numerous to count (TNTC) Q2- Holding time exceeded following receipt by lab
J2- Reported value failed to meet QC criteria for wither precision or accuracy: Estimated POL- Practical Ouentitation Limlt-subject to change due to Instrument sensitivity
4-The sample matrix interfered with the ability to make any accurate determination; Estimated U- Samples analyzed for this compoun. d but not detected ' -
X1- Semple not analyzed for this compound
JB-The lab analysis was from an unpreserved or improperly chemically preserved sample; Estimated
NI -The component has been tentatively identified based on mass spectral library search and has an estimated value
LAB MAR 1 7 2010
Laboratory Section 1823 Mail Service Center, Ralelgh, NC 27699-1423 19191 733-3908
Page 1 of 2 rEf. 1
.JI , :C,

GROUNDWATER FIELD/LAB FORM Department of EnvNorthironment
ent a na
and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code SAMPLE TYPE SAMPLE PRIORITY jolf 0 r 0�
County ❑ Water ❑ Routine Lab Number f ��
Quad No Serial No. ❑ Soil ❑ Emergency Date Received C-cl I
(D Ti : �a
Lat. Long. ❑Other Rec'd By: From:Bu ,Courier Hand Del„
❑ Chain of Custody Other:
Report To: ARO, FRO, MRO, RRO, aR�Q WiRO, Data Entry By: Ck:
WSRO, Kinston FO Fed. Trust, Central Off., Other: Date Reported:
Shipped by: Bus, ouri Hand Dal., Other: Purpose:
Collector(s):, /%'IA✓ — /1'%. 6.4/;e 4,,— Date2-a3 -/d Time Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES Owner fclr°1e°na)
pH 400 Spec. Cond.94 at 25°C Location or Site G
Temp.lo °C Odor Description of sampling point
Appearance Sampling Method G p'_,4bb Sample Interval
Field Analysis By: Remarks �___ _`
LABORATORY ANALYSES (Pumping lime, air lamp., elc.)
SOD 310 M91L
COD High 340 m91L
COD Low 335 mg1L
Colifarm: MF Fecal 31616 liooml
Coliform: MF Total 31504 1100ml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkatinity to pH 4.5 410 mg/L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg/L
Bicarbonate 440 m91L
Carbon dioxide 405 mg1L
Chloride 940 rrg/L
Chromium: Hex 1032 41-
Color: True 80 CU
Cyanide 720 mg1L
Lab Comments
Diss. Solids 70300 m91L
Fluoride 951 m91L
Hardness: Total 900 mgtL
Hardness (non-carb) 902 mg/L
Phenols 32730 ugll
specific Cond. 95 pMhoslcm
Sulfate 945 mg1L
Sulfide 745 mglL
Oil and Grease mg1L
NH3 as N 610 mg1L
TKN as N 625 mg1L
,NO + NO, as N 630 M91L
P: Total as P 665 m91L
Nitrate (NO3 as N) 620 mg1L
Nitrite (NOz as N) 615 rng1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write 'DrS' in block.
Ag-Silver 46566 u tL
AI -Aluminum 46557 u 1L
As -Arsenic 46551 u /L
Ba-Barium 46558 u 1L
Ca -Calcium 46552 mg1L
Cd-Cadmium 46559 u 1L
Cr-Chromium 46559 u 1L
Cu-Capper 46562 u 1L
Fe-lron 46563 u 1L
Hg-Mercury 71900 u 1L
K-Potassium 46555 m 1L
Mg -Magnesium 46554 m IL
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m IL
NI -Nickel u lL
Pb-lead 46564 u IL
Se -Selenium u lL
Zn-Zinc46567 u 1L
Or anochlorine Pesticides
Or ano hos horus Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics (VOA bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (°C): �� a

XC DWQ Laboratory Section 9;�fsufts Sample 10 AB55243
Location ID: WAROAPNLC Collect Date: 02312010
Lot. Dow.: N211`2 NEW COLONY Collett Time:: 11:15
Melt 10
CAS g Analyte Name POL Result qualifier Units AnalystfDate Approved By /Date
Sample temperature at recalpt by lab 1.2 T DSAUNDERS SMATHIS
Method Reference 2124110 2124110
NUT
NI-13 as N In liquid
0.02
0.05
nglL as N
MAJAYI
CGREEN
Method Reference Lac10.107.06.1-J
2125110
312110
Total Igeldahl N as N In 1lquld
0.2
1.3
ffV& as N
MOVERMAN
CGREEN
Method Reference Lechatl07-08.2-H
2IM10
312I10
NO2+NO3 as N In liquid
0.02
7.6
mpt as N
MAJAYI
CGREEN
Method Reference Lae10407404-1-c
V25110
3W1D
Phosphotus_total as P In liquid
0.02
0.17
mglL as P
GBELK
CGREEN
Method Reference - Lac10.115-01.1HF
3IV10
318110
Laboratory Section» 1623 Mall Service Center, Raleigh, NC 27099-1623 (919) 733a908 Page 2 of 2

North Carolina
GROUNDWATER FIELD/LAB FORM
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code
County P
Quad No.
Lat.
Serial No.
Long,
Report To: ARO, FRO, MRO, RRO, aR iRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other
Shipped by: Bus, Courier, and Del Other:
Collector(s): 0, Me, r �'
FIELD ANALYSES
pH 40c Spec. COnd.g4
Temp.to eC Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOD 370 mg1L
COD High 340 mg1L
COD Low 335 mg1L
CclJorm: MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100ml
TOC 680 mgrL
Turbidity 76 NTLI
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mglL
Carbonate 445 mg1L
Bicafbonate 440 mg1L
Carbon dioxide 405 mg/L
Chloride 940 mglL
Chromium: Hex 1032 uglL
Color: True 80 CL)
Cyanide 720 mglL
Lab Comments
SAMPLE TYPE SAMPLE PRIORITY
❑ Water ❑ Routine
❑ Soil ❑ Emergency
❑ Other ,
❑ Chain of Custody
Lab Number
Date Received Time:
Rec'd By: From:Bus, Courier, Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
Purpose:
Date� Time /t� , ,�;� Baseline, Complaint, Compliance, t_ Pesticide Study, Federal Trust, Other:
Owner u.6 � tcirc�e one )
at 250C Location or Site
Description of sampling point
Sampling Method Gay _ T �ipurno.�er. gin Sample Interval
Remarks
(Pumping time, air lemp., etc,) ,
Diss. Solids 70300 mg1L
Ag-Silver 46566 u 1L
Fluoride 951 mg1L
AI -Aluminum 46557 u 1L
Hardness: Total 900 mg1L
As -Arsenic 46551 u IL
Hardness (non-carb) 902 mg1L
Ba-Barium 46558 NIL
Phenols 32730 ugp
Ca-CaS6um 46552 m 1L
Specific Cond. 95 pMhoslcm
Cd-Cadmium 46559 u 1L
Sulfate 945 mg1L
Cr-Chromium 46559 u 1L
Sulfide 745 mg1L
Cu-Copper 46562 u 1L
Fe -Iron 46563 u 1L
Oil and Grease Mgt(
Hg-Mercury 71900 u IL
K-Potassium 46555 mg1L
Mg -Magnesium 46554 m fL
Mn-Manganese 46565 u IL
NH3 as N 610 mg1L
Na-Sodium 46556 m 1L
TKN as N 625 mg/L
Ni-Nickel u 1L
NO2 + NO3 as N 630 mg1L
Pb-Lead 46564 u )L
P: Total as P 665 mglL
Se -Selenium u 1L
Nitrate (NO3 as N) 620 mglL
Zn-Zinc 46567 u IL
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block.
Or anochtorine Pesticides
Or ano hos horus Pesticides
Nitrooen Pesticides
Semivo$atile
TPH-Dieset
Votatile
TPH-BTEX Gasoline
Temperature on arrival (°C):

GROUNDWATER FIELD/LAB FORM
Location code
County Z� Jllft'
Q o f Serial No.
Lat
Long,
❑ Water
❑ Soil
❑ Other
❑ Chain of Custody
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
❑ Routine �� Lab Number
Emergency
Date Received Time:
Rec'd By: From:Bus, Courier, Hand Del.,
Other:
Report To: ARO, FRO, MRO, RRO, WaRO, WiRO, Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported:
Shipped by: Bus, Courier, Hand Del., Other: Purpose:
COIIeCtOr(S): %�. /i'],g,/ /f7 5,¢/,,�� Date "�,3 /Q Time iD: 5� Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES _ �� Owner i tdr°le°ne)
PH 400 Spec. Cond.94 at 25°C Location or Site
Temp.lo °C Odor Description of sampling point
Appearance Sampling Method ae,4j, Sample Interval
Field Analysis By: Remarks um°. bailer. 91C,l
LABORATORY ANALYSES (Pumping time, air temp., etc.)
BOD 310 mg1L
COD High 340 mglL
COD Low 335 mg1L
Colitorm: MF Fecal 31616 1106ml
Conform: MF Total 31504 1100ml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mglL
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg1L
Bicarbonate 44D mglL
Carbon dioxide 405 mg1L
Chloride 940 mglL
Chromium: Hex 1032 ug/L
Color: True 80 Cu
Cyanide 720 mglL
Lab
Diss: Solids 70300 mg1L
Fluoride 951 mg1L
Hardness: Total 900 mglL
Hardness (non-carb) 902 mg1L
Phenols 32730 ugfl
Specific Cond. 95 pMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
NH3 as N 610 mglL
TKN as N 625 mg1L
NO2 + NO3 as N 630 mg11.
t/
P: Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg1L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
Ag-Silver 46566 u 1L
AI -Aluminum 46557 u /L
As -Arsenic 46551 u IL
Ba-Barium 46558 u IL
Ca -Callum 46552 m IL
Cd-Cadmium 46559 u IL
Cr-Chromium 46559 u IL
Cu-Copper 46562 u 1L
Fe-tron 46563 a IL
Hg-Mercury 71900 u IL
K-Potassium 46555 mg1L
Mg -Magnesium 46554 m IL
Mn-Manganese 46565 u 1L
Na-Sodium 46556 mg1L
Ni-Nickel u 1L
Pb-Lead 46564 u 1L
Se-Setenium u 1L
Zn-Zinc46567 a IL

GROUNDWATER FIELD/LAB FORM
Location code / SAMPLE TYPE
County / ri r'i' ! r/ _.._.. ._._ ❑ Water
Quad No Serial No. ❑ SoiS
Lat. Long. ❑ Other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, aRC WiRO,
WSRO, Kinston FO, Fed. Trus Central Off., Other:
Shipped by: Bus, Courier, d De , Other:
Collector(s): 1j,1na,1 — Dated- '/O Ti
FIELD ANALYSE
PH 400 Spec. Cond.94 at 250C
Temp., °C Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
BOO 310 mg1L
COD High 340 mgfL
COD Low 335 mg1L
Coliform: MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100mi
TOC 680 mgfL
Turbidity 76 NTU
Vkesioue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 m9111-
Bicarbonate 440 mgfL
Carbon dioxide 405 ni
Chloride 940 mg)L
Chromium: Hex 1032 ug/L
Color. True 80 Cu
Cyanide 720 mgfL
Lab Comments
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
❑ Routine n7��ft
❑ Emergency11
,
Lab Number
Date Received Time:
Rec'd By: From:Bus, Courier, Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
`O Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
Owner. (circle one)
Location or Site Description of sampling poin�t c
Sampling Method (rfL, _
Remarks ——Ipum°. sa rec etc.)
Diss- Solids 70300 ri
Fluoride 951 mg1L
Hardness: Total 900 ni
Hardness (non-carb) 902 mgfL
Phenols 32730 ugll
Specific Cond. 95 pMhoslcm
Sulfate 945 mg1L
Sulfide 745 mgfL
Oil and Grease mg1L
NH3 as N 610 mgfL
Ti as N 625 mgfL
NO? + NO3 as N 630 mg1L
P: Total as P 665 m91L
Nitrate (NO3as N) 620 mgfL
Nitrite (NOz as N) 615 mgfL
GW-54 REV. 7103 For Dissolved Analysis -submit Filtered sample and write "01S" in block.
{Pumping time, air temp., etc
Ag-Silver 46566 u 1L
N-Aluminum 46557 a 1L
As -Arsenic 46551 u 1L
Ba-Barium 46558 u 1L
Ca -Calcium 46552 m 1L
Cd-Cadmium 46559 u IL
Cr-Chromium 46559 u 1L
Cu•Copper 46562 u /L
Fedron 46563 a 1L
Hg-Mercury 71900 u 1L
K-Potassium 46555 ni
Mg -Magnesium 46554 m 1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m 1L
Ni-Nickel u IL
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zn-Zinc 46567 u fL
Sample Interva
Pesticides
Nitrogen Pesticides
Acid Herbicides
Volatile Orgar
TPH-Gasoline
TPH-BTEX G;
Temperature on arrival (°C):

GROUNDWATER FIELD/LAB FORM
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code
SAMPLE TYPE SAMPLE PRIORITY
County-/ZLe f
❑ Water 0 Routine
Lab Number
Quad No Serial No.
❑ Soil El Emergency
Date Received lime:
J
Lat. Long.
❑Other
Rec'd By: From:Bus, Courier, Hand Del.,
❑ Chain of Custody
Other.
Report To: ARO, FRO, MRO, RRO, CDWRO,
Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Date Reported:
Shipped by: Bus, ou Hand Del,, Other:
Purpose:
Collector(s) : — /1 / ,g l� €�` Date, -� /U Time iC: • 0 Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
�T
FIELD ANALYSES
Owner ;a
(circle one)
PH 400 Spec. Cond.94
at 25°C Location or Site
r o
Temp., 0 °C odor
Description of sampling point bf
/ 7 _
Appearance
Sampling Method G_ -j,,¢A
Sample Interval
Field Analysis By:
Remarks
(Flurrio. 1jailer. etc
LABORATORY ANALYSES
(Pumping lima, air temp., etc.)
BOD 310 mg1L
COD High 340 mgIL
COD Low 335 mg1L
Coliform: MF Fecal 3)616 1100ml
Coliform: MF Total 31504 1looml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg1L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg/L
Chloride 940 mg/L
Chromium: Hex 1032 ug/L
Color: True 80 CU
Cyanide 720 mg1L
Lab Comments
Diss. Solids 70300 mgIL
Fiuoride 951 mg1L
Hardness: Total 900 mg1L
Hardness (non -Cart)) 902 mgli_
Phenols 32730 ugh
Specific Cond. 95 NMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1t.
NH3 as N 610 mg1L
TKN as N 625 mg1L
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg/L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS' in block.
Ag-Silver 46566 _ u IL
AI-Xuminum 46557 u IL
As -Arsenic 46551 u /L
Ba-Barium 46558 u IL
Ca -Calcium 46552 m rL
Cd-Cadmium 46559 u /L
Cr-Chromium 46559 a lL
Cu-Capper 46562 u IL
Fe -Iron 46563 u 1L
Hg-Mercury 71900 u /L
K-Potassium 46555 mg1L
Mg -Magnesium 46554 m /L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m /L
Ni-Nickel u /L
Pb-Lead 46564 u 1L
Se -Selenium u /L
Zn-Zinc 46567 u 1L
Or anochlorine Pesticides
Or ano hos horns Pesticides
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile organics Ly0A bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (OC):
I

GROUNDWATER FIELD/LAB FORM
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code
SAMPLE TYPE
SAMPLE PRIORITY
County��
❑ Water
❑
Routine
Lab Number
_—........,__...,—.__.
Quad No Serial Na.
❑ Soil
El
Emergency
_�.. Date Received Time:
Lat. Long,
❑ Other
Rec'd By: From:Bus, Courier, Hand Del.,
❑ Chain
of Custody
Other;
Report To: ARO, FRO, MRO, RRO, aR0 iRO,
Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Date Reported:
Shipped by: Bus, Courier, 6and Other:
Purpose:
Coll ecto r(s) : • , f
Date4-33--/49 Time
%/ :,0 6 Baseline, Complaint, Compliance, E�UST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSE
Owner 1
cards°nej
pH 400 Spec. Cond.94
at 25°C
Locatian or Site
�c�
Temp.lo °C Odor
Description of sampling point
l -
Appearance
Sampling Method
Sample Interval
Field Analysis By:
Remarks
umo: ai er. etc.)
LABORATORY ANALYSES
(Pumping time, air temp.. etc.)
BOD 310 mg1L
Diss. Solids 70300
mg1L
Ag-Silver 46566
a 1L Or anochlorine Pesticides
COD High 340 mg1L
Fluoride 951
mgfL
AI -Aluminum 46557
a lL Or anp hos horns Pesticides
COD Low 335 mg1L
Hardness: Total 900
mg/L
As -Arsenic 46551
u IL Nitrogen Pesticides
Coliform: MF Fecal 31616 1140mi
Hardness (non-carb) 902
mg1L
Ba-Bafium 46558
u IL Acid Herbicides
Coliform: MF Total 31504 1100mi
Phenols 32730
ug1l
Ca -Calcium 46552
m 1L I PCBs
TOC 680 mg&
Specific Cond. 95
pMhoslcm
CC -Cadmium 46559
u IL
Turbidity 76 NTU
Sulfate 945
mg1L
Cr-Chromium 46559
u 1L
Residue, Total Suspended 530 mgfL
Sulfide 745
mg1L
Cu-Copper 46562
u 1L
Fe -Iron 46503
u 1L Semivolatile Organics
Oil and Grease
mg/L
Hg-Mercury 71900
u !L TPH-Diesel Range
pH 403 units
K-Potassium 46555
m 1L
Alkalinity to pH 4.5 410 mg1L
Mg -Magnesium 46554
m 1L
Alkalinity to pH $.3 415 mg/L
Mn-Manganese 46565
u 1L Volatile Organics CVOA bottle
Carbonate 445 mg/L
NH, as N 610
mg1L
Na-Sodium 46556
mg1L TPH-Gasoline Range
Bicarbonate 440 mg1L
TKN as N 625
mg1L
Ni-Nickel
u 1L TPH•BTEX Gasoline Range
Carbon dioxide 405 mg1L
NO2 4 NO3 as N 630
mg/L
Pb-Lead 46564
u 1L
Chloride 940 mg/L
P: ToW as P 665
mg/L
Se -Selenium
a !L
Chromium: Hex 1032 ug1L
Nilrale (NO3 as N) 620
mg1L
Zn-Zinc 46567
u 1L
Color: True So CU
Nitrite (NO2 as N) 615
mg1L
LAB USE ONLY
Temperature on arrival (°C):
Cyanide 720 mg1L
Lab Comments
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS" in block.

North Carolina
GROUNDWATER FIELD/LAB FORM Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code _ SAMPLE TYPE SAMPLE PRIORITY
County^l .iYY ❑ Water ❑ Routine Lab Number
Quad No Serial No. ❑ Soil ❑ Emergency Date Received Time:
Lat. Long, ❑ Other Rec'd By: From:Bus, Courier, Wand Del.,
❑ Chain of Custody Other:_
Report To: ARO, FRO, MRO, RRO,j&EDWiRO, Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust, Central Off., Other: Date Reported:
Shipped by: Bus, ouri Hand Del., Other: Purpose:
Collector(s): — Date a -�.3 /�� Time / CQ Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSE Owner (circle one)
pH 400 Spec. Cond.94at 25°C Location or Site ' d
Temp.to °C Odor Description of sampling point
Appearance Sampling Method &.4&h Sample Interval
Field Analysis By: Remarks umo. a er. a c.
LABORATORY ANALYSES
BOD 310 mg1L
COD High 340 mg1L
COD Low 335 mglL
Coliform: MF Fecat 31616 1100ml
Conform: MF Total 31504 1100m1
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg)L
pH 403 units
Alkalinity to pH 4.5 410 mglL
Alkalinity to pH 8,3 415 mg1L
Carbonate 445 mgtL
Bicarbonate 440 mg1L
Carbon dioxide 405 mg1L
Chloride 940 mglL
Chromium: Hex 1032 ug1L
Color: True 80 CU
Cyanide 720 mg1L
Lab Comments
Diss. S&ids 70300 mg1L
Fluoride 951 mg1L
Hardness. Total 900 mglL
Hardness (non-carb) 902 mglL
Phenols 32730 ugll
Specific Cond_ 95 pMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
H3 as N 61a mg1L
TKN as N 625 mg1L
NO, + NO3 as N 630 mg1L
P: Total as P 665 mglL
Nitrate (N033s N) 620 mg/L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write 'DIS' in block.
(Pumping time, air temp., etc,)
Ag-Silver 46566 u IL
AI -Aluminum 46557 u 1L
As -Arsenic 46551 a 1L
Ba-Barium 46556 u lL
Ca -Calcium 4 65 52 m 1L
Cd-Cadmium 46559 u 1L
Cr-Chromium 46559 u lL
Cu-Copper 46562 u IL
Fe -Iron 46563 u IL
Hg-Mercury 71900 u 1L
K-Potassium 46555 mg1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m !L
Ni-Nickel u 1L
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zn-Zinc46567 u IL
Or anochlorine Pesticides
Or ano hos horns Pesticides
Nitrogen Pesticides
Acid Herbicides
PC Bs
Semivolatlle Organics
TPH-Diesel Range
Volatile Organics(VOA bottle
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (eC):

GROUNDWATER FIELD/LAB FORM
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code
SAMPLE TYPE
SAMPLE PRIORITY
County.j[ y_C
Cl Water
❑ Routine
Lab Number
Quad No % Serial No.
❑ Soil
❑ Emergency
_ Date Received Time:
Lai Long.
❑ Other
Rec'd By: From:Bus, Courier, Hand Del.,
. ❑ Chain
of Custody
Other:
Report To: ARO, FRO, MRO, RRO, RO iRO,
Data Entry By: Ck:
WSRO, Kinston FO, Fed. Trust,_Qentral Off., Other:
Date Reported:
Shipped by: Bus. Courier, and Del Other:
Purpose:
Collector(s): jj"y,i /!% S'�r /� nor Date -3 "//' Time
Baseline, Complaint,
Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES—
Owner
(drela°ne>
PH 400 Spec. Cond.94
at 25°C
Location or Site
Temp.lo °C Odor
description of sampling paint
Appearance
Sampling Method
Sample Interval
Field Analysis By:
Remarks -
a er. a c.
LABORATORY
LABORATORY ANALYSES
(Pumping time, air temp, etc,)
SOD 310 mg1L
COD High 340 mg1L
OD Low 335 mg1L
Coliform: MF Fecal 31616 1100mf
Coliform: MF Total 31504 Montt
TOC 680 mg/L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mg/L
Carbonate 445 mg1L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg/L
Chloride 940 mg1L
Chromium: Hex 1032 ug/L
Color: True 80 Cu
Cyanide 720 mg1L
Lab Comments
Diss. Solids 70300 mg1L
Fluoride 951 mg/L
Hardness: Total 900 mg/L
Hardness (non-carb) 902 mg1L
Phenols 32730 ug1l
Specific Cond. 95 uMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
NH3 as N 610 mg1L
TKN as N 625 mg1L
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NC3 as N) 620 mg/L
Nitrite (NO2 as N) 615 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write " DIS" in block.
Ag-Silver 46566 u 1L
AI -Aluminum 4 65 57 u IL
As -Arsenic 46551 u IL
Ba-Barium 46558 u IL
Ca -Calcium 46552 mg1L
Cd-Cadmium 46559 u 1L
Cr-Chromium 46559 u 1L
Cu-Copper 46562 u 1L
Fedron 46563 /L
Hg-Mercury 71900 u 1L
K-Potassium 46555 m 1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m 1L
Ni-Nickel u 1L
Pb-Lead 46564 u 1L
Se -Selenium u 1L
Zn-Zinc 46567 u 1L
Pesticides
PCBs
Semivolat0e O
Volatile
I I TPH-BTEX Gasoline Ranoe I
LAB USE ONLY
Temperature on arrival (°C):

GROUNDWATER FIELD/LAB FORM Department p Noof Environment nmentaina
and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code
County
Quad No Serial No.
Lat.
Long.
SAMPLE TYPE
❑ Water
❑ Soil
❑ Other
11 ❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, aRO WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, qourie Hand Del., Other:
Collector(s): Date,4 -,q 1 -/Q Time
FIELD ANALYSES
pH 400 Spec. Cond.9.4 at 25°C
Temp.lo °C Odor
Appearance
Field Analysis By:
LABORATORY ANALYSES
800 310 mg/L
COD High 340 mglL
COD Low 335 mg/L
Coliferm: MF Fecat 31616 1100ml
Coldorm: MF Total 31504 1100ml
TOC 680 mg/L
Turbidity 76 NTU
Residue, Total Suspended 530 mg1L
pH 403 units
Alkalinity to pH 4.5 410 mg1L
Alkalinity to pH 8.3 415 mglL
Carbonate 445 mg/L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg/L
Chloride 940 mg1L
Chromium: Hex 1032 uglL
Color: True 80 Cu
Cyanide 720 mg1L
Lab Comments
SAMPLE PRIORITY
❑ Routine h_ 1.
❑ Emergency �I
Lab Number
Date Received Time:
Rec'd By: From:Bus, Courier, Hand Del.,
Other:
Data Entry By: Ck:
Date Reported:
_ Purpose:
`1 Baseline, Complaint, Compliance, (eircle onaj LUST, Pesticide Study, Federal Trust, Other:
Owner I �-'
Location or Site o
Description of sampling point Jj,'�
Sampling Method ii-vr3l<'
Remarks T �(FUMD. a' ere^�
Diss. Solids 70300 mg/L
Fluoride 951 mg/L
Hardness: Tota! 900 mg1L
Hardness (non-carb) 902 mglL
Phenols 32730 ugll
Specific Cond. 95 UMhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
,NH3 as N 610 mg1L
TKN as N 625 mg/L
NO2 + NO, as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg/L
Nitrite (NO2 as N) 615 mg1
GW-54 REV- 7103 For Dissolved Analysis -submit filtered sample and write "DIS" in block.
Sample Interval
(Pumping time, air temp., etc.)
Ag-Silver 46566 a 1L
AI -Aluminum 46557 ug1L
_
As -Arsenic 46551 u 1L
Ba-Barium 46558 u IL
Ca•Caldum 46552 m !L
Cd-Cadmium 46559 u !L
Cr-Chromium 46559 u 1L
Cu-Capper 46562 u 1L
Fe -Iron 46563 u 1L
Hg-Mercury 71900 u 1L
K-Potassium 46555 m !L
Mg -Magnesium 46554 ,n lL
Mn-Manganese 46565 u 1L
Na-Sodium 46556 mg1L
Ni-Nickel u !L
Pb-Lead 46564 a 1L
Se -Selenium u !L
Zn-Zinc 46567 u 1L
PCBs
TPH
Volatile Organics(VOA bottle
TPH.Gasoline Range
LAB USE ONLY
Temperature on arrival (°C):

GROUNDWATER FIELD/LAB FORM
Location code
County/I/ yros%l ❑ Water
Quad No Serial No. ❑ Soil
Lat. Long. ❑ Other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, RO WiRO,
WSRO, Kinston FO, Fed. Trust, Central Off., Other:
Shipped by: Bus, Courier, an De , Other:
Collector(s):4. ,� ,_1_ Date. -23 je Tim
FIELD ANALYSES
pH Opp Spec, Cond.94 at 25°C
Temp.lo °C Odor
Appearance
Field Analysis By:
LAWRATORY ANALYSES
BOD 3i0 mgIL
COD High 340 mgIL
COD Low 335 mg/L
Cofifow MF Fecal 31616 1100ml
Coliform: MF Total 31504 1100ml
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg/L
pH 403 units
Alkalinity to pH 4,5 410 mg1L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg/L
Bicarbonate 440 mg1L
Carbon dioxide 405 mg1L
Chloride 940 mg/L
Chromium: Hex 1032 ug1L
Color: True 80 Cu
Cyanide 720 mg1L
Lab Comments
North Carolina
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
SAMPLE PRIORITY
❑ Routine { 1
❑ Emergency �1J
Lab Number
Date Received Time:
Rec'd By: From:Bus, Courier, Hand Del.,
Other
Data Entry By: Ck:
Date Reported:
_ Purpose:
Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:_
Owner (arCle one)
Location or Site (,olgn
Description of sampling point
Sampling Method.
Remarks sumo, aaerer, it
Diss. Solids 70300 mg1L
Fluoride 951 m611.
Hardness: Total 900 mg1L
Hardness (non-carb) 902 mg1L
Phenols 32730 u911
Specific Cond. 95 pmhoslcm
Sulfate 945 mg1L
Sulfide 745 mg1L
Oil and Grease mg1L
NH3 as N 610 mg1L
TKN as N 625 - mg1L
NO2 + NO3 as N 630 mg1L
P: Total as P 665 mg1L
Nitrate (NO3 as N) 620 mg/L
Nitrite (NOz as N) 615 mg/L
GW-54 REV, 7103 For Dissolved Analysis -submit filtered sample and write'DIS' in block.
Sample interval,
(Pumping time, air temp„ etc,)
Ag-Silver 46566 u 1L
AI -Aluminum 46557 u IL
As -Arsenic 46551 u 1L
Ba-Barium 46558 u 1L
Ca -Calcium 46552 m IL
Cd-Cadmium 46559 u /L
Cr-Chromium 46559 u IL
Cu-Copper 46562 u IL
Fedron 46563 u 1L
Hg-Mercury 71900 u /L
K-Potassium 46555 mg1L
Mg -Magnesium 46554 m 1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 m /L
Ni-Nickel u IL
Pb-Lead 46564 a IL
Se -Selenium u IL
Zn-Zinc 46567 u IL
Pesticides
Acid
TPH-Diesel
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (°C):

North Carolina
GROUNDWATER FIELD/LAB FORM
Department of Environment and Natural Resources
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
Location code SAMPLE TYPE
County /; hY& _ ❑ Water
� ❑
Quad No Serial No. Soil
Lat. Long. ❑ Other
❑ Chain of Custody
Report To: ARO, FRO, MRO, RRO, aR WiRO,
WSRO, Kinston FO, Fed, Trust, Central Off., Other:
Shipped by: Bus, 6ouri Hand Del., Other:
Collector(s): '-n 6', -/„ ey— Date,,)-,3,3 -le Time Baseline, Complaint, Compliance, LUST, Pesticide Study, Federal Trust, Other:
FIELD ANALYSES �� Owners {circle one}
PH 400 Spec. Cond.94 at 25°C Location or Site
Temp.10 °C Odor Description of sampling
Appearance Sampling Method
Field Analysis By: Remarks
I'AROPATr)RY .4NAI YSI=-(Z
BOD 310 mg1L
COD High 340 mg7L
COD Low 335 mg7L
Coliform; MF Fecat 31616 1100ml
Coliform; MF Total 31504 1100mt
TOC 680 mg1L
Turbidity 76 NTU
Residue, Total Suspended 530 mg7L
pH 403 units
Alkalinity to pH 4.5 410 mg7L
Alkalinity to pH 8.3 415 mg1L
Carbonate 445 mg7L
Bicarbonate 440 mg7L
Carbon dioxide 405 mg1L
Chloride 940 mg7L
Chromium: Hex 1032 ug/L
Color- True 80 CU
Cyanide 720 mg1L
Lab Comments
Purpose:
Diss. Solids 70300 mg1L
Fluoride 951 mg1L
Hardness: Total 900 mg7L
Hardness (non-carb) 902 mg1L
Phenols 32730 ugll
Specific Cond. 95 pMhoslcm
Sulfate 945 mg7L
Sulfide 745 mg7L
Oil and Grease mgrL
NH3 as N 610 mg7L
TKN as N 625 mg7L
NO2 + NO3 as N 630 mg7L
P: Total as P 665 mg1L
Nitrate (NO3as N) 620 mg7L
Nitrite (NO2 as N) 515 mg1L
GW-54 REV. 7103 For Dissolved Analysis -submit filtered sample and write "DIS' in block.
SAMPLE PRIORITY
❑ Routine
❑ Emergency
3-�
Lab Number
Date Received_
Rec'd By:
Other:
Data Entry By:_
Date Reported:
Time:
From:Bus, Courier, Hand Del.,
Sample Interval
(Pumping We, air temp., elc.)
Ag-Silver 46566 u IL
At -Aluminum 46557 u 1L
As -Arsenic 46551 u 1L
Ba-Barium 46558 u 1L
Ca -Calcium 46552 mg1L
Cd-Cadmium 46559 u /L
Cr-Chromium 46559 u 1L
Cu-Coppef.46562 a 1L
Fe -Iron 46563 u 1L
Hg-Mercury 71900 u IL
K-Potassium 46555 mg1L
Mg -Magnesium 46554 mg1L
Mn-Manganese 46565 u 1L
Na-Sodium 46556 mg1L
Ni-Nickel u !L
Pb-Lead 46564 u IL
Se -Selenium u /L
Zn-Zinc 46567 u 1L
Nitrogen Pesticides
Acid Herbicides
PCBs
Semivolatile Organics
TPH-Diesel Range
Volatile Organics (VOA bottle)
)
TPH-Gasoline Range
TPH-BTEX Gasoline Range
LAB USE ONLY
Temperature on arrival (°C):
Ck: