WQ0018352_Renewal Application_20190603

INITIAL REVIEW
Reviewer Thornburg, Nathaniel
Project Number* WQ0018352
SUBMITTAL DATED: 5/31/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * David Odom
Email Address*
[e-mail]
Project Information
.... .............................
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
r
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number WQ0018352
currently has project
Applicant\Permittee * Tovvn of Boiling Springs
Facility Name * Town of Boiling Springs WWTP
Phone Number*
828-247-4495
r Modification (Major or Minor)
r Additional Information
r Other
r High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Attention Nathaniel Thornburg -
Hard Copy has already been received, this is "second Copy" as requested.
Thank You & Kind Regards
Pete Dickerson
Please attach all information required or requested for this submittal to be review here.

Application Form Engineering Rans, Specifications, Calculations, Rc.)
Boiling Springs Complete RLAP Application.pdf 4.78MB
upload only 1 RDF docurrent. K/Ultiple docurrents rrust be corrbined into one RDF file.
For new and modification permit applications, a paper copy may be required. If you have any questions
about what is required, please contact the reviewer or Tessa Monday. If a oaoer a1,olicaticn is recu'red,
be advised, applications accepted for pre -review until both the paper and elect-c-ii_ col, es -ave aee i
received. The paper copy shall include the following:
o Application Form
o All relevant attachments (cales, soils report, specs, etc.)
o One full-size engineering plan set
o One 11x27" engineering plan set
o One extra set of specifications
o Fee (if required)
MallinE address:
Division of Water Resources 1 Division of Water Resources
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - I - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
Non -Discharge Branch I Non -Discharge Branch
------- -----------
1617 Mail Service Center 1 Att: Nathaniel Thomburg, Y" Floor, C Rice #942W
Raleiih, NC 27699-1617 512 N. Salisbury St.
Far questions or problems contact Tessa Monday [e-mail] or 919.707.3560.
* I;W By checking this box I acknowledge that I understand the application will not be accepted
for pre -review until the paper copy (if required) and fee (if required) have been received by
the Non -Discharge Branch. I also confirm that the uploaded document is a single PDF with
all parts of the application in correct order (as specified by the application).
Signature
C 0�w
Submission Date 5/31/2019

Odom
Engineeringpuc
May 29, 2019
NCDEQ - Division of Water Resources
Water Quality Permitting Section - Non -Discharge Branch
Att: Nathaniel Thornburg — 9t" Floor, Office #942X
512 N. Salisbury St.
Raleigh, NC 27604
169 Oak Street • Forest City, NC 28043
office 828.247.4495 • fax [phone]
RE: Application for Renewal without Modification of Permit No. WQ0018352:
Town of Boiling Springs Land Application Program
To Whom It May Concern:
On behalf of the Town of Boiling Springs, North Carolina, Odom and Associates Engineering is submitting
this application, Form: RLAP 06-16, to renew non -discharge residuals land application program permit
WQ0018352, without modification.
Enclosed in the package are the following items:
1. The completed application
1.1. Residuals Source Certification
1.2. Land Application Site Certification
1.3. LOA
2. The Biosolids Spill Control Plan
3. Inspection Log
4. Operator Designation Form
5. Sampling Plan
6. Maps
7. TCLP Results
This application package is believed to contain all information necessary to complete the requested
renewal of the Town's permit. However, if you require any additional information or have further
questions about the included information, please contact me at [e-mail] or
phone number [phone].
Thank you in advance for your assistance with this renewal application.
Sincerely,
David Odom, P.E.

DWR State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources ISA NCAC 02T.1100— RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
1. APPLICANT INFORMATION:
1. Applicant's name: Town of Boiling Springs
Applicant type: Q Individual ❑ Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
Federal ❑ State 0 Municipal ❑ County
Signature authority's name per I5A NCAC 021 .0106: Lucas Shires Title: Town Manager
Applicant's mailing address: PO Box 1014
City: Boiling Springs State: NC Zip: 28017M
Telephone number: 704) 434-2357 Email Address: lucas.shires(a)boilingsorings.net
2. Consultant's name: David Odom License Number (for P.E.): NC 21130
Affiliation: .On Staff ■ Retained (Firm: Odom Engineering, PLLC)
Consultant's mailing address: 169 Oak Street
City: Forest City State: NC Zip: 28043-�
Telephone number: [phone] Email Address: davidodomAodomengineering.com
3. Agronomist's name: _ License Number:
Affiliation: N/A NOnStaff 0 Retained (Firm: _)
Agronomist's mailing address: _
City: — State: Zip:
Telephone number: M) Email Address: _
4. Soil Scientist's name: _ License Number: _
Affiliation: N/A N On Staff N Retained (Firm: �)
Soil Scientist's mailing address:
City: !_ State:Zip:
Telephone number: (_) = T Email Address:
5. Fee submitted: 0 (See Instruction B)
11. PERMIT INFORMATION:
1. Application is for (check all that apply): N new, ® modified, C9 renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00018352
Date of most -recently issued permit: February 06, 2015
Date of most -recently certified Attachment A (if different than the permit):
Date of most -recently certified Attachment B (if different than the permit):'
FORM: RLAP 06-16 Page I of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 2556 Rockford Road
City: Boiling Springs State: NC Zip: 28017M
Coordinates: Latitude: 35° W 49" Longitude: B° 41' 30"
Datum: ® Level of accuracy: —
Method of measurement: _
2. County where residuals land application program is headquartered: Cleveland
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Todd M. Humphries
Town of Boiling Springs
994587
Back -Up ORC
Mike F. Gibert
Town of Boiling Springs
14756
Additional Back -Up
ORCs
(if applicable)
_
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test: N/A
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 59 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
47.18
5,803
—
Five -Year Maximum Adjusted
66.06
8,126
b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
N/A
N/A
Row Crops
N/A
N/A
Hay
N/A
N/A
Pasture
39.98
_
Total:
39.98
_
Methods
Surface
39.98
_
Incorporation or Injection
N/A
N/A
Total:
N/A
_
FORM: RLAP 06-16 Page 2 of

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
((bs PAN/acyr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
5o
56
N/A
78
100
28
N/A
39
150
19
N/A
26
i
200
14
N/A
19
_
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation ofNorth Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.): =
7. Specify type of residuals program (See Instruction F): N Non -dedicated ® Dedicated
If Dedicated specify the following (check all that apply):
❑ Residuals progam contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain; Q
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and andd submit the following Residuals Source Certification and all associated documentation.
4^ I
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
Land Application Site
Certification.doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only.
VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM
1. The irrigation system is: 0 Spray 0 Drip
2. Disposal system is: 0 existing E proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: _ feet
below ground surface. Rules 15 A NCAC 02T .0505f o) requires at least one -foot vertical separation between SHW T and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
® Yes or NNo If Yes, please ex lain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified:
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
Fields within Soil Area
Recommended
Loading Rate
ia/hr
Recommended
Loading Rate
i r
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
N Yes or 0 No If No, explain why I SA NCAC 02T .0505(n) is not met: _
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field / Zone
Design Area
ft=
Number of
Nozzles
Maximum Application
Rate allons/hr
Design Annual Loading
Rate llons/ r
Total
—
Spray Irrigation Design Element
Plan Sheet
Number
Specification
Pate Number
Wetted diameter of nozzles
It
_
Wetted area of nozzles
— ft
_
Nozzle capacity
_ gpm
_
Nozzle manufacturer / model
_ / _
_
Elevation of highest nozzle
= ft
_
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ■ No, Explain; =
4 — Lucas Shires Town Manager
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for the land application of Class B Biosolids from the Town of Boiline Springs W WTP
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. 1 understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes §143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: -06" 01 LUZAS h. t'44; G9 Date: ttlMj 11 1 29I-1
FORM: RLAP 06- I6 Page 5 of 5

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water KeS*Mces RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: Town of Boiling Springs
Status
Code a
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current
Proposed
R
Town of Boiling Springs
Town of BoilingTP Springs
Cleveland
NCO071943
123
59
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

DWR
Division of Water KesoUFces
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Town of Boiling Springs
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ❑ Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain: _).
3. Facility contact person and title: Lucas Shires — Town Manager
Complete mailing address: PO Box 1014
City: Boiling Springs State: NC Zip: 28017-M
Telephone number: [phone] E-mail address: lucas.shiresnboilingsprings.net
4. Facility physical address: 2556 Rockford Road
City: Boiling Springs State: NC Zip: 28017-M
Coordinates: Latitude: 35' 14' 48" Longitude: 81° 4F 31"
Datum: _ Level of accuracy: _
Method of measurement: _
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: _ % industrial and _ % domestic)
other (explain: _ ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow:.300 MGD and facility average daily flow:.239 MGD
8. Average amount of residuals being generated at this facility 16 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Two aerobic digestors totaling 128,000 gallons of storage
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical and Date of analysis: 08/28/2015
Passed corrosivity test: yes no. pH: 6.5 s.u. (2 < pH < 12.5)
Passed ignitability test: yes no. Flashpoint: >200 OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(Mg/1)
TCLP Parameter
Limit
(Mg/1)
Result
(Mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0
0.36
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
?
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100.0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
?
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200.0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.0
?
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
0.5
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trichlorophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02
ND
2,4,5-TP (Silvex)
1.0
?
Heptachlor and its Hydroxide
0.008
ND
Vinyl Chloride
0.2
ND
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical and Date of analysis: 08/28/2015
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
ND
Cadmium
85
39
ND
Copper
4,300
1,500
230
Lead
840
300
ND
Mercury
57
17
ND
Molybdenum
75
n/a
ND
Nickel
420
420
24.6
Selenium
100
100
ND
Zinc
7,500
2,800
712
b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical and Date of analysis: 08/28/2015
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
11 > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
420
Result (mg/kg)
ND
ND
24.6
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 1.76 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical and Date of analysis: 08/28/2015
Parameter
Result
(mg/kg)
Aluminum
7460
Ammonia -Nitrogen
ND
Calcium
45,800
Magnesium
3,880
Nitrate -Nitrite Nitrogen
9,070
pH (Standard Unit)
6.5
Phosphorus
814
Potassium
ND
Sodium
2,290
Total Kjeldahl Nitrogen
48,400
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): .06
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This
rate is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: ii
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (111) Year PAN
Five -Year
Maximum Adjusted PAN
(mglkg)
(mg/kg)
Surface
23,590
33,032
Injection/Incorporation
N/A
N/A
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: none
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment.
❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106 i
3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ® aerobic digestion, air drying, ❑ anaerobic digestion,
❑ composting, oi I lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization.
Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
0 Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection.
❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

LAND APPLICATION SITE CERTIFICATION
Applicant's name: Town of Boiling Springs
Land application sites currently certified: 39.98 net acres and Total to be certified: 39.98 net acres.
I. LAND APPLICATION SITE INFORMATION (See Instruction B):
Status
Code
Site/Field
ID
Landowners
O
Lessees or Operator(s)
O
Net Acres
County
�'
Crop(s) s
pO
Predominant Soil
Series Name b
Mapping Unit
or Rep. Slope'
R
JP-1
James Petty
Boiling Springs
9.84
Cleveland
Pasture
Pacolet
B2
R
JP-2
James Petty
Boiling Springs
16.36
Cleveland
Pasture
Pacolet
B2
R
Jp-3
James Petty
Boiling Springs
13.78
Cleveland
Pasture
Pacolet
B2
N
N
N
i
N
N
k
a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted)
b Soil Series Name (i.e. Appling, Cecil, etc.)
Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2)
II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C):
Site/Field ID
Latitude
Longitude
Location
Datum
Location Method Code
Location Accuracy
Waterbody Subbasin and
Stream Index No.
Current and Proposed
p
Class
_
.°..
.°
NAD 83
ADD
Nearest Second
_
.°..
.°.
NAD 83
ADD
Nearest Second
_
.°..
.°.
NAD 83
ADD
Nearest Second
_
NAD 83
ADD
Nearest Second
_
NAD 83
ADD
Nearest Second
_
NAD 83
ADD
Nearest Second
_
° Mj NJ"
.° ..
NAD 83
ADD
Nearest Second
_
_
* a n,
won,
NAD 83
ADD
Nearest Second
_
Note: Please keep the site information (I.) and waterbody information (II.) of the same field on the same page.
FORM: LASC 06-16 Page 1

Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
15A NCAC 02T .1100 — LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitling Unit.
General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 15.A NCAC 02T .l 100. Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
❑ A copy of the completed and appropriate]% executed agreement must be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or his representative hereby permits:
Applicant's name: Town_ofBoilinq Springs
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Site/Field ID
Lease
es/no
(y )
Land Use or
Cro ie Patterns
pp' g
Intended Use ofCrops
Residuals Source
(optional)
Special note
(no-tilltover-seed/
pasture)
James B. Petty
no
Pasture
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Page] of 3

I. STIPULATIONS:
1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the site(s) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until ail of the site restrictions (under Section 11) are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail
Service Center, Raleigh, NC 27699-1617.
5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land
application site(s).
6. The Perminee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the
equipment used by the Permittee.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land
application event and a copy of the results of each soil analysis.
8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil
PH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the
specified crop.
9. The landowner or his representative and the Permince will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients
(e.g.. fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s).
11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application
events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining
compliance with the permit: establish monitoring facilities on or near the land application site(s) m required by the permit; copy any records
that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the
term of. and 12 months after termination of, this Agreement.
II. RESTRICTIONS:
1. Appropriate measures must be taken by the Permium and/or the landowner or his representative to control public access to the land application
site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of
signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application
events.
3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month
period following a residuals land application event.
5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application
event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application
event when the residuals remain on the land surface for less than four months prior to incorporation into the soil.
7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event.
IH,ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NC AC 02T .0105ih 1 allows the compliance
boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided
the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID:
(Please include the rationale for the requested re -location ofthe compliance boundary and attach a map showing the newly proposed compliance
boundary to the application package)
❑ A re -defined compliance boundary is not needed for this site.
IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
❑ The land application field(s) ID: is currently permitted under another
residuals land application program; Permit Number WQ: . The land owner hereby acknowledge that by signing this
agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred
into the new program;
(Name of the new program)
FORM: LOA 06-16 Page 2 of 3

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners QR that 1 am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name:
Address: 937 Colleee Avenue
City: Shelby State:
Phone: [phone] E-mail address:
Signature: Date:
NORTHCAROLINA, C�fV&IA.nd COUNTY
Zip:28152
1, the undersigned Notary Public do hereby certify that UY2rr,r S B . Te+
—a_2_—( q
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
„d
WITNESS my hand and official seal this the , a—
dayof Ju ne 20 L
Signature and seal: =iCLtwr�x•..�+i l"d • ) d�,L.e_�
My commission expires:
Lessee's/Operator's Certification:
I certify that 1 have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee/operator name
Address:
City:
Phone:
Signature:
Permittee's Certification:
State:
E-mail
Date:
Zip:
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing official name: L-Inc/'s A. �+a12E5� To��l l�IANAd.SiL
Signature: ' Date: 5'12!20Ili
FORM: LOA 06-16 Page 3 of 3

BIOSOLIDS SPILL CONTROL PLAN
Town of Boiling Springs, NC
IN THE UNLIKELY EVENT OF A SPILL, THE FOLLOWING ACTION SHALL BE
TAKEN IMMEDIATELY:
1. MANAGEMENT OF SPILL CLEAN-UP ACTIVATES:
The Public Works Director shall take immediate charge and initiate clean-up activates. The Town of
Boiling Springs labor and equipment is to be utilized. In the event additional labor and equipment is
required, assistance will be requested from HST Environmental Inc., the NC Department of
Transportation, and other private contractors as necessary. The Public Works Director shall also
communicate with the public on the scene, answering questions and advising in the clean-up.
2. HALT THE SOURCE OF THE SPILL:
Such as a ruptured container or damaged transport unit
3. CONTAIN THE SPILL:
Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may
be constructed to augment the straw bale containment area of the spill. The Public Works Director
or the person in charge on the spill site will advise the clean-up personnel where to get the straw
lime, and other necessary items to complete the clean-up operation, i.e., local farm supply centers,
nurseries, etc.
4. CLEAN-UP
Employ front-end loader, vacuum equipment, sludge application vehicle, and/or local septic tank
service to remove as much of the spilled material as possible. Straw and/or sand should be used
in the spill area to soak up the remaining material. The straw -and sand -soaked material will be col-
lected and removed to a disposal area approved by the Mooresville regional office of NCDENR.
5. FINAL CLEAN-UP
Employ rotary brush sweeper if needed, and apply lime to the spill area upon the approval of the
clean-up efforts by the Mooresville NCDENR representative. If the event occurs on private property,
the clean-up will be completed to the satisfaction of the property owner and the Mooresville NCDENR
representative. The ultimate goal will be to restore the spill area to its original condition if possible.
6. NOTIFICATION:
As soon as possible after the spill occurs, the Public Works Director will notify the Town Manager
and that person will then be responsible for notifying other key Town personnel and officials.
7. REPORTING:
The Public Works Director or the Town Manager will notify the Mooresville regional office of the
NCDENR by telephone as soon as possible, but not more than 24 hours after, or on the next
working day following the occurrence. The Public Works Director shall file a written report to the
Mooresville regional office of the NCDENR within 5 days of the occurrence.
page 2

TOWN OF BOILING SPRINGS
A. TOWN MANAGER: LUCAS SHIRES 704-434-2357 office
B. PUBLIC WORKS DIRECTOR MIKE GIBERT 704-300-8640 mobile
704-434-2357 office
C. PLANT CHIEF OPERATORS
Wastewater Supervisor: Todd Humphries 704-300-8641 mobile
704-434-5600 office
Utilities Supervisor: Joe Francis 704-300-8645 mobile
D. LOCAL POLICE/FIRE
911
E. CONTRACTORS HST ENVIRONMENTAL INC.
PHIL HARRIS 828-429-7802 mobile
828-453-0548 office
F. NCDENR MOORESVILLE REGIONAL OFFICE 704-663-1699
NC STATE WARNING POINT
(after hours, holidays, weekends)
( Revised May 2019 )
1-800-858-0368 (toll free)

Town of Boiling Springs, NC
LAND APPLICATION INSPECTION LOG
OK I X See Comments
DATE TIME DIGESTEFTRUCK SITE FIELD ORC COMMENTS

WATER POLLUTION CONTROL SYSTEM OPERATOR DESIGNATION FORM (WPCSOCC)
NCAC 15A 8G .0201
Press TAB to enter information
Permittee Owner/Officer Name: Lucas A Shires
Mailing Address: PO Box 1014 Phone: [phone]
City: Boiling Springs State: NC zip: 28017
Email Address: [e-mail]
Signature: &094...r Date: /o /$ 1
Facility Name: Town of Boiling Springs Permit # W00018352
County: Cleveland
YOU MUST SUBMIT A SEPARATE FORM FOR EACH TYPE AND CLASSIFICATION OF SYSTEM:
Facility Type: LA
Facility Grade: I
OPERATOR IN RESPONSIBLE CHARGE (ORC)
Print Full Name: Todd Michael Humphries Work Phone: [phone]
Certificate Type: LA Certificate Grade: I Certificate #: 994587
Email Address: to-ddd...hum/phrie/[e-mail]
Signature: Effective Date:
1 certify that / agree to my designation as the Operator in Responsible Charge for the facility noted. l understand and will abide by the
rules and regulations pertaining to the responsibilities of the ORC as set forth in 15A NCAC 08G .0204 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
BACKUP ORC
Print Full Name: Michael Franklin Gibert Work Phone:[phone]
Certificate Type: LA Certificate Grade: I Certificate #: 14756
Email Address: [e-mail]
Signature: Zir .14 Effective Date: / O 15 — t
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by
the rules and regulations pertaining to the responsibilities of the ORC as set forth in 15A NCAC 08G .0204 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Mail, fax or email WPCSOCC, 1618 Mail Service Center, Fax: [phone] Email: [e-mail]
ORIGINAL to: Raleigh, NC 27699-1618
Mail or Fax Asheville
Fayetteville
Mooresville
Raleigh
a COPY to: 2090 US Hwy 70
225 Green St., Suite 714
610 E. Center Ave., Suite 301
3800 Barrett Dr.
Swannanoa, NC 28778
Fayetteville, NC28301-5043
Mooresville, NC28115
Raleigh, NC27609
Fax:[phone]
Fax:[phone]
Fax:[phone]
Fax:[phone]
Phone:[phone]
Phone:[phone]
Phone:[phone]
Phone:[phone]
Washington Wilmington Winston-Salem
943 Washington Sq. Mall 127 Cardinal Dr. 45 W. Hanes Mall Rd.
Washington, NC 27889 Wilmington, NC 28405-2845 Winston-Salem, NC 27105
Fax:[phone] Fax:[phone] Fax:[phone]
Phone:[phone] Phone:[phone] Phone:[phone]
Revised 412016

SAMPLING PLAN
Samples are collected from the digester for TCLP analysis, Soil Fertility analysis, Metals, TKN, PAN,
Total Solids, (7) Fecal Coliform MPN once per permit cycle and sent to Pace Analytical for testing.
Samples are collected/tested from the digester for (7) Sour Tests and Ph in-house.

�i -
M
ACCESS RD
+JL
50' BUFFE
' BUFFE
® UNSUITABLE AREA
® APPLICATI❑N AREA
BUILDING
TOTAL PARCEL ACREAGE
JP1 22,41 ACRES
P2 35.93 ACRES
JP3 55.29 ACRES
TOTAL APPLICATI❑N
ACREAGE
op,
9,84 ACRES
P2 16,36 ACRES
JP3 13,78 ACRES
W
J 400' `�
BUFFER
UNNAMED
TRIBUTARY TO
GROG CREEK
100' BUFFER
BOILING SPRINGS
Odom
Engineering
PLLC
169 Oak Street, Forest City, N.C. 28043
ph: 828.247.4495 fax: [phone]
NC Firm#: P-0880
APPLICATION AREA OFF OF
MOUNT PLEASANT CHURCH
R
(JAMES PETTY PROPERTY)
05 16 2019
» >
SCALE: 1 =500

OdOYn
111
PROPERTY OWNED BY
JAMES PETTY & WILMA PETTY TO
BE USED FOR LAND APPLICATION
05/16/2019
Engineering
PLLC
169 Oak Street, Forest City, N.C. 28043
ph: 828.247.4495 fax: [phone]
NC Firm#: P-0880
OF SLUDGE FROM BOILING SPRINGS
WASTE WATER TREATMENT PLANT.
BOILING SPRINGS SOUTH
QUARANGLE (1971)
» >
SCALE: 1 =1000

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PROPERTY OWNED BY
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PLLC
169 Oak Street, Forest City, N.C. 28043
ph: 828.247.4495 fax: [phone]
NC Firm#: P-0880
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Odom
Engineering
PLLC
169 Oak Street, Forest City, N.C. 28043
ph: 828.247.4495 fax: [phone]
NC Firm#: P-0880
BOILING SPRINGS WASTEWATER
TREATMENT PLANT VICINITY MAP
05/16/2019
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Soil Map —Cleveland County, North Carolina
JAMES PETTY PROPERTY
U,3oA Natural Resources Web Soil Survey 9/29/2014
Conservation Service National Cooperative Soil Survey Page 3 of 3

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
August 28, 2015
Mr. Mike Gibert
Town of Boiling Springs
PO Box 1014
145 S. Main Street
Boiling Springs, NC 28017
RE: Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Dear Mr. Gibert:
Enclosed are the analytical results for sample(s) received by the laboratory on August 12, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, ^ Q Q
Tabitha M Dacal
[e-mail]
Project Manager
Enclosures
�pQ A«FO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
9eU �y
without the written consent of Pace Analytical Services, Inc..
Page 1 of 32

acmnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg,
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification M 41590
Arizona Certification M AZ0734
Arkansas Certification
California Certification M 04222CA
Colorado Certification
Connecticut Certification M PH-0694
Delaware Certification
Florida/TNI Certification M E87683
Georgia Certification M C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification M 391
Kansas/TNI Certification M E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DEQ/TNI Certification #: 4086
Maine Certification M PA00091
Maryland Certification #: 308
Massachusetts Certification M M-PA1457
Michigan/PADEP Certification
Missouri Certification M 235
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Charlotte Certification IDs
CERTIFICATIONS
PA 15601 Montana Certification #: Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/TNI Certification #: 2976
New Jersey/TNI Certification #: PA 051
New Mexico Certification #: PA01457
New York/TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188-14-8
Utah/TNI Certification #: PA014572015-5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: 8TMS-L
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
DIGESTER SLUDGE
92262954
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92262954001
DIGESTER SLUDGE
EPA 8081
SWB
8
PASI-C
EPA 8151
LJM
3
PASI-O
EPA 6010
JDA
13
PASI-A
EPA 6010
JDA
7
PASI-A
EPA7470
SH1
1
PASI-A
EPA7471
SH1
1
PASI-A
EPA 8270
BPJ
18
PASI-C
EPA 8260
GAW
14
PASI-C
SM 2540G
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 1010
TEP
1
PASI-A
EPA 9045
MLS
1
PASI-A
SM 2710B
EWS
1
PASI-A
EPA 350.1
SER
1
PASI-A
EPA 351.2
AES2
1
PASI-A
EPA 353.2
DMN
3
PASI-A
EPA 365.1
SER
1
PASI-A
92262954002
DIGESTER SLUDGE
SW-846 7.3.3.2
BMS
1
PASI-PA
SW-846 7.3.4.2
PAS
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Sample: DIGESTER SLUDGE Lab ID: 92262954001 Collected: 08/12/15 08:00 Received: 08/12/15 12:49 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 GCS Pesticides, TCLP
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5-TP (Silvex)
Surrogates
2,4-DCAA (S)
6010 MET ICP
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 08/21/15 15:00
ND
ug/L
0.50
1
08/23/15 12:40
08/26/15 00:18
58-89-9
ND
ug/L
3.0
1
08/23/15 12:40
08/26/15 00:18
57-74-9
ND
ug/L
0.50
1
08/23/15 12:40
08/26/15 00:18
72-20-8
ND
ug/L
0.50
1
08/23/15 12:40
08/26/15 00:18
1024-57-3
ND
ug/L
1000
1
08/23/15 12:40
08/26/15 00:18
72-43-5
ND
ug/L
3.0
1
08/23/15 12:40
08/26/15 00:18
8001-35-2
55
%
10-138
1
08/23/15 12:40
08/26/15 00:18
2051-24-3
48
%
10-110
1
08/23/15 12:40
08/26/15 00:18
877-09-8
Analytical Method: EPA 8151 Preparation Method: EPA 3510
ND
mg/L
0.010
1
08/19/15 15:35
08/20/15 06:20
94-75-7
ND
mg/L
0.010
1
08/19/15 15:35
08/20/15 06:20
93-72-1
91
%
42-142
1
08/19/15 15:35
08/20/15 06:20
19719-28-9
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
7460
mg/kg
441
1
08/13/15 19:30
08/18/15 00:34
7429-90-5
Arsenic
ND
mg/kg
44.1
1
08/13/15 19:30
08/18/15 00:34
7440-38-2
Cadmium
ND
mg/kg
4.4
1
08/13/15 19:30
08/18/15 00:34
7440-43-9
Calcium
49400
mg/kg
441
1
08/13/15 19:30
08/18/15 00:34
7440-70-2
Copper
230
mg/kg
22.1
1
08/13/15 19:30
08/18/15 00:34
7440-50-8
Lead
ND
mg/kg
22.1
1
08/13/15 19:30
08/18/1516:13
7439-92-1
Magnesium
3350
mg/kg
441
1
08/13/15 19:30
08/18/15 00:34
7439-95-4
Molybdenum
ND
mg/kg
22.1
1
08/13/15 19:30
08/18/15 00:34
7439-98-7
Nickel
24.6
mg/kg
22.1
1
08/13/15 19:30
08/18/15 00:34
7440-02-0
Potassium
ND
mg/kg
22100
1
08/13/15 19:30
08/18/15 00:34
7440-09-7
Selenium
ND
mg/kg
44.1
1
08/13/15 19:30
08/18/15 00:34
7782-49-2
Sodium
ND
mg/kg
22100
1
08/13/15 19:30
08/18/15 00:34
7440-23-5
Zinc
712
mg/kg
44.1
1
08/13/15 19:30
08/18/15 00:34
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010
Leachate Method/Date: EPA 1311; 08/18/15 03:30
Arsenic
ND
mg/L
0.050
1
08/19/15 02:05
08/19/15 18:10
7440-38-2
Barium
0.36
mg/L
0.25
1
08/19/15 02:05
08/19/15 18:10
7440-39-3
Cadmium
ND
mg/L
0.0050
1
08/19/15 02:05
08/19/15 18:10
7440-43-9
Chromium
ND
mg/L
0.025
1
08/19/15 02:05
08/19/15 18:10
7440-47-3
Lead
ND
mg/L
0.025
1
08/19/15 02:05
08/19/15 18:10
7439-92-1
Selenium
ND
mg/L
0.10
1
08/19/15 02:05
08/19/15 18:10
7782-49-2
Silver
ND
mg/L
0.025
1
08/19/15 02:05
08/19/15 18:10
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Leachate Method/Date: EPA 1311; 08/18/15 03:30
Mercury
ND
mg/L
0.00020
1
08/19/1516:20
08/26/1512:00
7439-97-6
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 08/28/2015 05:42 PM
without
the written consent of Pace Analytical Services,
Inc..
Page 4 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Sample: DIGESTER SLUDGE Lab ID: 92262954001 Collected: 08/12/15 08:00 Received: 08/12/15 12:49 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.94 mg/kg 0.23 1 08/19/1518:55 08/24/1514:58 7439-97-6
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 08/21/15 15:00
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
1*1414L,WAIts] I:
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
2540G Total Percent Solids
rir.M��rrn
Date: 08/28/2015 05:42 PM
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
106-46-7
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
121-14-2
L3
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
87-68-3
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
118-74-1
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
67-72-1
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
95-48-7
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
98-95-3
ND
ug/L
100
1
08/21/1513:18
08/24/1518:23
87-86-5
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
110-86-1
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
95-95-4
L3
ND
ug/L
50.0
1
08/21/1513:18
08/24/1518:23
88-06-2
L3
35
%
12-102
1
08/21/1513:18
08/24/1518:23
4165-60-0
42
%
13-107
1
08/21/1513:18
08/24/1518:23
321-60-8
45
%
21-132
1
08/21/1513:18
08/24/1518:23
1718-51-0
10
%
10-110
1
08/21/1513:18
08/24/1518:23
13127-88-3
10
%
10-110
1
08/21/1513:18
08/24/1518:23
367-12-4
19
%
27-108
1
08/21/1513:18
08/24/1518:23
118-79-6
SO
Analytical Method:
EPA 8260 Leachate Method/Date:
EPA 1311; 08/20/15
15:23
ND
ug/L
100
20
08/27/1512:59
71-43-2
ND
ug/L
200
20
08/27/1512:59
78-93-3
ND
ug/L
100
20
08/27/1512:59
56-23-5
ND
ug/L
100
20
08/27/1512:59
108-90-7
ND
ug/L
100
20
08/27/1512:59
67-66-3
ND
ug/L
100
20
08/27/1512:59
106-46-7
ND
ug/L
100
20
08/27/1512:59
107-06-2
ND
ug/L
100
20
08/27/1512:59
75-35-4
ND
ug/L
100
20
08/27/1512:59
127-18-4
ND
ug/L
100
20
08/27/1512:59
79-01-6
ND
ug/L
100
20
08/27/1512:59
75-01-4
102
%
70-130
20
08/27/1512:59
17060-07-0
102
%
67-135
20
08/27/1512:59
2037-26-5
101
%
70-130
20
08/27/1512:59
460-00-4
Analytical Method:
SM 2540G
1.8
%
0.000010
1
08/12/1517:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Sample: DIGESTER SLUDGE
Lab ID: 92262954001 Collected:
08/12/15
08:00
Received: 08/12/15 12:49 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
98.2 %
0.10
1
08/13/15 12:28
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200 deg F
70.0
1
08/21/15 13:00
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
6.5 Std. Units
0.10
1
08/13/15 14:35
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
10500 mg/kg
0.12
1
08/21/15 16:28
N2
350.1 Ammonia
Analytical Method: EPA 350.1
Nitrogen, Ammonia
ND mg/kg
537
1
08/18/15 06:16
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
48400 mg/kg
5070
5
08/21/15 14:35
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
9070 mg/kg
541
5
08/20/15 13:43
Nitrogen, Nitrite
ND mg/kg
270
5
08/20/15 13:43
Nitrogen, NO2 plus NO3
9070 mg/kg
541
5
08/20/15 13:43
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
814 mg/kg
507
5
08/19/15 08:25
7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
ANALYTICAL RESULTS
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Sample: DIGESTER SLUDGE Lab ID: 92262954002 Collected: 08/12/15 08:00 Received: 08/12/15 12:49 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/L 0.010 1 08/17/15 23:28
734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/L 1.0 1 08/17/15 15:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 32

aceAnalytical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: MERP/8216
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92262954001
METHOD BLANK: 1536849
Matrix: Water
Associated Lab Samples: 92262954001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/L
ND 0.00020
08/26/1511:56
LABORATORY CONTROL SAMPLE: 1536850
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/L
.0025 0.0023
94 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1536851 1536852
MS MSD
92263163010
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND
.0025 .0025 0.0022
0.0022 85 87 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: MERP/8214
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92262954001
METHOD BLANK: 1536822
Matrix: Solid
Associated Lab Samples: 92262954001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0062
08/24/1514:51
LABORATORY CONTROL SAMPLE: 1536823
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
.083 0.074
89 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1536824 1536825
MS MSD
92263109003
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 13.0
.052 .044 14.3
10.8 2330 -5020 75-125 28 M6, R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1536826 1536827
MS MSD
92263116007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.38 .15 .12 0.73 0.25 241 -106 75-125 99 M6,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: MPRP/19250 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92262954001
METHOD BLANK: 1533254
Associated Lab Samples: 92262954001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
08/17/15 22:47
Arsenic
mg/kg
ND
1.0
08/17/15 22:47
Cadmium
mg/kg
ND
0.10
08/17/15 22:47
Calcium
mg/kg
ND
10.0
08/17/15 22:47
Copper
mg/kg
ND
0.50
08/17/15 22:47
Lead
mg/kg
ND
0.50
08/17/15 22:47
Magnesium
mg/kg
ND
10.0
08/17/15 22:47
Molybdenum
mg/kg
ND
0.50
08/17/15 22:47
Nickel
mg/kg
ND
0.50
08/17/15 22:47
Potassium
mg/kg
ND
500
08/17/15 22:47
Selenium
mg/kg
ND
1.0
08/17/15 22:47
Sodium
mg/kg
ND
500
08/17/15 22:47
Zinc
mg/kg
ND
1.0
08/17/15 22:47
LABORATORY CONTROL SAMPLE:
1533255
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Qualifiers
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
500
484
97
80-120
50
46.5
93
80-120
50
47.6
95
80-120
500
491
98
80-120
50
48.1
96
80-120
50
47.8
96
80-120
500
484
97
80-120
50
48.0
96
80-120
50
47.1
94
80-120
500
ND
96
80-120
50
47.0
94
80-120
500
497J
99
80-120
50
47.9
96
80-120
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1533256
1533257
MS
MSD
92263109003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Aluminum mg/kg
5350
376
441
6570
6400
326
240
75-125 3 M1
Arsenic mg/kg
1.2
37.6
44.1
33.5
38.5
86
84
75-125 14
Cadmium mg/kg
ND
37.6
44.1
34.6
39.9
92
90
75-125 14
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 32

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1533256
1533257
MS
MSD
92263109003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
326
376
441
576
630
66
69
75-125
9 M1
Copper
mg/kg
2.0
37.6
44.1
37.3
42.5
94
92
75-125
13
Lead
mg/kg
6.2
37.6
44.1
38.7
43.9
86
85
75-125
12
Magnesium
mg/kg
104
376
441
504
550
106
101
75-125
9
Molybdenum
mg/kg
ND
37.6
44.1
33.6
39.1
88
88
75-125
15
Nickel
mg/kg
1.8
37.6
44.1
36.2
41.3
92
90
75-125
13
Potassium
mg/kg
ND
376
441
418
472
96
94
75-125
12
Selenium
mg/kg
ND
37.6
44.1
32.8
38.1
87
86
75-125
15
Sodium
mg/kg
ND
376
441
367J
424J
96
95
75-125
Zinc
mg/kg
3.6
37.6
44.1
38.9
44.0
94
92
75-125
12
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1533258
1533259
MS
MSD
92263116007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
16700
920
1400
20600
21200
425
320
75-125
3 M1,M6
Arsenic
mg/kg
ND
92
140
95.2
138
95
93
75-125
37 R1
Cadmium
mg/kg
ND
92
140
85.8
132
93
95
75-125
42 R1
Calcium
mg/kg
252000
920
1400
210000
121000
-4610
-9400
75-125
54 M6, R1
Copper
mg/kg
113
92
140
191
221
85
77
75-125
14
Lead
mg/kg
21.4
92
140
104
131
90
78
75-125
23 R1
Magnesium
mg/kg
990
920
1400
1820
1960
90
69
75-125
7 M1
Molybdenum
mg/kg
ND
92
140
90.5
130
88
86
75-125
36 R1
Nickel
mg/kg
27.1
92
140
111
138
92
80
75-125
22 R1
Potassium
mg/kg
4830
920
1400
5550
5770
79
67
75-125
4 M1
Selenium
mg/kg
ND
92
140
75.3
120
82
86
75-125
46 R1
Sodium
mg/kg
72100
920
1400
71500
66600
-65
-391
75-125
7 M6
Zinc
mg/kg
386
92
140
427
369
44
-12
75-125
15 M1,M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 32

aceAnalytical
-pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: MPRP/19278 Analysis Method: EPA6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92262954001
METHOD BLANK: 1536646
Matrix:
Water
Associated Lab Samples: 92262954001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
08/19/1517:59
Barium
mg/L
ND
0.25
08/19/1517:59
Cadmium
mg/L
ND
0.0050
08/19/1517:59
Chromium
mg/L
ND
0.025
08/20/1510:47
Lead
mg/L
ND
0.025
08/19/1517:59
Selenium
mg/L
ND
0.10
08/19/1517:59
Silver
mg/L
ND
0.025
08/19/1517:59
LABORATORY CONTROL SAMPLE:
1536647
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.6
105
80-120
Barium
mg/L
2.5
2.4
96
80-120
Cadmium
mg/L
2.5
2.5
98
80-120
Chromium
mg/L
2.5
2.5
99
80-120
Lead
mg/L
2.5
2.4
95
80-120
Selenium
mg/L
2.5
2.7
107
80-120
Silver
mg/L
1.2
1.3
105
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1536648
1536649
MS
MSD
92263163010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.8
2.9
113
116
75-125
3
Barium
mg/L
0.65
2.5
2.5
3.1
3.2
99
102
75-125
2
Cadmium
mg/L
ND
2.5
2.5
2.7
2.7
108
109
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.7
2.7
108
109
75-125
1
Lead
mg/L
ND
2.5
2.5
2.6
2.6
102
104
75-125
2
Selenium
mg/L
ND
2.5
2.5
2.8
2.9
113
115
75-125
2
Silver
mg/L
ND
1.2
1.2
1.4
1.4
113
115
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: MSV/33147 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV TCLP
Associated Lab Samples: 92262954001
METHOD BLANK: 1542935
Associated Lab Samples: 92262954001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1-Dichloroethene
ug/L
ND
5.0
08/27/15 12:43
1,2-Dichloroethane
ug/L
ND
5.0
08/27/15 12:43
1,4-Dichlorobenzene
ug/L
ND
5.0
08/27/15 12:43
2-Butanone (MEK)
ug/L
ND
10.0
08/27/15 12:43
Benzene
ug/L
ND
5.0
08/27/15 12:43
Carbon tetrachloride
ug/L
ND
5.0
08/27/15 12:43
Chlorobenzene
ug/L
ND
5.0
08/27/15 12:43
Chloroform
ug/L
ND
5.0
08/27/15 12:43
Tetrachloroethene
ug/L
ND
5.0
08/27/15 12:43
Trichloroethene
ug/L
ND
5.0
08/27/15 12:43
Vinyl chloride
ug/L
ND
5.0
08/27/15 12:43
1,2-Dichloroethane-d4 (S)
%
102
70-130
08/27/15 12:43
4-Bromofluorobenzene (S)
%
104
70-130
08/27/15 12:43
Toluene-d8 (S)
%
99
67-135
08/27/15 12:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1542936
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1-Dichloroethene
ug/L
50
50.8
102
66-135
1,2-Dichloroethane
ug/L
50
43.0
86
67-128
1,4-Dichlorobenzene
ug/L
50
45.5
91
78-130
2-Butanone (MEK)
ug/L
100
96.7
97
61-144
Benzene
ug/L
50
49.1
98
80-125
Carbon tetrachloride
ug/L
50
48.0
96
69-131
Chlorobenzene
ug/L
50
46.8
94
81-122
Chloroform
ug/L
50
48.8
98
73-127
Tetrachloroethene
ug/L
50
46.5
93
78-122
Trichloroethene
ug/L
50
45.9
92
78-122
Vinyl chloride
ug/L
50
45.5
91
58-137
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
100
67-135
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: OEXT/37251 Analysis Method: EPA 8081
QC Batch Method: EPA 3510 Analysis Description: 8081 GCS TCLP Pesticides
Associated Lab Samples: 92262954001
METHOD BLANK: 1539807
Associated Lab Samples: 92262954001
Parameter
Chlordane (Technical)
Endrin
gamma-BHC (Lindane)
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ug/L
ND
3.0
08/26/15 01:50
ug/L
ND
0.50
08/26/15 01:50
ug/L
ND
0.50
08/26/15 01:50
ug/L
ND
0.50
08/26/15 01:50
ug/L
ND
1000
08/26/15 01:50
ug/L
ND
3.0
08/26/15 01:50
%
75
10-138
08/26/15 01:50
%
101
10-110
08/26/15 01:50
LABORATORY CONTROL SAMPLE & LCSD:
1539808
1539809
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qualifiers
Endrin
ug/L
1.2
1.6
1.6
125
126
20-134
1 30
gamma-BHC (Lindane)
ug/L
1.2
1.4
1.3
112
105
20-118
6 30
Heptachlor epoxide
ug/L
1.2
1.3
1.3
103
106
22-133
3 30
Methoxychlor
ug/L
3.7
ND
ND
105
107
44-150
30
Decachlorobiphenyl (S)
%
76
72
10-138
Tetrachloro-m-xylene (S)
%
106
103
10-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: OEXT/23901 Analysis Method: EPA 8151
QC Batch Method: EPA 3510 Analysis Description: 8151 GCS Herbicides TCLP
Associated Lab Samples: 92262954001
METHOD BLANK: 1304729
Matrix:
Water
Associated Lab Samples: 92262954001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
2,4,5-TP (Silvex)
mg/L
ND
0.00019
08/19/15 11:23
2,4-D
mg/L
ND
0.00094
08/19/15 11:23
2,4-DCAA (S)
%
95
42-142
08/19/15 11:23
METHOD BLANK: 1306400
Matrix:
Water
Associated Lab Samples: 92262954001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
2,4,5-TP (Silvex)
mg/L
ND
0.00019
08/20/15 03:49
2,4-D
mg/L
ND
0.00094
08/20/15 03:49
2,4-DCAA (S)
%
94
42-142
08/20/15 03:49
Qualifiers
Qualifiers
LABORATORY CONTROL SAMPLE: 1304730
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
2,4,5-TP (Silvex) mg/L .012 0.014 117 27-170
2,4-D mg/L .06 0.062 104 23-163
2,4-DCAA (S) % 96 42-142
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1305103
1305104
MS
MSD
35202408001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4,5-TP (Silvex)
mg/L
0.00004 .012
.012
0.017
0.012
141
104
27-170 30
9U
2,4-D
mg/L
0.00022 .06
.06
0.074
0.054
124
90
23-163 31 R1
U
2,4-DCAA (S)
%
104
79
42-142
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: OEXT/37228 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 TCLP MSSV
Associated Lab Samples: 92262954001
METHOD BLANK: 1539355
Associated Lab Samples: 92262954001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
08/24/15 10:43
2,4,5-Trichlorophenol
ug/L
ND
50.0
08/24/15 10:43
2,4,6-Trichlorophenol
ug/L
ND
50.0
08/24/15 10:43
2,4-Dinitrotoluene
ug/L
ND
50.0
08/24/15 10:43
2-Methylphenol(o-Cresol)
ug/L
ND
50.0
08/24/15 10:43
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
50.0
08/24/15 10:43
Hexachloro-1,3-butadiene
ug/L
ND
50.0
08/24/15 10:43
Hexachlorobenzene
ug/L
ND
50.0
08/24/15 10:43
Hexachloroethane
ug/L
ND
50.0
08/24/15 10:43
Nitrobenzene
ug/L
ND
50.0
08/24/15 10:43
Pentachlorophenol
ug/L
ND
100
08/24/15 10:43
Pyridine
ug/L
ND
50.0
08/24/15 10:43
2,4,6-Tribromophenol (S)
%
90
27-108
08/24/15 10:43
2-Fluorobiphenyl (S)
%
80
13-107
08/24/15 10:43
2-Fluorophenol (S)
%
36
10-110
08/24/15 10:43
Nitrobenzene-d5 (S)
%
71
12-102
08/24/15 10:43
Phenol-d6 (S)
%
22
10-110
08/24/15 10:43
Terphenyl-d14 (S)
%
93
21-132
08/24/15 10:43
LABORATORY CONTROL SAMPLE:
Parameter
1539356
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,4-Dichlorobenzene
ug/L
500
397
79
10-110
2,4,5-Trichlorophenol
ug/L
500
572
114
39-108 LO
2,4,6-Trichlorophenol
ug/L
500
583
117
40-104 LO
2,4-Dinitrotoluene
ug/L
500
552
110
42-109 LO
2-Methylphenol(o-Cresol)
ug/L
500
336
67
31-110
3&4-Methyl phenol (m&p Cresol)
ug/L
500
316
63
30-110
Hexachloro-1,3-butadiene
ug/L
500
497
99
10-110
Hexachlorobenzene
ug/L
500
558
112
39-121
Hexachloroethane
ug/L
500
400
80
10-110
Nitrobenzene
ug/L
500
404
81
32-101
Pentachlorophenol
ug/L
1000
1000
100
18-108
Pyridine
ug/L
500
180
36
10-110
2,4,6-Tribromophenol (S)
%
120
27-108 SO
2-Fluorobiphenyl (S)
%
89
13-107
2-Fluorophenol(S)
%
49
10-110
Nitrobenzene-d5(S)
%
88
12-102
Phenol-d6 (S)
%
32
10-110
Terphenyl-d14(S)
%
100
21-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1539357
1539358
MS
MSD
92264092001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
500
500
398
377
80
75
30-150
5
2,4,5-Trichlorophenol
ug/L
ND
500
500
564
508
113
102
30-150
10
2,4,6-Trichlorophenol
ug/L
ND
500
500
551
475
110
95
30-150
15
2,4-Dinitrotoluene
ug/L
ND
500
500
572
536
114
107
30-150
6
2-Methylphenol(o-Cresol)
ug/L
ND
500
500
310
265
62
53
30-150
15
3&4-Methyl phenol (m&p
ug/L
ND
500
500
279
222
56
44
30-150
22
Cresol)
Hexachloro-1,3-butadiene
ug/L
ND
500
500
559
523
112
105
30-150
7
Hexachlorobenzene
ug/L
ND
500
500
552
518
110
104
30-150
6
Hexachloroethane
ug/L
ND
500
500
397
376
79
75
30-150
6
Nitrobenzene
ug/L
ND
500
500
426
366
85
73
30-150
15
Pentachlorophenol
ug/L
ND
1000
1000
969
881
97
88
30-150
9
Pyridine
ug/L
ND
500
500
98.0
148
20
30
30-150
40 M1,R1
2,4,6-Tribromophenol (S)
%
121
107
27-108
SO
2-Fluorobiphenyl (S)
%
90
70
13-107
2-Fluorophenol(S)
%
44
42
10-110
Nitrobenzene-d5(S)
%
88
78
12-102
Phenol-d6 (S)
%
30
26
10-110
Terphenyl-d14(S)
%
106
86
21-132
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1539359
1539360
MS
MSD
92264011001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1,4-Dichlorobenzene
ug/L
ND
500
500
345
354
69
71
30-150
2
2,4,5-Trichlorophenol
ug/L
ND
500
500
564
555
113
111
30-150
2
2,4,6-Trichlorophenol
ug/L
ND
500
500
547
524
109
105
30-150
4
2,4-Dinitrotoluene
ug/L
ND
500
500
523
527
105
105
30-150
1
2-Methylphenol(o-Cresol)
ug/L
ND
500
500
276
285
55
57
30-150
3
3&4-Methyl phenol (m&p
ug/L
ND
500
500
246
250
49
50
30-150
2
Cresol)
Hexachloro-1,3-butadiene
ug/L
ND
500
500
484
490
97
98
30-150
1
Hexachlorobenzene
ug/L
ND
500
500
561
560
112
112
30-150
0
Hexachloroethane
ug/L
ND
500
500
318
334
64
67
30-150
5
Nitrobenzene
ug/L
ND
500
500
374
383
75
77
30-150
2
Pentachlorophenol
ug/L
ND
1000
1000
981
1010
98
101
30-150
3
Pyridine
ug/L
ND
500
500
115
175
23
35
30-150
41 M1,R1
2,4,6-Tribromophenol (S)
%
122
120
27-108
SO
2-Fluorobiphenyl (S)
%
83
80
13-107
2-Fluorophenol(S)
%
43
44
10-110
Nitrobenzene-d5(S)
%
81
80
12-102
Phenol-d6 (S)
%
29
27
10-110
Terphenyl-d14(S)
%
87
85
21-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 17 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: PMST/8243 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92262954001
SAMPLE DUPLICATE: 1532484
92262985001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 5.0 5.0 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 18 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WET/39610 Analysis Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92262954001
SAMPLE DUPLICATE: 1539313
92263404001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 19 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WET/39452 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92262954001
SAMPLE DUPLICATE: 1532624
Parameter
pH at 25 Degrees C
92262701001 Dup
Units Result Result RPD Qualifiers
Std. Units 7.4 7.6 2 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 20 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/24148
Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92262954001
METHOD BLANK: 1535676
Matrix: Solid
Associated Lab Samples: 92262954001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Ammonia mg/kg
ND 10.0
08/18/15 06:00
LABORATORY CONTROL SAMPLE: 1535677
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg
500 546
109 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1535678 1535679
MS MSD
92262843002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND
45000 45000 51400
51500 114 114 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 21 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/24155
Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2
Analysis Description: 351.2 TKN
Associated Lab Samples: 92262954001
METHOD BLANK: 1535720
Matrix: Solid
Associated Lab Samples: 92262954001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 50.0
08/21/15 13:44
LABORATORY CONTROL SAMPLE: 1535721
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000 1060
106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1535722 1535723
MS MSD
92262843002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 21600
36700 36700 58800
62100 101 110 90-110 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 22 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/24178 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92262954001
METHOD BLANK: 1537689
Matrix:
Solid
Associated Lab Samples: 92262954001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND
2.0
08/20/15 13:24
Nitrogen, Nitrite
mg/kg
ND
1.0
08/20/15 13:24
Nitrogen, NO2 plus NO3
mg/kg
ND
2.0
08/20/15 13:24
LABORATORY CONTROL SAMPLE:
1537690
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
25
24.8
99 90-110
Nitrogen, Nitrite
mg/kg
10
10.0
100 90-110
Nitrogen, NO2 plus NO3
mg/kg
25
24.8
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1537691
1537692
MS
MSD
92263864001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
52.2
52.2
50.0
49.7
96
95
90-110
1
Nitrogen, Nitrite
mg/kg
ND
21.9
21.9
23.6
23.7
108
108
90-110
0
Nitrogen, NO2 plus NO3
mg/kg
ND
52.2
52.2
50.0
49.7
96
95
90-110
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/24151
Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92262954001
METHOD BLANK: 1535700
Matrix: Solid
Associated Lab Samples: 92262954001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 2.0
08/19/15 07:57
LABORATORY CONTROL SAMPLE: 1535701
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
50 54.8
110 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1535702 1535703
MS MSD
92263220001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 132
191 194 189
198 30 34 90-110 5 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 24 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/20931 Analysis Method: SW-846 7.3.3.2
QC Batch Method: SW-846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92262954002
METHOD BLANK: 938356 Matrix: Water
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/L ND 0.010 08/17/15 23:28
SAMPLE DUPLICATE: 938357
30156289001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/L ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 25 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
QC Batch: WETA/20932 Analysis Method: SW-846 7.3.4.2
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 92262954002
METHOD BLANK: 938359 Matrix: Water
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide, Reactive mg/L ND 1.0 08/17/15 15:15
SAMPLE DUPLICATE: 938360
30156289001 Dup
Parameter Units Result Result RPD Qualifiers
Sulfide, Reactive mg/L ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc..
Page 26 of 32

Pace Analytical Services, Inc
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, INC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical Services - Asheville
PASI-C
Pace Analytical Services - Charlotte
PASI-O
Pace Analytical Services - Ormond Beach
PASI-PA
Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TN accreditation for this parameter.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/28/2015 05:42 PM without the written consent of Pace Analytical Services, Inc.. Page 27 of 32

aceAnalytical
—pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DIGESTER SLUDGE
Pace Project No.: 92262954
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92262954001
DIGESTER SLUDGE
EPA 3510
OEXT/37251
EPA 8081
92262954001
DIGESTER SLUDGE
EPA 3510
OEXT/23901
EPA 8151
92262954001
DIGESTER SLUDGE
EPA 3050
MPRP/19250
EPA 6010
92262954001
DIGESTER SLUDGE
EPA 3010
MPRP/19278
EPA 6010
92262954001
DIGESTER SLUDGE
EPA 7470
MERP/8216
EPA 7470
92262954001
DIGESTER SLUDGE
EPA 7471
MERP/8214
EPA 7471
92262954001
DIGESTER SLUDGE
EPA 3510
OEXT/37228
EPA 8270
92262954001
DIGESTER SLUDGE
EPA 8260
MSV/33147
92262954001
DIGESTER SLUDGE
SM 2540G
OEXT/37081
92262954001
DIGESTER SLUDGE
ASTM D2974-87
PMST/8243
92262954001
DIGESTER SLUDGE
EPA 1010
WET/39610
92262954001
DIGESTER SLUDGE
EPA 9045
WET/39452
92262954001
DIGESTER SLUDGE
SM 2710B
WET/39621
92262954001
DIGESTER SLUDGE
EPA 350.1
WETA/24148
92262954001
DIGESTER SLUDGE
EPA 351.2
WETA/24155
92262954001
DIGESTER SLUDGE
EPA 353.2
WETA/24178
92262954001
DIGESTER SLUDGE
EPA 365.1
WETA/24151
92262954002
DIGESTER SLUDGE
SW-846 7.3.3.2
WETA/20931
92262954002
DIGESTER SLUDGE
SW-846 7.3.4.2
WETA/20932
Date: 08/28/2015 05:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
GCSV/22358
GCSV/15523
ICP/17311
ICP/17335
MERC/7891
MERC/7887
MSSV/11123
Page 28 of 32

Document Name:
aceAivlAical' Sample Condition Upon Recei
Document Number:
F-CHR-CS-003-rev.16
Document Revised: May 18, 2015
Page 1 of 2*
Issuing Authority:
Pace Huntersville Qualitv Office
Client Name: �V1�y
* Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ C ercial❑ e
Other
Custody Seal on Cooler/Box Present: El yes no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble VDp _ B bble Bags ❑ None ❑ Other
Thermometer used: IR Gun 140 Type of Ice: et lue None Q,'6a'mples on ice, cooling process has begun
L/
Temn Correction Factor T1401 No Correction )
Date and Initials of person exa
i tnwg
_
Temp should be above freezing to 6°C Comments:
contents: -
Chain of Custody Present: ves No 21 NIA
1.
Chain of Custody Filled Out: Yes No NIA
2.
Chain of Custody Relinquished: es o ❑N1A
3.
Sampler Name & Signature on COC: es ' o ❑NIA
4.
Samples Arrived within Hold Time: Ores ❑No gM<
5.
Short Hold Time Analysis (<72hr): Dyes o NIA
6.
Rush Turn Around Time Requested: Dyes No PWA
7.
Sufficient Volume: Dyes o El NIA
18. all
Correct Containers Used: Yos% � E3NlA
-Pace Containers Used: ❑Y No ❑NIA
9,
Containers Intact: Yes ❑No ❑NIA
10.
Filtered volume received for Dissolved tests Dyes ❑
11.
Sample Labels match COC: es No ❑NIA
-Includes date/time/ID/Analysis Matrix:
12.
All containers needing preservation have been checked.
Dyes ❑Na WIA
All containers needing preservation are found to be in Dyes ❑No NI
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, VVI-DRO (water) Dyes ❑
,
Samples checked for dechlorination: Dyes ❑No NIA
Headspace in VOA Vials( >6mm): Dyes ❑No 1[3I
Trip Blank Present: Dyes ❑Na <NIA
Trip Blank Custody Seals Present Dyes ❑No -16NIA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review:
Plana lahal hero
w®#g92262954
Note: Whenever there is a discrepancy affecting North Carolina compliance HIM
111111111111111samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp, 9Z26�g54
incorrect containers)
Page 29 of 32

ITEM #
m
ro
a
o
n m
i3
a9
3
N
1 )
b 4
O
a
t
a n
G
p
o
oIL
n
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