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WQ0001489_Residual Annual Report 2014_20150302
may. i UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER BOX 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER 5090/07202 LN . gVbruary 24, 2015 Division of Water Resources MAN 0 2 2015 Information Processing Unit 16.17 Mail service Center 9NPORfl�ATDWR SECTION 10NPROCESSINGUN(T Raleigh, NC 27699 SUBJECT: TREATMENT AND LAND APPLICATION OF RESIDUALS Marine Corps Air Station (MCAS) Cherry Point submits the enclosed original and two (2) copies of our 2014 Treatment and Land Application of Residuals Report for permit WQ0001489. During the 2014 reporting year, 475.40 dry tons were land applied on 87.46 acres of Sites 1 through 4 of our ten permitted application sites that encompass 417 acres. The applied sludge was only from the approved residual source Cherry Point wastewater treatment plant (WWTP), permit NC0003816. The other permit approved residual sources (WQ0005233, WQ0004240, and WQ0007217) did not generate any sludge requiring land application, thus no source analysis was required. The analysis for total phosphorus was unintentionally omitted during the August 4, 2014 sampling event. The total phosphorus calculations are therefore based on the most recent analytical results (January 14, 2014; 40,100 mg/kg). This value is significantly higher than the five year average (2010-2014) of 29,220 mg/kg. Under permit NC0003816, MCAS Cherry Point completed a project to convert the anaerobic digesters to aerobic. This project generated residual sludge which was applied to sites 3 and 4 with concurrence of Will Hart (DWR-Washington). Due to the length of time the sludge resided in the off-line digesters (June 2010 to March 2014), we assumed that the pathogen reduction criteria established in 15A NCAC 02T.1106(c)(2) was met for a minimum residence cell time of 15 days at 103 OF and that volatile reduction was met through anaerobic digestion. Upon review of the completed surveys of the applications to Site 4, it was noted that a small portion of sludge was applied outside of the permitted area. Follow-up investigation of the affected areas (approximately 0.05 acres) showed that the cover crop had quickly recovered from the application and the areas had fully stabilized with no significant impact to the environment. This was reported to Will Hart (DWR-Washington) via phone on January 14, 2015. In review of past data in preparing this report, two spreadsheet errors were found in previously submitted reports. The first error was the annual application pounds per acre of all loading criteria on Field 4 for CY2010 was not captured in the CY2011 prior year's cumulative loading, and thus carried through to. CY2013. The second error was the annual application pounds per acre for Zinc on Field 1 for CY2013 did not accurately sum the -loading for all events. These errors have been corrected and the accurate cumulative totals are provided in this report. For additional information, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at (252) 466-2754. Sincerely, CA G. W. D Environm nt 1 Affairs Officer By direc i of the Commanding Officer Enclosure: 1. 2014 Annual Land Application of Residuals Report Copy to: EPA Region 7, Biosolids Center ` N Y 2014 ANNUAL SLUDGE REPORT PACKAGE ORDER 1. the ACF 2. the RSSF 3. the MFLSF 4. the FSF 5 . Lab Report (3 copies) a. the Residuals lab report (general chemistry) b. the TCLP lab report 6. the PVRF 7. the PVRF Supporting Documents (Lime Stabilization): Lab Analysis Bench Sheets 8. the PVRF Supporting Documents (Anaerobic Digestion): Lab Analysis Bench Sheets 9. the Soils test lab report (3 copies) 10. the Triennial Groundwater Monitoring (3 copies) � � r ANNUAL LAND APPLICATION CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0001489 County: Facility -Name (as shown, on permit): Land Application Operator: Craven Year: 2014 US Marine Corps - Cherry Point Patricia T. Davis Phone: (252) 466-6787 Land application of residual solids as allowed by the permit occurred during the past calendar year? X Yes L3 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 10 Total number of fields land application occurred during the year: 4 Total amount of dry tons applied during the year for all application sites: 475.40 Total number of acres land application occurred during the year: 1 87.46 Part B: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. X Yes ® No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." G.W. ford, Environmental ?erry(itteb Name and Title (t Signature of Preparer* (if different from Permitte) * Preparer is defined in 40 CFR Part 503.9 (r) I �o? of the /5 lal 2 Q ,e b Direction Date Officer Date Signature of Land Applier Date (if different from Permittee and Preparer) DENR FORM ACF (5/2003) A RESIDUAL SAMPLING SUMMARY FORMS ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001489 Laboratory: 1) "PACE Analytical Services, Inc. Facility Name: US Marine Corps - Cherry Point NPDES # or NC0003816 WQ#: WWTP Name: USMCAS - Cherry Point WWTP Recirinni Annivaic data 2) 3) 4) 5) MMMMMMMMMMMM .. _ .. ®�®��� "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qua ' d personnel properly gathered and evaluated the information submitted. I am aware that there are sig ' i nt penalties fors tting false information, including the possibility of fines and imprisonment for knowing violations." j Y_., ignature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0001489 Laboratory: 1) PACE Analytical -Services, Inc. Facility Name: US Marine Corps - Cherry Point 2) NPDES # or WQ#: NC0003816 WWTP Name: USMCAS - Cherry Point WWTP Residual Analvsis Data 3) 4) 5) ILComposite Sample or Date. NEWSTITE000�----- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system design to assure that qualifie rsonnel properly gathered and evaluated the information submitted. I am aware that there are si ni penalties for subm' ' g false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer Date DENR FORM RSSF-B (5/2003) METALS FIELD LOADING SUMMARY FORM ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 4.4.94 Acres Permitted: 44.94 Site #: 1 Field #: Residu naly ' Data avy tals d 'Total osph sus g/k "0 50l" use w Y nt #) 1 2 3 Sample 4 5 6 7 S 9 10 11 12 or Com- posite Date 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 1/14/14 '1/14/14 % Solids 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 0.00921 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 0.0092 Chromium 0 1 0 0 0 0 0 0 0 0 0 0 0 Copper 820 820 820 820 820 820 820 820 820 820 820 820 Lead 0 0 0 1 0 0 0 0 0 0 1 0 0 1 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0. Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 56.6 56.6 56.6 56.6 56.6 56.6 56.6 56.6 56.6 56.6 56.6 56.6 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 1030 Total Phos- 40100 40100 40100 40100 40100 40100 40100 40100 40100 40100 40100 40100 horus Annual Heald Metal Field Loadings (Calculated in lbs/acre): M o 11 2 L3J 1 41 51 1617 1 1 81 1 91 10 11 12 CD ;v 0 0.2145 0.1871 0.171 0.1583 0.1938 0.1637 0.2262 0.2051 0.2186 0.2098 0.1644 0.1898 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 4E-06 3E-06 3E-06 3E-06 4E-06 3E-06 4E-06 4E-06 4E-06 4E-06 3E-06 3E-06 4E-05 Chromiurr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.3517 0.3068 0.2805 0.2597 0.3178 0.2685 0.371 0.3364 0.3586 0.3441 0.2696 0.3112 3.7757 Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 .0 0 0 0" Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0243 1 0.0212 0.0194 0.0179 0.0219 0.0185 0.0256 0.0232 0.0248' 0.0237 0.0186 0.0215 0.2606 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.4418 0.3854 0.3523 0.3262 0.3991 0.3372 0.466 0.4225 0.4504 0.4322 0.3386 0.3909 4.7426 Total Phos- 17.201 15.004 13.718 12.7 15.539 13.128 18.141 16.45 17.536 16.826 13.182 15.218 ' 184.64 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the inform on submitted. I am aw that there are significant penalties for submitting false information, inc u i t e Assibility of finid imprison ent for knowing violations" ay Signature of Land Appli r Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Forin jo be submitted in Annual Report Facility Name: USMCAS Cherry Point WWTP Total Dry Tons Applied (Annual): 146.273175 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 44.94 Acres Permitted: 44.94 Site #: 1 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date [-J] 1/14/14 z 1/14/14 [ s 1/14/14 1%14/14 8/4/14 [6] 0 ® Fs ,o „ ,2 % Solids 1 1.7 1.7 1.7 1.7 1.3 0 0 0 0 0 ium 0.0092 0.0092 0.0092 0.0092 0.014 kenic mium 0 0 - 0 0 0 per 820 1 820 820 1 820 1520 Lead 0 0 0 0 55.5 Mercury 0 0 0 0 0 Molyb- denum 0 0 0 0 0 Nickel 56.6 56.6 56.6 56.6 97.7 Selenium 0 0 0 0 0 Zinc 1030 1030 1030 1030 1320 Total Phos- horus 40100 40100 40100 40100 40100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): u c� c� c� c� a L� o ,o ,2 w co ° > o' 0.2004 0.1831 0.1898 0.2038 0.1758 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 4E-06 3E-06 3E-06 4E-06 5E-06 0 0 0 0 0 0 0 2E-05 Chromiurr 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.3287 0.3002 0.3112 0.3342 0.5344 0 0 0 0 0 0 0 1.8087 Lead 0 0 0 0 0.0195 0 0 0 0 0 0 0 0.0195 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 denum (0 Nickel 0.0227 0.0207 0.0215 0.0231 0.0343 0 0 0 0 0 0 0 0.1223 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 0.4129 0.3771 0.3909 0.4198 0.464 0 0 0 0 0 0 0 2.0648 Total Phos- 16.075 14.682 15.218 16.343 14.097 0 0 0 0 0 0 0 76.416 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that -qualified personnel properly gathered and evaluated the inform r9n submitted. I am aw a that there are significant penalties for submitting false information, in u o5sibility of fi s nd imprisonment for knowing violations" 01 Signature of Land Appli Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 34.197336 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 19.14 Acres Permitted: 23.40 Site #: 2 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft M110*0 Total Phos- .. Annual Heavv Metal Field Loadings (Calculated in lbs/acre): 2 3 4 5 6 7 8 9 10 11 12 o CD d :: o' 0.4266 0.4721 0.4235 0.4643 1 0 0 0 1 0 0 0 0 Arsenic • 0 0 0 0 0 0 0 0 0 0 0 .0 0 Cadmium 8E-06 9E-06 8E-06 9E-06 0 0 0 0 0 0. 0 0 3E-05 Chromium 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.6997 0.7743 0.6945 0.7614 0 0 0 0 0 0 0 0 2.9299 Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0, 0 0 0. 0 0 0 denum Nickel 0.0483 1 0.0534 0.0479 0.0526 0 0 0 0 0 0 0 0 0.2022 Selenium 0 0 0 0 1 0 0 0 0- 0 0 0 0 0 Zinc 0.8789 0.9726 0.8724 0.9564 0 0 0 0 0 0 0 0' 3.6802 Total Phos- 34.216 37.864 33.964 37.235 0 0 0 0 0 0 0 0 143.28 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordan with a system designed assure that qualified personnel properly gathered and evaluated the inform i n submitted. I am aw that there are significant penalties for submitting false information, in i t e possibility of fins imprisonment imprisonment for knowing violations" Signature of Land Applier Date * See bottom of FSF For for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 85.4650674 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 16.80 Acres Permitted: 16.80 Site #: 3 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 1/14/14 2 1/14/14 3 1/14/14 4 J- 1/14/14 1/14/14 61 8/4/14 LZJ8 8/4/14 8/4/14 9 8/4/14 10 8/4/14 11 12 % Solids 1.7 1.7 1.7 1.7 1.7 1.3 1.3 1.3 1.3 1.3 Arsenic 0 0 0. 0 0 0 0 0 0 0 Cadmium 0.0092 0.0092 0.0092 0.0092 0.0092 0.014 0.014 0.014 0.014 0.014 Chromium 0 0 0 0 0 0 0 0 0 0 Copper 820 820 820 820 820 1520 1520 1520 1520 1520 Lead 0 0 0 0 0 55.5 55.5 55.5 55.5 55.5 Mercury 0 0 0 0 0 0 0 0. 0 0 Mol'yb- denum 0 0 0 0 0 0 0 0 0 0 Nickel 56.6 56.6 56.'6 56.6 56.6 97.7 97.7 97.7 97.7 97.7 Selenium 0 0 0 0 0 0 0 0 0 0 Zinc 1030 1030 1030 1030 1030 1320 1320 1320 1320 1320 Total Phos- horus 40100 40100 40100 40100 40100 40100 11 40100 40100 40100 40100 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): 0 1 2 3 L4j 5 6 7 L8j L2J10 Lj 1121 �y o ►�= o 0.278 1 0.5058 0.563 0.5594 1.0.5755 0.3664 0.5594 1 0.529 0.4575 0.6934 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 5E-06 9E-06 1E-05 1E-05 1E-05 1E-05 2E-05 1E-05 1E-05 2E-05 0 0 0.0001 Chromium 0 0 0 0 0 0 0 0 0 0 0 0 0 Copper 0.4559 0.8294 0.9232 0.9174 0.9438 1.1137 1.7005 1.6081 1.3908 2.108 0 0 11.991 Lead 0 0 0 0 0 0.0407 0.0621 0.0587 0.0508 0.077 1 0 0 0.2892 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.0315 0.0573 0.0637 0.0633 0.0651 0.0716 0.1093 0.1034 0.0894 0.1355 0 0 0.7901 Selenium 0 0 0 0 1 0 0 0 0 0. 0 0 0 0 Zinc 0.57271 1.0419 1.1597 1.1523 1.1854 0.9672 1.4768 1.3965 1.2078 1.8306 0 0 11.991 Total Phos- 22.296 40.562 45.149 44.862 46.152 29.382 44.862 42.425 36.692 55.612 0. 0 407.99 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infor ion submitted. I am re that there are significant penalties for submitting false information, inc di t e possibility of n and imp isonment for knowing violations" Signature of Land App ' r Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS -'Cherry Point WWTP Total Dry Tons Applied (Annual): 209.4645804 Permit .#: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 6.58 Acres Permitted: 8.00 Site #: 4 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . MEN11H ' 0 0�1'0 u iv .. os- . . Annual Heavv Metal Field Loadings (Calculated in lbs/acre): k y 1 2 3 4 L6j 7 1:11-Jil Loi i1j 1121 Y RL -0 c t7 cu y .. y o r 1.4839 11.502 4.0586 14.809 Arsenic 0 0 0 0 0 0 0 0 0 0 0 0 0 Cadmium 3E-05 0.0002 7E-05 0.0003 0 0 0 0 0 0 0 0 0.0006 Chromium 01 0 0 0 0 0 0 0 0 0 0 0 0 Copper 2.4335 18.863 6.6561 24.286 0 0 0 0 0 0 0 0 52.239 Lead 0 0 0 0 0 0 0 0 0 0 0 0 0 Mercury 0 0 0 0 0 0 0 0 0 0 0 0 0 Molyb- 0 0 0 0 0 0 0 0 0 0 0 0 0 denum Nickel 0.168 1.302 0.4594. 1.6764 0 0 0 0 0 0 0 0 3.6057 Selenium 0 0 0 0 0 0 0 0 0 0 0 0 0 Zinc 3.0567 23.693 8.3607 30.506 0 0 0 0 0 0 0 0 65.617 Total Phos- 119 922.43 325.5 1187.7 0 0 0 0 0 0 0 0 2554.6 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infor a ion submitted. I a ware that there are significant penalties for submitting false information, in d' g e possibility o fi es and imprisonment for knowing violations" . a � Signature of Land App ier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 24.00 Site #: 5 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 2 3 4 aF L.§J- 7 8 9 10 11 12 % Solids Arsenic Cadmium Chromium Copper Lead Mercury Molyb- denum Nickel Selenium Zinc Total Phos- phorus Annual Heavy Metal Field Loadings Calculated in lbs/acre : mill �0000000�000�0 •' 0000000000000 • 0�00��0000000 ... - 000�00000�000 �000000�000000 �0000000000000 �0000000000�00 ��0��000000�0� ®0000000000000 Total Phos- phorusEENEENEENEENE. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am awa hat there are significant penalties, for submitting false information, in 1 ' g e ossibility of fin d imprison ent for knowing violations" Signature of Land Applie Date * See bottom of FSF Form or helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 8.10 Site #: 6 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): OMEN 000,1NIMEN Total hM ..ENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): , Moulin in �000000�0�0000 �000000�00000� n 00�0000000000 ... - 0000�0000��00 �0000��000�000 �0000000000000 VIM 0000000000000 �0000000�00000 ®0000000000000 Total Phos- phorusEENEENEENEENE. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infor on submitted. I.am aware at there are significant penalties for submitting false information, incl di ossibility of fines imprisonment for knowing violations" /_f /.5 Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 35.00 Site #: 7 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . 0 Is 0 13 a MIN 'd TotalNon Phos- .. �� �� Annual Heaw Metal Field Loadings (Calculated in lbs/acre): '�00000��000000 ��00000�000000 • 0000�0000�000 ... - 00�000000000� �0���0�0000000 �00000�0000000 �000�000000�00 �0000000000000 ®���000�000000 Total Phos- phorusEEMENEEMENEEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the informat' submitted. I am aware at there are significant penalties for submitting false information, in _bility of fines impris ment for knowing violations" Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report . r Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual):. 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point' Acres Used: 0.00 Acres Permitted: 110.00 Site #: 8 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): .] 13 0 .. .. Annual Heaw Metal Field Loadings (Calculated in lbs/acre): t�tI ll"I oil I I �000�0�0000000 �0000000�0000� • 000�0�0000000 ... - 0000000000000 �0���000000000 ��00�000000000 �0�00�00000000' �00000000�00�0 ®�0000�000000� .. Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infor on submitted. I am aw that there are significant penalties for submitting false information, inc di g e possibility of fi s d impri onment for knowing violations" /S ignature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically, linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ00,01489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner_ : US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 28.00 Site #: 9 Field. #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Total hM ..ENEEMENEENE. Annual Heavy Metal Field Loadings (Calculated in lbs/acre): i131 3 a Ulu am �0��0000000000 ©000000000000 000�0000000�0 ... - 0�0000000��00 �0000000�00000 �000000�0000�0 �000�0000�00�0 ��0000000�0000 ®0000000000000 Total P o h' orus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified _personnel properly gathered and evaluated the info" a on submitted. I am aw re that there are significant penalties for submitting false information, i e ossibility of fi es and imprisonment for knowing violations" r� d Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: USMCAS - Cherry Point WWTP Total Dry Tons Applied (Annual): 0 Permit #: WQ0001489 Cation Exchange Capacity (non 503 only): Operator: Patricia T. Davis Owner: US Marine Corps - Cherry Point Acres Used: 0.00 Acres Permitted: 119.00 . Site #: 10 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): N9100000000 `uI nolinoinn RPM is ��o���■�� Total ..ENEEMENEENE. M Annual Heaw Metal Field Loadings (Calculated in lbs/acre): s ii� Q n ii� logo �0000000�00000 • : 000000�000000 0000000000000 ... - 0000000000000 �0�00000000000 �000�000000000 �00000�0000�00 �0000000000�0� ®00000�0000000 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the infornX§bn submitted. I am awar that there are significant penalties for submitting false information, i 1 d' g t e ossibility of fine a d imprison ent for knowing violations" oZ5% Signature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY.FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: Owner: US Marine Corps - Cherry Point Operator: Site #: 1 Field #: Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: 44.94 Acres Permitted: 44.94 o y o �s Q :: S eci Totals Per Acre % . Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 - PAN 2 Must Select Crop 1 or Crop p p 2 Gal. - Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 1/10/141 72000 1602.2 3.21 0.21447146 WWTP dry 0 S 0.5 0.2 85200 9780 0 8.56771 0 Fescue 1 1/20/14 72000 1602.2 2.8 0.187077909 WWTP dry 0 S 0.5 0.2 85200 9780 0 7.47339 0 Fescue 2 2/10/14 72000 1602.2 2.56 0.17104266. WWTP dry 0 S 0.5 0.2 85200 9780 0 6.83281 0 Fescue 3 2/17/14 72000 1602.2 2.37 0.158348087 WWTP dry 0 S 0.5 0.2 85200 9780 0 6.32569 0 Fescue 4 2/20/14 72000 1602.2 2.9 1 0.193759263 WWTP dry 0 S 0.5 0.2 85200 9780 0 7.7403 0 Fescue 5 2/24/14 72000 1602.2 2.45 0.16369317 WWTP dry 0 S 0.5 0.2 85200 9780 0 6.53921 0 Fescue 6 2/27/14 75000 1669 3.25 0.226191668 WWTP dry 0 S 0.5 0.2 85200 9780 0 9.0359 0 Fescue 7 5/22/14 72000 1602.2 3.07 0.205117565 WWTP dry 0 S 0.5 0.2 85200 9780 0 18.19404 0 Fescue 8 5/29/14 66000 1468.7 3.57 0.218647306 WWTP dry 0 S 0.5 0.2 85200 9780 0 8.73452 0 Fescue 9 6/5/14 72000 1602.2 3.14 0.209794512 WWTP dry 0 S 0.5 0.2 85200 9780 0 8.380871 0 Fescue 1 10 6/12/141 72000 1602.2 2.46 0.164361306 WWTP dry 0 S 0.5 0.2 85200 9780 0 6.56591 0 Fescue 11 6/19/14 72000 1602.2 2.84 0.189750451 WWTP dry 0 S 0.5 0.2 85200 9780 0 7.58015 0 Fescue 12 TOTALS: 19160 :::::::::::::::: As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied 77 Annuallbs/acre subtotal "Permitted P. L. R.*** 0 4.2E-05 0 3.7757 0 0 0 0.26062 0 4.74265 184.641 91.9705 0 36 34 N/A 1338 267 15 N/A 374 89 2498 250 Date lbs/ac Permit PAN Limit 1st/2 n d Cro p "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system desig to assure that qualifie ersonnel properly gathered and evaluated the information submitted. I am aware that there are s' f a en#lties for sub t ng false information, including the ossibility of fines and imprisonment for knowing violations." e;7S *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature f Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point Operator: Site #: Field #: Permit #: WQ0001489 Patricia T. Davis Acres Utilized: 44.94 Annual Dry Tons Applied:: 146.273175 Cation Exchange Capacity (non 503): Acres Permitted:': 44.94 o y , o QAcre S eci Totals Per % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate* * Miner" ali- nation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN I PAN 2 Must Select Crop 1 or Crop 2 * Gal. - Cu.Yd. Report Totals ] inGal. Crop 1 Crop 2 6/26/14 72000 1602.2 3 0.200440617 WWTP dry 0 S 0.5 0.2 85200 9780 0 8.0072 0 Fescue 13 7/9/14 72000 1602.2 2.74 0.183069097 WWTP dry 0. S 0.5 0.2 85200 9780 0 7.31324 0 Fescue 14 7/17/14 72000 1602.2 2.84 0.189750451 WWTP dry 0 S 0.5 0.2 85200 9780 0 7.58015 0 Fescue 15 7/24/14 72000 1602.2 3.05 0.203781294 WWTP dry 0 S 0.5 0.2 85200 9780 0 8.14066 0 Fescue 16 7/31/14 66000 1468.7 2.87 0.175775285 WWTP dry 0 S 0.5 0.2 85100 6930 0 16.71426 0 Fescue 1 17 0 0 S 0.5 0.2 0 0 0 18 0 0 S 0.5 0.2 0 .0 0 19 0 0 S 0.5 0.2 0 0 0 20 0 0 S 0.5 0.2 0 0 0 21 0 0 S 0.5 0.2 0 1 0 0 1 22 0 0 S 0.5 0.2 0 0 0 23 0 0 S 0.5 -0.2 0 0 0 24 TOTALS: 7878 :: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 I PAN 2 Lime Applied Annuallbs/acre subtotal 0 1.9E-05 0 1.8087 10.01951 0 0 0.12231 0 2.06475 76.4159 37.75551 0 Date lbs/ac Current Cumulative lbs/ac 0.586338995 2.85571 0 62.382 4.75179 0.240711 0 6.68843 0.67 77.7034:::::::::::::::::::::::::::::::::::::: 0.586338995 2.85565 0 56.7976 4.73228 0.24071 0 6.30551 0.67 70.896 36 34 N/A 1338 . 267 15 1 N/A 374 89 2498 250 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** r o Permit PA N Limit 1st/ 2nd Cop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designe to assure that qualified ersonnel properly gathered and evaluated the information submitted. I am aware that there are sig i c n penalties fo4Land g false i formation, including the ossibility of fines and imprisonment for knowing violations." + ice *Application Method: S - Surface, IN - Injection, INC - Incorporation ,17 Signatureplier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A"'IN A•BLANK OR BOX WHEN NOT APPLICABLE. Facility. Name: US Marine Corps` -Cherry Point Permit;#: 'WQ0001489 - Annual Dry Tons Applied: 34.20 Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503): Site #: 2 Field #: Acres Utilizeds ` 19.14 = Acres Permitted: 23.40 o A 4) � � o Q S eci Totals Per Acre oInches /o Solid s Dry Tons Per Acre Residual Sources (Summarize) ite Cond. Dr y' Wets Precip. Past 24 Hrs. Appli- cation Meth- od* Vola= tili- zation Rate** Miner- ali- zation Rate - TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 Gal. Cu.Yd. : Report Totals in Gal. Crop 1 Crop 2 4/23/14 72000 3761.4 2.72 0.426628774 WWTP dry 0 S 0.5 0.2 85200 9780 0 17.043 0 Fescue 1 4/28/14 72000 3761.4 3.01 0.472114931 WWTP dry 0 S 0.5 0.2 85200 9780 0 18.86 0 Fescue 2 5/2/14 72000 3761.4 2.7 0.423491798 WWTP dry 0 S 0.5 , 0.2 85200 . 9780 0 16.9177 0 Fescue 3 5/9/14 72000 3761.4 2.96 0.46427249 WWTP dry 0 S 0.5 0.2 85200 9780 0 18.5468 0 - Fescue 4 0 S 0.5 0.2 0 0 0 5 0 S 0.5 0.2 0 0 0 6 0 0 S 0.5 0.2 0 0 0 7 0 0 S 0.5 0.2 0 0 0 8 0 0 S 0.5 0.2- 0 0 0 9 0 0 S 0.5 0.2 0 0 0 10 0 0 S 0.5 0.2 0 0 0 11 0 6 0 S 0.5 0.2 0 0 0 12 TOTALS: :::::::::::::::: As Cd Cr Cu Pb H Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annual lbs/acre 0 3.3E-05 0 2.92987 0 0 0 .0.20223 0 ' 3.68021 143.278 71.3674 0 Date lbs/ac Current Cumulative lbs/ac 0.963097176 5.0406 0 94.0027 19.9907 0.29352 0 9.62431 0.54 124.073:::::::::::::::::::::::::::::::::::::::::::::::::::':: 0.963097176 1 5.04057 0 91.0728 19.9907 0.29352 0 9.42208 0.54 120.393:::::::::::::::::: 36 34 N/A 1338 267 15 N/A 374 89 249.8 ................ 250 Prior Years Cumulative,lbs/ac Permitted C. P. L. R.*** Permit PAN L' tmtt 1st/2 nd Cro P «t L_ ,_ JL Cenuy, under penalty of law, rnar finis aocument was prepared under mydirection or supervision in accordance with a system designe,glo assure that qualified ersonnel properly gathered and evaluated the information submitted. I am aware that there are Sig ► c t altkes for subm' 1 g false in ormation, including th possibility of fines and imprisonment for knowing violations." �� ✓ *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of and Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incornoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point Operator: Site #: Field #: Permit #: WQ0001489 Annual Dry Tons Applied: 85.47 Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: 16.80 Acres Permitted: 16.80 o y a Q :: s eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo ma- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop P P 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 3/10/14 66000 3928.6 1.697 0.278004964 WWTP dry 0 S 0.5 0.2 85200 9780 0 11.1057 0 Fescue 1 3/21/14 72000 4285.7 2.83 0.505761429 WWTP dry 0 S 0.5 0.2 85200 9780 0 20.2042 0 Fescue 2 3/27/14 72000 4285.7 3.15 0.56295 WWTP dry 0 S 0.5 0.2 85200 9780 0 22.4887 0 Fescue 3 4/2/14 72000 4285.7 3.13 0.559375714 WWTP 'dry 0 S 0.5 0.2 85200 9780 0 22.3459 0 Fescue 4 4/11/141 72000 4285.71 3.22 0.57546 WWTP dry 0 S 0.5 0.2 85200 9780 0 122.9885 0 Fescue 5 8/14/14 60000 3571.4 2.46 0.366364286 WWTP dry 0 S 0.5 0.2' 85100 6930 0 13.9944 0 Fescue 6 10/6/14 72000 4285.7 3.13 0.559375714 WWTP dry 1 S 0.5 0.2 85100 6930 0 21.367 0 Fescue 7 10/10/14 72000 4285.7 2.96 0.528994286 WWTP dry 2 S 0.5 0.2 85100 6930 0 20.2065 0 Fescue 8 10/20/14 72000 4285.7 2.56 0.457508571 WWTP dry 3 S 0.5 0.2 85100 6930 0 17.4759 0 Fescue 9 11/3/141 72000 4285.7 3.88 0.693411429 WWTP dry 4 S 0.5 0.2 85100 6930 1 0 26.4869 0 Fescue 10 0 - 0 S 0.5 0.2 0 0 0 11 0 0 S 0.5 0.2 0 0 0 12 TOTALS: 41786 ::::: "': As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0.00012 0 11.9909 0.28923 0 0 0.79006 0 11.9909 407.994 198.664 0 Date lbs/ac Current Cumulative lbs/ac 9988 0.324356487 3.62287 0 70.3869 5.14025 0.23312 0.223 8.38232 0.35_ ::::::::::::::::::::::::::::::::::::::: 0.324356487 3.62299 0 82.3778 5.42948 0.23312 0.223 9.17238 0.35 98n2498 36 34 N/A 1338 267 15 N/A 374 89 25 0 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Perms t PAN Limit 1st/2 n d Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designe o assure that qualified ersonnel properly gathered and evaluated the information submitted. I am aware that there are si ni c t enalties for sub ' ti false information, including the possibility of fines and imprisonment for knowing violations." /3 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into .the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point. Permit #: WQ0001489 Annual Dry Tons Applied: Owner: US Marine Corps - Cherry Point Operator: Site #: 4 Field #: Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: 6.58 209.46 Acres Permitted: 8.00 o Q specifv Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) site Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- . tili- zation Rate** Miner- ali- zation Rate TKN Ammo ma- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. CuNd. Report _ inoGal. Crop 1 Crop 2 2/28/14 72000 10949 3.25 1.483850365 WWTP dry 0 S 0.5 0.2 85200 9780 0 59.2769 0 Fescue 1 3/19/14 59196.7 9001.9 30.64 11.50165955 WWTP dry 0 S 0.5 0.2 85200 9780 0 459.468 0 Fescue 2 3/28/14 59196.7 9001.9 10.81 4.058614331 WWTP dry 0 S 0.5 0.2 85200 9780 0 162.134 0 Fescue 3 3/31/14 59196.7 '9001.9 39.45 14.80876206 WWTP dry 0 S 0.5 0.2 85200 9780 0 591.58 0 Fescue 4 0- 0 S 0.5 0.2 0 1 0 0 .5 0 0 S 0.5 0.2 0 0 0 6 0 0 S 0.5 0.2 0 0 0 1 7 0 0 S 0.5 0.2 0 0 0 8 0 0 S 0.5 0.2 0 0 0 9 0 0 S 0.5 0.2 0 0 0' 10 0 0 S 0.5 0.2 0 0 0 11 0 0 S 0.5 0.2 0 0 0 12 TOTALS: 37955 ._-..::::.:., As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0.00059 0 52,2387 0 0 0 3.60575 0 165.6169 2554.6 1272.46 ." 0 Date lbs/ac Current Cumulative lbs/ac 0.339889659 3.31906 0 114.252 4.95525 0.21454 0.223 11.4927 0.35 142.105 0.339889659 3.31847 0 62.0129 4.95525 0.21454 0.223 7.88694 0.35 76.4878:::::::::::::::::::::::::::::::::::: 36 34 N/A 1338 267 15 N/A 374 89 2498 250 Prior Years Cumulative lbs/ac . Permitted C. P. L. R.*** 2 r Permit PAN Limit 1st/ nd C o P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designe to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are s'gn' is n penalties for sub ' i g false infor ation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature and Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point Operator: Site #: 5 Field #: Permit #: WQ0001489 Annual Dry Tons Applied: 0.00 Patricia T. Davis Acres Utilized: 0.00 Cation Exchange Capacity (non 503): Acres Permitted: 24.00 o o Q Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources - (Summarize) site Cond. Dry, Wet, Moist Inches Precip. Past 24 Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 * -Specify Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 0 0 Fescue 1 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 0 0 Fescue 2 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 0 0 Fescue 3 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 0 0 Fescue 4 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 1 0 0 Fescue 5 0 0 WWTP dry 0 S 0.5 0.2 85200 9780 0 0 0, Fescue 6 0 0 S 0.5 0.2 85200 9780 0 0 0 1 7 0 0 S 0.5 0.2 85200 9780 0 0 0 8 0 0 S 0.5 0.2 85200 1 9780 0 0 0 9 0 0 S 0.5 0.2 85200 9780 0 1 0 0 10 0 0 S 0.5 0.2 85200 9780 0 0 0 111 0 0 S 0:5 0.2 85200 9780 0 0 0 12 TOTALS: 0 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0 0 0 0 0 0 0 0 0 1 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0.583796014 2.84326 0 53.8666 2.86497 0.22851 0.18 7.20884 0.33. 61.7303:::::::::::::::::::::::::::::::::::::::::: 0.583796014 2.84326 0 53.8666 2.86497 0.22851 0.18 7.20884 0.33 61.7303 36 34 N/A 1 1338 1 267 15 1 N/A 374 89 2498 2 50 Prior Years Cumulative lbs/ac Permitted C. P. L..R.*** i 1 't PAN Lim t stl2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designe assure that qualified perso I properly gathered and evaluated the information submitted. I am aware that there are signaaltie ' ns for submitting is nformation including the'possib'lity of fines and imprisonment for knowing violations." G�J T *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, In i ection/Incori)o ration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point Operator: Site #: 6 Field #: Permit #: WQ0001489 Patricia T. Davis Acres Utilized: 0.00 Annual Dry Tons Applied: 0.00 Cation Exchange Capacity (non 503): Acres Permitted: 8.10 o �, o Q S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1te Cond. Dry, Wet Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo ma- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. CuNd. Report in Gal. Crop 1 Crop 2 0 0 WWTP S 0.5 0.2 85200 9780 0 0 0 Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 0 ::........ As Cd Cr Cu Pb _ Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 36 34 N/A 1338 267 15 1 N/A 374 1 89 2498 250 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Perm P........................................ Permit AN Limit 1 s t/2nd Cro P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system desig o assure that qualifl personnel properly gathered and evaluated the information submitted. I am aware that there are s' 6ic n Ities for sub i ing false information, including the possibility of fines and imprisonment for knowing violations." s �J� *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into .the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE. MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point Site #: 7 Field #: Permit #: WQ0001489 Annual Dry Tons Applied: 0.00 Operator: Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: am Acres Permitted: 35.00 o y N _ o A s eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN I -PAN 2 Must Select Crop I or Crop p p 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 0 0 S 0.5 0.2 85200 9780 0 0 0 Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 .0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 1 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 0 ::::::::: As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 1 0 0 0 1 0 0 .0 1 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0.53048 2.84476 0 41.6074 2.73256 0.24012 0 7.43444 0.3 60.9268::::::::::::::::::: 0.53048 2.84476 0 41.6074 2.73256 0.24012 0 7.43444 , 0.3 60.9268 ::::::::::::::::::::::::.................... ::: 36 34 N/A 1338 267 15 N/A 374 89 2498 250 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Perm i it PAN Limit 1 sb2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system design to assure that qualifi personnel properly gathered and evaluated the information submitted. I am aware that there are si ' is n penalties for sub i ting false information, including the possibility of fines and imprisonment for knowing violations." ZL. *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature Uland Applier . Date **Volatilization Rate: Surface - 0.5, Iniection/Incorvoration -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into -the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Owner: US Marine Corps - Cherry Point _ Operator: Site #: 8 Field #: Permit #: WQ0001489 Annual Dry Tons Applied: 0.00 Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: 0.00 Acres Permitted: 110.00 o � y o Totals Per Atalscre % Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop p p 2 * -Specify Gal. Cu.Yd._ = Report in Gal. Crop 1 Crop 2 0 0 WWTP S 0.5 0.2 85200 9780 0 0 0 Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS:. 0 :::: `:' As Cd Cr Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0 0 0 0 1 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 0 0 0" 0 0 0 0 1 0 1 0 0 0 0 0 0 0 0 0 0 0 36 34 N/A 1338 267 15 N/A 374 89 2498 250 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** e it PAN Limit 1 st/2nd Cro Prrri P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system design o assure that qualified nnel properly gathered and evaluated the information submitted. I am aware that there are si i c nt enalties for submit ng alse information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S -Surface, IN -Injection, INC -Incorporation Signature of tand Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incomoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate . * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into -the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. lie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003).. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A.COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: Owner: US Marine Corps - Cherry Point Operator: Site #: 9 Field #: Patricia T. Davis Cation Exchange Capacity (non 503): Acres Utilized: - 0.00 ME Acres Permitted: 28.00 o Y o A Specify Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) t e Cond. Dry, Wet, Moist Inches . PrecipPast 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 Crop p or p 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 0 0 WWTP S 0.5 0.2 85200 9780 0 0 0 Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0' 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 0 :<: As Cd Cr Cu Pb H Mo N1 Se Zn P PAN 1 PAN 2 Lime Ap lied Annuallbs/acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 0 0 0 0 0 1 0 1 0 0 1 0 o 0 0 0 0 0 0 0 0 0 36 34 N/A 1338 267 15 N/A 374 89 1 2498 25 0 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** PermitPAN Limit is t/2nd Cro p "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system desigM to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are si 'ti nt enalties for subm' g false infor ation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of -Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are. mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: US Marine Corps - Cherry Point Permit #: WQ0001489 Annual Dry Tons Applied: 0.00 Owner: US Marine Corps - Cherry Point Operator: Patricia T. Davis Cation Exchange Capacity (non 503): Site#: 10 Field #: Acres Utilized: 0.00 Acres Permitted: 119.00 o y y o Q S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1te Cond. Dry, Wet Moist Inches Precip. Past 24 Hrs. - Appli- cation Meth- od* Vola- tili- zation Rate* * Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1. 'PAN 2 Must Select Crop 1 or Crop 2 Gal. CuNd. >: Report Totals in Gal. Crop 1 Crop 2 0 0 WWTP S 0.5 0.2 85200 9780 0 0 0. Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0. 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 '12 TOTALS: 0 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs%acre 0 0 0 0 0 0 0 0 0 0 0 0 0 Date lbs/ac Current Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 36 34 N/A 1338 267 15 N/A 374 89 2498 =: 250 Prior Years Cumulative lbs/ac Permitted C. P. L. R. i Permit it PAN Limit 1 s t/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system design to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are sign' is nt enalties for submitt' g alse information, including the possibility of fines and imprisonment for knowing violations." �-S *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature o and Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. DENR FORM FSF (5/2003) LABORATORY REPORT (3 COPIES) 1) RESIDUALS LABORATORY DRY WEIGHT TEST 2)TOXICITY CHARACTERISTIC LEACHING PROCEDURE acmnalytical www.pacelabs.com Pace Analytical Services, Inc., 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TCLP SLUDGE Pace Project No.: 92186447 Sample: MCAS 001 SLUDGE Lab ID: 92186447001 Collected: 01/14/14 12:30 Received: 01115/14 10:00 Matrix: Solid Results reported on a "dry -weight"' basis Parameters Results Units ReportLimit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 gamma-BHC (Lindane) ND ug/L 0.50 1 01/21/14 10:40 01/23/14 15:13 58-89-9 Chlordane (Technical) ND ug/L 3.0 1 01/21/14 10:40 01/23/14 15:13 57-74-9 Endrin ND ug/L 0.50 1 01/21/14 10:40 01/23/14 15:13 72-20-8 Heptachlor epoxide ND ug/L 0.50 1 01/21/14 10:40 01/23/1415:13 1024-57-3 Methoxychlor ND ug/L 1000 1 01/21/14 10:40 01/23/14 15:13 72-43-5 Toxaphene ND ug/L 3.0 1 01/21/14 10:40 01/23/14 15:13 8001-35-2 . Surrogates Decachlorobiphenyl (S) 74 % 10-138 1 01/21/14 10:40 01/23/14 15:13 2051-24-3 Tetrachloro-m-xylene (S) 56 % 10-110 1 01/21/14 10:40 01/23/14 15:13 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-D ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 94-75-7 2,4,5-TP (Silvex) ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 93-72-1 Surrogates 2,4-DCAA (S) 95 % 70-130 1 01/22/14 08:05 01/23/14 01:33 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 01/16/14 15:45 Arsenic ND mg/L 0.050 1 01/17/1412:55 01/21/1417:51 7440-38-2 Barium ND mg/L 0.25 1 01/17/1412:55 01/21/1417:51 7440-39-3 Cadmium 0.0092 mg/L 0.0050 1 01/17/1412:55 01/21/1417:51 7440-43-9 Chromium ND mg/L 0.025 1 01/17/1412:55 01/21/1417:51 7440-47-3 Lead ND mg/L 0.025 1 01/17/1412:55 01/21/14 17:51 7439-92-1 Selenium ND mg/L 0.10 1 01/17/1412:55 01/21/1417:51 7782-49-2 Silver ND mg/L 0.025 1 01/17/1412:55 01/21/1417:51 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/16/14 15:45 Mercury ND ug/L 0.20 1 01/17/14 13*35 01/17/14 20:15 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 1,4-Dichlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 106-46-7 2,4-Dinitrotoluene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 121-14-2 Hexachloro-1,3-butadiene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 87-68-3 Hexachlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 118-74-1 Hexachloroethane ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-48-7 3&4-Methyl phenoI(m&p Cresol) 128 ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 Nitrobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 98-95-3 Pentachlorophenol ND ug/L 100 1 01/21/14 09:40 01/22/14 17:25 87-86-5 Pyridine ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 110-86-1 2,4,5-Trichlorophenol ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-95-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 T. accAnalytical www.pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TCLP SLUDGE Pace Project No.: 92186447 Sample: MCAS 001 SLUDGE Lab ID: 92186447001 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 88-06-2 51 % 12-102 1 01/21/14 09:40 01/22/14 17:25 4165-60-0 51 % 13-107 1 01/21/14 09:40 01/22/14 17:25 321-60-8 82 % 21-132 1 01/21/14 09:40 01/22/14 17:25 1718-51-0 28 % 10-110 1 61/21/14 09:40 01/22/14 17:25 13127-88-3 33 % 10-110 1 01/21/14 09:40 01/22/14 17:25 367-12-4 70 % 27-108 1 01/21/14 09:40 01/22/14 17:25 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 20 01/17/1413:36 71-43-2 ND ug/L 200 20 01/17/1413:36 78-93-3 ND ug/L 100 20 01/1711413:36 56-23-5 ND ug/L 100 20 01/17/1413:36 108-90-7 ND ug/L 100 20 01/17/1413:36 67-66-3 ND ug/L 100 20 01/17/1413:36 106-46-7 ND ug/L 100 20 01/17/1413:36 107-06-2 ND ug/L 100 20 01/17/1413:36 75-35-4 ND ug/L 100 20 01/17/1413:36 127-18-4 ND ug/L 100 20 01/1711413:36 79-01-6 ND ug/L 100 20 01/17/1413:36 75-01-4 109 % 70-130 20 01/17/1413:36 17060-07-0 97 % 67-135 20 01/17/14 13:36 2037-26-5 98 % 70-130 20 01/1711413:36 460-00-4 Analytical Method: ASTM D2974-87 98.3 % 0.10 1 01/24/1412:13 Sample: MCAS 001 SLUDGE Lab ID: 92186447002 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 21500 mg/kg 539 1 01/16/14 10:55 01/16/1419:58 7429-90-5 Arsenic ND mg/kg 53.9 1 01/16/14 10:55 01/16/1419:58 7440-38-2 Cadmium 6.9 mg/kg 5.4 1 01/16/14 10:55 01/16/1419:58 7440-43-9 Calcium 20600 mg/kg 539 1 01/1611410:55 01/16/14 19:58 7440-70-2 Copper 820 mg/kg 27.0 1 01/16/14 10:55 01/16/1419:58 7440-50-8 Lead ND mg/kg 27.0 1 01/16/14 10:55 01/16/1419:58 7439-92-1 Magnesium 3200 mg/kg 539 1 01/16/14 10:55 01/16/1419:58 7439-95-4 Molybdenum ND mg/kg 27.0 1 01/16/14 10:55 01/16/1419:58 7439-98-7 Nickel 56.6 mg/kg 27.0 1 01116/1410:55 01/16/1419:58 7440-02-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 aceAi?aly�ical www.paaela�s.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TCLP SLUDGE Pace Project No.: 92186447 Sample: MCAS 001 SLUDGE Lab ID: 92186447002 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Potassium ND mg/kg 27000 1 01/16/1410:55 01/16/1419:58 7440-09-7 Selenium ND mg/kg 53.9 1 '01116/1410:55 01/16/14 19:58 7782-49-2 Sodium ND mg/kg 27000 1 01/16/1410:55 01/1611419:58 7440-23-5 Zinc 1030 mg/kg 53.9 1 01/16/1410:55 01/16/1419:58 7440-66-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.55 mg/kg 0.23 1 01/17/14 12:25 01/1711418:28 7439-97-6 Percent Moisture Analytical Method:ASTM D2974-87 Percent Moisture 98.3 % 0.10 1 01/17/14 09:30 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 1.7 % 0.000010 1 01/16/14 13:13 9045 pH Soil Analytical Method: EPA9045 pH at 25 Degrees C 7.1 Std. Units 0.10 1 01/21/14 15:45 Plant Available Nitrogen Analytical Method: 40CFR PART 432.2 Plant Available Nitrogen 27600 mg/kg 1.0 1 01/30/14 12:19 350.1 Ammonia Analytical Method: EPA350.1 Nitrogen, Ammonia - 9780 mg/kg 604 1 01/21/14 04:44 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA351.2 Nitrogen, Kjeldahl, Total 85200 mg/kg 9750 5 01/28/14 13:45 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrate ND mg/kg 120 1 01/29/14 22:54 Nitrogen, Nitrite ND mg/kg 60.2 1 01/29/14 22,54 Nitrogen, NO2 plus NO3 ND mg/kg 120 1 01/29/14 22:54 365.1 Phosphorus, Total .. Analytical Method: EPA 365.1 Phosphorus 40100 mg/kg 1290 10 01/24/14 16:05 7723-14-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. N2 ItLTA Page 6 of 27 acEAnalytical mmpacelebsxom c ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8681 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 08/18/14 15:15 gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Aluminum Arsenic Cadmium Calcium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury Date: 08/20/2014 05:06 PM ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 58-89-9. ND ug/L 30.0 10 08/19/1410:01 08/20/1410:25 57-74-9 ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 72-20-8 ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 1024-57-3 ND ug/L 10000 10 08/1911410:01 08/20/1410:25 72-43-5 ND ug/L 30.0 10 08/19/1410:01 08/20/1410:25 8001-35-2 . 0 % 10-138 10 08/19/1410:01 08/20/1410:25 2051-24-3 D3,S4 0 % 10-110 10 08/19/1410:01 08/20/14 10:25 877-09-8 Analytical Method: EPA 8151 Preparation Method: EPA 3510 ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 94-75-7 ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 93-72-1 86 % 42-142 1 08/13/14 08:05 08/14/14 05:38 19719-28-9 Analytical Method: EPA 6010 Preparation Method: EPA 3050 25200 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7429-90-5 67.6 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-38-2 14.0 mg/kg 6.5 1 08/07/14 17:20 08/08/14 03:29 7440-43-9 31800 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7440-70-2 1520 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7440-50-8 55.5 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-92-1 3480 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7439-95-4 ND mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-98-7 97.7 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7440-02-0 ND mg/kg 32700 1 08/07/14 17:20 08/08/14 03:29 7440-09-7 ND mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7782-49-2 ND mg/kg 32700 1 '08/07/14 17:20 08/08/14 03:29 7440-23=5 1320 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-66-6 Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 08/07/14 20:00 ND mg/L 0.050 1 08/08/14 14:30 08/09/14 00:29 7440-38-2 0.53 mg/L 0.25 1 08/08/14 14:30 08/09/14 00:29 7440-39-3 0.014 mg/L 0.0050 1 08/08/14 14:30 08/09/14 00:29 7440-43-9 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-47-,3 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7439-92-1 ND mg/L 0.10 1 08/08/14 14:30 08/00/14 00:29 7782-49-2 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-22-4 Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 08/07/14 20:00 ND ug/L 0.20 1 08/08/1415:05 08/12/1415:26 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 28 acicAnalytical wmpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.79 mg/kg 0.28 1 08/08/14 17:20 08/12/14 13:53 7439-97=6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 08/18/14 15:15 1,4-Dichlorobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 106-46-7 2,4-Dinitrotoluene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 121-14-2 Hexachloro-1,3-butadiene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 87-68-3 Hexachlorobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 118-74-1 Hexachloroethane ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 Nitrobenzene ND ug/L 500 10 08/19/14 10:01 .08/20/14 11:56 98-95-3 Pentachlorophenol ND ug/L 1000 10 08/19/14 10:01 08/20/14 11:56 87-86-5 Pyridine ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 110-86-1 2,4,5-Trichlorophenol ND ug/L 500 10 08/19/14 10:01 08120/1411:56 95-95-4 2,4,6-Trichlorophenol ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 12-102 10 08/19/14 10:01 08/20/14 11:56 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 13-107 10 08/19/14 10:01 08/20/14 11:56 321-60-8 Terphenyl-d14 (S) 0 % 21-132 10 08/19/14 10:01 08/20/14 11:56 1718-51-0 Phenol-d6 (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 13127-88-3 2-Fluorophenol (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 367-12-4 2,4,6-Tribromophenol (S) 0 % 27-108 10 08/19/14 10:01 08/20/14 11:56 118-79-6 8260 MSV TCLP Analytical Method: EPA8260 Leachate Method/Date: EPA 1311; 08/14/14 11:03 Benzene ND ug/L 5.0 1 08/18/14 14:30 71-43-2 2-Butanone (MEK) 12.3 ug/L 10.0 1 08/18/14 14:30 78-93-3 Carbon tetrachloride ND ug/L 5.0 1 08/18/14 14:30 56-23-5 Chlorobenzene ND ug/L 5.0 1 08/18/14 14:30 108-90-7 Chloroform ND ug/L 5.0 1 08/18/14 14:30 67-66-3 1,4-Dichlorobenzene ND ug/L 5.0 1 08/18/14 14:30 106-46-7 1,2-Dichloroethane ND ug/L 5.0 1 08/18/14 14:30 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1 08/18/14 14:30 75-35-4 Tetrachloroethene ND ug/L 5.0 1 08/18/14 14:30 127-18-4 Trichloroethene ND ug/L 5.0 1 08/18/14 14:30 79-01-6 Vinyl chloride ND ug/L 5.0 1 08/18/14 14:30 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 08/18/14 14:30 17060-07-0 Toluene-d8 (S) 101 % 67-135 1 08/18/14 14:30 2037-26-5 4-Bromofluorobenzene (S) 107 % 70-130 1 08/18/14 14:30 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.7 % 0.10 1 08/07/14 15:12 Date: 08/20/2014 05:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 28 /- �-;aca Analytical / wvnvpacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1010 Flash point, Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 08/19/14 03:00 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 1.3 % 0.000010 1 08/07/14 09:36 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.2 Std. Units 0.10 1 08/07/14 13:56 Plant Available Nitrogen Analytical Method: 40CFR PART 432.2 Plant Available Nitrogen 26900 mg/kg 1.0 1 08/18/14 11:30 N2 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 6930 mg/kg 773 1 08/07/14 17:16 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 85100 mg/kg 7020 5 08/13/14 15:40 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrate ND mg/kg 154 1 08/15/14 22:38 Nitrogen, Nitrite ND mg/kg 77.1 1 08/15/14 22:38 Nitrogen, NO2 plus NO3 ND mg/kg 154 1 08/15/14 22:38 733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/L 0.010 1 08/18/14 19:24 734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/L 1.0 1 08/15/14 15:00 Date: 08/20/2014 05:06 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 28 ,�;aceAnalyticaI ..pacelabsxom Project: TCLP SLUDGE Pace Project No.: 92186447 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 '1 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: E218644'001 Collected: 01/14/14 12:30 Received: 01/15l14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 gamma-BHC (Lindane) ND ug/L 0.50 1 01/21/14 10:40 01/23/14 15:13 58-89-9 Chlordane (Technical) ND ug/L 3.0 1 01/21/14 10:40 01/23/14 15:13 57-74-9 Endrin ND ug/L 0.50 1 01/21/14 10:40 01/23/14 15:13 72-20-8 Heptachlor epoxide ND ug/L 0.50 1 01/21/14 10:40 01/23/14 15:13 1024-57-3 Methoxychlor ND ug/L 1000 1 01121/1410:40 01/23/14 15:13 72-43-5 Toxaphene ND ug/L 3.0 1 01/21/14 10:40 01/23/14 15:13 8001-35-2 Surrogates Decachiorobiphenyl (S) 74 % 10-138 1 01/21/14 10:40 01/23/14 15:13 2051-24-3 Tetrachloro-m-xylene (S) 56 % 10-110 1 01/21/14 10:40 01/23/14 15:13 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA8151 Preparation Method: EPA 3510 2,4-D ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 94-75-7 2,4,5-TP (Silvex) ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 93-72-1 Surrogates 2,4-DCAA (S) 95 % 70-130 , 1 01/22/14 08:05 01/23/14 01:33 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 01/16/14 15:45 Arsenic ND mg/L 0.050 1 01/17/1412:55 01/21/14 17:51 7440-38-2 Barium ND mg/L 0.25 1 01/17/1412:55 01/21/14 17:51 7440-39-3 Cadmium 0.0092 mg/L 0.0050 1 01/17/1412:55 01/21/14 17:51 7440-43-9 Chromium ND mg/L 0.025 1 01/17/1412:55 01/21/14 17:51 7440-47-3 . Lead ND mg/L 0.025 1 01/17/14 12:55 01/21/14 17:51 7439-92-1 Selenium ND mg/L 0.10 1 01/1711412:55 01/21/14 17:51 7782-49-2 Silver ND mg/L 0.025 1 01/17/1412:55 01/21/14 17:51 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/16/14 15:45 Mercury ND ug/L 0.20 1 01/17/14 13:35 01/17/14 20:15 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 - Leachate Method/Date: EPA 1311; 01/16/14 14:00 1,4-Dichlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 106-46-7 2,4-Dinitrotoluene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 121-14-2 Hexachloro-1,3-butadiene ND ug/L 50.0 1 01/21/14.09:40 01/22/14 17:25 87-68-3 Hexachlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 118-74-1 Hexachloroethane ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-48-7 3&4-Methyl phenol (m&p Cresol) 128 ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 Nitrobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 98-95-3 Pentachlorophenol ND ug/L 100 1 01/21/14 09:40 01/22/14 17:25 87-86-5 Pyridine ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 110-86-1 2,4,5-Trichlorophenol ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-95-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 �aceAnalytical wwwpacelabs.com i Project: TCLP SLUDGE Pace Project No.: 92186447 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE LabID: 92186447001 Collected: 01/14/14 12:30 Received: 01/ 15/ 14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared, Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzenb 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Analytical Method,: EPA8270 Preparation Method: EPA3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 88-06-2 51 % 12-102 1 01/21/14 09:40 01/22/14 17:25 4165-60-0 51 % 13-107 1 01/21/14 09:40 01/22/14 17:25 321-60-8 82 % 21-132 1 01/21/14 09:40 01/22/14 17:25 1718-51-0 28 % 10-110 1 01/21/14 09:40 01/22/14 17:25 13127-88-3 33 % 10-110 1 01/21/14 09:40 01/22/14 17:25 367-12-4 70 % 27-108 1 01/21/14 09:40 01/22/14 17:25 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 20 01/17/1413:36 71-43-2 ND ug/L 200 20 01/17/1413:36 78-93-3 ND ug/L 100 20 01/17/1413:36 56-23-5 ND ug/L 100 20 01/17/1413:36 108-90-7 ND ug/L 100 20 01/17/1413:36 67-66-3 ND ug/L 100 20 01/17/1413:36 106-46-7 ND ug/L 100 20 01/17/1413:36 107-06-2 ND ug/L 100 20 01/17/1413:36 75-35-4 ND ug/L 100 20 01/17/1413:36 127-18-4 ND ug/L 100 20 01/17/1413:36 79-01-6 ND ug/L 100 20 01/17/1413:36 75-01-4 109 % 70-130 20 01/17/1413:36 17060-07-0 97 % 67-135 20 01/17/14 13:36 2037-26-5 98 % 70-130 20 01/17/1413:36 460-00-4 Analytical Method: ASTM D2974-87 98.3 % - 0.10 1 01/24/14 12:13 Sample: MCAS 001 SLUDGE Lab.]D: 92186447002 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 21500 mg/kg 539 1 01/16/1410:55 01116/1419:58 7429-90-5 Arsenic ND mg/kg 53.9 1 01/16/1410:55 01/1611419:58 7440-38-2 Cadmium 6.9 mg/kg 5.4 1 01/16/1410:55 01/16/1419:58 7440-43-9 Calcium 20600 mg/kg 539 1 01/1611410:55 01/16/1419:58 7440-70-2 Copper 820 mg/kg 27.0 1 01/16/1410:55 01/16/1419:58 7440-50-8 Lead ND mg/kg 27.0 1 01/16/1410:55 01/16/1419:58 7439-92-1 Magnesium 3200 mg/kg 539 1 01/16/1410:55 01/16/1419:58 7439-95-4 Molybdenum ND mg/kg 27.0 1 01/16/1410:55 01/1611419:58 7439-98-7 Nickel 56.6 mg/kg 27.0 1 01/16/1410:55 01/16/1419:58 7440-02-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 Pace Analytical Services, Inc. Pace Analytical Services, Inc. �al,eAnalytical ® 205 East Meadow Road -Suite A 2225 Riverside Dr. 1�.7Eden, NC 27288 Asheville, NC 28804 www.pacelabs.com (336)623-8921 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: TCLP SLUDGE Pace Project No.: 92186447 Sample: MCAS 001 SLUDGE Lab ID: 92186447002 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters . Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3050 Potassium ND mg/kg 27000 1 01/16/1410:55 01/16/1416:58 7440-09=7 Selenium ND .mg/kg 53.9 1 01/16/14 10:55 01/16/14 19:58 7782-49-2 Sodium ND mg/kg 27000 1 01/1611410:55 01116/1419:58 7440-23-5 Zinc 1030 mg/kg 53.9. 1 01/16/14 10:55 01/16/1419:58 7440-66-6 7471 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury 0.66 mg/kg 0.23 1 01/17/14 12:25 01/17/14 18:28 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.3 % 0.10 1 01/17/14 09:30 254OG Total Percent Solids Analytical Method: SM 2540G Total Solids 1.7 % 0.000010 1 01/16/14 13:13 9045 pH Soil Analytical Method: EPA9045 pH at 25 Degrees C 7.1 Std. Units 0.10 1 01/21/14 15:45 Plant Available Nitrogen Analytical Method: 40CFR PART 432.2 PlaritAvailable Nitrogen . 27500 mg/kg 1:0 1 01/30/14 12:19 N2 350.1 Ammonia Analytical Method: EPA350.1 Nitrogen, Ammonia 9780 mg/kg 604 1 01/21/14 04:44 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 85200 mg/kg 9750 5 01/28/14 13:45 7727-37-9 M1 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 ' Nitrogen, Nitrate ND mg/kg 120 1 01/29/14 22:54 Nitrogen, Nitrite ND mg/kg 60.2 1 01/29/14 22:54 Nitrogen, NO2 plus NO3 ND mg/kg 120 1 01/29/14 22:54 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 40100 mg/kg 1290 10 01/24/1416:05 7723-14-0 Date: 01/30/2014 12:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without,the written consent of Pace Analytical Services, Inc.. Page 6 of 27 aceAnalytical wwwpacelabs.com I ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA8081 Preparation Method: EPA3510 Leachate Method/Date: EPA 1311; 08/18/14 15:15 gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP Aluminum Arsenic Cadmium Calcium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury Date: 08/20/2014 05:06 PM ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 58-89-9. ND ug/L 30.0 10 08/19/1410:01 08/20/1410:25 57-74-9 ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 72-20-8 ND ug/L 5.0 10 08/19/1410:01 08/20/1410:25 1024-57-3 ND ug/L 10000 10 08/19/1410:01 08/20/1410:25 72-43-5 ND ug/L 30.0 10 08/19/1410:01 08/20/1410:25 8001-35-2 0 % 10-138 10 08/1911410:01 08/20/1410:25 2051-24-3 D3,S4 0 % 10-110 10 08/19/14 10:01 08/20/14 1'0:25 877-09-8 Analytical Method: EPA8151 Preparation Method: EPA3510 ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 94-75-7 ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 93-72-1 86 % 42-142 1 08/13/14 08:05' 08/14/14 05:38 19719-28-9 Analytical Method: EPA6010 Preparation Method: EPA3050 25200 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7429-90-5 67.6 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-38-2 14.0 mg/kg 6.5 1 08/07/14 17:20 08/08/14 03:29 7440-43-9 31800 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7440-70-2 1520 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7440-50-8 55.5 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-92-1 3480 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7439-95-4 ND mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-98-7 97.7 mg/kg 32.7 1 08/07/14 17:26 08/08/14 03:29 7440-02-0 ND mg/kg 32700 1 08/07/14 17:20 08/08/14 03:29 7440-09-7 ND mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7782-49-2 ND mg/kg 32700 1 08/07/14 17:20 08/08/14 03:29 7440-23-5 1320 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-66-6 Analytical Method: EPA6010 Preparation Method: EPA3010 Leachate Method/Date: EPA 1311; 08/07/14 20:00 ND mg/L 0.050 1 08/08/14 14:30 08/09/14 00:29 7440-38-2 0.53 mg/L 0.25 1 08/08/14 14:30 08/09/14 00:29 7440-34-3 0.014 mg/L 0.0050 1 08/08/14 14:30 08/09/14 00:29 7440-43-9 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-47-3 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7439-92-1 ND mg/L 0.10 1 08/08/14 14:30 08/09/14 00:29 7782-49-2 ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-22-4 . Analytical Method: EPA7470 Preparation Method: EPA7470 Leachate Method/Date: EPA 1311; 08/07/14 20:00 ND ug/L 0.20 1 08/08/1415:05 08/12/1415:26 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 28 aceAnalytical ( wmvpacelabs.com ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace AnalyticalServices, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: 92212120001. Results reported on a "dry -weight" basis Parameters Results Units Collected: 08/04/14 17:00 Report Limit ' DF Received: 08/06/14 09:20 Matrix: Solid Prepared Analyzed CAS No. Qual 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.79 mg/kg 0.28 1 08/08/1417:20 08/12/1413:53 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA8270 Preparation Method: EPA3510 Leachate Method/Date: EPA 1311; 08/18/14 15:15 1,4-Dichlorobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 106-46-7 2,4-Dinitrotoluene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 121-14-2 Hexachloro-1,3-butadiene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 87-68-3 Hexachlorobenzene ND ug/L 500 10 08/19/14 10:01 08/2011411:56 118-74-1 Hexachloroethane ND ug/L 500 10 08/19/14 10:01 08/20%14 11:56 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 Nitrobenzene ND ug/L 500 10 08/19/14 10:01 08/2011411:56 98-95-3 Pentachlorophenol ND ug/L 1000 10 08/19/14 10:01 08/20/14 11:56 87-86-5 Pyridine ND ug/L 500 10 08/19/1410:01 08/2011411:56 110-86-1 2,4,5-Trichlorophenol ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 95-95-4 2,4,6-Trichlorophenol ND ug/L 500 ` 10. 08/19/14 10:01 08/20/14 11:56 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 12-102 10 08/19/14 10:01 08/20/14 11:56 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 13-107 10 08/19/14 10:01 08/20/14 11:56 321-60-8 Terphenyl-d14 (S) 0 % 21-132 10 08/19/14 10:01 08/20/14 11:56 1718-51-0 Phenol-d6 (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 13127-88-3 2-Fluorophenol (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 367-12-4 2,4,6-Tribromophenol (S) 0 % 27-108 10 08/19/14 10:01 08/20/14 11:56 118-79-6 8260 MSV TCLP Analytical Method: EPA8260 Leachate Method/Date: EPA 1311; 08/14/14 11:03 Benzene ND ug/L 5.0 1 08/18/14 14:30 71-43-2. 2-Butanone (MEK) 12.3 ug/L 10.0 1 08/18/14 14:30 78-93-3 Carbon tetrachloride ND ug/L 5.0 1 08/18/14 14:30 56-23-5 Chlorobenzene ND ug/L 5.0 1 08/18/14 14:30 108-90-7 Chloroform ND ug/L 5.0 1 08/18/14 14:30 67-66-3 1,4-Dichlorobenzene ND ug/L 5.0 1 08/18/14 14:30 106-46-7 1,2-Dichloroethane ND ug/L 5.0 1 08/18h414:30 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1, 08/18/14 14:30 75-35-4 Tetrachloroethene ND ug/L 5.0 1 08/18/14 14:30 127-18-4 Trichloroethene ND ug/L 5.0 1 08/18/14 14:30 79-01-6 Vinyl chloride ND ug/L 5.0 1 08/18/14 14:30 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 08/18/14 14:30 17060-07-0 Toluene-d8 (S) 101 % 67-135 . 1 08/18/14 14:30 2037-26-5 4-Bromofluorobenzene (S) 107 % 70-130 1 08/18/14 14:30 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.7 % 0.10 1 08/07/14 15:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/20/2014 05:06 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 28 ® - ;aceAnalytical m1w.pacelabs.com ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1010 Flash point,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 08/19/14 03:00. 254OG Total Percent Solids Analytical Method: SM 254OG Total Solids 1.3 % 0.000010 1 08/07/14 09:36 9045 pH Soil Analytical Method: EPA9045 pH at 25 Degrees C 7.2 Std. Units 0.10 1 08/07/14 13:56 Plant Available Nitrogen Analytical Method:40CFR PART432.2 Plant Available Nitrogen 26900 mg/kg 1.0 1 08/18/14 11:30 N2 350.1 Ammonia Analytical Method: EPA 350.1 Nitrogen, Ammonia 6930 mg/kg 773 1 08/07/14 17:16 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Nitrogen, Kjeldahl, Total 85100 mg/kg 7020 5 08/13/14 15:40 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Nitrogen, Nitrate ND mg/kg 154 1 08/15/14 22:38 Nitrogen, Nitrite ND mg/kg 77.1 1 08/15/14 22:38 Nitrogen, NO2 plus NO3 ND mg/kg 154 1 08/15/14 22:38 733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/L 0.010 1 08/18/14 19:24 734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/L 1.0 1 08/15/14 15:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/20/2014 05:06 PM' without the written consent of Pace Analytical Services, Inc.. Page 6 of 28 �acuoAnalytical www.pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: TCLP SLUDGE Pace Project No.: 92186447 Sample: MCAS 001 SLUDGE Lab ID: 32186441001 Collected: 01114/14 12:30 Received: '01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Sildex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury , 8270 MSSV TCLP Sep Funnel 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methyl phenol (m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol Date: 01/30/2014 12:20 PM Analytical Method: EPA8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 ND ug/L 0.50 1 01/21/1410:40 01/23/1415:13 58-89-9 ND ug/L 3.0 1 01/21/1410:40 01/23/1415:13 57-74-9 ND ug/L 0.50 1 01/21/1410:40 01/23/1415:13 72-20-8 ND ug/L 0.50 1 01/21/1410:40 01/23/1415:13 1024-57-3 ND ug/L 1000 1 01/2111410:40 01/23/1415:13 72-43-5 ND ug/L 3.0 1 01/21/1410:40 01/23/14 15:13 8001-35-2 74 % 10-138 1 01/21/1410:40 01/23/1415:13 2051-24-3 56 % 10-110 1 01/21/1410:40 01/23/1415:13 877-09-8 Analytical Method: EPA 8151 Preparation Method: EPA 3510 ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 94-75-7 ND mg/L 0.010 1 01/22/14 08:05 01/23/14 01:33 93-72-1 95 % 70-130 1 01/22/14 08:05 01/23/14 01:33 19719-28-9 Analytical Method: EPA6010 Preparation Method: EPA3010 Leachate Method/Date: EPA 1311; 01/16/14 15:45 ND mg/L 0.050 1 01/17/1412:55 01/21/1417:51 7440-38-2 ND mg/L 0.25 1 01/17/1412:55 01/21/1417:51 7440-39-3 0.0092 mg/L 0.0050 1 01117/1412:55 01/21/1417:51 7440-43-9 ND mg/L 0.025 1 01/17/1412:55 01/21/1417:51 7440-47-3 ND mg/L 0.025 1 01/17/1412:55 01/21/1417:51 7439-92-1 ND mg/L 0.10 1 01/17/1412:55 01/21/1417:51 7782-49-2 ND mg/L 0.025 1 01/1711412:55 01/21/1417:51 7440-22-4 Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/16/14 15:45 ND ug/L 0.20 1 01/17/14 13:35 01/17/14 20:15 7439-97-6 Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 106-46-7 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 121-14-2 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 87-68-3 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 118-74-1 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 67-72-1 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-48-7 128 ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 98-95-3 ND ug/L 100 1 01/21/14 09:40 01/22/14 17:25 87-86-5 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 110-86-1 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 95-95-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 27 raceAnalXical J/ "mpacelabs.com 1 Project: TCLP SLUDGE Pace Project No.: 92186447 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab iD: 92186447001 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 8270 MSSV TCLP Sep Funnel 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Percent Moisture Percent Moisture Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 ND ug/L 50.0 1 01/21/14 09:40 01/22/14 17:25 88-06-2 51 % 12-102 1 01/21/14 09:40 01/22/14 17:25 4165-60-0 51 % 13-107 1 01/21/14 09:40 01/22/14 17:25 321-60-8 82 % 21-132 1 01/21/14 09:40 01/22/14 17:25 1718-51-0 28 % 10-110 1 01/21/14 09:40 01/22/14 17:25 13127-88-3 33 % 10-110 1 01/21/14 09:40 01/22/14 17:25 367-12-4 70 % 27-108 1 01/21/14 09:40 01/22/14 17:25 118-79-6 Analytical Method: EPA 8260 ND ug/L 100 20 01/17/1413:36 71-43-2 ND ug/L 200 ' 20 01/17/1413:36 78-93-3 ND ug/L 100 20 01/17/1413:36 56-23-5 ND ug/L 100 20 01/17/1413:36 108-90-7 ND ug/L 100 20 01117/1413:36 67-66-3 ND ug/L 100 20 01/1711413:36 106-46-7 ND ug/L 100 20 01/17/1413:36 107-06-2 ND ug/L 100 20 01/17/1413:36 75-35-4 ND ug/L 100 20 01117/1413:36 127-18-4 ND ug/L 100 20 01/17/1413:36 79-01-6 ND ug/L 100 20 01/17/1413:36 75-01-4 109 % 70-130 20 01/17/1413:36 17060-07-0 97 % 67-135 20 01/17/14 13:36 2037-26-5 98 % 70-130 20 01/17/1413:36 460-00-4 Analytical Method: ASTM D2974-87 98.3 % 0.10 1 01/24/1412:13 Sample: MCAS 001 SLUDGE Lab ID: 92186447002 Results reported on a "dry -weight" basis Parameters Results Units Collected: 01/14/14 12:30 Received: 01/15/1410:00 Matrix: Solid Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 21500 mg/kg 539 1 01/16/1410:55 01/16/1419:58 7429-90-5 Arsenic ND mg/kg 53.9 1 01/16/1410:55 01/16/1419:58 7440-38-2 Cadmium 6.9 mg/kg 5.4 1 01/16/1410:55 01/1611419:58 7440-43-9 Calcium 20600 mg/kg 539 1 01/16/1410:55 01/16/1419:58 7440-70-2 Copper 820 mg/kg 27.0 1 01/1611410:55 01/16/1419:58 7440-50-8 Lead ND mg/kg 27.0 1 01/16/1410:55 01/16/1419:58 7439-92-1 Magnesium 3200 mg/kg 539 1 01/16/1410:55 01/1611419:58 7439-95-4 Molybdenum ND mg/kg 27.0 1 01/1611410:55 01/16/1419:58 7439-98-7 Nickel 56.6 mg/kg 27.0 1 01/16/1410:55 01/16/1419:58 7440-02-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01/30/2014 12:20 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 27 5aceAnalytical t/ www.pacelabs.com I Project: TCLP SLUDGE Pace Project No.: 92186447 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab iDs 9218644 0002 Collected: 01/14/14 12:30 Received: 01/15/14 10:00 Matrix: Solid Results reported on a Yty- weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Potassium Selenium Sodium Zinc 7471 Mercury Mercury Percent Moisture Percent Moisture 254OG Total Percent Solids Total Solids 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen 350.1 Ammonia Nitrogen, Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, NO2/NO3 Nitrogen, Nitrate Nitrogen, Nitrite Nitrogen, NO2 plus NO3 365.1 Phosphorus, Total Phosphorus Date: 01/30/2014 12:20 PM Analytical Method: EPA6010 Preparation Method: EPA3050 ND mg/kg 27000 1 01/16/1410:55 01/16/1419:58 7440-09-7 ND mg/kg 53.9 1 01/16/1410:55 01/16/1419:58 7782-49-2 ND mg/kg 27000 1 01/16/1410:55 01/16/1419:58 7440-23-5 1030 mg/kg 53.9 1 01/16/14.10:55 01/16/1419:58 7440-66-6 Analytical Method: EPA7471 Preparation Method: EPA7471 0.55 mg/kg 0.23 1 01/17/14 12:25 01/17/14 18:28 7439-97-6 Analytical Method: ASTM D2974-87 98.3 % 0.10' 1 01/17/14 09:30 Analytical Method: SM 254OG 1.7 % 0.000010 1 01/16/1413:13 Analytical Method: EPA 9045 7.1 Std. Units 0.10 1 01/21/14 15:45 Analytical Method: 40CFR PART 432.2 27500 mg/kg 1.0 1 01/30/14 12:19 Analytical Method: EPA 350.1 6780 mg/kg 604 1 01/21/14 04:44 7664-41-7 Analytical Method: EPA 351.2 85200 mg/kg 9750 5 01/28/14 13:45 7727-37-9 Analytical Method: EPA 353.2 ND mg/kg 120 1 01/29/14 22:54 ND mg/kg 60.2 1 01/29/14 22:54 ND mg/kg - 120 1 01/29/14 22:54 Analytical Method: EPA 365.1 40100 mg/kg 1290 10 01/24/1416:05' 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. N2 M1 Page 6 of 27 �ao'eAnalyical ( wmvpace/abs.com 1 ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab [D: 92212120001 Collected: 08/04/14 17:00 Received: 08,105/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 08/18/14.15:15. gamma-BHC (Lindane) ND ug/L 5.0 10 08/19/14 10:01 08/20/14 10:25 58-89-9. Chlordane (Technical) ND ug/L 30.0 10 08/19/14 10:01 08/20/14 10:25 57-74-9 Endrin ND ug/L 5.0 10 08/19/14 10:01 08/20/14 10:25 72-20-8 Heptachlor epoxide ND ug/L 5.0 10 08/19/14 10:01 08/20/14 10:25 1024-57-3 Methoxychlor ND ug/L 10000 10 08/19/14 10:01 08/20/14 10:25 72-43-5 Toxaphene ND ug/L '30.0 10 08/19/14 10:01 08/20/14 10:25 8001-35-2 , Surrogates Decachlorobiphenyl (S) 0 % 10-138 10 08/19/14 10:01 08/20/14 10:25 2051-24-3 D3,S4 Tetrachloro-m-xylene (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 10:25 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA8151 Preparation Method: EPA3510 2,4-D ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 94-75-7 2,4,5-TP (Silvex) ND mg/L 0.010 1 08/13/14 08:05 08/14/14 05:38 93-72-1 Surrogates 2,4-DCAA (S) 86 6/. 42-142 1 08/13/14 08:05 08/14/14 05:38 19719-28-9 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050 Aluminum 25200 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7429-90-5 Arsenic 67.6 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-38-2 Cadmium 14.0 mg/kg 6.5 1 08/07/14 17:20 08/08/14 03:29 7440-43-9 Calcium 31800 mg/kg 655 1 08/07/14 17:20 08/08/14 03:29 7440-70-2. Copper 1520 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7440-50-8 Lead 55.5 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-92-1 Magnesium 3480 mg/kg 655. 1 08/07/14 17:20 08/08/14 03:29 7439-95-4 Molybdenum ND mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7439-98-7 Nickel 97.7 mg/kg 32.7 1 08/07/14 17:20 08/08/14 03:29 7440-02-0 Potassium ND mg/kg 32700 1 08/07/14 17:20 08/08/14 03:29 7440-09-7 Selenium ND mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7782-49-2 Sodium ND mg/kg 32700 1 08/07/14 17:20 08/08/14 03:29 7440-23-5 Zinc 1320 mg/kg 65.5 1 08/07/14 17:20 08/08/14 03:29 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 08/07/14 20:00 Arsenic ND mg/L 0.050 1 08/08/14 14:30 08/09/14 00:29 7440-38-2 Barium 0.53 mg/L 0.25 1 08/08/14 14:30 08/09/14 00:29 7440-39-3 Cadmium 0.014 mg/L 0.0050 1 08/08/14 14:30 08/09/14 00:29 7440-43-9 Chromium ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-47-3 Lead ND mg/L 0.025 1 08/08/14 14:30 08/09,/14 00:29 7439-92-1 Selenium ND mg/L 0.10 1 08/08/14 14:30 08/09/14 00:29 7782-49-2 Silver ND mg/L 0.025 1 08/08/14 14:30 08/09/14 00:29 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 08/07/14 20:00 Mercury ND ug/L 0.20 1 08/08/1415:05 08/12/1415:26 7439-97-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/20/2014 05:06 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 28 Pace Analytical Services, Inc. ® 9800Hulnte sville, NCSuite 28078 •_�Pa>✓eAnalytical wympacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Project No.: 92212120 nPace nn SQlllple: IYICMS OV 1 SLUDGE LabID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 7471 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury 0.79 mg/kg 0.28 1 08/08/14 17:20 08/12/14 13:53 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA8270 Preparation Method: EPA3510 Leachate Method/Date: EPA 1311; 08/18/14 15:15 1,4-Dichlorobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 106-46-7 2,4-Dinitrotoluene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 121-14-2 Hexachloro-1,3-butadiene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 87-68-3 Hexachlorobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 118-74-1 Hexachloroethane ND ug/L 500 10 08/19/14 10:01 08/2011411:56 67-72-1 2-Methylphenol(o-Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 Nitrobenzene ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 98-95-3 Pentachlorophenol ND ug/L 1000 10 08/19/14 10:01 08/20/14 11:56 87-86-5 Pyridine ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 110-86-1 2,4,5-Trichlorophenol ND ug/L 500 10 08/19/14 10:01. 08/20/14 11:56 95-95-4 2,4,6-Trichlorophenol ND ug/L 500 10 08/19/14 10:01 08/20/14 11:56 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 12-102 10 08/19/14 10:01 08/20/14 11:66 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 13-107 10 08/19/14 10:01 08/20/14 11:56 321-60-8 Terphenyl-d14 (S) 0 % 21-132 10 08/19/14 10:01 08/20/14 11:56 1718-51-0 Phenol-d6 (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 13127-88-3 2-Fluorophenol (S) 0 % 10-110 10 08/19/14 10:01 08/20/14 11:56 367-12-4 2,4,6-Tribromophenol (S) 0 % 27-108 10 08/19/14 10:01 08/20/14 11:56 118-79-6 8260 MSV TCLP Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 08/14/14 11:03 Benzene ND ug/L 5.0 1 08/18/14 14:30 71-43-2 2-Butanone (MEK) 12.3 ug/L 10.0 1 08/18/14 14:30 78-93-3 Carbon tetrachloride ND ug/L 5.0 1 08/18/14 14:30 56-23-5 Chlorobenzene ND ug/L 5.0 1 08/18/14 14:30 108-90-7 Chloroform ND ug/L 5.0 1 08/18/14 14:30 67-66-3 1,4-Dichlorobenzene ND ug/L 5.0 1 08/18/14 14:30 106-46-7 1,2-Dichloroethane ND ug/L 5.0 1 08/18/14 14:30 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1 08/18/14 14:30 75-35-4 Tetrachloroethene ND ug/L 5.0 1 08/1811414:30 127-18-4 Trichloroethene ND ug/L 5.0 1 08/18/14 14:30 79-01-6 Vinyl chloride ND ug/L 5.0 1 08/18/14 14:30 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 08/18/14 14:30 17060-07-0 Toluene-d8 (S) 101 % 67-135 1 08/18/14 14:30 2037-26-5 4-Bromofluorobenzene (S) 107 % 70-130 1 08/18/14 14:30 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.7 % .0.10 1 08/07/14 15:12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/20/2014 05:06 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 28 J_Y aceAnalXical wmvpacelabs.com ANALYTICAL RESULTS Project: MCAS 001 SLUDGE Pace Project No.: 92212120 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS 001 SLUDGE Lab ID: 92212120001 Collected: 08/04/14 17:00 Received: 08/06/14 09:20 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 1010 Flash point,Closed Cup Analytical Method: EPA 1010• Flashpoint >200 deg F 70.0 1 08/19/14 63:00 2540G Total Percent Solids Analytical Method: SM 254OG Total Solids 1.3 % 0.000010 1 08/07/14 09:36 9045 pH Soil Analytical Method: EFA9045 pH at 25 Degrees C 7.2 Std. Units 0.10 1 OS/07/14 13:56 Plant Available Nitrogen Analytical Method: 40CFR PART432.2 Plant Available Nitrogen 26900 mg/kg 1.0 1 08/18/1411:30 N2 350.1 Ammonia Analytical Method: EPA350.1 Nitrogen, Ammonia 6930 mg/kg 773 1 08/07/14 17:16 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA351.2 Nitrogen, Kjeldahl, Total 85100 mglkg 7020 5 08/13/14 15:40 7727-37-9 353.2 Nitrogen, NO2/NO3 Analytical Method: EPA353.2 Nitrogen, Nitrate ND mg/kg 154 1 08/15/14 22:38 Nitrogen, Nitrite ND mg/kg 77.1 1 08/15/14 22:38 Nitrogen, NO2 plus NO3 ND mg/kg 154 1 08/15/14 22:38 733C Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/L 0.010 1 08/18/14 19:24 734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/L 1.0 1 08/15/14 15:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/20/2014 05:06 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 28 PATHOGEN/VECTOR ATTRACTION REDUCTION FORM 1) LIME STABILIZATION 2) ANAEROBIC DIGESTION ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: US Marine Corps - Cherry Point Permit Number: WQ0001489 VVWTP Name: USMCAS - Cherry Point WWTP NPDES Number: NC0003816 Monitoring Period: From 1/1/2014 To, 12/31/2014 Pathogen Reduction (40 CFR 503.32) -'Please indicate level achieved and alternative performed: Class A: Alternative 1 El Alternative 2 E3 Alternative 3 Ci Alternative 40 Alternative 5 E3 Alternative 6 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost D T-Heat Drying 0 Heat Treatment El Thermoplrilic a Ray Gamma Ray Pasteurization ation E3Be Class B: Alternative 1 E3 Alternative 2 X Alternative 3El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying El Composting E3 Aerobic Digestion i Anaerobic D es tion g If applicable to alternative performed (Class A or Class B) completethe following monitoring data: Parameter Allowable Level in Sludge Pathogen Density um er o Excee- dences requency of Analysis Sample TYe a ica Tech- nicue Geo. MeanMaxim Units Fecal Coliform —Minimum 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU per gram of 1000 mpn per' gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei ht Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 Option 2 ® Option 3 0 Option 4 E3 Option 5 Option 6 X Option 7 Option 8. Option 9 Option 10 No vectorattraction reduction options ions were performed CERTIFICATION STATEMENT (please check the appropriate statement) X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Patricia T. Davis - ORC Pre er ame and Title (ty or print Land Applier Name and Title (if applicable)(type or print) u� digs Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: US Marine Corps - Cherry Point Permit Number: WWTP Name: USMCAS - Cherry Point WWTP NPDES Number: Monitoring Period: From 3/8/2014 To 3/31/2014 WQ0001489 NC0003816 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ ..................... Alternative 4❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens"•. Compost ❑ Heat Drying ❑ Heat Treatment ❑ Theimoplulic ❑ Beta Ray Gamma Ray Pasteurization ❑ Class B: Alternative 1 ❑ Alternative 2 X Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization OT Air Drying ❑ 1 Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion X . ....... ......ed If applicable to alternative perform (Class A or Class B),complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- deuces Prequency of Analvsis Sample Type Analytical Tech - ni ue Minimum inimu Geo. MeanMaximui Units Fecal Coliform 2x 10tothe 6th power MPN per gram of total solids or 2 x 10 to the 6th power CFU pet gram of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 Option 2 Option 3 ❑ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑. Option'9 ❑ Option 10 ❑ options wereperformed No vector attraction reductionp CERTIFICATION STATEMENT (please check the appropriate statement) X "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Patricia T. Davis - O In Wr��er ame and Title (ty or rint) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer Date Signature of Land Applier (if applicable) Date DENR FORM RF (5/2003) PATHOGEN/VECTOR ATTRACTION REDUCTION SUPPORTING DOCUMENTATION (LIME STABILIZATION) : LAB ANALYSIS BENCH SHEETS 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 16 SOLIDS ANALYSIS BENCH SHEET ANALYST ARMISTEAD/JONES/BEHAN JDATE SAMPLE HOLDING TANK TYPE TIME 1115 VOLUME WO/LIME W/LIME PERCENT SOLIDS 3.21 BEGINNING CALIBRATION RECORD EVENT 6 1/6/2014 GRAB 100 PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.020 12.471 11.06 PH MONITORING REPORT 95.6 SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 1ST 2ND FINAL 1/6/2014 1115 1427 1630 14351 7.23 12.42 12.48 12.25 22 17 17 15 -0.09 -0.24 -0.24 -0.31 7.14 MJ 1/6/2014 12.18 RA 1/6/2014 1/7/20141 12.24 JB 11.951 MJ FINAL CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 1 12-.45F 11.00 SLOPE My/Ph % AGREEMENT 10.091 12.471 11.05 104.1 SOLIDS WORKSHEET HOLDING TANK WITH LIME WEIGHT OF DISH AND WET SAMPLE f WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WO/LIME W/LIME grams 167.7701 grams 95.811 0 grams 71.9591 grams 98.1233 grams 95.811 0 grams 2.3123 WEIGHT OF DRIED SAMPLE: 0 lgrams X 100 2.3123 WEIGHT OF WET SAMPLE: 0 lgrams 71.9591 3.213353 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 16 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL/CHARETTE/JOKES DATE EVENT 6 1/17/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1020 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.51 % 2.83% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.46 11.00 SLOPE My/Ph % AGREEMENT 10.000 12.46 11.04 PH 97.4 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 1/16/2014 1020 7.19 15 -0.30 6.89 MJ 1ST 1/17/2014 1319 12.4 16 -0.30 12.10 FS 2ND 1 1117/20141 15251 12.35 16 -0.301 12.051 AC FINAL 11/18/,20141 14001 FINAL 12.32 CALIBRATION 15 -0.33 11.99 MJ RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.03 12.46 11.03 94.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 170.0581 grams 145.1714 WEIGHT OF DISH 95.8115 grams 94.902 WEIGHT OF WET SAMPLE 74.2466 grams 50.2694 WEIGHT OF DISH AND DRIED SAMPLE 97.6754 grams 96.3244 WEIGHT OF DISH 95.8115 grams 94.902 WEIGHT OF DRIED SAMPLE 1.8639 grams 1.4224 WEIGHT OF DRIED SAMPLE: 1.8639 grams X 100 1.4224 WEIGHT OF WET SAMPLE: 74.2466 grams 50.2694 2.510418 2.829554 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 181 SOLIDS ANALYSIS BENCH SHEET ANALYST ARMISTEAD/ WADE DATE EVENT 1 2/3/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1310 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.96% 2.56% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 1 .11.00 SLOPE My/Ph % AGREEMENT 10.030 12.47 11.04 PH 95.1 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 1/26/2014 1310 7.12 16 -0.27 6.85 EW 1ST 2/3/2014 1308 12.59 16 -0.27 12.32 RA 2ND 2/3/20141 1310 12.65 15 -0.30j 12.35 RA FINAL 2/4/20141 13301 FINAL 12.41 15 CALIBRATION -0.31 12.101 RA RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6110.04 12.471 11.02 94.7 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 195.3268 grams 173.4459 WEIGHT OF DISH 104.2414 grams 95.7527 WEIGHT OF WET SAMPLE 91.0854 grams 77.6932 WEIGHT OF DISH AND DRIED SAMPLE 106.0287 grams 97.7407 WEIGHT OF DISH 104.2414 grams 95.7527 WEIGHT OF DRIED SAMPLE 1.7873 grams 1.988 WEIGHT OF DRIED SAMPLE: 1.7873 grams X 100 1.988 WEIGHT OF WET SAMPLE: 91.0854 grams 77.6932 1.9622241 2.558782 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER i�" SOLIDS ANALYSIS BENCH SHEET ANALYST NOEUCHARETTE DATE IEVENT 2/13/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 2100 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.74% 2.37% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 9.950 12.47 11.01 PH 96.1 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 2/10/2014 2100 6.86 12.7 -0.36 6.50 FS 1ST 2/13/2014 1249 12.73 12.8 -0.36 12.37 AC 2ND 1 2/13/20141 15021 12.781 13.4 -0.361 12.421 AC FINAL 2/14/2014 13081 FINAL 12.61 14.5 CALIBRATION -0.331 12.271 AC RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 60"1005 12.47 11.01 95.6 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 154.2306 grams 144.0216 WEIGHT OF DISH 104.2404 grams 95.7527 WEIGHT OF WET SAMPLE 49.9902, grams 48.2689 WEIGHT OF DISH AND DRIED SAMPLE 105.1102 grams 96.8974 WEIGHT OF DISH .104.2404 grams 95.7527 WEIGHT OF DRIED SAMPLE 0.8698 grams 1.1447 1 7- WEIGHT OF DRIED SAMPLE: 0.8698 grams X 100 1.1447 WEIGHT OF WET SAMPLE: 49.9902 grams 48.2689 1.7399411 2.371506 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 18 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL/WADE/ARMISTEAD DATE EVENT 3 2/17/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1535 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS 1.75% 2.90% BEGINNING CALIBRATION RECORD PH -METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.060 125.5-2t 11.09 94.9 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH : 2/17/2014 1535 7.04 12.9 -0.36 6.68 FS 1ST 2/17/2014 2010 12.87 13.6 -0.33 12.54 EW 2ND 1 2/17120141 22101 12.631 13.8 -0.331 12.301 EW FINAL 2/18/20141 20401 FINAL 12.18 15 CALIBRATION -0.31 RECORD 11.881 RA PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.031 12.46F 11.03 94.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 138.2658 grams 153.2005 WEIGHT OF DISH 95.809 grams 94.4288 WEIGHT OF WET SAMPLE 42.4568 grams 58.7717 WEIGHT OF DISH AND DRIED SAMPLE 96.5516 grams 96.1361 WEIGHT OF DISH 95.809 grams 94.4288 WEIGHT OF DRIED SAMPLE 0.7426 grams 1.7073 WEIGHT OF DRIED SAMPLE: 0.7426 grams X 100 1.7073 WEIGHT OF WET SAMPLE: 42.4568 grams 58.7717 1.749072 2.90497 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 191 SOLIDS ANALYSIS BENCH SHEET ANALYST WADE DATE EVENT 1 2/21/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1305 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS 1.68% 2.45% BEGINNING CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT "10030 12.471 1 92.9 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS' INITIAL PH 2/21/2014 0835 7.17 17.3 -0.24 6:93 EW 1ST 2/21/2014. 1310 12.49 17.8 -0.21 12.28 EW 2ND 1 2/21/20141 15101 12.681 17.1 -0.241 12.44 EW FINAL. 2/22/20141 13101 12.071 17.7 FINAL CALIBRATION -0.211 11.861 EW RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 60"1004 12.481 11.041 92.7 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 180.843 grams 179.2912 WEIGHT OF DISH 94.902 grams 94.4287 WEIGHT OF WET SAMPLE 85.941 grams 84.8625 WEIGHT OF DISH AND DRIED SAMPLE 96.3467 grams 96.5057 WEIGHT OF DISH 94.902 grams 94.4287 WEIGHT OF DRIED SAMPLE 1.4447 grams 2.077 WEIGHT OF DRIED SAMPLE: 1.4447 grams X 100 2.077 WEIGHT OF WET SAMPLE: 85.941 grams 84.8625 1.6810371 2.447489 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC, TASK ORDER 18 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN JDATE SAMPLE HOLDING TANK ITYPE TIME 1800 VOLUME WO/LIME W/LIME jPjEjRCLIDS 1 3.25% BEGINNING CALIBRATION RECORD EVENT 5 2/24/2014 GRAB 100 PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 1 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.050 m 12.46 10.98 PH MONITORING REPORT 97.5 -- i SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 1ST 2ND FINAL 1807 2015 18101 12.25 12.41 12.081 17.2 17.4 16.1 0.00 -0.24 12.01 -0.24 12.17 -0.27 11.81 JB JB JB 2/25/2014 2/25/2014 2/26/20141 FINAL CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.031 12.461 11.03 94.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE grams 176.0369 WEIGHT OF DISH grams 95.8135 WEIGHT OF WET SAMPLE 0 grams 80.2234 WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE grams 0 grams 0 grams 98.4171 95.8135 2.6036 WEIGHT OF DRIED SAMPLE: 1 0 Igrams X 100 2.6036 WEIGHT OF WET SAMPLE: 0 grams 80.2234 3.245437 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER SOLIDS ANALYSIS BENCH SHEET ANALYST BA & JEB DATE EVENT 2/28/2014 1 7- SAMPLE HOLDING TANK TYPE- GRAB TIME VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.39% 3.25% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.040 12.471 11 PH 100.3 MONITORING REPORT SAMPLE DATE TIME ANAL PH 'TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 2/28/2014 0950 7.09 14 -0.33 6.76 RA 1ST 2/28/2014 1600 12.41 16.5 -0.27 12.14 JB 2ND 1 2/28/20141 18051 12.361 15.3 -0.301 12.061 JB FINAL 3/1/20141 16051 12.381 17.1 -0.241 12.141 JB PH METER CALIBRATION BUFFER INITIAL 10.00 .12.45 11.00 SLOPE My/Ph % AGREEMENT 6010.03 12-.4-6t 11.03 94.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 174.6072 grams 157.1053 WEIGHT OF DISH 94.4294 grams 95.7733 WEIGHT OF WET SAMPLE 80.1778 grams 61.332 WEIGHT OF DISH AND DRIED SAMPLE 96.3474 grams 97.7657 WEIGHT OF DISH 94.4294 grams 95.7733 WEIGHT OF DRIED SAMPLE 1.918 grams 1.9924 WEIGHT OF DRIED SAMPLE: 1.918 grams X 100 1.9924 WEIGHT OF WET SAMPLE: 80.1778 lgrams 61.332 2.3921831 3.248549 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 19 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL/CHARETTE DATE EVENT 5 3/16/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1410 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.96% 2.83% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK _ BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6 "10050 12.471 10.97 PH 98.9' MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 3/16/2014 1412 7.14 17 -0.24 6.90 ASC 1ST 3/17/2014 1317 12.46 15 -0.30 12.16 ASC 2ND 1 3/17/20141 15171 12.39 16 -0.271 12.121 ASC FINAL 3/18/20141 =14301 12.23 17 FINAL CALIBRATION -0.24 11.99 FS RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.041 12.47 10.97 99 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 165.1916 grams 151.7301 WEIGHT OF DISH 95.8156 grams 94.9357 WEIGHT OF WET SAMPLE 69.376 grams 56.7944 WEIGHT OF DISH AND DRIED SAMPLE 97.1725 grams 96.5438 WEIGHT OF DISH 95.8156 grams 94.9357 WEIGHT OF DRIED SAMPLE 1.3569 grams 1.6081 WEIGHT OF DRIED SAMPLE: 1.3569 grams X 100 1.6081 WEIGHT OF WET SAMPLE: 69.376 lgrams 56.7944 1.9568641 2.831441 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 19 SOLIDS ANALYSIS BENCH SHEET ANALYST WADE/ARMISTEAD/NOEL DATE EVENT 6 3/24/2014 SAMPLE HOLDING TANK TYPE GRAB TIME VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.33% 3.15% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 9.990 12.47 10.94 PH 98.5 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 3/23/2014 1415 6.72 18 -0.21 6.51 EW 1ST 3/24/2014 1830 12.34 17 -0.24 12.10 RA 2ND 1 3/24/20141 20351 12.41 16 -0.271 12.141 RA FINAL FINAL 3/25/2014 1835 12.39 17 CALIBRATION -0.24 RECORD 12.15 BN PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6 "0912.62F 11.03 96.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 192.0668 grams 170.8657 WEIGHT OF DISH 94.8976 grams 104.2412 WEIGHT OF WET SAMPLE 97.1692 grams 66.6245 WEIGHT OF DISH AND DRIED SAMPLE 97.1658 grams 106.3432 WEIGHT OF DISH 94.8976 grams 104.2412 WEIGHT OF DRIED SAMPLE 2.2682 grams 2.102 WEIGHT OF DRIED SAMPLE: 2.2682 grams X 100 2.102 WEIGHT OF WET SAMPLE: 97.1692 grams 66.6245 2.334279 3.154996 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 1 9 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 7 4/2/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1015 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.26% 3.13% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.46 11.00 SLOPE My/Ph % AGREEMENT 10.050 12.47 11.05 PH 94.9 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 4/2/2014 1015 6.82 18 -0.21 6.61 JB 1ST 4/4/2014 1726 12.27 20 -0.15 12.12 FS 2ND 4/4/20141 1930 12.25 191 0.15 12.101 FS FINAL 1 4/5/20141 17301 FINAL 12.16 20 CALIBRATION -0.151 12.011 FS RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6010.05 12.471 11.07 94.3 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 139.0575 grams 156.0943 WEIGHT OF DISH 94.4295 grams 95.8134 WEIGHT OF WET SAMPLE 44.628 grams 60.2809 WEIGHT OF DISH AND DRIED SAMPLE 95.4402 grams 97.6999 WEIGHT OF DISH 94.4295 grams 95.8134 WEIGHT OF DRIED SAMPLE 1.0107 grams 1.8865 WEIGHT OF DRIED SAMPLE: 1.0107 grams X . 100 1.8865 WEIGHT OF WET SAMPLE: 44.628 grams 60.2809 2.2647221 3.129515 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 19 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL/CHARETTE DATE EVENT 8 4/11/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 900 VOLUME -100 WO/LIME W/LIME PERCENT SOLIDS1 2.29% 3.22% BEGINNING CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.040 12.471 11.04 96.4 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP COR - ACT PH INITIALS INITIAL PH 4/11/2014 0900 7.03 18.4 -0.21 FS 1ST 4/14/2014 1311 12.27 21 -0.12 FS 2ND 1 4/14/20141 1511 12.221 21.2 -0.12 1 AC FINAL 4/15/20141 13301 FINAL 12.091 21.9 CALIBRATION -0.09 AC RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 9.99 12.47 11.04 95.8 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 154.0498 grams 181.1457 WEIGHT OF DISH 95.8109 grams 95.758 WEIGHT OF WET SAMPLE 58.2389 grams 85.3877 WEIGHT OF DISH AND DRIED SAMPLE 97.1421 grams 98.505, WEIGHT OF DISH 95.8109 grams 95.758 WEIGHT OF DRIED SAMPLE 1.3312 grams 2.747 WEIGHT OF DRIED SAMPLE: 1.3312 grams X 100 2.747 WEIGHT OF WET SAMPLE: 58.2389 grams 85.3877 2.2857571 3.217091 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 191 SOLIDS ANALYSIS BENCH SHEET ANALYST WADE DATE EVENT 9 4/21/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1430 VOLUME 100 -- --- WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.84% 2.72% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.040 12.471 11.11 PH 95.9 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 4/20/2014 1330 6.91 18 -0.21 6.70 EW 1ST 4/21 /2014 1430 12.32 20 -0.15 12.17 EW 2ND 1 4/21/20141 16301 12.24 21 -0.121 12.121 RA FINAL 4/22/20141 16301 FINAL 12.23 22 CALIBRATION -0.091 12.141 JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6M1"003 12.461 11.03.1 94.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 195.5552 grams 193.8254 WEIGHT OF DISH 95.8104 grams 94.4235 WEIGHT OF WET SAMPLE 99.7448 grams 99.4019 WEIGHT OF DISH AND DRIED SAMPLE 97.6451 grams 97.1291 WEIGHT OF DISH 95.8104 grams 94.4235 WEIGHT OF DRIED SAMPLE 1.8347 grams 2.7056 WEIGHT OF DRIED SAMPLE: 1.8347 grams X 100 2.7056 WEIGHT OF WET SAMPLE: 99.7448 grams 99.4019 1.8393941 2.72188 % TOTAL 2014 • MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 19 SOLIDS ANALYSIS BENCH SHEET ANALYST NOEL DATE EVENT 10 4/26/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1810 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.25% 3.0.1 % CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT "j030 12.47 11.02 PH 94.6 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 4/25/2014 0650 7.02 18.8 -0.18 6.84 EW 1ST 4/26/2014 1330 12.25 21.3 -0.12 12.13 JB 2ND j 4/26/2014j 1530j 12.23j 21.3 -0.12 1 12.11 j JB FINAL 4/27/20141 16301 FINAL 12.151 CALIBRATION 22.3 -0.09 12.0-61 BN RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT "10050 12.581 11.07 93.8 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 193.1352 grams 196.7172 WEIGHT OF DISH 94.4127 grams 95.7568 WEIGHT OF WET SAMPLE 98.7225 grams 100.9604 WEIGHT OF DISH AND DRIED SAMPLE 96.6307 grams 98.795 WEIGHT OF DISH 94.4127 grams 95.7568 WEIGHT OF DRIED SAMPLE 2.218 grams 3.0382 WEIGHT OF DRIED SAMPLE: 2.218 grams X lool 3.0382 WEIGHT OF WET SAMPLE: 98.7225 lgrams 100.9604 2.2467021 3.009299 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST EW/JB/RA DATE EVENT 2 4/30/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 940 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.51 % 2.70% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.040 12.54 11.09 PH 93.7 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 4/30/2014 0940 6.92 21.2 -0.12 6.80 EW 1ST 4/30/2014 1300 12.23 22.1 -0.09 12.14 EW 2ND 1 4/30/20141 15001 12.361 22.3 -0-091 12.271 JB FINAL 5/1 /20141 13001 FINAL 12.21 24 CALIBRATION -0.031 12.181 RA RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE MV/Ph % AGREEMENT 6010.04 12.561 11.091 92.4 SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 184.755 grams 195.11 WEIGHT OF DISH 95.7566 grams 94.902 WEIGHT OF WET SAMPLE 88.9984 grams 100.208 WEIGHT OF DISH AND DRIED SAMPLE 97.9909 grams 97.6029 WEIGHT OF DISH 95.7566 grams 94.902 WEIGHT OF DRIED SAMPLE 2.2343 grams 2.7009 WEIGHT OF DRIED SAMPLE: 2.2343 grams X 100 2.7009 WEIGHT OF WET SAMPLE: 88.9984 grams 100.208 2.5104951 2.695294 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 201 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 1 3 5/6/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1235 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.13% 2.96% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT "10030 12.471 11.04 PH 95 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 5/6/2014 1235 7 22.6 -0.09 6.91 JB 1ST 5/6/2014 1520 12.33 23.4 -0.06 12.27 MJ 2ND 5/6/2014 17201 FINAL 12.29 23.2 CALIBRATION -0.061 12.231 EW RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.03 12.46 11.03 94.4 FINAL 5/7/2014 17221 1213 24.2 -0.03 1212.97 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 133.768 grams 178.676 WEIGHT OF DISH 95.2781 grams 104.2408 WEIGHT OF WET SAMPLE 38.4899 grams 74.4352 WEIGHT OF DISH AND DRIED SAMPLE 96.0963 grams 106.4406 WEIGHT OF DISH 95.2781 grams 104.2408 WEIGHT OF DRIED SAMPLE 0.8182 grams 2.1998 WEIGHT OF DRIED SAMPLE: 0.8182 grams X 100 2.1998 WEIGHT OF WET SAMPLE: 38.4899 11100 2,125752 grams 74.4352 2.956322 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 4 5/19/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1008 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS 2.31 % 3.07% BEGINNING CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.46 11.00 SLOPE My/Ph % AGREEMENT 9.990 12.47 11.06 96.3 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 5/19/2014 1008 7 22.6 -0.09 6.91 EW 1ST 5/20/20141 13001 12.33 23.4 -0.06 12.27 EW 2ND 5/20/20141 15001 FINAL 12.291 23.2 CALIBRATION -0.061 12.23 •JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 1005.00 12.47 11.01 95.2 FINAL 5/21/2014 13001 12.111 24.8 -0.03 127378F JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 169.7335 grams 193.5833 WEIGHT OF DISH 94.9026 grams 95.76 WEIGHT OF WET SAMPLE 74.8309 grams 97.8233 WEIGHT OF DISH AND DRIED SAMPLE 96.6317 grams 98.7598 WEIGHT OF DISH 94.9026 grams 95.76 WEIGHT OF DRIED SAMPLE 1.7291 grams 2.9998 WEIGHT OF DRIED SAMPLE: 1.7291 grams X 100 2.9998 WEIGHT OF WET SAMPLE: 74.8309 2.3106761 grams 97.8233 3.06655 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 5 5/27/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 945 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 3.03% 3.57% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.010 12.46 11.01 PH 94,8 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH' 5/27/2014 0945 7.1 24 -0.03 7.07 RA 1ST 5/27/2014 1300 12.06 26 0.03 12.09 CR 2ND 5/27/20141 15001 FINAL 12.02 271 0.03 12--05F CR CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT FINAL 5/28/2014 13001 11.921 271 0.03 11.951 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 170.8228 grams 196.539 WEIGHT OF DISH 104.2398 grams 95.2792 WEIGHT OF WET SAMPLE 66.583 grams 101.2598 WEIGHT OF DISH AND DRIED SAMPLE 106.2595 grams 98.8934 WEIGHT OF DISH 104.2398 grams 95.2792 WEIGHT OF DRIED SAMPLE 2.0197 grams 3.6142 WEIGHT OF DRIED SAMPLE: 2.0197 grams X 100 3.6142 WEIGHT OF WET SAMPLE: 66.583 lgrams 3.033357 101.2598 3.569235 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL DATE EVENT 6 6/2/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 2030 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS 2.53% 3.14% BEGINNING CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.050 12.471 10.97 94.6 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS . INITIAL PH 6/2/2014 2030 6.98 23 -0.03 6.95 FS 1ST 6/3/2014 1245 12.19 24.5 -0.03 12.16 MJ 2ND 6/3/2014 1445 12.16 25 FINAL CALIBRATION 0.00 12.16 JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE MV/Ph % AGREEMENT 10.01 12.46 11.01 94.7 FINAL 6/4/2014 12501 12.021 26.31 0.03 12.051 MJ SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 155.3168 grams 195.165 WEIGHT OF DISH 95.281 grams 95.816 WEIGHT OF WET SAMPLE 60.0358 grams 99.349 WEIGHT OF DISH AND DRIED SAMPLE 96.7982 grams 98.9333 WEIGHT OF DISH 95.281. grams 95.816 WEIGHT OF DRIED SAMPLE 1.5172 grams 3.1173 WEIGHT OF DRIED SAMPLE: 1.5172 grams X 100 3.1173 WEIGHT OF WET SAMPLE: 60.0358 2.527159 grams 99.349 3.137727 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST SHIMMEL DATE EVENT 7 6/9/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1318 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.81 % 2.46% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 6 10.010 12.47 11.02 PH 93.8 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 6/9/2014 1900 6.85 24.7 0.00 6.85 EW 1ST 6/10/2014 1320 12.21 26.9 0.06 12.27 FS 2ND 1 6/10/20141 15201 FINAL 12.131 CALIBRATION 28.1 0.091 12.221 FS RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.01 12.46 11.01 94.7 FINAL 6/11/2014 13301 12.11 28.11 0.09 12.19 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 193.8004 grams 155.4609 WEIGHT OF DISH 94.9043 grams 95.7613 WEIGHT OF WET SAMPLE 98.8961 grams 59.6996 WEIGHT OF DISH AND DRIED SAMPLE 96.6917 grams 97.2323 WEIGHT OF DISH 94.9043 grams 95.7613 WEIGHT OF DRIED SAMPLE 1.7874 grams 1.471 WEIGHT OF DRIED SAMPLE: 1.7874 grams X 100 1.471 WEIGHT OF WET SAMPLE: 98.8961 1.8073511 grams 59.6996 2.464003 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST WADE/BEHAN DATE EVENT 8 6/17/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 900 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.13% 2.84% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.0001 12.47 11.01 PH 93.5 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 6/17/2014 0902 7.23 26 0.03 7.26 EW 1ST 6/17/2014 1235 12.12 28 0.09 12.21 JB 2ND 6/17/20141 14351 FINAL 12.191 281 0.091 12.281 JB CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.01 12.47 10.97 90.4 FINAL 6/18/2014 12401 .12.071 281 0.09 12.161 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME . W/LIME WEIGHT OF DISH AND WET SAMPLE 192.113 grams 196.7921 WEIGHT OF DISH 94.4311 grams 95.8197 WEIGHT OF WET SAMPLE 97.6819 grams 100.9724 WEIGHT OF DISH AND DRIED SAMPLE 96.5119 grams 98.6883 WEIGHT OF DISH 94.4311 grams 95.8197 WEIGHT OF DRIED SAMPLE 2.0808 grams 2.8686 WEIGHT OF DRIED SAMPLE: 2.0808 grams X 100 2.8686 WEIGHT OF WET SAMPLE: 97.6819 2,130181 grams 1 100.9724 2.840974 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 9 6/24/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 845 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.23% 3.00% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT J01"0.020 12.47 10.98 PH 95 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL. PH 6/24/2014 0845 7.03 26.7 0.03 7.06 JB 1ST 6/24/2014 1315 12.13 27.3 0.06 12.19 JB 2 N D 1 6/24/20141 15151 12.071 FINAL CALIBRATION 27.91 0.061 121.131 JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.00 12.47 10.98 90.4 FINAL 6/25/2014 13201 12.031 29.11 0.12 12.15 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 192.6848 grams 194.8252 WEIGHT OF DISH 95.2828 grams 94.9058 WEIGHT OF WET SAMPLE 97.402 grams 99.9194 WEIGHT OF DISH AND DRIED SAMPLE 97.4527 grams 97.9061 WEIGHT OF DISH 95.2828 grams 94.9058 WEIGHT OF DRIED SAMPLE 2.1699 grams 3.0003 WEIGHT OF DRIED SAMPLE: 2.1699 grams X 100 3.0003 WEIGHT OF WET SAMPLE: 97.402 2.2277781 grams 1 99.9194 3.00272 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 10 7/l /2014 SAMPLE HOLDING TANK TYPE GRAB TIME 815 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.12% 2.74% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 9.990 12.47 11 PH 92.6 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 7/1/2014 0817 6.99 25.4 0.00 6.99 JB 1ST 7/l/2014 1410 12.2 27.1 0.06 12.26 JB 2ND 7/l/2014 16101 FINAL 12.131 28.1 0.091 12.221 JB CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.04 12.46 10.92 90 FINAL 7/2/2014 14101 12.091 28.5 0.09 12.18 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 193.7986 grams 194.932 WEIGHT OF DISH 94.4324 grams 95.8171 WEIGHT OF WET SAMPLE 99.3662 grams 99.1149 WEIGHT OF DISH AND DRIED SAMPLE 96.5419 grams 98.5376 WEIGHT OF DISH 94.4324 grams 95.8171 WEIGHT OF DRIED SAMPLE 2.1095 grams 2.7205 WEIGHT OF DRIED SAMPLE: 2.1095 grams X 100 2.7205 WEIGHT OF WET SAMPLE: 99.3662 2.122955 grams 99,1149 2.74479, % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 20 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 11 7/15/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 0905 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.13% 2.84% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 1 11.00 SLOPE My/Ph % AGREEMENT 10.020 12.46 11.031 PH 95 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 7/15/2014 0905 7.09 26.6 0.03 7.12 JB 1ST 7/15/2014 1215 12.16 28.7 0.09 12.25 JB 2ND 7/15/2014 14151 FINAL 12.081 27.61 CALIBRATION 0.061 12.14 JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.03 12.47 11 92.4 FINAL 7/16/2014 12151 121 25.81 0 12.00 JB SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 193.8462 grams 195.076 WEIGHT OF DISH 94.4351 grams 94.9087 WEIGHT OF WET SAMPLE 99.4111 grams 100.1673 WEIGHT OF DISH AND DRIED SAMPLE 96.5501 grams 97.7525 WEIGHT OF DISH 94.4351 grams 94.9087 WEIGHT OF DRIED SAMPLE 2.115 grams 2.8438 WEIGHT OF DRIED SAMPLE: 2.115 grams X ;100 2.8438 WEIGHT OF WET SAMPLE: 99.4111 2.1275291 grams 1 100.1673 2.83905 %TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 201 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 12 7/21/2014 SAMPLE. HOLDING TANK TYPE GRAB TIME 1410 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.19% 3.05% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.050 12.471 10.93 PH 90.5 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 7/21/2014 1410 6.96 25.8 0.00 6.96 JB 1ST 7/22/2014 1240 12.23 26.2 0.03 12.26 JB 2ND 7/22/20141 14451 FINAL 12.131 271 0.061 12.19 JB CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.03 12.47 11 92.4 FINAL 7/23/2014 13001 11.971 291 0.12 12.09 JB WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 192.5906 grams 195.8105 WEIGHT OF DISH 94.4323 grams 95.282 WEIGHT OF WET SAMPLE 98.1583 grams 100.5285 WEIGHT OF DISH AND DRIED SAMPLE 96.5866 grams 98.3507 WEIGHT OF DISH 94.4323 grams 95.282 WEIGHT OF DRIED SAMPLE 2.1543 grams 3.0687 WEIGHT OF DRIED SAMPLE: 2.1543 grams X 100 3.0687 WEIGHT OF WET SAMPLE: 98.1583 2.194721 grams 100.5285 3.052567 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 211 SOLIDS ANALYSIS BENCH SHEET ANALYST NOEL DATE EVENT 1 7/28/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1300 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS 3.95% 2.87% BEGINNING CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 1 11.00 SLOPE My/Ph % AGREEMENT 10.030 12.471 10.95 92,6 PH MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 7/28/2014 1300 6.65 29.6 0.15 6.80 BN 1ST 7/29/2014 1305 12.13 27.1 0.06 12.19 MJ 2ND 7/29/20141 15051 FINAL 12.1 27.61 CALIBRATION 0.091 12.19 MJ RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.00 12.46 11.03 92.5 FINAL 7/29/2014 15151 12.011 28.11 0.09 12.101 BN SOLIDS WORKSHEET HOLDING TANK WITH LIME WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 167.8 grams 152.6664 WEIGHT OF DISH 94.9081 grams 95.2858 WEIGHT OF WET SAMPLE 72.8919 grams 57.3806 WEIGHT OF DISH AND DRIED SAMPLE 97.7908 grams 96.9343 WEIGHT OF DISH 94.9081 grams 95.2858 WEIGHT OF DRIED SAMPLE 2.8827 grams 1.6485 WEIGHT OF DRIED SAMPLE: 2.8827 grams X 100 1.6485 WEIGHT OF WET SAMPLE: 72.8919 3,95476 grams 57.3806 2.872922 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 21 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 2 8/5/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 0900 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.64% 2.46% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.46 11.00 SLOPE My/Ph . % AGREEMENT 10.000 12.461 11.01 PH 95.1 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 8/5/2014 0915 7.1 24.4 -0.03 7.07 JB 1ST 8/5/2014 1300 12.16 26.7 0.03 12.19 JB 2ND 8/5/20141 1,5001 FINAL 12.21 26.81 CALIBRATION 0.03r12.231 JB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.02 12.47 11.01 92 FINAL 8/6/2014 13001 12.081 27.61 0.06 12.141 JB WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 192.8785 grams 195.1441 WEIGHT OF DISH 94.4357 grams 95.8178 WEIGHT OF WET SAMPLE 98.4428 grams 99.3263 WEIGHT OF DISH AND DRIED SAMPLE 96.0541 grams 98.26 WEIGHT OF DISH 94.4357 grams 95.8178 WEIGHT OF DRIED SAMPLE 1.6184 grams 2.4422 WEIGHT OF DRIED SAMPLE: 1.6184 grams X 100 2.4422 WEIGHT OF WET SAMPLE: 98.4428 1.6441 grams 1 99.3263 2.458766 % TOTAL 2014 e MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 221 SOLIDS ANALYSIS BENCH SHEET ANALYST WADE DATE EVENT 3 10/3/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1515 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.53% 3.13% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT "10030 12.47 10.92 PH 91.5 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 10/1/2014 1000 5.57 25.4 0.00 5.57 EW 1ST 10/3/2014 1520 12.05 26.9 0.06 12.11 EW 2ND 1 10/3/2014 17301 FINAL 12.081 27.1 CALIBRATION 0.061 12.141 JB , RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.04 12.48 10.95 92.4 FINAL 10/4/2014 15101 11.941 271 0.06 12.00 EW WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 162.2791 grams 199.1029 WEIGHT OF DISH 95.818 grams 99.6557 WEIGHT OF WET SAMPLE 66.4611 grams 99.4472 WEIGHT OF DISH AND DRIED SAMPLE 97.5027 grams 102.7727 WEIGHT OF DISH 95.818 grams 99.6557 WEIGHT OF DRIED SAMPLE . 1.6847 grams 3.117 WEIGHT OF DRIED SAMPLE: 1.6847 grams X 100 3.117 WEIGHT OF WET SAMPLE: 66.4611 Nool 2.534866 grams 99.4472 3.134327 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 221 SOLIDS ANALYSIS BENCH SHEET ANALYST BEHAN DATE EVENT 4 10/8/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 0820 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.88% 2.96% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.010 12.47 10.96 PH 91.6 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 10/8/2014 .0820 6.58 23.6 -0.03 6.55 DB 1ST 10/8/2014 1300 12.21 25.8 0.00 12.21 JB 2ND 10/8/2014 15001 FINAL 12.061 26.41 CALIBRATION 0.031 12.09 DB RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.02 12.46 10.99 90.4 FINAL 10/9/2014 13001 121 26.91 0.06 12.06 DB WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 197.5869 grams 195.8843 WEIGHT OF DISH 95.8193 grams 95.7661 WEIGHT OF WET SAMPLE 101.7676 grams 100.1182 WEIGHT OF DISH AND DRIED SAMPLE 97,735 grams 9-.6165 WEIGHT OF DISH 95.8193 grams 95.6557 WEIGHT OF DRIED SAMPLE 1.9157 grams 2.9608 WEIGHT OF DRIED SAMPLE: 1.9157 grams X 100 2.9608 WEIGHT OF WET SAMPLE: 101.7676 11110 1.8124261 grams 100.1182 2.957304 % TOTAL 2014 MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 221 SOLIDS ANALYSIS BENCH SHEET ANALYST ARMISTEAD DATE EVENT 5 10/14/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1000 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 1.97% 2.56% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 10.020 12.461 10.96 PH 91.6 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C 'EMP CORI ACT PH INITIALS INITIAL PH 10/13/2014 1000 4.37 26.5 0.06 4.43 RA 1ST 10/14/2014 1357 12.02 28 0.09 12.11 RA 2ND 10/14/2014 16101 FINAL 12.061 27.1 CALIBRATION 0.061 12.12-1 FS RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE My/Ph % AGREEMENT 9.99 12.46 11.03 91.6 FINAL 10/15/2014 14101 12.021 25.61 0 12.021 JB WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 171.4389 grams 177.5212 WEIGHT OF DISH 95.7641 grams 95.2852 WEIGHT OF WET SAMPLE 75.6748 grams 82.236 WEIGHT OF DISH AND DRIED SAMPLE 97.2585 grams 97.3897 WEIGHT OF DISH 95.7641 grams 95.2852 WEIGHT OF DRIED SAMPLE 1.4944 grams 2.1045 WEIGHT OF DRIED SAMPLE: 1.4944 grams X 100 2.1045 WEIGHT OF WET -SAMPLE: 75.6748 1.9747661 grams 1 82.236 2.559098 % TOTAL 2014 ' MARINE CORPS AIR STATION CHERRY POINT NC TASK ORDER 22 SOLIDS ANALYSIS BENCH SHEET ANALYST BRIGMAN DATE EVENT 6 11/3/2014 SAMPLE HOLDING TANK TYPE GRAB TIME 1220 VOLUME 100 WO/LIME W/LIME PERCENT SOLIDS BEGINNING 2.74% 3.88% CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER INITIAL 10.00 12.45 11.00 SLOPE MV/Ph % AGREEMENT "10050 12.47V 10.9 PH 90.7 MONITORING REPORT SAMPLE DATE TIME ANAL PH TEMP C EMP CORI ACT PH INITIALS INITIAL PH 11/3/2014 1230 5.83 22 0.09 5.92 DB 1ST 11/4/2014 1445 12.22 22.8 0.06 12.28 DB 2ND 1 11/4/2014-1 16451 FINAL 12.131 22.41 0.091 12.221 MJ CALIBRATION RECORD PH METER CALIBRATION ELECTRODE CHECK BUFFER FINAL 10.00 12.45 11.00 SLOPE MV/Ph % AGREEMENT 9.99 12.46 11.03 91.6 FINAL 11/5/2014 14501 11.961 22.91 0.06 12 021 DB WO/LIME W/LIME WEIGHT OF DISH AND WET SAMPLE 191.7303 grams 191.1566 WEIGHT OF DISH 95.2901 grams 95.7658 WEIGHT OF WET SAMPLE 96.4402 grams 95.3908 WEIGHT OF DISH AND DRIED SAMPLE 97.9344 grams 99.4646 WEIGHT OF DISH 95.2901 grams 95.7658 WEIGHT OF DRIED SAMPLE 2.6443 grams 3.6988 WEIGHT OF DRIED SAMPLE: 2.6443 grams X 100 3.6988 WEIGHT OF WET SAMPLE: 96.4402 2.7419061 grams 1 95.3908 3.877523 % TOTAL PATHOGEN/VECTOR ATTRACTION REDUCTION SUPPORTING DOCUMENTATION (ANAEROBIC DIGESTION): LAB ANALYSIS BENCH SHEETS C MCAS CHERRY POINT VOLATILE REDUCTION BENCHSHEET BENCH SHEET VOLATILES IN ANALYST SHIMMEL / CHARETTE DATE 3/8/2014 SAMPLE DISH # N/A WAS WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE ANALYST SAMPLE DISH # WO SHIMMEL / CHARETTE HT WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE VOLATILE REDUCTION CALCULATION WAS % VOLATILE WAS % VOLATILE TYPE TIME IN OVEN 1642 TIME OUT OVEN 1642 193.8720 GRAMS TOTAL HOURS IN OVEN 24 95.8138 GRAMS 98.0582 GRAMS CALCULATIONS 96.4623 GRAMS DRIED SAMPLE 0.6485 GMSX100 95.8138 GRAMS WET SAMPLE 98.0582 GMSX100 0.6485 GRAMS IGNITED SAMPLE 0.4612 GMSX100 96.4623 GRAMS DRIED SAMPLE 0.6485 GMSX100 96.0011 GRAMS 0.4612 GRAMS %TOTAL SOLIDS 1 0.6613 % VOLATILE SOLIDS 1 71.1180 VOLATILES OUT DATE 3/8/2014 TYPE TIME IN OVEN 1639 TIME OUT OVEN 1639 192.8546 GRAMS TOTAL HOURS IN OVEN 94.4297 GRAMS 98.4249 GRAMS CALCULATIONS 96.1004 GRAMS DRIED SAMPLE 1.6707 GMSX100 94.4297 GRAMS WET SAMPLE 98.4249 GMSX100 1.6707 GRAMS IGNITED SAMPLE 0.8823 GMSX100 96.1004 GRAMS DRIED SAMPLE 1.6707 GMSX100 95.2181 GRAMS 0.8823 GRAMS %TOTAL SOLIDS 1.697436 VOLATILE SOLIDS 52.8102 MINUS HOLDING TANK %VOL 1 0.531 0.18 INUS WAS % VOL X HT % VOL REDUCTION 1 54.55 Pathogen Reduction Compliance per 15A NCAC 02T.1106(C)(2) 40 -- - - - - — — -- -... -- - x I 35 30 I i t 25 �o d E 20 a f- 15 10 5 0 0 20 40 60 . 80 100 120 140 Residence Time (days) ♦ Aerobic (.1106(C)(2)(a)) ■ Anaerobic (.1106(C)(2)(c)) — — — Aerobic Compliance Line Anaerobic Compliance Line X 8-Mar MCAS CHERRY POINT VOLATILE REDUCTION BENCHSHEET BENCH SHEET VOLATILES IN ANALYST JEB/ M1 DATE 3/19/2014 SAMPLE DISH #-J RAS WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE TYPE GRAB TIME IN OVEN 1230 TIME OUT OVEN r 1230 141.8501 GRAMS TOTAL HOURS IN OVEN 24 95.7583 GRAMS 46.0918 GRAMS CALCULATIONS 96.1175 GRAMS DRIED SAMPLE 0.3592 GMSX100 95.7583 GRAMS WETSAMPLE 46.0918 GMSX100 0.3592 GRAMS IGNITED SAMPLE 0.2251 GMSX100 96.1175 GRAMS DRIED SAMPLE 0.3592 GMSX100 95.8924 GRAMS 0.2251 GRAMS %TOTAL SOLIDS 1 0.7793 VOLATILE SOLIDS 1 62.6670 VOLATILES OUT ANALYST JEB/ MJ DATE 3/19/2014 SAMPLE DISH # DIG 3 WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE VOLATILE REDUCTION CALCULATION WAS % VOLATILE WAS % VOLATILE TYPE GRAB TIME IN OVEN 1630 TIME OUT OVEN 1630 110.8268 GRAMS TOTAL HOURS IN OVEN 24 104.2403 GRAMS 6.5865 GRAMS CALCULATIONS 106.2584 GRAMS DRIED SAMPLE 2.0181 GMSX100 104.2403 GRAMS WET SAMPLE 6.5865 GMSX100 2.0181 GRAMS IGNITED SAMPLE r 1.0102 GMSX100 106.2584 GRAMS DRIED SAMPLE 2.0181 GMSX100 105.2482 GRAMS 1.0102 GRAMS %TOTALSOLIDS 1 30.63995 VOLATILE SOLIDS 1 50.05698 MINUS HOLDING TANK % VOL 1 0.501 0.13 MINUS WAS % VOL X HT % VOL REDUCTION 1 40.29 45 40 35 30 ai 25 co a E 20 d Pathogen Reduction Compliance per 15A NCAC 02T.1106(C)(2) 15 \ 10 -- -- - --- — - --- - - ---- - - -- I-- - --- \' \ 5 - - - - - - -- - - - - - - —I -- -- - { f \ 0 0 20 40 60 80 100 120 140 Residence Time (days) ♦ Aerobic (.1106(C)(2)(a)) ■ Anaerobic (.1106(C)(2)(c)) _ _ Aerobic Compliance Line Anaerobic Compliance Line X 19-Mar MCAS CHERRY POINT VOLATILE REDUCTION BENCHSHEET BENCH SHEET VOLATILES IN ANALYST JEB DATE 3/28/2014 SAMPLE DISH # RAS WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE TYPE GRAB TIME IN OVEN 1230 TIME OUT OVEN 1230 145.8763 GRAMS TOTAL HOURS IN OVEN 24 94.8996 GRAMS 50.9767 GRAMS CALCULATIONS 95.3896 GRAMS DRIED SAMPLE 0.49 GMSX100 94.8996 GRAMS WET SAMPLE 50.9767 GMSX100 0.49 GRAMS IGNITED SAMPLE 0.3108 GMSX100 95.3896 GRAMS DRIED SAMPLE 0.49 GMSX100 95.0788 GRAMS 0.3108 GRAMS TOTAL SOLIDS 1 0.9612 % VOLATILE SOLIDS 1 63.4286 VOLATILES OUT ANALYST JEB DATE 3/28/2014 SAMPLE DIG 3 TYPE ' GRAB DISH # TIME IN OVEN 1630 TIME OUT OVEN 1630 WEIGHT OF DISH AND WET SAMPLE 131.6827 GRAMS TOTAL HOURS IN OVEN 1 24 WEIGHT OF DISH 95.808 GRAMS WEIGHT OF WET SAMPLE 35.8747 GRAMS CALCULATIONS WEIGHT OF DISH AND DRIED SAMPLE 99.6868 GRAMS DRIED SAMPLE 3.8788 GMSX100 WEIGHT OF DISH 95.808 GRAMS WETSAMPLE 35.8747 GMSX100 WEIGHT OF DRIED SAMPLE 3.8788 GRAMS IGNITED SAMPLE 2.0045 GIVISX100 WEIGHT OF DISH AND DRIED SAMPLE 99.6868 GRAMS DRIED SAMPLE 3.8788 GMSX100 WEIGHT OF DISH AND IGNITED SAMPLE 97.6823 GRAMS WEIGHT'OF IGNITED SAMPLE 2.0045 GRAMS VOLATILE REDUCTION CALCULATION WAS % VOLATILE WAS % VOLATILE %TOTALSOLIDS 1 10.81208 VOLATILE SOLIDS 1 51.67835 MINUS HOLDING TANK % VOL 1 0.521 0.12 NUS WAS % VOL X HT % VOL REDUCTION 1 38.34 Pathogen Reduction Compliance per 15A NCAC 02T.1106(C)(2) 4540 ----- --------T —..— --f --- --- ---- -- j { � j 35 30 ---- - j -- _.. - - --- — - 25 -- ---- - ���_.________ ___ _____ �__—`-- --_-- _ __-- -- ..—_ __ _ ___ _ _ ♦ Aerobic (.1106(C)(2)(a)) � . I ■ Anaerobic (.1106(C)(2)(c)) 20 Aerobic Compliance Line Anaerobic Compliance Line 15 X 28-Mar 10 -- --- — --- -- - i — — --- ----- — o ``I` ` — --- -- ---- _ — — 5 -- -- ---- -- - — - -- --- - ----- —� - -- ---- — I 0 0 20 40 60 80 100 120 140 Residence Time (days) MCAS CHERRY POINT VOLATILE REDUCTION BENCHSHEET BENCH SHEET VOLATILES IN ANALYST RILEY DATE 3/31/2014 SAMPLE DISH # RAS WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE TYPE GRAB TIME IN OVEN 1110 TIME OUT OVEN 1145 144.9853 GRAMS TOTAL HOURS IN OVEN 24.5 95.8124 GRAMS 49.1729 GRAMS CALCULATIONS 96.1202 GRAMS DRIED SAMPLE 0.3078 GMSX100 95.8124 GRAMS WET SAMPLE 49.1729 GMSX100 0.3078 GRAMS IGNITED SAMPLE 0.1875 GMSX100 96.1202 GRAMS DRIED SAMPLE 0.3078 GMSX100 95.9327 GRAMS 0.1875 GRAMS % TOTAL SOLIDS 1 0.6260 % VOLATILE SOLIDS 1 60.9162 VOLATILES OUT ANALYST BEHAN DATE 4/1/2014 SAMPLE DIG 3 TYPE GRAB DISH # �.. TIME IN OVEN 1125 TIME OUT OVEN 1155 WEIGHT OF DISH AND WET SAMPLE WEIGHT OF DISH WEIGHT OF WET SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH WEIGHT OF DRIED SAMPLE WEIGHT OF DISH AND DRIED SAMPLE WEIGHT OF DISH AND IGNITED SAMPLE WEIGHT OF IGNITED SAMPLE VOLATILE REDUCTION CALCULATION WAS % VOLATILE WAS % VOLATILE 109.453 GRAMS TOTAL HOURS IN OVEN 24.5 95.7603 GRAMS 13.6927 GRAMS CALCULATIONS 101.1621 GRAMS DRIED SAMPLE 5.4018 GMSX100 95.7603 GRAMS WET SAMPLE 13.6927 GMSX100 5.4018 GRAMS IGNITED SAMPLE 0.8381 GMSX100 101.1621 GRAMS DRIED SAMPLE 5.4018 GMSX100 100.324 GRAMS 0.8381 GRAMS %TOTAL'SOLIDS 1 39.45022 % VOLATILE SOLIDS 1 15.5152 MINUS HOLDING TANK % VOL 1 0.161 0.45 MINUS WAS % VOL X HT % VOL % REDUCTION 1 88.22 Pathogen Reduction Compliance per 15A NCAC 02T.1106(C)(2) 45 40 35 30 u 25 3 m d E 20 a 15 10 5 0 ' 0 20 40 60 80 100 120 140 Residence Time (days) ♦ Aerobic (.1106(C)(2)(a)) ■ Anaerobic (.1106(C)(2)(c)) — — — Aerobic. Compliance Line Anaerobic Compliance Line SIC 31-Mar STANDARD SOIL FERTILITY ANALYSIS REPORT (3 COPIES) �aceAnalytical www pacelabs.com ANALYTICAL RESULTS Project: Fieldsl-7 Pace Project No.: 92203926 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS FIELD #1 Lab ID: 92203926001 Collected: 06/03/14 10:00 Received:. 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 511 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7440-70-2 2.0 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7440-50-8 132 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7439-95-4 5.4 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7439-96-5 ND mg/kg 482 1 06/06/14 16:10 06/10/14 00:58 7440-09-7 ND mg/kg 482 1 06/06/14 16:10 06/10/14 0d:58 7440-23-5 3.3 mg/kg 0.96 1 06/06/14 16:10 06/10/14 00:58 7440-66-6 Analytical Method: ASTM D2974-87 21.4 % 0.10 1 06/18/14 16:36 Analytical Method: EPA 9045 6.3 Sid. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 121 mg/kg 5.8 1 06/16/1413:47 7723-14-0 M1 Sample: MCAS FIELD #2 Lab ID: 92203926002 Collected: 06/03/14 10:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Date: 07/08/2014 09:48 AM Analytical Method: EPA 6010 Preparation Method: EPA3050 1200 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7440-70-2 2.6 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7440-50-8 126 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7439-95-4 6.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7439-96-5 ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-09-7 ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-23-5 5.4 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:01 7440-66-6 Analytical Method: ASTM D2974-87 14.4 % 0.10 1 06/18/14 16:37 Analytical'Method: EPA 9045 6.4 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 35.2 mg/kg 2.2 1 06/16/14 13:51 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1 Page 4 of 15 lacAAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: Fieldsl-7 Pace Project No.: 92203926 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS FIELD #3 Lab ID: 92203926003 Collected: 06/03/14 10:30 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 799 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7440-70-2 2.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7440-50-8 99.2 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7439-95-4 6.1 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7439-96-5 ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-09-7 ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-23-5 5.6 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:05 7440-66-6 Analytical Method: ASTM D2974-87 16.0 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 6.3 Sid. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 34.1 mg/kg 2.1 1 06/1611413:51 7723-14-0 Sample: MCAS FIELD #4 Lab ID: 92203926004 Collected: 06/03/14 10:45 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Calcium 4060 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7440-70-2 Copper 15.5 mg/kg 0.57 1 06/06/14 16:10 06/10/14 01:09 7440-50-8 Magnesium 217 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7439-95-4 Manganese 36.2 mg/kg . 0.57 1 06/06/14 16:10 06/10/14 01:09 7439-96-5 Potassium ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-09-7 Sodium ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-23-5 Zinc 32.6 mg/kg 1.1 1 06/06/14 16:10 06/10/14 01:09 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 30.8 % 0.10 1 06/18/14 16:37 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.2 Std, Units 0.10 1 06/05/14 16:57 365.1 Phosphorus, Total Analytical Method: EPA365.1 Phosphorus 864 mg/kg 34.4 5 06/16/14 14:23 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 09:48 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 aclet, lytical www.pacelabs.com ANALYTICAL RESULTS Project: Fieldsl-7 Pace Project No.: 92203926 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: WAS FIELD #5 Lab ID: 92203926005 Collected: 06/03/14 11:00 Received: 06/04/14 09:40 Matrix: Solid Parameters 6010 MET ICP' Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 6010 Preparation Method: EPA 3050 169 mg/kg 7.2 1 06/13/14 15:50 06116/1416:01 7440-70-2 0.96 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7440-50-8 123 mg/kg 7.2 1 06/13/14 15:50 06/16/14 16:01 7439-95-4 M1 2.8 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7439-96-5 ND mg/kg 361 1 06/13/14 15:50 06/16/14 16:01 7440-09-7 ND mg/kg 361 1 06/13/14 15:50 0611611416:01 7440-23-5 2.3 mg/kg 0.72 1 06/13/14 15:50 06/16/14 16:01 7440-66-6 Analytical Method: ASTM D2974-87 14.4 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 5.4 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 36.8 mg/kg 4.9 1 06/16/14 13:53 7723-14-0 Sample: MCAS FIELD #7 Lab ID: 92203926006 Collected: 06/03/14 11:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Date: 07/08/2014 09:48 AM Analytical Method: EPA 6010 Preparation Method: EPA3050 2050 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7440-70-2 8.2 mg/kg 0.27 1 06/13/14 15:50 06/16/14 16:10 7440-50-8 223 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7439-95-4 20.7 mg/kg 0.27 1 06/13/14 15:50 06/16/14 16:10 7439-96-5 ND mg/kg 268 1 06/13/14 15:50 06/16/14 16:10 7440-09-7 ND mg/kg 268 1 06/13/14 15:50 06/1611416:10 7440-23-5 12.1 mg/kg 0.54 1 06/13/14 15:50 06/16/14 16:10 7440-66-6 Analytical Method: ASTM D2974-87 6.9 % 0.10 1 06/18/1416:37 Analytical Method: EPA 9045 6.9 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA365.1 723 mg/kg 23.3 5 06/16/14 14:25 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 Page 1 of 4 Report Number: 14-156-0628 Y . Account Number: 05755 aleastert�.carn Send To: PACE ANALYTICAL CHARLOTTE (for Tat TABITHA M DACAL 9800 KINCEY AVE - STE 100 HUNTERSVILLE NC 28078 n.ta Roraivart• nF/fly/9f11A natp Of Annlvsis' 06/06/2014 A&L Eastem Laboratories 7621 Whitepine Road Richmond, Yrginia 23237 (804) 743.9401 Fax (004) 271.6446 Grower: 92203926 FIELDS 1-7 MCAS SOIL ANALYSIS REPORT Date Of Reoort: 06/06/2014 Submitted By: TABITHA M DACAL Farm ID: Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number ° /° Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate p H Index meg1100g meq/100g 1 18297 1.3 L 70 58 H 46 L 46 L 643 H 16 VL 6.4 0.4 4.2 MCAS I NC = 48 NC = 24 2 15 L 34 VL 42 VL 1027 H 16 VL 18298 2.8 M 97 6.2 0.8 6.4 MCAS NC = 12 NC = 17 3 18299 2.8 M 97 17 L 34 VL 128 VL 922 H 17 VL 5.9 6.83 1.0 F6.0 MCAS NC = 14 NC = 17 4 18300 3.4 M gg 1351 VH 56 VL 106 L 2597 VH 18 VL 7.4 0.0 14.1 MCAS NC = 292 NC = 29 5 18301 1.5 L 75 10 VL 29 VL 141 L 394 M 123 L 5.3 6.82 1.1 3.6 MCAS NC = 8 NC = 15 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl Al Field ID % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm- 1 8 VL 1.6 L 5 L 100 VH 1.5 M 0.1 VL WAS 2.8 9.1 76.5 1.7 8.8 NC = 17 NC = 40.0 1 NC = 31 1 1 NC = 75.0 2 7 VL 1.6 L 5 L VH 1.5 M 0.4 L MCAS 1.4 5.5 80.2 1.1 12.2 NC = 15 NC = 40.0 NC = 31 1126 NC = 75.0 3 L 1.8 L 4 L VH 1.8 H VL MCAS 1.5 3.9 76.8 1.2 17.3 113 NC = 27 NC = 45.0 NC = 25 1149 NC = 90.0 10.2 4 L 21.4 VH 9 L VH VH M MCAS 1.0 6.3 92.1 0.6 0.0 113 NC = 27 NC = 535.0 NC = 56 �399 17.3 NC = 365.0 10.8 5 9 VL L 3 VL VH 1.2 M VL MCAS 2.1 9.5 54.7 2.8 31.1 11.4 NC=19 NC=35.0 NC=19 �304 NC=60.0 10.2 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. flip Enc GpoMg/ H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. i (j C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 4 Report Number: 14-156-0628 vftyl, A L Eastern Laboratories Account Number: 05755 141, 7621 Whitepine Road Richmond, Virginia 23237 {8041,743.301 Fax {BOAI271-G4d6 wwW.aieastern.cor1 Send To: PACE ANALYTICAL CHARLOTTE (for Tat Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KINCEYAVE - STE 100 MCAS HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N PZO s K O z M 9 S Zn Mn Fe Cu B Field JD Tons Tons/A Ib/A Ib/A Ib/A IbIA Ib/A Ib/A IbIA Ib/A IblA Ib/A 1 Hay 4 0.0 50 30 160 34 21 2.5 3 0 0 0.5 MCAS 2 Hay 4 0.0 50 78 160 38 22 2.5 3 0 0 0 MCAS 3 Hay 4 0.8 50 74 160 52 16 2.0 3 0 0 0.5 MCAS 4 Hay 4 0.0 50 0 180 0 16 0 3 0 0 0 MCAS 5 Hay 4 0.8 50 89 160 39 20 2.5 4 0 0 0.5 MCAS Comments: Sample(s) :2 Crop: Hay Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 2,3,4,5 Crop: Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. Sample(s) : 3,5 Crop: Hay Apply dolomitic lime to raise pH and improve the magnesium level. Boron recommendations are on a broadcast basis. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 4 Crop: Hay Cation Exchange Capacity may be over -estimated due to high pH and free lime in the soil. Use ammonium sulfate as all or portion of the N requirement to reduce pH. Use K-Mag as part of the potassium source to increase magnesium level "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4� Report Number: 14-156-0628 v Account Number: 05755 MYwAleastent.com Send To: PACE ANALYTICAL CHARLOTTE (for Tat TABITHA M DACAL 9800 KINCEY AVE - STE 100 HUNTERSVILLE NC 28078 nary Paraivo i• nF/nF/9n1A Data Of Analvsis: n6/176/2014 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginla 23237 (Bo4) 743 9401 Fax (004) 2711-6614G Grower: 92203926 FIELDS 1-7 MCAS SOIL ANALYSIS REPORT Date Of Report: 06/06/2014 Submitted By: TABITHA M DACAL Farm ID: Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number ° /° Rate Ibs1A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g 7 18302 5.1 H 132 342 VH 59 VL 94 VL 2522 VH 18 VL 6.9 0.2 13.8 MCAS NC = 285 NC = 30 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl AI Field ID ° /° % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate'ppm Rate ms/cm Rate ppm Rate ppm 7 13 L 6.9 H 8 L 337 VH 6.5 VH 0.6 M WAS 1.1 5.7 91.4 0.6 1.4 NC = 27 NC = 172.5 NC = 50 NC = 325.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. PW« H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 4 of 4`� Report Number: 14-156-0628 A&L Eastem Laboratories . v Account Number: 05755 _ 7621 Wbitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (8041271.8446 www.aleasterti.com + Send To: PACE ANALYTICAL CHARLOTTE (for Tat Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KIN CEYAVE - STE 100 MCAS HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N PZ05 KO Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A VA . Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A VA 7 Hay 4 0.0 50 0 180 0 16 0 3 0 0 0 MCAS Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary TRIENNIAL GROUNDWATER MONITORING REPORTS (3 COPIES) �j4le A nalytic. al t www.pac-labs.com 1 ANALYTICAL RESULTS Project: Fieldsl-7 Pace Project No.: 92203926 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: ICAS FIELD #1 Lab ID: 92203926001 Collected: 06/03/14.10:00 Received:. 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed , CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method:. EPA 3050 511 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7440-70-2 2.0 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7440-50-8 132 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7439-95-4 5.4 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7439-96-5 ND mg/kg 482 1 06/06/14 16:10 06/10/14 00:58 7440-09-7 ND mg/kg 482 1 06/06/14 16:10 06/10/14 00:58 7440-23-5 3.3 mg/kg 0.96 1 06/06/14 16:10 06/10/14 00:58 7440-66-6 Analytical Method: ASTM D2974-87 21.4 % 0.10 1 06/18/14 16:36 Analytical Method: EPA 9045 6.3 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 121 mg/kg 5.8 - 1 06/16/1413:47 7723-14-0 M1 Sample: MCAS FIELD #2 Lab ID: 9,2203926002 Collected: 06/03/14 10:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results . Units Report Limit DF Prepared Analyzed CAS No. . Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050 Calcium 1200 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7440-70-2 Copper 2.6 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7440-50-8 Magnesium 126 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7439-95-4 Manganese 6.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7439-96-5 Potassium ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-09-7 Sodium ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-23-5 Zinc 5.4 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:01 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 14.4 % 0.10 1 06/18/14 16:37 9045 pH Soil Analytical'Method: EPA 9045 pH at 25 Degrees C 6.4 Std. Units 0.10 1 06/0511.4 16:57 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 35.2 mg/kg 2.2 1 06/16/14 13:51 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 09:48 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 0 �Y✓- .aceAnalXical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Fieldsl-7 Pace Project No.: 92203926 Sample: 1V1CAS FIELD #3 Lab ID: 92203926003 Collected: 06/03/14 10:30 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Methotl: EPA 6010 Preparation Method: EPA 3050 Calcium 799 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7440-70-2 Copper 2.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7440-50-8 Magnesium 99.2 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7439-95-4 Manganese 6.1 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7439-96-5 Potassium ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-09-7 Sodium ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-23-5 Zinc 5.6 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:05 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 16.0 % 0.10 1 06/18/14 16:37 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 6.3 Std. Units 0.10 1 06/05/14 16:57 365.1"Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 34.1 mg/kg 2.1 1 06/16/1413:51 7723-14-0 Sample: MCAS FIELD #4 Lab ID: 92203926004 Collected: 06/03/14 10:45 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Date: 07/08/2014 09:48 AM Analytical Method: EPA 6010 Preparation Method: EPA 3050 4060 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7440-70-2 15.5 mg/kg 0.57 1 06/06/14 16:10 06/10/14 01:09 7440-50-8 217 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7439-95-4 36.2 mg/kg . 0.57 1 06/06/14 16:10 06/10/14 01:09 7439-96-5 ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-09-7 ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-23-5 32.6 mg/kg 1.1 1 06/06/14 16:10 06/10/14 01:09 7440-66-6 Analytical Method: ASTM D2974-87 30.8 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 7.2 Std.-Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 864 mg/kg 34.4 5 06/16/14 14:23 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 laceAnalytical ..pacelabs.com t I ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Fieldsl-7 Pace Project No.: 92203926 Sample: MCAS FIELD #5 Lab ID: 92203926005 Collected: 06/03/14 11:00 Received: 06/04,114 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF . Prepared Analyzed CAS No. Qua[ 6010 MET ICP` Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 169 mg/kg 7.2 1 06/13/14 15:50 06/16/14 16:01 7440-70-2 0.96 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7440-50-8 123 mg/kg 7.2 1 06/13/14 15:50 06/16/14 16:01 7439-95-4 M1 2.8 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7439-96-5 ND mg/kg 361 1 06113/1415:50 06/16/14 16:01 7440-09-7 ND mg/kg 361 1 06/13/14 15:50 06/16/14 16:01 7440-23-5 2.3 mg/kg 0.72 1 06/13/14 15:50 06/16/14 16:01 7440-66-6 Analytical Method: ASTM D2974-87 14.4 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 5.4 Std. Units 0.10 1 06/05/14 16:57' Analytical Method: EPA 365.1 36.8 mg/kg 4.9 1 06/16/1413:53 7723-14-0 Sample: MCAS FIELD #7 Lab ID: 92203926006 Collected: 06/03/14 11:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Date: 07/08/2014 09:48 AM Analytical Method: EPA 6010 Preparation Method: EPA 3050 2050 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7440-70-2 8.2 mg/kg 0.27 1 06/13/14 15:50 06/16/14 16:10 7440-50-8 223 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7439-95-4 20.7 mg/kg 0.27 1 '06/13/14 15:50 06/16/14 16:10 7439-96-5 ND mg/kg 268 1 06/13/14 15:50 06/16/14 16:10 7440-09-7 ND mg/kg 268 1 06/13/14 15:50 06/16/14 16:10 7440-23-5 12.1 mg/kg 0.54 1 06/13/14 15:50 06/16/14 16:10 7440-66-6 Analytical Method: ASTM D2974-87 6.9 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 6.9 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 723 mg/kg 23.3 ' 5 06/16/14 14:25 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 Page 1 of 4 Report Number: 14-156-0628 ) Y Account Number: 05755 Send To: PACE ANALYTICAL CHARLOTTE (for Tat 'aleasterlt.com TABITHA M DACAL 9800 KINCEYAVE - STE 100 HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Analysis: 06/06/2014 A&L EastLaboratories 7621 Whitepine Road Richmond, Virginia 23237 (004) 743.9401 Fa%(004) 271-13446 Grower: 92203926 FIELDS 1-7 MCAS SOIL ANALYSIS REPORT Date Of Report: 06/06/2014 Submitted By: TABITHA M DACAL Farm ID: Analytical Method(s): Mehlich 3 Sample ID Lab Organic Matter'••, Phosphorus Potassium'. Magnesium' Calci6m:.',11 Sodium pH. Acidity C.E.0 Field ID Number % Rate ENR Mehlich 3 Reserve K : Mg -Ca Na Soil Buffer H- lbs/A - ppm Rate -ppm Rate ppm Rate pp m -Rate ppm � ,,Rate. ppm Rate pH Index megl1009 meq/100g 1 18297 1.3 L 70 58, H 46 L 46 L 643 H 16 VL WAS NC = 48 NC = 24 6.4 0.4 4.2 2 18298 2.8 M 97 . 15 L 34 VL 42 VL. 1027 H 16 VL MCAS NC = 12 NC = 17 6.2 0.8 1 6.4 j 3 18299 2.8 M 97 17 L 34 VL 28 VL 922 H 17 VL MCAS NC = 14 NC = 17 5.9 6:83 1.0 6.0 4 18300 3.4 M 98 351 VH 56VL 106 L 2597 VH 18 VL MCAS NC = 292 NC = 29 7 4 0.0 14.1 5 18301 1.5 L 75 10 VL 29 VL 41 L 394 M 23 L MCAS NC=8 NC=15 5.3 6.82 1.1 3.G Sample Percent Base Saturation •' .' 'Nitrate Sulfur Zinc. Manganese -'Iron:' Copper Boron Soluble Sans , Chloride Aluminum;: ID Field ID K Mg Ca ;' Na H NO3N S Zn, Mn Fe'--.- � - "-,;.Cu B 5S - Cl AI . % ppm Rate ppm Rate, pp m .. Rate pprri Rate ppm Rate ppm: •� Rate pPrrt - Rate ms/cm Rate ppm Rate ppm;. 1 2.8 9.1 76.5 1.7 8.8 8 VL 1.6 L 5 L 100 VH 1.5 M 0.1 VL MCAS. NC = 17 NC = 40.0 NC = 31 NC = 75.0 2 1.4 5.5 80.2 1.1 12.2 7 VL 1.6 L 5 L 126 VH 1.5 M L MCAS NC=15 NC=40.0 NC=31 NC=75.0 10.4 FMCAS 1.5 3.9 76.8 1.2 17.3 13 L 1.8 L 4 L 149 VH 1.8 H 0.2 VL NC=27 NC=45.0 NC=25 NC=90.0 4 1.0 6.3 92.1 0.6 0.0 113 L 21.4 VH 9 L '= 1399 VH 17.3 VH 10.8 M MCAS NC = 27 NC = 535.0 NC 56 NC = 365.0 5 2.1 9.5 54.7 2.8 31.1 9 VL 11.4 L 3 VL 1304 VH 1.2 M 10.2 VL MCAS NC=19 NC=35.0 NC=19 NC=60.0 vdiues un mis iepurt represent me plant avaname nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (VeryLow), L (Low), M (Medium), (pounds per acre), ms/am (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Pam« m G Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Pauric McGroary Page 2 of 4 Report Number: 14-156-0628 uM A L Eastern Laboratories Account Number: 05755 ATLA: 7621 Whitepine Road Richmond, Virginia23237 (904) 743.9401 Fa%(8041271 G446 »L t9 www.altastern,coin Send To: PACE ANALYTICAL CHARLOTTE (for Tat Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KINCEYAVE - STE 100 MCAS HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS Sample ID Yield.Goal ' "Lime Nitrogen Phosphate Potash "' Magnesium Sulfur Zinc Manganese "' Iron , Copper Boron Field ID Intended Crop Tons Tons/A N` P205 KZO Mg . ' S Zn Mn Fe Cu B . ^Ib/A. Ib/A Ib/A Ib/A Ib/A Ib/A IblA Ib/A Ib/A IlilA FMCASHay 4 0.0 50 30 160 34 21 2.5 3 0 0 0.5 2 MCAS Hay 4 0.0 50 78 160 38 22 2.5. 3 0 0 0 3 MCAS Hay 4 0.8 50 T74 160 52 16 2.0 3 0 0 0.5 4 MCAS Hay 4 0.0 50 0 180 0 16 0 3 0 0 0 5 MCAS Hay 4 0.8 50 . ] 89 160 39 20 2.5 4 0 0 0.5 VVI I I I I ICI I Lb. Sample(s) : 2 Crop: Hay Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 2,3,4,5 Crop: Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. Sample(s) : 3,5 Crop: Hay Apply dolomitic lime to raise pH and improve the magnesium level. Boron recommendations are on a broadcast basis. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 4 Crop: Hay Cation Exchange Capacity may be over -estimated due to high pH and free lime in the soil. Use ammonium sulfate as all or portion of the N requirement to reduce pH. Use K-Mag as part of the potassium source to increase magnesium level "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4--;... ,.w. Report Number: 14-156-0628 Y Account Number: 05755 Y www,aleastent.com Send To: PACE ANALYTICAL CHARLOTTE (for Tat TABITHA M DACAL 9800 KINCEYAVE - STE 100 HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Analvsis: 06/06/2014 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (004) 743-9401 Fax (004) 271-6446 Grower: 92203926 FIELDS 1-7 MCAS SOIL ANALYSIS REPORT Date Of Rannrt- 0fi/nr,19n1f Submitted By: TABITHA M DACAL Farm ID: Analytical Method(s): Mehlich 3 Sample ID Lab Organic Matter Phosphorus Potassium Magnesium: Calcium Sodium pH Acidity -C:E.0 Field ID Number • . . ENR % Mehlich3 - Reserve K Mg' Ca Na Soil Buffer H - - -":.Rate :Ibs/A ppm Rate. ppm Rate ppm Rate m Rate pp ppm Rate ppm pH Index - meq/100g ,ineq/100g 7 18302 5.1 H 132 342' VH 59 VL 94 VL 2522 VH 18 VL MCAS NC = 285 NC = 30 6.9 0.2 13.8 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron •' Soluble Salts Chloride`. ,.Aluminum Sample ID " Field ID K Mg ; Ca Na H NON S Zn Mn Fe - Cu B = SS Cl Al % % % " %" % ppm Rate ppm Rate ppm Rate ppm. Rate ppm,'Rate ppm Rate 'ppm •Rate mslcm Rate ppm Rate ppm '. 7 13 L 6.9 H 8 L 337 VH 6.5 VH 0.6 M 1.1 5.7 91.4 0.6 1.4 MCAS NC=27 NC=172.5 NC=50 NC=325.0 values on tnis report represent the plant available nutrients in the soil. Rating after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). ENR - Estimated Nitrogen Release. C.E.C. - Cation Exchange Capacity. Explanation of symbols: %.(percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by: Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. 1 AWra �1 Pauric McGroary Page 4 of 4 ' Report Number: 14-156-0628 Y ,� � Eastem La or��ories Account Number:05755 X,. .-�.--- _ 7621 whitepine Road Richmond; Virginia 23237 (804) 743.9401 Fax (004) 271<6446 wwmaleastenl.com Send To: PACE ANALYTICAL CHARLOTTE (for Tat Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KIN CEYAVE - STE 100 MCAS HUNTE.RSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS Sample ID Yield Goal =Lime Nitrogen Phosphate Potash Magnesium Sulfur _ Zinc Manganese Iron Copper Boron Field ID Intended Crop Tons Tons/A N P205 "K20 Mg _ S Zn- Mn Fe Cu B Ib/A Ib/A . Ib/A :, Ib/A lb/A. Ib/A Ib/A MIA Ib/A- Ib/A 7 MCAS Hay .4 0.0 507— 0 180 0 16 0 3 0 07 0 %,ommenl:s: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the p�Jcc I'•� �� work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary TRIENNIAL GROUNDWATER MONITORING REPORTS (3 COPIES) aceAnalytical. www.pacelabs.com ANALYTICAL RESULTS Project: Fieldsl-7 Pace Project No.: 92203926 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MC FIELD 1-1 Lab IC: 92203926001 Collected: 06,103/14 10:00 Received:. 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 511 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7440-70-2 2.0 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7440-50-8 132 mg/kg 9.6 1 06/06/14 16:10 06/10/14 00:58 7439-95-4 5.4 mg/kg 0.48 1 06/06/14 16:10 06/10/14 00:58 7439-96-5 ND mg/kg 482 1 06/06/14 16:10 06/10/14 00:58 7440-09-7 ND mg/kg 482 1 06/06/14 16:10 06/10/14 00:58 7440-23-5 3.3 mg/kg 0.96 1 06/06/14 16:10 06/10/14 00:58 7440-66-6 Analytical Method: ASTM D2974-87 21A % 0.10 1 06/1811416:36 Analytical Method: EPA 9045 6.3 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 121 mg/kg 5.8 - 1 06116/1413:47 7723-14-0 M1 Sample: MCAS FIELD #2 Lab ID: 92203926002 Collected: 06/03/14 10:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Date: 07/08/2014 09:48 AM Analytical Method: EPA 6010 Preparation Method: EPA 305b 1200 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7440-70-2 2.6 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7440-50-8 126 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:01 7439-95-4 6.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:01 7439-96-5 ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-09-7 ND mg/kg 340 1 06/06/14 16:10 06/10/14 01:01 7440-23-5 5.4 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:01 7440-66-6 Analytical Method: ASTM D2974-87 14.4 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 6.4 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 35.2 mglkg 2.2 1 06116/1413:51 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4. of 15 �- ai eAnalytical www.pacbiabs.com i ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Fieldsl-7 Pace Project No.: 92203926 Sample: � ACAS FIELD #3 Lab ID: 92203926003 Collected: 06/03/14 10:30 Received: 0610A 14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Copper Magnesium Manganese Potassium Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 799 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7440-70-2 2.9 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7440-50-8 99.2 mg/kg 6.8 1 06/06/14 16:10 06/10/14 01:05 7439-95-4 6.1 mg/kg 0.34 1 06/06/14 16:10 06/10/14 01:05 7439-96-5 ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-09-7 ND mg/kg 342 1 06/06/14 16:10 06/10/14 01:05 7440-23-5 5.6 mg/kg 0.68 1 06/06/14 16:10 06/10/14 01:05 7440-66-6 Analytical Method: ASTM D2974-87 16.0 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 6.3 Std. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 34.1 mg/kg 2.1 1 06/16/1413:51 7723-14-0 Sample: MCAS FIELD #4 Lab ID: 92203926004 Collected: 06/03/14 10:45 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units . Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Calcium 4060 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7440-70-2 Copper 15.5 mg/kg 0.57 1 06/06/14 16:10 06/10/14 01:09 7440-50-8 Magnesium 217 mg/kg 11.5 1 06/06/14 16:10 06/10/14 01:09 7439-95-4 Manganese 36.2 mg/kg . 0.57 1 06/06/14 16:10 06/10/14 01:09 7439-96-5 Potassium ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-09-7 Sodium ND mg/kg 573 1 06/06/14 16:10 06/10/14 01:09 7440-23-5 Zinc 32.6 mg/kg 1.1 1 06/06/14 16:10 06/10/14 01:09 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 30.8 % 0.10 1 06/18/14 16:37 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 7.2 Std. Units 0.10 1 06/05/14 16:57 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 864 mg/kg 34.4 5 06/16/1414:23 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 09:48 AM without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project:. Fieldsl-7 Pace Project No.: 92203926 Sample: MCAS FIELD #5 Lab ID: 92203926005 Collected: 06/03/14 11:00 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP` Calcium Copper Magnesium Manganese Potassium . Sodium Zinc Percent Moisture Percent Moisture 9045 pH Soil pH at 25 Degrees C 365.1 Phosphorus, Total Phosphorus Analytical Method: EPA 6010 Preparation Method: EPA 3050 169 mg/kg 7.2 1 06/13/14 15:50 06/16/14 16:01 7440-70-2 0.96 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7440=50-8 123 mg/kg 7.2 1 06/13/14 15:50 06/16/14 16:01 7439-95-4 M1 2.8 mg/kg 0.36 1 06/13/14 15:50 06/16/14 16:01 7439-96-5 ND mg/kg 361 1 06113/1415:50 06/16/14 16:01 7440-09-7 ND mg/kg 361 1 06/13/14 15:50 06/16/14 16:01 7440-23-5 2.3 mg/kg 0.72 1 06/13/14 15:50 06/16/14 16:01 7440-66-6 Analytical Method: ASTM D2974-87 14.4 % 0.10 1 06/18/14 16:37 Analytical Method: EPA 9045 - 5.4 Sid. Units 0.10 1 06/05/14 16:57 Analytical Method: EPA 365.1 36.8 mg/kg 4.9 1 06/16/14 13:53 7723-14-0 Sample: MCAS FIELD #7 Lab ID: 92203926006 Collected: 06/03/14 11:15 Received: 06/04/14 09:40 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Calcium 2050 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7440-70-2 Copper 8.2 mg/kg 0.27 1 06/13/14 15.50 06/16/14 16:10 7440-50-8 Magnesium 223 mg/kg 5.4 1 06/13/14 15:50 06/16/14 16:10 7439-95-4 Manganese 20.7 mg/kg 0.27 1 06/13/14 15:50 06/16/14 16:10 `06/16/14 7439-96-5 Potassium ND mg/kg 268 1 06/13/14 15:50 16:10 7440-09-7 Sodium ND mg/kg 268 1 06/13/14 15:50 06/16/14 16:10 7440-23-5 Zinc 12.1 mg/kg 0.54 1 06/13/14 15:50 06116/1416:10 7440-66-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 6.9 % 0.10 1 06/18/14 16:37 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 6.9 Std. Units 0.10 1 06/05/14 16:57 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 723 mg/kg 23.3 5 06/16/14 14:25 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/08/2014 09:48 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 Page 1 of 4 ' Report Number: 14-156-0628 LA, Account Number: 05755 '+JVJNf.� I0 � StB rI1.0 0 t11 Send To: PACE ANALYTICAL CHARLOTTE (for Tat TABITHA M DACAL 9800 KINCEY AVE - STE 100 HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date OfAnalvsis: 06/06/2014 L. Eastern-Laboraivnes 7621 Whiteptne-Road Richmond, Virginia 23237 (004) 747.9401 Fax'(004) 271-6446 Grower: 92203926 FIELDS 1-7 MCAS SOIL ALY•SIS REPORT Date Of Report: 06/06/2014 Submitted By: TABITHA M DACAL Farm ID: Analytical Method(s): Mehlich 3 Sample ID Lab Orgariic Matter Phosphorus 4r.Potassium'• Magnesium- Calcium- '° Sodium pH. Acidity - C.E.C- ' Field ID Number % :Rate ENR ' ' ,' Mehlich 3 Reserve - 1< '. '; . :Mg . Ca; ;: Na Soil Buffer ; H ., Ibs1A ppm : -'-Rate ppm Rate, ppm' ^' Rate pp m . Rate pp,m'-; r:f Rate, ppm Rate pH Index , meq/100g meg/100g: 1 18297 1.3 L 70 58 H 46 L 46 L 643 H 16 VL 6.4 0.4 4.2 MCAS NC = 48 NC = 24 FMCAS18298 2.8 M 97 15 L 34 VL 42 VL 1027 H 16 VL NC = 12 NC = 17 6.2 0.8 6.4 3 18299 2.8 M 97 17 L 34 VL 28 VL 922 H 17 VL 5.9 6.83 1.0 6.0 MCAS NC = 14 NC = 17 4 18300 3.4 M 98 351 VH 56VL 106 L 2597 VH 18 VL MCAS NC = 292 NC = 29 7.4 0.0 14.1 5 18301 1.5 L 75 10 VL 29 VL - 41 L 394 M 23 L MCAS NC = 8 NC_ 15 5.3 6.82 1.1 3.G Percent Base Saturation = :" '. Nitrate Sulfu r. i Zinc.. ' Manganese _ "Iron:. : -;;Copper';` ; . Boron ' - . Soluble,Salts . '.-,Chloride -' - Alumintim'.; Sample ID '' Field ID K "Mg, Ca .' ., Na H :" ..NO3N• S '' Zn, Mn .;' Fe , .,., .Cu B- % % % .: %`. % ' ppm-' ,Rate ppm Rate ppm.; ,.Rate pp m, rRate ppm ,' Rate pprW .Rafe .:.-; ppm " Rate mslcm Rate ppm Rate ppm; . ,. 1 8 VL 1.6 L 5 L 100 VH 1.5 M 0.1 VL 2.8 9.1 76.5 1.7 8.8 MCAS NC=17 NC=40.0 NC=31 NC=75.0 2 7 VL 1.6 L 5 L 12G VH 1.5 M L 1.4 5.5 80.2 1.1 12.2 10.4 MCAS NC=15 NC=40.0 NC=31 NC=75.0 3 L L 4 L 149 VH H 0.2 VL 1.5 3.9 76.8 1.2 17.3 113 11.8 ' 11.8 MCAS NC = 27 NC = 45.0 NC = 25 NC = 90.0 4 L VH 9 L VH 7.3 VH M 1.0 6.3 92.1 0.6 0.0 113 121.4 1399 10.8 MCAS . NC = 27 NC = 535.0 NC = 56 NC- 365.0 5 9 VL L 3 VL 304 VH 1.2 M 0.2 VL 2.1 9.5 54.7 2.8 31.1 11.4 MCAS NC=19 NC=35.0 NC=19 NC=60.0 values on finis report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by. FW" C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary Page 2 of 4 Report NL. umber: 14-156-0628 £ A Eastet^Y1 Laboratories AIL Account Number: 05755 • l 1-!� 7621 Whitepine Road Richmond, Virgini823237 (1304)743.9401Fax (004) 271,6446 wwwa71easteroxom Send To: PACE ANALYTICAL CHARLOTTE (for Tat Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KINCEY AVE - STE 100 MCAS HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS " ' ''... " `Nifrogen Phosphate Potash '; Magnesium :;"Sulfur, 2inc Manganese,`, " , Iron' Copper Borori " Sample -ID Field ID , Intended Crop Yield Goal :.. -,Lime- Tons/A `:::.'".., N.. P205 K20 Mg' `' :. S Zn Mn": : '; - ;Fe Cu B - Ib/A= " "" Ib/A Ib/A . Ib/A,., %. _" ,lb/A Ib/A lb/A-"', .• r':A/A Ib/A Ib/A 1 MCAS Hay 4 0.0 50 30 160 34 21 2.5 3 0 0 0.5 2 Hay 4 0.0 50 78 160 38 22 2.5 3 0 0 0 MCAS 3 " MCAS Hay 4 0.8 50 74 160 52 16 2.0 3 0 0 0.5 4 " Hay 4 0.0 50 0 180 0 16 0 3 0 0 0 MCAS 5 ' MCAS Hay 4 0.8 50 89 160 39 20 2.5 4 0 0 0.5 Comments: Sample(s) : 2 Crop: Hay Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 2,3,4,5 Crop: Hay Apply additional 50 pounds of nitrogen after every cutting and harvest of hay. Sample(s) : 3,5 Crop: Hay Apply dolomitic lime to raise pH and improve the magnesium level. Boron recommendations are on a broadcast basis. If dolomitic lime is not used,.apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : 4 Crop: Hay Cation Exchange Capacity may be over -estimated due to high pH and free lime in the soil. Use ammonium sulfate as all or portion of the N requirement to reduce pH. Use K-Mag as part of the potassium source to increase magnesium level "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 144Uf« work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of 4 Report Number: 14-156-0628 Y 1. Account. Number:05755ww ' Send To: PACE ANALYTICAL CHARLOTTE (for TTa v`aleastern.com TABITHA M DACAL 9800 KINCEYAVE - STE 100 HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Analysis: 06/06/2014 L astern Laborator 7621VhitepineRoad RicNmonp,;Virglnia'23237 (804]743-§,40i Fah(60,),271644G Grower: 92203926 FIELDS 1-7 WAS SOIL ANALYSIS REPORT Date Of Report: 06/06/2014 Submitted By: TABITHA M DACAL . Farm ID: Analytical Method(s): Mehlich 3 Organ,icMattet Phosphorus:'' '_<.,_, t. , _.;Potassium'.. -;Magnesium,_ :.Calcium _ -Sodium..::;,;_ =; pH Acidity::: Sample ID :Field ID Lab Number ;ENR % Rate Mehlich 3 Reserve` - K Mg .,' Ca Na Soil' Buffer H Ibs/A ppm Rate ppm - • 'Rate .ppm'.. Rate., ppm Rate' ppm : -•Rate ppm Rate pH, Index meq/100g_ -_ineq/100g 7 18302 5.1 H 132 342 VH 59 VL 94 VL 2522 VH 18 VL 6.9 0.2 13.8 MCAS NC = 285 NC = 30 - ... Percent:8ase$aturatlon Nitrate ,.; -Sulfur; Zin c_ ;' Manganes e' .:.Iro n "' Copper - =: Boron''n- soluble salts Chloride'':; -,'Aluriiinum:== Sample ID Field ID K Mg : ; - l :Ca ` .;: Na - H NO, _`::.. 3 .., _ a. S, ; ..:' i ;; Zn ? . ; ` Mnt:;;. ; _;; ''::.:; Fe '- Cu LL SS - CI % ., % pp m Rate pp m -Rate ppm ,Rate , ppm " -Rate ppm Rate ppm Rate ppm Rate '•ms/cm Rate ppm` ,Rate ` "ppm 7 13 L 6.9 H 8 L 337 VH 6.5 VH 0.6 M 1.1 5.7 91.4_ 0.6 1.4 MCAS NC = 27 NC = 172.5 NC = 50 NC = 325.0 Values on this report represent the plant available nutrients in the Explanation of symbols: %.(percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g - maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by PAWr` m G C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary Page 4 of 4 Report Number: 14-156-0628 Y J A &L Eastem- Laboratories - v S Account Number: 05755 7621 Whitepine Road Richmond; Virginia 23237 (004)743.9401 Fax (0041271-64d6 - a Send To: PACE ANALYTICAL CHARLOTTE (for Tat `aleastern:corn. Grower: Submitted By: TABITHA M DACAL TABITHA M DACAL 92203926 FIELDS 1-7 Farm ID: 9800 KINCEY AVE - STE 100 MCAS HUNTERSVILLE NC 28078 Date Received: 06/05/2014 Date Of Report: 06/06/2014 SOIL FERTILITY RECOMMENDATIONS Sample ID Yield Goal -_ `.,- Lime Nitrogen Phosphate' : Potash Magnesium Sulfur _. . ;Zinc Manganese Iron -Copper. Boron Field ID Intended Crop Tons "„_ ..Tons/A N P205 KZO Mg S. " Zn _ Mn Fe Cu = = B Ib/A Ib/A . .. lb/A, Ib/A lb/A .- Ib/A lb/A Ib/A lb/A-: . Ib/A 7 MCAS Hay 4 0.0 50 0 180 0 16 0 3 0 0 0 t,omments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary TRIENNIAL GROUNDWATER MONITORING REPORTS (3 COPIES) r a � UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090-/07109 LN March 18, 2014 ,North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center 1617 Mail 'Service Center Raleigh, NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring.and.reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the original and one copy of the GW-59-A report and the four GW-'59 reports (one each for monitoring wells 1, 2, 3, and 5). for the triennial reporting for February 2014.. Should you have any questions, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at your earliest convenience at (252) 466-2154. Sincerely, G. W. FOjD Env on enta1 Affairs Officer By dire t 8n of the Commanding Officer: Enclosure: (1) GW-59-A (2) GW-59 for MW=l (3) -GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-59 for MW-5 GNV-59A COMPLIANCE REPORT -FORM Permit # WQ0001489 (Submit one each monitoring pe'rion frith GW-59 fora nsJ Enter date monitoring results were due. (0 /31/14 Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO X . SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: e. ; ,.: DEPARTMENT_OF.ENVIRONMENTB NATURAL RESOURCES . ,, • DIVI$ION-OF WATER•QUALiTY INFORMATION PROCESSING UNIT . COMPLIANCE REPORT FORM .,;1617•:MAILSERVICE•CENTER=: =RALEIGH. NC'27699.1617 '- : " ''' PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cherry Point. Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Cherry Point, NC 28533=0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remedlation: Infiltration Gallery (city) (auto( (ZIP) ❑ .Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone M 252-466-4599 ❑ Rotary Distributor Q Land Application of Sludge Well Location/Site Name: Site 21,'MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ water Source Heat Pump ❑ Other: (n� SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter: 2 pH 00400 6.73 units Temp 00010: - 20 "C DRY at time of Depth to Water Level 82546: 3.5 R below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: 630 µMhos sampling; Measuring Point is 3 ft, above land surface Relative M.P. Elevation: 12 Odor 00085: NONE check Volume of water, pumped/bailed before sampling: 5 Gal. Appearance: TURBID here: ❑ Samples for metals were collected unfi8en:d YES Fj NO and field acidified YES Ej NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 - mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn = Zinc 01092 - mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as R00665 mg/L (Note: Use MPN matlwdfor h-rghy turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids;, Total 70300 -176 mg/L AI - Aluminum 01105 mg7L pH (Lab) 00403 6.73 units Ba - Barium 01007 µg1L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 17.4 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L . ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron.01045 µglL (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µglL Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L , Method# Total Ammonia 00610 3.13 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; Wh as N; Ammonia Nitrogen Tot* Mn -Manganese 01055 µglL ,Method# TKN as N 00625 mg/L Ni - Nickel 01067 . µglL Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis -Utility Systems Operator. - 3113/Z014 Permittee (or Authorized Agent) Name and Title - Please print or,type Signature of Permittee (or Authorized Agent) (Dale) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY rr , ;;DEPARTMENT OF ENVIRONMENT tIs NATURALRESOURCES . GROUNDWATER QUALITY MONITORING: , ;i..DNIStON.OF WATER 441A11TY-INFORMATION PROCESSING UNIT%-' . COMPLIANCE REPORT FORM SERVICE CENTER..:: .. RALEIGH, N6'276994617 ' PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different):. NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remedlation: Infiltration Gallery County: Craven ia+rt (WM•t (ZIP) ❑ Spray Field ❑ Remediatlon: Contact Person: Patricia T. Davis Telephone #: 2624664599 [] Rotary Distributor 0 Land Application of Sludge Well Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water Source Heat Pump Other. timm PEM SAMPLING INFORMATION If WELL WELL. ID NUMBER (From Permit): MW-3 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: aC WAS DRY . well Depth 25.58 ft. Well Diameter: 2 pH 00400 6.51 units Temp 00010: 17 Depth to Water Level 82546: 4 ft below measuring point Screened Interval: -11.7 ft to -21.:7 R Spec. Cond. 00094: 294, µMhos Measuring Point is 1.46 ft. above land surface Relative M.P. Elevation: 3.1 Odor 00085: NONE e Volume of water pumpedlbailedbefore sampling: 5Gal. Appearance: TURBID "•�• Samples for metals were collected unfiltered Lj YES 0 NO and field acidified El YES NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00515 mglL Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml. Phosphorus: Total as P 00665 mg/L '(Note: Use MPNniftodtorhighVIurbWsam*s) Orthophosphate70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 152 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.51 units Ba - Barium 01007 µg/L TOC 00680 rtig/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mglL Cd = Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L , Method# Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nibogem NH,as N; AmmarM N'aragen, Totaii Mn - Manganese 01055 (rglL , Method# TKN as N 00625 mg/L Ni - Nickel.01067 µg/L , Method# For Remedlation Systems -Only (Attach Lab Reports): Influent Total VOCs: - Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator" % -`- 3/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Pennittee (or Authorized Agent) (Date) GW-59 Rev.212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: s. • , DEPARTMENT'OF ENVIRONMENT & NATURAL RESOURCES ,. ` =; DIVISION OF WATER QUALITY4NFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1017-MAIL SERVICE CENTER, RAWdH, NC 27fi99-1617 PHONE: (919)733�3221 - FACILITY INFORMATION Please Print Clearly or Type '. PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cher Point Non -Discharge UIC Permit Name (if different): NPDES WQ0601489 Other Facility Address: MCAS Cherry Point,' NC 2853370006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑Remediatlon:InfiltrationGallery ISM) Is+wl (4) ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone M 252-466-4599 E] Rotary Distributor ❑✓ Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water Source Heat Pump ❑ Other: {ttomy SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-2 Date Sample Collected: 2/24/2014 : FIELD ANALYSIS: WAS Well Depth 26.58 ft. Well Diameter: 2 pH 00400 6.15 units Temp 0oo10: 20'C. DRY . Depth to Water Level 82646: 8 ft. below measuring point Screened Interval: -1.03 ft. to -11 1 Spec. Cond. 00094: 993 µMhos Measuring Point is 11.28 ft.'above land surface Relative M.P. Elevation. 14.8 Odor 00085: NONE, .-. Volume of water pumped/bailed befon: sampling: 5 Gal. Appearance: CLEAR ^ •' • : ❑ Samples for metals were collected unfiltered LiYES 0 NO and field acidified YES NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point /Pace Analytical Certification Number: 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Colifonn: MF Fecal 31616 -0 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /10DmL . Phosphorus: Total as P 00665 mg/L theta: u.ernPN matrwdOar highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:. Total 70300 424 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 ' 6.15 units Ba - Barium 01007 µg/L TOG 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13.9 mg/L Cd - Cadmium: Tota101027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy : Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L .. (Specify test and method M ATTACH LAB REPORT.) Sulfate 00945 o mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00610 297 mg/L Mg - Magnesium 00927 mg/L Method# (Ammorda Nift"etj: NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 µg/L Method#- TKN as N 00625 mglL Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% i cprtify that to the bcsk of my knov.4-2doe and belief tho Information submilleci in this report is true, accurate, wid complote. and that the la!borator-y anal0ril dala was prodUCed Using approved methods of analysis by a D010-cortified labo�atory, I an) i"Iarc that II'Lle, are sionificanil ppnahes for subrilill-n1p false infoinnation, including the possibility offines and imprisonment for knowing violahons, Patricia T. Davis -. Utility Systems Operator '�` - 3/13/2014 Permittee (or Authorized Agent) Name and Tide - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: e, :-DEPARTMENT OF ENVIRONMENT-:& NATURAL RESOURCES OF •. , : ., DIVISION WATER:QUAUTY.INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM :.. 1617MAIL.SERVICECENTER::.:=.::: . ' RALEIGH, NC 27699-1517 : - PHONE: (919)733-3221 FACILITY INFORMATION Please PdntClearfyorType PERMIT Number: Expiration Date: 7/31/2014 Facility Name: _ MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED - County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery MY) Ishm) Rol ❑ Spray Field ❑ Remedlatfon: Contact Person: Patricia T. Davis Telephone #: 252A66-4599 ❑. Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water Source, Heat Pump ❑ other: {prom p SAMPLING INFORMATION : If WELL WELL ID NUMBER (From Permit):- MWA Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 28.66 ft. Well Diameter. 2 pH 00400 6.68 units temp 00010: 23 °C DRY -� Depth to Water Level 82546: 3 fL below measuring point Screened Interval: -0.17 ft. to -15.2. ft. Spec. Cond. 00094: 70 µMhos Measuring Point is 1.33 fL above land surface. Relative M.P. Elevation: 10.78 Odor 00085: NONE -� Volume of water pumped/hailed before sampling: 5 Gal. Appearance: CLEAR ❑ Samples for metals were collected unfiltered YES El NO and field acidified M YES Lj NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point I Pace Analytical _ Certification Number: 201 137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L: Pb - Lead 01051 µg/L . Coliform: MF Fecal 31616. <1 /100mL Nitrate (NO3) as N 00620 0.07 mg/L Zn - Zinc 01092 mg/L Coliform' MF Total 31504 _ /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for hthlyt rbld samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 60 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd - Cadmium: Total 01027 µg/L� Arsenic 01002 µg/L Chromium: Total 01034 pg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Speclfy:test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 - µglL Lab Report Attached? ❑ Yes(1) ❑ no (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L , Method# (Ammon N"gen. NH,aa N.Ammo">a Na"en, Totap . Mn - Manganese 01055 µg1L , Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: - VOC Removal% I cedify that to the best of my knovtodge and belic-f the informaJon stibynittjd in ihis report is tnje, ,cc;,jr@12, and complete. and that the lalboraiory analy[Ticildiala was produced tistnq approved melhods ofanalyEis by a MND-ceVied Iabofatar;. f air) a�vare IhP.! thee are. signifi--ant pcnalhes for SLItbrnittvig fa!�e nformat;on, inchiding the pos�0,1 1yof fines and imprisonmert for Mov.-ing violat ons. Patricia T. Davis - Utility Systems Operator ""` ` - 3/13I2D14 Permittee (or Authorized Agent) Name and Title.- Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-56 Rev.2/2010 i UNITED STATES MARINE .CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/07109 LN March 18, 2 01,4 North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center 1617 Mail Service Center Raleigh, NC 2769971617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MICAS Cherry Point's Non-NPDES permit WQ00,01489 for Land Application of Wastewater Residuals, enclosed are the original and,one copy of the GW.59-A report and the four GW-59 reports (one each for monitoring wells 1, 2, 3, and 5.) for the triennial reporting for February-2014. Should you have any questions, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at,your earliest Convenience at (252) 466-2754. sincerely, j� G. W. FOLD Envi, on entfal Affairs Officer By dire tI n of the Commanding_ Officer Enclosure: (1) GW-59-A (2) GW-59 for MW-1 ( 3 ) -GW-59 . for' MW-2 (4) GW-59 for MW-3 - (5) GW-59 for MW-5 GW-59A CONIPLIANCF, REPORT FORM Perinit # WQ0001489 (Submit one each monitoring period frith GW-59 fornts.) Enter date monitoring results were due. (03/31/14) Will this monitoring report ((:W-59 and GIV-59A) be submitted after YES NO 1 the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged easing, unlocked -or missing cap, missing YES NO 3 identification plate, area overgrown, etc.)? lfthe answer is 1'es", contact the Regional USIc•eforguidance. X 4 Are any monitored constituents equal to or above the established standards? YES iYo X If the answer to question 4 is "NO", skip to section 8. It the answer to question 4 is'°1'F.S" list the affected walls individually %%ith constituent(s) and concentration(s) exceeding standards in the space provided below. MW-2 NH3 2.92 mg/L 14W-5 NH3 3.13 mg/I. For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) YES 'NO 5 in the same well(s) in the last two years? X if the ansiver to question 5 is "NO", skip to section 8 If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the lust two years). MW-2: Nov. 2013 N113 2.95, June 2012 NH3 2,67; Feb, 2012 NH3 2.75 MW-5: June 2013.NH3 2.45; Feb. 2013 NH3 2.25; June 2012 NH3 3.41; Feb. 2012 N1I3 3.78 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO G X If the answer is "YES", a groundwater quality problem may he occurring, CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional office. Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 prohlem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines. and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with li GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the informatiorfv6mitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge, Patricia T. Davis, Utility Systems Operator Supervisor Signature of Permittee or Authorized Agent) Date 3/13/2014 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: :.• DEPARTMENT:OF.ENVIRONMENTS NATt1RAL RESOURCES . " DIVI$ION.OF WATER QUAUT(-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM :;:'isai:iviAlI:SERVICEBENTER;: .' RALEIGH, NC'27699-1617-.- `""' PHONE: (919)733-3221 ' FACILITY INFORMATION Please Print ClearfyorType PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cher Point Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address:* MCAS Cher Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remedlation: Infiltration Gallery (cnn (sate) IUP) , - ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone M 252-466-4599 Rotary Distributor E] Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑water Source Heat Pump ❑Other: {vom p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter: 2 pH 00400 6.73 units Temp 00010: 20'C DRY at time of Depth to Water Level 82546: 3.5 fl. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: 630 . NMhos sampling, Measuring Point is 3 fL above land surface Relative M.P. Elevation: 12 Odor 00085: NONE check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: TURBID here: ❑ Samples for metals were collected unfiltered YES Q NO and field acidified n YES' Q NO LABORATORY INFORMATION Date sample analyzed: 2124/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. .201137706 COD 60335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: use MPN melhodfor highyturNd sampies) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 176 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.73 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 17.4 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L . ORGANICS (by GC, GC/MS, HPLC) Pheno131730 µg/L Fe - Iron 01045 µglL (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L , Method# Total Ammonia 00610 3.13 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia NlVogen; Nryes N; Ammonia Nivogerl recap Mn - Manganese 01055 µg/L Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis -Utility Systems Operator _ Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 F���e•; : ' ; = ` —. 3113/Z014 Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: ?DEPARTMENT OF ENVIRONNOENTlt<NATURALtiESOUR6E3 . -'• •:. [.. DIVISt01V.OF WATER UAUTY4NFORMATION PROCESSING UNIT:: • ' COMPLIANCE REPORT FORM :';1617:IIAAILSERVICE CENTER. .` RALEIGH, NC'27699-1677 ' PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS CherryPoint Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Che Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery j0a'i (51stel inoi ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone #: 252-466-4599 Rotary Distributor Q Land Application of Sludge Well Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water Source Heat Pump Other. (t_ p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-3 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 25.58 ft. Well Diameter: 2 pH 00400 6.51 units Temp 00010: 17 oC DRY a Depth to Water Level 82546; 4 ft below measuring point Screened Interval: -11.7 fL to -21.7 ft Spec. Cond. 00094: 294 µMhos Measuring Point is .1.46 f. above land surface Relative M.P. Elevation: 3.1 Odor00085: NONE Volume of water pumpediballed before sampling: - 5 Gal. Appearance: TURBID Samples for metals were collected unfiltered YES F1 NO and field acidified YES Lj NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS CherryPoint / Pace Analytical Certification Number. 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform:- MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 '0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504. /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPNmedtodfor hignlyturbWsamples). Orthophosphate 70507 ' mglL Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 76300 152 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.51 units Ba- Barium 01007 µg/L TOC 006BO mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd :Cadmium: Total 01027 µg/L . Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy- Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) . Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) [].No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L , Method# (Ammonia Nitrogen; NH3as N; Ammonia Nitragenjotaq Mn - Manganese 01055 µg/L ,Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L , Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% . . Patricia T. Davis - Utility Systems Operator '-*`' ';` "` 3/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: e � DEPARTMENTOr£ F,ENVIRONMENTNATURALRESOURCESOF WATER QUALITY -INFORMATION PROCESSINt1� UNIT COMPLIANCE REPORT FORM �:1617 MAIL$ERVICECENTER.':NC2' 99-1617' :. `PHONE:(919j733-3221FACILITY [Non-.Rallii±1611, INFORMATION Please Print Clearly or Type ERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cher Point Disch_ arge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cher Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediatlon: Infiltration Gallo ry IoMI (st.r.l t>Ja1 ❑ Spray Field ❑ Remedialion: Contact Person: Patricia T. Davis Telephone M 252-466A599 ❑ Rotary Distributor 0 Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 Water Source Heat Pump ❑ Other: Ittom p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permlt): .MW-2 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 26.58 it. Well Diameter: 2 pH 00400 6.15 units Temp 00010: 20 rC DRY .� Depth to Water Level 82546: 8 ft. below measuring point Screened interval: -1.03 ft, to -11 ft Spec. Cond. 00094: 993 µMhos • o. a mpll�g, Measuring Point is 1.28 ft above land surface Relative M.P. Elevation. 14.8 Odor 00085: NONE �� •� Volume of water pumpedlbailed before sampling: 5 Gal. Appearance: CLEAR "•�^ Samples for metals were collected unfiltered Lj YES Ll NO and field acidified Lj YES NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform:. MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 424 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.15 units Ba - Barium 01007 pg/L TOC 00680 mg/L Ca - Calcium 00915 mg1L Chloride 00940 13.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS; HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 pg/L Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00510 2.97 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NHras N; Ammonia Nihogei Totep Mn - Manganese 01055 µg/L , Method# TKN as N 00625 mg/L Nt- Nickel 01067 pg/L Method# ror ttemearation systems Unly (Attach Lab Reports): Influent Total'VOCs: Effluent Total VOCs: VOC Removal% M. Opis by a Patricia T. Davis -Utility Systems Operator ^ w~� ; - "" 3113/2D14 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 GROUNDWATER QUALITY MONITORING: (COMPLIANCE REPORT FORM Name: MCAS Name (if different): Address: MCAS SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type NC 28533-0005 County: Craven act Person: Patricia T. Davis Telephone M 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: r: utMAKI MENT OF ENVIRONMEIR:S.NATURAL RESOURCES DIVISION OF WATER:gUAUTY-INIFORMATION PROCESSING UNIT .;'.1617MAIL, SERVICE CENTER ,,.;; :: '• RALEIGH,.NC 27699-1617 ' • PHONE: (919)733-3 PERMIT Number. Expiration Date: 7/311201, n-Limcnarge UIC DES, WQ0001489 Other PE OF PERMITTED,OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor 0 Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION . If WELL WELL ID NUMBER (From Permit): MW-1 Date Sample Collected; 2/2412014 FIELD ANALYSIS: WAS Well Depth 26.66 ft. Well Diameter. 2 pH 00409 6.68 units Temp 000'10: 23 'C DRY -� Depth to Water Level 82546: 3 R below measuring point Screened Interval: -0.17 ft. to -15.2. ft. Spec. Cond. 00094: 70 µMhos vmc ^r Measuring Point is 1.33 fL above land surface. Relative M.P. Elevation: 10.78 Odor 00085: NONE � m P1Ing. .. ^ Volume of water pumpedibailed before sampling: 5 Gal. Appearance: CLEAR Sam les for metals were collected unfiltered YES ❑ NO and field acidified n .YES n NO 30RATORY INFORMATION e sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. - COD 00335 mglL 'Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 0.07 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly t rbld samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 60 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 pg/L Grease and Oils 00552� mg/L Cy - Copper 01042 . mg/L Phenol 32730 µglL Fe - Iron 01045 µg/L Sulfate 00945 mg/L Ho - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen. Total) Mn - Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LA8 REPORT.) Lab Report Attached? . ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: - VOC Removal% Patricia T. Davis -Utility Systems Operator �-��' """' 3/1312014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 , UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533-00113 IN REPLY REFER TO: 5090/07109 LN March 18, 2014 North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center 1617 Mail Service Center Raleigh,,NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MICAS Cherry Point's Non-NPDES.permit WQ0001489 for Land Application of.Wastewater Residuals, enclosed are the original and one copy of the GW-59-A report and the four GW759 reports (one each for monitoring wells 1, 2, 3, and 5) for the triennial reporting for February 2014. Should you have any questions, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at your earliest convenience at (252) 466-2754. Sincerely, _J /2.J 1 � G. W. RA]7FO�D Envi onf�ental Affairs Officer By diretkon of the Commanding Officer Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) -GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-59 for MW-5 GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489 (Submit one each monitoring period frith GW-59 jornu.) Enter date monitoring results were due. (03/31/14) Will this monitoring report (GIVV-59 and GW-59A) be submitted after YES NO 1 the established due date? X Was any required information missing on the GIV-59 report forms? YES NO 2 X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification numher(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged easing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown, cte.)? !%the atinveris "Yes". contact the Regional Ufceforguidance. X 4 Are anv monitored constituents equal to or above the established standards? YES NO X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below.. MW-2 NH3 2.92 mg/L MW-5 NH3 3.13 mg/f. For the constituents identified in question 4 above, have standards been exceeded previously for the some constituent(s) YES NO 5 in the same well(s) in the. last two years? X If the answer to question 5 is "NO", skip to section 8 If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the lust two years). MW 2: Nov. 2013 -I13 2.95, June 2012 NH3 2.67; Feb, 2012 NH3 2.75 11W 5; June 2013 NH3 2.45; Feb. 2013 NH3 2.25; June 2012 NH3 3.41; Feb. 2012 NIB 3.78 Are the monitoring Wells listed in section 5 located at or.beyond the review boundary? YES NO G X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 dayst an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines. and/ur penalties. The person completing this portion (G)V-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW 59A) is true and complete to the best of my knowledge. Patricia T. Davis, Utility Systems Operator Supervisor f �.� Signature of Permittee or Authorized Agent)Date 3/13/2014 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING:-u�r-Ar��mtni �r.>=roviKurvmkN.T�rwtuRAtRESOURCe5 . DIVISION -OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE'REPORT FORM :v=1677:MA1LSERVICE'CENTER RALEIGH. NC'27699-1617. °-' PHONE: (919)7333221 ' FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/3112014 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remedlation: Infiltration Gallery (`"r) Rut.) wpl - - ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone M 252-466-4599 Rotary Distributor Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 Water Source Heat Pump ❑ Other: _ lttam p -L ID NUMBER (From Permit): MW-5 Date Sample Collected: 2/24/2014 I Depth 13 ft. Well Diameter: 2 th to Water -Level B2546: 3:5 ft. below measuring point Screened Interval: 3 _ ft. to 13 ft. tsuring Point is 3 IL above land surface Relative M.P. Elevation: 12 lme of water pumped/bailed before sampling: 5 Gal. iples for metals were collected unfiltered. n YES n_NO and field acidified n YES n NO 30RATORY INFORMATION If WELI. FIELD ANALYSIS: WAS pH 00400 6.73 units Temp 00010: 20 °C DRY at time of Spec. Cond. 00094: 630 pMhos samplint Odor 00085: NONE - check Appearance: TURBID here: ❑ e sample analyzed: 2/24/2014 . Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706 tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations - COD 00335 mg/L Nitrite (NO2) as N 00615 . trig/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Nole: Use MPNmethod for highly lutbidsamples) Odhophosphate70507 mg/L Dissolved Solids: Total 70300 176 mg/L AI - Aluminum 01105 mg/L PH (Lab) 00403 6.73 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 17.4 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µglL Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 - µg/L Fe.- Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 3.13 mg/L Mg - Magnesium 00927 mg/L (Ammanla Nllrogen; NH, as N; Arrimonia Niboger% Tatap - Mn - Manganese 01055 µg/L TKN as N 00625 mg/L . Ni - Nickel 01067 µglL Pb - Lead 01051 µg/L Zn -Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by -GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# For. Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% dnpigni �fr kn vinrl v0aliqns. r Patricia T. Davis - Utility Systems Operator r e.•.t., .t:i ...�_ — 3/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: a DEPARTMENT OF ENVIRONMENT.& NATURALRESOUR¢ES . : '• •.. � � � � ?. DIVIStON.OF WATER QIJAUTY INFORMATION PROCESSING UNIT':': COMPLIANCE REPORT FORM :`;1617:MAILSERViCECENTER..:'•-'.-- RALEIGH, NC-27699-1617 ' :: ' '' . PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2014 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0005 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery ledyl (51a1•1 (ZIP) ❑ Spray Field EJ,Remediatlon: Contact Person; Patricia T. Davis Telephone #. 252-466-4599 D Rotary Distributor Land Application of sludge Well Location/Site Name: Site 21 MCAS Cherry Point —_ No.of Wells to be Sampled: 1 Water Source Heat Pump Other. 0.•m p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-3 Date Sample Collected: 2/24/2014 FIELD ANALYSIS: WAS Well Depth 25.58 ft. Well Diameter: 2 pH 0040D 6.51 units Temp 00010: 17 PC DRY •1 Depth to Water Level 82546: 4 ft below measuring point Screened Interval: -11.7 R to -21.7 fL Spec. Cond. OD094: 294 µMhos • Measuring Point is 1.45 ft. above land surface Relative M.P. Elevation: 3.1 Odor 00085: NONE �+ •�. Volume of water pumped/bailed before sampling: 5 Gal. - Appearance: TURBID "• El Samples for metals were,coliected unfiltered YES Lj NO and field acidified Lj YES Lj NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mglL Pb - Lead 01051 i.19/L Coliform: MF Fecal 31616 <1 1100mL Nitrate (NO3) as N 00620 0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 11 OOmL Phosphorus: Total as P 00665 mg/L (Note: UmMPNmedtodfor highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 152 mg/L At - Aluminum 01105 mg/L pH (Lab) 00403 6.51 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 . mg/L Cd = Cadmium: Total 01027 µg/L Arsenic 01002 • µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GCIMS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µglL (Specify test and method A ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑• No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L , Method# ' (Ammonia Nilmgen; NHS as N; Ammonia Nitrogen, Tenon Mn - Manganese 01055 µg/L - , Method# ' TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator r."�'' ;t''`{`"`- 3/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Type Name: MCAS Cherr)r Point Name (if different): Address: MCAS Cherry Point, NC County: Craven (City?(suer Wnt act Person: Patricia T. Davis Telephone #:' 252-466-4599 Location/Site Name:. Site 21, MCAS Cherry Point No.of Wells to be Sampled: te.m vcrnn�.nlcry v,•rpl7vimvr4lvjrrj 1 di OVA 1 UKAL Kt5UUKGE5 f:; DIVISION OF WATER QUALITY -INFORMATION PROCESSINQ UNIT` rZ'1617 MAIL SERVICE CENTER, i t2ALEIdH, Nd 27699-1617 PHONE: (919)733-3221 ' PERMIT Number: Expiration Date: 7/31/2014 Non -Discharge UIC NPDES WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ---�,- ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑✓ Land Application of Sludge ❑ Water Source Heat Pump . ❑Other: SAMPLING INFORMATION WELL ID NUMBER (From Permit): MW-2' Date Sample.Collected: 2/24/2014 FIELD ANALYSIS: Well Depth 26.58 ft. Well Diameter: 2 pH 00400 6.15 units Temp 00010: Depth to Water Level 82546: 8 ft. ,below measuring point Screened interval: -1.03 ft. to -11 ft Spec. Cond. 00094: 993 Measuring Point is 1.28 fL above land surface Relative M.P. Elevation. 14.8 Odor 00085: NONE Volume of water pumped/bailed before sampling: 5 Gal. Appearance: CLEAR Samples for metals were collected unfiltered n YES ❑ NO and field acidified ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 , mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L ` (Note: Use MPNmethod for highly "Wdsamples) Orthophosphate70507 _mg/L Dissolved Solids: Total 70300 424 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.15 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca- Calcium 00.916 mg/L Chloride 00940 13.9 mg/L Cd - Cadmium: Total 01027 pg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 pg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 2.97 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Totep Mn - Manganese 01055 pg/L TKN as N 00625 mg/L Nt - Nickel 01067 pg/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Patricia T. Davis - Utility Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 WELL 20 PC DRY .s z�m... µMhos a —pt,ng n.,.: ❑ / 37706 Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L 1 Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ ljo (0) Method# Method# Method# Method# Effluent Total VOCs: VOC Removal% W13/2014 Signature of Permittee (or Authorized Agent) (Data) For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Patricia T. Davis - Utility Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 WELL 20 PC DRY .s z�m... µMhos a —pt,ng n.,.: ❑ / 37706 Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L 1 Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ ljo (0) Method# Method# Method# Method# Effluent Total VOCs: VOC Removal% W13/2014 Signature of Permittee (or Authorized Agent) (Data) SUBMIT FORM ON YELLOW PAPER ONLY UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM Please Print Clearly or Type Name: MCAS Cherry Point Name (if different): Address: MCAS Cherry Point, NC 28533-0006 County: Craven act Person: Patricia T. Davis Telephone M 252-4664599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: teom PMM `: utrAKl MINT OF ENVIRONMENT4 NATURAL RESOURCES :. D!VlStON OF WATER:gUAUTY-INFORMATION PROCESSING UNIT .1617 MAIL, SERVICE CENTER';.:',, RALEIGH,•NC 27699-1617 "4` PHONE: (919)7334 PERMIT Number: Expiration Date: 7/31/201, in-ulscnarge UIC DES WQ0001489 Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remedlation: ❑ Rotary Distributor Q Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: LL ID NUMBER (From Permit): MW-1 Date Sample Collected: 2/24/2014 1 Depth 26.66 ft. Weil' Diameter. 2 th to Water Level 82546: 3 R below measuring point Screened Interval: -0.17 fL to -15.2. ft. isuring Point is 1.33 ft. above land surface. Relative M.P. Elevation: 10.78 ime of water pumpedibailed before sampling: 5 Gal. iples for'metals were collected unfiltered ❑ YES ❑ NO and field acidified ❑ YES ❑ NO 30RATORY INFORMATION FIELD ANALYSIS: 'r""zo pH 00400 6.68 units. Temp 00010: 23 °C DRY m vmp er Spec. Cond. 00094: 70 - pMhos , m p r, ,, o • Odor00085: NONE «.« Appearance: CLEAR "-•^ ❑ e sample. analyzed: 2/24/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: - 201137706 tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 . <1 /100mL Nitrate (NO3) as N 00620 0.07 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPNmethod for highly turbldsamples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 60 mg/L. AI -Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Be - Barium 01007. µglL TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002�µg/L Chromium: Total 01034 µg1L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L 'Fe - Iron 01045 pg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen. Totail Mn - Manganese 01055 pg/L TKN as N 00625 mg/L Ni - Nickel 01067 pg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg1L Other (Specify Compounds and Concentration Units)': ORGANICS (by GC, GC/MS, HPLC) (Specify test and method It. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# I -or Remedlation systems Unly (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Rik Patricia T. Davis - Utility Systems Operator ;"" 3/13/2014 Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent) (Dale)- GW-59 Rev.212010 UNITED STATES MARINE CORPS ' MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA,28533.0007 IN REPLY REFER TO: June 13, 2014 North Carolina Department of Environment and Natural Resources Division of Water,Quality Information,Process.ing Center 1617 Mail Service Center Raleigh, NC'2-7699-1617 . Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry_Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals_, enclosed are the original and one copy .of the GW-59-A report and_the four GW-59 reports (one each for monitoring wells 1, 2, 3,. and 5) for the triennial reporting.for June 2014. Should you have any questions, please contact Mr. Timothy _Lawrence of the Environmental Affairs Department at your earliest. convenience.at (252) 466-2754. Sincerely, /J airs Officer he Commanding Officer Enclosure: (1) GW-59-A (2) GW-59-for MW-'1 (3) GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-5.9 for MW-5 GW-59A COMPLIANCE REPORT FORM I'erinit.# WQ0001489 (Su6ntii one each wonitoring period x uh @; fi 59 jorn sj Enier date monitoring results were due. 07/( 31/141 Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO 1 the established .dtie:date? . X Was any required information missing on the GW-59 report forms? . YES NO 2 X 1F the answer to question 1 or 2 is "YES". list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing VFS NO 3- identification plate, area overgrown, cte.)? Ijthe answer is "Yes'; contact the Regional Office Jorguidance. X . 4 Are any monitored constituents equal to or above the established standards? YES \O X If the answer to question 4 is "NO", skip to section 8. if the answer to question 4 is,"1'KS" list the alllrtcd wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW-5 NiB 2.71 mg/l. For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) VES NO 5 in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip, to suction 8. If the answer to question 5 is "YES", list in the space provided below,.ench well with constituent(s) exceeding standards; concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-5: Feb. 2014 N H3 3.13; .tune 2013 NH3 2.45; Feb. 2013 NH3 2.25; June 2012 N113 3.41; Feb. 20.12 NH3 3.78 Are the monitoring wells listed in section 5 located at or beyond the review. boundary? YES NO 6 X. If the answer is "YES", a groundwater quality problem may be occurring. CONTACT.THE REGIONAL OFFICE, IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may he improperly located; contact the. Regional Office. Is the permittee implementing previously approved actions required by the -Division involving this groundwater quality YES NO 7 problem? X If the unswer to question 7is "YES", describe'those actions in the space provided below. If the answer to question 7 is "NO", contact the Reeioual Office within 90 days; an evaluation may he required to determine the impact the waste disposal system is having at'the review and compliance boundaries surrounding this facility. Failure to do so may sublect the permittee to a'Nodce or Violation, fines..and/or penalties. The person' completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for,required wells to the address provided at the. top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report OW-59A) is true and complete to the best of my knowledge. Patricia T, Davis, Utility Systems Operator Supervisor Signature of Permittee (or Authorized Agent) Date 6/13/2014 SUBMIT FORM ON YELLOW PAPER ONLY : DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING:, DIVISION OF"WATER.QUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAILSERVICECENTER S RALEIGH, NC 27699-1617 . PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/ 2014 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES VV00001489 Other Facility Address: MCAS Cher ' Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven - ❑ Lagoon ❑ Remediation: Infiltration Gallery (cm) (et.t.) 001 ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone #: 252-466-4599 ❑ Rotary Distributor. Q Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point, No.of Wells, to be Sampled: 1 ❑. Water Source Heat Pump ❑ Other: Inom pmm SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-1 Date Sample Collected: 6/4/2094 FIELD ANALYSIS: WAS Well Depth 26.66 ft. Well Diameter: 2 pH 00400 6.68 units Temp 00010: 26 eC DRY at time of Depth to Water Level 82546: 4 ft below measuring point -Screened Interval: -0.17 ft. to -15.2 ft. Spec. Cond. 00094: 125 µMhos sampling, Measuring Point is 1.33 ft. above land surface Relative M.P. Elevation: 10.78 Odor 000W. none check Volume of.water pumped/bailed before sampling: 5 Gal. Appearance: clear here: ❑ Samples for metals were collected unfiltered YES NO and field acidified n YES- - NO LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical. Certification Number:. 201 137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100ml. Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Nate: Use MANmethodrorhifthnbidsamples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 44 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Ba - Barium 01007 µ & TOC 00680 mg/L - Ca - Calcium 00916 mg/L Chloride 00940 10.1 ring/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy -Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L: - Method# 'Total Ammonia'00610 <1.0 mg/L Mg - Magnesium 00927 mg/L Method# (AmmoniaN"en; NH,as N;Ammonia Nitropen.Totaq Mn - Manganese 01055 µg/L •, Method# - TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCS: VOC Removal% Patricia_ T. Davis Utility Systems Operator Permittee,(or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) . GW-59 Rev.212010 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITYdNFORMATION.PROCESSING UNIT . COMPLIANCE REPORT FORM 167 MAIC'SERVICE CENTER RALEIG14, NC 27699.1617 PHONE: (919)733.3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 1/2 4 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: infiltration Gallery Icgl _ (s�.�.( (to) ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone #: 25246SA599 ❑ Rotary Distributor [✓ Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water source Heat Pump ❑ Other: o.m SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-2 Date Sample Collected: 614/2014 FIELD ANALYSIS: WAS Well Depth 26.58 ft. Well Diameter. 2 pH 00400 6.09 units Temp pool0: 28 °C DRY at time of Depth to Water Level 82546: 9 fL below measuring pant Screened Interval: -1.03 ft. to -11 ft. Spec. Cond. 00094: 69D pMho's sampling, Measuring Point is 1.28 ft. above land surface Relative M.P. Elevation: 14.8 Odor 00085: none - check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here, Samples for metals were collected unfiltered YES NO and field acidified YES F1 NO LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 1100mL Phosphorus: Total as P 00665 mg/L . (Note: Use MPN method m highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 200 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.09 units Be - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11.4 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 pg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) . Sulfate 00945 mg/L Hg - Mercury 71900 µg/L lab Report Attached? ❑ Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L , Method# Total Ammonia 00610 1.07 mg/L Mg - Magnesium 00927 mg/L , Method# (AmmonlaNurogen:NH, asN:AmmmiaNiftgeRT°t Mn - Manganese 01055 pg/L Method# TKN as N 00626 mg/L Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): . Influent Total VOCs: Patricia T. Davis - Utility Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.212010 Effluent Total VOCs: VOC Removal% 'Y - j c. 6/13/2014 Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT,OF-ENVIRONMENT,& NATURAL RESOURCES. GROUNDWATER QUALITY MONITORING:. DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM '1617-MAILSERVICECENTER_ RALEIGH;•NC 27699.1617 r PHONE: (919)7333221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 1/2014 Facility Name: MCAS Cherry Point Non -Discharge U1C Permit Name {if different): NPDES W00001489 Other Facility Address: MCAS Cherry Paint, NC 2853370006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery rSI.Wr frmr ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone M 252-466-4599 ❑ -Rotary Distributor 0 Land Application of Sludge Well Location/Site Name: .Site 21 MCAS Cherry Point No.ofWells to be Sampled: 1 Q Water Source Heat Pump ❑ Other: prom SAMPLING INFORMATION if WELL WELL ID NUMBER (From Permit): MW-3 Date Sample Collected: 61412014. FIELD.ANALYSIS: WAS Well Depth 25.5E fL Well Diameter:, 2 pH 00400 6.54 units Temp 00010: 26 eC DRY at time of Depth to Water Level 82546: 0 fiL below measuring point Screened Interval: -11.7 IL .to -21.7 ft. Spec. Cond. 00094: 277 µMhos sampling, Measuring Point is 1.46 ft. above land surface Relative M.P. Elevation: 3.1 Odor 00085: none - - check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: turbid here: a Sam les for metals were -collected unfiltered El YES 0 NO and field acidified D YES NO LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb -Lead 01051 µg/L Coliform: MF Fecal 31616 <1. /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc D1092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P b0665 mgtL (Note: UseMPN megwdfori,orytobidaamplec) _ Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total70300 128 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.54 units . Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: 'Total 01034 µg/L Grease and Oils 00552 Ing/L Cy - Copper 01042 mg/L ORGANICS ,(by GC, GC/MS, HPLC) Phenol 32730. µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ ,Yes(1) ❑ No (0) Specific Conductance 00095 µMhos - K - Potassium 00937 mg/L Method# Total Ammonia 00610 0.0 mg/L Mg - Magnesium 00927 mg1L Method# (Ammonia NMogem NHs as N; Ammonia Nitrogen, Tout) - Mn - Manganese 01055 µg7L , Method# TKN as N 00625 mglL Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% I cerfify(hat to the best of my kno\vledne and belief, the informalion Eubmided in lhis ropo't is hrue, accurale.and complete, arid that the laboratory analytical dala vias produced using approved mothods of analysis by a Patricia T. Davis'- Utility Systems,Operator 6113/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENT $ NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617'MAIL SERVICE CENTER RALEI6H; NC 27699-1617 • : PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type. PERMIT Number: Expiration Date:, 7/31 01 Facility 'Name: . MCAS CherryPoint Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Cher Point,. NC 28533-0006 TYPEAF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery County: Craven tcry� islalei tzpr ❑ Spray Field ❑ Remediation: Contact Person: Patricia T. Davis Telephone #: 252-466-4599 ❑ Rotary Distributor �. Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water source Heat Pump ❑ other. loam p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 6/4/2014 FIELD ANALYSIS: e-- WAS DRY at Well Depth 13 ft. Well Diameter- 2 pH 00400 5.26 units Temp 00010: 25 time of Depth to Water Level 82546: 8 ft. below measuring point Screened Interval: 3 ft. to 13 ff. Spec, Cond. 00094: 642 µMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 12 Odor 00085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: 0 Sam les fog metals were collected unfiltered YES' NO and field acidified YES NO LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 0.08 mglL Zn -Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: use MPH meftdler highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total70300 172 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 5.26. units Ba -Barium 01007 . µg/L . TOC 00680 mg/L Ca -'Calcium 00916 mg/L Chloride 00940 11.4 mg/L Cd : Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730. µg/L Fe - Iron 01045 µg/L (Specify test and method#. ATTACH LAB REPORT.), Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) ❑ No (0)' Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# . Total Ammonia 00610 . 2.71 mg/L Mg- Magnesium 00927 mg/L Method# ' (Ammonia Nitrogen; NH, a: N; Ammonia NWogea,Totaq - - Mn -Manganese 01055 µg/L Method#.. TKN-as N 00625 mg/L Ni -Nickel 01067 µg/L ,Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: laboratory data Ipproved VOC Removal% methods of analysis by a I cedify that to the best of rny knov&dgL arid beliefthe information submWed in tWs report is DVVO-ceiliried laboratory I am avare that (heie we s-an4cam penall,cs f&r sutimilflng false true, accurate. and complete, and thatthe information, inclUding the possibiNty of analytical was prc)(fuc .2d using fines and imprisonment for tuio%,,ing violations, Patricia T. Davis = Utility Systems Operator, ` '— 6/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 . UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/07109 LN . June 13, 2014 North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center 161-7 Mail Service Center Raleigh, NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting . requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the original and one copy of the GW-59-A report and the four GW-59 reports (one each for monitoring wells 1, 2, 3, and 5) for the triennial reporting for June 2014. Should you have'any questions, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at your earliest convenience at (252) 466-2754. . Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) GW-59 for MW-2 (4) GW-59 for MW-3 (,5) GW-59 for MW-5 Sincerely, airs Officer he Commanding Officer M-59A C'OMPLIANC E REPORT FORM Perinit # WQ0001489 (Submit one each monitoring period with GtV39jarjnxj Enfer date monitoring results were due. 07/(_ 31114l Will this monitoring report (GVV-59 and'GW-59A) be submitted after YES NO I the established due date? X 2 Was any'required information missing on the GW-59 report forms? YES NO X 1F the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown, etc.)? If the answer is "Yes ". rontact the Regional Ojr1ce for guidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO X If the answer to question 4 is "NU", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(q) and concentration(s) exceeding standards in the Space provided below. kiW-S Nf 13 2.71 mg/l. For the constituents identified in question 4 above, have standards been exceeded previously for the same constitucnt(s) YES NO 5 in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last nvo years). MW-5: Feb. 2014 NH3 3.13; June 2013 NH3 2.45; Feb. 2013.NH3 2.25; June 2012 N113 3.41; Feb. 2012 NH3 3.78 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO X 1f the answer is "YES", a groundwater quality problem may be occurring. COS -ACT. I HE REGIONAL OFFICE IMMEDIATELY FOR G1:IDANCE. if the answer is "NO", monitoring wells may he improperly located; contact the Regional Office. Is the permitter implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may he required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may sublect the permittee to a Notice of violation, fines, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my Knowledge. Patricia T. Davis, Utility Systems Operator Supervisor Signature of Permittee (or Authorized Agent) Date 6/13/2014 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Name: MCAS Cherry Point Name (if different): Address: MCAS Cherry Point, NC 28533-0006 County: Craven act Person: Patricia T. Davis Telephone #: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: Pmm WILING INFORMATION L ID NUMBER (From Permit): Depth . 26.60 ft. h to Water Level 82546: MW-1 4 fL below measuring point ng Point is 1.33 ft. above land surface of water pumped/bailed before sampling: 5 Gal. 'DIVISION OF•WATERQUAUTY-INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER s'RALEIGH, NC 27699-1617 . PHONE: (919)733-3 Non -Discharge UIC S WQ0001489. Other OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Spray Field ❑ Rotary Distributor ❑ 'Water Source Heat Pump Date Sample Collected: 6/4/2014 Well Diameter: 2 Screened Interval: -0.17 ft. to _15.2 R. Relative M.P- Elevation: 10.78 ❑ Remediation: Infiltration Gallery ❑ Remediation: Q Land Application of Sludge ❑ Other: FIELD ANALYSIS: pH 00400 6.68 units Temp 00010: _ 26 eC Spec. Cond. 00094: 125 pMhos Odor OD085: none Appearance: clear Samples for metals were collected unfiltered [ -YES NO and field acidified n YES U NO LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point I Pace Analytical Certification Number: 201 137706 PARAMETERS NOTE. Values should reflect dissolved and colloidal concentrations. _ COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 1100ml- Nitrate (NO3) as N 00620 <0.05 mg/L Coliform: MF Total 31504 AOOmL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method forhighytudbid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 44 mg/L AI --Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Be - Barium 01007 µgIL . TOC 00680 mg/L - Ca - Calcium 00916 mg/L Chloride 00940 10.1 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 pg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen.Totaq Mn - Manganese 01055- µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L If WELL WAS DRY at time of sampling, check here: ❑ Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# For Remediation Systems Only (Attach Lab Reports): Influent Total V.00s: Effluent Total VOCs: VOC Removal% • r ,r Patricia T. Davis -Utility Systems Operator .�~f�`_""'' •f='``""`-- 6/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: MCAS Cherry Point, NC Please Print Clearly or County: Craven Contact Person: . Patricia T. Davis Telephone #: 252-466-4599 Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: p,om WELL ID NUMBER (From Permit): MW-2 Well Depth 26.58 fL Depth to Water Level 82546: 9 ft. below measuring point Measuring Point is 1-28 ft. above land surface Volume of water pumped/bailed before sampling: 5 Gal. Samples for metals were collected unfiltered LjYES LABORATORY INFORMATION DIVISION OF WATER QUALITY INFORMATiON.PROCESSING UNIT 1617 MAIUSERVICE CENTER RALEIG14 Nt: 27699.1617 PHONE: (919)733-3 n-Discharge UIC DES W00001489 Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ✓❑ Land Application of Sludge ❑ Water source Heat Pump ❑ Other: Date Sample Collected: 6/4/2014 Well Diameter: 2 Screened Interval: -1.03 ft. to -11 ft. Relative M.P. Elevation: 14.8 and field acidified If WELL FIELD ANALYSIS: WAS pH 00400 6.09 units Temp 00010: 28 eC DRY at time of Spec. Cond. 00094: 690 pMhos sampling Odor00085: none check Appearance: clear here: ❑ Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 PARAMETERS NOTE: Values should reflect dissolved and eolloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mglL Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L. (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total70300 200 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 6.09 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11.4 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GCIMS, HPLC) Phenol 32730 µg/L Fe -Iran 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00.945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? El Yes(1) ❑ ND (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L , Method# Total Ammonia 00610 1.07 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NH3 asN:Ammonia NitrcgerkTotaq Mn - Manganese 01055 µg/L Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# certify that to the best of mylk.novi edge and bebef, IheNiuifgtmation s-idmilled in this report is 1Ne, ac4urlatei and co lele,'and Itia� the laborato i nab lical data v:as rod' c d using approved r i p ry�^Ip g pproved methods o analysi by a DWO-certified laboratory. I ain anare that thole are sion�ficant penalties for subinilh(g fat^se infor(nation Imclt{d nlg Ih possibllily of lines and imp sonhler l fo knowing Violali Patdcia D. Operator 1 14 Permittee (or Authorized Agent) Name and Title - Please pant or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 212010 ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Facility Name: MCAS Cherry Point Permit Name (if different)t Facility Address: MCAS Cherry Point SUBMIT'FORM ON YELLOW PAPER ONLY Please Print Clearly or Type NC 28533-0006 County: Craven act Person: Patricia T. Davis Telephone #: 252-466-4599 Location/Site Name: Site 21 MCAS Cherry Point No. of Wells to be Sampled: SAMPLING. INFORMATION WELL ID NUMBER (From Permit): MW-3 Well Depth 25.58 ft Depth to Water Level 82546: 0 ft. below measuring poini Measuring Point is 1.46 ft. above land surface Volume of water pumped/bailed before sampling: 5 Gal. 11 Samples for metals were collected unfiltered LlYES LABORATORY INFORMATION DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617•MAIL SERVICE CENTER . RALEIGH;'NC 27699.1617 : PHONE: (91911733-3 on -Discharge UIC PDES WQ0001489 Other (PE OF PERMITTED OPERATION BEING MONITORED 0 Lagoon ❑ Remedlation: Infiltration Gallery [I Spray Field Remediation: ' Rotary Distributor Q Land Application of Sludge Water Source Heat Pump other: Date Sample Collected: 6/4/2014 Well Diameter: 2 Screened Interval: -11.7 ft. .to -21.7 ft. Relative M.P. Elevation: 3.1 field NO FIELD ANALYSIS: WAS pH 00400 6.54 units Temp 00010: 26 CC DRY at . Spec. Cond. 00094: 277 ptime of Mhos sampling, Odor00085: none check Appearance: turbid here: ❑ e sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 tAMETERS NOTE: Values should reflect dissolved and colloidal conicn t ft COD 00335 mg/L era ons. Nitrite (1402) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (1403) as. N 00620 <0.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN melhod for highly turbid -samples) Orthophosphate 70507 mg(L Dissolved Solids: Total 70300 128 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.54 units Ba - Barium 0100'7 µg/L TOC 00680 mg/L Ca -Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002. µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Atnmonia Nitrogen; NH3 as N; Ammonia Nitrogen, Tow Mn- Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Qther (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator 6/13/2014 Permiltee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) OW-59 Rev.2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: s ` ` ` ` vcr/UtI IYICIv 1- Vr =mvlKV1VrvIGry 1 6 NA I UKAL KESOURGE5 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT ` COMPLIANCE REPORT FORM 1617'MA1LSERVICE CENTER RALEIGH; NC 27699-1617 PHONE: (919)7333221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31 014 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery (ceyl tstmel tzh). ❑ Spray Field ' ❑ Remediation: Contact Person: Patricia T. Davis Telephone #: 252-466A599 ❑ Rotary Distributor Q Land Application of SOudge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: tVom FTmrri 1 ❑ Water Source Heat Pump El Other. SAMPLING INFORMATION if WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 6/412014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter. 2 pH 00400 5.26 units Temp 00010: 25 e- DRY at De Depth to Water Level 82546: 8 ft. below measuring P g point Screened Interval: 3 ft. to 13 ft. Speer Cond, 00094: 642 µMhos time of sampling, Measuring Point is 3 fL.above land surface Relative M.P. Elevation: 12 Odor 60085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: Clear here: ❑ Samples for metals were collected unfiltered YES _' ❑ NO and field acidified ❑ YES ❑ No LABORATORY INFORMATION e sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.08 mg/L .Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 . mg/L Dissolved Solids: Total 70300 172 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.26 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 11.4 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium:_ Total 01034µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00931 mg/L Total Ammonia 00510 2.71 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH�asN:Ammonia Nitrogen. Tolat Mn- Manganese 01055 µg/L . TKN as.N 00625 mg/L . Ni - Nickel 01067 µglL Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method#. ATTACH LAB REPORT.). Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# . Method# _ Method# Method# ror Kemeolatlon bystems unly (Attacn Lab Keports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator -'�� ' u '`_ 6/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533.0003 IN REPLY REFER TO: 5090/07109 LN June 13, 2014 North Carolina Department of Environment and Natural Resources Division of Water.Quality Information Processing Center 161-7 Mail Service Center Raleigh, NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the original and one copy of -the GW-59-A report and the four GW-59 reports (one each for monitoring wells 1, 2, 3, and 5) for the triennial reporting for June 2014. Should you have any questions, please contact Mr. Timothy Lawrence of the Environmental Affairs Department at your earliest convenience at (252) 466-2754. Sincerely, Commanding Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-59 for MW-5 airs he Officer Of f icer M-59A COMPLIANCE REPORT FORM Permit 4 WQ0001489 (Suhmir ane each monitoring period x ith Glf'-59 jbnnr./ Enter date monitoring results were due. 07/( 31/la) Will this monitoring report (GW-59 and CW-59A) be submitted after YES NO 1 the established due date? 2 Was any required information missing on the GIVV-59 report forms? YES NO ' X 1F'the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information, Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown, etc.)? Ij the onstrer is "Yes", contact the Regional Ujj<ce jorguidance. X Are any monitored constituents equal to or above the established standards? YES NO X. If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the afTected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 4MW-5 NI13 2.71 mg/l. For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(%) YES NO 5 in the same well(s) in the last two years? X Ifthe answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding stundards, conecntration(s) reported, and sample collection duce for each occurrence (for the last two yeah). M%V-5: Feb. 2014 -NH3 3.13, .tune 2013 NH3 2.45; Feb, 2013 NH3 2.25; June 2012 N113 3.41; Feb. 2012 NH3 3.78 6 Are the monitoring wells listed in section 5 located -at or beyond the review boundary? YES NO X If the answer is "YES", a groundwater quality problem may be occurring. CON'TACT.THE REGIONAL OFFICE, IMMEDIATELY FOR GUIDANCE. 11 the answer is "NO", monitoring wells may he improperly located; contact the Regional Office. 1s the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the ReEioual Office within 90 days: an evaluation may he required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 8 GW-59 forms for required wells to the address provided; at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance. Report GW-59A) is true and complete to the best of my knowledge, Patricia T. Davis, Utility Systems Operator Supervisor Signature of Permittee (or Authorized Agent) Date 6/13/2014 GROUNDWATER QUALITY MONITORING:' COMPLIANCE REPORT FORM Please Print Clearly or Name: MCAS Cherry Point Name (if different): Address: MCAS Cherry Point, NC 28533-0006 SUBMIT FORM ON YELLOW PAPER ONI Y County: Craven act Person: Patricia T. Davis Telephone #: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled:' 1 prom Plan L ID NUMBER (From Permit): MW-1 Depth . 26.66 ft. h to Water Level 82546: 4 It. below measuring point wring Point is 1.33 ft. above land surface ne of water pumped/balled before sampling: 5 Gal. Dies for metals were collected unfiltered ❑ YES [ -DIVISION OF•WATER.QUALITY-INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER ..'RALEIGfi NC 27699-1617 . • P PHONE: (919)733-3 •—••••••• •-•-•••-••••• �nN11oI1V11 I101G. r/J IrLU IY Non -Discharge UIC NPDES WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: _ ❑ Rotary Distributor Q Land Application of Sludge ❑ Water Source Heat. Pump ❑ Other: Date Sample Collected: 6/4/2014 Well Diameter: 2 Screened Ipterval: -0.17 ft. to -15.2 ft. Relative M.P_ Elevation: 10.78 NO and field acidified II YES If WELL FIELD ANALYSIS: WAS pH 00400 - 6.68 units Temp 00010; 26 eC DRY at Spec. Cond. 00094: 125 µMhos time of sampling, Odor00085: none check Appearance: clear here: ❑ e sample analyzed: 614/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 ItAMET .., ERS NOTE. values should reflect dissolved and colloidal concentrations. COD 00335 mg1L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 70.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mgIL (Note: Use MPN method for highly turEid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 44 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.68 units Ba - Barium 01007 µg/L TOC 00680 mg/L. Ca - Calcium 00916 mg/L Chloride 00940 10.1 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 pg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercur)r 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH,ar N;Ammonia Nltrogen•Tolaq Mn - Manganese 01055 pg/L TKN as N 00625 mg/L Ni - Nickel 01067 pg/L Pb - Lead 01051 pg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC). (Specify test and method #. -ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes(1) _ ❑ No (0) Method# _ Method# Method# _ Method# laa.,l1 aryl 11l Willy t•+ttat:rl l_mo rceporCsl: mnuent i otai vuE;s: Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator `%`'`-""`-- 6/13/2014 Permittee (or Authorized,Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 'GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: MCAS Name (if different): Address: MCAS Please Print Clearly or Point Point, NC 28533-0006 County: C SUBMIT FORM ON YELLOW PAPER ONLY act Person: Patricia T. Davis Telephone #: 252466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled DIVISION OF WATER QUALITY INFORMATION.PROCESSING UNIT 16 T MAIL'SERVICE CENTER RALEIGFI; NC 27699-1617 PHONE: (919)733-3221 PERMIT Number: - Expiration Date: 7 31/2 4 Non -Discharge UIC NPDES W00001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Q Land Application of Sludge 1 ❑ Water Source Heat Pump ❑ Other SAMPLING INFORMATION' If WELL WELL ID NUMBER (From Permit): MW-2 Date Sample Collected; 614/2014 FIELD ANALYSIS: WAS Well Depth 26.58 ft. Well Diameter: 2 pH 00400 6.09 units Temp 00010: 28 eC DRY at De Depth to Water Level 82546: 9 fL below measurin P g point Screened Interval: -1.03 ft. to -11 ft. Spec. Cond. 00094: 690 µMhos time of ' Measuring Point is 1.28 IL above land surface Relative M.P. Elevation: 14.8 Odor 00085: none sampling, check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: ies for metals were collected unfiltered YES [I NO and field acidified n YES n NO 1-1Sam e sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number. 201 / 37706 tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /1 OOmL Phosphorus: Total as P 00665 mg/L . (Note: Use MPN method for hlghly turWd samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total70300 200 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 6.09 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca, -Calcium 00916 mg/L Chloride 00940 11.4 mg1L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L. Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mei*cury 71900 µg/L Lab Report Attached? 0 Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Method# Total Ammonia 00610 1.07 mg/L Mg - Magnesium 00927 mg/L _ Method# (Ammonia Nitrogen: NH, as N: Ammonla Nitrogen. Total - Mn— Manganese 01055 µg/L ,Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg1L Method# .. . .ikeports): Influent . •Cs: Effluent Total VoCs:e 1+l ' I r I +••I e t LI! re I' s„ �. I I . I ,, I certify that to the best of my knoeJedge and beb. lhe,information sUniilled in this mr;.ii �s f4d Iacrdi[late• and�co pI te,;and Ilialilhe laboratory I nalylical Bala 14as producRd using approved melhotls o�analysi by a D1ND-cerlifetl laboratory. I am aware that the/e are si�njricanl �endiies for subhitung false Inior�ation� inelcidi,jg Ih pcssib(lily of lines and impns peril for, knot+;ing violate Igps• I. •. 6 , I I I e Patricia T. Davis Operator Permittee (or Authorized 'gprint or type. .f Permittee (or Authorized •.c (DatGW-59 Rev. e) 1 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: MCAS Cherry Point Name (if different): Address: MCAS Cherry Point SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type NC 28533-0006 County: Craven ict Person: Patricia T. Davis Telephone M 252-466-4599 " Location/Site, Name: Site 21 MCAS Cherry Point No,of Wells to be Sampled: IPLING INFORMATION LID NUMBER (From Permit): Depth . 25.58 fL MW-3 h to Water Level 82546: 0 ft. below measuring point curing Point is 1.46 ft. above land surface ne of water pumpedibailed before sampling: 5 Gal. pies for metals were collected unfiltered n vFs I DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 1617•MAIL SERVICE CENTER _ RALEIGH;= 27699.1617, PHONE: (919)733-3 n-umunarge UIC DES VV00001489 Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remedlation: Infiltration Gallery ❑ Spray. Field ❑ Remedlation: ❑ Rotary Distributor 0 Land Application of Sludge Water Source Heat Pump ❑ Other: Date Sample Collected: 61412014' Well Diameter: 2 Screened Interval: -11.7 ft. ..to -21.7 ft. Relative M.P. Elevation: 3.1 and field acidified I I YES FIELD ANALYSIS: WAS pH 00400 6.54 units Temp 00010; 26 oC DRY at time of Spec. Cond. 00094: 277 )jMhos sampling, Odor00085; none check Appearance: turbid here: ❑ e sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 ET Z 411 ERS NOTE. Vaiues should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (1402) as N 00615 , mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN melhad for highly turbid samples) Orlhophosphate 70507 mg/L Dissolved Solids: Total 70300 128 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 6.54 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 pg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 pg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Ndrogen; NH3 as N:'Ammonia Nibogen, T-1) Mn - Manganese 01055 µg/L TKN as N 00625 _ mg/L Ni - Nickel 01067 µg/L Pb - Lead, 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT:) Lab Report Attached? ❑ Yes(1) ❑ No (0) Method# Method# Method# Method# For Remediation Systems.Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% INN 1101KIIHM a ra r Patricia T. Davis - Utility Systems Operator 6/13/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev, 2/2010 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: , MCAS Cherry Point Name (if different): Address: MCAS Cherry Point, NC SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type County: Craven act Person: Patricia T. Davis Telephone ##: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 %DIVI$IOM OF WATER QUALITY INFORMATION PROCESSING UNIT ' 1617'MAIL SERVICE CENTER RALEIGH; NC 27699-1617 :' PHONE: (919)733-3221' m-uiscnarge UIC 'DES WQ0001489 Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor [,] Land Application of Sludge. ❑ Water Source Heat Pump ❑ Other. SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 6/4/2014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter. 2 pH 00400 5.26 units Temp 00010: 25 eC DRY at De Depth to Water Level 82646: 8 ft. below measuring P g point Screened Interval: 3 ft. l0 13 ft. Spec. Cond. 00094: 642 µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: 12 Odor 00085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: Samples for metals were collected unfiltered YES ❑ _NO_ . and field acidified .n YES (� NO ❑ LABORATORY INFORMATION Date sample analyzed: 6/4/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201137706 nw `L41WETERS NOTE. Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as'N 00620 0.08 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg1L . (Note: Use MPN method fcr highly turbid samples) Orthophosphate 70507 mg/L Dissolved. Solids: Total70300 172 mg/L Al -Aluminum 01105 mg/L' PH (Lab) 00403 5.26 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L. Chloride 00940 11.4 mg/L Cd : Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034'µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 231 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; Ntf,asN;Ammonia NArogen,Tolat Mn - Manganese 01055 _µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg1L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method•#. ATTACH LAB REPORT.). Lab Report Attached? ❑ Yes(1) ❑ No (0) . Method# . , Method# Method#' Method# For Remediation Systems Only (Attach Lab Reports):, Influent Total VOCs: Effluent Total VOCs: VOC Patricia T. Davis - Utility Systems Operator /�`' ~ = r "" • = 6/13/2014 Pennittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method•#. ATTACH LAB REPORT.). Lab Report Attached? ❑ Yes(1) ❑ No (0) . Method# . , Method# Method#' Method# For Remediation Systems Only (Attach Lab Reports):, Influent Total VOCs: Effluent Total VOCs: VOC Patricia T. Davis - Utility Systems Operator /�`' ~ = r "" • = 6/13/2014 Pennittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28633-0003 IN REPLY REFER TO:, 5090./0.7109 LN October 31, 2014 North Carolina Department of Environment and Natural Resources .Division of.Water Quality. Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 'Subj:.TRIENNIAL GROUNDWATER MONITORING In accordance.with the groundwater monitoring and,reporting requirements 'of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application.of Wastewater Residuals, enclosed are the - original and one copy of the GW-59-A report and the four.GW-59: reports (one each for monitoring wells 1., 2, 3; and 5) for the. - triennial reporting' for October-2014. Should you have any questions, please.contact.Mr. Timothy . Lawrence, PE of the'Environmental Affairs 'Department 'at your earliest convenience at .(252) 466-2754. Sincerely, TByO n ent 1 A airs.Officerre ti of the Commanding Officer Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) GW-59 for_MW-2 (4) GW-59 for,MW-3 . (.5) GW-5'9 for MW-5 (6) Lab Report GW-59A COMPLIANCE REPORT FORM Permit. #. WQ0001489 ' (Submit one each monitoring period H ith GW-59 forms.) Enter date monitoring results were due. 11/31/14 Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO 1 the established due date? . X Z Was any required, information missing on the GW-59 report forms? . YES NO X IF the answer to question 1 or 2 is "YFS", list in the spaceprovided below the well identification number(i) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown,etc.)? If the answer is "Yes", contact the Region! Ufj1cefor guidance. X 4 Are any monitored constituents equal to or above the established standards? YES. NO X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES". list the affected wells individually with constituent(s) and conecntration(s) exceeding standards in the space provided below MW-I Chloroform 4,7 ug/I. MW-2.N113 1.73 mg/l, ' MW-5 NH3 2.99 m /L For the constituents identified in question. 4_above, have standards been exceeded previously for the some constituent(s) YES NO 5 in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-5; Feb. 2014 NH3 3.13; June 2013 NH3 2.45; Feb. 2013 NH3 2.25 MW-2: Feb. 2014 NH3 2.97; Oct 2013 NH3 2.95; Feb 20I3 NH3 1.74, ' 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO, X Ifthe answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater -quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and ,compliance boundaries surrounding this facility. Failure to do so may subject the nermittee to a Notice of Violation, fines, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with, $ GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby aclaiowledge. that the above information was evaluated and the information su_nitted in this report•(Cor pRfance • .; �.,. Report GW-59A) is true and corpAWto the best of my know*hdge. Patricia T. Davis, Utility S ysterns Operator Supervisor Signature of Permittee (or Authorized Agent) Date 10/30/2014 . SUBMIT FORM ON YELLOW PAPER ONLY to t .P4PARTt1tLENT OF,ENVIRONMENT & NATURAL RESOURCES •.. .: -. ' GROUNDWATER QUALITY MONITORING: a DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ' .1t317 MAIL'SERVICE CENTER RALEIGH, NC`27699-1617 PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: 'Expiration Date: 7 /2019 Facility Name: MCAS Cher Point Non -Discharge. UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PER OPERATION BEING MONITORED County:, Craven El Lagoon ❑ Remedlation: infiltration Gallery May) (stare) (zip) ❑ Spray Field ❑ Remedlation: Contact Person: Patricia T. Davis Telephone #: 252-466-4599 ❑ Rotary Distributor Q Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 El Water Source Heat Pump ❑ Other: t-m p SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-1 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 26.66 1t. Well Diameter: 2 pH 00400 5.96 units Temp 00010: 25 oC DRY at time of Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: -0.17 ft. to -15.2 ft. Spec. Cond. 00094: 108 µMhos sampling, Measuring Point is 1.33 R. above land surface Relative M.P. Elevation: 10.78 Odor 00085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here., Samples for metals were collected unfiltered n YES EJ NO and field acidified M YES NO LABORATORY INFORMATION Date sample analyzed: 10/872014 Laboratory Name: MCAS .Cherry Point / Pace Analytical Certification Number: 201137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 1100mi- Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPNmethod for highly h,rbldSamples) Orthophosphate 70507• mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 64 mg/L Al - Aluminum 01,105 mg/L pH (Lab) 00403 5.96 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Pheno132730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? ❑ Yes(1) . ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC Method# SM 6200B Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L. Method# (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 µg/L - , Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent.Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 10/30/2014 Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY e r_ DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES. GROUNDWATER QUALITY MONITORING: • • bIVISI¢N.t7F WATER QUALITY -INFORMATION PROCESSING UNIT' ' COMPLIANCE REPORT FORM `:16771NAILSERVICE CENTER . =: RALEIGH, NC 27699-1617 PHONE: (919)7334221 FACILITY INFORMATION Please Print CfeadyorType PERMIT Number: Expiration Date: 7l 1/2 19 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery (CRY) (Sute) Rol ❑ Spray,Fleld [J Remedlation: Contact Person: Patricia T. Davis, Telephone #: 252-466-4599 Rotary Distributor 0 Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 Water Source Heat Pump ❑ other: (ROm R SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-2 Date Sample Collected: 10/812014 FIELD ANALYSIS: WAS Well Depth 26.58 ft. Well Diameter. 2 pH 00400 6.29 units Temp 00610: 23 oC DRY at time of Depth to Water Level 82546: 6.5 ft. below measuring point Screened Interval: -1.03 ft. to -11 ft. Spec. Cond. 00094: 713 pMhos sampling, Measuring Point is 1.28 f<. above land surface Relative M.P. Elevation:- 14.8 Odor 00085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: Clear here: ❑ Samples for metals were collected unfiltered YES F1 NO and field acidified YES n NO LABORATORY INFORMATION Date sample analyzed: 10B/2014 Laboratory Name: MCAS Cherry Point I Pace Analytical Certification Number. 201 137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb,- Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0"05 mg/L Zn - Zinc 61092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L .(Note: Use MPNmethodfor Nghyturbid sernpies) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 160 mg/L AI -Aluminum 01105 mg/L pH (Lab) 00403 6.29 units Ba = Barium 01007 µg/L TOC 00680 ' mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg1L ORGANICS (by GC, GUMS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg -Mercury 71900 µg/L Lab Report Attached? 0 Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L. VOC Method# SM 6200B Total Ammonia 00610 1.73 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen: NFt, as N: Ammonia Nitrogen, Total Mn - Manganese 01055 µg/L Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% I certify that to the best of my kno;iledge and belief the information submitted in this report is true, accurate, and complete, and lhalthe lalboralory,analytical data (vas Produced using approved methods of analysis by a. CWO—certified laboratory. I am aware that there are significant penalties for subme.fng false reformation„ ncluci^g the possibility of fines and imprisonment for knowing vio;aiions 10/30/207141 Patricia T. Davis - Utility Systems Operator Jv�,/_, �; . 7 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of.Permittee (or Authorized Agent) t GW-59 Rev. 1 1 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT_l7F ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: -DIVISION.OF WATER:QUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM M.-RALEIGHiNC27692-113317 :. fail twat. SERVICEcENrER 'PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number. Expiration Date: 7/31/2019 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES W00001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven 0 Lagoon ❑ Remediation: Infiltration Galley (CM (ewa (ao) 0 Spray Field E] Remediation: Contact Person: Patricia T. Davis Telephone•#: 252-466A599 Rotary Distributor 0 Land Application of Sludge - Well Location/Site Name:. Site 21 MCAS Cherry Point No.of Wells to be Sampled: 1 0 Water Source Heat Pump Other: SAMPLING INFORMATION IP WELL WELL ID NUMBER (From Permit): MW-3 Date -Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 25.58 ft. Well Diameter. 2 pH 00400 6.32 units Temp 00010: 25 °C DRY at time of Depth to Water Level 82546: 0 ft. below measuring point Screened Interval: -11.7 ft. to -21.7 , ft. Spec. Cond. 00094: 301 µMhos sampling, Measuring Point is I A6 IL above land surface Relative M.P., Elevation: 3.1 Odor 00085: stagnant check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: turbid here, O Samples for metals were collected unfiltered YES 0 NO and field acidified Lj YES Lj NO LABORATORY INFORMATION Date sample analyzed: 10/8/2014 Laboratory Name: MCAS Cherry. Point / Pace Analytical Certification Number: 201 /,37706 PARAMETERS . NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb -• Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn -Zinc 01092 mg1L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Nola: Use MPNmethod for hig*turbid samp(ea) Orthophosphate 70507 mg/L ,. Other (Specify Compounds and Concentration- Units): Dissolved Solids: Total 70300 160 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 6.32 units Ba -.Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC; GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L . (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg r Mercury 71900 µg/L Lab Report Attached? 0 Yes(1) • ❑ No (0) , Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC , Method# SM 6200B Total Ammonia 00610 1.13 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total Mn - Manganese 01055 µg/L Method# TKN as N 00625 mg/L Ni - Nickel 01067 .. µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal% Patricia T. Davis - Utility Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type 6W-59 •Rev..2/2010 �,. �^X�— 10/30/2014 Signature of Permittee (or Authorized Agent) (Date) . ! i SUBMIT FORM ON YELLOW PAPER ONLY • . :.DEPARTMENT OFgNVIRONMi NT R NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: :t ,DIVISION OF WATEkQUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM :;is17.MnIL sERVICE CENTER RALEIGH; NC.2769SA617 PHONE: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2019 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES - WQ0001489 Other Facility Address: MCAS Cherry Point; NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED.' County: Craven ❑ Lagoon ❑ Remediation: Infiltration Gallery tcfN1 (srat•1 rztv) [] Spray Fleld ❑ Remediation: Contact Person: Patricia T. Davis Telephone #:• 252-466-4599 ❑ Rotary Distributor 0 Land Application of Sludge Well Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water Source Heat Pump ❑ Other: trtom SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MI Date Sample Collected: 10/812014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter: 2 pH 00400 6.55 units Temp 00010: 29 eC DRY at time of Depth to Water Level 82546: 9 ft. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: 741 µMhos sampling, Measuring Point is 3 fl. above land surface Relative M.P. Elevation: 12 Odor 00085: none check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: Clear here. ❑ Samples for metals were collected unfiltered YES NO and field acidified n YES 0 NO LABORATORY INFORMATION Date sample analyzed: 10/812014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201137706 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: use MPNmeu,oafor highly turbidsamples) _ Orthophosphate 70507- mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 274 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.55 „ units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.4 mg/L Cd - Cadmium: Total 01027 µglL Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L' Hg - Mercury 71900 µg/L Lab Report Attached? El Yes(1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC Method# SM 6200B Total Ammonia 00610 2.99 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NHS as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 µg/L Method# TKN as N 00625 mg/L Ni - Nickel 01067 pg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Rernoval% certify that to the best of my kne+.!edge and belief, the nfo�matioii submit!ed'inihis report Is true, accyatz, and complete, and that the IaC�ratory°analytical dot =�rdes proddced Uslr,e approved me1111111 thods or analysis by a Q�YQ•ceit�fied 18bo[aloy. Lam a�;,are thzrthete are-s�gniGcantpenalties for sutim!4Bng false information. including the poss;bility of tines and imprisonment for kr,a,�i{;tg viclations. " 10/3012014 Patricia T. Davis - Utilii!� Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 1 1 e aeeAna"Cal e rvww.peee/abs.twm ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1Q0 Huntersville, NC 28078 (704)875-9092 Sample: MCAS MW-1 Lab ID: 92220940001 Collected: 10/08/14 11:05 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B. Benzene ND ug/L 0.50 1 10/15/14 08:11 7143-2 Bromobenzene ND ug/L 0.50 1 10/15/14 08:11 108-86-1 Bromochtoromethane NO ug/L 0.50 1 10/15/14 08:11 74-97-5 Bromodichloromethane ND ug/L 0.50 1. 10/15/14 08:11 75-27-4 Bromoform ND ug/L 0.50 1 10/15/14 08:11 75-25-2 Bromomethane NO ug/L 5.0 1 10/15/14 08:11 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/15/14 08:11 104-51-8 sea-Butylbenzene ND ug/L 0.50 1 10/16114 08:11 135-98-8 tert-8utylbenzene ND ug/L 0.50 1 10/15/14 08:11 98-06-6 Carbon tetrachloride NO ug/L 0.50 1 10/15/14 08:11 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/15/14 08:11 108-90-7 Chloroethane NO ug/L 1.0 1 10/15/14 08:11 75-00-3 Chloroform 4.7 ug/L 0.50 1 10/15/14 08:11 67-66-3 Chloromethane NO ug/L 1.0 1 10/15/14 08:11 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/15/14 08:11 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/15/14 08:11 10643-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/15/14 08:11 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10115/14 08:11 124-48-1 1,2-Dibromoethane (ED8) ND ug/L 0.50 1 10/15/14 08:11 106-93-4 Dibromomethane ND ug/L 0.50 1 10/15/14 08:11 74-95-3 1.2-Dichlorobenzene ND ug/L 0.50 1 10/15/14 08:11 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/15/14 08:11 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10115/14 08:11 106-46-7 Dichlorodifluoromethane NO ug/L 0.50 1 10/15/14 08:11 75-71-8 1,1-Dichloroethane NO ug/L 0.50 1 1011511408:11 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/15/1408:11. 107-06-2 1, 1 -Dichloroetherie ND ug/L 0.50 1 10/15/14 08:11 75-35-4 cis-1,2-Dichlorcethene ND ug1L 0.50 1 10/1511408:11 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/15/14 08:11 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/15/14 08:11 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 1011511408:11 142-28-9 2,2-Dichloropropane NO ug/L 0.50 1 10/15/14 08:11 594-20-7 1,1-Dichloropropene NO ug/L 0.50 1 10/15/14 08:11 563-58-6 cis-1,3-Dichloropropene NO ug/L 0.50 1 10/15/14 08:11 10061-01-5 trans-1,3-Dichloropropane NO ug/L 0.50 1 10/15/14 08:11 10061-02-6 Dilsopropyl ether NO ug/L 0.50 1 10/15/14 08:11 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/15/14 08:11 100-41-4 Hexachloro-1,3-butadiene NO ug/L 2.0 1 1011511408:11 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 10115/14 08:11 98-82-8. Methylene Chloride ND ug/L 2.0 1 10/15/14 68:11 75-09-2 Methyl-tert-butyl ether NO ug/L 0.50 1 10/15/14 08:11 1634-04-4 Naphthalene NO ug/L 2.0 .1 10/15/14 68:11 91-20-3 n-Propylbenzene NO u9/L 0.50 1 10/15/14 08:11 103-65-1 Styrene NO ug/L 0.50 1 10/15/14 08:11 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 1011511408:11 630-20-6 1,1,2,2-Tetrachloroethane NO ug/L 0.50 1 10/15114 08:1.1 79-34-5 Tetrachloreethene NO ug/L 0.50 1 10/15/14 08:11 127-18.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/28/2014 03:29 PM without the written consent of Pace Analybeal Services, Inc.. Page 4 of 23 ;-alceAna"cal' Pace Analytical Servicee, Inc. 9800 Kincey Ave. SuRe lo0 wwwpace sucarr Hunlersville, NC 2807a (704)875-9092 ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: MCAS MW-1 Lab ID: 92220940001 Collected: 10/08/14 11:05 Received: 10/10/14 09:45 Matrix: Water. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Toluene ND ug/L 0.50 1 10/15/14 08:11 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/15/14 08:11 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/15/14 08:11 120-82-1 1,1,1-Trichloroethene ND ug/L 0.50 1 10/15114 08:11 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/15/14 08:11 79-00-5 Trichioroethene ND ug/L 0.60 1 10/15/14 08:11 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/15114 08:11 75-69-4 1,2,3-Tdchloropropane ND ug/L 0.50 1 10/15/14 08:11 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0:50 1 10/15/14 08:11 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 1 10/15/14 08:11 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/15/14 08:11 75-01-4 m&p-Xylene ND ug/L 1.0 1 10/15/14 08:11 179601-23-1 o-Xylene ND ug/L 0.50 1 10/15/14 08:11 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 10/15/14 08:11 17060-07-0 4-Bromofluorobenzene (S) 9.8 % 70-130 1 10/15/14 08:11 460-00-4 Toluene-d8 (S) 104 % 70-130 1 10/15/14 08:11 2037-26-5 Sample: MCAS MW-2 Parameters Lab ID: 92220940002 Collected: 10/08/14 10:20 Results Units Report Limit DF Received: 10/10/14 09;45 Matrix: Water. Prepared Analyzed CAS No. Qual 62008 MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/18/14 18:13 71-43-2 Bromobenzene ND ug/L 0.50 1 10/18/14 18:13 108-86-1 Bromochloromethane ND ug/L 0.50 1 10/18/14 18:13 ' 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10118/1418:13 75-27-4 Bromoform ND ug1L 0.50 1 10118/1418:13 75-25-2 Bromomethane ND ug/L 5.0 1 10/18/14 18:13 74-83-9 n-Butyibenzene ND ug/L 0.50 1 10/18114 18:13 104-51-8 seo-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/18114 18:13 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:13 108-90-7 Chloroethane ND ug/L 1.0 1 10/1811418:13 75-00-3 Chloroform ND ug/L 0.50 1 10118/14 18:13 67-66-3 Chloromethene ND uglL 1.0 1 10/18/14 18:13 74-87-3 2-Chlorotoluene ND ug/L -0.50 1 1Of18/14 18:13 95-4941 4-Chlorotoluene ND ug/L 0.50 1 10/18/14 18:13 106-43-4 1,2-Dibromo-3-chlompropane ND ug/L 1.0 1 10/1811418:13 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10118/1418:13 124-48-1 1.2-Dibromoethane (EDS) ND ug/L 0.50 1 10/18/14 18:13 106-93-4 Dibromomethane ND ug/L 0.50 1 10/18114 16:13 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/1811416:13 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10118/1418:13 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:13 10646-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 23 aceAnalytical o www!pscelalu,com ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kinsey Ave. Suite lo0 Huntersviile, NC 28078 (704)875-9092 Sample: MCAS MW-2 Lab ID: 92220940002 Collected: 10/08/14 10:20 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200E MSV Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis- 1,2-Dichl oroethene trans-1, 2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1.1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlo robenzene 1,1,1-Tdchloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoro methane 1,2,3-Trichlo ropropane 1,2,4-Trimethylbenzene 1,3,5-Trlmethy (benzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 10/28/2014 03:29 PM Analytical Method: SM 6200B NO ug/L 0.50 1 10/18/14 18:13 75-71-8 NO ug/L 0.50 1 10/18/14 18:13 75-34-3 . NO ug/L 0.50 1 10/18/1418:13 107-06-2 NO ug/L 0.50 1 10118/1418:13 75-35-4 NO ug/L 0.50 1 10/18/1418:13 156-59-2 NO ug/L 0.50 1 10/18/14 18:13 156-60-5 NO ug/L 0.50 1 10/18/14 18:13 78-87-5 ND ug/L 0.50 1 10/18/14 18:13 142-28-9 ND ug/L 0.50 1 10/18/14 18:13 594-20-7 ND ug/L 0.50 1 10/18/14 18:13 563-58-6 NO ug/L 0.50 1 10/18/14 18:13 10061-01-5 ND ug/L 0.50 1 10/18/14 18:13 10061-02-6 NO ug/L 0.50 1 10118/1418:13 108-20-3 ND ug/L 0.50 1 10/18/14 18:13 100-41-4 NO ug/L 2.0 1 101181141813 87-68-3 NO ug/L 0.50 1 1011811418:13 98-82-8 ND ug/L 2.0 1 10/1811418:13 75-09-2 ND ug/L 0.50 1 10/18/14 18:13 1634-04-4 ND ug/L 2.0 1 10/18/14 16:13 91-20-3 NO ug/L 0.50 1 1011811418:13 103-65-1 ND ug/L 0.50 1 10/1811418:13 100-42-5 ND ug/L 0.50 1 10/18/14 18:13 630-20-6 ND ug/L 0.50 1 10/18/14 18:13 79-34-5 ND ug/L 0.50 1 10/18/14 18:13 127-18-4 ND ug/L 0.50 1 10/18/14 18:13 108-88-3 ND ug/L 2.0 1 10/18/14 18:13 87-61-6 NO ug/L 2.0 1 10/1811418:13 120-82-1 NO ug/L 0.50 1 10/18/14 18:13 71-55-6 ND ug/L 0.50 1 10/18/14 18:13 79-00-5 ND ug/L 0.50 1 1011811418:13 79-01-6 NO ug/L 1.0 1 10/18/14 18:13 75-69-4 ND ug/L 0.50 1 10/18/14 18:13 96-18-4 ND ug/L 0.50 1 10118/1418:13 95-63-6 ND ug/L 0.50 1 10/18/14 18:13 108-67-8 ND ug/L 1.0 1 1011811418:13 75-01-4 NO ug/L 1.0 1 1011811418:13 179601-23-1 NO ug/L 0.50 1 10/18114 18:13 95-47-6 123 % 70-130 1 1011811418;13 17050-07-0 100 % 70-130 1 10118/1418:13 460-00-4 105 % 70-130 1 10118/1418:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 23 aceAmIgica! www.peoela6s:cmn ANALYTICAL- RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite ion Huntersville, NC 25078 (704)875-8092 Sample: MCAS MW-3 Lab ID:.•92220940003 Collected: 10/08/14 11:40 .Received: 10/1Oil 4 09:45 Matrix! Water Parameters Results Units . Report Limit_ DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 ,' 1 10/1811418:29 71-43-2 Bromobenzene ND ug/L 0.50 1 10/18/14 18:29 108-86-1 Bromochloromethane . ND ug/L 0:50 1 10/18/14 18:29 74-97-5 Bromodichloromethane ND ug/L 0:50 1 10/18/14 18:29 75-27-4 Bromofonn ND ug/L 0.50 1 10/18/14 18:29 75-25-2 Bromomethane ND ug/L 5.0 1. 10118/1418:29 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10118/1418:29 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/18/14 18:29 135-98-8 test-Butylbenzene ND ug/L 0.50 1 10118/14 18:29 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/18/14 18:29 56-23-5, Chlorobenzene ND ug%L 0'.50 11. 10/18114 18:29. 108-904 Chloroethane ND ug/L 1.0 1 10/16/14 18:29 75-00-3 Chloroform ND ug/L 0.50. 1 10/18/14 18:29 67-66-3 . Chloromethane . ND ug/L 1.0 • •1 10/18/14 18:29 74-87-3 ' 2-Chlorotoluene ND ug/L 0.50 ' .'l 10/18/14 18:29 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/18/14 18:29 106-43-4 1,2-Dibromo-3-chloropropane ND'ug/L 1.0 1 10/18/14 18:29 96-12-8 Dibromochloromelhane ND ug/L 0.50, 1 10118/1418:29 124-48-1 1,2-Dlbromoethane (EDB) ND ug/L 0.50. 1 10118114 18:29 106-93-4 Dibromomethane ND ug/L 0.50 1 10118/1418:29 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/18/1418:29 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:29 541-73-1 . 1,4-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:29 106-46-7 Dichlorodi0uoromethane ND ug/L .0.50 A 10/1811418:29 75-71-8 1,1-Dichloroethane ND ug/L . 0.50 1 10/18/14 18:29 75-34 3 1,2-Dichloroethane ND ug/L 0.50. 1 10/1811418:29 107-06-2. 1,1-Dichloroethene ND ug/L 0.50 1 10/18/14 18:29 75-354 cis-1,2-Dichloroethene ND ug/L 0.50 1 10118/1418'.29 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50. 1 10/18/14.18:20 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/18/14 18:29 78-87-5 1,3-Dichloropropane.. ND ug/L 0.50 1 10/18/141829 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/18/14 18:29 594-20-7 1,1-Dichloropropene . ND ug/L 0.50 1 10/18/1418129 563-58-6 cis-1,3-Dichloropropene . ND ug/L 0.50 1 1011811418:29 10061-01=5 trans- 1, 3-Dichloropropene ND ug/L 0.50 1 10/1811418:29 10051-02-6 Diisopropyl ether ND ug/L 0'50 1 10/18/14 18:29 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/18/14 18:29 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10118/1418:29 87-68-3 Isopropylbenzene(Cumene) .. ND ug/L 0.50 1 1Oil 8/14-18:29 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/18114 18:29 75-09-2 Methyl-tert-butyl ether, ND ug/L 0.50 1 10/18/14 18:29 1634-04-4 Naphthalene ND ug/L 2.0 1 10/18/14 18:29 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10118/1418:29 103-65-1 Styrene ND ug/L 0.50 1 10/18/1418:29 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 10/18/1418:29 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 1011811418:29 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10118/14 18:29 , 127-18-4 REPORT OF LABORATORY. ANALYSIS This report shall not be reproduced, except in full. Date: 10/28/20114 03:29PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 23 ;-alceAnalytical � wwxpece/abs.cam r ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Klncey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS MW-3 Lab ID: 92220940003 Collected: 10/0811411:40 Received: 10/10114 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ 6206B MSV Analytical Method: SM 6200B Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Tdmethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1;2-Dichioroethere-d4 (S) 4-Bromofluorobenzene (S) . Toluene-d8 (S) ND ug/L 0.50 1 10/1811418:29 108-88-3 NO ug/L 2.0 1 10/18/14 18:29 87-61-6 NO ug/L 2.0 1 10118/1418:29 120-82-1 ND ug/L 0.50 1 10/18/14 18:29 71=55-6 NO ug/L 0.50 1 10/18/14 18:29 79.00-5 ND ug/L 0.50 1 1011811418:29 79-01-6 ND ug/L 1.0 1' 10/18/14 18:29 75-69A NO ug/L 0.50 1 10/18/14 18:29 96-18A NO ug/L 0.50 1 10/18/14 18:29 95.63-6 ND ug/L 0.60 1 10/18/14 18:29 108-67.8 ND ug/L 1.0 1 10/18/14 18:29 75-01-4 ND ug1L 1:0 1 10/18/14 18:29 179601-23-1 NO ug/L 0.50 1 10118/1418:29 95-47-6 124 % 70-130 1 -10/1811418:29 17060-07-0 100 % 70-130 1 10/18/14 18:29 460-00-4 104 % 70-130 1 10118/1418:29 2037-26-5 Sample: MCAS MW-5 Lab ID: 92220940004 Collected: 10/08/14 14:35 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/18/14 18:46 71-43-2 Bromobenzene ND ugfL 0.50 1 10/18/14 18:46 108-86-1 Bromochloromethane NO ug/L 0.50 1 10/18/14 18:46 74-97-5 Bromodichioromethane ND ug/L 0.50 1 10/18/1418:46 75-27-4 . Bromoform ND ug/L 0.50 1 10/18/14 18:46, 75-25-2 Bromomethane NO ug/L 5.0 1 10118/1418:46 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10118/1418:46 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/18/14 18:46 135-98-8 terl-Butylbenzene ND ug/L 0.50 1 10118/1418:46 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 1011811418:46 56-23-5 Chlorobenzene ND ug/L 0.60 1 10118/14 18:46 108-90-7 Chloroethane ND ug/L 1.0 1 10/18/14 18:46 75-00-3 Chloroform ND ug/L 0.50 1 10/1811418:46 67-66-3 Chloromethane ND ug/L. 1.0 1 10/18/14 18:46 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/18/14 18:46 95-49-8 4-Chlorotoluene ND .ug/L 0.50 1 10/18/14 18:46 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/18/14 18:46 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10/18/14 18:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/18/14 18:46 108-93-4 Dibromomethane ND ug/L 0.50 1 10/1811418.46 74-95-3 1.2-Dichlorobenzene ND ug/L 0.50 1 10/1811418:46 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/18/1418.45 541-73-1 IA-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:46 1M-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/2812014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 23 aceAnalytical xwwpscefebs.com ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS MW-5 Parameters Lab ID: 92220940004 Collected: 10/08/14 14:35 Results . Units Report Limit DF Received: 10110114 09:45 Matrix: Water Prepared Analyzed CAS No. Qua[ 6200B MSV Analytical Method: SM 6200B Dichlorodifluoromethane ND ug/L 0.50 1 10/18/14 18:46 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 10/18/14 18:46 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/18/14 18:46 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/18/14 18:46 75-35-4 cis- 1,2-Dichloroelhene ND ug/L 0.50 1 10/18/14 18:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/18/14 18:46 156-60.5 1,2-Dichloropropane ND ug/L 0.50 1 10110/1418:46 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/18/14 18:46 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/18/14 18:46 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/1811418:46 563-58-6 cis- 1, 3-Dichloropropene ND ug/L 0.50 1 10/1811418:46 10061-01-5 trans- l,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:46 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10118/14 18:46 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/1811418:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/18/14 18:46 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 10/18/14 18:46 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/18/14 18:46 75-09-2 Methyl -tent -butyl ether ND ug/L 0.50 1 10/18/14 18:46 1634-04-4 Naphthalene ND ug/L 2.0 1 10/18/14 18:46 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10118/1418:46 103-65-1 Styrene ND ug/L 0.50 1 10/18/14 18:46 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 10/18/14 18:46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 1011811418:46 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/18/14 18:46 127-18-4 Toluene ND ug/L 0.50 1 10/18/14 18:46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/18/14 18:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10118/1418:46 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 10/1811418:46 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/1811418:46 79-00-5 Trichloroethene ND ug/L 0:50 1 1011811418:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/18/14 18:46 75-69.4 1,2,3-Trichloropropane ND ug/L 0.50 1 10/18/14 18:46 96-18-4 1,2,4-Trimethylben7ene ND ug/L 0.50 1 1011811418:46 95-63-6 1,3,5-Trime1hylbenzene ND ug/L 0.50 1 10/1811418:46 10M7-8 Vinyl chloride ND ug/L 1.0 1 10/18/14 18:46 75-01-4 . m&p-Xylene ND ug/L 1.0 1 1011811418:46 179601-23-1 o-Xylene ND ug/L 0.50 1 10M8/14 18:46 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 124 % 70-130 1 10/18/14 18:46 17060-07-0 4-Bromofluorobenzene (S) 100 % 70-130 1 10/18/14 18:46 460-00-4 Toluene -dB (S) 104 % 70-130 1 1011811418:46 2037-26-5 Date: 10/28/2014 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 23 R UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533.0003 IN REPLY REFER TO: 5090/07109 LN October 31, 2014 North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center 1617 Mail Service Center Raleigh, NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MCAS Cherry Point's Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the original and one copy of the GW-59-A report and the four GW=59 reports. (one each for monitoring wells 1, 2, 3, and 8) for the triennial reporting for October 2014. Should you have any questions, please contact Mr. Timothy Lawrence, PE of the Environmental Affairs Department at your earliest convenience at (252) 466-2754. Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-59 for MW-5 (6) Lab Report Sincerely, W. O Envir n ent 1 A airs Officer By dire ti of the Commanding Officer GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489 (Submit one each monitoringReriod with GW-59forms.) Enter date monitoring results were due. 11D /14 Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO, 1 the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question I or 2 is "YF,S", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown, etc.)? if the answer is "Yes ", contact the Regional guidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituents) and conecntration(s) exceeding standards in the space provided below: MW-I Chloroform 4.7 ug/l, MW-2 NIB 1.73 mg/I, ' !NW-5 NH3 2.99 m /L For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) YES NO 5 in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section S. _ If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MVH-5: Feb. 2014 NH3 3.13, June 2013 NH3 2.45; Feb. 2013 NH3 2.25 MW-2: Feb. 2014 NH3 2.97; Oct 2013 NH3 2.95; Feb 2013 NH3 1.74 6 Are the monitoring.wells listed in section 5 located at or beyond the review boundary? YES NO X Irthe answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells nay be improperly located; contact the Regional Otiice. Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this ficility Failure to do so may subject the nermittee to it Notice of Violation, fines, and/or penalties. The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with 11 GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby icknowledge that the above infoni aiion was evaluated and the information s%lwtted in this report•(Corripllance Report OW-59A) is true and cotiiplete to the best of my knt Qa dge. Patricia T. Davis, Utility Systems Operator Supervisor Signature of Permittee (or Authorized Agent) Date 10/30/ 0014 SUBMIT FORM ON YELLOW -PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Facility Name: MCAS Cherry Point _ Permit Name (if different): Facility Address: MCAS Cherry Point, NC 28533-0006 or Type County: Craven act Person: Patricia T. Davis v Telephone #: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: 1 v •!..}ems• vr,�r�p�nvrrmary I onN7UKAL KtSVUKGtS •., .., DIVISION;OF WATER QUALITY -INFORMATION PROCESSING UNIT 1.1617•MAIL'SERVICE CENTER' J. RALEIGH; NC`27699-161T r PHONE: (9191733-3221 •—^••••• ^•••••��•• cwruauvn vaar: (/J I/GV 17 Non -Discharge UIC NPDES WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediatlon: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Q Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-1 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 26.65 11- Well Diameter. 2 pH 00400 5.96 units Temp 00010: 25 eC DRY at Depth to Water Level 82546: 3.5 ft. below measuring point Screened Interval: -0.17 fl. to -15.2 ft. Spec. Cond. 00094: 108 pMhos time of Measuring Point Is 1.33 ft. above land surface Relative M.P. Elevation: 10.78 Odor 00085: none sampling, check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: Samples for metals were collected unfiltered ❑YES. ❑ NO and field acidified ❑ YES ❑ NO ❑ LABORATORY INFORMATION Date sample analyzed: 10/8/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 CA NOTE: values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620. <0.05 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MFNmethod for highly turwdsomplas) Orthophosphate70507• mg/L Dissolved Solids: Total 70300 64 _ mg/L Al - Aluminum 01106 mg/L pH (Lab) 00403 5.96 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils•00552 mg/L Cy - Copper 01042 mg/L Pheno132730 µg/L Fe- Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 <1.0 _ mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NNE as N; Ammonia Nitrogen, Totaq Mn - Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 Yes(1) ❑ No (0) VOC Method# SM 6200B Method# Method#, Method# For Remedlation Systems Only Reports): Influent T. •Cs: Effluent Total VOCs:• • . I certify that to the best of my kriowiedge and belief, the in urination sti�bmilted In'this repoii s lrbe,�acc�ri(e; iantl c' mplele andStl al ii a labor'atoiy ana�y(icai data Chas prblduced using approved method+s of a alysis by a t, DVI+Q•ce ti(Ied laboratory. I am aware that there are sigr if cant per.ail�es for submitting fats informal(onI incliiding t e posrsibdiiy or fines and impins nment.for noyving vi Ilaiions. l 1 GW-59 Rev. 2/2 1 • SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - Please Print Clearly or -Type Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: MCAS Cherry Point, NC 28533-0006 County: Craven (stet.) (A) act Person: Patricia_ T. Davin Telephone#: 252-466-4599 Location/Site Name. Site 21, MCAS Chevy Point No.of Wells to be Sampled: 1 trtom DPRIR -- vr\e\L 1\L'vV VRVI�A, DIVISION.OF WATER QUALRY-INFORMATION PROCESSING UNIT' 161ZMAIL SERVICE CENTER RA[.E1G9; NC•27699-1617 : PHONE: (919)733.322 .—.•••••• ••�•••��•. �ANuuuvn Wdle: 1fO I/GU -IU Non -Discharge UIC NPDES WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon - ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remedlation:. ❑ Rotary Distributor ❑✓ Land Application of Sludge ❑ Water Source beat Pump ❑ Other: SAMPLING INFORMATION - If WELL WELL ID NUMBER (From Permit): MW-2 Date Sample Collected: 10/812014 FIELD ANALYSIS, WAS Well Depth 26.58 ft. Well Diameter. 2 pH 00400 6.29 units Temp 00610: 23 aC DRY at Depth to Water Level 82546; 6.5 ft below measurin p g point Screened Interval: -1.03 ft. to -11 ft. Spec. Cond. 00094: 713 .µMhos time of ! Measuring Point is 1.28 .ft. above land surface Relative M.P. Elevation: 14.8 Odor 00085: none sampling, check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: Samples for metals were collected unfiltered ❑ YES NO and field acidified [I YES ❑ NO ❑ LABORATORY INFORMATION Date sample analyzed: 10/8/2014 Laboratory Name:_ MCAS Cherry Point I Pace Analytical Certification Number. 201137706 PARAMETERS NOTEV 1 h Id a ues s ou reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.05 mg/L Coiiform: MF Total 31504 /100mL Phosphorus: Total as P 00665Y mg/L (Note: Use MPN melhad for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70.300. 160 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.29 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L . Chromium: 'Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 lig/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 1.73 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen: NH, as N: Ammonia Nitrogen. Total) Mn - Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 )iglL Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACK LAB REPORT.) Lab Report Attached? Q Yes(1) ❑ No.(0) VOC Method# SM 6200B Method# Method# Method# For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removaia/o Patricia T. Davis -,Utility Systems Operator 10I3012014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: 'MCAS Cherry Point, NC 28533-0006 SUBMIT FORM ON YELLOW PAPER ONLY t DEPARTME or Type County: Craven Contact Person: Patricia T. Davis Telephone #: 252-466-4599 Well Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled: tnom SAMPLING INFORMATION WELL ID NUMBER (From Permlt): MW-3 Well Depth 25.58 ft. Depth to Water Level 82546: 0 ft. below measuring point Measuring Point is 1.46 ft. above land surface Volume of water pumped/bailed before sampling: 5 Gal. Samples for metals were collected unfiltered ❑ YES n NO LABORATORY INFORMATION 1617• MAIL SERVICE•CENTER FIXtAlGH; NC 27699-1617 . PROCESSING UNIT PHONE: 01911733-3 Non -Discharge UIC NPDES WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑Remediation: Infiltration Gallery ❑ spray Field ❑ Remediation: . ❑ Rotary Distributor Q Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date Sample Collected: 10/8/2014 Well Diameter. 2 Screened Interval: -11.7 ft. to -21"7 ft. Relative M.P. Elevation: 3.1 field acidified If WELL FIELD ANALYSIS: WAS pH 00400 6.32 units Temp 00010: 25 oC DRY at time of Spec. Cond. 00094: 301 µMhos sampling, Odor 00085: stagnant check Appearance: turbid- here: ❑ Date sample analyzed:' 10/8/2014 Laboratory Name: MCAS Cherry. Point / Pace Analytical Certification Number: 201 1.37706 ZAMETERS NOTE: Values should reflect dissolved and colloidal concentratlon s. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 1100ml- Nitrate (NO3) as N'00620 <0.05 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note; use MPH method for Eighty turbid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 160 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.32 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 1.13 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 µg/L TKN as N 00625 mg/L . Ni - Nickel 01067 µg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) ,Lab Report Attached? Yes(1) ❑ No (0) VOC , Method# SM 6200B Method# Method# Method# For Remediation Systems Only (Attach Lab Reportsy Influent Total VOCs: Effluent Total VOCs: VOC Removal°/a Patricia T. Davis - Utility Systems Operator10/3o/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: MCAS Cherry Point, NC 28533-0006 County: Craven act Person: Patricia T. Davis Telephone #: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point. No.of Wells to be Sampled: :1i DIVISION OF WATER-QUALITY-INOORMA "1617.IYIAIL SERVICE CENTER.-:'.- ; RALEIGH,'NC.27699=1617 ' PROCESSING UNIT . PHONE: (9'191733-3221 Non -Discharge UIC NPDES _ WQ0001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED' ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field E] Remediation: ❑ Rotary Distributor [?] Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (From Permit): MW-5 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 13 ft. Well Diameter: 2 pH 00400 6.55 units Temp 00010: 29 uC DRY at Depth to Water Level 82546: 9 R. below measuring point Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: 741 µMhos of. Measuring Point is 3 fl. above land surface Relative M.P. Elevation: 12 Odor 00985: none sampling, check Volume of water pumped/bailed before sampling: 5 Gal. Appearance: clear here: Sam les for metals were collected unfiltered YES _ ❑ NO and field acidified n YES n . NO ❑ LABORATORY INFORMATION Date sample analyzed: 10/8/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical .Certification Number: 201 / 37706 nw RANIETERS NOTE. Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1- /100mL Nitrate (NO3).as N 00620 <0.05 1.mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPNmethod for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 274 mg/L, Al = Aluminum 01105 mg/L pH (Lab) 00403 6.55 units Ba - Barium 01007 itg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L .Chloride 00940 10.4 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 pg/L Chromium: Total 01034 µglL Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 2.99 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonla Nitrogen, Totaq Mn - Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 pg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC,.GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? El Yes('I) ❑ No (0) VOC Method# SM 6200B Method# Method* Method# For Remediation Systems Only .. • t I I t ry • = f. 1 Il�I r'il Itl vt• I` , Ir +r I 1 �' " 't �7 I certify that to the best of my knowledge and ,bdiet, the inlf Irmal on s bmil!ed in this repori Is true accur Izt alInd co plele,'ai d (flat the laboratory, dInalylical data ��as prAjded uslno 6pproved methods of an lysis by a DWG-cedified laboraloy. I am aavare that there are s gnitcant penaltlLjfor submitting false inform lion, nclUdir�g tl�e poss;bility oflfines and imprllsdnment for kno,ving y" lations. Patricia T. Davis - Vtility Systems • •10/30/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 212010 Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC,.GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? El Yes('I) ❑ No (0) VOC Method# SM 6200B Method# Method* Method# For Remediation Systems Only .. • t I I t ry • = f. 1 Il�I r'il Itl vt• I` , Ir +r I 1 �' " 't �7 I certify that to the best of my knowledge and ,bdiet, the inlf Irmal on s bmil!ed in this repori Is true accur Izt alInd co plele,'ai d (flat the laboratory, dInalylical data ��as prAjded uslno 6pproved methods of an lysis by a DWG-cedified laboraloy. I am aavare that there are s gnitcant penaltlLjfor submitting false inform lion, nclUdir�g tl�e poss;bility oflfines and imprllsdnment for kno,ving y" lations. Patricia T. Davis - Vtility Systems • •10/30/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 212010 A aceAnalyiical msw.psca;abs.cotn ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 1Q0 Huntersville, NC 26078 (704)875-9092 Sample: MCAS MW-1 Lab ID: 92220940001 Collected: 10/08/14 11:05 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV . Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/15/14 08:11 71-43-2 Bromobenzene ND ug/L 0.50 1 10/15/14 08:11 108-86-1 Bromochloromethane N❑ ug/L 0.50 1 10115/14 08:11 74-97-5 Bromodichloromethane ND ug/L 0.50 1. 10/15/14 08:11 75-27-4 Bromofonn ND ug/L 0.50 1 10/15/14 08:11 75-25-2 Bromomethane ND ug/L 5.0 1 10/15/14 08:11 74-83.9 n-Butylbenzene ND ug/L 0.50 1 10/15/14 08:11 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/16/14 08:11 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 1011511408:11 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/15/14 08:11 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/15/14 08:11 108-90-7 Chioroethane ND ug/L 1.0 1 10/15/14 08:11 75-00-3 Chloroform 4.7 ug/L 0.50 1 10115/14 08:11 67-66-3 Chloromethane ND ug/L 1.0 1 10/15/14 08:11 74-87-3 2-Chlorotoluene ND ug1L 0.50 1 10/15/14 08:11 95-49-8 4-Chlorotoluene ND ugfL 0.50 1 10/15/14 08:11 106-43-4 1,2-Dibromo-3-chforopropane ND ug1L 1.0 1 10/15/14 08:11 96-12-8 Dibromochloromethane - ND ug/L 0.50 1 10/15/14 08:11 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/15/14 08:11 106-93-4 Dibromometha,ne ND ug/L 0.50 1 10/15114 08:11 74-95-3 1.2-Dichtorobenzene ND ug/L 0.50 1 10/15/14 08:11 95-50-1 1,3-Dichiorobenzene ND ug/L 0.50 1 10/15/14 08:11 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/15/14 08:11 108-46-7 Dichlorodifluoromethane ND ugiL 0.50 1 10/15/14 08:11 75-71-8 1,1-Dichloroethene ND ug/L 0.50 1 10/1511408:11 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/15/14 08:11 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/15/14 08:11 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/1511408:11 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/15/14 08:11 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/15/14 08:11 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/15/14 08:11 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/15/14 08:11 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/1511408:11 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 10/1511408:11 10061.01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 10/15/14 08:11 10061-02-6 Dilsopropyl ether ND ug/L 0.50 1 10/15/14 08:11 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/15/14 08:11 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/15/14 08:11 87-68-3 Isopropyibenzene (Cumene) ND ug/L 0.50 1 10/15/14 08:11 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/15/14 08:11 75-09-2 Methyl-terf-butyl ether ND ug/L 0.50 1 10/15/14 08:11 1634-04-4 Naphthalene ND ug/L 2.0 1 10/15/14 08:11 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10115/14 08:11 103-65-1 Styrene ND ug/L 0.50 1 10115/14 08:11 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 1011511408:11 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 1 Ott 5114 08:11 79-34-5 Tetrachlorcethene ND ug/L 0.50 1 10/15/14 08:11 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 23 aceAnalylical waw.pacelebs.C= ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MCAS MW-1 Parameters Lab ID: 92220940DOI Collected: 10/08/14 11:05 Results Units Report Limit OF Received: 10/10/14 09:45 Matrix: Water Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Toluene ND ug/L 0.50 1 10/15/14 08:11 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/15/14 08:11 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/15/14 08:11 120-82-1 1,1,1-Trichloroethane NO ug/L 0.50 1 10/15/14 08:11 71-55-6 1,1,2=Trichloroethane ND ug/L 0.50 1 10/15/14 08:11 79-00-5 Trichloroethene ND ug/L 0.50 1 10/15/14 08:11 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/15/14 08:11 75-69-4 1,2,3-Tdchloropropane ND ug/L 0.50 1 10/15/14 08:11 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10/15/14 08:11 95-63-6 1,3,5-Trimethylbenzene ND uglL 0.50 1 10/15/14 08:11 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/15/14 08:11 75-01-4 map-Xylene NO ug/L 1.0 1 10/15/14 08:11 179601-23-1 o-Xylene NO ug/L 0.50 1 10/15/14 08:11 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 105 % 70-130 1 10/15/14 08:11 17060.07-0 4-BromoAuorobenzene (S) 9.8 % 70-130 1 10/15/14 08:11 460-00-4 Toluene-d8 (S) 104 % 70-130 1 10/15/14 08:11 2037-26-5 Sample: MCAS MW-2 Lab ID: 92220940002 Collected: 10/08/14 10:20 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed .CAS No. Qua[ 6200B MSV Analytical Method: SM 62008 Benzene ND ug/L 0.50 1 10118/14 18:13 71-43-2 Bromobenzene ND ug/L 0.50 1 10/18/14 18:13 108-86-1 Bromochloromethane ND'ug/L 0.50 1 10/1811418:13 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/18/14 18:13 75-27-4 Bromoform NO ug/L 0.50 1 10/18/14 18:13 75-25-2 Bromomethane ND ug/L 5.0 1 10/18/14 18:13 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 98-05-6 Carbon tetrachloride NO, ug/L 0.50 1 10/18/14 18:13 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:13 108-90-7 Chloroethane NO ug/L 1.0 1 1011811418:13 75-DO-3 Chloroform ND ug/L 0.50 1 10/18/14 18:13 67-66-3 Chloromelhane ND ug/L 1.0 1 10/18/14 18:13 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/18/14 18:13 95-49-8 4-Chlorotoluene ND ug/L 050 1 10118/1418:13 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/18/14 18:13 96-12-8 Dibromochloromethane ND ug/L 0.50 1 1011811418:13 124-48-1 i,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/18/14 18:13 106-93-4 Dibromomethane ND ug/L 0.50 1 10/18/14 18:13 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/18114 18: 13 95-50-1 1,3-Dichloro6enzene ND ug/L 0.50 1 10/18/14 18:13 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:13 106-46-7 Date: 10/28/2014 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 23 1_,,Kace Analytical aww.psce/ebs.com i Project: MW Pace Project No.: 92220940 Sample: MCAS MW-2 Parameters 62008 MSV Dichlorodifluoromethane 1,1-Dichlaroethane 1,2-Dichloroethane .1,1-Dichloroethene cis-1,2-Dichicroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichloro benzene 1,1,1-Tdchloroethane 1,1,2-Tdchloroethane Trichloroethene Trichlorofluoro methane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichloroethane-d4 (S) 4-Bromoflucrobenzene (S) Toluene-d8 (S) Date: 10/28/2014 03:29 PM Pace Analytical Services, Inc, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92220940002 Collected: 10/08/14 10:20 Received: 10/10/14 09:45 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Analytical Method: SM 6200B ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND Ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND uglL ND ug/L ND ug/L ND ug/L 123 % 100 % 105 % 0.50 1 10/18/14 18:13 75-71-8 0.50 1 10/18/14 18:13 75-34-3 0.50 1 10/18/14 18:13 107-06-2 0.50 1 10/1811418:13 75-35-4 0.50 1 10/18/14 18:13 156-59-2 0.50 1 10/1 B/14 18:13 156-60-5 0.50 1 10/1811418:13 78-B7-5 0.50 1 10/18/14 18:13 142-28-9 0.50 1 10/1811418:13 594-20.7 0.50 1 10/18/14 18:13 563-58-6 0.50 1 10/18/14 18:13 10061-01-5 0.50 1 10/18/14 18:13 10061-02-6 0.50 1 10/18/14 18:13 108-20-3 0.50 1 10/18/14 18:13 100-41-4 2.0 1 10/18/1418:13 87-6B-3 0.50 1 10/1811418:13 98-82-8 2.0 1 10/1811418:13 75-09-2 0.50 1 10/18/14 18:13 1634-04-4 2.0 1 10/18/14 18:13 91-20-3 0.50 1 10/18/14 18:13 103-65-1 0.50 1 10/18/14 18:13 100-42-5 0.50 1 10/18/14 18:13 630-20-6 0.50 1 10118/1418:13 79-34-5 0.50 1 10/18/14 18:13 127-18-4 0.50 1 10/18/14 18:13 108.88-3 2.0 1 10/18/1.418:15 87-61-6 2.0 1 10/18/14 18:13 120-82-1 0.50 1 10/18/14 18:13 71-55-6 0.50 1 10/18/14 18:13 79-00-5 0.50 1 10/18/14 18:13 79-01-6 1.0 1 1011811418:13 75-69-4 0.50 1 10/18/14 18:13 96-18-4 0.50 1 10/18/14 18:13 95-63-6 0.50 1 10/1811418:13 108.67-8 1.0 1 10/18/14 18:13 75-01-4 1.0 1 10/18/14 16:13 179601-23-1 0.50 1 10/18/14 18:13 95-47-6 70-130 1 10/18/14 18:13 17060-07-0 70-130 1 1011811418:13 460.00-4 70-130 1 10/18/14 18:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Without the written consent of Pace Analytical Services, Inc.. Qual Page 6 of 23 aceAnalytical xwwpecelaDs.mm ANALYTICAL RESULTS Project: MW 'Pace Project No.: 92220940 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Sample: MCAS MW-3 Lab ID: 92220940003 Collected: 10/06/14 11:40 Received: 10110114 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Benzene NO ug/L 0.50 1 10/16/14 18:29 71-43-2 Bromobenzene NO ug/L 0.50 1 10/18/14 18:29 108-B6-1 Bromochloromethane ND ug/L 0.50 1 10/18/14 18:29 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/18/14 18:29 75-27-4 Bromoform NO ug/L 0.50 1 10/18/14 18:29 75-25-2 Bromomethane NO ug1L 5.0 1 10/1 B/1418:29 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/18/14 18:29 104-51-8 sec-Butylbenzene NO ug/L 0.50 1 1011811418:29 135-98-8 tert-Butylbenzene NO ug/L 0.50 1 10118/14 18:29 9B-06-6 Carbon tetrachloride NO ug/L 0.50 1 10/18/14 18:29 56-23-5 Chloroberizene ND ug/L 0.50 1 10/18/14 18:29 108-90-7 Chloroethane ND ug/L 1.0 1 10/16/14 18:29 75-00-3 Chloroform ND ug/L 0.50 1 10/18/14 18:29 67-66-3 Chloromethane ND ug/L 1.0 1 10/18/14 18:29 74-87-3 2-Chlorotoluene NO ug/L 0.50 1 10/1811418:29 95-49-8 4-Chlorotoluene NO ug/L 0.50 1 10118/1418:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/18/14 18:29 96-12-8 Dibromochloromethane NO ug/L 0.50 1 10/18/14 18:29 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 0.50 1 10/18/14 1,8:29 106-93-4 Dibromomethane NO ug/L 0.50 1 10/18/14 18:29 74-95-3 1,2-Dichlorobenzene NO ug/L_ 0.50 1 10/18/1418:29 95-50-1 1,3-Dichlorobenzene NO ug/L 0.50 1 10/1811418:29 541-73-1 1,4-Dichlorobenzene NO ug/L 0.50 1 10118/1418:29 106-46-7 Dichlorodiiluoromethane ND ug/L 0.50 1 1011811418:29 75-71-8 . 1,1-Dichloroethane NO ug/L 0.50 1 10118/1418:29 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/1811418:20 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/1811418:29 75-35.4 cis-1,2-Dichloroethene NO ug/L 0.50 1 10/18/14 18:29 156-59-2 trans-1,2-Dichloroethene NO ug/L 0.50 1 10/1811418:29 156-60-5 1,2-Dichloropropane NO ug/L 0.50 1 10/16/14 18:29 7B-87-5 1,3-Dichloropropane NO ug/L 0.50 1 10/181141829 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 . 10/1811418:29 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/18/14 18:29 563-58-6 cis- 1,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:29 10061-01-5 trans- 1, 3-Dichloropropene NO ug/L 0,50 1 10/18/14 18:29 10061=02-6 Diisopropyl ether ND .ug/L 0.50 1 10/18/14 18:29 108-20-3 Ethylbenzene NO ug/L 0.50 1 10/18/14 18:29 100-41-4 Hexachloro-1,3-butadiene NO ug/L 2.0 1 10/18/14 18:29 87-68-3, Isopropylbenzene (Cumene) ND ug/L 0.50 1 10/16/14 18:29 98-82-8 Methylene Chloride NO ug/L 2.0 1 10/*18114 18:29 75-09-2 Methyl-tert-butyl ether NO ug/L' 0.50 1 10/18/14 18:29 1634-04-4. Naphthalene ND ug/L 2.0 1 10/18/14 18:29 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/18/14 18:29 103-65-1 Styrene NO. ug/L 0.50 1 10/18/14 18:29 100-42-5 1,1,1,2-Tetrachloroethane NO ug/L 0.50 1 10/18/1418:29 630-206 - 1,1,2,2-Tetrachloroethane IVD ug/L D.50 1 1011811418:29 79-34-5 Telrachloroethene NO ug/L 0.50 1 10/18/14 18:29 127-18-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 23 Pace Analytical Services, Inc. a7ceAnalytieal m 9800Huntersville, NC 28078 wwwpacelabs.carn i (704)875-9092 ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: MCAS RAW-3 Lab iD: 92220940003 Collected: 10/08/1411:40 Received: 1 D/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[ 6200B'MSV Analytical Method: SM 6200B Toluene NO ug/L 0.50 1 10/18/14 18:29. 108-88-3 1,2,3-Trichlorobenzene NO ug/L 2.0 1 10/18/14 18:29 87-61-6 1,2,4-Trichlorobenzene NO ug/L 2.0 1 1011811418:29 120-82-1 11,1-Trichloroethane NO ug/L 0.50 1 10/18/14 18:29 71-55-6 1,1,2-Trichloroethane NO ug/L 0.50 1 10/18/14 18:29 79-00-5 Trichtoroethene NO ug/L 0.50 1 10/18/14 18:29 79-01-6 Trichlorofluoromethane NO ug/L 1.0 1 10/18/14 18:29 75-69A 1,2,3-Trichloropropane NO ug/L 0.50 1 10/18/14 18:29 96-18A 1,2,4-Trimethylbenzene NO ug/L 0.50 1 10/18/14 18:29 95-63-6 1,35-Trimethyfbenzene NO ug/L 0.50 1 1011811418:29 108-67-8 Vinyl chloride ND ug/L 1.0 1 10118/1418:29 75-01-4 m&p-Xylene NO ug/L 1.0 1 10118/1418:29 179601-23-1 o-Xylene NO ug/L 0.50 1 10118/1418:29 95-47-6 Surrogates 1,2-Dichloroethene=d4 (S) 124 % 70-130 1 1011811418:29 1706D-07-0 4-Bromofluorobenzene (S) 100 % 70-130 1 10/18114 18:29 460-00-4 Toluene-d8 (S) 104 % 70-130 1 10/18/14 18:29 2037-26-5 Sample: MCAS MW-5 Lab ID: 92220940004 Collected: 10/08/14 14:35 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua] 6200B MSV Analytical Method: SM 6200B Benzene NO ug/L 0.50 1 10/18/14 18:46 71-43-2 Bromobenzene NO ug/L 0.50 1 10/1811418:46 108-86-1 Bromochloromethane IND ug/L 0.50 1 10/18/14 18:46 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/1811418:46 75-27-4 Bromoform ND dg/L 0.50 1 10/18/14 18:46 75-25-2' Bromomethane ND ug/L 5.0 1 10/18/14 18:46 74-83-9 n-Butylbenzene NO ug/L 0.50 1 10/18/14 18:46 104-51-8 sec-Butylbenzene NO ug/L 0.50 1 10/18/14 18:46 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 10118/1418:46 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/18/14 18:46 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:46 108-90-7 Chioroethane ND ug/L 1.0 .1 10/18/14 18A6 75-000.3 Chloroform ND ug/L 0.50 1 10/181.1418:46 67-66-3 Chloromethane NO ug/L 1:0 1 10/18/14 18:46 74-87-3 2-Chlorotoluene NO ug/L 0.50 1 10/18/14 18:46 95-49-8 4-Chlorotoluene NO ug/L 0.50 1 10/18/14 18:46 105-43-4 hloropropane 1,2-Dibromo-3-c ND ug/L 1.0 1 10/18/14 18:46 96-12-8 Dibromochloromethane NO ug/L 0.50 1 10/18/14 18:46 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/1S/14 18:45 1D6-93-4 Dibromomethane NO ug/L 0.50 1 10118/1418:46 74-95-3 1.2-Dichlorobenzene ND ug/L 0.50 1 1011811418:46 95-50-1 1.,3-Dichlarobenzene ND ug/L 0.50 1 10/18/14 18:46 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:46 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/28/2014 03:29 PM without the written consent of PaceAnalytical Services, Inc.. Page 8 of 23- ' e _ aeei4lpscsfa com www.pacelabs.com Project: MW Pace Project No.: 92220940 " ANALYTICAL RESULTS Pace Analytical, Services, Ific. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092' Sample: MCAS MW-5 Lab ID: 92220940004 Collected: 10/08/14 14:35 Received: 10110114 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 62008 MSV Analytical Method: SM 6200B Dichlorodifluoromethane ND ug/L 0.50 1 10/18/14 18:46 75-71.8 1,1-Dichloroethane ND ug/L 0.50 1 1011811418:46 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/18/14 18:46 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/18/14 18:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/18/1418:46 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/18/14 18:46 156-60.5 1,2-Dichloropropane ND ug/L 0.50 1 10/18/14 18:46 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 1011811418:46 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/18/1418:46 594-20-7 1,1-Dichloropropene ND uglL' 0.50 1 10/1811418:46 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 10/18/1418,46 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:46 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/18/14 18:46 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/18/14 18:46 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/18/14 18:46' 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 10118/1418:46 98-82-8 Methylene Chloride ' ND ug/L 2.0 1 10/18/14 18:46 75-09-2 Methyl -tent -butyl ether ND ug/L - 0.50 1 10/18/14 18:46 1634-04-4 Naphthalene ND ug/L 2.0 1 10/18/14 18:46 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/18/14 18:46 103-65-1 Styrene ND ug/L 0.50 1 10/1811418:46 100-42-5 1. 1. 1, 2-Tetrachloroethane ND ug/L 0.50 1 10118/14 18;46 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/1811418:46 79-34-5 Tetrachloroethene ND ug/L . 0.50 1 10/18/14 18:46 127-18-4 Toluene ND ug/L 0.50 1 10/18/14 18;46 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10118/1418:46 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10118/1418:46 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 1011811418:46 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 1011811418:46 79-00-5 Trchloroethene ND ug/L 0,50 1 10118/1418:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/1811418:46 _75-69-4 1,2,3-Tdchloropropane ND ug/L 0.50 1 1011811418:46 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10118/1410:46 95-63-6 1,3,5-Trimethyibenzene ND ug/L 0.50 1 1011811418:46 108-67-8 Vinyl chloride ND ug/L 1.0 1, 10/18/14 18:46 75-61-4 . m&p-Xylene ND ug/L 1.0 1 10118/1418:46 179601-23-1 o-Xylene ND ug/L 0.50 " 1 1011811418:46 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 124 % 70-130 1 10/18/14 18:46 17060-07-0 4-Bromofluorobenzene (S) .100 % 70-130 1 10/18/14 18:46 460-00-4 Toluene-d8 (S) 104 % 70-130 1 10/18/14 18:46 2037-26-5 Date: 10/28/2014 03:29 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 23 , 1. UNITED STATES MARINE CORPS MARINE CORPS AIR STATION POSTAL SERVICE CENTER 8003 CHERRY POINT, NORTH CAROLINA 28533-0003 IN REPLY REFER TO: 5090/07109 LN October 31, 2014 North Carolina Department of Environment and Natural Resources Division of Water Quality Information Processing Center. 1617 Mail Service Center Raleigh, NC 27699-1617 Subj: TRIENNIAL GROUNDWATER MONITORING In accordance with the groundwater monitoring and reporting requirements of MICAS Cherry Point:s.Non-NPDES permit WQ0001489 for Land Application of Wastewater Residuals, enclosed are the original and one copy of the GW-59-A report and the four G;%7-59 reports (one each for monitoring wells 1, 2, 3, and 5) for the triennial reporting for October 2014. Should you'have any questions, please contact Mr. Timothy Lawrence, PE'.of the Environmental Affairs Department at your earliest convenience at (252) 466-2754. Sincerely, fO n ent I A airs Officer re ti of the r Commanding Officer Enclosure: (1) GW-59-A (2) GW-59 for MW-1 (3) GW-59 for MW-2 (4) GW-59 for MW-3 (5) GW-59 for MW-5 ( 6 ) Lab. Report GW-59A COMPLIANCE REPORT FORM Permit # WQ0001489 (Submit one each monitoring period with GW-59 Enter date monitoring results were due. 11/31/14) Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO 1 the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO X IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO 3 identification plate, area overgrown,, etc.)? If the answer is "Yes", contaci the Regional Ofricefor guidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO X If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constitucnt(s) and conccntration(s) exceeding standards in the space provided below MW-I Chloroform 4.7 ug/l, MW-2 N113 1.73 n►g/l, MW-5 NH3 2.99 m /L For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) YES NO 5 in the same well(s) in the last two years? X If the answer to question 5 is "NU", skip to section S. If the answerto question 5 is "YES", list in the space provided below, each well with constituenl(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW-5: Feb. 2014 NH3 3.13; June 2013 NH3 2.45; Feb. 2013 NH3 2.25 MW-2: Feb. 2014 NH3 2.97; Oct 2013 NH3 2.95; Feb 2013 NH3 1.74 6 Are the monitoring welts listed ire section 5 located at or beyond the review boundary? YES NO X Ir the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL, OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells moy be improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this groundwater quality YES NO 7 problem? X If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is *'NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the nermittee to a Notice of Violation, fines, and/or penalties. The person completing this portion (GW-59A) ol'the monitoring report should sign below and submit this form with S GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acltnowledge that the above informaton was evaluated and the information sii Witted in this rep ort•(Compliiance Report OW-59A) is true and cortiplete to the best of my knoir&dge, Patricia T. Davis, Utility Systems Operator Supervisor ,J Signature of Permittee (or Authorized Agent) Date I OB 0/2014 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: MCAS Cherry Point, NC 28633-0006 SUBMIT FORM ON YELLOW PAPER ONLY Clearly or Type County: Craven act Person: Patricia T. Davis Telephone #: 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point No.of Wells to be Sampled: SAMPLING INFORMATION WELL ID NUMBER (From Permit): , MW-1 Well Depth 26.66 ft- Depth to Water Level 82546: 3.5 ft. below measuring point Measuring Point Is " 1.33 ft. above land surface Volume of water pumped/bailed before sampling: 5 Gal. Samples for metals were collected unfiltered ❑ Y ES LABORATORY INFORMATION I apmwaaan 1 a lanr uKNL KCSUUKG t� •., ;:, I QUALIIY-IQIFORMATION PROCESSING UNIT CENTER •.�; • . 1ti77 PHONE: (919)733-3221 n-r�rsenarge UIC DES W00001489 Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: infiltration Gallery ❑ Spray Field ❑ Remedlation: ❑ Rotary Distributor Q Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date Sample Collected: 10/8/2014 Well Diameter: 2 Screened Interval: -0.17 ft. to -15.2 ft. Relative M.P. Elevation: 10.78 acidified If WELL FIELD ANALYSIS: WAS pH'00400 5.96 units Temp 00010: 25 °C DRY at Spec. Cond. 00094: 108 _pMhos time of sampling, Odor00085: none check Appearance: clear here: ❑ e sample ana(yzeo: 1u/tt/ZU14 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201 / 37706 tAM h i EMS NOTE. Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 rng/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L • (Nola: Use MPN mathod for highly turUd Samples) Orthophosphate 70507• mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 70300 64 mg/L Al - Aluminum 01105 mglL pH (Lab) 00403 5.96 units Ba - Barium 01007 µg/L TOC 00680 mglL Ca - Calcium 00916 mg/L Chloride 00940 13.9 mg/L Cd - Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils'00552' mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) PhenD132730 µg/L Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Lab Report Attached? [A Yes(1) ❑ No (0), Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC Method# SM 6200B Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn'- Manganese 01055 µg/L , Method# TKN as N 00625 mg/L Ni - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total VOCs: VOC Removal°/a _Patricia T. Davis - Utility Systems Operator���^� -- 10/30/2014 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev.2/2010 SUBMIT FORM ON YELLOW.PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - FACILITY INFORMATION Please Print Clearly or. Facility Name: MCAS Cherry Point Permit Name (if different): Facility Address: WAS Cherry Point, NC 28533-0006 , County: Craven Contact Person: : Patricia T. Davis Telephone #: 252-466-4599 Well Location/Site Name: Site 21, MCAS Cherry Point No -of Wells to be Sampled: 1 `, :,UIVISION.OF WATER QUALITY -INFORMATION PROCESSING UNIT' ' 160MAIL SERVICE CENTER RALEIGH, NC 27699-1617 PHONE: (919)7334221 PERMIT Number: Expiration Date: 7/31/2A19 Non -Discharge UIC NPDES W00001489 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remedlation: ❑ Rotary Distributor . Q Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: IPLING INFORMATION If WELL L 1D NUMBER (From Permit): MW-2 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Depth 26.58 ft. Well Diameter. 2 pH 00400 6.29 units Temp 00010: 23 oC DRY at h to Water Level 82546: 6.5 ft. below measuring point Screened Interval: -1.03 ft. to -11 ft. Spec. Cond. 00094: 713 µfWtos time of :wring Paint is 1.28 ft. above land surface Relative M.P. Elevation: 14.8 Odor 00085: none sampling, ne of water pumped/bailed before sampling: 5 Gal. check � Appearance: clear here: ❑ ales for metals were collected unfiltered YES NO and Field acidified YES NO ORATORY INFORMATION - Date sample analyzed: 10/8/2014 Laboratory Name: MCAS Cherry Point I Pace Analytical "4AMHTERS NO Certification Number. 201137706 — TE. Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (1403) as N 00620 <0.05 mg/L Coliform: MF Total 31504 1100mL Phosphorus: Total as P 00665 mg/L (Note: use MPNmelhodfor ttighiyturbid samples) Orthophosphate70507 mg/L Dissolved Solids: Total 70300 160 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.29 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034--7 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg/L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 1.73 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen: NH2as N: Ammonia Nitrogen, Total) Mn -Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 µg/L For Remediation Systems Only (Attach Lab Reports):' Influent Total VOCs: Patricia T. Davis - Utility. Systems Operator Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 Pb - Lead 01051 µg/L Zn -Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? El Yes(1) ❑ No (0) VOC Method# SM 6200B Method# Method# Method# Effluent Total VOCs: VOC Removal% 10/30/2014 Signature of Permittee (or Authorized Agent) (Date) SUBMIT FORM ON YELLOW.PAPER ONLY GROUNDWATER QUALITY MONITORING: e r r ` DEPARTMENT_aF ENVIRONMENT II; NATURAL. RESOURCES DIMS[ON.OFWATER=ALITY-fNFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM j.161TMAILSERVIC9-dENTER RAClJIdH; NC Y7699-1617 'PHONE: IS19)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number. Expiration Date: 7/31/2 19 Facility Name: MCAS Cherry Point Non -Discharge UIC Permit Name (if different): NPDES WQ0001489 Other Facility Address: MCAS Cherry Point, NC 28533-0006 TYPE OF PERMITTED OPERATION BEING MONITORED County: Craven ❑ Lagoon ❑ Remediation: infiltration Gallery (Ctry) (6te1e) (ZIP) ❑ Spray Field ❑ Remedlation: Contact Person: Patricia T. Davis Telephone #: 252-466A599 ❑ Rotary Distributor ❑✓ Land Application of Sludge Well Location/Site Name: Site 21 MCAS Cherry Point No.of Wells to be Sampled: 1 ❑ Water source Heat Pump ❑ Other: from SAMPLING INFORMATION If WELL WELL lD NUMBER (From Permit): MW-3 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 25.58 ft. - Well Diameter: 2 pH 00400 6.32 units Temp 00010: 25 °C DRY at Depth to Water Level 62546: 0 ft. below measuring point Screened Interval: -11.7 ft. to -21.7 ft.. Spec. Cord. 00094: 301 µ Mhos time of sampling, Measuring Point is I A6 ft. above land surface Relative M.P. Elevation: 3.1 Odor 00085: - stagnant check Volume of water pumped/balled before sampling: 5 Gal. Appearance: turbid here: El for metals were collected unfiltered YES NO and field acidified YES NO LABORATORY INFORMATION Date sample. analyzed:. 10/8/2014 Laboratory Name: . MCAS Cherry Point / Pace Analytical Certification Number: 201 1.37706 PARAMETERS NOTE: -Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 µg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note; Use MPH method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify'Compounds an&Concentration Units): Dissolved Solids: Total 70300 160 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.32 units Ba -Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 7.9 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 µg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L ORGANICS (by GC, GC/MS, HPLC) Phenol 32730 µglL Fe - Iron 01045 µg/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury.71900 µg/L Lab Report Attached? p ❑ Yes(1) . ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC Method# SM 6200B Total Ammonia 00610 1.13 mg/L Mg - Magnesium 00927 mg/L Method# (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Tolan Mn - Manganese 01055 µg/L- , Method# TKN as N 00625 mg/L NI - Nickel 01067 µg/L Method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Patricia T. Davis - Utility Systems Operator. Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.2/2010 Effluent Total VOCs: VOC Removal% 10/30/2014 Signature of Permittee (or Authorized Agent) (Date) I 'I GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: • MCAS Cherry Point Permit Name (if different): Facility Address: MCAS Cherry Point Please Print SUBMIT FORM ON YELLOW PAPER ONLY or Type County., Craven act Person: Patricia T. Davis Telephone * 252-466-4599 Location/Site Name: Site 21, MCAS Cherry Point. No.'of Wells to be Sampled: 1 (rtom MM •: vGrn.�.m�•r. yr clrrlrtlJnrnG•Ir r"oa rlMl Yr{f►L K�SVUKlaSCi •• L ,DIVI510N OF WATER'QUAUTY4,10ORMATION PROCESSING UNIT 1617.MAIL SERVICE CENTER RAL•EIGH' NC.27699A6 ' PHONE: (9'19)733-3 ••••••• •��•••��••• �nr..auv.. •ia lG. IIJ IrLL 1.7 �n-Discharge UIC DES - WQ0001489 Other PE OF PERMITTED OPERATION BEING MONITORED' ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑� Land Application of Sludge ❑ Water Source Heat Pump ❑ other: SAMPLING INFORMATION If WELL WELL ID NUMBER (From PermiQ: MW-5 Date Sample Collected: 10/8/2014 FIELD ANALYSIS: WAS Well Depth 13 It. Well Diameter: 2 pH 00400 6.55 units Temp 00010: 29 oC DRY at Depth to Water Level 82546: 9 ft. below measuring point Screened Interval: 3 ft. to 13 ft.Spec. Cond. 00094: 741 _µMhos of. sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ' 12 - Odor 00085: none check Volume of water pumped/balied before sampling: 5 Gal. Appearance: clear here: for metals were collected unfiltered _ _YES _ ❑ NO and field acidified n YES n NO ElSamples e sample analyzed: 10/8/2014 Laboratory Name: MCAS Cherry Point / Pace Analytical Certification Number: 201137706 tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 <1 /100ml- Nitrate (NO3) as N 00620 <0.05 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Dissolved Solids: Total 70300 .274 mg/L -At - Aluminum 01105 mg/L pH (Lab) 00403 6.55 units Ba - Barium 01007 µg/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 10.4 mg/L Cd -Cadmium: Total 01027 µg/L Arsenic 01002 pg/L Chromium: Total 01034 µg/L Grease and Oils 00552 mg/L Cy - Copper 01042 mg/L Phenol 32730 µg/L Fe - Iron 01045 µg1L Sulfate 00945 mg/L Hg - Mercury 71900 µg/L Specific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 2.99 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 µg/L TKN as N 00625 mg/L Ni - Nickel 01067 pg/L Pb - Lead 01051 µg/L Zn - Zinc 01092 mg/L . Other (Specify Compounds and Concentration Units): ORGANICS (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Laic Report Attached? ❑ Yes(,[) ❑ No (0) VOC Method# SM 6200B Methodic Method# Method; For Remediation Systems • .:• Reports): 1 i•Cs: Effluent Total VOCs:• l t: r j.- � C I l r. , I t o I. • 1I,I ta io I cerlily that to the best of my know,edae and belief, the inf or kafion submil!edNin this repo i Is truepaccurate;and co plele lahtl hat the Iabore�o j analylicaFl dita •riaspio�uced uslna approved methods of an lysis by a I ;;� 0WQ•ce tified laboratory. i am aware that therepre s'gndicanl penalhLs fof submilling fel- nform;liori� inch g t e doss bilily_oflfines and impr�is �n(nent for kno.fin� yjo atior.s. DavisPatricia T. - Operator 10/30/2014 GW-59 Rev. Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) 2ce Pace Analytical Services, Inc. Analytical ® 9800 Kincey Ave. Suite 1p0. _ Huntersville, NC 28078 www.pecdobs.com (704)8759092 ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: RAGAS MW-1 Lab ID: 92220940001 Collected: 10/08/14 11:05 Received: 10/10/14 09:45 Matrix: Water c Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual 6200B MSV Analytical Method: SM 6200E Benzene' ND ug/L 0.50 .1 10/15/14 08:11 7143-2 Bromobenzene ND uglL 0.50 1 10/15/14 08:11 108416.1 Bromochloromethane ND ug/L 0.50 1 10/15/14 08:11 74-97-5 Bromodichloromethane ND ug/L 0.50 1. 10/15/14 08:11 75-27-4 Bromoform ND ug/L 0.50 1 10/15/14 08:11 75-25.2 Bromomethane ND ug/L 5.0 1 10/15/14 08:11 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/15/14 08:11 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/15/14 08:11 135-98-8 tert-Butylbenzene NO ug/L 0.50 1 10/15114 08:11 98-06.6 Carbon tetrachloride NO ug/L 0.50 1 10l15/14 08.11 56-23-5 'Chlorobenzene NO ug/L 0:50 1 10/15/14 08:11 108-90-7 Chloroethane NO ug/L 1.0 1 10/15/14 08:11 75-00-3 Chloroform 4.7 ug/L 0.50 1 10115/14 08:11 67-66-3 Chloromelhane NO ug/L 1.0 1 10/15/14 08:11 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10/15/14 08:11 .95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/15/14 08:11 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/15/14 08:11 96-12-8 Dibromochloromethane ND ug/L . 0.50 1 10/15/14 08:11 124-48-1 ' 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 10/16/14 08:11 10&93-4 Dibromomethane ND ug/L 0.50 1 10/15/14 08:11 74-95-3 1.2-Dichlorobenzene ND ug/L 0.50 1 10/15/14 08:11 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/15/14 08:11 541-73-1 1,4-Dichlorobenzene ND ug/L 0,50 1 10/15/14 08:11 106-46-7 Dichlorodifluoromethane NO ug/L 0.50 1 10/15/14 08:11 75-71-8 1,1-Dichloroethane NO ug/L 0.50 1 10/151-1408:11 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/15/14 08:11 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/15/14 08:11 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10115/1408:11 156-59-2 trans-1,2-Dichloroethene NO ug/L 0.50 1 10/15/1408:11 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/15/14 08:11 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/15114 08:11 142-28-9 2,2-Dichloropropane NO ug/L 0.50 1 10/15114,08:11 594-20-7 1,1-Dichloropropene NO ug/L 0.50 1 10/15/14 08:11 563-58-6 cis-1,3-Dichloropropene NO ug/L. 0.50 1 10/15/14 08:11 10061.01-5 trans-1,3-Dichloropropene NO ug/L 0.50 1 10/15/14 08:11 10061-02-6 Dilsopropyl ether NO ug/L 0.50 1 10/15/14 08:11 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/15/14 08:11 100-41-4 Hexachloro-1,3-butadiene NO ug/L 2.0 1 10/1511408:11 87-68-3 isopropytbenzene (Cumene) ND ug/L 0.50 1 10/15/14 08:11 98-82-8 Methylene Chloride ND ug/L .2.0 1 10/15/14 08:11 75-09-2 Methyl-terl-butyl ether ND ug/L 0.50 1 10/15/14 08:11 1634-04-4 Naphthalene ND ug/L 2.0 1 10/15/14 08:11 91-20-3 n-Propylbenzene NO ug/L 0.50 1 10/15/14 08:11 103-65-1 Styrene ND ug/L 0.50 1 10/15/14 08:11 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 1011511408:11 630-20-6 1,1,2,2-Tetrachloroethane NO ug/L 0:50 .1 1011511408:11 79-34-5 Tetrachloroethane NO ug/L 0.50 1 10/15/14 08:11 127-184 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 23 Pace Analytical Services, lnc, aCe 9800 Kincey Ave. Suite 100 Analyr�C81 Huntersville, NC 28078 wwwpaCelabs.carrf (704)875-9092 ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: RflCAS RA1Rl-1 Lab ID: 92220940001 Collected: 10/08/14 11:05 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared 6200B MSV Toluene 1,2,3-Tichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1, 2,3-Tdchloropropane 1,2,4-Trimethylbenzene 1.3, 5-Trimethylbenzene Vnyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichioroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B Analyzed CAS No. Dual ND ug/L 0.50 1 10/15/14 08:11 108-88-3 ND ug/L 2.0 1 10/15/14 08:11 87-61-6 ND ug/L 2.0 ' 1 1011&1408:11 120-82-1 ND ug/L 0.50 1 10/15/14 08:11 71-55-6 NDug/L 0.50 1 10/15114 08:11 79-00-5 NO ug/L 0.50 1 10/15/14 08:11 79-01-6 ND ug/L 1.0 1 10/15/14 08:11 75-69-4 NO ug/L 0.50 1 10/15/14 08:11 96-18-4 ND ug/L 0.50 1 10/15/14 08:11 95-63-6 ND ug/L 0.50 1 10/15/14 08:11 108-67-8 ND 'ug/L 1.0 1 10/15/14 08:11 75-01-4 NO u9/1- 1.0 1 10/15/14 08:11 179601-23-1 NO ug/L 0.50 1 10/15/14 08:11 95-47-6 105 % 70-130 1 10/15/14 08:11 17060.07-0 . 9.8 61. 70-130 1 10/15/14 08:11 460-00-4 1,04 % 70-130 1 10%15/14 08:11 2037-26-5 Sample: MCAS MW-2 Lab ID: 92220940002 Collected: 10/08/14 10:20 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Dual 6200B MSV Analytical Method: SM 62008 Benzene ND ug/L 0.50 1 10/18/14 18:13 71-43-2 Bromobenzene NO ug/L 0.50 1 10/18/14 18:13 108-86-1 Bromochioromethane NO ug/L 0.50 1 10/18/14 18:13 74-97-5 Bromodichloromethane NO ug/L 0.50 1 10/1811418:13 75-27-4 Bromoform NO ug/L 0.50 1 10/18/14 18:13 75-25-2 Bromomethane ND ug/L 5.0 1 10/18/14 18:13 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/18/14 18:13 104-51-8 ser-Butylbenzene NO ug/L 0.50 1 10/18/14 18:13 135-98-8 tert-Butylbenzene NO ug/L 0.50 1 . 10/18/14 18:13 98-05-6 Carbon tetrachloride NO ug/L 0.50 1 10/18/14 18:13 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:13 108-90-7 Chloroethane NO ug/L 1.0 1 10/1811418:13 75-00-3 Chloroform NO ug/L 0.50 1 10/18/1418:13 67-66-3 Chloromelhane NO ug/L 1.0 1 10/18/14 18:13 74-87-3 2-Chlorotoluene NO ug/L 0.50 1 10/16/14 18:13 95-49-8 4-Chlorotoluene NO ug/L 0.50 1 10/18/14 18:13 106-43-4 1,2-Dibromo-3-chloropropone NO ug/L 1.0 1 1011811418:13 96-12-8 Dibromochloromethane NO ug/L 0.50 1 10118/1418:13 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 0.50 1 10/18/14 18:13 106-93-4 Dibromomethane ND ug/L 0.50 1 10/18/14 18:13 74-95-3 1,2-Dichlorobenzene NO ug/L 0.50 1 10/18/14 18:13 95-50-1 1,3-Dichloro6enzene ND ug/L 0.50 1 1011811418:13 541-73-1 1,4-Dichlorobenzene NO ug/L 0.50 1 10/18/14 18:13 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 23 tAA Pace An Services, Inc, 11!aceAnaiyticaie 9900 KinceyAve. Suite Joe Huntersville, NC 28079 wwwpaanlftcan • (704)875-9092 i . ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: MCAS RAW-2 Lab ID: 92220940002 Collected: 10/08/1410:20 Received: 10/10/14 09:46 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 62009 MSV Analytical Method: SM 620DB Dichlorodifluoromethane ND ug/L 0.50 1 10/18/14 18:13 75-71-B 1,1-Dichloroethane ND ug/L 0.50 1 10/18/1418:13 75-34-3 1,2-Dichloroethane NDug/L 0.50 1 10/18/14 18:13 107-06-2 1,1-Dichloroethene ND ug/L 0.56 1 1011811418:13 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/18/1418:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/18/1418:13.156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/1811418:13 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/18/14 18:13 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/18/14 18:13 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/18/14 18:13 663-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:13 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:13 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/18/14 18:13 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/18/14 1 B:13 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/1811418,13 87-68-3 Isopropylbenzene (Cumene) ND 6g/L 0.50 1 1011811418:13 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/18/14 18:13 75-09-2 Methyl-tert-butyl ether ND ug1L 0.50 1 10/18/14 18:13 1634-04-4 Naphthalene' ND ug/L 2.0 1 10/18/14 18:13 91-20-3 n-Propyiberizene ND ug/L 0:50 1 1011811418:13 103-65-1 Styrene ND ug/L 0.50 1 10/1811418:13 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0,50 1 10/18/14 18:13 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/1811418:13 -79-34-5 Tetrachloroethene . ND ug/L 0.50 1 10/18/14 18:13 127-18.4 Toluene ND ug/L 0.50 1 10/18/14 18:13 108-88-3 1,2,3-Trichiorobenzene ND ug/L 2.0 1 10/18/14 18:13 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/1811418:13 120-82-1 1,1,1-Trichloroethene ND ug/L 0.50 1 10/1811418:13 71-55-6 1,1,2-T6chloroethane ND ug/L 0.50 1 10/18/14 18:13 79-00-5 Trichloroethene ND ug/L 0.50 1 10/18/14 18:13 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/18/14 18:13 75-69-4 1,2,3-Tdchloropropane ND ug/L 0.50 1 10/18/14 18:13 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10/18/14 18:13 95-63-6 1,3,5-Trimethylbenzene ND ug(L . 0.50 1 10/18/14 18:13 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/18/14 18:13 75-01-4 m&p-Xylene ND ug/L 1.0 1 10118/1418:13 179601-23-1 o-Xylene ' ND ug/L 0.50 1 -1011811418:13 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 123 % 70-130 1 1011811418:13 17060-07-0 4-Bromofluorobenzene (S) 100 % 70-130 1 10/18114 18:13 460-00-4 Toluene-d8 (S) 105 % 70-130 1 10/18/14 18:13 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 23 ' ;Ialce Pace Analytical Services, Inc. Kincey Ave. Suite 100 Analy�ical 9900 Huntersvilie, NC 28078 xww'pscelalSs_rom (704)875-9092 ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: IWCAS MW-3 Lab ID: 92220940003 Collected: 10/08/14 11:40 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/18/14 18:29 71-43-2 Bromobenzene ND ug/L 0.50 1 10/18/14 18:29 108-86-1 Bromochloromethane ND ug/L 0.50 1 10/18/14 18:29 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/18/14 18:29 75-27-4 Bromoform. ND ug/L .0.50 1 10/1'8/14 18:29 75-25-2 Bromomethane ND ug/L 5.0 1 10/18/14 18:29 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10118/1418:29 104-51-8 sec-Butyibenzene ND ug/L 0.50 1 10118/1418:29 135-98-8 tent-Butylbenzene ND ug/L 0.50 1 10/18/14 18:29 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/18/14 18:29 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:29 108-90-7 Chloroethane ND ug/L 1.0 1 10/18/14 18:29 75-00-3 Chloroform ND ug/L 0.50 1 10/18/14 18:29 67-66-3 Chloromethane ND ug/L 1.0 1 10/18/14 18:29 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 10118/1418:29 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10118/1418:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/18/14 18:29 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10/18/14 18:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 1011811418:29 106-93-4 Dibromomethane ND ug/L 0.50 1 10/18/14 18:29 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/1811418:29 95-50-1 1,3-Dichlorobenzene ND ug%L 0.50 1 10118/1418:29 541-73-11 1,4-Dichlorobenzene ND ug/L 0.50 1 - 10/18/14 18:29 106-46-7 Dichlorodinuoromethane ND ug/L 0.50 1 10118/1418:29 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 10118/1418:29 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/1811418:29 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 10/1811418:29 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10118/1418:29 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/18/14 18:29 156-60-5 1,2-Dichloropropane . ND ug/L 0.50 1 10/18/14 18:29 76-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/181141829 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/1811418:29 594-20-7 1,1-Dichloropropene ND uglL 0.50 1 10118/1418:29 563-5B-6 cis-1,3-Dichloropropene. ND ug/L 0.50 1 10/18/14 18:29 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 10/18/14 18:29 10061-02-6 Diisopropyi ether ND ug/L 0.50 1 10/18/14 18:29 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/1811418:29 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/1811418:29 87-68-3 Isopropylbenzene (Cumene) ND ug/L '0.50 1 10/18/14 18:29 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/'18/14 18:29 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 10/18/14 18:29 1634-04-4 Naphthalene ND ug/L 2.0 1 10/18/14 18:29 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/18/14 18:29 103-65-1 Styrene ND ug/L 0.50 1 10/18/14 18:29 10042-5 1,1,1;2-Tetrachloroethane ND ug/L 0.50 1 10/1811418:29 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/18/1418:29 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/18/14 18:29 127-18.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 23 Pace Analytical Services, Inc. Kincey Ave. Suite 100 __ aceAnalytical o 9800Huntersville, NC 2e07a wwwpacelabs.cam (704)875-9082 i ANALYTICAL RESULTS Project: MW Pace Project No.: 92220940 Sample: MCAS MW-3 Lab ID: 92220940003 Collected: 10/08/14 11:40 Received: 10/10/14 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No.. Qua[ 6200B MSV Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroe(hane 1,1,2-Tdchloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Tdmethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichioroethone-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B NO ug/L 0.50 1 10/18/14 18:29 108-88-3 NO ug/L 2.0, 1 '10/18/14 18:29 87-61-6 NO ug/L 2.0 1 10118/1418:29 120-82-1 NO ug/L 0.50 1 10/18/14 18:29 71-55-6 ND .ug/L 0.50 1 10/18/14 18:29 79-00-5 ND uglL 0.50 1 10118/1418:29 79-01-6 ND ug/L 1.0 1 10/18/14 18:29 75-69A ND ug/L 0.50 1 10/18/14 18:29 96-18A ND ug/L 0.50 1 10118/1418:29 95-63-6 ND ug/L 0.50 1 10118/1418:29 108-67-8 NO ug/L 1.0 1 10118/1418:29 75-01-4 NO ug/L 1.0 1 10118/1418:29 179601-23-1 NO ug/L 0.50 1 10118/1418:29 95-47-6 124 1/6 70-130 1 1011811418:29 17060-07-0 100 % 70-130 1 10/1811418:29 460-00-4 104 % 70-130 1 10118/1418:29 2037-26-5 Sample: MCAS MW-5 Lab ID: 92220940004 Collected: 10/08/14 14:35 Received: 10110/14 09:45 Matrix: Water Parameters - Results Units Report limit OF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 10/18/14 18:46 71-43-2 Bromobenzene NO ugfL 0.50 1 10/18/14 18:46 108-86-1 Bromochloromethane NO ug/L 0.50 1 10/18/14 18:46 74-97-5 Bromodichloromethane ND ug/L 0.50 �1 10/18/14 18:46 75-27-4 Bromoform ND ug/L 0.50 1 10/18/14 18:46 75-25-2 Bromomethane NO ug/L 5.0 1 10/18f1418:46 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/18/14 18:46 104-51.8 sec-Butylbenzene ND ug/L 0.50 1 10/18/14 18:46 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 10/1811418:46 98-06-6 Carbon tetrachloride NO ug/L 0.50 1 10f18f1418.46 56 23-5 Chlorobenzene ND ug/L 0.50 1 10/18/14 18:46 108-90-7 Chloroethane ND ug/L 1.0 1 1011811418:46 75-00-3 Chloroform ND ug/L 0.50 1 10/18/1418:46 67-66-3 Chloromethane NO ug/L 1.0 1 10/18/14 18:46 74-87-3 2-Chlorotoluene NO ug/L 0.50 1 10/18/14 18:46 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/18/14 18:46 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 1.0 1 10/18/14 18:46 96-1278 Dibromochloromethane NO ug/L 0.50 1 10/18/14 18:46 124-48-1 1,2-Dibromoethene (EDB) ND ug/L 0.50 1 10/18114 18:46 106-93-4 Dibromomethane NO ug/L 0.50 1 10/18/14 18:46 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10118/1418:46 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:46 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/18/14 18:45 105-45-7 REPORT OF LABORATORY ANALYSIS - This report shall not be reproduced, except in hill. Date: 10/28/2014 03:29 PM withoutthe written consent of PaceAnalytical Services, Inc.. Page 8 of 23 a - �aceAnalytical- www nww.pacefebs.com Project: MW Pace Project No.: 92220940 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078'' (704)875-9092 Sample: MCAS MW-6 Lab ID: 92220940004 Collected: 10/08/14 14:35 Received: 10/10114 09:45 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Dichlorodifluoromethane ND ug/L 0.50 1 10/18/14 18:46 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 1011811418:46 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/18/14 18:46 107-06-2 1,1-Dichloroethene ND ug/L 0,50 1 10118/1418:46 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 loll 8/1418:46 156-59-2 trans-1,2-Dichloroethene NO ug/L 0.50 1 10/18/14 18:46 156-60-5 1,2-Dichloropropane ND ug/L 0.50' 1 10/18/14 18:46 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/18/14 18:46 142-28-9 2,2-Dichloropropane ND ug/L 0.5d 1 10/18/14 18:46 594-20-7 1,1-Dichloropropene ND ug/L' -0.50 1 10/1811418:46 563-58-6 cis- 1,3-Dichloropropene NO ug/L 0.50 1 10/18/14 18:46 10061.01-5 trans- l,3-Dichloropropene NO ug/L 0.50 1 10/18/1418.46 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/18/14 18:46 109-20-3 Ethylbenzene ' ND .ug/L 0.50 1 10/18/14 18:46 100-41-4 Hexachloro-1,3-buladiene ND ug/L 2.0 1 10/18/14 18:46 87-68-3 Isopropyibenzene (Cumene) NO ug/L 0.50 .1 10118/1418:46 98-82-8 Methylene Chloride NO ug/L 2.0 1 10/18/14 18:46 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 10/18/14 18.46 1634-04-4 Naphthalene ND ug/L 2.0 1 10/18/14 18:46 91-20-3 n-Propylbenzene ND ug/L 0.50 1 1011811418:46 103-65-1 Styrene NO ug/L 0.50 1 10/18/1418*46' 100-42.5 1,1;1,2-Tetrachloroelhane ND ug/L 0.50 1 10/18/14 18:46 ,630-20-6 11,2,2-Tetrachloroethane ND ug/L 0.50 1 10/18/14 18:46 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/18/14 18:46 127-18-4 Toluene ND ug/L 0.50 1 10/18/14 18:46 108-88-3 1,2,3-Trichlorobenzene NO ug/L 2.0 1 1011811418:46 87-61-6 1,2,4-Trichlorobenzene NO ug/L _ 2.0 1 1011811418:46 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 10/1811418:46 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/18/14 18:46 79-00-5 Trchloroethene ND ug/L 0.50 1 1011811418:46 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/1.8114 18:46 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 .10/18/14 18:46 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10118/14 18:46 95 63-6 1,3,5-Trimethylbenzene NO ug/L 0.50 1 10/18/14 18:46 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/18/14 18:46 75-01-4 . m&p-Xylene ND ug/L 1.0 1 10/1811418:46 179601-23-1 o-Xylene ND ug/L 0.50 1 10/18/14 18:46 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 124 % 70-130 1 10/18/14 18:46 17060-07-0 4-Bromofluorobenzene (S) 100 % 70-130 1 10/18/14 18:46 460-00-4 Toluene-d8 (S) 104 % 70-130 1 10/1811418:46 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/28/2014 03:29 PM without the written consent of Pace Analytical Services, Inc.. 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