DANFORD BROTHERS_CORRESPONDENCE_20171231

CORRESPONDENCE
NORTH AROL.INA l u�l
DoportInnnt of Envlmn

r
Division of Hnvirommntal Hann emec
8 C T 2 t9�
CHAIN OF qSTODY RECORD r' 'V. MANAGEMENT
For Investigation of � °� EiTEVILLE REG. OFFICE
�u
Samples collectod and * iorxa cowlet• - bys
b Orly I Statioa. /
No. of
Lab' Ho. NO. Stations Location Date tine Bottles '
Ralinquis by i ture}:
u ed bk 0 1 Wye):
Date Time
'fi 4•' ti
I
Rec y
1
Ric by
Rrl
Rec by (Lab)
Chod of Shipment:
Seal by;. Broken
Security Sbne and Condition: Lock by: Dnea by:
TAR i1S1C t Vf.Y
V._i F� Lam,.
ON roa1r

For Lab Use ONLY
DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY 13I", .Ca
PRIORITY
�
SAMPLE TYPE
R1Vf3i BASIN r 1-
❑ AMBIENT
❑
❑ STREAM �`>�FL(SENT
REPORT TO: ARf FRO RO RRO WaRO W1RO WSHO TS
QA
+
AT BM
❑COMPLIANCE
I� CHAIN
❑ LAKE ❑ VUIX1FNC
Other
❑EMERGENCY
OF CUSTODY
❑ ESTUARY
Shipped by: s Caarler, tail, Other
COLLECTORS)- lIJI�J y�,
Estimated BOD Range: 0-5/5-25/25-65/40-130 or 100 plus STATION LOCATION: . /"Q-
Seed: Yes ❑ No ❑ Cblarioated: Yes ❑ No ❑ REMARKS: -
Lab Number.
( ! i i 5.;) V j
Date Received:
.. Jfn 9) Time: J. -Y
Rec'd by;
Sue-C-Hand Del_
From:oo�r
_
DATA ENTRY BY:
3
�if * CK;
DATE REPORTED:
�rbf I f A
Station # iDate Begin (yy/mm/dd) I Time Begin I Date End I Time End I Depth DM DE DBM l Value Type I Composite `Sample Type
1
DS 310 �+A mg/l
f J
2
COD High 340 m9R
3
COD Low 335 mg/1
4
Coliform: MF Fecal 31616 /l /100012
[ I
5
Coliform: MF Total 31504 /100m1
6
Coliform: Tube Fecal 31615 /100m1
7
Coll form: Fecal Strep 31673 /100m1
8
Residue: Total 500, ` mg/1
9
Volatile 505 mg/I
10
Fixed 510 mg/1~
11
Residue: Suspended 530 ms/I
12
Volatile 535 mg/I
13
Fixed 540 mg/I
14
PH 403 units
15
Acidity to pH 4.5 436 mgA
16
Acidity to pH 8.3 435 ms/I
17
Alkalinity to pH 8.3 415 Mon s
18
Alkalinity to pH 4.5 410 ntg%1
19
TOC 680 mg/1
20
Turbidity 76 NTU
Chloride 940 mg/i
Chi a: Tri 32217 USA
Chi a: Corr 32209 USA,.
Pheophytin a 32213 pg/I
Color. True SO "Pt -Co
ColorapH ) 83 ADMI
Color. pH 7.6 82 ADMI
Cyanide 720- mgL1—
Fluoride 953 m9
Formaldehyde 71880 mg/1
Grease and Oils $56 mg/I
Hardness Total900 mgJl`
Specific Cond. 95 uMhos/cm2
MBAS 38260 Ono
Phenols 32730 ag/t
Sulfate 94S mg/!
Sulfide 745 mg/1•—
A H L
NH3 as N 610 mg/I
TKN as N fi25 UMA
NO2 plus NO3 as N 630 mg/I
P: Total as P 665 m10
PO4 as P 70507 mgA
P. Dissolved as P 666 mg/1
Cd[admlum 1027 USA
s
Cr(3uom1um:Tota11034 ug/I
CtrCopper 1042 ug/1
NMlickel 1067 USA
Pb-Lead 1051 ouA
Z,n-Ziac i092 ug/l
A9411ver 1077 USA
Al-Aluminam 1105 USA
Be4uryilium 1012 agA
Ca -Calcium 916 MA
Co -Cobalt 1037 USA
F04ron 1045 U*A '
I T S B I C G GNXX I
Sampling Point X
Conductance at 25
Water Temp matme C
D.O. mg/)
pH
Alkalinity
Acidity
Air Temperature 40
pH8.3• pH4.5
pH4.5 pH9.3
2
94
10
300 I
400 IN
$22" 431
92243 192242
21)
Salinity X
Precipidon &WdwA
Cloud Cover X
Wind Dhection 0)eW
Cream Flom Severity
Turbidity Severity
Wind Velocity M/H ears Stream Depth ft.
Stream WkMh fL
480
45
32
36
1351
1350
35 64
4
DM1/Rev1sed 10/36 4—
A �

DIVISION OF ENVIRONMENTAL MANAGEMENT WATER QUALITY FIELD -LAB FORK! (DM1)
r-} p
COUNTY a._,! PRIORITY
RIVER BASIN i
REPORT TO: ARO FRO IKRO RRO WaRO WIRO WSRO TS ❑AMBIENT ❑ OA
AT Otheerr ❑COMPLIANCE �1 IN
ot
OF CUSTODYShipped by: �C..rl Staff, Other ❑EMERGENCY
COLLECTOR(S):
Estimated SOD Range: 0.5/5-25/25�5/40-130 or 100 plus STATION LOCATION: ell .
Seed: Yea [Q No ❑ Chlorinated: Yes © No ❑ REMARKS,
SAMPLE TYPE
❑ STREAM ENT
❑ LAKE ❑ INFLUENT
LI ESTUARY
,i'C li X —
Fnr rah rl.o AHr V
Lab Number,
Date Received:
Time:
R_ec'd bv-
From: Bus-Courie{rJ-�Hand Del
DATA ENTRY :
DATE REPORTED:
IC �Lt I (f l o
1
5tattnn #/ Date Begin (yy/mm/dd) Time Begin
Date End Time End
Depth DM DB DBM
Value Type
Composite
Sample Type
?,
t I
A H L
T S B
C G GNXX
1
—Aelf
mgA
DOD5 310 7A
2
COD High 340 m2/1
3
COD Loan 335 moll
4
G011form: MF Fecal 31616 /100m1
5
Coliform: MF Total 31504 11GOml
6
Coliform: Tube Fecal 316I5 /100m1
7
Coliform: Feral Strep 31673 /loom]
8
Residue: Total 500 mgA
9
Volatile 505 mg/l
1 D
Fixed 510 mall
11
Rssidue: Suspended 530 tag/l
12
Volatile 535 mg/l
13
Fixed 540 ma/1
14
PH 403 units
I5
Acidity to pit 4.5 436 mgA
16
Acidity to pH 8.3 435 mg/I
17
Alkalinity to pH 9_3 415 mall
1$
Alkalinity to pH 4.5 410 mg/i
19
TOC 6" mgA
20
Turbidity 76 Nllf
Chloride 940 moll
Chi a: Tri 32217 ug/1
Chi a: Corr 32209 ug/il
Pheophytin a 32213 ng/1
Color: True 80 Pt-00
Color:(pH ) 83 ADM]
Color: pH 7.6 R2 ADM[
Cyanide 720- mg/
r<
Fluoride 951
?
Formaldehyde 71880 mg/1
Grease and Oils 556 mgA
Hardness Total900 mg/l
Specific Cond. 95 uMhos/cin2
MR" 38260 - m9A
Phenols 32730 og/1"
Sulfate 945 mg/]
Sulfide 745 mg/r
NH3 as N 610 mgA
TKN as N 625 M9A
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mg/l
PO4 as P 70507 mg/]
P: Dissolved as P 666 utgA
Cd-Cadmium 1027 u9A
Cr{3tromfuarTotai 1034 ugA
C r Copper 1042 ug/1
Ni-Nickel 1067 ng/1
Pb-Lead 1051 ugA
Zn-Zinc 1092 ug/1
P41-18fiver 1077 ug/f
Al -Aluminum 1105 og/1
Be -Beryllium 1012 ugA
Ca -calcium 916 MGA
Co -Cobalt 1037 ugA
Fe -Iron 1045 u9A
Li -Lithium 1132 USA
Mg-Magneslum 927 mgA
Mu -Manganese 1055 a9/1
Na-Sodlum 929 moll
ArsenimTotal 1002 ugA
Se -Selenium 1147 ug/I
Hg-Mercury 71900 u9/1
Organoehlorine Pesticides
Organoph-Whmueftsticides
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle re 'd)
Phytoplanktnn
f�►f t �►.\ �IatllTul a►lf f
Sampling Point X
Conductance at 25 C
Water Temperatue V
D.O. mgA
pH
- AlkaiiniV
Acidity FAYETTEVII
b5
PH 93 pit 4.5
pH 4.5 PH 8.3
2
94
10
300
400 1•
82244 431
82243 182242
20
Salinity X
Precipition Oa/day)
Cloud Cover X
Wind Direction oeg)
Stream Flom Severity Turbidity Severity
Wind Velocity M/Ff
Stream Depth ft.
Sneam Width fL
480
45
32
36
1351 1350
35
[ean
4
4
J
DMI/Revised 10/86

0
•
11

For Lab Use ONLY
DIVISION OFF MANAGEMENT WATER QUALITY FIELD -LAB FORM (DM1)
COUNTY RA, 411,
RA,
PRIORITY
SAMPLE TYPE
U/
RIVER BASIN
-❑AMBIENT
❑ QA
Q'�TREAM[ ❑ EFFLUENT
REPORT TO: ARO Fi;O R0 RRO AIaRO WlRO WSRp TS
AT BM
❑COMPLIANCE
CHAIN
❑ LAKE ❑ 0VFL11FTIT
Other
❑EIMERGENCY
OF CUSTODY
❑ ESTUARY
Shipped by: Bos CottHer taff, Other
Lab Number: :'�_
Date Received, U, <;�te> Time:
Rec'd b . From: Bus -Courier -Hand Del
DATA ENTRY Y: � i at. _
DATE REPORTED: I0h h _
COLLECTOR(S)- !.��XF /
Estimated SOD Range: O-5/5-25/25-65/40-130 or 100 plus STATION LOCATION:
Seed: Yes ❑ NoO Chlorinated: Yea© No ❑ REMARKS:
Station # Date Begin (yy/mm/dd) Time Begin Date End Time End Depth DM DB DBM Value Type Composite Sample Type
�6 � 9 �q ADrd�rr A H L T s B C G GNXX
2
COD High MO mg/1
S
COD Low 335 mg/l
4
W
oliform: MF Fecal 31616,4 jk /100m1
�)
5
Conform: MF Total 31504 /100m1
b
Conform: Tube Fecal 31615 /loom]
7
Conform: Fecal Strep 31673 /100mi
8
Residue: Tots! SW 09/1
9
Volatile 505 ' mg/l
10
Fixed 510 mg/l
1 I
Residue. Suspended 530 mg/l
12
Volatile 535 mg/l
13
Fixed 540 mg/1
14
pH 403 units
15
Acidity to pH 4.5 436 mSA
16
Acidity to pH 8.3 435 mgA
17
Alkalinity to pH 8.3 415 m9/1
18
Alkalinity to pH 4.5 410 mg/l
19
TOC 680 00
20
Turbidity 76 NTU
Chloride 940 mg/1
Chi a: TO 322I7 Ug/t
Chi a: Con 32209 usn.
Pheophytin a 32213 ug/I
Color. True 80 Pt -Co
Color -(pH ) 83 ADMI
Color, pH 7.6 82 ADM
Cyanide 720>
5�.
Fluoride 951
Formaldehyde 71880 mg/!
Grease and Oils 556 mg/I
Hardness Total900 mgA
Specific Cond. 95 uMhos%tm2
MSAS 38260 m 9A
Phenols 32730 ug/1
Sul"f a 945 MA
Sulfide 745 man-
NH3 as N 610 mgA
TKN as N 625 a►g/1
NO2 plus NO3 as N 630 mg/1
P. Total as P 665 W
PO4 as P 70507 mgA
P. Dissolved as P 666 -SA
Cd- admium 1W7 ug/l
t]rClrromlum:Total1034 ug/I
CaCopper 1042 ug/1
Ni-Mickel 1067 USA
Pb-Lead 1051 ug/i
Z ranc 1092 ug/I
Ag•611ver 1077 USA
Al -Aluminum 1105 119A
Be-Berynium 1012 ug/!
Ca -Calcium 916 - m2/1
Co -Cobalt 1037 USA
Fe4ron 1045 ag/!
Sampling Point S
Conductance at 25 C
Water Temp
D.O. mg/1
pH
Alkalinity
6.3 4.5
ENV. 1vU,4.Pl&%gq&QWv
Acldpty , MEVILL
REG. OFFICE
vH pH
pH 4.5
2
94
10
300
400 •
822" 431
82243 192242
20
Sallnity %
Precipltiou On/da
bi0hcdon 9*q)yk(
Cream L1our Sevrrtty
Turbidity Severity
Wind Velocity MM
u Stream Depth tL
Soeem Width N
480
145
132
136
11351
1350
135
64
14

0
0

LOWY
Division of Snvizoaaaatal llsaagesent MIL 27 1990
cHulx OF ctssromr R WORD FAw��A��G� o�Flc�
For Inv" tiSation of
Samples co?lactad mW Dill forms cosplatsd b s
v ME
Rr "OVA
��
rw
rture).
i
F
Rec
by (Lab)
PI. 7W
. •
t'l1i»
r�

f
V130 JDU WIVJ TNAl

For Lab Use ONLY
DIVISION OF ENVJInONMENTAL MANAGEMENT WATNIUALITY FIELD -LAB FORM (DM1)
D
COUNTY �J.�.g /
PRIORITY
TYPE
RIVER BASIN
❑AMBIENT ❑
jjS��AjMf/PLE
El
REPORT TO: ARO FRO MRO RRO WaRO WiRO WSRO T5
QA
L' ISTREAM
EFFLUENT
AT BM
❑ A N
❑ LAKE
❑ INFLUENT r
Other
COMPLIANCE Lt !�C
OF CUSTODY
❑ EMERGENCY
❑ ESTUARY
E
FAV[
Shipped by: Bps Other
Couri, Staff,
�i GG
COLLECTOR[-S): [ �7_ 0�
1
Estimated BOD Range: 0-5/5-25/25-65/40-130 or 100 plus
STATION LQCATION: (ye«e•r
Seed: Yes ❑ No ❑ Chlorinated: Yes ❑ No ❑
REMARKS:
-
!�s *U Z' T rIv— t— /
] 4o
---
JL!Jjjj€
- e - ----_ J
Station] Date Begin (yy/mm/dd) Time Begin Date End Time End Depth DM DB DBM Value Type
A H L
1
i
•130135 310 !',� mgn
�t
2
COD High 340 mgA
3
COD Low 335 moll
- 4
Collform: MF Fecal 31616 5[w� /100ml
' i
5
Collform: MF Total 31504 /100ml
6
Coliform: Tube Fecal 31615 /100ml
7
Coliform: Fecal Strep 31673 /100ml
8
Residue: Total SW mg/I
9
Volatile 505 1. mgA
10
Fixed 510 moll
11
Residue: Suspended 530 mg/i
i2
Volatile 535 moll
13
''
Fixed 540 moll
14
pH 403 units
15
Acidity to pH 4-s 436 mg/1
16
Acidity to pH 8-3 435 moll
17
Alkalinity to pH 8.3 415 moll
i8
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mg/I
20
Turbidity 76 NTU
Chloride 940 moll
Chi a: Tri 32217 ug/1
Chi a: Corr 32M USA
Pheophytln a 32213 ug/I
Color: True 80 Pt -Co
ColorApH ) 83 A_DMI
Color. pH 7.6 82 ADM]
Cyanide 720 mg/1
Fluorkie 951 m�
Formaldehyde 7I880 mg/1
Grease and Oils 556 mgA
Hardness Total900 moA
Specific Cond. 95 uMhos/em2
MBAS 38260 =sA
Phenols 32730 ugA
Sulfate 945 mg/I
Sulfide 745 mg/1
NH3 as N 610 moll
TKN as N 625 mgA
NO2 plus NO3 as N 630 moll
P: Total as P 665 moll
PO4 as P 70507 moll
R Dissolved as P 666 moll
Cd-Cadmium 1027 don
Cr<rrvm1urn:Tota11034 USA,,-
Cu-Copper 1042 ugA
Ni-Nickel 1067 USA
Pb-Lend 1051 USA
Zn-zinc 1092 ugA
Ag-Silver 1077 ugA
AI -Aluminum 1105 u9A
Be -Beryllium 1012 .� doll -
Ca-Caicium 916 '�-ti mgA
Co -Cobalt 1037 ugA
Fe -Iron 1045 USA
Composite Sample Type
T S B C G GNXX
Li-Lithlum 1132 doll
Mg -Magnesium 927 moll
Mn-Manganese 1055 usA
Na-Sodium 929 moll
Arsenic:Total 1002 ug/i l
Se-Selenlum 1147 ugA
Hg-Mercury 71900 ugA
Organochlorine Pesticides
Org..Vhosptrmu, Pesticides
Arid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoptankton
Sampling Point X
Conductance at 25NC
Water TemperaWm 40
D.O. mg/I
pH
Alkalinitym
I Acidity
Air Temperature 40
pH 4-5 pH 8.3
2
94
10
300 .'g
400 .
82244 1431
82243 182242
20
Salinity X
Precipitlon 0a/day)
Cloud Cover %
Wird Direction (peg)
Sbeam Flour Severity
Turbidity Severity
Wind Velocity MAf
can Stream Depth ft.
Stream Width I'
480
45 132
136
11351
11350
135
64
14
11
DMI/Revised 1.0/86

a
0
IRN. 0

f For Lab Use ONLY
DIVISION OF ENVIRONMENTAL MANAGEMENT
WA I�
UALITY FIELD
-LAB FORM (DM
COUNTY G 1,
PRIORITY
SAMPLE YPE
D
RIVER BASIN -
❑AMBIENT
❑
STREAM
REPORT TO: ARO FRO MRO RRO WaRO WiRO WSRO TS
QA
4 w�r
R
AT BM
❑COMPLIANCE
CHAIN
❑LAKE
❑ INFLUENT
Other
��
❑EMERGENCY
7 Y
❑ESTUARY
ENV. MAMA
/
Shipped by: Bus Course Staff, Other
FAYETTEVILLE R
COLLECTOR(S): _ - ij_,
Estimated SOD Range: 0-5A5/25-65/40-130 or 100 plus
Seed: Yes ❑ NOD Chlorinated. Yes ❑ No ❑
Station
1
2
3
4
f/ /
BOD5 310
COD High 340
con Low 335
Coliform: MF Fecal 31616
,
Coliform: MF Total 31504
6
Coliform: Tube Fecal 31615
7
8
Coliform: Fecal Strep 31673
Residue: Total 500
Volatile 505
I Bui,-Cou i rer�-Hand Del
jjFrom:
AJY BY: I%! CKe!\
TED-
'4 LOCATION
Begin ( /mm/dd) Time Be In Date End Time End De th DM DB DBM
yy 9 P
mg/I
mg/I
(100ml
/loos]
/100mI
/loom]
mgA
10
Fixed 510 mg/v
11
12
Residue: Suspended 530 mg/1
i
Volatile 535 mg/I
13
Fixed 540 mg/1
14
PH 403 units
•15
Acidity to psi 4.5 436 mg/1
16
Acidity to pH 8.3 435 mgA
17
Alkalinity to pH 8.3 415 mgA
} 18
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mgA
20
Turbidity 76 NTU
Chloride 940 mg/1
Chi a: Tri 32217 ug/l
Chi a: Corr 32209 USA
Pheophytin a 32213 ug/1
,.w
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color. pH 7.6 82 ADM]
Cyanide 720 mg/1
Fluoride`951 mg/l
Formaldehyde 71880 _01
Grease and Oils 556 m9A
Hardness Total900 mg/I
Specific Cond. 95 amos/cm2
M AS 38260 _ mg/l
Phenols 32730 ngA
Sulfate %5 f mgA '
Sulfide 745 mg/1
re Type
A H L
NH3 as N 610 mg/1
TKN as N 625 mgA
NO2 plus NO3 as N 630 mg/I
P: Total as P 665 mSA
PO4 as P 70507 mgA
P: Dissolved as P 666 mgA
Cd{;admium 1027 ug/I
Cr-Chromfum:Totai ION ug/1
Cu Copper 1042 ugA
Ni-Nickel 1067 ug/1
Pb-Lend 1051 ugA
Za-Zinc 1092 ngA
Ift-gliver 1077 ug/i
Ai -Aluminum 1105 u9/1
Be -Beryllium 1012 USA
Ca -Calcium 916 mgA
Co -Cobalt 1037 ugA
Fe -Iron 1045 _, : - ugA
i.!
Composite
T S 13
Sample Type
C G GNXX
Li -Lithium 1132 ug/l
Mg-Magneslum 927 mgA
Mn-Manganese 1055 ug/I
Na-Sodium 929 mgA
Arsenir.Total 1002 ug/1
Se -Selenium 1147 ug/1
Hg-Mercury 71900 u2/1
Organochlorine Pesticide.
Organaphaspirmus Pesbddes
Acid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton
Sampling Point X6
Conductance at 25 C
Water Temperature 00
D.O. mgA
pH
%' Alkalinity
Acidity
Air Temperature 40
PH &3 pH 4.5
pH 4.5 pH 8.3
2
94
10
300 .
400 is
82244 1431
82243 J82242
20
Salinity X
Precipition (In/day)
Cloud Cover %
Wind Direction (Deg)
Stmmm Flow Severity
Turbidity Severity
Wind Velocity MAi
can Stream Depth fL
Strum Width ft.
484
45
132
36
1351
1350
35
64
4
1
v
DM1/Revised 10/86

�.
t-�
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ti
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DIVISION OF12E��NVIR�'ONMENTAL MANAGEMENT WAUALITY FIELD -LAB FORM (DM1)
F
COUNTY r-54,k1`
PRIORITY
SAMPLE TYPE
RIVER BASIN 'F I —
❑AMBIENT
❑
1 iJ STREAM
❑
REPORT TO: ARO
F,a MRO RHO WaRO WIRO WSRO TS
QA
AT
❑COMPLIANCE
LAKE
❑
OtherM
CHAIN
O T DY
T; . lak II.- /]Nl V
Lab Number - 61l //i��-'I�
ec d From: Bu *Courier -Hand Del
r
nR a CK!
DATER r � f
EMERGENCY
F cus a ;
ESTUARY
Shipped by: Bus Courier, Staff, Other
ANy.FAMA
mom
COLLECTOR(S): t�
ILLE R
Estimated SOD Range: 0-5/5-25/25-65/40-130 or 100 plus STATION LOCATION:
YE
r
Seed: Yes ❑ No ❑ Chlorinated: Yes ❑ No ❑ REMARKS:
Station #
Date Begin (yy/mm/dd) Time Begin
Date End
Time End Depth DM DB DBM
Value Type
Composite
Sample Type
f I �? �i}%i
A H L
T S
8
C G GNXX
1
RODS 310 1316
mg/1
2
COD High 340
mg/1
3
COD Low 335
mg/1
4 f
Coliform: MF Fecal 31616 r i f1
/100m1
5
Coliform: MF Total 315M
/loom]
6
Coliform: Tube Fecal 31615
/loom)
-,
CoIiform: Fecal Strop 31673
/Ioom]
S
Residue: Total500 myi
9
Volatile 505 pmg/1
10
Fixed 510 mg/l
11
Residue: Suspended 530 mg/l
12
Volatile 535 mg/l
13
Fixed 540 mg/i
14
pH 403 units
15
Acidity to pH 45 436 mg/l
16
Acidity to pH 8.3 435 mg/I
17
Alkalinity to pH 8.3 415 mg/1
1s
Alkalinity to pH 4.5 410 mg/l
19
TOC 690 mg/l
20
Turbidity 76 NW
Chloride 940 mg/l
Chi a: Tri 32217 USA
Chi a: Corr 322D9 ug/I
Pheophytin a 32213 ug/1
Color: True 80 Pt -Co
Color.(pH ) 83 -ADM]
Color. pH 7.6 82 ADMI
Cyanide 720 mg/I
Fluoride 951 Y49n
Formaldehyde 71880 mg/l
Grease and Oils 556 mg/l
Hardness Total900 mg/1
Specific Cond. 95 umos/cm2
MBAS 38M mg/i
Phenols 32730 ug[i
Sulfate 945 Warn
Sulfide 745 mg/1
l� 1
NH3 as N 610 mgA
TKN as N 625 mg/1
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mSA
PO4 as P 70507 mgA
P. Dissolved as P 666 mgA
Cd-Cadmium 1027 ug/1
Cr Chromium Total 1034 USA
Cu4Copper 1042 ug/1
Ni-Nickel 1067 no
Pb-Lead 1051 USA
Zu-Zinc 1092 ugA
liver 1077 ugA
AI -Aluminum 1105 ug/i
Be-Beryillum 1012 ag/l
Ca -Calcium 916 WSA
Co -Cobalt 1037 ugA
Fe -Iron 1045 , ug/I
Li -Lithium 1132 ug/1
Mg -Magnesium 927 mg/1
Mn-Manganese 1055 u9/1
Na-Sodium 929 mg/l
ArsenicTotal 1002 ug/l
Se -Selenium 1147 ugA
Hg-Mercury 71900 ug/1
Organochlorfne Pesticides
Organophasphmrrs Pesticides
Add Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle reg'd)
Phytoplankton
Sampling Point X
Conductance at 25 C
Water Temperature 40
D.O. mg/l
pH
s Alkalinity
Acidity
Air Temperature a
PH 8.3 pH 4Z
pH 45 pH 8.3
2
94
10
300 1
400 10
$2244 1431
82243 182242
20
Salinity X
Precipitlon On/day)
Cloud Cover 76
Wind Direction (Deg)
Strearn Flow Severity
Turbidity Severity
Wind Velocity MAI
Kean Stream Depth ft
Stream Width ft.
480
145
32
136
113SI
1350
135
64
14
IF
DM1/Revised 10/86

e
�A

ya SSA7L w
d �rw"n
State of North Carolina
Department of Environment, Health, and Natural Resources
Fayetteville Regional Office
James G. Martin, Govemor
DIVISION OF ENVIRONMENTAL, MANAGEMENT
March 19, 1990
CERTIFIED MAIL
RETURN RECEIPT REQU STED
Mr. Hugh Danford
Danford Brothers Dairy Farm
Route 3, Box 428
Bladenboro, NC 28320
William W. Cobey, Jr., Secretary
SUBJECT: Notice of Violation
Violation of Water Quality Standards
(143-215.1 (a)(6)
Danford Brothers Dairy Farm
Bladenboro, North Carolina
Bladen County
Dear Mr. Danford:
As the result of citizen complaint regarding an animal waste discharge
from your dairy operation, an investigation was conducted by the Fayetteville
Regional Office on February 14, 1990 and Brown Marsh Swamp was sampled to
determine water quality impact. This sample results revealed that the
dissolved oxygen level downstream of the runoff from your dairy was below the
water quality standard for Class "C Swamp" waters.
According to Administrative Code Section: 15 NCAC 2B.0100, the Standard
for dissolved oxygen levels in designated "C swamp" waters such as.,Brown Marsh
Swamp is an average of 5.0 mg/1 and an instantaneous low of 4.0 mg/l. Our
sampling revealed the dissolved oxygen level to be 0.25 mg/1 downstream of the
dairy and 'the upstream (collected above your dairy) was 4.6 mg/l. These
results indicate that the wastewater discharge from your dairy operation did
result in a violation of water quality standards.
This represents a direct violation of NCGS 143-215.1 (a)(6) for which a
civil penalty may be.assessed in accordance with NCGS 143-215.6.
Wachovla Building, Suite 714 • Fayetteville, N.C. 28301-5043 • Telephone [phone]
An Equal Opportunity AEfirmadve Action Employer

-P 42-3 027
RECEIPT FOR CERTIFIED MAIL
NO INSURANCE COVERAGE PROVIDED
HOT FOR INTERNATIONAL MAIL
(See Reverse)
"
Sent to
MR HUGH DANF'ORD
slrreletldo3 SOX 428
P.oiHt�USUaILMORO NC 28320
Postage
S
Certitied Fee
.85
Special Delivery Fee
Restricted Delivery Fee
Return Receipt showing
to whom and Date Delivered
.90
Return Receipt showing to whom,
Date, and Address of Delivery
TOTAL_ Postage and Fees
5
f�(f
Postmark or Date
LL
fi

s
Mr. Hugh Danford
Page 2
March 19, 1990
It is requested that you initiate waste manegement
practiill
eliminate the runoff of the waste from your dairy into surface cwater es that
of wthe
State, It is requested that you provide our office with a :response by no
later than March 31 1990 proposing corrective action.
I would like to point our that this letter in no way absolves you of the
responsibility for allowing wastewater to enter surface waters Of the State
resulting in a violation of water quality standards.
A copy of this letter is being sent to the Bladen County Agriculture
Extension Service, and to the Biological and Agricultural Engineering
Department, NCSU for their information and to aid them in providing technical
assistance to you to eliminate the existing problems from your facility.
Should you have any questions regarding this matter, feel free to notify
Mr. Grady Dobson, Environmental. Engineer of Our office at (919)" 48'6-1541.,
• Si erel
J. No],.an ,= E.
Regional 9ii ervisor•:....... '
MJN/G➢/mla
cc: Mr. Keith Dennis
Dr. Jim Barker
SENDER: Complete Items 1 and 2 when additional services are desired, and complete items
3 and 4.
Put your address in the "RETURN TO" Space on the r vorse siderFeilure to do this will prevant this card
from being returned to you, The return receiRtt fee will 11rovide you the name of the erson delivered to and
the date of deViver . For additional" Tees The following services are available.onsu t postmaster for Tees
and check ox es or additional services? requested.
1. ❑ Show to whom delivered, date, and addressee's address. 2. ❑ Restricted Delivery
{Extra charge) (Extra charge)
3. Article Addressed to:
4'. Article Number
MR HUGH DANFORD
P 423 027 836
DANFORD DAIRY FARM
Type of Service:
ROUTE 3 BOX 428
❑ Registered ❑Insured
®Certified ❑
BLADENBORO NC 28320
RDDfn Recei t
❑ Express Mail ❑fartuMerchandise
Alwaysfpbtain signature of addesseo
or agent and DATE DELIVERED.
5. Signature — Addressee
8. A essee's Address (ONLY if
X
(e 4ed and fee paid)
C :-
B. Siansturek4s Agen
x
7. Date of Daery
.,PS Form 3811, Apr. 1989 = *u.s.a.P.o,1069-238-e15 DOMESTIC RETURN RECEIP7s^;

DIVISION OF ENVIRONMENTAL MANAGEMENT
March 19, 1990
M E M 0 R A N D U M
TO: Chuck Wakild, Deputy Director
Division of Environmental Management
THRU: Steve Tedder, Chief
Water Quality Section
FROM: M. J. Noland, Regional ^fic
Fayetteville Regional
SUBJECT: Concentrated Animal Operation
Danford Dairy Farm
Bladen County
On February 26, 1990, Mr. Grady Dobson, Environmental Engineer, and
Mr. Ricky McLamb, Monitoring Technician, conducted an investigation in
response to a,local resident's complaint. Our investigation revealed that the
Danford Dairy. Farm had - a discharge of wastewater from a man-made drainage
ditch into Brown Marsh Swamp, Class "C" Swamp, Lumbee River Basin. The flow
in the ditch, consists of surface runoff from the dairy barn complex and
surrounding pasture land during rainfall events..
The farm is a 429-milk cow dairy farm operation consisting of feeding
barns, containment barns, and milk barns. All cow manure is scraped from
these containment barns and milk barns into a concrete pit and mixed with
water and pumped into a 1.0-MG capacity holding tank. The wastewater from
this tank is applied via honey wagons to farm land during planting season and
after summer and fall harvest seasons. During this inspection, waste was
being removed from the tank and land applied to farm fields. The manure
which spilled on the ground will be imbedded in tractor tires and deposited
onto farm haul roads and eventually diverted into the man-made drainage
ditches. The sample analysis for samples collected on this date indicates
that wastewater from the dairy farm does enter state surface waters via the
drainage ditches.
It is our opinion that the ditch collects surface water runoff from the
barn area and adjacent pasture and would receive wastewater from farm haul
roads during rainfall events. There were no point sources of discharge except
that of the drainage ditch outlet(s) to surface waters.

Mr. Chuck Wakild
Page 2
March 19, 1990
During the course- of the inspection, determinations were made in
accordance with NC Administrative Code 2H .0123(a)(3). The investigation did
reveal the following:
1. It was determined that a pollutant discharge had occurred from the
Danford Dairy Farm resulting in a violation of water quality standards,
as a result of any rainfall event less severe than a 25-year, 24-hour
event. The following represents the sample data taken on February 14,
1990, inspection:
Pasture Drainage
Ditch from Dairy
Upstream Complex Downstream
BOD5 (mg/1) 1.6 170 76
Fecal Coliform (/100 ml) 10.0 320,000 100
Dissolved Oxygen (Field 4.6 0.20 0.25
Parameter) (mg/1)
2. The state's surface waters (Brown Marsh Swamp, Class C Swamp,.Lumbee
River Basin) are impacted by the subject dairy farm (see above sample
analysis). This stream impact occurs as the result of improper waste
management practices --more specifically --the runoff of waste from the
barn, wastewater holding tank, and adjacent pasture. This problem is not
the result of a 25-year, 24-hour rainfall event.
In accordance with field evaluation and the "Concentrated Animal Feeding
Operation Regulation," the owner should be given notice in accordance with
Subchapter 2H, Section .0123(b).
It is recommended that the attached Letter to Mr. Hugh Danford, Danford
Dairy Farm, be sent notification stating that this dairy operation needs to
have a permit application submitted or the discharge eliminated within 60 days
in accordance with the NC Administrative Code and Code of Federal Regulations.
MJN/GD/tf X
Enclosures

d as STATE o
State of North Carolina
Department of Environment, Health, and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor
William W. Cobey, Jr., Secretary
March 19, 1990
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
Mr. Hugh Danford
Danford Dairy Farms
Route 3, Box 428
Bladenboro, NC 28320
George T. Everett, Ph.D.
Director
SUBJECT: Concentrated Animal Feeding Operation
Designation
Double J. Dairy Farm
Sampson County
Dear Mr. Danford:
This letter is to notify you that your dairy farm was investigated on
February 26, 1990, by members of the -,staff of the Fayetteville Regional Office
and Mr. Keith Dennis, Bladen County Extension Director, and determined to be a
concentrated animal feeding operation in accordance with Title 15, North
Carolina Administrative Code 2H .0123, and adopted Federal Regulations 40
CFR 122.23. The inspection showed that you had established a concentrated
animal feeding operation requiring such designation based upon the following
facts:
1. Wastewater entered Brown Marsh Swamp, Class C Swamp, Lumbee
River Basin, via a man-made drainage ditch from rainwater
runoff originating from surrounding pasture land and from the
dairy barn confinement area.
2. Your facility consists of approximately 429 dairy cows (1.4 x
429 = 601 animal units).
3. Animal waste was observed leaving the dairy barn confinement
area and pasture land.
Pollution Prevention Pays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Mr. Hugh Danford
Page 2
A National Pollutant Discharge Elimination System (NPDES) permit is
required for discharges of waste to the surface waters of the state. However,
if you can permanently eliminate the discharge of wastewater through the
drainage ditch by implementing changes within sixty (60) days of your receipt
of this notice, including, but not limited to, modifications to waste facility
and the implementation of a final waste disposal plan, a permit application
will not be required. If compliance has been achieved, you must notify us in
writing within sixty (60) days describing in detail the changes or modifica-
tions you made.
If the discharge of waste to the surface waters of the state is not
permanently eliminated within sixty (60) days of receipt of this notice, a
NPDES permit application must be submitted within that time.
Permit applications should be submitted in duplicate to the Director,
Division of Environmental Management, P.O. Box 27687, Raleigh, NC 27611.
Assistance, if desired, can be obtained by contacting Mr. Tommy Stevens, Water
Quality Regional Supervisor, Suite 714, Wachovia Building, Fayetteville,
NC 28301-5043, [phone]. The applications should be accompanied by
construction plans for the nondischarging animal waste management system.
For your information, the following items are enclosed:
1. One copy of the Federal Register - Concentrated Animal Feeding
Operations, 40 CFR 122.23.
2. Three copies of NPDES Discharge Permit application - Short
Form B.
If you need advice or technical assistance with regard to managing animal
waste, you should contact your county extension chairman or North Carolina
State University's Department of Biological and Agricultural Engineering at
[phone].
If you wish to contest this Designation, you must request an administra-
tive hearing within thirty (30) days of your receipt of this notice. This
request must be in the form of a written petition, conforming to Chapter 150E
of the North Carolina General Statutes, and filed with the Office of Adminis-
trative Hearings, P.O. Drawer 11666, Raleigh, NC 27604. A copy of the peti-
tion should be filed with this office.
If you do not request an administrative hearing, this Designation will
become final in thirty (30) days.

Mr. Hugh Danford
Page 3
A copy of this letter is
tives for information and to
Should you have any questions
contact us.
being sent to agricultural agency representa-
aid them in providing cooperative assistance.
regarding this matter, please do not hesitate to
Sincerely,
George Everett
Director
GE/GD/tf
Enclosures
cc: Fayetteville Regional Office
M. Keith Dennis
Dr. Jim Barker

-tm

+w STATt n
wn
State of North Carolina
Department of Environment, Health, and Natural Resources
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor
William W. Cobey, Jr., Secretary
March 19, 1990
CERTIFIED MALL
RETURN RECEIPT REQUMTED
Mr. Hugh Danford
Danford Dairy Farms
Route 3, Box 428
Bladenboro, NC 28320
George T Everett, Ph.D.
Director
1 !217,4
P1990
ENV MANAGEMENT
FAYETTEVILL.E REG. OFFICE
SUBJECT: Concentrated Animal Feeding Operation
Designation
Double J. Dairy Farm
ounty
,g AWIA1
Dear Mr. Danford:
This letter is to notify you that your dairy farm was investigated on
February 26, 1990, by, members of the staff of the Fayetteville Regional Office-:
and Mr. Keith Dennis, Bladen County Extension Director, and determined to be a
concentrated animal feeding operation in accordance with Title 15, North
Carolina Administrative Code 2H .0123, and adopted Federal Regulations 40
CFR 122.23. The inspection showed that you had established a concentrated
animal feeding operation requiring such designation based upon the following
facts-
1. Wastewater entered Brown Marsh Swamp, Class C Swamp, Lumbee
River Basin, via a man-made drainage ditch from rainwater
runoff originating from surrounding pasture land and from the
dairy barn confinement area.
2. Your facility consists of approximately 429 dairy cows (1.4 x
429 = 601 animal. units).
3. Animal waste was observed leaving the dairy barn confinement
area and pasture land.
Pollution Prevention Pays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

��Tn ���: a��������������_
...,.
��, � y
r t:,� fps � �, r �,

r
Mr. Hugh Danford
Page 2
A National Pollutant Discharge Elimination System (NPDES) permit is
required for discharges of waste to the surface waters of the state. However,
if you can permanently eliminate the discharge of wastewater through the
drainage ditch by implementing changes within sixty (60) days of your receipt
of this notice, including, but not limited to, modifications to waste facility
and the implementation of a final waste disposal plan, a permit application
will not be required. If compliance has been achieved, you must notify us in
writing within sixty (60) days describing in detail the changes or modifica-
tions you made.
If the discharge of waste to the surface waters of the state is not
permanently eliminated within sixty (60) days of receipt of this notice, a
NPDES permit application must be submitted within that time.
Permit applications should be submitted in duplicate to the Director,
Division of Environmental Management, P.O. Box 27687, Raleigh, NC 27611.
Assistance, if desired, can be obtained by contacting Mr. Tommy Stevens, Water
Quality Regional Supervisor, Suite 714, Wachovia Building, Fayetteville,
NC 28301-5043, [phone]. The applications should be accompanied by
construction plans for the nondischarging animal waste management system.
For your information, the following items are enclosed:
1. One copy of the Federal Register - Concentrated Animal Feeding
Operations, 40 CFR 122.23.
2. Three copies of NPDES Discharge Permit application - Short
Form B.
If you need advice or technical assistance with regard to managing animal
waste, you should contact your county extension chairman or North Carolina
State University's Department of Biological and Agricultural Engineering at
[phone].
If you wish to contest this Designation, you must request an administra-
tive hearing within thirty (30) days of your receipt of this notice. This
request must be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Adminis-
trative Hearings, P.O. Drawer 11666, Raleigh, NC 27604. A copy of the peti-
tion should be filed with this office.
If you do not request an administrative hearing, this Designation will
become final in thirty (30) days.

Mr. Hugh Danford
Page 3
A copy of this letter is being sent to agricultural agency representa-
tives for information and to aid them in providing cooperative assistance.
Should you have any questions regarding this matter, please do not hesitate to
contact us.
Sincerely,
Original Signed Byl
George T. EYI ItIl
George Everett
Director
GE/GD/tf
Enclosures
cc: Fayetteville Regional Office
M. Keith Dennis
Dr. Jim Barker

?or Invast1gatioa of
Samples collected aad
Division of Environmental Management
CHAIN OF CUSTODY R=RD
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Date Tim
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SAMPLE TYPE
RIVER BASIN-< f
❑AMBIENT
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1 /
Date Received:�?_
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DATA ENTRY BY:
1 J-1 CK:
DATE REPORTED:-
ZC" C i
COLLECTOR(S):. __1-e1
Estimated BORange: 0-5/5-25125-65/40130 or I00 plus STATION LOCATION:
D
Seed: YesEl NoO Chlorinated: Yes ❑ No ❑ REMARKS:
Station` Date Begin (yy/mm/dd) Time Begin pate End Time End Depth DM DB DBM Value Type Composite Sample Type
{ rya C u 9 t" �d h�f A H L T S B C G GNXX
BODS 310 mgA
COD High 340 mg/1
4
X
Coliiorm: MF Fecal 31616 416 /loom]
5
Coliform: MF Total 31SO4 /300m1
6
Coliiorm: Tube Fecal 31615. /1ooml
7
Coliiorm: Fecal Strep 31673 /100ml
8
Residue: Total 500 mg/I
9
Volatile 505 mgA
10
Fiz0'510 mg/1
11
Residue: Suspended 530 mg/1
12
Volatile 535 mg/I
13
Fixed S40 mg/1
14
PH 403 units
15
Acidity to pH 4S 436 mgA
16
Acidity to pH 8.3 435 mg/l
17
Alkalinity to pH 8.3 415 mgA
18
Alkalinity to pH 4.S 410 mg/1
19
TOC 690 mgA
20
Turbidity 76 NTU
Chloride 940 "A"mgA
Chi a: TO 322I7 USA
Chi a: Corr 32209 sigh
Pheophytin a 32213 Ug/1
Color: True 80 Pt -Co
Color:(pH ) 83 ADM[
Color. pH 7.6 82 ADMI
Cyanide 720 mg/I
_i9_-
Fluoride 951 mg/I
Formaldehyde 71890 mg/I
Grease and Oils 556 ✓--mgA
Hardness Total9D0 mg/I
Specific Cond. 95 UMhos/cm2
MBAS 38260 mgA
Phenols 32730 USA
Sulfate 945 66/1.
Sulfide 745 MSA
NH3 as N 610 mgA
TKN as N 625 mgA
NO2 plus NO3 as N 630 mg/l
P: Total as P 665 mg/i
PO4 as P 70507 mgA
P: Dissolved as P 666 mgA
Cd-Cadmium 1027 USA
Cr-Chramium:Total1034 t ngA
Cu•Copper 1042 USA
NMIckel 1067 USA
Pb-Lead 1051 USA
Zn Zinc 1092 USA
Ag-Silver 1077 USA
AI -Aluminum 1105 ug/I
Be -Beryllium 1012 USA
Ca -Calcium 916 mg/I
Co -Cobalt 1037 USA
Fe -iron 1045 USA
Sampling Point X
Conductance at 25 C
Water Tempwrture n
D.O. mg/I
pit �
Alkalinity
Acidity
pH R3 pH 4s
pH 4.5 oFAMETTEVIL
REQ OFFI
2
94
10 f
300 •
400 •
82244 431
82243 82242
20
Salinity X
Precipition On/day)
Cloud Cove X
Wild D (Deg)
imam Flow Severity
Turbidity Severity
Wind Velocity MA1
Mean Stream Depth it.
Silesia Width it
490
45
32
36
1351 -
1350
35
64
4
R 4"

0
r

For Lab Use ONLY 1,6! ,
DIVISION OF ENVIRONMENTAL MANAGEMENT WATEALITY FIELD -LAB FORM (DMi)
'11j�L
4
COUNTY
PRIORITY
W_
SAMPLE TYPE
RIVER BASIN
[]AMBIENT
❑
❑
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QA
STREAM
EFFLUENT
AT BM
❑COMPLIANCE
' CH
❑ LAKE
❑ INFIJ.IENT
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❑
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❑
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Shipped by; Bvs�C`u�ii. :staff, Other
EMERGENCY
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Lab Number-
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Date Received:
Time:
Rec'd by:
From: Bus -Courier -Hand Del
DATA ENTRY BY:�
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CK: 1 'I
DATE REPORTED:
3 -� f
COLLECTOR(S)
Estimated BOD Range: 0 5/5-25/25-65l40-130 or 100 plus STATION LOCATION:
Seed: Yes ❑ No ❑ Chlorinated: Yes ❑ No[] REMARKS:
Statloa $ Date Begin (yy/mm/dd) I Time Begin I Date End Time End Depth DM DB DBM Value Type Composite [Sample Type
A H L T S B C G GNXX
1
BODS 310 e1 mgA
2
COD High 340 moll
3
COD Low 33S mg/1
4
Coliform: MF Feral 31616 ! /100m1
5
Coliform: MF Total 31504 /looml
6
Coliform: Tube Fecal 31615 /norm
7
Coliform: Fecal Strep 31673 /loom
8
Residue: Total 500 mg/l
9
Volatile SOS mgA
10
Fixed 510 mg/1
11
Residue: Suspended 530 mg/I
12
Volatile 535 mg/I
1$
Fixed S40 mg/1
14
PH 403 units
15
Acidity to pH CS 436 mgA
16
Acidity to pH 8.3 435 mg/1
17
Alkalinity to pH 9.3 415 moll
18
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mg/l
20
Turbidity 76 N1U
Chloride 940
Chi a: Tri 32217 ug/1
Chi a: Corr 32209 agA
Pheophytin a 32213 ug/[
Color: True 80 Pt -Co
Color:(PH ) 83 ADMI
Color. pH 7.6 82 —ADM]
Cyanide 720 mg/1
Fluoride 951 mg/F
Formaldehyde 71880 mg/I
Grease and Oils 556
Hardness Total900 mg/I
Specific Cond. 95 uMhos/cm2
MBAS 38260 _mg/I
Phenols 32730 ug/f
Sulfate 945 mg/I
Sulfide 745 mg/1
NH3 as N 610 mg/l
TKN as N 625 mg/l
NO2 plus NO3 as N 630 m9A
P: Total as P 66S mgA
PO4 as P 70507 mg/I
P: Dissolved as P 666 mgA
y�
Cd-Cadminm 1027 ug/1
Cr4;hromium Total ION ug/1
Cu-Copper 1042 ug/I
NI -Nickel 1067 ugA
Pb-Lead 1051 ugA
Zn-Zinc 1092 ug/1
A ilver 1077 ugA
AI -Aluminum 1105 ugA
Be -Beryllium 1012 agll
Ca -Calcium 916 m9A
Co -Cobalt 1037 uSA
Fe -Iron 1045 USA
Sampling Paint
Conductance at 25 C
Water Temperature 40
/
D O. mg/l
PH
L f
Alkalinity
PH 93 PH 4.5
Acidity
pH 4.5 pH 9.3
Temperature (c}
2
94
10
300 .
400 0
82244 1431
82243 182242
20
Salinity X
Precipition (InMay)
Cloud Cover S
'Wind Dhection (Deg)
Stream Flow Severity
Turbidity Severity
Wind Velocity M/H
Kean Stream Depth ft.
Stream Width ft.
480
145
32
36
1351 µ
1350
35
64
4
DMl/Revised 10/86

9
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DIVISION OF ENVIRONMENTAL MANAGEMENT WATEVALITY FIELD -GAB FORM (DM1)
COUNTY
JF-
PRIORITY
SAMPLE TYPE
RIVER BASIN
❑AMBIENT ❑
❑STREAM
❑
REPORT TO: ARO FRO MRO RRO WaRO WIRO WSRO TS
, Q4
EFFLUENT
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�
E d D R 0-5 25 G5/40-13 1
STATION LOCATION- ='
stimate BO ange. /5- /25 0 or 00 pins
r.
Seed: Yes ❑ No ❑ Chlorinated: Yes ❑ No ❑ REMARKS:
Station # Date Begin (yy/mm/dd) Time Begin I Date End Time End Depth DM DR DBM
.- ffff
_._.. .... - •1 1 � � 1 1 T.J. �I� �Y'j 1 i
1
) y
vt
RODS 310 i I` i) mg/I
t
2
COD High 340 mg/l
3
COD Lour 335 mg/l
4�i
Coliform: MF Fecal 31616 # , : , ; " r/100m1
(J/100m1
5
f
Coliform: MF Total 315M
6
Calif arm: Tube Fecal 316I5 /100m1
7
Coliform: Fecal Strep 31673 /100mI
8
Residue: Total 500 mg/I
9
Volatile 505 mg/I
10
Fixed 510 mg/1
11
Residue: Suspended 530 mg/I
12
Volatile 535 mg/I
13
Fixed 540 mg/I
14
pH 403 units
15
Acidity to pH 4.5 436 mg/I
16
Acidity to pH 9.3 435 mg/I
17
Alkalinity to pH 8.3 415 mg/I
18
Alkalinity to pH 4.5 410 mg/I
19
TOC 680 mg/l
20
Turbidity 76 NTU
Chloride 940 mg/l
Chi a: Tri 32217 USA
Chi a: Corr 32209 u9/1
Pheophytin a 32213 ug/I
Color: True 80 Pt -Co
Color:(pH ) 83 ADMI
Color. pH 7.6 82 :7, ` ADMI
Cyanide 720 mg/l
Fluoride 951 - _ mg/I
Formaldehyde 71880 mg/I
Grease and Oils 556
Hardness Total900 mg/1
Specific Cond. 95 uMhos/cm2
MBAS 38260 mg/l
Phenols 32730 - ugA
Sulfate 945 mgA
Sulfide 745 mg/I
Fnr fah flxe t1Nt V
fJ U CX
Lab Number:
Date Receive
Time:
Rec'd bg
From: Bus_ -Courier -Hand Del
DATA ENTRY BY.
CK:
DATE REPORTED:
3 - 7o — I t
le Type
A H L
:✓ 1
NH3 as N 610 mg/l
TKN as N 625 mg/I
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mgA
PO4 as P 70507 tog/1
P: Dissolved as P 666 mg/I
Cd- admlum 1027 ugA
Cr0tromfuunTotalI= u10
[Srcopper 1042 ugA
NI -Nickel 1067 USA
Pb-Lead 1051 ugA
Za-Zinc 1092 ugA
Ag6fiver I077 agA
AI -Aluminum 110S ugA
Be-BeryRfum 1012 ug/I
Ca -calcium 916 m8/I
Co�Cobalt 1037 ugn
Fe -Iran 1045 ogA
Composite Sample Type
T S B C G GNXX
Sampling Point X
Conductance at 25 C
Water TemperaLne 40
D.O. mg/1
pH
Alkalinity
Acidity
Air Temperature 40
pH 83 pH 4.5
pH 4.5 pH 8.3
2
94
10
S00 ,
400 .
82244 431
$2243 82242
20
Salinity X
Precipition On/day)
Claud Cover S
Wind Dire n (Deg)
tivam flow Se%eztty
Turbidity Severity
Wind Velocity M/H
can Stream Depth it
Stream Width it.
490
145
132
36
1351
1350
35
64
14
Dbll/Revised 10/86

0
i

lk
Division of Environmental Management
CHAIN OF CUSTODY RECORD
For Investigation of .
SssPls• collect*d sadDK forms co■�pleted byt
O:ilf Station.
b'No.No. Station Location
La
Doterims
No. of
bottles
(o
WiD
2
Ral! tte by( gnature):
eived �j�(Si"ture)s
l'��dc�1y�-
Date Time
r a
1
Re byj
l
Rac by
l
Rec by (Lab)
l
i A % 114C V nlar_r
r�

I "

~
DIVISION OF ENVIRONMENTAL MANAGEMENT WATEFALITY
FIELD -LAB FORM (DM1) !
7
1
COliNil'Y'�
PRIORITY
_
SAMPLE TYPE
_
r~_
RIVER BASIN i
❑AMBIENT ❑
❑�
❑
REPORT TO: ARO FRO�MRO RHO WaRO WiRO WSRO TS
QA
STREAM
EFFLF3ENT
AT BM �"
Other
©COMPLIANCE U
CHAIN
OF CUSTODY
❑ LAKE
❑ INFLUEN T
11
Fn. I w6 rl•e nlut V
Lob Number. /
/I ��
e-% f
Date Received.- J I� Time: �• /
Rec'd tby
From: Bus:C_C e�r-baud Dal
DATA ENT BY-
CKA
DATE REPORTED:
.- ---^
Shipped br.1Bus-Courier; Staff, Other
EMERGENCYESTUARYVIP-*
COLLECT(1R(S): i -- � �
ti
_
Estimated SOD Range: 04/5 25/25-55/40-130 or lOD plus
STATION LOCATION:
Seed: Yes 0 No[:] Chlorinated: Yea ElNo ❑
REMARKS:
Station # Date Begin (yy/mm/ddi Time Begin
Date End
Time Ead
Depth DM DB DBM
Value Type Composite
Sample Type
A H L T 5
B
C G GNXX
1
RODS 310 mg/1
2
COD High 340 mg/1
3
COD Low 335 mg/l
4
)(
/�
Coliform: MF Fecal 31616 �__cWlooml
5
Coliform: MF Total 31504 /I00m1
Coliform: Tube Fecal 31615 /loom]
7
Coliform: Fecal Strep 31673 /100ml
8
Residue: Total 500 mg/I
9
Volatile 505 mg/1
10
11
Fized 510 mg/1
Residue: Suspended 530 mg/1
12
Volatile 535 mg/1
13
Fixed 540 mg/l
14
pH 403 unite
15
Acidity to pH 4.5 436 mwl
i6
Acidity to pH 8.3 435 mg/1
17
Alkalinity to pH 8.3 415 MO
18
Alkalinity to pH 4.5 410 mg/1
19
TOC 680 mg/l
20
J
Turbidity 76 NTU
Chloride 940 mgA
Chi a: Tri 32217 ug/l
Chi a: Corr 32209 ug/I
Pheophytiu a 32213 ag/i
Color. True 80 Ptfio
Color:ipH j 83 ADMI
Color. pH 7.6 82 ADMI
Cyanide 720 mg/I/1
Fluoride %t mg
Formaldehyde 71880 mg/l
Grease and Oils 556 mgA
Hardness Total900 mg/1
Specific Cond. 95 uMhos/cm2
MBAS 38260 % tag/]
Phenols $2730 ogA
Sulfate 9" Clio
Sulfide 745 mRA
NH3 as N 610 mg/I
TKN as N 625 mgA
NO2 plus NO3 as N 630 mg/I
Ptal : Toas P 665 mRA
PO4 as P 70507 _9A
P: Dissolved as P 666 mqA
Cd-Cadmium 10Z7 u9/1
Ct`Chramiu,=Totai lamtMA
Cu-Copper 1042 ttg/l
NI, -Nickel 1067 ug/1
Pb-Lead 1051 ag/I
ZnrZInc 1092 09A
After 1077 ug/1
Al -Aluminum 1105 ug/i
Be-Beryflium 1012 ttgA
Ca -Calcium 916 m9A
Co-Cohalt 1037 ug/l
Fe -Iron 1045 ug/l
Sampling Point X
Conductance at 25 C
Water Temperature 0
D"O- mg/l
pH
Alkalinity
Aci
am
pH 8.3 pH 4.5
pH 4.5 W.3
2
94
10
So0 1. 2.0
400 ! 1j
82244 1431
82243 182242
20
Salinity X
Precipitfon an/day)
Claud Cover S
Wind Direction Q?egj
re
tam Flow Severity
Turbidity Severity
Wind Velocity M/H
can Stream Depth ft.
Stream Width ft.
4f
490
145
132
136
11351
1350
135
64 14
DM1/Revised

DIVISION OF ENVIRONMENTAL MANAGEMENT WATE
ALITY FIELD -LAB FORM (DM1)
COliN[1'.i:' i
PRIORITY
SAMPLE TYPE
RIVER BASIN
❑AMBIENT
❑
(�
EYSTREAM
❑
REPORT TO: ARG FRO MRO RRO WaRO WiRO WSRO TS
QA
EFFLUENT
AT BM
❑COMPLIANCE
❑ CHAIN
❑ LADLE
❑ INFLUENT
Other
❑ F�IERGENCV
OF CUSTODY
❑ESTUARY
/1.
Shipped byA Bus Courier, S& tf, Other
tr- 1 rh rle AMr V
Lab Number: l/ Jf/l/ �f
Date Recelved.P/%rSrtl Time.• r J
Rec-d bV-_AX From: Bu*�Coprier-Hand Del
F V �__�4 CK: DATA ENTRY BY:
DATE REPORTED: Z' 71 ' rt
COLLECTOR(S)- ,w t! r/,e� .,� j
Estimated BOA Range 0-5/5-25/25-65/40-130 or 100 plus STATION LOCATION: f �:Prr�.� �tTiiu :."�l f✓•� /�7��i1h
Seed: Yea ❑ Na ❑ Chlorinated: Yes ❑ No 0 REMARKS: l ���F ���,.. aid .LDS :���i � t %� �r'�� �'� -'�., '`-�`%sue - .•r� ��'�--i�l:_�,
Stettaa ?�
Date Begfa (yyfmm/dd) Time Begta
Late End
Time End
Depth DM DB DBM
e Type
Composite
Sample Type
Q1� i? I�1 :�'G✓
H L
rA
T S B
C G GNXX
2
COD High 340 mg/1
3
COD Loa 335 mg/l
r
4
Coliform: MF Fecal 31616 - ry /100m1
tJ
5
Collform: MF Total 31504 /100m1
6
Coliform: Tube Fecal 31615 /]OGMI
7
CaIiform: Fecal Stmp 31673 /100ml
S
Residue: Towel 50D ms/I
9
Volatile 505 mgA
to
Fixed 510 mg/l
11
Residue: Suspended 530 mg/l
12
Volatile 535 mgA
13
Fixed 540 mg/1
14
pH 403 units
15
'.
Acldlty to pH 4Z 436 mgA
16
Acidity to pH 8.3 435 mg/l
17
Alkalinity to pH 8-3 415 mtl/1
18
Alkaiinity to pH 4.5 410 mgA
19
TOC 690 mg/l
20
Turbidity 76 NTU
Chloride 940 mg/I
Chi a: Tri 32217 ug/i
Chi a: Can 32209 ug/1
Pheophytin a 32213 ug/l
Color. True 80 Pt -Co
Color:(PH ) 83 ADMI
Color. pH 7.6 82 ADMI
Cyanide 720 mg/l
Fluoride 951 mg/l-
Formaldehyde 71880 mg/l
Grease and Oils 556 mgA
Hardness Total900 m8A
Specific Cond. 95 umos/cm2
MBAS 38260 Ing/I
Phenols 32730 ugA
Suffabe 945 _311
Sulfide 745 mgJl
NH3 as N 610 mgA
TKN as N 625 msA
NO2 plus NO3 as N 630 mgA
P: Total as P 665 mg/l
PO4 as P 70SO7 mgA
P: Dissolved as P 666 mgfl
Cd-Cadmlum 1027 ugA
CrChromium Total. 1034 ug/I
CUCopper 1042 ugA
NHVkkel 1067 ag/l
Pb-i�.ad I051 uRA
Zo-Zinc 1092 ugA
A tiver 1077 ugA
Al -Aluminum 1105 ug/I
Be -Beryllium 1012 ug/I
Ca -Calcium 916 m9A
Co -Cobalt 1037 ugJ1
Fr iron 1045 USA
Li -Lithium 1132 ugA
Mg-Magnestum 927 M9A
Mn-Manganese 1055 ug/l
Na-Sodlum 929 m9n
Arsenic -Total 1002 419/1
Se -Selenium 1147 agA
Hs-Mervary 71900 u9A
Organochlorine Pesticides
0lpnopteolpitolus Pesticides
Arid Herbicides
Base/ Neutral Extractable Organics
Acid Extractable Organics
Purgeable Organics (VOA bottle;tey'd)
V
%qj
-»
Sampling Point X
Conductance at 25 C
Water Temperaoae 40
D.O. nisi a
pH
Alkalinity
ANA
Ac;0&,Aall
�1!
%
pli
pH 4.5 RE
2
94
10
300 fl •?<-
4W /n •
82M 431
82243 182242
20
Salinity x
Precipition Wday)
Cloud Coves %
Wind Direction Oeg)
tream Flom Severity
Turbidity Severity
Wind Velocity M/H
4ean Stream Depth ft.
Stream Width ft.
480
45
32
36
MI
1350
35
64
4
DM1/Revised 10/86

0
r
mw---""
LA

V. r,.1, toes nwry
DIVISION OF ENVIRONMENTAL MANAGEMENT WATE*ALITY FIELD -LAB FORM (DM1)
COUNTY
PRIORiTY
SAMPLE TYPE
RIVER BASIN
❑AMBIENT
El
❑
REPORT TO: ARO FRO'MRO RRO WaRO WtRO WSRO TS
QA
STREAM
AT BM �
❑COMPLIANCE
❑ CHA1N
❑ LAKE
Other
❑F�iERGENCY
OF CUSTODY
ESTUARY
Shipped by: Bas CStaff, Other
COLLECTOR(S);
STATION LOCATION:
Estimated BOD Range: 0-5/5-25/25fi5/4il-130 or 100 plus
Seed: Yea D No Chlorinated: Yes❑ Na Q
REMARKS:y-
❑ EFFLUENT
❑ >Nl"131F1VT
Lab Number:
%
/]Cj�/G�/�`Y
[�
Date Rec�eiv]ed•,' ` "5 ! !( Time. / !
Rec'd +by _ /
From: _Bus-Cgu ier�r-Hand Del_
DATA ENTRY BY:
CW
DATE REPORTED:
��1�
y
/ • % 3 ` f)
�cf1�-•-r ..j �.vC�
kstation ,#' Date Begin (yy/mm/dd) Time Begin Date End Time End Depth DM DB DBM Value Type
I 9�i bt . l,,, i2•' ZJ A H L
1
✓
BOD5 310 y mall
. S
2
COD High 340 Mall
3
COD Low 335 M9A
4
V
Coliform: MF Feral 31616 /100M1
5
Coliform- MF Total 31504 _ /100m1
6
Coliform: Tube Fecal 31615 /loom]
7
Colliorm: Fecal Strep 31673 /lDOml
Residue. Total SOD MSn
9
t Volatile 50� , Mg/1
10
Fixed 510 mg/l `
11
Residue: Suspended 530 mall
12
Volatile 535 innA
13
Fixed 540 mg/1
14
pH 403 units
is
Acidity to pH 4 5 436 mall
16
Acidity to pH 8.3 435 mg/1
17
Alkalinity to pH 8.3 415 Mall
18
Alkalinity to pH 4.5 410 mall
19
TOC 690 MaA
,,,.
Turbidity 76 NTU
Chloride 940 mg/I
Chi a: TO 32217 ug/l
Chi a: Corr 322D9 u9A
Pheophytin a 32213 ug/l
Color. True 80 Pt -Co
Color.(pH ) 83 ADM]
Color: pH 7.6 82 ADM]
Cyanide 720 MgA
Fluoride 951 - mall
Formaldehyde 71880 mall
Grease and Oils 556 MSA
Hardness Total900 Mall
Specific Cord. 95 umos/cm2
MRAS 38260 Mali
Phenols 32730 ugA
Sulfate 945 MgA
Sulfide 745 mall
NH3 as N 610 019/1
TKN as N 625 m9/1
NO2 plus NO3 as N 630 MgA
P: Total as P 665 mall
PO4 as P 70507 _9A
P: Dissolved as P 666 Mali
Cd-Cadmium 1027 u9A
Cruut dumToud 1034 yam. u9A
C-C-Ppes 1042 .%A
NI -Nickel 1067 ugA
Pb-Lead 1051 us[A
7.n-Zlnc 1092 ug/I
A ilver 1077 ugA
AI -Aluminum 1105 ug/i
fie-Seryfitum 1012 ugn
Ca -Calcium 916 Mall
Co -Cobalt 1037 ngA
FeAron 1045 ug/I
Composite Sample Type
T S B I C G GNXX
Sampling Point
Conductance at 25 C I
Water Temperatute C
D.O. mall
pH
Alkalinity
AeidY�
pH 8 3 pH 4.5
pH 4.5 .3
2
94
10 ~'
f
SOD % . /
400 • i�
82244 431
82245 182242
20
Salinity %
Precipltion Wday)
Cloud Cow %
Wind Direction Mkeg)
[ream Flom Severity
Turbidity Severity
Wind Velocity M/M
can Stream Depth ft.Stream
Width fL
a
490
145
132
136
11351
1350
135
64
14
w
DM1/Revised 10/86

_J
I

ffi

aw, wwk-

rl

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ti::
".,

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l_i 7
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�cr

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r !�v
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