WQ0001026_Residual Annual Report 2014_20150223

MA
resources, Inc.
February 12, 2015
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2014 Annual Report - Washington
Treatment and Land Application of Residuals
Permit No. WQ0001026
Dear Sir or Madam:
RF0F_1 ED
Fp I 2015
p1�R S�GE`OAi
j*VhqATIONPROCESSING00VT
Enclosed are three copies of the 2014 Annual Report for the above referenced land
application permit.
During 2014 EMA Resources, Inc. land applied 325.01 dry tons of wastewater residuals
to 122.5 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincere
Brent Collins
Director of Technical Services
brent.collinskemaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

W�Ov@
City of Washington
2014 Annual Report
Residuals Land Application
Permit No. WQ0001026
Prepared By:
EMA Resources, Inc.
Phone [phone]— Fax 336.75I o 1442
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICAT+ION CERTIFICATION FORM
Permit#: WQ0001026 County: Beaufort County Year: 2014
Facility Name (as shownon permit): City of Washington
f^ Land Application Operator: EMA Resources Inc. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calender year?
F1 0 Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
56
Total number of fields land application occurred during the year:
5
Total amount of dry tons applied during the year for all application sites:
325.01
— "
Total number of acres land application occurred during the year:
122.5
Part B:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. 0 Yes ❑ No
I If no please, provide a written description -why the -facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
0 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
�I 5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
D Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
y�! 8. All operations and maintenance requirements in the permit were complied with or, in "the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
}
Lin accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property, or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
ft including the possibility of fines and imprisonment for knowing violations."
Adam Waters - Water Resources Superintendent �ri+. Z — J = Is-
Permittee Name and Title (type or print) Signature of Permittee Date
1 /22/2015
Signature of Preparer* Date Signiture of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)
DENR FORM ACF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001026 Laboratory: 1) A&L Laboratories
Facility Name: City of Washington 2)
NPDES # or NCO020648 3)
WQ#:
4)
WWTP Name: Washington WWTP 5)
Recidnal Analvcic Dntn
Sample or
Composite Date
6/12/14
6/18/14
June
Average
11/11/14
11/13/14
Nov.
Average
Percent Solids
4.7
4.43
4.565
4.13
4.1
4.115
Arsenic
6
6
6
6
6
6
Cadmium
3
2
2.5
2
2
2
Chromium
56
55
55.5
53
62
57.5
,b
Copper
199
208
203.5
207
210
208.5
Lead
37
31
34
36
36
36
Mercury
0.8
1
0.9
1.1
1.2
1.15
s
Molybdenum
5
6
5.5
5
5
5
Nickel
30
28
29
26
30
28
Selenium
5
5
5
5
5
5
Zinc
541
579
560
593
603
598
Total Phosphorus
17000
18200
17600
15200
15300
15250
TKN
33600
35900
34750
33700
33700
33700
Ammonia -Nitrogen
7660
7900
7780
6540
5120
5830
Nitrate and Nitrite
160
31.6
95.8
2
2
2
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Aa-n�2 J�, .� Z - 5-- L S
Signature of Preparer Date
DENR FORM RSSF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0001026 Laboratory: 1) A&L Laboratories
Facility Name: City of Washington 2)
NPDES # or 3)
W Q#; NC0020648
4)
WWTP Name: Washington WWTP 5)
Residual Analvsis Data
Sample or
CompositeDate
Potassium
Magnesium
------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer Date
DENR FORM RSSF-B (512003)

IF-, ANNUAL METALS FIELD LOADING SUMMARY FORM*
,
i f Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
acility Name:
ermit #:
Operator:
acres Used:
1�
City of Washington - Total Dry Tons Applied (Annual): 193.23
WQ0001026 Cation Exchange Capacity (non 503 only):
JD Briley Owner: JD Briley
62.4 Acres Permitted: 62.4 Site #: BF207 Field #: 4
1--tesidual
Analysis Data (Heavy
Metals and Total Phosphorus
use mg/kg,
% Solids
use Raw Percent #):
Sample
1
2
3j
4j
L5J6
7
8
9
10
11
12
r Corn-
June
Avg.
Iposite
- Date
'o Solids
4.57
Arsenic
6
admium
2.5
hromium
55.5
Copper
204
Lead
34
�Aercury
0.9
_ Molyb-
5.5
'denum
Nickel
29
Selenium
5
Zinc
560
Total
Phos-
17600
horns
_ i .nual
Heavy Metal Field Loadings
(Calculated
in lbs/acre):
0
11
L2J3
J
4
L5J
6
7
8
9
10
11
12
C7
y
N
A'+
o
3.0967
senic
0.0372
0
0
0
0
0
0
0
0
0
0
0
0.0372
Cadmium
0.0155
0
0
0
0
0
0
0
0
0
0
0
0.0155
�romi
0.3437
0
0
0
0
0
0
0
0
0
0
0
0.3437
Copper
1.2635
0
0
0
0
0
0
0
0
0
0
0
1.2635
Lead
0.2106
0
0
0
0
0
0
0
0
0
0
0
0.2106
fercury
0.0056
0
0
0
0
0
0
0
0
0
0
0
0.0056
dolyb-
denum
0.0341
0
0
0
0
0
0
0
0
0
0
0
0.0341
Nickel
0.1796
0
0
0
0
0
0
0
0
0
0
0
0.1796
zlenium
0.031
0
0
0
0
0
0
0
0
0
0
0
0.031
Zinc
3.4683
0
0
0
0
0
0
0
0
0
0
0
3.4683
Total
Phos-
109
0
0
0
0
0
0
0
.0
0
0
0
109
Iphorus
I certify, under penalty of law, that this document was prepared under
my direction
or supervision in
_�cordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
j',cluding the possibilitv of fines and imprisonment for knowing violations"
'ignature of Land Applier Date
fir --"See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematical M L%F (512003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington Permit #: WQ0001026 Annual Dry Tons Applied: 193.23
Owner: JD Briley Operator: JD Briley Cation Exchange Capacity (non 503):
Site #: BF207 Field #: 4 Acres Utilized: 62.4 Acres Permitted: 62.4
o
N
Y
Q
Specify
Totals
er
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
lte
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate* *
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop
p 1 or Crop
2
+�
Gal.
Ll
CuNd.
::
Re ort
Totals
in Gal.
Crop 1
Crop 2
6/17
39000
625
4.57
0.1191
Washington WWTP
Dry
<.51''
S
0.5
0.3
34750
7780
96
2.87688
#######
Beans
1
6/18
214500
3437.5
4.57
0.6551
Washington WWTP
Dry
<.5"
S
0.5
0.3
34750
7780
96
15.8228
#######
Beans
2
6/19
221000
3541.7
4.57
0.6749
Washington WWTP
Dry
<.5"
S
0.5
0.3
34750
7780
96
16.3023
#######
Beans
3
6/27
149500
2395.8
4.57
0.4566
Washington WWTP
Dry
<.5"
S
0.5
0.3
34750
7780
96
11.028
#######
Beans
4
7/2
234000
3750
4.57
1 0.7146
Washington WWTP
Dry
1 <.5"
S
1 0.5
0.3
34750
1 7780
96
17.2613
1 #######
Beans
1
5
7/3
156000
2500
4.57
0.4764
Washington WWTP
Dry
<.5"
S
0.5
0.3
34750
7780
96
11.5075
#######
Beans
6
0
0.0000
0
0
7
0
0.0000
0
0
8
0
0.0000
0
0
9
0
0.0000
0
0
1
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
16250
::::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.0372
0.0155
0.3437
1.2635
0.2106
0.0056
0.0341
0.1796
0.0310
3.4683
109.004
74.7988
0
Date
lbs/ac
Current Cumulative lbs/ac
0.1172 0.0421 0.8385 4.6891 0.6440 0.0320 0.1331 0.4677 0.0889 12.8989::::::::::::::...
0.0800 1 0.0266 0.4948 3.4256 0.4334 0.0264 0.0990 0.2881 0.0579 9.4306
36 34 1338 1 267 15 374 89 2498 .......................................
20 0 50
2000
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Perm rt PAN Limit lst/2nd Crop
p
"1 certily, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for subm t ing false information, including the possibility of fines and imprisonment for knowing violations."
"z.o1/22/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
acility Name:
ermit #:
Operator:
Icres Used:
City of Washington Total Dry Tons Applied (Annual): 17.87
WQ0001026 Cation Exchange Capacity (non $03 only):
Will Congleton Owner: Will Congleton
7.8 Acres Permitted: 7.8 Site #: PI201 Field #: 10
'Residual Analysis Data (Heavy
Metals and Total
Phosphorus
use mg/kg,
% Solids
use Raw Percent #):
ample
1
2
3
4
5
6
7
8
9
10
11
12
;r Com-
Nov
I-posite
Avg
Date
! `o Solids
4.12
Arsenic
6
-admium
2
' __chromium
62
Copper
209
I Lead
36
�Aercury
1.15
_Molyb-
5
' jenum
jNickel
28
Selenium
5
Zinc
598
Total
,Phos-
15250
�)horus
nnual Heavy Metal Field Loadings
(Calculated
in lbs/acre):
c
1
2
3
4
5
6
7
8
9
10
11
12
o
2.2907
��rsenic
0.0275
0
0
0
0
0
0
0
0
0
0
0
0.0275
Cadmium
0.0092
0
0
0
0
0
0
0
0
0
0
0
0.0092
llronlluz
0.284
0
0
0
0
0
0
0
0
0
0
0
0.284
opper
0.9575
0
0
0
0
0
0
0
0
0
0
0
0.9575
Lead
0.1649
0
0
0
0
0
0
0
0
0
0
0
0.1649
Zercury
0.0053
0
0
0
0
0
0
0
0
0
0
0
0.0053
-Jolyb- I
0.0229
0
0
0
0
0
0
0
0
0
0
0
0.0229
denum
Nickel
0.1283
0
0
0
0
0
0
0
0
0
0
0
0.1283
—:lenium
0.0229
0
0
0
0
0
0
0
0
1 0
0
0
0.0229
_. Zinc
2.7397
0
0
0
0
0
0
0
0
0
0
0
2.7397
Total
-Phos-
69.866
0
0
0
0
0
0
0
0
0
0
0
69.866
horus
certify, under penalty of law, that this document was prepared under my direction or supervision in
cordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
I luding the possibilitv of fines and imprisonment for knowing violations"
1/22/2015
jgnature of Land Applier Date
See bottom of FSF Form for helpful instructions for this 1VIFLSF Form and the mathematical EbF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington Permit #: WQ0001026 Annual Dry Tons Applied: 17.87
Owner: Will Congleton Operator: Will Congleton Cation Exchange Capacity (non 503):
Site #: PI201 Field #: 10 Acres Utilized: 7.8 Acres Permitted: 7.8
o
Q
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
rte
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
A 11
pp
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
ma-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 Crop
p or p
2
Gal.
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
11/14
104000
13333
4.12
2.2907
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
48.9664
#######
SG
1
0
0.0000
0
0
2
0
0.0000
0
0
1
3
0
0.0000
0
0
4
0
0.0000
1
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
7
0
0.0000
0
0
1
8
0
0.0000
0
0
9
0
0.0000
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
13333
:::::::::::::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0275
0.0092
0.2840
0.9575
0.1649
0.0053
0.0229
0.1283
0.0229
2.7397
69.8664
48.9664
0
Date
lbs/ac
Current Cumulative lbs/ac
0.0275 0.0092 0.2840 0.9575 0.1649 0.0053 0.0229 0.1283 0.0229 2.7397 :::
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
36 34 1338 267 15 374 89 2498 .............................
100 1 50
2000
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties o submitting false information, including the possibility of fines and imprisonment for knowing violations."
wZ. 1/22/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant LoadinS Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this infoiEmation needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
r
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
,-' facility Name: City of Washington Total Dry Tons Applied (Annual):
ermit #: WQ0001026 Cation Exchange Capacity (non 503 only):
Operator:
Icres Used:
17.87
Will Congleton Owner: Will Congleton
9 Acres Permitted: 9 Site #: P1201 Field #: 12
Mesidual
Analysis Data (Heavy
Metals and Total
Phosphorus
use mg/kg,
% Solids
use Raw Percent #):
-Sample
1
_2j
3
4j
5
6
7
8
9
10
11
12
r Com-
Nov
'posite
Avg
Date
o Solids
4.12
Arsenic
6
ladmium
2
r
;hromium
62
Copper
209
Lead
36
r
-Mercury
1.15
Molyb-
5
`ienum
Nickel
28
Selenium
5
j zinc
598
Total
Phos-
15250
chorus
nnnual
Heavy Metal Field Loadings
(Calculated
in lbs/acre):
c
1
L2J
L 3
4 J
L5J
L6j7
L8J
9 J
10
Ill 1
12
`a�
y
o
1.9853
--. xsenic
0.0238
0
0
0
0
0
0
0
0
0
0
0
0.0238
Cadmium
0.0079
0
0
0
0
0
0
0
0
0
0
0
0.0079
wonnum
0.2462
0
0
0
0
0
0
0
0
0
0
0
0.2462
popper
0.8299
0
0
0
0
0
0
0
0
.0
0
0
0.8299
Lead
0.1429
0
0
0
0
0
0 1
0
0
0 1
0
0
0.1429
lercury
0.0046
0
0
0
0
0
0
0
0
0
0
0
0.0046
ivlolyb- I
0.0199
0
0
0
0
0
0
0
0
0
0
0
0.0190
denum
Nickel
0.1112
0
0
0
0
0
0
0
0
0
0
0
0.1112
�,zlenium
0.0199
0
0
0
0
0 1
0
0 1
0
0
0
0
0.0199
--., Zinc
2.3744
0
0
0
0
0
0
0
0
0
0
0
2.3744
'Total
60.552
0
0
0
0
0
0
0
0
0
0
0
60.552
IPhos-
__nhorus
1 ' ` certify, under penalty of law, that this document was prepared under my direction or supervision in
Aecurtla" e WILL U MjV3LG111 UVAlgHWU LU 435U1-C LURSL gU41111CU PUL-JUllllCI Pl-UPCI-ly g2LLllC1-CU 2LIM CV211U2LLCU LUC
1*�formation submitted. I am aware that there are significant penalties for submitting false information,
cluding the possibility of fines and imprisonment for knowing violations"
Z-z 1/22/2015
�gnature of Land Applier Date.
aee bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematica
PtWVM KWTSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington Permit #: WQ0001026 Annual Dry Tons Applied: 17.87
Owner: Will Congleton Operator: Will Congleton Cation Exchange Capacity (non 503):
Site #: PI201 Field #: 12 Acres Utilized: 9 Acres Permitted: 9
o �
oPer
s eci
Totals
Acre
%
Solid
s
Dry Tons Per
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
ma-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
*
�
Gal.
CuNd.
TRe__
poAcre
Totals
n Gal.
Crop 1
Crop 2
11/14
26000
2888.9
4.12
0.4963
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
10.6094
#######
SG
1
11115
78000
8666.7
4.12
1.4890
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
31.8282
#######
SG
2
0
0.0000
0
0
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
7
0
0.0000
0
0
8
0
0.0000
0
0
9
0
0.0000
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
11556
:::::::::::
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.0238
0.0079
0.2462
0.8299
0.1429
0.0046
0.0199
0.1112
0.0199
2.3744
60.5517
42.4376
0
Date
lbs/ac
Current Cumulative lbs/ac
0.0238 0.0079 0.2462 0.8299 1 0.1429 0.0046 1 0.0199 1 0.1112 0.0199 2.3744
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000:::::::::::::::::::::::::::::::::::::::
36 34 1338 267 15 374 1 89 2498 .............................
100 50
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1/22/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

' ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
',acility Name:
ermit #:
Operator:
'cres Used:
City of Washington Total Dry Tons Applied (Annual): 14.52
WQ0001026 Cation Exchange Capacity (non 503 only):
Will Congleton Owner: Will Congleton
6.7 Acres Permitted: 6.7 Site #: . P1201 Field #: 13
`residual Analysis Data (Heavy Metals and Total
Phosphorus
use mg/kg,
% Solids
use Raw Percent #):
Sample
11
2
3
4
5
6
7
8
9
10
11
12
r Corn-
Nov
posite
Avg
-> Date
o Solids
4.12
Arsenic
6
admium
2
hromium
62
Copper
209
Lead
36
Mercury
1.15
_Molyb-
5
denum
- 'Nickel
28
Relenium
5
Zinc
598
LTotal
-" Phos-
15250
chorus
-annual Heavy Metal Field Loadings (Calculated
in lbs/acre):
2
3
4
5
6
7
8
9
10
11
12
y
y
o
2.1668
1
_arsenic
OA26
0
0
0
0
0
0
0
0
0
0
0
0.026
dmium
0.0087
0
0
0
0
0
0
0
0
0
0
0
0.0087
ornium
k
0.2687
0
0
0
0
0
0
0
0
0
0
0
0.2687
opper
0.9057
0
0
0
0
0
0
0
0
0
0
0
0.9057
Lead
0.156
0
0
0
0
0
0
0
0
0
0
0
0.156
4ercury
0.005
0
0
0
0
0
0
0
0
0
0
0
0.005
IMolyb-
0.0217
0
0
0
0
0
0
0
0
0
0
0
0.0217
denum
Nickel
0.1213
0
0
0
0
0
0
0
0
0
0
0
0.1213
selenium
0.0217
0
0
0
0
0
0
0
1 0
0
0
0
1 0.0217
- Zinc
2.5915
0
0
0
0
0
0
0
0
0
0
0
2.5915
Total
66.087
0
0
0
0
0
0
0
0
0
0
0
66.087
IPhos-
nhorus
1 rertifv. under penalty of law, that this document was prepared under
my direction
or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
formation submitted. I am aware that there are significant penalties for submitting false information,
l ieluding the possibilitv of fines and imprisonment for knowing violations"
1/22/2015
Ignature of Land Applier Date
See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematica&l* O L%F (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington Permit #: WQ0001026 Annual Dry Tons Applied: 14.52
Owner: Will Congleton Operator: Will Congleton Cation Exchange Capacity (non 503):
Site #: PI201 Field #: 13 Acres Utilized: 6.7 Acres Permitted: 6.7
o y
Y o
Q
Specify
Totals
Per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
ite
Cond.
Dry,
Wet,
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
ma-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 Crop
p or p
2
Gal.
Cu.Yd.
Report
7: Totals
in Gal.
Crop 1
Crop 2
11/13
26000
3880.6
4.12
0.6667
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
14.2514
#######
SG
1
11/14
58500
8731.3
4.12
1.5001
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
32.0657
#######
SG
2
0
0.0000
0
0
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
1 0
16
0
0.0000
0
0
7
0
0.0000
0
0
8
0
0.0000
0
0
9
0
0.0000
0
0
1
1
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
12612
::::::::
As
Cd
Cr
Cu
Pb
H
Mo
I Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.0260
0.0087
0.2687
1 0.9057
0.1560
0.0050
0.0217
0.1213
0.0217
2.5915
66.0874
46.3171
0
Date
lbs/ac
Current Cumulative lbs/ac
0.0260 0.0087 0.2687 0.9057 0.1560 0.0050 0.0217 0.1213 0.0217 2.5915 ::::
0.0000 1 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
36 34 1338 267 15 374 89 2498
100 50
2000
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.
mit imit 1 st/2nd Crop
Perms PAN Li
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1/22/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
i` Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
:-_`;acility Name:
ermit #:
Operator:
z acres Used:
'icesidual Ana
r Com-
posite
Date
', Solids
Arsenic
Nov
Avg
4.12
6
idmium
aromium
2
C2
Copper
Lead
ivIercury
209
36
1.15
Molyb-
lenum
�Jickel
5
28
Selenium
zinc
5
598
LL Phos- 115250
City of Washington - Total Dry Tons Applied (Annual): 81.52
WQ0001026 Cation Exchange Capacity (non 503 only):
Will Congleton Owner: Will Congleton
36.6 Acres Permitted: 36.6 Site #: P1201 Field #: 14
Data (Heave Metals and Total
.annual Heave Metal Field LoadinLys
l:
use m2/ka, % Solids use Raw Percent #):
c
11
121L3J
4
5
1 71
1819
10
11
12
a�
_6j
y
CD
o
2.2273
_arsenic
0.0267
0
0
0
0
0
0
0
0
0
0
0
0.0267
Cadmium
0.0089
0
0
0
0
0
0
0
0
0
0
0
0.0089
1romi
0.2762
0
0
0
0
0
0
0
0
0
0
0
0.2762
popper
0.931
0
0
0
0
0
0
0
0
0
0
0
0.931
Lead
0.1604
0
0
0
0
0
0
0
0
0
0
0
0.1604
lercury
0.0051
0
0
0
0
0
0
0
0
0
0
0
0.0051
Molyb-
0.0223
0
0
0
0
0
0
0
0
0
0
0
0.0223
lenum
lickel
0.1247
0
0
0
0
0
0
1 0
0
0
0
0
0.1247
�Delenium
0.0223
' 0
0
0
0
0
0
0
0
1 0
0
0
0.0223
Zinc
2.6639
0
0
0
0
0
0
0
0
0
0
0
2.6639
Total
Phos-
67.933
0
0
0
0
0
0
0
0
0
0
0
67.933
'7khor uS
i certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
r ­Iormation submitted. I am aware that there are significant penalties for submitting false information,
fcluding the possibility of fines and imprisonment for knowing violations"
r Z�t 1/22/2015
I gnature of Land Applier Date
(= See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematicak %F (5/2003)

am
ANNUAL LAND APPLICATION FIELD SUMMARYFORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Washington Permit #: WQ0001026 Annual Dry Tons Applied: 81.52
Owner: Will Congleton Operator: Will Congleton Cation Exchange Capacity (non 503):
Site #: PI201 Field #: 14 Acres Utilized: 36.6 Acres Permitted: 36.6
o
o
0
A
Specify:
per
Acre
%
Solid
s
Dry Tons Per
Acre
Residual
Sources
(Summarize)
lte
Cond.
Dry,
Wet
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate **
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
*
21 Gal. .Totals
Cu.Yd.
Report'
Totals
in Gal.
Crop 1
Crop 2
11/11
78000
2131.1
4.12
0.3661
Washington WWTP
Dry
<51
S
0.5
0.3
33700
2880
2
7.8266
#######
SG
1
11/12
240500
6571
4.12
1.1289
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
24.132
#######
SG
2
11/13
156000
4262.3
4.12
0.7323
Washington WWTP
Dry
<.5"
S
0.5
0.3
33700
2880
2
15.6532
#######
SG
3
0
0.0000
0
0
4
0
0.0000
0
0
5
0
0.0000
0
0
6
0
0.0000
0
0
7
0
0.0000
0
0
8
0
0.0000
0
0
9
0
0.0000
0
0
10
0
0.0000
0
0
11
0
0.0000
0
0
12
TOTALS:
12964
:::::::::::::::
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime A
lied
Annuallbs/acre
0.0267
0.0089
0.2762
0.9310
0.1604
0.0051
0.0223
0.1247
0.0223
2.6639
67.9327
47.6118
0
Date
lbs/ac
Current Cumulative lbs/ac
0.0267 0.0089 0.2762 0.9310 0.1604 0.0051 0.0223 0.1247 0.0223 2.6639 ::
0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
36 34 1338 267 15 374 89 2498
100 so
2000
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
P ermit PA N Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z�f4;2 - 1/22/2015 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

Page: 1 of 2
Report Number: 14-164-0203
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: -EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 55900
Sample, Id: WASHINGTON WWTP
ARL
wwwaleastem.com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road, Richmond, Virginia 23237 (804) 7434)401 Fax (804) 271-G446
Project: WASHINGTON NC
NC CERT # 257
REPORT OF ANALYSIS
Total Solids *
4.70
47000
100.0
JM
Moisture *
95.30
100.0
JM
Total Kjeldahl Nitrogen
3.36
33600
10.0
JM
Total Phosphorus
1.70
17000
100
KM
Total Potassium
0.23
2300
100
KM
Total Sulfur
0.58
5820
100
KM
Total Calcium
1.47
14700
100
KM
Total Magnesium
0.28
2750
100
KM
Total Sodium
0.17
1700
100
KM
Total Iron
111000
100
KM
Total Aluminum
31300
100
KM
Total Manganese
852
5
KM
Total Copper
199
5
KM
Total Zinc
541
5
KM
Ammonia Nitrogen
0.77
7660
10.0
JM
Organic N
2.59
25940
10.0
Nitrate+Nitrite-N
160
2.00
JM
Total Cadmium
3.0
2.0
KM
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Date Sampled: 6/12/2014 09:30:00
Date Received: 06/13/2014 00:00
Date Reported: 06/19/2014
06/13/2014 14:44
06/13/2014 14:44
06/16/2014 09:04
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 14:53
06/16/2014 09:04
06/16/2014 09:04
06/16/2014 09:05
06/16/2014 14:53
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM4500-NH3C
CALCULATION
SM-450ONO3F
SW 6010C

L _ _J
Page: 2 of 2
Report Number: 14-164-0203
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: 'EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 55900
Sample'ld : WASHINGTON WWTP
s
www.aleastern.com
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: WASHINGTON NC
NC CERT # 257
REPORT OF ANALYSIS
Date Sampled: 6/12/2014 09:30:00
Date Received: 06/13/2014 00:00
Date Reported: 06/19/2014
Total Chromium
56
5
KM
06/16/2014 14:53
SW 6010C
Total Nickel
30
5
KM
06/16/2014 14:53
SW 6010C
Total Lead
37
5
KM
06/16/2014 14:53
SW 6010C
Total Arsenic
6.0
3.0
KM
06/16/2014 14:53
SW 6010C
Total Mercury
0.8
0.4
KM
06/16/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
06/16/2014 14:53
SW 6010C
pH (Standard Units) * 7.35
2.00
JM
06/16/2014 09:00
SW-9045D
Total Volatile Solids 42.59
425900
100.0
JM
06/13/2014 14:44
SM-2540G
Total Molybdenum
5
5
KM
06/16/2014 14:53
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NO3/NO2-N".THE
MATRIX SPIKE WAS OUT OF
LIMITS FOR "Cr" AND "Ni". ALL OTHER QC DATA IS
ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

WL
BI( SOLIDS SAi1rr "r'rT3AXrlAXTT`T"AiPC)RM/rt'I--fAT-N Off' C'UST�
Al A�
,fin 7621 Whitepine ��innf �'� 48246A-o3o9 Ir1Gsi, I�ICfab�-ea�;tert,.��xT;
EMA RESOURCES WC Qs-13-207a
WASHINGTON WWTp 12:14:52
Subrrtitteci E3,Cop
y To
ENIA Resources Inc EMA Resources hic
755 Yadkinville Rd 755 Yadkinville Rd
Mocksville, NC 27028 Mocksville, NC 27028
Project q
N
Sample Information
Lab Number Collection Irtformatfon Container Information Please Check Desired %sts
Swrtpta !D (Lab use
se
Type VdUrr 5Lt 5!? 803 Nitrogen Volatile
On(y) Type bate TIM ogert
(](� ofBotties Metals Series pN Solids Qthers
��lv _Grab ) oz
- __zComposite ���� 9 L 36l� i [ass
iGrab.
-- oz
_ Composite
„Glass
Plastic
---pinl
t
— Grab
Glass
— ox
Composite
_
Plastic
--pint
t
Grab
Glass
I
—, 0z
Composite
_
_ Plastic
---Vint
Test Package Details -
.1, total -Solids (Moistare) Total KjOdahi Nitrogen. Phosphorus and Potassium
,2: 13asic lest SLl Phts Sulriu. Calcium, Iron, Aluminum, Manganese. Copper And Zinc
3 Metals, Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in 51-2)
trrxgcn Series: Total Kjeldahl, Ammonium, N-itraty & Organic Nitrogen.
Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
instructio is or Remarks

Page: 1 of 2
Report Number: 14-171-0200
Account Number: 46245
Submitted By: BRENT COLLINS
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 56030
Sample Id: WASHINGTON
AFL
Wwrwaleastemcom
A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 2323T [phone]. Fax [phone]
Project: WASHINGTON
NC CERT#257
REPORT OF ANALYSIS
Total Solids *
4.43
44300
100.0
JM
Moisture *
95.57
100.0
JM
Total Kjeldahl Nitrogen
3.59
35900
10.0
JM
Total Phosphorus
1.82
18200
100
KM
Total Potassium
0.28
2790
100
KM
Total Sulfur
0.63
6300
100
KM
Total Calcium
1.49
14900
100
KM
Total Magnesium
0.29
2880
100
KM
Total Sodium
0.16
1620
100
KM
Total Iron
117000
100
KM
Total Aluminum
42300
100
KM
Total Manganese
892
5
KM
Total Copper
208
5
KM
Total Zinc
579
5
KM
Ammonia Nitrogen
0.79
7900
10.0
JM
Organic N
2.80
28000
10.0
Nitrate+Nitrite-N
31.6
2.00
JM
Total Cadmium
2.0
2.0
KM
All values are on a dry weight basis except as ngte�d by asterisk. Detection limit on all N series is on a wet basis.
Date Sampled: 6/18/2014 09:00:00
Date Received: 06/20/2014 00:00
Date Reported: 06/26/2014
06/20/2014 13:34
06/20/2014 13:34
06/23/2014 08:50
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 08:50
06/23/2014 08:50
06/23/2014 08:40
06/23/2014 10:20
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SM-2540G
SM-2540G
SM-4500-NH3C-TKN
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SM-4500-NH3C
CALCULATION
SM-450ONO3F
SW 601 OC

Page: 2 of 2
Report Number: 14-171-0200
Account Number: 46245
Submitted By: BRENT COLLINS wwwaleastern.com
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 56030
Sample Id: WASHINGTON
A&L Eastern Laboratories, Inc.
ism
7621 Whitepihe Road Richmohd, Virginia 23237 [phone] Fax [phone]
Project: WASHINGTON
NC CERT#257
REPORT OF ANALYSIS
Total Chromium 55
5
KM
Total Nickel 28
5
KM
Total Lead 31
5
KM
Total Arsenic 6.0
3.0
KM
Total Mercury 1.0
0.4
KM
Total Selenium <5.0
5.0
KM
pH (Standard Units) * 7.30
2.00
JM
Total Volatile Solids 42.26 422600
100.0
JM
Total Molybdenum 6
5
KM
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE.
Date Sampled: 6/18/2014 09:00:00
Date Received: 06/20/2014 00:00
Date Reported: 06/26/2014
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/23/2014 10:20
06/24/2014 12:00
06/23/2014 10:20
06/23/2014 08:50
06/20/2014 13:34
06/23/2014 10:20
All values are on a dry weight basis'except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SW 6010C
SW 6010C
SW 6010C
SW 6010C
SW-7471 B
SW 6010C
SW-9045D
SM-2540G
SW 6010C

F� rvn" wq
" wi 01 d
ItIt IIII I{I{ ��II IIll II ��IIII
.. ~ s' II !l1 IN � I II.NIJ 46245 Q
A&L Easteni
EMA RESOURCES INC 11.48:1 1
7021 Whitepine (toad Richmond VA 2.3,237 Tel: 804• WASHMTON
EMA Resources Inc EMA .Resources Inc
755 Yadkinville Rd 755 YadkinvilIe Rd
Mocksville, NC 27028 Mocksville. NC 27028
Project Iai
Lab (Number
Collection
Information
SwIf e.li7
(Lab Use
Only)
Type
bate
T'me
w
t«S�
`
vComposite
_ _
_ Grab
Composite
Grab
Composite
— Grab
_ Composite
Sample Informat on
Container Information
Number
5f Bottles
type
volume
Glass
— 0z
✓'Mastic
int
�t
Glass
— oz
_
Plastic
qt
Glass
— oz
_
Plastic
---pint
qI
Glass
— oz
Plastic 1:—pint
at
Please rAeck Desired Tests
51-1 SL2 503 Nitrogen PH WE Ag CI votatlle
Metals Seim Solids Ctehers
Reltaquishea 8 St nature
Date
Time
Received By (Si mature)
Date
Time
t31S0
Test Package Details S ectal Instructions or Remarks
SLl : l otal Solids (Mmsture) Toral Kjeldahl Nitrogen, Pltobpljorus and Potassium
SL2: B35w Tess SLI plus 5u11111r. C'alciurn, MAgnesium,Sodiun). Iron. Aluminum_ Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Mckcel, Selenium.
(Capper & Zinc included in SL2)
Nitrogen Series: "l'otal K eldatrl. Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)

Page: 1 of 2
Report Number: 14-318-0213
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 58728
Sample Id: WASHINGTON NC WWTP
A&L Eastern Laboratories, Inc.
7d21.Whitepine Road Richmond, Virginia 23237' '(804) 743-94U Fax (804) 271-WS
wwwaleastern.com
Project: WASHINGTON NC
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 11/11/2014 17:00:00
Date Received: 11/14/2014 00:00
Date Reported: 11/20/2014
Total Solids *
4.13
41300
100.0
BW
11/14/2014 14:10
SM-2540G
Moisture"
95.87
100.0
BW
11/14/201414:10
SM-2540G
Total Kjeldahl Nitrogen
3.37
33700
10.0
JM
11/17/2014 08:55
SM-4500-NH3C-TKN
Total Phosphorus
1.52
15200
100
KM
11/18/2014 12:19
SW 6010C
Total Potassium
0.22
2190
100
KM
11/18/2014 12:19
SW 6010C
Total Sulfur
0.50
4980
100
KM
11/18/2014 12:19
SW 6010C
Total Calcium
1.28
12800
100
KM
11/18/2014 12:19
SW 6010C
Total Magnesium
0.23
2310
100
KM.
11/18/2014 12:19
SW 6010C
Total Sodium
0.17
1710
100
KM
11/18/2014 12:19
SW 6010C
Total Iron
96000
100
KM
11/18/2014 12:19
SW 6010C
Total Aluminum
39000
100
KM
11/18/2014 12:19
SW 6010C
Total Manganese
854
5
KM
11/18/2014 12:19
SW 6010C
Total Copper
207
5
KM
11/18/2014 12:19
SW 6010C
Total Zinc
593
5
KM
11/18/2014 12:19
SW 6010C
Ammonia Nitrogen
0.65
6540
10.0
JM
11/17/2014 08:55
SM-4500-NI3C
Organic N
2.72
27160
10.0
11/17/2014 08:55
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
11/17/2014 08:50
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
11/18/2014 12:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk.
Detection limit on all N series
is on a wet basis.
9�/w
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-318-0213
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 58728
Sample Id: WASHINGTON NC WWTP
99LJ A&L Eastern Laboratories, Inc.
7621.Whitepine Road Richmond, Virginia'23237 [phone] Fax [phone]
wwwaleastem.op. m
Project: WASHINGTON- NC
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 11/11/2014 17:00:00
Date Received: 11/14/2014 00:00
Date Reported: 11/20/2014
Total Chromium
53
5
KM
11/18/2014 12:19
SW 6010C
Total Nickel
26
5
KM
11/18/2014 12:19
SW 6010C
Total Lead
36
5
KM
11/18/2014 12:19
SW 6010C
Total Arsenic
6.0
3.0
KM
11/18/2014 12:19
SW 6010C
Total Mercury
1.1
0.4
KM
11/18/201409:00
SW-7471B
Total Selenium
<5.0
5.0
KM
11/18/2014 12:19
SW 6010C
pH (Standard Units)"
7.21
2.00
JM
11/17/2014 08:55
SW-9045D
Total Volatile Solids
41.50 415000
100.0
BW
11/14/2014 14:10
SM-2540G
Total Molybdenum
5
5
KM
11/18/2014 12:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N" AND "Ca".
ALL OTHER
QC DATA IS ACCEPTABLE.
All values are on a dry weight. basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

BI0SOLI DS SAMPLE TR.1NNSMITT/
nto A&L Eastern
7621 Whitepine (toad Richmond VA 23237 TO: 8(9-
lot11111111111111 I111111111111111111IN1111111111111 � 4-0;4
EW RESOURCES INC 13:08:72
WASHINGTON NC
AccoUnt ..
Customer Infcrmatic
Submitted By By
Ch uge To
Copy To
EMA Resources Inc
EMA Resources Inc
755 Yadkinville Rd 755 Yadkinville Rd
Mocksville, NC 27028 Moeksvilie, NC 27028
ectj
Sample information
Lab Number
Collection Information
container Informabon
Please check Desired Tests
Zple ll)
(Lab Use
Only)
Type
lute
Tere
Number
of 0otttes
Type
Volume
SLY
SL2
50:3
Metals
Nitwgen
Series
pH
CCE
Ag
Cl
Volattia
Sofi�ts
Utriers
Grab
Plastic
oz
t
�'
—Composite
Grab
_ Glass
O2
— Composite
Plastic
_Pint
t
Grab
Glass
flz
Composite
Plastic
--ant
I at
Grab
Glass
— oz
Composite
_
Plastic
Dint
I at
, ell ui ed By-, W&Lature}
Data,
Tune
FO-.wjved AY- (S. r+ature)
Date
Tune
r �p
a OeAx
�30
Test Package Details
Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorv't and Patawium
Basic Test SLl Plus Sniinr, Calcium, M28nesimn.5adiIIM. VM Alitminum. ManganesC. Copper And :Lint
lAetals; Arsenic, Cadmium, Chromium, Metcury, Molybdenum, Lead, Nickel, Selenium.
(.Copper & Zinc included in SL2)
rgen Series: Total Kjeldahl, Ammonium, "Nitrate & Organic Nitrtgen.
Calcium Carbonate Equivalent or Total neuValiz-ation Value (For Lime Treated Sludge)
SDecial I

Page: 1 of 2
Report Number: 14-318-0214
Account Number: 46245
Submitted By: ROY WHITAKER
Send To EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
L
www.aleastem.com
A&L Eastern Laboratories, Inc.
7921 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Project: WASHINGTON NC (2)
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 11/13/2014 10:00:00
Lab Number: 58729 Date Received: 11/14/2014 00:00
Sample Id: WASHINGTON NC WWTP (2) Date Reported: 11/20/2014
Total Solids *
4.10
41000
100.0
BW
11/14/2014 14:10
SM-254OG
Moisture *
95.90
100.0
BW
11/14/2014 14:10
SM-254OG
Total Kjeldahl Nitrogen
3.37
33700
10.0
JM
11/18/2014 08:55
SM-4500-NH3C-TKN
Total Phosphorus,
1.53
15300
100
KM
11/18/2014 12:19
SW 6010C
Total Potassium
0.21
2050
100
KM
11/18/2014 12:19
SW 6010C
Total Sulfur
0.49
4920
100
KM
11/18/2014 12:19
SW 6010C
Total Calcium
1.26
12600
100
KM
11/18/2014 12:19
SW 6010C
Total Magnesium
0.22
2240
100
KM
11/1.8/2014 12:19
SW 6010C
Total Sodium
0.16
1630
100
KM
11/18/2014 12:19
SW 6010C
Total Iron
98200
100
KM
11/18/2014 12:19
SW 6010C
Total Aluminum
35700
100
KM
11/18/2014 12:19
SW 6010C
Total Manganese
862
5
KM
11/18/2014 12:19
SW 6010C
Total Copper
210
5
KM
11/18/2014 12:19
SW 6010C
Total Zinc
603
5
KM
11/18/2014 12:19
SW 6010C
Ammonia Nitrogen
0.51
5120
10.0
JM
11/17/2014 08:55
SM-4500-NH3C
Organic N
2.86
28580
10.0
11/17/2014 08:55
CALCULATION
Nitrate+Nitrite-N
<2.00
2.00
JM
11/17/2014 08:50
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
11/18/2014 12:19
SW 6010C
All values are on a dry weight basis except as noted by asterisk.
Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

Page: 2 of 2
Report Number: 14-318-0214
Account Number: 46245
Submitted By: ROY WHITAKER
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE , NC 27028
Lab Number: 58729
Sample Id: WASHINGTON NC WWTP (2)
s
www aleastem.com
A&L Eastern Laboratories, Inc.
A21 Whitepine Road Richmond, Virginia 23237 [phone] ' Fax [phone]
Project: WASHINGTON NC (2)
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 11/13/2014 10:00:00
Date Received: 11/14/2014 00:00
Date Reported: 11/20/2014
Total Chromium
62
5
KM
11/18/2014 12:19
SW 6010C
Total Nickel
30
5
KM
11/18/2014 12:19
SW 6010C
Total Lead
36
5
KM
11/18/2014 12:19
SW 6010C
Total Arsenic
6.0
3.0
KM
11/18/2014 12:19
SW 6010C
Total Mercury
1.2
0.4
KM
11/18/201409:00
SW-7471B
Total Selenium
<5.0
5.0
KM
11/18/2014 12:19
SW 6010C
pH (Standard Units)"
7.21
2.00
JM
11/17/2014 08:55
SW-9045D
Total Volatile Solids
41.03 410300
100.0
BW
11/14/2014 14:10
SM-2540G
Total Molybdenum
5
5
KM
11/18/2014 12:19
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "NO3/NO2-N"
AND "Ca". ALL OTHER
QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

BIOSO.LIDS SA:WLE TR.ANSNUTTAL FORIvUt..HA rnI n
4-5
7621 Whitepino Road Richmond VA 23237 Tel: 804- 11�,il;,01a
Account
..
_.
twit fiilV Wff rw....--- __
Customer lnforrndtlo rwRFsauRcesit c
a.......—._
WASNIW-TON NC 121
Submitted By
10
EMA
Resources Inc
EMA Resources Inc
755 Yadkinville Rd
755 Yadkinville Rd
Miacksville, NC 27028
Macksville, NC 27028
Sample Information
Lett Number
Caliedior•1 Information
Container Information
Please Check Desired 'Tests r
1ple U
(Lab Use
Only)
Type
Date
itrte
Num6Wr
Type
Volume
SO
SL2 -
5W
dhtrwen
pH
GCE
Ag
C
Volatile
Others
of Bott'1es
wetals
aeries
Solids
iEC.+G�
4i
"Grab
f
J`
`GOz
_
p��s
� t
Composite
jl
1D:DOA
Grab
Glass
oz
Composite
Plastic
__Putt
t
Grab
Glass
oz
_ Composite
Plastic
—pint
Grab
_ Glass
— oz
Composite
_ Plastic
---Pint
®r
ffffA
Test Package Details
Total Solids (Moisture) Twal Kieldshl Nitrogen; Phosphorus and Potassium
Basic Test SLI plus Sul fur, Uciun. tr1Wes4urt,Sodium, Iron. Aluminum, Wriganese, Copper And Zinc
Metals. Arsenic, Cadmium, Chromium, Mercury, Moipbdenum, Lead, Nickel, Selenium
(Copper & Zinc included in SL2)
agen Series: Total i jeldahl, Ammonium, Nitrate &- Organic Nitrogen.
Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
0r

i
i
OESC
L•A-B S•C•t•E-N-C•E•S
i
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Report Summary:
Friday June 20;. 2014
Report Number-:.L7,04279.
Samples Received: 06/12J 14
Client Project:
Description: Washington NC
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
The analytical results in this report are based upon information supplied
by you, the client, and are for your exclusive use. If you have any
questions regarding this data package, please do not hesitate to call.
Entire Report Reviewed By:
Terrie Fudg2/1 ESC presentative
Laboratory Certifca tion Numbers
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197,
FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016,
NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002,
SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612,
MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1,
TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02
Accreditation is only applicable to the test methods specified on each scope of accreditation held
by ESC Lab Sciences.
This report may not be reproduced, except in full, without written approval from ESC Lab Sciences.
Where applicable, sampling conducted by ESC is performed per guidance provided
in laboratory standard operating procedures: 060302, 060303, and 060304.
Page 1 of 3

I� '1
i k
JOESC
L•A-8 5•0•1-M,N,C•E,S
i
REPORT OF ANALYSIS
Mr. Brent Collins
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
Date Received June 12, 2014
Description Washington NC
Sample ID WASHINGTON WWTP
Collected By Roy Whitaker
Collection Date 06/10/14 13:30
12065 Lebanon Rd.
Mt. Juliet, TN 37122
[phone]
1-800-767-5859
Fax [phone]
Tax I.D. 62-0814289
Est. 1970
June 20,2014
ESC Sample # L704279-01
Site ID
Project
Parameter
Result Det. Limit
Units
Limit
Method
Date/Time By
Dil
Corrosivity
Non-Corrosiv
9045D
06/14/14
0906 SDC
1
Ignitability
See Footnote
Deg. F
D93/101
06/18/14
1400 DR
1
Reactive CN (SW846 7.3.3.2)
BDL
0.125
mg/kg
9012B
06/16/14
1417 ASK
1
Reactive Sulf.(SW846 7.3.4.1)
BDL
25.
mg/kg
9034/90
06/16/14
1431 DJD
1
TCLP Extraction
-
1311
06/16/14
1408 LJN
1
Mercury
BDL
0.010
mg/l
0.20
7470A
06/18/14
1015 BRJ
1
Arsenic
BDL
0.45
mg/l
5.0
6010C
06/18/14
1054 JDG
1
Barium
BDL
1.4
mg/l
100
6010C
06/18/14
1054 JDG
1
Cadmium
BDL
0.45
mg/l
1.0
6010C
06/18/14
1054 JDG
1
Chromium
BDL
0.45
mg/l
5.0
6010C
06/18/14
1054 JDG
1
Lead
BDL
0.45
mg/l
5.0
6010C
06/18/14
1054 JDG
1
Selenium
BDL
0.45
mg/l
1.0
6010C
06/18/14
1054 JDG
1
Silver
BDL
0.45
mg/l
5.0
6010C
06/18/14
1054 JDG
1
TCLP ZHE Extraction
-
1311
06/15/14
1439 LJN
1
TCLP Volatiles
Benzene
BDL
Carbon tetrachloride
BDL
Chlorobenzene
BDL
Chloroform
BDL
1,2-Dichloroethane
BDL
1,1-Dichloroethene
BDL
2-Butanone (MEK)
BDL
Tetrachloroethene
BDL
Trichloroethene
BDL
Vinyl chloride
BDL
Surrogate Recovery
Toluene-d8
102.
Dibromofluoromethane
98.0
a,a,a-Trifluorotoluene
102.
4-Bromofluorobenzene
97.0
TCLP Pesticides
Chlordane
BDL
Endrin
BDL
Heptachlor
BDL
L704279-01 (IGNITABILITY)
- did not ignite @ 170
0.050
mg/l
0.50
8260B
06/16/14
1602
JC 1
0.050
mg/l
0.50
8260B
06/16/14
1602
JC 1
0.050
mg/l
100
8260B
06/16/14
1602
JC 1
0.25
mg/1
6.0
8260B
06/16/14
1602
JC 1
0.050
mg/1
0.50
8260B
06/16/14
1602
JC 1
0.050
mg/1
0.70
8260B
06/16/14
1602
JC 1
0.50
mg/1
200
8260B
06/16/14
1602
JC 1
0.050
mg/1
0.70
8260B
06/16/14
3.602
JC 1
0.050
mg/1
0.50
8260B
06/16/14
1602
JC 1
0.050
mg/1
0.20
8260B
06/16/14
1602
JC 1
% Rec.
114.
8260B
06/16/14
1602
JC 1
% Rec.
125.
8260B
06/16/14
1602
JC 1
% Rec.
114.
8260B
06/16/14
1602
JC 1
6 Rec.
128.
8260B
06/16/14
1602
JC 1
0.0050
mg/1
0.030
8081A
06/19/14
1027
CBB 1
0.0050
mg/1
0.020
8081A
06/19/14
1027
CBB 1
0.0050
mg/l
0.0080
8081A
06/19/14
1027
CBB 1
Page 2 of 3

1
12065 Lebanon Rd.
Mt. Juliet, TN 37122
1 OESC [phone]
1-800-767-5859
Fax [phone]
L•A-B S•C-I•E•M-C•E•5
Tax I.D. 62-0814289
i
Y Est. 1970
REPORT OF ANALYSIS
- Mr. Brent Collins June 20,2014
EMA Resources
755 Yadkinville Road
Mocksville, NC 27028
ESC Sample # L704279-01
Date Received June 12, 2014
Description Washington NC
- Site ID
Sample ID WASHINGTON WWTP
Project
Collected By Roy Whitaker
Collection Date 06/10/14 13:30
Parameter Result Det. Limit Units Limit Method Date/Time By Dil
Lindane BDL 0.0050 mg/l 0.40 8081A 06/19/14 1027 CBB 1
Methoxychlor BDL 0.0050 mg/1 10. 8081A 06/19/14 1027 CBB 1
Toxaphene BDL 0.010 mg/l 0.50 8081A 06/19/14 1027 CBE 1
Surrogate Recovery
Decachlorobiphenyl 101. t Rec. 123. 8081A 06/19/14 1027 CBB 1
Tetrachl'oro-m-xylene 83.6 16 Rec. 114. 8081A 06/19/14 1027 CBB 1
TCLP Herbicides
2,4,5-TP (Silvex) BDL 0.0020 mg/l 1.0 8151A 06/19/14 2154 KLM-1
2,4-D BDL 0.0020 mg/l 10. 6151A 06/19/14 2154 KLM 1
Surrogate Recovery
2,4-Dichlorophenyl Acetic Acid 65.4 °s Rec. 8151A 06/19/14 2154 KLM 1
TCLP Semi-Volatiles
1,4-Dichlorobenzene BDL 0.10 mg/l 7.5 8270D 06/18/14 0757 ADF 1
2,4-Dinitrotoluene BDL 0.10 mg/l 0.13 8270D 06/18/14 0757 ADF 1
Hexachlorobenzene BDL 0.10 mg/l 0.13 8270D 06/18/14 0757 ADF 1
Hexachloro-1,3-butadiene BDL 0.10 mg/l 0.50 8270D 06/18/14 0757 ADF 1
Hexachloroethane BDL 0.10 mg/l 3.0 8270D 06/18/14 0757 ADF 1
Nitrobenzene BDL 0.10 mg/l 2.0 8270D 06/18/14 0757 ADF 1
Pyridine BDL 0.10 mg/l 5.0 8270D 06/18/14 0757 ADF 1
3&4-Methyl Phenol BDL 0.10 mg/l 400 8270D 06/18/14 0757 ADF 1
2-Methylphenol BDL 0.10 mg/l 200 8270D 06/18/14 0757 ADF 1
Pentachlorophenol BDL 0.10 mg/l 100 8270D 06/18/14 0757 ADF 1
2,4,5-Trichlorophenol BDL 0.10 mg/l 400 8270D 06/18/14 0757 ADF 1
2,4,6-Trichlorophenol BDL 0.10 mg/l 2.0 8270D 06/18/14 0757 ADF 1
Surrogate Recovery
- 2-Fluorophenol 41.9 o Rec. 87.0 8270D 06/18/14 0757 ADF 1
Phenol-d5 28.8 o Rec. 67.0 8270D 06/18/14 0757 ADF 1
Nitrobenzene-d5 46.1 o Rec. 120. 8270D 06/18/14 0757 ADF 1
2-Fluorobiphenyl 57.3 °s Rec. 122. 8270D 06/18/14 0757 ADF 1
2,4,6-Tribromophenol 65.7 o Rec. 148. 8270D 06/18/14 0757 ADF 1
p-Terphenyl-dl4 64.1 o Rec. 149. 8270D 06/18/14 0757 ADF 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Limit - Maximum Contaminant Level as established by the US EPA
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Reported: 06/20/14 09:53 Printed: 06/20/14 10:38
L704279-01 (IGNITABILITY) - did not ignite ® 170
Page 3 of 3
I

1
`fSIS
ier f i""
ative
➢t9�Y _
NA Resources Mr. Srd it Calling
755 Yadkinville Road
A",
55 Yadkinville Rind Mocksville, NC 27028
M,
.
e rartt{r:ai6Tff:brcmt.�okiing0$niat�tar�irktatcic�
`c
BGG Coillnsphone,
y�
Y
z�
-
i��r}t�R,aSrna�Sa
,�u. h
f" �#� .'y5y3§
Nils
$Ara
s��
s,
Ph�na; 15.7 , 5$5 ,.
e'
Oo-ns��is�sae5;
4
rejtLltYtate
�€�SGritloFa: �_u
..���
S
a
A t
''
}�
N
,*,A -:
i �1
.t
r r v
Y ilk "' ` 'x
'2�Jr
lii�+t �rjt :# tab l�rbjCt
hone:336-VU �?l1''
�
r0062
� ��s
���
��f
� ' �t��
��
.j t gl .+f y0�pg+y-
ax: 3SA'/ Y �•S B6
NO
:cll ed prrn.ti. Slte/FecilitY IE31i PiMF��
*
ski,
,a9leot 4. Is` red t? lid, d[i,
i%r�ffiFtr �tabt�iJST�elotettd)
«sj,Pr
"ri
,ON
ry gqryry00tt
_ 5arroe Day ...............INS
_ N�.xtCaay...... ....... ..............70g4G Ennait?—No X Yes
m _T�+rvo Day .�..,....«.,.,,..... .,...... 5t193 V Pkd�_-
Fa�CRetl ort ! hl Y _ Three Day_ ...•.............. _._. 2 FAX
�.�'
".��
°
�
4
hp ri'
"��
..
s
'.�
:>r=
� � ?, W
*
Data
Tarne
ntrs
hernrisngat!nlna�t
.$a�crpleq�da'faw�ly}
Sample ID
P
Dom, /13rab
�
Matrix
Oe ,th
�
Y
�
���
���
�!,���,
,Si'�'�.�rt
�Ykl
TCLP
iu`s
12
_
,✓ '
�;��'
rj . .b'.�
�A}��
ate„ �r
s ,� ��a$$^y''��uu�y� ' "�i"
IN
" Matrix: SS • Srrountdwater ;DW - DrinkingWater OT - Other
Ipa.t$t:,;pH T,e.�P
7
'
Flow Other
�
t w ,.a �• ,rx�.> , x..;,
--lt�elverd
ftelinqu SI ature
Date:
Tinge:
b :� Sl ngure
Samples retumed via: 0 OYaS
ffFedEx 0 Courier
Y4y ItlN�iW : ..r,* 1 q���". �.
to y r
���,, y��6 �� J.
- : .:'
&fat'
ma:a
Aecelued :ISi B
_ �4.
f�'� �', �, `y�++� � � ��f'`('k�5 ,�� r��
��„�T!��� t� i"�"y A1��, �
y' P✓�' f7 Jtq� �� - ''�K{
Relinquished by t jai "� '� ' �.,
Date:
Time:
��ti' ���- # �� �a � s��a ��
�3 :, Yx � ��if N, ���m�. Q� � �
�'�IS" �?�'q�,"�
`�
�n�
,,�
� d47 -y
M"'�+ti

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: City of Washington Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 6/8/2014 To 6/8/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
......
Alternative 4❑
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed. (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophihc ❑
Beta
B Ray ❑
Y
Gamma Ra Y
Pasteurization ❑
Class B:
Alternative 10
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobicestion❑ Di
g
�or �Class�
If applicable to alternative performed (Class
B complete the following monitoring pp ble p ( )g g data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number o
Excee-
dences
requency
of
Analysis
Sample
Type
Analytical
Tech-ni ue
q
Minim -urn
Geo_ Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power WN per
gram of total
solids or 2 x 10 to
the 6th power
CFU per ram of
4,918
5,137
5,571
MPN/g
0
QuarterlyG
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4
grams total solid
wei t
Vector Attraction Redaction (40 CFR 503.33) -Please indicate option performed:
Option 1 p Option. 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 ❑Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
P
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 And the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
_ "This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
Signature of Preparer Date
Brent Collins - Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
Z�f 1/22/2015
Signature of Land Applier (if applicable)
Date
DENR FORM RF (5/2003)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: City of Washington Permit Number:
WWTP Name: Washington WWTP NPDES Number:
Monitoring Period: From 7/5/2014 To 7/5/2014
WQ0001026
NCO020648
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
......................
Alternative 4❑
Alternative 5 ❑
Alternative 6 ❑
.............
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray
Gamma Ray
Pasteurization ❑
Class B:
Alternative 10
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B onI ) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
D Anaerobic r estr on❑
o
If ap licable to alternative performed (Class A or Class B) complete the following monito ing data:
Parameter
Allowable Level
in Sludge
g
- Pathogen Density
Number o
Excee-
es
Frequency
of
AnalysisType
Sample
Analytical
Tech-ni ue
9
'nimu
Geo: Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power NMNper
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
5,863
5,969
6,536
MPN/g
0
Quarterly
G
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 Q Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
- system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
Signature of Preparer
I�
Brent Collins - Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
2 -s--� ZGtz 4� 1/22/2015
Date Signature of Land Applier (if applicable)
Date
DENR FORM RF (5/2003)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Ll
t
Facility Name: City of Washington Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 11/4/2014 To 11/4/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 E3.
Alternative 2 ❑
Alternative 3 ❑
............
Alternative 40
Alternative 5 ❑
Alternative 6 ❑
.............
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta a Ra Y
Gamma Ra Y ❑
Pasteu ' rizatio n ❑
Class B:
f Alternative 1 R1
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative erformed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAerobic Digestion ❑
Anaerobic D' e 'stton❑ i
g
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
� Pathogen Density
g
Number o
Excee-
dences
requency
of
Analysis
Sample
T e
Analytical
Tech-nique
ininm
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power WNper
gram of total
solids or 2 x 10 to
the 6th power
CFU per gram of
3056
6753
31161
MPN/g
0
Quarterly
G
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ✓❑ 10ption 2 01 Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ 10ption 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were p
erformed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
- this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
j used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
-' Preparer Name and Title (type or print)
Signature of Preparer
Brent Collins - Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
_s Z�fz 41�-� 1/22/2015
Date Signature of Land Applier (if applicable)
Date
�I
DENR FORM RF (5/2003)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: City of Washington Permit Number: WQ0001026
WWTP Name: Washington WWTP NPDES Number: NCO020648
Monitoring Period: From 11/12/2014 To 11/12/2014
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 40
r Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
BetaRay
Y
Gamma a
R ❑
Y
Pasteurization
Class B:
Alternative 10
Alternative 2 ❑
Alternative 3 ❑
..............
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic esti er on❑ Di
g
..................................................................................................................
If applicable to alternative performed
(Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number ot
Excee-
dences
FrequencySample
of
Anal sis
Type
Analytical
Tech-ni ue
q
inimu
Geo_ Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power NTNper
gram of total
solids or 2 x 10 to
the 6th power
CFU er aram of
4,444
4,568
4,938
MPN/g
0
Quarterly
G
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 WN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 Rr❑ Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction
were options performed ❑
p
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Adam Waters - Water Resources Superintendent
Preparer Name and Title (type or print)
Signature of Preparer
Date
Brent Collins - Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
z�f 1/22/2015
Signature of Land Applier (if applicable)
Date
DENR FORM RF (5/2003)

January 2014 Average AVG.
R.S. 1 & 2 R.S. 3 R.S. 4
78.86% 77.81% 75.86% 77.51%
February 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
77.75 % 78.10% 78.00% 77.95%
1 March 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
78.86% 77.67% 79.52% 78.68%
April 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
t 77.14% 75.86% 78.76% 77.25%
May 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
77.86% 1 75.00% 74.71% 75.86%
June 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
76.24% 74.70% 76.52% 75.82%
July 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
71.82% 71.73% 71.45% 71.67%
August 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
71.38% 69.95% 68.67% 70.00%
September 2014 Average
R.S. 1 & 2 R.S. 3 R.S. 4
71.43% 71.19% 69.43% 70.68%
I
October 2014 Average
� R.S. 1 & 2 R.S. 3 R.S. 4
71.87% 71.87% 68.70% 70.81%
November 2014 Average
FI
S. 1 & 2 R.S. 3 R.S. 4
3.41% 74.00% 71.35% 72.92%
December 2014 Average 2014 AVERAGE 74.51%
R.S. 1 & 2 R.S. 3 R.S. 4
J 75.48% 76.52% 73.00% 75.00%

' VS in
0.7451
VS out
0.4259
VSFR=
0.75
VS in
0.7451
VS out
0.4226
VSFR=
0.75
VS in
0.7451
VS out
0.415
VSFR=
0.76
VS in
0.7451
VS out
0.4103
VSFR=
0.76

J
Summary Sheet
Fe'cat Collfdrm-4.,
Pathop.n Reductio'n,
Date
J
Location #
MPN/g
Log
3,-:459
51 tt- 3
-
3. L-9 qZ.
"J�
-57w<
Geometric Meanslg
Total Dry Solids
L/tuA,
Signature

_J
No
DATE. /I TIME
SampW-Ry
Received. By
i2Q35
Analyzed By. (AL LIJ
Calculated By
Recorded By
Checked By. -��n
,- Z.
Temp S19. Q"C
9C
SampleLqcation
241tr. Check �v&:A, N�PAW!Samgle Type: Grab x Composite.
48 hr. Check
72, hr. Che k- 2-
FECAL COLIFORM.MT
22nd edition Sta ndard: Methods 9221 C.F,-20Q,6(MPN)(Aquequs)
Presumbfivib Test
mL Satuple
-0.60
0.0, . ... .
001
.6.
-00,101
, 0�.
.000.01
0..0000001.
0.00000001
AIPNII
2.4 hours
—1
-7-]
48-hours
+
Fecal Coliform Test
I mL Sample 0.001
.0016.60000t 0.0000001 O.QOOOOOOi� WN
.241,ours 14-1 1 1 —1 —'1 �io
NPN'Fecal Coliform/.9= 10 x MPN index /100 ml KPN19lox
largest volume % dry.'s6lidsItested
c), vo 1- x 3; 59
Sterility Control
Wterotrophic Plate Count
1.0 WE
I mL
0.1 mL
0.01 mL
Dilution Water Blank
Standard Methods. Agar
.1mution Water Blank
Quality Control Tubes
Double Strength (DS) Control
Single -Strength (SS) -Control
o ECBroth.Control
Revised 2 28-13
1

Sampled By
Received By
Ana.lyzed,'By
Calculated By
Recorded By
Checked By
V
Temp Sq Oc
i PC.
Sample Location. _q.&dCV
24 br. Check_4',-to Dna) Samplq Type: Grab -x Composite
48hr. ChecitG-Il-iq,3..'6cl.pilt� Preservation
72. lir. Check 6-f 2-il, 211zw
FECAL COLIFORM TEST
22nd edition. Standard Methods 9.221 C.E-2006(MPN)(Aqqeous)
Prp-mmntive T6-qt
mL Sample
0.00
0.0061
�040
0., 90001
0.6.0000
0.00000001
MPN
I
24 hours
I I
i
-tl'
A
48 hours
+
+
Fiunil Vnlifarm Tact
mL Sample
0.60,1
0.0061
0.66001
0.000001
4.0000001
0.000001
WN.
14 hours
MPN Fecal ColiforWg = 10 x MPN index/ 100 ml
largest volume- X % dry solids tested
MPN/g= I9x 1-`ir 5, C)
01 pp I dk 3. S:�,
Sterility Control
fleterotvophic Plate Count
10 int
ImL
0.1 ML
0.01 mL
Dilution Water Blank
Standard Method& Agar
Dilution Water Blank
Quality Control. tubes
Double Strength (DS) Control
c
Single Strength (SS) Control
i
EC Broth Control
Aevis.ed 2-28-13

N DATE / TIME
Sampled B
Received By
Analynd,By, D
Calculated By
Rocorded.By
2-Y
Checked By
_J
Temp 3492- C) -C
OC
Sample Location
0
24 hr. Check N1W Sample Type: Grab. x ColuppAtc.
48 hrj Check 6 -iocl, Preservation
72 hr. Check
FECAL COLIFORM TEST
22nd edition Standard- Methods 922.1 C E-2006(WN)(Aqueous
Presumptive Test
mL 0 Sample 01 :0.000 040001 6.0,00001 0.00000,01: "0t0000.0. MPN
I IJP I I-IH
Sample
24 hours
48 hours 13
Fecal Coliform Test
0.061
0.0001
0:00001
0.0000.01
0 0.060001,
0.00000001
WN
24bours
I
I
I
I
I I
MPN Fecal Coliform/g = 10 x MPN index / 100 rnl
largestvolumeX % dry solids. tested.
MPNIR C lox 5)
CO I )t-
qtt,wilitv. Cantrn]
Oe'terotrophier . Plate Count
. 10 mL
I mL
0.1 mL
0.01 mL
Dilution, Water Blank
Standard Method&Apr
z—
Dilution Water Blank
L
Quality Control Tubes
Double Streqgth (D$) Control
I'x 0 C-4
Single. Streuth-(SS) Control
EC Broth Control.
Revised 228!-13

Temp, SAA . C eC
AME DATE/TIME 41+,.(( "C.
le -
Sampled By --- �$:"� / • .) At Sample Location. -�. llc
Received By [' }- (' `?.•' m 24. hr. Check, 6 jo o.9 .,Ygjm kmuJ Sample Type; Grab x Composite.
Analyzed By `�(� �� 48 hr..Checic G -11- y, 3 1y� p/ptp Preservation /LAS_R---
Calculated By 72-hr. C_ heck 6-Ii-(q.:z:,f3 DA14
Recorded By
Checked By
FECAL COLIFORM TEST
12nd edition Standard -Methods 9221 CE-2006(MPl)(Aqueous)
Presumptive Test
mL Sample 0.001 t).0001 O.M-0, ; 0:000001 0.0000001 0.00000001 MPiiN
24 hours
48 hours 4-
Fern 1. ('nlifnrm: TP_Ct
mL
Sample
0.001
.6.0001
0:00.001
0.0000.01
0.0000001
0.00000001
MPN
24
hours
:..:
_
-ter, g
MPN Fecai.Coliformf 10 x AN index / 100 ml *PNf 10 x - �f - j
g u - ° 5C ti�PN/
largest volume X % dry, solids tested aco I
fitnriiifv ('nntrnl
Heterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water-Blanit
Standard Methods Agar
Dilution Water Blank
-c f
Quality Control -Tubes
Double Strength (DS) Control
Single Stren h (SS) Control
EC Broth Control-t-l-
U
Revised 2-28-13

t
Temp 3-7, - 0 Oc
NA E DATA /TIME
O-C
Sampled By e -0 S /OL-4/ Sample Location
3Sp.,., 24,hr am Grab x Composite,
Received By - Check ple:Type.
Analygeq By 48 hr. Check 6 -ff it Pil`''reservation
Calculated By Uf )Iq U)SRP 72 hr. Check, 6 �2, yq >W
Rccordpe
. 0 By
Checked By
/7
FECAL COLIFORM TEST
22nd edition Standard Nketh6d.s. 9121 C E-2.006(MPN)(Aque-dus)
Pro-virnfiti V'P Tt-.-Qt
ihL Sample
0.001
0.0.001
0.00001
.0.000001
Q.000000!
0.0
'MPN
.24 hours
49'hours
J
EI—L
-
H
7'�i
Fecal Coliform Test
mL Sample U01 0.0001 0.00001 6.0006 0.006-0601 0.060000.01
01 MPN
:14 hours
MPN Fecal Coliform/g = 10x MPN index / 100 ml NWN/g.= lox J''K'
Wrgest volume X %.dry solids tested -3 (-,4
Sterility
terilitv Cnntraf
Metotrophic, Plate Count
10 mL
I mL
: % 1 mL
0.'61 mL
Dilution Witter Blank
Standard Methods Agar
Dilution Water Blank
< I
Quality Control Tubes
Double Strength (DS) Control'
Single Strength.(SS) Control
L—EC Broth Control
CJ
Revised 2-28-13
b

Sampled.By
Received By
Analyzed By
Calculated By
Recorded By
Checlwd'By
DATE TIME
2 V.
Temp, Sq. OC.
Sample Location
24,hr.Check 4-la -IV,9"5'$,I. Sample Type: Grah x Composite
4-8. hr. Check 4-10V 3gtj 1PreservationQ
72.1ir-Cifeck
FECAL COLIF ORM TEST
22nd. I edition Standard Methods 9221 C E-2006(MPN)(AqueOus)
Presumptive.Test
mL-Sample 01.001 0.0001 0.00001- 0.000001 0.0000001 0."00000. 01 WN
24 hours
+ I
481 + +
Fecal C-oliforni Test
mL Sample
0.001
0.0001
6.0-0001
0.000001
0.0900001
0.0.000.0001
MPN
-24 hours
XPN Fecal Coliform/g = 10 x MPN index / 100 ml MPNIg = to x
/VkI
largest volume X'%. dry solids tested -x, 3. 5'9 0, Oq3sci.
Sterility Control
Hetprotroph 16 Plate C. ou int
10 -m L
I mL
0.1 mL
0. 01 mL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quality Control Tubes
Double Strength� _(PS),Control
Single Strength (SS) Control
EC Broth. Control
,Revised 2-28-13

Sampled -By
Received -'By
Analyzed By
Calculated. By
Recorded By
Checked. By
w
Temp 55-019 C
71
Sample-Lpeatipp -S-& A;, 7
Sample.Type:.-Grab ..x- colnodgite
48 hr. C PresgrYAtiOn
71 hr. Checl;
FECAL COLIFORM TEST
22nd edition Standard Mpth d&9221 C-E-2006(MPN)(Aqp00us)
mL Sample
'0.001
0.-0000
0.0.000001
0.0,0000001
MPNI
24 hours
F.7
- I
I
46 hours
--I-
I
I--
I A-
RiL $a;up0e
0.001
I 0.000i
M00001.
0.000001
U000001,
'0.00060-0.01
W N
'
-1
. --I-
V I I I
I
24 fiours
- -
t 1-
1
MPN fecal Coliforul/9 = 10 x MPN index / 100:ml
largest volume X,..%-.dry solids tested
Wterotrophic Plate coulit
16 mL
I:inL.
Oil mL
.0.01: mL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quallt;Conirbl Tubes
Double-Strength (DS) Control
Sin Ie Strength (SS), Control
EC'Broth Control
Aey!Ped 2-2843

CITY OF WASHINGTON
SLUDGE
20th edition Standard Methods..2.1540-.B-1997(Aqueou's,.),
ame Date/Time
Sampled By
Received By
Analyzed By k
Calculated By Zb,6tjnL G-/0-I W H I -a5 phi
Recorded By. 44'`.Lsp
Checked 'By
Time on Water Oath. 6-10 -1 .1-f , q..155A f,
Time in;Oven -&I(i It(III
Time out of Oven
ss/l/I
Time Wbighed
Sample #
Eva p Dish
WPt Weight,+
Dish Weight
Dish Weight
Wet Weight
Dry Weight t
Dish Weight.
Dish Wei2ht
Dry We! ght
% Dry Solids
-136,7-3la-
5 0 q.*
-S
1330c,
11 Lt 25
Sn. i-ff
?%s'3 9,4-
130, 1 a-c-q
G32o
Revised 6-9-14

Sampled By.
Received By
Analyzed By
Calculated 'By
Recorded By
Checked By
CITY OF
WASHINGTON
SLUDGE
20t.h ed.i.b.on. Standard Methods 2540 &-1,997(Aqueous)
Date/Time
1.
Time on Water. Bath AIL!(
77�
Time in Oven )'�,!)Q Pei
Time,out- of Oven 6-46-4 q,
Time Weighed 6 114, -Lq' 2.S PM..
Sam ple:#,
Eva p Dish #
55
Wet'Weight t
Dish Weight
1130
Dish Weight
Wet. Weiqht.
So, I a3c�
ry., . q ight +
D. -W
Dish Weight
S ),191-93c,
Dish Weight
_qj oq -c,
- --------------
Dry Weight
/,,,7 -1 (.,7r-
% Dry-:So(ids
S., q ge
Revised 6-9-14

i
CITY OF WASHINGTON
SLUDGE
20th edition; Standard Methods 2540 B-1997{Aqueous).
Date/Time
Sampled BY
Received By q s :•,
Time on Water Bath _ ! mil f�- � � j(') i ykg
Analyzed By?-=(4
r -��_ _ Time in,Oven
Calculated By 6� 16- 4 4 ,` Pm Time. out of Oven
Recorded` By 16 �"` '
.�=. i���M Time Weighed _ 6 jo-jq, ' L ,3SPM
Checked By Q-1j, 0'�,p/�-i.
Sample #
Evap Dish*
Y_
Wet Weight +
Dish Weight
r.�'fNw11,
Dish Weight
. SSA I
Wet Wei ht
So. 0 5 11
Dry Weight+
Dish. Weight
Dish Weight
7�Ss1 t
Dr Weight
I is oc
% D Solids
�.
Revised 6-9A4

• CITY OF WASH ' INGTON
SLUDGE
20.th edition. Standard Methods 2540 R-4997(AcIijeous)
ame Date/Time
Sampled. By
Received By
Analyzed By -&-10-lq.
Calculated. By
66 11-' 14
Recorded By
Checked By
Time on Water Bath -10-
Time. in Qv6n -1
-11 OIPM
Time otit:of oven-"-I�. L-u-1.y . OpA
Time We! hod, 6,:
Sample #
Eva Dish Dish #
Wet Weiqht +
Dish Wei ght
125, 5 1 -1
Dish Wel2ht
Wet Weight
I IV
Dry V..Vel 9,ht-.+
-
Dish Might
Dish Weight.
Dr.. Weight
'7 ci �,s sg
Revised 6-9A4

'
,
CITY OF -,'--'''N-r^-~.~
�����
�
_�____
Time
TimeinOVen
Tme o-utof Ove
Sample. #
Evap Dish,#
Wet Weight +
Dish'Weight
Dish Weldht
Wet Weight
Dish Weight
Dish Wei ht
Dry Weight
% Dry Solids.,
ReuisedGrg-4

L
CITY" OF WASHINGTON
SLUDGE
20th edition .Standard Methods .2540 B-1 9,.97(AqpeQUS)
N M. Date/Time
Sampled By- ;Iz5
Received: By
Analyzed By
Calculated By L
Recorded By
Chedked By
Time on Water Bath. 10_4�_ 0! L(f A JN
Time -in , Ovqn 6-1_0-lLt;3.aloppjh
Time - out.& oven &LQ-14. wLt()pM
Time Weighed lll� 141 2
Samp)e.#
Ey4p Dish #
Wet. Weight +
Dish, Weight
Dish Weight
Wet Weight
Dry Weight +
Dish-W-6ight
Dish We]2hL
ga Weight
%o.D Solids
9 c
Revised 6-9-14

CITY OF WASHINGTON
SLUDGE
20th edition Standard Methods, -2540 13-1 997(Aqueous)
`ice 7- W110-7 113, Mll
Time on Water%.Bath A6-10-1:t4. it) ".qpp�
Time in Oven C-1 0- 1 q k of N,
Time out of Oven 6-10-i q-, L q 0 p vff
Time Weighed a�
Sample #
Eva p Dish
Wet Weight t
Dish Weight
a.% 114 1
Dish Wei ht
9
ClS3
Wet Weight
0 39
'
Dry Weight +
i I sh Weight
Dish
1,0 q4c,
Dish Weight..
-3
29- 0 75
Dry Wei g j
3Ljl
D r y Solids-
Revised 6444

bate. 14
Location.;#*.
SuMmary'Sheet
Fecal C611-fdrms
Pat.hogen Reduction
Log
10
-16 9. 1
3, 33:
qs
3,2
,-� - , , 07 qs
SS 'U-3- -
Ge'Or'hetd,C,Mea ' nsfg
TOW Drv,Solids.

T6MP
4�2NA W' D TUYIE LOT11
Sample. (y Z-, 14XI-1 t Iq Sample Location
Received By -7 /-QJ I 10";LqJ3 24 hr. Cheek7---3-— '59viSample Type: Grab x Composite
Analyzed By I 1pin 48 hr.,.Check Preservat' o iv
Calculated BY 72 in, check 15-iql-h "60AM
Recorded BY
Checked By
FECAL COLIFORM TEST
22nd edition, Standard Methods.9221 C Rm2006(MT.N)(Aqticous)
Presumptive Test
0.001- 0001 0.60001 0.000001 0.qQ'O00.01 0.0000.0091 WN
24 hours.
48,hours I' F I Lq C
ripen[ Volifnrm TP-qf-
IF Sample
0.001
10001
- 0.00001
0 OOOOQ1
0.6000001
0.00000001
MPN
24 hours
7-71
— ]L--
1 —1
1 - ---I
.—F
..WN-FecalColiform/10 x MPN index / 100 ml MPN/10.x 1, "Y is:-39= g =
largest volumeX % dry solids tested 0' 0 0/ Y' 3, 0.6 0,00306
qtprifitv Cmitmil
,Heterotrophic Plate Count-
10 mL
ImiL
OJ mL
.0.0.1.mL
Dilution WaterSlank
Standard Methods Agar
Dilution Water Blank
Quality -Control Tubes
Double Strength (DS) Control
Strength (SS) Control
.Single.
EC Broth Control
V c-
Revised 2-28-13

Sampled By
Received. By
Analyzed By
Calculated By
Recorded :By
Checked. By
TeMP3222COC
DATE TIME C
Sample Location
A .24.hr. Check 7-3-1q, /;i:f4Vv, Sample T-Ype;.Grab X.- Composite
7 3 i,"A, 48.hr. Check: N-4-rescryation
72 hr. Check 9
-71,5-h q-1EL35-121—M
FECAL COLIFORM TEST
22nd edition Standard Methods. 922.1 C E-29QO(KPN)(Aqqeous)
Presumptive Test
mL Sample
0.661
0.000x
0.00001
9.000001
0.0000001.
F 0100000001,
MPN
24 hours
1.+-
T-7
-t-
413 hours
1
4-
1.JA
I'—
1�
I
I—
I
..I
I J
7t,
Fecal"Coliform Test
mL Sample
0.*0 . 01
0.0001...
0.00001
01 .000001
0.0000001,
0.0.0000001
--MPN
24, hours
!9 , — CJ
MPN Fecal Coliform/g 10 x MPN index 100 ml MPNIg 10 x 112 , 17 9 7 �
largest volume X Wd I j.-Y solids tested 0. G
Sterilitv Control
HeterotrD phic'Plate Count
10 mL
I mL
0.1 mL
O.'Ol mL
Dilution Water'Blank
eL
Standard Methods Agar
Dilution' 'Water Blank
Quality Control Tubes
Double Strength (D.S) Control
Sin gle,Strength (SS) Control
EC Broth Control
Revised 2-28-13

Temp. 35,Lr°C
E jI)ATE / T1ME�
Sampled B c/i"�'� Sample Location
Received -By r :' 4�rj¢ryt: 24 hr.. Check W,Sample:Type. Grab X. Composite
Anaiyzed.By '7.Z .!q 48 hr. Check.Z:j�� „ .33,, , Lw'Preservation
Calculated By ),1'4'& rya 72 hr. Check
Recorded. By i {I f LF 171 9,14ti-
Checlied By
f E CAL COLIFORM TEST.
22nd.edition.Standard Methods .9221 C E4006(MPN)(Atlueous)
'Prncu rn of ivPTest
mL Sample
0.001
0:0.001
0.00001 .
0.000001
0.0000001
.0.00000 Of
MPN -
24 hours.
�-
—
-4-
-I-
}—
_i
A
11
48 hours
P.-Pnl f''nlifnrm Teat
mL Sam le
0.00t
0.0001
.0.00001
0.000001
0:0000001
0.'000900.01
MPN.
14 hours
'
1' c—
t�lJ
MPN Fecal Coliformlg = 10 x MPN index / 100 ml MPN/g. 10 x
largest -volume X" %•dry solids tested U, v I ,! :3. o26 6. o03i 1-
Cfaril. f nnfrA
Heterotropliie:Plate Count
10 ntL
1 mL
QA mL
0.0.1 m'G
Dilution Water Blank
Standard Methods Agar
L
Dilution Water Blank
Quality Control Tubes
Double Strength S Control.
Single Strength (SS) Control
/
EC Broth Control
v
,Revised 2.28-13

Tenip-35,Z) OC
DATE TME OC
Sampled By //4/, /01,00 Sample Location
Received By tc AO :24 hr. Check 7­3,jo/, b.; i6A >-t'Sample Type: Crab x Compos—
AuAjy?A'Ay pq 48 kri ChqckO ' Lk -IL
�-WIPrese - tion
. D "a.
Calculated By vt, on, 72 hr.. Check
4 1.
Recorded By
Checked By
FECAL COLIFORM TEST
22.nd edlition, Standard Methods.9221 C E-2006 (WN).(Aqueous)
Presumptive Test
mL,'Sample
0.001
'..0.0001
:0..0000i
0.000.0 1
0.00O.QQ61.
1 0.0.0.000001.
MPN
24.houn
+
4-1
+1
+-1
1
1
-
1­
1 :7:j
-
14-
Af
I
q3-I
48'ho
T-1
I I
Fecal Coliform Test
mL Sample]
0.001
0.0001
0.00001
0.0000001
O.OQQQQOOI j - MPN.
1 24 hours'
14
1
1 —1
—
1 —1
1
1.
1
1
1
1
1 ­­ 1
MPN Fecal Coliform/g 10 x MPN,index / 100 ml
)a rgest volume X % dry s,oji Os tesIqd
MP 10 x
CO 3.0
8terifitv Control
Heterotrophic Plate Count
10 mL
I mL
0.1 mL
6.01 mL
Dilkti on'Woter Blank
Standard Methods AgEkr
Dilution Water Blank
Quality Control Tubes
Double Strength'(DS) Control
Single Strength (SS) Control
EC Broth Control
Revised 2-2&13

DATE TEVIE
Sampled By
2OS—A
Received By
Analyzed By
Calculated, By
Recorded By
awN,
Checked By
T, ,nlp IDC
Sampte, Location
24hr. Check 7-3-g/ /1 1.2.1 A�mple.Type; Grab Composite
48hr. Check '7-
72 hr. Check-S-M XojdnDl W
FECAL COLIFORM TEST
22nd, edition Standard Methods 9221 C E-2006(MPN)(Aqueol s)
PresnmDtive Test
mL Sample-
0.001
0.0001
0.00001
0.00-0-r9-0I 1�
070000001
MPN
24 hours
I
.
4—
Ilk4816Urs
—
I —E0.0E000001
I
I
Vpen] rnliffirm Teat
mL,Sample
0.001
0.0.001 T-
. 0-.00001
0.000001, .0.0000.001
0.60000061
110-N
24
hours
MPN Fecal ColiforOg = 10 x MPN index / 100 ml MPN/g = 10 x
largest volume X. dry. solids tested
qh-rilift Control
Heterotrop.lic Plate Count
10 ML
I -mL
0,1 WL
0.01 HIL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quality'Contro''I Tubes
Double Strength (DS) Control
-Single Strength (SS) Control
EC Broth Control
Revised 228-13

TOMP
DA
TE! TM'
Sampled BY 7 o° 1/0 A_L4l-Sample Locad n J�
Received By 10:, Zfd-ai 24 hr. Check -7 mpleType: Grab x Composite
Analyzed By 2, 2f. p m 48, fir. Check f- V-- tq 'pservation
Calculated By
Recorded.By
Checkedroy
FECAL COLIFORM TEST
* ­ - ' ' ­ ; i - 22nd edition Standard Methods.9221 C'E, -209,6 (MPN)(Aque,ous)
PresUal-DtiVe Test
mL Sample
0.001
OXOOI
0x0001
OWN
Q.0000001
QA900W- 1,*
_MPN
24 hours
+I+-
j-
492hours
Fecal Coliform Test
0. 00,00, 1 FAII�w
mL Sample0. -0.0000.001:
.001 0.0001 0.00901 0.000091, Q,00
24
4, . hours —
MPN Fecal Coliform/g = Wx WN, index / 100 ml MPN/g = 10 x
== 5KL- -_3
largest-volume-X % dry solids tested C) - C) C, 1 4-
U _per 1,
Sterility Control
Heterotrophic. Plate Count
10:mL
I AIL
.6.1 mL
0,0,1 mL.
Dilution'Water'Blank
Standard: Methods Agar
Dilution Water Blank
Quality.Control Tubes
Double Str7ongth (!?S).Control
Single Streng!h (88).Control
9C Broth Control
V
Revised 2-28-13

9
CITY OFWASHINGTON
SLUDGE
20th edition Standard Methods 2540 G-1997(Aqueous)
Sampled, By
7f1-ne 921T'6K
Received By
7 22 1L
Analyzed By
�J 7%2„(f �; II 67x*
Calculated By
LJQ . 4- li IL
Recorded By
LAA.P IM_ i4 a;_�M
Checked By
'7 �! : 10 p��
Time on Water Bath _!('(j'�'4t�
Time in Oven
Time, out of Oven _ 3' i
Time Weighed �14
713114 R' a-,
Sample #
Evap Dish #
Wet. Weight +
Dish Weight.
Dish °Wei ht
VVet Wei ht
Dry Weight +
Dish 'Weight
Dish Weight
Dry Weight
% Dry Solids
13.8
gyp ; y.7
,50. 264,1
�a,3:83`
'b.-.�t`r
1-535
3..tatp:
far. Zi s 3
A01
FCC - lab
1-54a.
Revised 6-9-14

CITY OF WASHINGTON
SLUDGE
20th- edition -Standard Methods 2540 G-1 997,(Aq u-eous)
Sampled By
71AIlY 7,'3OAv-
Received By
/p,
Analyzed By
./,I
Calculated By kt
4 1
11
Recorded By
-3L/ ?, / I
Checked By
Time on Water Bath. 4 tn
Time in Oven
Time out of Oven. �3i 4 s 12'M
Time Weighed . -7.hj- iq- q-'bkam
Sample #
Eva p Dish
Wet Weight t
Dish Weight
Dish -Weight
Wet VVpight
Dry Weight +
Dish Weight
Dish WeiRht
Dry Weight
% D!y Solids
A—
Y
7 0 -4 53
42,
6 j '3L
Y 153
9-q3-3
3.05
Revised 6-9-14

CITY OF WASHINGTON
SLUDGE
20th edition Standard Methods.:254.0 G-:1997(Aqueous)
NDate/Time
Sampled. By/:.St
Received By. Time on Water Bath 3R"4fK
T
Analyzed. By 4 T
, 1 r = 3,�' Time in Oven
Calculated By (/ 1 4, 'p : 6,qA, Time out of Oven 3.4-9
Recorded By�/J1�;, 3�Dry, Time: Weighed :. S 111h,
Checked, By
Sample #
Eva Dish #
Wet Weight +
-Dish Wei ht
Dish Weight
Wet Weight
Dry Weight;.+
Dish Weight
Dish Weight
Dry Weight
%. Dry Solids
3
13 7 94
s'o, E.-4
'Fri &�qp
2.
3.d�
Revised 6-9A4

5ampled. By
Received: By
Analyzed By
Cal.culptqd By
Recorded By
Checked By
MUMMIRMA
CITY OF WA,SHINGTQN
SLUDGE
20th- edition St-p-ndar-cl MethQ-0s. 2540 G-1 997(AquppLis)
e
►0 100 AM
Time on Water Bath f I I.- SR aly•.
Time in Oven Q.* 3'& An
Time out Oven 'A
Time Weighed )4-� 43
Sample #
Eva p Dish. 0
W,et,:W,eigbt +
Dish Weight
Dish Weight
Wet -Weight
Dry - Vyelght' +
Dish -Weight
Dish Wei oht
Wei ght
q
_Dry
_%-D!y.Solids
Revised:6-9-14

J I
CITY OF WASHI.NQTO,N
SLUDGE
20t.h edition Standard Methods,2540, G-1997-(Aq.kjpoLj.$)
Na Date/Time
4-
SampteOBy )tw."
;7.
.Received By ?L/:4,/� /o., z Time on,water Bath
Analyzed By 7)J-/) 4
- Tima-in.0ven a1S'0
Calculated By Time:out�of Oven
q_-, . . -; ... . V,
Recorded By Time.. eighpq
Sample #
Eva p Dish #
Wet We'lght +
Dish Weight
Dish Weight<
Wet .Wei ght
Dry
Dish Might
Dish Wei dht-
Q!Y'Weidht,
%,Dry.-$olids,.
Revised 6-9-14

Sampled By
Received B,
Analyzed B)
Calculated
Iculat d, I
Recorded,B
Checked. %
CITY OF WASHINGTON
SLUDGE
20th edition Standard Methods.2540 G-1997(Aqueou.$)
Time on; ,Water Bath —A30A,
Time, in Oven + NS-
Time. Qpt�bt 0 4 ,-+g- *.,I ypn
Timo.-Weighpq --!�-3,-)4, 10:164 a,^,
Sample 4
Eva Dish
Wet Weight
Dish Weight
Oish,Woight
Wet Weight
Dry Weight',+
Dish Wejdht
Dish Weight
Dry Weight
% Dr Solids.
773
8- 3 5 f,b
5-Z6 `b
.5 4'� A,
3 o
Revised 6-9-14

Sampled E37y—
Received By
Analyzed, By
Calc4lated. By
Recorded By
Checked By
-QITY OF WASHINGTON
SLUDGE
20th edition Standard Methods 254Q 0-1 997(Aq.ue.Qus)
MAIM
Time on Water Baths
Time in Olv.en
Timp.out of Oven 4-: 51 en
Time Weidhed 213114 9111:'�&A-N
Sample. #
Eva p Dish-#
Wet-, . Weight.+
Dish Wei ght
Dish Weight:
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
Dry ;Solids
4:9.- q-7 �jqod
5(), 5�96.p
�q, .3
3, OG
Revised 6r9-14

Date- 14
Location
I
S-u-m-ma-ty.Shoet
Fecal: Cbllforms:
Pathogen. k6d'uptl6n.
MPN/J..
23 5
Log,
3,!543
53
Geoffietri.cWe'anilg
Toital, Dry, Solids,
Signature

CITY OF WASHINGTON
SLUDGE
2pth edition Slandw.d, Mpthods 2 G-
540 1,997( queous)
Name Dateffime
.Sampled By tonojc A),Pv 4IJ 0, P,
Received By �
Analyzed By
calculated By �2ttwe V ll-S.-/ 'I - '0A
Record d B
- I Recorded y
Time_ qn Water, Bath JQ,',4qh-M
Time., in Men 0,337PN
T.imp.,Put:of.0+ven .41,30PrN
Time Weig
hed
Sam p-le #
Eva e Dish #
Wet- Weight+
Dish Weight
Dish Weight
Wet -Weight
Dry Weight . ,,+
Dish Wb I ight
Dish Weight
DrV:Wei ght
C).
- JA
143
Revised 6-9A4

CITY OF WA$.HING,TQN
SLUDGE
20th edition Standard Methods 2540. G_1997(Aqueous)
Name Date/Time
Sampled By
Recpivpd By
Analyzed By
Calculated By
Recorded By
Checked -By
i
Time. on - Water Bath 10,15M
Time in Oven
Time. out of Oven * LfljoPk
Time Weighed. I i cl','Lf 3{i ik
Sample #
Evap. Dish #
Wet -Weight +
Dish Weight
Dish Weight
Wet Weight
Qry Weight +
Dish Weight
Dish Weight
Dry Weight
Dry Solids:
?603q
2 7# 5ro
aOt 3'000g�
'8Q 60,
0 9
6o9c.
TI 9
L
-------------
Revised 6-9-14

CITY OFWASHIN . GTO ' N
SLUDGE
20th edition.Sta.no.a.rd Methods. 2,540 Q,-1.997(Aq4qq.us)
Name Date/Time
Sampled By tool.,%"t Ow-.10-J— flw-4--lq P " 14,0 A aA
Received By "'Lu
.An,alyxeo By 2c
Q-alculated By
Recorded By
i,,A
Qbe.ckod : By Lr- Y3'P
Time on Water Bath
Time in Oven 9,faaPP\
Time out of Oven (_f.',30.Pk
Time Weighed
Sample #
Evap,DM4
'Wet Weight +
Dish Weight
Dish Weight
Wet -Weight
Pry wmight,+
Dish -Weight
Dish Weight
Qry,-Weight
olids:_
:% Dr.y Solids
U 2024
50 jt2 6
22,354
19, 3. q
g q-9.
Revised.6-944

Sampled .By
.Received. By
Analyzed By
Calculated By
Recorded By
Checked.By
Wn,
CITY OF WASHINGTON
SLUDGE
2.0th edition Standa rd Methods 2540 G,1 997(Aqueous)
Time.on-Water Bath
Time. in Oven "Ca Pik)
Time out of Oven 11-25-4 S:4 S 3 SA
Time_ Weighed. J0!oon�
Sam ple#
Eva p Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet. Weight
Dry Weight +
Weight
Dish Weight
Dry Weight
Dry Solids
-A�- LA
131.aq3FA
UJ52
_Dish
2, V
-
----------
4,9.9-
Revised 6;9-14

CITY OF WASHINGTON
SLUDGE
.20th:edition Stwidard Methods 25.4.0 G-1'997(Aqueous
Name PatelTime
Sampled By Z.k.
q,, S
Received By Time on Water Bath Analyzed, By j f-4-IL(,11 .11 &#m Time in Qveq (70 PM
Calculated By 11-�-/Y' I '-14Pk Time out -ofoven A)A
Recorded By adbo 1 L'3� 1 11 14PAk.. Time Weighed H-S-4ce)
Checked By 0
Sample,#
Eva p Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
% Dry Solids
1 67
60P 17307
SO, C460
L4 I cl.
J, .7.13 Qa�
6-1-91T?4-
Revised :6-9-14

Name
Sampled By
Recelyed By
Analyzed By
Calculated By
Recorded .By
Checked By
CITY OF WASHINGTON
SLUDGE
20th edition Standard Methods,- 2540 G-1.997(Aq4eous)
Date/Time
q! 55.41K
Time on Water Bath I
Time. in.Oven 509h'�
Time out of Oven 5!35#K-
TimeWei bed
Sample.#
Eva p.Dish #
Wet Weight +
Dish Weight.
Dish Weight
Wet Weight
Dry Weight +
Dish Wei ht
Dish Weight
Dry Weight
%-Dry.-Solids
I 1
5C)
TJr
Revised 679-14

���F�'��' — __' ..0 �
CITY ' _' , .~~ . ,~..
_____E
Time on Water Bath
Time
Sample #
Evap Dish #
Wet Weight +
Dish Weight
Dish Weight
Wet.Welght
Dry Weight +
Dish Weight
Dish Weight
Dry Weight
Dry .8plids
R$visedG-Q-4

Telnp3s 125 DO
NAME DATE / TTNIE 1-44 4. S - PC
$gmpled By I I-q - 14 9 '3 O-A, #I Sample.Location
Received By Eau I L4,, 10,'l S A-Wk 24br. Type; Grab x composite
Analyzed By 1D:P3Aq,-% 48. hr. Check Pros a ery tion
Calculated By It'-s-OwN 72 bk. ClIeCIOP744, 11Ohm
Recorded By j -7 -dr,-U^ tAyv\
Checked By
FECAL COLIFORM TEST
22nd edition Standard Methods 9221 C.E-2006(MP.N)(Aqueous)
Presumptive -Test
mL
Sample 01001 0.0001 0.000D1 0.000001- 0.0000 oi- 0.,00000,001 MPN
24 hours
48.hours
FernlValiffirm Text
mL Sample
0. - 001
0.0001
0.000001
0.0000001
0.- 0 001
TI..
MPN
24 ours
-T---,T---.
T
I
1
Foo
,
I -F
K
MPN FecalC91-i,form/9 10 x MPN index / 100 ml MPN/g = 10.x '6
largest volume X % dry. solids tested C) x if.
Sterilitv Control
Heterotrophic- Plate Count
10 mL
I mL
0.1 mL
0.01 mL,
Dilation Water Blank
Standard Methods Agpr
41
Dilution. Water Blank
Quality Control Tubes
Double Strength (DS) Control
Single Strength (SS) Control
EC Broth Control '411,,-I
Revised 2-28-13

- --J -- -- __
Tem P 3&:6 °C
Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked.By
DATE I TIME y y j° C
1136A4-11 Sample Location ,,
24 hr..Check �_ � ��fJ,�Sample Type: Grab x Composite
f L I j *t -M 48 hr.:Check. f tt6-j�(,. �o� -.91 Preservation
An 72 hr. Check
11-1114 $;32Ar
FECAL. COLIFORM TEST
22nd edition Standard Methods.9221 C E-2006(MPN)(Aqueous)
Presumntive Test
mLSample
0.001,
OA001
0.00001'
0.000001
OAl}.00001
0.000;00.01
MPN
24 hours
--
+
f-
-�
--
—
—
—
4s�hours
4 .
_
_
4 5
Fecal Coliform Test
n iL Sample 0.001 0.0001 0.00001 0.000001 0.0000001 0.000.00001 MPN
24 hours I
MPN Fecal Coliform/g = 10 xMPN index / 100 ml MPN/g = 10 x
largest volu, me.'X % dry solids, tested I x 3. _ p pOt {'. �3'. 3)
Sferility [_antrnl
Heterotro hic .Plate Count
10 mL
1 mL
0;1 mL
0.01.mL-
Dilution Water Blank
1
Standard Methods.A ar
G
Dilution Water:Blank
L
Quality Control Tubes
Double -Strength S Control
Single Strength (SS) Control
w
EC'Broth: Contra
U
Revised 2-28-13

I !NAME, h
Sampled By.
Received By
Analyzed By
Calculated By
Recorded By
Checked -By
PATE / TIME
/1-77-1 . q-,- L-'-5-Mim
A-7 -4 411A
naip 39.ZS. Oc
04.5 Oc
Sampl6location
24 11r.Check ampje..Type:.-Gra4�. x Composite.
/1-5'-(1 1'?-'(wMDNk(k
48 7 reservation hr. Check IL-�-tq (b ; ISS4
7.2 hr. Check
FECAL COLIFORM TEST
22nd edition Standard Methods,9221 C-E-720*06(MFN)(Aqueous)
Presumptive -Test
mL Sample.' 0.-00 0.0.001 0.00061 0. - 00000 - I 0.0000001 0.00000 01 MTN
24�bo- rs - , �4 J4,
48 h rs + OU
Fecal Coliform Test
mL Sample
0.001
0.0001
0;00001
0.900.001
0.000 01
0.00000001
1 WN
_24 hours
WN Fecal Coliform/g,,= 10 x MPN Index 100 ml MPN/g = 10 x
largest volume X Wdry solids. tested 3)05(
6, 0.() 1 D 05-T 01
Sterilitv Control
Heteroirophic Plate Count
10 mL
I -mL
0.1 mL
6.01. mL
Dilation Water -'Blank
Standard Methods Agar
Dilution Water Blank
Quality-ControiI.Tibes,
Double Strength TS) Control
Sin gle'Mrength (S$)::Coutrol
EC Btotk'Cd ntr ol
Revised 2r28-13

� lkvkrjl[�ilil
Sampled By
Received 1y,
Aqaly.zed,py
Calculated Ay
Recorded By
Checked By
GATE /ww
I 45A k
It, . I T511A
Temp 39.25 PC
4CP5 O-C
Sample Location Lf
74 hr. Sample..Type: Grab x Composite
48. hr. Chock -II -6-1 Im 54-&&, Dreservation AZ YL-P
72 hr. Check 11:72-1 'PKUj
FECAL COLIFORM TEST
22nd edition,Stitadard:Metliods.:9221 C`E-2006(MPN)(Aqueous)
Presmuntive Test
mL Sample
0.061
0.0001
0.'00001.
0.060001,
0.0000001
0: 6000001
MPN
24 hours
48 houirs
+
I
I
Fecal Coliform Test
ML sample
-0.001
0.0001
0.00001
0.000001
0.0000001
'0,60000001
*
MPTq
'24 hours
14
1 �
I �—
I �
I —:I
I
I
I --- �
I �—
U
I I
I
I
I
I
I
F ,
1' .1
1
1
�Q..O
-YWN Fecal, ColiformIff = 10 x MPN,index 1100 ml MPN/g = 10 x
largest! -volume X %. dry, solids, tested Oo 0.01 )e I.;)-
SteriliN Control
Heterotrophic Plate Count
10 mL
1 mL
.0.01 mL
Dilution Water Blank
Standard Methods Agar
Dilution Water Blank
Quality Control Tubes
Double ;Strength (DS.) Control
Single Strength (SS) Control
EC Broth Control
C)
Revised 2-28-13

Sampled By
Received By
Analyzed By
COculst.e.d- By
Recorded By
Checked By
NAME OATE, I TIME
It 44-- 11
LI 611. YL
Temp'35". Z5 Oc
W'5 OC
S , ample Location
24 Samp e. Ty I ,pe:-Grak _x Composite
48 hr. Check, if Preservation
Wj
72,hr.Check,((--2-& J. q
FECAL COLIFORM TEST
22ud,gdition St.and.ard Methods. p2i C E -20,Q0(bWN)(Aqucqus
Presumntive Test
mL'Sample
0.0001
0.00001
0.000001
0.0000001
0100000901
M[PN
14 hours
141
14
1-
14-'
48 hours.
1 +-1
-1
-1
41
-
--
-
33
Vot-M Cnliffirm TLO
mL Sample
0.0011
0.000
0..00,0-01
.6.000001
O.QQQQOOI
0.00000001
NwN
hours
T
MPN Fecal Coliform/g 10 x AVN,Index / 100 ml
O/q.
MPN/g.=- 10 x -q , '3-
largeqt volume-X fty.g?Ilds. tested
X 3,31
Sterilitv Control
Heterotrophic Plate Count
10 mL
I mL
0.1 mL
0.01, mL
Dilution Water Blank
Standard. Methods Azar
-J-
Dilution Water Blank
6
Quality Control Tubes
Double,Strength (DS),Control
Single Strength _(SS) Control
EC Broth Control
Revised 2-28A 3

NAME
Sampled By
Received By
Analyzed By
Calculated. BY
Recorded By
Checked By
Temp. -$S. 25 ac
DATEW TIME IfIf 5 01C.
0-44- I- CU 55 A Y" Samplelocation#
4-1 24 h,., Check _L-54 M-2qo IWI�Sainple Type: Grab x Composite
q 11 fq- o 48lIr.Check tf-7fP-ry. I-,g3,jn_PWPrese.rva.tion vla 9-
--7--f if',Sq rtry 7; hr. Check 11-7-14,. 1) -.1 Oamw�
II-7j'f, Ii : -I;q&K
FECAL COLT FORM TEST
22nd.edition Standard Methods.. . 9221 C E-2606(W_:N)(AquCous)
Presumptive Test
mL'pskm#le- 0.09 01.000-1 0.00001 0.000001 0.0000001 0.00460001. WN
24 hours .1 4
48'hours I +
Fecal.Collforni Test,
mL Sample
0.001
0.0001
0000E
0.0.000.01 . . ...
I .. .. .
0.0000001
0.06000061
MPN
I 24 hours
WN Fecal Coliform/g.= 10 x-A W index wmlg.= 10 x W Vf �
largest volume X Wdry. solids tested 01001 'K 3153 o. ov.3$3 3
Sterilitv Control
Heterotrophic Plate Count
10,mL
I mL.
0.1 mL
9.01 ML.
Dilution' Water Blank
Standard Methods Agar
Dilution Water Blank
Quality: Couirollubcs,
Double.�Strength (DS) Control
Single Streng!h (8S) Control
EC Broth Control
C.j
Revised 2-28-13

Sampled. By
Received.By
Analyzed By
Calculated lay
Recorded By
Checked By
NAME, DATE /TOR Temp 3 5, -6 �c
15 qC
'4 -ILI Sampletocation
13 A tt .241ir. Check /I ample -Type: Grab x Composite
1 _47�141_1Checlt P_&�1�4 L1.12'M*ieseryation
COOVY1 72.hr. Check 11<7-14gj),
FECAL COLIFORM TEST
22n,d edition Standard Methods j!21 C FM6(WN)(Aquqous)
ML Sample,
'0.001
0.0001,
O.qQO f
.01 00,0001
0.0000001,
010000 0001
24 hours
LEI
L__
48 -hours
+
I
I
I .—I
_-1
�1_.
�1
2
—1
—.1
1 —
Fecal Califarm Ti--;t
ML Samold
0.'001
0.0001
&00001.-,
000001
0.0000007-F
, 9.0060 1
fMYN
MPN Fecal Coliform/g 10 x MPN index 1100 mil
!prgp#vqlqIn e,k%.d. ,
. . .r y solids.tested
mpi-qg= 10 x- C)
f5 )Lf( Ap�/ 5
AfArifitv Vantral
HeterotrophicTlate Count
10 ML
I mL
0.1 _WL
Dilution Water Blank
Standard Methods:Agar
Dilation "Water, Blank
Ouglity, Control Tubes
Double Strength, (D5 .Control A
Single Strength (SS). Control
E C BroWControl
Revised 2-28.43

1,
Summary She ' et,
Fecal �Cdflfbrmt
Pathogen RedUction-
'Locsifion #
MPN/g
Log'.
�3
I&I
-7 1
' 4, 6-s. 4
Geior4et,ricMeans/g
Total Dry Solids,
Signature

7 Temp 36-, L °c
/*wy, DATE, -Z TIME, .0c
Sampled By
A/; 91100-A Sample Location
Received. By J 4� Whwk 74 hr. Check -13 Sample Type; Grab Composite
Analyzed By .48 hr. Check I Klv$reservatlon
Calculated By J d 72hr. Check
Recorded By OET ri
Checked B 3,qla,.,
y
mL Samp
24 hours
48'hours
FECAL COLIFORM TEST
22nd edition Standard Methods' 9221 t &200O(MPN)(Aqueous)
PresulUntive Test
WN
gfllilllij �I I11111 IY'III 111III
Fecal Coliform Test
MPN Fecal Coliform/g 10 xMPN index.4100 ml MPN/g..=.- 10 x It 3 <3 PA
largest volume X - % dry -solids tested 0' 6 C) D 5C) C) 05
Sterilitv Control
Reterotrophic Plate Count
10 mL
1 mL
0.1 mL
0.01 mL
Dilution Water Blank
standard, Methods,Agar
Dilution Water Blank
Quality ControlTubes
Double-Streng!h.(DS)'Contr61
jVIU
Sin le Strength (S§2,c-bntrol
EC Broth Control
U,
ju
tevised 2-28-13

I
Sampled By
lRegelveo, By
Analyzed By
Calculated By
Recorded By
Checked By
Temp. 3 0 OC
PAT -1 TIME ' O.c
,Ir Y
Sample Location
kN 24 hr. Check gimole Type: Grab x Composite
48 hr. Check
IVI 72. hr. Che,ck 9
FECAL COLIEFORM TEST
22n.d.edition $tan0ard,Methods 9221 C E-200,6(WN)(Aqqeous)-
Presumptive Test
mL,Samp I le. 0.0.01 0.0001 0.00601 1 '0:000001 0:00000% 0.,00000.001 MPN
"I — 17 — 1.--1 1 �j
24 hours I + I _�d �_, — � I 1� I 1 —1 1 —1
48 hours f 33
Ferid Cnfiffirm Teat.
wLsamp,le�
9.001
0.0001
0.00001
0.000
U000001
.0.QQQQQqO1
MPN
I 24hours
1 -1
-J,
I
J
-J�=
-T7F-
10 x,NWN index 10 ml W-Nlg= 10x Y IR
MPN Fecal Coliformig = 0- . , Zi 3.q 0 PA_ (F 0
0 . 0
largest volume X % dry solids tested t
SteriliN Cnntral
fleterotrophie Plate Count
10 mL
YML
0.1 mL
0.0.1 ML.
Dilution Water Blank
Standard Method$, Aga r
F—Dilution Water 'Blank
Quality Control Tubes
Double Strenalh,O)SIControl
qVA, AWL
Single Strength (SS) Control
Ast
I EC. Broth Control
Revised 2,28-13

Temp 3Y,-O oC
/jKA)4E
DATE/ TZE,
lrly 0c,
sampled By
Sample.Location,
llegeivedft
AA
h-jo,.63A.
�4.'hr.6qck 11-13- 7,441p,eType:
$ Grab x
Composite.
knal zed By
48hrXhqek)(-kr-(L-jO'.Y9-M' Preservation
calculated By
72 hr. Check
Recorded By
I -I Lf. -.
-.hecked.By
LIU
17
FECAL COLIFORM TEST
22nd edition StandardMethods.9221C E-2006(MPN)(Aqueous)
Presumptive Test
MIL Sample
0.001
6.0601
'0.00001,
O.00OQQI
.00000001
MPN
24 hours'
i
48'hours
Fecal Coliform.Test
mL Sample
0.001
0.-0001
0.0.0001
OA00001
0.0000001
0.00600001
24 lion rs
4PN.Fecal Coliform/g 10 x,MPN index [ 100 mi MPN/g= 10x,
20 M
]a Lt-
rge,stvolume X Wdry solids tested 01001
Sterilitv Contra]
Heterotraphic.Plate, Count
10 mL
1'ML*
-0.1 me
10.bl mL
Dilution Water Blank
L
Standard Methods Agar
Dilution.water Blank
Quality Control.Tubes
Double- Strength TS) Control
Single Strength (SS) Control
EC Broth Control
evised 2-28-13

Sampled. By.
Received By
Analyzed By
Calculated By,
Recor*o Py
Checked By
mLSamp]
24 hours
48 hours
:Temp 36-, 0 OC
DATE./TIME PC
XV, //Z/ F'/10 /11,f,( Sample Location
11 11� 114, 9:30hfit 24hr.ChecQ/-/3j JO "S.9 AMS.an pie Type:- Grab x. Compqsite
IH-J,(D V4- AM- 49 hr. Check I H 1k5reservation
72 hr. Check
xal dol
FECAL COLEFORM TEST
22nd edition Standard. Methods, 9221 CZ?-2006(MPN)(Aqueoms)
Presumptive Test
0.0001 0-000O1 e'V 0._QOOqQ1-
Coliform:Test
mL' Sample 0'001 0.00 001, 0.06601 0.000001 0091. U. 000.00.0,001. WN
24 hours- —1 --1 71 1 1 1 1 1 1 1 1 1 1 1 F _j I I I
MPNFec;al,Cq11ifOrm/g = 10 x.MPN index / 100 ml AVV/g = 10 - x < I i
largest:volume X% dry solids tested cola
Sterilitv Control
Heterotrophic Plate Count
1.0 mL
I mL
O.i int
.6.01 mL
Dilution Water Blank
Standard Methods Agar.
Dilution Water Blank
Quality Control Tubes
Double Strengtit (DS)Control
-Single Strength (9S) Control
HC'Broth Control
U
Revised 2-28-13

Sampled .By
Received By
Analyzed: By
Calculated By
Recorded By
Checked By
Temp 3S, 0 'C
DATE TIME
$amiple..Loc.ation
lit 24 hr. Check, 11113 4Y JJJIPI M Sample Type: Grab x. Composite..
48 hr.. Check 1.0'. Tj MI. Preservation .
Opyn 72 hr. Check
I A
FECAL COLIPORM TEST
22nd edition Standard . M.ethods,9221 CE-2(
.606' MPN)(Aqu eous)
PresuinDtive-Test
mL Sample
1. 0011
0,0001
0.0.0001-
'0.0000.101
0.00000.01
0..0 0000.01
MPN
24hours
481to6rs
Fe.cat,Coliform Test
mL Sample
0.001
0.0001
0.00001
0.060001
010600001
0.060000.01
MPN
24'hours
I—
I
I
I
I ,
I
I
I
I
I
I
I
I
I
I
UFPN-Feqal Co.] iformIg = 10 x MPN index 1100 ml
largest volume % dry. solids tested
MFN/g= 10,x -/- ( t R —= I g -- � r.) -- ( ` m C ( Ia
010M. 543,q.R o, D. 0 -3 q q
Sterility Control
Heterotro' Phic;Plate Count
10'mL
I mL
OJmL
0.01 mL
Dilution Water Blank
L
Standard Methods .Agar
Dilution Water Blank
I
Quality Control Tubes
D . ouble Stre ngth (DS) Control
Single. Strength On Control
EC Broth Control
2evlsed 2r28-18.

Sampl.qd.]3y
Received By
Analyzed By
Calculated By
Recorded By
Checked By
mL SaMol
2 4,hours
49 hours
mL
Temp! 35; 0 -OC
7 D TE TIME, Le�, OG
t T,,O Aw Sample Location
24 hr. Check it 11:0 Sample Type:. Grab Composite
t '2,� q- - �0;0 48 hn Check 'reservation
V-9 4 ��/, K.-f W) 72,hr.,Check
—1
FECAL COLIFORM TEST
22nd edition Standard Methods 9221C E-2006(MPN)(Aqueous)
Presumptive Test
Fecal Coliform Test
MPN r, e,"I Co.] ifo.rmlg = 10 x WK index 100 ml NWN/g = 10 x -/ I- , g -
_5_
5,
largest volumeX % dry solids -tested L >eC). 6 D 5
,
Sterility C-antrni
Heterot,rophie,Plate Count
IO.mL
1 mL
0.3 mL
0.01 mL
Dilution Water Blank
Standard Methods.A ar
Dilution Water Blank
Quality Control Tubbs
Double Strength.(2Sj Control
Single Str.englh (SS Control
EC Broth Control
Revised 2-28-13

Sampled. By
Received By
knalyzed By
Calculated By
Recorded By
Cliqcl.ced By
Temp 311T,
E DATE/TLWE, Oc
C
adS Samplq,Location
it 9!'CO�IK 24.br.Check .)1-1j-1.-J11. 7AMSample: Type: Grab 'x Composite
&W- 48hr.Check )-/Y-IYAO:-SVPreservation jKef-vU---j
72 hr. Check
22nd.edition. Standard Metbods,n2l C
mL Sample 0.601 0.00.01 0.00001 6.' 000001 0.0000001 1 0.00000001 1 MPN I
NON Fecal Coliform/g 10 x AIIPN index /100, ml
largest volume..X % dry:solids tested
Fecal-Coliform Test
11111111171 �1�
I - I , -�?
WNIg =1 10, x
Sterilitv Control I
DID q
Heterotrophic Plate Count
.10 WIL
1 mL
0.1 mL
0.01 mt
Dilution WaterElank
Standard Methods Agar
Dilation 'Water Blank
Quality Control Tubes
Double Strength (DS) Control
Single Strength (SS) -Control
ECBroth Control
Revised,2-28-13

Sampled By
Recelyed By
Analyzed By
Calculated By
Recorded - -By
'heeked-By
mL
48 hours
mL'S4mp]
24 hours
Temp 367. cc
DATE I TIME � r C
/'A/ Sample Location
I.IA 9K-! K 24.hr..Check 11-13-IY' W-11ftIT\. Sampiplypp: Grab x COMP010#
V&4 'c' MI 48hr. jQheek.) -I.V-I1:006MPreservation
I q.-f �j 72hr. Check I -If
FECAL COLIFORM TEST
22n0 edition ion Standard A leffiod s' 9121
-
Presuup'tive, Test
0.'001 0.0001 0.00001 O-POOOK
LfL
Fecal Coliform Test
4PN Fecal Coliform/g = 10 x MPN index / 100 ml MTN-lg = 10 x /- i '� = - - I -� — - � E I � Me
largest volume X %,dry. solids tested X
R.
Sterility Cnntrni
Heterotropliic,Plate Count
1.0 mL.
1 mL
0.1 mL
0.01 mL.
DIN tion Water Blank
Standard Methods Agar
Dilution Water Blank
Quality Control -Tubes
Double.Strenlph DS) Control
Single Strength (SS) Control
EC Broth Contro I
'evised 2-28-13

CITY OF WASHINGTON
SLUDGE
20th edition Standard. Methods 2.540 GA 99.7(Aqueous)
Daterri.mip
Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked, By
qp AA
Time, Water Bath 9i'l 0.
Time. in Oven I I 13 O'A K
Tme out.of Oven III � PN
The. Weighed 3 ! 9-q P tv-,,
Sam ple4
Eva p Dish #
Wet Weight+
Dish. Wei ght
Dish Weight
Wet Wei2ht .
Pry. Weight +
Dish Weight
Dish ,Wei ght
Dry Weight
% Dry Solids
130 q6g 1.30,
Z4q-4
&.0,10-.1915,
go, 9419d
A,09-6c!5
4, 51
6
a9 96a
11-6
77 7. SC I
allo6g8j5
Ll., to
Revised 6-9-44

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked. By
CITY OF %SHIN.GTON
SLUDGE
20th edition Standard Methods.2540 G-1997{-Aqpoo.qs)
lik,hy' ?'.-oS,fw
Time. on,Water Bath Toopm
A Time inOven -1 U. 304M
Time, out of Oven f,'fS PM
-
I 6-t/44 3i4itt Time Weighed 1'012*
Sample #
Eva p Dish #
Wet.Wellght:+
Dish Weight
Dish Wei ght.
Wet, Wei qht
Dry Weight +
Dish Weight
Dish Weiqht
Dry Wpight
0/b,Dry..Solids
2-
136, L40
26,35121-2
A 0 A -
Revised 6-9A4

Sampled By
Received By
,Analyzed By
Calculated By
Recorded By
Checked By
CITY OF. WASHINGTON
SLUDGE
2.0th- edition Standard. Methods. 254.0. Gl 997(Aqueous
Date/T'ime
�A //9' K. 10 A'4
hn-
. Sf.,Prn
. ptl\
it w
Time on, Water Bath 44#41\;
TimelnOven 11110fil'A
Time out of Oven. V I SPA
Time Weighed 32DIPA4,
Sample #
Eva p Qish.#
Wet Weight +
Dish Weight
Dish Weight
Wet Weight
Dry ,Weight +
Dish , Weight
Dish Wei ght
Dry., Weight
Dry Solids
11 q.,6 a 73o
PlS4R 5
30.L41 a-U-
-11, 1290
6 21.1314U431L4,05-
..k7
Revised 6-9-14

i
' CITY OF WASHINGTON
SLUDGE
20th .edition Standard Methods 254.0 G-1997(Aqueous)
a Pate/Time
Sampled By
Received By 11 ll,� 1-14, t, Time on Vitater-`Bath 24S A
Analyzed, ,By Time in Oven 1 r 11 pot
Calculated BY 1.1 I2. (4u41P& f.0vTie out on 31.3 Inc
Recorded By aW 1.4.1 4I k IPAlk Time Weighed !4 , 314' om
Checked By
Sample #
Eva Dish. #
Wet Weight +
Dish Weight.
Dish Weight
Wet Weight ht
Dry Weight +
Dish -Wei ht
Dish. Wei ht
Dr . Wei ht
% Qq Solids
l3 �32C1
�'j . 3 90 .
I. H'�U,
29X055
240311b.
Revised 6-9-14

Sampled By
Received By
Analyzed By
Calculated By
Recorded By
Checked By
J
CITY OF WASKNOTON
SLUDGE
-20th edition Standard. Mpthods.25.40 Q--1-997(Aqpeow.s,)
Dat M e.
51A UAM
Ii 1112t1w, q'j -571 Apt
J
Time onWater Bath 1-010.3&K
Time. in: Oven VA, I'IPtvx
Time outof.Oven 1.1 -114hLi., a"foo-
Time..Wei ghed _ It 1 /W/�-­9 to
Sam ple*
Evolj Dish #
Wet: Weight
Dish Wei - ght
Dish Weight
Wet Weight
Dry Weight.-+
Dish `W.61ght
Dish Wei 2ht
Dry Weight
% DSolids
ry
5'5
13- 0 �-Q-
9 9 37'1
-5 as
11 Ila
I. 2`29q.
3195,
Revised 6-9-14

Sampled By
Received By
Analyzed,,py
Calculated 'BY
Recorded By
0 , hecked By
QITY OF VVA T(i1 --- - -----
SLUDGE
20th edition, Standard Methods 2540 G-1997(Aqueous)
-rimp on Water bath., I (Xra�
Time in Oven I f`7 Pm
Tlme:Qut:of Oven .1, '60kq
I 1/311qj'
J#
Time .Weighed 17, 1
,;S-ample #
Eva p Dish.# .—Dish-Weight
Wet Weight +
Dish Weight
Wet Weiht
Dry Weight +
Dish Might
Di6h Wei ght
p Vlleic iht;
/6 Dry, Solids.
Revised 6-9-14.

- -' --ti - - _ - -
{ CITY ' OF .WASH I NGTON
SLUDGE
20th edition. Standard Methods 2540. G 4997(Aqueous)
Sampled By -
11. / �' 30 k<<
Received B
1 h , $�5QA�
�f
Anal zed B
Y Y
i .%1�f, I� U' f3; in
Calculated., By
'�-if � 1 i. Jl f ►i"i,t1 °fff IN.
RecaCded. By
a�. ll� �iU�G�t.��.
Cheeped _By
Time.on Water Bath, I0,'J_6:PL
Time in Oven , 1'7 PES
Tim e`o otf v n ` " i 1t/t•3 t4 $�'p�
Time igVpighed. I iLt. l't 43 IG�G'S nit
Sam left
-Evap Dish #,
Wet Weight +
Dish Wei I�t.
Dish Weight
Wet Weight
Dry Weight
Dish Weight
Dish Weight
D °.Wei ht.
-%:-Diy Solids
0,
.-WVV
1. 1���'. :I'
L � Q
V
- �'�'
3 q CI
Revised 6-9;-14

of
Report Number: 14-323-0729 v
Account Number:46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE NC 27028
Date Received: 11/19/2014
AFL
wwwaleastem.com
A&L.-_Eastern _Laboratoies
7641 WhitepineRoad Richmond, Viigiieia 23237 (804)- 743-9401 Fax`(804) 271-.W6,
Grower:
HARVEY WILLIAMSON Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Analysis: 11/20/2014 Date Of Report: 11/20/2014
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds peracre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: m� G0r
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble L6
Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary

i>3<C;� _ _ _)not, -- ivisi� � ! �e: I _ i'33-r_ . �.. � . — �lebsia � . �'rww ,..�
_ _ '.gov�._ 'hom � r.� _
r rt Ni
t;J TJkj.'i14
Predictive
Client: Will Congleton
c/o Congleton Farms
Advisor:
EMA Resources, Inc.
755 Yadkinville Rd
PO Box 205
Mocksville, NC 27028
` } Soil Report
Mehlich-3 Extraction
stokes, NC 27884
�rk�y'FyyS,_
Sampled County: Pitt
Sampled: Received:
11/19/2014 Completed: 12/24/2014
Farm: NC-PI-201
Links to Helpful Information
Sample ID: 00010
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P205
K20 Mg S
Mn Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.5 80-100 0
20 0 0
0 0
0
0
Note: 3
2-
Test Results [units - WN in g/cO; CEC and Na in meq/100
crri3; NO3-N in mg/dnr3]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.71 1.19 6.7 83 1.2 5.6
75 67 70 8
70 64 48
87 87
90
0.1 1
Sample ID: 00012
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P205
K20 Mg S
Mn Zn
Cu
B
Information
Lime History:
1 -Small Grain (SG)
0.0 80-100 0
0 0 0
0 0
0
0
Note: 3
2-
Test Results [units - WN in g/crrf; CEC and Na in meq/100
crrr3; NO3-N in mg/dO]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-1 Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I
Na ESP SS-1 NO3-N
1.49 1.16 10.3 91 0.9 6.2
93 91 67 20
132 44 34
48 48
63
0.1 1
North Carolina
1*xcko Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

11 ,1 of
Report Number: 14-323-0715
Account Number: 46245
Send To: EMA RESOURCES INC
755 YADKINVILLE RD
MOCKSVILLE NC 27028
A&L-.Ea.stem,,L,abor*at.o,rie,s
7621 Whitepine Road Richmond; Vitgioia 23237 [phone] Faz_(804) 27116446
Grower:
WILL CONGLETON Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Received: 11/19/2014 Date Of Analysis: 11/20/2014 Date Of Report: 11/20/2014
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by. ?4�io OF 6�
C.E.C. - Cation Exchange Capacity. Salts ms/em x 640 = ppm. Analysis prepared by: A&L Eastern Laboratories, Inc.
Pauric McGroary