WQ0000783_Residual Annual Report 2014_20150302

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Jikr 'S- i �,..g�°RijA i air 3 � ' ;4j1 �w s
3868 Business 17
P.O. Box 8
Bolivia, NC 28422
1-910-253-4689
February 25, 2015
N.C. Dept of Environment and Natural Resources
Division of Water Resources
Water Quality Permit Section
Non-Discharge Permitting Unit
512 N. Salisbury St.
Raleigh, NC 27604
Dear Sir/Madam
•
S&B Maintenance, LLC is sending in the required forms for our DWQ permit for this past
year. This report is for the land application of residuals for the reporting year of 2014. If
you have questions or need more information you can reach the office at the provided
phone number.
RECEIVED/DENR/DINR
Sincerely, MAR - 2 2015
"matting sec n
Sammy P Carteret

'' *Q erniit#: WQ0000783 County: Brunswick Year: 2014
Facility Name(as shown on permit): S&B Maintenance
Land Application Operator: Sammy P Carteret Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
El Yes 0 No -If No,skip Part A,and Part B and proceed to Part C. Also,If residuals were
generated but not land applied,please attach an explanation on how the residuals were handled.
Part A-Residuals Application Summary:
Total number of application fields in the permit:
Total number of fields utilized for land application during the year:[
Total amount of dry tons applied during the year for all application sites:
Total number of acres utilizes for land application during the year:
Part B-Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below)issued by the Division of Water Resources. El Yes ® No
If no please,provide a written description why the facility was not compliant,the dates,and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied(if needed)to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three(3)copies of
laboratory results are attached.
4) Annual TCLP analysis(if required)was performed and three(3)copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three(3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1105(a)or the Pollutant Loading
Rates in 15A NCAC 02T.1105(b)(applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with(applicable to 40 CFR Part 503
regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with(applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or,in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals,as specified in
the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C-Certification:
"I certify,under penalty of law,that the above information is,to the best of my knowledge and belief,true,accurate,
and complete.I am aware that there are significant penalties for submitting false informatio including the possibility
of fines and imprisonment for knowing violations."
Sammy P Carteret/Operator a)-/b
Permittee Name Titl 9(type or print) Signa of Permittee • Date
Co6e,...__ (2-257-47 5„ __),m.a__,,,lc.L.5-.
Signa a eparer* Date ignature of Land Applier Date
(if differ t from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 02T.1102(26)
DENR FORM ACF(12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF- B
WQ Permit Number: WQ0000783 Laboratory: 1) Envirochem Chemist
Facility Name: S&B Maintenance 2)
Residual Source WQ#or WQ0005790 3)
NPDES#: 4)
WWTP Name: Oak island WWTP 5)
Residual Analysis Data
Ceiling Sample or Composite Date
Parameter Conc. 1-15-14
(mg/kg) Limit
Percent Solids (%) NA 0.77
Arsenic 75 11
Cadmium 85 11
Copper 4,300 586 _
Chromium NA 29.1
Lead- 840 20 _
Mercury _ 57 3.77 _
Molybdenum 75 _ 11
Nickel 420 29
Selenium 100 11
Zinc _ 7,500 1260 .
Total Phosphorus NA 5,100
TKN NA 12,000
Ammonia-Nitrogen NA 547
Nitrate and Nitrite NA 142
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system dI
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significan
penalties for su,a itti false information, including the possibility of fines and imprisonment for knowing violations."
%Rd, w _.,iloic
P-d5:1,5-
Signatur,'reparer* Date
*Preparer is defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
DENR FORM RSSF (12/2C1OM

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF- B
WQ Permit Number: WQ0000783 Laboratory: 1) Envirochem Chemist
. Facility Name: S&B Maintenance 2)
Residual Source WQ#or NC0007064 3)
NPDES#: 4)
WWTP Name: Duke Energy 5)
Residual Analysis Data
Ceiling Sample or Composite Date
Parameter Conc.
(mg/kg) Limit 1-2-14
Percent Solids (%) NA 1.08
Arsenic 75 8
Cadmium 85 8
Copper 4,300 162 _
Chromium NA 0
Lead 840 8
Mercury 57 0.37 _
Molybdenum 75 8
Nickel 420 15.3
Selenium 100 8
Zinc 7,500 823
Total Phosphorus NA 19,300 _
TKN NA 88,500
Ammonia-Nitrogen NA 3 840
Nitrate and Nitrite NA 52.7
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system di
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significan
pen lti s for sub ein_ false 'nformation, including the possibility of fines and imprisonment for knowing violations."
�� ' -o?5:,T
ik Signature o parer* Date
*Preparer defined in 40 CFR Part 503.9(r)and 15A NCAC 2T.1102(26)
namo =rionn Dec= /a)/)nna\

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance Total Dry Tons Applied(Annual): 3:90
Permit#: WQ0000783 Cation Exchange Capacity(non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret Predominant Soil Series: Baymeade
Acres Used: 17.2 Acres Permitted: 17.2 Site#: Field#: 1A
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample 1 2 3 4 5 6 7 8 9 10 11 12
or Com-
posite
Date 1/2/14 1/2/14 1/15/14 1/2/14 1/2/14
%Solids 1.08 1.08 0.77 1.08 1.08
Arsenic 8 8 11 8 8
Cadmium 8 8 11 8 8
Copper 162 162 586 162 162
Chromium 0 0 29.1 0 0
Lead 8 8 20 8 8
Mercury 0.37 0.37 3.77 0.37 0.37
Molyb- 8 8 11 8 8
demon
Nickel 15.3 15.3 29 15.3 15.3
Selenium 8 8 11 8 8
Zinc 823 823 1260 823 823
Total
Phos- 19,300 19,300 5100 19,300 19,300
chorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1 2 3 4 5 6 7 8 9 10f 11 12
DT/Ac./ 0
App.
Event 0.02 0.02 0.16 0.02 0.02
J
Arsenic '0:000 0:000 0.00.4; th000; ' 0:000 =0.000 ` `0.000 0..000, 0.000 0:000 0.000' ,:0.000 0.005.
Cadmium 0000 0:000 ''0.004 10.000; 0.000. 0.000 „0.000 ,0:000` 0.000 0,000 0:000 0 000
Copper 0:0.05 `,<<0.005. . 0:191'' 0:005 0:005 . .',0.000 ,0:000 '.0 000.: 0:000.'. 0:000 ,0:000" "0 000`': .0.212-
Chromium 0 000 , _0.000`, 0.009 0:000. 0.000' _ 0.000. 0:000 ' 0.000.�° . 0:000 0:000 0:000
Lead 0:000 :.,:0".000;. 0 007; 0.000' 0.000 :;01000. 0000 0000 '0:000 0:000' 0:000 ;..0.000 0.008 •
Mercury ',0000:°- -0.0:00 : .'0 001. 0:000 0.000 ' ,0.000' "0000 0.000';: 0:000 .0:000 0:000- „:0 000 0.001
Molyb- 0:000 ` .0:0;00 . 0 004: . 0.000 .;0:000 0.000 0.000 • 0:000 0.000 0.000. 0:000 ,0.000 ' 0 005',
denuxn _ =
Nickel °0:000, "0.000'. .:0:009° 0.000 , 0 000. ,0.000 s. .0.000 0.000 "0.000 0.0:00: ;0:000: f.0 0hL
Selenium ' 0:000 0 000'; 0 004: _ 0:000 0:000 0.000;` 0:000 : ,.0 000.; ``0,000 0.000 0:000; 0 000,..:0.04:
Zinc :0.026 0.026. '0;41'1 0,026 0026 r '0.000' :0.000 0.000' " 0.000 0.000Y 0.000,-,=0 000`. :0.516;:
Total 5
Phos- 0:618_ :0.618 .1:663 0:618,. 0.618- O:d00'. 0::000' 0:000. 0.000 0.000 0.000.
phorus
"I certify,under penalty o'law,that this document was prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted.I am
aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonme t for knowing viol Lions".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

'`Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance,LLC Total Dry Tons Applied(Annual): 4.20
Permit#: WQ0000783 Cation Exchange Capacity(non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret Predominant Soil Series: Baymeade
Acres Used: 19.8 Acres Permitted: 19.8 Site#: Field#: 1D
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/lig, % Solids use Raw Percent#):
Sample or: 1 2 3 , 4 5 6 7 , 8 9 10 ,11 12
Com-
posite
Date 1/2/14 1/15/14
%Solids 1.08 0.77
Arsenic 8 11
Cadmium 8 11
Copper 162 586
Chromium 0 29.1
Lead 8 11
Mercury 0.37 3.77
Molyb- 8 11
denim
Nickel 15.3 29
Selenium 8 11
Zinc 823 1260
Total
Phos- 19,300 5,100
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total 1 2 4 5 -di- 7 8 9 '10 111 12
DT/Ac./
App.
Event 0.02 0.20
Arsenic 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Cadmium 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Copper 0.005 0.230 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.235
Chromium 0.000 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011
Lead 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Mercury 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Molyb- 0.000 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
denum
Nickel 0.000 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012
Selenium 0.000 0.004 , 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005
Zinc 0.026 0.494 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.520
Total
Phos- 0.618 1.999 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.617
phorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowi 'olations".
a2.3^-/ Y
Signature of Land App ier Date DENR FORM MFLSF(12/2006)

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance Total Dry Tons Applied(Annual): 5.88
Permit#: WQ0000783 Cation Exchange Capacity(non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret Predominant Soil Series: Baymeade
Acres Used: 10.07 Acres Permitted: 10.07 Site#: Field#: 2A
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 i ; 3 4 = 5 j 6 7i '8 9 10 11 1 i
Com-
posite
Date 1/15/14 1/15/14
%Solids 0.77 0.77
Arsenic 11 11
Cadmium 11 11
Copper 586 586
Chromium 29.1 29.1
Lead 20 20
Mercury 3.77 3.77
Molyb- 11 11
dennm
Nickel 29 29
Selenium 11 11
Zinc 1260 1260
Total
Phos- 5100 5100
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total jj L2] 3 4 5 Al7] 8 10 11 j y
DT/Ac./
App.
Event 0.31 0.28
Arsenic 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Cadmium 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Copper 0.357 0.327 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.684
Chromium 0.018 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034
Lead 0.012 0.011 0.000 0.000 0.000 ` 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023
Mercury 0.002 0.002 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.004
Molyb- 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
dPlilim -
Nickel 0.018 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034
Selenium 0.007 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013
Zinc 0.769 0.703 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.472
Total
Phos- 3.111 2.846 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.957
horns
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowing violations".
Signature of Land App ter Date DENR FORM MFLSF(12/2006)

"Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance,LLC Total Dry Tons Applied(Annual): 1.59
Permit#: WQ0000783 Cation Exchange Capacity(non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret Predominant Soil Series: Baymeade
Acres Used: 20.92 Acres Permitted: 20.92 Site#: Field#: 2B
Residual Analysis Data(Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or 1 2 3 • 4 5 6 7 8 9 10 11 12
Com-
posite
Date 1/2/14 1/2/14 1/2/14 1/2/14 1/2/14 1/2/14
%Solids 1.08 1.08 1.08 1.08 1.08 1.08
Arsenic 8 8 8 8 8 8
Cadmium 8 8 8 8 8 8
Copper 162 162 162 162 162 162
Chromium 0 0 0 0 0 0
Lead 8 8 8 8 8 8
Mercury 0.37 0.37 0.37 0.37 0.37 0.37
Molyb- 8 8 8 8 8 8
clemim
Nickel 15.3 15.3 15.3 15.3 15.3 15.3
Selenium 8 8 8 8 8 8
Zinc 823 823 823 823 823 823
Total
Phos- 19,300 19,300 19,300. 19,300 19,300 19,300
phorus
Annual Heavy Metal Field Loadings (Calculated in lies/acre):
Total jj. 2 3 5_1 _6 7 8 9 10 11 12
DT/Ac./ y,
App. -� y
Event 0.01 0.01 0.01 0.02 0.01 0.01
Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Copper 0.004 0.003 0.003 0.006 0.004 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.025
Chromium 0.000 0.000 0.000 0.000 0.000 0..000 0.000 0.000 0.000 0.000 , 0.000 0.000 0.000
Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.001
Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000
Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
1ennm
Nickel 0.000 0.000 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Selenium 0.000 0.000 0.000 0.000 . 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001
Zinc 0.021 0.016 0.016 0.028 0.021 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.125
Total
Phos- 0.502 0.386 0.386 0.656 0.502 0.502 0.000 0.000 0.000 0.000 0.000 0.000 2.934
phorus -
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonm t for knowing eons".
P-0/.5 V,,5-
Signature of Land tier Date DENR FORM MFLSF(12/2006)

' 'Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: S&B Maintenance Total Dry Tons Applied(Annual): 3.62
Permit#: WQ0000783 Cation Exchange Capacity(non 503 only):
Operator: Sammy P Carteret Owner: Sammy P Carteret Predominant Soil Series: Baymeade
Acres Used: 10.87 Acres Permitted: 10.87 Site#: Field#: 2C
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent#):
Sample or i� 3 4 ; 5 Ai 7 8 ; 9 j 10 I 11 j 12
Com-
posite
Date 1/2/14 1/15/14 1/2/14 1/2/14 1/2/14
%Solids 1.08 0.77 1.08 1.08 1.08
Arsenic 8 11 8 8 8 _
Cadmium 8 11 8 8 8
Copper 162 586 162 162 162
Chromium 0 29.1 0 0 0
Lead 8 11 8 8 8
Mercury 0.37 3.77 0.37 0.37 0.37
Molyb- 8 11 8 8 8
denim
Nickel 15.3 29 15.3 15.3 15.3
Selenium 8 11 8 8 8
Zinc 823 1260 823 823 823
-
Total
Phos- 19,300 5,100 19,300 19,300 19,300
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total _11 3 L 5i jj 2j A 10 j Ill lj 12
©
.4.
su
Event 0.03 0.24 0.02 0.02 0.03
Arsenic 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Cadmium0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.000 0.007
Copper 0.008 0.280 0.007 0.007 0.008 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.311
Chromi • 0.000 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014
Lead 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Mercury 0.000 0.002 0.000 0.000 0.000 . 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002
Molyb- 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007
Nickel 0.001 0.014 0.001 0.001 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017
Selenium 0.000 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007_
Zinc 0.041 0.602 0.036 0.036 0.041 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.757
Phos-Total
0.965 2.438 0.849 0.849 0.965 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.066
shorus
"I certify,under penalty of law,that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information,including the possibility of fines and
imprisonment for knowin 'olations".
..4.._ ,/,4,1_,...„1
5-0- 02,-00-3/5-
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance WQ Permit#: WQ0000783 Field#: 1A Acres Utilized: 17.2
Land Owner: Sammy P Carteret Annual Dry Tons Applied: 3.890.4; - : Site#: Acres Permitted: 17.2
Operator: Sammy P Carteret Predominant Soil Series: Baymeade Cation Exchange Capacity(non 503):
Crop 1 Name: Bermuda Hay Crop 1 Max.PAN: 300 Crop 2 Name: Winter Rye Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. a o p Z Y Nitrate Name of Crop Type
a b El PAN Applied
5 , % Cond. Past 24 E. w i7, V A TKN �o B and lbs/acre Receiving Residual
(enter one)Solids/ Applied per (NPDES#,WQ#,
.I gl (Dry, o' o 6 ( )
i Liquid Solids Acre Fert.,Animal Wet, Hrs. °a * op �• Nitrite Application
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) inches p o * &' mg/kg mg/kg mg/kg Crop1 Crop2 Crop1 Crop2
Moist)
0 9 9 9 9 9 9
April 6,000 1.08 :-0,016 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 :0.860;.- „0.860
Vlay 6;000 1.08 _'0.016, . - NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 -..0;860..- :0 860
lune 87,500 0.77 =0:163. WQ0005790 Dry 0 S 0.5 0.3 12,000 547 142 _ 1.258'-- - 1.258 •
:,tober 6,000 1,08 °0:0.16- NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0:860; __ 0.860.•"
;ember 6,000 1.08 0.016 ' NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 =';,0.860' -.0;860:
0.000 - 0000' : 0.Q00'...
- -0.000. ` 0,000 '0:000 -
0.000 'O.o0o__ -0:000
o.000- . o.000- ,o.000
- -0:oo0- . • .0',00o:" 0,000.
- ;`"0:000. - ."0:00.0` `-0,000 _
0:000 .- 0.000'-' : 0,000
- .._ Residuals Applications totals on FORM FSF suppattach FORM FSF suppto this form): . .
PP ( ) ._
: 4: 98.: 4:698:. ' Lime Applied
���� �o ':" 11.1500 ` > <'' As Cd Cu Cr Pb HgMo Ni Se Zn P G. ., , - pp
mual lbs/acre . -0.005' ' - 0:005" -.0:212', `:0:009 _ .0:008.- b,001 : :0 005'__ 0.01.1 -.0.005 0,51;6 .-4-,133 ':: .«;.'•: :.::: ; •. ; Date lbs/ac
+ + +
70 -01 28.10015 0 1.44E 01 5.51E-02 1.29E 00 2.92E 00 4.62E-01 56.4753 « 's:'?:"< :>:?<�>>'.>> °;> `.` :<.>,
ior Years Cumulative lbs/ac 7.89E-01 s. E
. - 1`2- 2. �30- 0,467 5 1-. :? >: :: r< >'>:>:<><: .>>: :;.::: >
arrent Cumulative lbs/ac .0:794 _ 0.874 28,3�12 0:009 14.451- 0.056: . 96 9 6 99 , ,,
�i
15 NA 374 89
i C. P L. R.
36 34 1338 NA 2672498
;rm tted
2nd Cro -300 -rm i PAN Limit 1st/ 50-t
certify, under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
talified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation including the poss. ility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
a OS�J **Volatilization Rate: Surface-05 InJection/Incorporation-fl0
Signature of Land Applier Date
*** Mineralization Rates: Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3, raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
•
DENR FORM FSF(19/9nnR)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance WQ Permit#: WQ0000783 Field#: 1D Acres Utilized: 19.8
Land Owner: Sammy P Carteret Annual Dry Tons Applied: 3.6417 Site#: Acres Permitted: 19.8
Operator: Sammy P Carteret Predominant Soil Series: Baymeade Cation Exchange Capacity(non 503):
Crop 1 Name: Coastal Bermuda Crop 1 Max.PAN: 300 Crop 2 Name: Winter Rye Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. Y o Z Nitrate Name of Crop Type
5 (enterone) % Appliedper (NPDES#,WQ#, Cond. c b m • 0 PAN Applied
Solids/ Past 24 co TKN o and Receiving Residual
o (Dry, o ; - �'• = (lbs/acre)
Liquid Solids Acre Pert.,Animal Wet, Hrs. a if c �. Nitrite Application
Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches * -
Cu. # p mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
larch 6,000 1.08 0.014 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.747 0.747
vember 105,000 0.77 0.170 WQ0005790 Dry 0 S 0.5 0.3 12,000 547 142 1.312 ' 1.312
0.000 0.000 0.000 l'
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 _ 0.000
0.000 0.000 0.000'
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
;_ •° Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): K`
iTALS: 01 : 111000 wr As Cd Cu Cr Pb Hg Mo Ni Se Zn P 2.059 12.059 Lime Applied
nnual lbs/acre 0.005 '0.005 0.235 0:011 `0.005 0.001 0.005 0Al2 0.005 0.520 2.617 ': Date lbs/ac
ior Years Cumulative lbs/ac 7.78E-01 1.08E+00 32.20292 0.000482 2.77E+01 1.14E-01 1.25E+00 4 58E+00 5.85E-01 61.7247,;' .�`--- _ -..
anent Cumulative lbs/ac 0.783 1.081 32.438 0.012 27.740 0.116 1.251 4.589 0.589 62.245 -/-: p:. :� ' ,-�;- �. ��-` >:°�
;rmitted C.P.L.R.**** 36 34 1338 NA 267 15 NA 374 89 2498
,rmit PAN Limit 1 st/2nd Crop I , , .. . .. 300 50
:certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ialified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
[formation,including the ibility of fines and imprisonment for knowing violations."
‘,{ 5_ j *Application Method:S-Surface,IN-Injection,INC-Incorporation
*J2//
n **Volatilization Rate: Surface-0.5,Iniection/Incornoration-1.0
Signature of Land Applier Date '**Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
r1rM P rnp0n Cec/4o/onnc%

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS ':LANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance WQ Permit#: WQ0000783 Field#: 2A Acres Utilized: 10,07
Land Owner: Sammy P Carteret Annual Dry Tons Applied: 5:8759 Site#: Acres Permitted: 10.07
Operator: Sammy P Carteret Predominant Soil Series: Baymeade Cation Exchange Capacity(non 503):
Crop 1 Name: Coastal Bermuda Crop 1 Max,PAN: 300 Crop 2 Name: Winter Rye Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. Y c Z• Y Nitrate Name of Crop Type
PAN Applied
5 Y (enter one)Solids/ % Applied per (NPDES#,WQ# Cond. Past 24 ' ,?,',I 'a, w 5TKN o and Receiving Residual
o Liquid Solids Acre Fert.,Animal (Dry, Hrs. c. a V # N Nitrite (ibs/acre) Application
lit
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches # e °� # g mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
bruary 95,500 0.77 0.305 WQ0005790 Dry 0 S 0.5 0.3 12,000 547 142 2.346 ` 2.346
ugust 87,500 0.77 0.279 WQ0005790 Dry 0 S 0.5 0.3 12,000 547 142 2.149 2.149 --
0.000 0.000 0:000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 , 0.000.` 0.000
0.000. , J MOO 0.000
0.000 MOO _ 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000.
iTALS: 0 183000 As Cdduals Cu licatioCnY totals Pb FORM FSF supp
Ni Se p P 4: '
L Applications pp(attach FORM FSF sup to this form): 6
- g _ .-M __ Zn 495 4.495 Lime Applied
nnual lbs/acre 0.013 ,0.013 0.715- 0.036 0.024- 0.005 0.013 0.035 0.013 ' 1.53'7 ' 6.222 .. Date lbs/ac
for Years Cumulative lbs/ac 2.12E-01 1.32E-01 4.128594 0.022376 4.67E+00 1.57E-02 1.06E-01 4.22E-01 6.54E-02 11.84107 - - .
.irrent Cumulative lbs/ac 0.225 0.146 4.844 0.058 4.694 0.020 0.119 0.458` 0.079 13.378 ' .
:rmitted C.P.L.R.**** 36 34 1338 NA 267 15 NA 374 89 2498
rmit PAN Limit lst/2nd Crop e` - 300 50
certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ialifiied personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation including the p ibility of fines and imprisonment for knowing violations."
*Application Method: S-Surface,IN-Injection,INC-Incorporation
- �/� **Volatilization Rate: Surface-0.5.Iniection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L,R.: Cumulative Pollutant Loading Rate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance WQ Permit#: WQ0000783 Field#: 2B Acres Utilized: 20.92
Land Owner: Sammy P Carteret Annual Dry Tons Applied: 1.5763 Site#: Acres Permitted: 20.92
Operator: Sammy P Carteret Predominant Soil Series: Baymeade . Cation Exchange Capacity(non 503):
Crop 1 Name: Coastal Bermuda Crop 1 Max.PAN: 300 Crop 2 Name: Winter Rye Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. b o Z 1 Nitrate Name of Crop Type
(enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 b �' �; -� PAN Applied
TKN o and ReceivingResidual
ri cc e+ lbs/acre
! i Liquid Solids Acre Pert.,Animal (Dry' Hrs. a N a, Nitrite ( ) Application
Wet, to
* p iF
Cu.Yds Gallons (Dry Tons/Ac) Waste,etc) Moist) inches 0 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
bruary 6,000 1.08 0.013_ NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.107 0.707
vlarch 4,500 1.08 0.010 NC0007064 _ Dry 0 S 0.5 0.3 88,500 3840 52.7 0.530 0.530
-
vlarch 4,500 1.08 0.010 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.530 0.530 _
vlarch 8,000 1.08 0.017 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.943 0.943
April 6,000 1.08 0.013 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.707 0.707
April 6,000 1.08 0.013 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 0.707 _ 0.707
0.000 0.000 0. 00
0.000 _ 0.000 0.000
0.000 _ 0.000 0.000
0.000 0.000 0:000
0.000 _ 0.000 -0.000
0.000 0.000 0.000
'-. - Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): f'_ -
)TALS: 0 35000 `-; As Cd Cu Cr Pb Hg,_ Mo Ni Se Zn P 4.125 : 4.125 Lime Applied ,v
nnual lbs/acre 0.001 0.001 0.025 0.000 0.001 0:000• 0.001 0.002 0.001 0.125 2.934 ': . ".'_'.=, °=' Date lbs/ac
nor Years Cumulative lbs/ac 6.50E-02 6.31E-02 2.554016 0.006025 1.18E+00 8.25E-03 1.15E-01 2,01E-01 1.07E+00 9.28757 4'6'k tl
urrent Cumulative lbs/ac 0.066 0:064 2.579 0,006 1.185 0.008 0.116 0.204 1.075 9.413
armitted C.P.L.R.**** 36 34 1338 NA 267 15 NA 374 89 2498
unit PAN Limit 1 st/2nd Crop _ ;1;:,--',--, -,:,, , . . . . ., 300 50
[certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
aalified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
tformation,includin possibility of fines and imprisonment for knowing violations."
GI.-a S r/5 *Application Method: S-Surface,IN-Injection,INC-incorporation
;0‘..........,
**Volatilization Rate:Surface-0.5,Iniection/Incorporation-1.0
Signature of Land Applier Date ***Mineralization Rates:Compost-0.1,anaerobially digested-0.2,
aerobically digested-0.3,raw sludge-0.4
****C.P.L.R.: Cumulative Pollutant Loadino Rate
IIFNR MPI14 FP'(19I9nnnI

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS ; LANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A"N/A"IN A .:•LANK OR BOX WHEN NOT APPLICABLE.
Facility Name: S&B Maintenance WQ Permit#: WQ0000783 Field#: 2C Acres Utilized: 10.87
Land Ow i er: Sammy P Carteret Annual Dry Tons Applied: 3.6276 Site#: Acres Permitted: 10.87
Operator: Sammy P Carteret Predominant Soil Series: Baymeade Cation Exchange Capacity(non 503):
Crop 1 Name: Coastal Bermuda Crop 1 Max.PAN: 300 Crop 2 Name: Winter Rye Crop 2 Max.PAN: 50
Volume applied Volume Residual Sources Soil Precip. , c 5 z Yg Nitrate PAN Applied
Name of Crop Type
5 (enter one)Solids/ % Applied per (NPDES#,WQ#, Cond. Past 24 '� r g w TKN R O and (lbs/acre) Receiving Residual
Liquid Solids Acre Fert.,Animal (D Hrs. a kt # Nitrite Application
Wet, Sy
* o
Cu.Yds GallonsTons/Ac) Waste,etc) Moist) mg/kg mg/kgCropCropCrop Crop
(Dry inches o o mg/kg m Ik 1 2 1
June 6,000 1.08 - 0.025 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 1.361 1.361
June 81,000 0.77 0.239 WQ0005790 _ Dry 0 S 0.5 0.3 12,000 547 _ 142 1.843 1.843
July 5,400 1.08 0.022 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 1.225 1.225
ugust 5,400 1.08 - 0.022 NC0007064 Dry 0 S 0.5 0.3 88,500 _ 3840 52.7 1.225 1.225
aember 6,000 1.08 0.025 NC0007064 Dry 0 S 0.5 0.3 88,500 3840 52.7 1.361 1.361 _
0:000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0:000 0.00.0
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0:000
Residuals Applications totals on FORM FSF supp(attach FORM FSF supp to this form): -
PTALS: 0 ,103800 ;: : As Cd Cu Cr Pb Jig Mo Ni Se Zn P :_7.014 7.014 Lime Applied
nnual lbs/acre 0.007 0.007 0.311 - 0.014 0:007 '0:002 0.007 0.017 0.007 0.757 :6.066 Date lbs/ac
ior Years Cumulative lbs/ac 1.67E-01 1.73E-01 9.722141 0 7.87E+00 1.29E-02 2.21E-01 7.98E-01 1.68E-01 16.68385
anent Cumulative lbs/ac 0.174 0.180 10.033 0.014 7.881 _ 0.015 0.228 0.815 0.175 17.441 „
;rmitted C.P.L.R.**** 36 34 1338 NA 267 15 NA 374 89 2498 - .
;rmit PAN Limit lst/2nd Crop - - a • -. „: 300 50
certify,under penalty of law,that this document was prepared under my direction or supervision in accordance with a system designed to assure that
ialified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
formation,including the po ibility of fines and imprisonment for knowing violations."
------ ®3 37 *Application Method: S-Surface,IN-Injection,INC-Incorporation
1f4c-N- L.-R-._. -'- _
**Volatilization Rate: Surface-0.5.Injection/Incorporation-1.0
*** Mineralization Rates:Compost-0,1,anaerobially digested-0.2,
Signature of Land Applier Date aerobically digested-0.3,raw sludge-0.4
****C.P.L.I2.:Cumulative Pollutant Loading Rate
nrn,n rannu. rnr i•n..+...+.,.

•
BSF Sewage Analysis for 2014
Sample 01/02/2014 Envirochem report#2014-00070
BSF Sewage Sludge Analysis Results Converted from ug/L to mg/L
Conversion Formula (ug/L) X(1 mg/1000 ug) = mg/L
Example Conversion: (4980 ug/L)X(1 mg/1000 ug)=4.98 mg/L
1 mg/kg = 1 ppm 1% = 10,000 ppm (used to convert rng/kg to%)
Test Performed Results
Aluminum 1490 mg/kg Organic Nitrogen 84660
Ammonia-N(dry-weight) 3840 mg/kg
Arsenic <8.70 mg/kg NH4% 0.384
Cadmium <8.70 ring/kg
Calcium 15500 mg/kg k 0.5
Copper 162 mg/kg
Lead <8.7 mg/kg NO3% 0.00527
Magnesium 2440 mg/kg
Mercury(dry weight) 0.37 mg/kg Organic Nitrogen% 8.466
Molybdenum <8.7 mg/kg
Nickel 15.3 mg/kg f 0.2
Nitrate-Nitrite(dry weight) 52.7 mg/kg
pH 50%Solution 6.94 S.U.
Phosphorus,Total (dry weight) 19300 mg/kg PAN 37.8094
Potassium 6370 mg/kg
Selenium <8.70 mg/kg
Sodium 18500 mg/kg
T.K9eldahl Nitrogen (dry wt) 88500 mg/kg
Zinc 823 mg/kg
Percent Dry Weight 1.08
Plant Available Nitrogen 37.8094 lbs/dry ton

Environmental Chemists, Inc.
enviro ehem 6602 Windmill Way • Wilmington,NC 28405
[phone](Lab) • [phone](Fax)
® 710 Bowsertown Road•Manteo,NC 27954
ANALYTICAL&CONSULTING [phone]
CHEMISTS NCDENR DWQ CERTIFICATE#94.DLS CERTIFICATE#37729
•
Town of Oak Island Date of Report: Feb 14,2014
4601 East Oak Island Drive Customer PO#:
Oak Island NC 28465 Report#: 2014-00636
Attention: David Kelly, II Report to: David Kelly, II
Project ID: Fish Factory VUWTP
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
14-01573 Site:Sludge 1/15/2014 10:45 AM Solid/Sludge Steve Poarch
Test Method Results Date Analyzed
Sludge Residuals
Aluminum EPA200.7 8230 mg/kg 02/04/2014
Arsenic EPA 200.7 <11.6 mg/kg 01/22/2014
Cadmium EPA 200.7 <11.6 mg/kg 01/22/2014
Calcium EPA200.7 92900 mg/kg 02/05/2014
Chromium EPA200.7 29.1 mg/kg 01/22/2014
Copper EPA 200.7 586 mg/kg 01/22/2014
Lead EPA 200.7 20.0 mg/kg 01/22/2014
Magnesium EPA 200.7 4690 mg/kg 02/05/2014
Molybdenum EPA200.7 <11.6 mg/kg 01/22J2014
Nickel EPA 200.7 29.0 mg/kg 01/22/2014
Potassium EPA 200.7 6960 mg/kg 02/06/2014
Selenium EPA 200.7 <11.6 mg/kg 01/22/2014
Sodium EPA 200.7 6790 mg/kg 02/05/2014
Zinc EPA 2007 1260 mg/kg 02/04/2014
Ammonia Nitrogen EPA350.1 547 mg/kg 02/10/2014
Total Kjeldahl Nitrogen(TKN) EPA 351.2 12000 mg/kg 01/27/2014
Nitrate+Nitrite-Nitrogen EPA 353.2 142 mg/kg 02/03/2014
Total Solids(%) SM 2540 B 0.77% 01/20/2014
pH SM 4500 H B 7.28 units 01/23/2014
Total Phosphorus SM 4500 P F 5100 mg/kg 01/28/2014
Mercury SW8467471B 3.77 mg/kg 01/17/2014
Comment: Results,except pH,reported on a dry weight basis. pH reported on an as received basis.
r
Reviewed by: P10. O r AP----
Report#:: 2014-00636 Pagel of1

eitVirechem ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington,NC2e405
" ..,J. OFFICE:910-3924223 FAX [phone]
Analytical&Consulting Chemists NCOENR:DWQ CERTIFICATION 9 94 NCDHHS:DLS CERTIFICATION*37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT:Town of Oak Island PROJECT NAME: tFtih W P' REPORT NO: /63(D'
ADDRESS:4601 East Oak Island Drive CONTACT NAME: David Kelly,II(Director) PO NO:
Oak Island,NC 28465 REPORT TO:Tray Bivins([e-mail] PHONEIFAX:201.8041f 278.7438
Permit#W00005790 _email:dkellyyci.oak-island.nc.us
►
Sampled Byk S 1-eue Z hCAr-- , SAMPLE TYPE I=Influent,E=Effluent,W=Well,ST=Stream,SO=Soil.SL=Sludge,Other:
Collection 4 g • PRESERVATION
Sample identification 5 4 1.k 1 i s i t m w i d s ANALYSIS REQUESTED
Date Time Temp = s u` , z
C P
''-~Eff aenr G , G X X ,
C P
—.Effluent— G G - . X
• C P
r G G
G G
F. 1-w+N i NIA- C , (E) {�
e R .
s_ 1,1
".�M. : uu.�. �1 ,u UGC ,-,5-�4 _o:�5 ' 5L � C� G 15-q3 � �1 v 9
C P
�. G G o X, X
C P
G G
•
C P
G G
C P
G G
C P
G G , _
LIMITS(daily)!B0D 15 mglL,NH3 5 mgtL,TSS 10 mgl.,Fecal 25 colonINt100 ml
Transfer iinquished By: DatelTime Received By: Date/Time
1. il:-- -sPtIke Ait"Ji\ NSW/A‘60
2,
Temperature when Received: Accepted: Rejec ample Requested•
/.~--" red By: Received By: pate: — ci Time:
diveents: TURNARO ND:

Annual Pathogen and Vector Attraction Reduction Form
Facility Name S&B Maintenance Permit Number WQ0000783
WWTP Name Town of Oak Island NPDES 0 WQ0005793
Monitoring Period: From_1 l 01 ! 14 - To 12 f 31 i 14 _
pathogen Reduction(40 CFR 503.32)-Please indicate level achieved and alternative performed.
Class A
Alternative 1 Alternative 2 Alternative.3
Alternative 4 Alternative 5 Alternative 6
Class B x
Alternative 1 Alternative 2 x Alternative 3
i If applicable to alternative performed(Class B only)indicate`Process to Significantly Reduce
Pathogens":
. Aerobic Digestion Air Drying Anaerobic Digestion
Composting x Lime Stabilization
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Atlaaable Level Pathogen Denasly Nrm6erer Requencyof Sample Analytical '
in Midge tetra Arnie Maximum Untts Errs Analysis Type Tedrnigue
Fecal 2 x 105 MPN per
Coliform gram of total
solklsor2xl13a CFO per per gram
ofWelsolids
1000 MPN per
gram eftalat
salad(dry
Salmoaef!a 3MPNper4
bacteria(i grams total said
lieu of� (&y weight)
Vector Attraction Reduction(40 CFR S03.33)-Please indicate option performed
Option 1 Option 2 Option 3 Option 4
Option 5 Option 6 x Option 7 Option 8
Option 9 Option 10 -
No vector attraction reduction options were perforated
Certification Statement(please check the appropriate statement) .
x „ `I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the
vector attraction reduction requirement in 40 CFR 503.33 have been met.`
I certify,under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in Oft CFR 503.33 have not been meta(Please note if you check this statement
attach an explanation why you have not met one or both ante requirements."
• "This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment"
x i)Vc+7. KaLY �- _ Ire.. YYit t01ty asrst,,k,1- „jaw_
Preparer Name and (type or print) Land A Name and e Of applicable)(type or print)
•, zsr-fc , d5-1,-nature of4": 1_,..--...____pi‘--
Date Signature of er applicable) Date
I

Annual Pathogen and Vector Attraction Reduction Form
Facility Name S&B Maintenance Permit Number CQ0000783
tltlt(FTP Name Duke Energy NPDES g NC0007064
Monitoring Period: From_'l f 01 1 14 To_12 l 31 / 14
Pathogen Reduction(40 CFR 503.32)-Please indicate level achieved and alternative performed.
Class A
Alternative# Alternative 2 Alternative 3
Alternative 4 Alternative 5 Alternative 6
Class B x
Alternative 1 Alternative 2 x Alternative 3
If applicable to alternative performed(Class B only)indicate Process to Significantly Reduce
Pathogens":
Aerobic Digestion Air Drying Anaerobic Digestion
Composting x Lime Stabilization
If applicable to alternative performed(Class A or Class B)complete the following monitoring data:
Parameter Allowable Level Pathogen Density Number of Frequency of Sample Analytical ,
in Sludge Minimum Average Maximum Units E ceedences Analysis Type Technique
Fecal 2 x 10a MPrd per
Calr:onn gram of total ,
gn(t1 or2x1QIx
CFtI per gram
of total solids
lCCO MPMI per
gram of total
= solid(dry
weight)
Salmonella i 3 MPN per 4
bac aria(in grams fatal solid
lieu f fecal (day weight)
coil orris)
V-ctor Attraction Reduction(40 CFR 503.33)-Please indicate option performed
Option 1 Option 2 Option 3 Option 4
Option 5 Option 6 ex O'ptian 7 Option 6
Option 9 Option 10
No vector attraction reduction options were performed
C rtification Statement(place check the appropriate statement)
"t certify under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the
ve •r attraction reduction requirement in 40 CFR 503.33 have been met:"
"I certify, under penalty of law,that the pathogen requirements in 40 CFR 503.32 and the vector
a rx -ctian reduction requirement in 40 CFR 503.33 have not been met"(Please note if you check this statement
att•ch an explanation why you have not met one or both of the requirements.")
is determination has been made under my direction and supervision in accordance with the system
d=�igned to ensure that qualified personnel properly gather and evaluate the information used to determine
th..tthe pathogen and vector dttidction reduction requirements have been met t am aware that there are
si.nificant penalties for false certification including fine and imprisonment."I '
x+H ,Cs 6, rvrA4-5. 5G.rwni `Y ctl'tw C wn�'
P -parer Name and Title(type or print) Land Ap lierdarme and T" a(if applicable)(type or print)
Si.nature of Preparer Date nature of Land Applier(if applicable)

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomcl Report No. FY15-SL020323
t�,,,,,, Client: Sam Carteret Advisor:
• a` `�',t Heavy Metals CIO S&B Maintenance
o i' :,y' 3579 Lewis Loop Rd.S.E.
>�',� �� d Mehlich-3 Extraction Bolivia,NC 28422
A. tt 'fl Soil Report
4 ",X•4, ,... Sampled County: Brunswick
I Sampled: 12/30/2014 Received: 12/31/2014 Completed: 01/21/2015 Farm: 1473 Links to Helpful Information
Agronomist's Comments:
This report contains both routine soil test information as well as heavy metals data in a section labeled as Heavy Metals under soil test lab results.Using Mehlich 3 as a soil test
extractant,background levels of these metals typically seen in NC soils when analyzed are as follows:arsenic(As)-4.5 ppm,cadmium(Cd)-0.1 ppm,chromium(Cr)-0.2 ppm,lead
(Pb)-4.2 ppm,nickel(Ni)-0.8 ppm,&selenium(Se)-0.2 ppm(FY2005-2007).Note elevated zinc(Zn)in sample 1A.Although the above metals here are not believed to pose a
concern for plant growth,continue to monitor these and note where elevated above background levels.Where soil test phosphorus(P)is very high(P-I>100),crops will not respond to
additional P applied.Tissue testing is advised where pH is elevated and where Zn levels are of concern as in samples found here;small grains are especially sensitive to Mn deficiency
: caused by high pH.Additionally there is Mn concern noted in samples 2A and 2C .Note any lime and fertilizer recommendations. Jagathi Kamalakanthan 1/13/2015
Sample ID: 1A Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past.,M 0.0 180-220 0 190 0 0 pH$ 0 0 0 Note: 12 Note:$
2-Small Grain(SG) 0.0 80-100 0 100 0 0 pH$ 0 0 0 Note:3 Note:$
Test Results[units-WIV in g/cn3;CEC and Na in meq/100 cm3;NO3-N in mgldm3]: Soil Class: Mineral
HM% WA/ CEC BS% Ac pH P-I K-1 Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-1 Na ESP SS-I NO3-N
0.36 1.08 75.1 100 0.0 7.7 280 18 98 2 90 77 37 30 1306 1306 924 0.1 0
Heavy Metals(parts per million): Arsenic, 0.2 Cadmium, 0.2 Nickel, 0.7 Chromium, 0.2 Lead, 1.6 Selenium, 0.4
Sample ID: 2A Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past.,M 0.0 180-220 30 240 0 0 $ 0 0 0 Note: 12 Note:$
2-Small Grain(SG) 0.0 80-100 30 140 0 0 $pH 0 0 0 Note:3 Note:$
Test Results [units-WA/in gicni3;CEC and Na in meq/100 cn ; NO3-N in mg/drn3]: Soil Class: Mineral
' HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.27 1.45 29.1 100 0.0 8.0 48 2 98 2 36 39 10 3 94 94 71 0.1 0
Heavy Metals(parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.2 Chromium, 0.1 Lead, 0.7 Selenium, 0.4
North Carolina Reprogramming of the laboratory-information-management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
\=y Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
•• •,;.. - Steve Troxler, Commissioner of Agriculture
k'l.:cco Tru‘i lluni CiNtI,t1Y\'tt151

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY15-SL020323
Sam Carteret Page 2 of 3
Sample ID: 2B Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past.,M 0.0 180-220 0 240 0 0 pH$ 0 0 0 Note: 12 Note:$
2-Small Grain(SG) 0.0 80-100 0 140 0 0 pH$ 0 0 0 Note:3 Note:$
Test Results[units-WN in g/c► ;CEC and Na in meq/100 cns3; NO3-N in mg/dn$]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.27 1.37 80.5 100 0.0 8.1 62 4 98 2 74 81 34 27 166 166 105 0.1 0
Heavy Metals(parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.3 Chromium, 0.3 Lead, 0.6 Selenium, 0.4
Sample ID: 2C Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past.,M 0.0 180-220 0 240 0 0 $ 0 0 0 Note: 12 Note:$
2-Small Grain(SG) 0.0 80-100 0 140 0 0 $pH 0 0 0 Note:3 Note;$
Test Results[units-WIV in g/cn3;CEC and Na in meq!100 cnr3; NO3-N in mg/dnv3]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.41 1.40 30.1 100 0.0 8.0 76 4 98 2 38 63 24 17 88 88 59 0.1 0
Heavy Metals(parts per million): Arsenic, 0.1 Cadmium, 0.0 Nickel, 0.1 Chromium, 0.1 Lead, 0.8 Selenium, 0.4
Sample ID: 1D Recommendations: Lime Nutrients(lb/acre) More
Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information
Lime History: 1 -Bermuda hay/past.,M 0.0 180-220 0 230 0 0 pH$ 0 0 0 Note: 12 Note:$
2-Small Grain(SG) 0.0 80-100 0 130 0 0 pH$ 0 0 0 Note:3 Note:$
Test Results[units-WIV in glcm3;CEC and Na in meq/100 cnr3; NO3-N in mg/drrt3]: Soil Class: Mineral
. HM% WIV CEC BS% Ac pH P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-I NO3-N
0.46 1.23 86.2 100 0.0 7.9 156 7 99 1 103 113 56 49 532 532 406 0.1 0
' Heavy Metals(parts per million): Arsenic, 0.2 Cadmium, 0.1 Nickel, 0.3 Chromium, 0.2 Lead, 1.1 Selenium, 0.4

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY15-SL020323
Sam Carteret Page 3 of 3
Understanding the Soil Report:explanation of measurements,abbreviations and units
. Recommendations Report Abbreviations
Lime Ac exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated,a lime recommendation will be given in units of either B boron
ton/acre or lb/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% %CEC occupied by basic cations
; For no-till or established plantings where this is not possible,apply no more than 1 to 1.5 ton/acre (50 lb/1000 sq ft)at Ca% %CEC occupied by calcium
one time,even if the report recommends more.You can apply the rest in similar increments every six months until the CEC cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index
ESP exchangeable sodium percent
' Fertilizer HM% percent humic matter
' Recommendations for field crops or other large areas are listed separately for each nutrient to be added(in units of K-I potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B)are based on research/field studies K20 potash
' for the crop being grown, not on soil test results. K-I and P-I values are based on test results and should be>50. If they Mg% %CEC occupied by magnesium
are not,follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22(11.5% Mg)is MIN mineral soil class
an excellent source; 175 to.250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-I levels appear Mn manganese
only on reports for greenhouse soil or problem samples. Mn-All Mn availability index for crop 1
Mn-AI2 Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If$,pH$, $pH, C or Z M m
M-O mi n nerral-oal-orrgg indexanic soil class
notations appear on the soil report, refer to $Note:Secondary Nutrients and Micronutrients. In general, homeowners do not N nitrogen
need to be concerned about micronutrients.Various crop notes also address lime fertilizer needs;visit Na sodium
ncagr.gov/agronomi/pubs.htm. NO3-N nitrate nitrogen
ORG organic soil class
Recommendations for small areas,such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot pH current soil pH
, find the exact fertilizer grade recommended on the report,visit www.ncaar.aov/agronomi/obpart4.han#fs to find P-I phosphorus index
information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer. P205 phosphate
S-I sulfur index
Test Results SS-I soluble salt index
INN weight per volume
The first seven values[soil class, HM%,W/V, CEC, BS%,Ac and pH]describe the soil and its degree of acidity.The Zn-Al zinc availability index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-Al2,Zn-I, Zn-Al, Cu-I, S-I, SS-I, Na, ESP, SS-I, NO3-N (not Zn-I zinc index
routinely available)]indicate levels of plant nutrients or other fertility measurement.Visit www.ncaaraov/adronomiluyrst.htm
for more information.

• • I
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF MVP NPDES Permit#NC 0007064
0 b
Approximate Total Gallons •5 (-{
I
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
NOTE: Ali pH measurements are in Standard Units(S.U.).
, 11
I
I
I
—7--------
Tank identification #-1 Digester #2 Digester c#2 ClarifieriCirole One)
t Calculated
Sample Analysis pH Temperature
Date pH Operator
Time Time (S.11) (M I (S.U.)
pH prior to
Lime Addition A-)-R-i i Z.5'7 I xs5 7,3 ( ii, j) 7. 1 t
pH after initial •
Lime addition 2-34'1 1 3)7 r 3 31 (.11-fq 1 5, Li` 12._ 2 0 i.„ d
pH..2 Hours
after Lime 2,1-, l'i fpf tr try t. 114'7 / 7. 2- /2. 3) •
Addition i
—7 pH?_24 Hours
after Lime 1.4.ILI I,i./s40 i if Lit- . 11.,1) i Li. 3 et.4 3 1 cit,,,alc 44-4
Addition ,•'" i
Tank Identification #1 Digester 61rDi7nlester #2 Clarifier (Circle One) ,
i I Calculated 1
I Date Sample Analysis pH Temperature
Time Time (S.U.) (C°) pH Operator
1 (S.U,)
I pH prior to
Lime Addition -2-3',Y. t 25"7 I 3 civ 7-or / C't j K. 7) ctre,,,5-4 s
pH after initial
Lime Addition 12-)-1 Y - i 3 3.7 t 340 1,2ssit 1 ci, 0 1 . 41 ck- 4.-,4
1 ,
pH?..2 Hours I
after Lime 01.1.-Of i pf 11 11(17 14-17 / Lir 3 14--
Addition
pH pH 24 Hours
after Lime 2'11-ri1i 9 40 I titi3 IA,L0 / 3, 0 / ,2 • i 3 cliej. 14—A—
Addition I
OE&RC-3241 Rev. 14 Page 35 of 40
1

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF\AREVIP NPDES Permit#NC 0007064
Approximate Total Gallons tn)
0 NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
I NOTE- Ali pH measurements are in Standard Units(S.U.).
Tank Identification #1 Digester #2 Digester( aer One)
Calculated
Sample Analysis pH Temperature
DatepH Operator
Time Time (S.U.) (Ce) (S.U.'
pH prior to
Lime Addition 3-3-1 y o re?, 743 0 . r t7 °Lime addition pH after after initial
3-3.4 y )tior 116 7 11.30 4.76 A,df c,cc
pH? 2 Hours
after Lime . 441 fcV (440 es 3 11. 07 cie-4.„,4
Addition
pH .?24 Hoursl
after Lime 11.. 143) /4) 6. 12.31I 2,16
Addition
Tank Identification #1 Digester 2 Digester #2 Clarifier (Circle One)
Calculated
Date
Sample Analysis pH Temperature
Time Time (S.U.) (C°) pH Operator
(S.U.)
pH prior to
Lime Addition ) jI 7.0f
pH after initial
Lime Addition 3.3.1y Nos- rgiog (A.524- tiC 6 12.a t tAT
pH?2 Hours
after Lime 3
.,3,ify (01
ii I
Addition
pH?24 Hours
after Lime 3... 13 ) /0 7 0. 0 121' ( 2.11.
Addition
OESLRC-3241 Rev. 14 Page 35 of 40 1

ATTACHMENT 9
Page 'I of 1
Sewage Sludge pH Adjustment
Sludge Source BSF V\P TP NPDES Permit# NC 0007064
Approximate Total Gallons C. i uv
I NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221). f
NOTE: All pH measurements are in Standard Units(S.U.).
Tank Identification # 1 Digester #2 Digester #2 Clarifier (Circle One)
I Calculated i
Date Sample Analysis I pH Temperature pH Operator
Time Time I (S.U.) (C') (S.U.)
pH prior to Lime Addition 3-fa.1`1 orav I I 70 � C•77 '21. 0 G, 7 I c4 k/
pH after initial -
Lime addition 13-l2-t`1 (!aO j II ,2 1-- Is.LI3 j 6.5 IA. 17 G(+: +-,./ -
i
LpH>_2 Hours
after Lime IY-Iz-N 1341 t 3 `f`i i •3-1t l , I a. o- I G 1 1-
Addition
pH>_24 Hours
after Lime ?,./).t+i 11 c r 1 `l i e 0.1 o f tI 6' q f i-rye 4 c r r.,✓ `.
1 Addition ' i _1
Tank identification # 1 Digester #2 Digeste #2 Clarifier (Circle One)
I I i I Calculated
Date
Sample Analysis pH Temperature pH Operator
I Time Time (S.U.) (C°) (S.U.)
pH prior to
Lime Addition 13-.ir1K o re:N 0 5-0 3 6-t;7 2 c, LI !�?. i �(�
f �
J.--
pH after initial _t l t l D ! ( g 3 ( 6. 5
Lime Addition 3 12 (A..3 f P. I D I C r r'" —
pH>_2Hours
after Lime 3-i2--IK I341 t31r 12.2t, Ia'. I I •Z - u1 C1' k- -
Addition
pH z 24 Hours I
after Lime 3-13-11 1 fof 1jo7 1.1.7Ll tI, ( I,2. o 4/ . Ci' 4, .,‘
I Addition ( I
OE&RC-3241 Rev. 14 Page 36 of 40
1

. . I
1
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WVVTP NPDES Permit# NC 0007064
Grp ct
Approximate Total Gallons ,..0
II
l, NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart DE&RC-3221). ,
NOTE: All pH measurements are in Standard Units(S.U.).
Tank Identification #1 Digester #2 Digester t.C_If.._jifier Circle( One)
Sample 1 Analysis pH Temperature Calculated ' 1
pH Operator I Date Time Time (S.U.) (C°) (S.U.)
pH prior to
Lime Addition 3-iir-i'I 6'NZ 0 "ft? 7.. J-6 2r-a Tr‘ t 4.,,.2 --
pH after initial i I 4 .
Lime addition , e 11)7 1 r I f 1 t2. 0 i 4, ?
pH 2 Hours _
after Lime 7-20-/Y er23 ef Yr t:2.gr I.A.
Addition
pH pH a 24 Hours —1
after Lime )_2c,t-t 1 i 51-6 ("TY (2.4-7 , y. o
Addition . . .
Tank Identification #1 Digester -) #2 Clarifier (Circle One)
I '
Sample Analysis pH Temperature [Calculated
Date pH Operator
Time Time (SAL) (C°) IS.U.)
pH prior to „ Of.`fq
Lime Addition J--t y-er 0 el q 7-11 2 r.0 7 5-3 I
— _
pH after initial 1 ,.,
Lime Addition 3-0.4 1 I rn I FLEO (2.)I I C I (-N.0 i 176 41_,id
pH 2 Hours
after Lime 7..2,0,0 of)) or 3,c Q.,-i Li I .7. f • 12. //-
Addition
pH_.24 Hours
after Lime 7_20 ..14 1 s-r4 r
fi) 1 " 12,)1 n. 0 0
L Addition 3 i
i. .,
1
1 OE&RC-3241 . Rev. 14 Page 35 of 40
I
I

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF INOTTP
- NPDES Permit# NC 0007064
Approximate Total Gallons
I NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
i 1
NOTE: All pH measurements are in Standard Units(S.U.).
Tank Identification #1 Digester #2 Digester Clarifie (Circle One)
Calculated I i
Sample Analysis pH Temperature Date pH Operator
Time Time (S.U.) (Cc) (S.U.)
pH prior to
Lime Addition 3-.67Y 10 2- C/r09 1 7. 31 a S. a 7. 3/ =w
pH after initial
Lime addition 3_20 1 02-0 io yZ I(2.7) (I- d /2. 33 1 etr`q',
}
I pH?2 Hours ] r E
after Lime 3-,2 4•%'i f J y)3 ill 7 r i a (5.if
Addition
pH?24 Hours
after Lime
j).z7.,y fvtfc i 10 f3 f .71 is. P F26 f ce Addition
Tank Identification #1 Digester #2 Digester #2 Clarifier (Circle One)
Calculated
Sample Analysis pH Temperature Date pH Operator
Time Time (S.U.) (CC) (S.U.)
pH prior to
Lime Addition 3`2 6-iv O9'al I e f oi— 7-07 T. 0 7. 7 a
i r
pH after initial i
6
Lime Addition ' , u
-f'r 1u 1023 12. 7 /0.
pH?.2 Hours
after Lime 11'-26-14 iY33 I113r' 12.53 j 3. g l . 19 c
Addition 11
pH>24 Hours r
after Lime 713411 `ow 1 f0Lill 12 t 2.- /2.2ti eke.
l Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WV/TP NPDES Permit# NC 0007064
Approximate Total Gallons 5ti fro
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
NOTE: Ail pH measurements are in Standard Units(S.U.),
Tank Identification #1 Digester #2 Digester(1i2Clarifi (Circle One)
Date pH Operator
Sample Analysis pH Temperature Calculated
Time Time (S.U.) (C*) (SU.)
pH prior to
Lime Addition '1,:a-114 0 yip 0?5-3 7 0 2 o 7,20 741,
pH after initial y
Lime addition I ir ( 017
pH_?2 Hours
after Lime
Addition /3 oi 1311 [24-6 1, 1 2• (-17 CI
pH 24 Hours
after Lime I I la pay 20,7 1).3o r t
Addition
Tank Identification #1 Digester ii....(-1.27;---ge-S-t - #2 Clarifier (Circle One)
I Sample Analysis pH Temperature
Calculated
Date pH Operator
Time Time (S.U.) (C°) (S.U.)
pH prior to
Lime Addition ti Dr!0 try 741 2,r, -0 7. (1
I I
pH after initial
1+74
Lime Addition uf-1-(4 ( I 2 ff: i
c K
pH.?2 Hours
after Lime E,i 30 i 3 12. i
Addition cec
pH 24 Hours
after Lime Li-)--Of (12,6 INC, 11 11. 1 V.27 Ca z4A, •
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
• Sludge Source BSF WWTP NPDES Permit# NC 0007064
Approximate Total Gallons
MOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
NOTE: All pH measurements are in Standard Units(S.U.). '
Tank Identification #i Digester #2 Digester Clarifier (Circle One)
Sample Analysis pH Temperature Calculated
Date Time Time (S.U.) (C°) pH Operator
(S.U.)
pH prior to
Lime Addition 's'7-/cf /(aP fLia 7.2 i 21`f I 7'2 C
•
pH after initial �
Lime addition 4"('di ( .01 (`t 5-3 12. f tt .20 .3 12.3 v G t�
pH 2 Hours
after Lime t f,.. _f j Ur f 70 7 2..rt) 6. © 0 , 37 C'(t4
Addition i
pH>_24 Hours
aAdditionfter Lime i Ic,dFrf i3 3> I57,7_, 112.4e al.2_ I .� G
Tank Identification #1 Digester E2. Digeste #2 Clarifier (Circle One)
Sample Analysis pH Temperature
Date pH Operator
Time Time (S.U.) (C°) (S.U.)
i
priorp
to L i J 6 te'� c�
Lime
Addition Addition �-'�('(� f t j 0 1 tf�� �s` f �0 f
pH after initial I G
+�{ -E� i1;i /'fry (a.30 h�
Lime Addition .�
i .• (a.. I t
pH?2 Hours I ^�
after Lime [f,. r�1 r-m r- ��ci tc/ h2.36 I?. 7 i�+�.o O G4
Addition
pH=24 Hours
after Lime tf-10N114 IS ) 15)G 2.24 a /2.t r" Gil e--tj
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit# NC 0007064
Approximate Total Gallons 5 t
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221). I{
i'
NOTE: All pH measurements are in Standard Units(S.U.).
Tank Identification #1 Digester #2 Digester ( C nal nal fie (Circle One)
Calculated
Date Sample Analysis pH Temperature pH Operator
} { Time { Time (S.U.) I (C') (S.U.)
{ pH prior to c_13. 'f I 7.�� �, b 1
Lime Addition I`f c1 f t of G.� ` TI c
pH
LEme of ta ddstionl 5,(3.r 4.1 �( 1,1 ) 1.,/ t,2.14 7 2,7, 5 I� . a g.r
� (
pH>_2Hours ! ii f�• � 1 `�
after Lime 1S-f -Pt Z( f it) r c.. i
Addition
pH?24 Hours!
after Lime I5 i 9'1�1 (`� `ti , t
l I f G( a
Addition I
Tank Identification # 1 Digester #2 Digester #2 Clarifier (Circle One)
Sample Analysis pH Temperature Calculated
Date Time Time (S.U.) (C°) pH Operator
(S.U.)
pH prior to ��.t 4A,,,4
Lime Addition - ( K 06 d tf o ta(-: (1'
`' <<
pH after initial 5,1 3-/Y � tr- 11 f 2 4 , 5 12. .�1 } C%t
Lime Addition l'a � i
pH>_2 t
after LimoeHours ,j- t i_i(f f 042_ l t �I f j 2.3 6 7. 3 /o , 't3 I mo.
Addition •
pH>24 Hours
after Lime r r 1 'fa id? 1-7 , 0 (a, i 3
Addition
OE&RC-3241 Rev. 14 Page 35 of 40 I

. ,
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF VANTP NPDES Permit#NC 0007084
Approximate Total Gallons 5
II i.
I NOTE: pH TEMPERATURE CORRECTION REQUIRED (see correction chart OE&RC-3221). i-
1 t
1
"I NOTE: All pH measurements are in Standard Units(S.U.).
Tank Identification # 1 Digester #2 Digester ,Circle One)
4CP
I Date Sample Analysis pH Temperature I Calculated
pH Operator
Time Time (S.U.) (Ce) (ali.)
pH prior to r• iu ..,
Lim.,Addition 6'CO 17.CI 6 ..2 I. 0
I
pH after initial I _ .),.., CO
, Lime addition (..) 't''' ' i 0) I 7 of 14) 111.13 .2 ..r. I'I
i 1 .
1 pH P...2 Hours iafter Lime Lime 6-IX-111 t op-f torr a,7 2 Y.2, t ).....ri cl
Addition II_
pH?_24 Hours
after Lime 64344 or,,70 4r)i f.2,cf 7 ,,?J. 1 12. v3 Cc c.,r,./....4
Addition i
Tank Identification .# 1 Digester ( Dic77;;) #2 Clarifier (Circle One)
I Calculated
Sample Analysis pH Temperature
Date pH Operator
' Time Time (S.U.) (C') (S.U.)
1
pH prior to r
Lime Addition i6-(1-1 tf I 0,ff 2 Cr trrY 7-13 I. til
1 i
pH after initial j .„ 1 7.1-d° <I. 7 I ).--1-
Lime Addition Addition 6,/1-t`f 105 il
} 1
pH k 2 Hours
after Lime 1)--II-Ict I Of'1 I 91(' / )• j',.0 /-7-
Addition I
I i -
pH;-.-..-24 Hours 2
1
after Limef— 2 3. 0 2-
Addition
OE&RC-3241 Rev. 14 Page 35 of 40

_
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit#NC 0007064 1
Approximate Total Gallons .1 t
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
I I
z
NOTE: All pH measurements are in Standard Units(S.U.).
r
Tank Identification #1 Digester #2 Digester2 Ciarifie)(Circle One)
i = I Calculated
Date I Sample Analysis pH Temperature pH E Operator
i Time ; Time (S.U.) (CD) (S.U.)
1 {
I pH prior to 1 4
Lime Addition $-I'i i U so 9 j es-II 1.43 7 ,2 s.S- 7• o; r fr a, ,
1 pH after initial 3 i 3 PTO I ,7. 3
Lime addition 17 ?-' i 053 r'1 c r,� 1
IpH?2 Hours I ` q }'
after Lime 4.Iy ; t00d� ! 0tv f . 31 7• I !A . `1 ri
j Addition I ;
i pH>_24 Hours i
j afterAddi Litimone 1-10_ y opY6 6 r 4 7 1 (2.2 7 2.s.jr- l2-�,.`7 Ct��.
Tank Identification #1 Digester 2 Digester #2 Clarifier (Circle One)
Sample 1 Analysis pH Temperature f Calculated '
pDate Time Time (S.U.) (Ce) (S.U.) Operator
pH prior to i
VLime Addition .7.7-01 b:01 I O�/1 , 7. 3: 2 .5. } 7. 38 c t 4,-,�
pH after initial i
t
Lime Addition .-I d J c .�.�(� f 1-r� €
pH>2 Hours I
after Lime -47'Iy ( ° L o !i 12.2
i. 36 ` Er/ �K
Addition l
pH>_24 Hours I I i
after Lime f-tci.t`/I -4 01-`f �'` I .Ll2 2`-. ! . 4. l . c it�.,)-
Addition
OE&RC-3241 I Rev. 14 Page 35 of 40

ATTACHMENT 9
~-- Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF t VI TP NPDES Permit#NC O007O64
Approximate Total Gallons E
0-0
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart QE&RC-3221).
NOTE: All pH measurements are in Standard Units(S.U_)_
Tank Identification #I Digester #2 Digester #2 Clarit<er (Circle One)
Sample Analysis pH Temperature Calculated
Date Time Time (S.U.) (C') PH Operator
(S.U_)
pH prior to
Lime Addition .e.-41-ry f 2$f (L17 717 3f, j 7- 77
pH after initial
Lime addition f f T l y , l 117 131, 1. ,jam( J o.7 f 2.7 e
pH?2 Hours
after Lime 8-e1-(y f cP/ 16'lc ILO 3 t-5 /2 -er
Addition
pH>24 Hours
' after Lime b 2 Y ` riff/7 Et.-�1 31,1 13 . (3 c e
Addition
Tank Identification #1 Digester it 2 Digester #2 Clarifier (Circle One)
Sample Analysis pH Temperature
Date Calcpul led Operator
Time Time (S.U.) (GO)
(S.U.)
pH prior to
Lime Addition -1 E y- t ..�r (2 IF 7 Co t 3 /-5 ?- 2 Z ce,j,
1
pH after initial
Lime Addition 8 f?-d y.J 3/7 /32 C? f 2., � r l 12. 3? le- �✓`I
pH>2 Hours
after Lime q,(�-f`f j‘/`f ( 6 a( (. ,6 L y 1.2.. 'o C f �i
Addition
pH 24 Hours (fit j
after Lime &t s /
(5L Addition `� f ( - �` f�. ( y( t� t-v
OE&f G-3241 1 Rev. 14 Page 35 of 4G J

1
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF WWTP NPDES Permit#NC 0007064
Approximate Total Gallons S Li cru
4 NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart of&RC-3221).
INOTE: AU pH measurements are in Standard Units(S.U.)_
r---4-._
Tank Identification #1 Digester #2 Digester #2 Clarifier ircte One)
Calculated
Sample Analysis ; pH Temperature pH Operator
Date pH
Time (S.U.) (Ce) (S.U.)
pH prior to I
Lime Addition `r-IY-iY Ofor 65-07 7•5_1 ' . 2 7 7- y7 CI`c-,4
pH after initial �f
Lime addition I.-pi-Pt o S 3
S) 2 . O ' 12 S,Y 2 E; 1 t•�- G t'r it .,
� 3
pH z 2 Hours
after Lime /.�1 y-14 to Lib/ 1 O cf. ? Ns ? .2 5, 4 1 d. 5? K 4.<34,
Addition -----
pH -24 Hours
after Lime q'l 3-4 y Ida 3 1 v 2 6 1,?.5 2-` a. it ? i a•S I c,E t.'-.-
Addition
Tank Identification #1 Digester E.61g-e—sD#2 Clarifier (Circle One)
I Calculated 1 I
Date Sample Analysis i pH Temperature pH ; Operator
Time Time 1 (S.U.) (C°) (S.U_)
3
pH prior to
/�
Lime Addition q,j(pi ei , 6 5 p j"- 6SS-o 5 j r1.1 f ifLI• 7-L7 2 AFC L,,i,
i
pH after initial j �� � �• � /�_© 2 �r � ,`,
Lime Addition q !,f f yi !3 S 3 2- 6 c 3,) f •5` 1
pH-2 Hours ..
after Lime 1 05� t�.S` 6// © jd.. ‘z rrf U
Addition -1Y"r`t : {o�t� 1 I
pH?24 Hours
after Lime ,9_i�,,/ ( o a 3 ; va.b� 1.2.5 3 : 5 ,0 1). 5 3 i A--
L Addition
OE&RC-3241 I Rev. 14 Page 35 of 40
i

ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF VVVVTP NPDES Permit#NC 0007064
Approximate Total Gallons Grt7
NOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
NOTE. All pH measurements are in Standard Units(S.U.).
Tank Identification #1 Digester 42 Digester #2 Clarifier (Circle One)
Sample Analysis pH Temperature Calculated
Date Time Time (S.U.) (C°) pH Operator
1 (S.U.)
pH prior to
Lime Addition to-a7-c y (a o cr 10 6 66 7.3 C i.f ?G ty tcjc-t-
pH after initial
Lime addition t Q-2747 to(7 I Ol (2.Fl I ?. 2- l a Ji
pHa2Hours
fterLime to 2?_'N 1a41 / c13 11.?�' a l_ I �, Con �
pH a 24 Hours
after Lime (6.7 X't 9 1`o 6 ifci d L 11.24' .11.1161 P.- 3 4 C(r
Addition
Tank Identification #1 Digester €Di-g-els--te3#2 Clarifier (Circle One)
Sample Analysis pH Temperature Z Calculated
Date Time Time (S.U-) (Ce) pH Operator
(S.U.)
pH prior to , jU07
Lime Addition fo_yp-i'f (Ua C9°51) t 2 I 6. �Z Ce
e�-1T it
pH after initial WIT T p2,f� l is 12.3 f
Lime Addition (o-2?-f`l ( o j 7
pHa2Hours
after Lime 0-2?_iy t2 Lit rayq 12.Y6 L /. 3 31 cis I
Addition
pH a 24 Hours
after
1.6
_2-)'11 ("10 l'463 (1.4 ( a `f_ G l ' Liv C. '
E' t P t4' Ltd 84. e4e(4 CP' j4e 4.t'Ca rrg -2S E.Ke fd-23-1r) 7, 93,E�►
OE&RC-3241 Rev. 14 Page 35 of 40

. , I. ._,
ATTACHMENT 9
Page 1 of 1
Sewage Sludge pH Adjustment
Sludge Source BSF\WITP NPDES Permit# NC 0007064
Approximate Total Gallons
li
INOTE: pH TEMPERATURE CORRECTION REQUIRED(see correction chart OE&RC-3221).
li
I NOTE: All pH measurements are in Standard Units(S.U.).
--
Tank Identification # 1 Digester #2 Digester 162—C;;;(Cirole One)
1 ; Calculated
Sample Analysis • pH Temperature
Date pH Operator
Time Time (S.U.) (C1 (S.U.)
pH prior to
Lime Addition
pH after initial e----1 .
Lime addition (1.1.5,111 67) 2- 071 q I... .32- I 3. L la: il Cie
pH 2 Hours
after Lime
0 k -5.'14 li4;0 114 , ( 2 34 f .7 ••Addition
pH 24 Hours
after Lime IL'19103 I-1 OV° Il-ri I?, 0
Addition
Tank Identification # 1 Digester /t 2 Digester #2 Clarifier (Circle One)
Sample Analysis pH Temperature latedT
Time Time (S.U.) (C°) Calcu
Date pH Operator
• (S.U_)
pH prior to , 1.,„r,,,I.r:
Lime Addition ' 602-, 60-( 6-°2- IJ• 7
f---
pH after initial , 1,..3.1441
Lime Addition 1 - 0'71"-- 1)-0 1 S-17 i a ,27 cif
pH a 2 Flours
after Lime 11.1.1.'/1 if 0 G 1 10 9' (2.fo I jr. P•2-2- H-
Addition
pH 24 Hours
after Le ,2„).6-Pif 06y n I 0 s LI 1 ‘ 3 41, 1 g/y 1 1..1 , 1 j 1 c,r 1.,,,•Q I 1
Addition ' I 1
. i
i OE&RC-3241 I Rev. 14 Page 35 of 40 1
i

Lime Stabilization pH Test Results
Town of Oak Island
S & B Maintenance : Hauler
Sludge Source:Fish Factory Rd WWTP Permit t:W00005790
Approx.Gallons: iT IVO �),
Initial pH Test
Date: f .�- 77-/It Time: rjl.`3a pm Operator. 57P/
pH /a. 7 Temp. /.7e -c
Converted pH to 25cc / 33 3 PH l 2,y
Conversion Factor(cf)=(Temp reading"c-250c)x 0.03_ (724 'c-25'c) x 0.03=1 37 (cf)
Converted pH=measured pH+f-the Correction Factor. 12.7 pH(+ ) .37 (GI)= /233 pH
2 Hour pH Test
Date: 2-2?I/ Time: 6=35 1 Operator. /2 a
pH i24a Temp. f 3) 'c
Converted pH to 25"c /2 ,2 pH
Conversion Factor(cf)_(Temp reading c-25"c)x 0.03. ( i(3 "c-25'c) x 0.03=d,3fo.(CO
Converted pH=measured pH +f-the Correction Factor. 04 pH(+4O 34 (cf)= /22-pH
24 Hour pH Test
Date: 62-GCS- Time: 14.WPM Operator. I
pH ,. 3 Temp. a .c .
Converted pH to 25"c /j.92 pH
-12.5
Conversion Factor(cf)=(Temp reading'c-25"c)x 0.03. ( la.5 'c-25"c) x 0.03= 6 (cf)
Converted pH=measured pH+!-the Correction Factor. L.2.3 pH (+t)) ,3' (cf)= 1)97,pH
Initial and 2 Hour test must be above a converted pH of 12 and 24 Hour test must be above a converted pH of 11.5
Operator Signature for release: i Date/Time c2 "
Hauler Signature of Acceptance: Date/Time

Lime Stabilization pH Test Results
Town of Oak Island
S & B Maintenance : Hauler
•
Sludge Source: Fish Factory Rd WWTP Permit#:WQ0005790
Approx. Gallons: Yc,,P c)c2
Initial pH Test
Date: " 9- rr' Time: / 0/3 Operator 5` of
pH ,1 Temp. :% 67: °c
Converted pH to 25°c / ;24 f 5 `/ pH
Conversion Factor(cf) =(Temp reading°c-25°c)x 0.03. (0261S °c-25°c) x 0.03 = .Cs-V(cf)
Converted pH= measured pH +/-the Correction Factor. /Z./ pH (+/-) ,G5' (cf) =/L./5'1(pH
2 Hour pH Test
Date: l v ' �-7 Time: /.2-_115P /f% Operator: 1 / /f
pH 1 2, Q Temp. 8,& °c
Converted pH to 25°c lea 0 `' pH t
Conversion Factor(cf) _ (Temp reading°c-25°c) x 0.03. ( 0°c-25°c) x 0.03 = i (cf)
Converted pH= measured pH +/-the Correction Factor. %2,0 pH (+/-) eC°t (cf)= I zc r pH
24 Hour pH Test
Date: £ _ 1 ` / t( Time: /0.`3 0 .4-714 Operator.
pH Temp. 2. 7, / °c
Converted pH to 25`c /1--: /13 pH
Conversion Factor(cf) = (Temp reading°c-25°c)x 0.03-. ( ;<<I °c-25°c) x 0.03 = t•G'33(cf)
Converted pH = measured pH +/-the Correction Factor. P,cS pH (+/--) ;©63 (cf)=j.21/_j pH
Initial and 2 Hour test must be above a converted pH of 12 and the 24 Hour test must be above a converted pH of 11.5
�z 1 • /144
Operator Signature for release:- /�, . � Date/Time ((-ID f
Hauler Signature of Acceptance: () i Date/Time l67•D /
dekii5/2/12

Lime Stabilization pH Test Results
Town of Oak Island
S & B Maintenance : Hauler
•
Sludge Source: Fish Factory Rd WWTP Permit#: WQ0005790
Approx. Gallons: c;,S col—)
J
Initial pH Test
Date: d-f72-J---/g Time: F.'s- ! Operator. 5 kJ
pH 0-, l l Temp. ,2-s °c
Converted pH to 25°c f 2 pH
Conversion Factor(cf) = (Temp reading°c-25°c) x 0.03. (2.-g °c-25°c) x 0.03 = /o% (cf)
Converted pH = measured pH +1-the Correction Factor. 1 a,t I pH (+l-) ros (cf)= 12.2- pH
, / 2 Hour pH Test
1 7-
Date: 2.5-- f ` Time: I ei DO iiii,1 _ Operator: 1 1 -
pH /, -, / 0 Temp. �,'Y °c
Converted pH to 25°c f.2-, l ? pH i
Conversion Factor(cf) = (Temp reading°c-25°c).x 0.03. (.-cj) °c-25°c) x 0.03 = ,0 y (cf)
Converted pH =measured pH +1-the Correction Factor. la-,/0 pH (+l-) /0 7 (cf)=1 A / pH
24 Hour pH Test
4
Date: R. -V-6 4_/471 Time: r1 - 6,0 Operator. J 6c}
pH /a,0 - Temp. a 9 °c
Converted pH to 25°c l , Pi: pH
Conversion Factor(cf) _ (Temp reading°c-25°c) x 0.03. ( G2 T °c- 25°c) x 0.03 = , 12-(cf)
Converted pH = measured pH +l-the Correction Factor. /3-,v Z-pH (+/-) :/„4 (cf) = 72<if pH
Initial and 2 Hour test must be above a converted pH of 12 and the 24 Hour test must be above a converted pH of 11.5
Operator Signature for release: 1--e-,-7-.-- -i-l.,-/-/;/.
,n Date/Time --' (0/44
Hauler Signature of Acceptance: ( 4 ,--;:= -- ?ate/Time — 6
dekn512J12 �'

Lime Stabilization pH Test Results
Town..of Oak Island
rw S & B Maintenance : Hauler
Sludge Source: Fish Factory Rd WWTP Permit#:.W00005790
Approx..Gallons: elopo .
c 20 1 t Initial pH Test
Date: '. . ► l Time: e3W Operator: k v-
pH 1,2-, I Temp. o2'"I.i °c
Converted pH.to 25°c (2-,2-9 pH
Conversion Factor(cf)=(Temp reading°c-25°c)x 0:03. ( i.r °c=25°c) x 0.03= .I44 (cf)
Converted pH =measured pH+/-the Correction Factor. {Z.( pH Or) ,i�t'{ (cf)= 12.Z4t pH •
2 Hour pH Test
_Date: Time: 1 a:39 -Operator: �•� -
pH 12,D Temp- 29- .c •
Converted pH to 25°c t 2-. )4 pH 1
Conversion Factor(cf)=(Temp reading°c-25'c)x 0.03_ (2 .(r°c-25°c) x 0.03= .l4`1 (cf)
Converted pH=measured pH+/-the Correction Factor. t 2.0 pH ph) .toy. (cf)= 12,I4�f pH
24 Hour pH Test
Date: gl` Zt- Time: 0800 Operator: KV
pH 102. 2. Temp. 27,7 "c
Converted pH to 25°c pH
Conversion Factor(cf)_ (Temp reading'c-25°c)x 0.03. (2.27c-25°c) x 0.03= ' ' (cf)
Converted pH=measured pH +/-the Correction Factor. (2. pH (+/--) j (cf)= 12.3&pH
• Initial and 2 Hour test must be above a converted pH 12 and the 24 H ur t st be above a converted pH of 11.5
Operator Signature for release: - - /.• Datefrime B.-
Hauler Signature of Acceptance: Dateff'ime
dekii5f2112

Mink
Lime Stabilization pH Test Results
Town of Oak Island
S & B Maintenance : Hauler
Sludge Source: Fish Factory Rd DTP Permit#: Q0005790
Approx.Gallons:
Initial pH Test
Date: IL -3 • i'} Time: 6 :So o gov Operator
pH 1a,7
Temp. /6, 1 °c
Converted pH to 25'c /.2,5- pH
Conversion Factor(cf) = (Temp reading'c 25'c)x 0.03. ( I ,t 'c 25°c) x 0.03 = 6,2..1 (cf)
Converted pH = measured pH +/-the Correction Factor. 1 a.� PH (�/-) ,2 (of) = 1 2..s pH
2 Hour pH Test
Date: t i. 3 Time: 1 ;CIO 41 m - Operator: ,,,,,, i VIA)Vru .
pH /a,5- Temp. ./g,0 °c
! '
Converted pH to 25°c f a,Z pH
Conversion Factor(cf) = (Temp reading"c-25'c) x 0.03. ( /8,o°c- 25°c) x 0.03 = ill .21 (cf)
Converted pH = measured pH +/-the Correction Factor. 12,5pH (+/-) 6,2.1 (cf) = )a.2_ pH
24 Hour pH Test
Date: if .q, i- Time: 6:S.S Ain. Operator. .., lick; , -;
pH ! �.,4 Temp. 17 0 °c . {-:
Converted pH to 25.c /;3, 1 pH Y,a
Conversion Factor (cf) = (Temp reading"c-25°c) x 0.03. ( !7Q_'c 25°c) x 0,03 _ to) �`,(of) ..
Converted pH = measured pH +/_the Correction Factor. ) (cf) = /raj pH
Initial and 2 Hour test must be above a converted pH of 12 and 24 ur Est must be above a converted Everted PH of 11.5
Operator Signature for release: 7,, _ t ,,
Hauler Signature of Acceptance
Date/Time