WQ0000702_Residual Annual Report 2014_20150220

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City of Havelock, NC
2014 Annual Report
Residuals Land Application Program
Permit WQ0000702
NC 0021253

BIO-NOMIC SERVICES, INC.
k Specializing in today's needs for environmental protection.
516 Rountree Road • Charlotte, North Carolina 28217-2133 •
(704)-529-0000 • Fax [phone]
February 10, 2015
North Carolina Department of Environment and Natural Resourses
Division of Water Resources
Water Quality Permit Section
Non -Discharge Permitting Unit
512 N. Salisbury Street
Raleigh, NC 27604
RE: Annual Report, Land Application of Biosolids 2014
City of Havelock, NC WWTP WQ0000702, NC0021253
Dear Agency Representative,
Bio-Nomic Services, Inc. is submitting the monitoring and reporting information as specified in the
above referenced permit for the City of Havelock, NC WWTP of their land application of biosolids.
The report includes: 1) Certification Form, annual operations summary, facility and land application
contractor contact information, 2) Annual Residual Sampling Information Forms, 3) Annual Field
Summary Forms, 4) Laboratory Analysis Results, 5) Pathogen and Vector Reduction Forms and
Certifications, 6) Soil Analysis Data.
Bio-Nomic Services land applied biosolids to a total of (7) seven permitted fields in Pamlico
County, NC in 2014. A total of 151.37 dry tons(137.23 dry metric tons) of wastewater treatment
residual solids were land applied.
If any further information is required regarding this land application program, please contact our
office at 704 529 0000 for assistance.
Vona
rely
ld L. Greene
Land Application Compliance
Bio-Nomic Services, Inc
A Carylon Company

BIO-NOMIC SERVICES, INC.
Specializing in today's needs for environmental protection.
516 Rountree Road • Charlotte, North Carolina 28217-2133 •
(704)-529-0000 • Fax [phone]
February 10, 2015
Clean Water Act Enforcement Section
Water Programs Enforcement Branch
Water Management Division
U.S. EPA Region 7
Attn: Biosolids Center
Lenexa, Kansas 66219
RE: Annual Report, Land Application of Biosolids 2014
City of Havelock, NC WWTP WQ0000702, NC0021253
Dear Agency Representative,
Bio-Nomic Services, Inc. is submitting the monitoring and reporting information as specified in the
above referenced permit for the City of Havelock, NC WWTP of their land application of biosolids.
The report includes: 1) Certification Form, annual operations summary, facility and land application
contractor contact information, 2) Annual Residual Sampling Information Forms, 3) Annual Field
Summary Forms, 4) Laboratory Analysis Results, 5) Pathogen and Vector Reduction Forms and
Certifications, 6) Soil Analysis Data.
Bio-Nomic Services land applied biosolids to a total of (7) seven permitted fields in Pamlico
County, NC in 2014. A total of 151.37 dry tons(137.23 dry metric tons) of wastewater treatment
residual solids were land applied.
If any further information is required regarding this land application program, please contact our
office at 704 529 0000 for assistance.
Simerely
kLan
1'ld L. Greene
Application Compliance
` Bio-Nomic Services, Inc
A Carylon Company

City of Havelock, NC
2014Annual Report
Residuals Land Application Program
Permit WQ0000702
NC 0021253

r--
City of Havelock, NC
Residuals Land Application Program
2014 Annual Report
Table of Contents
1. Certification Forms, Annual Operations Summary, Facility and Land
Application Contact Information
2. Annual Residual Sampling Summary Forms, Residual Analysis
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
S. Pathogen and Vector Attraction Reduction
6. Soil Analysis

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0000702 County: h' Craven Year: 2014
Facility Name (as shown on permit): City of Havelock W WTP NCO021253
Land Application Operator: Bio-Nomic Services, Inc.
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes (J No - If No, skip Part A, and Part IB and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part -A.- Residuals Application Summary:
Total number of application fieldi s n the ennit: 28
R_ Total number of fields utilized for land application during the year: 7
Total amount of dry tons applied during the year for all application sites: 151.37
Total number of acres utilizes for land application during the year: 68.9
Part B -.Annual Compiance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Resources.
21 Yes If no please, provide a written description why the facility was not compliant, the dates, and explain orrective�act on
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Resources.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of flues and imprisonment for knowing violations."
Frank Bottorff, City Manager 4�,
Permittee Name and Title r print 1 ( S
r
(type p 1 � Signature of Permitt Date
-Z . /to
Signature of Preparer* Gj' Date Sign ure of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T. i 109 01�) _ _ .

City of Havelock, NC
WWTP NC 0021253
WQ 0000702 Annual Report, 2014
Land Application of Class "B" Biosolids
Aerobically Digested Liquid
Month
Amount Unit
Dry Tons
Unit
Metric. Dry Tons
Feb. 14
408,000 Gal.
70.10
DT
63.55
Sept. 14
534,000 Gal.
81.27
DT
73.68
Total 942,000 Gal. 151.37 DT 137.23

2014 Annual Report
Project: City of Havelock, NC
Facility: Havelock WWTP
304 N. Jackson Drive
Havelock, NC 28532
252 444 6421
NPDES:
RESPONSIBLE OFFICIAL:
ORC WWTP:
Land Applier and
Report Preparation:
NCO021253
Mr. Frank Bottorff
City Manager
PO Drawer 368
Havelock, NC 28532
252 444 6401
Art Hough
WWTP Superintendent
304 N. Jackson Drive
Havelock, NC 28532
252 444 6421
Bio-Nomic Services, Inc
516 Rountree Road
Charlotte, NC 28217
704 529 0000, Buck Stevenson

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0000702 Laboratory: 1)
Facility Name: City of Havelock WWTP 2)
Residual Source WQ # or NCO021253 3)
NPDES #: 4)
WWTP Name: City of Havelock WWTP 5)
Residual Analvsis Data
Environment 1, Incorporated
Parameter .
(mg/kg)
Conc.
Limit
m )a
Sample or Composite Date
2/10/14
4/28/14
7/14/14
10/20/14
Percent Solids (%)
NA
4.12
4.11
3.65
4.06
Arsenic
75
3.4
2.5
6
9
Cadmium
85
1.3
1.3
1
1
Copper
4,300
739
723
863
861
Chromium
NA
10
10
11
12
Lead
840
10
9.6
11
16
Mercury
57
0.24
0.48
0.52
0.56
Molybdenum
75
5
5
5
5
Nickel
420
7
8
8
9
Selenium
100
5
5
5
5
Zinc
7,500
1412
1565
1557
1640
Total Phosphorus
NA
16954
14436
15837
17445
TKN
NA
11335
17623
45831
44499
Ammonia -Nitrogen
NA
4853
5054
4145
4128
Nitrate and Nitrite
NA
3.79
3.92
5.61
3.87
4 For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties fors bmitting false inf rm tion, including the possibility of fines and i pris nmeent for knowing violations."
leldjlv��-11111-5
Signature of Preparer * ate
*Prenarer is defined in 40 CTF Parr Sn3 0(r) and 1 SA MCAr, 7T .I In2'16"
.7 ROO 1

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0000702 Laboratory: 1)
Facility Name: City of Havelock WWTP 2)
Residual Source NCO021253 3)
NPDES # or WQ#: 4)
WWTP Name: City of Havelock WWTP 5)
Emvironment 1, Incorporated
1\rJlY {1Nl L1- Jlu Y
Parameter
Sample or Composite Date
2/10/14
4/28/14
7/14/14
10/20/14
Aluminum
Calcium
35312
28101
35262
28730
40318
34643
42733
34141
Magnesium
2092
2357
2448
2107
Potassium
4002
4469
4501
3603
Sodium
3683
5513
3739
3912
Sod. Adsorp. Ratio
0.18
0.27
0.2
0.01
Surf. PAN
4371
6298
14585
10138
pH Units
6.7
6.4
6.3
6.7
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility o fines and imprisonment for knowing violations."
I
Signature of Preparer * / ate
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PO BOX 7085, 14 OAKMONT DRIVE PHONE [phone]'
GREnE M111_L E, N.C. 278.85-7685 FAX [phone]
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
ID#: 204 F
DATE COLLECTED: 02/10/14
DATE REPORTED : 03/28/14
REVIEWED BY:
Sample Sample
Sludge
Analysis
Metbod
PARANIETERS
#6 #7
Sample
Date Analyst
Code
PH, Units
6.7
02/12/14 TRB
4500HB-00
Total Residue, mg/I
33820 34020
02/11/14 CMC
2540B-97
Aluminum, (dry wt. basis), mg/kg
35312
03/05/14 LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
3.4
03/24/14 MEL
311313-04
Calcium (dry wt. basis), mg/kg
28701
03/05/14 LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
1.3
03/19/14 MEL
311313-04
Copper (dry wt. basis), mg/kg
739
03/05/14 LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
10
03/05/14 LFJ
EPA200.7
Lead (dry weight basis), mg/kg
10
03/21/14 MEL
311313-04
Magnesium (dry wt. basis), mg/kg
2092
03/05/14 LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.24
02/26/14 ADD
245.1 R3-94
Nickel (dry wt, basis), mg/kg
7
03/07/14 LFJ
EPA200.7
Potassium (dry, wt. basis), mg/kg
4002
03/05/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
03/25/14 MEL
31138-04
Sodium (dry wt. basis), mg/kg
3683
03/07/14 ADD
3111B-99
Zinc (dry wt. basis), mg/kg
1412
02/21/14 ADD
3111B-99
Sodium Adsorption Ratio
0.18
03/24/14 LFJ
Total Solids, %
4.12
02/11/14 CMC
2540G-97
TKN (dry wt.), mg/kg
11335
02/13/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
4853
02/13/14 ANO
350.1 112-93
Phosphorus, T. (dry wt.), nig/lig
16954
02/13/14 ALB
365.4 -74
Nitrate -Nitrite (dry wt.), mg/kg
<3.79
02/12/14 ANO
353.2 R2-93
Plant Available Nitrogen, mg/kg
4371
02/20/ 14 SEJ
Fecal Coliform (MPN), /gram Solids
103489 51189
02/11/14 CMC
9221E-06
Molybdenum (dry wt. basis), mg/kg
<5.0
03/05/14 LFJ
EPA200.7

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GT'eLnrilli . NC 27858
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MR, ART -HOUGH
WASTEWATER TREATMENT. PLANT
304 X. JACKSON DRIVE
HAVELOCK NC 285.32
PA %k ME, T K R S
P11, units
Total Residue, mg/1
Ahuni!ium, (dry wt. basis), ing/kg
Arsenic. (dry wt. basis), mg/kg
Cakium.(dry wt. basis), mg/kg
Cadmitun, (dry wt. basis), ing/kg,
Copper (dry wt.. basis), M&g
Chromium, T.(dry wt. ),mg/kg
Lead (dry weight Basis), mg/kg
Nlagne.sium (dry wt. basis), -nTg1kg
mcretjry (dry wt. basis), mg/kg
^. Nlickel (drys. wt. basis),. niafkg
(d t,
.Pqtassilun (dry
ry wt. basis), mg/kg
Selenium (dry wt. basis), n1gf1(g
Sodium (dry wt. basis), mg/kg
Z 'e- ry ing/4
111- #1 -wt. basis
Sod . imri Adsbrpti'011 Ratio
Total Solids, %
T14PN (dry wt.), nig/kg-
Ammonia Nitrogen '(dry IYO,mg/4 Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/ka,
Plant Available Nitrogen, mg/kg
Fecal. Coliforin (MPN, /gram Solids
Molybdenum (dry wt. basis), mg/kg
Sample
#6
36460
35656
DATE COLLECTED: 04/28/14
DATE REPORTED -. 05/19/14
REVIEWED BY./_�
Sample Sludge Analysis Method
#7 Sample Date Analyst' Code
6,4
04/30114 TRB
45001-IB-00
35720
04129/14 XIDD
2540B-97
35262
05/06/14 LFJ
EPA200.7
< 2.5
05/07/14 MEL
311313-04
28730
05/06/14 LrkJ
EPA200.7
1.3
05/15/14 MEL
31,13B-04
723
05100/14 LF.j
EPA-200.7
10
6510/14 LFJ
EPA200.7
9.6
05106114 MEL
311313-04
2357
05106114 LFJ
EPA200.7
0.48
05/08/14 INITIVI
245.1 113-94
8
05/0,6/14 i,rj
EPA200.7
4469
05/06/1.4 LFJ
EPA200.7
<5.0
05/14/14 MEL
311313-04
5513
05/06/14 NITM
3111B-99
1565
05/07/14 MT M
3111W99
0.27
05/15/14 LFJ
4.11
041,2911,4 CMC'
2540G-97'
17023
05/05/14 ANO
351.2 R2�93
5054
05101/14 ANO
350.1 R2-93
14436
65/05114 ALB
365.4 -74
< 3.92
05/02114 ANO
353,2 R2-93
6298
05/13/14 SEJ
19599
04/291.14 MDD
9221E-06
< 5.0
05106114 LFJ
BPA260.7

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MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
Sample Sample
PARAMETERS #6 #7
PH, Units
Total Residue, mg/l
Aluminum, (dry wt. basis), 'mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite .(dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Fecal Coliform (MPN), /gram Solids
Molybdenum (dry wt. basis), mg/kg
31540
10397
30040
5011
ENE [phone]
FAX [phone]
ID#: 204 F
DATE COLLECTED: 07/14/14
DATE REPORTED : 08/11/14
REVIEWED BY:
Sludge Analysis Method
Sample Date Analyst Code
6.3
07/17/14 TRB
4500HB-00
07/15/14 LW
254OB-97
40318
07/18/14 LFJ
EPA200.7
6
07/22/14 CMF
3113E-04
34643
07/18/14 LFJ
EPA200.7
1
07/21/14 CMF
31138-04
863
07/18/14 LFJ
EPA200.7
11
07/18/14 LFJ
EPA200.7
11
07/27/14 C1VIF
3113B-04
2448
07/18/14 LFJ
EPA200.7
0.52
07/24/14 MTM
245.1 R3-94
8
07/18/14 LFJ
EPA200.7
4501
07/18/14 LFJ
EPA200.7
<5.0
07/31/14 CMF
3113E-04
3739
07/22/14 MTM
3111E-99
1557
07/22/14 MTM
3111B-99
0.2
08/11/14 LFJ
3.65
07/15/14 LW
254OG-97
45831
07/21/14 ANO
351.2 R2-93
4145
07/17/14 ANO
350.1 R2-93
15837
07/21/14 ALB
365.4 -74
5.61
07/18/14 ANO
353.2 R2-93
14584
07/22/44 SEJ
07/15/14 LW
9221E-06
<5.0
07/18/14 LFJ
EPA200.7

Environment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Pox 7055, 114 Oalanont Dr.
. Pate —A— of'
l rlo c0
anviro.:mentl inc.com
DISINFECTION
CHLORINE NEUTRALIZED ATCOLLECTION
Phone [phone] ° Fax [phone]
CHL0I2INL
—
CLIENT: 204 F Week: 30
pH CHECI<(LAB)
UV
CITY OF HAVE,
N0NE
P
P
P
P
P
P
P
P
P
CONTAINER TYPE, P/G
MR. ART HOUGH
WASTEWATER TREATNIENT PLANT
CHEMICALPRESERVATION
304 N. JACKSON DRIVE
IJ
A
A
A
A
A
A
A
A
A
A
HAVELOCK NC 28532
A - NONE D -NAOH
—
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cn
(252) 444-642I
L1 U
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COLLECTION
¢
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cc
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SAMPLE LOCATION
DATE
TIME
Sample #I
_1 -1
C)qq
2
CLASSIFICATION:
WASTEWATER (NPDES)
DRINI<INGWATER
Sample #2
-1 u -I
1050
2
's
Sample #3
_
-14 -I Li
109i
2
Sample #4
_l y-I
I OS2
2
DWQ/GW
::.
:..;...
Sample #5
-tl-1-
6 C}S
,�j
2
<:
SOLID WASTE SECTION
Sample #6
-I
w54
�(
2
}
'
Sample #7
2
CHAIN OF CUSTODY MAINTAINED
DURING S PMENT/DELIVERY
Y N
Sludge Sample
- j i-I LI
0 �
(�
5
<:.
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....
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-
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SAMPLES COLLECTED BY:
(Please Pdnt)
:Denn"� 0(�1
SAMPLES RECEIVED IN LAB AT °C
RELIT UI ED BY (y IG.) ( MPLER)
DATFITIME
RECEIV (SIG.)
DATE/TIME
COMMENTS:
-I4-I44
411/i
R � QUISHED BY (SIG.)
DATE(TIME
RECEIVED BY (SI
DATE[TIME
RELINQUISHED BY (SIG.)
DATEITIME
RECEIVED BY (SIG.)
DATUTIME
.a u r it s n, tf e F L P _ _ I

if-aw [MEW �Jodo
)h 705, 11�1 vrlYflVT Ds,,i1/E. PHCtV�
FP
IViLLE<I�1'�:`2(835'-°10Ei5�>��
ID#: 414
CITY OF HAVELOCK(SLUDGE)
MR. ART HOUGH
WASTEWATER TREATMENT PLANT DATE COLLECTED: 10/20/14
304 N. JACKSON DRIVE DATE REPORTED : 11/26/14
HAVELOCK ,NC 28532
REVIEWED BY:
Sample Sample Sludge Analysis Method
PARAn1ETERS #6 #7 Sample Date Analyst Code
PH, Units 6.7 02/23/14 TRB 4500HB-00
Total Residue, mg/1 31200 33060 10/21/14 CMC 2540B-97
Aluminum, (dry wt. basis), mg/kg 42733 11/04/14 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg 9 11/21/14 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 34141 11/04/14 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1 11/22/14 MTM 3113B-04
Copper (dry wt. basis), mg/kg 861 11/04/14 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 12 11/04/14 LFJ EPA200.7
Lead (dry weight basis), mg/kg 16 11/25/14 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 2107 11/04/14 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.56 10/30/14 MTM 245.1 113-94
Nickel (dry wt. basis), mg/kg 9 11/04/14 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 3603 11/04/14 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 11/17/14 LFJ 3113E-04
Sodium (dry wt. basis), mg/kg 3912 11/04/14 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 1640 11/04/14 LFJ EPA200.7
Sodium Adsorption Ratio 0.01 11/07/14 LFJ
Total Solids, % 4.06 10/21/14 CMC 2540G-97
TKN (dry wt.), mg/kg 44499 10/23/14 ANO 351.2 112-93
Ammonia Nitrogen (dry wt.),mg/kg 4128 10/23/14 ANO 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg 17445 10/23/14 AKS 365.4-74
Nitrate -Nitrite (dry wt.), mg/kg <3.87 10/22/14 ANO 353.2 R2-93
Plant Available Nitrogen, mg/kg 10138 11/03/14 SEJ
Fecal Coliform (MPN), /gram Solids 44872 48665 10/21/14 CMC 9221E-06
Molybdenum (dry wt. basis), mg/kg <5.0 11/04/14 LFJ EPA200.7
C:

Lmvironmew CHAIN OF CUSTODY RECORD
P.O. Box 7101' -, ., Oakmont Dr.
Greenville, NC 27858 Page i of i
enV uvnilieH t 1nC.Com
Phone [phone] d Fax [phone]
DISINFECTION
��
CHLORINE NEUTRALIZED AT COLLECTION
CI4LORINE
�
pH CHECK (LAB)
CLIENT: 414 Week: 43
UV
P
P
P
P
P
P
P
P
P
CONTAINER TYPE,P/G
Y OF HAVELOCK(SLUDGE)
NONE
VIR. ART HOUGH
XASTEWATER TREATNIENT PLANT
iO4 N. JACKSON DRIVE
A
A
A
A
A
A
A
A
A
A
CHEMICAL PRESERVATION
3AVELOCK NC 28532
z
�o
A -NONE D-NAOH
�
252) 444-6421
z �
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M
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3
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COLLECTION
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SAMPLE LOCATION
DATE
TIME
( Sample #1
C) ''
r6 7/U
.,,S
2
CLASSIFICATION:
Lj WASTEWATER (NPDES)
DRINKINGWATER
( Sample #2
0 j
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2
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Sample #3
0-�,v
A
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Sample #4
6 ' Qi
2
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Sample #5
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2
DWQ/GW
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j
Sample #6
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2
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Sample #7
7
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CHAIN OF CUSTODY MAINTAINED
DURING SHIPMENT/DELIVERY
Sludge Sample
%Q
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SAMPLES COLLECTED BY:
(Please Print)
SAMPLES RECE D IN LAB AT Q ` °C
RELINQUI 'ED BY ($IG.) AMPUE
DAI E/TIME
i
I D BY (SI `_
DATE111ME
COMMENTS:
I
% v� / ld l s
ILIl �G
RELINQUISHED BY (SIG.)
DA ME
RECEIVED B SIG.)
DATEMME
RELINQUISHED BY (SIG.)
DATE FIME
RECEIVED BY (SIG.)
DATE[rIME
PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a T" for composite sample or a "G" for Q 2
FORD! #5 Grab samnlp in the hlnrkS abnvp fnr pa(:h nar Mefar rpntigFtarl

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock WWTP WQ Permit #: WQ 000072 Field #: SF PA24A Acres Utilized: 10
Land Owner: Spencer Farms Annual Dry Tons Applied:26t$ir12;,:.;E" :_-;;;?;'u?-° ':•`-ia,;,;.:;
Site #: Acres Permitted: 10
Operator: Spencer Fames Predominant Soil Series: Yonges Cation Exchange Capacity (non 503): _
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN: _
w
o ��
y a
m o
A
Volume applied (enter
one) Solids/ Liquid
Cu. Yds Gallons
ova Solids
Volume
Applied
per Acre
(Dry
TonslAc)
Residual Sources
DES #, W #, Fert.,
Q
Animal Waste, etc)
Soil Cond.
D Wet,
(Dry,
Moist)
Precip.
Past 24
Hrs.
inches
a
,fl
o
'o'
o
C
o
„
*
5
11 "
*
• -
TKN
m /k
9 9
Z 9
iX
o w
o
0 �.
m 9/k9
Nitrate and
Nitrite
m 8lk9
PAN Applied
]bs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop I
Crop 2
2/14
48000
4.12
--' 0.825,1-
NCO021253
Dry
0
S
0.5
0.3
11335
4853
3.79
- , 7;216a: *
::: a NA `:
Rye
9/14
120000
1 3.65
'4-,I:826,
NCO021253
Dry
0
S
1 0.5
0.3
45831
4145
5.61
'j753.274''
; -NA:;`--'
Rye
" '-0:000":=
;,10:000' �
j s,0:000 zl
!V0004"
":O:000, x `
• ;:'0:000';[;
.0.000'a
+0,000`.`r
.0.000:,
r,-^0:000i:i
:., .
"' •; -:„x.
:.•,-.,,:=n-..
,At ,`-�•':
h FORM FSF su to this form
Residuals )�
Applications totals on FORM FSF supp (attach O pp
TOTALS,
;o
<t.ies000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
<60'4s9
r 'Ot000 _
Lime Applied
Annual lbs/acre
30:028
�.� . -„ k:
=.O:OOti ; r
: 4:37-V "
_
-A'057 '3"
``
'" 0:057,<':;
: - 0:002'
; 0:027"-,�
3.0 041- F;
_ 0:027u
't8;01 6 ;`
="85 8 -
1 ]
s
Date
1 s/ac
b
Prior Years Cumulative Ibs/ac
0.018
0.01
5.247
0.109
0.064
0.007
0.037
0.064
0.028
10.091
Current Cumulative lbs/ac
a°0.046s�
-:'0:016_;�,;
--::9.618.,_..-
�.0.166,;:-,
�-.0.121fw
.-. .....:
��"0.009 .-e..
r0.064�,�
µ--
- 0i05zy,`.;
:0:055 ;ia
''.'t8s167:v>
Permitted C. P. L. R.****
36.6
34-8
1339
267.9
15
375
89
2500
Permit PAN Limit 1 sU2nd Crop
=�9
--i cernry,- unuer
oI iaw, Inal MIS UUCUIIICUL WaS pl CPHI-CU UIIUCI
Applier
�VIAIIIII Vl- 3UPWI VIJI"ll All 4V 1-14— —AA u .OJOL-11 —.r,.— w waiu. A.— yuuu—..
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
City of Havelock W WTP Total Dry Tons Applied (Annual): QS s' ' 26 5WIN ;` s
Facility Name: tY ���`�
Permit #: WQ 0000702 Cation Exchange Capacity (non 503 only):
Operator: Spencer Farms Owner: Spencer Farms Predominant Soil Series: Yonges
Acres Used: 10 Acres Permitted: 10 Site #: SF PA2 Field #: 1A
r _.xa-._. A .....-...:., "..- /II......v AT..r.J......A Ta4o1 U6a 6nrae nea ma/Ira 0/ Cnlide nee Raw Percent 91:
Sample or
Com-posite
2/10/14
4128/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739
1 723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
phorus
16954
14436
15837
17445
Total
c
DT/Ac./
App. Event
0.83
0.00
1.83
0.00
Arsenic
n 0.006aP,
0:000,?
k;0.U22r;°i
,t=0:000 F
,-;0'QOO;
0:000
6000
.;,0'.000
"'
� 0000 <,;
0000r.
0:000 �
0:000"."
0.028
Cadmium
=,`0 002.,
0,000
' 0 Ob4, ;.
._ 0 000
k;0i000,;;
OOOr .
0:000.
0 006"�
: 0 OOO, is
"x_0 OOOp:
r 0;000.
O':000
;0.006ia
Copper
,
1 219,
; ,
0 000 ;
z 3" 152r,:
t :0 000.;
0:000,
„0
`"`' 0A00� ;
� O.000 ,
.� , 000
0.000 a
" 0:000
0 OOOn
,;,0:000<4:37I
s;
Chromium
04U
0:000
,,;Q 000:
", 0,000.,:.
'.,?0 000,
';' 0 00"'-i
� -000
w,.0.000t=
"
0.000
Q`.000k
„i3O:057 "
Lead
<°;'; 0 017, ,
r•__. rw
`,. ;0:000;
_ .:
x 0 040
q_ ... �F
0:000€ ,
3 -.
x 0?000
Q ,,
,0 000,,
,,,.0:000 "-
9 0 000".v
4 0 000 :
; „<OiQ00a
0 000 -;
0 000 ;
i 0A57 ,�
Mercury
.
`."`0 000 -
0.000`
.EO 002 ;,;'
; 0 000
""6600 4
„s0':000 ,.,
, ;0:000,8
; 0 000„
0 QOOs,'
A.000:
,0:000
0`000..
Mol b-
'``'`i.e ,
.c.- ,• a.
018 "
sr
000 '
'4z
0000:000sa
`'k,
{�. €
000 =
„'z"x' ­yw i
0
S'
000
000
0 OOOr
O 027
denum
' `§;0 008
0 000 y
0
0
quay .0 OQO
p 0
fi
," h0 s
000
w0,
0
Nickel
`0 012 x
x, 0 000
,0'029� ,
„ ,0 000
0:000 ,
, x0.000 t.
.0 000
f ,:0 000,, ,
"00 0K
� 0 000 ;
e 0.600`,
� `O,:000r� -
Selenium
y= 0 009w,
.: ,0 000,,.,.
`;w,_f0 018!
,,,k0 000R,
;. 0:000;,=.s
;,$r; 0:000, „000.,,x
ti .0 000
;`OM?,0
000
MOOOw'„:
,
`
'.s,0.000,
b:000
OWN",
0 000
0 000„
0000
0.000"
8:016
Zinc
?>2 330 .;
? 0 000 ;,
. 5 686,. y
0.000=`
.
,Os000. ,
.
Total Phos
":
`
0
t 27 974
0000 .
57 837
0 O00 s
0 000
0 000
Kk 0 000'
0 OOOg
000
0 0000�00
phoms
a. "
#,
E
x
s
m "xs,l
x, M1u
.
:x�
"1 certify, under penalty of law, that tuns document was prepared under my mrecrion or supervrswu II al"l'UrUALCC W..0 ]l JyJWW ucJsucu w .JJ..
Signat6A of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock W WTP WQ Permit #: WQ 000072 Field #: SF PA2-1B Acres Utilized: 9.3
Land Owner: Spencer Farms Annual Dry Tons Applied: 26;7464r'<sw w K 5;. r^ .' • Site #: Acres Permitted: 9.3
Operator: Spencer Farms Predominant Soil Series: Yonges Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN:
,.
Volume applied (enter
Volume
Precip. y o ❑ 9.. � Nitrate and PAN Applied (
Residual Sources Soil Cond. pyst 24 b w �f R TKN o w
Name of Crop Type
Receiving Residual
v a
O
one) Solids/ Liquid
u
/o Solids
Applied
Acre
�? Nitrite lbs/acre)
(NPDES #, WQ#, Fert., (Dry, Wet, Hrs, o w . -••
Application
Crop 1 Crop 2
A
per
(pry
,
Animal Waste, etc) Moist) a 0 * o' " o• mg/kg mg/kg mg/kg Crop 1 Crop 2
Cu. Yds Gallons
Tons/Ac)
inches °
2/14
1 60000
4.12
r.1r1Q8i'r'
NCO021253 Dry 0 S 0.5 0.3 11335 4853 3.79 , 9s698%w`, NuNAr w
Rye
10/14
108000
3.65
1768
W0021253 D 0 S 0.5 0.3 45831 4145 5.61 „51655?
Rye
r0:000r' u.
A.000'' .' ;aA000� "'
r0.000: rv°'
0.000;';4�4VIJ01000;'111
•Oi000'wR. .'r.0':000 :,
iAo. 000 1'
11,0.000k-*0:000;�sf
.t: D.DOD .:
r.y0:o00z
r ;, - <: ,..
, a;ta�:„;.;;t:=-•
s;
.
3 �'-;a'
Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): ;; .;„il..."_„ d� 'F `�' ;a.•<:
ftbs000
As
g 61254, 0 000 - ;i
Cd Cu Cr Pb H Mo Ni Se Zn P
died,..
Lime Applied
P
TOTALS
Annual lbs/acre
Is* , ,. o ,
, �0:029
i-= 0:0064+ x: 4:689: =0 061 } r11.061't , AA02 ,z 0:029• _ 0 044, ,0029 8.635 r.; 93 570
� :... ,: � ��� �. , � <<, ., �, �,.: r .., _ ...
0.01 5.27 0.113 0.065 0.007 0.037 0.067 0.03 9.978 y ,
016 '9;959 0 174 - 0 126' �. 0 009_ 0 066 O lai l0:059, .,i8 613
Date Ibs/ac
Prior Years Cumulative lbs/ac
x
0.018
Current Cumulative lbs/ac
0:097
Permitted C. P. L. R****
36.6
w0 • ,•
34.8 1339 267.9 15 375 89 2500
Permit PAN Limit 1st/2nd Crop
r.....>
....... .........
*that
ao o.l�*..n..al:fiPd nersnnnel
nrnnerly
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
to *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate
UUU

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name City Total D Tons Applied(Annual):
Ci of Dry PP
Permit #: WQ 0000702 Cation Exchange Capacity (non 503 only):
Operator: Spencer Farms Owner: Spencer Farms Predominant Soil Series: Yonges
Acres Used: 9.3 Acres Permitted: 9.3 Site #: SF PA 2 Field #: 1B
irr___.__ ➢,r..a..r_ --A T..a..t DL.. ..L.. ..a .r/4o o/ Cnlidc nep Raw Porrrnt #li
Sample or
Com-posite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739 1
723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
phorus
16954
14436
15837
17445
Total
o
DT/Ac./
(A
App. Event
1.11
0.00
1.77
0.00
Arsenic
.0:0081.y
'.`; O 000 ;r.
,'"„A 021
> A;000""
0:000 t
u0,i000" "
0 000,"„
0 000" ;e
- ""0 000,
_. =0:000
. OfObO"
w0000
0`029
Cadmium
;0:0034'
to 0 000 i
004,,;
;'r;".0:00' t
; 0 000,,;
000;_.
, 2'0 OOp ..'..
0 000 ;:
0 000"{
O OQO: -
0 Q00
0;000: a
` ,0 006 k
Copper
," .0
_',,0
0 000;"
0 000
" 0:000"
Chromium
0 022
0 000
0 039
0 000
0 0066
0°000
Y�0 000
ha 0 000
lAW
n0 000
L "0:000
0 000"
0"061
Lead?0.022.;*.,;0'000�w�-0032
�0000,a
,,,_0:000
;0:000„
0000,'''e"0;0¢0.`�aQOOOf
"_,0'06.1
;
0
` 0;002kxv
0 000 _
'
0:000,
-0 000
`0 000
k O000
0 000 . ,
�0:000
go., 002$
Mercury
Molyb
,` :0:001
0
z Q00, ;"
O'OI8 `s
e, ,
_.0.000+
000
0 0000
,"0`900
000"
' 0 000
0 000
0"000
0 000'0
000
0`029
011
0000
0('0
0 0deman
,-
a
t
..
f .0
NickelAQ°
Selenium
O,1xh .„
0 000 s
0 018
:
0, 000,;
,0:000
Or00Q
0 OQO
„0' 0 O.
0 000
0�000
0 000
0 000
0 029
Zinc
: c-,0
:v'3 129
. a.
+,: 0 000 ;
..
: 5 506
,O:Q00,
" 0:000,?,
r „0:000 ,
_
0 000
" 0"000 �,
��
;� 0 000
0 000 ` "
. 0:000
, :
. _,0.000s'
k.. j3
tY'xa°S
, r _
d"
,0'060
Total Phos
37 570 r
0 000 "
SG000
0 000
0 0000
000
0 000
i 0 000
0 00�
0 000€
0 000
0 00¢
f 93 57OP,
phorus
r.
sr�
'.
3t
"1 certif and r penalty of law, tnat LmS aocument was preparcu unuer my urrccuuu ur aupo■ v.a.vu .n -- ua... o o u.... 'J �..... .. �.6 .. .
.� 2 .a 5
SignaturUfLandApplier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City ofHavelock WWTP WQ Permit #: W0000072 Field #: SF PA2-1C Acres Utilized: 10.3
Land Owner: Spencer Fauns Annual Dry Tons Applied: �20 353t�, Site #: Acres Permitted: 10.3
Operator: Spencer Farms Predominant Soil Series: Yonges Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN:
Volume
Precip. y o K z Nitrate and PAN Applied (
Name of Crop Type
s.
o
Volume applied (enter
Applied
PP
v S
Residual Sources Soil Cond. past 24 v " TKN o w
o Nitrite lbs/acre)
Receiving Residual
g
q
o
one) Solids/ Liquid
o
/o Solids
per Acre
DES' #, W # Fert., Wet, �' o o �.
� Q , �rY, Hrs. o � * � * ...
Application
Crop 1 Crop 2
A
(Dry
Animal Waste, etc) Moist) ao' * �. * mg/kg mg/kg mglkg Crop 1 Crop 2
inches ❑
Cu. Yds Gallons
Tc)
ons/A
0 o
2/14
60000
4.12
ril'.00U-�
4853 3.79
NC0021253 D 0 S 0.5 0.3 11335 . �8757 " ;.,N' ; �
R e
10/14
66000
3.65
��,k0.9.7,5.; �.
NCO021253 D 0 S 0.5 0.3 45831 4145 5.61 28:4A7 � :`�NKf't'
R e
0:000 i z0.000=1i
K0:000 „'� o A: 000"'�
,0:000"&
�;i=s0000S4000;;re.'
.'
0:000te;
uf0:000-'rt"
-�:0:000;
Residuals Applicationsto this form totals on FORM FSF supp (attach FORM FSF supp ):
`
`
T
'' "0"o00`=
Cr Pb Hg Mo Ni Se Zn P 9 37:2o4s
Lime A lied
pp
TOTALS:
::;rw .; _. z6000
o
.
As
Cd Cu
d `• ; : Q020 5:863 64824'.
Date lbs/ac
Annual lbs/acre
`2Ob4°1R` : °0:04i<f, 0.001 0;020> ti ;';0:030 t:.
0.011 5.489 0.124 0.073 0.005 0.033 0.079 0.041 9.005
Prior Years Cumulative lbs/ac
0.022
Current Cumulative Ibs/ac
�,,0.041�
O;Qi6� ��Ar,8;651.0 165 ,0114 t 0.006,fi 0053- 0:309;,;M0;06F t1d:868w� ;,
Permitted C. P. L. R.****
36.6
34.8 1339 267.9 15 375 89 2500
Permit PAN Limit lst/2nd Crop
a—E .od th.+ n —1M—di narcnnnel
nrnne.rly
" 1 ce� unaer pertaig oI 111W9 L11s1L LHIS UMULILGLLL W03 p■ opa. w uu.+......J
*Application Method: S - Surface, IN - Injection, INC - Incorporation
t/ ©66 's **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier ate *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate
�� Ci'Ll -

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Havelock W WTP Total Dry Tons Applied (Annual):
Permit #: WQ 0000702 Cation Exchange Capacity (non 503 only):
Operator: Spencer Farms Owner: Spencer Farms Predominant Soil Series:
Acres Used: 10.3 Acres Permitted: 10.3 Site #: SF PA2 Field #:
A lha.. M.... , Mnfolc n,.d Tnf. 1 Ph-hnr..e nce mo/ko_ o Cnlids use Raw Percent #):
Yonges
1C
Sample or
Corn- osite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739
723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
photos
16954
14436
15837
17445
Total
c
DT/Ac./
H
App. Event
1.00
0.00
0.98
0.00
Arsenic
==,.0:007,::.."�.0,000;;.s:<:0:012�_,=`are=0.000,,;:;i�0:000�',;"'-<0:000:''s
e�:0:000:;�;
�„0:000<`��:
-
Cadmium
,; ;0:003
-.`.E.O 000 =i
1.0'002_ E
4%:0:000'
0.0_00- - .
= 0:000 "
-� 0 000,,_
:=:0 000
=' 0:000 "
, :,0:000
4 0:000 %
.0:000 ,
tt :0`.005
Copper
'1.i479i':,-
; : O:000:;i;.:;={1
683` _
;0:000;«r
v,
's;0:000,,,
r„;,,
; ;.0.000`;
:;:.0`=0003
0;000
,
=H0.000. ;
„r -
>,0,000 '
-;
. A:000x'.
r0:000' :
_ ,
'3€162;i;.
Chromium0:000
, ,
,.=0 OOQ,
, : 0"000„_;
' <0;000
_' 0.000Z
lk0:000
0:000.
„ 0:041 Via.
Lead
a0:020 ,
: O OOOi
<%."Oi021; J
:. fi0i000; s
,4k 0`00
;::, 0.000:;
;; 0:000; A't
r 0:000 4
0.000:(
r ,,6:000
0:000
r0 000
Mercury
`�;0:000 »
;V= , 000 `
,z aQ:001'
0`.000
0:000 `
a.0:b00"
0:000 ':
r`z 0 000 ", a
6 000 `•_,
,t O:OOQ_ `i
„ 0 000,E
0.000
O'001 e,
Molyb _
„y,,",
y.,,.
o:oio•:
:
q:000°`'
'_:j b
b:oio
�: J'a:'.,•
/r y,r S,:;..`.'.v',„.j'�.-
;o:000
e-k'u^. a
o:oob
:k.:.: -
o:aoo
-•=-S
zo'.000
.=Y
�. fi-, w'u•:
0000.
. u,'-
40:00o z,
3y" .1:.. }
F
Mn
z-:° r
,ti-y•.iE;:',�7
?`
denum
=�;. :;?j�
�`�--<,
;,
-
�,;,
-- .�-� .
-
-
-
-
Nickel
'=.z
�0:0.14-�"
:0:000�'.�`
�0:016;;
n= 4i.
--:0:000.,,w
s.
=0.000-
�:
��0000";
<_^��;0'
� v0:000';,
.OQ 0.�,:
'0:000:*�
�
:�0:000..-'
�,
r0:000,3;
Selenium
, y0:000
000,, •
,?,0 000.,..0:000
n-O:000;t ',
;`i0000;
0`020`c';
Zinc
,:;2ss827q ,
.. 0:0. OOs '
?3 036i
0.`000
b_ :b00''=x
t0:000 ,
` 0:000'
M: 0 000„=-1
,_, 0:000` ;
Q OQO,,;.
,y10:000�
< 0.'000
'
At
Total Phos-
^ =�_
r
33 942
:0 000
30 882
r
0 b00
a_
0 Ob0
0 000
" 0 000
0 000
0 000�
"0 OOOr
0 000
�0 000 t
photos
2.. 'f:},
z3.,: S..
�t•P'. F' rt
,M u;= =
_ h
,
,
.
N_. •_
'.',
;_
'-fix tbraC
i;
,. k.
-
"I certi y, un r penalty of law, that this document was prepared under my direction or supervision ioG`accoroance wrcu a system ueslgucu w assu. c
!� L 5
SignaturOf Land Applier ate

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock WWTP WQ Permit #: WQ 000072 Field #: SF PA2-ID Acres Utilized: 11.8
Land Owner: Spencer Farms Annual Dry Tons Applied: 73-53182k3 „-,<y ;T t ` sx t Site #: Acres Permitted: 11.8
Operator: Spencer Farms Predominant Soil Series: Yonges Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 . Crop 2 Name: Crop 2 Max. PAN:
c
Volume applied (enter
Volume
Applied
Residual Sources
Soil Cond.
Precip.
Past 24
Y
4 �
o
w
o
ay
TKN
a
o m
Nitrate and
PAN Applied (
lbs/acre)
Name of Crop Type
Receiving Residual
o
one) Solids/ Liquid
o
/o Solids
PP
per Acre
(NPDES #, WQ#, Fert.,
(Dry, Wet,
Hrs.
o w•
w
*
o
a '•
Nitrite
A lication
PP
Crop 1
P
Crop 2
P
Crop 1
P
Crop 2
P
A
(Dry
Animal Waste, etc)
Moist)
inches
°* o'
} o'
m /k
9 9
mg/kg
m
mg/kg
Cu. Yds Gallons
Tans/Ac)
o
0
0
2/14
78000
4.12
r1=136°ti.;
NCO021253
D
0
S
0.5
0.3
11335
4853
3.79
:;9:93�1
tiy'9NA S=:'
Rye
9/14
144000
3.65
r"3,1 857 ;
NCO021253
D
0
S
0.5
0.3
45831
4145
5.61
'S4:'1.7,7�.;
:NA
R e
Y,fo 000 :ae
y0c000= .
X"'A000
L00.000- cnr`Ot000`y'
m.0:000q;
.'0:0ooi;'
s= _`";;. 1,•' "rks "
`; ;
Residuals Applications totals on FORM FSF su attach FORM FSF supp to this form):
. _z"a=:`
Cu Cr Pb Hg Mo Ni Se Zn P 64r1i'4;: ;.:;o 000`<a
Lime Applied
TOTALS: o zzz000 :
As
Cd
0 030
��„
0 064+ ;0 002 "0„ 30, 0 046 0030;.` ° °' 899,1 :' 9T:33.8
" ' ' ' ' 0 064 .W 0
"A:407=e 4;884
Date lbs/ac
Annual lbs/acre
,•
. , ..
: ; _ .. _ .,
r_ .. �, _ . ,, ,
0.01 4.839 0.118 0.065 0.005 0.029 0.074 0.038 7.876 c
�s
Prior Years Cumulative lbs/ac
0.02
Current Cumulative lbs/ac
0:050"
0�017�--„9.723,,, , 0 182 0 129 , 0QO?_ .; 0059, 0,.10 ,0;068 �s16:867:;
Permitted C. P. L. R****
36.6
34.8
1339
267.9
1 15
375
89
2500
Permit PAN Limit 1 st/2nd Crop
.�"_ ...a ..d a..., o �Mn♦ .. nl.�nd n rennnal
nrnnarly
--1 cermy, unahrpenairvOl la , Iflat tnlS UUCUUMIL Was PrcPa. oU U11Uc. .Uy UA.11000 v. .-P— 1— ..
/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
6 0&5 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R: Cumulative Pollutant Loading Rate

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Havelock W WTP Total Dry Tons Applied (Annual):
Permit #: WQ 0000702 Cation Exchange Capacity (non 503 only):
Operator: Spencer Farms Owner: Spencer Farms Predominant Soil Series:
Acres Used: 11.8 Acres Permitted: 11.8 Site #: SF PA2 Field #:
. ITT...._... 1%4_ 1......a •rs..i U6..o..6n—, ..moo mn1tra o/ Cnlidc nce Raw Perrent #l!
Yonges
1D
Sample or
Com-posite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739
723
863
1 861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
phorus
16954
14436
15837
17445
Total
DT/Ac./
App. Event
1.14
0.00
1.86
0.00
o
(A
Arsenic
0:008-;
ai0`OOb
;`a'.>a0;022;;-
000$;
:_ O'.000.
0;000:.,°t'0006
'
." 0"000 3
0:000
0 030 k:
Cadmium
0 003
,{
�r, 0 000. 5
; "0 004.
,0
� 0 00,0
! 0:000,
0.000
', �0 OOO
„ 0 000,„
0 000 �
- 0 00Q, "
0:000 ,
' 0:000,
0 00Vq
CopperO'000
, ..
0 000000
"
0 000 "',
- A 000
0`000
0 000� :.
k 0.000, '
. 4 884 .:
Chromium
,�0 023„
`. 04i 4
;
;. 0 000,
000'
0 000�:,,
� 0 C
0 000;=
0 000 ,
._ A�OOOx
Lead
„ , .:
=�0 023`
��0.000 ..
„0
„„,Q000
„
,u;_0 ,
7-7—
,=0000v,�0
000
-0 000;=
0.0,00'
"0 000".-
`.Q:000 '.
:0'064-W
Mercury
O'001
0 000
: 0 002
`` 0:000„,
0.000 .,
0:000-' - .
, 0 000 -
010 =
0 000 `
0 000 "
.- 0 000g
:. 0:000i
01 002
Molyb0
Ol 1�>0
;>
00�00
019
.:. , ,
0 000.0
000�
0 000;
0 000
0 00�0
0 000� `0000
0 030 -
de
,, r ,. ,..:>-
��. ttr ,
r'
�,. ��
,.,.
A , . ....
T _k:.
Nickel
`0 016.3
0 OOQ
0:000',
`0.000*.,
, .;0:000 ,`
OOOQ .
.. 0,000 - .
_ 0 000
0 000
F 0 000, ,
. ,;0 046
Selenium
0,11;
000 - s
=,;.,0 019.
0.000
0000 �„
„n 0:000
b 000.,E
�0 000.
�0 000;
O 000
0 000
Zinc
.•�y0
3 208,:
�1;�0
0:000; `=
•
5: 783;`
,w
0 OOQ
;, �;
O':000t
0 000 r�
� � .0.000 �
st 0 000,
0 000
00000
r,
d°''
,
i t..a,,
:O:Q00,
-`' ,'z`r
'
• : '•,z
y,s �'
s,�'
`x..y-
."
Total PhoS
38 519
' 0 000
58 819
0 000
0 000,
.afi„a-cs
: 0 000
0 000
,, 0 000=
6- 000
0000
0 000
0 000
97t338s
phorus
-
k
ka x
v
��
t-
...`sf9
"I cerfi y, un penal of law, that tuffs document was preparea unaer my arrecuon or supervs,Z"n
cwraaucoQ�
Signatur,of Land Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock W WTP WQ Permit It: WQ 000072 Field #: SF 1`A2-1E Acres Utilized: 10
Land Owner: Spencer Farms Annual Dry Tons Applied: 16 4932; Y _ ' „`'x`' mr= ': " Site #: Acres Permitted: 10
Operator: Spencer Farms Predominant Soil Series: Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN:
Volume
Precip. a - o z Y Nitrate and PAN Applied (
Name of Crop Type
o w
Volume applied (enter
Applied
pp
-cs 5
Residual Sources Soil Cond. pit 2q a w x TKN o
o Nitrite ]bs/acre)
Receiving Residual
g
a) Q
G
one) Solids/ Liquid
o
/o Solids
per Acre
a �;
(NPDES #, WQ#, Fert., (Dry, Wet, Hrs. o
Application
PP
A
(Dry
Animal Waste, etc) Moist) inches a °o t o o mg mglkg mg/kg Crop 1 Crop 2
Crop 1 Crop 2
Cu. Yds Gallons
Tons/Ac)
o
2/14
96000
4.12
1:649: u�1
NCO021253 Dry 0 S 0.5 0.3 11335 4853 3.79 14C43,1 -. ' '; i NA 'v
R e
`.000s:
0:000 .zc' •.0 000 t
i iw,
Ei0000: ,
, 0-000`;iy ;' oA00„?"
':s0:00W;
', o-ijk Oio009":'
a 0?000„S:
o:000. <a; 0:000
n o.000n€r.
JIM400041o 000
0 000
Residuals Applications totals on FORM FSF sup (attach FORM FSF supp to this form):
Cd Cu Cr Pb H Mo Ni Se Zn P 14 431, 0 000
Lime Applied
TOTALS
Annual Ibs/acre
o . 9b000
As
0 01 f
0 004 .2:d37 +, _ ,`5 ; 0 033 0:033 7 7'. 0, 0,01 ` e7 Q 01"6 Oc023s" 0.076 4 657 ' 55 914;, t .
ear",
0.009 4.467 0.112 0.06 0.005 0.027 0.07 0.035 7.248
°;Y;O:d13 ?' 6,904 0,145
Date lbs/ac
Prior Years Cumlbs/ac
0.019
ulative
Current Cumulative lbs/ac
<sro:o3og,,
Permitted C. P. L. R. ****
36.6
34.8 1339 267.9 15 375 89 2500
Limit lst/2nd Crop
j 97.,2 ..
Permit PAN
Tenn-1
nrnnerly
"I ce ty, der p ally of law, that tors aocument was prepareu unuer ally .0
11...E _
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Havelock W WTP Total Dry Tons Applied (Annual):
Permit #: WQ 0000702 Cation Exchange Capacity (non 503 only):
Operator: Spencer Farms Owner: Spencer Fauns Predominant Soil Series: Yonges
Acres Used: 10 Acres Permitted: 10 Site #: SF PA2 Field #: J E
Rec:d..al Analvcie Data t"p5mv Metals and Tntnl Phoenhnrne use mu/ku. % Snlids use Raw Percent ft
Sample or
Com-posite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739
723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
phorus
16954
14436
15837
17445
A no..al Ann , Mntal Field i nadin c !('almJated in the/anrel•
Total
0
DT/Ac./
iv
App. Event
1.65
0.00
0.00
0.00
y
Arsenic
„ 0 01:1;';`;
<:.0:000?;;;
" : 0.000 ".x
r
" 0 000
. 0,000"
0 000
:0:000. F,
0 000',
0 000'
":.; W0:000,�,,
;0 000 ,<
60 6-
Cadmium
x`,,0:004T
.t m 0-000_ '
'',0:000::
;5A000
0:000,
;„.., 0 000;:n,
_; '0'.000,at
i
OOO.
: 00'
i 000 v"
"
000
':0 000",h,
Copper
2 437
c<0 000 ,+
„ 0 000 ;
.'0:000
0.`000
s ,,0A00
>0
,�,0 0
�0
0`.000. ,
;;;,0
.,
"
OOO;
O'.000
O:OOO:
x:0 033
Chromium0,000
O f
„0.000
;
b:000v
b'000°
K00000;000"
0:000,
0:000.
0000',;,
00331;
Lead
i0033,.,
,.0`000,a
,y
;0:000,
0000:0.000
,,
,
.,
'r„0
::
_. O:Q00.„
0 000'r
M 0 000;
'0 000
0;000
0 000
",
Mercury
000;,
'VON
: x0 OOO;r.
.x ,0:000:,„
,.0:000
,0001
Mol b
016
0 000
' 0 000
0 000
0 000
0
a s
0 000
_ i��d
; 0
0 000.^
0 000
3
0.000
0 016
de
0
_ .., u,
k 000
..,
000
s.,
r
,4000 a
xj'
Nickel
023'
w Q:000°ems
;.0.00,0,
Selenium
„�:0 016 ,
0 000„
, 0 000
�� 0 000,,,
77,0;000 ,�
O aOQ
;0 0004
; ,,Q 0004 1
° W0 000 ,
a , 0 000
V 000
6
000 :,
0 0_ QOR
b Q:400,s
0 000
';
Zinc
4'657,7E,
JZ""' 0007,;,
000 {;
;
.r,
ya .`4 ;657
�k" rA�' �k
3, Y ,'' 3 B'
f .{
-+ $ ,.
i-4 ,��,;
'. '}
2`.s.
�'�:�
Total Ph
,ii,
55 914'
0 000
0 000
<'F }
0 000
0 000
0 000
0 000.
0 000`
i'
0 000 '
.t.
0 000
,"k6
oo0a:
0 000 a55
914
phorusE.".frt�..,rt
'' €`
w�
SO
'
d
"U
fy, u er pe fly f law, that this document was prepared under my direction or supervision in accordance with a system aeslgnea to assure
t® l
SignatutckLandApplier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock W WTP WQ Permit #: WQ 000072 Field #: SF PA2-IF Acres Utilized: 9.8
Land Owner: Spencer Farms Annual Dry Tons Applied: l l {3391=1P+ :' � ` ` 1 =r`` sg'#° Site #: Acres Permitted: 9.8
a.. sa
Operator: Spencer Farms Predominant Soil Series: Yonges Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN:
s.
Volume applied (enter
Volume
Applied
Residual Sources
Soil Cond.
Preci p
Past 24
a
<
o
a
`°
TKN
z Y
q w
Nitrate and
PAN Applied (
Name of Crop Type
ReceivingResidual
o
o
one) Solids/ Liquid '
% Solids
per Acre
(NPDES #, WQ#, Fert.,
(Dry, Wet,
�•
�, ?
c
=
t
w
*
o
�•
Nitrite
lbs/acre)
Application
Crop 1
Crop 2
Crop 1
Crop 2
A
(Dry
Animal Waste, etc)
Moist)
inches
°.-.
`
mg/kg
mg/kg
mg/kg
Cu. Yds Gallons
Tons/Ac)
o
2/14
66000
4.12
= 1i15,7==
NCO021253
D
0
S
0.5
0.3
11335
4853
3.79
'k 10.124;—
�i::NA =
R e
=:0:000;'i
0:000=. k :
;r,;�� 0.0001 :..'"0:00&"i;`
Of000`
0.000r::
3a000�''1=:
,i" r0i000:�%{a
�•-
FORM FSF su to this attach FO form):
Residuals Applications totals on FORM FSF supp ( pp
"
Mo
Ni
Se
Zn
P10124r
o 000
Lime Applied
TOTALS:w
;' e o
�. 6600o
As
Cd
Cu
Cr
Pb
Hg
Annuallbs/acre0:008
+
;,0.003
0:023;;,
,r 0023<v
OOOI b
-,0°OI2t_
; 0;016_
r;012r
:,3267, r
39:232',".,'•;:; <;":
Date
lbs/ac
Prior Years Cumulative lbs/ae
0.019
0.009
x„1:7;10;?>�
4.514
0.11
0.06
0.005
0.027
0.069
0.035
7.345
C1nll1atlVe 1bS/aC
2
Al2
6:224�
tiQ1
as.,... :..,
O0
`
85
Lc
0
„0Cllrrent
41
Permitted C. P. L. R.****
36.6
34.8
1339
,
267.9
15
375
89
2500
.
Permit PAN Limit 1 stl2nd Crop,
, �.:< •-••
"1 Cer[II , UDUe pens ly uI 'slW, UIiIL II■■3 UVI:Wucu■.1'aJ p■cpa■cu wwm uy ..
"�� 2 lie
of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
I **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
City of Havelock WWTP
Total Dry Tons Applied (Annual):
Permit #:
WQ 0000702
Cation Exchange Capacity (non 503 only):
Operator:
Spencer Farms Owner:
Spencer Farms Predominant Soil Series:
Yonges
Acres Used:
9.8 Acres Permitted:
9.8 Site #: SF PA2 Field #:
1F
13—M-11 A
n.,r., /U.—I Mptal..end Tn4o1 Phnenharne ncp
ma/lra_ °/ Ralide nee. Raw Percent #L•
Sample or
Com-posite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
1 739
723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412
1565
1557
1640
Total Phos-
phorus
16954
14436
15837
17445
Anneal Hpaw Metal Vipld 1 .nadinae IL'alrninted in Inclnerel:
Total
"3
0
DT/Ac./
m_
App. Event
1.16
0.00
0.00
0.00
y
Arsenic
`rs'0,008,i,;„
w`,s0:000 ,
.",-a';0:000 :;c
;,
,, ,0:000;4 ,
M„'0:000`,G
, „0:000 ";,
0 000 `
" ,0 000
w
„ 0 0w-16
4'
, 00 ,::;_;O,OQO,
;000,
"` 0'
O'008;
Cadmium
. „'0t003 ,y ,
v. i0.000a =
A 00,0
b , O'000.,
; '0.000` x
µ0 000 ;
0 OOOrt
>" 0 OOOr,,;}
:; „ OAOOrh
, 0.000, ,
0' 000, ;_
a0.000,
000
000
000
x
0:000_l.7,10;w„
Copper
, 1:7:10 <'
',:, 0 000.;.
k .. 0 000 G;;
av0:00Q .,
„ O000 ,
_ 0:000 , ,
._, 0 000
,; 0
, 0
„0
0000,
�,0.000.�.
Chromium000,
Lead
0 023:
". ; 0 000
0 000, a
" ,O:OOQv
O:Q00
.0;000 *.
0`000" ,_
:O:QQQ
.;0 000,.E
0 000 „
:,r 0:000�
" ; ;0 000, ;
0 023, ,Y.
:> `'0 000
OOQ,;,:
„0`000_ "
'0 000
0:000
30 001,
Mercury
:A10 00,1, .,
; O OOOr
0 000
� 0=000,+2
� ,0:000 �
_.. Oi000 q
r_ O
,
_
.
'.r" 0:000
Mo Y
" 012
0 000
0 000
0 000
0-000
0 000 #6 r
0 000'
"
0 000
0 000Oh000
O 000
0 012
denum0
10000
Nickel
0;000 .
; 0:000r;;
, `0 000 ",
,, ,0 000,,; !
„=r0 000„
;',,;0 000 ` °
"_,0 000„; .
0.000�;
�, „0 6 '
Z0 016 �x
v
k,64900 ",
: 0 000: ;
O0
OW
z0`.000,,
;964W
VA Q12 '
Selenium
4,1:0 012„E,;
, :;0 000uM'
�,,,0 00.0 .,
N 0 OOq g
0 OQO„ ;
t.`_0:000`
,
x
_r
u
;
`„A:000
0.000
0 000;,;
0 000 „
000„
0,000
Zinc
,"�,3267 ,
;; 0 000
Q'000;,
.r
0`D00; ,
,
,, ",0"000-,;
,.,A
,O:Q00 .
„w
Total Phos
u
*9
" 0 000
Q Q00
0 000
0 000
1
0 000
0 000 r
0 000 i,
0 000
Q 000
232
phorus''3'9
"I certify and penalty of law that this document was prepared under my direction or supervislo m accordance with a system aeslgnea to assure
l� ak, �
SignaturcULand Applier Date

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Havelock W TP WQ Permit #: WO 000072 Field #: SF PA2-IG Acres Utilized: 7.7
W
U Acres Permitted: 7.7
Land Owner: Spencer Farms Annual Dry Tons Applied: ?=P4 61,1„7r .; " x w _ :; ? ; Site #:
Operator: Spencer Farms Predominant Soil Series: Yonges Cation Exchange Capacity (non 503):
Crop 1 Name: Rye Crop 1 Max. PAN: 97 Crop 2 Name: Crop 2 Max. PAN:
z Name of Crop Type
o
o
A
Volume applied (enter
one) Solids/Liquid
Cu. Yds Gallons
9/14
96000
TOTALS:
Annual lbs/acre
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R****
Permit PAN Limit 1 st/2nd Crop
"1 ceMt Y. una pen
Volume
Residual Sources
Soil Cond.
Precip.
pit 2q
y
b
o
o =
in
T
_
°' o
Nitrate and
Nitrite
PAN Applied
lbs/acre)
Receiving Residual
% Solids
Applied
per Acre
(NPDES #, WQ#, Fert.,
(Dry, Wet,
Hrs.
1.w°
Application
(Dry
Animal Waste, etc)
Moist)
inches
; 0•
❑
o•
mglkg
mglkg
mglkg
Crop 1
Crop 2
Crop 1
Crop 2
3.65
As Cd
01023.E +;0."004
0.021 0.01
36.6 34.8
document was
Signature of Land Applier
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
Cu Cr Pb Hg Mo Ni Se Zn. P .55.349 ; ;`.o:000 Lime Applied
Date lbs/ac
:'0'.002r.` -0;019. 0:030:r i0i019 . 91
5 086 0.121 0.068 0.005 0.031 0.076 0.039 8.3
4.:
'
-
,r 058_ .1 4:210=-
40. O50': 07 1339 267.9 15 1 375 89 2500
c' s
cared under my dir ction or supervision in accordance with a system designed to assure that qualified personnel properly
/ [ *Application Method: S -Surface, IN- Injection, INC- Incorporation
Zl�' G J **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3,
****C.P.L.R.: Cumulative Pollutant Loading Rate

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
City of Havelock W WTP
Total Dry Tons Applied (Annual):
Permit #:
WQ 0000702
Cation Exchange Capacity (non 503 only):
Operator:
Spencer Farms Owner:
Spencer Farms Predominant Soil Series:
Yonges
Acres Used:
7.7 Acres Permitted:
7.7 Site #• SF PA2 Field #:
1G
Residual Analysis Data (Heavy Metals and Total Phosphorus use mH/ke, % Solids use Raw Percent #):
Sample or
Com-posite
2/10/14
4/28/14
7/14/14
10/20/14
% Solids
4.12
4.11
3.65
4.06
Arsenic
3.4
2.5
6
9
Cadmium
1.3
1.3
1
1
Copper
739
723
863
861
Chromium
10
10
11
12
Lead
10
9.6
11
16
Mercury
0.24
0.48
0.52
0.56
Molyb-
denum
5
5
5
5
Nickel
7
8
8
9
Selenium
5
5
5
5
Zinc
1412'
1565
1557
1640
Phos-
Total phorus
phorus
16954
14436
15837
17445
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
H
DT/Ac./
iv
App. Event
0.00
0.00
1.90
0.00
Arsenic
;=; 0 000 x ;
. ;':Oi000'
°0 023;
Cadmium
}0"OOOv„..
0 000
0 004
0;000;
0.000
,
.
Copper
.O:OQOJ?
000i
3, 276"5,
, 0.`OOO,.,.
; b, 000r „
s;, 0 ;000
O OOOk r*
Oa000r
:0 0Q0
, v0.000
0000
,„` ;0's000
`µ.,3 276, ;'
Chromium
-:<O;000 x
0 000.<,w'
0 042`
0
,`; ,
�, 000
�_ .'0.00Q, ,
„O:OQO; .0,',000,„
Lead0:000e.t„'0
000
z 0,000§0
000 ,
-, A:000 ',
., 0:000 .;,
N -0 000_
0=042
Mercury
--"0.000
000
Q 0of,
p OOQ
MOW
�0 0.0,0;,.F,
0
,��0 :„
..
000 _„
0 000`',0,00,0+
Molyb'
0:000
0 000 `
0 019�`
, 000
u 0 000>s
OOQ
0 000
0 000,;;
�0 0#00
0�000°�_0
000
O:Ol9r
denum
"�^
4 :y, _,_
3.. . r :
:ems,
�0
,s:
a.� aM.•
.O
,. .pp ��
"'aiT➢ .Li„A'4
.YrzK ° e "v'^i�'
$ .`bb
0000
, •�--k!.b ,
Nickel
GO'000 „ &42
0,00 r
0:000
,s-0:0,OOr r
0 000"
0 000,E
;0 000,
0 000
Selenium
-;0;000
s'0 000","
'Gs ,0 019:;
0 000
,„. Q 0001 ,
,.0 000. ,;
10 OQO,
k 0 000„
„,0 000 :k=
,c _0 000,E
O.00Q,
0 Q00 ',
'0 019
Zinc
0000,';j0.b00;;
5-910,;
OQ00
Y„0:000,
T0Q00
�0d00it0000
„:0000
:0000,'4:Q00
5 910
TotalPhos
:'s�f
r zrR
phorus
000
000
60 17.0
000
0 000
0 000
0 q00,
0 000
0 0000
000
000
0 000
t id0 1,1�/
A`:0
'0
F
2,.=.
�.t
.0
�.�_;
_,na,s
a>._n,.r a>
.
+.P-. <t K. _ _s-�-..�:5�
kas�,tzf
,c s.,�'
,.�, ?'k�._ 33
. .k?.-��.."�.
LL ;
a st.'",i'*. a'�•�
11 certify, under penalty o w, t t this document was prepared under my direction or supeision in accordance with a system designed to assure
Signatur o Land Applier Date

February 26, 2014
Deedee Woolard
Environment 1, Inc.
114 Oakmont Dr
P.O. Box 7085
Greenville, NC 27858
TEL: [phone]
FAX: [phone]
RE: City of Havelock
Dear Deedee Woolard:
Srtnunil Etrrironmental Technologies, htc.
3310 GVirt St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX- [phone]
FVebsite: h11P.-Mvrvtv.settek.com
Order No.: 14021296
Summit Environmental Technologies, Inc. received 1 sample(s) on 2/18/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A21-A 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PFI-0105, Delaware, Florida NELAC E87688, Georgia
E87683 and 943. Idaho OF100923. Illinois 200061 and Reg.5, Indiana C-Oli-13, Kan5as E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA 12004, Maine 2012015, Marylmrd 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey 01-1006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 63-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04019, Texas T104704466-1 I-5, Region 8 8TMS-
L, USDVAPHIS 1`330-11-00244, Utah 014009232011-1, Vennont VT-87688, Virginia 00,140 and 1581, Washington C891, West Virginia 248 and 9957C
and E37688, Wisconsin 399013010
Page 1 of 7

Suninift Environmental Technologies, Inc.
Workorder
33 10 lVin St.
Sample Summary
Cuyahoga Falls, Oltio 44223
TEL: [phone] FAX. [phone]
WO#: 14021296
Websile: h1fp.-11ivw1i,.seitek.com
26-Feb-14
CLIENT: Environment 1, Inc.
Project: City of Havelock
LabSamplell) Client Sample lD Tag No Date Collected Date Received Matrix
14021296-001 Sludge Sample 2/10/2014 12:42:00 PM 2/18/2014 11:45:00 AM Sludge
c-
r
Page 2 of 7

Summit Environnrenml Technologies, lrrc. Case Narrative
:.: 1
3310 Win St.
14021296
CrryahogcrFalls, Ohio 11233 WO#'
TEL: (330) 253 S?! 1 FAa": (330J 353-d 1S9 Date: 2/26/2014
61'ebsite: hup.-Ilinvivsettek.conr
CLIENT: Environment 1, Inc.
Project: City of Havelock
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original
Page 3 of 7

"
Summil Environmental Technologies, Inc.
CVO#:
14021296
'- - - {::,. ,� • �r i�,,,� ° fit:;-•"
3310 Win St.
Date Reported:
2/26I2014
Cuyahoga Falls, Ohio 4=1223
TEL: [phone] / FAX: [phone]
Company:
Environment 1, Inc.
Websile: http://ivuw.settek.com
Address:
114 Oakmont Dr
Greenville NC 27858
Received: 2/18/2014
Project#: City of Havelock
SVOC SW-846: 8081-TCLP Pesticides
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001
2/10/2014 Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030.
2/24/2014
JBN
Sludge Sample
001
2/10/2014 Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
2/24/2014
JBN
Sludge Sample
001
2/10/2014 Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
2/24/2014
JBN
Sludge Sample
001
2/10/2014 gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
2/2412014
JBN
Sludge Sample
001
2/10/2014 Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/24/2014
JBN
Sludge Sample
001
2/10/2014 Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
2/24/2014
JBN
Sludge Sample
001
2/10/2014 Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
2/2412014
JBN
VOC by GC/MS (8260)-TCLP
Client 1D#
Lab ID#
Collected Analyte
Rep Lint
Result Units
Matrix
Method
DF
RegLvl
Run Analyst
Sludge Sample
001
2/10/2014 1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
2/24/2014
MES
Sludge Sample
001
2/10/2014 1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/24/2014
MES
Sludge Sample
001
2/10/2014 Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/24/2014
MES
Sludge Sample
001
2/10/2014 Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/24/2014
MES
Sludge Sample
001
2110/2014 Chlorobenzene
0A0
ND mg/L
Sludge
EPA 8260 B
1
100
2/24/2014
MES
Sludge Sample
001
2/10/2014 Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
2/24/2014
MES
Sludge Sample
001
2/10/2014 Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
2/24/2014
MES
Sludge Sample
001
2/10/2014 Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
2/24/2014
MES
Sludge Sample
001
2/10/2014 Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
2/2412014
MES
Sludge Sample
001
2/10/2014 MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
2/24/2014
MES
SVOC 8270
TCLP BNA List
_
Client ID#
Lab ID#
Collected Analyte
Rep Lmt
Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sludge Sample
001
2/10/2014 1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
2/26/2014
AKE
Sludge Sample
001
2/10/2014 2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
2/26/2014
AKE
Sludge Sample
001
2/10/2014 2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
2/26/2014
AKE
Sludge Sample
001
2/10/2014 2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/26/2014
AKE
Sludge Sample
001
2/10/2014 Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
2/26/2014
AKE
Sludge Sample
001
butadiene
2/10/2014 Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
2/26/2014
AKE
Sludge Sample
001
2110/2014 Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
2/26/2014
AKE
Sludge Sample
001
2/10/2014 Nitrobenzene
0,10
ND mg1L
Sludge
EPA 8270 C
1
2.0
2/26/2014
AKE
Sludge Sample
001
2/10/2014 Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100
2/26/2014
AKE
Sludge Sample
001
2/10/2014 Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
2/26/2014
AKE
Page 4 of 7

-ownental Technologies, Inc. Summit Envit
WO#:
14021296
33 0 Win St.
C11.1whoga Falls, Ohio 44223
Date Report ed:
2/26/2014
-8211 FAX: [phone] TEL: (330) 253
Company:
Environment 1, Inc.
Websile: hup://www.setlekcom
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
2/18/2014
Project#:
City of Havelock
Client ID4
Lab ID# Collected Analyte
Result Units
Matrix
Method DF RL
Run Analyst
Sludge Sample
001 2110/2014
Flashpoint (140T)
>200 T
Sludge
1
2/20/2014 TJR
Sludge Sample
001 2/1012014
Cyanide, Reactive
ND ppm
Sludge EPA9014 1 0.50
2/2012014 TIR
Sludge Sample
001 2/10/2014
pH
7.8 s.u.
Sludge EPA 9045 D 1
2/1912014 AYS
Sludge Sample
001 2/10/2014
Sulfide, Reactive
ND ppm
Sludge EPA 9034 1 25
2/20/2014 TIR
Page 5 of 7

liuvironnierEt 1, 111r.
I,.(). lint 7085, 114 Oat:MIME C)r-
;rccnville, NC 2785h
I'h�x�r [phone] • 1=ax C'>
C I , 1 204 F tiVe
CITY OF HAVELOCK
J 11Z, ART HOUGII
tYAS'[ EWA'I'TIt TREATNIE
304 N. JACKSON DRIVE
t-IAVLI,OCK NC 28532
[phone]
5Am,PLE LOC.ATIC41
Sample NI
Sample _ e #2
�Sa:np` IL, #3-_
Sample !l4
Sample 5S
Sample #6
Sample N7
r
Sludge Sample
CHAIN OF CUSTODY RECORD
■
N
1
n�C
IS
I � •
I
I
� RELitJCD H '? 0A• P ER) gATDTihtE R EI ED BY.J-
OATUMIL
RE � J 1E � G) AECEflEDB'; I 1
1 ,' i5 ED tS i DIffPTIME RECENE 3Y ( IG)
a�t.0 �u
I
( PLEASE READ Instructions for completing this form on the reverse side.
(D FOSit.4 n5
0
C01MMENTS.
CHLORINE NEUTRALIZED AT COLLECTIphq
pH CHECK (LAB)
p
p
p
p
G
G
CONTAINER TYPE, P,'G
CHEM,CAL PRESEITATIC,td
A -NONE D•NAOH
A
A
A
A
A
A
-'
V
l3•HNC, E -HCL
• �,
x
r
>
h
a
i
C • H,SO. F - !t-IC r`t,^_.FTAT&MAOIJ
U
U
a G- INA TH1OSULFATF
c
U
a
CIASSIFICATICty:
bVASM'111I ER (NFDFS)
DRlnKlI,tiG WATER
DYJrlri4':
SCILID WASTE SECTION
CHAIN OF
CUSTODY MAINTA11,1ED
DURING St�IEN- DE; IVFRY
%1"/ N
SAMPLES C0t'LCTED £Y:
SAMPLES RECEtVtiD 1N LAC3Ai , c�
Sampler must place a "C" for composite sample or a "G' for Nu 268 26 O
Grab sample in the blocks above for each parameter requesterd.
„,,�` Page 1

LTJ
<:57
S k,�) t-� =--A 1(07, D Al L %i
1 vir -r. sz:tj *. em- twr-0-
Page 2 of 2

Surninil Envii -onviental Technologies, Inc.
Workorder
3310 Win St.
Sample Summary
Citywhoga Falls, Ohio 44223
[phone] -8211 FAX. TEL: (330) 253
WO#: 14021296
fflebsite: hilo:llii,it7iv.seltek.coni
04-Mar-14
CLIENT: Environment 1, Inc.
Project: City of Havelock
LabSaniplell) Client Sample lD Tag No Date Collected
14021296-001 Sludge Sample 2/10/2014 12:42:00 PM
Date Received Matrix
2/18/2014 11:45:00 AM Sludge

Sunmzil Environmental Technologies, Inc.WO#:
3310 Win St,
Date Reported:
Cuyahoga Falls. Ohio 44223
TEL: [phone] FAX: [phone] Company:
Websile: h(lo:/hmviv.sellek.com
Address:
TCLP Metals Analysis (6010)
14021296
3/4/2014
Environment 1, Inc.
114 Oakmont Dr
Greenville NC 27858
Received: 2/18/2014
Project#: City of Havelock
Client 1D#
Lab 1D# Collected Analyte
Rep Lint Result Units
Matrix
Method
DP'
RegLvl
Run
Analyst
Sludge Sample
001
2/10/2014 TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Badum(Ba)
5.0
ND mg/L
Sludge
EPA 6010 C
1
100
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Lead(Pb)
0.50
ND' mg/L
Sludge
EPA 6010 C
1
5.0
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
3/3/2014
WK
Sludge Sample
001
2/10/2014 TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
3/3/2014
WK
TCLP Mercury Analysis (1311/7470)
Client 1D# Lab 1D# Collected Analyte Rep Lmt Result Units ' Matrix Method Dd+ RegLvl Run Analyst
Sludge Sample 001 2/10/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 3/3/2014 ALJ

P.O. Box 7085, 114 Oakmont IX.
Greenville, NC 27858
Pace 1 of 1
Phone [phone] - Fax [phone]
DISINFECTION
�
CHLORINE NEUTRALIZED AT COLLECTION
CI iLUItINI�
—
zoa r Week- 1
pH CHECK (LAB)
•
' -I V
G
CONTAINER TYPE, PIG
CITY OF HAVELOCK
NONE
MR. ART HOUGH
CHEMICAL PRESERVATION
WASTEWATER TREATIINIENT PLANT
304 N. JACKSON DRIVE
?
A
HAVELOCK NC 28532
E
A - NONE D -NAOH
[phone]
z LLf
z
B - HNO� E - HCL
rr J
,�
d
v
z
w C- FinSO, F- ZINC ACETATE/NAOH
COLLECTION
a
o
s a
iw ¢
it.o
a
H
G- NATHIOSULFATE
C
SAMPLE LOCATION
DATE-
TIME
Sludge Sample
'Jr
0 13r�S'
f (,
1
'`�%'
CIJISSIFICATION:
WASTEWATER (NPDES)
DRINIKING WATER
—
DW9GW
SOLID WASTE SECTION
CHAIN OF CUSTODY MAINTAINED
DURING SHIPMENT/DELIVERY
D N
SAMPLES COLLECTED BY:
(Please Print)
71�nniS
_
SAMPLES RECEIVED IN LAB°C
EF KIN UISHED BY, ) (SAMPLER)
DATFJiIME
YRECI-I/ED Y,SI(
ATE/11ME
OMMENTS:��
a ��
ELI ISF Y G
ATE/I lM E
RECEIVED BY (SIG.)
DATEJTIME
•
f"'41DATA
RELINQUISHED BY (SIG.)
RECEIVED BY (SIG.)
DATE[FIME
PLEASE READ Instructions for completing this form on the reverse side.
FORM H5
Sampler must place a "C" for composite sample or a °G" for n 276531
(crab sample in the blocks above for each parameter requested.

`, s`ai'�"Y� .:'r-"��'• } I`;;s E, :';:; ,,$F h-1 '%: iKm `X-i1
3;.3'J`_i?s
March 19, 2014
Deedee Woolard
Environment 1, Inc.
1 ] 4 Oakmont Dr
P.O. Box 7085
Greenville, NC 27858
TEL: [phone]
FAX: [phone]
no
Dear Deedee Woolard:
Sunmrit Enrh•onmental Technologies, Inc.
3310 Hein St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX: [phone]
Website: hito://xntnv.settek.com
Order No.: 14030434
Summit Environmental Technologies, hie. received 1 sample(s) on 3/6/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Comiecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idalio OI-100923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA 12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
HampsWre 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH200001, Pemuvkania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah 011009232011-1, Vernront VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010

Summit Environmental Technologies, Inc.
Workorder
33 10 Win St.
R'i
Cuyahoga Falls, Ohio 44223
Sample Summary
-8211 FAY: [phone]
TEL: (330) 253 AX.
WO#: 14030434
Websife: littp:llii--iinp.settek.coni
19-Mar-14
CLIENT: Environment 1, Inc.
Project:
Lab Samplell) Client Sample ID Tag No Date Collected Date ReceNed Matrix
14030434-001 Sludge Sample 3/5/2014 9:38:00 AM 3/612014 9:50:00 AM Sludge

6g ",
Stmunit Environmental Technologies, Inc.
A p
Case Narrative
. n*. ,.;
..:, ;i' Y'-5e,,,,d iy:7y 4¢y'r�l' 1' ,@G'�:
y'•3310
kVin
._ .�� ib %sh1lYrs! ?.a�� r•+ r
R
Oh Falls, Cuyahoga Cu �7 )' g Ohio 44....3
WO#• 14030434
-wir h;.:.i ,_: sc;,,-.t, ;
TEL: [phone] FAX: [phone]
Website: http:/hviviv.seltekcorn
Date: 3/19/2014
CLIENT:
Environment 1, Inc.
Project:
This report in its entirety consists of the documents listed below. All documents contain the Summit
Environmental Technologies, Inc. Work Order Number assigned to this report.
_- Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality
Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample
set.
Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation
(LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty
associated with these results and data should be considered as estimated.
Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods.
Estimated uncertainty values are available upon request.
Any comments or problems with the analytical events associated with this report are noted below.
Original

"".
JK
Slinunil Environmental Technologies, Inc.
WO#:
14030434
3310 Win St.
Cuyahoga Falls, Ohio 44223
Date Reported:
3/19/2014
TEL: [phone] F4X.- [phone]
Company:
Environment 1, Inc*.
[Yebsile: htip.-Mvitiv.settek.com
Address:
114 Oakmont Dr
Greenville NC 27858
Received:
3/6/2014
Project#:
SVOC SW-846: 8321 Herbicides-TCLP
Client ID9 Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvI Run Analyst
Sludge Sample 001 3/5/2014 2,4-D 5.0 N I D mg/L Sludge EPA 8321 A 1 10 3/18/2014 ANIZ
Sludge Sample 001 3/5/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 3/18/2014 AMZ

CHARN OF ctls,roi)y jIECORD
G10:11ville- iN(: --785WLCC! IONAI
CIA ENT- 204 F
CITY OF, IIAVE -,I,OClk
ua HOUGH
AVAS'I'ENVjVFFR TREATIMM' PLANT
A
4 DRIVE A ,;04 N..TACKSO1
HAVILOCK ,C 28532
[phone]
1 -5
iiC1c,U. F>V, E
r -001-1
DAI I
t ytI(Ige swilp e I ILI
S'i 64,"0 Ell "NIPU
E'-:,i:C ilulN
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G:QC SFPRE D[Dzc.,,.unernl Tempwe-z - TracjtinukCz:,Ie-,- rerai-ot trn Pee -Q 07-27-1 5 C�O-1 Page 1 of 2

(" ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
0
Facility Name: City of Havelock, NC WQ Permit Number:
WWTP Name: City of Havelock, NC WWTP NPDES Number:
Monitoring Period: From 1/1/2014 To 3/31/2014
WQ0000702
NCO021253
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:71
Alt. A (time/temp) ®
1 Alt B (Alk Treatment)
0
Alt. C (Prior Testing)9
- .
A1t.D (No Prior Test) El
Process to Further Reduce Pathogengs
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost El
Heat Drying 0
Heat Treatment 1l
Thernzophilic
Beta Ray El
Gamma Ray 1l
Pasteurization 1�
Class B:
Alt. (1) Fecal Density }
Alt. (2) Process to Significantly Reduce Pathogens [I
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying El
Composting El
jAerobie Digestion
es ionAnaerobic Dr El
g
............................................................................................ .
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
dense -es
enc
Frequency
of Analysis
Sample
Type
a ytica
nia e
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
21123
57544
115207
MPN/g
0
4 x year
Grab
SM9221E.
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) Ej
Alt: 2 (40-day bench) E3
Alt. 3 (30-daybench) Cl
jAlt. 4 (Spec. 02 uptake) Cal
Alt. 5 (14-Day Aerobic) C
Alt. 6 (Alk. Stabilization 0
Alt 7 (Drying - Stable)
Alt. 8 (Drying - Unstable) i1
Alt. 9 (Injection)
Alt. 10 (Incorporation) C]
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
>, "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T 1107 have been met."
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Art Hough, WWTP Superintendent
Preparer Name and Tkl (type or print)
Signature of Preparer*
j it I-S')
Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
0 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

P.O. 60.A 7035, 1114. OAKIl IC N I DRIVE
GRE�NVILLE, N.C. 27835-7O85
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
..wastewater„-zv lu
PI-i0{Vc_(252) 7,56 6208
FAX [phone]
ID#: 204 F
DATE COLLECTED: 02/10/14
DATE REPORTED : 03/28/14
s
REVIEWED BY:
Sample
Sample
Sample
Sample
Sample
Analysis
Method
PARAMETERS #1
#2
#3
#4
#5
Date Analyst
Code
Total Residue, mg/l 31480
31700
32100
30380
33140
02/11/14 CMC
2540B-97
Fecal Coliform (MPIN), /gram Solids 34943
69401
74766
115207
21123
02/11/14 CMC
9221E-06
0

2 ;>1 �W,F,IT11"D MI- ���G�i11.1L l�r �13����t1�(i���� ���I
`s ,f.
.t
r
k n Wate''" 3`7,7-I.5
:Was.t'ewater .ID: '•10
PC).bOX 7085, -114 OAKMOnrr nFt�vE' "' P�aoiNc C252i 7 56-62ti8
GREENViLL.E,' N.C. 27835-7085 FAX [phone]
ID#: 204 F
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT DATE COLLECTED: 02/10/14
304 N. JACKSON DRIVE DATE REPORTED : 03/28/14
HAVELOCK ,NC 28532
REVIEWED BY:
Sample Sample
Sludge
Analysis
Method
PARAMETERS
#6 #7
Sample
Date Analyst
Code
PH, Units
6.7
02/12/14 TRB
4500HB-00
Total Residue, mt'
33820 34020
02/11/14 CMC
2540B-97
Aluminum, (dry wt. basis), mg/kg
35312
03/05/14 LFJ
EPA200.7
.Arsenic (dry wt. basis), mgfkg
3.4
03/24/14 ME
3113B-04
Calcium ((try wt. basis), mg/kg
28701
03/05/14 LFJ
EPA200.7
—Cadmium (dry wt. basis), mg/kg
1.3
03/19/14 NIEL
3113B-04
-Copper (dry wt. basis), tang/kg
739
03/05/14 LFJ
EPA200.7
—Chromium, T.(dry wt. basis),mg/kg
10
03/05/14 LFJ
EPA200.7
,-Lead (dry weight basis), mg/kg
10
03/21/14 ME
3113B-04
Magnesium (dry wt. basis), mg/kg
2092
03/05/14 LFJ
EPA200.7
..-Mercury ((try wt. basis), mg/kg
0.24
02/26/14 ADD
245.1 113-94
-� Nickel ((try wt. basis), mg/kg
7
03/07/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4002
03/05/14 LFJ
EPA200.7
Selenium (dry wt. basis), mg/kg
<5.0
03/25/14 MEL
3113B-04
Sodium ((try wt. basis), mg/kg
3683
03/07/14 ADD
3111B-99
�- Zinc (dry wt. basis), mg/kg
1412
02/21/14 ADD
311113-99
Sodium Adsorption Ratio
0.18
03/24/14 LFJ
Total Solids, %
4.12
02/11/14 CMC
2540G-97
_TICK (dry wt.), mg/kg
11335
02/13/14 ANO
351.2 112-93
�s Ammonia Nitrogen (dry wt.),mg/kg
4853
02/13/14 ANO
350.1 112-93
Phosphorus, T. ((try wt.), mg/kg
16954
02/13/14 ALB
365.4 -74
—Nitrate-Nitrite (dry wt.), mg/kg
<3.79
02/12/14 ANO
353.2 112-93
Plant Available Nitrogen, mg/kg
4371
02/20/14 SE.I
Fecal Coliform (MPN), /gram Solids
103489 51189
02/11/14 CIVIC
9221E-06
Nlolvbdenum (dry wt. basis), mg/kg
<5.0
03/05/14 LFJ
EPA200.7

00
,
Environment 1, Inc.
P.O. Box 709.5, 114 Oakmont Dr.
Greenville, NC 27858
CHAIN OF CUSTODY RECORD
Page I of 2
Phone [phone] ° Fax [phone]
DISINFECTION
CHLORINE NEUTRALIZED AT COLLECTION
Ij CHLORINE
pH CHECK (LAB)
CLIENT: 204 F Week: 4
UV
P
P
P
P
P
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CONTAINER TYPE, P/G
CITY OF HAVELOCK
NONE
N1R. ART HOUGH
WASTEWATER TREATMENT PLANT1:1
304 N. JACKSON DRIVE
A
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CHEMICAL PRESERVATION
HAVELOCK NC 28532
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DATEfTIME
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PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for i\l u

Fecal Data Sheet 1st Qtr. 2014
Lab Result
Log Min. 21123
34943
4.54 Max. 115207
69401
4.84 Geometric Mean 57544
74766
4.87
115207
5.06
21123
4.32' -
103489
5.01
51189
4.71
Average
4.79

�J
Digester Oxygen Uptake ( Sours
Test # / Test #,
Collection Time: _ Collection Time: D
Collection Temp: 73 Collection Temp:
Start Time: /036 Start Time: ) I;
Start Temp: i ( Start Temp:1
Start DO: `/ Start DO:
Min Min
rr
2 2
3 Iry 3
4 4
5 5
6 6
7 L, q 7
8 tarC�C� 8
9
10
11
12
13
14
15
Stop
Temp
Date
9
10
11
12
13
14
15
Stop
Temp
Date
� •d,
Test # 3
Collection Time.- 1 :�3 ti
Collection Temp:
Start Time: / ,� ��•
Start Temp: 13,
Start DO: G
Min
1
2
3
4
5
6
7
8
9
10
11
12
�z
Stop
Temp 13,
Date
13
14
15

Digester Oxygen Uptake (Sours)
Test # Test #
� � Test #
Collection Time: M Collection Time: �36'��,
Collection Temp:�' , Collection Time: �1)
, b 6 Collection Temp: /�- ,� Collection Tern . c.
Start Time: 3 nm p
Start Time: a, �-M Start Time:
Start Tem �,
Start DO: p r, 0 Start Temp: . y Start Temp:l� '
Start DO: LI Start DO:
Min Min
1 � � 1 - Min
2 ,L1 7
2 s 3 2 '
�� 3
5 �2 5 L 5 4 1
6 " 6 ', 5'
.L.., 3 e 7 y'�
8 � � 8 s K I Ll
10 -5 C, C S.9 � 0
10 10 .1 12,E
11 ,� �., 11
12
13 12? 12
13
14 ' 13 3'
15 14 n �� 14 3,3
Stop
� Stop 15 15 .�
Temp /� Stop
Temp �j / Temp�-
Date 5l Date D
--T_ ate

Digester Oxygen Uptake (Sours
Test # Test
��
st # Test # C�\
Collection Time: d `�', � � ��� Time: % Collectpn Time:
Collection Temp: Co ction Temp: Collection Temp:
Start Time: �4�M Start Time: Start Time:
Start Temp: 5 "C, Start m
p. Start Temp:
Start D©: 1 =; M�JLStart D Start DO:
Min Min. Min
1 1
2 Cy 2 2
3 ��
3 3
4 ,�� 4 `
4 r
5 �` U5 5 !'
6 <� �' 6 6
j1
7 7
8
81 8
9 9 9
10
i 10 10
11`�� 11
12 12 j 12
13 13 13
,
14 �.c�S 14 / 14`f
15 77 15
7 LQ s
15
Stop
c. Stop Stop
Temp r —� Temp ,�Temp
Date / Date
Date

Digester Oxygen
Uptake ( Sours
)
Test #
Test # Q
Test #
i c-)
Collection Time:
Collection Time: i
Collection Time: % 02 2
Collection Temp: i -.,t-i Collection Temp: rs.uti
Collection Temp: , jc6
StartTime: o,-ry 2
Start Time: jooi�
Start Time: Lo2L
Start Temp: , s. w 6
StartTemp: t.5 -�3
Start Temp: i s- 5 (�
StartDO: 9 zo
Start DO: �s-Ici
Start DO: _ �L
Min
Min
Min
1
1 Z
1
L.
2
2
2
�
3
3
3
's
4 1®
4
4
5
5
6
6
6
Z
7 2
8 s®
7
8 .6S,
7
8
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g 5 .1
g
9
CS . 0
10
10
10
11 �
11 cam,
11
U
12
12 �,0
12
13 s©
13 i
13
OT
N E M
14
14 3 r3
14
z..i-L
15
15
15
Stop
Stop
Stop
Temp
Temp
Temp
.
Date 3- -►y
Date-►o-tLA
Date
-

r
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
0 3/5/20141
9 3/5/20140,
3/5/2014 11:03
iur Hough
750 milliliters
1.74 % Dry Solids
14.21 ,degrees Celsius
13.47 degrees Celsius
Slope: 0.5
Intercept: 9.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 30.36 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.33 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 3. 9 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
01
q 3/5/2014H
ur
h
750 milliliters
1.79 % Dry Solids
13.73 degrees Celsius
13.4.,degrees Celsius
Slope: 0.4
Intercept: 9.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 26.13 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.95 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: =---2-92 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
13.77
3/5/2014 11::23 AM
Arthur Hough
3/5/2014 11=2
1.7
Slope: 0.5
Intercept: 9.3
Correlation Coefficient: 1.0
iilliliters
j Dry Solids
egrees Celsius
eqrees Celsius
Oxygen Uptake Rate: 27.13 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.06 mg Oxygen/g/hr
Average Temperature: 13 degrees Celsius
Temperature Correction Factor: 1.605781476
Temperature Corrected Specific Oxygen Uptake Rate:F 3.32 Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
9.81
9.69
9.09
8.72
8.26
7.88
7.4
6.56
6.09
5.64
5.22
4.7
4.22
3.74
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ0000702
3/5/2014
14
3/5/2014 1447
Arthur Hough
3/5/2014 1453
Arthur Hough
750
if 1.738
0.4
10.0
1.0
liliters
Dry Solids
Drees Celsius
frees Celsius
26.68 mg Oxygen/hr
2.05 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 3.07z mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock
Biosolids Permit Number: W00000'
Digester Temperature: 14.36
Sampling Date/Time: 3/7/2014 1430
Sampled By: Arthur Hough
Analysis Date/Time: 3/7/2014 1432
Analyzed By: Arthur Hough
Sample Volume: 750 milliliters
Total Solids: 1.59 % Dry Solids
Beginning Temperature: 14.42 degrees Celsius
End Temperature:p 14.87degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.5
9.8
1.0
30.21 mg Oxygen/hr
2.53 mg Oxygen/g/hr
15 degrees Celsius
1.402551731
Temperature Corrected Specific Oxygen Uptake Rate:mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP #6
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
WQ0000702
3/10/2014
15.46
3/10/2014 0855
Arthur Hough
3/10/2014 0859
Arthur Hough
750 milliliters
1.516 % Dry Solids
Beginning Temperature: 15.45 degrees Celsius
End Temperature: 16.12 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.4
9.6
1.0
26.70 mg Oxygen/hr
2.35 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
ypq,-Ve� � tz �,, 4 G,
Temperature Corrected Specific Oxygen Uptake Rate: 3.08 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP #7
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time.
Sampled By:
Analysis Date/Time:
Analyzed By:
WQ0000702
3/10/2014
15.08'
�3/ 20 090918
M10:1
Hough
014 0920Hough
Sample Volume: 750milliliters
Total Solids: 1.548 % Dry Solids
Beginning Temperature: 15.07 degrees Celsius
End Temperature: 15.75 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
0.5
9.5
1.0
Oxygen Uptake Rate: 27.13 mg Oxygen/hr
0 Ambient Specific Oxygen Uptake Rate: 2.34 mg Oxygen/g/hr
Average Temperature: 15 degrees Celsius
Temperature Correction Factor: 1.402551731
Temperature Corrected Specific Oxygen Uptake Rate: 3.2Wmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP #8
Biosolids Permit Number: W00000702
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
3/10/2014'
15.47
3/10/2014 0940
Arthur Hough
Analysis Date/Time: 3/10/2014 0942
Analyzed By: Lrthur Hough
Sample Volume: 750 n
Total Solids: 1.608
Beginning Temperature: 15.46 d
End Temperature:, 16.7 1
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.4
9.3
1.0
liliters
Dry Solids
grees Celsius
wees Celsius
25.34 mg Oxygen/hr
2.10 mg Oxygen/g/hr
16 degrees Celsius
1.31079601
Temperature Corrected Specific Oxygen Uptake Rate:mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP #9
Biosolids Permit Number: WQ0000702
Date: 3/10/2014
Digester Temperature: 15.96
Sampling Date/Time: 3/10/2014 1004
Sampled By: Arthur Hough
Analysis Date/Time: 3/10/2014 1006
Analyzed By: Arthur Hough
Sample Volume: 750,milliliters
Total Solids: 1.544 % Dry Solids
Beginning Temperature: 15.53 degrees Celsius
End Temperature: 15.87 degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mg/1)
0 8.79
1 8.32
2 7.82
3 7.52
4 7.22
5 6.91
6 6.52
7 6.14
8 5.68
9 5.23
10 4.83
11 4.54
12 4.09
13 @ 3.61
14 3.13
15 2.51
Slope: 0.4
Intercept: 8.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 24.03 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.08 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: 2.72i mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
C

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP #10
Biosolids Permit Number: W00000702
Date: 3/10/2014
Digester Temperature: 15.68
Sampling Date/Time: 3/10/2014 1022
Sampled By: Arthur Hough
Analysis Date/Time: 3/10/2014 1024
Analyzed By: Arthur Hough
Sample Volume: 750 milliliters
Total Solids: 1.566 % Dry Solids
Beginning Temperature: 15.56 degrees Celsius
End Temperature: 16.05 degrees Celsius
Dissolved Oxygen Level
YJJ,
Slope: 0.4
Intercept: 8.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 26.38 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.25 mg Oxygen/g/hr
Average Temperature: 16 degrees Celsius
Temperature Correction Factor: 1.31079601
Temperature Corrected Specific Oxygen Uptake Rate: ��= 2.9fmg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Havelock, NC WQ Permit Number: WQ0000702
WWTP Name: City of Havelock, NC WWTP NPDES Number: NCO021253
Monitoring Period: From 4/1/2014 To 6/30/2014
Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ®
I Alt B (Alk Treatment)[]
Alt. C (Prior Testing)1
A1t.D (No Prior Test) 0
1 Process to Further Reduce Pathogengs El
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost El
Heat Drying El
Heat Treatment ®
Thermophilic El
Beta Ray 1
Gamma Ray C1
Pasteurization El
Class B:
Alt. (1) Fecal Density RI
Alt. (2) Process to Significantly Reduce Pathogens El
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization 1l
Air Drying ®
Composting El
jAerobic Digestion El
Anaero
bic Digestion ElIf
applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
deucesnigue
Frequency
of Analysis
Sample
Type
Analytical
Tee -
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
19599
32359
35656
MPN/g
0
4 x year
Grab
SM9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction)
Alt. 2 (40-day bench)
Alt. 3 (30-daybench) ED
I Alt. 4 (Spec. OZ uptake) R!
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) C
jAlt. 8 (Drying - Unstable) 11
Alt. 9 (Injection)
Alt. 10 (Incorporation) (
No vector attraction reduction alternatives were performed 0
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty"of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Art Hough, WWTP Superintendent
Preparer Name and Title (ty e or print) 1
OAS Z,/Amil-
Signature of Preparer* (Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

!kSt #r`rs,' "gs Yfu.�5 �Y� .0
z
F'4 Gn' 5
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 X. JACKSON DRIVE
HAVELOCK NC 28532
ID#: 204 F
DATE COLLECTED: 04/28/14
DATE REPORTED 05/19/14
REVIEWED BY:
Sample Sample
Sludge
Analysis
Method
PARR-NIE TERS #6 #7
Sample
Date Analyst
Code
Pff, Units
6.4
04/30/14 TRB
4500HB-00
Total Residue, mg/l 36460 35720
04/29/14 MDD
-7-540D-97
Aluminum, (dry wt. basis),. mg/kg
35262
05106/14 LFJ
-LPA-200.7
Arsenic dry wt. basis), mg/kg
<2.5
05/07/14 ME 1,
3113B-04
calchnn-(dry wt. basis), mg/kg
28730
05/06/14 TFJ
EPA200.7
wt. basis), ing/kg
Cadmium r,
1.3
0511,5114 NIEL
311311-04
.(dry
Copper (dry wt. basis), mg/kg
723
05106114 LF 3
EPA200.7
Cbroul , Itun, T.(dry wt. basis),mg/kg
10
05/00114 LFJ
ri PA-7 oo. 1
Lead (dry weight basis), mg/kg
9.6
05/06/14 TNIE L
3113B-04
A,jagnesiu , in (dry wt. basis), 1119/k9
2357
05/06/3.4 LFJ
EPA200.7
Njercury (dry wt. basis), mg/ko
0.48
05/08/14 MITM
245.1 R-1-94
N ickel (dry wt. basis), mg/kg
8
05/06/14 LFJ
EPA200.7
Potassium (dry wt. basis), mg/kg
4469
05/06/14 LFJ
EPA200.7
Selenium (dry *wt. basis), mg/kg
<5,0
05/14/14 NTEL
311313-04
Sodium. (dry wt., basis), mg/kg
5513
05/06/14 TVITM
311113-99
Zinc "(dry- wt...bus1s), mg1kg
1565
05/07/14 I%ITM
311113-99
SodiumAdsorption Rv-tio
027
.
05115/14 LFJ
Total Solids, %
4.11,
04129i14 CHIC
2540G-97
TKN (dry --Q, mg/ka,
17623
05/05/14 ANO
351.2 R2-93
Ammonia Nitrogen (dry wt.),nig/lg
5054
051101/14 ANO
3503 R2-93
Phosphorus, T. . (dry wt.), mg/4
14436
05/05/14 ALB
365.4 -74
Nitrate-NiTitrite (dry wt.), mg/l(gg
< 3.92
05/02/14 ANO
353.2 112-93
Plant Available Nitrogen, mg/kg
6298
05/13/14 SEJ
Fecal Coliforin (IvffN), /grain Solids 35656 19599
04/29/14 WIDD
9221Ll-06
Molybdenum (dry wt. basis), mg/kg
< 5.0
05/06114 LFJ
EPA200.7

�CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLA14T
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
Sample Sample Sample
PAR201ETERS #1 #2 #3
Total.Residue, mg/l 32980 35400 35420
Fecal Goliforth OVUM, /gram Solids 28502 13842 .47995
ID#: 204 F
DATE COLLECTED. 04/28/14
DATE REPORTED 05/19/14
REVIEWED BY:
Sample Sample Analysis Method
#4 #5 Date' Analyst Ede
36040 35460 04/29/14 MDD 2540U-97
19423 22279 04/29/14 MI DD 9221E-06

EnviroDi—nen"', I, Inc.
P-0, Box 708-5, 414 Oakmont, Dr.
CHAIN OF CUSTODYRE.CORD
Page 1 of ''.1
Phone [phone] r-ax [phone]
DISKFECTION
TCOH ECTION
CHLORINE NEUTRALIZED A
'C
CLIENT: 20411F NN'eek: 17
pH CHECK (LAB)
UV
CITY OP -HAVELOCK
NONE
' .
.
I P
P
P
I
;-.
P
P
P
P
P.- ,
-
CONTAINER TYPE, P/G
NIR. ART HOUGH
iWASTENYATE' R,TRL1 ATIVIEN'T PLANT
r
A
CHEMICALPRESERVATION
304 N. JACKSON,I)MVE
A
A
A
A
A
A
A
A
A
UAVE4 LOCK NC 28532
A - NONE D - NAOH
E
[phone]
Ld
z J.
Uj Z'
ED
B - HNO, E-HCL
0
0
z
zc
U)
cc
C - H,-SO, F - ZINC-ACETATE/NAOH
T
0
z
z
G-NATHIOSULFATEGoLLEGON
SAMPLE LOCATION
DATE
TIME
Sample #1
LI -22-1114
w4-3
CLASSIFICATION:
DRINKINGMTER
Sample #2
Li14
2
aWASTEWATER(NPI)ES)
Sample #3-
H-2HL4
I Lis
2,
2
Sample #4.
H Iq
t if4
LU
DWQ/GW
2
Sample #5
—8
L3 SOLID WASTE SECTION
Sam0e #6
L 114
1
.1 C-
CHAIN OF CUSTODY MAINTAINED
m
Saple #7.
I I Hrq4
2
DURING 'SH PMENTIDELIVERY
Y�. N
5
a
Sludge.Sam
--4
SAMPLES COLLECTED ED BY:
oat,,
SAMPLES RECEIVED IN LABAT-IL�---C
�§C. (SAMPLEP)
R i N" 01 HED.B . Y -k
Q
DATEfTIME
M
'REC Il (SIG
DAI TIME
=Y(81Q.)
:L
P6LINQUISHED Y iSIG
DATETIME
RELINQUISHEP BY (SIG:)
DATETIME
10,EC
'�EIVEDEY(SIGI
DAI-Mi ME
PLEASE READ Instructionsthe reverse side,
for completing this form on
.the
s3ampler must -place a,'C" for composite sample or a "CT; for N 2- 75) 9 2
Grab, sample -In the blocks above for each parameter requested.

CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT'PLANT
304 X. JACKSON DRIVE
HAVELOCK NC 28532
Sample Sample
PARAMETERS #1 fl2
Total Residne, mg/1 16600 16820
ID#: 204 E
DATE COLLECTED: 06/02/14
DATE REPORTED : 06/04/14
11V
REVIEWED BY:
Sample Sample Sample Analysis Method
#3 #4 #5 Date Analyst Code'
16940 1.6620 16640 06/03/14 CMC 2546B-97

ID#: 204 E
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT DATE COLLECTED: 06/02/14
304 N. JACKSON DRIVE DATE REPORTED : 06/04/14
HAVELOCK ,NC 28532
PARAMETERS:
Total Residue, mg/l
REVIEWED BY: s��,✓".
Sample Sample Sample Sample Sample Analysis Method
#6 #7 #g #9 #10 Date Analyst Code
16340 17220 Missing Missing Missing 06/03/14 CMC 254013-97

CITY OF HAVELOCK
MR.. ART HOUGH
WASTEWATER TREATMENT PLANT
3'04 N. JACKSON DRIVE
RAVELOtK,NC 28532
-PARAMTERS
.,130% mg/1
rlecal'.C611fbrm (1411% /100, Nils
'TO" Residue, ing/1
TOM -Suspended Residue, mg/l
Ammonia Nitrogen as N, mg/l
Influent Effluent
285 < 2.0
< 1
169 < 2.5
0.05
ID#: 204 A
DATE COLLECTED: 06/16/14
DATE REPORTED : 06/23/14
REVIEWED BY:
Sample Sample Sample Analysis 'Method
#8 #9 #10 Date Analyst Code
06/16114 TRB 5219-01
06/16/14 LIV 92211)-97
15900 15720 16500 06117/14 CMC 25401347,
06/17/14 L'"' 2540D-97
06/17114 ALB 350.1 R2-93

Fecal Data Sheet 2"d Qtr. 2014
Lab Result
Log Min. 19599
32980
4.52 Max. 35656
35400
4.55 Geometric Mean 32359
35420
4.55
36040
4.56
35460
4.55
35656
4.55
19599
4.29
Average
4.51

A j)
Digester Oxygen Uptake ( Sours)
Test # I Test #
Collection Time: Collection Time: _
Collection Temp: Collection Temp:
StartTime: 9 y (-fn Start Time:
Start Temp: i 'C- Start Temp:
Start DO: - Start Do:
Min
Min
1
LL
1
2
21
2
4
c
4
5
5
f
6
6
7
7
8
4,3(
8
9
Q
9
10
3,
10
12
3, o ,)-
12
13
13
14
14
15
by
15
Stop
Temp I
Date
Stop
Temp
Date
Test #
Collection Time:
Collection Temp:
Start Time:
Start Temp:
Start Db:
Min
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Stop
Temp
Date

Digester Oxygen Uptake (Sours
Test # - CY Test # 9 (; Test #
Collection Time: '©� Collection Time:' -�, Collection Time:
Collection Temp: Collection Temp: I. 17 Collection Temp:
Start Time: - O Start Ti:meStart Time:
Start Temp: Z' Start Temp: .3 Start Temp: .
�
Start DO: . Start DO: Start DO: Ell
Min �, Min Min �� L 1
1 1 (5, f
2
n c. 2 ,s 6 t 2
3 3 3 3 C)
4 '�%, 4 , 4
5 5 (�, r 5
6 � 6 � % 715-
6
7 7
g - 8 c 8 r
9
9 J 3 9 #-3
10 10 1011 11 11
12 n 12 12 9
13 �13 13
14 3.3.5 14 14
15 "� 15 15
Stop Stop Stop
Temp �, ��� Temp , Temp-� -�
Date �
I Date �P Date
�
r

Digester Oxygen Uptake ( Sours �
Test # 15 Test #
Collection Time: CALAP Collection Time: 4ft ioo3
Collection Temp: 2,`ig Collection Temp: 9"T5
Start Time: ALt9 Start Time: too --
Start Temp: ,4 g Start Temp:
Start DO: a Start DO: N
Test #
Collection Time:
Collection Temp:
Start Time:16'�,3 c)
Start Temp: o�,-'5'<
Start DO:_
Min Min Min
1 � ►�a 1 � � 1
2 2 ,IDIO 2
3 _ 3 3
4 r`n® 4 4
5 5 . G 5
6 01 6 6
791. 7 - a 7
8 J5 8 �- 8
9 9 5 9
10 10 vj 10
11 11 - 11
12 12 12
13 13 _ 13
14 '3� 14 , � (14
15 15 , , `1 15
Stop Stop Stop
Temp t Temp Temp
Date Date Date
56
3, ;2,

Digester Oxygen Uptake ( Sours
Test # Test #
Collection Time: 95 b Aw, Collection Time:
Collection Temp: c� 6 L Collection T
Start Time: r'Start TimE
StartTemp: Start Tem
Start DO: _J, �� _ Start DO:
Min
M, C�
nn )
Min < <<
2
2 t
3
3
4
4
5
<
5
6
6
7
7
8
8
9
9
10
10
11
3;L
11
12
3,
12
13
3
13
14
�
14
15
X, S
15
Stop
Temp C, 0,s ,
Date 6 //Y
Stop
Temp
Date
Test #
Collection Time
CollectionlTemf
Start Time-`% �
Start Temp..7\--1
Start DO: ', i
Min
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Stop
Temp
Date
V
r

Digester Oxygen Uptake (Sours
Test # Test # ( a
Collection Time: .V b ,Am Collection Time: 15so FM
Collection Temp: �� �,3 ° `- Collection Temp: �S.?S®�-
Start Time: ; I(,,) r,m Start Time: 055,yM
Start Temp: Start Temp:fiS,?�� ry
Start DO: nt ` �- Start DO:.
Min
1
2
3
I
4
5
( bd6d
6
7
3,
9
10
(�
11
12
13
3 5l
3,
14
15
a,M
Stop
Temp
�,L,36,
Date
Min
2
3
7 /�
4
5.
6
S
7
3
r% .
9
4_4 i
10
31g6.
11
:3,5/
12
3, 0,
13
14
, g3
15
Stop
Temp
Date'
Test it
Collection Time: _
Collection Temp:
Start Time:
Start Temp:
Start DO. -
Min
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Stop
Temp
Date

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
' Sampling Date/Time:
Sampled By:
Analysis Date/Time
Analyzed By
Sample Volume.
Total Solids
Beginning Temperature
End Temperature
Time
(minutes)
0
1
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
7.
F.
5.1
4.E
3.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
750 milliliters
1.66 % Dry Solids
2.71 degrees Celsius
1:03 deorees Celsius
0.4
7.7
1.0
23.61 mg Oxygen/hr
1.90 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate, mg Oxygen/g/hr
0
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake
Rate
SOUR
Facility Name: Havelock WWTP
Biosolids Permit Number: WQ0000702
Date: 6/2/201
Digester Temperature
22.56
Sampling Date/Time: 06/02/14 805
Sampled By: ah
Analysis Date/Time: 06/02/14 807
Analyzed By: AH
Sample Volume:
750 milliliters
Total Solids:
1.68 % Dry Solids
Beginning Temperature
22.56 degrees Celsius
End Temperature
21.58 degrees Celsius
Dissolved Oxygen Level
7.9
7.7
4.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.4
8.4
1.0
21.28 mg Oxygen/hr
1.69 mg Oxygen/g/hr
22 degrees Celsius
0.907029478
Temperature Corrected Specific Oxygen Uptake Rate 1.53 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids.
Beginning Temperature
End Temperature
Dissolved Oxygen Level
1 6/2/2014
22.71
106/02/14 0836 1
8.11
7.67
5.
4
3.73
750 milliliters
E22
%Dry Solids
.36 degrees Celsius
21.49 degrees Celsius
Slope: 0.4
Intercept: 8.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 21.62 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.71 mg Oxygen/g/hr
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.907029478
Temperature Corrected Specific Oxygen Uptake Rate 1.55 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number
Digester Temperature
Sampling Date/Time: 06
Sampled By: ah
Analysis Date/Time. 06
Analyzed By: AF
Sample Volume:
Total Solids:
Beginning Temperature
End TemperatureL.
Dissolved Oxygen Level
(mg/1)
8.12
7.94
7.59
7.3
6.96
6.56
6.19
5.81
5.45
5.07
4.69
4.3
3.93
3.57
3.17
2.81
40908
6/2/2014
22.71
milliliters
% Dry Solids
degrees Celsius
deqrees Celsius
Slope: 0.4
Intercept: 8.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 21.87 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.76 mg Oxygen/g/hr
Average Temperature: 22 degrees Celsius
Temperature Correction Factor: 0.907029478
Temperature Corrected Specific Oxygen Uptake Rate[­­1.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
.15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
7
7
H
4.27
4.01
3.58
3.19
7
750 milliliters
L66 % Dry Solids
1.98 degrees Celsius
?.71 dearees Celsius
Slope: 0.4
Intercept: 8.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 21.44 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.72 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Temperature Corrected Specific Oxygen Uptake Rate 1.49 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Ha
W Biosolids Permit Number: I
Date:
Digester Temperature
Sampling Date/Time: 06
Sampled By: ah
Analysis Date/Time: 06
Analyzed By: F
Sample Volume:
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
■
R1
5.94
5.57
5.2
4.8
3.67
3.46
2
22.7
750 milliliters
1.63 % Dry Solids
2.78 degrees Celsius
22.5 dearees Celsius
Slope: 0.4
Intercept: 8.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 21.54 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.76 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
Qffi
Temperature Corrected Specific Oxygen Uptake Rate 1.52 mg .Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
75 7.5
5.891
4.76
4.38
4.01
41
d
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
Slope: 0.4
Intercept: 7.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 22.55 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.75 mg Oxygen/g/hr
Average Temperature: 23 degrees Celsius
Temperature Correction Factor: 0.863837599
i
- Temperature Corrected Specific Oxygen Uptake Rate 1.51 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature
End Temperature
Dissolved Oxygen Level
1
5
5
16/16/14 0950 1
741
750 milliliters
1.59 % Dry Solids
25.6 degrees Celsius
24.1 decrees Celsius
Slope: 0.4
Intercept: 7.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 21.91 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.84 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate 1.44 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
2
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Havelock WWTP
Biosolids Permit Number: W00000702
Date: 6/16/201
Digester Temperature 25.23
Sampling Date/Time: 6/16/14 1008
Sampled By: ah
Analysis Date/Time: 6/16/14 1010
Analyzed By: AH
Sample Volume: 750 milliliters
Total Solids: 1.57 % Dry Solids
Beginning Temperature 25.23 degrees Celsius
End Temperature: 24.36 degrees Celsius
Dissolved Oxygen Level
m
.15�
.41
6
5.38
5.12
4.89
4.36
Slope: 0.4
Intercept: 8.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 23.03 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.96 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate 1.53 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
(Y

Time
(minutes)
0
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Number
Date
Digester Temperature
Sampling Date/Time
Sampled By
Analysis Date/Time
Analyzed By
Sample Volume
Total Solids
Beginning Temperature
End Temperature
Dissolved Oxygen Level
m
Specific Oxygen Uptake Rate
SOUR
: Havelock WWTP
1 6/16/20141
16/16/14 1055 1
7.7
7.19
6.78
5.43
4.81
4.59
3.86
2.63
2.24
750 milliliters
1.65 % Dry Solids
25.75 degrees Celsius
24.36 degrees Celsius
Slope: 0.4
1 ntercept: 8.3
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 25.07 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.03 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate 1.59 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Havelock, NC WQ Permit Number: WQ0000702
WWTP Name: City of Havelock, NC WWTP NPDES Number: NCO021253
Monitoring Period: From 7/1/2014 To 9/30/2014
Pathogen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative Derformed:
Class A:
Alt. A (time/temp) D
Alt B (Alk Treatment) ®
Alt. C (Prior Testing)13
j
A1t.D (No Prior Test) ®
Process to Further Reduce Pathogengs ®
S
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ®
Beta Ra ®
Y
Heat Drying D
Gamma Ra D
Y
Heat Treatment D
Pasteurization ®
Thermophilic D w' ,
. .. �.�.,.
Class B:
I Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens E3 �u
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying D
Composting D
jAerobic, Digestion D
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
deuces
Frequency
of Analysis
Sample
Type
Analytical
nec -
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
5011
20417
31520
MPN/g
0
4 x year
Grab
SM9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A 1NUAC: U2'1' .11U7) - Please indicate alternative Derformed:
Alt.1 (VS reduction) ElAlt.
2 (40-day bench) ®
Alt. 3 (30-day bench) D
7lt. 4 (Spec. 02 uptake) [
Alt. 5 (14-Day Aerobic) D
Alt. 6 (Alk. Stabilization D
Alt 7 (Drying - Stable) ®
1 Alt. 8 (Drying - Unstable) D
Alt. 9 (Injection) D
Alt. 10 (Incorporation) D
No vector attraction reduction alternatives were performed D
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
D "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Art Hough, WWTP Superintendent
Preparer Name and T' le type o print)
Signature of Preparer Da e
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

n
. oo0Q@1NH@10 TU hConol oo
P.O. BOX"7085, 11.4:OAKMO.NT�
GREEIVVILLC; N.C. 27835-7085
CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
PARAME
PH, Units
Total Residue, mg/l
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), mg/kg
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio
Total Solids, %
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/kg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Fecal Coliform (MPN), /gram Solids
Molybdenum (dry wt. basis), mg/kg
Sample Sample
#6 #7
DNE [phone]
FAX [phone]
ID##: 204 F
DATE COLLECTED: 07/14/14
DATE REPORTED : 08/11/14
REVIEWED BY:
4 ---
Sludge Analysis Method
Sample Date. Analyst Code
6.3
07/17/14 TRB
45001-EB-00
31540 30040
07/15/14 LW
2540B-97
40318
07/18/14 LFJ
EPA200.7
6
07/22/14 CMF
3113B-04
34643
07/18/14 LFJ
EPA200.7
1
07/21/14 CAS
311313-04
863
07/18/14 LFJ
EPA200.7
11
07/18/14 LFJ
EPA200.7
11
07/27/14 CMF
3113B-04
2448
07/18/14 LFJ
EPA200.7
0.52
07/24/14 MTM
245.1 113-94
8
07/18/14 LFJ
EPA200.7
4501
07/18/14 LFJ
EPA200.7
<5.0
07/31/14 CMF
3113E-04
3739
07/22/14 MTM
3111B-99
1557
07/22/14 MTM
3111B-99
0.2
08/11/14 LFJ
3.65
07/15/14 LW
254OG-97
45831
07/21/14 ANO
351.2 R2-93
4145
07/17/14 ANO
350.1 112-93
15837
07/21/14 ALB
365.4 -74
5.61
07/18/14 ANO
353.2 R2-93
14584
07/22/44 SEJ
10397 5011
07/15/14 LW
9221E-06
<5.0
07/18/14 LFJ
EPA200.7

O
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GREENVILLE, N.C. 27835-7085
i
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CITY OF HAVELOCK
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
Sample
PARAMETERS #1
Total Residue, mg/l 29600
Fecal Coliform WN), /gram Solids 4392
i
t .
FC 6
F(:�, -g * '7
(-,
Sample
#2
31520
2475
Sample
#3
31360
1435
/o�V
S® it
FAX
ID#: 204 F
DATE COLLECTED: 07/14/14
DATE REPORTED : 08/11/14
756-6208
756-0633
REVIEWED BY:
Sample Sample
Analysis
Nlethod
#4 #5
Date Analyst
Code
31000 31120
07/15/14 LW
2540B-97
6774 3535
07/15/14 LW
9221E-06

P.O.'BOX 7085, 114-OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27835-7085 FAX [phone]
ID#: 204 F
CITY OF HAVELOCK
' MR. ART HOUGH
WASTEWATER TREATMENT PLANT
DATE
COLLECTED: 07/14/14
304 N. JACKSON DRIVE
DATE
REPORTED
08/11/14
HAVELOCK ,NC 28532
REVIEWED BY:
Sample Sample
Sample Sample
Sample
Analysis
Method
PARAMETERS #1 #2
#3 #4
#5
Date Analyst
Code
Total Residue, mg/l 29600 31520
31360 31000
31120
07/15/14 LW
2540E-97
Fecal Coliform WIN), /gram Solids 4392 2475
1435 6774
3535
07/15/14 LW
9221E-06
r

;Cnvironment 1, Inc. CHAIN OF CUSTODY RECORD
P.O. Box 7085, 114 Oalanont Dr. page of
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Phone [phone] °Pax [phone]
DISINFECTION
F7
CHLORINE NEUTRALIZED AT COLLECTION
CHLORINE
CLIENT: 204 F Week: 30
I
pH CHECK (LAB)
� UV
CITY OF HAVELOCK
NONE
P
P
P
P
P
P
P
P
P
CONTAINER TYPE,P/G
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
CHEMICAL PRESERVATION
304 N. JACKSON DRIVE
A
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HAVELOCK NC 28532
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SAMPLE LOC
DATE
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Sample #1
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CLASSIFICATION:
WASTEWATER (NPDES)
DRINKINGWATER
Sample #2
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Sample #3
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Sample #4
2
DWQ/GW
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Sample #5
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Sample #7
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SAMPLES COLLECTED BY:
(Please Print)
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SAMPLES RECEIVED IN LAB AT °C
RELI UI ED BY (%IG)(MPLER)
DATE/TIME
RECEIV (SIG.j
/ DATE/TIME
COMMENTS:
OWW
—ly-►y 4' I
IIUt/ C)
R , QUISHED BY (SIG.)
DATE/TIME
RECEIVED BY (SI
DATEITIME
RELINQUISHED BY (SIG)
DATEI TIME
RECEIVED BY (SIG.)
DATE(TIME
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'
Fecal Data Sheet 3rd Qtr. 2014
Lab Result
Log
Min. 5011
29600
4.47
Max. 31520
31520
4.50
Geometric Mean 20417
31360
4.50
31000
4.49
31120
4.49
10397
4.02
5011
3.70
Average
4.31

Digester Oxygen Uptake ( Sours )
Test # Test #
Collection Time: CA 30, Collection Time: 6q55
Collection Temp: 93 Collection Temp: 26• 2-5
Start Time: MM Start Time: o'--c 5
Start Temp: �3 4440 Start Temp: 2S • 95
Start DO: Start DO:
Test # S
Collection Time:
Collection Temp:
Start Time: Wao
Start Temp: 09 • (03
StartDO:
Min Min Min
2 2 2
3 q .�'`� 3 3
4 4 4
5 t 5 5 ;
6 6 6 _
7 7 7®
8 8 8 5, '�-
9 Co 9 9
10 10,gej 10 g.0
11 11 11
12 1,0,10 12 �,, 12®
13 13 319 13 q
14 Yn. 13 14 14 ?�
15 15 f 15
Stop Stop i1`j �p Stop
Temp �� Temp �� Temp
Date 1A , I Date Date

Digester Oxy erg Uptake ( Sours )
Test # Li Test #
Collection Time: IDS Collection Time: ►05-- _
Collection Temp: 2j Collection Temp: 4A,Lty
Start Time: lOLIO Start Time: 4 k o0
StartTemp: 21 StartTemp: ?q, L D
Start DO: Start DO: I . o(P
Min
1
, b
2
�L
3
4
5
6
7
8
9
10
�, A
11
12
13
14
3
15
Q
Stop
Temp
Date 8,fi, P
Test # �0 V
Collection Time: 112'S
Collection Temp:7S
Start Time: 11 9cl
Start Temp: q, S
Start DO: 01��
Min
Min
1
2� , o�r
3
3
4
G0� - �
4��
(Q i®
5
�
5
%®
6
6
(01
7
7
8
sci
8
9
9
5,
10
10
y,
11
11
,4
12
r
12
ah
13
3
13
14
ir,1
14
15
15
0' Stop
Stop
Temp
Temp
Date Date 9, Lt,14

Digester Oxygen Uptake (Sours ) ✓
Test # ---I- 1% Test # 9 Test #
Collection Time: -It--,I Collection Time: o`T Collection Time: of S
Collection Temp: • a Collection Temp:. 99,g g Collection Temp: ,
Start Time: hQu Start Time: 0110 Start Time: 0130
Start Temp: fdH-93 Start Temp: rN•.LAq Start Temp: a - 4
Start DO: (9 • G(P' StartDO: $, 05 Start DO: S.
Min Min Min
1 C�1 1 1 ,ieL
2 2 2
3 3 3,
4 4 4 .�
5 ®® 5 '(,® 5 1
6 , 66 41
7 7 7
8 5, ' �1 s s r� $
10 10
10
11 11 11
12 i.j,1� 12 ,qk 12 t
13 13 ILL 13
14 3 14 I 14
15 j 8 15 15 Gt
Stop Stop Stop
Temp Temp • , Temp
Date 6 tk Date Date

Digester Oxygen Uptake ( Sou' rs
Test # 110 Test # Test #
Collection Time: 61 S Collection Time: Collection Time:
Collection Temp: .oG Collection Temp: Collection Temp:
Start Time: 01 Start Time: Start Time:
Start Temp: o& Start Temp: Start Temp:
Start DO: C6 , 'No Start DO: Start DO:
Min Min Min
1 2. ato 1 1
2 9 .bl 2 2
3 3
3
4 4® 4
5 (n� 5
5
6 6 6
7 ► 7 7
8
8 8
9 9 9
10 10 10
11 ,� 11 11
12 1 12 12
13 3►$ 13 13 ®_
14 14 14 .�
15 15 15
Stop Stop Stop
Temp Temp Temp
Date Date Date

Digester Oxygen
Uptake ( Sours
Test # �
Test # , 7
Test #��
_i
Collection Time: c c
Collection Time: -; z�;
Collection Time:
Collection Temp'.
Collection Temp: _%-h iAc,,_ __
Collection Temp:
Start Time: �- �,L
Start Time: c, ,;_.
Start Time: �!-
-
Start Temp: 2 ; o­{ -
Start Tem p: �-��
Start Temp: ;J
Start DO: -7.35
Start DO: _ i .c.
Start DO: �c
Min
Min
Min
1 �
1
1
2 FJ�
2 c
2
3
3
3
�
4
4
5 9
5
6
5 c
6 r
5 _ r,
7
7
7
8
Q
8 c -
t• �1) -
C 7
9
9
9
10
10
10
11
11
11
12
12
12 �.
13 �.
3
13.�
13
14
14
14
15 0
15 -
15
Stop
Stop
Stop
Temp
T.0
Temp ? 6•b
Temp
Dateg--�—I-
Date Ci— S—ILL
Date
0

Digester Oxygen Uptake ( Sours
Test # i t Test #
Collection Time: �o c., Collectio Time:;_
Collection Temp: 26 s�, Collection tQ p:
Start Time: IC; c_ i, Start Time:
Start Temp: 26 �, Start Terry{5:
Start DO: 7 Start DO.
Test # _
Collection,Time.
Collection T\en}o:
Start Time: V'_
Start Temp:
Start DO,,
Min
Min
Min
2
. 7`d
2�\
3
3
4
6
4 `
4\
5
r
5
5 1
6
6
6 \
7
7
7
8
r . �-
8
8 \
9
r
9
9
10
10
10
11
y
11
11
12
12
12
13
13
13
14
14
14
15
15
15
Stop
St p
St p
Temp
6.
T mp
T rnp
Date
ly
'Date `
-Date

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name
Biosolids Permit Numbei
Digester Temperate
Sampling Date/Tin
Sampled
Analysis Date/Tin
Analyzed I
Sample Volun
Total Soli(
Beginning Temperatu
End Temperatu
Dissolved Oxygen Level
L
5.1
4.8
3.5
2.
2.
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
9/8/2014 9:0
9/8/2014 9:0
A
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.3
7.2
1.0
19.91 mg Oxygen/hr
1.67 mg Oxygen/g/hr
26 degrees Celsius
0.746215397
Temperature Corrected Specific Oxygen Uptake Rate � 1,25 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
_ 14
15
Facility Name:
Biosolids Permit Number
Digester Temperature 26
Sampling Date/Time: 9/8/2014 9
Sampled By: DS
Analysis Date/Time: 06/02/14 0745
Analyzed BY:IDS
Sample Volume: 7
Total Solids: 1.
Beginning Temperature 26.
End Temperature: 26.
Dissolved Oxygen Level
A
4.151
iilliliters
o Dry Solids
egrees Celsius
egrees Celsius
Slope: 0.3
Intercept: 7.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 16.91 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.38 mg Oxygen/g/hr
Average Temperature: 27 degrees Celsius
Temperature Correction Factor: 0.71068133
LRffi®caLT.f3ti'Sr '
Temperature Corrected Specific Oxygen Uptake Ratel 0.98 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
\/
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Datefrime:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
)issolved Oxygen Level
7.5
7.08
6.8
6.51
6.24
5.96
5.05
4.74
3.68
3.38
3.12
26.57
9/8/2014 9A
750 milliliters
1.62 % Dry Solids
6.57 degrees Celsius
6.22 degrees Celsius
Slope: 0.3
Intercept: 7.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 17.26 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.42 mg Oxygen/g/hr
Average Temperature: 26 degrees Celsius
Temperature Correction Factor: 0.746215397
Temperature Corrected Specific Oxygen Uptake Ratel 1.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
1 9/8/20141
1 9/8/2014 10:08
7.44
7.1
6.78
6.49
6.22
5.94
5.64
5.35
5.05
4.75
4.47
4.18
H58
750 milliliters
1.65 % Dry Solids
26.56 degrees Celsius
26.16 degrees Celsius
Slope: 0.3
Intercept: 7.4
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 17.64 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.43 mg Oxygen/g/hr
Average Temperature: 26 degrees Celsius
Temperature Correction Factor: 0.746215397
Temperature Corrected Specific Oxygen Uptake Rate 1.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Havelock, NC WQ Permit Number: WQ0000702
WWTP Name: City of Havelock, NC WWTP NPDES Number: NCO021253
Monitoring Period: From 10/1/2014 To 12/31/2014
Pathozen Reduction (15A NCAC 02T .1106)- Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) -0-7
Alt B (Alk Treatment)®
Alt. C (Prior Testing)
A1t.D (No Prior Test} ®
Process to Further Reduce Pathogengs ®
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost l3
Heat Drying 0
Heat Treatment ®
Thermophilic
Beta Ra Y I�
Gamma Ra C�
Y
Pasteurization
W ,
Class B:
jAlt. (1) Fecal Density —R71
Alt. (2) Process to Significantly Reduce Pathogens :=f; ; r
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ®
Air Drying ®
Composting ®
jAerobic Digestion
Anaerobic Digestion g
st on
...........................................................................................................
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ol
Excee-
dence
Frequency
of Analysis
Sample
Type
Analytical
T h-
ue
Minimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
31500
36308
48665
MPN/g
0
4 x year
Grab
SM9221E
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NUAU U2T .11U7) - Please indicate alternative Derformed:
Alt.I (VS reduction)
Alt. 2 (40-day bench) (3
Alt. 3 (30-daybench) 0
Alt. 4 (Spec. OZ uptake) D
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ®
Alt 7 (Drying - Stable) El
Alt. 8 (Drying - Unstable) Q
Alt. 9 (Injection) 13
Alt. 10 (Incorporation) lI
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .110,7 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Art Hough, WWTP Superintendent
Preparer Name an Ti e (type or print)
� 9
I��
Signature ofPrepar Da,e
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

I Emokmill�@0 11, hu wromomid
CITY OF HAVELOCK(SLUDGE)
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
L
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
Sample Sample
PARAMETERS #6 #7
PH, Units
Total Residue, mg/1
Aluminum, (dry wt. basis), mg/kg
Arsenic (dry wt. basis), mg/kg
Calcium (dry wt. basis), mg/kg
Cadmium (dry wt. basis), mg/kg
Copper (dry wt. basis), mg/kg
Chromium, T.(dry wt. basis),mg/kg
Lead (dry weight basis), mg/kg
Magnesium (dry wt. basis), mg/kg
Mercury (dry wt. basis), mg/kg
Nickel (dry wt. basis), mg/kg
Potassium (dry wt. basis), m,&g
Selenium (dry wt. basis), mg/kg
Sodium (dry wt. basis), mg/kg
Zinc (dry wt. basis), mg/kg
Sodium Adsorption Ratio
Total Solids,
TKN (dry wt.), mg/kg
Ammonia Nitrogen (dry wt.),mg/lcg
Phosphorus, T. (dry wt.), mg/kg
Nitrate -Nitrite (dry wt.), mg/kg
Plant Available Nitrogen, mg/kg
Fecal Coliform (MPN), /gram Solids
y� Molybdenum (dry wt. basis), mg/kg
31200
44872
33060
48665
ID#: 414
DATE COLLECTED: 10/20/14
DATE REPORTED : 11/26/14
REVIEWED BY:
Sludge Analysis Method
Sample Date Analyst Code
6.7
02/23/14
TRB
4500HB-00
10/21/14
CMC
254OB-97
42733
11/04/14
LFJ
EPA200.7
9
11/21/14
MTM
3113B-04
34141
11/04/14
LFJ
EPA200.7
1
11/22/14
MTM
3113B-04
861
11/04/14
LFJ
EPA200.7
12
11/04/14
LFJ
EPA200.7
16
11/25/14
MTM
3113B-04
2107
11/04/14
LFJ
EPA200.7
0.56
10/30/14
MTM
245.1 R3-94
9
11/04/14
LFJ
EPA200.7
3603
11/04/14
LFJ
EPA200.7
<5.0
11/17/14
LFJ
3113B-04
3912
11/04/14
LFJ
EPA200.7
1640
11/04/14
LFJ
EPA200.7
0.01
11/07/14
LFJ
4.06
10/21/14
CMC
2540G-97
44499
10/23/14
ANO
351.2 R2-93
4128
10/23/14
ANO
350.1 R2-93
17445
10/23/14
AKS
365.4-74
<3.87
10/22/14
ANO
353.2 R2-93
10138
11/03/14
SEJ
10/21/14
CMC
9221E-06
<5.0
11/04/14
LFJ
EPA200.7

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ID#: 414
CITY OF HAVELOCK(SLUDGE)
MR. ART HOUGH
WASTEWATER TREATMENT PLANT DATE COLLECTED: 10/20/14
304 N. JACKSON DRIVE DATE REPORTED : 11/26/14
HAVELOCK ,NC 28532
REVIEWED BY:
Sample Sample Sample Sample Sample Analysis Method
PARAMETERS #1 #2 #3 #4 #5 Date Analyst Code
Total Residue, maZ / 31500 33420 32880 32800 34540 10/21/14 CHIC 2540B-97
Fecal Coliforcn (MPN), /gram Solids 41270 23639 21290 39634 69485 10/21/14 CMC 9221E-06
(561
Fc,

R0., pox
GREENV
CITY OF HAVELOCK(SLUDGE)
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
ID#: 414 A
DATE COLLECTED: 11/20/14
DATE REPORTED : 11/25/14
REVIEWED BY:
3
Sample
Sample
Sample
Sample
Sample
Analysis
Method
PARAMETERS #5
#6
#7
#8
#9
Date Analyst
Code
Total Residue, mg/l 16180
16000
16000
14440
16160
11/24/14 KKF
2540B-97
C

Lim L ME& rn il, howpo w Ond
P.O, ,BG)( 7385, ,i.l4 _PAL<MONT,'DRIVE,'
Gr"i- Edit/[LLE,'N.C. 27835-7085..
CITY OF HAVELOCK(SLUDGE)
MR. ART HOUGH
WASTEWATER TREATMENT PLANT
304 N. JACKSON DRIVE
HAVELOCK ,NC 28532
PARAMETERS
Total Residue, mg/1
Sample Analysis Method
#10 Date Analyst Code
16260 11/24/14 KKF 2540B-97
FAX (252) 7,56=0633
ID#: 414 A
DATE COLLECTED: 11/20/14
DATE REPORTED : 11/25/14
REVIEWED BY:

R(.). Box 70' -.- , , Y Uakmont Dr.
Greenville, NC 27558
CHAIN OF CUSTODY RECORD
Ya;ce ._1_ of ---1--
CTIV11,011nu:llt 1 111C.Cc?m
Phone [phone] m Fax [phone]
DISINFECTION
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CHLORINE NEUTRALIZED AT COLLECTION j
CHLORINE
pH CHECK (LAB)
CLIENT: 414 Week: 43
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DATErfIME
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PLEASE READ instructions for completing this form on the reverse side. Sampler must place a "C" for composite sample or a"G" for 0 n
1-ow 05 G—k snmol , tt �l

Fecal Data Sheet 41h Qtr. 2014
Lab Result
Log Min. 31500
31500
4.50 Max. 48665
33420
4.52 Geometric Mean 36308
32880
4.52
32800
4.52
34540
4.54
44873
4.65
48665
4.69
Average
4.56

Digester Oxygen Uptake ( Sours �
Test # 1 0 Test #
Collection Time: ) 5 RIv) Collection Time: 4r �
Collection Temp: A' a, Collection Temp: b
Start Time: `� Js�; Start Time: /y 0�I'-1''11
Start Temp: C�, `"� Start Temp:,
Start DO: Start DO: K. 3
Min Min
1 �,31
2?, 2 n
3 3 Cv
44
5 5
6 ,/ 6
7 7
8 8 5,93
9 9
10 51 10
11
12 12
13 30 13
14 3, 9 14,
15 15 3.t
Stop Stop
Temp, �, `�� G Temp
Date 0 �% f Date
Test # 3
Collection Time:
Collection Temp:
Start Time:
Start Temp:
Start DO:
Min
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Stop
Temp
Date

Digester Oxygen Uptake ( Sours
Test # Test # > Test #
Collection Time: �. 3' /� Collection Time: �; �� Collection Time: ; -f
Collection Temp: J,C),2,q Collection Temp: 13, "��� Collection Temp: / 3.
Start Time: /Q' o �n.� StartTime: a VO p.,,v) Start Time: 7
Start Temp: Start Temp: Start Temp: i3,C/ 6C.
Start DO: 331 q q 0,4, StartDO: Start DO,
Min (V" Min �' �" Min
1 g 3 1 c�,53
2 13 2 2
3 3 11� 9 3
4 4 r' 4 c
5 5 ? 5 �. P
6 C.0 6 ' 6
7 S5 7 �',r 7 r%
9 9 i 3� 9
10 S , - 10 ' 10
11 1 Lay. 11 c 3
12 5 12 ; 12
13 13 13 af3
14 ,, 14 S, P.5 14
15 3,`i'5 15 S'_ 5 15
Stop �. Stop d Stop
Temp d, �� �` Temp Temp
�� Date /� , �� Date //�
Date /o. i / ,

Digester Oxygen Uptake ( Sours
Test # Test #
Collection Time: P"� Collection Time: _
Collection Temp: Collection Temp:.
Start Time: Start Time:
Start Temp: Start Temp
Start DO: R,(. Start DO:
Min
1
�?1.
2
( c-
3
1.53
,J
5
6
719 q
7
,'
8
5'
9
'
10
11
12
13
S
14
Q CI
15
�, f
Stop
Temp 3_
Date
Date
Test #
Collection Tim
Collection Ter �p:
Start Time:
Start Temp:
Start DO:
Min
3\ i
4 \
5.
6 �. 1
7
8
9
10
11 't
12
13
14
15
Stop J
Temp
Date

Liciaofcr wxygen UptaKe ( Sours
Test #
Test #
Collection Time: aa5 Collection Time: )3z
Collection Temp: Start Time: Collection Temp:
p:
S
—� tart Time: _ , � �;� _
Start Temp: _! 2 , �-� Start Temp:
Start DO: _ V .4,5 Start DO: 5,
Test # ! o
Collection Time. -
Collection Temp:
StartTime: i o 55
Start Temp: 13 : 3 r,
Start DO: �,e
Min(Viin
1
Min
2
`1 0
1
1
,� � v
3
t
2
r
2
. 5�
3
3
;.�,�'
S
5
6
7
6
6
s
7
8
7
a
9
10
LiCt
9.
9,
1.p
10
12
1 x1.w6c<
14
13�`
L
13
k.,
15
14
P
15
5
.Stop-
Temp
.,.:,Stop
Temp
i y , q
Stop
Temp
W cl
Date
Date
,,_ , _„�
Date

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Digester Temperature:.
Sampling Date/Time: 10/27/14 0915
Sampled By: ah
Analysis Date/Time: 10/27/14 0915
Analyzed By: AH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temoerature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
W.
0.3
8.9
1.0
illiliters
Dry Solids
agrees Celsius
:arees Celsius
20.39 mg Oxygen/hr
1.67 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rater 1.59�mg Oxygen/g/hr
------� -�--�
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

I
Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: `Havelock WWTP
Biosolids Permit Number: WO0000702
Date: 10/
Digester Temperature:
Sampling Date/Time: 10127/14 1000
Sampled By: ah
Analysis Date/Time: 10/27/14 1002
Analyzed By: AH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
20.
750 milliliters
1.65 % Dry Solids
0.77 degrees Celsius
0.97 dearees Celsius
0.3
8.6
1.0
20.75 mg Oxygen/hr
1.68 mg Oxygen/g/hr
21 degrees Celsius
0.952380952
Temperature Corrected Specific Oxygen Uptake Rate: 1.60 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
i�
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:,—.750
Total Solids:
Beginning Temperature:
End Temperature:
Havelock WWTP
milliliters
% Dry Solids
degrees Celsius
dearees Celsius
WQ0000702
10/27/2014
20.29
10/27/14 1020
ah
10/27/14 1022
AH
1.68
20.29
20.39
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.3
8.9
1.0
19.03 mg Oxygen/hr
1.51 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate: + ,y 1.515himg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
10/27/2014
20.27
0/27/14 1038
h
0/27/141040
,H
750 milliliters
1.67 % Dry Solids
20.29 degrees Celsius
20.39 degrees Celsius
0.3
8.7
1.0
18.86 mg Oxygen/hr
1.51 mg Oxygen/g/hr
20 degrees Celsius
1
Temperature Corrected Specific Oxygen Uptake Rate:; 1.51' mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Havelocl
Biosolids Permit Number: W0000(
Date:
Digester Temperature:
Sampling Date/Time: 11/20/20
Sampled By: ah
Analysis Date/Time: 11/20/20
Analyzed By: AH
Sample Volume:
Total Solids.
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
11 /20/2014
13.84
4 0845
4 0846
750 milliliters
1.62 % Dry Solids
13.841degrees Celsius
14.2611dearees Celsius
0.3
9.8
1.0
Oxygen Uptake Rate: 16.80 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.38 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 2.07 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
V
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Havelock V
Biosolids Permit Number: WQ00007C
Date:
Digester Temperature:
Sampling Date/Time: 11/20/2014
Sampled By: ah
Analysis Daterrime: 11/20/2014
Analyzed By: AH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
11 /20/2014
05
750 milliliters
1.6 % Dry Solids
13.4 degrees Celsius
4. 22 degrees Celsius
0.2
9.4
1.0
14.09 mg Oxygen/hr
1.17 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.76wmg Oxygen/g/hr
A-- --- .01
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Digester Temperature:
Sampling Date/Time: 11
Sampled By: ah
Analysis Date/Time: 11
Analyzed By: Al -
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
14 0929
1
13.41
Ililiters
Dry Solids
grees Celsius
grees Celsius
Slope: 0.2
Intercept: 9.0
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 11.32 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.94 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.42 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
' (minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Havelock WWTP
Biosolids Permit Number: W00000702
Date: 11/20/201
Digester Temperature:
Sampling Date/Time: 11/20/2014 0954
Sampled By: ah
Analysis Date/Time: 11/20/2014 0955
Analyzed By: AH
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
750 milliliters
1.44 %Dry Solids
12.77 degrees Celsius
13.95 degrees Celsius
0.2
9.2
1.0
Oxygen Uptake Rate: 11.77 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.09 mg Oxygen/g/hr
Average Temperature: 13 degrees Celsius
Temperature Correction Factor: 1.605781476
Temperature Corrected Specific Oxygen Uptake Rate: 1.7 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: H�
Biosolids Permit Number: W
Date:
Digester Temperature:
Sampling Date/Time: 11
Sampled By: al -
Analysis Date/Time: 11
Analyzed By:Al'
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes)
(mg/1)
0
8.92
1
8.8
2
8.65
3
8.47
4
8.3
5
8.14
6
7.87
7
7.66
8
7.46
9
7.22
10
6.98
11
6.71
12
6.47
13
6.24
14
5.99
15
5 7Fi
11 /20/201
750 milliliters
1.61 % Dry Solids
13.25 degrees Celsius
14 449 degrees Celsius
Slope: 0.2
Intercept: 9.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 13.02 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.08 mg Oxygen/g/hr
Average Temperature: 14 degrees Celsius
Temperature Correction Factor: 1.500730352
Temperature Corrected Specific Oxygen Uptake Rate: 1.62 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name: Havelock WWTP
Biosolids Permit Number: WO0000702
Date: 11 /20/2014
Digester Temperature: 13.84
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
11 /20/2014 1054
ah
11 /20/2014 1055
AH
750 milliliters
Total Solids: 1.62 % Dry Solids
Beginning Temperature: 13.36 degrees Celsius
End Temperature: 14.49 degrees Celsius
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.2
9.0
1.0
13.04 mg Oxygen/hr
1.07 mg Oxygen/g/hr
14 degrees Celsius
1.500730352
Temperature Corrected Specific Oxygen Uptake Rater 161,mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Page 1 of 4
Report Number: 1.4-050-0657
L
Account Number: 45671
Www.aleastern.com
Send To: BIO-NOMIC SERVICES INC
Joel Coert
516 ROUNDTREE RD
CHARLOTTE NC 28217
14 AMA4A n�{e of A-Ivc
rc• n9/90/9rf9d
A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
Grower:
HAVELOCK NC
SPENCER FARMS
SOIL ANALYSIS REPORT
rlatp of Rpnnrt- n2/2n/2n14
Submitted By: DON GREENE
Farm ID:
Analytical Method(s):
Mehlich 3
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t -Ca•.<•
Soil°:µw°
`r
=,Buffer°
x
FIeId,ID.
...
Number
o f.<.Rate.
b
i
,a•
Rate
cis'.
`m Rate
rrr Rate
Pm Rate:
pH
m 10
eq/ 9g,
m' 10
eq� Og
m ate -
m
pq.
.pp
1A
3.0
177 VH
141 M
M
1652 H
6.6
0.6
10.4
A
Sf fiU-1A
08344
M 95
NC=147
NC=72
1134
1 B
146 VH
117 M
96 L
1101 M
5.6
6.73
2.0
8.6
/
.P j � " /�
08345
2.9 M 96
NC = 122
NC = 60
1 C
169 VH
135 H
97 L
1259 M
5.8
6.75
1.8
9.2
IT C
08346
3.0 M 97
NC=141
NC=69
ID
151 VH
129 H
103 L
1156 M
5.8
6.77
1.6
8.6
ri-j
PA
08347
I
2.8 M 94
I
(b
NC=126
NC=66
1 E
]a�`
08348
2.9 M 95
1127 VH
122 M
C=62
104 L
1169 M/5.6
6.72
2.1
9.2
bNC
= 106
'�BaSe:Satu�ation �&;Nitrate
.Sulfur
>ra Ztric��
Man e:,
ro�gres�Percent
;
,
B
' °s
umiru �.
ui
Z
Mn
wCu
"`C
;
S �
i'
k, .,
..t
Fteld ID.
>,
3,
'�rn:
'"m�=
:£
.�
m
0
/o,
0.� .''-�'
,
r -�,/o= ,
;�:,.•/o
/o
rn ul2ate
E.,,Rates.
'
,Rate
tPP m a-��,Rate'i
PPm. 4Rate
�..
ter,
-
pP"
,P P m >
,/o„w
1A
3.5
10.7
79.4
5.9
1B
3.5
9.3
64.0
23.3
1C
3.8
8.8
68.4
1D
3.8
10.0
67.2
19.0
1E
3.4
9.4
63.5
23.2
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. - Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by; �ptue� me G4 (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
Salts ms/cm x 640 = ppm.

Page 2 of 4
Report Number: 14-050-0657
Account Number: 45671
Send To: BIO-NOMIC SERVICES INC
Joel Coert
516 ROUNDTREE RD
CHARLOTTE NC 28217
Date Received: 02/19/2014
JAL- �{ A&L Eastern Laboratories
7621 Whitepine Rdad Richmohd, Virginia 23237 (804) 743-'9401 Fax[phone]
wwwaleasfern:caln Submitted B DON GREENE
Grower: Y
HAVELOCK NC Faun ID:
SPENCER FARMS
ACML FERTILITY RECOMMENDATIONS
`hate,.
:W^^�
�Sulfuc;...
Zinc
''ri anese ,
Iroru�.=-
pP er
3
oron =,
.,. ...'§-.. 43
- .>, 1 .. .. fi. .,., to , sr,-,..,.;
,.�.,..e .Ch ..... ...,. .x.r,
". ,„ w..,:. ... ..:'
..
..:w. '.''
x..x '• n:
a�»,. =..r',°:
4 n•i
.,,:"y'..
,..6•
�
,,.s ;;i„
`
,Sam Ie;,ID`.,
:
.e ...: x
-�Yteld •G �
._:�.
,� ,�
�... _
'O.
_ �. • �
M
_ { �� � .
S..
Zn
.,�IIAn P
3 .
. Fe W.:
.� � ;
...,..
F el tl ID
�,.
E
,.f,4sY
b
.i ..
1A
Corn
180
0.0
202
0
92
0
1B
Corn
180
1.3
202
30
93
0
1 C
Corn
180
1.0
202
0
80
0
1D
Corn
180
1.0
203
0
.84
0
1 E
Corn
180
1.3
202
30
89
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q me Gar
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1r�
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary

Page 3 of 4
Report Number: 14-050-0657
AV
Account Number: 45671 I
LL
www,aleastern.com
Send To: BIO-NOMIC SERVICES INC
Joel Coert
516 ROUNDTREE RD
CHARLOTTE NC 28217
Date Rpr_PivPde n9/19/9014 Date Of Analysis' 02/20/2014
A&L (Eastern Labaratones
7621 Whitepine Road Richmond,Vfrglnia 23237 [phone] Fax.[phone]'
Grower: Submitted By: DON GREENE
HAVELOCK NC Farm ID:
SPENCER FARMS
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Date Of Report: 02/20/2014
j;
@Oi'` a"riic
q.
4
s". aPFios ho�us-�..•. J'
:''Potassium..
v—
•:�Ma nesu
i °m
Calcium""
odium
S: �
�
x p,
� Acidi
;�--
t
��
?mot :, ; .. . ,: „- , ., ,,, a. L
•,tz•,. a
_ ,t :
.1.;
:�•
€�,. ,�
:Sam ` le p
�_,
2'
```�
Reserve•=�
�s K •.,.:.,,;�.
� M r„i
v
C -�
a>
}
Na �r
Soil�,
Buffer:
�
"ram
=Numtie
s ��;
/o°• Rae -�
.:�.
'
�t..
?
..�
'
,,.... ,...�
.fr>
.;, .u,x_«.,-�w�•�:r wwlbs/A F"Index
�
;men 1100
..me�%100
1 F
194 VH
145 H
108 L
1233 M
d
08349
2.9 M 95
5.7
6.73
2.0
9.4
� PA-1 -
NC = 162
NC = 74
1
1 G
/gA
08350
2.9 M 96
163 VH
128 H
195 L
1085 M
5.6
6.73
2.0
8.5
�,
J�" rj*�6J.
F
NC = 136
NC = 65
. ".
rr k•,in=.<
Percent Base,Saturatlon
Nitrate
Sulfur
Zmc:r<.,
:,Mangariese<
Iron'
copper
Boron
§olulile:salts u
: `"''Clilb�ide. _
.Aluminum'.
P
K�
N
Fe
Gu:'
B
x
$$ �x
,~� CI a, ".
AI-A1:
Sa a
p -
F.e d .
� ar.s
=C
�� tJ
FI �
NON
S ,�,.:y:�.�.;Zn
�.:
:� . Mh;�
,�•.:r„
,
, . � e:
"-•
,
✓_o
"
`
'K
mRate
:}
nRatpPe
PP«m T 5,
E
h
t
,
fig•
3
1F
4.0
9.6
65.6
21.1
1G
3.9
9.3
63.8
23.4
Values on this report represent the plant available nutrients in the
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
H (High), VH (Very High). ENR - Estimated Nitrogen Release.
C.E.C. -Cation Exchange Capacity.
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
(pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
(milli -equivalent per 100,grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
Salts ms/cm x 640 = ppm.
by: 'QWia mF Gewr
Pauric McGroary

Page 4 of 4
Report Number: 14-050-0657
Account Number: 45671
Send To: BIO-NOMIC SERVICES INC
Joel Coert
516 ROUNDTREE RD
CHARLOTTE NC 28217
Date Received: 02/19/2014
nnE o.t•• noionionld
- A&L Eastern Laboratories
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax-(804).271-8446
mrwwaleastem.-Com Submitted B DON GREENE
Grower: Y
HAVELOCK NC Farm ID:
SPENCER FARMS
SOIL FERTILITY RECOMMENDATIONS
3� ,9.
X PFi s 'hate~
0
.Pofash
-Ma"' nesium
<Su _
'Zmcstx
a n anese4s
9
. Iro
pp,,,
`orori
<�B
am
'Y
R
:i1 rV
C"
le
s
_K
`�r
M
-
- x.;,..;,:,,
�.
, ....,,,,E , � ' ., ... v
^s,'..;: •• ,.�
� xx� � ,..� _
., ..;,'Fix ��
.., /A;,..
•.:...:r � ...
�
,�,�:`u
h,:-<
v
...y
.� 1..,rc,..,�
y}:.
1F
Corn
180
1.3
202
0
73
0
[VG
Corn
180--]
1.3
202
0
85
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." nt
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the ?of;. rm0
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary