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HomeMy WebLinkAboutWQ0000672_2014 Residual Annual Report_20150212CITY OF LUMBERTON, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0000672 2014 ANNUAL REPORT City of Lumberton, NC Residuals Land Application Program 2014 Annual Report TABLE OF CONTENTS 1. Certification Form, Annual Operations Summary, Facility and Land Applier Contact Information 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH & Lime Application Records 7. Soil Analyses ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00000672 County Robeson Year 2014 Facility Name (as shown on permit) City of Lumberton WWTP &WTP NPDES No. NC0024571& 03-78-010 Land Application Operator Synagro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A — Residuals Application Summary: Total number of application fields in the permit: 83 Total number of fields utilized for land application during the year: 10 Total amount of dry tons applied during the year for all application sites: 958.45 Total number of acres utilized for land application during the year: 350.0 Part B — Annual Compliance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C — Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Jim Walters. Director of EUS Dept. Permittee Name and Title (type or print) Signature of Preparer* Date (if different from Permittee) 1nn�l jjjjjj���- ''.�—�--1 a Pe ittee DDa�tei It 20 -157 Signature of L d Applier rr�� DD��Dat �e (if different from Permittee and Preparer) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION LUMBERTON, NC LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID MONTHNEAR March 2014 April 2014 October 2014 YEARLY TOTAL 1,302,000.00 G 719,200.00 G 1,413,600.00 G 3,434,800.00 G LUMBERTON, NC WWTP LIME STABILIZED LIQUID MONTHNEAR May 2014 June 2014 July 2014 YEARLY TOTAL AMOUNT UNIT 1, 271, 000.00 G 843,200.00 G 1,134,600.00 G 3,248,800.00 G DRY TONS UNIT 174.30 D 96.28 D 160.91 D 431.49 D DRY TONS `.'UNIT 206.16 D 136.77 D 184.03 D 526.96 D DRY METRIC TONS 158.08 87.32 145.96 391.36 DRY METRIC TONS 187.00 124.05 166.93 477.98 1 /28/2015 2014 ANNUAL REPORT PROJECT: City of Lumberton, NC FACILITY: Lumberton WWTP 700 Lafayette St. Lumberton, NC 28358 910-671-3859 NPDES PERMIT NUMBER: RESPONSIBLE OFFICIAL: FACILITY OPERATOR: LAND APPLIER AND PREPARER OF LAND APPLICATION ANNUAL REPORT: NCO024571 Jim Walters, Director EUS Dept. City of Lumberton PO Box 1388 Lumberton, NC 28359 910-671-3856 Jon Locklear, WWTP Operator City of Lumberton 700 Lafayette St. Lumberton, NC 28359 910-671-3859 Synagro Central, LLC Contact: Marshall Puryear (336) 998-7150 ext. 17 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0000672 Laboratory Facility Name: LUMBERTON, NC A&L Eastern Laboratories Inc. NPDES# : NCO024571 or WQ# (residual only) WWTP Name: LUMBERTON WWTP Residuals Analysis Data Product Type AEDLIQ LSLIQ AEDLIQ AEDLIQ Date Sampled (grab) or 01/17/14 05/06/14 06/05/14 08/25/14 Date Composited Percent Solids 3.21 3.89 2.61 2.73 PARAMETERS (mg/kg dry weight) Arsenic 4 3 5 6 Cadmium <2 <2 <2 <2 Mercury 0.7 0.7 0.4 0.4 Chromium 280 213 244 331 Copper 289 227 302 372 Lead 17 12 17 26 Molybdenum 5 <5 6 6 Nickel 33 25 43 58 Selenium <5 <5 <5 <5 Zinc 536 421 482 385 Total Phosphorus 18300 15600 17400 19200 TKN 54200 47800 67000 42900 Ammonia -Nitrogen 5610 5910 13000 1830 Nitrate and Nitrite 1640 18 <2 114 "I certify, under penalty of law, that thisdocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X ,TP,RE OF PREPARER) Date a - 4 '-�o tJ DENR FORM RSSF (5/2003) Printed: Wednesday -January 28, 2015 at 11:25:14 for: 2101 01 ANNUAL RESIDUALS SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0000672 Laboratory Facility Name: LUMBERTON, NC A&L Eastern Laboratories Inc. NPDES# : NCO024571 or WQ# (residual only) WWTP Name: LUMBERTON WWTP Residuals Analysis Data Product Type AEDLIQ LSLIQ AEDLIQ AEDLIQ Date Sampled (grab) or 01/17/14 05/06/14 06/05/14 08/25/14 Date Composited Percent Solids 3.21 3.89 2.61 2.73 PARAMETERS (mg/kg dry weight) Aluminum 27300' 23600 27000 28000 Calcium 14700 94900 10900 23000 Magnesium 2080 6200 2580 3080 pH 6.67 11.56 7.56 7.44 Potassium 3680 2830 3910 2830 Sodium 11200 5620 8420 10300 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." X (S NR - Data Not Reported or Data Not Required Date ®2 . Y-- a v / )� DENR FORM RSSF-B (7/2002) Printed: Wednesday -January 28, 2015 at 11:25:52 for: 2101 01 Page: i of 2 Report Number: 14-022-0202 Account Number: 46525 Submitted By: EDWARD STEPHENS Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 97589 Sample Id: LUMBERTON @9, A&L Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804)'743-9401 Fax (804) 271-6446 wwwaleastem.com Project: LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/17/2014 10:30:00 Date Received: 01/22/2014 00:00 Date Reported: 01/27/2014 Total Solids * 3.21 32100 100.0 JM 01/22/2014 13:30 SM-2540G Moisture" 96.79 100.0 JM 01/22/201413:30 SM-2540G Total Kjeldahl Nitrogen 5.42 54200 10.0 JM 01/23/2014 07:39 SM-4500-NH3C-TKN Total Phosphorus 1.83 18300 100 KM 01/23/2014 15:23 SW 6010C Total Potassium 0.37 3680 100 KM 01/23/2014 15:23 SW 6010C Total Sulfur 1.01 10100 100 KM 01/23/2014 15:23 SW 6010C Total Calcium 1.47 14700 100 KM 01/23/2014 15:23 SW 6010C Total Magnesium 0.21 2080 100 KM 01/23/2014 15:23 SW 6010C Total Sodium 1.12 11200 100 KM 01/23/2014 15:23 SW 6010C Total Iron 23400 100 KM 01/23/2014 15:23 SW 6010C Total Aluminum 27300 100 KM 01/23/2014 15:23 SW 6010C Total Manganese 328 5 KM 01/23/2014 15:23 SW 6010C Total Copper 289 5 KM 01/23/2014 15:23 SW 6010C Total Zinc 536 5 KM 01/23/2014 15:23 SW 6010C Ammonia Nitrogen 0.56 5610 10.0 JM 01/23/2014 07:39 SM-4500-NH3C Organic N 4.86 48590 10.0 01/23/2014 07:39 CALCULATION Nitrate+Nitrite-N 1640 2.00 JM 01/23/2014 07:40 SM-450ONO3F Total Cadmium Q.0 2.0 KM 01/23/2014 15:23 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made 8 to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-022-0202 Account Number: 46525 Submitted By: EDWARD STEPHENS Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Lab Number: 97589 Sample Id: LUMBERTON Y A&L Eastern Laboratories,. Inca 7621 Whitepine Road Richmond, Virginia.23237 (804) 743-9401 Fax (804) 271.WG VAMaleastern.com Project: LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/17/2014 10:30:00 Date Received: 01/22/2014 00:00 Date Reported: 01/27/2014 Total Chromium 280 5 KM 01/23/2014 15:23 SW 6010C Total Nickel 33 5 KM 01/23/2014 15:23 SW 6010C Total Lead 17 5 KM 01/23/2014 15:23 SW 6010C Total Arsenic 4.0 3.0 KM 01/23/2014 15:23 SW 6010C Total Mercury 0.7 0.4 KM 01/23/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 01/23/2014 15:23 SW 6010C pH (Standard Units) ` 6.67 2.00 JM 01/23/2014 07:39 SW-9045D Total Volatile Solids 68.88 688800 100.0 JM 01/22/2014 13:30 SM-2540G Total Molybdenum 5 5 KM 01/23/2014 15:23 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Mg", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt ------ ---- sAMPLI V).G Vj, Ambb. A & ff MVE 7621i 2-p20Z ME):& ANALYSIS 6)"NAGRO SOUTHEAST Richi 46525 .2014 CUSTOMER:: 80�5, LLOCOMBERTON 12,,��43 SY NAGRO-CENTRAL MBERTON tafoplIng �iqcqdures PROJEOT I�ANAGE9,'- -�,mcrtdon,of thaseisam, plbs, Phone.. A ER �SAMPLING SAMPLE. 40E-� SAMPL-1140: METHO VET -LAS SAMPLE 1U. LOCATIOW TYPE- CONTAINERS DATE TIME', PRESERV-E�b,SHfP.PEb .jr X-V Reli N bd by; .9 ke"r" Date Tme Becleved'by, REMARKS: , SPEbJAC*_.STRU'CT(0NS! For —ftnitori . qdl_pqrposep. po#: SAMPLE -ANALY.-sis BEQUEST '80, 6172, 'NH,441 NO;�-N. Organic Cd 'Cr Ni Pb As H9 so _pH_ equiv. Ma cl, . ... . 10, 01- Total Solids Phospljprus', and: Pbtb�§s; S lurn bbsic'tert, lu ultor,:Pal�ium,MebriQsiur,$bdium,-Iron,Alumlnum� Gopper and,7 W —A 8L —MANAOUI COPY hite I L Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 1/17/2014 111/2014-4130/2014 4.0939 LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (11200 x 3.2100) = 100 = 359.52 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (14700 x 3.2100) = 100 = 471.87 Mg mg/I = (mg mg/kg x % Solids) = 100 = (2080 x 3.2100) =100 = 66.768 Na meq = Na mg/I = Molec.Wgt.Na = 359.52 = 23 = 15.6313 Ca meq = Ca mg/I -= Molec.Wgt.Ca = 471.87 _ 20 = 23.5935 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 66.768 = 12 = 5.564 SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 15.6313 = SgrRoot[0.5(23.5935+5.564)] = 4.09388 Printed: 1/28/2015 Page 1 11:29 Page: 1 of 2 Report Number: 14-129-0205 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55272 Sample Id: LUMBERTON LIME STAB A&L Eastern Laboratories,. Inc.. 7621 Whitepine Road Richmond, Virginia 23237 (804)743-9401 Fax (804) 271-6446 wwwaleastern.com Project: LUMBERTQN NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/6/2014 13:00:00 Date Received: 05/09/2014 00:00 Date Reported: 05/15/2014 Total Solids * 3.89 38900 100.0 JM 05/09/2014 13:59 SM-2540G Moisture * 96.11 100.0 JM 05/09/2014 13:59 SM-2540G Total Kjeldahl Nitrogen 4.78 47800 10.0 JM 05/12/2014 08:39 SM-4500-NH3C-TKN Total Phosphorus 1.56 15600 100 KM 05/12/2014 13:47 SW 6010C Total Potassium 0.28 2830 100 KM 05/12/2014 13:47 SW 6010C Total Sulfur 0.78 7800 100 KM 05/12/2014 13:47 SW 6010C Total Calcium 9.49 94900 100 KM 05/12/2014 13:47 SW 6010C Total Magnesium 0.62 6200 100 KM 05/12/2014 13:47 SW 6010C Total Sodium 0.56 5620 100 KM 05/12/2014 13:47 SW 6010C Total Iron 19100 100 KM 05/12/2014 13:47 SW 6010C Total Aluminum 23600 100 KM 05/12/2014 13:47 SW 6010C Total Manganese 170 5 KM 05/12/2014 13:47 SW 6010C Total Copper 227 5 KM 05/12/2014 13:47 SW 6010C Total Zinc 421 5 KM 05/12/2014 13:47 SW 6010C Ammonia Nitrogen 0.59 5910 10.0 JM 05/12/2014 08:39 SM-4500-NH3C Organic N 4.19 41890 10.0 05/12/2014 08:39 CALCULATION Nitrate+Nitrite-N 18.0 2.00 JM 05/12/2014 08:40 SM-450ONO3F Total Cadmium <2.0 2.0 KM 05/12/2014 13:47 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-129-0205 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary -Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55272 Sample Id: LUMBERTON LIME STAB A&L. Eastern Laboratories, Inc._ 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwWaleastern.Com Project: LUMBERTON NC CERT#257 REPORT OF ANALYSIS Date Sampled: 5/6/2014 13:00:00 Date Received: 05/09/2014 00:00 Date Reported: 05/15/2014 Total Chromium 213 5 KM 05/12/20.14 13:47 SW 6010C Total Nickel 25 5 KM 05/12/2014 13:47 SW 6010C Total Lead 12 5 KM 05/12/2014 13:47 SW 6010C Total Arsenic 3.0 3.0 KM 05/12/2014 13:47 SW 6010C Total Mercury 0.7 0.4 KM 05/14/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 05/12/2014 13:47 SW 6010C pH (Standard Units) * 11.56 2.00 JM '05/12/2014 08:39 SW-9045D Calcium Carbonate Equivalent 19.10 191000 100 JM 05/13/2014 09:20 AOAC 955.01 Total Molybdenum <5 5 KM 05/12/2014 13:47 SW 6010C Comments: CCE, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Cr", "Ni", AND "Pb". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2101-01-LSLIQ-NC LUMBERTON, NC WWTP LIME STABILIZED 5/6/2014 511/2014-7131/2014 0.9306 LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (5620 x 3.8900) _ 100 = 218.618 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (94900 x 3.8900) = 100 = 3691.61 Mg mg/I = (mg mg/kg x % Solids) = 100 = (6200 x 3.8900) + 100 = 241.18 Na meq = Na mg/I = Molec.Wgt.Na = 218.618 = 23 = 9.50513 Ca meq = Ca mg/1= Molec.Wgt.Ca = 3691.61 + 20 = 184.581 Mg meq = Mg mg/I + Molec.Wgt.Mg = 241.18 + 12 = 20.0983 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.50513 = SgrRoot[0.5(184.581+20.0983)] = 0.939586 Printed: 1/28/2015 Page 1 11:30 Page: 1 of 2 Report Number: 14-161-0204 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55833 Sample Id : LUMBERTON WWTP 9A&LL Eastern Laboratories, Inc. .7621 Whitepine Road Richmond, Virginia.23237 (804) 743-9401 Fax (804) 271-W6 - - ® -- www,aleastern.com Project: LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/5/2014 14:20:00 Date Received: 06/10/2014 00:00 Date Reported: 06/17/2014 Total Solids * 2.61 26100 100.0 JM 06/10/2014 14:35 SM-2540G Moisture * 97.39 100.0 JM 06/10/2014 14:35 SM-2540G Total Kjeldahl Nitrogen 6.70 67000 10.0 JM 06/11/2014 08:30 SM-4500-NH3C-TKN Total Phosphorus 1.74 17400 100 KM 06/11/2014 12:15 SW 6010C Total Potassium 0.39 3910 100 KM 06/11/2014 12:15 SW 6010C Total Sulfur 0.84 8390 100 KM 06/11/2014 12:15 SW 6010C Total Calcium 1.09 10900 100 KM 06/11/2014 12:15 SW 6010C Total Magnesium 0.26 2580 100 KM 06/11/2014 12:15 SW 6010C Total Sodium 0.84 8420 100 KM 06/11/2014 12:15 SW 6010C Total Iron 25700 100 KM 06/11/2014 12:15 SW 6010C Total Aluminum 27000 100 KM 06/11/2014 12:15 SW 6010C Total Manganese 228 5 KM 06/11/2014 12:15 SW 6010C Total Copper 302 5 KM 06/11/2014 12:15 SW 6010C Total Zinc 482 5 KM 06/11/2014 12:15 SW 6010C Ammonia Nitrogen 1.30 13000 10.0 JM 06/11/2014 08:30 SM-4500-NH3C Organic N 5.40 54000 10.0 06/11/2014 08:30 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 06/11/2014 08:30 SM-450ONO3F Total Cadmium <2.0 2.0 KM 06/11/2014 12:15 SW 6010C All values are on a dry weight basis except as noted by asterisk.' Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-161-0204 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 55833 Sample Id : LUMBERTON WWTP @P. A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 wwwaleastern.com Project. LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 6/5/2014 14:20:00 Date Received: 06/10/2014 00:00 Date Reported: 06/17/2014 Total Chromium 244 5 KM 06/11/2014 12:15 SW 6010C Total Nickel 43 5 KM 06/11/2014 12:15 SW 6010C Total Lead 17 5 - KM 06/11/2014 12:15 SW 6010C Total Arsenic 5.0 3.0 KM 06/11/2014 12:15 SW 6010C Total Mercury 0.4 0.4 KM 06/12/2014 12:00 SW-7471 B Total Selenium <5.0 5.0 KM 06/11/2014 12:15 SW 6010C pH (Standard Units) * 7.56 2.00 JM 06/11/2014 08:24 SW-9045D Total Molybdenum 6 5 KM 06/11/2014 12:15 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "As". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 6/5/2014 / / - / / 3.0340 LIQUID Na mg/1= (Na mg/kg x % Solids) : 100 = (8420 x 2.6100) + 100 = 219.762 Ca mg/1= (Ca mg/kg x % Solids) + 100 = (10900 x 2.6100) + 100 = 284.49 Mg mg/I = (mg mg/kg x % Solids) + 100 = (2580 x 2.6100) + 100 = 67.338 Na meq = Na mg/I + Molec.Wgt.Na = 219.762 + 23 = 9.55487 Ca meq = Ca mg/I + Molec.Wgt.Ca = 284.49 + 20 = 14.2245 Mg, meq = Mg mg/I + Molec.Wgt.Mg = 67.338 + 12 = 5:6115 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 9.55487 + SgrRoot[0.5(14.2245+5.6115)] = 3.03398 Printed: 1/28/2015 Page 1 11:30 Page: i of 2 Report Number: 14-240-0202 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 57265 Sample Id: LUMBERTON WWTP A&L Eastern Laboratories, Inc:. 7.621 Whitepine Road Richmond, Virginia,23237 (804)143.9401, Fax (804) 271.6446 wwwaleastern.com Project: LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 8/25/2014 08:50:00 Date Received: 08/28/2014 00:00 Date Reported: 09/03/2014 Total Solids * 2.73 27300 100.0 JM 08/28/2014 14:30 SM-2540G Moisture * 97.27 100.0 JM 08/28/2014 14:30 SM-2540G Total Kjeldahl Nitrogen 4.29 42900 10.0 JM 08/29/2014 08:19 SM-4500-NH3C-TKN Total Phosphorus 1.92 19200 100 KM 08/29/2014 11:49 SW 6010C Total Potassium 0.28 2830 100 KM 08/29/2014 11:49 SW 6010C Total Sulfur 0.86 8640 100 KM 08/29/2014 11:49 SW 6010C' Total Calcium 2.30 23000 100 KM 08/29/2014 11:49 SW 6010C Total Magnesium 0.31 3080 100 KM 08/29/2014 11:49 SW 6010C Total Sodium 1.03 10300 100 KM 08/29/2014 11:49 SW 6010C Total Iron 19400 100 KM 08/29/2014 11:49 SW 6010C Total Aluminum 28000 100 KM 08/29/2014 11:49 SW 6010C Total Manganese 252 5 KM 08/29/2014 11:49 SW 6010C Total Copper 372 5 KM 08/29/2014 11:49 SW 6010C Total Zinc 386 5 KM 08/29/2014 11:49 SW 6010C Ammonia Nitrogen 0.18 1830 10.0 JM 08/29/2014 08:19 SM-4500-NH3C Organic N 4.11 41070 10.0 08/29/2014 08:19 CALCULATION Nitrate+Nitrite-N 114 2.00 JM 09/02/2014 08:15 SM-450ONO3F Total Cadmium <2.0 2.0 KM 08/29/2014 11:49 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. % Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Page: 2 of 2 Report Number: 14-240-0202 Account Number: 46525 Submitted By: MARSHALL PURYEAR Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE , NC 27028 Lab Number: 57265 Sample Id: LUMBERTON WWTP �L A&L Eastern- Laboratories, Inca 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-8446 wwwaleastem.com Project: LUMBERTON WWTP NC CERT#257 REPORT OF ANALYSIS Date Sampled: 8/25/2014 08:50:00 Date Received: 08/28/2014 00:00 Date Reported: 09/03/2014 Total Chromium 331 5 KM 08/29/2014 11:49 SW 6010C Total Nickel 58 5 KM 08/29/2014 11:49 SW 6010C Total Lead 26 5 KM 08/29/2014 11:49 SW 6010C Total Arsenic 6.0 3.0 KM 08/29/2014 11:49 SW 6010C Total Mercury 0.4 0.4 KM 08/29/2014 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 08/29/2014 11:49 SW 6010C pH (Standard Units) * 7.44 2.00 JM 08/29/2014 09:00 SW-9045D Total Molybdenum 6 5 KM 08/29/2014 11:49 . SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Ca", "P", AND "S". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2101-01-AEDLIQ-NC LUMBERTON, NC WWTP AEROB. DIGESTED 8/25/2014 1011/2014-12131/2014 2.7900 LIQUID Na mg/I = (Na mg/kg x % Solids) + 100 = (10300 x 2.7300) + 100 = 281.19 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (23000 x 2.7300) + 100 = 627.9 Mg mg/I = (mg mg/kg x % Solids) + 100 = (3080 x 2.7300) + 100 = 84.084 Na meq = Na mg/I + Molec.Wgt.Na = 281.19 + 23 = 12.2257 Ca meq = Ca mg/I + Molec.Wgt.Ca = 627.9 + 20 = 31.395 Mg meq = Mg mg/I + Molec.Wgt.Mg = 84.084 + 12 = 7.007 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 12.2257 + SgrRoot[0.5(31.395+7.007)] = 2.79004 Printed: 1/28/2015 Page 1 11:31 E C FACILITY NAME: LUMBERTON, NC OWNER: THOMAS MAYNOR SITE #: NC RO 00016 FIELD# : RO 00016 0020 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: WAGRAM PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 54.77 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 8.60 ACRES PERMITTED: 8.60 Page: 1 Lune Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (pp-) Crop MONTH Total Per Acre Solids 3/13/14 254,200.00 (G) 29558.140 3.21 3.957 LUAEDL MOIST 0-<I/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 I BERMUDAGRASS, COASTAL - HAY 3/14/14 155,000.00 (G) 18023.256 3.21 2.413 LUAEDL MOIST 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 1 BERMUDAGRASS, COASTAL - HAY Mar-14 1 409,200.00 (G) 47,581.396 Total Gallons/Ac: 47,581.40 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.051 0.025 3.567 3.681 0.217 0.009 0.064 0.420 0.064 6.828 233.11 242 Cumulative lbs/acre 0.194 0.059 6.429 11.244 0.810 0.026 0.248 1.345 0.152 20.987 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 3$75.0 89.0 2500.0 LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID XS- (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 r�] ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: WAGRAM OWNER: THOMAS MAYNOR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 39.84 SITE #: NC RO 00016 FIELD# : RO 00016 0021 OPERATOR: OZELL BAKER CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 25.00 ACRES PERMITTED: 25.00 Page Lune Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/12/14 130,200.00 (G) 5208.000 3.21 0.697 LUAEDL MOIST 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 I BERMUDAGRASS, COASTAL - HAY 3/14/14 105,400.00 (G) 4216.000 3.21 0.564 LUAEDL MOIST 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 I BERMUDAGRASS, COASTAL - HAY 3/15/14 62,000.00 (G) 2480.000 3.21 0.332 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 BERMUDAGRASS, COASTAL - HAY Mar-14 1 297,600.00 (G) 11,904.000 Total Gallons/Ac: 11,904.00 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.013 0.006 0.892 0.921 0.054 0.002 0.016 0.105 0.016 1.708 58.32 61 Cumulative lbs/acre 0.164 0.048 4.493 9.932 0.698 0.018 0.209 1.104 0.127 18.045 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop` �r t i 264 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 =P ` ' 1339.0 267.9 15.0 + 375.0 89.0 2500.0777" LUAEDL = LUMBERTON, NC W WTP AEROB. DIGESTED LIQUID X (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or m&g * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: JOHNS OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 138.79 SITE #: NC RO 00017 FIELD# : RO 00017 0001 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 36.40 ACRES PERMITTED: 36.40 Page Lime Applied x.s Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/23/14 124,000.00 (G) 3406.593 3.89 0.553 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 SOYBEANS Jun-14 124,000.00 (G) 3,406.593 7/2/14 136,400.00 (G) 3747.253 3.89 0.608 LULSL WET 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 7/14/14 210,800.00 (G) 5791.209 3.89 0.939 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 7/15/14 186,000.00 (G) 5109.890 3.89 0.829 LULSL WET 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 7/17/14 198,400.00 (G) 5450.549 3.89 0.884 LULSL MOIST 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 SOYBEANS Jul-14 731,600.00 (G) 20,098.901 Total Gallons/Ac: 23,505.49 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: ' Annual lbs/acre 119 0.023 0.015 1.624 1.731 0.092 0.005 0.038 0.191 0.038 3.210 118.96 Cumulative lbs/acre 0.090 1 0.040 1 5.745 1 11.175 . 1.870 1 0.020 0.624 1 1.052 0.078 8.745 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 147 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LULSL = LUMBERTON, NC WWTP LIME STABILIZED LIQUID x 0200Z / (SIGNATURE OF LAND APPLIER) 'DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: LUMBEE OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 65.56 SITE #: NC RO 00017 FIELD# : RO 00017 0002 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 25.40 ACRES PERMITTED: 25.40 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (WT) (specify) oho Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 4/2/14 279,000.00 (G) 10984.252 3.21 1.470 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 1 54,200. p 5,610.00 p 1,640.00 p 19022 I SOYBEANS 4/3/14 210,800.00 (G) 8299.213 3.21 1.111 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19122 1 SOYBEANS Apr-14 489,800.00 (G) 19,283.465 Total Gallons/Ac: 19,283.46 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: 98 Annual lbs/acre 0.021 0.010 1.445 1.492 0.088 0.004 0.026 0.170 0.026 2.767 94.47 Cumulative lbs/acre 0.077 1 0.034 4.266 13.123 1 1.342 0.025 0.285 1.355 0.071 9.952 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 174 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID X JPDZ o2 (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate : Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: LUMBEE OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 30.71 SITE #: NC RO 00017 FIELD# : RO 00017 0003 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 28.00 ACRES PERMITTED: 28.00 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (VM (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 4/3/14 80,600.00 '(G) 2878.571 3.21 0.385 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 SOYBEANS 4/4/14 148,800.00 (G) 5314.286 3.21 0.711 LUAEDL DRY 0-<I/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 SOYBEANS Apr-14 1 229,400.00 (G) 8,192.857 Total Gallons/Ac: 8,192.86 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.009 0.004 0.614 0.634 0.037 0.002 0.011 0.072 0.011 1.176 40.14 42 Cumulative lbs/acre 0.009 0.004 1 0.614 0.634 1 0.037 0.002 0.011 1 0.072 0.011 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 174 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 .Y LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID X I s . (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, lnjection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: JOHNS OWNER: CITY OF LUMBERTON (AIRPOR PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 182.04 SITE #: NC RO 00017 FIELD# : RO 00017 0004 OPERATOR: DELOIS ALLEN CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 47.70 ACRES PERMITTED: 47.70 Page Lime Applied *** Date Lbs/Ac allons (G) or Cubic Yards (CY) Dry Site Inches Appli- Vola- Miner - or Wet Tons (VM (specify) % Tons Cond. Precip. cation tili- ali- Ammonia Nitrate PAN DATE or Per Residual Dry, Wet, Past 24 Method zation zation TKN Nitrogen and (ppm) Crop MONTH Total Per Acre Solids 6/26/14 285,200.00 (G) 5979.036 3,89 0.970 LULSL WET 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 6/27/14 124,000.00 (G) 2599.581 3.89 0.422 LULSL WET -1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 SOYBEANS 6/30/14 310,000.00 (G) 6498.952 3,89 1.054 LULSL WET 0-<I/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 SOYBEANS Jun-14 1 719,200.00 (G) 15,077.569 7/1/14 285,200.00 (G) 5979.036 3.89 0.970 LULSL WET 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 7/2/14 37,200.00 (G) 779.874 3,89 0.127 LULSL WET 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I SOYBEANS 7/14/14 80,600.00 (G) 1689.727 3.89 0.274 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 11140 SOYBEANS Jul-14 403,000.00 (G) 8,448.637 Total Gallons/Ac: 23,526.21 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 119 0.023 0.015 1.626 1.733 0.092 0.005 0.038 0.191 0.038 3.213 119.07 Cumulative lbs/acre 0.157 0.073 7.956 28.421 1.750 0.017 0.461 1.698 0.108 16.430 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 147 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6• 34.8 f L_ 1339.0 267.9 15.0 375.0 89.0 2500.0 LULSL = LUMBERTON, NC WWTP LIME STABILIZED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mgAcg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: LUMBERTON, NC OWNER: R G HAMMONDS SITE #: NC RO 00020 FIELD# : RO 00020 0003 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: WAKULLA PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 85.49 OPERATOR: R G HAMMONDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 26.10 ACRES PERMITTED: 26.10 Page Lime Appfied *** Date Lbs�Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/8/14 229,400.00 (G) 8789.272 3.89 1.426 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I BERMUDAGRASS 5/9/14 217,000.00 (G) 8314.176 3.89 1.349 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I BERMUDAGRASS 5/19/14 80,600.00 (G) 3088.123 3.89 0.501 LULSL MOIST 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15140 BERMUDAGRASS May-14 527,000.00 (G) 20,191.571 Total Gallons/Ac: 20,191.57 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN • TOTALS: Annual lbs/acre 102 0.020 0.013 1395 1.487 0.079 0.005 0.033 0.164 0.033 2.758 102.19 Cumulative lbs/acre 0.145 0.061 4.542 9.962 0.694 0.026 0.201 1.093 0.127 17.007:;;�',,f Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 147 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 Lr 1339.0 267.9 15.0 375.0 89.0 2500.0 LULSL = LUMBERTON, NC WWTP LIME STABILIZED LIQUID X o.21 ez/ rS (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: LUMBERTON, NC OWNER: R G HAMMONDS SITE #: NC RO 00020 FIELD# : RO 00020 0004 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: WAKULLA PERMIT #: WQ0000672 ANNUAL DRY TONS APPLIED: 79.67 OPERATOR: R G HAMMONDS CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 33.40 ACRES PERMITTED: 33.40 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) % Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 3/15/14 99,200.00 (G) 2970.060 3.21 0.398 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 I BERMUDAGRASS, COASTAL - HAY 3/20/14 285,200.00 (G) 8538.922 3.21 1.143 LUAEDL MOIST 0-<1/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 I BERMUDAGRASS, COASTAL - HAY 3/21/14 210,800.00 (G) 6311.377 3.21 0.845 LUAEDL MOIST 0-<I/2" SUR 0.5 0.30 54,200. p 5,610.00 p 1,640.00 p 19022 BERMUDAGRASS, COASTAL - HAY Mar-14 595,200.00 (G) 17,820.359 Total Gallons/Ac: 17,820.36 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 91 0.019 0.010 1.336 1.379 0.081 0.003 0.024 0.157 0.024 2.557 87.30 Cumulative Ibs/acre 0.237 0.076 6.170 14.369 1.061 0.037 0.305 1.668 0.170 25.495 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 196 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID X ®�r9Ji �Jl (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 ANNUAL LAND APPLICATION FIELD SUMMARY FORM FACILITY NAME: LUMBERTON, NC PREDOMINANT SOIL SERIES: RAINS OWNER: ROBERT BASKERVILLE, JR PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 160.93 SITE #: NC RO 00028 FIELD# : RO 00028 0002 OPERATOR: CARNELL LOCKLEAR CATION EXCHANGE CAPACITY (NON-503): RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 56.90 ACRES PERMITTED: 56.90 Page Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppnl) Crop MONTH Total Per Acre Solids 10/14/14 310,000.00 (G) 5448.155 2.73 0.620 LUAEDL DRY 0-<I/2" SUR 0.5 0.30 42,900. p 1,830.00 p 114.00 p 13350 I WHEAT 10/17/14 303,800.00 (G) 5339.192 2.73 0.608 LUAEDL MOIST 0-<1/2" SUR 0.5 0.30 42,900. p 1,830.00 p 114.00 p 13350 I WHEAT 10/20/14 303,800.00 (G) 5339.192 2.73 0.608 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 42,900. p 1,830.00 p 114.00 p 13350 I WHEAT 10/21/14 334,800.00 (G) 5884.007 2.73 0.670 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 42,900. p 1,830.00 p 114.00 p 13350 I WHEAT 10/22/14 161,200.00 (G) 2833.040 2.73 0.323 LUAEDL DRY 0-<1/2" SUR 0.5 0.30 42,900. p 1,830.00 p 114.00 p 13310 WHEAT Oct-14 1,413,600.00 (G) 1 24,843.586 Total Gallons/Ac: 24,843.59 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN TOTALS: Annual lbs/acre 0.034 0.011 1.872 2.104 0.147 0.002 0.034 0.328 0.028 2.178 108.60 76 Cumulative lbs/acre 0.034 0.011 1 1.872 2.104 1 0.147 1 0.002 0.034 1 0.328 0.028 17 2.178 °" Ng "" Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop106 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LUAEDL = LUMBERTON, NC WWTP AEROB. DIGESTED LIQUID (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg * * Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 FACILITY NAME: LUMBERTON, NC OWNER: PATRICK BULLARD SITE #: NC RO 00039 FIELD# : RO 00039 0009 RESIDUAL SOURCE(S):* See list at bottom of report ANNUAL LAND APPLICATION FIELD SUMMARY FORM PREDOMINANT SOIL SERIES: WAGRAM PERMIT #: W00000672 ANNUAL DRY TONS APPLIED: 120.69 OPERATOR: PATRICK BULLARD CATION EXCHANGE CAPACITY (NON-503): ACRES UTILIZED: 62.50 ACRES PERMITTED: 62.50 Page : 1 Lime Applied *** Date Lbs/Ac DATE or allons (G) or Cubic Yards (CY) or Wet Tons (WT) (specify) oho Dry Tons Per Residual Site Cond. Dry, Wet, Inches Precip. Past 24 Appli- cation Method Vola- tili- zation Miner - ali- zation TKN Ammonia Nitrogen Nitrate and PAN (ppm) Crop MONTH Total Per Acre Solids 5/12/14 142,600.00 (G) 2281.600 3.89 0.370 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 715540 I BERMUDAGRASS 5/13/14 155,000.00 (G) 2480.000 3.89 0.402 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I BERMUDAGRASS 5/14/14 260,400.00 (G) 4166.400 3.89 0.676 LULSL DRY 0-<1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15540 I BERMUDAGRASS 5/15/14 186,000.00 (G) 2976.000 3.89 0.483 LULSL WET >=1/2" SUR 0.5 0.30 47,800. p 5,910.00 p 18.00 p 15140 BERMUDAGRASS May-14 744,000.00 (G) 11,904.000 Total Gallons/Ac: 11,904.00 TOTALS: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN Annual lbs/acre 0.012 0.008 0.823 0.877 0.046 0.003 :Q;019 0.097 0.019 1.626 60.25 60 Cumulative lbs/acre 0.034 0.019 1.564 2.503 0.145 0.007 0.052 0.278 0.047 3.846 Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop 264 FD Cumulative Pollutant Loading Rate Limit (lbs/acre) 36.6 34.8 1339.0 267.9 15.0 375.0 89.0 2500.0 LULSL = LUMBERTON, NC WWTP LIME STABILIZED LIQUID x D2 OZ (SIGNATURE OF LAND APPLIER) DATE "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 * Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015 Summit Environmental Technologies, Inc. ,Mj`SUMMAIT 3310 Win St. t .°3hPIR0hlfa9! NY'J!L'T C##ldfiLt GltS, INC Cuyahoga Falls, Ohio 44223 ?�rt�l�%iI aP t'.ct"�fc7a'15" TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: hitp://wivw.settek.com January 30, 2014 Edward Stephens Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Lumberton, NC Dear Edward Stephens: Order No.: 14011402 Summit Enviromnental Technologies, Inc. received 1 sample(s) on 1/22/2014 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, N� Dr. Mo Osman Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky 90146, Louisiana 04061 and LAI2004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-11-5, Region 8 8TMS- L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT-81688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C and E87688, Wisconsin 399013010 Page 1 of 8 Summit Environmental Technologies, Inc. IT3310 Win St. Pd IIRC741Pt1E 11IiL 1"P HC3@[ tlG.cS; jt c, Cuyahoga Falls,'Ohio 44223 t°ni,�ta^�1 L9ka'px'i�l�a$� TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: http:/hvivw.settek.com CLIENT: Synagro Project: Lumberton, NC Lab SampleID Client Sample ID 14011402-001 Lumberton, NC WWTP Tag No Date Collected 1/17/2014 10:30:00 AM Workorder Sample Summary WO#: 14011402 31-Jan-14 Date Received Matrix 1/22/2014 9:50:00 AM Sludge Page 2 of 8 Su iniit Environmental Technologies, Inc. Case Narrative 3310 Win St. lv tPShcrtt3tJh7Eh7'PALt''cCHtdXad;G S,me, Cuyahoga Falls, Ohio44223 WO#: 14011402 +fit i$:tj+ i'1—sirs66'5 TEL: (330) 253-8211 FAX.- (330) 253-4489 Website: huy.-Iliviviv.settek.coin Date: 1/30/2014 CLIENT: Synagro Project: Lumberton, NC This report in its entirety consists of the documents listed below. All documents contain the Summit Environmental Technologies, Inc. Work Order Number assigned to this report. Paginated Report including: Cover Letter, Case Narrative, Analytical Results, Applicable Quality Control Summary Reports and copies of the Chain of Custody Documents supplied with this sample set. Concentrations reported with a J flag in the Qual field are values below the Limit of Quantitation (LOQ) but greater than the established Limit of Detection (LOD). There is greater uncertainty associated with these results and data should be considered as estimated. Method numbers, unless specified as SM (Standard Methods) or ASTM, are EPA methods. Estimated uncertainty values are available upon request. Any comments or problems with the analytical events associated with this report are noted below. Revision v1 Page 3 of 8 Summit Environmental Technologies, Inc. 3310 Win St. WO#: 14011402 t �I:QkiE#�TS1L�13C�L�tGj Bf Cuyahoga Falls, Ohio44223 T Date Reported: 1/30/2014 ,'Fr rt'rraj,j'tt±tiKrlr�t r TEL: (330) 253-8211 FAX: (330) 253-4489 Company: Synagro Website: http://Wwiv.settekcom Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Lumberton, NC TCLP Metals Analysis (6010) Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton, NC 001 1/17/2014 TCLP Arsenic(As) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Barium(Ba) 5.0 ND mg/L Sludge EPA 6010 C 1 100 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Cadmium(Cd) 0.10 ND mg/L Sludge EPA 6010 C 1 1.0 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Chromium(Cr) 0.20 ND mg/L Sludge EPA 6010 C 1 5.0 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Lead(Pb) 0.50 ND mg/L Sludge EPA 6010 C 1 5.0 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Selenium(Se) 0.50 ND mg/L Sludge EPA 6010 C 1 1.0 1/27/2014 WK WWTP Lumberton, NC 001 1/17/2014 TCLP Silver(Ag) 0.50 ND mg/L Sludge EPA 6010 G 1 5.0 1/27/2014 WK WWTP TCLP Mercury Analysis (1311/7470) Client ID# Lab IN Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run , Analyst Lumberton, NC 001 1/17/2014 TCLP Mercury 0.0020 ND mg/L Sludge EPA 7470 A 1 0.20 1/27/2014 ALJ WWTP SVOC SW-846: 8081-TCLP Pesticides Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton, NC 001 1/17/2014 Chlordane, total 0.010 ND mg/L Sludge EPA 8081 B 1 0.030 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 Toxaphene 0.10 ND mg/L Sludge EPA 8081 B 1 0.50 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 Endrin 0.0020 ND *mg/L Sludge EPA 8081 B 1 0.020 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 gamma-BHC 0.0020 ND mg/L Sludge EPA 8081 B 1 0.40 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 Heptachlor 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 Heptachlor epoxide 0.0020 ND mg/L Sludge EPA 8081 B 1 0.0080 1/27/2014 JBN WWTP Lumberton, NC 001 1/17/2014 Methoxychlor 0.0020 ND mg/L Sludge EPA 8081 B 1 10 1/27/2014 JBN WWTP Page 4 of 8 Summit Environmental Technologies, Inc. WO#: 14011402 l+ fb4�IRClN1e7UTgLr §iic9[7ti Ott"C 3310 Win St. Cuyahoga Falls, Ohio 44223 Date Reported: 1/30/2014 -r�rlglrsa IE�araleirds TEL: (330) 253-8211 FAX.- (330) 253-4489 Company: Synagro Website: htta:/fiviviv.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Lumberton, NC VOC by GC/MS (8260)-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton, NC 001 1/17/2014 1,1-Dichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 1,2-Dichloroethane 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Benzene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Carbon tetrachloride 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Chlorobenzene 0.10 ND mg/L Sludge EPA 8260 B 1 100 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Chloroform 0.10 ND mg/L Sludge EPA 8260 B 1 6.0 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Tetrachloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.70 1/27/2014 MES WWTP Lumberton, NC 001 1/17/2014 Trichloroethene 0.10 ND mg/L Sludge EPA 8260 B 1 0.50 1/27/2014 MES '"/WTP umberton, NC 001 1/17/2014 Vinyl chloride 0.20 ND mg/L Sludge EPA 8260 B 1 0.20 1/27/2014 MES JWTP Lumberton, NC 001 1/17/2014 MEK 2.0 ND mg/L Sludge EPA 8260 B 1 200 1/27/2014 MES WWTP SVOC 8270 TCLP BNA List Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLvl Run Analyst Lumberton, NC 001 1/17/2014 1,4-Dichlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 7.5 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 2,4,5-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 400 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 2,4,6-Trichlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 2.0 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 2,4-Dinitrotoluene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Cresols, Total 5.0 ND mg/L Sludge EPA 8270 C 1 200 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Hexachloro-1,3- 0.10 ND mg/L Sludge EPA 8270 C 1 0.50 1/29/2014 AKE WWTP butadiene Lumberton, NC 001 1/17/2014 Hexachlorobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 0.13 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Hexachloroethane 0.10 ND mg/L Sludge EPA 8270 C 1 3.0 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Nitrobenzene 0.10 ND mg/L Sludge EPA 8270 C 1 2.0 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Pentachlorophenol 0.25 ND mg/L Sludge EPA 8270 C 1 100 1/29/2014 AKE WWTP Lumberton, NC 001 1/17/2014 Pyridine 0.25 ND mg/L Sludge EPA 8270 C 1 5.0 1/29/2014 AKE VWTP Page 5 of 8 Summit Environmental Technologies, Inc. st-WAam.17 3310 Win St. 1-HVlftCiNMENTAL IECHNOL.OGJ:-:SrInc Cigahoga Falls, Ohio 44223 Anaryfrcaf Life raw es TEL: (330) 253-8211 FAX. • (330) 253-4489 Website: htto:/hviviv.settek.com WO#: 14011402 Date Reported: 1/30/2014 Company: Synagro Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Lumberton, NC SVOC SW-846: 8321 Herbicides-TCLP Client ID# Lab ID# Collected Analyte Rep Lmt Result Units Matrix Method DF RegLA Run Analyst Lumberton, NC 001 1/17/2014 2,4-D 5.0 ND mg/L Sludge EPA 8321 A 1 10 1/29/2014 AMZ WWTP Lumberton, NC 001 1/17/2014 2,4,5-TP 0.50 ND mg/L Sludge EPA 8321 A 1 1.0 1/29/2014 AMZ WWTP Page 6 of 8 Sun:n:it Environmental Technologies, Inc. WO#: 14011402 3310 Win St. Ft14Vl,RONfitEN'rALTEC9it`�OLad1 �,5Pto Cuyahoga Falls, Ohio44223 Date Reported: 1/30/2014 - 4naf}:kcal f_aC4xair�ric s TEL: (330) 253-8211 FAX. • (330) 253-4489 Company: Synagro Wehsite: hito:/hviviv.settek.com Address: 284 Boger Rd. Mocksville NC 27028 Received: 1/22/2014 Project#: Lumberton, NC Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst Lumberton, NC 001 1/17/2014 Flashpoint (140°F) >140 T Sludge EPA 1010 1 1/24/2014 TAH WWTP Lumberton, NC 001 1/17/2014 Cyanide, Reactive WWTP Lumberton, NC 001 _ 1/17/2014 pH WWTP Lumberton, NC 001 1/17/2014 Sulfide, Reactive WWTP ND ppm Sludge EPA 9014 1 0.50 1/23/2014 TIR 5.9 s.u. Sludge EPA 9045 D 1 1/22/2014 AYS ND ppm Sludge EPA 9034 1 25 1/23/2014 TIR Page 7 of 8 0 0 10 CD 00 0 h 00 3ii aujt.nvironinentat jeennowgies, Inc. -is- Request/Cha.�n. of Custody iA. S 33 10, Win Street, Y F' r.SurilmitEm;iron ert 1*,IAchnol gies, Ina USe,0111N' RI' Cuvalioga.-Falls, Ohio 44223 Tel:,313025182.11 Rm.: 330,253.4489Pace J cif fspr No. ,coinpanyxamc` (Please Print) -Project Name Analytical Paramter-2ild NICHIO.dS Co pauy�Addcass J ProjecL-Address- �v I Client-Pfione,No., Report to' Client Fax No; Pease I ax Results_E1 Po# fl CkierLt Inail- vjmj Ll_-� m 1 a JResults Quota No. V1.4 Sampled by Qhe�4 if -Ohio -NAP samples �f' 13 2 M w Z. N. n R '; Date §ample Identific-Aen C 0116cleD # d FC,111,ctdj 0 Time Lusted Bv: Mum b-. iipp"OYC Stj Rush: Requested - bylab jwat'%qr Date _NN!hitc,-,md yzllow FUD!s, shbuld DcCbulplwy sarliolcq' [.0 MeAa�pmkary"Tile diellE ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: WQ0000672 WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571 s Monitoring Period: From 01/01/14 To 03/31/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlienhle to alternative nerfarmed Wlasc Aar C ass RI cam Mete the fallowinu manitarinu data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6h MPN MPN/g Coliform power per gram of total solids CFU 28800 31100 33700 CFU/g 0 quarterly grab 9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt.3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jim Walters. Director of EUS Dent. Preparer Name and Title (type or print) , .2- - q, :)Lo IJ' ignature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Cameron Tdsting Services; Inc. Laboratory Report: NC DENR -8654 NC PHHS -4137799 US F-PA;WG01915 roj Synagro . CTS 140054 Lumberton Q1 REigula.tory Yes &nmple. Information Sampled E. Stephens Datil 01117/14 C. Cameron DA6 OM7114 Analyses and Results `Lab, ID Sarhple ID E, E A a3qW, Result 'E 14 w Std. MRHW� 140054 01 8:1dg1 Gt Fee, Coliform-S 28800 ul.lkj 2a5:0 D1117114 DPK 9222D - MF <33700 CF U19 337oa D.111 7114 DPK <30400 CPLJ/9 30-100 01117114 DPK d <3 1 500 UUto 315"-Id 01117114 EiPK <31 00() crurg 310zo 0 11"17114 DPK f <33000 CFLI.*,3 3200D 01117114 DPK 9 <29600 vrw :?mw 01117114 DPK Geomean <31100 140054 01 a siudg- or Ts No) 2.96% 'A 0-01 01117114 DPK 2540 G -T$ b 2.88% :/, 0.1)1 OW7114 DPK 0 2.93% A -1) DI 01117A4 DPK d 01117114 DPK 2.93% h 0.01 0 J'fl 7)Ig 4 DPK f 2,97% ss o.6i 01/17114 DPK 9 2.98% h. imm 01/1M4 DPK Date Review Lab Technician ate Rep Oft Review Lab Director Date 219 S. Sicelc SLr, -51 N9-208-4240 Cil 9TUIlIeS till R. C0111 Sanford NC 27330 Report Sheet'. Pr6jied.t: 1'40054-01 3D DAY Pe.nchtop Te.st CTIS Prbi. C116n& "synagro iF_P,A,,625fR-92101­3,, Appendix,D) RegulaiOTT S drn p-j e�d Received Due Ref, Methods. Std. Meth.. 1 91h. ed- By, E. SWphens 13Y C. Cameron., 2540'G -TS Dhfe! 01'/,17)14 Date 0411,71,14 ba­6a. '020114 Is1s Anav-, 254.0 G=11S Type 'Q(ab. Matrix, -Sludge,, 8, VA A InA 140054. 01. 1.89% 7 , 0;7% 01-18-14 68.9% 01-27-14 'Opk, OM/a '6f—.5%- _02-10-14 -FVS11,(rn.b4 '6.1'41% 'P9s`-S,-<t5%l' -POK- bk_ii-J4 QPKl -,Sanford., NC 2733O CameeOn Tdstin- S" g, ervices, Inc. NO APMGbV,Cert. A54 NIC PkHS:Cert-* 377099.d&EPA NC01918 Chain, Of Custddy pggia 6f' :C40PAnk-*�' Synagrb­ E�Stp6hen§Cw Vn4�ro,66m, —T ;'Pse�Onl EdStephens '336-403-4324 284 964dr-Rd: . Mockw e, NC" 27028 j_ ------------- 4 t - -'In orma ow R evue t d Araatys�s:. E sa*lei ID E E� 0 rn i U) wz 5k 13 77777 _rc 'IMP ------ - 14 J ReqdiV-qdi Rush. %4mrk -wK req Wi-e prior .-approval. - Add ffjona I charges Will -a p Ply" ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: WQ0000672 WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571 Monitoring Period: From 04/01/14 To 06/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion it upwicauie to a[rernailve pertormett uass A or uass is com Jere the ionowing monitoring aara: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee= of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 ('Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jim Walters, Director of EUS Dept. Preparer Name and Title (type or print) k 0-�'rleJ1 ignature of Preparer* Date Land Applier Name and Title (if applicable) (type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) CASS P pH LOG SF4 Using a p.H Meter with Two -point Standardization an Automatic EET atron (ATC) Probe m C r1 Analysis Method: SW-846 Mothod 9040B, poi Electrometric Measurement u MOA]Ti-tIYEAR; �,� ! &?01V SAMPLiNGLOCATION: FACILRYILOCATFON� A��ur D��Un„her�on i,UAs�ie ao�-���7'` �e.�•�Y C ' %� L ,'---�� ✓ 3 J C C o CD Date Ri1e 'CiRae Sampler lfnitials Start PH Testing Analyst Initials Start PH Adjusted Mr.. pH! AdjiUsted 24-Hi pH�'l� Adasted mp Ec Start PH Tenip BC 2-Hr-p H*, Term EC.. Z4-E[r pH* art 2 Mrs 24 Hrs CD 3'S°1�i o1CCl. tit' �, 2 _. .®... A s ' � i � a�. r.. 0 3 1 UP 5 =4tt CYD .ell z - w w ' L C Equivalent pH value aiZaEC; Correction Factor (CF) = 0.03 pH units ( x Zempaca#ure measurement-25EC); EcPtiva(ent pH = A,Qeasured 114 0--the CF. CID If the reading Is not done 24 hours after the Start Time, note (he time {arid date if not pertorrned the day €allowing the inifial sample date} the reading was taken_ i o Comments: CLASS SlPSRP pH LOG sFIEIE'r hi Ni Using a phi TWD-Point ftndardixafion and A�rtormfic Temperature d 'i o MONTHMM� May 201 q Compgresation .4mlys-es Methcda SW-846 lVleffiod 90408, p(j EleciYcunetric Mea��rererent (ATC) probe o SAMPIINd €-QCATioN. FACILIT'YILDCATIML- �-� a tt ,f 0o Kc1. -- -- -�- N O - - CD PH Testing- ple Sampler Tea ¢ ��� kittals Time s%P!.i1 Adjusted 2-Hrr. T� EC S pf°I! 5AdjusEted=MpE"��j�sted tart Analyst Initials 214 . F TempEC 21$ PH* Settfirs HIM .y2.1 K Jul �2_� 1c. Lo co OD 00 00 o m z w w a � I I �T—rt—I— —1— 0 CIDLo �unhs °-. Ecla�ivalenf �H ��te at 2�correction Factor(G� 8.U3 pBC 'Tempecaf+.rrre measuiement • 25EC)• 0 If the -reading � net done 24 hogs alter thL. Start Time, Rote the tirno' (and date If not.parformed the day follvuring the niiial sample d��rth pH +/-the CF. - comments: - ) he r�aciing w tal��n_ 0� co 0 LO 0 0 0 cm 0 0 0 CL- Ln co m co r- co r- 0 M F— z LU F— LU LLI I — co I 0 LL. -t cm 0 MONTHNEAR: SAMPLINd LOCA-nom. Using a P IU�Ie�eY wttfl Tv�a-��ir�t CLASS BIPSRP PH L®� SHEET dardi,atiDrt and Airfornafm TempeiatUre Compensation (ATC� Analysis Method; SW-845 Metbod 9040B, pN �lectrurrretric ft�east�tert�ent Probe 6v? Lai I EquivalentpH VRJUle at25EC; CDrreDt n B uP C o `g if €fie �eeng nit done 24 fours avere Stan i«, �obe fhe film (ar1� date if not pe�e�yned fhe da folio ' -03 PH units x ( em eot pee measurement - 2 0win the ini -w pii _ Measured re di the C1=: comments. - Xg the initial sample date) the reading c8i1. cm 0 u MUNTHNOur Lc�o SAMPLING LOC,A tC N: 0 0 d- 0 0 CLASS BIPSRP pH LOG Sf{I;E-r Using a IH Meter with Two -pa hi Standardization and Autornift Tempetatute Compensa#io� (��C� probe 1 Analysis Method.- SW-846 Methad 9a40I3, pK Electrometria il<ieas�arement l FACE !L!9 Aii �,' Ir Date ete Sarnpfat Ad�sted $m Sfax Start Date o Wtials Time Temp Ec Start pw i Curn ~ � i 'Q:�t~ 3W1-��� a � to . � � �.._ . r. - . — - • - xM !!szia L0 co r~ cm r` 0 M PH Te.stfng 2-Hrr . H/ Adfusted Temp BC 2a1ir PW 12.0 2S. l2A Anafyst In#tials 24-HrpH,'! Adjusf,� 2 24 Temp EC 21"r PH* ft1j Mrs firs z W Q W a W CJ7 Q � O • Of LL L0 .` f aumn Equivalent pH vaI♦t$ at 2�EC; Carte-oti�rt Factor (CF) = 0.03 PH units x 1Bc 7e�perature rneast�remer<t - 25EC '� It the raiding !s not done 24 hours alfer the SYatt Time, nQle the time (and date If not peffOrrneri the daft follavAng thu�i�lfiat sample date hId ereading } tht OF. 0 Comments'. ) Was taken. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: WQ0000672 WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571 Monitoring Period:, From 07/01/14 To 09/30/14 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 31C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density Alt, (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization X Air Drying Composting Aerobic Digestion Anaerobic Digestion it appucavie to alternative periormeu t- ass A or uass it5p complete the ionowing monitoring data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10 to the 6` MPN MPN/g Coliform power per gram of total solids CFU CFU/g 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) (40-day bench) (30-day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) X (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jim Walters, Director of EUS Dept. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) S' ature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) m CLASS BJPSRP PH LOG SHEET o using a ItiH Meter with Two -Point Standardization and Rtttomafc Temperature Compensation (ATC) Probe Analysis Method: SW-846 Method 9040E, riff Electrnmetric Measurement o IONTHly : OUIV -J114 PACILITY1L®GARD14. CD AMPLIAIG LocATnGfVI.! - O 0 0 n O LO CO m r 0 m z w w I— w CO I O LL- LD m 0 V- Liz �I 0 cm 0 Data • Sample lame am 1 • am Samp[sr h1itials i i � KCk PH Tes#in� r S Start pW Adjusted 2-1°!rr PH/ Adlasted 24-HrpH101 Adjusted Time Temp BC Start PH* Tamp EC 2-Hr pH�' Temp EC 244tr pH® CA v.rn 2.OQ'�2�. 12..�3 a� Analyst Initials 2 24 Start Mrs Hrs 1CC L kcL nrr..�. t _. • _-' Equiwdlent pH value at 25Rc; Correction Factor (CF) = 0.03 DH unils Y (RG •iiamneb mil rro r.,a�r...... �. �a , . d_••,•,, „t ten = 1vLrasureu pri ff- the cF Irme fea n * no axe ours after The Start Time, note the timerk (adate •tf tt, '--;rfiorrned the dayfolfawing the initia[ sample date) thereading wa:- ;n. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Lumberton WQ Permit Number: WQ0000672 WWTP Name: City of Lumberton WWTP NPDES Number: NCO024571 91 Monitoring Period: From 10/01/14 To 12/31/14 • Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/13 (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion ii appncame to alternative periormea lass A or Giass is complete the jonowing monitoring aata: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2xl0 to the 6` MPN MPN/g Coliform power per gram of total solids CFU 25200 26800 29100 CFU/g 0 quarterly grab 9222D 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Mt.3 Option/Alt.4 (VS reduction) (40-day bench) (30-day bench) X (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14-Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying — Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Jim Walters, Director of EUS Dept. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable) (type or print) Suture of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) 0 El Cameron Testing SeMces, Inc. Laboratory Report 4,C7 Synagro Car RNj.?;-- e6--F P Lumberton %NWTP X—R b'd U I a t b rV, Sample information �7 - M. Puryear 08/25/14 Analyses and Results 141016 01 141016 01 a b C d e f 9 a b C d e f 9 NC DENR *654 NC PHHS #37799 US EPA#NC01918 141016 Yes S. Bullard 08/25114 R f < 3ludge Gr Fec. Coliform-S 29100 CFU/g 29100 08/26/14 DPK 9222D - MF 26900 Cruig 26900 25600 CFU/g 25600 -25200 CFU/g 25200 26100 CFulg 26100 26300 CFWg 26300 28400 cl-ulg 28400 Geornean 26800 Sludge Gr TS(%) 2.89% % 0.01 08126114 DPK 2540 G -TS 2.94% 0.01 2.92% % 0.01 2.91% % OV 2.88% % 0.01 2.89% % 0.01 2.85% 0.01 Data Review OCIF 0� /-(Ci Labtechnicianbate, Report Review C)5 La b Director Date 219 S, Steele Str. Sanford NC 27330 919-208-4240 chri-,@catnerotitestiiig.coni (9 30D Report Shdet Project Lumberton 30 Day Benchtop-Test CTS Proj. -Client: Synagro JEPA 6251111=921Q,13, Appendix D) Regulatory Sampled Received Due Ref. Methods Std. Meth. 19t'ed. "'WRO'!;.,I, "MIS By M.Puryear, By S. Bullard '2540 G- TS 'Date 'Requested Date'— 08/25114 08/25/14 Date 09/29114 Analysis 2540 G - VS Type Grab Matrix Sludge --q �0 64 f i0i, 00 t 1.99W 61.09/0 08126/14 1.00% 59.2% 69/02114 6014% 09109/14 FVSR (Vk) .13.7% 'Pass, < 150/6' 1 .78%. 73. 09/6 06/15M4 11.66% 57.5% 09/29114 Lab Director Date: Notes: 'Sample, started, at-TS :5 2%. Pagp-1 • • • 219S.-Steele Str.- 5anford, NC 27330 .oAM .Cameron Testing Services;* Inc. .Nd-VW /GW Cert. #654 NC:PHHS Ced #-3_7799.US EPA NC01918 C h ai nof'Custody Page'____ `i�a-.:�,. ottljy,„�µt Gr •"` u�eplfl,2?Y;4 o"I iy.�.- Y o �,��n � ` ' `: �,.' '� Sample Temp , �! x'G�Sttf ta'F { - p Phone• (� r '.. � ? , • °TJ `. . f` !I` "-(Vi. r7- r�i's�1, Pgnll,yry Tv' ACIti{[BSs,�Gjl)gt�3!e ,I �Nptes : �• y e.,' - _ _ �- Regulatory,,,,t ;Due : .: J-e.,4 , ` z4PO ctM';.6^'t�l�!�f IerCted4�'Narrie: Signature: t > _ dw�., u�',:�l��.a�Ar�!1{.L��1:q^:'c''t+P,,qsit•k �_�av�l. .�—,9r!"}�'t',a:^t Svc:�3a.0,..�:t.�.Y<11.-$y.Ris�31. S "," P ASppPt�.. ��eT{?� l- iiformatiun��� ur.; .G �,.� - 1'..v ,e,�,x.r��.. tra.^4, t :�., L..��`.y.. ,:��3d"Vt1�'ii.'i. '.T�:�Fri..e � o• �t.�k.'� «f a �n ,E,.7 �m! Ii �t s+Ytij ' fi ..ifd t e+p�. N - C'f'SkLab � �- i � O Occ m'CD 0 a �' Requested Analysis - FAG: cc 'yaiat,:,irii.,a;`«N 'Sample ID: '% �' to N c0 E J "N. O �- ,,:.= ' I ,�; ON A °, { V Preservatnres: (U)npresery H(C)I H2(S)04 = `,'z3`'x I t (Na)Thiosulfate Na(0)H (X)Othei; indicate r.»H i F-I -'--- .,..-v.,...vr..,,a.v; , a..p_ ., .. ,. > ` ��,., ,. ��... p'-;aZ,::,<-,.yw r"�., w 12 � ittS e �sx�cws-�q� .a,_....,, .,�� r. s. - ..} ,. a r, .� _,��*,. .. -,, i.J' -;s_ _ — '-- s.r! p y...; � ' c.f^l; ,. r- s<...< r ,, ..„:r': k�,�.5,... x 's Jl" :.:t-,! �}r,E« , ,, ., -z ',, „ 7; vs'°}, ,1 ,In.-a4 .a .,,�.. �.. #�.r u. S:.�;.�_'r�+ n"."4. . C�e��i�s ';',aa ntA,R ^3� .6t'y' _ der.., • - - '.� ' �3tk' •-4.t?+..�f� �.; �iV ;,¢. F'„:.�. , i ••`i,^(>' `) �7 ` /f 1 ` 1 Rush woik will, require prior approval. Additional charges -will apply Lumberton, NC WWTP Lime Log for 2014 Field Date Tested pH Lime Req in Tons Lime Applied RO-16-20 01/06/14 5.1 1.8 RO-16-21 01/06/14 5.2 1.3 RO-17-01 08/07/14 5.9 0.3 RO-17-02 06/16/14 7.1 0 N/A RO-17-03 06/16/14 5.8 0.5 RO-17-04 08/07/14 6.5 0 N/A RO-20-03 06/13/14 5.5 0.9 RO-20-04 12/22/14 5.5 1.5 RO-28-02 12/22/14 5.2 1.8 RO-39-09 12/22/14 6.3 0 N/A 11 r � L Page 1 of 2 Report Number: 15-005-0554 Account Number: 46525 RL wwwaleastem.com Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/05/2015 Date Of Analysis: 01/06/2015 A&L Eastern Laboratories 7621, Whitepine Rod Richmond, Virginia 23237 (804).743-9401 Fax (804) 271.644E Grower: THOMAS MAYNOR LUMBERTON SOIL ANALYSIS REPORT Date Of Report: 01/07/2015 Submitted By: CREIGHTON BROWN Farm ID: RO-16 Analytical Method(s): Mehlich 3 ' Organic Matter ` Phosphorus Potassium Magnesium: , Calcium Sodium pH Acidity. C:E;C Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Solt Buffer H: Field ID Number ° Rate /o' Ibs/A. ,ppm Rate ppm f2ate - , ppm 'Rate_ .ppm • Rate ppm Rate 'ppm Rate 'pH Index ' , meq/100g meq/1009 RP-16-20 23496 4.3 M" 128 33 VH 41 VL 60 L 558 L 16 VL 5.1 6.72 2.1 5.6 NC=282 NC=21 RP-16-21 23497 4.1 M 125 358 VH 63 L 1 49 L 538 M 15 VL 5.2 6.76 1.7 5.0 NC = 298 NC = 27 Percent'Base'Saturation Nitrate Sulfur "~Zinc Manganese _`' Iron Copper._, Boron -w Soluble Salts_..' Chloride Aluminum Sample ID Field K Ca Na N " NO3fV S, ' , Zn Mn Fe Cu B . SS ' - Cl Al ID _'Mg % % % ppm Rate ppm - -Rate ppm Rate ppm Rate ppm Rate _ppm Rate ,'ppm ' . Rate ms/cm Rate ppm Rate ppm . RP-16-20 26 H 16.8 VH 15 M 298 VH 4.7 VH 0.4 L 0.11 VL 1.9 8.9 49.8 1.2 37.2 NC=54 NC=420.0 NC=94 I NC=235.0 RP-16-21 M VH 16 M 290 VH 4.5 VH VL VL 2.7 8.2 53.8 1.3 34.2 �23 111.6 10.3 10.11 NC=48 NC=290.0 NC=100 NC=225.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. by: ppylia me Gswr Pauric McGroary Page 2 of 20 Report Number: 15-005-0554 T Account Number:46525L wwwaleastem:com Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 - 0 A&L Eastern Labora_ tones 7621 Whitepine.Road Richmond, Virginia 23237 (804).743-9401 Fax (804) 271.SW Grower: Submitted By: CREIGHTON BROWN THOMAS MAYNOR Farm ID: RO-16 LUMBERTON Date Received: 01/05/2015 Date Of Report: 01/07/2015 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron, Sample ID Intended Crop Yield Goal time N PA K20 . Mg,-, - S w Zn Mn Fe � Cu � �B " Field;ID _- Tons/A Ib/A Ib/A`_ - Ib/A.w Ib/A Ib/A Ib/A Ib/A , Ib/A Ib/A 161A - RP-16-20 Adjust pH to 6.0 0 1.13 20 2 0 RP-16-21 Adjust pH to 6.0 0 1.3 31 2 0 Comments: Sample(s) : RP-16-21 Crop: Adjust pH to 6.0 Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag,or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." � Q� me V / r� Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary NCDA&CS . _,.gnomic Division Phone: (919) 733-2655 Website: www. _;.gov/agronomi/ Report No. FY' _ ._ :'.001829 Predictive { f k 4 F Client: Delois/Pete Allen 688 Deep Branch Rd. Lumberton, NC 28360 Advisor: Creighton Brown Synagro Central 284 Boger Rd i3 't's p Soil Report • 'Y�i:L'Lt�� Mehlich-3 Extraction Sampled County: Robeson Mocksville, NC 27028 Sampled: 06/01/2014 Received: 07/30/2014 . Completed: 08/07/2014 Farm: Lumberton Links to Helpful Information Sample ID: R0171 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.3 0 30 110 0 0 10 0 0 0 Note: 3 2- 0 Test Results [units - WN in g/crrt3; CEC and Na in meq/100 cd; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 1.49 1.23 7.5 77 1.8 5.9 47 16 57 19 33 23 24 67 67 93 0.0 Sample ID: R0174 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Soybean 0.0 0 0 110 0 0 $pH 0 0 0 Note: 3 Note: 2- Test Results [units - WN in glcrrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 1.31 1.25 9.5 90 0.9 6.5 99 14 76 13 29 19 14 114 114 182 0.0 .v,'Nonh Carolina 1i51�cac�Tiu+s l'u�t� Coarl�iSSslcr@ Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Page 1 of 210 Report Number: 15-005-0559Is Account Number:46525 ALN tnil Send To: SYNAGRO CENTRAL LLC/LUMBERTOWN aleastern.com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 01/05/2016 Date Of Analysis: 01/06/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: CITY OF LUMBERTON AIRPORT LUMBERTON SOIL ANALYSIS REPORT Date Of Report: 01/07/2015 0 Submitted By: CREIGHTON BROWN Farm ID: RO-17 Analytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample 1D Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meq/100g meq/100g, RO-17-2 52 H 47 VL 44 VL 774 M 17 VL 23504 3.6 M 111 5.0 6.62 3.1 7.5 NC=43 NC=24 RO-17-3 26 L 31 VL VL 695 L 16 VL 23505 2.9 M 98 134 4.8 6.59 3.4 7.3 NC=22 NC=16 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS CI All Field ID ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm RO-17-2 15 L 2.9 M 3 VL 201 VH 1.1 M 0.2 VL 0.09 VL 1.6 4.9 51.6 1.0 40.9 NC=31 NC=72.5 NC=19 NC=55.0 RO-17-3 M M 2 VL VH 1.0 M 0.2 VL 0.08 VL 1.1 3.9 47.6 1.0 46.7 �24 12.3 �282 NC=50 NC=57.5 NC=13 NC=50.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a / soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: AaL Eastern Laboratories, Inc. (� C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 Report Number: 15-005-0559 A.&L- Eastem Laboratories Account Number:46525 1 i 7621.WhitepineRoad Richmond, Virgin ia23237 (804).74379401 Fax (804)271-6446-" wwwaleastemcom Send To: SYNAGRO CENTRAL LLC/LUMBERTON Grower: Submitted By: CREIGHTON BROWN Mary Brewer CITY OF LUMBERTON Farm ID: RO-17 284 BOGER RD AIRPORT MOCKSVILLE NC 27028 LUMBERTON Date Received: 01/05/2015 Date Of Report: 01/07/2015 SOIL FERTILITY RECOMMENDATIONS Nitrogen ' Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID IntendedCrop"� Yield Goal Lime Tons/A- N" �Pz05 K20 Mg S Zn � Mn_ . Fe Cu B'� Field ID Ib/A. IbIA Ib/A Ib/A " Ib/A Ib/A Ib/A Ib/A Ib/A 161A - RO-17-2 Adjust pH to 6.0 0 2.0 36 4 0 RO-17-3 Adjust pH to 6.0 0 2.2 46 4 0 Comments: Sample(s) : RO-17-3 Crop: Adjust pH to 6.0 Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the �« work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary NCDA&CSMrFonomic Division Phone: (919) 733-2655 Website: www.xwr.gov/agronomi/ Report No. FYMW037221 Predictive Client: R G (Ronald) Hammonds 1218 Hammond Rd Lumberton, NC 28358 Advisor: Creighton Brown Synagro Central 284 Boger Rd Mehlich-3 Soil Report Extraction Mocksville, NC 27028 Sampled County: Robeson Sampled: Received: 06/05/2014 Completed: 06/13/2014 Farm: Lumberton Links to Helpful Information Sample ID: R0203 Recommendations: Lime Nutrients (Iblacre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Bermuda hay/past., KA 0.9 180-220 0 140 0 0 0 0 0 0 Note: 12 2-Bermuda hay/past., K 0.0 180-220 0 140 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/crif; CEC and Na in meq/100 cO; NO3-N in mg/do]: Soil Class: Mineral HM% WIV CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 . Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N 0.81 1.37 10.3 80 2.0 5.5 459 40 66 12 62 112- 84 84 1184 1184 551 0.1 1 -00ah Carolina, kh3cco Trust FWLd CtW11WS'.1I011 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture Page 1 of 2 __ Report Number: 14-353-0659 A� Account Number: 46525 aleastern.com Send To: SYNAGRO CENTRAL LLC/LUMBERTOWN Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 nata Rnrmva& 17/1Q/9n14 Date OfAnalvsis: 12/22/2014 A&L Eastern Laboratories 7621. Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271.6446 Grower: RG HAMMONDS LUMBERTON . SOIL ANALYSIS REPORT Date Of Reooit: 12/22/2014 Submitted By: CREIGHTON BROWN Farm ID: RO-20 Ana!ytical Method(s): Mehlich 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate P H Index meq/100g meq/100g RO-20-4 16066 3.9 M 116 537 VH 57 L 121 M 968 M 22 VL 5.5 6.72 2.1 8.2 NC=447 NC=29 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NOaN S Zn Mn Fe Cu B SS CI AI Field ID % % - % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm RO-20-4 24 M 32.4 VH 20 M 293 VH 9.9 VH 0.5 L 0.14 VL 1.8 12.3 59.0 1.2 25.8 NC = 50 NC = 810.0 NC = 125 NC = 495.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: PO.". i e 60wr H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 r Report Number: 14-353-0659 p Y4 � v LIJ. Account Number: 46525 T Send To: SYNAGRO CENTRAL LLC/LUMBERTON wwwaleastern.com Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (904) 271.6446 Grower: Submitted By: CREIGHTON BROWN RG HAMMONDS Farm ID: RO-20 LUMBERTON Date Received: 12/19/2014 Date Of Report: 12/22/2014 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons/A lb/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A ib/A Ib/A Ib/A RO-20-4 Adjust pH to 6.0 0 1.5 0 2 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." MM Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of A Report Number: 14-353-0658 Account Number: 46525 wwwaleastemcom Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 12/19/2014 Date Of Analysis: 12/22/2014 A.&L. Eastern Laboratories 7621 Whitepine.Road Richmond, -Virginia 23237- (804) 743-9401 Fax (804) 271-ji446 Grower: Submitted By: CREIGHTON BROWN CARNELL LOCKLEAR Farm ID: RO-28 LUMBERTON SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 12/22/2014 Organic Matter " Phosphorus Potassium Magnesium Calcium_ Sodium pH Acidity C.E.0 Sample 6' Field ID. Lab Number % Rate . ENR - Mehl_ich 3 -Reserve- K 'Mg Ca Na Soil, Buffer H , Ibs/A ppm. Rate ppm _ Rate_ ppm Rate ppm Rate ;ppm. Ratea ppm Rate pH Index ,, meq/100g _meq%100g RO-28-2 196 VH 110 M 129 M 741 L 22 VL 16065 2.7 M 93 5.2 6.66 2.7 7.8 NC=163 NC=56 Percent Base Saturation Nitrate Sulfur Zinc Manganese "- - Iron Copper Boron Soluble"Salts Chloride Aluminum-, IDID ��_ -F a dple "_, K Mg Ca _n -� Na H NO3N S Zn Mm. Fe Cu _ B SS CI Al % % %- % °�a ppm Rate ;ppm Rate ppm Rate ppm Rate- ppm_ Rate ppmw- Rate ppm Rate ms/cm Rate -ppm Rate ppm RO-28-2 19 M 8.3 VH 17 M 184 VH 3.1 VH 0.4 L 0.19 VL 3.6 13.8 47.5 1.2 34.3 NC = 40 NC = 207.5 NC = 106 NC = 155.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. me H(High), VH (VeryHigh). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: m x 2 = Ibs/A, Soluble by: Pw« 0w g ( q p g ) pp Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Pauric McGroary Page 2 of 2 • go- wwwaleasterc-comReport Number: 14-353-0658 Account Number:46525 Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 A&L Eastern _Laboratories_ T621 Whitepine Road' Richmond, Virginia 23237 (804),743.9401 Fax (804),271-6446 Grower: Submitted By: CREIGHTON BROWN CARNELL LOCKLEAR Farm ID: RO-28 LUMBERTON Date Received: 12/19/2014 - Date Of Report: 12/22/2014 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Pot,ash Magnesium Sulfu_ r Zinc Mangane"se `Iron Copper Boron Sample ID Intended Crop Yield Goal Lime_ N P205 KZO Mg S ' Zn Mn Fe Cu B Field ID, - Tons/A Ib/A Ib/A - Ib/A Ib/A Ib/A Ib/A Ib/A , Ib/A Ib/A JbIA RO-28-2 Adjust pH to 6.0 0 1.8 0 2 0 Comments "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." {� M Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the work,the results, or the company in any advertising,news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of 2 • Report Number: 14-353-0657 RL Account Number:46525 www.aleastern.com Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 Date Received: 12/19/2014 Date Of Analysis: 12/2212014 .A&L Eastern Laboratories_ _ 7621 Whitepine.Road Richmond, Virginia 23237 (804).743.9401 Fax'(804)'27l-6446 Grower: Submitted By: CREIGHTON BROWN PATRICK BULLARD Farm ID: RO-39 LUMBERTON SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 12/22/2014 °ID Organic Matter Phosphorus Potassium, Magnesium Calcium Sodium pH. Acidity C.EC- _ Sample Field ID Lab Number % Rate ENR Mehlich 3 Reserve _ _ K Mg Ca Na Soil- Buffer H Ibs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm,. Rate ppm Rate pH Index meq/100g. meq/100g R039-9 194 VH 45 L 59 M 483 H 14 VL 16063 1.5 L 75 6.3 0.4 3.4 NC=162 1 NC=23 Percent Base Saturation . Nitrate Sulfur Zinc ,° Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample1D K Mg Ca Na, ,. H ^. NO3N., S Zn Mn Fe Cu. B SS Cl" Al Field ID %. % % %% ;,ppm Rate ppm Rate ppm Rate° ppm Rate .ppm Rate ppm Rate ;ppm Rate ms/cm Rate ppm' Rate ppm TM R039-9 12 L 8.2 VH 11 M 128 VH 3.0 H 0.2 VL 0.07 VL 3.4 14.5 71.0 1.8 10.7 NC=25 NC=205.0 NC=69 I I NC=150.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. ��` me �� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 2 0 Report Number: 14-353-0657 RL Account Number:46525 www.aleastem.com Send To: SYNAGRO CENTRAL LLC/LUMBERTON Mary Brewer 284 BOGER RD MOCKSVILLE NC 27028 A&L Eastern Laboratories 7621 Whitepine_Road Richmond, Virginia 23237 (804),743-9401 Fax (804) 27176446 Grower: Submitted By: CREIGHTON BROWN PATRICK BULLARD Farm ID: RO-39 LUMBERTON Date Received: 12/19/2014 Date Of Report: 12/22/2014 SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magriesium �_$ulfur - Zinc Manganese Iron Copper..Boronw, Sample ID Intended Crop Yield Goal Lime N P205 KZO Mg S Zn Mn Fe Cu B° Field'ID Tons/A lb/A- Ib/A Ib/A Ib/A IbIA Ib/A lb/A Ib/A Ib/A Ib/A R039-9 Adjust pH to 6.0 0 0.0 1 1 1 21 2 0 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." 9 Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 Gam« or Ile work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary