HomeMy WebLinkAboutWQ0000543_Residual Annual Report 2014_20150302CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2014 ANNUAL REPORT
City of Sanford, NC
Residuals Land Application Program
2014 Annual Report
TABLE OF CONTENTS
1. Certification Form, Annual Operations Summary, Facility and
Land Applier Contact Information
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH-& Lime Application Records
7. Soil Analyses
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00000543 County Carteret Year 2014
Facility Name (as shown on permit) City of Sanford WWTP NPDES No. NCO024147
Land Application Operator Synaero Phone# (336) 998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and PartB and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 58
Total number of fields utilized for land application during the year: 9
Total amount of dry tons applied during the year for all application sites: 364.47
Total number of acres utilized for land application during the year: 242.6
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting false information, includi g the possibility of fines and imprisonment for
knowing violations." . f f I
Hal Hegwer, Public City Manager
Permittee Name and Title (type or print)
AMUR
2015
Signature of Preparer* Date . Wignature of Lan7Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)
2014 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION
SANFORD, NC
SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
A37►��9aLo
MONTHNEAR
AMOUNT UNIT
DRY TONS
UNIT
TONS
April 2014
675,800.00
G
63.98
D
58.02
May 2014
1,531,400.00
G
144.96
D
131.46
July 2014
1,680,200:00
G
15553
D
141.07
YEARLY TOTAL
3,887,400.00
G
364.47
D
330.55
1 /31 /2015
2014 ANNUAL REPORT
PROJECT:
FACILITY:
NPDES PERMIT NUMBER:
RESPONSIBLE OFFICIAL:
FACILITY OPERATOR:
LAND APPLIER AND
PREPARER OF LAND
APPLICATION ANNUAL REPORT:
City of Sanford
Sanford, NC
Big Buffalo WWTP
5327 Iron Furance Road
Sanford, NC 27331
(919) 775-8305
NC0024147
Scott Siletzky, Superintendent
5324 Iron Furance Road
Sanford, NC 27331
(919) 775-8305
Scott Siletzky, Superintendent
5324 Iron Furance Road
Sanford, NC 27331
(919) 775-8305
Synagro Central, LLC
Contact: Marshall Puryear
(336) 998-7150 ext. 17
ANNUAL RESIDUALS SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000543 Laboratory
Facility Name: SANFORD, NC A&L Eastern Laboratories Inc.
NPDES# : NCO024147
or WQ# (residual only)
WWTP Name: BUFFALO CREEK WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Date Sampled (grab) or 01/20/14 04/22/14 07/10/14 10/09/14
Date Composited
Percent Solids 1.74 2.27 2.22 2.29
PARAMETERS (mg/kg dry weight)
Arsenic
6
6
5
6
Cadmium
2
2
2
2
Mercury
1.1
0.9
1.2
2.1
Chromium
221
224
174
227
Copper
643
591
562
648
Lead
40
31
32
34
Molybdenum
17
20
13
21
Nickel
80
76
73
83
Selenium
5
<5
6
5
Zinc
1080
896
800
975
Total Phosphorus
26900
25000
26800
25300
TKN
73000
79700
88700
76000
Ammonia -Nitrogen
37400
33500
45000
31400
Nitrate and Nitrite
402
79.3
72.1
175
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
X g �: L&L_� Date
(_SICNATURE OF PREPARER)
DENR FORM RSSF (5/2003) Printed: Saturday - January 31' 2015 at 10:48:17 for: 2039 01
ANNUAL RESIDUALS SAMPLING SUMMARY FGRM
Attach this form to the corresponding Annual Report.
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0000543 Laboratory
Facility Name: SANFORD, NC A&L Eastern Laboratories Inc.
NPDES# : NCO024147
or WQ# (residual only)
WWTP Name: BUFFALO CREEK WWTP
Residuals Analysis Data
Product Type AEDLIQ AEDLIQ AEDLIQ AEDLIQ
Date Sampled (grab) or, 01/20./14 04/22/14 07/10/14 10/09/14
Date Composited
Percent Solids 1.74 2.27 2.22 2.29
PARAMETERS (mg/kg dry weight)
Aluminum
21900
18900
20300
15600,
Calcium
19200
16800
17400
18300
Magnesium
4220
3520
3960
3350
pH
8.43
8.14
8.10
8.20
Potassium
5870
5900
6790
5380
Sodium
5220
5240
4820
5100
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
x o1W4T( L.
(SIGNATURE OF PREPAR
NR - Data Not Reported or Data Not Required
Date g a�--*%,5--
DENR FORM RSSF-B (7/2002) Printed: Saturday - January 31 2015 at 10:48:40 for: 2039 01
Page: 1 of 2
Report Number: 14-022-0205
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97592
Sample Id: SANFORD
29,
A&L 'Eastern Laboratories, Inc._7W Whitepine Road Richmond, Virginia 23237 (804) 743-9401' Fax (804) 271-6446
M
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/20/2014 13:00:00
Date Received: 01/22/2014 00:00
Date Reported: 01/27/2014
Total Solids *
1.74
17400
100.0
JM
01/22/2014 13:30
SM-2540G
Moisture *
98.26
100.0
JM
01/22/2014 13:30
SM-2540G
Total Kjeldahl Nitrogen
7.30
73000
10.0
JM
01/23/2014 07:39
SM-4500-NH3C-TKN
Total Phosphorus
2.69
26900
100
KM
01/23/2014 15:23
SW 6010C
Total Potassium
0.59
5870
100
KM
01/23/2014 15:23
SW 6010C
Total Sulfur
1.26
12600
100
KM
01/23/2014 15:23
SW 6010C
Total Calcium
1.92
19200
100
KM
01/23/2014 15:23
SW 6010C
Total Magnesium
0.42
4220
100
KM
01/23/2014 15:23
SW 6010C
Total Sodium
0.52
5220
100
KM
01/23/2014 15:23
SW 6010C
Total Iron
33000
100
KM
01/23/2014 15:23
SW 6010C
Total Aluminum
21900
100
KM
01/23/2014 15:23
SW 6010C
Total Manganese
1070
5
KM
01/23/2014 15:23
SW 6010C
Total Copper
643
5
KM
01/23/2014 15:23
SW 6010C
Total Zinc
1080
5
KM
01/23/2014 15:23
SW 6010C
Ammonia Nitrogen
3.74
37400
10.0
JM
01/23/2014 07:39
SM-4500-NH3C
Organic N
3.56
35600
10.0
01/23/2014 07:39
CALCULATION
Nitrate+Nitrite-N
1402
2.00
JM
01/23/2014 07:40
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
01/23/2014 15:23
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-022-0205
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 97592
Sample Id : SANFORD
A&L Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia.23237 (804) 743-9401 Fax (804) 271-6446
wwW,aleastern.com
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 1/20/2014 13:00:00
Date Received: 01/22/2014 00:00
Date Reported: 01/27/2014
Total Chromium
221
5
KM
01/23/2014 15:23
SW 6010C
Total Nickel
80
5
KM
01/23/2014 15:23
SW 6010C
Total Lead
40
5
KM
01/23/2014 15:23
SW 6010C
Total Arsenic
6.0
3.0
KM
01/23/2014 15:23
SW 6010C
Total Mercury
1.1
0.4
KM
01/23/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
01/23/2014 15:23
SW 6010C
pH (Standard Units) *
8.43
2.00
JM
01/23/2014 07:39
SW-9045D
Total Molybdenum
17
5
KM
01/23/2014 15:23
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Mg", "Na", AND "S". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
SAMPLING'LiOG
14-02-02as
-
lll11:1111iJili111l "122
22 a
1iUa71-OMER: `I'�lY�`SOUTH
EAST"-
SYNAGP.O.CENTRAL
LI CISAMFORD 12'36:49
-
-
rr
`SANFORD
-- -
ape xfeldsamppcedur
PROJECT MANAGER".
mrdLr:eo uinj
cotlecton-osamples.
4' _ J
3
=
- - SAMPLER'
-
-- _Ft
A & L, C1JS'f08ViEMPt,1NG
SA, -
-
SAMPLE '
# f3F SAtiPLtNG
METHODMETHOD
tAR4 ', SAMPRE�t.01
L®CATI
l` PE� -
CONTAAINERS L7A!E. `TlhKE =
PRESERVED. :&HIPPED
l
Relinquish6d by Sarrlpler,
hate Time
j
Recieyed=by: -
REMARKS;
j' Relinquished. by: - -- -
— ---
date Time
Recievt~d' by;
Relinquished by; afe Time Recieved by:
;SPECIAL tNS (RUCTION- S:
,, n _n
For = rrionitorirsg purposes. PO#:
ANALYSIS REQUEST '
SAMPLE','
N}14-IY
903' 1
Otg�nic
Cd
Q�
I Ni "
Pb'
As
H'g .
Se
--
PH
-
CaCtJ
equiv�
Volatile
,Soliids
Mo
Cl
NO2 iV
-51,1-
T-11-d
SLi: Total Solids (Moj$Wre)', Total. K: 0d�ahl Nitrogen; Phosphorus, and. Potasslu6 -
SI_2: Basic Test'SL1 plus�Sulfur, Calcium, Mag[nesium,, Sodium, Iron, Aluminum ^manganese, Copper and=zinc
While, - A & L -_Canary. - MAhIAGSR COPY
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 1/20/2014 11112014-3/31/2014 1.1690
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x % Solids) + 100 = (5220 x 1.7400) + 100 = 90.828
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (19200 x 1.7400) =100 = 334.08
Mg mg/I = (mg mg/kg x % Solids) = 100 = (4220 x 1.7400) _ 100 = 73.428
Na meq = Na mg/I = Molec.Wgt.Na = 90.828 = 23 = 3.94904
Ca meq = Ca mg/I -= Molec.Wgt.Ca = 334.08 + 20 = 16.704
Mg meq = Mg mg/I'= Molec.Wgt.Mg = 73.428 _ 12 = 6.119
SAR = Na meq -= SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.94904 = SgrRoot[0.5(16.704+6.119)] = 1.16902
Printed: 1 /31 /2015
Page 1 10:49
Page: 1 of 2
Report Number: 14-115-0204
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55030
Sample Id: SANFORD
�L A&L Eastern Laboratories, Inc..
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastern.com
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/22/2014 12:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Solids *
2.27
22700
100.0
JM
04/25/2014 14:30
SM-2540G
Moisture *
97.73
100.0
JM
04/25/2014 14:30
SM-2540G
Total Kjeldahl Nitrogen
7.97
79700
10.0
JM
04/28/2014 09:40
SM-4500-NH3C-TKN
Total Phosphorus
2.50
25000
100
KM
04/28/2014 13:09
SW 6010C
Total Potassium
0.59
5900
100
KM
04/28/2014 13:09
SW 6010C
Total Sulfur
1.18
11800
100
KM
04/28/2014 13:09
SW 6010C
Total Calcium
1.68
16800
100
KM
04/28/2014 13:09
SW 6010C
Total Magnesium
0.35
3520
100
KM
04/28/2014 13:09
SW 6010C
Total Sodium
0.52
5240
100
KM
04/28/2014 13:09
SW 6010C
Total Iron
26200
100
KM
04/28/2014 13:09
SW 6010C
Total Aluminum
18900
100
KM
04/28/2014 13:09
SW 6010C
Total Manganese
898
5
KM
04/28/2014 13:09
SW 6010C
Total Copper
591
5
KM
04/28/2014 13:09
SW 6010C
Total Zinc
896
5
KM
04/28/2014 13:09
SW 6010C
Ammonia Nitrogen
3.35
33500
10.0
JM
04/28/2014 09:40
SM-4500-NH3C
Organic N
4.62
46200
10.0
04/28/2014 09:40
CALCULATION
Nitrate+Nitrite-N
79.3
2.00
JM
04/28/2014 09:40
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
04/28/2014 13:09
SW 6010C
All values are on a dry weight basis lexcept as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-115-0204
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 55030
Sample Id : SANFORD
99,
A&L EasternLaboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
WWwaleastern.cotn
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 4/22/2014 12:00:00
Date Received: 04/25/2014 00:00
Date Reported: 04/30/2014
Total Chromium
224
5
KM
04/28/2014 13:09
SW 6010C
Total Nickel
76
5
KM
04/28/2014 13:09
SW 6010C
Total Lead
31
5
KM
04/28/2014 13:09
SW 6010C
Total Arsenic
0.0
3.0
KM
04/28/2014 13:09
SW 6010C
Total Mercury
0.9
0.4
KM
04/28/2014 09:00
SW-7471 B
Total Selenium
<5.0
5.0
KM
04/28/2014 13:09
SW 6010C
pH (Standard Units) *
8.14
2.00
JM
04/28/2014 09:40
SW-9045D
Total Molybdenum
20
5
KM
04/28/2014 13:09
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 4/22/2014 4/1/2014-6/30/2014 1.4420
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (5240 x 2.2700) _ 100 = 118.948
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (16800 x 2.2700) _ 100 = 381.36
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3520 x 2.2700) =100 = 79.904
Na meq = Na mg/I— Molec.Wgt.Na = 118.948 + 23 = 5.17165
Ca meq = Ca mg/I = Molec:Wgt.Ca = 381.36 = 20 = 19.068
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 79.904 _ 12 = 6.65867
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.17165 = SgrRoot[0.5(19.068+6.65867)] = 1.44196
Printed: 1 /31 /2015
Page 1 10:49
Page: i of 2
Report Number: 14-196-0203
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56469
Sample Id: SANFORD
�L A&L Eastern Laboratories, Inc.
7.621 Whitepine Road Richmond, Virginia,23237 (804) 743-9401 Fax (804) 271-6446
www.aleastern.com
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 7/10/2014 15:00:00
Date Received: 07/15/2014 00:00
Date Reported: 07/21/2014
Total Solids *
2.22
22200
100.0
BW
07/15/2014 15:00
SM-254OG
Moisture *
97.78
100.0
BW
07/15/2014 15:00
SM-2540G
Total Kjeldahl Nitrogen
8.87
88700
10.0
MW
07/16/2014 07:59
SM-4500-NH3C-TKN
Total Phosphorus
2.68
26800
100
BW
07/16/2014 09:30
SW 6010C
Total Potassium
0.68
6790
.100
BW
07/16/2014 09:30
SW 6010C
Total Sulfur
1.18
11800
100
BW
07/16/2014 09:30
SW 6010C
Total Calcium
1.74
17400
100
BW
07/16/2014 09:30
SW 6010C
Total Magnesium
0.40
3960
100
BW
07/16/2014 09:30
SW 6010C
Total Sodium
0.48
4820
100
BW
07/16/2014 09:30
SW 6010C
Total Iron
28000
100
BW
07/16/2014 09:30
SW 6010C
Total Aluminum
20300
100
BW
07/16/2014 09:30
SW 6010C
Total Manganese
639
5
BW
07/16/2014 09:30
SW 6010C
Total Copper
562
5
BW
07/16/2014 09:30
SW 6010C
Total Zinc
800
5
BW
07/16/2014 09:30
SW 6010C
Ammonia Nitrogen
4.50
45000
10.0
MW
07/16/2014 07:59
SM-4500-NH3C
Organic N
4.37
43700
10.0
07/16/2014 07:59
CALCULATION
Nitrate+Nitrite-N
72.1
2.00
MW
07/16/2014 08:00
SM-450ONO3F
Total Cadmium
2.0
2.0
BW
07/16/2014 09:30
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-196-0203
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 56469
Sample Id: SANFORD
@P.A&L EasternLaboratories, Inc._
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
wwwaleastern,com
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 7/10/2014 15:00:00
Date Received: 07/15/2014 00:00
Date Reported: 07/21/2014
Total Chromium
174
5
BW
07/16/2014 09:30
SW 6010C
Total Nickel
73
5
BW
07/16/2014 09:30
SW 6010C
Total Lead
32
5
BW
07/16/2014 09:30
SW 6010C
Total Arsenic
5.0
3.0
BW
07/16/2014 09:30
SW 6010C
Total Mercury
1.2
0.4
JM
07/16/2014 08:30
SW-7471 B
Total Selenium
6.0
5.0
BW
07/16/2014 09:30
SW 6010C
pH (Standard Units) *
8.10
2.00
MW
07/16/2014 09:04
SW-9045D
Total Volatile Solids
61.40 614000
100.0
BW
07/15/2014 15:00
SM-2540G
Total Molybdenum
13
5
BW
07/16/2014 09:30
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "AP' AND "Cr". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 7/10/2014 711/2014-9/30/2014 1.2747
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (4820 x 2.2200) _ 100 = 107.004
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (17400 x 2.2200) _ 100 = 386.28
Mg mg/I = (mg mg/kg x % Solids) _ 100 = (3960 x 2.2200) =100 = 87.912
Na meq = Na mg/I _ Molec.Wgt.Na = 107.004 _ 23 = 4.65235
Ca meq = Ca mg/1 _ Molec.Wgt.Ca = 386.28 _ 20 = 19.314
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 87.912 = 12 = 7.326
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.65235 + SgrRoot[0.5(19.314+7.326)] = 1.27474
Printed: 1 /31 /2015
Page 1 10:49
Page: 1 of 2
Report Number: 14-289-0205
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58186
Sample Id: SANFORD BASIN
' A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743.9401 Fax (804) 271-6446
wwwaleastemxonn
Project; SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/9/2014 09:30:00
Date Received: 10/16/2014 00:00
Date Reported: 10/23/2014
Total Solids `
2.29
22900
100.0
BW
10/16/2014 14:39
SM-2540G
Moisture *
97.71
100.0
BW
10/16/2014 14:39
SM-2540G
Total Kjeldahl Nitrogen
7.60
76000
10.0
JM
10/17/2014 09:20
SM-4500-NH3C-TKN
Total Phosphorus
2.53
25300
100
KM
10/20/2014 12:46
SW 6010C
Total Potassium
0.54
5380
100
KM
10/20/2014 12:46
SW 6010C
Total Sulfur
1.29
12900
100
KM
10/20/2014 12:46
SW 6010C
Total Calcium
1.83
18300
100
KM
10/20/2014 12:46
SW 6010C
Total Magnesium
0.34
3350
100
KM
10/20/2014 12:46
SW 6010C
Total Sodium
0.51
5100
100
KM
10/20/2014 12:46
SW 6010C
Total Iron
26600
100
KM
10/20/2014 12:46
SW 6010C
Total Aluminum
15600
100
KM
10/20/2014 12:46
SW 6010C
Total Manganese
791
5
KM
10/20/2014 12:46
SW 6010C
Total Copper
648
5
KM
10/20/2014 12:46
SW 6010C
Total Zinc
975
5
KM
10/20/2014 12:46
SW 6010C
Ammonia Nitrogen
3.14
31400
10.0
JM
10/17/2014 09:20
SM-4500-NH3C
Organic N
4.46
44600
10.0
10/17/2014 09:20
CALCULATION
Nitrate+Nitrite-N
175
2.00
JM
10/22/2014 08:20
SM-450ONO3F
Total Cadmium
2.0
2.0
KM
10/20/2014 12:46
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Page: 2 of 2
Report Number: 14-289-0205
Account Number: 46489
Submitted By: WILL VARNER
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 58186
Sample Id: SANFORD BASIN
Av� A&L Eastern Laboratories, Inc.
7621 Whltepine Road Richmond, Virginia 23237 (804)743-9401 Fax (804)271-6446
wwwaleastern.com
Project: SANFORD
NC CERT#257
REPORT OF ANALYSIS Date Sampled: 10/9/2014 09:30:00
Date Received: 10/16/2014 00:00
Date Reported: 10/23/2014
Total Chromium
227
5
KM
10/20/2014 12:46
SW 6010C
Total Nickel
83
5
KM
10/20/2014 12:46
SW 6010C
Total Lead
34
5
KM
10/20/2014 12:46
SW 6010C
Total Arsenic
6.0
3.0
KM
10/20/2014 12:46
SW 6010C
Total Mercury
2.1
0.4
KM
10/17/2014 09:00
SW-7471 B
Total Selenium
5.0
5.0
KM
10/20/2014 12:46
SW 6010C
pH (Standard Units) *
8.20
2.00
JM
10/17/2014 09:20
SW-9045D
Total Molybdenum
21
5
KM
10/20/2014 12:46
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
QUALIFIER: THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al", "Fe", "P", "Se", "S", "NH4-N". ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 10/9/2014 1011/2014-12/31/2014 1.3732
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (5100 x 2.2900) =100 = 116.79
Ca mg/I = (Ca mg/kg x % Solids) _ 100 = (18300 x 2.2900) _ 100 = 419.07
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3350 x 2.2900) =100 = 76.715
Na meq = Na mg/1 + Molec.Wgt.Na = 116.79 = 23 = 5.07783
Ca meq = Ca mg/I _ Molec.Wgt.Ca.= 419.07 = 20 = 20.9535
Mg meq = Mg mg/I = Molec.Wgt.Mg = 76.715 -= 12 = 6.39292
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.07783 = SgrRoot[0.5(20.9535+6.39292)] = 1.37323
Printed: 1 /31 /2015
Page 1 10:50
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SANFORD, NC PREDOMINANT SOIL SERIES: CID
OWNER: HENRY STINSON PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 15.26
SITE #: NC CH 00049 FIELD# : CH 00049 0007 OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 18.80 - ACRES PERMITTED: 18.80
Page
Lime Applied ***
Date
Lbs/A6
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/4/14
161,200.00 (G)
8574.468
2.27
0.812
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
Apr-14
1 161,200.00 (G)
8,574.468
Total Gallons/Ac: 8,574.47
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
50
Annuallbs/acre
0.010
0.003
0.364
0.959
0.050
0.001
0.032
0.123
0.008
1.454
40.58
Cumulative lbs/acre
0.083
0.108
1.287
10.726
0.642
0.058
0.613
0.983
0.111
23.661
i,.
"
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
u �±
41
.,
133
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
g
1339.0
267.9
15.0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN- Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: SANFORD, NC
OWNER: STINSON, JR HENRY
SITE #: NC CH 00066 FIELD# : CH 00066 0001
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NANFORD-BADIN
PERMIT #: W00000543
OPERATOR: HENRY STINSON
ANNUAL DRY TONS APPLIED: 48.13
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 31.70 ACRES PERMITTED: 31.70
Page : 1
Lime Apphed ***
Date Lbs/Ac
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
%
Dry
Tons
Per
Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
Ammonia
Nitrogen
Nitrate
and
PAN
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/12/14
173,600.00 (G)
5476.341
2.27
0.518
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
I FESCUE
5/13/14
167,400.00 (G)
5280.757
2.27
0.500
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
I FESCUE
5/14/14
167,400.00 (G)
5280.757
2.27
0.500
SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
May-14
508,400.00 (G)
16,037.855
Total Gallons/Ac: 16,037.85
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
93
Annuallbs/acre
0.018
0.006
0.680
1.794
0.094
0.003
0.061
0.231
0.015
2.720
75.91
}
;
Cumulative lbs/acre
0.018
0.006
0.680
1.794
0.094
0.003
0.061
0.231
0.015
2.720
135
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Lijection/Incorporation 1.0
* `Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: SANFORD, NC
OWNER: STINSON, JR. HENRY
SITE #: NC CH 00066 FIELD# : CH 00066 0002
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NANFORD-BADIN
PERMIT #: W00006543 ANNUAL DRY TONS APPLIED: 27.00
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 19.90 ACRES PERMITTED: 19.90
i
Page : 1
Lime Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/9/14
254,200.00 (G)
12773.869
2.27
1.209
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
5/12/14
31,000.00 (G)
1557.789
2,27
0.147
SBCAEDL
DRY
0-<I/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
May-14
285,200.00 (G)
14,331.658
Total Gallons/Ac: 14,331.66
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
83
Annuallbs/acre
0.016
0.005
0.608
1.604
0.084
0.002
0.054
0.206
0.014
2.431
67.83
Cumulativelbs/acre
0.016
0.005
0.608
1.604
0.084
0.002
0.054
0.206
0.014
2.431
F k
r;
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
ft
++'"Y
R-101
135
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
"3
SBCAEDL = NANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: SANFORD, NC
OWNER: STINSON, JR. HENRY
SITE #: NC CH 00066 FIELD# : CH 00066 0003
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NANFORD-BADIN
PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 22.89
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 16.80 ACRES PERMITTED: 16.80
Page
Lime Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/6/14
217,000.00 (G)
12916.667
2.27
1.223
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 ' p
30689
F30689
I FESCUE
5/7/14
24,800.00 (G)
1476.190
2.27
0.140
SBCAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
I FESCUE
May-14
241,800.00 (G)
14,392.857
Total Gallons/Ac: 14,392.86
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
"
84
Annuallbs/acre
0.016
0.005
0.'610
1.610
0.084
0.002
0.055
0.207
0.014
2.441
68.12
Cumulative lbs/acre
0.016
0.005
0.610
1.610
0.084
0.002
0.055
0.207
0.014
2.441
;
135
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15 0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = pp- or mg/kg ** Volatilization Rate: Surface 0.5, Injectiordhicorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
FACILITY NAME: SANFORD, NC
OWNER: STINSON, JR. HENRY
SITE #: NC CH 00066 FIELD# : CH 00066 0004
RESIDUAL SOURCE(S):* See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PREDOMINANT SOIL SERIES: NANFORD-BADIN
PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 46.95
OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED: 30.80 ACRES PERMITTED: 30.80
Page : 1
Lune Applied ***
Date Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
%
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
5/7/14
241,800.00 (G)
7850.649
2.27
0.743
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
5/8/14
254,200.00 (G)
8253.247
2.27
0.781
SBCAEDL
MOIST
0-<1/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
30689
FESCUE
May-14
496,000.00 (G)
16,103.896
Total Gallons/Ac: 16,103.90
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
94
Annuallbs/acre
0.018
0.006
0.683
1.802
0.095
0.003
0.061
0.232
0.015
2.732
76.22
Cumulative lbs/acre
0.018
0.006
0.683
1.802
0.095
0.003
0.061
0.232
0.015
2.732
` ` A
135
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
* .
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN - In'corporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SANFORD, NC PREDOMINANT SOIL SERIES: CID
OWNER: CYNTHLA/ANGELA STORY/EADES PERMIT #: WQ0000543 ANNUAL DRY TONS APPLIED: 38.73
SITE #: NC CH 00066 FIELD# : CH 00066 0006 OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 21.60 ACRES PERMITTED: 21.60
Page
Lune Applied ***
Date
Lbs/Ac
allons (G) or Cubic Yards (CY)
Dry
Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
"�o
Tons
Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
Per -
Residual
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MONTH
Total
Per Acre
Solids
4/2/14
142,600.00 (G)
6601.852
2.27
0.625
SBCAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
79,700. p
33,500.00 p
79.30 p
F 30689
I FESCUE
4/3/14
266,600.00 (G)
12342.593
2.27
1.168
SBCAEDL
MOIST
0-<I/2"
SUR
0.5
0.30
79,700, p
33,500.00 p
79.30 p
30689
1 FESCUE
Apr-14
1 409,200.00 (G)
18,944.445
Total Gallons/Ac: 18,944.44
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
TOTALS:
Annual lbs/acre
0.022
0.007
0.803
2.120
0.111
0.003
0.072
0.273
0.018
3.214
89.66
110
Cumulative lbs/acre
0.022
0.007
1 0.803
2.120
1 0.111
0.003
0.072
1 0.273
0.018
3.214
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
i.
r
178
FD Cumulative Pollutant Loading Rate Limit (Ibs/acre)
36.6
34.8
1339.0
267.9
15.0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
'1,- 71 - f-
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SANFORD, NC PREDOMINANT SOIL SERIES: CID
OWNER: CYNTHIA/ANGELA STORY/EADES PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 9.98
SITE #- NC CH 00066 FIELD# • CH 00066 0008 OPERATOR: HENRY STINSON CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report
allons (G) or Cubic Yards (CY)
Dry
or Wet Tons (WT) (specify)
%
Tons
DATE or
Per
Residual
MONTH
Total
Per Acre
Solids
4/4/14
105,400.00 (G)
17278.689
2.27
1.636
SBCAEDL
Apr-14
1 105,400.00 (G)
17,278.689
Total Gallons/Ac: 17,278.69
TOTALS:
Annual lbs/acre
Cumulative lbs/acre
ACRES UTILIZED: 6.10 ACRES PERMITTED: 6.10
Site
Inches
Appli-
Vola-
Miner-
Cond.
Precip:
cation
tili-
ali-
Ammonia
Nitrate
PAN
Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(ppm)
Crop
MOIST
0-<1/2"
SUR
1 0.5
0.30
1 79,700. p
33,500.00 p
79.30 p
30689
I FESCUE
Page : 1
Lime Applied ***
Date
Lbs/Ac
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN
100
0.020
0.007
0.733
1.933
0.101
0.003
0.065
0.249
0.016
2.931
81.78
0.020
0.007
0.733
1.933
0.101
0.003
0.065
0.249
0.016
2.931
Permit PAN Limit (lbs/acre) 1 st Crop/2nd Crop
178
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
36.6
34.8
L
1339.0
267.9
15.0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations."
N/A = Not Applicable NR = Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Metlmod: SUR - Surface, INJ - Injection, SURIN - Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Page : 1
Lime Applied ***
FACILITY
NAME: SANFORD, NC
PREDOMINANT SOIL SERIES: MASADA
105.61
Date Lbs/Ac
OWNER:
BERTRAM COFFER
PERMIT #:
W00000543
ANNUAL DRY
TONS APPLIED:
SITE #:
NC MR 00003 FIELD# : MR 00003
0001 OPERATOR:
RONALD TEAGUE
CATION EXCHANGE CAPACITY (NON-503):
ACRES UTILIZED:
66.30
ACRES PERMITTED:
66.30
RESIDUAL SOURCE(S):* See list at bottom of report
allons (G) or Cubic Yards (CY)
Dry Site
Inches
Appli-
Vola-
Miner -
or Wet Tons (WT) (specify)
Tons Cond.
Precip.
cation
tili-
ali-
Ammonia
Nitrate
PAN
DATE or
%
Per Residual Dry, Wet,
Past 24
Method
zation
zation
TKN
Nitrogen
and
(pprn)
Crop
MONTH
Total Per Acre
Solids
7/17/14
155,000.00 (G) 2337.858
2.22
0.216 SBCAEDL DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
45,000.00 p
72.10 p
35682
I FESCUE
7/18/14
316,200.00 (G) 4769.231
2.22
0.442 SBCAEDL DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
45,000.00 p
72.10 p
35682
I FESCUE
7/23/14
254,200.00 (G) 3834.087
2.22
0.355 SBCAEDL DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
45,000.00 p
72.10 p
35682
I FESCUE
7/24/14
210,800.00 (G) 3179.487
2.22
0.294 SBCAEDL DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
45,000.00 p
72.10 p
35682
jl FESCUE
7/28/14
204,600.00 (G) 3085.973
2,22
0.286 SBCAEDL DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
45,000.00 p
72.10 p
35682
FESCUE
Jul-14
1,140,800.00 (G) 1 179206.636
Total Gallons/Ac: 17,206.64
TOTALS:
Annual lbs/acre
Cumulative lbs/acre
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
FD Cumulative Pollutant Loading Rate Limit (lbs/acre)
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn P
PAN
114
0.016
0.006
0.554
1.790
0.102
0.004
0.041
0.233
0.019
2.549 85.38
0.155
0.075
4.569
17.660
1.035
0.044
0.521
1.843
0.190
25.906
uEP
'gEy ft
3.Y+i'
141
{
36.6
34.8
1339.0
267.9
15.0
375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required %= percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ - hijection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
FACILITY NAME: SANFORD, NC PREDOMINANT SOIL SERIES: MASADA
OWNER: BERTRAM COFFER PERMIT #: W00000543 ANNUAL DRY TONS APPLIED: 49.93
SITE #: NC MR 00003 FIELD# : MR 00003 0002 OPERATOR: RONALD TEAGUE CATION EXCHANGE CAPACITY (NON-503):
RESIDUAL SOURCE(S):* See list at bottom of report ACRES UTILIZED: 30.60 ACRES PERMITTED: 30.60
DATE or
allons (G) or Cubic Yards (CY)
or Wet Tons (WT) (specify)
oho
Dry
Tons
per Residual
Site
Cond.
Dry, Wet,
Inches
Precip.
Past 24
Appli-
cation
Method
Vola-
tili-
zation
Miner -
ali-
zation
TKN
MONTH
Total Per Acre
Solids
7/29/14
241,800.00 (G) 7901.961
2.22
0.732 SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
7/30/14
204,600.00 (G) 6686.275
2.22
0.619 SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
7/31/14
93,000.00 (G) 3039.216
2.22
0.281 SBCAEDL
DRY
0-<1/2"
SUR
0.5
0.30
88,700. p
Jul-14
539,400.00 (G) 17,627.452
Total
Gallons/Ac: 17,627.45
TOTALS:
Annual lbs/acre
Cumulative lbs/acre
Ammonia
Nitrogen
45,000.00 p
45,000.00 p
45,000.00 p
As
Cd
Cr
Cu
Pb
Hg
Mo
0.016
0.007
0.568
1.834
0.104
0.004
0.042
0.133
0.054
4.485
15.428
0.820
0.038
0.433
Nitrate
pAN
and
(rpm)
Crop
72.10 p
35682
I FESCUE
72.10 p
35682
Ij FESCUE
72.10 p
35682
FESCUE
Ni
Se
Zn
Page : 1
Lane Applied ***
Date LbYAb
P PAN
116
0.238 0.020 2.611 87.47
2.097 0.153 21.269
141
Permit PAN Limit (lbs/acre) 1st Crop/2nd Crop
.
FD Cumulative Pollutant -Loading Rate Limit (lbs/acre)
36.6
34.8
C
{
1339.0
267.9
15.0 375.0
89.0
2500.0
SBCAEDL = SANFORD, NC BUFFALO CREEK WWTP AEROB. DIG. LIQUID
X
(SIGNATURE OF LAND APPLIER) DATE
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and
evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
N/A = Not Applicable NR= Not Reported or Not Required % = percent p = ppm or mg/kg ** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
* Application Method: SUR - Surface, INJ -Injection, SURIN -Incorporation *** See Site pH & Lime Application Records Section of Report for Fields where Lime is to be applied in 2015
- Su x ', lam!
�CC4�IR04�P�lE�IYtIL`�C:�+3JOU��irS� itds.
t�rraf�ti�t?P t�ca�r�Prt'l�s'
January 22, 2014
Edward Stephens
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Sanford
Dear Edward Stephens:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: http:lAviviv.settek.com
Order No.: 14010506
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/10/2014 for the analyses
presented in the following report.
There were no problems with the analytical events associated with this report unless noted in the
Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits except
where noted.
If you have any questions regarding these tests results, please feel free to call the laboratory.
Sincerely,
N�
Dr. Mo Osman
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
A2LA 0724.01, Alabama 41600, Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH-0105, Delaware, Florida NELAC E87688, Georgia
E87688 and 943, Idaho OH00923, Illinois 200061 and Reg.5, Indiana C-OH-13, Kansas E-10347, Kentucky (underground Storage Tank) 3, Kentucky
90146, Louisiana 04061 and LA12004, Maine 2012015, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, Montana CERT0099, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, Ohio 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon
OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina 92016001, Tennessee TN04018, Texas T104704466-I1-5, Region 8 8TMS-
L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vennont VT-87688, Virginia 00440 and 1581, Washington C891, West Virginia 248 and 9957C
and E87688, Wisconsin 399013010
SununitEnvironmental Technologies, Inc.
�. 3310 Win St.
ENVIR[7 VAE�TrALPM, Cuyahoga Falls, Ohio 44223
tiruE ct€+:r?i F ao+ltlr 5 TEL: (330) 253-8211 FAX.- (330) 253-4489
Website: htW.-Iliviviv.settek.com
CLIENT: Synagro
Project: Sanford
Lab SampleID Client Sample ID
14010506-001 Sanford
Tag No Date Collected
1/6/2014 3:35:00 PM
Workorder
Sample Summary
WO#: 14010506
22-Jan-14
Date Received Matrix
1/10/2014 9:52:00 AM Sludge
`f
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14010506
`
�'P§lflf[C? ES;.3K4',
Cuyahoga Falls, Ohio94223
Date Reported:
1/22/2014
Anatlfiv,afit°Fiaratiri
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro
y
Wehsite: htty.11www.settekcon:
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Sanford
TCLP Metals Analysis (6010)
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sanford
001
1/6/2014
TCLP Arsenic(As)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Barium(Ba)
5.0
5.1 mg/L
Sludge
EPA 6010 C
1
100
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Cadmium(Cd)
0.10
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Chromium(Cr)
0.20
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Lead(Pb)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Selenium(Se)
0.50
ND mg/L
Sludge
EPA 6010 C
1
1.0
1/16/2014
VVK
Sanford
001
1/6/2014
TCLP Silver(Ag)
0.50
ND mg/L
Sludge
EPA 6010 C
1
5.0
1/16/2014
VVK
TCLP Mercury Analysis (1311/7470)
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sanford
001
1/6/2014
TCLP Mercury
0.0020
ND mg/L
Sludge
EPA 7470 A
1
0.20
1/16/2014
ALJ
SVOC
SW-846: 8081-TCLP
Pesticides
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sanford
001
1/6/2014
Chlordane, total
0.010
ND mg/L
Sludge
EPA 8081 B
1
0.030
1/17/2014
JBN
Sanford
001
1/6/2014
Toxaphene
0.10
ND mg/L
Sludge
EPA 8081 B
1
0.50
1/17/2014
JBN
Sanford
001
1/6/2014
Endrin
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.020
1/17/2014
JBN
Sanford
001
1/6/2014
gamma-BHC
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.40
1/17/2014
JBN
Sanford
001
1/6/2014
Heptachlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/17/2014
JBN
Sanford
001
1/6/2014
Heptachlor epoxide
0.0020
ND mg/L
Sludge
EPA 8081 B
1
0.0080
1/17/2014
JBN
Sanford
001
1/6/2014
Methoxychlor
0.0020
ND mg/L
Sludge
EPA 8081 B
1
10
1/17/2014
JBN
VOC by GC/MS (8260)-TCLP
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
_ RegLvl
Run
Analyst
Sanford
001
1/6/2014
1,1-Dichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/16/2014
MES
Sanford
001
1/6/2014
1,2-Dichloroethane
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/16/2014
MES
Sanford
001
1/6/2014
Benzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/16/2014
MES
Sanford
001
1/6/2014
Carbon tetrachloride
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/16/2014
MES
Sanford
001
1/6/2014
Chlorobenzene
0.10
ND mg/L
Sludge
EPA 8260 B
1
100
1/16/2014
MES
Sanford
001
1/6/2014
Chloroform
0.10
ND mg/L
Sludge
EPA 8260 B
1
6.0
1/16/2014
MES
Sanford
001
1/6/2014
Tetrachloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.70
1/16/2014
MES
Sanford
001
1/6/2014
Trichloroethene
0.10
ND mg/L
Sludge
EPA 8260 B
1
0.50
1/16/2014
MES
Sanford
001
1/6/2014
Vinyl chloride
0.20
ND mg/L
Sludge
EPA 8260 B
1
0.20
1/16/2014
MES
Sanford
001
1/6/2014
MEK
2.0
ND mg/L
Sludge
EPA 8260 B
1
200
1/16/2014
MES
1. �.
Summit Environmental Technologies, Inc.
3310 Win St.
WO#:
14010506
I� '5
�k�tGVlfiOtJAa7ENTv1L'6EL�`�#$�.i3_ L�'G1�Ca,.1i�ECa
Cuyahoga
uJ' a Falls, Ohio 44223 g
Date Reported:
1/22/2014
tkr3,y.Pica; L C7'prAipr3t
TEL: (330) 253-8211 FAX. (330) 253-4489
Company:
Synagro
Website: httn://wiviv.settek.com
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
Project#:
Sanford
SVOC 8270 TCLP BNA List
Client ID#
Lab ID#
Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sanford
001
1/6/2014
1,4-Dichlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
7.5
1/17/2014
AKE
Sanford
001
1/6/2014
2,4,5-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
400
1/17/2014
AKE
Sanford
001
1/6/2014
2,4,6-Trichlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/17/2014
AKE
Sanford
001
1/6/2014
2,4-Dinitrotoluene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/17/2014
AKE
Sanford
001
1/6/2014
Cresols, Total
5.0
ND mg/L
Sludge
EPA 8270 C
1
200
1/17/2014
AKE
Sanford
001
1/6/2014
Hexachloro-1,3-
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.50
1/17/2014
AKE
butadiene
Sanford
001
1/6/2014
Hexachlorobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
0.13
1/17/2014
AKE
Sanford
001
1/6/2014
Hexachloroethane
0.10
ND mg/L
Sludge
EPA 8270 C
1
3.0
1/17/2014
AKE
Sanford
001
1/6/2014
Nitrobenzene
0.10
ND mg/L
Sludge
EPA 8270 C
1
2.0
1/17/2014
AKE
Sanford
001
1/6/2014
Pentachlorophenol
0.25
ND mg/L
Sludge
EPA 8270 C
1
100 .
1/17/2014
AKE
Sanford
001
1/6/2014
Pyridine
0.25
ND mg/L
Sludge
EPA 8270 C
1
5.0
1/17/2014
AKE
SVOC
SW-846: 8321 Herbicides-TCLP
Client ID#
Lab ID# Collected Analyte
Rep Lmt Result Units
Matrix
Method
DF
RegLvl
Run
Analyst
Sanford
001
1/6/2014
2,4-D
5.0
ND mg/L
Sludge
EPA 8321 A
1
10
1/20/2014
AMZ
Sanford
001
1/6/2014
2,4,5-TP
0.50
ND mg/L
Sludge
EPA 8321 A
1
1.0
1/20/2014
AMZ
-
SununitEnvironmental Technologies, Inc.
3310 Win Si.
WO#:
14010506
ruwmoui,i ENrAL TECHNO S, 1.11C
M'SUMNU1101
Cuyahoga Falls, Ohio 44223
Date Reported:
1/22/2014
TEL: (330) 253-8211 FAX.- (330) 253-4489
Company:
Synagro,
Website: hity.-Ilivww.settek.coni
Address:
284 Boger Rd.
Mocksville NC 27028
Received:
1/10/2014
ProjecW:
Sanford
Client ID# Lab ID# Collected Analyte Result Units Matrix Method DF RL Run Analyst
Sanford 001 1/6/2014 Flashpoint (140°F) >140 *F Sludge EPA1010 1 1/13/2014 TAH
Sanford
001
1/6/2014
Cyanide, Reactive
Sanford
001
1/6/2014
pH
Sanford
001
1/612014
Sulfide, Reactive
ND pprn Sludge EPA 9014 1 0.50 1/10/2014 TIR
8.1 s.u. Sludge EPA 9045D 1 1/13/2014 AYS
ND pprn Sludge EPA 9034 1 25 1/10/2014 TIR
gg
Summit Etivironmient-al Technologies,- hic. Analysis Request/Chain of Custody
331 O"Ar, n Sa rcet R)rSunvnit Environnienral Inc. use-4111N
Cuvaho�p Fills. Ofiio,44223 Tel: 330.253.821:1 FOx.:.330..2531�4489- . I I- I .. C I 'T
pne__L_Of�_�- ISL
_(;(*iI?;wVMme (Please Print),
Protect. Vatne
6
Z
K3
E
-Analytical Parameters and Methods
Company Address
project Address-
it
-Z
Zrt
-
Z
'It
A
2.
1
Client'llhone- No
Client Fax No .111case F.1"Ar-milt-S-Z
PO#
Ufl6iifEn-u61Please Entail Results V
Quote-Na
Contact Pq
Sampled 11-
Check if OWO �A P samplLq
Sample Idenfification
pate
Collected
Notes[Conutients-
Nlust beappi-mvil 1
Received itt Iab by: ate Rush;Requested By:
Date by Int) 111,lmger
shotdd Lecampany-baruple., Sc 111C fabamtory.. The .cliew TPtaijl, die Pink page:
8, -1 1. ;�-g.
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
- Monitoring Period: From 01/01/14 To 03/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. l/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
i�l_ ♦ .. !'1.. .. D\ .. ..1..4.. F6o {:.11., i+nrinrt .la4a•
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6h
CFU
34600
47300
56700
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
(VS reduction) X
Option/Alt. 2
(40-day bench)
Option/Alt. 3 Option/Alt.4
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
(Injection)
Option/Mt. 10
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title (type, or print)
ads
Signature of Preparer* d Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Carfteeon Testirig SerViceis, .lnc. La'borAtory Report
- I i Synaqro qT9 Rroj. 140009
Sanford RegqlptoTy Yes
Sample I nfo rihnati Q' n
1AY V:Rrnpr 0.11061.14 Received s C. Cameron
Analyses and Results
LAID Saqple,lv
r= -Aninlyte Result
Z
E
1400Q9 01- Sanford
El
Sludge Gr' Fec.,rc)IIfbrr6-S <51200
GFUIp
10
449200
cmg
10
<42800
cru,@
la.
d
<34600
cRkla
10
-48900
'rFU,'g
iG
f
<5670.0
ULMg
1a
9
<W400
c F u k,-
10
<47300
140009 01 0
d
e
f
9
NO DEP R #6.54
NC'PHHS **7799
US EPAIINC01918
01/06/04
�2 'Ui � 'E . I , Methods
.3
Z
.51200 OPK 92221) - MF
4920D DPK 92221)- MF
4260D' DPK 9222Q - PAF
346D0 DPK 9222D - MF
48900 D.PKI 9222D - MF
56,700 DPK 9222D - MF
51400 DPK 9222D - NIF
,SW,dq( Gr TS 1.91%
O1I071-14
DPK.
2540'G JS
1.87%
' %
om
D1i07114
DPK
2640,G =TS
1.970%
s,;
0.01
01107114
DPK
2540 0 -TS
1.99%
%
ooi
() 1 J07114
OT-k
2540. G, -TS
1.86%
-A
ooi
01107114'
UPK
2540 G -TS
;866/6
0.01
011D7/14
DPK
2546 G 48
2,00%
(.)1f0.71!4
DPK
254 D G -T' ;
Data
Review
L2b-Fechnldan
Report
Review
6
L i c or
Date
%9-20S-4240
219 S. Steak SET.
Sa:ijbed hNC 17330
219 S. Staela.-Str.- - Cameron Testing Services, Inc. Chailn.of Custody,
Sanford, NC 27,330 ' j ' .1 of
Phone. 919-208-4240 NC ViVUIGVV Cert. #Od Nd PHHS Cert# 37799 LJ5 EPA NG0_918.
.co:m pja�Y'.-
Contact:`
state'zo)-
W4r
sample-
Temp,(q)
T bldbk"-
)N
C Ts_`Ialb`u`s
- - I
r-?.
I Due:
F'hone:
R4.
Notes,
r
`Gollbbted:
2�
Sample -ID
ca,
Q)
E
m
CL L< i JS
E m z
z
>1
rV,�:�
71
1
None,(Oy
HNO3,,(N
L-L
1
Relinquished.,
--- Received:-
Qatel-Tirhe.-
n.
U
Rush work will eequire-orj6r approval. Additional chargeswill ap',bly
City of Sanford
Big Buffalo WWTP
Sludqe Calculations
IN
3/10/2014
W1
DISH
115.3062
W2
WET
215.6433
W3
DRY
116.2570
W4
ASH
115.5453
0.947606
PERCENT VOLITILE SOLIDS 0.748528
OUT
VV1
DISH
115.5844
VJ2
WET
214.1066
W3
DRY
120.5002
W4
ASH
118.0968
PERCENT SOLIDS 4.989535
PERCENT VOLITILE SOLIDS 0.488913
PERCENT VOLITILE SOLIDS REDUCTION 67.36192
VSR = 67.86192
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 04/01/14 To 06/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If annlirahip to alternative nerfnrmed trlace A nr rlace R) rmmnlete the fallawina mnnitorina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'h
CFU
35500
41500
43800
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Ait. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title type o print)
\ 9Z76
�S
Signature of Preparer* Da
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc. Lalaoratory Report
NC DFNR 41654
NC PHHS #37799.
US EPA #NC01916
Clierifi:
Synagro
CTS Proj.
140422
Project:-
Sanford
Regulatory
Yes
Sample
Information
Sampled
W. Varner Date
04122114 -
Received
J. Jackson
Date
04122/14
Analyses and Results
rA
Lab ID
CL
Sample ID . o �°
Analyte
Result
��, E'
x.
Std .Methods
Reference
L r�
-
kc
--
140422 01
Sanford
S-1 si guy( Gr
Fec. Coliform-S
<4340D
cru,j,
43400
04122/14
JLJ
92221) - MF
S-2
Fec. Coliforrn-S
•-3550D
cF'-11;
35500
04/22114
JLJ
9222D - MF
S-3
Fec- Coliform-S
<4380D
crulr
43i1U0
041221/4
JLJ
9222D - MF
S-4
Fec. Coliform-3
•<40000
CFwo
40000
d412.7114
JLJ
9222D - TOF
3_5
Fec. Coliform-S
<42900
cFu,;y
42900"
04122/14
JLJ
9222D - NIF
S-6
Fac. Coliform-S
<42900
Crum
42900
04/22114
JU
92220 - NAF
S-7
Fec- Coliform-S
<42700
cr-u,g
42700
04122114 JLJ '
92220, - NIF
Geomean
<415D0
140422 01
S-1.
TS (cYo)
2.21 %
n-,
D4122114
MRG
2540 G = rS
2.22%
:s
am
04122114
MRG
25410 -TS
8-3
TS
2,22%u
o.oi
04122114
MRG
2542 G -T5
S-4
TS (%)
2.21 %
a,ai
04122114
MRG
2543 G -TS
S-5
TS {%a)
2-.23%
6 a-,
04/22114
MRG
2544 G -TS
S_6
TS {°;,)
2.24%
e
o of
04122114
41R0
2545 G -TS
:.
S_7
a
TS {%o)
2.22%
%
0.01
04122,114
MRG
2546 G -TS
Data
Reviewj(�I�f
I /
Lab echnician
Date
Report
Review
///
05%�7l! '"�
_ "
Lab R eolor
Date
219 S. Steele S1r
Sanlbrd NIC 2bN
919-205-4240
chris(t�r:n)3Ct 0a1C5lan �,.C4n1
C in-,O'f'CLJ§tOd 219 S.',-Gt , eel-6 GV,' Cameron Testing- Services,, Inc. Y,
�; -'r). , Nr ,I lard.- 2733.0 Pa' of
Plione:._91S-208-4240 N(� VVMGW Cert P,654. N-_ PP.HS C;_�H # 37799 U.S' EPA NC01 918 ge
S' nagro
y
A
..CTS`11A`u!3�ip,OrAy
4 3 �2
Cc3Mac Phone;
filj
-Sainple
Tamp (C.)
To,
j dd el ", ,BO�brd,
- 284'R
T, id- !ik, ,
;A rnve:
Mbbksville, NC 27028Notes:
CPitr:
ulq6r.y
-:lush
twd� Namb"
-Sig! W
7a. re
'Sample I'D-
LLI
:G
Ripqd.ested: Afialy!Ms
CTS! Lab
E
LL
RbI i hed:
DaI617nie
17. 1
Rush- work v.,H 1-rei -- ke.,prior.approval, Addifid' nEikharop-swMap' y
jui, . -1 . Ok
City of'Sanford
Big Buffalo WWTP
Sludge Calculations
IN 24-Jun-14
VSR = 51.92195
W1
DISH
110.8613
W2
WET
210.1188
W3
DRY
111.3888
W4
ASH
111.0571
0.531446
PERCENT VOLITILE SOLIDS 0.628816
OUT
W1
DISH
118.4692
W2
WET
217.9846
W3
DRY
122.9457
W4
ASH
120.9363
PERCENT SOLIDS 4.498299
PERCENT VOLITILE SOLIDS OA48877
PERCENT VOLITILE SOLIDS REDUCTION 51.92195
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: WQ0000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 07/01/14 To 09/30/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying' Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class $ only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If ---1irahlo *n al*arna*G— narfnrmad !('lace A nr (lace M ramnla*n *ha fallnwina mnnitnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
CFU
37700
42900
46400
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0ption/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X_ reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification inclding fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Z
arer Name and Title �ty e or 1 int) Land Applier Name and Title (if applicable) (type or print)
e V- q. *ates—
Si� ature of Preparer* Signature of Land APPlier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Tes ifn y
�abbiif&Report
rr a ,Ameron
#37799
.
NG 'HHS
,
agro
- a ple,inform—
fia h
;
i £ arrFSd v
11�lifl.V�arllei
r to
Di£'!t?9 (ac su I�ri C
in raan
t�a:e`;
6ff10�14
An8lv es
and Results"
'Rb-t3:arit'pf
e.i�
.
X���d�te� Rflt1#
.140800 01
Sanford
- 4.4500 duip
W1a1T�
4�6l�€�}0 cF%J
�:Pw,
43cOOOL' c1=w
13£x]
f
: 46400 r,i.urri:
461" .
-4200.0 ' OtJjq
4^[.u41
»rsl xr4 ; 42000
i40800 Ol
a
T6 q ,(%) 2:19% °,:
0 0;
0711/114
NPAF
1-540 G -`rS
b
2,18% %
001
{
2, 1 O%. s 'a
0,01
.d
2
;,4+1
,e
sr
2. 1 MXS k,
poI
..
9
2.23 /, r
d7
9ieview r.
QaC4ia' []S�/'
S3epoet
Rev3vr�.S %l
Date-
�195;���4�[c51Ct �3147 l`F1{•-G34i'�
Sahruid NC 2733Q 06is; mil'
299'S.'-Stde ; CS. *V. Cha'in'of C-ustody
Cameron Test! ng:Se.rv[ces, Inc-
'esi' __- --
NC tVVdjG3V-J Ear. #654 N-C PHHS r;,,, 4 37796 Us F-PA -Ncd �8 Pbgr:,.% of
irr
Erna
'Sample
.'miane:
Temp
e-, , �` P rGj.
Arr�jer
PrOjki.
J,
YIN) �WN)
Collected- P.10016; tL,/ 4 L--ei7
z
NuMlierof1bottleg.
&
0
-�s
>
U)
b-
-arnplia,11D.
>7
ak
Re uie:ste d Aiia I ysil s
I D
0
5V
17,
Rolinmfthed,:,
1P
Received:
DatWTiim_
—P3Sri
-R'ush-.work will require prior. approval. Add ibon al charges -will -a pp-,y
Ilk
City of Sanford
Big Buffalo WWTP
Sludge Calculations
N 22-Sep-14
VSR =
W1
DISH
111.3963
W2
WET
212.0376
W3
DRY
111.8880
W4
ASH
111.5682
0.488567
PERCENT VOLITILE SOLIDS 0.650397
OW,
W1
DISH
113.0746
W2
WET
213.4040
W3
DRY
130.9675
W4
ASH
127.2466
PERCENT SOLIDS 17.83415
PERCENT VOLITILE SOLIDS 0.207954
PERCENT VOLITILE SOLIDS REDUCTION 85.38716
35:3F7-1 G
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
WWTP Name: Big Buffalo WWTP NPDES Number: NCO024147
Monitoring Period: From 10/01/14 To 12/31/14
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
TP ......i:.... i.1.. 4--1-.......,- Wi—, A .,r rin c Rl n mnlafa tha fnllnwina mnnifnrina data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6 th
CFU
4190
4620
4830
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt. 3 Option/Alt. 4
(VS reduction) X
(40-day bench)
(30-day bench) (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky, WWTP Superintendent
Preparer Name and Title type or rint)
lS-
Signature of Preparer* Da
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc.
Laboratory Report
NCDENR#654
NC PHHS #37799
US EPA #NC01918
;K r.
.F'= l6n,
Synagro
:: 'crs;Pr
141220
=; __. _
0,01IN"R,
132—
Sanford
'�_M
Yes
Sample Information
am6ri
W. Varner Date
s.-?�
.�i ���',iY3
10/01/14 Received; C. Cameron Date
10/01/14
Analyses and Results
141220 01
a
sludge Gr Fec. Coliform-S <4760
CFUIg
4750 10/02/14 SB 9222D - MF
b
<4790
CFu1g
4790
C
<4670
CFUIg
4670
d
<4520
CFU19
4520
e
<4830
CFUIg
4830
f
<4590
CFUIg
4690
9
<4190
CFulg
4190
Geomean <4620
141220 01 a
Sludge Gr TS (%) 2.04%
Y.
0.01 10/02/14 SB 2540 G -TS
b
2.08%
h
0.01
C
2,07%
o
%
0.01
d
2.13%
,s
o.o1
e
-2.02%
"k.
o.o1
z
f
2.09%
9
2.07%
°%
. D-ot
Data
n
Review
q"�
Q
f �i
--
Lab IcIan"
-
Date
Report
Review
^�
Lab Director
1
Date
219 S. Steele Str. 919-208-4240
Sanford NC 27330 chrisCacamcrontcsting.com
21b-8. stdele,-Str.
'Senf6rd,-NC 27330
1 — nAO'�AnAn
Cameron, Testing. Sprvices',* Inc..
NC,MN/GW Cert. #664 NC PHHS !Cert-ft 37799 USEPA. NCOT9 , 18
Chain of , Cu ptody"
Page, :of �-- =:
MlOrle:vlz�e_vuY4 v
-7-7 77-7
Be,,on 1.
!Synagro-
O]Varner@syna�ro.com
C t
'Will Vefrher
3 -'qbb�-,8627
36
-40
284 Boger Rd.
AT�
Mbtksville, NC 27028
N�
Name:
a
m
d A
-F tS S
P C), F- 2'
S ,
JCD
0
3'�' =-
z i
/N
HNO3,,(N). '
-7—
R
t
u
ecelve -7
R d'
Rush.workmill require priorapproval. Additional .charges will apply
12- l q J'
City ®f Sanford-
Big, Buffalo WWTP
Sludge Calculations
!N
W1
DISH
115.5965
W2
WET
215.8672
W3
DRY
116.0011
W4
ASH
115.7155
0.403508
PERCENT VOLITILE SOLIDS
0.70 r882
OUT
W1
DISH
110.8862
W2
WET
211.3182
W3
DRY
116.8085
W4
ASH
113.6628
PERCENT SOLIDS
5.896826
PERCENT VOLITILE SOLIDS
0.631162
PERCENT VOLITILE SOLIDS REDUCTION 52.7944.8
VSR = 52.79443
Agricultural Lime Application Log
Year: 2014
Project: Sanford
Field Soil Lime Requirement Tons/Acre Date Applied
(state -county -site -field) pH (from soil analysis) Applied
NC-CH-49-7
NC-CH-66-1
N C-C H-66-2
NC-CH-66-3
NC-CH-66-4
N C-C H-66-6
NC-CH-66-8
NC-MR-3-1 5.1 1.7
NC-MR-3-2 6.1 0.0
* To be applied when field conditions improve.
Page 1 of 4 . ___
Report Number: 15-036-0503 ��
Account Number: 46489
www.aleastern.com
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
nnta Rwr_eivarL n9/05/2n15 Date Of Analvsis: 02/06/2015
A_&L Eastern Laboratories
762t V11hitepine Rbad Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6448
Grower:
STINSON
SOIL ANALYSIS REPORT
Date Of Report: 02/06/2015
Submitted By: WILL VARNER
Farm ID:
Analytical Method(s):
Mehlich 3
Organic
Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C:E.C„
Sample'ID
"Field
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil;
Buffer
; H
ID
Number
o Rate
/o
IbslA .
ppm Rate
ppm Rate
ppm Rate
ppm - Rate
ppm
Rate
ppm
Rate
H:
p..
Index
meq/100g
meq/100g
CH-49-7
15913
5.1 H 136
379 VH
271 VH
237 H
1475
M
39
VL
6.4
1.0
11.2
NC=316
NC=139
CH-66-1
15914
7.1 VH 150
181 VH
202 VH
1184 M
1322
M
131
VL
5.9
6.75
1.8
10.6
NC=151
INC =103
CH-66-2
15915
6.4 H 150
203 VH
236 VH
160 M
1 1148
M
126
VL 1
5:7
6.72
2.1
9.9
NC=169
NC=121
CH-66-3
15916
6.7 H 150
206 VH
338 VH
1211 H
1143
M
27
VL
5.5
6.64
2.9
11.4
NC=172
NC=173
CH-66-4
15917
5.9 H 150
1265VH'I'
338 VH
1217 H
1304
M
131
VL
5.9
6.74
1.9
11.3
NC=221
NC=173
Percent
Base
Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
:.
` Soluble
Salts
`-Chloride
Aluminum,
Sample ID
" K
Mg "
Ca
Na.
H -
NO3N'
S
Zn
Mn
Fe - .
Cu
�'B
S$.
'Cl
Al
Field ID
%
%, r
%
ppm Rate
ppm , Rate
ppm , Rate
ppm Rate
ppm :
Rate
ppm = .Rate
ppm'
Rate
' ms/cm Rate.
ppm Rate
,, ppm
CH-49-7
27 H
21.3 VH
55 VH
420
VH
6.7 VH
1.0
M
0.15
VL
6.2
17.6
65.8
1.5
8.9
NC=56
I NC=532.5
NC=344
NC=335.0
CH-66-1
H
VH
VH
VH
VH
M
VL
4.9
14.5
62.4
1.3
17.2
133
NC=69
116.7
NC=417.5
176
NC=475
1205
14.7
NC=235.0
10.6
10.14
CH-66-2
VH
16.8 VH
87 VH
200
VH
5.0 VH
M
VL
6.1
13.5
58.0
1.1
21.0
141
NC = 85
NC = 420.0
NC = 544
NC = 250.0
10.6
10.17
CH-66-3
VH
VH
60 VH
VH
7.1 VH
M
VL
7.6
15.4
50.1
1.0
25.7,
149
NC = 102
123.8
INC = 595.0
1 'NC: 375
1167
NC = 355.0
10.6
10.19
CH-66-4
M
VH
VH
277
VH
VH
0.7
M
VL.NC=46
7.7
16.0
57.7
1.2
17.1
122
120.2
NC=505.0
184
NC=5251.8.3
NC=415.0
1.0.17
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: ppuria n%c 60w4 H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 2 of 4 /�
Report Number: 15-036-0503 T —A&L .E_astern Laboratories
Account Number:46489 A�
7621 Whitepine Read Richmond, Virginia 23237 (804) 743-9401 Fax (804) 277.6446
wwwaleastern;com
Send To: SYNAGRO CENTRAL LLC/SANFORD Grower: Submitted By: WILL VARNER
Mary Brewer STINSON Farm ID:
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 02/05/2015
Date Of Report: 02/06/2015 SOIL FERTILITY RECOMMENDATIONS
Nitrogen`
Phosphate
Potash
Magnesium
Sulfur
Zinc,
Manganese
Iron.
Copper
.` Boron
Sample ID
I
Intended Crop
Yield_ Goal ,
Lime
N
P¢05
K20
Mg
S
Zn
Mn
Fe
Cu
B •,°
Field ID
Tons/A
Ib/A
Ib/A
Ib/A
lb/A,
Ib/A
Ib/A
Ib/A
fb/A
Ib/A
Ib/A'
CH 49-7
Adjust pH to 6.0
0
0.0
0
Q
0
CH-66-1
Adjust pH to 6.0
0
1.0
0
0
0
CH-66-2
Adjust pH to 6.0
0
1.3
0
0
0
CH-66-3
Adjust pH to 6.0
0
1.8
0
0
0
CH-66-4
Adjust pH to 6.0
0
1.0
0
0
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q me Gr
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the 1 ofc-
work,the results, or the company in any advertising, news release, or'other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary
Page 3 of 4 Report Number: 15-036-050399.
Account Number: 46489
www.aleastern:com
Send To: SYNAGRO CENTRAL LLC/SANFORD
Mary Brewer
284 BOGER RD
MOCKSVILLE NC 27028
nato Racnivari• rro/ns/2n1s Datp Of Analvsis: 02/06/2015
An&L -Eastern Laboratories-
7621__ Whitepine Road Richmond; Virginia 23237 (804).743.9401 Fax (804) 271-6446
Grower:
STINSON
SOIL ANALYSIS REPORT
Date Of Report: 02/06/2015
Submitted By: WILL VARNER
Farm ID:
Analytical Method(s):
Mehlich 3
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
!Sodium
T
pH
Acidity
C.E..G
Samp"le ID-
Lab
ENR
Mehlich 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H-
Field ID
Number
o
/o Rate lbs/A
ppm Rate
ppm Rate
'.ppm; 'Rate
ppm -Rate
ppm
Rate
ppm`
Rate
p H
`Index
meq/100g
meq%100g
CH-66-6
15918
6.4 H 150
347 VH
183 VH
273 H
1358
M
49
VL
6.1
1.5
11.3
NC=289
NC=94
CH-66-8
322 VH
94 L
284 H
1499
M
VL 1
6.2
1.4
11.7
15919
7.1 VH 150
NC = 268
NC = 48
1
1
132
Percent
Base Saturation.
Nitrate
Sulfur
Zinc
Manganese
Iron
- , .
-Copper
Boron
Soluble Salts
`Chloride
Aluminum
Sample ID`
K
Mg =
Ca
Na
H
`:NO3N
S
Zn
IVIn
'Fe
Cu
B _ ,
SS ..
Cl
AI° `
Fie1d,ID
ova
%
ppm Rate
ppm Rate
ppm- •Rate
ppm, Rate
ppm
Rate
ppm , Rate,
ppm
Rate,
ms/cm_ Rate
ppm Rate
ppm,
CH-66-6
31 H
28.8 VH
70 VH
241
VH
12.4 VH
0.8
M
0.12 VL
4.2
20.1
60.1
1.9
13.7
NC=64
NC=720.0
INC =438
NC=620.0
CH 66-8
M
VH
H
VH
13.4 VH
M
VL
2.1
20.2
64.1
1.2
12.1
117
NC = 35
132.9
NC = 822.5
146
NC = 288
1289
NC = 670.0
10.8
10.09
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to samples) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm.
Pauric McGroary
Page 4 of 4 __
Report Number: 15-036-0503 �r n A&L Eastern -Laboratories
Account Number: 46489 LI 7621 Whitepine Road Richmond; Virginia 23237 (804) 743-9401 Fax (804)_271.Wii
Send To: SYNAGRO CENTRAL LLC/SANFORD WWW.81E15terfl.COti1 Grower: Submitted By: WILL VARNER
Mary Brewer STINSON Farm ID:.
284 BOGER RD
MOCKSVILLE NC 27028
Date Received: 02/05/2015
Date Of Report: 02/06/2015 SOIL FERTILITY RECOMMENDATIONS
Nitrogen
Phosphate .
Potash
MagnesiumSu
ur
me
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P O
2 5
K 2O
M g
S
2n
Mn
Fe
Cu
B
Field ID
TonslA
'Ib/A -
Ib/A
Ib/A
,
Ib/A
Ib/A`
Ib/A
Ib/A
Ib/A
Ib/A
&A
CH-66-6
Adjust pH to 6.0
0
0.0
-
0
0
0
CH-66-8
Adjust pH to 6.0
0
0.0
0
0
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Q
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.
Pauric McGroary
N . CDA&CS'—,,.,Zaomic Division Phone: (919) 733-2655
Website: www.i...u..goviagronomi/
Report No. FY':'----L'003221
Predictive
Client: Ronald Teause
495 Davis Dr
Siler City, NC 27-344
Advisor: Synagro ATTN: Will
Varner
2828 Tryon Rd
Mehlich-3 Extraction
Soil Report
/284 Boger Rd
Raleigh, NC 27603
Sampled County: Chatham
aai
Sampled: 08/13/2014 Received: 08/13/2014
Completed: 08/22/2014
Farm: MR-3
Links to Helpful Information
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
K20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 1.7
120-200 0
0 0 0
0
0
0 0
Note: 12
2-
$pH
Test Results [units - WN in g1cnf; CEC and Na in meq/100 ca; NO3-N in mg/da]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac PH P-1 K-1
Ca% Mg%
S-1 Mn-1 Mn-All Mn-Al2
Zn-1
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.71 1.00 .
10.8 73 2.9 5.1 434 103
50 18
70 w 180' 125
1015
1015
589 0.1 1
Sample ID: 2
Recommendations- Lime
-
Nutrients (lb/acre)
More
Crop (tons/acre)
N P206
X20 Mg S
Mn
Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, 1 0.0
120-200 0
10 0 0
0
0
0 0
Note: 12
2-
$pH
Test Results [units - WN in g1ca; CEC and Na in meq/100 crrP; NO3-N in mgidffP]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac PH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-1
Zn-Al
Cu-I Na ESP SS-1 NO3-N
0.41 1.06
11.3 89 1.3 6.1 365 76
63 22
48 113 83
906
906
397 0.1 1
'br-th'.Car -'o 11na,
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxier, Commissioner of Agriculture
NCDA&CS .`.: ite: www.r.__,..gov/agronomi/ Report No. Fft__',003221
Ronald Teause Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations I Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton%acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
Mn-All
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations forsmall areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft. If you cannot
pH
current soil pH
find the exact fertilizer grade recommended on the report, visit www.ncagr.gov/agronomi/oboart4.htm#fs to find
P-1
phosphorus index
information that may help you choose a comparable alternate.For more information, readA Homeowner's Guide to Fertilizer.
P206
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-1, K-1, Ca%, Mg%, Mn-1, Mn-All, Mn-Al2, Zn-I, Zn-Al, Cu-I, S-1, SS-1, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uvrsthtm
for more information.