Loading...
HomeMy WebLinkAboutWQ0000455_Residual Annual Report 2014_20150227r 1 ` 2014 ANNUAL REPORT LAND APPLICATION PROGRAM LEWIS FARMS AND LIQUID WASTE, INC. PERMIT #WQ0000455 C Prepared For: Lewis Farms and Liquid Waste, Inc. 8155 Malpass Comer Road Currie, North Carolina 28435 Compiled By: S&ME, Inc. 8646 West Market Street, Suite 105 Greensboro, North Carolina 27409 February 2015 February 23, 2015 NCDENR-DWQ 1636 Mail Service Center Raleigh, North Carolina 27699-1636 Attention: Non -Discharge Permitting Unit Reference: 2014 LAND APPLICATION ANNUAL REPORT Lewis Farms and Liquid Waste, Inc. Permit No. WQ0000455 S&ME, Inc. Project No. 1588-95-010 Non -Discharge Permitting Unit: S&ME, Inc. (S&ME) is submitting all monitoring and reporting requirements as specified in the above referenced permit on behalf of Lewis Farms and Liquid Waste, Inc. (Lewis Farms). S&ME compiled this report using data gathered during the compliance year by Lewis Farms. This data includes: 1) certification form, 2) residuals analyses and pathogen / vector data, 3) i application summaries and field loading rate reports, and 4) soil analyses. If there is any further information required or questions regarding this annual report please do not hesitate to contact Lewis Farms or S&ME, Inc. for further assistance. Sincerely, S&ME, Inc. Martin Mabe Rob Willcox, L.S.S. NC Land Application/Residuals Operator Senior Project Manager 922753 Enclosures T:\Projects\1995\ENV\1588-95-010 LewisFarms\Annual Report 2014\2014 ANNUAL REPORT.doc r a S&ME, INC. / 8646 W. Market Street, Suite 105 / Greensboro, NC 27409 / p 336.288.7180 f 336.288.8980 / www.smeinc.com TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Residuals Analyses & Pathogen / Vector Attraction Data III 2014 Application Summary and Field Loading Rate Reports IV Soil Analysis r- CERTIFICATION FORMA ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: W00000455 County: Pender Year: 2014 .Facility Name .(as shown-oa-permit): Lewis Farms.and Liquid Waste, Inc.. Land Application Operator: Mr. Wesley Wooten Phone: 910-283-5444 Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were _ generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 18 Total number of fields utilized for land application during the year: 11 Total amount of dry tons applied during the year for all application sites: 380.60 Total number -of -acres utilizes-for,land application during-the-yean 230.-8 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain, corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T A 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached -to -include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." oe -Mr._Wesley-Wooten, President Permittee Name and Title (type or print) Signature o ermittee Date ' c Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) �^—RM „,­� i a i RESIDUAL ANALYSES TCLP ANALYSES IF REQUIRED AND PATHOGEN AND VECTOR ATTRACTION REDUCTION j hi ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding laboratory analysis. Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number W00000455 Facility Name Lewis Farms and Liquid Waste, Inc. Laboratory 1 Envirochem2 Environment 1 NPDES # See Below WINTP Name See Below 2014 DATA 3 RESIDUAL ANALYSIS DATA NPDES # WWiP Name Composited/Grab Percent Solids PARAMETERS (mo/kc WQ0000193 Bald Head Island 08/57/14 1.8 dry wei ht NCO065480 Beau Rivage 12/01/14 1.5 NCO074837 Bridgeton 12/03/14 0.5 WQ0018755 Castle Bay 12/02/14 1.3 NCO21610 Clarkton 55/29/14 0.23 NCO055107 Dolphin Bay 12/01/14 2.16 WQ0022052 Hampstead Pines 11/25/14 1.77 W00032115 Hampstead Town 09/15/14 1.15 NCO051969 NC0003344 Hermitage House House of Raeford 11 /19/14 11 /19/14 0.5 0.76 Arsenic Cadmium Copper Lead Mercury Molybdenum Nickel Selenium Zinc TKN Ammonia -Nitrogen Nitrate -Nitrogen Total Phosphorus RESIDUAL ANAL Ysts 5.50 5.50 839.00 21.80 0.66 8.78 21.80 6.72 1,690.00 28,200.00 74.70 826.00 48,700.00 nATA 7.53 7.53 299.00 11.30 6.20 7.53 12.30 8.00 643.00 69,800.00 5,570.00 46.40 19,200.00 2.50 2.00 464.00 22.00 0.23 5.00 13.00 5.00 1,783.00 8,563.00 285.00 3.86 9.641.00 7.58 7.58 134.00 18.40 1.53 7.58 13.70 7.94 1,060.00 63,500.00 462.00 161.00 17,500,00 37.00 37.00 288.00 37.00 3.07 37.00 37.00 37.00 1,870.00 140,000.00 1,743.00 36,800.00 82,600.00 3.89 3.89 427.00 25.90 0.93 3.98 11.90 7.96 731.00 58,300.00 485.00 127.00 17,400.00 4.07 4.07 236.00 15.50 1.02 4.24 11.60 10.70 1,020.00 59,500.00 326.00 19.90 24,500.00 7.13 7.13 289.00' 8.61 0.35 7.13 12.30 7.13 4,630.00 22,900.00 16,000.00 16.40 4,650.00 18.50 12.90 18.50 12.90 370.00 241.00 18.50 12.90 3.91 1.45 18.50 12.90 23.00 18.40 18.50 813.00 12.90 253.00 3,580.00 18,200.00 43.70 866.00 1,440.00 74.00 2,340.00 5,250.00 NPDES # WWTP Name Composited/Grab Percent Solids PARAMETERS (ma/ka NCO030813 Kenwood 11/18/14 1.96 dry weiahtl WQ0030088 Majestic Oaks 01/10/14 0.26 NCO021482 Maysville 08/14/14 1.02 NCO026611 Morehead City 02/18/14 19.5 NCO042251 Pender HS 10/66/14 0.33 NCO023230 Richlands 11/18/14 1.97 NCO030406 Riverbend 11/20/14 2.84 NC0022462 Sherwood MHP 05/24/14 1.33 Arsenic 4.29 33.80 2.50 9.44 23.30 5.03 7.44 Cadmium 4.29 33.80 1.30 0.51 23.30 5.03 7.44 Copper 497.00 239.00 635.00 862.00 539.00 228.00 26.00 Lead 12.40 33.80 20.00 8.77 92.10 12.90 =4.657.44 22.30 Mercury 0.46 6.15 0.43 2.00 6.06 0.51 0.23 Molybdenum 4.29 33.80 5.00 5.07 23.30 5.03 Nickel 14.70 33.80 22.00 8.72 23.30 12.90 11.40 22.20 Selenium 9.18 33.80 5.00 5.64 23.30 7.97 8.98 7.44 Zinc 1,470.00 946.00 944.00 990.00 688.00 924.00 845.00 5,290.00 TKN 71,100.00 74,200.00 6,960.00 8,350.00 152.00 68,500.00 71,600.00 134,000.00 Ammonia -Nitrogen 2,680.00 772.00 1,871.00 1,350.00 156.00 7,850.00 5,490.00 155.00 Nitrate -Nitrogen 549.00 1,440.00 3.89 13.30 6,140.00 664.00 144.00 80.80 Total Phosphorus 12,900.00 53,100.00 8,067.00 6,480.00 759.00 15.000.00 18,700.00 62,300.00 W00029475 WQ0023261 Sterling Farms Swansboro 04/09/13 03/05/14 5.08 2.68 1.97 3.32 1.97 3.32 109.00 451.00 7.15 17.60 0.15 2.16 3.03 5.74 7.40 12.40 4.80 6.98 1,200.00 3,720.00 29,700.00 27,000.00 1,550.00 302.00 7.70 5,220.00 10,300.00 1,060.00 Page 1 of 2 RESIDUAL ANALYSIS DATA NPDES # WWiP Name NCO047759 Taylor Ext. Care Composited / Grab 01/14/14 Percent Solids 1.9 PARAMETERS Arsenic50 Cadmium60 Copper5.00 TIdlwej-ht' Lead00 Mercury60 Molybdenum.00 Nickel 17.00 Selenium 5.00 Zinc 809.00 TKN 14,367.00 Ammonia -Nitrogen 1,049.00 Nitrate -Nitrogen Total Phosphorus 34.53 5,127.00 luuub//03 The Cape Co, Health Dept. Topsail Greens WQ0032930 Topsail High School NC0021342 Trenton NCO023825 Webb Apartments NC0062642 Webb Creek 12/02/14 11/19/14 09/29/14 03/20/14 11/18/14 01/21/14 1.47 1.54 0.36 4.26 1.02 3.61 5.17 6.10 20.80 2.50 8.63 2.60 5.17 6.10 20.80 1.10 8.63 2.60 265.00 187.00 769.00 213.00 490.00 285.00 12.30 12.30 26.40 45.00 15.80 5.37 1.29 1.36 5.56 0.48 0.78 0.08 5.17 6.10 20.80 5.00 8.63 2.60 20.30 10.70 30.60 9.00 15.90 6.23 6.94 20.80 5.00 16.30 2.60 584.00 1,500.00 746.00 6,240.00 2,170.00 17,700.00 =58,300.00 63,100.00 23,195.00 42,800.00 48,000.00 5,670.00 1,080.00 285.00 3,820.00 2,140.00 458.00 8,000.00 103.00 22,600.00 10.82 3,314.00 551.00 16,500.00 5.50 18.600.00 Page 2 of 2 X N/A due to number of sources (SIGNATURE OF PREPARER) DATE I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: August 7, 2014 Bald Head Island Permit No. WQ0000455 Mineralization Rate 0.30 1.80 % Solids 6.73 pH Parameter i % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 2.820 28,200.000 56.400 Phosphorus 4.870 48,700.000 97.400 Potassium 0.461 4;610.000 9.220 PAN (injected)* 0.934 9,338.290 18.677 PAN (surface)* 0.930 9,300.940 18.602 Ammonia Nitrogen 0.007 74.700 0.149 Calcium 2.910 29,100.000 58.200 Calcium Carbonate E . --- ___ --- Magnesium --- 6,780.000 13.560 Sodium 4,000.000 8.000 Sulfur ___ Nitrate N / Nitrite N --- 826.000 1.652 Barium ___ Chloride ___ ___ Iron ___ --- Aluminum --- 33,300.00 66.600 Arsenic --- 5.50 0.011 Cadmium --- 5.50 0.011 Chromium --- 42.700 --- Copper --- 839.00 1.678 Lead --- 21.80 0.044 Mercury --- 0.66 0.001 Molybdenum --- 8.78 0.018 Nickel --- 21.80 0.044 Selenium --- 6.72 0.013 Zinc --- 1,690.00 3.380 Environmental Chemists, Inc. # 2014-09533 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. r7-77 1 Environmental Chemists, Inc. envirochem 6602 Windmill Way a Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 l3owsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729 The Village Of Bald Head Island 106 Lighthouse Wynd Bald Head Island NC 28461 Attention: David Suther Date of Report: Aug 29, 2014 Customer PO #: Customer ID: 08100149 Report #: 2014-09533 Project ID: Sludge - Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-23470 Site: Sludge 8/7/2014 8:40 AM Solid/Sludge David Suther Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 33300mg/kg 08/13/2014 Arsenic EPA 200.7 <5.50 mg/kg 08/18/2014 Cadmium EPA200.7 <5.50 mg/kg 08/18/2014 Calcium EPA200:7 29100mg/kg 08/15/2014 Chromium EPA200.7 42.7 mg/kg 08/18/2014 Copper EPA200.7 839mglkg 08/18/2014 Lead EPA200.7 21.8 mg/kg 08/18/2014 Magnesium EPA200.7 6780mg/kg 08/16/2014 Molybdenum EPA 200.7 8.78 mg/kg 08/26/2014 Nickel EPA 200.7. 21.8 mg/kg 08/18/2014 Potassium EPA200.7 4610mg/kg 08/15/2014 Selenium EPA2003 6.72mg/kg 08/18/2014 Sodium EPA200.7 4000mg/kg 08/16/2014 Zinc EPA200.7 1690mglkg 08/13/2014 Ammoniar Nitrogen EPA350.1 74.7mglkg 08/13/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 28200 mg/kg 08/21/2014 Nitrate+Nitrite-Nitrogen EPA353.2 826mg/kg 08/27/2014 Total Solids (%) SM 254013 1.80 % 08/08/2014 pH SM 4500 H B 6.73 units 08/19/2014 Total Phosphorus SM4500PF 48700mg/kg 08/21/2014 Mercury SWM7471B 0.6560mg/kg 08/14/2014 Report #:: 2014-09533 Page 1 of 3 l Environmental Chemists, Inc. ■ 6602 Windmill Way • Wilmington, NC 28405 (910)392-0223 (Lab) • (910) 392-4424 (Fax) 9M 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 The Village Of Bald Head Island Date of Report: Aug 29, 2014 106 Lighthouse Wynd Customer PO M Bald Head Island NC 28461' Customer ID: 08100149 Attention: David Suther Report #: 2014-09533 Project ID: Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-23471 Site: 1 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Totai Solids (°10) SM 2540 B 1.90 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 47369 MPN/g 08/08/2014 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-23472 Site: 2 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 S. 2.07 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 106281 MPN/g 08/08/2014 Lab ID Sample ID: Collect DateMme Matrix Sampled by 14-23473 Site: 3 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 S 1.96 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 45219 MPN/g 08/08/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14 23474 Site: 4 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.04 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 68628 MPN/g 08/08/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-23475 Site: 5 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 2.02 % 08/0812014 Fecal Density SM 9221C E MPN 24 hr 503 44656 MPN/g 08/08/2014 Report #:: 2014-09533 Page 2 of 3 Environmental. Chemists, Inc. • �. 6602 Windmill Way • Wilmington, NC 28405 ® (910)392-0223 (Lab) • (910) 392-4424 (Fax) (( 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 The Village Of Bald Head Island Date of Report: Aug 29, 2014 106 Lighthouse Wynd Customer PO #: Bald Head Island NC 28461 Customer ID: 08100149 Attention: David Suther Report #: 2014-09533 Project ID: Sludge Lab 1D Sample ID:, Collect Date/Time Matrix Sampled by 14-23476 Site: 6 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.99 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 45227 MPN/g 08/08/2014 Lab 1D Sample ID: Collect Date/Time Matrix Sampled by 14-23477 Site: 7 8/7/2014 8:45 AM Solid/Sludge David Suther Test Method Results Date Analyzed Total Solids (%) SM 2540 a 1,98 % 08/08/2014 Fecal Density SM 9221C E MPN 24 hr 503 45919 MPN/g 08/08/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. - Reviewed Report #:: 2014-09533 Page 3 of 3 Analytical S Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTERCCATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT:The Village of Bald Head Island PROJECT NAME: Sludge REPORT NO:j If "6f5%� ADDRESS: P.O. box 3009 Bald Head Island N.0 28461 CONTACT NAME -David Suther PO NO: REPORT TO: David Suther PHONEIFAX: (910) 457-7352/457-735 COPY TO: David Suther E-MAIL:dsuther@viilagebhi.org Sampled By: David Suther SAMPLE TYPE: I = Influent, E- Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Collection - m s ®--. PRESERVATION Sample.ldentification ° a F' n °, 0ii _ a __ = E c m f° g g z u, i7 0 o c w ANALYSIS. REQUESTED Date Time Temp v U" z z x= Z o. 8/7/2014 8:40 p Sludge G 3 X Annual Analysis 8/7/2014 8:45 p 7 Sludge G A x Fecal Density P G 3 - 7— C P G G 61, 3 C P G G C P G G $ C P lop G G C P G G:20�W C P G G C P G G DTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be de chlorinated (0 2 ppm or less) In the field Transfer at the time of collection. See reverse for instructions Relinquished By: - Date/Time Received 8 • Y• Date/Time 1. 2. Temperature when Received: Accepted: Delivered By: Received By: ^- - Tim 3 I- LEWIS FARMS WQ0000455 Bald Head Island ..... ................... . t K R -ra UA. 08/07/14 47,369 4.6755 08/07/14 106,281 5.0265 08/07/14 45,219 4.6553 08/07/14 68,628 4.8365 08/07/14 44,555 4.6489 08/07/14 45,227 4.6554 08/07/14 45,919 4.6620 Total 33.1601 Average 4.7372—] Geometric Mean ffl Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen for Reduction requirement. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farris di: Liquid Waste, Irtc. WQ Permit Number. WQ0Wo455 WW'!iQ Name. Bald Head Island NPDES Number:, WQ0000193 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved d an alternative rformed: Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Trea_ tment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If livable to alternathe performed (Class A only) Indicate "Process to Further Reduce Pathogens": Compost Cl Heat Drying ❑ Heat Treatment ❑ 2Thmophilic ❑ Beta El Ea ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density 54 1 Alt. (2) Process to Si 'ficantl Reduce Patho ens p If aPPliable to alternative Performed (Class B only) indicate "Process to significantly Reduce Pathogens": Lime Stabilization ❑ Air g.❑ Comoostina ❑ Aerobic Di estion ❑ Anaerobic Di on ❑ If a pplicable to alternative Performed (Cl-- A or Class B) com lete the owinZ monitoring data: Allowable Level Pathogen Density nm o Parameter Frequency Sample Am in Sludge Nfinimurr Geo. Mean Mhximun Units ofAnalysis Type Tech- 26th o wa um 44,555 54,595 106,281 MPN/g 0 Anne � SM 9221 Po per gram of Fecal Coliform total solids CFU 1000 mpn per tram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grnms (in lieu of fecal total solid (dry Conformweight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑Ali 2 (40-day bench) ❑ Alt, 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptaloe) ❑ Alt. 5 (14-Day Aerobic) ❑ Art. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑Alt 8 (Drying Unstable) ElAlt 9 (Injection) ❑ Ait. 10 (Im:otporation) p No vector attraction reduction alternatives were peuformed ❑ CERTIFICATI eTATFttwhrr i...- _,.__._ At.- -------- - ----- �r•...a..wC,�ppropnatestatement) , 1] "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC.02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in ISA-NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." David Suther, ORC Wesley Wooten, President Prepauer Name and Title (type or t) Land-Appirer an utle (if applicable)(type or print) Signature of r* 's P Date Signal = of Land Applier (if applicable) Dam "parer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l lot (26) DENR FORM PVRF 02T (12200e) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 1, 2014 Beau Rivaee 1.50 % Solids 6.74 PH Permit No. Parameter % Mg/Kg Dry Weight % x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 6.980 69,800.000 139.600 Phosphorus 1.920 19,200.000 38.400 Potassium 0.378 3,780.000 7.560 PAN (injected)* 2.489 24,885.400 49.771 PAN (surface)* 2.210 22,100.400 44.201 Ammonia Nitrogen 0.557 5,570.000 11.140 Calcium 0.249 2,490.000 4.980 Calcium Carbonate E . --- --- --- Magnesium - 2,340.000 4.680 Sodium - 3,970.000 7.940 Sulfur --- --- Nitrate N / Nitrite N --- 46.400 0.093 Barium --- Chloride --- --- --- Iron --- Aluminum --- 2,790.00 5.580 Arsenic --- 7.53 0.015 Cadmium --- 7.53 0.015 Chromium --- 10.500 --- Copper 299.00 0.598 Lead --- 11.30 0.023 Mercury --- 6.20 0.012 Molybdenum --- 7.53 0.015 Nickel --- 12.30 0.025 Selenium --- 8.00 0.016 Zinc --- 643.00 1.286 Environmental Chemists, Inc. # 2014-14772 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate.)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. F"O" 11 Environmental Chemists Inc. envirochem 6602 Windmill Way Wilmington, NC 28405 (910)392-0223(Lab) 9 (910)392-4424(Fax) -' 710 Bowsertown Road - Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERrIFICATE #37729 Aqua America of North Carolina Date of Report: Dec 11, 2014 105 Hampstead Village BLDG 24-1 Customer PO M Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report #• 2014-14772 Project ID: Beau Rivage WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-36210 Site: Sludge 12/1/2014 12:46 PM Solid/Sludge Kirklyn Fields Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 2790 mg/kg 12/09/2014 Arsenic EPA 200.7 <7.53 mg/kg 12/03/2014 Cadmium EPA200.7 <7.53 mg/kg 12/03/2014 Calcium EPA200.7 2490 mg/kg 12/03/2014 Chromium EPA 200.7 10.6 mg/kg 12/03/2014 Copper EPA200.7 299 mg/kg 12103/2014 Lead EPA200.7 11.3 mg/kg 12/03/2014 Magnesium EPA200.7 2340mg/kg 12/03/2014 Molybdenum EPA200.7 <7.53mg/kg 12/03/2014 Nickel EPA200.7 12.3 mg/kg 12/03/2014 Potassium EPA200.7 3780mg/kg 12JO312014 Selenium EPA200.7 8.00 mg/kg 12/03/2014 Sodium EPA 200.7 3970 mg/kg .12/03/2014 Zinc EPA200.7 643mg/kg 12/03/2014 Ammonia Nitrogen EPA 360.1 5570 mg/kg 12/08/2014 Total Kjeldahl Nitrogen (TKN) EPA361.2 69800mg/kg 12/08/2014 Nitrate+Nitrite-Nitrogen EPA353.2 46.4mg/kg 12/09/2014 Total Solids (%) SM 2640 B 1.50 % 12/01/2014 PH sM4600 H B 6.74 units 12/05/2014 Total Phosphorus sM 4500 P F 19200 mg/kg 12/09/2014 Mercury SW046 7471 a 6.20 mg/kg 12/05/2014 Comment Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Y.� Report #:: 2014-14772 Page 1 of 1 i � ENVIRONMENTAL CHEMISTS, INC OFF Windmill-32 z 3"FAX9,o: gz-44z45 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com 1-hi I =i—rinm Amn t-UAIn1 nC -i leTnnv Client: A uaNC PROJECT NAME:Annual �4 :1nal sis • REPORT NO: ADDRESS: 0 51 R.Pv &W� 6,wff CONTACT NAME: PO NO: REPORT TO: Don Williams PHONE/FAX: �' is , C�12,X.ff t15 COPY TO: email: 5arnwed By, 64 IZ--,N . 1,A C CAMCI C TVDC. I - I..FI. c - aar - - Sample Identification P Collection E a E a. r o a< _ r �0 ,, 20, z E a ao m z' PRESERVATION ANALYSIS REQUF-STE13 Date Time Tem m z n o x o ? x m a-u' C P G Sludge JC6 jZGb Nutrients/metals C P G G _ C P G G C P G G C P G G C P G G C P' G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: DateMme �. 2. l 2-l (q Ur 'Icy Temnnrsiurn a hnn 0--- [—A. w-_--`- '- - r<esample Keq Delivered By: Received By:- _ Date: %%i TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Beau Riviage P.O.# s atch Size (gallons). zu,000 Lbs. or Gallons Used: 200 IDS Material Used For Stabilization: lime Co U�Y' O U O O f/J > FL N v O N > a: O M O f/1 > a co M O Vl > n. M M O tlJ > a O cM O fA > a. n N O fA > a '[t N O Vl > a- N O UJ 2 n. aD O V) > a e- O . N 7 a. N O N > a. M O O N > a. O O O y 7 a M O O N 7 5- O 0 O o N C w o 0 Al C m 0 0 N C N 0 0 C E u� 0 N C 2 m .- 0 N C N 0 w C 2 v N 0 U) C 2 n N 0 w C o r� 0 w 7 s M � 0 W C w c� 0 W 7 C rn Cn 0 0 > C N v 0 0 > C in v 0 w > C U Q E O ,t O (o Mr*- M M O LM M M "T M -M M N M r M O M O N a0 N ti N (0LO N N q- N M N N N �- N O N O a0 O Lo ICT M N �- O I— LEWIS FARMSAND-LIQUID WASTE .INC. !Q CV go,'75- cn —6, 'N. Cl) -T Tto '; - lo ;; ..; , 6 . , E: rL rL. rL AL. a: E E EL TIC61, E -0) co N6 CV3: co -cr): Lo mj 0 Cl", CO00 to ul) C', CV: CV —u) 7c —o —— _ i c — :,�• —0 —* co Ci 7,c"—D _0) q 5 O. :,5 odo ci d oo C- 102; co", 00, . . . Ol 1 oz, .5 0.4 'D C14 0' Co I` (D ED C;4' Ci- LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Beau Riviage P.O.# Batch Size (gallons): 20,000 Lbs. or Gallons Used: 200 IbS Material Used For Stabilization: lime 00 L_ to t: N �t O CM O C) M M O M r• N N O N m O Co O M O Com o 0 m o N 00 �n ao N v N N o M M M co m rn N a in U O O O O O 1 O O O O O O O O O O 0 0 0 0 C 0 0 6 6 0 0 0 0 0 O N 0 N N 0 w N 41 N N N N N N �- 7 'a 7 7 C C C C C 7 _ > C > C > C > C 7 C to C 7 C > C > C ci a U r- E O 'IT CA Co t.- CO I LO v M N T- O CA 00 r­ CO Lo "Y Co N O CA 00 r` (0 � �t M N O Co Co m Co M CM M Co cM MN N N N N N, N N N N r- t- H LEWIS FARMS AND LIQUID'-WAS:TE INC. WQ':00004.55 ALKALINE STABILIZATION OF'WASTEWA.TER B10SOLIDS Facility Name: Beau Riviage: P1,04 Batch Size:(gellons):_ 28,000. Lbs::or'Galloim.Used:�6009bS. Material Used ForStabilizat m! f1ma. M M .'lQ`1 ..I_ '. � `VCV'. _ 0' • r . tD "T-- CO.N r ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Fauns and Liquid Waste, Inc. WQ Permit Number. WQ0000455 WWTP Name: Beau Rivage NPDES Number: NC0065480 Monitoring Period: From l/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and nitPrna*1wP nnrFnrm®rl- Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A onl) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray 131 Gamma Ray ❑ Pasteurization ❑ ...............................................: Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed Class B only indicate "Process to SignificantlySigniflcan#y Reduce Pathogens": Lime Stabilization M Air Drying ❑ Compos!!!jS ❑ JAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed Class A or Class B complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NumberOf d cee- Frequency ofAnalYsis Sample Type �' Tech- ' ue Minimum Geo. Mean axim Units Fecal Colifonm 2 x 10 to the 6th power per gram of total solids MPN CFu 1000 mpn per gram of total solid (dry weight) ISalmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .11071- Please indicate alternative nerfnrmPd. Alt.l (VS reduction) ❑ - Alt. 2 (40-day bench) [3 Alt. 3 (30-day bench) [3 r- JAIL 4 (Spec. Q2 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization [3 Alt 7 (Drying - Stable) '❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ® No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law,, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including flue and imprisonment." Wesley Wooten, President Prep arer N7d T' a (type or print) Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date - - *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) M1 ` DENR FORM PVRF 02T (12/2006) I LEWIS FARMS LANK APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 3, 2014 Brideeton Permit No. WQ0000455 0.46 % Solids Co." Parameter % Mg/Kg Dry Weight Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.856 8,563.000 17.126 Phosphorus 0.964 9,641.000 19.282 Potassium 0.531 5,305.000 10.610 PAN injected)* 0.277 2,772.260 5.545 PAN (surface)* 0.263 2,629.760 5.260 Ammonia Nitrogen 0.029 285.000 0.570 Calcium 3.051 30,514.000 61.028 Calcium Carbonate E . --- Magnesium 0.341 3,392.000 6.784 Sodium 1.670 25,429.000 50.858 Sulfur ___ ___ Nitrate N / Nitrite N --- 3.860 0.008 Barium ___ ___ Chloride ___ ___ Iron ___ ___. Aluminum --- 4,800.00 9.600 Arsenic --- 2.50 0.005 Cadmium --- 2.00 0.004 Chromium --- 15.000 --- Copper --- 464.00 0.928 Lead --- 22.00 0.044 Mercury --- 0.23 0.000 Molybdenum --- 5.00 0.010 Nickel --- 13.00 0.026 Selenium --- 5.00 0.010 Zinc --- 1,783.00 3.566 Environment 1, Inc. 440 A *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. pp:�.t�tv.ly��.,,CCi l'k,�rC.��J��/r't�tCrFyi 1C3'l.f F!Z,i:;C TOWN OF BRIDGETON HYDRO SERVICES & CONSULTING MR. KEVIN MULLINEAUX P.O. BOX 317 HAVELOCK ,NC 28532 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH (not to be used for reporting) 6.9 12/03/14 TRB 4500HB-00 Aluminum, (dry wt. basis), rng/kg 4800 12/18/14 LFJ EPA200.7 Arsenic (dry wt. basis), mglkg <2.5 12/18/14 MTM 3113B-04 Calcium (dry wt. basis), nrg/kg 30514 12/18/14 LFJ EPA200.7 Cadmium (dry wt, basis), mglkg 2 12/19/14 A M 3113B-04 Copper (dry wt, basis), mg/kg 464 12/18/14 LFJ EPA200.7 Chromium, T.(dr-y wt, basis),rng/kg 15 12/18/14 LFJ EPA200.7 Lead (dry weight basis), mg/kg 22 12/15/14 AITINI 3113B-04 Magnesium (dry wt. basis), mg/kg 3392 12/18/14 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.23 12/19/14 LIMM 245.1 R3-94 Nickel (dry wt. basis), mg/kg 13 12/18/14 LFJ EPA200.7 Potassium (cry wt, basis), mg/kg 5305 12/18/14 LFJ EPA200.7 Selenium (dry wt. basis), nrg/kg <5.0 12/15/14 AITAI 3113E-04 Sodium (dry wt. basis), mg/kg 25429 12/16/14 AITAI 3111E-99 Zinc (dry wt. basis), mg/kg 1783 12/18/14 WIM 3111B-99 Sodium Adsorption Ratio 1.2 12/22114 LFJ Total Solids, % 0.46 12/09/14 KKF 2540G-97 TI{N (dry wt.), mg/kg 8563 12/11/14 AKS 351.2 R2-93 Ammonia Nitrogen (dry wt.),mg/kg 285 12/09/14 KDB 350.1 R2-93 Phosphorus, T. (dry wt.), mg/kg 9641 12/11/14 KDB 365.4-74 Nitrate -Nitrite (dry wt.), mg/kg 3.86 12/10/14 KDB 353.2 R2-93 Molybdenum (dry wt. basis), nrg/kg 5 12/18/14 LFJ EPA200.7 ID#: 440 A DATE COLLECTED: 12/03/14 DATE REPORTED : 12/23/14 REVIEWED BY: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Town of Bridgeton P.O.# Batch Size (gallons): 11,500 +!- Lbs. or Gallons Used: Material Used For Stabilization: Lime OC L, C6 O N > a O M > a O u) > a O (n > M M O w 0- 1 O O q > a O cn > a O Vl 7 a O V) 7 a O tl) 27 a O u) 7 a O u) 7 M O tl) 7 M (0 O O V) 7 M O N 7 M O ) O N 7 C co 0 N 7 C rn 0 N 7 C N 6 y C n 0 41 7 C O N 7 C O N 7 C � N 0 U) C 2 N O N 7 C C) .0 U) 7 C oM 0 0 7 C co r) 0 U) 7 C 2 rn M0 O N 7 C Na 0 n 7 C Lvn 0 U) 7 C 2 U O NV O 0) CM 00 M r__ M CO M LO CM 1-t CM M M J04,; C N r CV NNN O 0) oD 1l- (0 n -ItM O i l _1 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: WQ Permit Number: I i WWTP Name: `T ,,, „� �l NPDES Number: J16O071 fn Monitoring Period: From /- J—/) To Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time)temp) ❑ 1 Alt B (Alk Treatment) ❑ 'Alt. (Prior Testing)❑ A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 131 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density L31 Alt. (2) Process to Significantly Reduce Pathogens Er If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ® Air Drying ❑ _ Composting ❑ 1 Aerobic Digestion ❑ Anaerobic Die' h n s o ❑ .............. If applicable to alternative performed (Class A or Class B) complete the following monito ng data: Parameter Allowable Level in in Sludge Pathogen Density Number of Excee- Frequency of Analysis Y Sample Type Analytical Tech - maue Minim Geo.,Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wei t) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei t Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt I (VS reduction) ❑ Alt. 2 (40-day bench) ❑Alt. 3 (30-day bench) ❑ Alt- 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ INo vector attraction reduction alternatives were performed ❑ CERT9ICATION STATEMENT (please check the appropriate statement) C'� "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." and Title (type of print) Land Applier Name and Title (if applicable)(type or print) Sigr aitum of Preparer* Date Signature of Land Applier (if applicable) Date *Prepaier is defined in 40 CFR Part 503.9(r) and 15A NCAC 27.1102 (26) DENR FORM PVRF 02T (12/2006) { LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 2, 2014 Castle Bay 1.31 % Solids 7.08 off Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight (% x 10,000) Pounds/Dry Ton __(MZ/Kg x 0.002) Nitrogen (TKN) 6.350 63,500.000 127.000 Phosphorus 1.750 17,500.000 35.000 Potassium 0.390 3,900.000 7.800 PAN (injected)* 1.953 19,534.400 39.069 PAN (surface)* 1.930 19,303.400 38.607 Ammonia Nitrogen 0.046 462.000 0.924 Calcium 2.820 28,200.000 56.400 Calcium Carbonate E . --- ___ Magnesium --- 2,350.000 4.700 Sodium --- 13,100.000 26.200 Sulfur -__ Nitrate N / Nitrite N --- 161.000 0.322 Barium ___ -__ Chloride ___ -__ Iron ___ Aluminum --- 3,920.00 7.840 Arsenic --- 7.58 0.015 Cadmium --- 7.58 0.015 Chromium --- 13.000 Copper --- 134.00 0.268 Lead --- 18.40 0.037 Mercury --- 1.53 0.003 Molybdenum --- 7.58 0.015 Nickel --- 13.70 0.027 Selenium --- 7.94 0.016 Zinc -- 1,060.00 2.120 Environmental Chemists, Inc. # 2014-14806 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % F Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Il y envirochem Q ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 .(252) 473-5702 NCDENR DWQ CERTIFICATE #94. DI.S CERTIFICATE #37729 Aqua America of North Carolina Date of Report: Dec 11, 2014 105 Hampstead Village BLDG 24-1 Customer PO #: - Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report #A: 2014-14806 Project ID: Castle Bay Lab ID Sample 1D: Collect DatelTlme Matrix Sampled by 14-36289 _ Site: Sludge 12/2/2014 8:25 AM Solid/Sludge Kirklyn Fields Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 3920 mglkg 12/04/2014 Arsenic EPA200.7 <7.58 mg/kg 12/03/2014 Cadmium EPA200.7 <7.58 mg/kg 12/03/2014 Calcium EPA 200.7 28200 mg/kg 12/03/2014 Chromium EPA200.7 13.0mg/kg 12/03/2014 Copper EPA200.7 134 mg/kg 12/03/2014 Lead EPA 200.7 18.4 mg/kg 12/03/2014 Magnesium EPA200.7 2360 mg/kg 12103/2014 Molybdenum EPA200.7 <7.58 mg/kg 12/03/2014 Nickel EPA200.7 13.7 mg/kg 12/03/2014 Potassium EPA200.7 3900 mglkg 12/03/2014 Selenium EPA 200.7 7.94 mg/kg 12/03/2014 Sodium EPA200.7 13100mg/kg 12/03/2014 Zinc EPA200.7 1060Ing/kg 12/03/2014 Ammonia Nitrogen EPA350.1 462 mg/kg 12/07/2014 Total Kjeldahl Nitrogen (TKN) EPA 3512 63500 mg/kg 12/10/2014 Nitrate+Nitrite-Nitrogen EPA353.2 161 mg/kg 12/09/2014 Total Solids (%) SM 2540 B 1.31 % 12/06/2014 pH SM 4500 H B 7.08 units 12/05/2014 Total Phosphorus SM 4540 P F 17500 mg/kg 12/10/2014 Mercury SW8487471B <1.53mg/kg 12/05/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Ohl ti Report#:: 2014-14806 Page 1 of 1 ! mington ENVIRONMENTAL CHEMIST'S, INC OFFICEt 10i392-02 3i1FAX910-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info®onvironmentalchemists.com P ni 1 Ce%T1f1Al AA1r% f%UAn11 nC ^11@Tf9rav/ Client: A uaNC PROJECT NAME: Annual Sludge Analysis qs EPORT NO: 14- ADDRESS: gg 91 {tign� C�y'C P CONTACT NAME: ONO: JLD REPORT TO: Don Williams PHONE/FAX: p� AV - 9- Kctq3 COPY TO: email: 7+amp1aC1 t3V: I(- "(/✓l Fei /a° S SAM01 1: TVDD• 1 = L,Fl..o..4 = -. tul.. ..a iai -- SAN 11 --r _ �a___� nw _ Identification Collection 01 W - rfi r m C d .0 xf 1r W0 m PRESERVATION ION NASample LYSIS REQUESTED Date Time Temp L, a U 00 Sludge C P VC Nutrients/metals 1-a-f $li�S � G C P G G C P G G C P G G C P G G C P G C G P G G C P G G C P IT G G Transfer Relinquished By: Date/Time Received By- Date/Time 9. 2. T,n... r...,...6........L..... �� mod. s _ ---•- --- 1 -1_-- - AUVWJJ404• - r%Wj •L6a: Kesamp Delivered By: _ 1 ,y-t��V�`e Received By: L. Date Comments- i Time: LEWIS FARMS AND LIQUID WASTE, INC. WO 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Castle Bay P.O.* Batch Size (gallons): 16,000 Lbs. or Gallons Used: 500 LBS Material Used For Stabilization: lime MENEM ME'N'RE, MENEM o L_ U - V' O > a N V O > a - C7 O > a O C`') O > a co C7 O 7 a O M O > a r� N O > a 't N O > a N O 7 a W O 7 a to �"' O 7 a N O a CA O O 7 a CO O O 7 a M O O 7 a O oM O o N m O 0 U1 rn O 0 fp N 0 y 2 �n '2 0 M O s- 0 Ul 2 N 0 V) 2 v N 0 01 2 n N 0 N 2 O M 0 N 2 � ch 0 fd 2 co M o W rn CM O N N V' o Vl u� a O w 2 U Nis O d O M 00 M r- M (O M LO M "' C'7 Ch M N M �- M O M CA N 00 N f� N O N Cn N v N C'7 N N N r- N O Nr- O O I` CO Lp M N r O H ---- —_'J G) (M coo m Aol. C! to cl,..l I 1. T .. ......... ----... .................. _____.........._--_ WQ 0000455° ALKA'UIVE STABIL:IZATiON' OF WAS°TEUYATER BIOSOLIDS Faclllty Name: ::Castle='Bay: Batch Size (gallons): 1.6,000, Lbs. or Gailons.Used.c 5Ob -LBS Material::Used For. Stabiilzation:. LilY1@. IAA, :N " "Cl.-':,Cp M: =M` MM .0. 'h '.'Q :r-.' -OD In N O) f0 M`•' M.: 'tp: . 07. i N. T ::, c0 tl' ti, O,-W .. °° .. N', �n �'� " C �C"�.,C ,M C''; C�., 'O:• O ;O' .C7 C� 'C,- �. ;O' O,; `G'- O. -C"�':,C': '.o., 'C1 .'� b � :O: :O_. .G' Ci'. ��O :O,'. :'C"'=0 :.� .:.� tlx: tA� N "' '.7.:'7.�.'. N :. 'W i/1' N '.fA' ^"N N ' � Ol All ' Vl � Vl' -G �. tll ' O- . _,, ''Vl y .N:,• O) ::: 'tll' N''. .O m -. tl! " tl):. .'N" .N �:M-�- W �'N , ,' ...C:. C,. :C...C,., .. C,. :'C.:'CC. C-C C'.'CtG• t'. C .a::a.'a"sa`'a.'a:;a n: :`a.'n.: a:: n`'."a n., IL; .'. ,g:.;: :_�.':2_. "` ''.�..' . ice" -(O 1p' :'Q" .M `N :s.`. CflSO'"tb 'ti `.'M M 'M `M M. M �.M' c4 :M M'N;'N N ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Castle Bay NPDES' Number: WQ0018755 Monitoring Period: From 1/l/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra [3Gamma Ea ❑ Pasteurization ❑ Class B: JAlt. (1) Fecal Density ❑ Alt. (2) Process to SignificantlySignificangy Reduce Pathogens If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Path ens": Lime Stabilization ® Air Drying ❑ Com ostin ❑ Aerobic Digestion ❑ Anaerobic Digestion estio n ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- deuces Frequency of Analysis Sample Type Analytical' T�h_ i ue MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power perof total solids MPN C>:U 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry wei t vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ LAlt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL lNo 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 8 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified, personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Wesley Wooten, President Preparer N e d Title a or print Signature Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM ' RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: May 29, 2014 Clarkton 0.23 % Solids d Qd .,A Permit No. WQ0000455 >marameter A °Io: j ; Mg/Kg`Dry Weight I'ouindlDry Ton Nitrogen (TKN) 14.000 140,000.000 280.000 Phosphorus 8.260 82,600.000 165.200 Potassium 0.804 8,040.000 16.080 PAN (injected)* 8.002 80,020.100 160.040 PAN (surface)* 7.915 79,148.600 158.297 Ammonia Nitrogen 0.174 1,743.000 3.486 Calcium 3.800 38,000.000 76.000 Calcium Carbonate E . --- ___ --- Magnesium --- 4,570.000 9.140 Sodium --- 18,800.000 37.600 Sulfur -__ ___ Nitrate N / Nitrite N --- 36,800.000 73.600 Barium _ __- --- Chloride ___ ___ Iron --- --- Aluminum --- 8,170.00 16.340 Arsenic --- 37.00 0.074 Cadmium --- 37.00 0.074 Chromium --- 37.000 --- Copper --- 288.00 0.576 Lead --- 37.00 0.074 Mercury --- 3.07 0.006 Molybdenum --- 37.00 0.074 Nickel --- 37.00 0.074 Selenium --- 37.00 0.074 Zinc --- 1,870.00 3.740 0 Environmental Chemists, Inc. # 2014-06253 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. V LEWIS FARMS WQ0000455 Clarkton WWTP Oa 05/29/14 13,254 4.1223 05/29/14 7,273 3.8617 05/29/14 8,731 3.9411 05/29/14 13,542 4.1317 05/29/14 5,512 3.7413 05/29/14 3,279 3.5157 05/29/14 11,966 4.0779 Total 1 27.3918 Average 1 3.9131 Geometric Mean jX'7 Fecal Coliform MPN / gram Geometric Mean of Less than 2,000,000 meets Class B - Alternative 1 Pathogen Reduction requirement. Environmental Chemists, Inc.. f 1envirochem 6602 Windmill Way • Wilmington, NC 28405 (910)392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of Clarkton Date of Report: Jul 16, 2014 PO Box 307 Customer PO #: Clarkton NC 28433 Customer ID: 08100292 Attention: Alton Boswell Report #- 2014-06253 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15103 Site: Aeration Basin 5/29/2014 10:40 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Chlordane SW 846 Method 80818/3510 <0.005 mg/L 06/05/2014 Endrin SW846 Method 8081 BI3610 <0.00005 mg/L 06/05/2014 Heptachlor SW 846 Method 6081B13510 <0.00005 mg/L 06/05/2014 ` Heptachlor epoxide SW 846 Method 8081 B13510 <0.00005 mg/L 06/05/2014 Lindane' SW846Method 8081Bf3510 <0.00005 mg/L 06/05/2014 Methoxychlor SW 846 Method 8081B13510 <0.00005 mg/L 06/05/2014 Toxaphene SW 846 Method 8081 B13510 <0.005 mg/L 06/05/2014 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.05 ing/L 06/04/2014 2,4,5-Trichlorophenol (TCLP) r SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 2,4,6 Trichlorophenol (TCLP) SW 846 method 8270/3610 <0.05 mg/L 06/04/2014 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 Cresol (TCLP) SW 846 method 827013510 <0.05 mg/L 06/04/2014 Hexachloro-1,3-butadiene (TCLP) SW 846 method 8270MIO <0.05 mg/L 06/04/2014 Hexachiorobenzene (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 Hexachloroethane (TCLP) SW846 method 827013510 <0.05 mg/L 06/04/2014 m + p-Cresol (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 o-Cresol (TCLP) SW 846 method 8270/3510 <0.05 mg/L 06/04/2014 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.25 mg/L 06/04/2014 Pyridine (TCLP) SW846method 827o13510 <0.05 mg/L 06/04/2014 2,4,5-TP SW848 Method 8161A <0.0003 mg/L 06/0912014 2, 4-D SW846 Method 8151A <0.0003 mg/L 06/09/2014 1,1-Dichloroethylene SW846 Method 826015030 <0.01 mg/L 06/18/2014 1,2-Dichloroethane SW846Method 826015030 <0.01 mg/L 06/18/2014 Benzene SWM Method 8260/5030 <0.01 mg/L 06/18/2014 Carbon Tetrachloride SW846 Method 8260/5030 <0.01 mg/L 06/18/2014 Report#.: 2014-06253 ' i Page 1 of _i envirochem sr� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910)392-0223(Lab) 0 (910)392-4424(Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 NCDENR. DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town .of Ctarkton Date of Report: Jul 16, 2014 PO Box 307 Customer PO #: Clarkton NC 28433 Customer ID: 08100292 Attention: Alton Boswell Report #: 2014-06253 Project ID: Sludge Chlorobenzeine SW046 Method 826015030 <0.01 mg/L 06/18/2014 Chloroform Sw846 Method 8260/5030 <0.01 mg1L 06/18/2014 Methyl ethyl ketone Sw846 Method 8260/6030 <0.05 mg/L 05/18/2014 Tetrachloroethylene Sw846 Method8260/5030 <0.01 mg/L 06118/2014 Trichloroethylene Sw846 Method 8260/5030 <0.01 mg/L 06/18/2014 Vinyl Chloride SW846 Method 626015030 <0.01 mg1L 06/18/2014 RCI Cyanide EPA 335.4 <0.130 mg/kg 06/04/2014 pH SM 4500 H B 4.94 units 06/05/2014 Sulfide SM 45DD S D <0.260 mg/kg 06/04/2014 Ignitability SW 846 method 1010 >212 OF 06/0-6/2014 Sludge Residuals Aluminum EPA200.7 8170 mg/kg 06/1612014 Arsenic EPA 200.7 <37.0 mg/kg 06/03/2014 Cadmium EPA200.7 <37.0 mglkg 06/03/2014 Calcium EPA 200.7 38000mg/kg 08/09/2014 Chromium EPA200.7 <37.0 mg/kg 06/0312014 Copper EPA2.00.7 288mg/kg 06/03/2014 Lead EPA200.7 <37.0 mglkg 06/03/2014 Magnesium EPA200.7 4570 mg/kg 06/09/2014 Molybdenum EPA 200.7 <37.0 mg/kg 06/03/2014 Nickel EPA200.7 <37.0mg/kg 08/0312014 Potassium EPA200.7 8040 mg/kg 06/09/2014 Selenium EPA200.7 <37.0 mg/kg 06/03/2014 Sodium EPA200.7 18800 mglkg 05/17/2014 Zinc EPA 200.7 1870 mg/kg 06/03/2014 Ammonia Nitrogen EPA350.1 <1743 mg/kg 06/05/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 140000 mg/kg 06110/2014 Nitrate+Nitrite-Nitrogen EPA353.2 36800 mg/kg 06/11/2014 Report #:: 2014-06253 Page 2 of 4 p . 4 ]Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Pax) sM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. Dl S CERTIFICATE #37729 M Town of Clarkton Date of Report: Jul 15, 2014 PO Box 307 J Customer PO #: Clarkton NC 28433 Customer ID: 08100292 Attention: Alton Boswell Report #: 2014-06253 Project ID: Sludge Total Solids (%) SM 2540 B 0.23 % 05/30/2014 Total Phosphorus sM4500PF 82600'mg/kg 06/11/2014 Mercury Sw807471B 3.07mg/kg 06/09/2014 TCLP Metals Arsenic EPA200.7 <0.100mg/L 08/03/2014 Barium EPA20o.7 <0.100 mg/L 06/03/2014 . Cadmium EPA200.7 <0.100 mg/L 06/03/2014 Chromium EPA200.7 <0.100 mg/L 06/03/2014 Lead EPA 200.7 <0.100 mg/L 06103/2014 Selenium EPA200.7 <0.100 mg1L 06/03/2014 Silver EPA200.7 <0.100 mg/L 06/03/2014 Mercury EPA 245.1 <0.002 mg/L 06/04/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15104 Site: # 1 5/29/2014 10:43 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2640 B 0.83 % 05/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 13254 MPN/g 05/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15105 Site: # 2 5/29/2014 10:46 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed 1z Total Solids (%) SM 2640 B 1.10 % 05/30/2014 Fecal Density SM 0221C E MPN 24 hr 503, 7273 MPN/g 05/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by a 14-15106 Site: # 3 i 5/29/2014 10:51 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.26 % 05/30/2014 Fecal Density SM92210EMPN 24hr503 8731 MPN/g 05/30/2014 Report #.: 2014-06253 Page 3 of 4 _1 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 © (910)392-0223 (Lab) • (910)392-4424 (Fax) s 710 Bowsertown Road = Manteo, NC 27954 (252)473-5702 ANALYTICAL &CONSULTING - CHEMISTS NCDENR: DWQ CERTIFICATE #94. DTS CERTIFICATE #37729 Town of Clarkton Date of Report: Jul 15, 2014 PO Box 307 Customer PO #: ,7 Clarkton NC 28433 Customer 1D: 08100202 t Attention: Alton Boswell Report #: 2014-06253 Project ID: Sludge Lab 1D Sample ID: Collect Daterrime Matrix Sampled by 14-15107 Site: # 4 6/29/2014 10:54 AM Solid/Sludge Alton Boswell Test S Method Results Date Analyzed Total Solids (%) SM 2540 B 0.96 % 05/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 13542 MPN/g 05/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15108 Site: # 5 5/29/2014 10:58 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1,27 % 05/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 5512 MPN/g, 05/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15109 Site: # 6 5/29/2014 11:04 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.22 % 05/30/2014 -- , Fecal Density SM 9221C E MPN 24 hr 503 3279 MPN/g 05/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-16110 Site: # 7 5/29/2014 11:08 AM Solid/Sludge Alton Boswell Test Method Results Date Analyzed Total Solids (%) SM 2540 s 1.17 % 05/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 11966 MPN/g 05/30/2014 Comment: Results reported on a d weight basis. Reviewed by: Report #:: 2014-06253 1 Page 4 of 4 • - t Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 hAl ! LP-TIA\I A \IR "A 1►J wr w■ •e•.�+w.w 6602Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: Town of Clarkton . ,t,„� VI VVVIVY PROJECT NAME: Annual Sludge REPORT NO:S-3 ADDRESS: CONTACT NAME: PO NO: REPORT TO: Alton Boswell, ORC PHONE/FAX: COPY TO: lemail. Sarnnlarl ku- A Sample Identification p Collection a a M .2- COLv ;, `oa 11111UCI1{, d ` = ocn V- -- a m ma z alrluent, PRESERVATION vv = irven, o i = stream, W = Soil, SL = Sludge, Other: - ANALYSIS REQUESTED Date Time Temp z a o M o x c o a w Sludge SL`/n 3 Full TCLP, RCI, Nutrients/metals fecal density, %TS - G - C G 2) fecal density, %TS (b G Q 9 4 S1U& Sr67 fecal density, %TS fecal density, %TS, ® G 5) 6) y d 9 fecal density, %TS fecal density, %TS fecal density, %TS C G 0 LAY c G I C G G G C P G G Transfer 2. Temperature when Received: Accepted: Delivered By Received Comments: me Received By: Date/Time mple R ques ed• ate_, 5 ! Time: �_ TURNAR UND. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP'Name: Town ofClarkton NPDES Number: NCO21610 Monitoring, Period: , From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level sachievo.i and al+orn4.;— - -r ......A Class A: Alt. A (time/temp) ❑ r..Y. uw�..Y tJYIV..II{4Y• Alt B (Alk Treatment) p Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) I - Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost DI Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ GammaLRa ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed Class B only) indicate "Process to Si niiicantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting, ❑ Aerobic Digestion ❑ Anaerobic tc Digestion on . If applicable to alternative perforwed Class A or Class B) complete the flowing..monitoring data: Parameter Allowable Level Pathogen DensityNumber m O° Frequency Sample T ti in Sludge ee deuces of Analysis Type Tech - Minimurr Geo. Mean Maximurr Units ; ue 2 x10 to the 6t h power MPN 3,279 .8,187 13,542 MPN/g 0 Annual Grab SM 9221 CE per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ AIt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7,(Drying -Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ !'VDTrtr-n'A:rrTINIV cgn-.•. Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑ t.Ll\L11'14Y111V111 0JL tilr tvir,i, 1 tptease cneCK ire appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed.to ensure that qualified personnel properly gather and evaluate the information used to determine that the.pathogen.and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and' imprisonment " Alton Boswell, ORC tl &7L `ram,fl Prep Nam nd ra or print) Land App er n itle (if applicable)(typ or, print) Signature of Prepay Date Signature of Land Applier (if applicable) Date *Preparer, is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) i LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 1, 2014 Dolphin Bay Permit No. WQ0000455 2.16 % Solids F 71 .,u Parameter % JMg/Kg Dry Weight (% x 10,000 Pounds/Dry Ton M /K x 0.002 Nitrogen (TKN) 5.830 58,300.000 116.600 Phosphorus 1.740 17,400.000 34.800 Potassium 0.402 4,020.000 8.040 PAN (injected)* 1.796 17,956.500 35.913 PAN surface)* 1.771 17,714.000 35.428 Ammonia Nitrogen 0.049 485.000 0.970 Calcium 2.520 25,200.000 50.400 Calcium Carbonate E . --- ___ Magnesium --- 2,660.000 5.320 Sodium --- 5,650.000 11.300 Sulfur ___ -__ Nitrate N / Nitrite N --- 127.000 0.254 Barium ___ -__ Chloride --- ___ Iron _-_ --- Aluminum --- 3,500.00 7.000 Arsenic --- 3.89 0.008 Cadmium --- 3.89 0.008 Chromium --- 11.400 --- Co per --- 427.00 0.854 Lead --- 25.90 0.052 Mercury -- 0.93 0.002 Molybdenum --- 3.98 0.008 Nickel -- 11.90 0.024 Selenium -- 7.96 0.016 Zinc -- 731.00 1.462 Environmental Chemists, Inc. it 2014-14770 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % F Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910)392-0223(Lab) • (910)3924424(Fax) 710 Bowsertown Road • Manteo, NC 27954 (252).473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Aqua America of North Carolina Date of Report: Dec 11, 2014 105 Hampstead Village BLDG 24-1 Customer PO #: Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report M 2014-14770 Project ID: Dolphin Bay Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-36206 Site: Dolphin Bay 12/1/2014 2:00 PM Solid/Sludge Kirkiyn Fields Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 3500 mg/kg 12/04/2014 Arsenic EPA 200.7 <3.89 mg/kg 12/03/2014 Cadmium EPA 200.7 <3.89mg/kg 12/03/2014 Calcium EPA20o.7 25200 mg/kg 12/03/2014 Chromium EPA 200.7 11.4mg/kg 12/03/2014 Copper EPA 200.7 427 mg/kg 12/03/2014 4 Lead EPA 200.7 25.9 mg/kg 12/03/2014 Magnesium EPA 200.7 2660mg/kg 12/03/2014' Molybdenum EPA 200.7 3.98mg/kg 12/03/2014. Nickel EPA 200.7 11.9 mg/kg 12/03/2014 Potassium EPA200.7 4020mg/kg 12/03/2014 Selenium EPA200.7 7.96 mg/kg 12/03/2014 Sodium ePA2o0.7 5650 mg/kg .12/03/2014 Zinc EPA 200.7 731 mg/kg 12/03/2014 Ammonia Nitrogen EPA350.1 485 mg/kg 12/08/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 58300mg/kg 12/08/2014 Nitrate+Nitrite-Nitrogen EPA 353.2 127 mg/kg 12/09/2014 Total Solids (%) SM2640a 2.16 % 12/01/2074 pH sM4s00It s J 6.71 units 12/05/2014 Total Phosphorus SM 4500 P F 17400 mg/kg 12/09/2014 Mercury sways 7471B <0.926 mg/kg 12/05/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report#:: ' 2014-14770 Pagel of 1 6602 ay ndmill mington ENVIRONMENTAL CHEMISTS, I N C OFFICE: 9 0 392-022311FAX 910- 92-44245 Analytical & Consulting Chemists , NCDENR: DWQ CERTIFICATION'# 94 NCDHHS: DLS CERTIFICATION # 37729 info@onvironmer talchemists.com COLLECTION AND CFi I OF CU TODY Client: AquaNC PROJECT NAME: A AnAuLrYSludge Ana"Iv J s REPORT NO: — !1— / ADDRESS: CONTACT NAME: PO NO: eallwdsfeok REPORT TO: Don Williams PHONEIFAX• COPY TO: email: va111pl a oy. Sample Identification k /. Collection SAMPLE -0• N a i; q c TYPE: C C9 o n "'" I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: c C '� PRESERVATION _ ci m .. —°� E m a g w ANALYSIS REQUESTED " 3 z = _ _ o Date Time Tempo Sludge C P Nutrients/metals 1,2-f / ,+,00 G C P G G C P G C G P G G C P G G C P G G J C P G C G P G G C P I G G _T1 Transfer Relinquished By: DateMme Received By: Daterrime 2. •--•..r..•.....•.. •••••,•• .�aV�I��iY. rncutspLau: KeJ@C R@sample Requested: Delivered By: Received By: --Date: _ r Time: ° Comments: TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Dolphin Bay P O # Batch size (gallons): 4,000 Lbs, or Gallons Used: 150 Ibs LEWIS FARMS AND LIQUID WASTE, INC. Q 0000455 ALKALINE STABILIZATION OF WASTEWATER BIO SOLIDS Facility Name: Dolphin Bay P Q # Batch Size (gallons): 4,000 Lbs. or Gallons Used: 150 Material tlsarl F.,r Q+�tirr—+;,,... I �_ • • . • • • p` ID M LL o N a 0 N n. 0 N a M4!,60: o `a ti a` a a o aw o d o 0 o Oo U o N M c'n ('7 m M Ch O N N N N N N N N N co 0 7 o �`ri, q N m m o 0 0 j N 41 o '✓1 m ci N v v o 0 p Facility Name: Dolphin Bay P.O.# Batch Size (gallons): 4,000 Lbs. or Gallons Used: 150 lbS __ _. Matarial IIcnA C... c � O u' U 4 o s (L /)N LL Q. V) n_ T a d IL 2 9 izD �r o) M M ('h Lo M -4- Co M N ON N N N N N N N Vh aD ti � O M CO Q) O 7 4) UI N N V) 4) C C C C C C C C C C C = O M 00 V' M N CD O N N r t WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLI®S Facility Name: Dolphin Batch Size (gallons): Bay P # 4,000 Lbs. or Gallons Used: 150 Ibs Material Used For Stabilization: Lime >12 H Corr.p Corrected 2 Hour pH 24 Hour pH Operato PH Temp C Time Con". Corrected Corr. Corrected Initials H Temp C Factor+ pH p p Factor pH Time pH Temp Factor+ pH Time 12.83 22.4 -0.09 12.74 9:40 12.71 22.1 -0.09 12.62 11:55 JMF Date 6/30/2014 Initial pH H TempC Corr. Corrected Factor + pH Time 6.81 20.5 -0.15 6.66 9;20 `O it- r O a V O 7 on. C7 O > a M o > a M CO 7 a CO a N O O a N O 7 a N 0 � a ems- O 7 a ems- O 3 a � O > a O O > L O O > L O O 7 L O o N C 2 0 Ci N C o o N N 0 O O a U H MY)M m � �`'� N N N N N N N N N CVO m O O O O Cl)M CJ N O N m O Ui M O v O w O Z LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WAS TEWATER BIOSOLIDS Facility Name: Dolphin Bay p # Batch Size (gallons): 4,000 Lbs. or Gallons Used: 150 Ibs Material Used For Srahtu��r ,• I ir„o V h O M (O O O o Ci Gj O O o Q 0000455 i. STABILIZATION i aTER BIOSOLIDS Facility Name: Dolphin Bay P.O.# Batch Size (gallons): 4.000 fibs. or Gallons Used: 150 IbS ®®11Gi�L'uii�:1��® • • Material Used For Stabilization: Lime U OC�-{-a` n o 7 N V O J M O rnTC:3:3 M O a M 6 M O d N O > N O > aa O 7 6 7 6MM D d 7 n.�no #,C, 3 7O V' u� cri w M r-- M co CO to M M M Co Co N N r. N N N N � � h- CD U7 V' Co N c- O O, n O t L R OO D Facility Name: Dolphin Bay p 0 # Batch Size (gallons): 4,000 Lbs. or Gallons Used: 150 Ibs Material Used For Stahiiiyafinn- I imm InitialpH >12 • O L U p V O V} a V m O o N (n 7 n r�Oi M Ci Ci N N O o N n N N N 0 0 o N N N co N F O N eN- o N M O 0 N CO fh O O o C'] to (J! a- O M O o N �p O 0 N rn O o m N a a o N o N N M Ci o y N N Ci N (07 o In M 0 M 0 N M 0 v 0 s a C U c ♦- O Cr (A a0 M ('') (� Cp M M to C'7 eT' M N M M Ch �-- M O M N N ti CO N N Lo N N N N N NO � � ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Fanms and Liquid Waste, Inc. WWTP Name: Dolphin Bay Monitoring Period: From l/l/2014 To WQ Permit Number: WQ0000455 NPDES Number: NCO055107 12131/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: 7 Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogengs ❑ If applicable to alternative performed Class A on[ ) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternativeperformed Class B only) indicate "Process to Significantly Reduce Path ens": Lime Stabilization El Air Drying ❑ Com ostin ❑ Aerobic Di estion ❑ An aerobic Digestion s❑ If applicable to alternative perdformed (Class A or Class B) complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency r� of Analysis Sample p Type yti Tech - e Minimum Geo. Mean Maximurr Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per grain of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grans total solid (dry wei 6 t) Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative nerformed: Alt -I NS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ©No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met" ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements, have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer Nam and"I". le (type or print) %.s Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26) 1 DENR FORM PVRF 02T (12/2006) LEWIS.FARMS LAND APPLICATION PROGRAM RESIDUALS' ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 25, 2014 Hampstead Pines 1.77 % Solids 6.98' pH Permit No. WQ0000455 Parameter % JMg/KgDryWeightJ x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 5.950 59,500.000 119.000 Phosphorus 2.450 24,500.000 49.000 Potassium 0.347 3,470.000 6.940 PAN (injected)* 1.810 18,098.100 36.196 PAN (surface)* 1.794 17,935.100 35.870 Ammonia Nitrogen 0.033 326.000 0.652 Calcium 4.250 42,500.000 85.000 Calcium Carbonate E . --- __- --- Magnesium 2,250.000 4.500 Sodium 10,200.000 20.400 Sulfur ___ Nitrate N / Nitrite N 19.900 0.040 Barium Chloride -_ ___ Iron ___ Aluminum --- 2,000.00 4.000 Arsenic --- 4.07 0.008 Cadmium --- 4.07 0.008 Chromium --- 10.600 --- Copper --- 236.00 0.472 Lead --- 15.50 0.031 Mercury --- 1.02 0.002 Molybdenum --- 4.24 0.008 Nickel --- 11.60 0.023 Selenium --- 1 10.70 0.021 Zinc --- 1,020.00 2.040 Environmental Chemists, Inc. # 2014-14594 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 ® '(910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252)473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729 Hampstead Pines 1004 Bally Bunion Lane Burgaw NC 28425 Attention: J. Marty Fritz Date of Report: Dec 10, 2014 Customer PO #: Customer ID: 09010034 Report #: 2014-14594 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-35795 Site: Digester Sludge 11/25/2014 9:00 AM Solid/Sludge J. Marty Fritz Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7. 2000mg/kg 12/02/2014 Arsenic EPA 200.7 <4.07mg/kg 12/02/2014 Cadmium EPA 200.7 <4.07mg/kg 12/02/2014 Calcium EPA 200.7 42500 mg/kg 12/03/2014 Chromium EPA 200.7 10.6 mg/kg 12/02/2014 Copper EPA 200.7 236 mg/kg 12/02/2014 Lead EPA 2W.7 15.6 mglkg 12/02/2014 Magnesium EPA 200.7 2250mg/kg 12/03/2014 Molybdenum EPA 200.7 4.24 mg/kg 12/03/2014 Nickel EPA200.7 11.6 mg/kg 12/02/2014 Potassium EPA 200.7 3470mg/kg 12/03/2014 - Selenium' EPA 200.7 10.7 mg/kg 12/02/2014 Sodium EPA 200.7 10200mg/kg 12/03/2014 Zinc EPA 200.7 1020 mg/kg 12/02/2014 Ammonia Nitrogen EPA 350.1 326 mg/kg 12/04/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 59500 mg/kg 12/04/2014 Nitrate+Nitrite-Nitrogen EPA353.2 19.9mglkg 12/08/2014 Total Solids (%) sM 2540 B 1.77 % 12/01/2014 pH sM4500 H B 6.98 units 11/28/2014 Total Phosphorus sM 4500 P F 24500 mg/kg 12/05/2014 Mercury 5WM7471B <1,02mg/kg 11/26/2014 Comment: Results, except pH, reported'on a dry weight basis. pH reported on an as received basis. Reviewed by: .� Report #:: 2014-14594 Page 1 of 1 Sample Identification Tri-annual r. = r;mneni DATE ENVIRONMENTAL CHEMISTS, INC Sample Collection and Chain of Custody 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4424 Collection d ^ 5a� d PRESERVATION ANALYSLS at � o d fro o REQUESTED TIlVIE TEMP v z- 0 � c G P G P G P G I G TDS, Cl " TOC . Nitrate G G NOTICE — DECHLORINATION : Samples for Ammonia, TKN, Cyanide, Phenol, and Bacteria must be dechlorinated 0.2 ppm or less in the field at the time of collection. See reverse side for instructions. Transfer ' ' Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature w ken Received: Accepted: V Regete : Resample Request d: Delivered B Received By. RL, Date: j I Time: f7(� Comments: . LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility -Name: Hampstead Pines P.O.# Batch Size (gallons): 8,000 Lbs. or Gallons Used: Material Used For Stabilization: Lime VA no 11 - ��E- - M1��Islljrqm! EE EMENSEEMEMEEM REM o U � LL- Lo O N V' O ('7 O (0 M O co M O O ('7 O f� N O '7 N O N O a0 O 2 O N c- O O O O (O O O M O lO O 10 O 0 CO O O 0 O 0 N 0 in 0 m 0 N 0 v N 0 N 0 o t`7 0 M O co f") 0 rn C7 0 N V' 0 u� V O U N O O M 00 M ti M (O M LO M d M (M M N M M O M O N a0 N N O N LO N N M N N N r- N O N W 00 f1- (0 (O M N c- O I- l ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) G Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Hampstead Pines NPDES Number: WQ0022052 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved 9nd alternative nnrrnrmaAo Class A: Alt. A (time/temp) ❑ 1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density [31 Alt. (2) Process to Sig!'ficantly Reduce Pathogens If applicable to alternative performed _(Class B only) indicate "Process to Significant Reduce Pathogens": Lime Stabilization 21 AirDrying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Di e n stio If applicable to alternative performed Class. A or Class B complete the following monitorin data: Parameter Allowable Level in Sludge Pathogen Density' Number o Excee BencofAnalysis Frequency Sample Type Analytical Tech - MinimumGeo. Mean Maximuml Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal colifonn) Vectnr Attrartinn 3 WN per 4 grams �4otatsolid (dry weight) Reri..oF:.,.. licA Wt! Arn11m „n.f� Alt.I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑ rF.RTIFrr~ATrnty erA rVXNVMnr _....., a <: a-"•aaL' a� 1 kPl— %;,,CCK the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met." ❑ "I certify; under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) : "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Prepare*ofeparer* it a or print) SignaturDate Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nrun r�nu n\ /nr nnT /.non nun\ LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: September 15, 2014 Hampstead Town Center Permit No. WQ0000455 1.15 % Solids 7.32 pH Parameter % Mg/Kg Dry Weight x 10,0001_ Pounds/Dry Ton (Mg/K2 (Mg/K2x 0.002 Nitrogen (TKN) 2.290 22,900.000 45.800 Phosphorus 0.465 4,650.000 9.300 Potassium 0.442 4,420.000 8.840 PAN injected)* 1.809 18,086.400 36.173 PAN (surface)* 1.009 10,086.400 20.173 Ammonia Nitrogen 1.600 16,000.000 32.000 Calcium 1.460 14,600.000 29.200 Calcium Carbonate E . --- ___ --- Magnesium 2,490.000 4.980 Sodium 13,700.000 27.400 Sulfur _ Nitrate N / Nitrite N 16.400 0.033 Barium --- Chloride ___ --_ Iron --- Aluminum --- 1,790.00 3.580 Arsenic --- 7.13 0.014 Cadmium --- 7.13 0.014 Chromium --- 19.400 --- Copper --- 289.00 0.578 Lead --- 8.61 0.017 Mercury --- 0.35 0.001 Molybdenum --- 7.13 0.014 Nickel --- 12.30 0.025 Selenium --- 7.13 0.014 Zinc --- 4,630.00 9.260 Environmental Chemists, Inc. I1 2014-11404 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. i It Environmental Chemists, Inc. ' 6602 WindmillWay - Wilmington, NC 28405 © (910)392-0223 (Lab) a (910) 392-4424(Fax) 710 Bowsertown Road - Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37n9 Lewis Farms & Liquid Waste, INC. Date of Report: Oct 07, 2014 8155 Malpass Comer Road Customer PO #: Currie , NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2014-11404 Project ID: Hampstead Shopping Center Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14 27989 Site: Sludge 9/15/2014 2:10 PM Solid/Sludge .fay Baker Test Method Results Date Analyzed t Sludge Residuals Aluminum EPA 200.7 1790 mg/kg 09/24/2014 Arsenic EPA 200.7 <7.13 mg/kg 09/22/2014 Cadmium EPA 200.7 <7.13 mg/kg 09/22/2014 Calcium EPA 200.7 14600mg/kg 09/23/2014. Chromium EPA 200.7 19.4 mg/kg 09/22/2014 Copper EPA 200.7 289 mg/kg 09/22/2014 Lead EPA 200.7 8.61 mg/kg 09/22/2014 Magnesium EPA2W.7 2490 mg/kg 09/23/2014 Molybdenum EPA 200.7 <7.13mg/kg 09/22/2014 Nickel EPA 200.7 12.3mg/kg 09/22/2014 Potassium EPA 200.7 4420mg/kg 09/23/2014 Selenium EPA 200.7 <7.13 mg/kg 10/01/2014 Sodium EPA 200.7 13700 mg/kg 09/2V2014 Zinc EPA200.7 4630mg/kg 09/24/2014 Ammonia Nitrogen EPA 350.1 16000 mg/kg 09/22/2014 Total Kjefdahl Nitrogen (TKN) EPA 351.2 22900 mg/kg 09/19/2014 Nitrate+Nitrite-Nitrogen EPA 353.2 16.4 mg/kg 09/19/2014 Total Solids (%) sM 2546 B 1.15 % 09/16/2014 PH sM 4500 H B 7.32 units 09/16/2014 Total Phosphorus sM 4500 P F 4650 mg/kg 09/22/2014 Mercury swe4e 7471E <0.348 mg/kg 09/17/2014 r Comment: Results, except pH, r ported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report#:: 2014-11404 Page 1 of 1 • - ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 f-f%1 1 Cf%-rl^ U ALir\ f`LIAIAI Ac f+1 •L+-r0%r1V 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: PROJECT NAME: C-.4. fIEPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: 04,. Iemail: " d y yt. 4 • o Sampled BV: J SAMPI I: TVPR- I = Inflnan4 C: - Cfflnnh• W - ul..0 car - ea......-- c--n - � -11 n• - .. Sample Identification Collection E ,� m► N H a a , e E c7 8 c° 0 a ° Q1 " l2 - o W °0 QJ i PRESERVATION ----- -- ----- -- --••---...,,n.,, .....�.. ANALYSIS REQUESTED Date Time Temp z z =__ d o c C o ie w o C P C P G G C P G I G a C I P G I G C I P G I G C I P G I G C I P G I G C I P G I G C P G G C P G G Transfer Relinquished BY: Date/Time Received By: Datefiime 1. 2. _ Delivered By.- By: Received By: Comments: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Hampstead Town Center P.O.# Batch Size (gallons): 8000 +/- Lbs. or Gallons Used: Material Used For Stabilization: Dne ®® 1 1 • �_� �_� 1 1 • 1 11 � • � 1 1 � 11 �_�__ C L O U7 �1 tll 7 a N V (q 7 a W ('7 f/) 7 a O CM fp 7 a ri ('M (n 7 a O CM O N a I� N O V1 7 a "T N O tll 7 a N O (q 7 a 00 O (/1 a In O fn 7 a N O Ul 7 a O O O tll 7 a 0 O O fq 7 a M O O (n 7 a () 0 O O N C (O O o y C W O O N C N a N J C In O N J C O o N 7 C N O N 7 C 't N o tll J C 1� N O y 7 C O C? o N 7 C lh (n 0 4! 7 C (D 'D o N J C m - O N J G N a O p1 J C o tl1 7 C U n O d O M 00 Cl) M O M V71,C) M co c7 N M co O M CA N Co N !� N CO N N, N t7 N N N �— N O N O �— 00 — I-- — O — � — — M �— N — r O ANNUAL. PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit.Number. WQ0000455 WWTP Name: Hamstead Town Center NPDES Number: WQ0032115 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 62T .1106) - Please indicate level achieved and 21tern9tive nerfarmeri- Class A: Alt.' A (time/temp) ❑ I Alt B (Alk Treatment) ❑ r- Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs [3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 0.1 Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑! Gamma Ra ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Si nifica4tly Reduce Pathogens": Lime Stabilization El Air D*g ❑ CompostingCompostiqg JAerobic Digestion ❑, Anaerobic Digestion on El If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ° d cee Frequency of Analysis SampleAnalytical Type Th- nie e inimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) ❑? Alt. 2 (40-day bench) ❑1 Alt. 3 (30-day bench) 0 Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑' Alt. 6 (Alk. Stabilization El! Alt 7 (Drying - Stable) ❑: Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑, Alt. 10 (Incorporation) ❑j No vector attraction, reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) Ell "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify,. under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." John Pruitt, ORC Preparer Name (type or print) Land Applier am tle applicable)(type or print) Si�&e of Preparer* Date Signature of 1,AfApplier if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: -November 19, 2014 Hermitaee House 0.46 % Solids 7.58 nH Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.358 3,580.000 7.160 Phosphorus 0.234 2,340.000 4.680 Potassium 0.446 4,460.000 8.920 PAN (injected)* 0.254 2,544.590 5.089 PAN surface)* 0.252 2,522.740 5.045 Ammonia Nitrogen 0.004 43.700 0.087 Calcium 4.480 44,800.000 89.600 Calcium Carbonate E . --- --- Magnesium --- 2,260.000 4.520 Sodium - 96,300.000 192.600 Sulfur _ ___ --- Nitrate N / Nitrite N --- 1,440.000 2.880 Barium ___ Chloride ___ --- Iron ___ --- Aluminum --- 1,880.00 3.760 Arsenic --- 18.50 0.037 Cadmium --- 18.50 0.037 Chromium - 18.500 --- Copper --- 370.00 0.740 Lead --- 18.50 0.037 Mercury --- 3.91 0.008 Molybdenum --- 18.50 0.037 Nickel --- 23.00 0.046 Selenium --- 18.50 0.037 Zinc --- 813.00 1.626 Environmental Chemists, Inc. 4 2014-14356 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424.(Fax) sM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252)473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Hermitage House Rest Home Date of Report: Dec 04, 2014 4724 Castle Hayne Road Customer PO #: Castle Hayne NC 28429 Customer ID: 08110003 Attention: Kevin Woodward Report #: 2014-14356 Project ID: Sludge Lab ID Sample 1D: Collect Date/Time Matrix Sampled by 14-35232 Site: Sludge 11/19/2014 9:00 AM Solid/Sludge Kevin Woodward Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 1880mg/kg 12/02/2014 Arsenic EPA20D_7 <18.5 mg/kg 11/21/2014 Cadmium EPA200.7 <18.5 mg/kg 11/21/2014 Calcium EPA20D.7 44800 mg/kg 11/26/2014 Chromium EPA200.7 <18.5 mg/kg 11/21/2014 Copper EPA200-7 370mg/kg 11/24/2014 Lead EPA200.7 <18.5 mg/kg 11/2112014 Magnesium EPA200.7 2260 mg/kg 11/26/2014 Molybdenum EPA200.7 <18.5mg/kg 11/21/2014 Nickel EPA 200.7 23.0 mg/kg 11121 /2014 Potassium EPA2oD_7 4460mg/kg 11/26/2014 Selenium EPA20D_7 <18.5 mg/kg 11/21/2014 Sodium EPA200.7 96300 mg/kg 11/26/2014 Zinc EPA200.7 813 mg/kg 11/21/2014 Ammonia Nitrogen EPA350.1 43.7mg/kg 11/20/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 3580 mg/kg 11/28/2014 Nitrate+Nitrite-Nitrogen EPA353.2 1440 mg/kg 12/02/2014 Total Solids (%) SM 2540 s 0.46 % 11119/2014 pH SM 4500 H e 7.58 units' 11/20/2014 Total Phosphorus SM 4500 P F 2340 mg/kg 11126/2014 Mercury SWB46747i8 <3.91 mg/kg 11/26/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis Reviewed by: M&kAld& (A a >� Report #:: 2014-14356 Page 1 of 1 ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 C('11 I FrTInAI AM-) r14A1At ni: ri icTnnv 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@cnvironmentaiGhemists.com Client: Hermitage House Rest Home PROJECT NAME: Annual Sludge Analysis REPORT NO: ADDRESS: CONTACT NAME: Kevin Woodward PO NO: REPORT TO: Lewis Farms / Wesley Wooten PHONE/FAX: 910-622-4848 COPY TO: email: kevinwoc)dward5l_@gmaii.com Sampled Bv: Kevin Woodwnrr CAMDI D TVDC• ur — ur_n -- Sample Identification Collection a d A y m o E `o `o a _o` 0, " E W O m g z PRESERVATION ANALYSIS REQUESTED Date Time Temp i $ _ o 0 z 0 o w o Sludge X Nutrients, Metals JO G Transfer Relinquished By: Daterrime Received By- Dateifime 1. 2. pie Delivered By: Received Comments: —ASAP to Wesley Wooten ,Time: LEWIS FARMS AND LIQUID WASTE, INC. WWQ 0000455 ALKALINE STABILIZATION OF WASTEWATER B/OSOL1®S Facility Name: Hermitage House P.O.# Batch Size (gallons): 2,500 Lbs. or Gallons Used: 200 Lbs Material Used For Stabilization: Lime EMENNEMEN WIN -mom Ct " O L aON s®4i Mtl1 *Cl) N EL CD fn 7 a. Iy 0 7 a O N(� 7 a O !n 7 a C5 V7 7 a O N 7 u C7 N 7 a 0 Iq 7 na. L 0 N7 C0 CU 7 a b O onVI C � ow4} CC O dN CC a oNCfn t ONG 7 n C Ca Moo C;N5C M7Cy7 0O U �- N F- O r M M 0D M r- M CO Mn X) 'qr M M () () (� N N N N N N N N N N r Or 1 r r i ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms d L' 'd I'll an tqut ante, Inc. WQ Permit Number. WQ0000455 WWTP Name: Hermitage House NPDES Number: NC0051969 Monitoring Period: From To Pathogen Reduction 05A NCAC 02T .1106) -Please indicate level achieved and alternative performed: Class A: Alt. A (tinie!temp) ❑. Alt B (Alk •Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) [] Process to Further Reduce Fathogengs ❑ If applicable to alternative performed (Class :1 only) indicate "Process to Further Reduce Pathogens-. Compost ❑ Heat Drying ❑ 11eat Treatment ❑ Tltztmophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ I Alt. (?) Process to Sigmificantly Reduce Pathogens R1 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization C] Air Drying ❑ Coru ostin ❑. Aerobic Disestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data:* Allowable Level Pathogen Density um er o na ytica Parameter R`- Frequency Sample in Sludge Minimu Geo. Mean aximu Units dences ofAnalysis Type lech- 2 x 10 to the MPN nicue 6th po%vcr per gram of Fecal Ctiiifotm total solids CFU 1000 mpn per gram oftotal solid (dry Salmonclla bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) yscight) Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed: All.I (VS reduction) #EIA11t. 2 (40-day bench) ❑ Alt. 3 30-da bench( Y ) ❑ Alt. 4 (Spec. O, uptake)Att. 5 (14-Day Aerobic) lt. 6 (Alk. Stabilization ❑Alt 7 D in Stable(n' g'- ) ❑ Alt. 8 (Drying -Unstable) ❑Alt. 9 (Injection) lt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) J "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in ISA NCAC 02T .1 106and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." J. Marty Fritz (ORC lime stabilization) 4�?"Vt_y&npr Preparer Nam and Title (type or print) '�`''Land A Ii"� ``nd Title (ifappe or int) a ��� —ZO /f— ignature reparer* Date Signature of Land A lier a PP ( if applicable) ) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 19, 2014 House of Raeford Permit No. WQ0000455 Wallace Plant 0.76 % Solids 8.29 nH Parameter I % lMg[KgDryWeightr x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 1.820 18,200.000 36.400 Phosphorus 0.525 5,250.000 10.500 Potassium 1.210 12,100.000 24.200 PAN (injected)* 0.787 7,873.600 15.747 PAN (surface)* 0.744 7,440.600 14.881 Ammonia Nitrogen 0.087 866.000 1.732 Calcium 1.870 18,700.000 37.400 Calcium Carbonate E . --- -__ --- Magnesium --- 19,600.000 39.200 Sodium --- 33.200 Sulfur --- --- Nitrate N / Nitrite N --- 4. 000 0.148 Barium --- it.0000 _-_Chloride ___ ___ Iron --- ___ --- Aluminum --- 14,200.00 28.400 Arsenic --- 12.90 0.026 Cadmium --- 12.90 0.026 Chromium --- 12.900 --- Copper --- 241.00 0.482 Lead --- 12.90 0.026 Mercury --- 1.45 0.003 Molybdenum --- 12.90 0.026 Nickel --- 18.40 0.037 Selenium --- 12.90 0.026 Zinc --- 253.00 0.506 Environmental Chemists # 2014-14368 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. ® 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 437729 House of Raeford -Wallace Facility Date of Report: Dec 15, 2014 Post Office box 40 Customer PO #: 34239 Rose Hill NC 28458 Customer ID: 13030026 Attention: Wayne Benton, ORC Report #: 2014-14368 Project ID: Annual Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-35252 Site: digestor sludge 11/19/2014 10:40 AM Solid/Sludge jay baker/envirochem Test Method Results Date Analyzed Chlordane SW 846 Method 8081BWlo <0.05 mg/L 11/26/2014 Endrin SW 846 Method 80816/3510 <0.0005 mg/L 11/26/2014 Heptachlor SW 846 Method 808113/3510 <0.0005mg/L 11/26/2014 Heptachlor epoxide SW846 Method 808IBMIO <0.0005mg/L 11/26/2014 Lindane SW 846 Method 8081 B/3510 <0.0005 mg/L 11 /26/2014 Methoxychlor SW 846 Method 8081 613510 <0.0005 mg/L 11 /26/2014 Toxaphene SW 846 Method 8081 B13510 <0.05 mg/L 11 /26/2014 1,4-Dichlorobenzene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/25/2014 2,4,5-Trichlorophenol (TCLP) SW 846 method 8270135 1 a <0.050 mg/L 11/25/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 11/25/2014 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11 /25/2014 Cresol (TCLP) SW 846 method 827013510 <0.050 mg/L 11/25/2014 Hexachloro-1,3-butadiene (TCLP) SW B46 method 827013510 <0.050 mg/L 11/25/2014 . Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 11/25/2014 Hexachloroethane (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/25/2014 m + p-Cresol (TCLP) SW 846 method 627013510 <0.050 mg/L 11/25/2014 Nitrobenzene (TCLP) SW 846 method 8270/3510 <0.050mg/L 11/25/2014 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11/25/2014 Pentachlorophenol (TCLP) SW 846 method 8270/3510 <0.250 mg/L 11/25/2014 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 11 /25/2014 2,4,5-TP SW846 Method 8151A <0.003mg/L 12/01/2014 2,4-D SW846 Method 8151A <0.003 mg/L 12/01 /2014 1,1-Dichloroethylene SW846 Method 828015030 <0.01 mg/L 12/11/2014 1,2-Dichloroethane SW846 Method 8260/5030 <0.01 mg/L 12/11/2014 Benzene SW646 Method 826D/5030 <0.01 mg/L 12111 /2014 Carbon Tetrachloride SW846 Method 826015030 <0.01mg/L 12/11/2014 Report #:: 2014-14368 Page 1 of 3 Environmental Chemists, Inc. envirochem(910) 6602 Windmill Way • Wilmington, NC 28405 392-0223 (Lab) • (910) 392-4424 (Fax) srn 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 House of Raeford Wallace Facility Date of Report: Dec 15, 2014 Post Office box 40 Customer PO #: 34239 Rose Hill NC 28458 Customer ID: 13030026 Attention: Wayne Benton, ORC Report #: 2014-14368 Project ID: Annual Sludge - Chloroberizene SW846 Method 826015030 <0.01 mg/L 12/11/2014 Chloroform SW846 Method$260/5030 <0.01 mg/L 12/11/2014 Methyl ethyl ketone SW846 Method 826015030 <0.05 mg/L 12111/2014 Tetrachloroethylene SW846 Method 8260/5030 <0.01 mg/L 12111 /2014 Trichloroethylene SW646 Method 0260/6030 <0.01 mg/L 12/11/2014 Vinyl Chloride SW846 Method 826015030 <0.01 mg/L 12/11/2014 RCI Cyanide EPA335.4 <0.125 mg/kg 11/26/2014 pH SM 4500 H B 8.29 units 11120/2014 Sulfide SM 4500 s n <0.250 mg/kg 11 /25/2014 Ignitability SW 846 method 1010 >212 °F 11/21/2014 Sludge Residuals Aluminum EPA200.7 14200 mg/kg 11/26/2014 Arsenic EPA200.7 <12.9 mg/kg 11/21/2014 Cadmium EPA200.7 <12.9 mg/kg 11/21/2014 Calcium EPA200.7 18700 mg/kg 11/26/2014 Chromium EPA200.7 <12.9 mg/kg 11/21/2014 Copper EPA200.7 241 mg/kg 11/24/2014 Lead EPA 200.7 <12.9 mg/kg 11 /21 /2014 Magnesium EPA200.7 19600 mg/kg 11/26/2014 Molybdenum EPA200.7 <12.9 mg/kg 11/21/2014 Nickel EPA200.7 18.4mg/kg 11/21/2014 Potassium EPA20o.7 12100 mg/kg 11/26/2014 Selenium EPA200.7 <12.9mglkg 11/21/2014 Sodium EPA200.7 16600 mg/kg 11/26/2014 Zinc EPA200.7 253 mg/kg 11/21/2014 Ammonia Nitrogen i EPA350.1 866 mg/kg 1112012014 Total Kjeldahl Nitrogen (TKN) L_ EPA351.2 18200 mg/kg 11/28/2014 Nitrate+Nitrite-Nitrogen EPA353.2 74.0mg/kg 12/01/2014 Total Solids (%) SM2540 B 0.76 % 11/24/2014 Report*: 2014-14368 Page 2 of 3 Environmental Chemists, I Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road a Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENRc DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 House of Raeford -Wallace Facility Date of Report: Dec 15, 2014 Post Office box 40 Customer PO #: 34239 Rose Hill NC 28458 Customer ID: 13030026 Attention: Wayne Benton, ORC Report #: 2014-14368 Project ID: Annual Sludge Total Phosphorus SM4500PF 5250mg/kg 11/26/2014 Mercury SW8467471B <1.45 mg/kg 11/26/2014 TCLP Metals Arsenic EPA20o:a < A00 mg/L 12/02/2014 Barium EPA200.6 <0.100 mg/L 12/02/2014 Cadmium EPA200.6 <0.100 mg/L 12/02/2014 Chromium EPA 200.E <0.100 mg/L 12/03/2014 Lead EPA 200.8 <0.100 mg/L 1210212014 Selenium EPA200.8 <0.100 mg/L 12/02/2014 Silver EPA 200.8 <0.100 mg/L 12/02/2014 Mercury EPA 245.1 <0.0020 mg/L 11 /29/2014 Comment: Sludge residuals reported on a dry weight basis. RCI results reported on an as received basis. Reviewed by: Report #:: 2014-14366 Page 3 of 3 • ENVIRONMENTAL CHEMISTS, INC Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 !till I FCTlnN ANTI CI -LAIN M: [_I ICTnnV - 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentalchemists.com CLIENT: � - /��-��r �- �✓� rl c L PROJECT NAME: REPORT NO: 141" lr•{3G� ADDRESS: CONTACT NAME: PO NO: 3y2 3 REPORT TO: l.�I.c q /f e,.�^i s7 /�- L PHONE/FAX: COPY TO: email: Samaled Bv: l '=� a.r: ro c. SAMPLE TYPE: I = Influent. E = Effluent_ W = WPIL ST = Stream Sfl = An;l s1 = - nacho.. Sample Identification Collection = m a l°a' N h a E o s o c v c � r E " o w rn 3 z PRESERVATION v ANALYSIS REQUESTED D to Time Temp z °_ h "= o r Yo o o DI`Lfi�� As^ J1s- C P 3SL� x G I G G G C P G G C P G �G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. I CIIIIJmcitu1C va11ml Li 1 aeU: AL;;epieu: v ejec ea: Kesample Kue ted: Delivered By: J Received Bv: Date: 1174Time:_ Comments: TU N OUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace P.O.# Batch Size (gallons): 30,000 +/- Lbs. or Gallons Used: Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operato Date PH Temp C Corr. lFactor + Corrected p H Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time 'PH Temp C Corr. Factor + Corrected pH Time Initials 1/1/2014 7.10 11.0 -0.42 6.68 742 12.60 11.1 -0.42 12.18 809 12.57 11.3 -0.41 12.16 1009 12.52 12.0 -0.39 12.13 812 WB 1/8/2014 7.14 9.7 -0.46 6.68 730 12.78 9.8 -0.46 12.32 744 12.69 9.9 -0.45 12.24 944 12.51 10.1 -0.45 12.06 744 WB 1/16/2014 7.40 9.7 -0.46 6.94 654 12.80 10.1 -0.45 12.35 710 12.65 10.2 -0.44 12.21 910 12.62 10.5 -0.44 12.19 712 WB 2/7/2014 7.08 9.5 -0.47 6.62 650 12.69 9.7 -0.46 12.231 700 12.7 9.9 -0.45 12.25 900 12.541 10.1 -0.45 112.09 705 WB 2/23/2014 7.44 10.3 -0.44 7.00' 659 12.57 10.4 -0.44 12.13 712 12.68 11.1 -0.42 12.26 912 12.521 11.2 -0.41 12.11 712 WB 3/5/2014 7.33 14.0 -0.33 7.00 644 12.44 14.2 -0.32 12.12 700 12.46 14.4 -0.32 12.14 900 12.37 14.0 -0.33 12.04 700 WB 3/12/2014 7.45 14.1 -0.33 7.12 731 12.41 14.4 -0.32 12.09 744 12.45 14.5 -0.32 12.14 944 12.42 14.4 -0.32 12.10 744 WB 3/19/2014 7.30 14.2 -0.32 6.98 652 12.53 14.6 -0.31 12.22 708 12.55 14.7 -0.31 12.24 908 12.51 14.8 -0.31 12.20 708 WB 3/25/2014 7.38 14.3 -0.32 7.06 644 12.57 14.7 -0.31 112.26 702 12.61 14.9 -0.3 12.31 902 12.51 14.7 -0.31 12.20 702 WB 3/27/2014 7.40 14.9 -0.3 7.10 715 12.33 15.3 -0.29 12.04 732 12.48 15.4 -0.29 12.19 932 12.42 15.5 -0.29 12.14 732 WB 4/7/2014 7.45 15.1 -0.3 7.15 639 12.52 15.6 -0.28 12.24 648 12.42 15.6 -0.28 12.14 948 12.521 15.7 -0.28 12.24 648 WB 4/16/2014 7.10 15.7 -0.28 6.82 622 12.44 18.3 -0.2 12.24 636 12.48 18.4 -0.2 12.28 936 12.361 18.3 -0.20 12.16 636 WB 4/30/2014 7.28 16.0 -0.27 7.01 638 12.22 21.5 ' -0.11 12.12 655 12.46 21.6 -0.1 12.36 855 12.52 21.5 -0.11 12.42 655 WB 5/7/2014 7.44 17.7 -0.22 7.22 652 12.31 22.4 -0.08 12.23 709 12.35 22.5 -0.08 12.28 909 12.22 22.3 -0.08 12.14 709 -WB 5/14/2014 7.30 17.9 -0.21 7.09 710 12.20 23.2 -0.05 12.15 722 12.28 23.4 -0.05 12.23 922 12.17 23.5 -0.05 12.13 722 WB 5/21/2014 E734 17.9 -0.21 6.98 638 12.34 24.4 -0.02 12.32 651 12.36 24:5 -0.02 12.35 851 12.1 24.4 -0.02 12.08 651 WB 5/2s/2o1a 18.2 -0.2 7.14 617 12.18 25.3 0.009 12.19 629 12.25 25.4 0.012 12.26 829 12.12 25.4 0.01 12.13 629 WB C L N CJ � V O 7 N ' 1' O 7 O M O 7 O M O 7 M M O 7 O M O 7 n N O 7 V N O 7 N O 7 a0 O 7 � .-- O 7 N �- O 7 O) O O 7 (O O O Cl) O O 7 O o7 O O C co O O C rn O O C N O C �n O C co O C N O C v N O C n N O C O M O C c+7 q O C O q O C rn (M O C N C O C �n O C 0 a- a. a M a a a d a a a a. a M a 2 2 2 r-� 2� 2�� 2 Z. 2 2i 2 U C- N O d M M M M f- M M M L0 M VY co M M N co <- co O co M N Co N f` N Co N rr) N 'I N M N N N N O Nc- CA OO fl- CD to T co N O f- LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace Batch Size (gallons): 30,000 +/- Lbs. or Gallons Used: P.O.# Material Used For Stabilization: lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operator Date pH Temp C Corr. Factor + Corrected pH Time pH Temp C I Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time pH Temp C Corr. Factor + Corrected pH Time Initials 6/4/2014 7.32 25.3 0.009 7.33 753 12.10 25.3 0.009 12.11 807 12.2 25.4 0.012 12.21 1007 12.1 25.2 0.01 12.11 807 WB 6/11/2014 7.22 25.5 0.015 7.24 648 12.10 25.6 0.018 12.12 700 12.05 25.7 0.021 12.07 900 12.13 25.5 0.02 12.15 705 WB 6/18/2014 7.18 26.0 0.03 7.21 638 12.26 26.1 0.033 12.29 662 12.23 26.2 0.036 12.27 852 12.18 26.1 0.03 12.21 652 WB 6/25/2014 7.04 26.1 0.033 7.07 708 12.32 26.2 0.036 12.36 722 12.29 26.3 0.039 12.33 922 12.25 26.1 0.03 12.28 722 W B 7/2/2014 7.22 26.2 0.036 7.26 718 12.19 26.3 0.039 12.23 731 12.17 26.4 0.042 12.21 931 12.22 26.2 0.04 12.26 735 WB 7/9/2014 7.07 24.3 -0.02 7.05 703 12.411 24.5 -0.02 112.40 715 12.38 24.5 -0.02 12.37 915 12.34 24.4 -0.02 12.32 735 W B 7/15/2014 7.15 23.9 . -0.03 7.12 733 12.38 24.1 -0.03 112.35 742 12.42 24.2 -0.02 12.40 942 12.38 24.1 -0.03 12.35 742 W B 7/23/2014 7.27 23.4 -0.05 7.22 703 12.21 23.5 -0.05 112.17 714 _ 12.23 23.6 -0.04 12.19 914 12.18 23.3 -0.05 12.13 714 WB 7/29/2014 7.44 21.8 -0.1 7.34 653 12.28 22.0 -0.09 112.19 705 12.23 22.1 -0.09 12.14 905 12.241 21.9 -0.09 112.15 705 WB 8/6/2014 7.08 21.1 -0.12 6.96 603 12.37 21.3 -0.11 12.26 617 12.41 21.3 -0.11 12.30 817 12.4 1 21.1 -0.12 12.28 617 WB 8/13/2014 7.46 20.2 -0.14 7.32 633 12.19 20.4 -0.14 12.05 643 12.22 20.6 -0.13 12.09 845 12.181 20.5 -0.14 12.05 643 W B 8/19/2014 7.06 19.7 -0.16 6.90 753 1 12.311 19.9 -0.15 12.16 802 12.34:20.1 -0.15 12.19 1002 12.3 19.9 -0.15 12.15 802 WB 8/27/2014 7.42 17.2 -0.23 7.19 718 12.271 17.3 -0.23 12.04 731 12.35 17.5 -0.23 12.13 . 931 12.38 17.4 -0.23 12.15 731 1 WB 9/3/2014 7.1 15.9 -0.27 6.83 748 12.461 16.1 -0.27 12.19 800 12.4 16.2 -0.26 12.14 1000 12.37 16.1 -0.27 12.10 800 1 W B 9/10/2014 7.2 14.7 -0.311 6.89 733 12.54 14.9 -0.3 112.24 743 12.51 15.0 -0.3 12.21 945 12.4 14.8 -0.31 12.09 743 WB I9/17/2014 7.43 13.2 -0.351 7.08 1 805 12.49 13.5 -0.35 12.15 815 12.43 13.6 -0.34 12.09 1015 12.391 13.4 -0.35 12.04 821 1 WB LE222a] 6.99 12.9 -0.361 6.63 1 654 12.64 12.3 -0.38 112.261 705 12.6 12.4 -0.38 L12.22 905 12.541 12.3 -0.38 12.16 718 W B c V 16 O y 7 N y 7 O O N 7 CO O y 7 M O fA 7 O O N 7 h N O y 7 eh N O y 7 N O N 00 O N 7 O O fA 7 N_ O W 7 O O O y 7 CO O O N 7 M O O y O m O O N 7 C m O O Vl 7 C m O O N 7 C N o o j C � C 10 7 C O O 10 7 C N O &* 7 C •t N O m 7 C r- N o tq > C o m o (p > C cn m O N 7 C co m O y 7 C m O W 7 C V C N 7 C V' O In 7 C U C- E O d O M 00 OM ti M O M In M [r C'M co M M M M N 00 N 1*- N 0 N In N d' N M N N N r- N O N O � 00 �- ti O - LO �- d' � M e- N �- O r- H LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: House of Raeford / Wallace P.O.# Batch Size (gallons): 30,000 +/- Lbs. or Gallons Used: Material Used For Stabilization: Lime Initial pH >12 pH 2 Hour pH 24 Hour pH Operato Date pH Temp C Corr. Factor+ Corrected pH Time pH Temp C Corr. Factor+ Corrected pH Time pH Temp C Corr. Factor+ Corrected pH Time pH Temp C Corr. Factor Corrected pH Time Initials 10/1/2014 7.45 19.1 -0.18 7.27 645 12.52 19.2 -0.17 12.35. 700 12.54 19.3 -0.17 12.37 901 12.51 19.2 -0.17 12.34 715 WB 10/8/2014 7.36 18.9 -0.18 7.18 633 12.34 19 -0.18 12.16 648 12.36 19.1 -0.18 12.18 848 12.38 19.0 -0.18 12.20 648 WB 10/13/2014 7.42 18.7 -0.19 7.23 625 12.40 18.8 -0.19 12.21 642 12.45 18.9 -0.18 12.27 842 12.42 18.7 -0.19 12.23 642 WB 10/15/2014 7.21 18.4 -0.2 7.01 654 12.49 18.5 -0.2 12.30 715 22.51 18.6 -0.19. 12.32 915 12.48 18.6 -0.19 12.29 718 WB 10/29/2014 7.18 18.1 -0.21 6.97 647 12.38 18.2 -0.2 12.18 705 12.39 18.3 -0.2 12.19 905 12.34 18.3 -0.20 12.14 705 WB 11/5/2014 7.34 17.0 -0.24 7.10 630 12.52 17.2 -0.23 12.29 644 12.53 17.3 -0.23 12.30 844 12.44 17.4 -0.23 12.21 644 WB 11/12/2014 7.46 17.2 -0.23 7.23 652 12.48 17.3 -0.23 12.25 708 12.5 17.4 -0.23 12.27 908 12.39 17.3 -0.23 12.16 708 WB 11/19/2014 7.1 16.9 -0.24 6.86 622 12.49 17 -0.24 12.25 638 12.49 17.1 -0.24 12.25 838 12.44 17.1 -0.24 12.20 644 WB 11/30/2014 7.51 16.5 -0.26 7.26 635 12.32 16.7 -0.25 12.07 645 12.36 16.8 -0.25 12.11 845 12.34 16.8 -0.25 12.09 645 WB 12/3/2014 7.46 16.3 -0.26 7.20 647 12.37 16.4 -0.26 12.11 702 12.39 16.5 -0.26 12.14 902 12.3 16.6 -0.25 12.05 702 WB 12/14/2014 7.33 16.5 -0.26 7.08 650 12.42 16.6 -0.25 12.17 705 12.41 16.7 -0.25 12.16 905 12.37 16.7 -0.25 12.12 715 WB 12/14/2014 7.69 16.7 -0.25 7.44 645 12.47 16.8 -0.25 12.22 700 12.46 16.9 -0.24 12.22 900 12.41 17.0 -0.24 12.17 703 WB C L U L- O a N O 7 a O O 7 m O O a O 7 a C) 7 a O a C)O 7 m 7 m 00 O 7 a Lo O O a. N C)O 7 a 0) O 7 a M C)O O 7 M Cl) O O 0- C)W c) O C 2 (0 O O N C 2 Q) O O N C 2 _ o C O 4) C c0 .- C;'V' tl1 C N O w C C N O w C n N O U) C O M O w C (h M 0 N C co M O y C 0)N (i O y C O V1 C tf) V O N C U OLcc,))) M M t`O(nM M M M M M N M r- M O M d) N a0 t` (O (!7 � M N �- O M c0 ti (p lf) d' M N �- O'c1 �- F- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) )Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP-Name: Wallace-Chicken-Processing-Plwd 'NPDES-Number: NC0003344 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/tem) ❑ I Alt B (Alk Treatment) ❑I Alt. C (Prior Testin )❑ AIt.D (No Prior Test) ❑ Process to Further Reduce Pathogeny ❑ Iif applicable to alternative performed Class A on indicate "Process to Further Reduce Path ens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra ❑ Gamma Ra ❑ Pasteurization ❑ Class B: 7AIt (1) Fecal Density ❑ Alt. (2) Process to Si 'fica d Reduce Pathogens ❑ If a hd9b-le'to alternative performed (Class'B only)-indicate'"Process to'SlgWBcantlyReduce-patbogens": Lime Stabilization ® 1 Air is ❑ Composting ❑ Aerobic Di estion ❑ Anaerobic Digestion on H applicable to alternative peerformed Class A or Class B con fete the followin monitorin data: 'Parameter Allowable Level in SludgeEx�- Pathogen Density um Of . Frequency. of Analysis is Sample Type Analytical Tech - Wave Minimum Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Sahnonella bacteria (in lieu of fecal coliform) 3 NWN per 4 grams total solid (dry Wei t vector Amraenon Reduction (15A MAC 02T .1107)- Please indicate,alternative performed: Alt.I (VS reduction) ❑ jAlt. 2 (40-day bench) ❑Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ jAlt. 6 (AIL Stabilization Q Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorponation) ❑ No vector attraction reduction alternatives were performed ❑ (:EKl'MIGATlUN STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met:' ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction -reduction -requirement-in 15A NCAC.02T..1.107-have -not4mn met." -(Please-note If you check this statement attach an explanation why you have not met one or both of the requirements) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine -that the pathogen and -vector attraction reduction requirements have'been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Wayne Benton, ORC Preparer ame an itle type or print) SilWatute of Preparer* Land Ap lie N : and Tid a (i plicable)(type or print) Signature o d Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 18, 2014 Kenwood 1.96 % Solids 7.14 pH Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight x 10,000 Pounds/Dry Ton M x 0.002 Nitrogen (TKN) 7.110 71,100.000 142.200 Phosphorus 1.290 12,900.000 25.800 Potassium 0.443 4,430.000 8.860 PAN injected)* 2.376 23,755.000 47.510 PAN surface)* 2.242 22,415.000 44.830 Ammonia Nitrogen 0.268 2,680.000 5.360 Calcium 2.420 24,200.000 48.400 Calcium Carbonate E . --- --- Magnesium --- 2,920.000 5.840 Sodium --- 14,700.000 29.400 Sulfur --- --- Nitrate N / Nitrite N --- 549.000 1.098 Barium --- --- Chloride --- --- Iron --- --- Aluminum --- 5,770.00 11.540 Arsenic -- 4.29 0.009 Cadmium --- 4.29 0.009 Chromium --- 11.400 --- Copper --- 497.00 0.994 Lead --- 12.40 0.025 Mercury --- 0.46 0.001 Molybdenum --- 4.29 0.009 Nickel --- 14.70 0.029 Selenium --- 9.18 0.018 Zinc --- 1,470.00 2.940 Environmental Chemists, Inc. # 2014-14256 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. F'"07 77 Environmental Chemists, Inc. envirochem 6602 Wmdmill Way • Wil.mi gtory NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252) 473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Onslow Water & Sewer Authority Date of Report: Dec 03, 2014 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2014-14256 Project ID: Kenwood WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-34959 Site: Sludge 11/18/2014 9:00 AM Solid/Sludge Johnathon D Witte Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 5770mg/kg 11/26/2014 Arsenic EPA200.7 <4.29 mg/kg 11/21/2014 Cadmium EPA200.7 <4.29 mg/kg 11J21/2014 Calcium EPA200.7 24200mg/kg 11/26/2014 Chromium EPA200.7 11.4mg/kg 11/21/2014 Copper EPA200.7 497 mg/kg 11/24/2014 Lead EPA200.7 12.4mg/kg 11/21/2014 Magnesium EPA200.7 2920mg/kg 11/25/2014 Molybdenum EPA200.7 <4.29mg/kg 11/21/2014 Nickel EPA200.7 14.7mg/kg 11/21/2014 Potassium EPA200.7 4430mg/kg 11/25/2014 Selenium EPA200.7 9.18mg/kg 11/21/2014 Sodium EPA200.7 14700 mg/kg 11/25/2014 Zinc EPA 2001 1470 mg/kg 11/26/2014 Ammonia Nitrogen EPA 350.1 2680 mg/kg 11/20/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 71100 mg/kg 11/2112014 Nitrate+Nitrite-Nitrogen EPA3532 549mg/kg 12101/2014 Total Solids (%) SM2540 B 1.96 % 11/19/2014 pH SM 4500 H B 7.14 units 11/2012014 Total Phosphorus SM 4500 P F 12900 mg/kg 11/24/2014 Mercury SW846 74718 0.4590 mglkg 11 /26/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: cP�ccaz Report#:: 2014-14256 Page 1 of 1 ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way } � Wilmington, NC 28405 Sample Collection and Chain of Custody Phone: (910) 392-0223 Fax (910) 392.4424 Client: ONWASA Kenwood WWTP (Mark Young) Collected BY: Johnathon Witte Report No:Z� Camnip Tvne? T = Tnflumf V = T.ffinPnt- W =WP11- RT=RtrPam_ Qn=.Cni1- CT.= C1mdcFP nf1 Pr- Sample Identification q w �+ d a Collection = „r. S e 1.. F E y e G a .S PRESERVATION ANALYSIS REQUESTED [� x .4 x G o � z p � o DATE TIME TEMPHpcq Digester � t* e�/01f �� S SL C P g Annual Sludge Analysis G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer linquished y: Date/Time eived By: Date/Time1 2. . emperatu>� MneYA_ftAccepted. 9/ 'ec esample Requested: Delivered By: / Received By Date: Time: f LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Kenwood WVVfP Batch Size (gallons): 4,000 Lbs. or Gallons Used: P.O.# 150 Material Used For Stabilization: Lime U O LL. V' O fn > V O N > M O Vl 7 M M O fn > M M O (q 7 O M O y > h N O N > V' N O fn > N O N 7 o0 r O fn O c[7 � O N 7 N .! O N 7 O O O N 7 O O O N M O O y O O co O O N 7 C c0 O O 41 7 C 0) O O tll 7 C N o o y 7 C cn O N 7 C ao O N 7 C N O f� 7 C v N O _7 C � N O N 7 C o M O N 7 C m 'i ' O f/1 7 C co Ci O 41 7 C rn m O f/1 7 C N a O 41 7 C cn O N 7 C a a a a a n a d M M M n. M M M Z 2 �'2 2 2 2i 2 2 i5 2 U Cti E O V O1 M 00 M f-- M CO M LO M 'd' M M M N M co CD co N 00. N 1- N O N LO NNN T M N r O N O CO r� 0 r In ;I- M r- H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Dumber: WQ0000455 WWTP Name: Kenwood NI'DES Number: NCO030813 Monitoring Period: From l/l/20.14 To 12/31/2014 .Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (tiv7eheunp) Atf B (Alk Treatment_ Alt. C (Prior TestiniLJ Alt_D (No Prior Test) L � Process to Further Reduce Pathogenp-0-1 If applicable to alternative performed (Mass A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat TreatmenitJ Thennophilic' Beta Ray Garnma Ra .1-J Pasteurization Class )B: Alt. (]) Fecal Density Ll Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization '''t Air Diving Composting Aerobic D.icgestiorP Anaerobic Digestion ..... .... .. .............. .... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density uffier o Frequency Sample Analyticalch- Parameter in Sludge ExNdm of Analysis yp Type Minimu Geo. Mean Maximu Units dense- deuces ni ue nique 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) I weight) Vector Attraction Red Alt.] (VS reduction) Alt. 5 (14-Day Aerobic) Alt. 9 (Iniection) 15A NCAC 02T .11f.7) - Please indicate alterna Alt. 2 (40-day bench) Alt. 6 (Alk. Stabilization Alt. 10 (Incormration) JAlt. 3 (30-day bench) Alt. 4 (Spec. 02 uptake) Alt 7 (Drying - Stable) IAlt. 8 (Drying - Unstable) No vector attraction reduction alternatives were performed CEO iTFFItCATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an.explanation why you have not met one or both of the requirements.) "This determination has been made sander illy direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mark Young, Supervisor PYpa NamVaT' (type or print) Land Applier Narne and Title (if applicable)(type or print) S S' satire of 6r pa r I l3ate Signature of Land Applier (if applicable) Date 'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 10, 2014 Majestic Oaks WWTP Permit No. W00000455 0.26 % Solids f 7 nu Parameter % Mg/Kg Dry Weight (% x 10,000 Pounds/Dry Ton (Mg/Kg x 0.002 Nitrogen (TKN) 7.420 74,200.000 148.400 Phosphorus 5.310 53,100.000 106.200 Potassium 1.580 15,800.000 31.600 PAN (injected)* 2.424 24,240.400 48.481 PAN (surface)* 2.385 23,854.400 47.709 Ammonia Nitrogen 0.077 772.000 1.544 Calcium 2.170 21,100.000 43.400 Calcium Carbonate E . --- --- --- Magnesium --- 5,650.000 11.300 Sodium --- 46,500.000 93.000 Sulfur --- --- Nitrate N / Nitrite N --- 1,440.000 2.880 Barium --- --- --- Chloride --- -- - - Iron --- --- --- Aluminum --- 1,920.00 3.840 Arsenic --- 33.80 0.068 Cadmium --- 33.80 0.068 Chromium --- 45.400 --- Copper --- 239.00 0.478 Lead --- 33.80 0.068 Mercury --- 6.15 0.012 Molybdenum - 33.80 0.068 Nickel - 33.80 0.068 Selenium --- 33.80 0.068 Zinc --- 946.00 1.892 Environmental Chemists, Inc. # 2014-00431 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or< detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. ® 6602 Windmill Way ® Wilmington, NC 28405 envitrheM (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sm 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Majestic Oaks - Integrawater Date of Report: Feb 14, 2014 PO Box 10127 Customer PO #: Birmingham AL 35202 Report #: 2014-00431 Attention: Michael Myers Report to: Michael Myers Project ID: Sludge Lab ID Sample ID: 14-01015 Site: Sludge Test Collect Date/Time 1/10/2014 Method Matrix Sampled by Solid/Sludge Client Results Date Analyzed Sludge Residuals Aluminum EPA200.7 1920 mg/kg 02/03/2014 Arsenic EPA2o0.7 <33.8 mg/kg 01/22/2014 Cadmium EPA200.7 <33.8 mg/kg 01/22/2014 Calcium EPA200.7 21700 mg/kg 01/20/2014 Chromium EPA200-7 45.4 mg/kg 01/22/2014 Copper EPA200.7 239 mg/kg 01/22/2014 Lead EPA 200.7 <33.8 mg/kg 01/22/2014 Magnesium EPA200.7 5650 mg/kg 01/20/2014 Molybdenum EPA200.7 <33.8 mglkg 01/22/2014 Nickel EPA200.7 <33.8 mg/kg 01/22/2014 Potassium EPA 200.7 16800 mg/kg 01120/2014 Selenium EPA200.7 <33.8mg/kg 01/22/2014 Sodium EPA200.7 46600 mg/kg 01/20/2014 Zinc EPA200.7 946mg/kg 02/04/2014 Ammonia Nitrogen EPA350.1 772mg/kg 01/16/2014 Total Kjeidahl Nitrogen (TKN) EPA351.2 74200 mg/kg 02/05/2014 Nitrate+Nitrite-Nitrogen EPA353.2 1440 mg/kg 02/03/2014 Total Solids (%) SM2540B 0.26% 01/15/2014 pH SM4500 H B 6.70 units 01/23/2014 Total Phosphorus SM 4500 P F 53100 mg/kg 01/24/2014 Mercury SW8467471B 6.15 mg/kg 01/1712014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2014-00431 Page 1 of 1 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COI I FCTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 info@environmentatchemists.com CLIENT: 0. PROJECT NAME: REPORT NO: I --Z�3f ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Ramnlarl Rv: SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other: Sample Identification Collection A w ;, m o W gZ PRESERVATION ANALYSIS REQUESTEDj Time Temp oz x h ZC` a ZDate ° C P G G C P G G C. P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: DatelTime Received By: Date/Time 1. 2. Temperature when Received: Accepted: R 1 t d: Resample Requested: Delivered By: Received By: C.I�J Date: 11O'I `! Time: 1'-[OC> Comments: TURNAROUND: LEWIS FARMS WQ0000455 Majestic Oaks WWTP ... .... ....... .... ....................... .................... I .................. ... ... ........ ............. ............. . ........... .. ...... ... . ... .................. .............. ............... ...... ........... 02/21/14 615,385 5.7891 02/21/14 2,906,977 6.4634 02/21/14 5,263,158 6.7212 02/21/14 1,896,552 6.2780 02/21/14 782,123 5.8933 02/21/14 670,732 5.8265 02/21/14 5,747,127 6.7595 Total 1 43.7311 Average 1 6.2473 Geometric Mean J["-7'..'."-' ....... :4Fecal Coliform MPN / gram ............. ......... .......... ........... Geometric Mean of Less than 2,000,000 meets Class B - Alternative I Pathogen Reduction requirement. 1 Environmental Chemists, Inc. R 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392 4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Majestic Oaks - Integrawater Date of Report: Mar 03, 2014 PO Box 10127 Customer PO #: Birmingham Al_ 35202 Report #: 2014-02106 Attention: Michael Myers Report to: Michael Myers Project ID: Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-05104 Site: 1 2/21/2014 12:30 PM Solid/Sludge Client Test Method Results Date Analyzed - Total Solids (%) SM 2840 B 1.30 % 02/24/2014 ` Fecal Density sM 9221C E MPN 24 hr 503 615385 MPN/g 02/21/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-05106 Site: 2 1 2/21/2014 12:30 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2640 B 1.72 % 02/24/2014 Fecal Density SM 9221C E MPN 24 hr 5D3 2906977 MPN/g 02/21/2014 Lab ID Sample ID: I Collect Date/Time Matrix Sampled by 14-05107 Site: 3 2/21/2014 12:30 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.71 % 02/24/2014 Fecal Density SM 9221C E MPN 24 hr 503 5263158 MPN/g 02/21/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-05108 Site: 4 2/21/2014 12:30 PM Solid/Sludge Client A Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.16 % 02/24/2014 Fecal Density SM 9221 C E MPN 24 hr 503 1896552MPN/g 02/21/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-05109 Site: 5 2/21/2014 12:30 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) SM 2540 B 1.79 % 02/24/2014 Fecal Density SM 9221C E MPN 24 hr503 782123 MPN/g 02/21/2014 Report #:: 2014-02106 Page 1 of 2 0 envirochem ANALYTICAL & CONSULTING CHEMISTS Majestic Oaks - Integrawater PO Box 10127 Birmingham AL 35202 Attention: Michael Myers Lab ID Sample ID: 14-05110 Site, 6 Environmental. Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473 5702 NCDENR: DWQ CERTIFICATE "4. DLS CERTIFICATE *37729 Test Method Date of Report: Mar 03, 2014 Customer PO #: Report #: 2014-02106 Report to: Michael Myers Project ID: Collect DatelTime Matrix Sampled by 2/21/2014 12:30 PM Solid/Sludge Client Results Date Analyzed Total Solids (%) SM 254o B 1.64 % 02/24/2014 Fecal Density SM 9221C E MPN 24 hr 503 670732 MPN/g 02/21/2014 Lab ID Sample ID: Collect Date/Time ' Matrix Sampled by 14-05111 Site: 7 2/21/2014 12:30 PM Solid/Sludge Client Test Method Results Date Analyzed Total Solids (%) Fecal Density SM 2540 B SM 9221C E MPN 24 hr 503 Comment: Results reported on a dry weight basis. Reviewed by: CA / 0.87 % 02/24/2014 6747127 MPN/g 02/21/2014 Report #: 2014-02106 Page 2 of 2, Analytical & Consulting Chemists 4= ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 ['nl 1 1=f_TInN AIUn PLJAIIU nC f1l lernnv 6602 Windmill Way Wilmington, NC 20405 OFFICE: 910-392-0223 FAX 910-3924424 inie@environmentalchemists.com QLIENT: PROJECT NAME:. REPORT NO:41 ADDRESS: CONTACT NAME: PO NO: REPORT TO: - PHONE/FAX: COPY TO: email: Sampled By: SAPAPI F TVPP- I = :I,e„enf r = u! -- Won QT - aF.,,...., an _ OF Sample Identification Collection ANALYSIS REQUESTED' MAM RelinquishedRy: -A Received By: 1 emperawre wnen meceivea: Aeeeptea; K@jecte esample Requested' Delivered By: Received By: Date:_ Z- ZE Time: Comments: -TURNAROUND: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Farms Lewis and Liquid Waste, Inc. WQ,Permit Number: WQ0000455 W WTP Name: Majestic Oaks NPDES Number: WQ0030088 Monitoring Period: From 1/1/2014 To 12/31/2014 Patboaen Reduction (15A NCAC 02T _11t161- Plpnce indientP 1pa,ol aohip.....1 anA .1to...at:. a ..era _... a. Class A: Alt. A (time temp) ❑ Alt B (All: Treatment) Ll Alt. C (Poor Testing) ;j Alt.D (No Prior Test) `1 I Process to Further Reduce Pathoeenas L7 If applicable to alternative performed (Class oniv indicate "Process to Further Reduce Pathogens": Compost Heat Dn•ing ❑ Heat Treatment J Thermo hiiic J Beta Ra Gamma Ray ❑ Pasteurization `_? Class B: JAIL (1) Fecal Density Z Alt. (2) Process to Significantly Reduce Pathogens =i If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Patho ens": Lime Stabilization J Air Dn,iu `! Com ostin8 J Aerobic Digestion Anaerobic Digestion Ll If applicable to alternative peirlormed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Sludge Pathogen Density um r Excee- den Frequency of, Sam le Type AnalYu hin - ni ue Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 615,385 1,767,243 5,747,127 MPN/g 3 Annual Grab SM 9221 CE CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry wei t . %M;9UA tltail A ;&Jinx i%ruua:uuu ri'H rv%—jxt- uL 1 _ i 1 al / 1 — rIPACP_ innt"re nivP.rnnrlvP rwrrnrmorl- Alt. I (VS reduction) Alt. 2 (40-day bench) It. 3 (30-day bench) TAMIL 4 (Spec. % uptake) Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization Alt 7 (Drying - Stable) lNo JAIL 8 (Drying - Unstable) Alt 9 (Injection) Alt. 10 (Incorporation) -0 vector attraction reduction alternatives were performed %-ZK l IV 11:A I IUIN b I ATEMJI N (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements_ in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Stanley E. Buck, ORC Preparer Name and ��)wprint) Land ApzrN� 'e le (if applicable)(type or print) Signature of Preparer* Date Signatu f Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .I 102 (26) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: August 14, 2014 Maysville Permit No. WQ0000455 1.02 % Solids pH (taken from lime stabilization event) Parameter. % Mg/Kg Dry Weight % x 10,000 Pounds/Dry Ton (Mg/Kg x 0.002 Nitrogen (TKN) 0.696 6,960.000 13.920 Phosphorus 0.807 8,067.000 16.134 Potassium 0.281 2,809.000 5.618 PAN injected)* 0.340 3,401.590 6.803 PAN (surface)* 0.247 2,466.090 4.932 Ammonia Nitrogen 0.187 1,871.000 3.742 Calcium 4.434 44,339.000 88.678 Calcium Carbonate E . --- --- Magnesium 0.226 2,256.000 4.512 Sodium 0.429 4,285,000 8.570 Sulfur --- --- --- Nitrate N / Nitrite N --- 3.890 0.008 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 8,348.00 16.696 Arsenic --- 2.50 0.005 Cadmium - 1.30 0.003 Chromium --- 12.000 --- Copper --- 635.00 1.270 Lead --- 20.00 0.040 Mercury --- 0.43 0.001 Molybdenum --- 5.00 0.010 Nickel --- 22.00 0.044 Selenium --- 5.00 0.010 Zinc --- 944.00 1.888 Environment 1, Inc. # 139A *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. (Oct. 21. 2014 8: 28AM vcp. $w RV1'1 J.LV1111 TOWN OF MAYSVILLE NI.No, 6500 P P. 1 G REEN1/1 Town Or MAX8VILLN PUSLIC WORKS DUMUTHUT P.O. Box 269 layovann ,NC 29555 PARANI1;TRUN A1111n1n11m, (dry wt. Lndb), 111gfkg Amenlc (dry ivt. basla), n'S'kg Cllleh1111 (dry lyt, hodli), InglkK CAdnllum (drys wt. bulls), mg/kg Copper (dry wt. bA31% 11191199 Chrunliutlf, T.(dry 19t. 11mb ulgllsg Lead (dry height MUM, 1112/4 Aingnmhmi (dcy nit. bAsts)1 11191119 Aiermey (dry 11-1. bavlc), nlglkg Nickel ((try Yrt. hnsish luglltg 190fa i11111 (dry w(. ba91s)y mgncg Selenium (dry wt. hash), mgncg 8011111111 (&-? wt. bas(5), 1ng/Gg %inc (dry wl. basis), tnglkg Tula) 8011(is, 'PION (dry-M.), nlgnrg Ammunia Nitrogen Olq 1vt.)oug1k9 rhosphoruF, T. (dry w(.), mgncg Nltrate•Nifrile (dry wlJ, 1ng/1g Plant Available Nitragon, tnglkg Molybilcunm (dry W. basis), mgncg h11111go Analysls Method S111111110 Unte Analyst Code 8348 09102/14 LFJ TPA200.7 <x,g 09/03/14 11+1Ii1, 3113E.04 44339 09102/14 1.10-1 EPA200.7 1.3 09109/14 1M L 31158.04 63s 09/02114 I,tr.1 RA200.7 12 0910;/14 LFJ RPA200,7 20 09111114 IVMI# 311311.04 2256 09102114 1,11.Y EPA200.7 0.43 08120114 =1 243,1 R3.94 22 09192114 LDJ RVA200.7 2909 09102114 LKY EPA200.1 <5.0 09105114 WML 31 W-04 4285 09104114 WIN 3111"9 944 09/03114 MUNI311)149 im, 00/18/14 C141C 25400-97 6966 08/21/14 ANO 351.2 R2-93 1871 09119/14 ALD 350.1 112-93 9067 n8/21114 ALI) 3ti5A 74 0.99 08120114 ANO 353.21tV0 2462 08/24114 OW <9.0 09/02114 L11d KPA200.7 Zvo 1 139 A DATE CO1.Tagl:TBI)1 08/14/14 DATE RNPORTED 1 09/18/14 REVIEWED aYl LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Town of Maysville P.O.# Batch Size (gallons): Lbs. or Gallons Used: 800 gallons Material Used For Stabilization: lime 24 Hour pH �.- . C O f� p O � u- O N 7 N N 7 O l'M N 7 tD M N 7 l'O q Nl 7 O M N 7 h N N 7 '� N N 7 N tll 7 m fA 7 lq .— N 7 N tll 7 O O d N 7 f0 . tll 7 O d N 7 O C p °j C O o m C O d q d in 7 d Co N d N 7 N d . 7 N d m > M d m > C! d . 7 M d dl 7 CD d m 7 d 'A S to d m 7 CU E F� v M c) M Cr)o M cCi M ch M N N N N N N N N N N LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Town of Maysville P.O.* Batch Size (gallons): Lbs. or Gallons Used: _800 gallons Material Used For Stabilization: Lime Ew==NM= O v u- er O o. O a p7 O p s O y p a. O fA .�.. a O 0 s O fp 2 n. N O W 7 a N O N a t O OWN O tll L o. W O N 3 a N N O Nl 7 a Ql O O fA 7 a to O O fA 7 a M O O N 7 a o /4 O C � o a 7 C m O C ue 7 C g ^ C O N � O w 7 C -m Ca G yy 7 C .- N C m C N C m 7 C g N C p� 7 C M C m 7 C g W G m 7 C l0 G m 7 C PJ O ae 3 � G rA C 6f G m 7 C g t� 0. EE 9 O ,� df M GO co ti M t0 M ICJ M M c7 N M r M O M IM N MT- N N Cfl N to N N M N N cV a- N O N 0 %- OD V.- i- %-%- O Lo %- 'Cr %- M V- CV "- O LEWIS FARMS AND LIQUID WASTE, INC. wo 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Town of Maysville P.O.# Batch Size (gallons): Lbs. or Gallons Used: 800 gallons Material Used For Stabilization: Lime O 9 O Cl •►' L- O s1' O W a N er O N a a M C7 O W a 10 CM O tl) a a M C7 O w a a. O C9 O M a W P N O w a 'a 'V' N O (a0 a a N O a a CO t- O 0 a it O O w a it N O w a a M O O w a a to O O N a a. CM Co O N a a O o G M a C o C M a C Co C M a C N o q a C C M 7 C m r O M a C 21,2 N O M a C N Ci M 7 C 2 N G Co 7 C 2 m C7 M 7 C 2 C M 7 C M 1 r�i C M 7.2 C 21 M 0 M > C N v C M > C M Q C M 7 C N U a O O 00 1- Co U) v CM N V- O a) Co n Co 1p d M N �- CDC3) Co ti Co LO 'Ch M NC) O 'd' co co M co M M C9 M M M N N N N N N N N_ N N r' T- � T- Y r r V- � T- oEi F- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 NN1NVTP Name: Maysville NPDES Number: NCO021482 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) F...1 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)LJ - Alt.D (No Prior Test) [Y] Process to Further Reduce Pathogengs El If applicable to alternative erformed Class A only) indicate "Process to Further Reduce Pathogens": Compost o Heat Drying © Heat Treatment F—1 Ther-mophilic ❑ Beta Ra ® } Gamma Ra ® y Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ® .... If applicable to alternative performed (Class B only) Indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Ri Air Drying © composting ® Aerobic Digestion 0 Anaerobic e ' Di s ton g t If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density g tY um er of Excee- dences Frequency of Analysis Sample Type na ytica Tech - ni we Minimui Geo. Mean aximun Units Fecal Colifortm 2 x 10 to the 6th power per gram of total solids WN CFU 1000 mpn per gram of total solid (dry welghl) Salmonella bacteria (in lieu of fecal coliform) 3 N0\1 per 4 grams total solid (dry Iveiglit) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: AIt.I (VS reduction) ❑ Alt. 2 (40-day bench) Ll Alt. 3 (30-day beach) © Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization RI Alt 7 (Drying - Stable) I7 Alt. 8 (Dr),ing - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) LI No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) R1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requiti•ement in 15A NCAC 02T .1107 have been met." ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if ,you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Brian Odum. ORC Preparer Name and Title (typ print) Land Applies• Name and Title (if applicable)(type or print) �--- Z -�- ld -lS Signature of Preparer" Date Signature of Land Applier (if applicable) Date `Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (1212006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: February 18, 2014 Morehead City 19.50 % Solids 6.77 pH Permit No. WQ0000455 Parameter I % JMg/KgDryWeightJ x 10,000 Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.835 8,350.000 16.700 Phosphorus 0.648 6,480.000 12.960 Potassium 0.312 3,120.000 6.240 PAN (injected)* 0.346 3,869.500 7.739 PAN (surface)* 0.279 3,777.000 7.554 Ammonia Nitrogen 0.135 1 1,350.000 2.700 Calcium 4.590 45,900.000 91.800 Calcium Carbonate E . --- --- --- Magnesium 0.364 3,640.000 7.280 Sodium 0.290 2,900.000 5.800 Sulfur --- --- --- Nitrate N / Nitrite N --- 13.300 0.027 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 1,570.00 3.140 Arsenic - 9.44 0.019 Cadmium --- 0.51 0.001 Chromium --- 18.500 --- Copper --- 862.00 1.724 Lead --- 8.77 0.018 Mercury --- 2.00 0.004 Molybdenum --- 5.07 0.010 Nickel -- 8.72 0.017 Selenium --- 5.64 0.011 Zinc --- 990.00 1.980 Environmental Chemists, Inc. 2014-01870 *Determination' of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. LEWIS FARMS WQ0000455 Morehead City WWTP r r=::: 02/18/14 862,069 5.9355 02/18/14 854,701 5.9318 02/18/14 835,074 5.9217 02/18/14 774,819 5.8892 02/18/14 832,900 5.9206 02/18/14 876,713 5.9429 02/18/14 852,425 5.9307 Total 41.4724 Average 1 5.9246 1 Geometric Mean Fecal Coliform MPN / gram Geometric Mean of Less than 2,000;000 meets Class B - Alternative 1 Pathogen Reduction requirement. F-7 11 Environmental Chemists, Inc. nVII6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 6M 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL &CONSULTING (252)473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 4137729 Town Of Morehead City Date of Report: Mar 21, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report#: 2014-01870 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-04550 Site: Sludge Class B 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Chlordane SW 846 Method 80816/3510 <0.005 mg/L 02/27/2014 Endrin SW 846 Method 8081B/3510 <0.00005 mg/L 02/27/2014 Heptachlor SW 846 MethodsomB/3s10 <0.00005mg/L 02/27/2014 Heptachlor epoxide SW 846 Method 8081 B13510 <0.00005 mg/L 02/27/2014 Lindane SW 846 Method Mal 6/3510 <0.00005 mg/L 02/27/2014 Methoxychlor SW 846 Method 80818/3510 <0,00005 mg/L 02/27/2014 Toxaphene SW846 Method 6081B/3510 <0.005 mg/L 02/27/2014 1,4-Dichlorobenzene (TCLP) SW846 method827013510 <0.050mg/L 02/25/2014 2,4,5-Trichlorophenol(TCLP) SW 846 method8270/3510 <0.050mg/L 02/25/2014 2,4,6-Trichlorophenol (TCLP) SW 846 method 827013510 <0.050 mg/L 02/25/2014 2,4-Dinitrotoluene (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/25/2014 Cresol (TCLP) SW 846 method 8270)3510 <0.050 mg/L 02/25/2014 Hexachloro-1,3-butadiene (TCLP) SW 845 method 8270I3510 <0.050 mg/L 02/25/2014 Hexachlorobenzene (TCLP) SW 846 method 827013510 <0.050 mg/L 02/25/2014 Hexachloroethane (TCLP) SW 846 method 827013510 <0.050 mg/L 02/25/2014 m + p-Cresol (TCLP) SW 646method827OJ3510 <0.050 mg/L 02/25/2014 Nitrobenzene(TCLP) SW 846 method827OM10 <0.050mg/L 02/25/2014 o-Cresol (TCLP) SW 846 method 8270/3510 <0.050 mg/L 0212512014 Pentachlorophenol (TCLP) SW 846 method8270MIO <0.250m /L 9 02/25/2014 Pyridine (TCLP) SW 846 method 8270/3510 <0.050 mg/L 02/25/2014 Paint Filter Test SW 846 Method 9095 A pass 02/20/2014 2,4,5-TP SW846 Method 8151A <0.0003 mg/L 02/26/2014 2,4-D SW846 Method 8151A <0.0003 mg/L 02/26/2014 1,1-Dichloroethylene SW846 Method 826015030 <10 mg/L 03/14/2014 1,2-Dichlorcethane SW846 Method 826015030 <10 mg/L 03/14/2014 Benzene SW846 Method8260/5030 <10mg/L 03114/2014 Report#:: 2014-01870 Page 1 of 5 F-7- � "7 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sM 710 Rowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252)473-5702 CHEMISTS NCDFNR: DWQ CERTIFICATE #94. DLS CERTIi11CATE #37729 Town Of Morehead City 706 Arendell Street Morehead City NC Attention: C. Sutton 28557 Date of Report: Mar21, 2014 Customer PO #: Report #: 2014-01870 Report to: C. Sutton Project ID: Sludge Carbon Tetrachloride SW846 Method 8260/5030 <10 mg/L 03/14/2014 Chlorobenzene SW846 Method 8260/5030 <10 mg/L 03/14/2014 Chloroform SW846 Method 8260/5030 18.6 mg/L 03/14/2014 Methyl ethyl ketone SW846 Method 82W15030 <50 mg/L 03/14/2014 Tetrachloroethylene SW846 Method 8260/50M <10 mg/L 03/14/2014 Trichloroethylene SW846 Method 8260/5030 <10 mg/L 03/14/2014 Vinyl Chloride SW646 Method 82NI5030 <10 mg/L 03/14/2014 RCI Ignitabili ty EPA 1030 <0.8 mm/sec 02/24/2014 Cyanide EPA 335.4 <0.124 mg/kg 02/28/2014 Sulfide SM 4500 s D <0.247 mg/kg 03/03/2014 pH SW 846 Method 9045D 6.77 units 02/20/2013 Sludge Residuals Aluminum EPA 200.7 1570mg/kg 03/04/2014 Arsen is EPA 200.7 9.44 mg/kg 02/27/2014 Cadmium EPA 200 7 <0.508 mg/kg 03/10/2014 Calcium EPA2.00.7 45900mg/kg 02/26/2014 Chromium EPA 200.7 18.5mg/kg 02/27/2014 Copper EPA 200.7 862 mg/kg 03/14/2014 Lead EPA 200.7 8.77 mg/kg 03/10/2014 Magnesium EPA 200.7 3640mg/kg 02/26/2014 Molybdenum EPA20D.7 <5.07 mg/kg 02/24/2014 Nickel EPA 200.7 8.72 mg/kg 02/24/2014 Potassium EPA 200.7 3120mg/kg 02/26/2014 Selenium EPA 200.7 5.64mg/kg 02/24/2014 Sodium EPA 200.7 2900 mglkg 02126/2014 Zinc EPA200.7 990mq/kg 03/04/2014 Ammonia Nitrogen EPA 350.1 1350 mg/kg 03/05/2014 Total Kjeidahl Nitrogen (TKN) EPA351.2 8350mglkg 03/11/2014 Report #.: 2014-01870 Page 2 of 5 envirochem ANALYTICAL & CONSULTING CHEMISTS Town Of Morehead City 706 Arendell Street Morehead City NC 28557 Attention: C. Sutton Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NIC 28405 (910)392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 NCDENR: DWQ CERTIFICATE #94. DTS CERTIFICATE #37729 Date of Report: Mar 21, 2014 Customer PO #: Report #: 2014-01870 Report to: C. Sutton Project ID: Sludge Nitrate+Nitrite-Nitrogen EPA353.2 13.3mg/kg 03/11/2014 Total Solids (%) SM2540e 1.9.6% 02/21/2014 Total Phosphorus SM 4500 P F 6480 mg/kg 03/11/2014 Mercury Sw8467471B 2.00 mg/kg 02/28/2014 TCLP Metals Arsenic EPA 200.7 <0.100 mg/L 02/25/2014 Barium EPA 200.7 <0.100 mg/L 02/24/2014 Cadmium EPA 200.7 <0.100mg/L 02/24/2014 Chromium EPA200.7 <0.100mg/L 02/24/2014 Lead EPA 200.7 <0.100 mg/L 02/24/2014 Silver EPA 200.7 <0.100 mg/L 02/27/2014 Selenium EPA200.8 <0.100mg/L 03/06/2014 Mercury EPA 245.1 <0.002 mg/L 02/24/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04551 Site: 1 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2540 B 18.6 % 02/21/2014 Fecal Density SM92210EMPN 24hr503 862069MPN/g 02/19/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04552 Site: 2 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) Fecal Density SM 2540 B SM92210EMPN 24hr503 18.7 % 02/21/2014 854701 MPN/g 02/19/2014 Report #:: 2014-01870 Page 3 of 5 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 -L (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 � ANALYTICAL &CONSULTING _ CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 21, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-01870 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04553 Site: 3 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM 2s4o s 19.2 % 02/21/2014 Fecal Density SM 9221C EMPN 24 hr503 835074 MPN/g 02/19/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by f 14-04554 Site: 4 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangertield j Test 1. Method Results Date Analyzed Total Solids (%) SM 2546 s 20.6 % 02/21/2014 Fecal Density SM92210EMPN 24hr503 774819MPN/g 02/19/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-04555 Site: 5 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield ? Test Method Results Date Analyzed Total Solids (%) SM2W B 19.2 % 02/21/2014 Fecal Density L SM92210EMPN 24hr503 832900MPN/g 02/19/2014 Lab 1D Sample ID: Collect Date/Time Matrix Sampled by 14-04556 Site: 6 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed Total Solids (%) SM2540 s 18.2 % 02/21/2014 Fecal Density SM92210EMPN 24hr503 876713MPN/g 02/19/2014 I_ _ Lab ID Sample ID: Collect Date/Time Matrix Sampled by j 14-04557 Site: 7 2/18/2014 10:00 AM Solid/Sludge C.Sutton & C.Dangerfield Test Method Results Date Analyzed r— Total Solids (%) SM 2540 a 18.8 % 02/21/2014 Fecal Density SM92210EMPN 24hr503 852425MPN/g 02/19/2014 Report #:: 2014-01870 i- i Page 4 of 5 r SM ANALYTICAL & CONSULTING _ CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way � � Wilmington, NC 284.05 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 N tCDENR DWQ CERTIFICATE ##94. DLS CERTIFICATE #37729 Town Of Morehead City Date of Report: Mar 24, 2014 706 Arendell Street Customer PO #: Morehead City NC 28557 Report #: 2014-01870 Attention: C. Sutton Report to: C. Sutton Project ID: Sludge Comment: Sludge residuals and Fecal density reported on a dry weight basis. RCI and Paint Filter Test reported on an as received basis. Reviewed by: & 06o A, /"4r Report*.: 2014-01870 Page 5 of 5 ENVIRONMENTAL CHEMISTS, INC OFFICE:9;a Way �'F,�91049 -4424 Analytical & ConsuJEing Chemists NCDEW- DWQ CERTIFICATION * 94 N013Et1-I3: DLS CERTIFICATION $ 37729 info@environmentatchemists.com COLLECTION AND CWAIN OF CUSTODY , CLIENT: X drtAa.•.( C: PROJECT NAME: REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Samnlad Rv: t,..�a j f r . l tncc.-d's/a% SAMPLE TYPE-- In Influent. E = Effluent W s Wall_ ST m Sfrnnm. SO c :Rnil_ SI a Rltirina. rlfhar- Sample Identification a Ion �N ion =i �ii�i I emperat Delivered mecelvea: Time: � ANAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQD000455 WWTP Name: Town of Morehead City NPDES Number: NC002661 l Monitoring Period: From I/1/2014 To' 12/31/2014 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 '..._r Alternative 2• ' _.; Alternative 3 r. Alternative 4 !' ; Alternative S '+ Alternative 6 i . ..,.... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment I : Thermophiiic Beta Ray Gamma Ra :.: ' Pasteurization Class B: Alternative 1 ''0j Alternative 2 ! If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ! Air n Drying*— composting L. Aerobic Digestion ; a Digestion- stion- Anaerobic S If applicable to alternative perfo ed Class A or Class B com Iete the following monitoring data: Parameter Allowable Level in Sludge Pathogen DensityNumber of Excee- Frequency of Analysis Sample Type AnappFar Tech- ninue hfinimurio Geo. Mean Maximun Units Fecal Colifonn 2 x 10 to the 6th power per g(2M Of total solids h1PN CFU 1000 mpn per gram of total solid (dry weight) 774,819 8402673 876,713 MPN/g 0 Annual Grab sM 9221C Salmonella bacteria (in lieu of fecal coliform) I 3 NON per 4 grams total solid (dry weight) vector Auracaon neauction t4v t xx 3u3.s31- Please indicate ontion nerformewl- AltI (VS reduction) ! _; Alt. 2 (40-day bench) 3 (30-daybencls) lt. 4 (Spec. O, uptake) Alt 5 (14-Day Aerobic) _ Alt, 6 (Allc Stabilization ; Alt 7 (Drying - Stable) L-: Alt. S (Drying - Unstable) .J Alt 9 (Injection) Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed '..r C:E1Z17r1CATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) ? "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine 1 that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Carl Dangerfield, WWTP Superintendent Wesley W oten, President Preparer Name and Title (type or print) Land Appl' r NEWhe Ad T' a (if applicable)(type or print) 1�:bZoif — /-I11T Stgttature of Pre er* D to Signature Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: October 6, 2014 Pender High School 0.33 % Solids 7.08 pH Permit No. WQ0000455 Parameter % lMg/KgDryWeight CLo x 10,000 Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 0.015 152.000 0.304 Phosphorus 0.076 759.000 1.518 Potassium 0.652 6,520.000 13.040 PAN (injected)* 0.629 6,294.800 12.590 PAN (surface)* 0.622 6,216.800 12.434 Ammonia Nitrogen 0.016 156.000 0.312 Calcium 1.620 16,200.000 32.400 Calcium Carbonate E . --- --- --- Magnesium --- 2,870.000 5.740 Sodium --- 28,800.000 57.600 Sulfur --- --- --- Nitrate N / Nitrite N --- 6,140.000 12.280 Barium --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 6,550.00 13.100 Arsenic --- 23.30 0.047 Cadmium --- 23.30 0.047 Chromium --- 23.300 --- Copper --- 539.00 1.078 Lead --- 92.10 0.184 Mercury 6.06 0.012 Molybdenum --- 23.30 0.047 Nickel --- . 23.30 0.047 Selenium --- 23.30 0.047 Zinc 688.00 1.376 Environmentatl Chemists, Inc. # 2014-12279 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. r- 77 Environmental Chemists, Inc. • LL 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) © 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CER'TINCATE #94. DLS CERTIFICATE #37729 Pender County Schools Date of Report: Oct 28, 2014 925 Penderlea Highway Customer PO #: $urgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2014-12279 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-30145 Site: Sludge 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Sludge Residuals r Aluminum EPA200.7 6550,mglkg 10/13/2014 Arsenic EPA200.7 <23.3 mglkg 10/08/2014 Cadmium EPA 200.7 <23.3 mg/kg 10/08/2014 Calcium EPA200.7 16200 mglkg 10/14/2014 Chromium EPA200.7 <23.3 mg/kg 10/08/2014 Copper EPA200.7 539 mg/kg 10/16/2014 Lead EPA20o.7 92.1 mglkg 10/08/2014 Magnesium EPA200.7 2870 mg/kg 10/14/2014 Molybdenum EPA200.7 <23.3mg/kg 10/0812014 Nickel EPA 200.7 <23.3 mg/kg 10/08/2014 Potassium EPA200.7 6520 mg/kg 10/14/2014 Selenium EPA200.7 <23.3 mg/kg 10/08/2014 Sodium EPA200.7 28800 mglkg 10/14/2014 Zinc EPA200.7 688 mg/kg 10/08/2014 Ammonia Nitrogen EPA350.1 156 mglkg 10/08/2014 Total K'eldahl Nitrogen (TKN) EPA351.2 <152 mg/kg 10/09/2014 N, NH3 agree within analytical uncertainty. Nitrate+Nitrite-Nitrogen EPA353.2 6140 mg/kg 10/24/2014 I' Total Solids (%) SM 2540 a 0.33 % 10/07/2014 pH SM 4500 H B 7.08 units 10/10/2014 Total Phosphorus SM 4500 P F 759 mg/kg 10/10/2014 Mercury Swe4e7471B <6.06mg/kg 10/08/2014 Report#.: 2014-12279 Page 1 of 0 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental. Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE 437729 Pender County Schools Date of Report: Oct 28, 2014 926 Penderlea Highway Customer PO #: Surgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2014-12279 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-30146 Site: 1 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.40 % 10/07/2014 Fecal Density SM 9221C E MPN 24 hr 503 2000000 MPN/g 10/07/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-30147 Site: 2 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.32 % 10/07/2014 Fecal Density SM 9221C E MPN 24 hr 503 1562500 MPN/g 10/07/2014 Lab ID Sample ID: Collect Daterrime Matrix Sampled by 14-30148 Site: 3 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 s 0.26 % 10/07/2014 Fecal Density SM 9221C E MPN 24 hrSw 5000000 MPN/g 10/07/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-30149 Site: 4 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 a 0.29 % 10/07/2014 Fecal Density SM 9221 C E MPN 24 hr 503 4482769 MPN/g 10/07/2014 Lab ID Sample 10: Collect Date/Time Matrix Sampled by 14-30150 Site: 5 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 a 0.30 % 10/07/2014 Fecal Density SM 02210 E MPN 24 hr 503 7333334 MPN/g 10/07/2014 Report #:: 2014-12279 Page 2 of 3 r71-7 Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 (252) 473 5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37929 J Pender County Schools Date of Report: Oct 28, 2014 925 Penderlea Highway Customer PO #: Surgaw NC 28426 Customer ID: 08100094 Attention: John Shepard Report #: 2014-12279 Project ID: Sludge - Lab ID Sample ID: Collect Date/Time Matrix Sampled by y 14-30151 Site: 6 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed -; Total Solids (%) SM 2640 s 0.21 % 10/07/2014 Fecal Density SM 9221C E MPN 24 hr 503 3333334 MPN/g 10/07/2014 Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-30152 Site: 7 10/6/2014 10:00 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2640 s 0.40 % 10/07/2014 Fecal Density SM 9221C E MPN 24 hr 503 1250000 MPN/g 10/07/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. l r Reviewed by: cvcc�Pi Report #:: 2014-12279 Page 3 of 3 ENVIRONMENTAL CHEMISTS, INC OFFI Windmill91-Way 3'FAX91o30z-"z4s Analytical & Consulting Chemists. NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 3 729 info@environmentatchemists.com COLLECTION AND CHAIN OF CUSTODY / Client: Pender County Schools PROJECT NAME: REPORT NO: -- ADDRESS: CONTACT NAME: John Shepherd PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Sampled Bv: i :A— SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludge. Other: Sample Identification p Collection d E a Nr 9 44 = o o" U S(9 :° g : N C- .o V, V e oW m m �Z PRESERVATION ANALYSIS REQUESTED Date Time Temp W z x o= N x y o w Sludge 0? �� C P X Isludge nutrients/metals lZ5 1) P ,! 3017 X fecal density/%TS G 2) Ze n' X fecal density/% TS G G lit 3) Uby. P I X fecal density/% TS G lv 4) P X fecal density/% TS oe G /0 7�i X fecal density/% TS R5 6 C P I IX Ifecal densit /% TS G G 7) CJ C X fecal densi /% TS G G 0.20.t5 C P G G Transfer Relinquished By: Date/Time Received By: DateMme 2. i emperaiure wne a eiveu: Accepted: ej etl: ResamplWRges Delivered By: Received By: bateComments: ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms and Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Pender High School NPDES Number: NCO042251 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) [IProcess to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying O 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens [�] If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization R1 Air Drying ❑ comPosting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o deuces Frequency of Analysis Sample Type Analytical Tech- ni ue MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal cwliform) TT_ ♦. 3 MPN per 4 grams total solid (dry wei t vector Attraction tceaucnon (1,A INCAU Ulf' .11W) - Please indicate alternative nerfnrmPd- Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization 0 Alt 7 (Drying - Stable) ❑ JAIL 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ C K1114ICA I1VN b"YATEMEINT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer / e/ itle (type or print) 3 / Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nr��n r�n�• n� mr tint i�n�nnnn� LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Pender High School P.O.# Batch Size (gallons): 5000 +/- Lbs. or Gallons Used: 150 Material Used For Stabilization: Lime c �' `) U LO V O M 7 N '�t O M 7 m CO O (n � O (M O (A 7 cr) (`M O U) 7 O M O (q 7 r` N O (n 7 V' N O M 7 N O tll 7 aD O N 7 O N 7 N O 0 7 m O O N 7 (O O O N 7 Cl) O O y 7 O co o 0 fA 7 C to 0 0 41 7 C rn 0 0 N 7 C N 0 0 y 7 C in 0 N 7 C ao — 0 N 7 C N 0 N 7 C v N 0 M 7 C N 0 N 7 C o r� 0 tll 7 C r� � 0 N 7 C co cM 0 N 7 C rn r� 0 w 7 C N 7 0 w 7 C in � 0 Ul 7 C U Q- N O d M M 00 M rl- M 0 M LO M d M M M N M M CD M N Co N r— N M N Lo N 'ITM N N N N N CD N- M r-- r (O c- LO c- 'cI' r M N r O H LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 18, 2014 Onslow Water & Sewer Authority Richlands Permit No. WQ0000455 1.97 % Solids 6.72 pH Parameter % JMg/KgDryWeightJPounds/Dry % x 10,000) Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 6.850 68,500.000 137.000 Phosphorus 1.500 15,000.000 30.000 Potassium 0.508 5,080.000 10.160 PAN (injected)* 2.671 26,709.000 53.418 PAN (surface)* 2.278 22,784.000 45.568 Ammonia Nitrogen 0.785 7,850.000 15.700 Calcium 1.630 16,300.000 32.600 Calcium Carbonate E . --- --- --- Magnesium --- 3,320.000 6.640 Sodium --- 9,700.000 19.400 Sulfur --- --- Nitrate N / Nitrite N --- 664.000 1.328 Barium --- --- --- Chloride - --- --- Iron --- --- --- Aluminum --- 4,420.00 8.840 Arsenic --- 5.03 0.010 Cadmium --- 5.03 0.010 Chromium 10.700 --- Copper --- 228.00 0.456 Lead --- 12.90 0.026 Mercury --- 0.51 0.001 Molybdenum - 5.03 0.010 Nickel --- 12.90 0.026 Selenium --- 7.97 0.016 Zinc - 924.00 1.848 Environmental Chemists, Inc. 2014-14253 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N +Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. ienvirodlem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Onslow Water & Sewer Authority Date of Report: Dec 03, 2014 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2014-14253 Project ID: Richlands WWTP Lab ID Sample ID: Richlands Collect Date/Time Matrix Sampled by 14-34954 Site: Digester Sludge 11/18/2014 8:20 AM Solid/Sludge Joe Stutts Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 4420mg/kg 11/26/2014 - Arsenic EPA200.7 <5.03mg/kg 11/21/2014 Cadmium EPA200.7 <5.03 mg/kg 11/21/2014 Calcium EPA200.7 16300 mglkg 11/25/2014 Chromium EPA200.7 10.7mglkg 11/21/2014 Copper EPA200.7 228mg/kg 11/2412014 Lead EPA200.7 '12.9 mg/kg 11/21/2014 Magnesium EPA200.7 3320 mg/kg 11/25/2014 Molybdenum EPA200.7 <5.03 mg/kg 11/21/2014 Nickel EPA200.7 12.9 mg/kg 11/21/2014 Potassium EPA200.7 5080 mg/kg 11/25/2014 Selenium EPA200.7 7.97mg/kg 11/21/2014 Sodium EPA200.7 9700 mg/kg 11/25/2014 ti Zinc EPA200.7 924 mg/kg 11/21/2014 Ammonia Nitrogen EPA350.1 7850mg/kg 11/20/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 68500mg/kg 11/21/2014 Nitrate+Nitrite-Nitrogen EPA353.2 664mg/kg 12/01/2014 Total Solids (%) SM 2540 B 1.97 % 11/19/2014 pH SM 4500 H B 6.72 units 11 /20/2014 Total Phosphorus SM4600 P F 15000 mg/kg 11/24/2014 Mercury SW8467471B <0.508 mg/kg 11/26/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by. - Report #:: 2014-14253 Page 1 of 1 ENVIRONMENTAL CHENIIST$ INC 4W Sample Collection and Chain of Custody Client: ONWASA Richlands WWTP (Mark Young} C1,. Te,..,.. T -'F n....-& W - Ti 4'+7......+ AW-j7Vo11 QTQn -.Qn;1 Q7.= Qlntltra n*har- 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4f 42 Rmnrt Nn- Sample Identification q w Collection y A v C v PRESERVATION ANALYSIS REQUESTED x z �" p DATE TIME TEMP Digester 1 1 !!��{'00 v�A� j 7 SL C P X Annual Sludge g Analysis G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time ceived By: Date/Time AOV Bury 1015 2. rir%tiv d JIl9 Temperature when Received:LL(Q'_ Accepted: (/ ec Resample Re e Delivered By: Received By: Date••Time: _ _I LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Richlands WWTP Batch Size (gallons): 80,000 Lbs. or Gallons Used: 2000 gallons Material Used For Stabilization: Lime � O a)- fd 7 C14 N 7 O M 0 7 O M V) 7 M MMN U) 7 N 7 O N 7 N N 7 O t/) 7 c O N 7 7 O V) 7 O 0 7 O O O 0 7 O O U) 7 M Oo O N 7 O w D C oO O N > C rnO o U) > C N 0 j C ) 0 V) 7 C 0 N 7 C 0 w 7 C IT 0 0) C N N 0 N 7 C O of 0 0 C CO c7 0 0 C (D 0) 0 U) C O) MO 0 w C Nv 0 U) C IvnC 0t 0 C U C- O M M M M r- M M M LO M 'IT M M M N M M O M 0 N 00 N ti N W N L0 N N co N N N N O N M 00 1— '0 M r— 'cr M N O r' F— Hour pH Operator Corr. Corrected Initials Time Factor + pH JDW -0.061 12.211 10:0 LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Richlands WVVfP Batch Size (gallons): 80,000 Lbs. or Gallons Used: 2000 gallons Material Used For Stabilization: Lime c ` O U t 0 �'- LD O fd 7 ,a O fA 7 n. M MMMMN O N n. M O M 7 a M O fq 7 a O O M 7 a O N 7 a N O fD 7 a O fn 7 a a2 O tl) 7 M O to 7 M O M 7 a CO O U/ 7 Q- CO O fA 7 n co O Ul 7 a O Cl) OO O N C :E to O Vl C 2 rn O O N C 2 C a O N C 2 -- O N C 2 NN O W C IT O N C :E � N O N C 2 O M O W C 2 r) q O tl1 C 2 co Co O W C 2 rn q O N C 2 N v O tll C 2 n 't O N C U n. N O O M M M r` M O M L0 M It M CM M CV M M O M CA N Co N I-- N CO N LO co N r- O M Co r` CO LO 'It CO N O I— LOWS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS 2 01 So ZZ Facility Name: ONWASA Richlands WWTP P.O.# 611194" Contact Name: Mark Young Phone: 910-340-9256 Batch Sine (gallons): Lbs. or Gallons used: 2000 gal Material Used For Stabli zation: Lime E2 pa ...: � O .► a O ao a.`. O w O w a O w a O w a O a a N O N Q. N O m a a co O vl o a it) O d� a O � > a O ul > a O W o a O en � O O � O O � O � $ N 4 [i � r O > O > N O � N O � N O � l+! O � O � W O 7 $ no O � 4O O � g O � U H O ECDO co O co �R M M N M M O th CD N c0 N 1- N c0r-OOCO1�tDM�}er N N N N N N N ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Mules) Facility dame: Lewis Farms and Liquid Waste, Inc. WWTP Name: Richlands WQ Permit Number: WQ0000455 NPDES Number: NC0023230 Monitoring Period: From 1/1/2014 To 12/31/2014 Alt_ 1 (VS reduction) x= Alt. 2 (40-day bench) Alt. 3 (30-day bench) l Alt. 4 (Spec. Oz uptake) Alt. 5 (14-Day Aerobic) j Alt. 6 (Alk. Stabilization [Y Alt 7 (Drying - Stable) i. l Alt. 8 (Drying - Unstable) 1 Alt. 9 (Injection) 1D Alt. 10 (Incorporation) L—] No vector attraction reduction alternatives were performed w) CERTIFICATION STATEMENT (please check the appropriate statement) G6I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ,- "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1. 106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "'Phis determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mark Young, Supervisor Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) S' nature of .�a& Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 20, 2014 River Bend 2.84 % Solids 7.46 nH Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight x 10,000 Pounds/Dry Ton Mg/KgMg/Kg x 0.002 Nitrogen (TKN) 7.160 71,600.000 143.200 Phosphorus 1.870 18,700.000 37.400 Potassium 0.255 2,550.000 5.100 PAN (infected)* 2.547 25,467.000 50.934 PAN surface)* 2.272 22,722.000 45,444 Ammonia Nitrogen 0.549 5,490.000 10.980 Calcium 5.770 57,700.000 115.400 Calcium Carbonate E . --- --- --- Magnesium --- 2,350.000 4.700 Sodium --- 5,000.000 10.000 Sulfur --- --- --- Nitrate N / Nitrite N --- 144.000 0.288 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 4,260.00 8.520 Arsenic --- 2.36 0.005 Cadmium --- 2.36 0.005 Chromium - 13.100 --- Copper --- 813.00 1.626 Lead --- 12.50 0.025 Mercury 1.02 0.002 Molybdenum --- 4.65 0.009 Nickel --- 11.40 0.023 Selenium --- 8.98 0.0] 8 Zinc --- 845.00 1.690 Environmental Chemists, Inc: 2014-14446 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Wmdmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) ® 710 Bowsertown Road • Manteo, NC 27954 ANALYTICAL & CONSULTING (252)473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Town of River Bend Date of Report: Dec 10, 2014 45 Shoreline Drive Customer PO #: New Bern NC 28562 Customer ID: 12110004 Attention: Brandon Mills Report #: 2014-14446 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-35426 Site: sludge 11/20/2014 10:30 AM Solid/Sludge Tom Harper Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 4260 mg/kg 12/02/2014 Arsenic EPA200.7 <2.36 mg/kg 12/02/2014 Cadmium EPA2W.7 <2.36 mgikg 12/02/2014 Calcium EPA200.7 57700mg/kg 12/03/2014 Chromium EPA200.7 13.1 mg/kg 12/02/2014 Copper EPA 200.7 813 mg/kg 12/04/2014 - Lead EPA 200.7 12.5 mg/kg 12/02/2014 Magnesium EPA200.7 2350 mg/kg 12/0312014 Molybdenum EPA200.7 4.65 mg/kg 12/03/2014 Nickel EPA20D•7 11.4 mg/kg 12/02/2014 Potassium f EPA200.7 2550 mg/kg 12/03/2014 Selenium, EPA200.7 8.98 mg/kg 12/02/2014 Sodium EPA200.7 5000 mg/kg 12/03/2014 Zinc EPA200.7 845mg/kg 12/02/2014. Ammonia Nitrogen EPA350.1 5490 mgikg 11/24/2014 Total Kjeldahl Nitrogen (TKN) EPA3512 71600mg/kg 11/28/2014 Nitrate+Nitrite-Nitrogen EPA$532 144mg/kg 12/08/2014 Total Solids (%) sM254oB 2.84% 11/24/2014 pH SM4500 H B 7.46 units 11/28/2014 Total Phosphorus SM4500 P F 18700 mgikg .11/26/2014 Mercury SW8467471B 1.02 mg/kg 11/26/2014 Comment: Results, except pH reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report #:: 2014-14446 Page 1 of i dml GM 9 ENVIRONMENTAL CHEMISTS, INC OFFICEIn910`32-42 3'IFAX 910392-44245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: Town of Riverbend WWTP PROJECT NAME: Annual Sludge REPORT NO: ADDRESS: 45 Shoreline Drive CONTACT NAME: Brandon Mills, ORC PO NO: New Bern, NC 28662 REPORT TO: PHONE/FAX: 252.229.2813 r— COPY TO: email: Sampled By. SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, Si_ = Sludge, Other: Sample Identification Collection y c `o C o "" c E " m U 3 z PRESERVATION ANALYSIS REQUESTED Date Time Temp z Z = _ _ c g = o e C XSlud msludge analpsis) -p'. G C P G G C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By, Dateffirne Received By: DateTme 2. Temperature when Received: Acc d: '� Re' Resample lge es d: Delivered By: Received B Date: gTim Comments: TUO ND: -LEWIS" FARMS OF R URGA W, INC. WQ0000455 ALKALEIT STABILIZATION OF WASTEWATER BIOSOLIDS Batch Size (gallons) Lbs. of Lime Initial pH - >12 pH 2 Hour pH 24 Hour pH - Operator Do tc PH Temp'C Corr- Factor r Cormtcd PH Time pH Tcmp'C Corr. Factor+ Corrected pH . Time P H Tan C P • �� Factor+ Co ntcted H Time pH Tcm C P Factor+ _ Corrected ed PH � tnitiak /if 1 F.3y C�•Y`� �i �o a' a / .13 1 7.1 :H� a. r 3A -,34 I�.v�. 10-,V5 1A.34 f3.1 r 36 i -d 3 I =At 4.3i 15, f • . 30 /J.0i 10,0,0 +� 1% -11-M. 7 ,9' 7/-S to, 4 . 6.3 _ Y� '.06 s3 .03 6_L? a3 7 IT 7, iH :o� Aoir s '93' 19-0 ;xtr 3.0o o / .3 : •D 9 Q•Q. 12.0 r-7 Z ab. 3 �. S 73 q 0.0� p.ol v�3 i S� 117.1 1 0_ 1 C .1 I�.�3 1�-30 16''1b yp S 8 art ' �S l.:St?t:is- 12. t4 a:2 !S f� ( $ 7. �7. ( ".'t> i).vo 1 0.06 Ia.So /a;10 Q :'�R i2�4 a 30 /o?=� (:oo Ia 3s A•K7 _�� _-,7 a.a3 N. a .7 &6.3 +.33 0_��; 10.1,qa: a7 •.:Oq 1,0.y5 1 0- 7. (g <o0 7. t9 : nv 3 aS.`f o J. `ff a:vo Comments: K. DATE Ay I A/ SOURCE _ ,VAJ 7",° . - 10 .O N h •--• O Q o `S O c•l o raj Ci rM'1 O M O N N C N O C o O C O M O O C O O 'O ••" p p Lo — ti N tl' N t� N O .� M M M M •.rr• v Ci C C. p G O p o O C c5 O C o 7 a 7 H 7 7 7 7 7 U G G C C C C_ C_ � C 7 7 7 _G _C U G O Q T M oo M r InIn .o M •.ry M v t1 M N — O O� 00 r` In IN � oa ' InM In N N N c4 N N N N . [� •O •.•1 Q 2 N O ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: River Bend NPDES Number: NC0030406 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt : A (time/temp) ; ° ❑.: ;Alt B• (A1k: Treatmeul)[]:: AIt.'.C: (Prior Testing) t' Alt: (No Prior. Test) ❑ ­piocess`fv )iurf iBr. Reduce ?at]ioobt s ..0 If applicable to altervative.performed(Class A . ): dicate:"Process to'Furthe'r*Reduce Pathogens Compost 131 464t Drying ❑ .�Ieaf. TTreatinent .❑ T iei nophilio Beta Ra 131 G��iiiina Ra ❑ Y Past6urization ❑ Class B: Alt(1) Fecal:Densi ❑. Alti.(2)Process to Si' 'ficanntl Reduce Pathogens ❑ If applicable to alternative erforiiied (Class B onl .indicate IT rocess-to "Si nificaiitl _Reduce•Patho ens" Lime Stabilization © Air. Drying ',❑ Golu _ostin 0: .. Aerobic bigesti'on ❑ Anaerobic Digestion. _;:}: 5. If applicable to alternative performed (Class A or Class B) complete the llowing monitoring data: Parameter Allowable Level in in Sludge Pathogen Density g tY Number o Excee- dences Frequency of Analysis y Sample Type Analytical Tech - ni ue Minimu Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) vector attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative uerformed: Alt,1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAIL 4 (Spec. OZ. uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ® Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ iNo Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ vector attraction- reduction alternatives were performed ❑ CERTIFICA11ON STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met" ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been net I am aware that there are significant penalties for false certification including fine and imprisonment." Brandon Mills, ORC _ Pre er Name and Title (type or print) Signature of Preparer* Land Applier Name and Title (if applicable)(type or print) Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: May 24, 2014 Sherwood Mobile Home Park Permit No. W00000455 1.33 % Solids 7.45 PH N°,=° F Parame#en � � °lo�: 11Ig/I{gDr��Ve�ght °1m i 3`0,00.0 Poueids/DryTon, i K x 0rQ02 Nitrogen (TKN) 13.400 134,000.000 268.000 Phosphorus 6.230 62,300.000 124.600 Potassium 0.405 4,050.000 8.100 PAN (injected)* 4.039 40,389.300 80.779 PAN (surface)* 4.031 40,311.800 80.624 Ammonia Nitrogen 0.016 155.000 0.310 Calcium 3.240 32,400.000 64.800 Calcium Carbonate E . --- --- Magnesium - 6,210.000 12.420 Sodium - 5,330.000 10.660 Sulfur --- --- --- Nitrate N / Nitrite N --- 80.800 0.162 Barium --- --- Chloride --- --- --- Iron - --- --- Aluminum - 7,400.00 14.800 Arsenic - 7.44 0.015 Cadmium --- 7.44 0.015 Chromium --- 23.400 --- Copper --- 226.00 0.452 Lead - - 22.30 0.045 Mercury - 0.23 0.000 Molybdenum --- 7.44 0.015 Nickel --- 22.20 0.044 Selenium - 7.44 0.015 Zinc - 5,290.00 10.580 Environmental Chemists, Inc. 2014-06240 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc, 6602 Windmill Way • Wilmington, NC 28405 envirochem(910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #194. DLS CERTIFICATE #37729 Lewis Farms & Liquid Waste, INC. Date of Report: Jun 18, 2014 8155 Malpass Corner Road Customer PO #: Currie NC 28435 Customer ID: 14020008 Attention: Wesley Wooten Report #: 2014-06240 Project ID: Sherwood MHP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-15074 Site: Sludge 5124/2014 9:50 AM Solid/Sludge J. Marty Fritz Test Method Results Date Analyzed Sludge Residuals Aluminum EPAM.7 7400 mg/kg 06/16/2014 Arsenic EPA200.7 47.44mg/kg 06/03/2014 Cadmium EPA200.7 <7.44 mg/kg 06/03/2014 Calcium EPA200.7 32400 mg/kg 06/09/2014 Chromium EPA200.7 23.4mg/kg 06/03/2014 Copper EPA200.7 226 mg/kg 06/03/2014 Lead EPA200.7 22.3 mg/kg 06/03/2014 Magnesium EPA200.7 6210 mg/kg 06/09/2014 Molybdenum EPA200.7 <7.44mg/kg 06/03/2014 Nickel EPA200.7 22.2 mg/kg 06/03/2014 Potassium EPA200.7 4050 mg/kg 06/09/2014 Selenium EPA200.7 <7.44 mg/kg 06/03/2014 Sodium EPA200.7 5330 mg/kg 06/17/2014 Zinc EPA200.7 5290 mg/kg 06/03/2014 Ammonia Nitrogen EPA 350A <165 mg/kg 06/05/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 134000 mglkg 06/05/2014 Nitrate+Nitrite-Nitrogen EPA353.2 80.8 mg/kg 06/11/2014 Total Solids (%) SM 2540 B 1.33 % 06/02/2014 pH SM 4500 H B 7.45 units 06/05/2014 Total Phosphorus SM 4600 P F 62300 mg/kg 06/05/2014 Mercury SVV8467471B <0.226 mg/kg 06/09/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Report*: 2014-06240 Page 1 of 1 6602 Windmill Way Wilmington, NC 28405 ENVIRONMENTAL CHEMISTS, I N C OFFICE: M 392-0 23 FAX 910-3 2-4424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Info@environmentalchemists.com Analytical & Consulting Chemists ^r%i r cf -rrnnl Arun f%LAAIIu r%= rl IQTr1nV CLIENT:w1 S PROJECT NAME: �J. REPORT NO: - a` ADDRESS: CONTACT NAME: PO NO: REPORT TO: PHONE/FAX: COPY TO: emall: T1 .. — . ram'_ ....- CA\.131 C TVDC. 1 .. Infl,—+ F = Kffhlnn+ W = Wall_ ST = Strpam_ SO = Soil SL = Sludae. Other: Sample Identification Collection d E a ~ Q `o �° O _ =C9 i0 `o O a CJ `�+ U E OW m J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp z 2 = c N 0 2 0 2 0W. 1 ti R ,�`/ / i5o G G C P G G C P ^� y G C G P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Recelvea: o% . Accep>:ea: N/ Delivered By:T. Wx& Erl k-7- _Received Comments: TURNAROUND: Q 00004.55 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIOS Facility Name: Sherwood Mobile Home Park P.O.# Batch Size (gallons): 20,000 Lbs. or Gallons Used: 950 Lbs Material Used For Stabilization: Lime c O C O � �-'- O [A = a O ff1 a M O N a M C7 N a f'7 O N a ON M O O (n N ii a N O a N o a b a O n_ O a C7 n_ C7 a ci 5- O m o y N o p o N t7 v1 N 0 N r 0 H N o ui M CJ N cM+> o y M o V M 0 ui o N d a N CD M M C 0 M I- M CD Co LO Cr Co M M C+7 N M c- M O Co M N C D N r- N C.O N tC> N It N M N N N N r M N CD ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number. WQ0000455 WWTP Name: Sherwood Mobile Home Park NPDES Number. NCO022462 Monitoring Period: From I/l/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) -Please indicate level achieved and alternative erformed• Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ p Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (glass A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thennopltilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens p If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Rl Air Drying ❑ Com ostino ❑ jAerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative performed Class A or Class B) complete the following monitoring data: Allowable Level en Density Pathogen g um c` ° Sample na ytrca Minimu Geo. Mean aximu Units in Sludge d n e Lrcquency f Analysis Type Tech- 2 x 10 to the MPN ni c 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) wei t) Vector Attractinn Y2PAnrfinn 17 C A Wt• A n nlf•r t t n.n Alt.I (VS reduction) ❑ -- , Alt. 2 (40- day bench) ❑ - •-�-----Ug%,a« aaaV.r uauve performea: Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. O, uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (injection) ❑ Alt. 10 (Incorporation) R1 No -vector attraction redaction alternatives were performed ❑ CERTIFICATI_0N STATFMFNT i..i__ ..>,, ---- ---- - kr.. 046 _ V.Lft auc appropriate statement) - "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in ISA NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." J. Marty Fritz, (ORC Lime Stabilization) _ Preparer Name and Title (type or print) Land A2Z��2�able)(ty a or print) gnature o parer# Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 25, 2014 Sterlin1l Farms WWTP Permit No. WQ0000455 2.29 % Solids 6.6 pH Parameter I % JMg/Kg Dry Weight x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 1.000 66,900.000 133.800 Phosphorus 2.020 25,400.000 50.800 Potassium 1.010 6,590.000 13.180 PAN (injected)* 0.342 3,419.700 6.839 PAN (surface)* 0.326 3,259.200 6.518 Ammonia Nitrogen 0.032 4.100 0.008 Calcium 8.720 25,200.000 50.400 Calcium Carbonate E . --- --- --- Magnesium --- 4,41a.000 8.820 Sodium --- 5,630.000 11.260 Sulfur --- --- --- Nitrate N / Nitrite N --- 195.000 0.390 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,770.00 5.540 Arsenic --- 3.23 0.006 Cadmium --- 3.23 0.006 Chromium --- 23.800 --- Copper --- 212.00 0.424 Lead --- 6.94 0.014 Mercury --- 0.87 0.002 Molybdenum --- 4.58 0.009 Nickel --- 12.90 0.026 Selenium --- 9.65 0.019 Zinc --- 4,590.00 9.180 Environmental Chemists, Inc. 2014-14675 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. • 6602 Windmill Way ' Wilmington, NC 28405 (910) 392-0223 (Lab) ' (910) 392-4424 (Fax) sM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Aqua America of North Carolina Date of Report: Dec 16, 2014 105 Hampstead Village BLDG 24-1 Customer PO M Hampstead NO 28443 Customer ID: 08110027 Attention: Don Williams Report #: 2014-14675 Project ID: Sterling Farms Lab ID Sample ID: Collect DatelTime Matrix Sampled by 14-36011 Site: Digester 11/25/2014 3:00 PM Solid/Sludge Client Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 2770 mg/kg 12/02/2014 Arsenic EPA 200.7 <3.23 mg/kg 12/02/2014 Cadmium EPA200.7 <3.23 mg/kg 12/02/2014 Calcium EPA 200.7 25200 mg/kg 12/03/2014 Chromium EPA 200.7 23.8 mg/kg 12/02/2014 Copper EPA200.7 212 mg/kg 12/02/2014 Lead EPA 200.7 6.94 mg/kg 12/02/2014 Magnesium EPA200.7 4410mg/kg 12/03/2014 Molybdenum EPA200.7 4.58mg/kg 12/03/2014 Nickel EPA200.7 12.9 mg/kg 12/02/2014 Potassium EPA200.7 6590 mglkg 12/03/2014 Selenium EPA200.7 9.65 mg/kg 12/02/2014 Sodium EPA200.7 5630 mg/kg 12/03/2014 Zinc EPA 200.7 4590 mg/kg 12/02/2014 Ammonia Nitrogen EPA350.1 4.1 mg/kg 12/03/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 66900 mg/kg 12/10/2014 Nitrate+Nitrite-Nitrogen EPA353.2 195mg/kg 12/15/2014 Total Solids {%) SM 2540 B 2.29 % 12/01/2014 pH SM450DHB 6.60units 11/28/2014 Total Phosphorus SM 4500 P F 25400 mg/kg 12/10/2014 Mercury SW0467471B <0.873 mg/kg 12/05/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. r Reviewed by: Report #:: 2014-14675 Page 1 of 1 Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCOENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 r+ni i er%1rinN ANn r•14Aiti n= (% QTnnv 6602 Windmill Way Wilmington, NC 26405 OFFICE: 910-392-0223 FAX 910-392-4424 ]nfo@environmentalchemists.com CLIENT: f c' A PROJECT NAME: REPORT NO: — ` u ADDRESS: lO5 a j'1='V v///, CONTACT NAME: %b.1 Wi�/r'�rMf PO NO: SaN 2Lf 17 REPORT TO: Pon W;lf 14"ff PHONEIFAX: 11a'1 5'f6z-d c Z fW 3 COPY 7'.O: email: �.....�i,.a 0— QAUP1 F TVPF- I = Influent- E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludge. Other. I Sample Identification Collection ANALYSIS REOUESTED Donegan Transfer Relinquished By: Temperature Delivered By. Comments:_ > Date: I TURNAROUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Sterling Farms P.O.# Batch Size (gallons): 40,000 Lbs. or Gallons Used: 500 Ibs Material Used For Stabilization: Lime - • • • • I HourPH.s. .. MENEM MEN - B M EMMEM ME M � C �, o T_J C � D � 'W O 7 a N rY O 7 a M o 7 a cD M o 7 n M M O 7 c O M o 7 e- h N b 7 M eY N O 7 a N o 7 a c0 0 7 M 0 7 a- N o 7 M W O C7 7 ii (O o O 7 P- c+] b O 7 `a O cn o G In o G Or a G C G - > G > C 7 C C > C > C > C ] C G C g � C s U rL O d CA M 00 c^ Ih M c0 M Lo"t M M M M N M M O M M N Go N�- rl- (9 �0 d' M N O O M t` Cfl et M N O F- LE.WIS'FARMS AN® LIQUID WASTE; INC. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Sterling Farms NPDES Number: WQ0029475 Monitoring Period: From 1/l/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt R (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) p .. Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost 131 Heat Drying ❑ 1 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ra ❑ . Pasteurization ❑ Class B: Alt. (1) Fecal Density ❑ � Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic ob c Digestion ge st on ............,..:...............:............::::.,:.....:....:.:;,::::.;.::..::::...::.:.;::..:.::.:::....:.:: If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number o Excee- dences Frequency 1ofAnalysis Sample Type Analytical Tech- i ue Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power. per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) I 3 MPN per 4 grams total solid (dry weight) vector Auracnon Reduction (15A iVCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ It. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) Q No vector attraction reduction alternatives were performed ❑ CEK IMkIC —FION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system T designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Preparer N me d itl type or rint 2 r Signature Preparer* Land Applier Name and Title (if applicable)(type or print) 3-/s- Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 5, 2014 Swansboro 2.68 % Solids 6.2 n14 Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight x 10,00�� Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 2.700 27,000.000 54.000 Phosphorus 0.106 1,060.000 2.120 Potassium 0.302 3,020.000 6.040 PAN (injected)* 1.353 13,531.400 27.063 PAN (surface)* 1.338 13,380.400 26.761 Ammonia Nitrogen 0.030 302.000 0.604 Calcium 3.880 38,800.000 77.600 Calcium Carbonate E . --- --- --- Magnesium - - 1,920.000 3.840 Sodium --- 3,630.000 7.260 Sulfur --- --- --- Nitrate N / Nitrite N -- 5,220.000 10.440 Barium --- --- --- Chloride --- --- --- Iron --- --- Aluminum --- 4,930.00 9.860 Arsenic --- 3.32 0.007 Cadmium --- 3.32 0.007 Chromium --- 16.900 --- Copper --- 451.00 0.902 Lead --- 17.60 0.035 Mercury --- 2.16 0.004 Molybdenum --- 5.74 0.011 Nickel --- 12.40 0.025 Selenium --- 6.98 0.014 Zinc --- 3,720.00 7.440 Environmental Chemists # 2014-02574 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Onslow Water & Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention: Todd Roberts Date of Report: Apr 07, 2014 Customer PO M Report M 2014-02574 Report to: Todd Roberts Project ID: Swansboro WWTP Lab 1D Sample ID: Collect Date/Time Matrix Sampled by 14-06236 Site: Sludge 3/5/2014 7:10 AM Solid/Sludge Aubrey Shirley Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 4930 mg/kg 03/13/2014 Arsenic EPA 200.7 <3.32mglkg 03/13/2014 Cadmium EPA 200.7 <3.32 mg/kg 03113/2014 Calcium EPA200.7 38800 mg/kg 03/12/2014 Chromium EPA 200.7 16.9 mg/kg 0311312014 Copper EPA 200.7 451 mg/kg 03/13/2014 Lead EPA 200.7 17.6 mglkg 03/14/2014 Magnesium EPA 200.7 1920mg/kg 03/12/2014 Potassium EPA 200.7 3020 mg/kg 03/1212014 Selenium EPA 200.7 6.98mg/kg 03/14/2014 Sodium EPA 200.7 3630mg/kg 03/12/2014 Zinc EPA 200.7 3720mg/kg 03/14/2014 Molybdenum EPA200.8 5.74mg/kg 3/28/2014 Nickel EPA200.8 12.4 mg/kg 3/20/2014 Ammonia Nitrogen EPA350.1 302 mg/kg 03/19/2014 Total Kjeldahl Nitrogen (TKN) EPA3512 27000mg/kg 03/26/2014 Nitrate+Nitrite-Nitrogen EPA353.2 5220mg/kg 03/21/2014 Total Solids (%) SM 2540 B 2.68 % 03/10/2014 pH SM4500HB 6.20units 03/11/2014 Total Phosphorus SM 4500 P F 1060 mg/kg 04/03/2014 Mercury SW04674718 2.16 mg/kg 04/01/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: Ili Report#:: 2014-02574 Page 1 of 1 Way ENVIRONMENTAL CHEMISTS, INC OFFICE: 9101-392-0223FIAX910-3 2-4424 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION * 94 NCDHHS: OLS CERTIFICATION * 37729 Info@envlronmentalchemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: ONWASA - PROJECT NAME: REPORT NO: ADDRESS: 228 Georgetown Road CONTACT NAME: A4,w LJ. £ PO NO: Jacksonville, North Carolina 28640 REPORT TO: / 1 0. ,94Vf PHONE/FAX: I D Q3 7 - 7S' 711 PO#: ICOPY TO: Todd A Roberts email: £ Vt1&1A4•?- • Samnled SAMPLE TYPE! 1 = Influant_ E = Effluant_ W = Walt. ST a Stream_ Rn Snil_ SI_ = SluAna_ no -are Sample Identification: MMMME8188818:11 ANALYSIS REQUESTED M. P75 �Ma� "'-) Relinquished By: A emperature c ved: o �- Accepted: Rejected: Resample Requested: 1 ` Delivered B . ' 3 Received By: Date: Time: Comments: ITURNAROUND: LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Swansboro WRF P.O.# Batch Size (gallons): 245,000 Lbs. or Gallons Used: 2000 Material Used For Stabilization: Lime C LO N O 't O (O M M 0 O N VN rN- OM MM 0M MM N w . OOOO v N V V ]co O O O o O O O O O O O O O O O N U O O O O O O O O O O O O O O OCU O �1 y N M1 N N N 41 N N f/1 N N N ql Ol N N fn fn N Vl V) N N fA Ul N fq 7 7 7 > > 3 7 7 7 7 7 7 7 7 LL 7 7 7 7 7 7 7 7 7 7 7 7 7 7 7 C C C C C C C C C C C .0 C C C a ELEL a a- a a a a a EL a a a FL2 2 2 2 2 2 2 2 2 2 2 U C)- O O CO M co N O O CO M LO d' CO N — O M 00 f— CD (n 'T co N CD I- LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Swansboro WRF P.O.# Batch Size (gallons): 150,000 Lbs. or Gallons Used: 2000 Material Used For Stabilization: Lillie MEE C L N U Cu � LO st U) 7 a N 'd' UI 7 M co U) 7 a w M U) 7 a n Cl) O U) 7 a O cM O U) 7 M f� N O U) 7 M sF N O U) 7 M N O N 7 M 00 O U) 7 M t!7 O U) 7 n. N_ O fA 7 a m O O U) 7 a (O O O U) 7 a M O O U) 7 0- O co O 0 N C 2i to O 0 W C 2 0) o 0 N C 2 N o 6 C 2 N 0 W C ao 0 W C 2- N 0 N C 2-'2 t N 0 W C f` N 0 N C 2 o ro 0 U1 C 2 c) M 0 fA C co C) fq C 2�� fn M 0 W C N a 0 rn C u) 0 y C 2 U C- O V O M Co M r` M (.0 M LO M M C') M N M M O M O N 00 N r` N (D N U) N V N M N N N N�- O M Co 1,- 10 � M N r O H LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Swansboro WRF P.O.# Batch Size (gallons): 200,000 Lbs. or Gallons Used: 2000 ibs Material Used For Stabilization: Lime MEE '�®®® '�®®® '�®®® • '�® U +•' N U CU 0a O fA O f/1 a O U1 a O p1 a O M a O tll a O fA a CD N o O M o O N d O fn a O to d O Ul a O tll n• O N a O O o N 3 O N 7 o N 7 o j o N 7 O V1 7 o 41 C O N 7 N O fq > o O y > co O N 7 co O N 7 ) c O N 7 v o f/1 > no v 0 N > U cL E O d M c7 co M ti M M c'M to M d' co M M N M M O M M N M N ti N CD N to N V N M N N N N O N (M Co 1- •- 0 �- LO 'It M r O H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Swansboro NPDES Number: WQ0023261 Monitoring Period: From l/l/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) [3 Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs 0Tin If applicable to alternative performed (Class -A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ;>:;: ° =- _ _ t. ,.. Class B: JAIL (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ "='r " If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization p Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Di est' ton b :.:: �::; P �. .. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge g Pathogen Density Number 01 Excee d nces Frequency of Analysis y Sample Tie �'ca Tech- ni ue Minimum Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.] (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization 21 jAlt 7 (Drying - Stable) ❑ Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 INo vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check theappropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Allen Rhue, ORC Preparer Name and Title (type or print). ,4l.Geil W. MW Signature of Preparer* Wesley Wooten, President Land Applier N� a itle (if applicable)(type or print) 6 Feb 15 w ,.fir /C"— Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 14, 2014 Taylor Extended Care Permit No. WQ0000455 1.90 % Solids 7.1 off Parameter % Mg/Kg Dry Weight (% x 10,000 Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 1.437 14,367.000 28.734 Phosphorus 0.513 5,127.000 10.254 Potassium 0.288 2,881.000 5.762 PAN (injected)* 0.508 5,078.930 10.158 PAN (surface)* 0.455 4,554.430 9.109 Ammonia Nitrogen 0.105 1,049.000 2.098 Calcium 2.338 23,379.000 46.758 Calcium Carbonate E . --- --- --- Magnesium - 2,575.000 5.150 Sodium --- 15,742.000 31.484 Sulfur --- --- --- Nitrate N / Nitrite N --- 34.530 0.069 Barium --- -- -- Chloride --- --- --- Iron - --- --- Aluminum --- 3,231.00 6.462 Arsenic --- 2.50 0.005 Cadmium - 0.60 0.001 Chromium --- 9.000 --- Copper -- 1,855.00 3.710 Lead --- 38.00 0.076 Mercury --- 3.60 0.007 Molybdenum --- 5.00 0.010 Nickel --- 17.00 0.034 Selenium --- 5.00 0.010 Zinc - 809.00 1.618 Environment I, Inc. # 381A *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. �.� y --7 4 t�iiir�441 I'£~41~x5. ff'�`f f�. rY'(^`ft; L..Lj�t� �Si £E'•€?J*i13=.ss!,j i� i�f.� £ii f�lii1 t.d?! i (£ aL% PARAMETERS PH, Units Aluminum, (dry wt, basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt, basis), nzglkg Cadmium (dry wt. basis), mg/lcg Copper (dry wt. basis), mg/kg Chromium, T.(dry wt. hasis),mg/kg Lead (dry weight basis), zug/kg Magnesium (dry wt. basis), zng/kg Mercury (dry wt. basis), mg/kg Nickel (dry At. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), zng/kg Zinc (dry wt. basis), mg/kg Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt,),nlg/kg Phosphorus, T. (dry wt.), nzg/kg Nitrate -Nitrite (dry wt.), mg/kg Molybdenum (dry wt, basis), mg/kg Sludge Analysis lYlethod Sample Date Analyst Code 7.1 01/16/14 TRB 4500HB-00 3231 01/29/14 LFJ EPA200.7 <2,5 01/30/14 MEL 3113B-04 23379 01/29/14 LFJ EPA200.7 0.6 02/06/14 MEL 3113B-04 1855 01/29/14 LFJ EPA200.7 9 01/29/14 LFJ EPA200.7 38 02/04/14 MEL 3113B-04 2575 01/29/14 LFJ EPA200.7 3.6 01/17/14 ADD 245.1 R3-94 17 01/29/14 LFJ EPA200.7 2881 01/29/14 LFJ EPA200.7 <5.0 02/03/14 MEL 3113B-04 15742 01/28/14 ADD 3111B-99 809 01/31/14 ADD 3111B-99 1.9 01/17/14 MJAB 2540G-97 14367 01/21/14 ANO 351.2 R2-93 1049 01/21/14 ANO 350.1 R2-93 5127 01/21/14 ALB 365.4 -74 34.53 01/17/14 ANO 353.2 R2-93 <5.0 01/29/14 LFJ EPA200.7 FAX ID#: 381 A DATE COLLECTED: 01/14/14 DATE REPORTED : 02/10/14 f. REVIEWED BY: fyrj 756- F0107— q7 ' Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473 5702 ANALYTICAL& CONSULTING CHEMISTS NCDLNR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Environment -1 Date of Report: Feb 06, 2014 Post Office Box 7085 Customer PO #: Greenville NC 27858 Report#: 2014-00716 Attention: Deedee Woolard Reportto: Deedee Woolard Project ID: heritage Healthcare a@ Taylor Place Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-01780 Site: Sludge Sample 1/14/2014 8:30 AM Solid/Sludge Patricia Davis Test Method Results Date Analyzed RCI Cyanide EPA335.4 <0.127mg/kg 01/3112014 pH sM 4600 11 s 7.43 units 01/23/2014 Sulfide SM4500 S D 0.45 mglkg 02/03/2014 Ignitability SW 840 mellmd 1010 >212 °F 0112912014 Comment; Results reported on an as received basis, Reviewed by: fie- Iitl; ��.12,r�C:1/wL ROPOMP- 20t4-00718 Page 101`1 Environment 1, Inc. P O. Box 7085, 114 Oakmont Dr. CHA3N OF CUSTODY RE' CORD Page 1 of i Pbone (252) 756-6208 • Fax (252 )756-0633 DIS1NFEC110N CHLORINE NEUTRAUZEDATCOLLECTION CHGO1tTNE C�,�' Iri'�: 381 A Week: 7 Q UVPH CHECK (LAB) EMt1TAGE 11EALTSCARE Q TAY] OR PL qMrNONE P' P P P P P r P P P CONTAINER TYPF, PIG ATIN. STACEY ELOT A A A A A A A A A A CHEMICALPRESERVATION P.O. BOX 100 SBA. LEVEL NC 23577 ❑ A -NONE D-NAOH a, {25� 7.7a-OlI2 F• zJv` LU B -.HNO, E - HCL o s S ,- � w z a � z .l;• � -� µ+ C- H2SOa F -ZINC ACECATEJNAOH COLLECTION ;C or o , !Z G - NATHIOSULFATE SAMPLELOCATION DATE TIME Sludge Sample / j 023 'j/A jse 6 R A' CLASSIFICATION: WASTEWATER (NPDES) DRINKINGWATER - DWCMW SOLIDWASTESECION CHAIN OF CUSTODY MAINTAINED DURING SHIPMENT/DELIVERY N SAMPLES COLLECTED BY: Please Pant) SAMPLES RECEIVED IN LAB AT o • 7 °C (SIC,) LER) F I U&E0 BY IN 1! DATEMME TSY(81,mDAMzMEa T! COMMENTS A /= i reap t`tto SHED BY D Tl1[WE RECEIVED17-1�1 DATErMAE Q I f3Y( �It7 M0 VED Y(SIG) It� DA E_ v PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a'V for composite sample or S "G" for N ? 274660 274Q60 Fnmm ffs Grab sample in the blocks above for each parameter requested. Plu:nic• i252) ? 6-(3-'08 - Fax t`'[ > ?56-,.)6'2,3 ; 1 CHLORINE-_iL^ IJEUTUZELMrWi-LFCTION C.:LIE Y: 381A Week:7 ! I f pHCHFCK L.A,3} _ HERITAGE HEALTHCARE TAYLOR PLF�/ ATTN': STACEY KRAFT SEA LEVEL NC 28577 C, <�, l ...,_._� _.„- A ! A Ii P 1 A I P A P A P A P A P A P I J .�,.,•..•� A JP A f ! I �araT.4lrlEn 7'�' F: PIG y` �4H�.il1I[CAL f I'{t;JE�"i ;'HTIlJ'�I I (L1 ' II IIE 1 f' ! A•NONE D -NA(i (252) 225-0112 w r. ! .,-J I ) — J i s 1 i ^ k •� ! •�' l 1 [ ! i Ito B - HNO, rE - HCL j t., = I-i.�-S()� i- ZiNC tU� ,JAL✓ I t 1P! k E AMPLC LOCATION DATE '-IPOF9 _:.- w K.014[ ' _.. i kJ T: � :1s i ' x c. Y. a lot 111j � "�. b� 2;f•.. ;79.. E• .. .7 %: r} j -;Z p Pk � k,. ii ;F .'cam .•�,y a .}F x a! �;p.... r~ ,F..,,; 1 � `.._....j l N1r` i H 10,1 F'i F I •-�S Sludge Sample 6 3 jej° 6 yg►y 3: t t 1. ANSI; IC,AT Il.nl: 'WASlg ab 0 E S) �--_ }.. ��:.,,_._,.�..a.._,�.:-�....., „s,.,.�..._.. �___. ,.,.�� _�.�.�,...,. �-�- !�.,� �.•—. _ _�.� � ._�.— I •__ 1 ! �_j C�RINKlt•JG4^:Ii+TF!? -.. SOLIDiVA� i t SEC:1'IOP�f CHAI,d Of CUSI-C,PY MAIN1AIP,!ED, i _..__ u!;!NU 8I=liPrtik_NTDE!.IVERY N i i ! � k:'t`L7ve LER) , fT?;!? iaF � R /., rV'•`Ctl'Y � ` j I DATF%TlME � ,. „ 1!�L .o - . L:lVLt:i knI i.n•[� ...� _�_ 'G r ! DATEFIME �fiELIPJ�t.1:1H�!.: a�i!:��! ',.} w -� s `!=vial I_L! 7�r I,�1� . t C?ATE-91ME Y--�,...�.�• - � _ .. _ _ f 3eI!EUNC U"'HED G,' su;.} OATE;�r M ! ! Rr_cL,jVE. ? ,y"S10.; i HT�-.rlrv+ �l t i 1 REP, ��� k �4 ; ( '=.(:� completing it ikii': Il fNiOi l llli�' /'e} ,f? ii Sampler lrlUsi lac a "C', for coo )side -sample rur a —` ," for �7 � 274960 � ry �+ -� - ? I1 5 tu�i t i -...,i .uwr� �. n r r reverse. I : j,=i. - R F I E 2@ 4 9 6 0 c.'.irab Si3.illple in (ill: I.11; cks -above for each p-arir-neter f?Ciueslod- 06 2C.15 09:08 252-66248L1 TCLVat?Ia P913E 01 r Qt E ..j O 1 O tPi ® ci �- � fl r c Q O +J Its t d Q 2 tL C r m NIA Bill i IMINMI1111 OF 11111111milli INS It IIYN 11■ �NRII 11 11 1 11 mt 111 WE Mill U11,191111011-10-11 WAIIIIIIIIIIIIII NNIIIIIIIIIIIIIII HIIIIIIIIIII NO $D'09nu" 01 BE'0 smnyy Z L Wo "M £ Ef.'a9riuNr! �L Y nc'0 snwyy � L VZ'A snuyY L L I.Z'o mu!w 8 L 9t 0 snug V 6 L, %,o inv it 0'L 8D"0u!W ZZ ao'o snv ty £Z so•oen,n}v YZ u 9Z C0'0 snIa 9Z 90"0 snld ZZ 60'0 Snld QZ ?i 0 snld 6Z 9> '0 snw OF 6i O"Id L£ LZ'0 snw Z£ iri'0 snBd £E LZ'O snld VE 0Va snici 9£ ££ 0 srnd 9E 9£'0 snld L£ WO snld 8£ cv 0 snld 6£ str'0 onld 0p JOj�E� dwel LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 $LKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Pea t }� I -I eA L "rdq � .�e� L P�1/�l P.O.# Batch Size (gallons): �c�Ca Lbs. or Gallons Used: �� Material Used For Stabilization: Lime MITT, M-Ow=N= CJAUffl RNFfMMNMIEN M.CD MkgPIA lr77iPA11V-C1!!,_[ END u r7m ffl 1, !��c�. ■i�� m c ` 0 - C GQ CS O . N O N o O O O O O O CIn oye gCCy pm r CmyC GNC Ca'cN n0,eN Oc Cc CC iCN? .0 Oo c O vc � U a EE O O) M Co M I- M (0 Cl) uA CO M CM N M M O M O) 'N Co N � N CO N O N Ne- M NN O O O ti (D in V CM N O F- P1r► 0'ctA `br°d-% o S/V 7 .54 8 L(. 01 y.o 1 lo.ol Z,v3 Il.614 12.5-0 10.01 ''!.o l i (. o o /2. 11i --r4r, 1 _ LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: PRUITT HEALTH To.r%� �,�„�_� C', P.O.# Batch Size (gallons): 3,000 Lbs. or Gallons Used: 200 Material Used For Stabilization: Lime •• m 1 I• 1 11 �m�� 1 1 • 1 ��� . 1 1 1 I I m c ` S it +-' N U (ti Lo V, O N 7 N '� O N 7 O Cl) O fq 7 t4 M O fA 7 M ('7 0 Vl 7 O M O M 7 ti N O (n 7 d' N O fq 7 N O (n 7 W O Vl =S O fA 7 N O U) 7 O O O V! =3 CO O O Nl 7 M O O N 7 O M O 0 In C m o 0 to C m 0 0 N C N 0 6 C u� 0 N C ao .- 0 W C N 0 Vl C �r N 0 N C n N 0 tl1 C O �n 0 tl) C r� M 0 tq C co m 0 N C rn 0 N C N a 0 Ul C Lo v 0 N C U CL E O T O co CO co 1,- co 0 co In co 'I M co CO N CO r- CO O CO CA N Co N ti N CO N to N 't N co N N N N O N M co N CO to d' co N O H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Taylor Extended Care NPIYES Number: NCO047759 Monitoring Period: Frown 1/112014 To 12/3 112014 Pathogen Reduction (I SA NC AC 02T .1.106) - Please indicate level achieved and alternative performed: Class A- I Alt, A (tirneheinp)' Alt B (Alk Treaunent) (Prior Testing) Od --r —Ait.l) (No Prior'l'est) j Process io Further Reduce Patlingeng If applicable to alternative performed (('lass A only) indicate "Process to Fuilher Reduce.Pathlwgens": C'onipost Elect DI-Vill- iD Heat Treatment --J ffict-mophilic 0 Beta Ray b (3 al irizatiou Fa,. ,lass B: Alt. (1) Fecal Density 0 Alt. (2) Process to Signifleantly Reduce Pathugens If applicable to alternative performed (("lass B only) indicate "Process to Significantly Reduce Pathogens": Lithe Stabilization i2i A-i r Drying S i Coaipostin? El jAerobic Digestion D Anaerobic Digestion IL"I ..... ....... ............... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of F'Xcec- dences Frequency or Sample V PC Analytical Tech - nioue Minimum Gco. Mean Maximun, Units Fecal Coliforni 2 x 10 to the 611) power per.graul Of total solids WIN 1000 mpn per grim of total said (dry weight) Salmonella bacteria (in ficu of fecal colifonn) 3 NIFN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt. I (\IS reduction) Alt. 2 (40-day bench) AIL 3 (30-day bench) Alt. 4 (Spec. 0, uptake) -- Alt. 5 (14-)day Aerobic) 'j Alt. 6 (Alk. Stabilization i All 7 (Drying - Stable) Oj JAlt. 8 (Drying - Unstable) i. Alt. 9 (hniection) 0 Alt, 10 (Incorporation) i, No vector attraction reduction alternatives were perfonned J CERTIFICAXION STATEMENT (please check the appropriate statement) "I certify, tinder penal4, of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in .15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1 106 and the 'Vector attraction reduction requirement in 15A NCACO2T.1 107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirement-,.) "This determination has been inade under my direction and supervision in accordance with the systcm designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." PatriciaT. Davis, ORC Prep, er "arne and "Title 6}1'pe Oar print) Land Applier Name and Title (ifapplieable)(q�pe or print) C— - — --- - - ---- ----- ------------------------- ...... . ........ . . . . ....... Sianatureof reparer" Date Signature of Land Applier (if applicable) Date *Preparer is delined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (1212006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: December 2, 2014 The Cape Permit No. 1.47 % Solids F 6 A nu Parameter % JMg/KgDryWeightJPounds/Dry x 10,000) Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 8.770 87,700.000 175.400 Phosphorus 1.800 18,000.000 36.000 Potassium 0.332 3,320.000 6.640 PAN injected)* 3.074 30,737.000 61.474 PAN (surface)* 2.790 27,902.000 55.804 Ammonia Nitrogen 0.567 5,670.000 11.340 Calcium 2.150 21,500.000 43.000 Calcium Carbonate E . --- --- --- Magnesium --- 2,610.000 5.220 Sodium --- 4,750.000 9.500 Sulfur - --- --- Nitrate N / Nitrite N --- 458.000 0.916 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 2,610.00 5.220 Arsenic --- 5.17 0.010 Cadmium --- 5.17 0.010 Chromium --- 19.300 --- Copper --- 265.00 0.530 Lead --- 12.30 0.025 Mercury --- 1.29 0.003 Molybdenum --- 5.17 0.010 Nickel --- 20.30 0.041 Selenium --- 6.94 0.014 Zinc --- 584.00 1.168 Environmental Chemists, Inc. # 2014-14834 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. I POOP, Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Aqua America of North Carolina Date of Report: . Dec 16, 2014 105 Hampstead Village BLDG 24-1 Customer PO #: Hampstead NC 28443 Customer ID: 08110027 Attention: Don Williams Report #: 2014-14834 Project ID: The Cape ' Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-36353 Site: Sludge 12/2/2014 10:00 AM Solid/Sludge Eric Youngs Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 2610 mg/kg 12/04/2014 Arsenic EPA 200.7 <5.17 mg/kg 12/03/2014 Cadmium EPA 200.7 <5.17 mg/kg 12/03/2014 Calcium EPA 200.7 21500mg/kg 12/03/2014 Chromium EPA 200.7 19.3 mg/kg 12/03/2014 Copper EPA 200.7 265 mg/kg 12/03/2014 Lead EPA200.7 12.3 mg/kg 12/03/2014 Magnesium EPA20D.7 2610mg/kg 12/03/2014 Molybdenum EPA 200.7 <5.17mg/kg 12/03/2014 Nickel EPA 200.7 20.3 mg/kg 12/03/2014 Potassium EPA 200.7 3320 mglkg 12/03/2014 Selenium EPA 200.7 6.94 mglkg 12103/2014 Sodium EPA 200.7 4750mg/kg 12/03/2014 Zinc EPA 200.7 584 mg/kg 12/03/2014 Ammonia Nitrogen EPA 35D.1 5670 mg/kg 12/09/2014 Total Kjeldahl Nitrogen (TKN) EPA 351.2 87700 mg/kg 12/1012014 Nitrate+Nitrite-Nitrogen EPA353.2 458mg/kg 12/15/2014 y' Total Solids {%) SM 2540 B 1.47 % 12/08/2014 _ pH SM 4500 H B 6.63 units 12/05/2014 Total Phosphorus SM 4500 P F 18000 mg/kg 12/10/2014 Mercury SW8467471B <1.29 mg/kg 12/05/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: ten. 1171e C2/ Report #:: 2014-14034 Page 1 of 1 mington ENVIRONMENTAL CHEMISTS, INC OFFICE: 910-3202 3iIFAX910392-44245 Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com COLLECTION AND CHAIN OF CUSTODY Client: AquaNC PROJECT NAME: Annual Sludge Analysis Caok REPORT NO: ADDRESS: CONTACT NAME: PO NO: REPORT TO: Don Williams PHONE/FAX: COPY TO: email: Sampled Bv: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection d A 'H E o d a (7 o IL" C ..� r E 9 ul m g z PRESERVATION ANALYSIS REQUESTED Date Time Temp z 0 i 0 r 0 Z o w o Sludge L C Nutrients/metals 4--)6 ([<� G C P I G G d C P G G C P G G C P G G C P G G C P G G C P G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: �26 , i Accepted: v OK Resample Requested: Delivered By: Received 13 ._ Date: iiwTime: ' ND: WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER RIOSOLI®S Facility fame: The Cape P.O.# Batch Size (gallons): 30,000 Lbs. or Gallons Used: 1500 gal Material Used For Stabilization: lime i • � ®■11•a��' ,�� ��� " � � ■iSiaQ� � � ®■COY -�_�- 0 i (0 LL Lo V' O > 0. N O > o O O 7 a o O > a M O j a O O 70 n_ rl CS n_ sF 7 a_ O 3 a. N O n O : IL N O 7 o- d'l O 5 a CO CD > o- M O > o- O M O cp O C rn O c N 0 y C rn o y C co o m C O N C O m C r� O y O O N C M O N C in O w C rn O rn C N O w rn o rn C v r E O ,r M 00 M I`- M (0 M LO M Iq M Cl)N co M O M a) N M N r- N (0 N L N 'q N M N N N e-' N O N— 0)00 — f\ CO Lr) 4- H LEWIS FARMS AND LIQUID WASTE, INC. i WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: The Cape P.O.# Batch Size (gallons): 30,000 Lbs. or Gallons Used: 1500 gal Material Used For Stabilization: Lime MEMM O v Ci U> C o 7 a N C' 0 a W M o 0 a 'i 0 _7 a M M o _7 a: o M 0 _7 a 1 N 0 _7 tz a N © _3 o_ o a W 0 _� a u1 0 j a N 0 7 n, cA 0 2 o. co O 0 7 a M O 0 7 s O r� o o N C_ � ro V1 _C � m O 0 N _C � N o © C s r 0 N C c m 0 N C � N 0 VY C _ `2 v N 0 V1 C 2 h N 0 N C S o m 0 n C L c7 0 M C � c^ M 0 N E � rn 0 0 Ut N 0 N Fn 0 rf� U Na O "Zr d7 M OD Cl) r— M to cM u') co IT (1) M M N M •- M d M D? N Cb N r- N CD N LO N It N OM N N N �- N O N 0) r co — ti UJ LO — �f M N r r- O .r- WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER EIOSOLIDS Facility Name: The Cape P.O.# s Batch Size (gallons): 30,000 Lbs, or Gallons Used: 1500 gal Material Used For Stabilization: Lime G ` (� O U ID U LL µj a' O 3 N C' O O 01 th O O (D C7 O 7 ('7 M O > M O > N O N O N O O �- O '- b O O O O co O C7 O M 0 (0 o 0 N a 0 N N o 0 N N 0 y +- 0 N N 0 N -, N 0 rry 1- N 0 y O M 0 N M M 0 c� (D cn 0 N nM 0 y N y 0 tI) 0 U n. Q. ii d Q. CL d 0- M Qr Q. d d d 4 2 2 U D N o CA cq I� Cl) (0 M � co V' co co co N co M O M G) N 00 N ti N (D N�- L d co N e- O CO f� M N c o F- Facility Name: The Ca Batch Size (gallons): 30,000 P.O.# Lbs. or Gallons Used: 1500 gal Material Used For Stabilization: Lime r •2 Hourr . r r •.- _ . iLO U V" O d (,j o 7 FL Q) O FL. cp o FL M Gi 7 Q. q M O D. h N o D_ <F N 07 EL N O ELd CO O Z O 7 N_ O n. Q> p O EL O O O O EL O o p C o Q C p C �v o J C 4� ,- 0 J C m c- 0 J C N 0 J C v N 0 J C I� N 0 J C o r� 0 J C r� M 0 J C M 0 J C Cii 0 J C v o J C d J C p- O V' M M 00 M r+ M Co cM L0 M -f M M M N M r M O M 47 N M N r. N t0 N Ln N It N CO N N N r N O N r OJ r`- Q0 r Ln r d' M N r O H LEWIS FARMS AND LIQUID WASTE, INC. I/ Q 000045.E ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility game: The Cape P.O.# Batch Size (gallons): 50,000 Lbs. or Gallons Used: 2000 gal Material Used For Stabilization: linne C o O U �i L- �fi V O N a N `�t O w O M 6 0 W M O w a M M O y ii O M O N n r- N O }/1 a V N O to ii N O IJ1 ii OD Y O N a L O N a. N Y O N 0- a) O O n) 0- (0 O O y CL M O O vj a C7 M O Vi lD 4 N . O v1 C+ w - v y - co Y N nF N N dl M n N Vr Z o M N 2 n M A M V1 T C) N fV N z �n N U a ¢� O CA O7 r� (0 c`") LO c) 'ct M M M N M t'- M O M O N Co N 1` N CD N L0 N `Cf' N M N N N r- N O N M — W I- co r- LO — 't M N r Y- O Y- H LEWIS FARMS AND LIQUID WASTE, INC. 3 { WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BI©S©LIDS Facility Name: The Cape P.O.# Batch Size (gallons): 50,000 Lbs. or Gallons Used: 2000 gal Material Used For Stabilization: Lime j Em o 0 ro0 c°) �- � a N fY � s C'h M � (L w 'i � M M M � M o M � M 1 ram- N � a- d � M > a ao > a, i!'l .- 7 a N w- � M � 0. tU a M a in _� o rn 0 c. � m n N v e. o to m rn [� U F� M (M M M LO M '[F M CO M N M — ('� O M G� N Co N T,,,(,o ((7 N 'ctN N N N N O N C.n — t0 r� (,D u7 r q' M NV r e- ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455 WWTP Name: The Cape NPDES Number. NCO057703 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ T Process to Further Reduce Pathogengs ❑ If appHeable to alternative performed (Class A only) indicate "Process to Further Reduce Path ens": Compost [3Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra [3Gamma Ray❑ Pasteurization [3 Class B: JAIt (1) Fecal Density ❑ Alt. (2) Process to Signi2cantly Reduce Pathogens ❑ If applicable to alternative performed Class B only) indicate "Process to S!pMcantly Reduce Pathogens": Lime Stabilization 0 Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion n If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NUMba ° Excee dences Frequency of Anal sis y I Sample Type Yu Tech - ni oue Geo. Mean aximu Units Units Fecal Coliform 2 x 10 to the 6th power per of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) vector Attraction Reduction (15A NCAC 02"1" .1107) -Please indicate alternative nerformed: Alt I (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (AIL Stabilization [3 It 7 (Drying - Stable) ❑ JAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ®No vector attraction reduction alternatives were performed ❑ CERTIMIC T1UN STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Prepare N e an Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November 19, 2014 Topsail Greens 1.54 % Solids 7.67 nH Permit No. WQ0000455 Parameter % JMg/Kg Dry Weight x 10,000 Pounds/Dry Ton M /K x 0.002) Nitrogen (TKN) 5.830 58,300.000 116.600 Phosphorus 1.790 17,900.000 35.800 Potassium 0.298 2,980.000 5.960 PAN (injected)* 1.755 17,553.180 35.106 PAN (surface)* 1.753 17,534.980 35.070 Ammonia Nitrogen 0.004 36.400 0.073 Calcium 7.790 77,900.000 155.800 Calcium Carbonate E . --- --- --- Magnesium --- 2,140.000 4.280 Sodium --- 27,100.000 54.200 Sulfur --- --- --- Nitrate N / Nitrite N - 37.700 0.075 Barium --- --- -- Chloride --- --- --- Iron --- --- --- Aluminum --- 3,420.00 6.840 Arsenic --- 6.10 0.012 Cadmium --- 6.10 0.012 Chromium - 12.100 --- Copper -- 187.00 0.374 Lead --- 12.30 0.025 Mercury --- 1.36 0.003 Molybdenum --- 6.10 0.012 Nickel --- 10.70 0.021 Selenium --- 10.80 0.022 Zinc --- 1,160.00 2.320 Environmental Chemists # 2014-14314 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. f envitrochem 6602 Windmill Way ** Wilmington, NC 28405 j (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 G.W. Water Services Date of Report: Dec 04, 2014 1219 Old Folkstone Road Customer PO #: Sneads Ferry NC 28460 Customer ID: 09020031 Attention: Gregory Wright Report #: 2014-14314 Project ID: Sludge Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-35105 Site: Sludge 11/19/2014 9:57 AM Solid/Sludge Stephen Crews Test Method Results Date Analyzed - Sludge Residuals Aluminum EPA200.7 3420 mg/kg 11/2612014 Arsenic EPA2°o.7 <6.10 mg/kg 11/21/2014 Cadmium EPA200.7 <6.10 mg/kg 11/21/2014 Calcium EPA200.7 77900 mg/kg 11/26/2014 t' Chromium EPA200.7 12.1 mg/kg 11/21/2014 Copper EPA200.7 187 mg/kg 11/24/2014 I Lead EPA200.7 12.3mg/kg 11/21/2014 -Magnesium EPA200-7 2140 mg/kg 11/26/2014 Molybdenum EPA200.7 <6.10mg/kg 11/21/2014 Nickel EPA200.7 10.7mg/kg 11/21/2014 1 I Potassium EPA200.7 2980mg/kg 11/26/2014 f Selenium EPA200.7 10.8mg/kg 11/21/2014 Sodium EPA200.7 27100mg/kg 11/26/2014 Zinc EPA200.7 1160mg/kg 11/21/2014 Ammonia Nitrogen EPA350.1 36.4mg/kg 11/20/2014 Total Kjeldahl Nitrogen (TKN) EPA351.2 58300 mg/kg 11/24/2014 i Nitrate+Nitrite-Nitrogen EPA353.2 37.7 mg/kg 12/02/2014 Total Solids (%) sM 2540 B 1.54 % 11/19/2014 pH SM4500 H B 7.67 units 11/20/2014 Total Phosphorus sM 4500 P F 17900 mg/kg 1112412014 j Mercury SW8467471B <1.36 mg/kg 11/26/2014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: U-J.l.Vi-2. Report #:: 2014-14314 Pagel of 1 I� ENVIRONMENTAL CHEMISTS, INC ImpSample Collection and Chain of Custody Client: GW WATER SERVICES EMAIL: ECHEMW(aaol.com Collected By: S��e�vti V, 0-rg,jc Report No: Qn =Qn11 ; i \liilla_��' r r. n__ __a T, .-_ r.•xn_.,..-� `[I!—'(I/..11 QT'—Cf.-on..� h nfhpr! 6602 Windmill Way Wilmington, NC 28405 Phone: (910) 392-0223 Fax (910) 392.4 4 (� I16L— / l3 Dil[ll iG 1t1U. 1 — lA uXAI Sample Identification ui w a Collection = Q N a v F U ,, fa c d p o - PRESERVATION ANALYSIS REQUESTED z x O" ,7,+ z p DATE TIME TEMP Topsail Greens 30 C P ' X G G Topsail Greens IL C P x G G Slli 11- -/t( q lyo C P . , �s C G P G G 'C P G G C P G G C P G G C P G G C P G Gt_ C P- G G Transfer Relinquished By: ' . Date/Time Received By: Date/Time 2. Temperature when Received:c�Z.T Accepted: - K sapppie tceques ea: Delivered By: Received By: ✓ Da#e: dG.1 / Time: ' 02/11/2015 15:53 9104517195 WASTEWATER PAGE 02/02 10. qb rQ ci �, Nonnia -, 11 IN 1—. 11�mml 111 1M11111�11�11 0 AIRall e�Hill 111111111 a1111111111 Y�1N111�1 IIAII�I�II @I INI'�111111 nil [Eglillnllll��� ANBII �NIII nilI�IN Mullin ��ou111N 01ui n 11/06/2014 16:06 Marine Federal Credit Union (FAX)910 794 8195 P.002/002 i !IIIINIIIIIINI� miirmm��0 unmmnm�� nunummiu� mm�nnnn�� IIIIINIIIIIIIIi �mmrmm�i�o NIIIIIIIIIIIIIIIH IIIIIIIIIIIIIIIIIN 11111111111111110.1 IIIIIIIIIIIIIIIII 111111111111111130 11111111111111112H 11111111011111111- let � o � M � r y y N b - d jL ~ M .m y C 3 y a 0 r t39 02/19/2015 12:34 9104517195 WASTEWATER PAGE 01/01 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) )Facility Name: LeMs Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: Topsail Greens Ni'DES Number: DEFT / Local Monitoring Period: Froem 1/1/2014 To 12/31/2014 i Pathogens Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: j Class A: Alt. A timPloem) ❑ Alt S (Ilk TM(t meat) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ 1f a licable to alternative etformed Glass A vialy IAdkcate "Process to Fortbex Redace Path ens'0: Compost ❑ 11eat2ryittg ❑ Hest -Treatment ❑ Thermo huilic ❑ Beta lie ❑ Gamma Ba ❑ Pasteurization ❑ Class B: Alt.(1) Fecal Demsity ❑ I Alt 2) Process to Si caatly Reduce path9jV ❑ if a pUcablee to alternative onmed Class 13 on ) indicate "1Procen to S' cap Reduce Path ens": me Stabilization D Air Drying❑ Co ❑ Aerobic stiou ❑ Anaerobic Dl ion ❑ r�2:��'!t^'^i'.:ti.::cc;a�A:..c: :fie. ^a :z i?z::Scfi•vc cF•.•:c..: ::�t-:< � .::�^:�C �•• ::i>�csx.••:.^.:::^(M:s:, �Sr'a'�^::�•�,:c,;..f:'V:4:j.:::>:•$;;:a::::�„ii:a:,,c• If applicable to alternative perfo Class A or Class B the wing monitorina data: Allowable Level Pathogen Density Numberof F Parameter requeacy Sample in Sludge MmmnitzGeo. M Units Eat of Analysis Tape Tech- 2 x 10 to the MIN 6th power per 8= of Fecal Cobberm tow solids CFU 1000 MP13 per pram . of total solid (dry weight . SalmoneAa bactexis 3 MM per 4 grmos (iu lieu of fecal total solid (dry . c%WA ^tWU%;uoa aceaucgoA (1Sp,1YCAC U2T .1107) - Please Indicate alternative edornred: Alt.l (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt 3 (30-day bench) ❑ Alt. 4 (Spec. % uptake) ❑ Alt 5 (14-Day Aerobic) ❑ Aft. 6 (Alk. Stabilization >] Alt 7 (Dryiung _ Stable) ❑ Alt 8 (Drying - Unstable) ❑ Alt 9 ectioa) ❑ Alt. 10 (lac oration) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met v ❑ - "I certify, under penalty of law, that the pathogen requirements In ISA NCAC 02T am and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note If you check this statement attach an "Pla"Stion wiry you have not iaret one or both of the i _-- requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the Information used to deterloatne that the pathogen and vector attraction reduction !requirements have been met. I am aware that there are siguiffcant penalties for false certification including fine and imprisonment." Stephen V. Crews, ORC Preparer Name and Title or print) (tYPe Pam) !:and Applier Name d Ti le ' applicablaxtype or print) 2 - /7—/S— Si of Preparer" ate Signature of d Applier (if applicable) Date •Prepamr is defused in 40 CPR Part 503.9(r) and 15A NCAC 2T .1102 (26) LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: September 29, 2014 Topsail HiEh School 0.36 % Solids ,7 ng ..0 Permit No. WQ0000455 Parameter % JMg/Kg Dry Weight x 10,000 Pounds/Dry Ton M /K x 0.002 Nitrogen (TKN) 6.310 63,100.000 126.200 Phosphorus 2.200 22,000.000 44.000 Potassium 1.240 12,400.000 24.800 PAN (injected)* 1.979 19,789.000 39.578 PAN (surface)* 1.925 19,249.000 38.498 Ammonia Nitrogen 0.108 1,080.000 2.160 Calcium 3.420 34,200.000 68.400 Calcium Carbonate E . --- --- --- Magnesium --- 4,140.000 8.280 Sodium -- 40,000.000 80.000 Sulfur --- --- Nitrate N / Nitrite N --- 103.000 0.206 Barium --- --- --- Chloride --- --- Iron -- --- Aluminum --- 3,890.00 7.780 Arsenic --- 20.80 0.042 Cadmium - 20.80 0.042 Chromium --- 20.800 --- Copper --- 769.00 1.538 Lead --- 26.40 0.053 Mercury --- 5.56 0.011 Molybdenum -- 20.80 0.042 Nickel --- 30.60 0.061 Selenium --- 20.80 0.042 Zinc --- 1,500.00 3.000 Environmental Chemists # 2014-11998 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 0 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 I Pender County Schools Date of Report: Oct 15, 2014 925 Penderlea Highway Customer PO #: Burgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2014-11998 Project ID: Topsail WWTP Lab 1D Sample ID: Collect Date/Time Matrix Sampled by 14-29453 Site: Sludge 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Sludge Residuals Aluminum EPA 200.7 3890mg/kg 10/06/2014 Arsenic EPA 200.7 <20.8 mg/kg 10/01/2014 Cadmium EPA200.7 <20.8 mg/kg 10/01/2014 Calcium EPA 200.7 34200 mg/kg 10/03/2014 I Chromium EPA 200.7 <20.8 mg/kg 10/01/2014 Copper EPA 200.7 769 mg/kg 10/01/2014 Lead EPA 200.7 26.4 mg/kg 10101 /2014 Magnesium EPA 200.7 4140 mg/kg 10/03/2014 Molybdenum EPA 200.7 <20.8 mg/kg .10/01/2014 Nickel EPA 200.7 30.6 mg/kg 10/01/2014 Potassium EPA 200.7 12400 mg/kg 10/03/2014 Selenium EPA 200.7 <20.8 mg/kg 10/01/2014 Sodium EPA 200.7 40000 mg/kg 10/03/2014 Zinc EPA 200.7 1600mg/kg 10/01/2014 Ammonia Nitrogen EPA350.1 1080 mg/kg 10/01/2014 ,I Total Kjeldahl Nitrogen (TKN) EPA351.2 63100 mg/kg 10/03/2014 Nitrate+Nitrite-Nitrogen I EPA363.2 103 mg/kg 10/13/2014 Total Solids (%) SM 2sao B 0.36 % 09/30/2014 pH SM 4500 H B 7.06 units 10110/2014 Total Phosphorus SM 4500 P F 22000 mg/kg 10/03/2014 Mercury SW0467471B <5.56 mg/kg 10/08/2014 1 ■ I I Report #:: 2014-11998 Page 1 of 3 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) _, SM 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 i ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #3M9 Pender County Schools Date of Report: Oct 15, 2014 925 Penderlea Highway Customer PO #: Burgaw NC 28425 A Customer ID: 08100094 Attention: John Shepard Report #: 2014-11998 - Project ID: Topsail WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-29454 Site: 1 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2640 B 0.52 % 09/30/2014 _ Fecal Density SM 9221 C E MPN 24 hr 503 5769231 MPN/g 09/30/2014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-29455 Site: 2 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 B 0.46 % 09/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 34782609 MPN/g 09/30/2014 t Lab ID Sample ID: Collect Date/Time Matra Sampled by 14-29456 Site: 3 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 B 0.38 % 09/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 42105264 MPN/g 09/3012014 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14 29457 Site: 4 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 B 0.36 % 09/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 13888889 MPN/g 09/30/2014 Z Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-29458 Site: 5 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 B 0.33 % 09/30/2014 Fecal Density SM92210EMPN 24hr503 9090910MPN/g 09/30/2014 Report #:: 2014-11998 Page 2 of 3 Environmental Chemists, Inc. ■ 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sM 710 Bowsertown Road ■ Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Pender County Schools Date of Report: Oct 15, 2014 925 Penderlea Highway 4 Customer PO M Burgaw NC 28425 Customer ID: 08100094 Attention: John Shepard Report #: 2014-11998 I Project ID: Topsail WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-29459 Site: 6 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 254D B 0.41 % 09/30/2014 Fecal Density SM 9221C E MPN 24 hr 603 12195122 MPN/g 09/30/2014 Lab ID Sample [D: Collect Date/Time Matrix Sampled by 14-29460 Site: 7 9/29/2014 11:20 AM Solid/Sludge John Shepard Test Method Results Date Analyzed Total Solids (%) SM 2540 B 0.38 % 09/30/2014 Fecal Density SM 9221C E MPN 24 hr 503 13157895 MPN/g 09/30/2014 Comment: Reviewed by: Report#:: 2014-1199B Page of ENVIRONMENTAL CHEMISTS, INC OFFI� ,9,03 z z Wilmington, NC Analytical &Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists.com rr%l' 1 PrTlnld Amn CHAIN AF CtISTnny Client: Pander County Schools PROJECT NAME: REPORT NO: ADDRESS: CONTACT NAME: John Shep erd PO NO: REPORT TO: PHONE/FAX: COPY TO: email: Samnlpd Rv: t.-, SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludqe, Other: Sample Identification Calla ion E F `o E n `o E c w m � PRESERVATION ANALYSIS REQUESTED Date Time Temp i v H o xo o = Sludge I C P I X isludge nutrients/metals G G 1) C P X fecal densi /% TS G G 2) C P X fecal density/% TS G G 3 C P X fecal density/% TS G G 4) C P X fecal density/% TS G G 6) C P X fecal density/% TS G G 6) C P X fecal density/% TS G G 7) C P X fecal density/% TS G G C P G G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: Accepted: Rejected: Resample Requested: Delivered By: Received By: Date: Time: 47 Comments: T. RNA OUND: LEWIS FARMS AND LIQUID WASTE, INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Topsail High School P.O.# Batch Size (gallons): 4000 / 12000 Lbs. or Gallons Used: 150 / 400 Material Used For Stabilization: Lime C O O U N U 0 u U) V O 7 a N V' O 7 a m CM O 7 a m CM O 7 a M C7 O CL O C? O 7 a r N O 7 n. d N O 7 a N C) 7 n. c0 r C) 7 n. r O 7 a N r O 7 s m O O 7 n. (o O O 7 a cr) O O 7 0- C) c) O o N C co O o N C c;)N O o tll C C in o N C m o f� C N o N C v N o t/1 C r, N o N C o M O N C c) 1l o Vl C co M o N C rn M o �/1 C N C o N C cn 't o M1 C 0 Q E O O M w M r` M 0 M U7 M 'It M M M N co c- M O M O N 00 N r` N (O N L0 N Nr N CO N N N N (D N 0) r- c0 r r` O LO d co N O �— ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTP Name: New Topsail High School Complex NPDES Number: WQ0032930 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathnaan Rerinetian (I NA NCAC 02T-11061 - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying 0 Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray - ❑ Pasteurization ❑ Class B: jAlt. (1) Fecal Density ❑ Alt. (2) Process to Significantly Reduce Pathogens Rl If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization (] Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ If applicable to alternative perdformed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis y Sample Type AnaiTic7a Tech - ni ue Minimu Geo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) vartnr Ottrartinn lltvrinehnn IISA N :Al : UZ l .l tir/1 - rlease lnalcaie alternative neriormea: Alt.1 (VS reduction) ❑ jAlt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ JAIt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ I Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Wesley Wooten, President Prepa;�� e or print) 2 - /3 - /s-- Signature of Preparer* Date Land Applier Name and Title (if applicable)(type or print) Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) prop ri+n�• n�inr nnT .wninnnn♦ LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: March 20, 2014 Trenton Permit No. WQ0000455 4.26 % Solids 12.1 pH (taken from lime stabilization event) Parameter I % JMg/KgDryWeight1Pounds/Dry x 10,000 Ton M /K x 0.002 Nitrogen (TKN) 2.320 23,195.000 46.390 Phosphorus 0.331 3,314.000 6.628 Potassium 0.176 1,760.000 3.520 PAN (injected)* 0.717 7,168.820 14.338 PAN (surface)* 0.703 7,026.320 14.053 Ammonia Nitrogen 0.029 285.000 0.570 Calcium 9.204 92,035.000 184.070 Calcium Carbonate E . --- --- --- Magnesium --- 44,248.000 88.496 Sodium --- 3,158.000 6.316 Sulfur --- --- --- Nitrate N / Nitrite N - 10.820 0.022 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum -- 7,003.00 14.006 Arsenic -- 2.50 0.005 Cadmium - 1.10 0.002 Chromium --- --- Copper - - 213.00 0.426 Lead - 45.00 0.090 Mercury --- 0.48 0.001 Molybdenum --- 5.00 0.010 Nickel - 9.00 0.018 Selenium - 5.00 0.010 Zinc --- 746.00 1.492 Environment 1, Inc. # 268 B *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. tr Emwok mgms[W To k@@* T TOWN OF TRENTON WWTP ATTN: TONY HAWKINS HAWKINS WASTEWATER 202 HWY. 41 W. TRENTON ,NC 28585 PARAMETERS Aluminum, (dry wt. basis), mg/kg Arsenic (dry wt. basis), mg/kg Calcium (dry wt. basis), ing/kg Cadmium (dry wt. basis), mg/kg Copper (dry wt. basis), mg/kg Lead (dry weight basis), mg/kg Magnesium (dry wt. basis), mg/kg Mercury (dry wt. basis), mg/kg Nickel (dry wt. basis), mg/kg Potassium (dry wt. basis), mg/kg Selenium (dry wt. basis), mg/kg Sodium (dry wt. basis), mg/kg Zinc (dry wt. basis), mg/kg Sodium Adsorption Ratio Total Solids, % TKN (dry wt.), mg/kg Ammonia Nitrogen (dry wt.),mg/kg Phosphorus, T. (dry wt.), mg/kg Nitrate -Nitrite (dry wt.), mg/kg Molybdenum (dry wt. basis), mg/kg PAN (Surface Applied), mg/kg PAN (Sub -surface Applied), mg/kg Digester Analysis Method Date Analyst Code 7003 04/02/14 LFJ EPA200.7 <2.5 04/15/14 MEL 3113B-04 92035 04/02/14 LFJ EPA200.7 1.1 04/14/14 MEL 3113B-04 213 .04/02/14 LFJ EPA200.7 45 04/30/14 MEL 3113B-04 44248 04/02/14 LFJ EPA200.7 0.48 03/28/14 MTM 245.1 R3-94 9 04/02/14 LFJ EPA200.7 1760 04/02/14 LFJ EPA200.7 <5.0 04/21/14 MEL 3113B-0,4 3158 04/16/14 MTM 3111B-99 746 04/02/14 MTM 3111B-99 0.07 04/19/14 -LFJ 4.26 03/21/14 CMC 254OG-97 23195 03/27/14 ANO 351.2 R2-93 285 03/25/14 ALB 350.1 R2-93 3314 03/27/14 ALB 365.4 -74 10.82 03/26/14 ANO 353.2 R2-93 < 5.0 04/02/14 LFJ EPA200.7 7026 03/28/14 SEJ 7169 03/28/14 SEJ ID#: 268 B DATE COLLECTED: 03/20/14 DATE REPORTED : 05/01/14 REVIEWED BY: i N Pathogen and Vector Attraction Reduction Log LEWIS FARMS OF BURGAW, INC. WQOOOO465 e Facility Name: Batch Size (gallons): Lbs. ornminna IInn•1. I,,- /L Im 10 in Operator In Responsible Charge Signature ' - ° m ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rota) Facility Name: Lewis Farms 6t Liquid Waste, Inc. WQ Permit Number: WQ0000455 WWTPName: Trenton ' NPDESNumber: NCO021342 Monitoring Period: From l/l/2014 To 12/31/2014 Pathogen Reduction (ISA NCAC OZT A I (IM - Moog& iwaioo•A ra.,A1 e..>.cA..Aa ....a Clues A: Alt. A time/tem) ❑ Alt B (Alk . teabnent) ❑ Alt. C (Prior Testing) ❑ .r A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogengs M Itapplkableto alternative erformed CLss A o ttndicete "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermo hiGa ❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ -.'..1-. :: Class lAlt (15 Fecal Density CI Alt. (2) Probess to Sigufficantly Reduce Pathogens ❑ f a ' lfcabk to alternative performed C9aes B o lndicate "Process to Significantly Reduce Pathogens" Lime Stabilization El Air Ci Com ostin ❑ JAembic Digestion ❑ Ong 7:y:yy:i•: Anaerobic �1d14G1 WtCi Digestion on . • •(Class If applicable to alternative perfermed A or Class B' complete the followin monitoring data: ParameterTech. Allowable Level LDensity Pathogen !3 uFxcee-o Frem'eII`y �Ple Sludge of Analysis Type ninue MinimumGeo. Mean u Units 2 x 10 to the MPN 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 31V1PN per 4 grams (in lleu of fecal total sblid (dry ooliform)wet t VA #-- A•1...._ /.!, 19I•.♦ /. Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) _ ❑ Alt. 4 (Spec. % uptake) ❑ Alt. 5 (14-Day Aerobic) . ❑ Alt. 6 (AUL Stabilization ®rN—o 7 (Drying - Stable) ❑Alt 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ vector attraction reduction alternatives were rformed ❑ _-•,•• •+AW1V"•.•. ;.p.wUM euocn me uppropnaie siasemeni) ® "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduedon requirement In 15A NCAC 02T 1107 have been met" ❑ KI certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement altsrch an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision In accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonm�en Tony Hawkins, ORC Haw W S Preparer Name and Title (type r pri t) Land App; • Sign re of Preparer* Date Signature 'Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) (if applicableXtype or print) iY✓��` Z'-S— /� Applier (if applicable) Date DENR FORM PVRF 02T (12120M) 1 a9ed S9Db-9E9-ES2 Xdd 131783Sd1 dH WdSl:21 sjo2 So qad RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: November.18, 2014 Webb Apartments Permit No. W00000455 NCO023825 1.02 %. Solids 7.14 nH Parameter % JMg/Kg Dry Weight x 10,000 Pounds/Dry Ton M x 0.002 Nitrogen (TKN) 4.280 42,800.000 85.600 Phosphorus 1.650 16,500.000 33.000 Potassium 0.318 3,180.000 6.360 PAN (injected)* 1.607 16,065.000 32.130 PAN surface)* 1.416 14,155.000 28.310 Ammonia Nitrogen 0.382 3,820.000 7.640 Calcium 4.600 46,000.000 92.000 Calcium Carbonate E . --- --- --- Magnesium - 1,970.000 3.940 Sodium --- 9,160.000 18.320 Sulfur --- --- --- Nitrate N / Nitrite N --- 551.000 1.102 Barium --- --- Chloride - --- --- Iron --- --- --- Aluminum --- 3,100.00 6.200 Arsenic -- 8.63 0.017 Cadmium --- 8.63 0.017 Chromium --- 13.800 --- Copper --- 490.00 0.980 Lead -- 15.80 0.032 Mercury --- 0.78 0.002 Molybdenum --- 8.63 0.017 Nickel --- 15.90 0.032 Selenium - 16.30 0.033 Zinc --- 6,240.00 12.480 Environmental Chem. # 2014-14257 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. { 1' Environmental Chemists, Inc. 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road • Manteo, NC 27954 (252) 473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Onslow Water & Sewer Authority Date of Report: Dec 03, 2014 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2014-14267 Project ID: Webb Apartments Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-34960 Site: Sludge 11/18/2014 9:05 AM Solid/Sludge Terri Maggard Test Method Results Date Analyzed Sludge Residuals Aluminum EPA200.7 3100 mg/kg 11/26/2014 Arsenic EPA200.7 <8.63 mg/kg 11/21/2014 s Cadmium EPA200.7 <8.63 mg/kg 11/21/2014 Calcium EPA200.7 46000 mg/kg 11/2512014 Chromium EPA200.7 13.8mg/kg 11/21/2014 Copper EPA200.7 490 mglkg 11/24/2014 Lead EPA200.7 15.8 mg/kg 11/21/2014 j 1 Magnesium EPA200.7 1970 mg/kg 11/25/2014 Molybdenum EPA2oo.7 <8.63 mg/kg 11/21/2014 Nickel EPA200.7 15.9 mg/kg 11/21/2014 Potassium EPA200.7 3180 mg/kg 11/25/2014 Selenium EPA200.7 16.3 mg/kg 11/21/2014 Sodium EPA200.7 9160mg/kg 11/25/2014 ' Zinc EPA200.7 6240mg/kg 11/26/2014 Ammonia Nitrogen EPA350.1 3820mg/kg 11/20/2014 i :' Total Kjeldahl Nitrogen (TKN) EPA351.2 42800mg/kg 11/24/2014 Nitrate+Nitrite-Nitrogen i EPA353.2 551 mglkg 12/01/2014 Total Solids (%) SM2540 B 1.02 % 11/19/2014 pH SM 4500 H 8 7.14 units 11/20/2014 Total Phosphorus SM 4500 P F 16500 mglkg 11/24/2014 Mercury SW846 7471 B <0.784 mg/kg 11/26/2014 _ Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by:cP.rc� " Report M: 2014-14257 Page 1 of 1 ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405 phone: (910)-392-0223 Sam ile Collection and Chain of Custod Fax; (910)-392•4424 � OR g -A- � 0- r L �" n `�" Report No: Collected BY: ^ #�i11 itCA�Cr.V►� E =Effluent, W =Well, ST =Stream, SO =Soil, SL= Sludge Other:,_ Sample Type: I =Influent, PRESERVATION W Collection == a+ y .. � ° C ►� a ANALYSIS T. REQUESTED Sample Identification ; z x x' z o DATE TIME TEMP C P G G C P G G C P G G C P G G G P G' G G P G G Transfer Relinquished By: Date/Time Received By: Date/Time 2. Resample Requested: e ed: (� � � Accepted: •�—'— Temperature e Time: S Pi Delivered B Received y: Date: LEWIS FARMS OF BURGAW INC. WQ 0000455 ALKALINE STABILIZATION OF WASTEWATER BIOSOLIDS Facility Name: Webb WV TP P.O.# Batch Size (gallons): 5,500 Lbs. or Gallons Used: 1000 gals. Material Used For Stabilization: Lime Corr. Corrected C 8� «7 C O tll 7 a N V' O fn 7 a O M O N 7 a 0 M O fn 7 a M CO O N 7 a O co O N 7 a "- N O M 7 a V' N O (n 7 a N O U) 7 M a0 O M 7 M O (n 7 M N O (A 7 M 0) O O M 7 M (0 O O W 7 a f) O O U) 7 n ` o O > C (o O 0 > C rn O 0 7 C N . 0 7 C !r . 0 > C ao . 0 > C N 0 > C v N 0 7 C � N 0 7 C O m 0 n C ` C m 0 7 C co M 0 7 C rn r� 0 7 C N v 0 7 C N V; O 7 C U a- O d 6� M 00 M I� M 0 M � M d M M M N M <— M O M M N 00 N r N (D N � N d N M N N N N O N M M r` T M T U) cr r M N CD H ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Lewis Farms & Liquid Waste, Inc. WQ Permit Number: W00000455 WWTPName: Webb Apartments NPDES Number: NCO023825 Monitoring Period: From 1/l/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ :M -1-71 _: L: Alt.D (No Prior Test) ❑ Process to u F rther Reduce Pathos� pp�� p�GG ❑ - �c ` E If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost E3 Heat Drying . ❑ Heat Treatment ❑ Thermophilic ❑ © ; Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: JAIL (1) Fecal Density ElAlt. (2) Process to Significantly Reduce Pathogens p ;c . QO If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization O Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion .;:.:::-:-;.>..::;:.;::.;>:.::- .:`t•'}�rj? iul `L ...:..:. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of e- Bences encni Frequency of Analysis Sample Type Analytical Tech - ue MinimumGeo. Mean aximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total -solid (dry weight Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) ❑ Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAlt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) p No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Allen Rhue, ORC Wesley Wooten, President Preparer Name and Title (type or print) Land App 'er a a T' le if applicable)(type or print) Aueh W 91W, 17 Feb 15 Signature of Preparer* Date Signature o and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) r\r��r� ram.-\.• .'\\ Tr nnT i�nw\nnn\ LEWIS FARMS LAND APPLICATION PROGRAM RESIDUALS ANALYSIS Residual Type: Wastewater Treatment Plant Date Sampled: January 21, 2014 Webb Creek 3.61 % Solids 11.80 pH Permit No. WQ0000455 Parameter % Mg/Kg Dry Weight x 10,000) Pounds/Dry Ton (Mg/Kg (Mg/Kgx 0.002 Nitrogen (TKN) 4.800 48,000.000 96.000 Phosphorus 1.860 18,600.000 37.200 Potassium 0.565 5,650.000 11.300 PAN (injected)* 1.590 15,903.500 31.807 PAN (surface)* 1.483 14,833.500 29.667 Ammonia Nitrogen 0.214 2,140.000 4.280 Calcium 8.230 82,300.000 164.600 Calcium Carbonate E . --- --- --- Magnesium --- 39,900.000 79.800 Sodium --- 2,290.000 4.580 Sulfur --- --- --- Nitrate N / Nitrite N --- 5.500 0.011 Barium --- --- --- Chloride --- --- --- Iron --- --- --- Aluminum --- 1,680.00 3.360 Arsenic --- 2.60 0.005 Cadmium --- 2.60 0.005 Chromium --- 6.230 --- Copper - - 285.00 0.570 Lead --- 5.37 0.011 Mercury --- 0.078 0.000 Molybdenum --- 2.60 0.005 Nickel --- 6.23 0.012 Selenium --- 1 2.60 1 0.005 Zinc --- 2,170.00 4.340 Environmental Chemists 2014-00863 *Determination of Plant Available Nitrogen (PAN): Injected Application: (Mineralization Rate)(TKN-Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN Surface Application: (Mineralization Rate)(TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN Note: Constituents N.D. (Not Detected) or < detection limits are listed as detection limits for calculation purposes. 03/02/2014 08:37 9103263132 WEBB CRK W&S INC. PAGE 02 1 EnvirOamental Chemists, Inc. "02 Wm IMM way • Vdmkoon, NC MW (910) 392-0223 (Lab) • (910) 892-4424+ (Fax) 710 Bo+ovsertown Road • Mmnteo, NC 27954 ANALY11CALA CCN9UL17NS (252) 473-5702 CHEMMM IJCDTNR DWOCMUMCATEOtD1SCH[i1TF7CATE4VW Webb Creek Water S Sewage Date of Report: Feb 19. 2014 260 Zachary Lane Customer PO V. Hubert NC 28639 Report#: 2014-00863 Attention: Bill Moody Reportto: Bill Moody Project ID: SLUDGE Lab ID Sample 10: Webb Collect Date/Time Matrix Sampled by 14-02140 Site: Sludge 1/21/2014 8:00 AM SolidlSludge Bill Moody Test Method Results Date Analyzed Sludge Residuals Aluminum EPA2007 1680 mglkg 02/1112014 Arsenic EPAaaa.T a2.60 mg*g 01/22/2014 Cadmium EPA2001 47-60moft 01/22/2014 Calcium EPA2007 82300mg/kg 02/05/2014 Chromium EPA200.7 6.23 mg/kg 11 22/2014 Copper EPA2KT 285 mgft 01/2?J2014 Lead EPA2007 &37mgnM 01J=014 Magnesium EPA20D7 39900mg/kg 02M5/2014 Molybdenum EPA200,7 <2.60mg/kg 01/22I2014 Nickel EPA200.7 6.23 mg/kg 011=014 Potassium EPA200.7 5550 mg/kg 02105/Z014 Selenium EPA200.7 Q.60 mg1kq 01/2212014 Sodlum EPA2W7 22g0 mgft 02/05/2014 Zinc $PA2007 2170 rng1kq 02/1112014 Ammonia Nitrogen EPA380.1 2140 mg/kg W1712014 Total Keldahl Nitrogen (TIW) EPASM2 48000 rnglkg 02/07/2014 Nitrate+Nitrite-Nitrogen EPA3532 <5.5 mg/kg 02105/2014 Total Solids 06) sir 2S40 a 3.61 % 01/2212014 pH seresoo H e 11.8 units 01/23/2014 Total Phosphorus SM4600 F P 18600 mg ft 02/0712014 Mercury SVOM 7470A 0.0780 mg/kg W1412014 Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis. Reviewed by: PRpadtk 2Dt"Om page! 011 LEWIS FARMr ",,BVRGAW, INC. , WQ000045S MXALM.R STAB =- ATlolf OF WA VJCWATM larosoLMS 00 Bs�rh �fae (gallons) 6 7 L s. of Lime , mmm m mm��r��■r��r��i�r� Comments: - DAB 0*� •.• u v o o c o c o d o ® o 0 0 e •d a d n r®•e c'dC4cap H e`i e`3 e`� oe •� eA n _o <a e+� N 10 N 01,64 a/,7/it '/y/iI /lojy a1A1f alvAj uRGAW, INC LE w,s FARm `J 'MsTAB#JUTIONopw WATERscosoLM yY OOOO SS Batch Size (galloes) � i bL of Lime ' DATBO• e�v I ' I m N N v I N I® A Ico L IA LoB'° CD k IQ MOO m w w N .a z c� D N en cn tD N m co n C t� to N N P7 0 WQ00004S L& WIS FfiR1 S - "% BURGA Wo VVC ALKALINE STAMM ZATION OF WASTEWATER BIOS®LMS Retch Size (gR�ons) Lbs.OfLime 4g1 o 0 0 0 in O f It :2 q o d ' Q � G O n .f A •K r�iT F• !. Q f.t b 't r7 f1 fM R f•1 M G �l�0�l10041,11 J�l�Jli=111 "1 ME ogo 04011111 UPS IE0111111 8�f1��aE� III� m�8����1111,milli 1 ussam -.0111111 UPPOSOMINI a 0 nfarynao I I Iu� WFIF111111 11 M-- 035SPRIIIIII Q�����=JlIIIII VA T --A �1 � i � ,r TO 3DVd 'ONI SWM AM 883M � rer.... b! �` • Ono mu.,w sr "i�•a ��TW st �� i� Oro WON Ll IVOO W 91 81'0!W 61 O S1,0" 1Y1t oz ram• zl•o��t tz so'o w cz ` £p•0 snni6Q t+Z 00''0 sr EO'0 =Id 9Z A90'd �Id l.Z 60'0=1d BE zT'O Mid 6z 61'O sate OE 910 Ltd 1 £ 1pro $old t£ 4Z'0 S+Nd DE ' QE•0 MId sE Ef'0 sold , 9£ 9C0 snld LE 6E'0Iid sc 010 C 4d 6f Sb'0 Ltd ON .I• ZEiE9ZEOT6 6I:60 KOZ/0E/tb0 �C ' 1T3o'sq'I G py (mood) a¢1S R�igS ✓ . sMosors HUYAWYA, fro Nolaymil"ss wimm SS�00011( � 03AI1 M V9 Wil Mr,,, .S1%I YVW .''Tiff Qr'r t. Lo r m N N Qn N r W N m w w N H vny� m m r N cn r. N m m .-I. CD Im to N .-e m n m LL'WIS FARMS t t BURSA W INC. WQ0000455 AUcALM sTAMm&TION OF WAMWAMM WOSOLOs Batch $in (gallons) t0 ��o Us. of Lime Comments: j .�j DATE`J-4 - ke pewo �Vlo s �a y(� ypPF/�LV�SS,f{ is w U 0 a F v e+�► C" Fi eft i''1 cn eft got N „ C� N� N M N N ey N N pp N '�: :: N •-, m a. 6 `� r!71, 3 7A 1 N m M UO N cv tn m N m m r• m LEt wiS FA. 5 r 7 BURGAW, INC 1 WQ p pp0455 ALKALINE STABILIZATION OR WASMWATRR BIOSOIdbS Batch Size (gallons) LbL of Lime �iii■��ii�ei��■�iiiii!!!!■�!!a Comments: - DA ei Vie'! Ir_ �M'! re'► 1 1 �`! rl e e o 0 o d e o e e d d d e i d �j�' ��'! R `7 'v Q. .0. d 0: a a, e!. 1 o IdAla c a. c a. g J S U ' Q o a► ee .e Ih .w M .r M M M rf 0% M e M a N aq iw ti tV� w N v N N [�f !V p lit �•R. w + M 4 2 m a U z M 3 Y 15 00 N M -4 M LO N M T � .r o�n�w a�no►.�mmno' v a i, 1, TITa R 1 oegoQ PIS. g �o� P®�/� 3L � aumN Alllas. w :ao�l�Ro18 li MOM ✓�� � � /� x jy� li���d �'�,/✓J7" 11 Stff90S�te'ai�''Mgd` �Q NCO1l+�-1/9W1S �Ni7�3I7V 5'0004 bM .:)Ni `ILSVAA 00011 QNVOUV-4 SIMV a LEWIS FARMS `AND LIQUID WASTE, INC. a WQ 0000455 ALKALINE STANLIZA770N G� BASTE;%'�T� �IIQS+�i.ID� Facility {datne0 "� +� i Mil _.n.n�.00 bonfire _S5 Matorlai Uaed For t fabff{�%9n: Lit118 N cn N N m T LEWIS FARMS'AAID LIQUID WASTE, INC WQ 0000456 ALKAUAfE STABILIZA-#70N OF WASMI'lATER 810SOLIDS Faaisty f4)Z, �!M �� Used ForStahf�iiaUan: lime _ . a— ... n■ltens Used: Lo r m W N Q� W r W N u LEWIS FcgRAIdAND LIQUID WASTE," C' Wo 0000455 ALKALINE SrABILtZATION OF WASTEWATER BI-OSOI-106 11 "$� P.®.# *,v } FaCURY Name jj,�'t q , matoeloi used For Stsb" UMRIM-1— to 1-0 Z P 9 PH r rol sUd6la i $rg# -* BWj� :uoA4s1i19eiS Jai PEA teN®{¢;il � ���,/� / ,i/%+�'�r 77-!T��8W@H a►11N���.N�,L'Vj 'iii:•�S3Atl7Y}i7V 99�'000 iM �fri?Oac�tS •ant! atnoll ONb Sit�j+dj SiM37 03/02/2014 08:37 9103263132 WEBB CiRK W&S INC. PAGE 01 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: ewis Farns & Liquid Waste, Inc. Permit Number: W00000455 WwrPFlame: .f Zfie. NPOES Number: A1C!M0CZeW . i' Monitoring Period: From 1 To�3t��� Patboaen Reduction (40 CFR S033Z)- Please indicate level achieved and alternative aerformed: Class A: Alternative 1 Ahmmative 2 Alternative 3 Alternative Alternative 5 El A I[a cable to alteru:ltive erformed (Class A only indicate "Process to Farther Reduce PathogeW-. Compost Heat Drying Heat•Trealment 13 Thermo hilic Beta Ray Gamma men Pastetui�tion .... Class lit: Alternative 113 1 Alternative 2 1 Alternative 3 Itapplicable to alternative performed (Class S ) indicate "Process to iGtxat Reduce Patbo gas Lime Stabilization A Air 1 composting 13 1Aerobic Digestion Anaerobic Digesdo f r , If aggricable to alternative lopesformed Class A or Class H ample" the fonowki a monito data: Parameter Allowable Levcl Pathagen Dmalty Exaea it vent � Y S ample Analytical Geo. Mean mdm Units in Sludge g of Analysiq Type Tech-niquc x to power MPN Per gran often) solids or 2 x 10 to Fecal Conform the 6tb power CFt1 ON grant of low mpn per gram of total solid Jdr weight) Salmon lie bWcda 3 MPN pew- 4-(in lieu of fecal grams total solid colif lm) (dry wei Vector Attraction Redaction (40 CFR 50333) - Please reakate option performed: tion 2 on 3 Option 4 pp�n g tion 8 O tion 9 Option10 were perforMed13- PNOvectlor attraction reduc-d.. apti,,. —.. -OWIIAWWS A %Finaac WUNCn; rag appropriate statement). certify, under penalty Oflaw, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction re uirement in 40 CFR 50333 have been met." LU "I certify, under penalty of law, that the pathogen requirements in 40 CFR S0332 and the vector attraction reduction requirement in 40 CFR W3.33 have not been met." (Please note if you check this statement attach an explagation wily you have not tnet one or both of the requirements.) "This determination has been made under my direction and supervision in acoalydaaee with the System designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have bee% met. 1 sat aware that there an Significant penalties for false certification including fine and im j .,/, ..� g prisooynent •• Pt+epzar+er l e and Ti (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of hvparlr 01 Date Signature of Land Applier (if applicable) Date dENR FORM RF (52003) 2014 APPLICATION SUMMARY LEWIS FARMS Permit # WQ 0000455 2014 RESIDUALS APPLICATIONS APPLICATION SUMMARY FIELD NO. ACRES USED TOTAL GALLONS TOTAL WET TONS TOTAL DRY TONS TOTAL PAN Cron! C L1 5.10 84,500 5.85 37.95 0.00 L2 14.30 243,500 10.58 3.15 16.74 L3 18.90 477,000 48.51 58.85 19.10 L4 24.50 145,500 14.38 12.54 8.76 L5 23.30 48,000 5.68 5.54 1 5.54 L6 5.80 146,000 9.81 53.09 32.49 L7 8.10 39,000 2.28 4.43 2.16 L8 31.80 859,000 75.43 1 56.14 3.83 W1 35.60 317,500 22.88 27.15 5.92 W2 39.20 960,000 33.09 16.24 1 2.88 W3 24.20 780 152.10 14.61 1 33.67 Totals 230.80 3,320,000 780 380.60 Metric Tons 345.20 FIELD APPLICATION SUMMARIES Lewis Fauns permit W00000455 2014 Field Application Summary FIELD NO. LI L2 L3 L4 L5 L6 L7 La L9 L10 JJ-1 JJ2 Wl W2 W3 W4 JR-Fl AWl Sorghum/Whe,d Cont/Wheat ComfWhwt ComfWheat Corn/Wheat ComN"wt ComfWbmt CoroAtfheat ComAW�t Com/Wheat Coastatfftyc Coastal/Rye Coun/Whe,u Coni/Whein Cont/Whwt CoruMhut ComrWhe,u Corn/Whvit ------------------ -- : t t t t • t t t t t ------------ FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 LIO JJ-1 JJ2 Wl W2 W3 W4 JR1 AW1 NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.90 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Crop -rghumAVhcat Com/Wheat Com/Wheat Corn/Wheat Corn/Wheat Com/Wheat Com/Wheat Com/Wheat Com/Whmt Com/Wheat Coasud/R a Coastat/Rve Com/Wheat CoMWhca( Com/Whud Com/Wheat Soyfwhmt So )Wheat Sou Morehead City Note: Hold R,d indicates .surface application with incorporation Ito satisfy vector attraction reduction monitoring) SOURCE: Bald Head FIELD NO. L1 NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Corn Wheat Rye Coastal Note Bold Red indicates surface application with incorporation Ito satisfy vector attraction reduction monitoring) 48,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Beau Rivage B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Com Wheat Rye Coastal 0000000000��®00000 Note: Bold Red indicates surface application with incorporation Ito satisfv vector attraction reduction monitoring) 80,000 SOURCE: Bridgeton FIELD NO. Ll L2 L3 L4 L5 L6 NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 11 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B L7 L8 L9 L10 JJ-1 8.10 31.80 36.70 14.20 48.10 B B B JJ2 W1 W2 W3 W4 JR-Fl AW1 Total 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons January March April May June July i September October November December Soybeans Sorghum Corn Wheat Rye Coastal 'Vote: Bold Red indicates surface application with incorporation Ito satisfy vector attraction reduction monitoring) Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Castle Bay B B B B B FIELD NO. Ll L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AWl Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I— I January 1 February March April May June July August 1 September October November1 December — Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 48,000 SOURCE: Clarkton FIELD NO. Ll NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons February March April May i July Se October November December Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 24,000 k Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Dolphin Bay B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons 10 July August 1 September: November December Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfv vector attraction reduction monitoring) 28,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Hampstead Pines B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons II April May June July October November Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 8,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Hampstead Town Center B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Corn Wheat Rye Coastal oo0 111 000000���00000 Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 20,000 I Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Hermitage House B B B B B FIELD NO. III L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons lanuaj February March April May June August September 1 November December Soybeans Sorghum Corn Wheat Rye Coastal Note: (fold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 2,500 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: House of Raeford (Wallace Plant) B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons II 90,000 60,000 1111 60,000 III 1111 I III 1 August1 111 120,000 September: 120,000 • o.' 1111 lr,0,000 November �111 90,000 December 111 III Soybeans Sorghum Com Wheat Rye Coastal �000000000����oo�o Note: Rold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 1,272,000 SOURCE: Kenwood FIELD NO. Ll NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit# WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons January February March April June August October - December Soybeans Sorghum Com Wheat Rye Coastal �000000000��00000 Note: Bold Red indicates surface application with incorporation Ito satisfy vector attraction reduction monitoring) 4,000 Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Majestic Oaks B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 1,10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I I Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 70,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Maysville B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I I Soybeans Sorghum Com Wheat Rye Coastal :Vote: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 134,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Town of Morehead City B B B B B FIELD NO. Ll L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Wet Tons I I January February March April i June July August V October November December Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy sector attraction reduction monitoring) Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Pender High School B B B B B FIELD NO. Ll L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AWl Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I I January 1 February I March April June July August September October November Soybeans Sorghum Corn Wheat Coastal Rye Note: Bold Red indicates surface application with incorporation (to satisfy sector attraction reduction monitoring) 14,000 SOURCE: Richlands FIELD NO. L1 NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit# WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 LIO JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AWl Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons October November Soybeans Sorghum Corn Wheat Rye Coastal Note: Bald Red indicates surface application H it incorporation Ito satisfy sector attraction reduction monitoring) 240,000 Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Riverbend B B B B B FIELD NO. Ll 112 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I I January March May June JUIV August Septembe October December Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation Ito satisfy vector attraction reduction monitoring) 48,000 SOURCE: Sherwood Mobile Home Park FIELD NO. Ll L2 L3 L4 L5 L6 NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 11 Lewis Farms Permit # W00000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons July August is October November December Soybeans Sorghum Com Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 31,000 Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Sterling Farms B B B B B FIELD NO. Ll L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons -• � �- ____________®_____ I III Soybeans Sorghum Corn Wheat Rye Coastal 000�oo�000��000000 Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 80,000 SOURCE: Swansboro FIELD NO. L1 NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Corn Wheat Rye Coastal �000000 111 00����00�0 Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 595,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Taylor Extended Care B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AWl Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Corn Wheat Rye Coastal 'Vote: Bold Red indicates surtacc application gith incorporation Ito satisfy vector attraction reduction monitoring) 12,000 Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: The Cape B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Corn Wheat Rye Coastal o®000�0000��o®0000 Note: Bold Red indicates surface application with incorporation Ito satisfy vector attraction reduction monitoring) 22Q000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Topsail Greens B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 IJ-1 .1J2 W1 W2 W3 W4 JR-F1 AW1 Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I- I i February March April May July August October November 0 December Soybeans Sorghum Corn Wheat Rye Coastal �00000 ll 000����oo�o Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 15,000 Lewis Farms Permit # WQ0000455 2014 Field Application Summary SOURCE: Topsail High School B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AWI Total NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons Soybeans Sorghum Com Wheat Rye Coastal ',ote: Bold Red indicates surface application" it incorporation Ito satisfy vector attraction reduction monitoring) 16,000 SOURCE: Trenton FIELD NO. Ll NET ACRES 5.10 L2 L3 L4 L5 L6 14.30 18.90 24.50 23.30 5.80 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B B B B L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AW1 Total 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons May June Julv August September October November December Soybeans Sorghum Com Wheat Rye Coastal �000000000��000000 Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 6,000 SOURCE: Webb Apartments FIELD NO. Ll L2 L3 L4 L5 L6 NET ACRES 5.10 14.30 18.90 24.50 23.30 5.80 11 Lewis Farms Permit # WQ0000455 2014 Field Application Summary B B L7 L8 L9 L10 JJ-1 8.10 31.80 36.70 14.20 48.10 B B B .IJ2 W1 W2 W3 W4 JR-F1 AW1 Total 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons April May June July August Septembe Soybeans Sorghum Com Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation (to satisfy vector attraction reduction monitoring) 5,500 M Lewis Farms Permit# WQ0000455 2014 Field Application Summary SOURCE: Webb Creek Water & Sewer B B B B B FIELD NO. L1 L2 L3 L4 L5 L6 L7 L8 L9 L10 JJ-1 JJ2 W1 W2 W3 W4 JR-Fl AWl Total NET ACRES 5.10 14,30 18.90 24.50 23.30 5.80 8.10 31.80 36.70 14.20 48.10 9.10 35.60 39.20 24.20 12.50 15.40 36.30 Gallons I I 19,500 32,500 • . __ 111 _______________ 39,000 13,000 June11 II July11 19,500 August 11 I 26,000 • ��- __ 111 _______________13,000 19,500 i �� III •. II �������������� � II Soybeans Sorghum Corn Wheat Rye Coastal Note: Bold Red indicates surface application with incorporation Ito satisfv vector attraction reduction monitoring) 292,_500 FIELD LOADING RATE DEPORTS - ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: WOOON455 Annual Dry Tons Applied: 5.85 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 4.6 Site #: 1 Field #: Ll Acres Utilized: 5.10 Acres Permitted: 5.10 Application Method*: S/1NVC Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant. Soil Goldsboro - GoA House of Raeford 40% :Dat»' PCs: Aeie: : F§ i4cde eurce:' iid; tri 'n 1 ' s; :A§:' :CA: :Cd :Bb: :H' :Mo :Ni Se:' :Zti::Pt1 11::PANS B: pKN: NH3� I�i3iQ3 2014 48,000 9,412 1.80 0.71 Bald Head bland G/D 0.008 0.008 1.185 0.031 0.001 0.012 0.031 0.009 2.388 13.19 68.81 39.84 0.11 1.17 2014 4,000 784 2.16 0.07 DOIP� Bay G/D 0.001 0.001 0.060 0.004 0.000 0.001 0.002 0.001 0.103 2:54 2.46 Kbum. 8.24 0.07. 0.02 2014 2,500 4" 0.46 0.01 Hermitage HOmc G/D 0.000 0.000 0.007 0.000 0.000 0.000 0.000 .0.000 0.015 0.05 0.04 0.07 O.OQ 0.03 2014 30,000 5,882 1.47 0.36 . The caPe G/D 0.004 0.004 0.191 0.009 O.QO1 0.004 0.015 0.005 0.421 22.17 12.98 Sorghum 63.25 4.09 0.33 Total 84,500 Annual Ibs/acre 0.012 0.012 1.444 0.044 0.002 0.017 0.048 0.016 2.928 37.95 0.00 Current Cumulative ibs/acre 0.39 0.20 39.79 3.65 0.09 0.46 1.00 0.44 61.16 160 50 Prior Years Cumulative Ibs/acre 0.37 0.19 38.35 3.61 0.09 0.45 0.95 0.42 58.24 Permitt C.P.L.R.*** 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." 84.29 !`"J JPermit PAN Limt lst/2nd Crop Lime App. Date Lbs/A x 2 --23 - /5--- (SignrtLYe of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit I/: W00000455 Annual Dry Tons Applied: 10.58 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 5.5 Site #: 1 Field #: L2 Acres Utilized: 14.30 Acres Permitted: 14.30 Application Method*: SANC Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Goldsboro - GoA House of Raeford 40% :Date :Gars: Acre: F$ tlicie eur¢e:' :�rtd; t'9/dc:� 'ti•led � 1 "9' : As : : :4i : 1'It :1ttlu A 3e: :2tt : :P,4N 1 :PAN 2 P : Cce l 2 FIdN : 1WH3 N2 iv3 2014 12,000 839 2.16 0.08 Dolphin Bay G/D 0.001 0.001 0.065 0.004 0.000 0.001 0.002 0.001 0.111 &90 1.81 2.63 Cam Wheat 8.81 0.07. 0.02 2014 30,000 2,008 0.26 0.02 oJestic Oaks G/D 0.002 0.002 0.011 0.002 0.000 0.002 0.002 0.002 0.043 0:59 0.51 2.42 Corn Wbbat 3.38 0.04 0.07 2014 134,000 9,371 1.02 0.40 MayMlie G/D 0.002 0.001 0.506 0.016 0.000 0.004 0.018 0.004 0.753 1:20 0.76 6.43 Com Wheat 5.55 1.49 0.00 2014 50,000 3,407 1.47 0.21 The Cape G/D 0.002 0.002 0.114 0.005 0.001 0.002 0.009 0.003 0.250 13.18 7.72 Wheat 37.59 2.43 0.20 2014 12,000 839 0.36 0.01 'ropsail High G/D 0.001 0.001 .0.019 0.001 0.000 0.001 0.001 0.001 0.038 0.48 0.55 Wheat 1.59 0.03 0.00 2014 5,500 385 1.02 0.02 Webb G/D 0.000 0.000 .0.016 0.001 0.0.00 0.000 0.001 .0.0011 0.204 0.46 0.54 Com 1.40 0.12 0.02 Total 243,500 Annual Ibs/acre 0.007 0.006 0.731 0.028 0.601 0.009 0.031 0.011 1.398 3.15 16.74 26.29 Current Cumulative ibs/acre 0.29 0.21 72.10 3.65 0.05 0.38 1.74 0.37 83.95 1.48 50 Permit PAN Limt 1st/2nd Crop 0.20 71.37 3.62 0.05 0.37 1.71 .0.36 82.55 Prior Years Cumulative lbs/acre E36 Permitt C.P.L.R*** 34 1.338 1 267 1 15 I n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." i / a Lime A Date Lbs/A 4!t9 ^ZT� X � /-r- (SignatWre of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (7/2002) Mod. S&ME, Inc. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 48.51 lwner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( nbn 503): 4.7 Site #: 1 Field #: L3 Acres Utilized: 18.9 Acres Permitted: 18.9 Predominant Soil Goldsboro - GoA Application Method": INC Volatil®tion Rate": 0.5 Mineralization Rate: 30 % House of Raeford 40% Gpls�l ; :go; OT/: : RgiiRdyak - � Coed; 114ete a/a :N6 fs 6 a �As: ' : �CiI � �Eit � �Pb: ' :� : Mu : = Ni : : S� : :fit � ipAN I: i'AN � :�: • Gro :x Gro :z : �YIC•1.7: • �I�I33: ' : At3 iV; 2014 150,000 7,937 0.76 0.25 Ouse ot G/D 0.006 0.006 0.121 0.006 0.001 0.006 0.009 0.006 0.127 3.74 2.64 Wheat 9.16 0.44 0.04 2014 90,000 4,233 L97 0.35 Richlands G/D 0.003 0.003 0.159 0.009 0.000 0.003 0.009 0.006 0.643 15.84 10.43 Corn 47.64 5.46 0.46 2014 247,000 13,069 3.61 1.97 Webb Creek GID 0.010 0.010 1.121 0.021 0.000 0.010 0.025 0.010 8.538 . 43.01 15.36 73.18 Corn Wheat 188.86 8.42 0.02 Total 477,000 Annual lbs/acre 0.020 0.020 1.401 0.037 0.001 0.020 0.043 0.022 Current Cumulative lbs/acre 0.67 0.28 77.88 4.18 0.04 0.58 2.08 0.56 Prior Years Cumulative lbs/acre 0.65 0.26 76A8 4.14 0.04 0.56 2.03 0 54 PermittC.P.LR.••• 36 34 1,338 267 15 1 n/a 374 89 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." 9.308 104.81.. 95.50 2,498 1 58.85 1 19.10 1 136 1 50 1PRrmit 86.26 '_:. •, _ :~ PAN Limt 1sOnd Crop Lime App. Date Lbs/A �✓ -Z3��� x 2 (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *$*C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 14.38 )wner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 12.4 Site #: 1 Field #: 14 Acres Utilized: 24.50 Acres Permitted: . 24.50 Application Method*: SANC Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Goldsboro - GoA House of Raeford 40% Dine 2014 Ears: 20,000 Gals.i: :Ar+ia :: 816 Tfi 1.15 T .4¢ce 0.04 tta�idital' :Soio'ee : .amp :Site Caod: G/D l�ietals Ifts/a Nutrients: ttis�ar: :As:' 0,001 C� 0.001 Cic 0.023 : P% 0.001 H 0.000 :Me: 0.001 Ni: 0.001 :Se 9.001 Za 0.363 FAN 1 0.32 PAlYx 0.47 : P 0.36 Cro' .1: Corn Crd Wheat : TIFAt : 1.79 L�I3: 1.25 N2=1V 0.00 2014 80,000 3,265. 1.97 0.27 Ricblaods G/D. 0.003 0.003 0.122 0.007 0.000 0.003 0.007 0.004 0.496 12.22 8.05 Corn 36.75 4.21 0.36 2014 45,500 1,857 3.61 0.28 Webb Creek GID. 0.001 0.001. 0.159 0.003 0.000 0.001 0.003 0.001 1.213 1 8.29 0.40 Wheat 26.84 1.20 0.00 Total 145,500 Annuallbs/acre 0.005 0.005 0.304 0.011 0.000 0.005 0.011 0.006 2.072 12.54 8.76 18.81 11 Current Cumulative Ibs/acre 0.51 0.26 56.31 0.56 0.30 56.94 3.77 0.05 2.51 .149 50 Permit PAN Limt 1�t/2nd Crop Prior Years Cumulative Ibs/acte 0.51 0.26 56.01 0.55 0.30 156.94 3.76 0.04 0.44 Permitt C.P.LR.*** 1 36 34 1 1,338 -F6-7-1 15 1 n/a 374 89 1 2,499 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." LimeAnn. Date Lbs/A X 7Z -Z 3 /.3-- (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. J ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 5.68 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 5.9 Site #: 1 Field #: L5 Acres Utilized: 23.30 Acres Permitted: 23.30 Application Method*: S/INC_ Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Goldsboro - GoA House of Raeford 40% :G�ts ( pry ; dT /. i�cre Rislda�l; 3jte : slate : t I'a Ibis/ :1t1i : ;Se : :Zit : PAN 9 PAN Z Il : iGro ' 1 x TKd!F : 1�1iI3 N2 N3 2014 48,000 2,060 2.84 0.24 River Bend GID 0.001 0.001 0.397 0.006 0.000 0.002 0.006 0.004 0.412 5:54 5.54 9.12 Com Wheat 34.94 2.68 0.07 Total 48,000 _ Annualibs/acre 0.001 0.001 0.397 0.006 0.000 0.002 0.006 0.004 0.412 5.54 5.54 9.12 ! : R :_;.. -. ,;-•:_.._.__..-F :� Current Cumulative Ibs/acre 0.41 0.24 29.33 2.17 0.11 0.27 1.99 0.31 52.55 1.48 50 Perrpit PAN Limt 1st/2nd Crop Prior Years Cumulative lbs/acrel 0A1 1 0.24 28.94 2.16 0.11 0.27 1.99 0.30 52.14 Permitt C.P.L.R.*** 1 36 1 34 1 1,338 1 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for,submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime App. Date Lbs/A R /ZV (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, InjectionMcorporation -1.0 ***C.P.L.R: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. - - - ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Owner: Lewis Farms Operator: Site #: 1 Field #: L6 Application Method*: S Permit #: W00000455 Lewis Farms Acres Utilized: 5.80 Volatilization Rate**: 0.5 Annual Dry Tons Applied: 9.81 Cation Exchange Capacity ( non 503): 4.7 Acres Permitted: 5.80 Mineralization Rate: 30 % Predominant Soil Goldsboro - GoA House of Raeford 40% .l 'AcI e: % 1 S >iTt i4cPe TZegl�a}si; enFce: ' =5�te: :CWd; :IVtc:t' I'9fsfc' tried S I '8' : Ai : 16 : :Zti PAN ! :PAN 2 S : ICce 1 lEl NH3 I+IfE 3 2014 16,000 2,759 0.26 0.03 Majestic Oala G/D 0.002 0.002 0.014 0.002 0.000 0.002 0.002 0.002 0.057 1.45 3.18 Wheat 4.44 0.05 0.09 2014 80,000 13,793 1.97 1.13 Richlands G/D 0.011 0.011 0.517 0.029 0.001 0.011 0.029 0.018 2.094 51.63 33.99 Wheat 155.23 17.79 1.50 2014 50,000 8i6211 1.47 0.53 The Cape G/D 10.005 0.005 0.280 0.013 0.601 0.005 0.021 0.007 0.617 32.49 1%02 Wheat 92.69 5." 0.48 Total 146,000 Annual lbs/scre 0.019 0.019 0.811 0.044 0.003 0.019 0.053 0.027 2.768 53.09 Current Cumulative Ibs/acre 0.38 0.07 13.33 1.47 0.94 0.20 0.62 0.15 28.66 136 Prior Years Cumulative Ibs/acre 0.36 0.05 12.52 1.42 0.64 0.18 0.56 0.12 25.89 Permitt C.P.L.R.*** 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for ]mowing violations." 32.49 56.19 :.:... 50 Permit PAN Limt lst/2nd Crop Lime A Date Lbs/A IN x Z- (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (7/2002) Mod. S&ME, Inc. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 2.28 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 3.6 Site #: 1 Field #: L7 Acres Utilized: 8.10 Acres Permitted: 8.10 Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Goldsboro - GoA House of Raeford 40% :DIaEa :gals;: Gals l:: Acre :: bto : TS: I Acere Besidit137: oteXee : :516e Emid: :MMetsls : lki a Nuirierits bstsc :As : Cil:' : Cp: : �b :: H : MCo::: Ni: : $e : :2;!* : PAiV:i �Ai�� F: Cr ' I G'RO' 2 :TitId NIR3: I NZ-N3 2014 15.000 1,852 1.54 0.12 Topsail Greens G/D 0.001 0.001 0.044 0.003 0.000 0.001 0.003 0.003 0.276 2.09 2.09 4.26 Cam Wheat 13.87 0.01 0.01 2014 14,000 1,728 0.33 0.02 Pender High G/D 0.001 0.001 0.026 0.004 0.000 0.001 0.001 0.001 0.033 0.21 0.07 0.04 Cam wheat 0.01 0.01 0.29 2014 4,000 494 0.36 0.01 Topsail High School G/D 0.000 0.000 0.011 0.000 0.000 0.000 0.0001 0.000 0.0221 0.29 0.33 Cam 0.94 0.02 0.00 2014 6,000 741 4.26 0.13 T-ton G/D 0.001 0.000 0.0561 0.012 0.0001 0.001 0.002 0.001 0.196 1.85 0.87 Cam 6.10 0.08 0.00 Total 39,000 Annual Ibs/acre 0.004 0.003 0.138 0.020 0.001 0.004 0.006 0.005 0.527 4.43 2.16 5A9 !, .:. '::_ = Current Cumulative Ibs/acre 0.10 0.07 35.15 2.08 0.01 0.17 0.87 0.13 50.68 148 50 JPermit PAN Limt lstlZnd Crop Prior Years Cumulative Ibs/acre 0.09 0.06 35.01 2.06 0.01 0.17 0.87 0.12 50.15 Permltt C.P.L.R.*** 36 1 34 1.338 267 15 n/a 1 374 1 89 1 2.498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in acoordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lune A P. Date Lbs/A x Z414Z -ZT -/-$-- (Signature of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization state: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R-: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 75.43 Lewis Farms Operator: Lewis Farms Cation Exchange Capacity( non 503): 9.4 Site #: 1 Field #: L8 Acres Utilized: 31.80 Acres Permitted: 31.80 Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 % Predominant Soil Grantham - Gr House of Raeford 40% Gem: :%: ATE )Zesidaa):' :Ste 1Gletais ac JQtHii¢nts: bs(ac' : ! fi;' 1: 2014 252,000 7,925 0.76 0.25 House of Raeford G/D 0.006 0.006 0.121 0.006 0.001 0.006 0.009 0.006 0.127 3.74 2.64 Wheat 9.14 0.43 0.04 2014 595,000 18,711 2.68 2.09 Swansbom G/D 0.014 0.014 1.886 0.074 0.009 0.024 0.052 0.029 15.557 55.96 4.43 Corn 112.92 1.26 21.83 2014 12,000 377 1.90 0.03 Taylor F.xten G/D 0.000 0.000 0.111 10.002 0.000 10.000 0.001 0.000 0.048 0.18 0.09 0.31 Com Wheat 0.86 0.06 0.00 Total 859,000 Annuallbslaere 0.021 0.020 2.118 0.082 0.010 0.031 0.062 0.036 15.733 56.14 3.83 1.38 �:.:_' .._..... �. _y 1 Current Cumulative lbslaere 0.24 0.11 12.50 1.16 0.03 0.22 0.82 0.23 37.05 138 50 Permlt PAN Limt lst/2pd CropDate Prior Years Cumulative Ibs/ecre 0.22 0.09 10.39 1.08 0.02 0.19 0.76 0.19 21.32 Permitt C.P.LR.*** 36 34 1,338 267 15 n/a 1 374 1 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated te information submitted. I am aware that these are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." LimeA . Lbs/Ac XZ� (Signs re of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation * *Volatilization Rate: Surface - 0.5. Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (7/2002) Mod. SBME, Inc. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit #: W00000455 Annual Dry Tons Applied: 22.88 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 4.0 Site #: W Field #: 1 Acres Utilized: 35.60 Acres Permitted: 35.60 ADalication Method*: INC Volatilization Rate"*: 0.5 Mineralization Rate: 30 % Predominant Soil Grantham - Gr House of Raeford 40% Date ::Gjds; :GIs;/.: :Acre: ='% : S D'I r Act+e ilel�o�l :9dtirce:' 3itle : Coral ctl' ' 1 9/A' : lYittii'o (bs :As: Cd :(:ti: Nb :H' :1ylo :N5 Se:' :7,u: PANT PAiV3 _ il: Cro'1:C tt'! TKN' 11Ii13 N2111$ 2014 80,000 2,247 1.50 0.14 Beau Pivage G/D 0.002 0.002 0.084 0.003 0.002 0.002 0.003 .0.002 0.181 '5.25 1.75 5.40 Soybean I Wheat 19.62 1.51 0.01 2014 11,500 323 0.46 0.01 Bridgeton Gil) 0.000 0.000 0.006 0.000 0.0001 0.000 0.000 0.000 0.022 0.03 0.12 Wheat 0.11 0.00 0.00 2014 48,000 1,348 1.31 0.07 Castle My G/D 0.001 0.001 0.020 0.003 0.000 0.001 0.002 0.001 0.156 036 1.92 2.58 Soybean Wheat 9.35 0.07 0.02 2014 19,000 10,000 0.23 0.10 cla'mon G/D 0.007 0.007 0.055 0.007 0.001 0.007 0.007 0.007 0.359 15.35 15.84 soybean 26.85 0.33 7.06 2014 12,000 337 2.16 0.03 DolPhln Bay GID 0.000 0.000 0.026 1 0.002 0.000 0.000 0.001 0.0001 0.044 0:73 1 0.36 1.06 Soybean wheat 3.54 0.03 0.01 2014 8,000 225 1.77 0.02 Hampstead Pines G/D 0.000 0.000 0.008 0.001 0.0.00 0.000 0.000 0.000 0.034 0.60 0.81 wheat 1.97 0.01 0.00 2014. 4,000 112 1.96 0.01 Kemvood G/D 0.000 0.000 .0.009 0.000 0.000 0.000 0.000 0.000 0.027 0.41 0.24 Wheat 1.31 0.05 0.01 2014 24,000 674 0.26 0.01 I'ticOaks G/D 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.014 0:24 0.12 0.78 Soybean wheat 1.08 10.01 0.02 2014 31,000 871 1.33 0.05 SheHe G/D 10.001 0.001 0.022 0.002 0.000 0.001 0.002 0.001 0.511 189 6.02 soybean 12.94 0.01 0.01 2014 80,000 2,247 2.29 0.21 werting Vanua WvfrTp GAD 10.001 0.001 0.091 0.003 0.000 0.002 0.006 0.0041 1.970 0:73 0.73 10.90 Soybean wheat 28.71 0.00 0.08 Total 317,500 Annual lbs/acre 0.013 0.013 0.324 0.021 0.603 0.014 0.022 0.017 3.318 27.15 5.92 43.74 _ _ ' _ _ _ Y_ .J Current Cumulative Ibs/acre 0.17 0.17 71.04 3.84 0.03 0.32 1.89 0.29 101.45 146 50 Permit PAN Limt Ist/3nd Crop Prior Years Cumulative Ibs/scre 0.16 0.15 70.72 3.82 0.03 0.31 1.87 0.28 98.13 Permitt C.P.L.R.*** 1 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am awdre that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime App Date Lbs/A x �V r (Sign lure of Land Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 SBME, Inc. DENR FORM FSF (7/2002) Mod. Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Lewis Farms Operator: Site #: W Field M 2 Application Method*: S Permit tl: W00000455 Lewis Farms Acres Utilized: 39.20 Volatilization Rate**: 0.5 Annual Dry Tons Applied: 33.09 Cation Exchange Capacity ( non 503): 5.2 Acres Permitted: 39.20 Predominant Soil Grantham - Gr Mineralization Rate: 30 % House of Raeford 40% Date :Gals.: :Aore: q: : 'DIE Acre:' ;I esitlttat :Spiuvte: :plc= Goad: o t...46 b./.e :As" :Ca:' Via:' :pb:' N :a�1a :IYE: Se :;6e:' TARia :Pi4C111:2:' :P:: :Cba':F * 2':�'[Ci�T::IY>Ei3:1.b 2014 870,000 22,194 0.76 0.70 House of Raeford G/D 0.018 0.018 0.339 0.018 0.0021 0.018 0.026 0.018 0.356 10.47 7.39 soybean 25.60 1.22 0.10 2014 90,000 2,296 1.47 0.14 The CRpe G/D 0.001 0.001 0.075 0.003 0.0001 0.001 0.006 0.002 0.164 5.77 2.88 5.07 soybean wheat 24.69 1.60 0.13 Total 960,000 Annuallbs/acre 0.020 0.020 .0.414 0.022 0.062 0.020 0.032 0.020 0.520 16.24 Current Cumulative lbs/acre 0.26 0.18 13.75 1.77 0.02 75.18 0.62 0.33 26.02 146 Prior Years Cumulative Ibs/acre 0.24 0.16 13.34 1.75 0.02 75.16 0.58 0.31 25.50 Permitt C.P.L.R.*** 36 34 1,338 267 1 15 1 n/a 1 374 89 1 2.498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 2.88 12.45 `" I 50 Permit PAN Limt lst/2nd Crop Lime A . Date Lbs/A x e 2 -- z 7 -15- (Signature of Land Applier) Date *Application Method: S - Surface, IN - injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1..0 ***C.P.L.R.: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 DENR FORM FSF (712002) Mod. SBME, Inc. ANNUAL LAND APPLICATION FIELD SUMMARY FORM Facility Name: Lewis Farms Permit tl: W00000455 Annual Dry Tons Applied: 152.10 Owner: Lewis Farms Operator: Lewis Farms Cation Exchange Capacity ( non 503): 4.1 Site #: W Field ll: 3 Acres Utilized: 24.20 Acres Permitted: 24.20 Predominant Soil Woodington - Wo Application Method*: S Volatilization Rate**: 0.5 Mineralization Rate: 30 % House of Raeford 40% Wig : W?'s.: Apra : I >x Acre :3oar c>b : t�tiod; : 7!l' tl 4 (1f /aC :As : Cd: ' Ca . : Yb: H : Mo: ' NI :lea : Za :PAN � : eM 2: : P. biro ' :1 C' 2:: �L'K1V: ' 111H3 : NZWa 6/30114. 240 10 19.50 1.93 Morehead "y G/D 0.037 0.002 3.334 0.034 0.009 0.020 0.03.4 0.022 3.829 14:97 25.06 Cam 32.30 5.22 0.05 10/9/14 280 12 19.50 2.26 Morehead City G/D 0.043 0.002 3.890 0.040 0.009 0.023 0.039 0.025 4.467 17.46 29.24 wheat 37.68 6.02 0.06 12/23/141 260 11 19.50 2.10 Morehead City G/D 0.040 0.002 3.612 0.037 0.008 0.021 0.037 0.024 4.148 16.21 27.15 wheat 34.99 5.66 0.06 Total 780 Annual lbs/acre 0.119 0.006 10.836 0.110 0.025 0.064 0.110 0.071 12.445 14.97 33.67 81.46 r__- _ �..---`3 Current Cumulative Ibs/acre 0.31 0.13 75.70 3.91 0.06 0.24 1.68 0.26 95.82 119 50 Permit PAN Limt lst/Znd Crop Prior Years Cumulative Ibslacre 0.20 0.12 64.87 3.80 0.03 0.17 1.57 0.19 83.38 Permitt C.P.L.R.*** 36 34 1,338 267 15 n/a 374 89 2,498 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations." Lime A . Date Lbs/A x 2 - 23 (Signature of Larid Applier) Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.IL: Cumulative Pollutant Loading Rate Bold denotes Incorporation and Volatilization Rate of 1.0 S&ME, Inc. DENR FORM FSF (7/2002) Mod. SOIL ANALYSIS REPORTS Page 1 of 4 Report Number: 15-027-0508 Account Number: 45819 ,L Send To: S&ME (1588) wwnaraleastern.com MARTIN MABE 3718 OLD BATTLEGROUND RD GREENSBORO NC 27410-2314 Date Received: 01/27/2015 A&L Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 27i-WG Grower: Submitted By: MARTIN MABE LEWIS FARMS Farm ID: JOB#1588-95-010 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Analysis: 01/28/2015 Date Of Report: 01/28/2015 Organic Matter Phospholrus ;:Potassium; _..:;_Magnesium " :',` =Calcium • ..:Sodium pH Acidity:'"•` -CcE:C. Sample ID Field ID Lab Number % Rate ENR Mdhiich 3 _: Reserve - 1C = Mg.. , ',' ; - ' . Ga'.:. Na, '' Soil" :=Buffed. H Ibs/A..ppm Rate.i ;ppm,: Rate; ppm, Rate; ;ppm ::Rate: zppm "Rate ` . m Rate;` pp : 'pH' . '.Index ,; meq/100g; 'meg/100g JJ01 390 VH 95 M 58 L 655 M 22 VL 11644 4.7 M 137 5.8 6.83 1.0 5.1 NC = 325 NC = 49 JJ02 11645 4.3 M 129 392 VH 81 M 56 L 1 641 M 124 L 1 6.0 6.86 0.7 4.7 NC=327 NC=41 L01 270 VH 145 VH L 512 M 17 VL 11646 3.3 M 109 1 135 1 1 5.4 6.80 1.3 4.6 NC=225 NC=74 L02 210 VH 156 VH L 779 H VL 11647 3.0 M 102 142 116 1 6.1 6.86 0.7 5.5 NC=175 NC=80 L03 VH 136 VH VL 535 M VL 11648 2.7 M 97 1207 1 1 132 1 116 1 5.4 6.80 1.3 4.7 NC = 172 NC = 70 Percent:BaseSaturation Nitrate;' °.`;, `:Sulfu[' .-,,.. .Zr%c;;:.', ;'Mangane'se = `s.. ;ih%oris-: ;''2.?Copper.. Boior. Sola6le;Salts,' `Chloride;;`, ^Aluminum. Sample ID Field ID K Mg Ca Na_ H zNO3Nr S Zn - Mn , , `:.. Fe;.` . Cu.. B` SS CI AI . "/° Ppm ; `. Rate :ppm ..''Rate pprtik .•` Rate ;ppm ,„ ,Rated Ppm';-"Rafe "ppm • = Rate :PPm. "Rate, ms/cm Rate pPm - : Rate _op"m JJ01 26 H 15.6 VH 11 M 270 VH 12.0 VH 0.3 VL 4.8 9.5 64.2 1.9 18.9 NC=54 NC=390.0 NC=69 NC=600.0 JJ02 M VH M VH 11.7 VH VL 4.4 9.9 68.2 2.2 15.4 125 117.0 113 1284 10.3 NC=52 NC=425.0 NC=81 NC=585.0 L01 M VH 11 M 302 VH VH VL 8.1 6.3 55.7 1.6 28.3 122' 19.5 15.5 10.3 NC=46 NC=237.5 NC=69 NC=275.0 L02 M H 8 L VH VH 0.3 VL 7.3 6.4 70.8 1.3 13.6 118 16.9 1307 14.4 NC = 37 NC = 172.5 NC = 50 NC = 220.0 L03 M H 8 L VH VH VL 7.4 5.7 56.9 1.5 28.2 120 17.8 1276 14.6 10.3 NC = 42 NC = 195.0 NC = 50 NC = 230.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after,each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. Pow;. n%° G�;J� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A&L Eastern Laboratories, Inc. v C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary Page 2 of 4 Report Number: 15-027-0508 Account Number:45819 Send To: S&ME (1588) MARTIN MABE 3718 OLD BATTLEGROUND RD GREENSBORO NC 27410-2314 SIX A&L Eastern Laboratories 7621 WhRepine Road Richmond, Virglhla23237 Fax 804 743 9401 804 271-wG 1 1 ( I I aleastern.com Grower: Submitted By: MARTIN MABE LEWIS FARMS Farm ID: JOB#1588-95-010 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 Date Of Report: 01/28/2015 Organic Matter Phosphorus Potassium ' --Magnesium' , `.Calcium:. Sodium; pH_. ., Acidity.; .CSE:C, ' Sample ID Lab ENR' % Rate Mehlich &. Reserve 'K•` M 9':'•' Ca. " ' Na :Soil Buffer>, H ` Field ID Number IbslA-_ ppm 'Rate pp"rn� . :Rate; •.ppin ; : `°Rafe= "ppm ' 'Rate' ;pprii ~ Rate`F ,ppm Rate • pH ` '16C16 , meg1.100g;1 .meg11'00g L04 11650 3.1 M 94 213 VH 124 M 178 M 2095 H 17 VL 7.2 0.0 12.4 NC = 177 NC = 63 L05 11651 1.7 L 76 152 H 1 173 L 59 L 542 L 17 VL 5.0 6.69 2.4 5.9 NC=43 NC=37 L06 11652 2.6 M 95 138 M 76 M 133 VL 481 M 119 VL 5.1 6.75 1.8 4.7 NC = 32 NC = 39 L07 11653 2.5 L 95 M 63 L 26 VL 236 L 16 VL 4.6 6.74 1.9 3.6 NC=28 NC=32 L08 11654 3.3 M 103 245 VH 147 H 134 M 1515 H 119 VL 6.8 1 rO. 1-9.4 NC=204 NC=75 Percent Base -Saturation Nitrate Sulfur: - 'Zinc ;- ;Manganese` ; : °.;Iron` . C'opper, `' `..B;oron ' ^ .Solu61e Silts, ; = Clil'orider=it Alamiriurrt . Sample ID Field ID K Mg Ca Na H NO3N S : 2n .,% MnFe : -- -Cu B SS:'. .Cl AI- % % % °7° ppm . ",Rate ppm; Rate ;ppm'='_ :Rate ';ppm' t ;Rates, ;ppm :, ,<Rite_ jppm Rate. Sppm ` Rate -ms/cm":Rate- ppm ' Rate / . ppm'- L04 16 M 16.1 VH 12 M 296 VH 6.0 VH 0.7 M 2.6 12.0 84.5 0.6 0.0 NC=33 NC=402.5 NC=75 NC=300.0 L05 H H 2 VL VH H VL 3.2 8.3 45.9 1.3 40.6 131 13.9 1217 12.1 10.2 NC=62 NC=97.5 NC=13 NC=105.0 L06 M M 1 VL VH 1.2 M VL 4.1 5.9 51.2 1.8 37.9 120 12.4 1392 10.2 NC=42 NC=60.0 NC=6 NC=60.0 L07 M L 1 VL 300 VH M VL 4.5 6.0 32.8 1.9 53.9 124 11.2 11.3 10.2 NC=50 NC=30.0 NC=6 NC=65.0 L08 M VH 5 L 355 VH17.6 VH 0.9 M4.0 11.9 80.6 0.9 2.9 116 113.0= NC=33 NC325.0 NC=31 NC=380.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by. ?0,;. me Gr C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: A&L Eastem Laboratories, Inc. Pauric McGroary Page 3 of 4 Report Number: 15-027-0508 Account Number: 45819 ERL Send To: S&ME (1588) wwwaleastem.com MARTIN MABE 3718 OLD BATTLEGROUND RD GREENSBORO NC 27410-2314 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 AFL Eastern Laboratories 7621 Whitepine Road Richmond, Virginia 23237 1804) 743-9401 Fax (804) 271b146 Grower: Submitted By: MARTIN MABE LEWIS FARMS Farm ID: JOB#1588-95-010 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 01/28/2015 OrgariicMatter P.liosphorus f?otassurri.-`, =,Magne'siiim;` ,,-'-Calcium4: - ""Sodium .: • ;.pH_, Acidity„ ; C:E:C, -Sample ID Field ID Lab Number ENR % Rate - 'Mehlich 3 Reserve ;f K Mg _ Ca Na' , :" $oih =`Buffer~ -,H Ibs/A ppm. :Rate; ppm Rate; :'PPm..: ' `,ltafes: pp mh ";:''-Rate i pp m;-= "Rate` '° ' rr1 :,Rate pp .` , pH , ; -- Ihdex;• ,'+ meg7100g `: meq/100g L09 11655 3.6 M 108 264 VH 150 H 123 M 1593 H 21 VL 6.8 0.3 9.7 NC = 220 NC = 77 L10 M 98 H M 479 L 15 VL 11656 3.3 M 109 149 169 5.2 6.76 1.7 5.0 NC=41 NC=50 W01 11657 1.8 L 80 40 M 58 L 64 M 1 435 M 121 L 1 5.5 6.83 1.0 4.0 , NC = 33 NC = 30 W02 11658 2.7 M 97 133 M 41 VL 47 L 633 M 118 VL 6.4 6.78 1.5 5.2 NC=27 NC=21 W03 70 H 12 43 L 440 M 16 VL 11659 2.7 M 98 5.4 6.81 1.2 4.1 NC = 58 NC = 62VH Percent Base.Saturation Nitrate- :-; - Sulfur- '"Zi'nc =,=Mangan'ese' _`-. , `IFon' ?Copps[' ` .:Boron -. _8oiubleSalts , Chloride .'; tfAluminurri Sample ID Field ID K Mg Ca Na H NO3N' $ - :. Zn<< �Mn" •;,,: Fe'°= -;Cu.. 'B :SS . - "/° % pplin Rate 'FPm ; : Rate PPm:' 'Rate. Ppm ;`., Rafe; `ppm°::. Rate. °ppm, .. Rate. ::,Rate 'm"s)cm `-Rate., 'PPm .<. : . PPm .. L09 18 M 17.5 VH 5 L 373 VH 8.4 VH 0.7 M 4.0 10.6 82.1 0.9 2.9 NC=37 NC=437.5 NC=31 NC=420.0 L10 M H 3 VL VH M VL 5.0 11.5 47.9 1.3 34.0 121 13.8 1293 11.3 10.3 NC=44 NC5.0 NC=19 NC=65.0 W01 M L 3 VL VH 1.2 M 0.2 VL 3.7 13.3 54.4 2.3 25.6 118 12.2 1295 NC=37 NC=55.0 NC=19 NC=60.0 W02 M H 2 VL VH 1.6 H 0.3 VL 2.0 7.5 60.9 1.5 28.4 118 17.1 1307 NC=37 NC=177.5 NC=13 NC=80.0 W03 H M 4 L VH VH VL 7.6 8.7 53.7 1.7 28.3 134 12.8 1260 13.7 10.2 NC=71 NC=70.0 NC=25 NC=185.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by Pam« �e �,,� H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble C.E.C. -Cation Exchange Capacity. Salts ms/cm x 640 =ppm. Analysis prepared by: A&L Eastern Laboratories, Inc. Pauric McGroary Page 4 of 4Rep@Do Acco ntNum r::4581 -0508A&L Eastern Laboratories. Account Number: 45819 - 7621 Whhpine.Road Richmond, Virginia 23237 (804) 743=9401 Fax (804) 271-WS www.aleastanl.com Send To: S&ME (1588) Grower: Submitted By: MARTIN MABE MARTIN MABE LEWIS FARMS Farm ID: 3718 OLD BATTLEGROUND RD JOB#1588-95-010 GREENSBORO NC 27410-2314 SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Received: 01/27/2015 Date Of Analysis: 01/28/2015 Date Of Report: 01/28/2015 Organic,Matter ::Pfios'pho'rus," - 'i?otasslum . ,' .a;Magnesium<. ,; - 1Calciurn , ' ;-.w Sodium'.-,. : pH= ,; _ "Acfdity,n CX.C- . Sample ID Field ID Lab Number ° �ENR :- /° Rate.' , Mehlich 3 Rese"rve K'-':,.,;" 'Mg : Ca Na :, Soil Buff_er,'H ;Ibs/A ... ..Rate`. PPm ppm" _Rate, .., . PPm Rate.° pPm> ";'Rate =.p .... pm'.; Rate: +PPm= .. Rate; . ,PH:; ",'Index:' .rrieq/100g? me4/100g,, W04 11661 2.4 L 81 170 VH 83 L 169 M 1983 VH 18 VL 71 0.0 11.6 NC=142 NC=42 AW-F1 11662 3.2 M 103 H 161 136 H 1159 H 1088 H 122 VL 6.6 0.5 7.7 NC=51 NC=70 JR-F1 11663 3.2 M 104 153 H 125 H 1142 H 1 913 M 121 VL 1 6.2 0.9 7.0 NC=44 NC=64 Percent Base.Saturation Nitrate -. ''•° ;'Sulfur,','a, : 'sZinc` :.,; ; :Manganese< .:::.;, ,Iron>.-; ,; ' :::Coppe'r':' ''.° `_Boson,:<` - Soluble`Salts?= `- Cfiloride',s `:Alurrtinum - Sample ID Field ID K Mg Ca Na H - NO N'' 3 ,,.� `'B' ASS �Ch� � AI' Pp m: Rate: p'pm'.Rate PPm;.,.....Rate:°'ppm:'...,Rate; pp•'m' .Rate iPPm Rate: ppm"'.' Ratei ms/cm ,:Rate; PPm. ~Rate .:: . mPPm W04 17 M 16.1 VH M 306 VH 4.6 VH 0.5 L 1.8 12.1 85.5 0.7 0.0 112 NC = 35 NC = 402.5 NC = 75 NC = 230.0 AW-F1 M H 7 L VH M C 4.5 17.2 70.6 1.2 5.9 120 15.2 1234 11.5 10.4 NC=42 NC=130.0 NC=44 NC=75.0 JR-F1 L H 6 L 212 VH 1.3 M VL 4.6 16.9 65.2 1.3 1 12.1 113 14.2 1 10.3 NC=27 NC=105.0 NC=38 NC=65.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by: p�c �c H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble Analysis prepared by: A8L Eastern Laboratories, Inc. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Pauric McGroary It should be noted that the majority of residuals land applied under NCDENR Permit No. WQ0000455 achieve pathogen reduction and vector attraction reduction requirements through alkaline stabilization. Therefore, the material being land applied is adding lime through most of the land application events. The pH's ranging from 4.6 to 7.1 on all fields is well suited for the growth of the corn, soybean, sorghum, wheat and coastal bermuda. 12". Martin Mabe Agronomist