WQ0006245_Residual Annual Report 2018_20190215

0.
CITY of% A�
NORTH' CAROLINA
January 30, 2019
too 0
REG
• u�
;Attention: Troy DobyR.'INCDQIQWR
NCDWR l�
Water QualityNon-DischargePermitting Unit FEB 5 2��9
1617 Mail Service Center
Raleigh, North. Carolina 27699-1636 . Non -Discharge
RE: Annual Report for 2018 Perrpiaing Unit
Alkaline Stabilization (WQ0006245)
Dear Mr. Doby:
Enclosed, you will find a copy of the required forms and lab data for the Alkaline Stabilization
program. Permit;#. WQ0006245.
This .permit was compliant for the year.
Should you require more information, or.if further action is required, please contact me at 704- 878-3438.
Sincerely,
Ken lows
Y
WWTP Supervisor, Fourth Creek WWTP
PO Box 1111 Statesville, NC 28687 ° ci,statesville:nc:us

GENERAL INFORMATION
ALKALINE STABLIZATION REPORT
CALENDER YEAR 2018
PERMIT NO. WQ0006245
FACILITY NAME: Fourth Creek WWTP NPDES NCO031836
LOCATION: 693 Bell Farm Road
MAILING ADDRESS: P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESPONSIBLE OFFICIAL: Andy Smith, Operations Manager
Water Resources
P.O. Box 1.111
Statesville, NC 28687-1111
[phone]
FACILITY OPERATOR: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
[phone]
RESIDUALS ORC: Ken Galloway
Plant Supervisor
P.O. Box 1111
Statesville, NC 28687-1111
APPLICATION: Class A Exceptional Quality Product
Test Data and Summary Operations
Attached

CLASS A �-.-p UAL DISTRIBUTION AND MARKETING/ SURFA(;., DISPOSAL CERTIFICATION':AND�SUMMARY�FO� :� .
WQ PERMIT #: WQ0006245 FACILITY NAME:
Fourth Creek Alkaline Stabilization
PHONE: [phone] COUNTY: Iredell OPERATOR: Ray Wyrick-`
FACILITY TYPE (please check one): 0 Surface Disposal (complete Part A (Source(s) and "Residual In". Volume only) and Part C)
2 Distribution and Marketing (complete Parts A; B, and C)
Was the facility in operation during the past calendar year? Yes 21 No 0 - * If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
4th Creek WWTP
38.88
84.34
123.22
Various Farmers
132.6
Farmland
February
NPDES# NCO031836
44.96
72.72
117.68
Various Farmers
54.4
Farmland
March
4th Creek WWTP
48.53
82.23
130.76
Various Farmers
40.8
Farmland
April
NPDES# NCO031836
26.07
41.65
67.72
Various Farmers
39.1
Farm / Landscape
May
4th Creek WWTP
44.58
86.19
130.77
Various Farmers
91.8
Farmland
June
NPDES# NCO031836
0
0
0
Various Farmers
0
July
4th Creek WWTP
0
0
0
Various Farmers
45
Farmland
August
NPDES# NCO031836
22.77
32.38
55.15
Various Farmers
103.7
Farmland
September
4th Creek WWTP
0
0
0
Various Farmers
0
October
NPDES# NCO031836
65.81
105.24
171.05
Various Farmers
13.6
Landscaping
November
4th Creek WWTP
0
0
0
Various Farmers
0
December
NPDES# NCO031836
66.59
95.36
161.95
Various Farmers
115.6
Farmland
Total from FORM DMSDF (sup)
0
0
0
0
Totals:
Annual (dry tons):,
358.19
600.11
958.3
636.6
Amendments used: Bulking Agent(s) used: Lime Kiln Dust
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)
Part C:
Facility was compliant during the past calendar -year with all conditions of the land application permit 21 Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: No ► If No, Explain in Narritive
I,, All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Permittee
Date Signature of Preparer *
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Z-1? -t
Date
DENR FORM DMSDF (12/2006)

ANNUAL S�TJ�.L SAI��g �JLANG SUli MARY. =F� 1VI
Please note that your permit may contain additional parameters to he -analyzed :The parameters can.bexeported �in FORM;.RSSF --B
WQ Permit Number: WQ0006245 . Laboratory:
Facility Name: Fourth Creek WWTP
Residual Source WQ # or NPDES # NC0031836
NPDES #:
WWTP Name:
Racirliial Analvcic data
1) 1Prism Labs
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Cone.
Limit
Sample or Composite Date
1/16/18
5/07/18
9/10/18
10/22/18
Percent Solids (%)
NA
69.40%
82%
95%
67%
Arsenic
75
26
<0.37
6.5
<0.46
Cadmium
85
<0.95
<0.082
<0.007
<0.10
Copper
4,300
47
170
35
42
Chromium
NA
N/A
N/A
N/A
N/A
Lead
840
14
5.1
3.6
<0.69
Mercury
57
0.049
0.24
0.13
0.11
Molybdenum
75
N/A
N/A
N/A
N/A
Nickel
420
10
10
6.1
11
Selenium
100
<17
<1.5
<0.12
<1.8
Zinc
7,500
76
76
34
79
Total Phosphorus
NA
3,600
3,200
2,300
3,200
- TKN
NA
6,000
4,800
3;400
1 <1100
Ammonia -Nitrogen
NA
180
2500
4100
380
1
Nitrate and Nitrite
NA
29
11
110
25
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a- system designed
to assure that qualified ersonnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for subm' g false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:' Fourth Creek WWTP Alkaline Stabilization WQ Permit Number: WQ0006245
WWTP Name: Fourth Creek WWTP NPDES Number: NCO031836
Monitoring Period: From 1/1/2018 To . 12/31/2018
Pathogen Reduction (15A.NCAC 02T .1106) - Please indicate level achieved and alternative performed:
a
Class A:
Alta A (timc/temp) o Alt B (Alk Treatment) 1.
Alt. C (Nor Testing) (�
..............................
Alt,) (No Prior Test) Ei
Process to -Further Reduce Patho cogs [3
If applicable to alternative± performed (Class :
6nly) indiente "Process to Further Reduce Pathot,ehs":
Compost [3teat
Ling, .
Heat (3
ermo Thhilic �
`.>.`:::.::: :
Beta Ray �l
Gamma R C�
"nation 0
Pastettrt
Class B:
Alt, (1) Fecal Density 0
Alt: (2) Process to Significantly Reduce Pathogens M
If applicable to alternative
performed (Class B
only) indicate "Process to Si iftieantl Reduce Patho ens":
Lime Stabilization Ci
Air Drying 0
Composting 0
Aerobic Digestion 0
AnaerobicDigestion Gl
If applicable to alternative performed (Class A or Class B) complete the
following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
dences
Frequency
of Analysis
Sample
Type
Yp
Analytical
Tech -
ni ue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
<0.3
<0.3
mpn/g
60 days
grab
'sm9221 e
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) [3
Alt. 2 (40-day bench) C(
Alt. 3 (30-day bench) [
Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization RI
Alt 7 (Drying - Stable) [3
jAlt..8 (Drying - Unstable) [
Alt. 9 (Injection) E�
Alt. 10 (Incorporation) [3
No vector attraction reduction alternatives were performed . , :
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name and litle (type or print)
Signature of Prepar
Land Applier Name and Title (if applicable)(type or print)
I
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

City Of Statesville Alkaline Stabilization Record For
Process to Further•Reduce Pathogens (PFRP)
PIN # 13aclk C°R..eR
Setup Date: I-1 a= I e
Removal From Bin Date: 1- 16 - i 8
Date
Time
pH >12.0 For 72 I-Irs.
TEMP: >52 Deg. C For 12 Hrs-
Operator .
I-12-1g
3 PM
Initial.pH: f�. d6
1- l a- /E
910° 3 Pr�l
1- 13- IS
g5° 03:oom
R� _.
Corrected pH: la.8Y
.II am
Final pH: 12, d ,/
Corrected pH: la s Sa
Hai 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been Met? ' N
BIN # L' OVER
Setup Date: /-,1a-/S
Removal From Bin Date: /-dff 8'
Date
Time
pi•I >12.0 For 72 Hrs:
TEMP. >52 Deg. C For 12 Hrs.
Operator
a AM
Initial pH: 12.91
/-a.2= j8'
goo �2:'�HPfn
g0° 07-'3Y
RLIJ
Corrected pHs 13, 0.1
1- a5-18
f : Y7 Pnq
Final pH: /d, '7 /
Corrected pH: /d. 8d
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72'H®ur.pH Criteria Been Met? ® N
BIN #C as R
Setup Date:. ,q-7- 18
Removal From Bin Date: d- la- 18
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
a- 7- I S
3: 05 Pm
Initial pH: U e7 -
a-?- IS
@ 3: o5 Pfn
a-8-i8
1?3 ° 07; 05
R.< w
Corrected pH: 12, SlitS3°
a - I a - 18
a : 13 Prr1
Final pWId. 57
R
kw
Corrected.pH: /,R. 71 : -
Has 12 Hour Ternp Criteria Been Met? Y N
Has 7.2 Hour pH Criteria Been Met? Y N
BIN # ,?,,,g p,' 1 e
Setup Date: a- g- I g
Removal From Bin Date; a- Id •-1 S
Date
Time
pH >12:0 For.72 Hrs.
TEMP. >52 Deg. C -For 12 Hrs.
Operator
a2- 8- 18
11: oo
Initial pH: Id.. 73
2-8- Is
86 ° iz; a7
d- ia- 18
71 a,@ 0 g:,jo
Rk w
Corrected pH: Ix, 9 1.
,1-12t- 18
121,13
Final pH: /d , 51
Corrected pH: f
Has 12 Hour Ternp Criteria.Been Met? Y
Has 72 Hour pH Criteria Been Met? `Y
BIN ##34 f ; Ie-
Setup Date: d- 4-1 ?
Removal From Bin Date: a- 13- 12
D;te
Time
' 14 :- 2' FOr 72 HrS.
i fVIP. >52 Deg. C FoP 1! Hrs*.,-,Operator
a-7- 18
10:30
Initial pH: /a, 6 4
,I- 4- I8
90°@ /Q:-/o
a- $a- 18
710 oe,19
RW
Corrected PH: 12.94
_ i it ' 1 8
11: 15
Final pA: l a.144.
Corrected pH: 12, 6 3
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour pH Criteria Been et? Y

€a*ti. ��•,: �a,a���a"��.'�r�+��_."�4.t�':.�,��..._=a��-'i�,� �.ar;;�" �,_ �, s�,a� �*'��'s�..rwx:`".�.�,
'City of Statesville Alkaline Stabilization Record For.
Processto Further -Reduce Pathogens (PFRP)
BIN # C,,4-a. Pa 9
Setup Date: 3- as -18
Removal From Bin Date: 3 - 2Z •• 0
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
3-a1-18
0q 3
Initial, pH: /a-. 11'7
-a a -1 S
90° @ W08
3 - .t 3 - 18
75°G" 07:10
��1'J.
Corrected pH: /2.97
3-26-1.g
10' Ltd
Final pH: 12.5?
Corrected pH: 12. 17,9
Has 12 Hour Ternp.Critei ria Been Met? Y N
Has 72 Hour PH Criteria Been Met?Vj
BIN # coa "Ea
Setup Date: 3-13- /8
Removal From Bin Date: 3- ,27- 19
Date
Time
pH >12.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
3-.13-18
AInitial
1o:ya +n
pH: U. 7 3
3-13---19
9006 it % 08
3- apt- 18
9y° w-20
Rui
Corrected pH: 0,93
3-ad-18
/0.'Sd
Final pH: /d, S 0
Rki'`1
Corrected pH:/,7,�0
Has 12 Hour Temp Criteria
Been Met? N
Has 72 *Hour.pH Criteria Beery Met? Y N
C OF
BIN ## BA
Setup Date: H-d 7- / S
Removal From Bin Date: q 30 -19
Date
Time
pH >12'.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
4-a7-19
09-56
Initial pH: Id, 6 8
0009 IV,2o
SL°@ 11,30
R4L�
Corrected pH: /a, 812
�-30-/8
I1� 3®
Final pH: /d, 65
�`'
Corrected.pH: /R. 8-3��
Has 12 Hour Temp Criteria Been Met'? Y N
Has 72 Hou.r pH Criteria Been Met? Y .
BIN # or 1;Ao
Setup Date: 5- 8- / $
Removal From Bin Date; 5- H- I g
®star
Time
pH >12:0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hors.
Operator
54- 18
12,08
InitialpH: ia.•55
5-S�- /8
90°@ 12.08
5-q-18
$,50 O'7.'00
R�>a/
Corrected pH: ia.`75.
0 8� y
finalpH: /2,53
R�IJ
Corrected pH: /a . eq
Has 12 Hoag Temp Criteria Been Met?
Has 72 Hour pH Criteria Been Met? Y
BIN ## a cN z E
Setup Date: 5 - q - 18
Removal .From Bin Date: 5- 1 q - 18
®ate
Time
� pH ?12.0 bir 72 Hrs.
iENIP. >52'Deg.0 Fok 12 Hrs'. "'
Operator'
5-4-18
il:Op
Initial pH: 1 J .5,2
5- Q - 18
SS° w 15
5-14 -12
90'& 07:30
Row
Corrected pH: 1a.70
5-1 q-18
07: 0 0
Final pk:
R
Corrected pH: AI. 65
Has 12 Hour Temp Criteria Been et? N
Has 72 Hour .p . �Crlterla Been et? Y. N

'City Of Statesville Alkaline Stabilization Record For.
Process's`® Further*Reduce Pathogens (PFRP)
BIN #
Setup ®ate: 8- 3o -18
Removal From Bin Date:
Date
Time
pH >12.0 For 72 hirs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
initial. pH: /W. -93
6- 3 o - 18 1
9 0 @ 09: 10
8 31- 18
?,20@ 0 S': 10
Corrected pH: Id. 83
9-14- 18
0 v 3 ®
Final pH: Id. 50
(�R�
Corrected pH: /a, 7
Has 12 Hour Temp Criteria Been Met? Y N
Has. 72 Hour pH Criteria, Been Met?
BIN 9
Setup Date: /0-15 18
Removal From Bin Date: /® - q-19
Date
Time
pH >12.0 For 72 Hrs:
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-15 18
II�uo
Initial pH: 1a.50
10-15-18
q0°@ 11:!5 .
!0-l6-lg
87*e0'7;y5
Ri,w
Corrected PH: Id.70
10-18-19
la;3o
Final pH: 1a. $14
1?��J
CorrecteilpH:1a,73
Has 12 Hour Temp Criteria
Been Met? N
Has 72'Hour-pH Criteria Beery Met? N
BIN ##
Setup Date: 10 -1'7 -18
Removal From Bin Date: /0
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
10-i7-1S
09,5©
Initial pH: /,,60
to-i7-i8
900@ 09%51
!0-1$-18
85°@ 08:145
Corrected pH: /a?,S0
l0-aa-18 110.13
iCorrected.pH:
Final pH la, 61
RZW
0,7
Has 12 Hour Temp Criteria Beery Met? Y N
Has 7.2 Hour -pH Criteria Been Met? Y N
BIN ##
Setup Date: /0 -18- ! 8
Removal From Bin Date; / 0- 2 2-
Date
time
pH >12k For' 72 Hrs.
TEMP. >52 Deg. C -For 12 Hrs.
Operator
/o-Ig-JcY
12:y�1
Initial pH: 12.. 51
10- i 8' 19
90°C' W tiq
$7° lo:oo
Corrected pH: Ia,71.
IO�ad-18
1 : 4 9
final pH: 1,2 912
R k w
Corrected pH:
Has 12 Hour Temp Criteria.Been et? Y
Has 72 Hour pH Criteria Been Met? Y
BIN ## / �'
Setup Date: is-a6-1
Removal From Bin Date: 11-31- 1$
®ate
..Time
.-pH->12.0 F®r 72 H' - .
TEIi1iP. >52Deg. C FoP 12 Hrs: "'
Operator
7
09:55
Initial pH: Id. 61�
90' @ 09; 00
We 09: 30
RkW
Corrected pH: %a. KR
Final pH: /) .53.
Corrected PH: 42.70
Has 12 Hour Temp Criteria Been Met? N
Has 72 Hour .p . Criteria Been Mqt? Y N

v¢iK'4iS.1R. 5'
City Of Statesville Alkaline Stabilization Record For
Process"to Further -Reduce Pathogens (PFRP)
BIN # 3 45
Setup Date: 12-9 7- I $
Removal From Bin Date: la - 31- 1-2
Date
Time
pH >12.0 For 72 Hrs.
TEMP: >52 Deg. C For 12 Hrs.
Operator .
11.00 .
Initial pH: /Z -94
�a•a 7- 18
SD°@ Il%/0
Id-aB- �8
860@ 0%iis
R,cW
Corrected pH: 12, 83
/a•3i-1.$
08%00
Final pH: fa. 53
!PAW
Corrected pH: /A 7 0
Has 12 Hour 'Temp Criteria Been Met? Y N
Has. 72 Hour pH Criteria Been Met? Y
Berl # ld 7 .
Setup Date: la-,28-/8
Removal From Bin Date:
Date
Time
pki >12.0 For 72 Hrs:
TEMP. >52 Deg.C For 12 Hrs.
Operator
a-aB--/8
09413
Initial pH: /a.7.2
I d - a'�� 1
90°@ 11;15.
R- 31- l8
80°@ o8706
R�IhI
CorrectedpHi 11.9a
Ix-31- J$
10:3®
Final pH: Id. 50
Corrected pH: 1a.67
Has 12 Hour Temp Criteria
Been Met? Y N
Has 72 'Hour.pH Criteria Been Met? Y N
BIN #
Setup Date:.
Removal From Bin Date:
Date
Time
pH >12-.0 For 72 Hrs.
TEMP. >52 Deg. C For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected.pH:
Has 12 Hour Temp Criteria Been Met? Y
Has 72 Hour pH Criteria Been Met? Y
BIN #
Setup Date:
Removal From Bin Date;
Date
time
pH >12:0 For.72 Hrs.
TEMP. >52 Deg. C.For 12 Hrs.
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hoag Temp Criteria Been Met? Y
Has 72 Hour pH Criteria Been Met? Y N
BIN #
Setup Date:
Removal From Bin Date:
Date
Time
pH >12.® F®r 72 Hrs.
1 Fillip. >52Deg. C Fos 12 Hrs: '
Operator
Initial pH:
Corrected pH:
Final pH:
Corrected pH:
Has 12 Hour Temp Criteria Been et? Y N
Has 72 Hour :pH. Criteria Been et? Y N

Jy \
RISM
_ABORATORIES$ INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 01/16/2018
Prism Work Order: 8010226
Case Narrative
01/26/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR = [ Na ] / SQRT { ( [Ca] + [Mg] ) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
[ 70/23 ] / SQRT { ([ 1300/20.04] + [ 0.03/12.15]) / 2 }
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 1 of 18

Data Qualifiers Key Reference:
BH MB greater than one half of the RL, but the sample concentrations are greater than lox the MB.
DM Sample diluted and RL increased due to the matrix.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

'
Sample Receipt Summary
0*k' ISM
Ism
Full -Service Analytical &
Environmental Solutions
01/26/2018
INC.
Prism Work Order: 8010226
Cl?--* Sample ID
Lab Sample ID
Matrix
Date Sampled Date Received
;, eFecal #1
8010226-01
Solid
01/16/18
01/16/18
StaLime Fecal #2
8010226-02
Solid
01/16/18
01/16/18
StaLime Fecal #3
8010226-03
Solid
01/16/18
01/16/18
StaLime Fecal #4
8010226-04
Solid
01/16/18
01/16/18
StaLime Fecal #5
8010226-05
Solid
01/16/18
01/16/18
StaLime Fecal #6
8010226-06
Solid
01/16/18
01/16/18
StaLime Fecal #7
8010226-07
Solid
01/16/18
01/16/18
StaLime
8010226-08
Solid
01/16/18
01/16/18
Samples were received in good condition at 2.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18

Full -Service Analytical &
;h ISM Environmental Solutions
LABORATORIES ING
Laboratory Report
01 /26/2018
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime Fecal #1
A idy Smith Prism Sample ID: 8010226-01
F. --jx 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time' Submitted: 01 /16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 67.3 % by 0.100 0.100 1 *SM2540 G 1/26/18 11:38 BJC P8A0406
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 18

{pp''�\\///A�'' Full -Service Analytical &
1-4a
`' z} I S 1 Y 1 Environmental Solutions
!LABORATORIES ING
Laboratory Report
01 /26/2018
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: StaLime Fecal #2
P idy Smith
Prism Sample ID: 8010226-02
F -_Ix 1111
Prism Work Order: 8010226
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
71.7 % by
0.100 0.100
1 *SM2540 G 1119/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.3
1 *SM9221 E 1/16/18 14:07 EGC
- P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. -
449 Springbrook Road- P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 18

.� Full -Service Analytical &
} I S M I Environmental Solutions
, ✓LABOHATOAIES. ING
Laboratory Report
01 /26/2018
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime Fecal #3
F idy Smith Prism Sample ID: 8010226-03
F Ix 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 65.8 % by 0.100 0.100 1 'SM2540 G 1/19/18 12:00 BJC P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 "SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] -Page 6 Of 8

, Full -Service Analytical &
R I S M Environmental Solutions
A�� ABORATORIES, ING
City of Statesville, NC
/ ndy Smith
)�x 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01/26/2018
1
Client Sample ID: StaLime Fecal #4
Prism Sample ID: 8010226-04
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result
Units
Report
MDL Dilution Method Analysis Analyst
Batch
Limit
Factor DatefTime
ID
General Chemistry Parameters
% Solids 65.9
% by
0.100
0.100 1 *SM2540 G 1/19118 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 1/16/18 14:07 EGC
P8A0222
i
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 18

�4 y
R' RFull -Service Analytical &
S M Environmental Solutions
LA90RATORIE3, ING
Laboratory Report
01 /26/2018
City of Statesville, NC
7 Ay Smith
F`. _ _ , _'->x 1111
Statesville, NC 28687
Client Sample ID: StaLime Fecal #5
Prism Sample ID: 8010226-05
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
General Chemistry Parameters
% Solids 68.2 % by 0.100 0.100 1 *SM2540 G 1/19/18 12:00 BJC P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 1/16/18 14:07 EGC P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 18

i 3 t Full -Service Analytical &
_ I S M I Environmental Solutions
��LABORATORIE$ ING
City of Statesville, NC
A ndy Smith
F _t)x 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
01 /26/2018
Client Sample ID: StaLime Fecal #6
Prism Sample ID: 8010226-06
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 69.8
% by
0.100
0.100 1
*SM2540 G 1/19/18 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 1/16/18 14:07 EGC
P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 9 of 18

4i 'n\/%'� Full -Service Analytical &
�R I S 1 1 Environmental Solutions
AM- s
�...ON TORIES, INC
Laboratory Report
01 /26/2018
City of Statesville, NC
"Andy Smith
. ' 0x 1111
Statesville, NC 28687
Project: StaLime (60 Day/7 Fecal)
Sample Matrix: Solid
Client Sample ID: StaLime Fecal #7
Prism Sample ID: 8010226-07
Prism Work Order: 8010226
Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
DateMme
ID
General Chemistry Parameters
% Solids 67.8
% by
0.100
0.100 1
"SM2540 G 1119118 12:00 BJC
P8A0288
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 1/16/18 14:07 EGC
P8A0222
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 18

_r
4R 1 M
'&�NLAeORATORIEs ING
Full -Service Analytical &
Environmental Solutions
Laboratory Report
01 /26/2018
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: StaLime
f ,ndy Smith Prism Sample ID: 8010226-08
F ,.)x 1111 Prism Work Order: 8010226
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/16/18 00:00
Time Submitted: 01/16/18 12:55
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1900
mg/kg dry
1100
230
10
*Calculation
1122118 10:49
CLB
[CALC]
% Solids
69.4
% by
0.100
0.100
1
*SM2540 G
1/19118 12:00
BJC
P8A0288
Weight
Ammonia as N
180
mg/kg dry
14
3.6
1
*SM4500-NH3 C
1118/18 14:00
BMS
P8A0246
Nitrate/Nitrite as N
29
mg/kg dry
7.2
0.79
1
*SM4500-NO3 F
1118/18 10:02
CLB
P8A0226
Phosphorus -Total
3600
mg/kg dry
72
10
20
*SM4500-P F
1/19118 9:20
CLB
P8A0225
Total Kjeldahl Nitrogen
6000
mg/kg dry
3600
770
10
*351.2
1122118 10:49
CLB
P8A0239
Total Metals
Mercury
SAR Soil Preparation
SAR Percent Moisture
Arsenic
Sodium Absorption Ratio
Cadmium
Calcium
Magnesium
Nickel
Selenium
Sodium
Sodium
Zinc
0.049
mg/kg dry
0.031
0.0030
1
*7471B
1/22118 17:12
JAB
P8A0298
Complete
g
1
*2-78-054
1/19/18 9:20
JAB
P8A0238
Complete
%by
0.100
0.100
1
*2-78-054
1/23118 15:20
JAB
P8A0333
Weight
26 DM, J
mg/kg dry
35
4.3
100
6010D
1/22/18 18:16
JAB
P8A0237
0.53
[blank]
0.30
0.016
1
*2-78-054
1125118 16:51
JAB
P8A0256
BRLDM
mg/kg dry
35
0.95
100
6010D
1/22/18 18:16
JAB
P8A0237
1300 BH
mg/L
10
1.0
100
*6010D
1125/18 16:51
JAB
P8A0256
47 DM, J
mg/kg dry
71
6.4
100
6010D
1/22/18 18:16
JAB
P8A0237
14 DM, J
mglkg dry
35
6.6
100
6010D
1/22/18 18:16
JAB
P8A0237
BRL
mg/L
0.10
0.0086
1
*6010D
1/23/18 12:26
JAB
P8A0256
10 DM, J
mg/kg dry
71
2.5
100
6010D
1122118 18:16
JAB
P8A0237
BRLDM
mg/kg dry
71
17
100
6010D
1/22/18 18:16
JAB
P8A0237
630 DM, J
mg/kg dry
2100
69
100
6010D
1/22/18 18:16
JAB
P8A0237
70 BH
mg/L
50
1.8
100
*6010D
1/23/18 12:18
JAB
P8A0256
79 DM, J
mg/kg dry
350
13
100
6010D
1/22/18 18:16
JAB
P8A0237
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18

' Level II QC Report
Full -Service Analytical & 1 /26/18
/RRI
S M I Environmental Solutions
L' 3 RATORIEa INC.
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Prism Work Order: 8010226
Al; `'+dy Smith Time Submitted: 1/16/2018 12:55:OOPM
P.1 _ _iK 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0237 - 3050B
Blank (P8A0237-BLK1)
Prepared: 01/18/18 Analyzed: 01/23/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.0543
0.50
mg/kg wet
J
Lead
0,0866
0.25
mg/kg wet
J
Nickel
0.0737
0.50
mg/kg wet
J
Selenium
BRL
0.50
mg/kg wet
Sodium
1.41
15
mg/kg wet
J
Zinc
0.188
2.5
mg/kg wet
J
LCS (P8A0237-BSI)
Prepared: 01/18/18 Analyzed: 01/23/18
Arsenic
25.6
0.25
mg/kg wet
25.00 102 80-120
Cadmium
26.1
0.25
mg/kg wet
25.00 104 80-120
Copper
27.0
0.50
mg/kg wet
25.00 108 80-120
Lead
26.0
0.25
mg/kg wet
25.00 104 80-120
Nickel
26.2
0.50
mg/kg wet
25.00 105 80-120
Selenium
24.4
0.50
mg/kg wet
25.00 98 80-120
Sodium
283
15
mg/kg wet
250.0 113 80-120
2
24.7
2.5
mg/kg wet
25.00 99 80-120
Batch P8A0238 - SAR 2-78-054
Blank (P8A0238-BLK1)
Prepared.: 01/18/18 Analyzed: 01/19/18
SAR Soil Preparation
Complete
g
Batch P8AO256 - 301 OA
Blank (P8A0256-BLKI)
Prepared: 01/18/18 Analyzed: 01/23/18
Sodium Absorption Ratio
BRL
0.30 [blank]
Calcium
1.68
0.10 mg/L BH
Magnesium
BRL
0.10 mg/L
Sodium
2.40
0.50 mg/L BH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 18

Full -Service Analytical
JEnvironmental Solutions
' ��LABOR TORIES, INC.
Level II QC Report
1 /26/18
City of Statesville, NC
Al -dy Smith
P., is 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: StaLime (60 Day/7 Fecal)
Prism Work Order: 801 Q226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting
Spike Source %REC RPD
Analyte
Result Limit
Units Level Result %REC Limits RPD Limit Notes
Batch P8AO298 - 7471 B
Blank (P8A0298-131-K1)
Prepared &Analyzed: 01/22/18
Mercury
BRL 0.020
mg/kg wet
LCS (P8A0298-BS1)
Prepared &Analyzed: 01/22/18
Mercury
0.462 0.020
mg/kg wet 0.4167 111 80-120
Batch P8A0333 - NO PREP
Duplicate (P8A0333-DUP1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/23/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 30 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 Of 18

Level II QC Report
/'90_1 t IFull-Service Analytical & 1/26/18
Environmental Solutions
LAC WCRIES. INC.
City of Statesville, NC
A Idy Smith
P _x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (60 Day/7 Fecal)
Prism Work Order: 8010226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8AO225 - SM4500-PB5
Blank (P8A0225-BLK1) Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8A0225-BS1) Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 95.6 2.5 mg/kg wet 100.0 96 90-110
Matrix Spike (P8A0225-MS1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 3160 72 mg/kg dry 144.2 3590 NR 80-120 MC
Matrix Spike Dup (P8A0225-MSD1) Source: 8010226-08 Prepared: 01/18/18 Analyzed: 01/19/18
Phosphorus -Total 3300 72 mg/kg dry 144.2 3590 NR 80-120 4 20 MC
Batch MOM - NO PREP
Blank (P8A0226-BLK1) Prepared &Analyzed: 01/18/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8A0226-BSI) Prepared &Analyzed: 01/18/18
Nitrate/Nitrite as N 48.3 5.0 mg/kg wet 50.00 97 80-120
Matrix Spike (P8A0226-MS1) Source: 8010226-08 Prepared &Analyzed: 01/18/18
1 litrite as N 97.3 7.2 mg/kg dry 72.10 29.4 94 80-120
1 Spike Dup (P8A0226-MSD1) Source: 8010226-08 Prepared &Analyzed: 01/18/18
Nitrate/Nitrite as N 97.8 7.2 mg/kg dry 72.10 29.4 95 80-120 0.5 20
Batch P8A0239 - 351.2
Blank (P8A0239-BLK1) Prepared: 01/18/18 Analyzed: 01/22/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 14 of 18

A,' Level II QC Report
A,
"5 Full -Service Analytical & 1/26/18
I oSplEs, INC.
Environmental Solutions
- 'E
City of Statesville, NC
At, dy Smith
P." k 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime (60 Day/7 Fecal)
Prism Work Order: 8010226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0239 - 351.2
LCS (P8A0239-BS1) Prepared: 01/18/18 Analyzed: 01/22/18
Total Kjeldahl Nitrogen 500 100 mg/kg wet 500.0 100 90-110
Batch P8AO246 - SM4500-NH3 B
Blank (P8A0246-BLK1) Prepared &Analyzed: 01/18/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8A0246-BS1) Prepared &Analyzed: 01/18/18
Ammonia as N 504 10 mg/kg wet 500.0 101 80-120
Batch P8AO406 - Solids, Dry Weight
Duplicate (P8A0406-DUP1) Source: 8010226-01 Prepared &Analyzed: 01/26/18
% Solids 67.5 0.100 % by Weight 67.3 0.3 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 18

,
/'Pl Full -Service Analytical &
I S Environmental Solutions
LA6ORATORIE^.$ INC.
City of Statesville, NC
At, sdy Smith
P. >c 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Project: StaLime (60 Day/7 Fecal)
Level II QC Report
1 /26/18
Prism Work Order: 8010226
Time Submitted: 1/16/2018 12:55:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8A0222 - NO PREP
Blank (P8A0222-BLK1) Prepared & Analyzed: 01 /16/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 16 of 18

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
80( `18
P8A0239
0.05 g
25 mL
01/18/18 10:00
Prep Method: SM4500-NI-13 B
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0246
1.01 g
50 mL
01/18/18 12:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0225
1 g
50 mL
01/18/18 7:08
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8010226-01
P8A0406
30 g
30 g
01/26/18 11:38
8010226-02
P8A0288
30 g
30 g
01/19/18 12:00
8010226-03
P8A0288
30 g
30 g
01/19/18 12:00
8010226-04
P8A0288
30 g
30 g
01/19/18 12:00
8010226-05
P8A0288
30 g
30 g
01/19/18 12:00
8010226-06
P8A0288
30 g
30 g
01/19/18 12:00
8010226-07
P8A0288
30 g
30 g
01/19/18 12:00
8010226-08
P8AO288
30 g
30 g
01/19/18 12:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8njn29r-08
P8A0256
50 mL
50 mL
01/19/18 9:20
8108
P8A0256
50 mL
50 mL
01/19/18 9:20
8 --08
P8A0256
50 mL
50 mL
01/19/18 9:20
8010226-08
P8A0256
50 mL
50 mL
01/19/18 9:20
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0237
2.04 g
50 mL
01/18/18 9:50
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0298
0.55 g
50 mL
01/22/18 10:55
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8010226-08
P8A0238
250 g
250 g
01/18/18 9:20
1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 17 of 18

CHAHN OF'CUSTODY RECORD
'7`9 ME 7
Full -Service Analytical &
Environmental Solutions p&aa Op a 4.1 To EMSURE PROPER 131111.11.11MG,
I S M I
co
`
T 0
V,LABORATORIES, INC.
Project Name:Recoivera
ON iNE00
i ICE?
449 Springbrook Road Charlotte, NC 26217 Short Hold Analysis: (Yes) (NO) LIST Project: (Yes) (NO)
Phone [phone] Fax:[phone]
P-Of
"Please ATTACH any project specific reporting (OC LEVEL 0 OR III IV)
C 3 pr 9 414-r
Client Company Name: a
provisions and/or QC Requirements
-"A,94
Report To/Contact Name: Invoice To:
4 S"r
Reporting Address: Address,
Phone: FaX 00 (NO): Purchase order No./[Billing Reference TO BE MLLED lM BY CUEMUSAMPUNG PERSONNEL
E-mail Address: Requested Due Date 0 1 Day Q 2 Days EI 3 Days Q 4 Days Q 5 Days Cefflication: MELAC_ DOD— FL_ MC
EDD Type: PDF Excel Other 11 El B-9 Days U Standard 10 days 0 Rush Work Must Be
"Working Days Pre -Approved
Sc OTHER MIA
Samples Site Location Marne: Ag_m Jh CdPFCP, received after 14:00 will be processed next business day.
Site Location Physical Address: d 13 "Big, Y1 5&�-,,,, '41 Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— NO —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) Sampie leed Upon CollectRon: YES— NO_
TIMEMAT
SAMPLE CONTAINER
PRESERVA_
ANALYSIS
REQUESTEDRIX
PRISM
LAB
CLIENT
DATE
COLLECTED
(SOIL,
REMARKS
SAMPLE
COLLECTED
MILITARY
HOURS
WATER OR
SLUDGE)
*TYPE
SEE BELOW
Mo.
SIZE
TIESSCRIPTION
41trp
ID NO.
As
'5
C2
aV
k � �6r
12,
Sampler's Signature Sampled By (Print Name) IF4 Affiliation
Upon relinquishing, this Chain of Custody is your authorization for Prism to proc with the analyses as requested above. Any changes -must be
initialized.
subm,�ted writing to th&,lPrism Project Manager. There will foe charges for any d an es after analyses have been
Relin,�(I_�hed gnatur
Received B, DI/e
Mi itional Comments:
tits our Add !'-te r
7(nMa�ap­
Relinquished Bvf (Signature) Re erved By: (Signature) DT e
1W Poo 09i"T,
Field' h�fe
Relinquishe2dy. (Signature) %Rec6fve�For Prism Laboratories By: D
Method of Shipment: 0 TA ALL SAMPLE COOLERS SHOULD BE FED SNU I WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT CCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
7313rism
S Field Service Ll Othero
OTHER:
NPDES: GROUNDWATER: DRINKING WXi ER: SOLID WASTE: RA: CERCLA LANDFILL
U NC 0 SC D A , SC LI NC SC 0 NC LI SC 0 NC 0 SC ICN C E El NC 0 SC J NC El SC Q NC Q SC
1
r_1 F_n 0 0 Ell EI %-_-�'GNAL
*rnkii-ramsp —a vp, F rnnr�-R- A = Arnhi-r (' = ('Ip;;r G= Glass P = Plastic: TIL = Teflon -Lined Car) VOA = Volatile Organics Analysis (Zero Head Space)

3
� 'PRISM �
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 01/29/2018
Prism Work Order: 8010426
Case Narrative
02/06/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/21
SAR = [ 92/23.0 ] / SQRT { ( [1200/20.0] + [0.039/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
7��- a- - &"_
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 10

Data Qualifiers Key Reference:
A Recovery of Low-level ICV (73%) is less than the lower limit (80%). Result might have a slight low bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 10

Full -Service Analytical &
- ,!JR I s Y , I Environmental Solutions
LA6ORATORIES, INC.
Sample Receipt Summary
02/06/2018
Prism Work Order: 8010426
C! 1­4 Sample ID Lab Sample ID Matrix Date Sampled
1
8010426-01 Solid 01/29/18
Samples were received in good condition at 3.6 degrees C unless otherwise noted.
Date Received
01 /29/18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 10

Full -Service Analytical &
P R ISM I Environmental Solutions
VLABORATORIEB, INC.
Laboratory Report
02/06/2018
C.P'Lnf Statesville, NC Project: StaLime Client Sample ID: StaLime
k; Andy Smith Prism Sample ID: 8010426-01
[m',_JDx 1111 Prism Work Order: 8010426
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 01/29/18 12:00
Time Submitted: 01/29/18 13:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Plant Available Nitrogen
1200
mg/kg dry
460
98
5
*Calculation
2/1/18 9:42
CLB
[CALC]
% Solids -
82.6
% by
0.100
0.100
1
*SM2540 G
1/30118 14:00
JLR
P8A0474
Weight
Ammonia as N
110
mg/kg dry
12
2.9
1
*SM4500-NH3 C
1/31118 11:45
BMS
P8A0478
Nitrate/Nitrite as N
6.3
mg/kg dry
6.1
0.67
1
*SM4500-NO3 F
2/1118 9:42
CLB
P8130001
Phosphorus -Total
2200
mg/kg dry
61
8.7
20
*SM4500-P F
2/2118 9:32
CLB
13860004
Total Kjeldahl Nitrogen
3900
mg/kg dry
1500
320
5
*351.2
1131118 11:09
CLB
P8A0479
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
1/30/18 10:09
BMS
P8A0481
Total Metals
Mercury
0.17
mg/kg dry
0.024
0.0023
1
*747113
2/2118 12:56
JAB
P8130039
SAR Soil Preparation
Complete
g
1
*2-78-054
2/1/18 10:00
JAB
P8130045
SAR Percent Moisture
67.2
% by
0.100
0.100
1
*2-78-054
2/2118 11:10
PJF
P8B0050
Weight
Arsenic
4.5
mg/kg dry
3.0
0.36
10
*6010D
211/18 14:47
JAB
P8A0464
Absorption Ratio
0.71
[blank]
0.30
0.016
1
*2-78-054
2/2/18 19:49
JAB
P8130046
n
BRL
mg/kg dry
3.0
0.080
10
*6010D
2/1/18 14:47
JAB
P8A0464
Calcium
1200
mg/L
1.0
0.10
10
*6010D
212/18 19:41
JAB
P8130046
Copper
29
mg/kg dry
6.0
0.54
10
*6010D
211/18 14:47
JAB
P8A0464
Lead
7.3
mg/kg dry
3.0
0.55
10
*6010D
2/1/18 14:47
JAB
P8A0464
Magnesium
BRL
mg/L
0.10
0.0086
1
*6010D
2/2/18 19:49
JAB
P8130046
Nickel
6.5
mg/kg dry
6.0
0.21
10
*6010D
2/1/18 14:47
JAB
P8A0464
Selenium
23 A
mg/kg dry
6.0
1.4
10
*6010D
2/1/18 14:47
JAB
P8A0464
Sodium
680
mg/kg dry
180
5.9
10
*6010D
2/1/18 14:47
JAB
P8A0464
Sodium
92
mg/L
0.50
0.018
1
*6010D
2/2/18 19:49
JAB
138130046
Zinc
68
mg/kg dry
30
1.1
10
*6010D
2/1118 14:47
JAB
P8A0464
This report should not, be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 10

� RFull -Service Analytical &
I S M I Environmental Solutions
�IABORATORIE& INC.
Level II QC Report
2/6/18
City of Statesville, NC Project: Stal-ime
At dy Smith
P.:K 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting
Analyte Result - Limit Units
Batch P8A0464 - 3050B
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P8A0464-BLK1)
Prepared &Analyzed: 01/31/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mglkg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8A0464-BS1)
Prepared &Analyzed: 01/31/18
Arsenic
12.2
0.25
mg/kg wet
12.50 97
80-120
Cadmium
12.4
0.25
mglkg wet
12.50 100
80-120
Copper
13.3
0.50
mg/kg wet
12.50 107
80-120
Lead
12.6
0.25
mg/kg wet
12.50 101
80-120
Nickel
12.7
0.50
mg/kg wet
12.50 102
80-120
Selenium
11.9
0.50
mg/kg wet
12.50 95
80-120
S2, "M
1280
15
mg/kg wet
1250 103
80-120
21i
12.4
2.5
mg/kg wet
12.50 99
80-120
Batch P8B0039 - 7471 B
Blank (P860039-13LK1) Prepared &Analyzed: 02/02/18
Mercury BRL 0.020 mg/kg wet
LCS (P8130039-BSI) Prepared &Analyzed: 02/02/18
Mercury 0.428 0.020 mg/kg wet 0.4167 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 -'Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 10

�P RismFull-Service Analytical snvironmental Solutions
R
Level II QC Report
2/6/18
City of Statesville, NC Project: Stal-ime
Al ' , dy Smith
P. x 1111
Statesville, NC 28687
Total Metals - Quality Control
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8B0045 - SAR 2-78-054
Blank (PBB0045-BLK1) Prepared & Analyzed: 02/01 /18
SAR Soil Preparation Complete g
Batch 138B0046 - 3010A
Blank (P8130046-BLK1)
Prepared &Analyzed: 02/02/18
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium
0.194 0.10 mg/L BH
Magnesium
BRL 0.10 mg/L
Sodium
1.74. 0.50 mg/L BH
Batch P8B0050 - NO PREP
Duplicate (P8B0050-DUP1)
Source: 8010426-01 Prepared &Analyzed: 02/02/18
SAR Percent Moisture
68.6 0.100 % by Weight 67.2 2 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 10

Level Il QC Report
PRISMFull -Service Analytical 2/6/18
�i Environmental Solutions
�l LAsoRATORIES, ING.
City of Statesville, NC
Aidy Smith
P. , -'x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch MOM - SM4500-NH3 B
Blank (P8A0478-BLK1)
Prepared &Analyzed: 01/31/18
Ammonia as N
BRL
10
mg/kg wet
LCS (P8A0478-BS1)
Prepared &Analyzed: 01/31/18
Ammonia as N
484
10
mg/kg wet
500.0 97 80-120
Batch P8A0479 - 351.2
Blank (P8A0479-BLK1)
Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen
BRL
25
mg/kg wet
LCS (P8A0479-BS1)
Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen
532
100
mglkg wet
500.0 106 90-110
Matrix Spike (P8A0479-MS1)
Source:
8010426-01
Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen
10700
1500
mg/kg dry
6055 3900 112 90-110 MI
Matrix Spike Dup (P8A0479-MSD1)
Source:
8010426-01
Prepared: 01/30/18 Analyzed: 01/31/18
Total Kjeldahl Nitrogen
11000
1500
mg/kg dry
6055 3900 117 90-110 3 20 MI
Batch P81B0001 - NO PREP
I P8B0001-BLK1
Naraiemlitrite as N
BRL 5.0 mg/kg wet
02/01 /18
LCS (P8B0001-BS1) Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N 48.9 5.0 mg/kg wet 50.00 98 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 10

PRISM
' -- Ye'LLASOR TORIES, INC.
Full -Service Analytical &
Environmental Solutions
Level II QC Report
2/6/18
City of Statesville, NC Project: StaLime
Al1dy Smith
F, x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8B0001 - NO PREP
Reporting
Result Limit Units
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P8B0001-MS1)
Source: 8010426-01
Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N
Matrix Spike Dup (P8B0001-MSD1)
68.2 6.1 mg/kg dry
Source: 8010426-01
60.55 6.30 102 80-120
Prepared &Analyzed: 02/01/18
Nitrate/Nitrite as N
Batch P8B0004 - SM4500-PB5
65.9 6.1 mg/kg dry
60.55 6.30 98 80-120 3 20
Blank (P8B0004-BLK1)
Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total
LCS (P8B0004-BS1)
BRL 2.5 mg/kg wet
Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total
Matrix Spike (P8130004-MS1)
96.3 2.5 mg/kg wet
Source: 8010426-01
100.0 96 90-110
Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total
Matrix Spike Dup (P8B0004-MSD1)
2480 61 mg/kg dry
Source: 8010426-01
121.1 2150 269 80-120 MC
Prepared: 02/01/18 Analyzed: 02/02/18
Phosphorus -Total
2560 61 mg/kg dry
121.1 2150 331 80-120 3 20 MC
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 10

�i
Full -Service Analytical &
l PAR ISM Environmental Solutions
/,zi ORATORIEs, INC.
City of Statesville, NC
A dy Smith
P" c 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
2/5/18
Prism Work Order: 8010426
Time Submitted: 1/29/2018 1:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8AO481 - NO PREP
Blank (P8A0481-BLK1) Prepared & Analyzed: 01/30/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
8010426-01 P8A0479 0.05 g 25 mL 01/30/18 9:40
Prep Method: SM4500-NI-13 B
Lab Number Batch Initial Final Date/Time
8010426-01
P8A0478
1.03 g
50 mL
01/31/18 11:45
Prep Method: SM4500-PBS
Ij ` ',�5mber
Batch
Initial
Final
Date/Time
l�—_ �'-01
P8130004
1 g
50 mL
02/01/18 9:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0474
30 g
30 g
01/30/18 14:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8130046
50 mL
50 mL
02/02/18 11:00
8010426-01
P860046
50 mL
50 mL
02/02/18 11:00
8010426-01
P8130046
50 mL
50 mL
02/02/18 11:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8A0464
2.03 g
50 mL
01/31/18 9:00
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8010426-01
P8130039
0.61 g
50 mL
02/02/18 9:33
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
>6-01 P8130045 250 g 250 g 02/01/18 10:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 10

Haail EW CUR)"TIMOV RP�CDRO
g_­! Full -Service Analytical &
OF (QUOTE 4 TO IEMSIIJ� 'WER ISULLUMS'
YF-, NJ" N/A
Environmental Solutions PAGE_
Sample s INTACT uport arrival?
LA30INFORIES, INC. Project Name:
�Re6�-lved ON WET ICE?
449 Springbrook Road « Charlotte, NC 28217
« rax: 704/52 5-0409 Short Hold Analysis: (Yes) (NO), USTProject: (Yes) (NO)
PROPER PRESERVATIVES indicated?
Phone [phone]
q *Please ATTACH any project specific reporting (OC LEVEL I li III IV)
C11-11IX
Received WITHIN HOLDING TIMES?
Client Company Name: 0-F, -
provisions and/or QC Requirements
CUSTODY SEALS INTACT?
I
Report To/Contact Ham( - Invoice
To:
VOLATI LES rer'd W/0IJT HEADSPACE' ;
Reporting Address: Address:
PROPER GONTAiNERS user.J?
L TEMP Lh2,,,, absented
C
Phorie:70','07'8-3q3(6 F=6 (No):702'272- U-1:5 Purchase Order No./Billing Reference— TO BE FILLED IN BY CLIENT/SAMPLONG PERSONNEL
Email Address: Requested Due Date 0 1 Day 0 2 Days 0 3 Days 0 4 Days D 5 Days Certification: NELAC_ Do®_
FL_ NO
EDD Type: PDF Excel Other "Working Days" 0 6-9 Days U Standard 10 days E, Rush Work Must Be
— — Pre -Approved
SIC OTHER
N/A
r,
Site Location Name: Fom rA CrC_�& Samples received after 14:00 will be processed next business day.
Water Chlorinated: YES— NO
Site Location Physical Address: 03 BIM F40m, ftl Turnaround
time is based on business days, excluding weekends and holidays.
—
(SEE REVERSE FOR & CONDITIONSRDING SERVICFS
I Sample iced Upon Collection: YES—
NO
RENDERED BY PRISMTERMS LABORATORIES, INCC. TO CLIENT)
—
TIME MATRIX
SAMPLE CONTAINER ANALYSIS REQUESTED
PRISM
CLIENT DATE COLLECTED (SOIL,
PRESERVA-
TIVES N
REMARKS
LAB
ID NO.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
*TYPE NO. SIZE
HOURS SLUDGE)
SEE BELOW
NAaSA03
As
PA N/
C C k
9
SA R
14
C Cw
�Ade /_1
Name) &A 0 k Affiliation
Sampler's Signature,:p Sampled By
(Print r-
=14=6_
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed'Ath theanalyses as requested above. Any changes must be
h U. analyses have been Initialized.
submitted in writing to the Prism Project Manager. There wilO be charges for any c a ges afte
_91�fitaryIHOuls;
7
D ate
Additional Comments:
Site Tiftte-,
Relin (Signature) Received By. (Slgnatuime�)�,
fished By: (Sig
Z,
�(Signature)
r
-Arri-Va
T
s I I b iMe:
Relirzqeished By: (Signature) Received
Date
By
.
iquished By: (Signature) i Received For Prism Lor tories By: Date
Field Tech Fes:
_U Is 1
d M TRANSPORTATION TO THE LABORATORY.
i (510) 3d—ofShipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SE FOR OOC Group NO.
—1
Mileage:
L
CD SAMPLES ARE NOTA,bEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY. .1) A
NOT
6CD
0 �d Ex 0 UPS L31 Hand -delivered Field Service 0 Other
DR6N SOLED WASTE: RCRA: CERCLA LANDFILL
GROUNDWATE KING WATER:
0 ES: U R:
6STC E] SC
— C 0 Sc ONC OSC ®NC USC
I®TiER:
UNC 0 SC UNCOSC ONC USC ©NC ©SCONCOSC
C)
WARKIFIR TVIPF-t CO DES: A = Amber C = Clear G= Glass
p = Plastic; T L = Teflon -Lined Cap VOA =Volatile Organics Analysis (Zero Head Space)
OF�,GINAL

Case Narrative
-ISM
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 02/12/2018
Prism Work Order: 8020215
02/20/2018
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
SAR = [ 84/23 ] / SQRT { ( [1100/20] + [0.022/12]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
t the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
) �_ a_. (?,
Robbi A. Jones
President/Project Manager
I c-
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 10

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
DM Sample diluted and RL increased due to the matrix.
Mc Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: 704/525,0409 Page 2 of 10

rx' .
Full -Service Analytical &
Sample Receipt Summary
..a 1
P ISM I Environmental Solutions
02/20/2018
,AP577­77777'�-_� LABORATORIES, INC.
Prism Work Order: 8020215
C'y--~' Sample ID Lab Sample ID Matrix Date Sampled Date Received
F ,
e 8020215-01 Solid 02/12/18 02/12/18
Samples were received at 21.3 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 10

I S M
Fun -Service Analytical s Environmental SolutionsORATOR
Laboratory Report
02/20/2018
Gi4y �f Statesville, NC Project: StaLime Client Sample ID: StaLime
11 lndy Smith Prism Sample ID: 8020215-01
_Jx 1111 Prism Work Order: 802021.5
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 02/12/18 12:00
Time Submitted: 02/12/18 15:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mg/kg dry
520
110
5
*Calculation 2119/18 9:20
CLB
[CALC]
% Solids
72.9
% by
0.100
0.100
1
*SM2540 G 2/13/18 15:11
BJC
P8B0256
Weight
Ammonia as N
96
mg/kg dry
14
3.4
1
*SM4500-NH3 C 2115/18 14:30
BMS
P8130325
Nitrate/Nitrite as N
21
mg/kg dry
6.9
0.76
1
*SM4500-NO3 F 2/16/18 10:58
CLB
P8B0287
Phosphorus -Total
2300
mg/kg dry
69
9.9
20
*SM4500-P F 2/14118 11:53
CLB
P880248
Total Kjeldahl Nitrogen
5600
mg/kg dry
1700
370
5
*351.2 2119118 9:20
CLB
P8B0321
Microbiological Parameters
Fecal Coliforms
Total Metals
BRL
MPN/g dry
0.3
1
*SM9221 E
2113/18 9:05
EGC
P860282
Mercury
0.13
mglkg dry
0.028
0.0026
1
*7471B
2/19118 12:17
JAB
P8130339
SAR Soil Preparation
Complete
g
1
*2-78-054
2119/18 9:00
JAB
P860279
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
2/19/18 8:00
JAB
P8130332
Weight
Arsenic
8.1 DM
mg/kg dry
3.4
0.41
10
*6010D
2/16/18 16:41
JAB
138130253
EX,"--, v Absorption Ratio
0.68
[blank]
0.30
0.016
1
*2-78-054
2/16/18 18:35
JAB
P8130324
i
(i n
BRLDM
mg/kg dry
3.4
0.091
10
*6010D
2/16/18 16:41
JAB
P860253
Calcium
1100 B
mg/L
1.0
0.10
10
*6010D
2116118 18:26
JAB
P8130324
Copper
37 DM
mg/kg dry
6.8
0.61
10
*6010D
2116118 16:41
JAB
P8B0253
Lead
5.2 DM
mg/kg dry
3.4
0.63
10
*6010D
2/16/18 16:41
JAB
P8B0253
Magnesium
BRL
mg/L
0.10
0.0086
1
*6010D
2/16/18 18:35
JAB
P8B0324
Nickel
8.4 DM
mg/kg dry
6.8
0.24
10
*6010D
2116118 16:41
JAB
P8130253
Selenium
23 DM
mglkg dry
6.8
1.6
10
*6010D
2/16118 16:41
JAB
P8130253
Sodium
720 DM
mg/kg dry
200
6.7
10
*6010D
2/16/18 16:41
JAB
P8130253
Sodium
84 B
mg/L
0.50
0.018
1
*6010D
2/16118 18:35
JAB
P8130324
Zinc
68 DM
mg/kg dry
34
1.2
10
.*6010D
2/16/18 16:41
JAB
P8130253
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 10

Aki
o7j1�ISFull-Service Analytical &
'--� Environmental Solutions
KVi ORATORIES ING.
Level 11 QC Report
2/20/18
City of Statesville, NC
A, '-,dy Smith
P.?. -.K 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8BO253 - 3050B
Project: Stal-ime
Reporting
Result Limit Units
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit
Notes
Blank (P8B0253-BLK1)
Prepared & Analyzed: 02/14/18
Arsenic
BRL
0.25
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P8130253-BS9)
Prepared &Analyzed: 02/14/18
Arsenic
12.7
0.25
mg/kg wet
12.50 101
80-120
Cadmium
12.9
0.25
mg/kg wet
12.50 103
80-120
Copper
13.5
0.50
mg/kg wet
12.50 108
80-120
Lead
13.1
0.25
mg/kg wet
12.50 105
80-120
Nickel
13.0
0.50
mg/kg wet
12.50 104
80-120
Selenium
12.3,
0.50
mg/kg wet
12.50 98
80-120
1320
15
mg/kg wet
1250 106
80-120
12.7
2.5
mg/kg wet
12.50 102
80-120
Batch P8B0279 - SAR 2-78-054
Blank (P8BO279-BLK1) Prepared: 02/15/18 Analyzed: 02/19/18
SAR Soil Preparation Complete g
Batch P8BO324 - 301 OA
Blank (P8B0324-BLK1)
Prepared &Analyzed: 02/16/18
Sodium Absorption Ratio
BRL 0.30 [blank]
Calcium
0.207 0.10 mg/L BH
Magnesium
BRL 0.10 mg/L
Sodium
1.05 0.50 mg/L BH
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 10

Level II QC Report
Full -Service Analytical &
/Z�-/L4BORATORIES, I S I�lI 2/20/18
Environmental Solutions
ING
City of Statesville, NC Project: Stal-ime Prism Work Order: 8020215
Ai, dy Smith Time Submitted: 2/12/2018 3:35:OOPM
P:__ �bK 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %BREC Limits RPD Limit Notes
Batch P8BO332 - NO PREP
Duplicate(P8B0332-DUP1) Sou_rce:8020215-01 Prepared:02/16/18 Analyzed: 02/19/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.2 200
Batch P8B0339 - 7471 B
Blank (PBB0339-BLK1) Prepared & Analyzed: 02/19/18
Mercury BRL 0.020 mg/kg wet
LCS (P8130339-13SI) Prepared &Analyzed: 02/19/18
Mercury 0.424 0.020 mg/kg wet 0.4167 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 10

Level II QC Report
Full -Service Analytical & 2/20/18
A/=�tM07LABOMTORIES,
R I S Environmental Solutions
INC.
City of Statesville, NC
A" Ay Smith
P"_ _� x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Analyte
Reporting
Result Limit Units
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit Notes
Batch P8BO248 - SM4500-PB5
Blank (P8130248-BLK1)
Prepared & Analyzed: 02/14/18
Phosphorus -Total
LCS (P8B0248-BS1)
BRL 2.5 mg/kg wet
Prepared &Analyzed: 02/14/18
Phosphorus -Total
Matrix Spike (P8B0248-MS1)
95.2 2.5 mg/kg wet
Source: 8020215-01
100.0 95
Prepared &Analyzed: 02/14/18
90-110
Phosphorus -Total
Matrix Spike Dup (P8B0248-MSD1)
2190 69 mg/kg dry
Source: 8020215-01
137.1 2330 NR
Prepared &Analyzed: 02/14/18
80-120 MC
Phosphorus -Total
2470 69 mg/kg dry
137.1 2330 100
80-120 12 20
Batch P8B0287 - NO PREP
Blank(P8B0287-BLK1) Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P860287-13SI) Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N 47.6 5.0 mg/kg wet 50.00 95 80-120
Matrix Spike (P8B0287-MS1) Source:8020215-01 Prepared: 02/15/18 Analyzed: 02/16/18
t litrite as N 87.4 6.9 mg/kg dry 68.57 21.2 97 80-120
I . . ';pike Dup (P8B0287-MSD1) Source: 8020215-01 Prepared: 02/15/18 Analyzed: 02/16/18
Nitrate/Nitrite as N 86.1 6.9 mg/kg dry 68.57 21.2 95 80-120 1 20
Batch P8B0321 - 351.2
Blank (P8130321-13LK1) Prepared: 02/16/18 Analyzed: 02/19/18
Total Kleldahl Nitrogen BRL 25 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 10

Vni� (1� 1n\//�, Full -Service Analytical &
R I V 1 �9 , I Environmental Solutions
�Y LABORATORIES, INC.
Level Il QC Report
2/20/18
City of Statesville, NC Project: StaLime
/ -" ,,idy Smith
F"IX 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8020215
Time Submitted: 2/12/2018 3:35:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8BO321 - 351.2
LCS (P8B0321-BSI) Prepared: 02/16/18 Analyzed: 02/19/18
Total Kjeldahl Nitrogen 513 100 mg/kg wet 500.0 103 90-110
Batch P8BO325 - SM4500-NH3 B
Blank (P8B0325-BLKI) Prepared &Analyzed: 02/15/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8130325-13SI) Prepared &Analyzed: 02/15/18
Ammonia as N 456 10 mg/kg wet 500.0 91 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 10

Level II QC Report
i y Full -Service Analytical & 2/20118
,PRISM I Environmental Solutions
�50MTONIES, INO.
City of Statesville, NC Project: StaLime Prism Work Order: 8020215
A,�- idy Smith Time Submitted: 2/12/2018 3:35:OOPM
P,i x 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch 138B0282 - NO PREP
Blank (P8B0282-BLK1) Prepared &Analyzed: 02/13/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
8020215-01 P8130321 0.05 g 25 mL 02/16/18 10:15
Prep Method: SM4500-NH3 B
Lab Number Batch Initial Final Date/Time
8020215-01 P8130325 1 g 50 mL 02/15/18 14:30
Prep Method: SM4500-PB5
l nber Batch Initial Final Date/Time
E i-01 P860248 1 g 50 mL 02/14/18 6:30
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
8020215-01 P860256 30 g 30 g 02/13/18 15:11
Prep Method: 3010A
Lab Number Batch Initial Final Date/Time
8020215-01
P860324
50 mL
50 mL
02/16/18 9:00
8020215-01
P860324
50 mL
50 mL
02/16/18 9:00
8020215-01
P860324
50 mL
50 mL
02/16/18 9:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8020215-01
P8130253
2.02 g
50 mL
02/14/18 8:25
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
8020215-01
P8130339
0.59 g
50 mL
02/19/18 9:10
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
15-01
P8130279
250 g
250 g
02/15/18 8:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 10

CUOUDDY RECORD
CHAN`dv..Sai^a'++-5>:bHIM,.::
td�". t s � '"�F�, 0 Z�,° �} � '� a'fib"��'�'•"-''�,,,."�rE`"g
z' S 1,1t s i 1l..m a1.W.1 S'e.efa,z.?°as6
.«
.,
I Environmental solutions I�AeE_ ®ff
RISMFull -Service Analyticali VO ED98URE I ROPER 13IGLLOVIG'.
IN'[y 4tt �rfiv�l?:: "
_
o
i,�T„',�.)w;''!•,i�.',v`;4+' - ':5'+'� LABORA(ORIES. ftdC. P7®�ect Nc�ffPEG�
Project: (Yes) (NO)
71
lot Gi? R P ESk §x3�E r a `ared�
-
449 Springbrook road a Charlotte, NC 28217
Phone 704I529-0364 ^Fax: [phone] Short p 9old Analysis: (Yes) (N®) UST
*Please ATTACK any project specific reporting (QC LEVEL 9 11 111 IV)
�dceiv�cl.WiTHlN.F1OLDING i'IMES7
- - tZ
liewt Company Name: C. �� e � prrovisions and/or QRC Requirements
GU iCJG7.V.SEAL�.IIV'CAC:"f7
�'rec.d DUT','HEADSPAC0
_ — —t1
;Report To/Contact Name: A vfy Invoice go:
VOt fiILE
?-RS use
—
epOPting Address: Address:::..
C)bS;n vcd: 2'
!' M:.. Thyrnr.t:4A :•_
Phone:70`7°079.9`439 Fall: es (No): 70"�'I"���° PuArchase Order Ne./Sillirlg Reference TO BE BILLED IN BY CLIENT/SAMP'LING PERSONNEL
Email Address: Requested Due Date ® 1 Day EI 2 Days 17 3 Days ® 4 Days ® 5 Days Certification: NELAC LIBGD
FL— NC
Rush Be
®® Type: P®F Eggcep ®tllv'P "Working Days" 126-9 Days O Standard 10 days E3Pre -Approved
SIC— OTHER
NIA
Site LOCatiOB>l Narne:°�� dg Q�(� �� Samples received after 14:00 will be processed next business day.
business days, excluding weekends and holidays.
Name:Physic1
Water Chilo iiiatted: YES_ V��)_
p� �y g�
Address: ��� �� d" b 1 ° Turnaround time is based on
Site Location (SEE REVERSE FOR TERMS a CONDITIONS REGARDING RENDERED BY PRISM LABORATORIES, INC. ® CLIENT)SERVBCES Sarnppe Iced Upon Coflecti®PO: YES_
NO_
ANALYSIS REQUESTED
PRISM
TIME MAT RIX SAMPLE CONTAINER PRESERVA-
��� V�EMARG®S LAB
CLIENT DATE COLLECTED (SOIL,.
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR "TYPE TIVES �
NO. SIZE
/Z
ID NO.
HOURS SLUDGE) SEE BELOW
�
PA Goy
C
CM
SA
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pp
7/`Uj 4u
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Sant led E3y {Print Name) 4�oc�0� Aifiiliation
Signafiure e P
tA
Sampler's
relinquishing, this Chain of Custody is your authorization tDr Prison t® proceed with the analyses as requested above. cAny changes must be
Upon reling g�
submitted in dvriting to the Prism Pr®sect Manager. There will be Charge _ `s ny changes after analyses have Green initialized.
litarylHours Additional Comments:
halua:Vf�
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SIti3 ,rf:iv�al Ti*ir
Reli is ad By: (Signet¢ re) w ace! d : (Si
171,
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Site DGpaYtlJre Time::
,,,tvj�, �,
Relin shed By: (Signature) Re eived By: (Signature)
Date
fg Field Tech Fee:
q. { ,
stories B :
`'sm Labor -I
Receive For i Y a
Relinquished By: (Signature) `` �-°' L �
�.: � �� ®.
.
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE APED SH I H STODY SEALS FOR TRANSPORTATION TO TI IE LABORATORY COC Group No.
T
SAMPLES ARE NOT A CEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
._,.._u
O Fed Ex ❑UPS nd-delivered Prism Field Service O Other
®RINKING �19ATER: SOLID WASTE; RC CERCLA LANDFILL
O T VEER:
r� °,"
t ; r���� P � I'� � °� ��:
NPOES: k GROUNDWATER:
DNC Ell SIC L:_- CSC ®NC ©SC ®NC ©SC DNC El SC DN( i; D NC D SC D NC ® SC
D NC D SC
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p= pInQtln• II = rP-'nnn-i lnC-n l.(lu vvM- v�tciu�c v�ua.uw....... v.�. . ,-•- •

%r
J
t'P R-\,,
I S M
14 ABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cart No. 37735 04/04/2018
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 03/26/2018
Prism Work Order: 8030410
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
SAR = [ 175/23 ] / SQRT { ( [2810/20] + [1.2/12.2]) / 2 }
SAR = 0.91
nitrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 17

P
a
Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration > RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
BL MB greater than one half of the RL, but the sample concentrations are less than the RL.
DM Sample diluted and RL increased due to the matrix.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 17

AAA
Environmental I S A '® Service Analytical s
' V' Environmental Solutions
7L BOBATORIES INO.
Sample Receipt Summary
04/04/2018
Prism Work Order: 8030410
C'--` Sample ID
Lab Sample ID
Matrix
Date Sampled
Date Received
.. a (and Fecal 1)
8030410-01
Solid
03/26/18
03/26/18
Fecal #2
8030410-02
Solid
03/26/18
03/26/18
Fecal #3
8030410-03
Solid
03/26/18
03/26/18
Fecal #4
8030410-04
Solid
03/26/18
03/26/18
Fecal #5
8030410-05
Solid
03/26/18
03/26/18
Fecal #6
8030410-06
Solid
`03/26/18
03/26/18
Fecal #7
8030410-07
Solid
03/26/18
03/26/18
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 17

AFull-Service Analytical &
ISM Environmental Solutions
ABORAMRIES, INC.
Laboratory Report
04/04/2018
Cif. , -' Statesville, NC
Project: StaLime (Qtrly, Biweekly,
Client Sample ID:
StaLime (and Fecal 1)
P' idy Smith
60Day
7 Fecal)
Prism Sample ID: 8030410-01
F. .-max 1111
Prism Work Order:
8030410
Statesville, NC 28687
Sample Matrix: Solid
Time
Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateTme
ID
General Chemistry Parameters
Plant Available Nitrogen
1700
mg/kg dry
510
110
5
*Calculation
412/18 14:40
CLB
[CALC]
% Solids
74.6
% by
0.100
0.100
1
*SM2540 G
3/28/18 15:00
BJC
P8D0021
Weight
Ammonia as N
1900
mg/kg dry
13
3.3
1
*SM4500-NH3 C
4/2/18 14:40
BMS
P8D0030
Nitrate/Nitrite as N
BRL
mg/kg dry
6.7
0.74
1
*SM4500-NO3 F
3/29/18 10:29
CLB
P8C0465
Phosphorus -Total
2800
mg/kg dry
67
9.7
20
*SM4500-P F
3129/18 7:07
CLB
P8C0413
Total Kjeldahl Nitrogen
4300
mg/kg dry
1700
360
5
*351.2
412/18 7:44
CLB
P8C0484
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
3/27118 9:48
BMS
P8C0486
Total Metals
Mercury
0:030
mg/kg dry
0.026
0.0025
1
*7471B
3/28/18 14:19
JAB
P8C0466
SAR Soil Preparation
Complete
g
1
*2-78-054
4/4/18 10:11
MMR
P8C0473
SAR Percent Moisture
Complete
%by
0.100
0.100
1
*2-78-054
4/2/18 9:52
MMR
P8D0007
Weight
Arsenic
BRLDM
mg/kg dry
6.7
0.41
10
*6010D
3/29118 16:43
JAB
P8C0462
Absorption Ratio
0.91
[blank]
0.30
0.016
1
*2-78-054
3/29/18 16:06
JAB
P8C0491
( n
BRLDM
mg/kg dry
3.3
0.089
10
*6010D
3/29118 16:43
JAB'
P8C0462
Calcium, SAR
2800 B
mg/L
1.0
0.10
10
*6010D
3129/18 16:06
JAB
P8C0491
Copper
33
mg/kg dry
6.7
0.60
10
*6010D
3/29118 16:43
JAB(
P8C0462
Lead
3.6
mg/kg dry
3.3
0.62
10
*6010D
3/29/18 16:43
JAB
P8C0462
Magnesium, SAR
1.2
mg/L
1.0
0.086
10
*6010D
3/29/18 16:06
JAB
P8C0491
Nickel
6.9
mglkg dry
6.7
0.24
10
*6010D
3/29/18 16:43
JAB
P8C0462
Potassium
2300
mglkg dry
170
6.0
10
*6010D
3/29118 16:43
JAB
P8C0462
Selenium
13
mg/kg dry
6.7
1.6
10
*6010D
3/29118 16:43
JAB
P8C0462
610
mg/kg dry
200
6.5
10
*6010D
3/29118 16:43
JAB
P8C0462
.Sodium
Sodium, SAR
180 B
mg/L
5.0
0.18
10
*6010D
3129/18 16:06
JAB
P8C0491
Zinc
59
mg/kg dry
33
1.2
10
*6010D
3129/18 16:43
JAB
P8C0462
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 17

/Al"
S FullService Analytical Environmental Solutions
�✓LABORATORIE� INC.
Citv of Statesville, NC
PV idy Smith
F Ix 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/04/2018
Client Sample ID: Fecal #2
Prism Sample ID: 8030410-02
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 68.3
% by
0.100
0.100 1
*SM2540 G 3/28/18 15:D0 BJC
P8D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 3/27/18 9:48 BMS
P8C0486
r—
i
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 17

:. Laboratory Report
Full -Service Anal tical & 04/04/2018
=I I S Environmental Solutions
, �LA60RAT0RIEs ING
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, Client Sample ID: Fecal #3
f 'Indy Smith 60Day 7 Fecal) Prism Sample ID: 8030410-03
1111 Prism Work Order: 8030410
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateTme ID
General Chemistry Parameters
% Solids 71.7 % by 0.100 0.100 1 *SM2540 G 3/28118 15:00 BJC P8D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3
1 `SM9221 E 3/27/18 9:48 BMS P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 17

i�RFull -Service Analytical &
'�_:l .l S M Environmental Solutions
LABORATORIES INa
Citv of Statesville, NC
idy Smith
F`'•_,. bx 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/04/2018
Client Sample ID: Fecal #4
Prism Sample ID: 8030410-04
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 75.3
% by
0.100
0.100 1
"SM2540 G 3128118 15:00 BJC
P8D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
`SM9221 E 3/27/18 9:48 BMS
PBC0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 17

InPJ \ Full -Service Analytical &
'-. ',� I Environmental Solutions
��V LABORATORIES INa
Laboratory Report
04/04/2018
City of Statesville, NC
F, ndy Smith
F=�.. F ux 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #5
Prism Sample ID: 8030410-05
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 73.9 % by 0.100 0.100 1 *SM2540 G 3/28/18 15:00 BJC P81D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.3 1 *SM9221 E 3/27/18 9:48 BMS P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 8 of 17

"x
141=11
R ISM Full -Service Analytical &
LABORATOPIE$ ING
r� Environmental Solutions
"�
Laboratory Report
04/04/2018
Citv of Statesville, NC
P idy Smith
F',. -'>x 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #6
Prism Sample ID: 8030410-06
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 72.9
% by
0.100
0.100 1
*SM2540 G 3128118 15:00 BJC
P8D0021
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 3/27/18 9:48 BMS
P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 17

'l
�P Full -Service Analytical &
Environmental Solutions
D-LABORATORIE$ INC.
Citv of Statesville, NC
F" Indy Smith
F
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
04/04/2018
Client Sample ID: Fecal #7
Prism Sample ID: 8030410-07
Prism Work Order: 8030410
Time Collected: 03/26/18 13:40
Time Submitted: 03/26/18 15:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 75.3 % by 0.100 0.100 1 *SM2540 G 3/28/18 15:00 BJC P8130021
Weight
Microbiological Parameters
Fecal Coliforms BRL MPNIg dry 0.3 1 *SM9221 E 3127/18 9:48 BMS P8C0486
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 10 of 17

�P/ 1I i Full -Service Analytical &
I Environmental Solutions
1— =71 ABOBATORIM INC
Level II QC Report
4/4/18
City_ of Statesville, NC
A` vidy Smith
P. 1111
Statesville, NC 28687
Total Metals - Quality Control
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8030410
Time Submitted: 3/26/2018 3:00:OOPM
Reporting
Spike Source
%REC RPD
Analyte
Result
Limit
Units
Level Result %REC
Limits RPD Limit Notes
Batch P8C0462 - 3050B
Blank (P8C0462-BLKI)
Prepared: 03/28/18 Analyzed: 03/29/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
BH
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
2.85
2.5
mg/kg wet
BH
LCS (P8C0462-BS1)
Prepared: 03/28/18 Analyzed: 03/29/18
Arsenic
13.2
0.50
mg/kg wet
12.50 105
80-120
Cadmium
13.5
0.25
mg/kg wet
12.50 108
80-120
Copper
14.2
0.50
mg/kg wet
12.50 114
80-120
Lead
13.6
0.25
mg/kg wet
12.50 109
80-120
Nickel
13.7
0.50
mg/kg wet
12.50 109
80-120
Im
1420
12
mg/kg wet
1250 114
80-120
n
12.0
0.50
mg/kg wet
12.50 96
80-120
1430
15
mg/kg wet
1250 115
80-120
Zinc
13.5
2.5
mg/kg wet
12.50 108
80-120
Batch P8C0466 - 7471 B
Blank (P8C0466-BLK1)
Prepared & Analyzed: 03/28/18
Mercury
BRL
0.020
mg/kg wet
LCS (P8C0466-BSI)
Prepared &Analyzed: 03/28/18
Mercury
0.438
0.020
mg/kg wet
0.4167 105
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 11 of 17

Full -Service Analytical &
I S M I Environmental Solutions
X,�LA ORATORIM INC.
Level II QC Report
4/4/18
City of Statesville, NC Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 8030410
A1,r ,dy Smith 7 Fecal) Time Submitted: 3/26/20.18 3:00:OOPM
Jr 1111
Statesville, NC 28687
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8CO473 - SAR 2-78-054
Blank (P8C0473-BLK1)
Prepared: 03/28/18 Analyzed: 04/04/18
SAR Soil Preparation
Complete
g
Batch P8CO491 - 301 OA
Blank (P8C0491-BLK1)
Prepared &Analyzed: 03/29/18
Sodium Absorption Ratio
BRL
0.30 [blank]
Calcium, SAR
0.386
0.10 mg/L BH
Magnesium, SAR
BRL
0.10 mg/L BL
Sodium, SAR
2.59
0.50 mg/L A
Batch P8D0007 - NO PREP
Duplicate (P8D0007-DUP1) Source: 8030410-01 Prepared &Analyzed: 04/02/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.4 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 17

Level II QC Report
I > > Full -Service Analytical & 4/4/18
�5 I S Environmental solutions
J�L48ORATORIES, INC.
City of Statesville, NC
A'r idy Smith
P' x 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8CO413 - SM4500-PB5
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 8030410
Time Submitted: 3/26/2018 3:00:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Blank (P8C0413-BLK1) Prepared: 03/28/18 Analyzed: 03/29/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8C0413-BSI) Prepared: 03/28/18 Analyzed: 03/29/18
Phosphorus -Total 96.0 2.5 mg/kg wet 100.0 96 90-110
Batch P8CO465 - NO PREP
Blank (P8C0465-BLKI) Prepared: 03/28/18 Analyzed: 03/29/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8C0465-BSI) Prepared: 03/28/18 Analyzed: 03/29/18
Nitrate/Nitrite as N 49.8 5.0 mg/kg wet 50.00 100 80-120
Batch P8C0484 - 351.2
Blank (P8C0484-BLK1) Prepared: 03/29/18 Analyzed: 04/02/18
Total Kjeldahl Nitrogen BRL 25 mg/kg wet
LCS (P8C0484-BS1) Prepared: 03/29/18 Analyzed: 04/02/18
Total Kjeldahl Nitrogen 548 100 mg/kg wet 500.0 110 90-110
Spike (P8C0484-MS2) Source: 8030410-01 Prepared: 03/29/18 Analyzed: 04/02/18
-local m/eldahl Nitrogen 11400 1700 mg/kg dry 6703 4290 106 90-110
Batch P8DO030 - SM4500-NH3 B
Blank (P8D0030-BLK1) Prepared &Analyzed: 04/02/18
Ammonia as N BRL 10 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 17

,�11 Full -Service Analytical &
�p h I Environmental Solutions
Y7LAB0RAT0RIE9, INC.
City of Statesville, NC
A idy Smith
P. Ex 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch MOM - SM4500-NH3 B
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
4/4/18
Prism Work Order: 8030410
Time Submitted: 3/26/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P8D0030-BS1) Prepared &Analyzed: 04/02/18
Ammonia as N 512 10 mg/kg wet 500.0 102 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 0f 17

iP}RR M
Full-Service Analytical &
SEnvironmental Solutions
ORATOR
Level 11 QC Report
4/4/18
City of Statesville, NC
A ' Ay Smith
P. .x 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8030410
Time Submitted: 3/26/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8C0486 - NO PREP
Blank (P8C0486-BLK1) Prepared &Analyzed: 03/27/18
Fecal Coliforms BRL 0.2 MPN/g wet
6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 17

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
801
P8C0484
0.05 g
25 mL
03/29/18 10:10
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8D0030
1.01 g
50 mL
04/02/18 14:02
C
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0413
1 g
50 mL
03/28/18 10:00
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8D0021
30 g
30 g
03/28/18 15:00
8030410-02
PBD0021
30 g
30 g
03/28/18 15:00
8030410-03
P8D0021
30 g
30 g
03/28/18 15:00
8030410-04
P8D0021
30 g
30 g
03/28/18 15:00
8030410-05
P8D0021
30 g
30 g
03/28/18 15:00
8030410-06
P8D0021
30 g
30 g
03/28/18 15:00
8030410-07
P8D0021
30 g
30 g
03/28/18 15:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0491
50 mL
50 mL
03/29/18 2:30
Sn�nn,�n_01
P8C0491
50 mL
50 mL
03/29/18 2:30
F thod:3050B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0462
2.01 g
50 mL
03/28/18 8:45
8030410-01
P8C0462
2.01 g
50 mL
03/28/18 8:45
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0466
0.61 g
50 mL
03/28/18 11:20
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8030410-01
P8C0473
250 g
250 g
03/28/18 14:14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 16 of 17

°
C AON OF CUSTODY RECORD _
°{ a Full -Service Analytical &
Environmental Solutions PAGE_ QUOTE# TO ENSURE PROPER BILLING: YES NO
S M Samples INTACT upon arrival?
NIA r,
T
=='raaorwToales INC. Received ON WET ICE?
Project Name:
r
449 Springbroolt Road - Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) PROPER PRESERVATIVES indicated?
Phone [phone] • Fax: [phone] Received WITHIN HOLDING TIMES?
r 'Please ATTACH any project specific reporting (QC LEVEL I II III IV)_
�+�d S•�A��sy+���
�
Client Company Name: A-P provisions and/or QC Requirements CUSTODY SEALS INTACT?
0-
�
Report To/Contact Name: A m A�5�1 i-Fh Invoice To: VOLATILES rec d WIOUT HEADSPACE7
Reporting Address: Address: PROPER CONTAINERS used? L
TEMP: Thenn'I0:1 rLP'i Observed: °C / Corr
Z 10,
Phone:7®Y• 97t-M& Fax es (No): 70+ $7 t• purchase Order No./Billing Reference TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day Cl 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Pr h Work dust Be ScpprovOTHER NIA
Site Location Name: JC00944 Cf ee-x- _ e� Samples received, alter 14:00 will be processed next bilsiness:day_
Site Location Physical Address: 693 Ef'i t'!7 RM [i Turnaround time is based on business days, excluding -weekends and holidays. Water Chlorinated: YES` NO_
SERVICES
(SEE REVERSE FOR TERMS ai CONDITIONS REGARDING
$lUpon Collection: YES_ NO_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ame Icedp
ANALYSIS REQUESTED
TIME MATRIX SAMPLE CONTAINER / /
PRESERVA- f Q /r �? f /
PRISM
LAB
CLIENT DATE COLLECTED (SOIL, /
Q / F�' REMARKS
SAMPLE DESCRIPTION COLLECTED AAILITARY WATER OR 'TYPE NO. SIZE TIVES/l / /
ID NO.
HOURS SLUDGE) SEE BELOW// ! 1
1`9fdarS,203
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I TA /J I Affiliation
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Sampler's Signature Sampled By (Print Name) /? 104
Upon relinquishing, this -Chain of Custody is your authorization for Prism to proceed ith th analyses as requested above. Any changes must be
°
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Relin ed:By: (Signal ) / / Recutved y,(S gnalure� /� Dpte ,Ma'+aryrryours Additional Comments: Site Arrival Time:
Time:
ReliaWAhed By: (Signature) Ruooivrf Sy: (Signature) D to r Site Departure
Field Tech Fee:
6d ( wature Receh�J For PHsm Lalw atbrre .B : f/.S 1� r Mileage:
R�-L
�Rslin
th ' Ipmenl: OTE: LL SAMP COOLERS.S�HOULD BE TAPED SHUT WITH CUSTODY SEALS FO TRANSPORTATiON T_ THE LABORATORY. oup No:
SAMPLES ARE NOT ACCEPTED AND. VERIFIED AGAINST COC UNTIL RECEIVED AT �E LABORATORY.
fVl :/II ►fit///
O Fed Ex O UPS I- delivered !B FHsm Field Service ❑ Olhur
NPDES: U: GROUNDWATER: DRINNG WATER: SOLID WASTE: RCRA CERCLA LANDFILL OTHER:
. -
❑NC❑SC ❑:`._ _SC ❑NC ❑SC I ❑NCKJ❑SC ONC ❑SC I El NC, ❑❑NC ❑SC I ONC ❑SC ❑❑NC ❑SC
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I
n n I] ■
_ _..__ ...�.- .......� .......-.._ A — A _•...- r+ — rr..... !_— em— P = Plastirr TI = Teflnn-Linea GaD VUH = VOIaUle ve9anu:5 r+uaiyaia I-

..rt
fJ ,
PRISM
�LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No.402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/07/2018
Prism Work Order: 8050101
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
; = [ 120/23.0 ] / SQRT { ( [1500/20.0] + [0.085/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project-Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 20

► IP Ism
�QLABOflATOflIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 05/07/2018
Prism Work Order: 8050101
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
= [ 120/23.0 ] / SQRT { ( [1500/20.01 +'[0.085/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
t�-
RobbiA.Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 20

Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration >1/2 RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
DM Sample diluted and RL increased due to the matrix.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
r
i Relative Percent Difference
_ Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 20

^1 ^ p w Sample Receipt Summary
I Fun -Service Analytical &
Environmental Solutions 02/11/2019
�%AAB_ ORATO_FIEA INC.
Prism Work Order: 8050101
!"i-rit Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
'_ime (and Fecal 1)
8050101-01
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #2
8050101-02
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #3
8050101-03
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #4
8050101-04
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #5
8050101-05
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #6
8050101-06
Solid
05/07/18 13:05
05/07/18 15:00
Fecal #7
8050101-07
Solid
05/07/18 13:05
05/07/18 15:00
Samples were received in good condition at 2.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 20

:, Laboratory Report
h I s Full -Service Analytical &
/ Environmental Solutions 02/11/2019
LABORATORM
Citv of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID:
StaLime (and Fecal 1)
Andy Smith
60Day
7 Fecal)
Prism Sample ID: 8050101-01
Box 1111
Prism Work Order:
8050101
Statesville, NC 28687
Sample Matrix: Solid
Time
Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Plant Available Nitrogen
2000
mglkg dry
470
100
5
*Calculation
5/10118 8:58
CLB
[CALC]
% Solids
81.5
% by
0.100
0.100
1
*SM2540 G
5110118 14:50
TJY
P8E0251
Weight
Ammonia as N
2500
mglkg dry
12
3.1
1
*SM4500-NH3 C
5/8118 14:08
BMS
P8E0162
Nitrate/Nitrite as N
11
mglkg dry
6.1
1.7
1
*SM4500-NO3 F
519/18 9:11
CLB
PBE0174
Phosphorus -Total
3200
mglkg dry
61
8.8
20
*SM4500-P F
6/8118 10:31
CLB
P8E0084
Total Kjeldahl Nitrogen
4800
mglkg dry
1500
330
5
*351.2
5110/18 8:58
CLB
P8E0178
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.2
1
*SM9221 E
5/8/18 9:39
BMS
P8E0184
Total Metals
Mercury
0.24
mglkg dry
0.025
0.0023
1
*7471B
6111/18 15:02
JAB
P8E0248
SAR Soil Preparation
Complete
g
1
*2-78-054
5/9/18 10:25
MMR
P8E0152
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
5/10/18 10:50
MMR
P8E0218
Weight
Arsenic
BRLDM
mg/kg dry
6.1
0.37
10
*6010D
5/9/18 21:46
JAB
P8E0182
- im Absorption Ratio
0.88
[blank]
0.30
0.016
1
*2-78-054
5111/18 14:49
JAB
P8E0188
iium
BRLDM
mg/kg dry
3.1
0.082
10
*6010D
5/9/18 21:46
JAB
P8E0182
Calcium, SAR
1500
mg/L
10
1.0
100
*6010D
5111/18 14:40
JAB
P8E0188
Copper
170 DM
mg/kg dry
6.1
0.55
10
*6010D
5/9118 17:42
JAB
P8E0182
Lead
5.1 DM
mg/kg dry
3.1
0.57
10
*6010D
5/9118 21:46
JAB
P8E0182
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
5/11/18 14:49
JAB
P8E0188
Nickel
10 DM
mglkgdry
6.1
0.22
10
*6010D
5/9/18 21:46
JAB
P8E0182
Potassium
2500 DM
mglkg dry
150
5.5
10
*6010D
5/11/18 15:31
JAB
P8E0182
Selenium
BRLDM
mg/kg dry
6.1
1.5
10
*6010D
5/9/18 17:42
JAB
P8E0182
Sodium
3800 DM
mglkg dry
180
6.0
10
*6010D
5/9118 17:42
JAB
P8E0182
Sodium, SAR
120 B
mg/L
5.0
0.18
10
*6010D
519/18 17:42
JAB
P8E0188
Zinc
76 DM
mg/kg dry
31
1.1
10
*6010D
5/9118 21:46
JAB
P8E0182
( �I
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 20

Laboratory Report
js Fun -Service Analytical &
Environmental Solutions
02/11/2019
ORATORIES, ING
City of Statesville, NC
Project: Stal-ime (Qtrly, BiWeekly,
Client Sample ID: Fecal #2
Andy Smith
60Day 7 Fecal)
Prism Sample ID: 8050101-02
Box 1111
Prism Work Order: 8050101
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 91.2
% by
0.100 0.100
1 *SM2540 G 6/10118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 5 of 20

aP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #3
Prism Sample ID: 8050101-03
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 89.6
% by
0.100
0.100 1
'SM2540 G 5/10/18 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 6 of 20

IAFull-Service Analytical &
RBI,
I S Environmental Solutions
�ABORATORIE$ INC.
City of Statesville, NC
Andy Smith
Box1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #4
Prism Sample ID: 8050101-04
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 89.1
% by
0.100
0.100 1
*SM2540 G 5110118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
`SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 20

Fuli-Service Analytical &
r� , 1 S M Environmental Solutions
--1 LABOBATCHIES, ING
Laboratory Report
02111 /2019
City of Statesville, NC
Andy Smith
_`. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #5
Prism Sample ID: 8050101-05
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 88.1
% by
0.100
0.100 1
'SM2540 G 5110118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1
'SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 20

i
r4 Full -Service Analytical &
S Environmental Solutions
LABORATORIES, ING
Laboratory Report
02/11 /2019
City of Statesville, NC
Andy Smith
__. Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: Fecal #6
Prism Sample ID: 8050101-06
Prism Work Order: 8050101
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 72.2
% by
0.100
0.100 1
*SM2540 G 5110118 14:50 TJY
P8E0251
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 5/8/18 9:39 BMS
P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 77777-1
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 20

!, Full -Service Analytical &
P' ism Environmental Solutions
4✓LABORATORIE$ ING
Laboratory Report
02/11 /2019
City of Statesville, NC
Project: StaLime (Qtrly, BiWeekly,
Client Sample ID: Fecal #7
ur Andy Smith
60Day 7 Fecal)
Prism Sample ID: 8050101-07
). Box 1111
Prism Work Order: 8050101
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 05/07/18 13:05
Time Submitted: 05/07/18 15:00
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Daterflme ID
General Chemistry Parameters
% Solids
85.9 % by
0.100 0.100
1 *SM2540 G 6/10/18 14:50 TJY P8E0251
Weight
Microbiological Parameters
Fecal Coliforms
BRL MPN/g dry
0.2
1 *SM9221 E 518/18 9:39 BMS P8E0184
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 20

, Level II QC Report
I'A
iFull-Service Analytical & 2/11/19
I � Environmental Solutions
�TRATORIES INC.
City of Statesville, NC
Andy Smith
_ "(3ox 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Batch P8E0152 - SAR 2-78-054
Blank (P8E0152-BLK1) Prepared: 05/08/18 Analyzed: 05/09/18
SAR Soil Preparation Complete g
Batch P8EO182 - 3050B
Blank (PBE0182-BLK1)
Prepared &Analyzed: 05/09/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
BH
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8E0182-BS1)
Prepared &Analyzed: 05/09/18
Arsenic
12.2
0.50
mg/kg wet
12.50 98
80-120
ium
12.5
0.25
mg/kg wet
12.50 100
80-120
r
13.1
0.50
mg/kg wet
12.50 105
80-120
Leao
12.4
0.25
mg/kg wet
12.50 99
80-120
Nickel
12.6
0.50
mg/kg wet
12.50 100
80-120
Potassium
1310
12
mg/kg wet
1250 105
80-120
Selenium
11.6
0.50
mg/kg wet
12.50 93
80-120
Sodium
1230
15
mg/kg wet
1250 98
80-120
Zinc
12.4
2.5
mg/kg wet
12.50 99
80-120
Matrix Spike (P8E0182-MS1)
Source: 8050101-01
Prepared &Analyzed: 05/09/18
Arsenic
20.7
6.1
mg/kg dry
15.35 4.93 103
75-125
Cadmium
15.2
3.1
mg/kg dry
15.34 0.476 96
75-125
Copper
59.5
6.1
mg/kg dry
15.35 166 NR
75-125
M
Lead
20.2
3.1
mg/kg dry
15.35 5.12 99
75-125
Nickel
25.3
6.1
mg/kg dry
15.35 10.4 97
75-125
Potassium
4240
150
mg/kg dry
1534 - 2500 113
75-125
Selenium
24.4
6.1
mg/kg dry
15.34 BRL 159
75-125
M
Sodium
2600
180
mg/kg dry
1534 3780 NR
75-125
M
Zinc
89.1
31
mg/kg dry
15.35 75.8 87
75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 20

Full -Service Analytical &
Environmental Solutions
LABORATORIES, I=
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
3Ox1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8EO182 - 3050B
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Matrix Spike Dup (P8E0182-MSD1)
Source: 8050101-01
Prepared &Analyzed: 05/09/18
Arsenic
21.2
6.1
mg/kg dry
15.35
4.93
106
75-125
3
20
Cadmium
15.5
3.1
mg/kg dry
15.34
0.476
98
75-125
1
20
Copper
59.9
6.1
mg/kg dry
15.35
166
NR
75-125
0.7
20 M
Lead
20.4
3.1
mglkg dry
15.35
5.12
100
75-125
0.8
20
Nickel
25.6
6.1
mg/kg dry
15.35
10.4
99
75-125
1
20
Potassium
3900
150
mg/kg dry
1534
2500
91
75-125
8
20
Selenium
24.2
6.1
mg/kg dry
15.34
BRL
158
75-125
0.8
20 M
Sodium
2660
180
mg/kg dry
1534
3780
NR
75-125
2
20 M
Zinc
90.0
31
mg/kg dry
15.35
75.8
92
75-125
1
20
Batch P8E0188 - 301 OA
Blank (P8E0188-BLK1) Prepared &Analyzed: 05/09/18
Calcium, SAR BRL 0.10 mg/L BH
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 4.05 0.50 mg/L A
-- b P8EO218 - NO PREP
'Icate (P8E0218-DUP1) Source: 8050101-01 Prepared &Analyzed: 05/10/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 3 200
Batch P8E0248 - 7471B
Blank (P8E0248-13LK1) Prepared &Analyzed: 05/11/18
Mercury BRL 0.020 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 20

P^R Full -Service Analytical &
�k.RJ� 1l I Environmental Solutions
-"LA00RATORIES, INC
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch MOM - 7471 B
LCS (P8E0248-BSI) Prepared &Analyzed: 05/11/18
Mercury 0.397 0.020 mg/kg wet 0.4167 95 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 13 of 20

Level II QC Report
Full -Service Analytical & 2/11/19
n
;�P R I S Environmental Solutions
�/'LABOR TORIES INC.
City of Statesville, NC
�'- Andy Smith
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: Stal-ime (Qtrly, BiWeekly, 60Day
7 Fecal)
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
Analyte
Result
Reporting
Limit
Units
Spike Source
Level Result %REC
%REC RPD
Limits RPD Limit Notes
Batch MOM - SM4500-PBS
Blank (PBE0084-BLK1)
Prepared & Analyzed: 05/08/18
Phosphorus -Total
LCS (P8E0084-BS1)
BRL
2.5
mg/kg wet
Prepared &Analyzed: 05/08/18
Phosphorus -Total
Batch P8EO162 - SM4500-NH3 B
103
2.5
mg/kg wet
100.0 103
90-110
Blank (P8E0162-BLK1)
Prepared: 05/07/18 Analyzed: 05/08/18
Ammonia as N
LCS (P8E0162-1331)
BRL
10
mg/kg wet
Prepared: 05/07/18 Analyzed: 05/08/18
Ammonia as N
Batch P8EO174 - NO PREP
482
10
mg/kg wet
500.0 96
80-120
Blank (P8E0174-BLK1)
Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N
LCS (P8E0174-BS1)
BRL
5.0
mg/kg wet
Prepared &Analyzed: 05/09/18
Nitrate/Nitrite as N
x Spike (P8E0174-MS1)
51.3
5.0 mg/kg wet
Source: 8050101-01
50.00 103
Prepared &Analyzed: 05/09/18
80-120
Nitrate/Nitrite as N
Matrix Spike Dup (P8E0174-MSD1)
74.4
6.1 mg/kg dry
Source: 8050101-01
61.37 11.4 103
Prepared &Analyzed: 05/09/18
80-120
Nitrate/Nitrite as N
71.9
6.1
mg/kg dry
61.37 11.4 99
80-120 3 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 ,
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 20

A,
hISICI
=LABORATORIES, INC.
Full -Service Analytical &
Environmental Solutions
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
rr Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch MOM - 351.2
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8050101
7 Fecal)- Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8E0178-BLK1)
Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen
LCS (P8E0178-BSI)
BRL 25 mg/kg wet
Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen
Matrix Spike (P8E0178-MS1)
469 100 mg/kg wet
Source: 8050101-01
500.0 94 90-110
Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen
Matrix Spike Dup (P8E0178-MSDI)
10600 1500 mg/kg dry
Source: 8050101-01
6137 4790 95 90-110
Prepared: 05/09/18 Analyzed: 05/10/18
Total Kjeldahl Nitrogen .
Batch P8EO251 - Solids, Dry Weight
11600 1500 mg/kg dry
6137 4790 111 90-110 9 20 M
Duplicate (P8E0251-DUP4)
Source: 8050101-01
Prepared &Analyzed: 05/10/18
% Solids
80.8 0.100 % by Weight 81.5 0.8 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 15 of 20

Axy-1Full-Service Analytical &
IEnvironmental Solutions
A.OR TORTES, ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Batch P8EO184 - NO PREP
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Level II QC Report
2111/19
Prism Work Order: 8050101
Time Submitted: 5/7/2018 3:00:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8E0184-13LK1) Prepared & Analyzed: 05/08/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 20

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
D1-01
P8E0178
0.05
g
25 mL
05/09/18 9:35
Prep Method: SM4500-NI-13 B
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0162
1
g
50 mL
05/08/18 9:00
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8060101-01
P8E0084
1
g
50 mL
05/08/18 6:15
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0251
30
g
30 g
05/10/18 14:50
8050101-02
P8E0251
30
g
30 g
05/10/18 14:50
8050101-03
P8E0251
30
g
30 g
05/10/18 14:50
8050101-04
P8E0251
30
g
30 g
05/10/18 14:50
8050101-05
P8E0251
30
g
30 g
05/10/18 14:50
8050101-06
P8E0251
30
g
30 g
05/10/18 14:50
8050101-07
P8E0251
30
g
30 g
05/10/18 14:50
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
^`^101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
ouou 101-01
P8E0188
50
mL
50 mL
05/09/18 11:10
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8050101-01
P8E0182
2
g
50 mL
05/09/18 8:20
8050101-01
P8E0182
2
g
50 mL
05/09/18 8:20
8050101-01
P8E0182
2
g
50 mL
05/09/18 8:20
Prep Method: 7471E
Lab Number
Batch
Initial
Final
Date/Time
8050101-01 P8E0248 0.6 g 50 mL 05/11/18 12:00
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Date/Time
8050101-01 P8E0152 250 g 250 g 05/08/18 10:25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 20

r ' CHATM OF CUSTODY RECORD
S I Full -Service Analytical &
r IPi" Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
% - 'LA60RATORIES ING
Project Name:
449 Springbrook Road • Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Phone [phone] Fax: [phone]
,� � S�'A�ESV� � /F *Please ATTACH any project specific reporting (QC LEVEL I II III IV)
Client Company Name: , . 5 o' l provisions and/or QC Requirements
Report To/Contact Name: A N Invoice To:
Reporting Address: Address:
YES NO N/A
N
Samples INTACT upon arrival? O
Received ON WET ICE? 00
PROPER PRESERVATIVES indicated? �" r
Received WITHIN.HOLDINGTIMES? '' 0
CUSTODY SEALS INTACT? 11
VOLAT.ILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm ID f Observed:, 67,c Carr Z:c)'C
Phone: 70' - 978• 31q3 8 Fa Ye (No): 7®J% 1179• k119£:f purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush WorkMust Be SC OTHER N/A
Site Location Name: Food h C'g,-FASamples received after 14:00 will be processed next business day.
Site Location Physical Address: 69 aP�+9 f. Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES $am le Iced Upon COIIeCtIOn' YE _:�(NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) P p —
ANALYSIS REQUESTED IL
TIME MATRIX SAMPLE CONTAINER i
DATE COLLECTED (SOIL, PRESERVA- f' y/ f %r REMARKS
PRISM
LAB
CLIENT
fID
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIZE TIVES Ae/
NO,
HOURS SLUDGE) SEE BELOW / � ,� i
9fA
7-J
gs10
a;w 4' 4'
01
.
If
As
AR&V 4
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ce
41-1-
S�i r
10 D q o-i / CIa
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P�
AIA
5
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Pbosp
0 7
Sr-
PAW
z"
SA
,o
`Sampled Affiliation
e.
Sampler's Signature 44e, WOZ By (Print Name) aQ (eL/ 6Q00
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
a
submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized.
Ra-pn9visha _y:.(Signat ). ReOe at! By: (Signature Date Mililarylyours Additional Comments: Site Arrival Time:
Rol' hed.By: (Sigrin ed y: (Signature) , Date Site Departure Time:
f
Field Tech Fee:
Relinq s By. (Signatur Received For Prism Labofeiar B t u CDate
r
C'✓ Y�� mil- !t��. J-%Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FORT N5PORTATION TQ THE LABORATORY. COC,Group No_
VERIFIED AGAINST COC UNTIL RECEIVED ATTHE LABORATORY.
SAMPLES ARE NOTA EPTED AND // c
(nJ�►}�)J0 I oil
❑ Fed Fit ❑ UPS ❑ n m Hand -delivered Field Service ❑ Othor
NPDES: U; GR U DWATER: DRINKING WATER: SOLID WASTE: RCRP • CERCLA LANDFILL OTHER:
❑ NC ❑ SC ❑. ;] Sc ❑ ❑ SC ❑ NC ❑ Sc ❑ NC .O Sc I ❑❑ NC ; I Ll NC ❑ SC I ❑❑ NC ❑ SC 0 NC ❑ SC
1C
❑ ❑ ❑ ❑ ❑ - •- • . • -

f ISM I Full 9®ryiro Analytical and
Enviroiuhentl Solutions
mr-
Plant Available Nitrogen
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: 704/52M364
1/8001529-6364
Fax: [phone]
www.prismlabs.com
Sample Numberl 8050101-01 1 Sample Namel Stal-ime
Mineralization
Rate TKN NH3 NOX
MAIL mg/L mm- /L
0.3 4791 2522 11.3
PAN Surface
2,000 mglkg
MR(TKN-NH3)+ 0.5(NH3)+NOX = PAN mg/kg
Calculated By:
Page 19 of 20

Main Office:
449 Springbrook Road
A';
!, i Full Sarvici� Analytical and
M Environtttonial Solutions
P.O. Box 240543
Charlotte, NC 28224-0543
, iP,R
=�;' �LWOBATOfIIE, t:a
Phone: [phone]
1/800/529-6364
Fax: [phone]
www.prismiabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 8050101-01 Sample Name Sta-Lime
Nam /L . CG m /L MgLm /L
Na: Sodium (mg/L) Equivalent weight: 23 123 1480 1 0.085
Ca: Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12 Na (ME) Ca (ME) M4 (ME)
5.35 74 0.01
Milli Equivalent (ME) = mg/L / Equivalent weight
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.88 (From mg/L entered above)
Calculated By: d-�
Page 20 of 20

p-_01
R1SM
!I/lABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime
Lab Submittal Date: 05/22/2018
Prism Work Order: 8050384
Case Narrative
02/11 /2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the first revised report dated 01/29/19. The SAR comment has been added
below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
`; = [ 100/23.0 ] / SQRT { ( [1500120.01 + [0.089/12.21) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 13

Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration >1/2 RL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1 Ox the MB.
MI Matrix spike outside of the control limits. Matrix interference suspected.
BRL Below Reporting Limit
MDL Method Detection Limit
oor) Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 13

Sample Receipt Summary
,'�*#-Ri
Full-Service Analytical $"'II S 1 d 1 Environmental solutions 02/11/2019
— ,bIW_ B_ ORATORIES INC
Prism Work Order: 8050384
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
%ime 8050384-01 Solid 05/22/18 12:06 05/22/18 13:26
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 13

r,P Full -Service Analytical &
�P Ism Environmental Solutions
'✓LABORATORIES, INC.
Laboratory Report
02/11 /2019
City of Statesville, NC Project: StaLime Client Sample ID: StaLime
Andy Smith Prism Sample ID: 8050384-01
Box 1111 Prism Work Order: 8050384
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 05/22/18 12:06
Time Submitted: 05/22/18 13:26
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
2100
mglkg dry
460
98
5
*Calculation 6/6/18 8:01
CLB
[CALC]
% Solids
83.7
% by
0.100
0.100
1
*SM2540 G 5/25118 15:55
TJY
P8E0562
Weight
Ammonia as N
1700
mg/kg dry
12
3.0
1
*SM4500-NH3 C 5124/18 14:30
BMS
P8E0518
Nitrate/Nitrite as N
BRL
mg/kg dry
6.0
1.6
1
*SM4500-NO3 F 5/25/18 8:20
CLB
P8E0497
Phosphorus -Total
3000
mg/kg dry
60
8.6
20
*SM4500-P F 5124118 8:31
CLB
P8E0432
Total Kjeldahl Nitrogen
5800
mg/kg dry
1500
320
5
*351.2 6/6/18 8:01
CLB
P8E0557
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
- 0.2
1
*SM9221 E 5/23/18 9:23
BMS
P8E0517
Total Metals
Mercury
0.17
mg/kg dry
0.024
0.0023
1
*7471B
5/30118 14:22
JAB
P8E0575
SAR Soil Preparation
Complete
g
1
*2-78-054
5125/18 14:25
MMR
P8E0482
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
5/25/18 14:25
MMR
P8E0537
Weight
Arsenic
BRL
mg/kg dry
5.9
0.36
10
*6010D
6/5/18 13:20
JAB
P8E0492
Q-1himAbsorption Ratio
0.71
[blank]
0.30
0.016
1
*2-78-054
5125/18 4:50
PJF
P8E0502
ium
BRL
mg/kg dry
3.0
0.080
10
*6010D
6/5/18 13:20
JAB
P8E0492
Calcium, SAR
1500 B
mg/L
1.0
0.10
10
*6010D
6/25118 4:50
PJF
P8E0502
Copper
34 BH
mg/kg dry
5.9
0.54
10
*6010D
616118 13:20
JAB
P8E0492
Lead
4.1
mglkg dry
3.0
0.55
10
*6010D
5129118 14:07
JAB
P8E0492
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
5125/18 4:58
PJF
P8E0502
Nickel
8.6
mg/kg dry
5.9
0.21
10
*6010D
5/29113 14:07
JAB
P8E0492
Potassium
2100
mg/kg dry
150
5.4
10
*6010D
615118 13:20
JAB
P8E0492
Selenium
18
mglkg dry
5.9
1.4
10
*6010D
5129/18 14:07
JAB
P8E0492
Sodium
590 BH
mg/kg dry
180
5.8
10
*6010D
5/29/18 14:07
JAB
P8E0492
Sodium, SAR
100 B
mg/L
5.0
0.18
10
*6010D
5125118 4:50
PJF
P8E0502
Zinc
61
mg/kg dry
30
1.1
10
*6010D
615118 13:20
JAB
P8E0492
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 13

.� Full -Service Analytical &
/6'�'�Ji
I S Environmental Solutions
�LABORATORIES, INC.
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime
Reporting
Result Limit Units
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P8EO482 - SAR 2-78-054
Blank (P8E0482-BLK1) Prepared: 05/23/18 Analyzed: 05/25/18
SAR Soil Preparation Complete g
Batch P8EO492 - 3050B
Blank (P8E0492-131LKI)
Prepared: 05/24/18 Analyzed: 05/25/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
0.601
0.50
mg/kg wet
BH
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mglkg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
BH
Zinc
BRL
2.5
mg/kg wet
LCS (P8E0492-13SI)
Prepared: 05/24/18 Analyzed: 05/25/18
Arsenic
12.2
0.50
mg/kg wet
12.50 97 80-120
Cadmium
12.4
0.25
mg/kg wet
12.50 99 80-120
Br
13.7
0.50
mg/kg wet
12.50 110 80-120
12.5
0.25
mg/kg wet
12.50 100 80-120
Nickel
12.6
0.50
mg/kg wet
12.50 101 80-120
Potassium
1270
12
mg/kg wet
1250 102 80-120
Selenium
11.5
0.50
mg/kg wet
12.50 92 80-120
Sodium
1230
15
mg/kg wet
1250 98 80-120
Zinc
12.4
2.5
mg/kg wet
12.50 99 80-120
Matrix Spike(P8E0492-MS1)
Source:8050384-01
Prepared: 05/24/18 Analyzed:05/29118
Arsenic
19.9
6.0
mg/kg dry
14.94 3.89 107 75-125
Cadmium
15.5
3.0
mg/kg dry
14.94 0.272 102 75-125
Copper
48.7
6.0
mg/kg dry
14.94 33.9 99 75-125
Lead
19.6
3.0
mg/kg dry
14.94 4.15 103 75-125
Nickel
23.3
6.0
mg/kg dry
14.94 8.63 98 75-125
Potassium
3750
150
mglkg dry
1494 2150 107 75-125
Selenium
32.2
6.0
mg/kg dry
14.93 18.5 92 75-125
Sodium
2100
180
mg/kg dry
1494 592 101 75-125
Zinc
73.0
30
mg/kg dry
14.94 61.1 80 75-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 13

Full -Service Analytical &
I Environmental Solutions
✓LABORATORIES, ING
Level II QC Report
2111/19
City of Statesville, NC
" Andy Smith
-Box 1111
5 atesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8E0492 - 3050B
Project: StaLime
Reporting
Result Limit Units
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P8E0492-MSD1)
Source: 8050384-01
Prepared: 05/24/18 Analyzed: 05/29/18
Arsenic
21.3
6.0
mg/kg dry
14.94
3.89
116
75-125
7
20
Cadmium
15.4
3.0
mg/kg dry
14.94
0.272
101
75-125
0.2
20
Copper
50.2
6.0
mg/kg dry
14.94
33.9
109
75-125
3
20
Lead
19.2
3.0
mg/kg dry
14.94
4.15
101
75-125
2
20
Nickel
23.5
6.0
mg/kg dry
14.94
8.63
99
75-125
0.6
20
Potassium
3820
150
mg/kg dry
1494
2150
112
75-125
2
20 t
Selenium
34.7
6.0
mg/kg dry
14.93
18.5
109
75-125
7
20
Sodium
2130
180
mg/kg dry
1494
592
103
75-125
2
20
Zinc
75.2
30
mg/kg dry
14.94
61.1
94
75-125
3
20
Batch P8EO502 - 3010A
Blank (P8E0502-BLK1) Prepared: 05/24/18 Analyzed: 05/25/18
Sodium Absorption Ratio BRL 0.30 [blank]
Calcium, SAR 1.00 0.10 mg/L BH
Magnesium, SAR BRL 0.10 mg/L A
Sodium, SAR 3.43 0.50 mg/L BH
h P8EO537 - NO PREP
Duplicate (P8E0537-DUP1) Source: 8050384-01 Prepared &Analyzed: 05/25/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.7 200
Batch P8EO575 - 7471 B
Blank (P8E0575-BLK1) Prepared &Analyzed: 05/30/18
Mercury BRL 0.020 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 13

tl.
IsFull-Service Analytical &
Environmental Solutions
��- ��L O8 TORIES, [Na
Level II QC Report
2/11/19
City of Statesville, NC Project: Stal-ime
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8EO575 - 7471 B
LCS (P8E0575-BS1) Prepared &Analyzed: 05/30/18
Mercury 0.387 0.020 mg/kg wet 0.4167 93 80-120
II
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 7 of 13

Level II QC Report
t .� Full -Service Analytical & 2/11/19
IS Environmental Solutions
��ORATORIES INC
City of Statesville, NC
"Andy Smith
)Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Project: StaLime
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8E0432 - SM4500-PB5
Blank (P8E0432-BLK1) Prepared: 05/23/18 Analyzed: 05/24/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (P8E0432-BSI) Prepared: 05/23/18 Analyzed: 05/24/18
Phosphorus -Total 103 2.5 mg/kg wet 100.0 103 90-110
Batch P8E0497 - NO PREP
Blank (PBE0497-BLK1) . Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N BRL 5.0 mg/kg wet
LCS (P8E0497-BS1) Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N 51.0 5.0 mg/kg wet 50.00 102 80-120
Matrix Spike (P8E0497-MSI) Source: 8050384-01 Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N 65.6 6.0 mg/kg dry 59.75 2.81 105 80-120
Matrix Spike Dup (P8E0497-MSD1) Source: 8050384-01 Prepared: 05/24/18 Analyzed: 05/25/18
Nitrate/Nitrite as N 62.8 6.0 mg/kg dry 59.75 2.81 100 80-120 4 20
Batch P8E0518 - SM4500-NH3 B
k (P8E0518-BLK1) Prepared &Analyzed: 05/24/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8E0518-BS1) Prepared &Analyzed: 05/24/18
Ammonia as N 487 10 mg/kg wet 500.0 97 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 13

/-roz/
> > Full -Service Analytical &
P I Environmental Solutions
17LASORATORIE3, INC.
Level II QC Report
2/11/19
City of Statesville, NC Project: Stal-ime
Andy Smith
3ox 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Analyte
Reporting
Result Limit
Units
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P8EO557 - 351.2
Blank (P8E0557-BLK1)
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
LCS (P8E0557-13SI)
BRL 25
mg/kg wet
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
Matrix Spike (P8E0557-MS1)
537 100 mg/kg wet
Source: 8050384-01
500.0 107 90-110
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
Matrix Spike Dup (P8E0557-MSD1)
11400 1500 mg/kg dry
Source: 8050384-01
5975 5840 92 90-110
Prepared: 05/29/18 Analyzed: 06/06/18
Total Kjeldahl Nitrogen
10700 1500
mg/kg dry
5975 5840 81 90-110 6 20 MI
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 13

> > Full -Service Analytical &
/e"_AM7LAB0RAT0R1Es,
IEnvironmental Solutions
ING
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime
Level II QC Report
2/11/19
Prism Work Order: 8050384
Time Submitted: 5/22/2018 1:26:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8E0517 - NO PREP
Blank (P8E0517-BLK1) Prepared &Analyzed: 05/23/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: 351.2
Lab Number Batch Initial Final Date/Time
8050384-01 P8E0557
0.05 g
25 mL
05/29/18 10:30
Prep Method: SM4500-NH3 B
Lab Number Batch
Initial
Final
Date/Time
8050384-01 P8E0518
1 g
50 mL
05/24/18 14:30
Prep Method: SM4500-PB5
-lumber Batch
Initial
Final
Date/Time
384-01 P8E0432 1 g 50 mL 05/23/18 10:45
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
8050384-01 P8E0562 30 g 30 g 05/25/18 15:55
Prep Method: 3010A
Lab Number Batch Initial Final Date/Time
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
8050384-01
P8E0502
50 mL
50 mL
05/24/18 14:15
Prep Method: 3050E
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
8050384-01
P8E0492
2.01 g
50 mL
05/24/18 8:20
Prep Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8050384-01
P8E0575
0.6 g
50 mL
05/30/18 9:45
Prep Method: SAR 2-78-054
( Number
Batch
Initial
Final
Date/Time
8050384-01 P8E0482 250 g 250 g 05/23/18 13:55
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 13

-Fu u ®M
�P��, I Full -Service Analytical &
Environmental Solutions PAGE_ OF QUOTE # TO ENSI TOPER BILLING:
NO NIA
_
q•a Samples INTACT upon arrival?
,�,:,,,~__'�y'•�' LABORATORIES ING
Project Name:, _Received ON WET ICE?
_ - - -
449 Springbrook Road • Charlotte, NC 28217 Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO) PROPER PRESERVATIVES indicated?
„
Phone 704I529.6364 • Fax: 704I525-0409 v Received WITHIN HOLDING TIMES?
p A V � �.�,� � J/�. Please ATTACH any project specific reporting (QC LEVEL I II III I!�
C
_
�
Client Company Name: r V D 7 CUSTODY SEALS INTACT?
provisions and/or QC Requirements
Report To/Contact Name: ANC v S n l H Invoice To: VOLATILES reed W/OUT HEADSPACE?
--
Reporting Address' Address: PROPER CONTAINERS used?
TEMP: Thenn,lb., Observed: _ -C I,Crarr "C
Phone: 70q • 97 T, 3 YJ 3 Fax es (No): 7r7,1• Is 78- 9455 Purchase Order No.fBilling Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD
FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
ue h Worvedk Must Be SC OTHER
NIA
Site Location Name: kaiT2A CR EE A Samples received after 14:00 will be processed next business day.
Site Location Physical Address' ii Q_3 lc /i FAR,,,� Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Upon Collection: YES
e Icedp
NO_
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
ANALYSIS REQUESTED
TIME MATRIX SAMPLE CONTAINER
CLIENT DATE COLLECTED (SOIL, PRESERVA- REMARKS
*TYPE /�/%
//Z
PRISM
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR 7
NO. SIZETIMES
�e�/
ID NO.
HOURS SLUDGE) SEE BELOW f f
WA - ,'tWLr
1 U
�� �g 0 E9
P1D. ®-3
I
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OI
A 5
2—
CM
N
i
SC
I
U O e e
Sampler's Signature � Sampled By (Print Name)' R�(.1 Affiliation
o •,
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be chargeAfor any changes after analyses have been initialized.
Re In shed By: (Signature) Receiv . B : {Slgriatur ��' Date IlRary/Huu(s Additional Comments:
;Site Arrival Time:
Rau had By: (Signature) Re6B y: (Sipature) D e
Site Departure Time:
141
Field Tech Fee:
Racily/gd r or Prism boraioria5 By: �j
�IW
Mileage:
rQ od of pment: NOTE: ALL SAMPLE CUOLhR5 SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY, iCOC GrquP No.
(D SAMPLES ARE NOT 14 CEPTED ANDNERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
f�
d Ex ❑ UPS ❑ Hand -delivered t Prism Field Service ❑ Other
ES: UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
�
w C Sc ❑ NC ❑ SC I ❑ NC ❑ Sc ❑ NC ❑ SC ❑ NC ❑ SC I 0 NC ❑ SIC E'NC ❑ Sc. I ® INC ❑ SC � Ll NG ❑ Sc
I
❑ V ❑ ❑ ❑
L1,TA o.,co �nc .-^nmo. A - A.,..k - r- - rlo r-- r_ — P = Plastic• TI = Tiflnn-I inPr1 Can V0A = Volatile Organics Analvsis (Zero Head Space)

!( I Full Service Analytical and
RRIISM Environmental Solutions
Sodium Absorption Ratio
Main Office:
449 Springbrook Road
P.O. Box 240543
Charlotte, NC 28224-0543
Phone: [phone]
1/8001529-6364
Fax: [phone]
www.prismlabs.com
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Numberl 8050384-01 Sample Name StaLime
Na: Sodium (mg/L) Equivalent weight: 23
Ca: Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L• Cam /L M m /L
100 1500 0.089
Na (ME)
Ca ME
Mg (MEA
4.35
75
0,01
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 0.71 (From mg/L entered above)
nn /7
Calculated By:
Page o

Main Office:
RRI\ /j I Full tio.alcn Analyllopl and 449 5pringbrook Road
I �/ I Envlrolumwnlal Solutions P.O. Box 240543
:.:."�_'1"'. `i/I�c,�:x •.:;t:4 l•.� Charlotte, NC 28224.0543
Phone: [phone]
1/800/529.6364
Fax: [phone]
www,prlsmlabs.com
Plaint Available Nitrogen
Sample Numberl 8050384701 1 Sample Namel Stal_ime
Mineralization
Rate TKN NH3 NOX
mg/L ma/L mcl%L
0.3 5800 1700 2.8
PAN Surface
2,083 me /kg
MR(TKN-NH3)+ 0.5(NH3)+NOX = PAN mg/kg
Calculated By:
Page 13 of 13

/P iISM
LABORATORIES, INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 02/11/2019
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, BiWeekly, 60Day 7 Fecal)
Lab Submittal Date: 09/10/2018
Prism Work Order: 8090114
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report dated 01/29/19. The SAR comment has been
added below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
_ [ 130/23.0 ] / SQRT { ( [16000/20.0] + [0/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Fecal Coliform test failed Quality Control and were cancelled by the laboratory.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 1 of 12

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
D RPD value outside of the control limits.
M Matrix spike outside of the control limits.
Mc Sample concentration too high for recovery evaluation.
PS Post Spike recovery is outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 12

Sample Receipt Summary
S M
IEnviservice Analytical $ environmental solutions 02/11/2019
ORATOF
Prism Work Order: 8090114
ant Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
ime (and Fecal 1)
8090114-01
Solid
09/10/18 8:25
09/10/18 13:15
Samples were received in good condition at 2.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 3 of 12

I s m I Fun -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Laboratory Report
02/11 /2019
city of Statesville, NC
Andy Smith
\�.0. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, BiWeekly,
60Day 7 Fecal)
Sample Matrix: Solid
Client Sample ID: StaLime (and Fecal 1)
Prism Sample ID: 8090114-01
Prism Work Order: 8090114
Time Collected: 09/10/18 08:25
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor DateMme ID
General Chemistry Parameters
Plant Available Nitrogen
1900
mg/kg dry
400
86
5
*Calculation
9/17118 8:34
CLB
[CALC]
% Solids
95.1
% by
0.100
0.100
1
*SM2540 G
9114/18 9:45
TJY
P810191
Weight
Ammonia as N
4100
mg/kg dry
10
2.6
1
*SM4500-NH3 C
9/14118 16:00
BMS
P810196
Nitrate/Nitrite as N
110
mg/kg dry
5.3
1.4
1
*SM4500-NO3 F
9/14/18 9:33
CLB
P810183
Phosphorus -Total
2300
mg/kg dry
53
12
20
*SM4500-P F
9113/18 7:23
CLB
P810138
Total Kjeldahl Nitrogen
3400
mg/kg dry
1300
280
5
*351.2
9/17118 8:34
CLB
P810167
Total Metals
Mercury
0.13
mg/kg dry
0.021
0.0020
1
*7471B
9/12118 11:21
MMR
P810134
SAR Soil Preparation
Complete
g
1
*2-78-054
9/12118 13:00
MMR
P810133
SAR Percent Moisture
59.7
% by
0.100
0.100
1
*2-78-054
9/13118 13:15
MMR
P810175
Weight
Arsenic
6.5
mg/kg dry
0.53
0.032
1
*6010D
9/12/18 14:47
JAB
P810136
Sodium Absorption Ratio
BRL
[blank]
2.0
0.016
1
*2-78-054
9/12118 15:54
JAB
P810146
Cadmium
BRL
mg/kg dry
0.26
0.0070
1
*6010D
9/12/18 14:47
JAB
P810136
SAR
16000 B
mg/L
10
1.0
100
*6010D
9/12/18 15:46
JAB
P810146
�r
35
mg/kg dry
0.53
0.048
1
*6010D
9112118 14:47
JAB
P810136
Lead
3.6
mg/kg dry
0.26
0.049
1
*6010D
9/12118 14:47
JAB
P810136
Magnesium, SAR
BRL
mg/L
0.10
0.0086
1
*6010D
9/12/18 15:54
JAB
P810146
Nickel
6.1
mg/kg dry
0.53
0.019
1
*6010D
9112/18 14:47
JAB
P810136
Potassium
1600
mg/kg dry
13
0.47
1
*601013
9/12118 14:47
JAB
P810136
Selenium
BRL
mg/kg dry
0.53
0.12
1
*6010D
9/12118 14:47
JAB
P810136
Sodium
460
mg/kg dry
16
0.52
1
*6010D
9112/18 14:47
JAB
P810136
Sodium, SAR
130 B
mg/L
0.50
0.018
1
*6010D
9/12118 15:54
JAB
P810146
Zinc
34
mg/kg dry
2.6
0.094
1
*6010D
9/12/18 14:47
JAB
P810136
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 12

f
? r, Full -Service Analytical &
p R I S Environmental Solutions
�,7L BOR TORIES. INC.
Level II QC Report
2/11 /19
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810133 - SAR 2-78-054
Blank (P810133-BLK1) Prepared: 09/11/18 Analyzed: 09/12/18
SAR Soil Preparation Complete g
Batch P810134 - 7471 B
Blank (P810134-BLK1) Prepared &Analyzed: 09/12/18
Mercury BRL 0.020 mg/kg wet
LCS (P810134-BS1) Prepared &Analyzed: 09/12/18
Mercury 0.489 0.020 mg/kg wet 0.4167 117 80-120
Batch P810136 - 3050B
Blank (P810136-BLK1)
Prepared &Analyzed: 09/12/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mglkg wet
sium
BRL
12
mg/kg wet
um
BRL
0.50
mg/kg wet
Sodium
BRL
15
mg/kg wet
Zinc
BRL
2.5
mg/kg wet
LCS (P810136-BSI)
Prepared &Analyzed: 09/12/18
Arsenic
12.2
0.50
mg/kg wet
12.50 98
80-120
Cadmium
12.4
0.25
mglkg wet
12.50 99
80-120
Copper
12.9
0.50
mg/kg wet
12.50 103
80-120
Lead
12.3
0.25
mg/kg wet
12.50 99
80-120
Nickel
12.5
0.50
mg/kg wet
12.50 100
80-120
Potassium
1250
12
mg/kg wet
1250 100
80-120
Selenium
12.1
0.50
mglkg wet
12.50 97
80-120
Sodium
1250
15
mg/kg wet
1250 100
80-120
Zinc
11.9
2.5
mg/kg wet
12.50 95
80-120
i
This report should: not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 12

} _ Level II QC Report
I S Full -Service Analytical & 2/11119
Environmental Solutions
�d LABORATORIES INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P810136 - 3050B
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 8090114
Time Submitted: 9/10/2018 1:15:OOPM
%REC RPD
%REC Limits RPD Limit
Notes
Matrix Spike (P810136-MS1)
Source: 8090114-01
Prepared &Analyzed: 09/12/18
Arsenic
19.6
0.53
mg/kg dry
13.15
6.47
100
75-125
Cadmium
9.78
0.26
mglkg dry
13.14
0.211
73
75-125
M
Copper
47.3
0.53
mg/kg dry
13.15
35.1
93
75-125
Lead
13.6
0.26
mglkg dry
13.15
3.59
76
75-125
Nickel
15.9
0.53
mg/kg dry
13.15
6.13
75
75-125
Potassium
3040
13
mg/kg dry
1314
1640
107
75-125
Selenium
14.5
0.53
mg/kg dry
13.14
0.332
108
75-125
Sodium
1770
16
mg/kg dry
1314
456
100
75-125
Zinc
45.1
2.6
mg/kg dry
13.15
33.8
86
75-125
Matrix Spike Dup (P810136-MSD1)
Source: 8090114-01
Prepared &Analyzed:
09/12/18
Arsenic
19.5
0.53
mg/kg dry
13.15
6.47
99
75-125
0.5
20
Cadmium
9.82
0.26
mg/kg dry
13.14
0.211
73
75-125
0.4
20
M
Copper
46.6
0.53
mg/kg dry
13.15
35.1
87
75-125
2
20
Lead
13.3
0.26
mg/kg dry
13.15
3.59
74
75-125
2
20
M
Nickel
16.0
0.53
mg/kg dry
13.15
6.13
75
75-125
0.3
20
Potassium
3010
13
mg/kg dry
1314
1640
104
75-125
1
20
um
15.1
0.53
mg/kg dry
13.14
0.332
112
75-125
4
20
m
1740
16
mg/kg dry
1314
456
98
75-125
2
20
Zinc
45.3
2.6
mg/kg dry
13.15
33.8
88
75-125
0.5
20
Post Spike (P810136-PSI)
Source: 8090114-01
Prepared
& Analyzed:
09/12/18
Arsenic
0.773
mg/L
0.5001
0.246
105
80-120
Cadmium
0.387
mg/L
0.5000
0.00804
76
80-120
PS
Copper
1.88
mg/L
0.5001
1.34
109
80-120
Lead
0.532
mg/L
0.5001
0.137
79
80-120
PS
Nickel
0.624
mg/L
0.5001
0.233
78
80-120
PS
Potassium
117
mg/L
50.00
62.5
110
80-120
Selenium
0.592
mg/L
0.4999
0.0126
116
80-120
Sodium
69.4
mg/L
50.00
17.3
104
80-120
Zinc
1.79
mg/L
0.5001
1.28
102
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 12

Level II QC Report
Jf
r Full -Service Analytical & 2/11/19
Ism
Environmental Solutions
�21�� I
-�VILABORATORIES, INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
P810146 - 301 OA
Project: StaLime (Qtrly, BiWeekly, 60Day
7 Fecal)
Reporting Spike Source
Result Limit Units Level Result
Prism Work Order: 8090114
Time Submitted: 9/10/2018 1:15:OOPM
%REC RPD
%REC Limits RPD Limit Notes
Blank(PB10146-BLK1) Prepared &Analyzed: 09/12/18
Sodium Absorption Ratio BRL 2.0 [blank]
Calcium, SAR 0.730 0.10 mg/L BH
Magnesium, SAR BRL 0.10 mg/L
Sodium, SAR 2.18 0.50 mg/L BH
Batch P810175 - NO PREP
Duplicate (P810175-DUP1) Source: 8090114-01 Prepared: 09/12/18 Analyzed: 09/13/18
SAR Percent Moisture 57.1 0.100 % by Weight 59.7 4 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O.. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 12

Level II QC Report
Full -Service Analytical & 2111/19
EI jP�I I S1 Environmental Solutions
LABORATORIES, INC.
City of Statesville, NC Project: StaLime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
Andy Smith 7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810138 - SM4500-PB5
Blank (P810138-BLK1)
Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total
BRL 2.5 mg/kg wet
LCS (P810138-BSI)
Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total
98.1 2.5 mg/kg wet
100.0 98 90-110
Matrix Spike (P810138-MS1)
Source: 8090114-01
Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total
2460 53 mg/kg dry
105.1 2320 127 80-120 MC
Matrix Spike Dup (P810138-MSD1)
Source: 8090114-01
Prepared: 09/12/18 Analyzed: 09/13/18
Phosphorus -Total
2420 53 mg/kg dry
105.1 2320 94 80-120 1 20
Batch P810167 - 351.2
Blank (P810167-BLK1)
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
BRL 25 mg/kg wet
LCS (P810167-BSI)
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
126 25 mg/kg wet
125.0 101 90-110
Matrix Spike (P810167-MS1)
Source: 8090114-01
Prepared: 09/13/18 Analyzed: 09/17/18
Cjeldahl Nitrogen
8310 1300 mg/kg dry
5257 3380 94 90-110
ivlainx Spike Dup (P810167-MSD1)
Source: 8090114-01
Prepared: 09/13/18 Analyzed: 09/17/18
Total Kjeldahl Nitrogen
4760 1300 mg/kg dry
5257 3380 26 90-110 54 20 D, M
Batch P810183 - NO PREP
Blank (P810183-BLK1)
Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 12

1 ..
ORATORIES, INC
Full -Service Analytical &
Environmental Solutions
Level II QC Report
2/11/19
City of Statesville, NC
Andy Smith
3Ox 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P810183 - NO PREP
Project: Stal-ime (Qtrly, BiWeekly, 60Day Prism Work Order: 8090114
7 Fecal) Time Submitted: 9/10/2018 1:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
LCS (P810183-BS1) Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 49.4 5.0 mg/kg wet 50.00 99 80-120
Matrix Spike (P810183-MS1) Source: 8090114-01 Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 170 5.3 mg/kg dry 52.57 108 119 80-120
Matrix Spike Dup (P810183-MSD1) Source: 8090114-01 Prepared &Analyzed: 09/14/18
Nitrate/Nitrite as N 168 5.3 mg/kg dry 52.57 108 114 80-120 2 20
Batch P810196 - SM4500-NH3 B
Blank (P810196-BLK1) Prepared: 09/13/18 Analyzed: 09/14/18
Ammonia as N BRL 10 mg/kg wet
LCS (P810196-BSI) Prepared: 09/13/18 Analyzed: 09/14/18
Ammonia as N 498 10 mg/kg wet 500.0 100 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 12

Sample Extraction Data
Prep Method: 351.2
Lab Number
Batch
Initial
Final
Date/Time
7 -1
114-01
P810167
0.05 g
25 mL
09/13/18 10:00
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810196
1.01 g
50 mL
09/13/18 10:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810138
1 g
50 mL
09/12/18 9:43
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810191
30 g
30 g
09/14/18 9:45
Prep Method:3010A
Lab Number
Batch
Initial
Final
DatelTime
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
8090114-01
P810146
50 mL
50 mL
09/12/18 13:00
Prep Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810136
2 g
50 mL
09/12/18 8:05
Method: 7471B
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810134
0.61 g
50 mL
09/12/18 8:45
Prep Method: SAR 2-78-054
Lab Number
Batch
Initial
Final
Date/Time
8090114-01
P810133
250 g
250 g
09/11/18 13:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 10 of 12

1
CHAIN, �17 �9�QSTO® Fi RECORD
°
i.� Full -Service Analytical &
i . NO
N/A
I Environmental Solutions PAGE_ OF _ QUOTE 9 TO ENSU DPER BILLING:
Samples INTACT upon arrival? I
=� =� :••'LneoRATORies wa
Project Name:
Received ON WET ICE?
-
-
449 Springbrook Road • Charlotte, NC 28217
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
PROPER PRESERVATIVES indicated?
Phone [phone]�364 Fax: [phone]
*Please ATTACH any project specific reporting (QC LEVEL I it III IV)
VAII--Si-31
�,--
Received WITHIN HOLDING TIMES? _
SEALS' INTACT?
Client Company Name: a-
—�
provisions and/or QC Requirements
CUSTODY
Report To/Contact Name: MCI, CA NO &V A Y Invoice
To:
VOLATILES reed W/OUT HEADSPACE?
Reporting Address Address: _
PROPER EONTAIN_ERS',ticerl? ,
TEMP: -Therm ID• :_Observed: 2 . °C tcorn.
°C
Phone:704V• 87,f JUS Fare (NO):70,9- M ,T49 Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Email Address: - Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other' "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rush
re h Work Must Be
Sc OTHER NIA
Site Location Name: F d at h t:r er lef Samples received after 14:00 will be processed next business day.
NO
_
Site Location Physical Address: 9 5P3 8i61 PI f'NZ> Tumamund time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES— —
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) la p -
TIME MATRIX
CLIENT DATE COLLECTED (SOIL,
SAMPLE CONTAINER ANALYSIS REQUESTED
PRESERVA- ,� {� REMARKS
PRISM
LAB
SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR
"TYPE NO SIZE TIMES {� / e, ,�
% /
ID NO.
HOURS SLUDGE)
SEE BELOW �/
Z w.L
14,29S,906
TS
1J�
ICE
�;J iv
a2
Wde_
Cat
GO 7 FEECA
03
01
SA R
zi
ram.
�dr?/r� Affiliation
D fa
e
Sampler's Signature Sampled By
(Print Name)
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted In writing to the Prism Project Manager. There will be charge,4ARr any changes after analyses have been initialized.
-MllitaryiHours
Rahn shed By:(Slgnature) Racei/ y:.(s+naturep
Additional Comments:::: SiteArrivalTime:
Rell�had By:,(Signature) �ReCbrved By: fgmIure) to
Site Departure Time:
ulshed By` (Signature) eEve ' p; Lebor.,taries By: Date
Field Tech Fee:
� t
_
Mileage:
d +p(ner t NOTE: SAMPLE COOLERS SHOULD BE TAPED SHUti
CUSTODY SEALS FOR TRANSPORT IDN 70 THE LABORATORY. COC.Oreyp No,
_ SA ARE NOT ACCEPTED AND VERIFIED AGAINST COCUNTIL RECEIVED ATTHE LABORATORY. /1 h 11,
yU` U
Ex ❑ Hand delivered Prism Field Service ❑ Othor
UST: G OUNDWATER: DRINKING WATER: LID WASTE: RCRA: CERCLA LANDFILL OTHER:
SO(NC
N C❑SC ❑NC ElO C ❑SC ❑NC El SC
I
❑SC I ElNC❑SCI El SC I El El SC El NC ❑SC
I
I ❑ ❑ ❑
❑ El
r,IUVAr.aMm rvno rnnCQ- A - A—K., rt = rtlo.. (,= rl'lacc
P = Plactir• TI = Taflnn-I inart (:an V0A = Vnlstile Organics Analvsis (Zero Head SDace)

Main Office:
449 Springbrook Road
�l I Full Service Analytical and P.O. Box 240543
1P:.R 9 s m I Environmental Solutions Charlotte, NC 28224-0543
'-. sou ru7GiECSfYG Phone:[phone]
1/800/529-6364
Fax: [phone]
www.prismiabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Number8090114-01 Sample Name Sta-Lime
Na: Sodium (mg/L) Equivalent weight: 23
Ca: Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam /L Cam /L M (g M L1
126 16300 1 0
Na (ME)
Ca ME
Mg (ME)
5.48
1 81 b.000
0.0
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = < 2 (From mg/L entered above)
Calculated By: 4c:,
6 or
Page 12of12

Case Narrative
�I, Ism
�:—] —O ATOR . INC.
City of Statesville, NC
Andy Smith
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cart No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (60 Day/7 Fecal)
Lab Submittal Date: 09/11/2018
Prism Work Order: 8090131
02/11 /2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised aboratory report dated 01/29.19 The SAR comment has been
removed. There was not an SAR request on this work order.
Please call if you have any questions relating to this analytical report.
pectfully,
PRISM LABORATORIES, INC.
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
i Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 1 of 11

Receipt Summary
mk-Sample
I
M
Full -Service Analyticals Environmental solutions
02/11/2019
LABOR
MM
Prism Work Order: 8090131
Sample ID
Lab Sample ID
Matrix
Date/Time Sampled DatelTime Received
__31 #1
8090131-01
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #2
8090131-02
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #3
8090131-03
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #4
8090131-04
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #5
8090131-05
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #6
8090131-06
Solid
09/11/18 12:00 09/11/18 14:35
Fecal #7
8090131-07
Solid
09/11/18 12:00 09/11/18 14:35
Samples were received at 23.0 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 11

Laboratory Report
i � Full Service Analytical &
ziP F I Environmental Solutions 02/11/2019
�a! SORATORIES. INC
Citv of Statesville, NC Project: Stal-ime (60 Day/7 Fecal) Client Sample ID: Fecal #1
Andy Smith Prism Sample ID: 8090131-01
Box 1111 Prism Work Order: 8090131
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 82.5 % by 0.100 0.100 1 *SM2540 G 9114/18 9:45 TJY P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
1 *SM9221 E 9/12/18 10:39 BMS P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 11

P Full -Service Analytical &
-P R I S M Environmental Solutions
LABORATOR
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #2
Prism Sample ID: 8090131-02
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result
Units
Report
MD Dilution Method Analysis Analyst
Batch
Limit
Factor Datemme
ID
General Chemistry Parameters
% Solids 99.5
% by
0.100
0.100 1 *SM2540 G 9/14/18 9:46 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 *SM9221 E 9/12118 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 11

Full -Service Analytical &
/z-�R I Environmental Solutions
�L-scm;rosms. ING
Laboratory Report
02/11 /2019
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample iD: Fecal #3
Andy Smith Prism Sample ID: 8090131-03
". Box 1111 Prism Work Order: 8090131
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 95.2 % by 0.100 0.100 1 *SM2540 G 9114/18 9:45 TJY P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 9/12/18 10:39 BMS P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 11

Laboratory Report
p t Full -Service Analytical &
UI� Ism I Environmental Solutions
02/11/2019
�LAEOMTORIE41NQ
o
City of Statesville, NC
Project: StaLime (60 Day/7 Fecal)
Client Sample ID: Fecal #4
Andy Smith
Prism Sample ID: 8090131-04
Box 1111
Prism Work Order: 8090131
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 95.1
% by
0.100 0.100
1 `SM2540 G 9/14/18 9:45 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 'SM9221 E 9/12/18 10:39 BMS
P810172
u
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 11

Laboratory Report
1-•9
Full -Service Analytical &
� M Environmental Solutions
02/11/2019
��A LABORATORIES ING
City of Statesville, NC
Project: Stal-ime (60 Day/7 Fecal)
Client Sample ID: Fecal #5
Andy Smith
Prism Sample ID: 8090131-05
Box 1111
Prism Work Order: 8090131
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 94.8
% by
0.100 0.100
1 *SM2540 G 9114118 9:46 TJY
P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.2
1 `SM9221 E 9112118 10:39 BMS
P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 11

1,ffl
5 Full -Service Analytical &
°R I S Environmental Solutions
x7 OHATOFIE$ INC.
City of Statesville, NC
Andy Smith
Box 1111
Statesville, NC 28687
Project: Stal-ime (60 Day/7 Fecal)
Sample Matrix: Solid
Laboratory Report
02111 /2019
Client Sample ID: Fecal #6
Prism Sample ID: 8090131-06
Prism Work Order: 8090131
Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 94.9 % by 0.100 0.100 1 *SM2540 G 9/14118 9:45 TJY P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2
1 *SM9221 E 9/12/18 10:39 BMS P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 11

I-N Full -Service Analytical &
16'?Mi
I Environmental Solutions
LABORATORIES ING
Laboratory Report
02/11 /2019
City of Statesville, NC Project: StaLime (60 Day/7 Fecal) Client Sample ID: Fecal #7
Andy Smith Prism Sample ID: 8090131-07
Box 1111 Prism Work Order: 8090131
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/11/18 12:00
Time Submitted: 09/11/18 14:35
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids 93.3 % by 0.100 0.100 1 *SM2540 G 9114/18 9:45 TJY P810191
Weight
Microbiological Parameters
Fecal Coliforms BRL MPN/g dry 0.2 1 *SM9221 E 9/12/18 10:39 BMS P810172
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 11

ALIJ
Full -Service Analytical &
IS Environmental Solutions
ONATONIES INC.
City of Statesville, NC
,Andy Smith
3ox 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Analyte
Project: StaLime (60 Day/7 Fecal)
Level II QC Report
2/11 /19
Prism Work Order: 8090131
Time Submitted: 9/11/2018 2:35:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P810172 - NO PREP
Blank (P810172-BLK1) Prepared &Analyzed: 09/12/18
Fecal Coliforms BRL 0.2 MPN/g wet
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
8090131-01
P810191
30
g 30 g
09/14/18
9:45
8090131-02
P810191
30
g 30 g
09/14/18
9:45
8090131-03
P810191
30
g 30 g
09/14/18
9:45
8090131-04
P810191
30
g 30 g
09/14/18
9:45
8090131-05
P810191
30
g 30 g
09/14/18
9:45
8090131-06
P810191
30
g 30 g
09/14/18
9:45
8090131-07
P810191
30
g 30 g
09/14/18
9:45
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 777-1
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 15 of 11

(CHAIN E! OF CUSTODY RC7CVRCC:/
Full -Service Analytical &
Environmental Solutions PAGE_ OF _ QUOTE # TO ENSURE PROPER BILLING:
'�I- EJORATORIE$ INC.
449 Springbrook Road - Charlotte, NC 28217
Phone [phone] - Fax: [phone] I
Client Company Name: C:�v o-1'a�E°Sw.I�C
Report To/Contact Name: Wej GA llowq
Reporting Address:
Phone:[phone]S Fax es (No):7041-97f,Vss
Email Address:
EDD Type: PDF Excel_ Other
Site Location Name: FoLA r 4i CR E e k
Site Location Physical Address: 643 E j9 'Gam E2
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
LAW USE, ONLY'
j
YES NO
NIF r
Samples INTACT upon arrival?
T
Received ON WET ICE?
r
PROPER PRESERVATIVES indicated?
_7C
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
_
a
VOLATILES rec'd W/OUT HEADSPACE?
PROPER CONTAINERS used?
'r
_
TEMP: Therm ID: lQ-T _ I _ Observed: 2:"3;-()C / Con:
°C
Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONNEL
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days U 4 Days ❑ 5 Days Certification: NELAC DOD FL NC
"Working Days" U 6-9 Days ❑ Standard 10 days ❑ RushWoPre-Approved Must Be SC OTIiER N/A
Samples received after 14:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES_ NO
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES SIced on Collection: YES— NO
—
BY PRISM LABORATORIES, INC. TO CLIENT Sample P P
TIME
*r`niuTaim= Tvl9F r_r1r1=C• A = Annhor r. = r:lpar r,= (+lacc P = Plaetin- TI = Taflnn_I inari (:on \/(lA = \/nloiilo 1-1—onine Anol—ic t7orn W—A Cnono)

1IR- ISM
�LABORATORIES, INC.
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: StaLime (Qtrly, & BiWeeklyl)
Lab Submittal Date: 10/22/2018
Prism Work Order: 8100388
Case Narrative
02/11 /2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
This is a Revised Report and supercedes the revised laboratory report datedl/29/19. The SAR comment has been
added below.
Analysis note for SAR:
SAR =[Na]/SQRT {([Ca]+[Mg])/2}
— .R = [ 120123.0 ] / SQRT { ( [1200/20.0] + [0/12.2]) / 2 }
Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates
taking the square root of the operand in parentheses.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Reviewed By Robbi A. Jones
President/Project Manager
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 18

Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 1Ox the MB.
BHL MB greater than one half of the RL, but sample concentrations are either less than the RL or greater than 1Ox the
MB.
MC Sample concentration too high for recovery evaluation.
BRL Below Reporting Limit
MDL Method Detection Limit
D Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

Full -Service Analytical &
S Environmental Solutions
.�iIAR, e! , OMTORIE$ INC.
Sample Receipt Summary
02/11 /2019
Prism Work Order: 8100388
1-Ii-nt Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
_'' -ime (and Fecal 1)
8100388-01
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #2
8100388-02
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #3
8100388-03
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #4
8100388-04
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #5
8100388-05
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #6
8100388-06
Solid
10/22/18 11:25
10/22/18 12:30
Fecal #7
8100388-07
Solid
10/22/18 11:25
10/22/18 12:30
Samples were received in good condition at 1.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone]-Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18

Laboratory Report
RFull -Service Analytical &
`l I S M I Environmental Solutions 02/11/2019
��LABOflATOflIE$ ING
city of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl) Client Sample ID: StaLime (and Fecal 1)
n: Ken Galloway Prism Sample ID: 8100388-01
* �.J. Box 1111 Prism Work Order: 8100388
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
DateRme
ID
General Chemistry Parameters
Plant Available Nitrogen
BRL
mg/kg dry
1100
330
5
*Calculation
10/29/18 9:15
CLB
[CALC]
Solids
66.6
% by
0.100
0.100
1
*SM2540 G
10/25/18 14:00
TJY
P8J0554
Weight
Ammonia as N
380
mg/kg dry
15
3.7
1
*SM4500-NH3 C
10/25/18 15:32
BMS
P8J0519
Nitrate/Nitrite as N
25
mg/kg dry
7.5
2.1
1
*SM4500-NO3 F
10/29/18 9:15
CLB
P8J0524
Phosphorus -Total
3200
mglkg dry
75
17
20
*SM4500-P F
10/26/18 8:39
CLB
P8J0495
Total Kjeldahl Nitrogen
BRL
mg/kg dry
3800
1100
5
*351.2
10/24/18 8:08
CLB
P8J0419
Microbiological Parameters
Fecal Coliforms
BRL
MPN/g dry
0.3
1
*SM9221 E
10/22/18 13:25
BMS
P8J0422
Total Metals
Mercury
0.11
mg/kg dry
0.030
0.0028
1
*7471B
10/24/18 15:25
MMR
P8J0448
SAR Soil Preparation
Complete
g
1
*2-78-054
10/25/18 14:15
MMR
P8J0504
SAR Percent Moisture
Complete
% by
0.100
0.100
1
*2-78-054
10/26/18 14:30
MMR
P8J0542
Weight
Arsenic
BRL
mg/kg dry
7.5
0.46
10
*6010D
10/29/18 22:52
JAB
P8J0453
"'gum Absorption Ratio
1.0
[blank]
0.80
0.016
1
*2-78-054
10/29/18 23:08
JAB
P8J0498
nium
BRL
mg/kg dry
3.7
0.10
10
*6010D
10/29/18 22:52
JAB
P8J0453
Calcium, SAR
1200 B
mg/L
1.0
0.10
10
*6010D
10/29/18 23:08
JAB
P8J0498
Copper
42
mg/kg dry
7.5
0.68
10
*6010D
10/29/18 22:52
JAB
P8J0453
Lead
BRL
mg/kg dry
3.7
0.69
10
*6010D
10/29/18 23:08
JAB
P8J0453
Magnesium, SAR
BRL
mg/L
1.0
0.086
10
*6010D
10/29/18 23:08
JAB
P8J0498
Nickel
11
mg/kg dry
7.5
0.27
10
*6010D
10/29/18 22:52
JAB
P8J0453
Potassium
2100
mg/kg dry
190
6.7
10
*6010D
10/29/18 22:52
JAB
P8J0453
Selenium
BRL
mg/kg dry
7.5
1.8
10
*6010D
10/29/18 22:52
JAB
P8J0453
Sodium
4500
mg/kg dry
220
7.3
10
*6010D
10/29/18 23:08
JAB
P8J0453
Sodium, SAR
120 B
mg/L
5.0
0.18
10
*6010D
10/29/18 23:08
JAB
P8J0498
Zinc
79
mg/kg dry
37
1.3
10
*6010D
10/29/18 22:52
JAB
P8J0453
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 18

A=Ak�nkjC
Full-Service Analytical &
S M IEnvironmental Solutions
RATORIES� ING
Laboratory Report
02/11 /2019
City of Statesville, NC
n: Ken Galloway
_ D. Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Client Sample ID: Fecal #2
Prism Sample ID: 8100388-02
Prism Work Order: 8100388
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 70.8
% by
0.100
0.100 1
*SM2540 G 10/25/18 14:00 TJY
138J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 18

Full -Service Analytical &
P R I
I'A'
Environmental Solutions
71 ABORATORIE$INC.
City of Statesville, NC
j Ken Galloway
\ Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #3
Prism Sample ID: 8100388-03
Prism Work Order: 8100388
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 70.3
% by
0.100
0.100 1
*SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 10/22/18 13:25 BMS
P8,10422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 6 of 18

f
Laboratory Report
Full -Service Analytical &
I S M I Environmental Solutions
02/11/2019
—Y-17U... ATCRIES, INC.
City of Statesville, NC
Project: StaLime (Qtrly, & BiWeeklyl)
Client Sample ID: Fecal #4
tn: Ken Galloway
Prism Sample ID: 8100388-04
D. Box 1111
Prism Work Order: 8100388
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 73.0
% by
0.100 0.100
1 `SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 "SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 7 of 18

Full -Service Analytical &
M I Environmental Solutions
LABORATORIES, ING
City of Statesville, NC
Ken Galloway
---- Box 1111
Statesville, NC 28687
Project: Stal-ime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #5
Prism Sample ID: 8100388-05
Prism Work Order: 8100388
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Solids 70.3
% by
0.100
0.100 1
'SM2540 G 10/25/18 14:00 TJY
138J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
*SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 18

V' Full -Service Analytical &
R I C I Environmental Solutions
��LABORATORIE$ ING
City of Statesville, NC
Ken Galloway
Box 1111
Statesville, NC 28687
Project: StaLime (Qtrly, & BiWeeklyl)
Sample Matrix: Solid
Laboratory Report
02/11 /2019
Client Sample ID: Fecal #6
Prism Sample ID: 8100388-06
Prism Work Order: 8100388
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids 72.3
% by
0.100
0.100 1
*SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1
'SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 9 of 18

Laboratory Report
A
-1P�rp I S 1 �7 , I Full -Service Analytical &
Environmental Solutions
02/11/2019
�'ILABORATORIES. INC.
City of Statesville, NC
Project: StaLime (Qtrly, & BiWeeklyl)
Client Sample ID: Fecal #7
tn: Ken Galloway
Prism Sample ID: 8100388-07
D. Box 1111
Prism Work Order: 8100388
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/22/18 11:25
Time Submitted: 10/22/18 12:30
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids 68.9
% by
0.100 0.100
1 *SM2540 G 10/25/18 14:00 TJY
P8J0554
Weight
Microbiological Parameters
Fecal Coliforms BRL
MPN/g dry
0.3
1 *SM9221 E 10/22/18 13:25 BMS
P8J0422
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 10 of 18

Level II QC Report
> > Full -Service Analytical & 2/11/19
_ I S Environmental Solutions
�Y�LABORATORIE% INC.
City of Statesville, NC
1: Ken Galloway
I. Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8JO448 - 7471 B
Project: Stal-ime (Qtrly, & BiWeeklyl)
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0448-BLK1) Prepared & Analyzed: 10/24/18
Mercury BRL 0.020 mg/kg wet
LCS (P8J0448-BSI) Prepared &Analyzed: 10/24/18
Mercury 0.417 0.020 mg/kg wet 0.4167 100 80-120
Batch P8J0453 - 3050B
Blank (P8J0453-BLK1)
Prepared: 10/24/18 Analyzed: 10/26/18
Arsenic
BRL
0.50
mg/kg wet
Cadmium
BRL
0.25
mg/kg wet
Copper
BRL
0.50
mg/kg wet
Lead
BRL
0.25
mg/kg wet
Nickel
BRL
0.50
mg/kg wet
Potassium
BRL
12
mg/kg wet
Selenium
BRL
0.50
mg/kg wet
Sodium
BRL
15
mglkg wet
Zinc
BRL
2.5
mg/kg wet
3 (P8J0453-BS1)
Prepared: 10/24/18 Analyzed: 10/26/18
;nic
11.7
0.50
mg/kg wet
12.50
93
80-120
Cadmium
12.3
0.25
mglkg wet
12.50
99
80-120
Copper
12.5
0.50
mg/kg wet
12.50
100
80-120
Lead
12.4
0.25
mg/kg wet
12.50
99
80-120
Nickel
12.3
0.50
mg/kg wet
12.50
98
80-120
Potassium
1290
12
mglkg wet
1250
103
80-120
Selenium
11.1
0.50
mg/kg wet
12.50
89
80-120
Sodium
1310
15
mg/kg wet
1250
105
80-120
Zinc
11.7
2.5
mg/kg wet
12.50
94
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 18

Full -Service Analytical &
S M I Environmental Solutions
�I ABORA ... ING
Level II QC Report
2/11119
City of Statesville, NC
Ken Galloway
Box 1111
Statesville, NC 28687
Total Metals - Quality Control
Analyte
Batch P8J0498 - 301 OA
Project: StaLime (Qtrly, & BiWeeklyl)
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0498-BLK1)
Prepared: 10/25/18 Analyzed: 10/29/18
Calcium, SAR
0.605 0.10 mg/L BH
Magnesium, SAR
BRL 0.10 mg/L BHL
Sodium, SAR
5.05 0.50 mg/L BH
Batch P8JO504 - SAR 2-78-054
Blank (P8J0504-BLK1)
Prepared: 10/24/18 Analyzed: 10/25/18
SAR Soil Preparation
Complete g
Batch P8JO542 - NO PREP
Duplicate (P8J0542-DUP1) Source: 8100388-01 Prepared &Analyzed: 10/26/18
SAR Percent Moisture Complete 0.100 % by Weight Complete 0.6 200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 12 of 18

PP1Full -Service Analytical &
I Environmental Solutions
�— ,'LABORATORIES, ING
Level II QC Report
2/11 /19
City of Statesville, NC
;r Ken Galloway
1. Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Analyte
Batch P8JO419 - 351.2
Project: StaLime (Qtrly, & BiWeeklyl) Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0419-BLK1) Prepared: 10/23/18 Analyzed: 10/24/18
Total Kjeldahl Nitrogen BRL 50 mg/kg wet
LCS (P8J0419-BSI) Prepared: 10/23/18 Analyzed: 10/24/18
Total Kjeldahl Nitrogen 124 50 mg/kg wet 125.0 99 90-110
Batch P8JO495 - SM4500-PB5
Blank (P8J0495-BLK1) Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total BRL 2.5 mg/kg wet
LCS (PBJ0495-BS1) Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total 106 2.5 mg/kg wet 100.0 106 90-110
Matrix Spike (P8J0495-MS1) Source: 8100388-01 Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total 3370 75 mg/kg dry 150.2 3230 88 80-120
Matrix Spike Dup (P8J0495-MSDI) Source: 8100388-01 Prepared: 10/25/18 Analyzed: 10/26/18
Phosphorus -Total 3460 75 mg/kg dry 150.2 3230 154 80-120 3 20 MC
Batch P8JO519 - SM4500-NH3 B
Ink (PBJ0519-BLK1) Prepared &Analyzed: 10/25/18
Ammonia as N BRL 10 mg/kg wet
LCS (P8J0519-BS1) Prepared &Analyzed: 10/25/18
Ammonia as N 515 10 mg/kg wet 500.0 103 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 18

> Full -Service Analytical &
I S Environmental Solutions
/�'MI�ORATORIES, INC.
Level II QC Report
2/11/19
City of Statesville, NC Project: Stal-ime (Qtrly, & BiWeeklyl) Prism Work Order: 8100388
l: Ken Galloway Time Submitted: 10/22/2018 12:30:OOPM
Box 1111
Statesville, NC 28687
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0519 - SM4500-NH3 B
Matrix Spike (P8J0519-MS1) Source: 8100388-01 Prepared &Analyzed: 10/25/18
Ammonia as N 1100 15 mg/kg dry 750.9 383 95 80-120
Batch P8JO524 - NO PREP
Blank (P8J0524-BLK1)
Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N
BRL 5.0 mg/kg wet
LCS (P8J0524-BS1)
Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N
48.7 5.0 mg/kg wet
50.00 97 80-120
Matrix Spike (P8J0524-MS1)
Source: 8100388-01
Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N
96.3 7.5 mg/kg dry
75.09 24.6 95 80-120
Matrix Spike Dup (P8J0524-MSD1)
Source: 8100388-01
Prepared: 10/26/18 Analyzed: 10/29/18
Nitrate/Nitrite as N
97.3 7.5 mg/kg dry
75.09 24.6 97 80-120 1 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 18

Full -Service Analytical &
f—I��RI S 1 Y, Environmental Solutions
-_'L7 ORATORIES,INa
Level II QC Report
2/11 /19
City of Statesville, NC Project: StaLime (Qtrly, & BiWeeklyl)
Ken Galloway
Box 1111
Statesville, NC 28687
Microbiological Parameters - Quality Control
Prism Work Order: 8100388
Time Submitted: 10/22/2018 12:30:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PBJ0422 - NO PREP
Blank (P8J0422-BLK1) Prepared &Analyzed: 10/22/18
Fecal Coliforms BRL 0.2 MPN/g wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 18

Prep Method: 351.2
Lab Number
Batch
Initial
Sample Extraction Data
Final Date/Time
)388-01
P8J0419
0.05 g
25 mL 10/23/18 11:25
Prep Method: SM4500-NH3 B
Lab Number
Batch
Initial
Final Date/Time
8100388-01
P8J0519
1.01 g
50 mL 10/25/18 8:55
Prep Method: SM4500-PB5
Lab Number
Batch
Initial
Final DatelTime
8100388-01 P8J0495 1 g 50 mL 10/25/18 10:30
Prep Method: Solids, Dry Weight
Lab Number Batch Initial Final Date/Time
8100388-01
P8J0554
30
g
30 g
10/25/18 14:00
8100388-02
P8J0554
30
g
30 g
10/25/18 14:00
8100388-03
P8J0554
30
g
30 g
10/25/18 14:00
8100388-04
P8J0554
30
g
30 g
10/25/18 14:00
8100388-05
P8J0554
30
g
30 g
10/25/18 14:00
8100388-06
P8J0554
30
g
30 g
10/25/18 14:00
8100388-07
PBJ0554
30
g
30 g
10/25/18 14:00
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8100388-01
P8J0498
50
mL
50 mL
10/25/18 14:10
n11)0388-01
P8J0498
50
mL
50 mL
10/25/18 14:10
._p Method: 3050B
Lab Number
Batch
Initial
Final
Date/Time
8100388-01 P8J0453 2.01 g 50 mL 10/24/18 8:50
8100388-01 P8J0453 2.01 g 50 mL 10/24/18 8:50
Prep Method: 7471B
Lab Number Batch Initial Final DatelTime
8100388-01 P8J0448 0.61 g 50 mL 10/24/18 10:05
Prep Method: SAR 2-78-054
Lab Number Batch Initial Final Date/Time
8100388-01 P8J0504 250 g
250 g 10/24/18 14:10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 16 of 18

Full -Service Analytical &
a � M
Environmental Solutions
.:._..,.___..,_...,i" LABORATORIES, INC.
449 Sprindbrook Road • Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: C-*4-v ,' V4"r Y; Ile
Report To/Contact Name: Ks J Cre;howAy
Reporting Address:
PAGE_ OF _ QUOTE # TO ENSI IOPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To
Address:
- - NO NIA
Samples INTACT upon arrival?
Received ON WETICE? -
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALSINTACT?
VOLATILES reed W1OUTfIF_ADSP6C
PROPER CONTAINERS used?'j_
TEMP: Therm'lb.: . � _,O�iser6ed:il� ,°C,/,Coir
Phone:70- 87t- 3" $ Fax es (No): !r0* f7L U5_ Purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: PtELAC DoD
FL NC
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days El Standard 10 days ❑ Rush Work Must Be
Pre -Approved
SC OTHER
N/A
Site Location Name: FO&A r.i � C a E t; k Samples received after 14:00 will be processed next business day.
y
Site Location Physical Address: 69.3'Ell egLq,rr dt ._ Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
Sample Iced Oro Collection: YES_
P p
NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSIS REQUESTED
%�GQ
�leeriREMARKS
/ / /
PRISM
LAB
*TYPE
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
NO.
SIZE
ID NO.
HOURS
SLUDGE)
SEE BELOW
/!
S 'r
10-aa-I
,as
14.2. 20.3
rKA1
41
�I
A
49 -
�Z
IAA d-
03
c,4
CA R
0�
-Pb
N.
�S
14Q
k
Ob
07
fO T.00
e•
Sampler's Signature / / Sampled By (Print Name) t• Affiliation -
Upon relinquishing, this Chain of ustody is your authorization for Prism to proceechwith the analyses as requested above. Any changes must be
submitted in writing to the Prism Project Manager. There will be charge a y'cha ges after analyses have been initialized.
nelin9uJO d By; (Signature) Q I�ec¢ivt By: (S' atura). Date/ - Milltewmaurs Additional Comments:
7Anival:
L
" -
Rel' ished By: (Signature) R elvedffy: (Slgnatu O e /
ime:
r
Field Tech Fee:
qulsh¢crEg: (Sig qr¢) R¢ Iv¢d FnrP ism born ar d• Date
/:Jfi
r
�
(Q d'of Sh)lament: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR NSPORTATION To'rHE LABORATORY. COC Group No.
Milea e:
g
-
(D / SAMPLES ARE NOT CCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY.
V d,Ex ❑'11PS ❑ Hand -delivered Prism Field Service ❑ Other
GE70UNDWATER: DRlNlCING WATER: SOLID WASTE: RCRA: CERCLPi LANDFILL. OTHER:C
❑NC ❑SC ❑5C ❑SC
JE7S:UST
❑SC I ONC❑SC ❑❑NC ❑SCI ®NC ❑SCI ANC ❑SCrAureo
ANC ANC ONC
-rvnc r•nnmc. A — A—k— 0 - 01— r--- r_I... C - GI —fin- TI = Tpflnn-1 inprt Ran VC)A = Vnlatilp OmAnir_s AnAlvRIS (Zero Head Space)

Main Office:
id- 449 Springbrook Road
Full Service Analytical and P.O. Box 240543
Environmental Solutions Charlotte, NC 28224-0543
;%LAgoFin�k.EE;iPic Phone:[phone]
11800/529-6364
Fax: [phone]
www.prismlabs.com
Sodium Absorption Ratio
The amount of exchangeable sodium ions versus the amount of exchangeable
calcium & magnesium ions in a given material.
Sample Number 8100388-01 1 Sample Nalrne Stal-ime Fecal 1
Na: Sodium (mg/L) Equivalent weight: 23
Ca : Calcium (mg/L) Equivalent weight: 20
Mg : Magnesium (mg/L) Equivalent weight: 12
Milli Equivalent (ME) = mg/L / Equivalent weight
Nam 1L Cam /L M (m /L
120.0 1 1190.0 -0.2
N'a UvIE)
Ca (MEJ
Nlq (ME)
5.22
1 50.50
I -0.01
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
SAR = 1.0 (From mg/L entered above)
rl _ _r--
e 1
Calculated By: "'��
r
7-771
Page 18 of 18

r ; ISM
— L bu"ATORIES, IN0.
City of Statesville, NC
Ken Galloway
P.O. Box 1111
Statesville, NC 28687
NO Certification No.402 Case Narrative
Full -Service Analytical & NO Drinking Water Cert No. 37735 11/02/2018
Environmental Solutions SC Certification No. 99012
Project: 3rd and 4th Creek Sludge TCLP Short List
Lab Submittal Date: 10/17/2018
Prism Work Order: 8100342
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
TCLP Herbicide analysis was subcontracted to GCAL. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
'1 LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 21

Sample Receipt Summary
P� c fl Full -Service Analytical &
R I �J 1 V 1 Environmental Solutions 11/02/2018
:✓LABORATORIES, INC.
Prism Work Order: 8100342
Sample ID
Lab Sample ID
Matrix
Date/Time Sampled
Date/Time Received
N. ;;ek Sludge
3rd Creek Sludge
8100342-01
8100342-02
Solid
Solid
10/17/18 8:45
10/17/18 9:00
10/17/18 16:15
10/17/18 16:15
ra
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001629-6364 - Fax: [phone] Page 2 of 21

Full -Service Analytical &
AP h-"ISM
Y 1 I Environmental Solutions
d LASORATORIE; ING
Laboratory Report
11 /02/2018
C'i-fxl -f Statesville, NC
Project: 3rd and 4th Creek Sludge
Client Sample ID: 4th Creek Sludge
fl an Galloway
TCLP Short List
Prism Sample ID: 8100342-01
F. _ox 1111
Prism Work Order: 8100342
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 10/17/18 08:45
Time Submitted: 10/17/18 16:15
Parameter Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Datemme
ID
TCLP Extraction by EPA 1311
TCLP Extraction Complete
N/A
1 *1311 10/23/18 8:40
MMR
P8J0412
TCLP Organochlorine Pesticides by GC/ECD
gamma-BHC BRL
mg/L
0.00050 0.000065
1 *8081B 10/26/18 19:00
ZRC
P8J0478
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
113 %
13-186
Tetrachloro-m-xylene
77 %
40-134
TCLP Semivolatile Organic Compounds by GUMS
2-Methylphenol BRL
mg/L
0.050 0.0018
1 *8270D 10/25/18 17:24
JMV
P8J0443
3/4-Methylphenol BRL
mg/L
0.050 0.0015
1 *8270D 10/25/18 17:24
JMV
P8J0443
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
95 %
43-140
2-Fluorobiphenyl
88 %
44-119
2-Fluorophenol
55 %
19-119
Nitrobenzene-d5
84 %
44-120
Phenol-d5
37 %
11-52
Terphenyl-d14
91 %
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 21

RiRATORIES.
Full-Service Analytical &
S, V'p\/%�', I Environmental Solutions
0✓OINC.
/Ar
Laboratory Report
11 /02/2018
City of Statesville, NC
'en Galloway
-i)x 1111
Statesville, NC 28687
Project: 3rd and 4th Creek Sludge
TCLP Short List
Sample Matrix: Solid
Client Sample ID: 3rd Creek Sludge
Prism Sample ID: 8100342-02
Prism Work Order: 8100342
Time Collected: 10/17/18 09:00
Time Submitted: 10/17/18 16:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
TCLP Extraction by EPA 1311
TCLP Extraction Complete N/A 1 *1311 10/23/18 8:40 MMR P8J0412
TCLP Organochlorine Pesticides by GC/ECD
gamma-BHC BRL mg1L 0.00050 0.000065 1 *8081B 10/26/18 19:12 ZRC P8J0478
Surrogate Recovery Control Limits
Decachlorobiphenyl
Tetrachloro-m-xylene
124 % 13-186
88 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2-Methylphenol BRL mg/L 0.050 0.0018 1 *8270D 10/25/18 17:47 JMV P8J0443
3/4-Methylphenol BRL mg/L 0.050 0.0015 1 *8270D 10/25/18 17:47 JMV P8J0443
Surrogate Recovery Control Limits
2,4,6-Tribromophenol
85 %
43-140
2-Fluorobiphenyl
85 %
44-119
2-Fluorophenol
56 %
19-119
Nitrobenzene-d5
81 %
44-120
Phenol-d5
37 %
11-52
Terphenyl-d14
85 %
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 4 of 21

I S n Full -Service Analytical
' V' Environmental Solutions
LABORATORIES• INC.
Level II QC Report
11 /2/18
City of Statesville, NC
Ail" n Galloway
P.h_ 1111
Statesville, NC 28687
Project: 3rd and 4th Creek Sludge TCLP
Short List
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P8JO443 - 351 OC MS
Prism Work Order: 8100342
Time Submitted: 10/17/2018 4:15:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P8J0443-BLK1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-T(chlorophenol
BRL
0.25
mg/L
2,4,6-Trichlorophenol
BRL
0.10
mg/L
2,4-Dinitrotoluene
BRL
0.012
mg/L
2-Methylphenol
BRL
0.050
mg/L
3/4-Methyl phenol
BRL
0.050
mg/L
Hexachlorobenzene
BRL
0.010
mg/L
Hexachlorobutadiene
BRL
0.050
mg/L
Hexachloroethane
BRL
0.050
mg/L
Nitrobenzene
BRL
0.050
mg/L
Pentachlorophenol
BRL
0.25
mg/L
Pyridine
BRL
0.25
mg/L
Surrogate:2,4,6-Tribromophenol
0.0804
mglL
0.1000
80
43-140
Surrogate:2-Fluorobiphenyl
0.0420
mg/L
0.05000
84
44-119
Surrogate:2-Fluorophenol
0.0549
mglL
0.1000
55
19-119
Surrogate: Nitrobenzene-d5
0.0405
mg/L
0.05000
81
44-120
Surrogate: Phenol-d5
0.0366
mg/L
0.1000
37
11-52
;." e: Terphenyl-d14
0.0448
mg/L
0.05000
90
50-134
L_ 'BJ0443-13S1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-Trichlorophenol
0.0435
0.25
mg/L
0.05000
87
53-123
2,4,6-Trichlorophenol
0.0426
0.10
mg/L
0.05000
85
50-125
2,4-Dinitrotoluene
0.0451
0.012
mg/L
0.05000
90
57-128
2-Methylphenol
0.0368
0.050
mg/L
0.05000
74
30-117
3/4-Methylphenol
0.0304
0.050
mg/L
0.05000
61
29-110
Hexachlorobenzene
0.0422
0.010
mg/L
0.05000
84
53-125
Hexachlorobutadiene
0.0283
0.050
mg/L
0.05000
57
22-124
Hexachloroethane
0.0268
0.050
mg/L
0.05000
54
21-115
Nitrobenzene
0.0375
0.050
mg/L
0.05000
75
45-121
Pentachlorophenol
0.0386
0.25
mg/L
0.05000
77
35-138
Pyridine
0.0219
0.25
mg/L
0.05000
44
10-53
Surrogate: 2,4,6-Tribromophenol
0,0841
mg/L
0.1000
84
43-140
Surrogate:2-Fluorobiphenyl
0.0403
mg/L
0.05000
81
44-119
Surrogate:2-Fluorophenol
0.0515
mglL
0.1000
51
19-119
Surrogate: Nitrobenzene-d5
0.0350
mg/L
0.05000
70
44-120
Surrogate: Phenol-d5
0.0348
mg/L
0.1000
35
11-52
Surrogate: Terphenyl-d14
0.0433
mg/L
0.05000
87
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 21

Full -Service Analytical 8
J R I Environmental Solutions
IAeQR TCRIES INC.
Level II QC Report
1112/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
A n Galloway Short List Time Submitted: 10/17/2018 4:15:OOPM
P. K 1111
Statesville, NC 28687
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8JO443 - 351 OC MS
LCS Dup (P8J0443-BSD1)
Prepared: 10/24/18 Analyzed: 10/25/18
2,4,5-Trichlorophenol
0.0435
0.25
mg/L
0.05000
87
53-123
0.02
20
2,4,6-Trichlorophenol
0.0445
0.10
mg/L
0.05000
89
50-125
4
20
2,4-Dinitrotoluene
0.0456
0.012
mg/L
0.05000
91
57-128
1
20
2-Methylphenol
0.0389
0:050
mg/L
0.05000
78
30-117
6
20
3/4-Methylphenol
0.0328
0.050
mg/L
0.05000
66
29-110
7
20
Hexachlorobenzene
0.0428
0.010
mg/L
0.05000
86
53-125
1
20
Hexachlorobutadiene
0.0306
0.050
mg/L
0.05000
61
22-124
8
20
Hexachloroethane
0.0299
0.050
mg/L
0.05000
60
21-115
11
20
Nitrobenzene
0.0386
0.050
mg/L
0.05000
77
45-121
3
20
Pentachlorophenol
0.0425
0.25
mg/L
0.05000
85
35-138
10
20
Pyridine
0.0224
0.25
mg/L
0.05000
45
10-53
2
20
Surrogate: 2,4,6-Tribromophenol
0.0869
mg/L
0.1000
87
43-140
Surrogate:2-Fluorobiphenyl
0.0427
mg/L
0.05000
85
44-119
Surrogate:2-Fluorophenol
0.0564
mg/L
0.1000
56
19-119
Surrogate: Nitrobenzene-d5
0,0368
mg/L
0.05000
74
44-120
Surrogate: Phenol-d5
0.0358
mg/L
0.1000
36
11-52
!e: Terphenyl-d14
0.0431
mg/L
0.05000
86
50-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 21

%Q Full -Service Analytical s
' I Environmental Solutions
�fL BORATORIE$ INC.
Level II QC Report
11/2/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP
Al n Galloway Short List
P. ( 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Prism Work Order: 8100342
Time Submitted: 10/17/2018 4:15:OOPM
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P8J0478 - 351 OC GC
Blank (P8J0478-BLK1)
Prepared: 10/25/18 Analyzed: 10/26/18
Chlordane
BRL
0.0025
mg/L
Dieldrin
BRL
0.00050
mg/L
Endrin
BRL
0.00050
mg/L
gamma-BHC
BRL
0.00050
mg/L
Heptachlor
BRL
0.00050
mg/L
Heptachlor Epoxide
BRL
0.00050
mg/L
Methoxychlor
BRL
0.00050
mg/L
Toxaphene
BRL
0.025
mg/L
Surrogate: Decachlorobiphenyl
0.00127
mg/L
0.001000 127 13-186
Surrogate: Tetrachloro-m-xylene
0.000837
mg/L
0.001000 84 40-134
LCS (P8J0478-1331)
Prepared: 10/25/18 Analyzed: 10/26/18
Dieldrin
0.000828
0.00050
mg/L
0.001000 83 69-130
Endrin
0.000892
0.00050
mg/L
0.001000 89 69-144
gamma-BHC
0.000895
0.00050
mg/L
0.001000 89 66-129
Heptachlor
0.000863
0.00050
mg/L
0.001000 86 61-136
HPntnrhlor Epoxide
0.000836
0.00050
mg/L
0.001000 84 69-131
P chlor
0.000865
0.00050
mg/L
0.001000 87 70-157
�_.._,__`e: Decachlorobiphenyl
0.00121
mg/L
0.001000 121 13-186
Surrogate: Tetrachloro-m-xylene
0.000801
mg/L
0.001000 80 40-134
LCS (P8J0478-BS2)
Prepared: 10/25/18 Analyzed: 10/26/18
Chlordane
0.00717
0.0025
mg/L
0.01000 72 50-160
Surrogate: Decachlorobiphenyl
0.000672
mg1L
0.001000 67 13-186
Surrogate: Tetrachloro-m-xylene
0.000728
mg/L
0.001000 73 40-134
LCS (P8J0478-BS3)
Prepared: 10/25/18 Analyzed: 10/26/18
Toxaphene
0.0106
0.025
mg/L
0.01000 106 50-150
Surrogate: Decachlorobiphenyl
0.000797
mg/L
0.001000 80 13-186
Surrogate: Tetrachloro-m-xylene
0.000854
mg/L
0.001000 85 40-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-8001629-6364 - Fax: [phone]
Page 7 of 21

Full Service Analytical ISM Environmental Solutions
^_1�80B TORIES, INC.
Level II QC Report
11 /2/18
City of Statesville, NC Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
At n Galloway Short List Time Submitted: 10/17/2018 4:15:OOPM
P., c 1111
Statesville, NC 28687
TCLP Organochlorine Pesticides by GC/ECD - Quality Control
Reporting
Spike Source
%REC
RPD
Analyte
Result
Limit
Units
Level Result
%REC
Limits
RPD
Limit Notes
Batch P8J0478 - 3510C GC
LCS Dup (P8J0478-BSD1)
Prepared: 10/25/18
Analyzed:
10/26/18
Dieldrin
0.000864
0.00050
mg/L
0.001000
86
69-130
4
20
Endrin
0.000940
0.00050
mg/L
0.001000
94
69-144
5
20
gamma-BHC
0.000928
0.00050
mg/L
0.001000
93
66-129
4
20
Heptachlor
0.000899
0.00050
mg/L
0.001000
90
61-136
4
20
Heptachlor Epoxide
0.000862
0.00050
mg/L
0.001000
86
69-131
3
20
Methoxychlor
0.000959
0.00050
mg/L
0.001000
96
70-157
10
20
Surrogate: Decachlorobiphenyl
0.000937
mg/L
0.001000
94
13-186
Surrogate: Tetrachloro-m-xylene
0.000838
mg/L
0.001000
84
40-134
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 8 of 21

Level II QC Report
I
A
Full -Service Analytical&
11/2/18
:1-
Environmental Solutions
�`7LASORATORIES, ING
City of Statesville, NC
Project: 3rd and 4th Creek Sludge TCLP Prism Work Order: 8100342
Al n Galloway
Short List
Time Submitted: 10/17/2018 4:15:OOPM
P. K 1111
Statesville, NC 28687
TCLP Extraction by EPA 1311 - Quality Control
Reporting Spike Source %REC RPD
Analyte
Result
Limit Units Level Result %REC Limits RPD Limit Notes
Batch P8J0412 -1311
Blank (P8J0412-BLK1)
Prepared: 10/22/18 Analyzed: 10/23/18
TCLP Extraction
Complete
N/A
Sample Extraction Data
Prep Method: 1311
Lab Number
Batch Initial
Final Date/Time
8100342-01
P8J0412 100 g
2000 mL 10/22/18 15:50
8100342-02
P8J0412 100 g
2000 mL 10/22/18 15:50
Prep Method: 3510C GC
Lab Number
Batch Initial
Final Date/Time
8100342-01
P8J0478 200 mL
10 mL 10/25/18 9:00
8100342-02
P8J0478 200 mL
10 mL 10/25/18 12:45
F I thod: 3510C MS
Lau Dumber
Batch Initial
Final Date/Time
8100342-01
P8J0443 200 mL
1 mL 10/24/18 9:10
8100342-02
P8J0443 200 mL
1 mL 10/24/18 9:10
Subcontracted Analyses
The following analyses
were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
8100342-01
Herbicides TCLP (Sub)
8100342-02
Herbicides TCLP (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] -Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 21

Full -Service Analytical &
Ri � ems' M1
Environmental Solutions
LABORATORIES,INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Fax: [phone]
Client Company Name:
Report To/Contact Name:
Reporting Address:
%C�PHABN OF CUSTODY RECORD
PAGE__ OF QUOTE # TO ENt OPER BILLING:
Project Name:
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
Please ATTACH any project specific reporting (QC LEVEL 1 II 111 IV)
provisions and/or QC Requirements
Invoice To:
Address:
NO N/A
Samples INTACT upon anival?
Received ON WET ICE?
PROPER PRESERVATIVESindicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
r VOLATILES rec'd W/dUT HEADSPACE?
PROPER CONTAINERS used?
TEMP; Therm ID:Ai- 5 Observed: 3. + - °C / Con: °C
Phone: Fax (Yes) (No):
Purchase Order NoJElilling Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address:
Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
EDD Type: PDF Excel Other
"Working Days" ❑ 6-9 Days ❑Standard 10 days CI�2ush Work Must Be
Pre Approved
Site Location Name:
Samples received after 14:00 will be processed next business day.
SC OTHER N/A
Site Location Physical Address:
Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES_ NO
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-t
.� I ANALYSIS LREQUESTED
` r
PRISM
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER
TIVES
- %� REMARKS
o� @ J
yVvz� , V �
LAB
`TYPE
HOURS
SLUDGE)
E)
SEE BELOW
NO.
SIZE
BLS
,�� R // `/
ID NO.
VA Carr4 Sla a
10-17-1
T: `1.5
S
G
NONE
✓
J
J
Tr- t P Tes It
b I
I
3,21Care k Sita t!
10-17-19 1
Oq;0 0
S
G-
t�orlE
I
J
bZ�
I
1
I
1
I
Sampler's
2
Signature
Sampled By (Print Name) V GU vrj c� Affiliation
Upon relinquishing, this Chain of Custody is your authorization
for Prism to proceed with the analyses as requested above. Any changes must be
©'
submitted in writing to the Prism Project Manager,
There will be chagrg any changes after analyses have been initialized.
R Jliyngpishad By; IS ufe)� 6
ReGQRad By: (Si natula) Di/le- titary/,Hyurs Additional Comments: Site Anivat Time:
Reel shed By: (Signature)
Raoelved t? : (Slgriature) Date I Site Departure Time:
lul8hed y: (�ature)
44bceived For Prism LaboralonDatey / 1 Field Tech Fee:
�
'! Mileage;
(Q A of Shipme�OTE: ALL,59IVIPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY SEALS FOR TRANS ORTATION TO THE LABO ORY. COG Group No.
(D SA ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LAe RATORY. !,
CD J F*c.-_;•LP Field Service
and-dellvnred P"Sm
❑ Other
DRINK
SOLIDWASTLANDFILL❑
1❑
I C ❑ SC ❑❑ NC ❑ SC El NC ❑ SC
to
CI
CI NC SC El
El NC ❑ SCE ❑ NC ❑ SC ❑ NC ElSC ❑ NC SC ❑ NC ❑ SC
❑ ❑ ❑ ❑ ❑ ❑
NTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastirr TI = Tpflnn-I it i Can VOA = Vnlatilp Ornanice Anolveie 17arn Hnnii Cnnnpl

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
8100342
Cl
LABORATORY REPORT NUMBER
218101921
DATE
10/31 /2018
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory# 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 218101921 Pa e 1 of 11
Page 11 of 21

It
LELAP CERTIFICATE NUMBER: 01955
GC,&L DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL LABORATORIES, LLC
PERFORMED BY
GCAL, LLC
7979Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 10/31/2018
GCNL Repor[2V18301921
Project 8100342
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
�Q3�cceFaf.�
1 S�
• 0
IA
tr �
Tesung
Lab Report#: 218101921 Pace 2 of
Page 12 of 21

Report#: 218101921
Project ID: 8100342 Report Date: 10/31/2018
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAl2s Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
" Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
GCAL Report 218101921
Lab Report#: 218101921
Page 13 of 21

Report#: 218101921
Project ID: 8100342
Certifications
Report Date: 10/31/2018
Certification
Certification Number
DOD ELAP
L16-398-R5
Alabama
01955
Arkansas
18-062-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
NIA
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 218101921
Paae 4 0
Page 14 of 21

Report#: 218101921
— - Project -ID: 8100342--"` Report -Date: "10/3172018'--
1 ANAIY'MAL LABORATORIES, LIX
r
Case Narrative
Client: Access Analytical Report: 218101921
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Lab Report#: 218101921
Page 15 of 21

C",(SCAL
&f nx cLl IWWIfn11.E3. LI
Report#: 218101921
Project ID: 8100342
Sample Summary
Report Date: 10/31/2018
GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time
21810192101 4th Creek Sludge Solid 10/17/2018 08:45 10/19/2018 09:35
21810192102 3rd Creek Sludge Solid 10/17/2018 09:00 10/19/2018 09:35
Lab Report#: 218101921 Page 6 of 11
Page 16 of 21

Report#; 218101921 —
® a ai,.+�ci, innaRs:est�q,�ac Project ID: 8100342'- "" Report Date: 1073112018
Summary of Compounds Detected
No analytes were detected for analyses performed by GCAL.
Lab Report#: 218101921
Page 17 of 21

Report#: 218101921
Project ID: 8100342 Report Date: 10/31/2018
l
Sample Results
Collect Date 10/17/2018 08:45 GCAL ID 21810192101
4th Creek Sludge ��E. ..,.: ...-:
Recelve Date 10/19/2018 09:35 Matrix Solid
EPA 1311/8151A
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
10/24/2018 11:00 646481 EPA 1311/8151A 1 10/30/2018 16:55 MFS 646954
CAS#
Parameter
Result DL
LOQ
Reg Limit
Units
94-75-7
2,4'-D
0.001000 0.00100
0.00500
10
mg/L
93-72-1
2,4,5-TP (Silvex)
0.00100U 0.00100
0.00500
1
mg/L
CAS#
Surrogate
Conc. Spiked Conc. Rec
Units
% Recovery
Rec Limits
19719-28-9
DCAA
0.02 .00737
mglL
37
18 - 136
Collect Date 10/17/2018 09:00 GCAL ID 21810192102
3rd Creek Sludge Receive Date 10/19/2018 09:35 Matrix Solid
EPA 131118151A
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
10/24/2018 11:00 646481 EPA 131118151A 1 10/30/2018 17:35 MFS 646954
CAS#
Parameter
Result DL
LOQ
Reg Limit
Units
94-75-7
2,4'-D
0.001000 0.00100
0.00500
10
mg/L
93-72-1
2,4,5-TP (Silvex)
0.001000 0.00100
0.00500
1
mg/L
CAS#
Surrogate
Conc. Spiked Conc. Rec
Units
% Recovery
Rec Limits
19719-28-9
DCAA
0.02 .0133
mg/L
67
18 - 136
Lab Report#: 218101921
Pa e 8 of 11
Page 18 of 21

��Report#: 218101921
t�z L, f lrRl l/. •d86/M'z�i�\6FCLP.3. LRL PropUt ID: 8100342
GC Semi-Volatiles QC Summary
R-®port Date: IW1/2018 -
'Aiiafytical Batch
Client ID'
MBfi4&48i,.
LC8646481 „
LCSD645481t
M664
GCAL'ID
186119d
1861131'
-:
LGSD:_;: -
Piop'Batch •.,
Sample Type'
MB ::
L'CS . ' .•; • : •, '
:=_
646481
Prep Date
10124/20;1811 00, �
10124/2018'1Ii00,'
10/241207811 )0
Prap Method
Analysis Date
10/25/20-18 22:41. _
90125/2018 23aO' `
:,`:
10125120I8_23 22: • t r'`
' '
Mai4
Water. _:- . =: ': _
V+laEe`r.:.. ,..:,: _:• ~''-
Wafer...,.=r•
,
- EPA 9 311181.59 A
ResuUnitll
mg L
Addike
Resuh
%R
Limas � l
:A d`e0
- Resuh
M
RPD
RmD
2,4'-D
94-75-7
0.001000
0.00100
0.00099
0.00075
75
45 - 152
0.00099
0.00079
80
5
30
2,4,5-TP (Slivex)
93-72-1
rv9719-28-9
b.b0100U
0.00100
0.00100
0.00074
74
51 -134
0.00100
0.00076
75
1
30
Surrogate
DCAA
.00112
56
.002
.00127
64
18 - 136
.002
.0013
65
NA
NA
Lab Report#: 218101921 Pa0e 9 of 11
Page 19 of 21

P�
Full -Service Analytical 8
"VM I 6vironmentat Solutions
€a�iaLfztirr*EMttit
SO1DCON7'RAe, .�........
Prism Lhboeatorles, Inc.
8100342
SENDING LARO"RATORYt RECEIVING LABORATORY';
Prism Laboratories, Inc: Gulf Coast Analytical: Labs, Itic_
P: O. B'ox240543 10781 Coursey Blvd
Charlotte, NC 28224,0543 Baton Rouge, LA 70816
Phone: [phone] Phone :[phone]
Pax,704-525-0409 rax: [phone]
Froject Manager, l2gbb A_ Jtgies
Analysis L)ne rk Laboratory lD 111 lent
Cell if eaddtt: ELAC MACC____ i
Ne+ Sc Otlter�
N/A If
9am�lc 1p: 81110333=111;.. Solltf SAmpic'dp D/1,.118118t4SG-itl, ,':�.� °Ur4
}ivUicidesiCiP,(Sub) 2,4-Dand2,4,3 j'P lre'L.P
Ca'ntq! ters'Snpplled• ' � ;
Sntiiple,I,A: 8i00:ti2-0
-
:Solid I
-
_
I fc- b0ddcs TCLP (sub)
;r'
_ _
' ; - i Q?24%1 B Q9eDD
-- •. _ :
_
2,4-Ib and 2,4,5 TP
7LP
:onr;alnerS,Supplied;
•t
l�
a
a
ltetc�srd 13j !:
pale `
ft&eived I3s'
Dite
v
ttdaisi i! I3y ' '
Received By
Ua-- -
h
- r
RelLa3ed'11y
Date
ReccNed By
Dala
�
Rvwhs111 Ily
l)ite
Rcceircd 13y'
Date
Page I d
1
Page 20 of 21

w
m
N
O_
N
SAMPLE RECEIVING CHECKLIST
SAMPLE DELJVERX GROUP
. 218101921
-CHECIdIST
YES
N
_
Client PM AEr-
Transport Method
Samples received with proper thermal preservation?
j
®
El_
4565 - Access Analytical
FIDIX
— —
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
I
FR
0
❑
❑
Profile umber
Received W
80251
Savage, Tiffany R
----
All containers received in good condition and within hold time?
All sample labels and containers receieed match the chain of custody?
0 i
�/❑
❑
❑
Line ltem(s)
Receive Date(s)
4 - Solid
10/19/18
" — —
Presenvati.e to
❑
added any containers?
If recei\ed, was headspace for VOC water containers < 6mm?
®
❑
Samples collected in containers prWded by GCAL? f
❑
COOLERS
DISCREPANCIES
'L-AB°PRESERVATIONS
Airbill Thermometer ID: E29
Temp °C
Nbne
None
7735-1386-5980
1.5
NOTES
Fbvision 1.6
Lab Report#:218101921
Page 1 of 1
Page 11 of 11

` NC Certification No. 402 Case Narrative
Full -Service Analytical & NC Drinking Water Cert No. 37735 09/26/2018
P__, R 11C, M I Environmental Solutions SC Certification No. 99012
LABORA10RIES, INC.
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Andy Smith
Project No.: 3rd Creek/4th Creek/StaLime
P.O. Box 1111
Lab Submittal Date: 09/10/2018
Statesville, NC 28687
Prism Work Order: 8090113
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Reactivity and flashpoint analyses were subcontracted to Gulf Coast Analytical Labs. Laboratory report is
attached.
TCLP 8151 analyses were subcontracted to Analytical Environmental Services. Laboratory report is
attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Angela D. Overcash For Robbi A. Jones
VP Laboratory Services
A Pass
D RPD value outside of the control limits.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
BRL Below Reporting Limit
MDL Method Detection Limit
Relative Percent Difference
Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/629-6364 - Fax: [phone] Page 1 of 30

1 www
, l I S Full -Service al Solutions
s
Environmental Solutions
E�-^_�-✓LABORATORIES INC
Cli--* Sample ID
le
4th Creek
3rd Creek
Sample Receipt Summary
09/26/2018
Prism Work Order: 8090113
Lab Sample ID Matrix Date/Time Sampled Date/Time Received
8090113-01
Solid
09/10/18
8:20
09/10/18 13:15
8090113-02
Solid
09/10/18
8:03
09/10/18 13:15
8090113-03
Solid
09/10/18
8:15
09/10/18 13:15
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 2 of 30

KIFull -Service Analytical &
i=R Environmental Solutions
�ABOR INC.
Laboratory Report
09/26/2018
Citv of Statesville, NC
/ ndy Smith
I ox 1111
Statesville, NC 28687
Project: Sludge (Hazardous Testing)
Project No.: 3rd Creek/4th Creek/Stal-ime
Sample Matrix: Solid
Client Sample ID: StaLime
Prism Sample ID: 8090113-01
Prism Work Order: 8090113
Time Collected: 09/10/18 08:20
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
95.3
% by 0.100
0.100 1
*SM2540 G
9/12/18 15:40
SLS
P810152
Weight
Corrosivity-pH
13
pH Units
1
*9045D
9114/18 16:09
CBP
P810221
Ignitability
BRLA
mmisec 0.10
1
*1030
9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1
*1311
9/13/18 7:20
MMR
P810153
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9/13118 14:04
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*601OD
9/13/18 17:53
JAB
P810157
Barium
BRL
mg/L
5.0
0.0040
1
*6010D
9/13118 17:53
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*6010D
9113118 17:53
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9113/18 17:53
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9/13/18 17:53
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*601OD
9/13/18 17:53
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*6010D
9/13/18 17:53
JAB
P810157
Organochlorine Pesticides
by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081B
9/20/18 17:08
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081 B
9/20/18 17:08
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081 B
9/20118 17:08
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081 B
9/20/18 17:08
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081B
9/20/18 17:08
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20/18 17:08
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081B
9/20/18 17:08
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081B
9/20/18 17:08
JMC
P810235
Surrogate
Recovery
Control Limits
Decachlorobiphenyl
81 %
13-186
Tetrachloro-m-xylene
59 %
40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9/17/18 17:41
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 17:41
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 17:41
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9117/18 17:41
JMV
P810203
3/4-Methyl phenol
BRL
mg/L
0.050
0.0015
1
*8270D
9/17/18 17:41
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17/18 17:41
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9117/18 17:41
JMV
P810203
Hexachioroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 17:41
JMV
P810203
:nzene
BRL
mg/L
0.050
0.0026
1
*8270D
9/17118 17:41
JMV
P810203
hlorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 17:41
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 Of 30

1 � Full -Service Analytical & Laboratory Report
/_V � f Environmental Solutions 09/26/2018
LABORATORIES. ING
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: StaLime
P idy Smith Prism Sample ID: 8090113-01
F )x 1111 Project No.: 3rd Creek/4th Creek/Stal-ime Prism Work Order: 8090113
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/10/18 08:20
Time Submitted: 09/10/18 13:15
Parameter
Result
Units
Report MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Pyridine
BRL
mg/L
0.25 0.0010
1
*8270D
9/17/18
17:41
JMV
P810203
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
77 %
43-140
2-Fluorobiphenyl
88 %
44-119
2-Fluorophenol
37 %
19-119
Nitrobenzene-d5
84 %
44-120
Phenol-d5
28 %
11-52
Terphenyl-d14
93 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1
*8260B
9/22/18
2:50
KDM
P810322
1,2-Dichloroethane
BRL
mg/L
0.025 0.00066
1
*8260B
9/22/18
2:50
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1
*8260B
9/22/18
2:50
KDM
P810322
Benzene
BRL
mg/L
0.025 0.00048
1
*8260B
9/22/18
2:50
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1
*8260B
9/22/18
2:50
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1
*8260B
9122118
2:50
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1
*8260B
9/22/18
2:50
KDM
P810322
thy[ Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1
*8260B
9/22/18
2:50
KDM
P810322
l xoethy[ene
BRL
mg/L
0.035 0.00098
1
*8260B
9122118
2:50
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1
*8260B
9/22/18
2:50
KDM
P810322
Vinyl chloride
BRL
mg/L
0.020 0.00097
1
*8260B
9122/18
2:50
KDM
P810322
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
80-124
Dibromofluoromethane
77 %
75-129
Toluene-d8
100 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 30

L-0RISM
�.-'�v LABORATORIES INa
Full -Service Analytical &
Environmental Solutions
Laboratory Report
09/26/2018
City of Statesville, NC Project: Sludge (Hazardous Testing) Client Sample ID: 4th Creek
/ ndy Smith Prism Sample ID: 8090113-02
F ox 1111 Project No.: 3rd Creek/4th Creek/Stal-ime Prism Work Order: 8090113
Statesville, NC 28687 Sample Matrix: Solid Time Collected: 09/10/18 08:03
Time Submitted: 09/10/18 13:15
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
% Solids
15.2
% by
0.100
0.100
1
*SM2540 G
9112/18 15:40
SLS
P810152
Weight
Corrosivity-pH
8.8
pH Units
1
*9045D
9/14/18 16:09
CBP
P810221
Ignitability
BRLA
mm/sec
0.10
1
*1030
9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
NIA
1
*1311
9/13/18 7:20
MMR
P810153
TCLP Extraction
Complete
N/A
1
*1311 ZHE
9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9/13/18 14:15
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*6010D
9/13/18 18:16
JAB
P810157
Barium
BRL
mg/L
5.0
0.0040
1
*6010D
9/13/18 18:16
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*601OD
9/13/18 18:16
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9/13/18 18:16
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9113/18 18:16
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*601OD
9/13/18 18:16
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*601OD
9/13/18 18:16
JAB
P810157
Organochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081B
9/20/18 17:20
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081B
9/20/18 17:20
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081 B
9/20/18 17:20
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20118 17:20
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081B
9/20/18 17:20
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20/18 17:20
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081 B
9/20/18 17:20
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081 B
9/20/18 17:20
JMC
P810235
TCLP Semlvolatile Organic Compounds by GC/MS
Surrogate
Decachlorobiphenyl
Tetrachloro-m-xylene
Recovery
78 %
58 %
Control Limits
13-186
40-134
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9/17/18 18:04
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 18:04
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 18:04
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9/17/18 18:04
JMV
P810203
3/4-Methylphenol
3.8
mg/L
0.50
0.015
10
*8270D
9/18118 10:14
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17/18 18:04
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9/17/18 18:04
JMV
P810203
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 18:04
JMV
P810203
-- •:mzene
BRL
mg/L
0.050
0.0026
1
*8270D
9/17/18 18:04
JMV
P810203
:hlorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 18:04
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 30

Full -Service Analytical &
I S M Environmental Solutions
EUOR TOFIES, ING
Laboratory Report
09/26/2018
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 4th Creek
ndy Smith
Prism Sample ID: 8090113-02
F 3x 1111
Project No.: 3rd Creek/4th Creek/StaLime
Prism Work Order: 8090113
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/10/18 08:03
Time Submitted: 09/10/18 13:15
Parameter
Result Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Pyridine
BRL
mg/L
0.25 0.0010
1 *8270D 9/17/18 18:04
JMV
P810203
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
76 %
43-140
2-Fluorobiphenyl
82 %
44-119
2-Fluorophenol
45 %
19-119
Nitrobenzene-d5
79 %
44-120
Phenol-d5
33 %
11-52
Terphenyl-d14
88 %
50-134
TCLP Volatile Organic Compounds by GUMS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1 *8260B 9/22/18 3:16
KDM
P810322
1,2-Dichloroethane
BRL
mg/L
0.025 0.00066
1 *8260B 9/22/18 3:16
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1 *8260B 9/22/18 3:16
KDM
P810322
Benzene
BRL
mg/L
0.025 0.00048
1 *826013 9/22/18 3:16
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1 *82606 9/22/18 3:16
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1 *8260B 9/22/18 3:16
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1 *8260B 9/22/18 3:16
KDM
P810322
P :thy] Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1 *8260B 9/22/18 3:16
KDM
P810322
Droethylene
BRL
mg/L
0.035 0.00098
1 *8260B 9/22118 3:16
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1 *8260B 9/22/18 3:16
KDM
P810322
Vinyl chloride
BRL
mg/L
0.020 0.00097
1 *8260B 9/22/18 3:16
KDM
P810322
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
99 %
75-129
Toluene-d8
100 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 30

.-J0--R ISM FunService Analytical
j Environmental Solutions
^7LABORATORIE$ INC.
Laboratory Report
09/26/2018
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 3rd Creek
%ndy Smith
Prism Sample ID: 8090113-03
3ox 1111
Project NO.: 3rd Creek/4th Creek/Stal_ime
Prism Work Order: 8090113
Statesville, NC 28687
Sample Matrix: Solid
Time Collected: 09/10/18 08:15
Time Submitted: 09/10/18 13:15
Parameter
Result
Units Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
General Chemistry Parameters
% Solids
17.1
% by 0.100 0.100
1 *SM2540 IS 9/14/18 9:45
TJY
P810191
Weight
Corrosivity-pH
6.7
pH Units
1 *9045D 9/14/18 16:09
CBP
13810221
Ignitability
BRLA mm/sec 0.10
1 *1030 9/20/18 13:14
BMS
P810286
TCLP Extraction by EPA 1311
TCLP Extraction
Complete
N/A
1 *1311 9113/18 7:20
MMR
P810153
TCLP Extraction
Complete
N/A
1 *1311 ZHE 9/21/18 15:10
KDM
P810314
TCLP Metals
Mercury
BRL
mg/L
0.010
0.000030
1
*7470A
9/13/18 14:19
MMR
P810159
Arsenic
BRL
mg/L
0.10
0.016
1
*601OD
9/13/18 18:25
JAB
P8I0157
Barium
BRL
mg/L
5.0
0.0040
1
*6010D
9/13/18 18:25
JAB
P810157
Cadmium
BRL
mg/L
0.025
0.00075
1
*6010D
9/13/18 18:25
JAB
P810157
Chromium
BRL
mg/L
0.25
0.0018
1
*6010D
9/13/18 18:25
JAB
P810157
Lead
BRL
mg/L
0.050
0.0040
1
*6010D
9/13/18 18:25
JAB
P810157
Selenium
BRL
mg/L
0.10
0.028
1
*6010D
9/13/18 18:25
JAB
P810157
BRL
mg/L
0.25
0.0020
1
*6010D
9/13/18 18:25
JAB
P810157
_-_ Drganochlorine Pesticides by GC/ECD
Chlordane
BRL
mg/L
0.0025
0.00086
1
*8081 B
9/20/18 17:32
JMC
P810235
Dieldrin
BRL
mg/L
0.00050
0.000070
1
*8081 B
9120/18 17:32
JMC
P810235
Endrin
BRL
mg/L
0.00050
0.000075
1
*8081 B
9/20118 17:32
JMC
P810235
gamma-BHC
BRL
mg/L
0.00050
0.000065
1
*8081B
9/20/18 17:32
JMC
P810235
Heptachlor
BRL
mg/L
0.00050
0.000085
1
*8081B
9/20/18 17:32
JMC
P810235
Heptachlor Epoxide
BRL
mg/L
0.00050
0.000065
1
*80816
9/20/18 17:32
JMC
P810235
Methoxychlor
BRL
mg/L
0.00050
0.00020
1
*8081B
9/20/18 17:32
JMC
P810235
Toxaphene
BRL
mg/L
0.025
0.00037
1
*8081B
9/20/18 17:32
JMC
P810235
Surrogate Recovery Control Limits
Decachlorobiphenyl 84 % 13-186
Tetrachloro-m-xylene 74 % 40-134
TCLP Semivolatile Organic Compounds by GC/MS
2,4,5-Trichlorophenol
BRL
mg/L
0.25
0.0016
1
*8270D
9/17118 18:26
JMV
P810203
2,4,6-Trichlorophenol
BRL
mg/L
0.10
0.0018
1
*8270D
9/17/18 18:26
JMV
P810203
2,4-Dinitrotoluene
BRL
mg/L
0.050
0.0014
1
*8270D
9/17/18 18:26
JMV
P810203
2-Methylphenol
BRL
mg/L
0.050
0.0018
1
*8270D
9/17/18 18:26
JMV
P810203
3/4-Methyl phenol
BRL
mg/L
0.050
0.0015
1
*8270D
9/17/18 18:26
JMV
P810203
Hexachlorobenzene
BRL
mg/L
0.050
0.0013
1
*8270D
9/17118 18:26
JMV
P810203
Hexachlorobutadiene
BRL
mg/L
0.050
0.0021
1
*8270D
9/17/18 18:26
JMV
P810203
Hexachloroethane
BRL
mg/L
0.050
0.0017
1
*8270D
9/17/18 18:26
JMV
P810203
I" Izene
BRL
mg/L
0.050
0.0026
1
*8270D
9117/18 18:26
JMV
P810203
I' dorophenol
BRL
mg/L
0.25
0.0012
1
*8270D
9/17/18 18:26
JMV
P810203
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 30

�P_ R I S, !7 Y I Fun -Service Analytical s
- Environmental Solutions
O!V�LAeOPATORIES ING
Laboratory Report
09/26/2018
City of Statesville, NC
Project: Sludge (Hazardous Testing)
Client Sample ID: 3rd Creek
%ndy Smith
Prism Sample ID: 8090113-03
3ox 1111
Project No.:
3rd Creek/4th Creek/Stal-ime
Prism Work Order: 8090113
Statesville, NC 28687
Sample Matrix:
Solid
Time Collected: 09/10/18 08:15
Time Submitted: 09/10/18 13:15
Parameter
Result
Units
Report MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Pyridine
BRL
mg/L
0.25 0.0010
1 *8270D 9/17/18 18:26
JMV
P810203
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
101 %
43-140
2-Fluorobiphenyl
99 %
44-119
2-Fluorophenol
65 %
19-119
Nitrobenzene-d5
93 %
44-120
Phenol-d5
41 %
11-52
Terphenyl-d14
96 %
50-134
TCLP Volatile Organic Compounds by GC/MS
1,1-Dichloroethylene
BRL
mg/L
0.035 0.00083
1 *8260B 9/22/18 3:42
KDM
P810322
1,2-Dichlorcethane
BRL
mg/L
0.025 0.00066
1 *8260B 9/22/18 3:42
KDM
P810322
1,4-Dichlorobenzene
BRL
mg/L
0.38 0.00050
1 *8260B 9122/18 3:42
KDM
P810322
Benzene
BRL
mg/L
0.026 0.00048
1 *8260B 9/22/18 3:42
KDM
P810322
Carbon Tetrachloride
BRL
mg/L
0.025 0.0011
1 *8260B 9/22/18 3:42
KDM
P810322
Chlorobenzene
BRL
mg/L
5.0 0.00062
1 *8260B 9122/18 3:42
KDM
P810322
Chloroform
BRL
mg/L
0.30 0.00076
1 *8260B 9/22/18 3:42
KDM
P810322
P" ' 7thyl Ketone (2-Butanone)
BRL
mg/L
10 0.0024
1 *8260B 9/22/18 3:42 ,
KDM
P810322
�Droethylene
BRL
mg/L
0.035 0.00098
1 *8260B 9/22/18 3:42
KDM
P810322
Trichloroethylene
BRL
mg/L
0.025 0.00078
1 *8260B 9/22/18 3:42
KDM
P810322
Vinyl chloride
BRL
mg1L
0.020 0.00097
1 *8260B 9/22/18 3:42
KDM
P810322
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
98 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]
Page 8 of 30

Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
80 )1 P810152
30 g
30 g
09/12/18 15:40
80.,,,,,.,-J2 P810152
30 g
30 g
09/12/18 15:40
8090113-03 P810191
30 g
30 g
09/14/18 9:45
Prep Method: 1311
Lab Number Batch
Initial
Final
Date/Time
8090113-01
P810153
100
g 2000 mL
09/12/18 14:25
8090113-01
P810314
12.5
g 250 mL
09/20/18 16:30
8090113-02
P810153
100
g 2000 mL
09/12/18 14:25
8090113-02
P810314
12.5
g 250 mL
09/20/18 16:30
8090113-03
P810314
12.5
g 250 mL
09/20/18 16:30
8090113-03
P810153
100
g 2000 mL
09/12/18 14:25
Prep Method: 3010A
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810157
10 mL
50 mL
09/13/18 10:10
8090113-02
P810157
10 mL
50 mL
09/13/18 10:10
8090113-03
P810157
10 mL
50 mL
09/13/18 10:10
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810159
20
mL
30 mL
09/13/18 10:00
8090113-02
P810159
20
mL
30 mL
09/13/18 10:00
8090113-03
P810159
20
mL
30 mL
09/13/18 10:00
F 'thod: 3510C GC
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810235
200
mL
10 mL
09/18/18 9:30
8090113-02
P810235
200
mL
10 mL
09/18/18 9:30
8090113-03
P810235
200
mL
10 mL
09/18/18 13:16
Prep Method: 3510C MS
Lab Number
Batch
Initial
Final
Date/Time
8090113-01
P810203
200
mL
1 mL
09/17/18 9:06
8090113-02
P810203
200
mL
1 mL
09/17/18 9:06
8090113-02
P810203
200
mL
1 mL
09/17/18 9:06
8090113-03
P810203
200
mL
1 mL
09/17/18 9:06
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
8090113-01 P810322 1 mL 10 mL 09/21/18 15:57
8090113-02 P810322 1 mL 10 mL 09/21/18 15:57
8090113-03 P810322 1 mL 10 mL 09/21/18 15:57
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone] Page 9 of 30

Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number
Analysis
W Herbicides TCLP (Sub)
80! Herbicides TCLP (Sub)
8090113-03 Herbicides TCLP (Sub)
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number
Analysis
8090113-01
Reactivity, Cyanide (Sub)
8090113-01
Reactivity, Sulfide (Sub)
8090113-02
Reactivity, Cyanide (Sub)
8090113-02
Reactivity, Sulfide (Sub)
8090113-03
Reactivity, Cyanide (Sub)
8090113-03
Reactivity, Sulfide (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 30

�Ir9d
IP[-,.Full-Service
i 'Ji ➢
s
Analytical &
I Environmental Solutions
1A8OPATORIEB, INC.
449 Springbrook Road • Charlotte, NC 28217
Phone [phone] • Fax: [phone] f
Client Company Name: C: �V a-P 5�4,rSv+ J(e
Report To/Contact Name:
Cr14 1110WA ae
Reporting Address:
PAGE OF QUOTE TO ENSURE PROPERBILL NGII:
Project Name�fA • �h �+] c !��'l' ' ✓'
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
Invoice To:
Address:
Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES indicated?
Received WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
TEMP: Therm 1D,`'1, j Observe
YES, NO NIA O
cY)
T
-- CZ
v IL
°C I Corr. °C
Phone:70Y- 87$ 343$ Fax es (No):70y-878-USS purchase Order No./Billing Reference
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Email Address: Requested Due Date ❑ 1 Day ❑ 2 Days ❑ 3 Days ❑ 4 Days ❑ 5 Days
Certification: NELAC DOD FL NC
V Mdust Be
EDD Type: PDF Excel Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days ❑ Rushh Work
Pre-ASite
OTHER N/A
Location Name: Fv IA Q•� Bt C Rg Lr k Samples received after 14:00 will be processed next business day. Site
Site Location Physical Address: 693 BOP F4raM Turnaround time is based on business days, excluding weekends and holidays.
Water Chlorinated: YES_ NO_
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
Sample Iced Upon Collection: YES NO_
p p
CLIENT
DATE
TIME
COLLECTED
MATRIX
(SOIL,
SAMPLE CONTAINER
PRESERVA-
ANALYSIS REQUESTED
J J
'
PRISM
LAB
�� J REMARKS
r
SAMPLE DESCRIPTION
COLLECTED
MILITARY
HOURS
WATER OR
SLUDGE)
'TYPE
BELOW
NO.
SIZE
TIVES
J ° i�
1
ID NO.
SEE
SiRl�:w91C
9-10-ii�
_L& 1J,df MCP
01
C3,QI C�y2�Lt'g��
OZ
II
�r
t>�.V
T o
03
F� �
Y
REGlK LA IYJ
rC l(
P i_r
e
V.
d
`set"
03
a
I
I
I
ire:°
w�ed� A
I
A C
I
I
I
ll"�iY U� Affiliation
Sampler's Signature ; Sampled By (Print Name) R rC�
Upon relinquishing, this Chain of Custody is your authorization for Prism4o roceed with the analyses as requested above. Any changes must be a
submitted in writing to the Prism Project Manager. There will be charp6s for�ny changes after analyses have been initialized.
Rellnquishe By (Signatu Recei By: (Sign ture) Dale MiUtarylHours Additional Comments: Site Arrival Time:
Resin nod By: (Signatura) �rvAd By„(SI nature) Date Site Departure Time:
Relloqujsh jam/ (Sign pure) f Rt calve or P Laho Dr es By: Dat 1 Field Tech Fee:
hrrd of Shl ent: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT WITH CUSTODY. SEALS FOR TRANSPORTATIOif TO THE LABORATORY. COG Group No.
SAMPLES ARE NOTACCEPTED AND VERIFIED AGAINST CDC UNTIL RECEIVED AT THE LABORATORY. O n O
V
PUFed
Fir ❑ UPS d-delivered •Prism Field Service ❑ Other
1.
NPDES: Ut GR UNDWATER: DRINKING WATER: j SOLID WASTE: RCW CERCLA LANDFILL OTHER:
❑NC❑S 11 U'_ =SC I ❑S ❑SC ❑❑NC ❑SC ❑❑NC aNC ❑SC oNC ❑SC ❑❑NC ❑SC
LlNC oNC E`
4AAS•TA \IL�� T/�C f•Ar1GC. A - A-k-, r — rl r-'- r-h.c D = Phe+ir• TI = Toflnn-I inori Can vnA = Vnlatile Omsnir•.S Analysis (LerD meaci JDace)--It,Iwl A I

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Terri W. Cole
)PROJECT ID
8090113
LABORATORY REPORT NUMBER
1809871
DATE
September 21, 2018
Primary Data Review By Secondary Data Review By
;� '
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDI-IEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab 11 FL-E87582,
NELAP certified laboratory # E87582
AIIIA-LAP,LLC Laboratory I13:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page
Page 12 of 30

�r^ ,,
ice A
Full -Service Anal tical &
y
,;��
P1S I
Full-
Solutions
n�
Y. •.)�J.. ii rKi1� �i�LOnri-ardes i?lr
SUBCONTRACT ORDER
Certificatio: 'NELAC_ USACE
Prism Laboratories, Inc. NC 'SC Ullter
8090113 N/A
SENDING LARORATOXY•
RECEIVING LAI30RATORY:
Prism Laboratories, Inc.
Analytical Environmental Services, Inc.
P. O. Box 240543
3080 Presidential Parkway
Charlotte, NC 28224-0543
Atlanta, GA 30340
Phone: [phone]
Phone :[phone]
Fax: [phone]
Fax: NA
Project Manager: Robbi A.
Jones
Analysis
Due Expires Laboratory ID Comments
Sample ID: 8090113-01
Solid Sampl$d:09/10/1803:20 ( ime—
Herbicides TCLP (Sub)
09/17/18 08:20
Containers Supplied:
/
Sample ID: 8090113-02 Solid
Herbicides TCLP (Sub)
Containers Supplied:
Sampled:09/10/18 08:03
09/17/18 03:03
Sample ID: 3090113-03 Solid Samplcd:09/1011308:15
Al
Herbicidcs TCLP (Sub) 09/17/18 08:15
Containers SupplieeL•
11CICaSl::1 13\'
U Ac
4j
2
Relcasell 5V I):IIC
Ilceeiy d BY I L
Dmi. l
© �+ C
Nekmscd 13y Daw
RecciliUd 11%�
Released By Dale
Received 13y
Dale
Paoe I of I
i
Page
Page 13 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
Sta Lime
Lab Order
1809871
Tag Number:
8090113-01
Project Name:
8090113
Collection Date:
9/10/2018 8:20:00 AM
Lab ID:
1809871-OOIA
Matrix:
Solid
Analyses
Result
Qual MDL
ReportingUnits
Limit
l3atchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
ing/L 267209
1 09/18/2018 17:05 UH
2,4-D
BRL
0.051
0.20
ing/L 267209
1 09/181201817:05 UH
Surr: DCAA
79.5
0
50.4-133
%REC 267209
1 09/18/2018 17:05 UH
Quulifters: • Value exceeds maxintunt contaminant level
BRL Not Detected at MDL
H Holding limes for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quaniilation range
S Spike Recovery outside lintus due to matrix
> Greater than Result value
1 Estimated value detected below Reporting Until
< Less than Result value
Page R `
Page 14 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
4th Creek
Lab Order
1809871
Tag Number:
8090113-02
Project Name:
8090113
Collection Date:
9/10/2018 8:03:00 AM
Lab ID:
1809871-002A
Matrix:
Solid
Analyses
Result
Qual MDL
Reporting
Limit
Units BatchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mg/L 267209
1 09/18/2018 17:26 UH
2,4-D
BRL
0.051
0.20
Ing/L 267209
1 09/18/2018 17:26 UH
Surr: DCAA
80.9
0
50.4-133
a/oREC 267209
1 09/18/2018 17:26 UH
Qunlilicm: Value exceeds maximum contaminant level
BRL Not Detected at MDL
i H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyle detected in the associated method blank
E Estimated value above quanlitation range
S Sptkc Recovery outside limits due to matrix
> Greater than Result value
] Estimated value detected below Reporting Limit
(-=than Rc:ull valuo
Page I `
Page 15 of 30

Analytical Environmental Services, Inc
Date: 20-Sep-18
Client:
Prism Laboratories
Client Sample ID:
3rd Creek
Lab Order
1809871
Tag Number:
8090113-03
Project Name:
8090113
Collection Date:
9/10/2018 8:15:00 AM
Lab ID:
1809871-003A
Matrix:
Solid
Analyses
Result
Qua] MDL
Reporting
Limit
Units BatchID
DF Date Analyzed Analyst
HERBICIDES, TCLP SW1311/8151A
(SW3510C)
2,4,5-TP (Silvex)
BRL
0.030
0.20
mC/L 267209
1 09/18/2018 17:46 UH
2,4-D
BRL
0.051
0.20
mg/L 267209
1 09/181201817:46 UH
Surr: DCAA
84
0
50.4-133
%REC 267209
1 09/18/2018 17:46 UH
Qualifiers: • Value exceeds maximum contaminant level E Estimated vnlue above quantitation range
BRL Not Detected at MDL S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysis exceeded > Greater than Result value
N Analyle not NELAC cenified 1 Estimated value detected below Reporting Limit
B Analyie detected in the associated method blank - Less than Result value
Page Page 16 of 30

;.. Clear. = - ue as..
[� 1ALWICAI.
IiNVIRONiII I -\TAT.
•'DES 1 SERVICES, INC.
1. Client Name: Access Analytical, Inc.
SAMPLE/COOLER RECEIPT CHECKLIST
2. Carrier: FedEx ❑d UPS ❑ USPS❑ Client❑ Courier❑ Othel'
von ti tire
3.
4.
S.
6.
7.
8.
9.
10.
11.
12.
AES Work Order Number: 1809871
natailc
Comments
Shipping container/cooler received in good condition?
o'
damaged ❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
I
lCooling
Temperature blanks present?Cooler
temperature(s) within limits of0-6°C? [See item 13 and 14for
temperature recordings.]
®
�
initiated for recently collected samples / ice
present ❑
Chain of Custody (COC) present?
o
Chain of Custody signed, dated, and timed when relinquished and received?
o
Relinquished: Signed/dated
Sampler name and/or signature on COC?
a
Were all samples received within holding time?
TAT marked on the COC?
•
If no TAT indicated, proceeded with standard TAT perTerms &Conditions. U
13. Cooler 1 Temperature 0.6 °C Cooler 2 Temperature
14. Cooler 5 Temperature °C Cooler 6 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
°C Cooler3Temperature °C Cooler 4 Temperature °C
°C Cooler 7 Temperature °C Cooler 8 Temperature °C
I certify that I have completed sections 1-15 (dated initials). MH 9/12/18
vow nv, nVa netnilc Comments
Were sample containers intact upon receipt?
e
Custody seals present on sample containers?
•
Custody seals intact on sample containers?
n
-
Do sample container labels match the COC?
Q
®
.0
incomplete info ❑ illegible ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
e
Were all of the samples listed on the COC received?
e)
©
®
samples received but not listed on CDC ❑
samples listed on COC not received ❑
Was the sample collection date/time noted?
o
Did we receive sufficient sample volume for indicated analyses?
•
Were samples received in appropriate containers?
•
Were VOA samples received without headspace (< 1/4" bubble)?
Were trip blanks submitted?
c
listed on CDC ❑ not listed on COC ❑
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). ED 9/12/18
checked at Sample Receipt. Yes No N/A Details Comments
29. Have containers needing chemical preservation been Checked - 0-
29. Containers meet preservation guidelines? Q I u•
!v 30. Was pH adjusted at Sample Receipt? n I n•
m ' Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
1 I certify that I have completed sections 28-30 (dated initials).
Checklist 6.9.17 Rev 2
W I 'Locked i
ED 9/12/18
Ij Page 6 of 7

Analytical Environmental Services, Inc Date: 20-Sep-l8
Client: Prism Laboratories ANALYTICAL QC SUMMARY REPORT
Project Name: 8090113
Workorder: 1809871 BatchID: 267209
Sample ID: MB-267209
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: MBLK
TestCode: BERHIC1DES,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8473938
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 0.3556 0 0.5000 71.1 50.4 133
Sample 1D: NiB-267209-2
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: NIBLK
TestCode: HERBICIDES,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8476476
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 0.4079 0 0.5000 81.6 50.4 133
Sample ID: LCS-267209
Client TD:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: LCS
TestCode: HERBIC1nES,TCLr SWI311l8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8473939
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4302
0.20
0.5000
86.0
49.1
119
2,4-D
0.4451
0.20
0.5000
89.0
50.9
129
Surr: DCAA
0.4377
0
0.5000
87.5
50.4
I33
Sample ID: 1809998-OO1BMS
Client ID:
Units: mg/L
Prep Date: 09/17/2018
Run No: 380289
SampleType: NIS
TestCode: HERBICIDEs,TCLP SW1311/8151A
BatchID: 267209
Analysis Date: 09/18/2018
Seq No: 8473941
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
2,4,5-TP (Silvex)
0.4443 0.20
0.5000
88.9
48.2 125
2,4-D
0.4892 0.20
0.5000
97.8
44.5 138
Surr: DCAA
0.4283 0
0.5000
85.7
50.4 133
Qualifiers: > Greater than Result value
< Less than Result value
BRL Belosv reporting limn
E Estimated (value above quantiation range)
1
J Estimated value detected below
Repuning Limit
N Analyte not NELAC certified
00
0
Rpt Lim Repuning Lumit
S Spike Recovery outside limits due to
matrix
H
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 7 of 7

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
8090113
LABORATORY REPORT NUMBER
218091310
DATE
09/18/2018
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B._Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL),
7979 Innovation Park Dr., Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955,
NELAP certified laboratory# 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be
directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 218091310 Page 1 of 12
Page 19 of 30

(ScZaL
ANALY'MAL LAB,RATORIES. ILC
LELAP CERTIFICATE NUMBER: 01955
DOD-ELA P A CCREDITA TION NUMBER: 74960
1 90 VIV Al "A rd i � W # 11 M,444
NJ t I I JkV AR - V N
PERFORMED BY
GCAL, LLC
7979 Innovation Park Dr.
Baton Rouge, LA 70820
Report Date 09/18/2018
GCAL Report 218091310
VIIMEY���Al�AIit11��11iiIII
Project 8090113
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
A
t
I S 0'Q1
r
-kI 17025,0
PJ1A
Testing
DOD FIAP
Lab Report#: 218091310 Page 2 of 12
Page

Report4: 218091310
Project ID: 8090113
ant, I, f'tlC rl ti•fl+a��.YIYi _f"
Laboratory Endorsement
Report Date: 09/18/2018
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution Is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in
full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results
are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work bath technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature,
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
GCAL Report 218091310
Lab Report#: 218091310 Page 3 of 12
Page 21 of 30

Report#: 218091310
Project ID: 8090113
Certifications
Report Date: 09/18/2018
Certification
Certification Number
DOD ELAP
L14-243
Alabama
01955
Arkansas
12-060-0
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
USDA Soil Permit
P330-10-00117
Lab Report#: 218091310
Page 4 of 12
Page 22 of 30

Report#: 218091310
GCLProject ID: 8090113
N .ht1-1-1.1, t
Case Narrative
Client: Access Analytical Report: 218091310
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Report Date: 09/18/2018
Lab Report#: 218091310 Page 5 of 12
Page 23 of 30

GCAL ID Client ID
21809131001 StaLime
21809131002 4th Creek
21809131003 3rd Creek
Report#: 218091310
Project ID: 8090113
Sample Summary
Matrix
Collect DatelTime
Solid
09/10/2018 08:20
Solid
09/10/2018 08:03
Solid
09/10/2018 08:15
Report Date: 09/18/2018
Receive Datefrime
09/13/2018 09:40
09/13/2018 09:40
09/13/2018 09:40
Lab Report#: 218091310 Page 6 of 12
Page 24 of 30

�Reports/: 218091310
a Project ID: 8090113
:�xl,• I:: tI LPi ::.. a.ilL.:I,C
Summary of Compounds Detected
Report Date: 09/18/2018
Collect Date 09/10/2018 08:03 GCAL ID 21809131002
4th Creek Receive Date 09/13/2018 09:40 Matrix Solid
EPA 9034
CAS# Parameter
18496-25-811 Reactivity Sulfide
Result DL
425 250
LOQ Units
250 mg/kg
Lab Report#: 218091310 Page 7 of 12
Page 25 of 30

Report#: 218091310
ZVI.,u�uru �er.a_:a,'.:..-
Project ID; 8090113 Report Date: 09/18/2018
Sample Results
Collect Date 09/10/2018 08:20 GCAL ID 21809131001
StaLime RecelveDate 09/13/201809:40 Matrix Solid
9012E
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:49 TMT 644001
CAS# Parameter Result DL LOQ Units
57-12-5R Reactivity Cyanide 25OU 250 250 mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAS# Parameter
18496-25-813 Reactivity Sulfide
Result DL LOQ
250U 250 250
4th Creek Collect Date 09/10/2018 08:03 GCAL ID 21809131002
Receive Date 09/13/2018 09:40 Matrix Solid
Ef
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:51 TMT 644001
CAS# Parameter
57-12-5R Reactivity Cyanide
EPA 9034
Result
DL
LOQ
Units
250U
250
250
mg/kg
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAS# Parameter
18496-25-8R Reactivity Sulfide
Result
DL
LOQ
Units
425
250
250
mg/kg
Lab Report#: 218091310
Page 8 of 12
Page 26 of 30

Report#: 218091310
Project ID: 8090113
Sample Results
Report Date: 09/18/2018
Collect Data 09/10/2018 08:15 GCAL ID 21809131003
3rd Creek Receive Date 09/13/2018 09:40 Matrix Solid
E{
D12B
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643869 EPA 7.3.3.2 (1997) 1 09/17/2018 12:53 TMT 644001
CAS# Parameter Result DL LOQ Units
57-12-5R Reactivity Cyanide 250U 250 250 mg/kg
EPA 9034
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
09/14/2018 12:31 643870 EPA 7.3.4.2 (1997) 1 09/17/2018 15:40 JRB 643979
CAS# Parameter Result DL LOQ Units
18496-25-8R Reactivity Sulfide 250U 250 250 mg/kg
Lab Report#: 218091310 Page 9 of 12
Page 27 of 30

Report#: 218091310
��
,�,�,.,,� s,,,,�_,��,�.�.t4t. ProjectlD: 8090113
General Chemistry QC Summary
Report Date: 09/18/2018
Analytical Batch Client ID
MB643870
LCS643870
643979 GCALID
1848779
1848780
Prep Batch Sample Type
MB
LCS
643870 Prep Date
09/141201812:31
09/14/2018 12:31
Prep Method Analysis Date
09/17/2018 15:40
09/17/2018 15:40
EPA 7.3.4.2 (1997) Matrix
Solid
Solid
EPA 9034
Units
mg/kg
Spike
IResult
%R
Control
Result
DL
Added
Limits%R
Reactivity Sulfide 1 4496-25-SR
250U
250
1000
1282
128
47 - 135
Analytical Batch Client ID
MB643869
LC3643869
644001 GCAL ID
1848776
1848777
Prep Batch Sample Type
MB
LCS
643869 Prep Date
09/14/201812:31
09/14/2018 12:31
Prep Method Analysis Date
09/17/201812:33
09/17/201812:35
EPA 7.3.3.2 (1997) Matrix
Solid
Solid
EPA 9012E
Units
mg/kg
Spike
Result
I
%R
Control
I
Result
DL
Added
Limits%R
Reactivity Cyanide 57-12-513
NDI
2501
2501
23.91
10
1 - 25
Lab Report#: 218091310 Page 10 of 12
Page 28 of 30

r
m
a,
I client ID: 4565 - Access.'Analytical`
664: 21-8U'q-1310
PH
1 I Full -Service Analytical a �P, .�iEC.
r" n I u �'
" Environmental Solutions ' — -•- .......
Lk00VATCnlcr%:r ,
SUBCONTRACT ORDER
Cerlilication: ELAC_ USACE__ _
Prism Laboratories, Inc. NC ( SC Other T
8090113 N/A
SENRING LA6ottAToRY: MCF]VINC LABORATORY:
Prism Laboratories, Inc. Gulf Coast Analytical Labs, Inc.
P. 0. Box 240543 10781 Coursey Blvd
Charlotte, NC 28224-0543 Baton Rouge, LA 70816
Phone',800-529-6364 Phone -[phone]
Fax: [phone] Fax: [phone]
Project Manager: Robbi A. Jones
Analysis Due Expires Laboratory ID Comments
Sample ID:8090113-01 Solid Sampled:09/10/1808:20 .'�;'.'+-'. `r:•!` 1' "—
Reactivity, Sulfide (Sub) 09/17/18 08:20
Reactivity, Cyanide (Sub) 09/24/18 08:20
Containers Supplier!.•
X Lq0Z_ 10­—
Satup)n1D;8090113-02
Reactivity, Sulfidc (Sub)
Reactivity, Cynnide (Sub)
COntoinet$' Supplied:
Solid Sanlpled:09/10/18 08:03
09/17/18 08:03
09/24/18 08:03
Sample ID: 8090113-03 1 Solid
Reactivity, Cyanide (Sub)
Reactivity, Sulfide (Sub)
Containers ,Supplied:
Salnpled:09/10/18 08:15
09/24/18 08.15
09/17/18 08:15
IBM
I%L:ck:- 4[7I.ty Date
Released 11% Date KCCclYc11 By Date
Iielea5ed By I)ntc Received By Date
Page I of I
Page 29 of 30

SAMPLE RECEIVING CHECKLIST
SAMPLE DELIVERY GROUP
218091310
CHECKLIST
YES
NO
Client PM AEC
Transport Method
Samples received with proper thermal preservation?
+/❑
❑
4565 - Access Analytical
F®DC
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including samplelDs, collect times, and sampler)?
Q
❑
Profile lumber
Received By
80251
Savage, Tiffany R
-
--
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
v❑
©
❑
❑
Line Item(s)
Receive Date(s)
2 - Solid
09/13/18
- -
Preservative added to any containers?
-
0
❑d
If received, was headspace for VOC water containers < 6mm?
®
❑
Samples collected in containers provided by GCAL? '
❑
0
COOLERS
DISCREPANCIES
LAB PRESERVATIONS
Airbill Thermometer 11Y E29
Temp °C
Wne
Nbne
T731-908E-6869
2.0
NOTES
lbvision 1.6
Page 1 of 1
Lab Report#: 218091310 Page 12 of 12

OMICROBAC@
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K810048
City of Statesville Project Name: Sta-lime/Sludge Sample - 4th Creek
WWTP
Mr Ken Galloway Project / PO Number: N/A
Post Office Box 1111 Received: 09/05/2018
Statesville, NC 28687-1111 Reported: 09/18/2018
Analytical Testing Parameters
Client Sample ID: Sludge
Sample Matrix: Sludge Collected By: Galloway
Lab Sample ID: K810048-01 Collection Date: 09/05/2018 12:00
Wet Chemistry
Method: SM 2540 G-11
% Solids
Analyses Subcontracted to: Microbac Laboratories, Inc. - Baltimore
Result RL Units Note
87.30 0.05 % by Weight
Analyzed Analyst
09/11/18 1551 09/12/18 1216 RDM
Microbiology Result RL Units Note Prepared Analyzed Analyst
Method: EPA 1682
Salmonella <0.030 0.030 MPN/4g dry 09/06/18 1720 09/07/18 1909 EMS
Dns
RL: Reporting Limit
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
e data and information on this, and other accompanying documents, represents
y the sample(s) analyzed. This report is incomplete unless all pages indicated
„, he footnote are present and an authorized signature is included.
Reviewed and Approved By:
':�? "Z L'-'-
Jeanne Overstreet
Client Relationship Specialist, Environmental
Reported: 09/18/2018 09:27
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 2

M
Microbac.Fayetteville SHD, '
LDS ACCEPTED MONDAY- THURSDAY UNTIL 1600
liCROBAC 2692 Hope MillsHAIN
OF CUSTODY RECf
Faye
Fayetteville, NCC 2838306
Number
II�II�III�IIl��1���,I«,,,�IlJfpr
Instructions on back
I jI
Lab Report Address Invoice Address
Turnaround Time TO BE COMPLETED SY M
Client Name: City of Statesville 41th Creek Client Name: City of Siatesvilie
>:I�outine (5 to 7 business days) Temp. Upon Receipt (°C)
Address: 693 Bell Farm Road Address. 693 Bell Farm Road
[j RUSH` (notify lab) Holding Time
City, State, Zip: Statesville. NC 28625 City, State, Zip: Statesville, NC 28625
(needed by) Samples Received on Ice? Yes
No NIA
Contact: Ken Galloway Contact: Ken Galloway
Report Type Custody Seals Intact? Yes No
NIA
Telephone No.: 704-878-3438 Telephone No: 704-578-3438
Results Only [ j Level 1 [ I Level 2 Leve13 [ ] Level 4 [ ] EDD
Send Report via: [ )Mai( ( ) Fax Dt'e-mail kaalloway@_! tatesvillenc.net Send Invoice
� j
via: (] Mail [ ]Fax L mail k allowav%i)statesvillenc.net
Project:
Location:
PO No.: Compliance Monitoring? ( ] Yes [ J NO [ ]Agency/Program
Sampled by (PRINT): Ken Gaillav
Sampler Signature
Sampler Phone No.: 704878.3438
Matrix Types: Soil/Solid (S),
ludge, Oil, Wipe, Drinking Water (DW), Groundwater (GW), Surface Water (SW), Waste Water (WW), Other (specify)
1*Preservative Types: (1) HNO3, (2)
2SO4, (3) HCI, (4) NaOH, (5) Zinc Acetate, (6) Methanol, (7) Sodium
Bisulfate, (8) Sodium Thiosulfate, (9) Hexane, (U) Unpreserved
RFr311FC1r9=r1 EUdI VCIC
Lab I
Client Sample ID
Date
ollected
Time
Collected
No, of
Containers
Matrix
Grab
or
Comptype"
t
Preservative
F o
m y
Addit;onal Nofes
1
4th Creek Sia-Lime
/5/2018
I
{ 1200
1
S
Grab
A
I
(
I
I
I
I
]
I
I
1
I
Possible Hazard Identiiicatiio []
[I Non -Hazardous [] Radioactive
(signature) _ DatelTime
By (slgnature) DateMme
By (signature) DatelTme
Sam [] Dispose as appropriate [] Return [j Archive
9/5)2018 /Z2
Received By (signature)
Received By (signature)
Received By (signature)
Date/Time
DatelTime
Daterrime
Page 2 of 2