WQ0004563_2018 Residual Annual Report_20190214

WVEOLIA
WATCER
January, 2019
Care of Non Discharge Permitting Group
1636 Mail Service Center, [P
Raleigh, N.C. 27699-1636 FEB 14 2015
Re: 2018 Annual Report - 40 Clt+R Part 503 Rule vjr'kS"':odTVV
For the Regional Compost Facility in Hickory, NC 1,1c0R'NNN1011 PROGERIN9 01 Cnit��n��
Dear Ladies and Gentlemen:
FEB �
Please find herein, the Regional Compost Facility (RCF) 2018 Annual Re orot_cg
accordance with the reporting requirements of 40 CFR Part 503, North Carolina
Monitoring Requirements, and Distribution and Marketing reporting for Permit No.
WQ0004563. This document was originally prepared by Veolia Water North America
Operating Services (Veolia) and submitted on behalf of the Sludge Consortium (Owner)
in Hickory, North Carolina for the above captioned facility.
VWNAOS provides full contract operations, maintenance, and management (OM&M)
services at the RCF in a contract agreement with the consortium, which became effective
January 1, 1995.
If you have any questions concerning this 2018 Annual Report and the information
contained herein, please contact me at the Regional Compost Facility at [phone]
or call Shawn Pennell, Public Services Director, City of Hickory, North Carolina at (828)
323-7427.
Respectfully submitted,
Paul Spencer
Veolia Project Manager
cc: Shawn Pennell, Hickory
Jimmy Clark, Conover
Barry Edwards, PE, Catawba County
Hickory Lab
Lewis Parrish, VWNAOS
SLUDGE CONSORTIUM- HICKORY, NORTH CAROLINA

REGIONAL COMPOST FACILITY
2018 - 40 CPR PART 503 ANNUAL REPORT
Monitoring, Record beeping, and Deporting for
Preparing Sewage Sludge for Beneficial Use
At In -Vessel Biosolids Composting Facility -
Presented to:
NCDEQ/DWR
WQ Regional Operations Section
610 E. Center Avenue
Mooresville, N.C. 28115
Submitted for:
City of Hickory, North Carolina
Public Services Department
P.O. Box 398
Hickory, North Carolina 28603-0398
Prelnared by:
Veolia Water North America Operating Services
Regional Compost Facility
3200 20th Avenue, SE
Newton, North Carolina 28658
January, 2019
REGIONAL COMPOST FACILITY
HICKORY NORTH CAROLINA
2

Environmental Permits:
NC DENR Distribution of Residuals Solids (503) Permit: No: WQ0004563
City of Hickory Industrial Pretreatment Permit No: 0050
NC DEHR Storm Water Discharges General Permit No: NCG110034
SOURCE AND PERMIT NUMBERS
The biosolids received at the Regional Compost Facility were generated from a variety of
permitted cities and towns within Catawba County, North Carolina. In 2018, the
Regional Compost Facility received biosolids from the following facilities and no other
source was accepted. The following approved sources also include their permit number.
i SOURCE PERMIT NUMBER
City of Hickory (Northeast) NC0020401
City of Hickory (Henry Fork) NC0040797
City of Hickory (Catawba) NC0025542
City of Newton (Clarks Creek) NC0036196
City of Conover (Northeast) NC0024252
City of Conover (Southeast) NC0024279
Town of Maiden NC0039594
Town of Claremont (North) NC0032662
Town of Claremont (McLin) NCOO81370
Catawba County Domestic Septage NA
City of Hickory Water Plant NC0044121
EXECUTIVE SUMMARY
As required under the authority of Section 405 (d) of the Clean Water Act (CWA), as
amended by U.S. EPA and promulgated at Title 40 CFR Part 503, please find herewith
the Monitoring, Record practices and Reporting practices and procedures in place for the

beneficial use of sewage sludge applied to land as finished compost at the Regional
Compost Facility (RCF) in Hickory, North Carolina.
The RCF is a twenty dry ton per day (20.0 DT/dy) in -vessel composting facility using the
Ashbrook-Simon-Hartly (A-S-H) Tunnel Reactor Technology. Three local governments,
comprised of the Cities of Hickory, Conover, and Catawba County, North Carolina, own
the RCF. These three local governments formed a Sludge Consortium to provide
centralized facilities for the management and disposal of their combined municipal
wastewater biosolids. Class A wastewater residuals are processed at the RCF and
distributed in full compliance and accordance with the provisions and requirements set
forth by Permit No. WQ0004563.
The RCF is built on a 15-acre site in Hickory at an equidistant location for all Consortium
members. The RCF is comprised of biosolids liquid storage, dewatering, in -vessel
composting, aerated curing and maturation, product storage, odor control, and
pretreatment effluent facilities. The biosolids are prepared for beneficial use as finished
compost, analyzed, classified, marketed, and distributed in bulk to a variety of land
applications. The pretreated effluent is discharged to the City of Hickory Henry Fork's
Wastewater Treatment Plant; permit number NC0040797, for final disposal.
The Sludge Consortium (Owner) entered into an agreement with Veolia Water North
America Operating Services (Veolia), to provide full contract operations, maintenance,
and management (OM&M) services at the RCF. Therefore, Veolia submits this annual
report to provide all available information and data for 2018 in accordance with and to
demonstrate compliance with Permit No.WQ0004563 and the 40 CFR Part 503 reporting
in Subpart 503.18 for land application.
Included herein, is a report of the biosolids that was processed in 2018 and a description
of the alternatives selected for compliance with the Pathogen Reduction (PFRP) and
Vector Attraction Reduction (VAR) requirements. Certification statements for
compliance with PFRP and VAR requirements are also provided for this Annual Report.
As a Class A Sludge Management Facility, the RCF prepares a Class A `exceptional
quality' biosolids compost product, in compliance with the requirements in 40 CFR Part
503 as documented herein. This 2018 Annual Report provides the required general
information as well as specific information on the amount of biosolids that was
processed; composted biosolids use and disposal practices; generators and preparers of
the biosolids as owner/operator of the biosolids management facilities; description of
selected alternative for pathogen reduction requirements; description of selected
alternative for vector attraction reduction requirements; process monitoring and record
keeping procedures; and listing of all relevant environmental permits. Supplemental data
has been provided to include bi-monthly laboratory reports (analytical data for metals,
nutrients and pathogen density), as well as TCLP and compost curing piles information.
We are pleased to report that the RCF achieved compliance with the general conditions
and performance standards of the NC DEQ/DWR Permit, as well as its O&M
requirements and the pollutant limits in Tables 1 and 3 of Subpart 503.13; the pathogen
4

reduction requirements in Subpart 503.33(b)(5). NC DWR Compliance forms, including
the bi-monthly PFRP compliance certification statements are provided within Exhibit 1.
Compliance with these standards in 40 CFR Part 503 for the pollutant limits, operation
standards for pathogen density reduction and vector attraction reduction, general
requirements, and management practices was demonstrated and documented by the
Monthly Operations Summary Tables for 2018, provided herein as Exhibit 2. Also
included is an annual summary of the 2018 Monthly Operations Report data for the RCF,
which provides detailed information on biosolids loadings and processing, in -vessel
composting, air/odor scrubbing, by-product liquids pre-treatment and Owner utilization.
Exhibit 2 also provides the compost curing piles data for retention time and temperatures.
Compliance with the frequency of monitoring, record keeping, and reporting of the 40
CFR, Part 503 regulatory standards have been in place since the RCF was placed into
service on January 3, 1995. Accordingly, bi-monthly laboratory reports are provided
herein as Exhibit 3 and the 2018 annual TCLP laboratory data is provided as Exhibit 4.
The RCF is certified for Field Certification for Temperature and pH. The North Carolina
State Laboratory Certification has approved these parameters. A copy of this NC State
Lab Certificate Number: 5466 (Lab Code: NCO1797) is provided herein, as Exhibit 5.
I. GENERAL INFORMATION
Facility, Name, Mailing Address and Location

Regional Compost Facility (RCF)
3200 20th Avenue, S.E.
Newton, North Carolina 28658
The Regional Compost Facility is a Class A Sludge Management Facility as defined in 40
CFR Part 503.9(c). This facility currently employs one method of biosolids management
that requires compliance with 40 CFR Part 503 requirements. The primary method of
sewage sludge disposal is its beneficial use at the on -site dewatering and in -vessel
composting facility, which prepares the wastewater residuals for land application.
Generators / Preparer of Biosolids
The Sludge Consortium, is comprised of three local governments, generates biosolids
during the treatment of domestic sewage at their publicly owned treatment works and
prepares materials (dewatered cake and finished compost) from biosolids. The RCF is
owned by the Sludge Consortium, which members include the City of Hickory, the City
of Conover and Catawba County, North Carolina. In January of 1995 the Consortium
entered into an agreement for operations, maintenance, and management (OM&M)
services of its RCF with Professional Services Group, Inc. (PSG) currently named Veolia
Water North America Operating Services (Veolia). Contract services were renewed on
July 27, 2017, February 20, 2007, March 5, 2002, and October 4, 2011, respectfully.
Consortium Ownership:
Owner / Generator:
2017
City of Hickory - 66.0%
City of Conover - 15.5%
Catawba County - 18.5 %
City of Hickory
Attn: Mr. Shawn Pennell
Asst. Public Services Director
P.O. Box 398
Hickory, NC 28603-0398
Tel. # (828) 302 - 3758
E-Mail - pennellghickor rmc.gov
Operator / Preparer: Veolia Water North America Operating Services
Attn: Paul Spencer, Project Manager
Regional Compost Facility
3200 20th Avenue, S.E.
Newton, NC 28658
Tel. # [phone]
E-Mail — [e-mail]
Environmental Permits
C

Regional Compost Facility:
NC DENR Distribution of Residuals Solids (503) Permit: No: W00004563
City of Hickory Industrial Pretreatment Permit No: 0050
NC DENR Storm Water Discharges General Permit No: NCG110034
II. BIOSOLIDS PROCESSED AND DISTRIBUTED
A. Biosolids Processed
The amount of biosolids received and processed for beneficial use and disposal at the
RCF during the 2018 annual reporting period was 2,014 metric dry tons (MDT). A
summary of the monthly biosolids dewatering data is provided in the Operations
Summary Performance Tables, Exhibit 2, for the belt filter press (BFP) and/or centrifuge
operations at the RCF will support documentation and information for the following
computation of the actual MDT of biosolids prepared for use and disposal in 2018.
2018 Operations — 2,014 AMT
1. Dry short tons of biosolids loaded to the belt filter presses and/or centrifuge:
Dry short tons = totalized centrifuge/belt press load (DT) from 01/01/18 - 12/31/18.
= 2,355 DT
2. Dry short tons of biosolids captured by the belt filter presses and/or centrifuge:
Dry short tons = totalized centrifuge/belt press load (DT) x avg . solids capture (%)
= 2,355 x 0.943
= 2,221 DT
3. Metric dry tons of biosolids processed for beneficial use:
Metric dry tons = total centrifuge/belt press captured dry short tons (DT) x conversion factor
= 2,221 x 0.907
= 2,014 MDT
B. Biosolids Compost Produced and Distributed
The amount of biosolids produced and distributed for beneficial use and disposal at the
RCF during the 2018 annual reporting period was 3,895 metric dry tons (MDT). A
summary of the monthly Class A biosolids compost marketing data is provided in the
Operations Summary Performance Tables (Exhibit 2). The 2018 annual compost
marketing and distribution activities at the RCF are summarized in the following
computation of the actual MDT of biosolids compost produced and distributed to market.
2018 Distribution — 3,895 MDT
1. Dry short tons of Biosolids compost produced and marketed
Dry short tons = total discharged material (DT) from 01/01/18 - 12/31/18.
= 4,294 DT
2. Metric dry tons of biosolids compost produced for beneficial use:
Metric dry tons = total production of dry short tons (DT) x conversion factor
= 4,294 x 0.907
— 3,895 MDT
The determination of the dry short tons of biosolids received and loaded to the belt filter
presses and/or centrifuge is shown in a computerized RCF Operations Performance
Summary report (as Exhibit 2). This biosolids loading has been determined by monitoring
7

W
the number of belt filter presses and/or centrifuge in service (1 or 2), the actual run time
hours each 24 hour operating day, direct flow metering of the volumetric rate of sludge
feed (gallons per day - GPD), and gravimetrically analyzing the time -composite sample of
feed sludge for total solids (% TS) using Standard Methods Part 2540 G., (APHA, 1992).
A composite of the feed solids, cake solids, and filtrate solids were obtained daily to
compute a materials balance around the belt filter presses and/or centrifuge to determine
solids capture (%). Since the RCF does not have a weigh belt on its sludge cake conveyor
belt, the generated amount of biosolids for in -vessel composting was determined by
performing a daily materials balance of the dewatering process. All of the dewatered
sludge cake was processed in the Tunnel Reactor in -vessel composting facility. Thus, all
biosolids loaded and captured at the BFP and/or Centrifuge represents the biosolids
generation and processing basis for the Annual Report and the amount of biosolids
prepared as finished compost for land application in accordance with 40 CFR Part 503.
The determination of the dry short tons of biosolids compost produced and distributed is
also shown in the Operations Performance Summary Report (as Exhibit 2). The dry tons
are calculated by obtaining composite outfeed samples daily and using the total solids and
density data for calculation. The dry ton totals are obtained by using the percent solids
content of the wet mass weight. (Total dry tons = total yards of compost produced x
density x % solids content of the wet mass.)
M. BIOSOLIDS USE & DISPOSAL PRACTICES
The biosolids received at the Regional Compost Facility (RCF) were beneficially used at
the on -site dewatering and in -vessel composting facility. The biosolids management and
disposal practices are the beneficial use of sewage sludge via composting to produce a
high quality soil product which was sold and, or distributed in bulk for application to the
land in accordance with 40 CFR Part 503, Subpart B regulations.
The biosolids processing train and management practices at the RCF consists of receiving
and storage of liquid biosolids and wood amendments, mechanical belt filter presses
and/or centrifuge dewatering, in -vessel biosolids composting, outside curing and
maturation product storage, foul air scrubbing, and wastewater pretreatment. The RCF is
a PFRP facility and produces a Class A `exceptional quality' biosolids compost product.
As will be certified herein, all of the composted biosolids achieve the minimum time and
temperature requirements to achieve both PFRP and VAR as an aerobic composting
process in which the in -feed mixture receives plug -flow treatment within the four tunnel
reactors over an average of 28 days to achieve the necessary biosolids stabilization levels.
Compliance certifications are provided in the NC DWR compliance forms (as Exhibit 1).
SUBPART B - LAND APPLICATION
8

Process Monitoring Record Keeping and Reporting Description
The Regional Compost Facility is substantially automated with numerous on-line and
continuous reading instruments (i.e. sludge flow meters, air flow meters, auger speeds) to
monitor the process and ensure that PFRP requirements are met. The various on-line
equipment and instrumentation were calibrated routinely by Veolia's electrical and
instrumentation staff and adjustments were made for calibration, if required. In
accordance with Veolia's standards for quality assurance/quality control (QA/QC),
precision and accuracy determinations were made to ensure that high quality reproducible
data is generated. The monitoring data from these devices were retrieved continuously by
a computer system, where data was archived and performance reports generated.
Daily and monthly operator log forms and computer reports document various operating
parameters required for demonstration of compliance with 40 CFR Part 503 Regulations.
These parameters include system mass (wet tons and dry tons) and volume (cubic yards)
amounts of biosolids, amendments, and compost; in -vessel A-S-H Tunnel Reactors;
composting and curing processes; in -vessel reactors and odor control system airflows, etc.
Monthly RCF operations and performance data are summarized in tables (as Exhibit 2).
Analytical Results for Monitored Pollutants
Veolia analyzed the finished compost produced at the RCF for various pollutants required
and listed in Tables 1 and 3 of 40 CFR Part 503.13. We are pleased to report that full
compliance was achieved in 2018 with these limitations and the corresponding
classification of the finished compost as a Class A `exceptional quality' biosolids residual
product (data in Exhibit 1 forms).
In accordance with Table 1 of 40 CFR Part 503.16, the frequency of monitoring,
composite sampling, and analysis of the composted biosolids for the pollutants listed in
Table 3 is bimonthly (6 times per year). This testing frequency was determined on the
basis of the 2,014 dry metric tons (DMT) of biosolids processed and the 3,895 DMT
marketed as finished compost to beneficial uses.
We have also analyzed on a routine and as needed basis, the essential nutrient, stability,
and maturity, decomposition, and odor parameters of the finished product to characterize
its quality for various beneficial uses, prior to its distribution. We have provided the
essential finished compost quality parameters and nutrients information to end users to
ensure the proper application as a suitable bulk organic product (data in Exhibit 1 forms).
Pathogen Reduction Requirements - Alternative A5 (PFRP)
E

As previously stated, the Regional Compost Facility is a "Process To Further Reduce
Pathogens" (PFRP) system for treatment and beneficial use of dewatered biosolids. This
section of the Annual Report states that W NAOS and the Consortium have utilized
Class A Pathogen Reduction using Alternative AS - PFRP via Composting to
demonstrate compliance with 40 CFR Part 503.32(a)(7) and in continuity with 40 CFR
Part 257 regulations. The temperature of the biosolids inside the Tunnel Reactors was
maintained at 55 deg. C (131 deg. F) or higher for at least three (3) days. Bi-monthly
PFRP compliance certification statements are provided in the DWR forms (as Exhibit 1).
The compost product is also placed on the outdoor curing pad for further maturation and
curing. Final curing temperatures were also maintained greater than 55 deg.0 (131 deg. F)
or higher for at least three days. Please refer to the Operations Performance Summary
Tables (Exhibit 2) of monthly data for the in -vessel composting time and aerobic process
temperatures, as well as the compost curing piles data retention times and temperatures.
The design capacity of the four A-S-H Tunnel Reactors is approximately 54,432 ft (2,016
yd.). The standard operating procedure (SOP) for processing biosolids in the A-S-H in -
vessel composting system employs a process using single stage horizontal plug flow. The
raw (in -feed) compost was deposited in the front of the Tunnel Reactors with the addition
of sawdust amendment and recycle material and discharged after active in -vessel
composting and initial curing (out -feed compost) from the end of each reactor. Thus, the
active composting phase occurs in the first two-thirds of each Tunnel Reactor and partial
curing occurs in the remaining third of each Tunnel Reactor. The material is then placed
on an outside curing pad for additional maturation, stabilization and cooling of the
compost product before being distributed to the end users.
Based upon site -specific monitoring of the bulk density of the in -feed mixture compost
and recording of the number of hydraulic ram pushes for each Tunnel Reactor, the
volumetric loading (cy/dy) is accurately determined for each processing day. This
volumetric loading was divided into the fixed total reactor capacity to compute the
"actual" Solids Retention Time (days). The actual SRT considering compaction and
materials compression in 2018 averaged 27.9 days as highlighted in the monthly
Operation Performance Summary Tables (Exhibit 2). During this in -vessel composting
period, at least three (3) days of processing time was continuously available to achieve
PFRP in the Tunnel Reactors as the in -feed compost traveled horizontal from the front to
the back of the 63 foot long reactor and eventually discharged as out -feed compost.. The
product is then discharge and moved to the final curing process for up to 60 additional
days before finished compost testing, and subsequent product marketing and distribution.
10

Seven sampling ports are installed along the length of each Tunnel Reactor to monitor
temperature within the compost biomass. A total of twenty-eight (28) discrete
measurements of temperature in the compost process are monitored and recorded by the
compost facility personnel for documentation. The side and top sampling ports give the
facility the ability to measure temperatures in each tunnel manually with an operator -
inserted probe. The average of certain aeration zone temperature readings provides the
daily determination of PFRP for the Tunnel Reactors. These daily PFRP temperature logs
were documented for each Tunnel Reactor and are reported on the monthly Operation
Performance Summary Tables (Exhibit 2) to document the composting process was
maintained at or above 55 deg. C during the period of January through December 2018 to
comply with Alternative A5 of 40 CFR Part 503.32. As shown in Exhibit 2, the average
PFRP temperature for all four Tunnel Reactors was 67.0 deg. C.
In accordance with 40 CFR Part 503.32(a)(7), the composted biosolids was analyzed for
Fecal Coliform at the time it was being prepared for sale and distribution into the market
place for final land application and was found to be below compliance limits. The
bimonthly composite samples were prepared for Fecal Coliform analysis on a dry weight
basis and analyzed in accordance with Standard Methods Part SM92210E. As shown in
Exhibit 1, the Fecal Coliform measured for discharged compost from the RCF in 2018
indicates no exceedences, all results were well below the acceptable limits. The
maximum Fecal Coliform density measured in 2018 for all samples was <697 MPN per
9-
The bi-monthly laboratory reports of pathogen testing results are provided as Exhibit 3.
Certification Statement - `I certify, under penalty of law, that the Class A pathogen
requirements in 40 CFR Part 503.32(a)(7) have been met. This determination has been
made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gather and evaluate the information used to
determine that the pathogen reduction requirements have been met. I am aware that there
are significant penalties for false certification including fine and imprisonment."
Undersigned.
A�
Paul Spencer.
Veolia Project Manager
11

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Vector Attraction Reduction - Option 5
The Regional Compost Facility uses the Aerobic Process (Thermophillic Composting) to
demonstrate and achieve compliance with the Vector Attraction Reduction requirements
set forth in 40 CFR Part 503.33(b)(5). Specifically, Option 5 as an Aerobic Process at
Greater Than 40 deg. C (104 deg. F) is most appropriate for achieving Vector Attraction
Reduction. As previously described in this Annual Report, the average Actual SRT in the
in -vessel compost reactors was 25.7 days for the reporting period of 2018. The dewatered
biosolids was composted and treated aerobically at thermophilic temperatures during this
period of in -vessel processing time.
The computerized composting performance reports document the aerobic processing of
the dewatered biosolids in accordance with 40 CFR Part 503.33(b)(5). The dewatered
biosolids have been aerobically treated for a minimum of 14.0 consecutive days during
which the daily minimum temperatures of the Tunnel Reactor have been maintained
above 40 deg. C and the average temperature maintained higher than 45 deg. C.
As highlighted in the monthly Operations Performance Summary Tables (Exhibit 2), the
average Vector Attraction Reduction (VAR) temperature for all Tunnel Reactors was
64.1 deg. C. Additional curing provided additional time to meet the requirements again.
The compost product is also placed on the outdoor curing pad for further maturation and
curing. Final curing temperatures were also maintained greater than 40 deg C. (104 deg.
F) or higher for at least fourteen days with an average of at least 45 deg C. (113 deg F).
Certification Statement - " I certify under penalty of law, that the Class A vector
attraction requirements in 40 CFR Part 503:33(b)(5) have been met. This determination
has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the vector attraction reduction requirements have been met. I am
aware that there are significant penalties false certification including fine and
imprisonment."
Undersigned.
10C�!%�iC_ _',�
Paul Spencer
Veolia Project Manager
IV. CERTIFICATION
12

P1F'li3P Certification Statement
`I certify under penalty of law that this document and all attachments were prepared under
my direction and supervision in accordance with the system designed that qualified
personnel properly gather and evaluate the information submitted. Based upon my inquiry
of the person or persons who manage the system or those persons directly responsible for
gathering the available information, the information submitted is, to the best of my
knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine and
imprisonment for knowing violation"
Undersigned. Date Signed:
-z&z g - r7- /
Paul Spencer r
Veolia Project Manager
Regional Compost Facility
3200 20th Avenue, S.E.
Newton, NC 28658
(828) 465 - 1401
E- Mail - [e-mail]
13

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
PERMIT #: WQ0004563 FACILITY NAME: Hickory Regional Compost Facility
PHONE: [phone] COUNTY: Catawba OPERATOR: Veolia Water North America Operating Services
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
El Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? El Yes ❑No No If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Vo
me (dry tons
Recipient Information
Amennt/
Bulking Agent
Residual In
Product Out
Name(s)
e
Volume (dry
tons)
Intended use(s)
January
See Attached Sheet
344
222.8
411
See Atached Sheets
411
See Attached
February
See Attached Sheet
337
223.71
321
See Atached Sheets
321
See Attached
March
See Attached Sheet
406
256.85
393
See Atached Sheets
393
See Attached
April
See Attached Sheet
403
238.63
421
See Atached Sheets
421
See Attached
May
See Attached Sheet
402
211.93
413
See Atached Sheets
413
See Attached
June
See Attached Sheet
343
185.37
422
See Atached Sheets
422
See Attached
July
See Attached Sheet
617.6
187.23
444
See Atached Sheets
444
See Attached
August
See Attached Sheet
365
199.35
349
See Atached Sheets
349
See Attached
September
See Attached Sheet
290
166.3
404
See Atached Sheets
404
See Attached
October
See Attached Sheet
296
190.48
401
See Atached Sheets
401
See Attached
November
See Attached Sheet
296
190.92
265
See Atached Sheets
265
See Attached
December
See Attached Sheet
69
81.11
50
See Atached Sheets
50
See Attached
Totals:
Annual d tons):
4168.6
2354.68
4294
..... ... ...... ..
4294
.....
Amendments used:
I Sawdust
Bulking Agent(s) used:
I Recycled Compost
* If more space than given is required, please attach additional information sheet(s). El Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2018 with all conditions of the permit (including but not limited to items 1-3 below) issued by the
Division of Water Quality. El Yes ❑ No If No, please provide a written description why the facility was not compliant.
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware
that there are s' n' scant Pena ies for submitting false information, including the pos ibility of fines and imprisonment for knowing violations."
1 1-22"!1l
Signature of Permittee Date Signature of Pre arer** Date
(if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r)
DENR FORM DMSDF (11/2005)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004563 Laboratory: 1) Pace Analytical Services
Facility Name: Hickory Regional Compost Facility - 2) Statesville Analytical
NPDES # or 3)
WQ#: WQ0004563
4)
WWTP Name: 5)
Residual Analvsis Data
Sample or
—Composite Date
1/25/18
2/6/18
3/8/18
4/19/18
5/24/18
6/21/18
9/13/18
7/12/18
9/25/18
10/4/18
11/8/18
12/18/18
Percent Solids
59.3
58.3
60.04
53.6
54.8
65.2
63.2
41.5
39
44.2
Aluminum
1410
1970
2840
3210
3000
2480
2660
2610
Calcium
7840
9030
5710
2980
5430
3350
3040
3360
Magnesium
1160
1470
882
588
937
459
512
479
,.d
Potassium
689
1210
1210
785
1520
542
620
448
Sodium
532
610
ND
ND
444
ND
ND
ND
Fecal Colliform
<34.4
<32
62.7
<51.9
<36
697
pH
8.4
8.1
7.8
7
5.1
7.6
7.6
y
PAN
4080
5120
9040
3090
2940
1860
2210
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties, for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparof Date
nFNR F(1RM RSRF_R rFir7nn141

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0004563 Laboratory: 1) Pace Analytical Services
Facility Name: Hickory Regional Compost Facility 2) Statesville Analytical
NPDDEQS# or WQ0004563 3)
WWTP Name:
Residual Analvsis Data
4)
5) -
Sample or
Composite Date
1/25/18
2/6/18
3/8/18
4/19/18
5/24/18
6/21/18
9/13/18
7/12/18
9/25/18
10/4/18
11/8/18
12/18/18
Percent Solids
59.3
58.3
60.04
53.6
54.8
65.2
63.2
41.5
39
44.2
Aluminum
1410
1970
2840
3210
3000
2480
2660
2610
Calcium
7840
9030
5710
2980
5430
3350
3040
3360
Magnesium
1160
1470
882
588
937
459
512
479
,.d
Potassium
689
1210
1210
785
1520
542
620
448
Sodium
532
610
ND
ND
444
ND
ND
ND
Fecal Colliform
<34.4
<32
62.7
<51.9
<36
697
PH
8.4
8.1
7.8
7
5.1
7.6
7.6
y
PAN
4080
5120
9040
3090
2940
1860
2210
Ila
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant ^penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Chi 'JVD-t-� ***9- v7- "I"
Signature of Preparer rDate
DENR FORM RSSF-B (512003)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: Hickory Regional Compost Facility Permit Number: WQ0004563
WWTP Name: NPDES Number:
Monitoring Period: From 1/1/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑
................. Alternative 4❑ Alternative 5 Rl Alternative 6 ❑
........
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost El
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 111
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑ jAerobic Digestion ❑
Anaerobic Digestion[]
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number or
Excee-
Frequency
of
SampleAnatyticaj
,type
Tech -
nimu
Geo. Mean
aximu
Units
Fecal Coliform
I u toM—eUW-
power IWN per
gram of total
solids or 2 x 10 to
the 6th power
1000 mpn per
eram of total solid
d wei ht
32
152.3
697
MPN/g
0
60 Days
Compost
M9221CI
Salmonella bacteria
(in lieu of fecal
coliform)
3 IvIPN per 4
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 ❑ Option 4 ❑ Option 5 L
Option 6 El Option 7 ❑ Option 8 ❑ Option 9 ❑ j0ption 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Paul Spencer - Project Manager
Prep r Name and Title (type or print)
Signature of Prepareif Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
DENR FORM RF (5/2003)

July 1, 2017 - June 30, 2018
iREC SCPS TOT YDS TOT
DATE NAME ALUM SOLD SCPS SOLD YDS
1/4/2018
PERENNIAL GROVES BG
859531
10.00
10.00
27.50
27.50
1/26/2018
BRUCE FOX
859532
1.00
11.00
2.75
30.25
1/30/2018
CHUE YANG
859533
0.50
11.50
1.83
32.08
1/31/2018
INGLE AND SON
182179
73.00
84.50
200.75
232.83
1/31/2018
CREATIVE LANDSCAPE
182180
20.00
104.50
55.00
287.83
1/31/2018
SOIL SUPPLY @1.50
182181
120.00
224.50
330.00
617.83
1/31/2018
SIGMON'S @ 2.53
182182
108.00
332.50
297.00
914.83
1/31/2-018
CC LANDFILL FREE
859539
39.00
371.50
113.10
1027.93
2/1/2018
CC LANDFILL FREE
859540
147.00
518.50
426.30
1454.23
2/2/2018
JAMES SIGMON
859534
1.00
519.50
2.75
1456.98
2/2/2018
PERENNIAL GROVES BG
859535
10.00
529.50
27.50
1484.48
2/8/2018
MAI MOUA
859536
0.50
530.00
1.83
1486.31
2/9/2018
JAMES SIGMON
859537
1.00
531.00
2.75
1489.06
2/9/2018
BRUCE FOX
859538
1.00
532.00
2.75
1491.81
2/14/2018
NENG MOUA
859541
0.50
532.50
1.83
1493.64
2/15/2018
JOHNNY REITZEL
859542
1.00
533.50
2.75
1496.39
2/15/2018
WILLIAM KANNUPP
859543
0.50
534.00
1.83
1498.22
2/19/2018
KEVIN ANNAS BG
859544
4.00
538.00
11.00
1509.22
2/21/2018
ALLEN MCREE
859545
2.00
540.00
5.50
1514.72
2/23/2018
JAMES SIGMON
859546
1.00
541.00
2.75
1517.47
2/23/2018
CHONG VANG
859547
0.50
541.50
1.83
1519.30
212712018
ARMANDT BOONSTRA
859548
2.00
543.50
5.50
1524.80
2/27/2018
PATRICK KISBY
859549
1.00
544.50
2.75
1527.55
2/28/2018
ROCK BRANCH BG
859550
24.00
568.50
66.00
1593.55
2/28/2018
INGLE AND SON
182183
59.00
627.50
162.25
1755.80
2/28/2018
CALDWELL LANDSCAPING
182184
2.00
629.50
5.50
1761.30
2/28/2018
SIGMON'S @ 2.53
182185
30.00
659.50
82.50
1843.80
2/28/2018
SOIL SUPPLY @1.50
182186
40.00
699.50
110.00
1953.80
3/2/2018
ARMANDT BOONSTRA
859551
2.00
701.50
5.50
1959.30
3/2/2018
KU VANG
859552
0.50
702.00
1.83
1961.13
3/5/2018
PAUL GREENE
859553
1.50
703.50
4.13
1965.26
3/5/2018
RON CRAIG
859554
0.50
704.00
1.83
1967.09
3/5/2018
RON CRAIG
859555
0.50
704.50
1.83
1968.92
3/5/2018
SEE YANG
859556
1.00
705.50
2.75
1971.67
3/5/2018
CHOU YANG
859557
1.00
706.50
2.75
1974.42
3/5/2018
GEORGE TOWNSEND
859558
1.00
707.50
2.75
1977.17
3/5/2018
PAUL GREENE
859559
1.50
709.00
4.13
1981.29
3/6/2018
KEVIN ANNAS BOGO
859560
8.00
717.00
22.00
2003.29

3/7/2018
PAUL GREENE
859561
1.50
718.50
4.13
2007.42
3/7/2018
RON CRAIG
859562
0.50
719.00
1.83
2009.25
3/7/2018
ROCK BRANCH BG
859563
24.00
743.00
66.00
2075.25
3/7/2018
KEVIN ANNAS BOGO
859564
8.00
751.00
22.00
2097.25
3/7/2018
ARMANDT BOONSTRA
859565
2.00
753.00
5.50
2102.75
3/9/2018
JOHN FORNSHELL
859566
2.00
755.00
5.50
2108.25
3/9/2018
ARMANDT BOONSTRA
859567
2.00
757.00
5.50
2113.75
3/9/2018
PAUL GREENE
859568
1.50
758.50
4.13
2117.87
3/13/2018
ARMANDT BOONSTRA
859569
2.00
760.50
5.50
2123.37
3/13/2018
ARMANDT BOONSTRA
8595701
2.00
762.50
5.50
2128.87
3/15/2018
DUAN FARMS
859571
2.00
764.50
5.50
2134.37
3/15/2018
KEVIN FULBRIGHT
859572
4.00
768.50
11.00
2145.37
3/15/2018
JOHN LENTZ
859573
1.00
769.50
2.75
2148.12
3/l5/2018
PAUL GREENE
859574
1.50
771.00
4.13
2152.25
3/15/2018
ARMANDT BOONSTRA
8595751
2.00
773.00
5.50
2157.75
3/15/2018
CHARLES WOOD
859576
6.00
779.00
16.50
2174.25
3/16/2018
CHER YANG
859577
0.50
779.50
1.83
2176.08
3/16/2018
PAUL GREENE
859578
1.50
781.00
4.13
2180.20
3/16/2018
DAVID CARPENTER
859579
2.00
783.00
5.50
2185.70
3/16/2018
CHOU YANG
8595801
0.50
783.50
1.83
2187.53
3/16/2018
THAO AMOUA
859581
0.50
784.00
1.83
2189.36
3/19/2018
DARRIN BOST
859582
2.00
786.00
5.50
2194.86
3/19/2018
JESSIE BEAL
859583
2.00
788.00
5.50
2200.36
3/19/2018
KAYING YANG
859584
1.00
789.00
2.75
2203.11
3/19/2018
LAKE NORMAN
859585
5.50
794.50
15.13
2218.24
3/19/2018
PAUL GREENE
859586
1.50
796.00
4.13
2222.36
3/20/2018
GLENN MULL
859587
1.00
797.00
2.75
2225.11
3/20/2018
LAKE NORMAN
859588
12.00
809.00
33.00
2258.11
3/20/2018
DUAN FARMS
859589
2.00
811.00
5.50
2263.61
3/21/2018
DUAN FARMS
859590
2.00
813.00.
5.50
2269.11
3/21/2018
DUAN FARMS
859591
2.00
815.00
5.50
2274.61
3/22/2018
PAUL GREENE
859592
1.50
816.50
4.13
2278.74
3/22/2018
CHONG VANG
859593
0.50
817.00
1.83
2280.57
3/22/2018
HOU XIONG
859594
0.50
817.50
1.83
2282.40
3/23/2018
NENG YANG
859595
0.50
818.00
1.83
2284.23
3/23/2018
PAUL GREENE
859596
1.50
819.50
4.13
2288.35
3/23/2018
CHONG YANG
859597
0.50
820.00
1.83
2290.18
3/23/2018
HLEE XIONG
859598
0.50
820.50
1.83
2292.01
3/23/2018
NENG VANG
859599
0.50
821.00
1.83
2293.84
3/23/2018
JESUS VICTORIO
859600
1.00
822.00
2.75
2296.59
3/23/2018
ARMANDT BOONSTRA
597801
2.00
824.00
5.50
2302.09
3/23/2018
SAI SUE VANG
597802
0.50
824.50
1.83
2303.92
3/26/2018
NENG VANG
597803
0.50
825.00
1.83
2305.75
3/26/2018
DOUA VANG
597804
0.50
825.50
1.83
2307.58
3/26/2018
CHUE YANG
597805
1.00
826.50
2.75
2310.33
3/26/2018
PAUL GREENE
597806
1.50
828.00
4.13
2314.46
3/26/2018
PHILLIP PARTIN
597807
0.50
828.50
1.83
2316.29

3/27/2018
NENG VANG
5978081
0.50
829.00
1.83
2318.12
3/27/2018
DOUA VANG
597809
0.50
829.50
1.83
2319.95
3/27/2018
PAUL GREENE
597810
1.50
831.00
4.13
2324.08
3/27/2018
NENG MOUA
597811
0.50
831.50
1.83
2325.91
3/27/2018
JERRY VANHORN
597812
2.00
833.50
5.50
2331.41
3/27/2018
NENG MOUA
597813
0.50
834.00
1.83
2333.24
3/27/2018
MAI VANG
597814
0.50
834.50
1.83
2335.07
3/28/2018
NENG VANG
597815
0.50
835.00
1.83
2336.90
3/28/2018
NENG VANG
597816
0.50
835.50
1.83
2338.73
3/28/2018
KAO VUE
597817
0.50
836.00
1.83
2340.56
3/28/2018
SOUA YANG
597818
0.50
836.50
1.83
2342.39
3/28/2018
SOUA YANG
597819
0.50
837.00
1.83
2344.22
3/29/2018
MAIKIA HER
597820
0.50
837.50
1.83
2346.05
3/29/2018
ARMANDT BOONSTRA
597821
2.00
839.50
5.50
2351.55
3/29/2018
SHER XIONG
597822
0.50
840.00
1.83
2353.38
3/29/2018
MAIKIA HER
597823
0.50
840.50
1.83
2355.21
3/29/2018
SHER XIONG
597824
0.50
841.00
1.83
2357.04
3/29/2018
DUAN FARMS
597825
2.00
843.00
5.50
2362.54
3/29/2018
DUAN FARMS
597826
2.00
845.00
5.50
2368.04
3/29/2018
JOHN LENTZ
597827
0.50
845.50
1.83
2369.87
3/15/2018
MICHAEL NEAL COUNTY
597855
2.50
848.00
6.88
2376.74
3/31/2018
TB YANG FREE
597856
0.50
848.50
1.83
2378.57
3/31/2018
MIDWAY NURSERY
182187
3.00
851.50
8.25
2386.82
3/31/2018
INGLE AND SON
182188
36.00
887.50
99.00
2485.82
3/31/2018
SOIL SUPPLY
182189
100.00
987.50
275.00
2760.82
4/2/2018
DOUA VANG
597828
0.50
988.00
1.83
2762.65
4/2/2018
MAAKIA HER
597829
0.50
988.50
1.83
2764.48
4/2/2018
NENA VANG
597830
0.50
989.00
1.83
2766.31
4/2/2018
EARL TYNDALL
597831
1.00
990.00
2.75
2769.06
4/2/2018
C&K ECP
597832
4.00
994.00
11.00
2780.06
4/2/2018
VAVUE LOR
597833
0.50
994.50
1.83
2781.89
4/2/2018
MOAI VANG
597834
0.50
995.00
1.83
2783.72
4/2/2018
LAKE NORMAN LWNS
597835
5.00
1000.00
13.75
2797.47
4/2/2018
CHONG VANG
597836
0.50
1000.50
1.83
2799.30
4/2/2018
C&K ECP
597837
5.00
1005.50
13.75
2813.05
4/2/2018
NHIA YANG
597838
2.00
1007.60
5.50
2818.55
4/2/2018
DENVER LANDSCAPING
597839
8.00
1015.50
22.00
2840.55
4/2/2018
VAVUE LOR
597840
0.50
1016.00
1.83
2842.38
4/2/2018
TRIA XIONG
597841
0.50
1016.50
1.83
2844.21
4/2/2018
BOUA VANG
597842
0.50
1017.00
1.83
2846.04
4/2/2018
MAI NOUA
597843
0.50
1017.50
1.83
2847.87
4/2/2018
MEE LOR
597844
0.50
1018.00
1.83
2849.70
4/3/2018
JOHN LENTZ
597845
0.50
1018.50
1.83
2851.53
4/3/2018
ROCK BRANCH BG
597846
20.00
1038.50
55.00
2906.53
4/3/2018
NAOKOR VANG
597847
0.50
1039.00
1.83
2908.36
4/3/2018
CHONG CHANG
597848
0.50
1039.50
1.83
2910.19
4/4/2018
DOUA VANG 15978491
0.50
1040.00
1.83
2912.02

4/4/2018
BLIA XIONG
597850
0.50
1040.50
1.83
2913.85
4/4/2018
MIAKIA HER
597851
0.50
1041.00
1.83
2915.68
4/4/2018
C&K ECP
597852
3.00
1044.00
8.25
2923.93
4/4/2018
SAM KEENER
597853
1.00
1045.00
2.75
2926.68
4/4/2018
LONNIE WHITE
597854
4.00
1049.00
11.00
2937.68
4/5/2018
DOUA VANG
597857
0.50
1049.50
1.83
2939.51
4/5/2018
BLIA XIONG
597858
0.50
1050.00
1.83
2941.34
4/5/2018
ARMANDT BOONSTRA
597859
2.00
1052.00
5.50
2946.84
4/5/2018
SAM KEENER
597860
0.50
1052.50
1.83
2948.67
4/5/2018
KEVIN ANNAS
597861
4.00
1056.50
11.00
2959.67
4/5/2018
RICHARD RIOS FREE
597862
1.00
1057.50
2.75
2962.42
4/5/2018
CHOU YANG
597863
0.50
1058.00
1.83
2964.25
4/6/2018
MIAKIA HER
597864
0.50
1058.50
1.83
2966.08
4/6/2018
NENG YANG
597865
0.50
1059.00
1.83
2967.91
4/6/2018
DOUA VANG
597866
0.50
1059.50
1.83
2969.74
4/6/2018
BAO VUE
597867
1.00
1060.50
2.75
2972.49
4/6/2018
LAKE NORMAN LWNS
597868
5.00
1065.50
13.75
2986.24
4/6/2018
ARMANDT BOONSTRA
597869
2.00
1067.50
5.50
2991.74
4/6/2018
TEU LO
597870
0.50
1068.00
1.83
2993.57
4/9/2018
MEE THAO
597871
0.50
1068.50
1.83
2995.40
4/10/2018
PEGGY GRANT
597872
6.00
1074.50
16.50
3011.90
4/10/2018
NENG YANG
597873
0.50
1075.00
1.83
3013.73
4/10/2018
MIAKIA HER
597874
0.50
1075.50
1.83
3015.56
4/10/2018
DOUA VANG
597875
0.50
1076.00
1.83
3017.39
4/10/2018
PAY THAO
597876
0.50
1076.50
1.83
3019.22
4/10/2018
PEGGY GRANT
597877
6.00
1082.50
16.50
3035.72
4/10/2018
DUAN FARMS
597878
2.00
1084.50
5.50
3041.22
4/10/2018
CHONG YANG
597879
0.50
1085.00
1.83
3043.05
4/10/2018
DOUA VANG
597880
0.50
1085.50
1.83
3044.88
4/10/2018
DUAN FARMS
597881
2.00
1087.50
5.50
3050.38
4/11/2018
KEVIN ANNAS
597882
2.00
1089.50
5.50
3055.88
4/11/2018
BLIA XIONG
597883
0.50'
1090.00
1.83
3057.71
4/11/2018
DUAN FARMS
597884
2.00
1092.00
5.50
3063.21
4/12/2018
ROCK BRANCH BG
597885
24.00
1116.00
66.00
3129.21
4/12/2018
DUAN FARMS
597886
2.00
1118.00
5.50
3134.71
4/12/2018
KEVIN ANNAS BOGO
597887
2.00
1120.00
5.50
3140.21
4/11/2018
DUAN FARMS
597888
2.00
1122.00
5.50
3145.71
4/13/2018
DOUA VANG
597889
0.50
1122.50
1.83
3147.54
4/13/2018
ARMANDT BOONSTRA
597890
2.00
1124.50
5.50
3153.04
4/13/2018
RONALD AUSTIN
597891
0.50
1125.00
1.83
3154.87
4/13/2018
MAY YANG
597892
0.50
1125.50
1.83
3156.70
4/13/2018
VOID
597893
0.00
1125.50
0.00
3156.70
4/13/2018
GREG GOODSON
597894
1.50
1127.00
4.13
3160.82
4/16/2018
ROCK BRANCH BG
597895
24.00
1151.00
66.00
3226.82
4/1712018
LEE YANG
597896
0.50
1151.50
1.83
3228.65
4/17/2018
CHONG VANG
597897
0.50
1152.00
1.83
3230.48
4/17/2018
DUAN FARMS
597898
2.00
1154.00
5.50
3235.98

4/17/2018
DUAN FARMS
597899
2.00
1156.00
5.50
3241.48
4/17/2018
DUAN FARMS
597900
2.00
1158.00
5.50
3246.98
4/17/2018
YOUR YANG
597901
0.50
1158.50
1.83
3248.81
4/1712018
LEE YANG
597902
0.50
1159.00
1.83
3250.64
4/18/2018
LAKE NORMAN
597903
25.00
1184.00
68.75
3319.39
4/19/2018
ARMANDT BOONSTRA
597904
2.00
1186.00
5.50
3324.89
4/19/2018
YENG XIONG
597905
1.00
1187.00
2.75
3327.64
4/19/2018
JAMES WITHERS CITY
597906
1.00
1188.00
2.75
3330.39
4/20/2018
ROCK BRANCH BG
597907
24.00
1212.00
66.00
3396.39
4/20/2018
ARMANDT BOONSTRA
597908
2.00
1214.00
5.50
3401.89
4/2012018
SEE YANG
597909
0.50
1214.50
1.83
3403.72
4/20/2018
JONATHAN MOUA
5979101
0.50
1215.00
1.83
3405.55
4/23/2018
CHUDA DHIMAL
597911
10.00
1225.00
27.50
3433.05
4/25/2018
ARMANDT BOONSTRA
597912
2.00
1227.00
5.50
3438.55
4/27/2018
SOUA YANG
597913
0.50
1227.50
1.83
3440.38
4/27/2018
RICHARD RIOS FREE
597914
1.00
1228.50
2.75
3443.13
4/27/2018
SOUA YANG
597915
0.50
1229.00
1.83
3444.96
4/30/2018
SAI LOTAKOON
597916
1.00
1230.00
2.75
3447.71
4/30/2018
ARMANDT BOONSTRA
597917
2.00
1232.00
5.50
3453.21
4/30/2018
DUAN FARMS
597918
2.00
1234.00
5.50
3458.71
4/30/2018
MIDWAY NURSERY
182190
21.00
1255.00
57.75
3516.46
4/30/2018
SOIL SUPPLY
182191
150.00
1405.00
412.50
3928.96
4/30/2018
CREATIVE LANDSCAPE
182192
15.00
1420.00
41.25
3970.21
4/30/2018
SIGMON'S
182193
3.00
1423.00
8.25
3978.46
5/1/2018
LT LINGLE BOGO
597919
93.00
1516.00
225.75
4204.21
5/1/2018
ARMANDT BOONSTRA
597920
2.00
1518.00
5.50
4209.71
5/1/2018
CHONG CHANG
597921
0.50
1518.50
1.83
4211.54
5/1/2018
RONNIE WILLIAMS
597922
1.00
1519.50
2.75
4214.29
5/1/2018
WILLIAM STUTTS
597923
4.00
1523.50
11.00
4225.29
5/2/2018
GABRIEL MURPHY
597924
0.50
1524.00
1.83
4227.12
5/2/2018
THOR LOR
597925
0.50
1524.50
1.83
4228.95
5/2/2018
ARMANDT BOONSTRA
597926
2.00
1526.50
5.50
4234.45
5/3/2018
CHER LEE
597927
0.50
1527.00
1.83
4236.28
5/4/2018
WILLIAM JOHNSON
597928
1.00
1528.00
2.75
4239.03
5/4/2018
PAO THAO
597929
0.50
1528.50
1.83
4240.86
5/7/2018
ROCK BRANCH BG
597930
24.00
1552.50
66.00
4306.86
5/8/2018
PEGGY GRANT
597931
6.00
1558.50
16.50
4323.36
5/9/2018
TOWN OF MAIDEN
597932
5.00
1563.50
13.75
4337.11
5/10/2018
DELLINGER GRADING
597933
10.00
1573.50
27.50
4364.61
5/10/2018
RAY FRANKLIN
597934
0.50
1574.00
1.83
4366.44
5/10/2018
RICHARD RIOS FREE
597935
2.00
1576.00
5.50
4371.94
5/11/2018
ROCK BRANCH BG
597936
24.00
1600.00
66.00
4437.94
5/11/2018
MAIKI HER
597937
0.50
1600.50
1.83
4439.77
5/11/2018
JIM OSTWALT
597938
2.00
1602.50
5.50
4445.27
5/11/2018
GENE WESSON
597939
3.00
1605.50
8.25
4453.52
5/11/2018
DENVER LANDSCAPING
597940
4.00
1609.50
11.00
4464.52
5/14/2018
SOUA VUE
597941
0.50
1610.00
1.83
4466.35

5/15/2018
CHOU YANG
5979427
0.50
1610.50
1.83
4468.18
5/16/2018
ARMANDT BOONSTRA
597943
0.50
1611.00
1.83
4470.01
5/22/2018
PERENNIAL GROVES BG
597944
10.00
1621.00
27.50
4497.51
5/24/2018
DOUA VANG
597945
0.50
1621.50
1.83
4499.34
5/24/2018
LONNIE DEAL
597946
5.00
1626.50
13.75
4513.09
5/29/2018
MIKE NEAL
597947
2.50
1629.00
6.88
4519.97
5/30/2018
MIKE NEAL
597948
2.50
1631.50
6.88
4526.85
5/31/2018
INGLE AND SON
182194
73.00
1704.50
200.75
4727.60
5/31/2018
NATURE'S EDGE
182195
28.00
1732.50
77.00
4804.60
5/31/2018
SIGMON'S @2.53
182196
68.00
1800.50
187.00
4991.60
5/31/2018
SOIL SUPPLY @1.50
182197
53.00
1853.50
145.75
5137.35
6/4/2018
JOHNNY REITZEL
597949
1.00
1854.50
2.75
5140.10
6/5/2018
NELSON CANIPE
597950
3.00
1857.50
8.25
5148.35
6/6/2018
LEE LAWING
597951
1.00
1858.50
2.75
5151.10
6/6/2018
LEE LAWING
597952
1.00
1859.50
2.75
5153.85
6/7/2018
NELSON CANIPE
597953
3.00
1862.50
8.25
5162.10
6/8/2018
NELSON CANIPE
597954
3.00
1865.50
8.25
5170.35
6/8/2018
BELMI PILIR
597955
0.50
1866.00
1.83
5172.18
6/8/2018
SUA THOR
597956
0.50
1866.50
1.83
5174.01
6/8/2018
RICHARD RIOS FREE
597957
1.00
1867.50
2.75
5176.76
6/11/2018
NELSON CANIPE
597958
3.00
1870.50
8.25
5185.01
6/11/2018
LAKE NORMAN
597959
6.00
1876.50
16.50
5201.51
6/11/2018
LEE LAWING
597960
1.00
1877.50
2.75
5204.26
6/13/2018
ARMANDT BOONSTRA
597961
2.00
1879.50
5.50
5209.76
6/14/2018
NELSON CANIPE
597962
3.00
1882.50
8.25
5218.01
6/14/2018
GREG POWER
597963
1.00
1883.50
2.75
5220.76
6/15/2018
NELSON CANIPE
597964
3.00
1886.50
8.25
5229.01
6/15/2018
PA YANG
597965
0.50
1887.00
1.83
5230.84
6/15/2018
GREG POWER
597966
1.00
1888.00
2.75
5233.59
6/18/2018
XAI XIONG
597967
0.50
1888.50
1.83
5235.42
6/18/2018
CHONG CHONG
597968
0.50
1889.00
1.83
5237.25
6/19/2018
NENG YANG
597969
0.50
1889.50
1.83
5239.08
6/19/2018
KEVIN ANNAS BOGO
597970
4.00
1893.50
11.00
5250.08
6/21/2018
CHIA VUE
597971
1.00
1894.50
2.75
5252.83
6/25/2018
NELSON CANIPE
597972
3.00
1897.50
8.25
5261.08
6/25/2018
US LAWNS
597973
2.00
1899.50
5.50
5266.58
6/26/2018
DENEVER LANDSCAPE
597974
4.00
1903.50
11.00
5277.58
6/26/2018
GREG POWER
597975
1.00
1904.50
2.75
5280.33
6/29/2018
INGLE AND SON
182198
45.00
1949.50
123.75
5404.08
6/29/2018
NATURE'S EDGE
182199
48.00
1997.50
132.00
5536.08
6/29/2018
SIGMON'S @2.53
182200
65.00
2062.50
178.75
5714.83
6/29/2018
SOIL SUPPLY @ 1.50
925851
12.00
2074.50
33.00
5747.83
6/29/2018
LT LINGLE BOGO
925852
55.00
2129.50
151.25
5899.08
6/29/2018
MIDWAY NURSERY
985253
9.00
2138.50
24.75
5923.83
2138.50
5,923.83

REGIONAL COMPOST FACILITY
MARKET AUDIT 2018 - 2019
July 1, 2018 - June 30, 2019
REC
NUM
SOPS
SOLD
TO
SCPS
YDS
SOLD
TOT
YDS
DATE
NAME
7/2/2018
SHUE THAO
597976
0.50
0.50
1.83
1.83
7/5/2018
LAMANG CHANG
597977
1.00
1.50
2.75
4.58
7/6/2018
NELSON CANIPE
597978
3.00
4.50
8.25
12.83
7/6/2018
RICHARD RIOS FREE
597979
4.00
8.50
11.00
23.83
7/9/2018
PEGGY GRANT
597980
6.00
14.50
16.50
40.33
7/9/2018
DUAN FARMS
597981
2.00
16.50
5.50
45.83
7/10/2018
CHONG
597982
0.50
17.00
1.83
47.66
7/11/2018
ARMANDT BOONSTRA
597983
2.00
19.00
5.50
53.16
7/13/2018
NENG YANG
597984
0.50
19.50
1.83
54.99
7/18/2018
NELSON CANIPE
597985
3.00
22.50
8.25
63.24
711912018
KEVIN ANNAS BOGO
597986
4.00
26.50
11.00
74.24
7/25/2018
JEFF LINK
597987
1.00
27.50
2.75
76.99
7/25/2018
JAMES SCOTT
597988
2.00
29.50
5.50
82.49
7/25/2018
JAMES SCOTT
597989
2.00
31.50
5.50
87.99
7/25/2018
JAMES SCOTT
597990
2.00
33.50
5.50
93.49
7/26/2018
JAMES SCOTT
597991
2.00
35.50
5.50
98.99
7/26/2018
JAMES SCOTT
597992
2.00
37.50
5.50
104.49
7/26/2018
JAMES SCOTT
597993
2.00
39.50
5.50
109.99
7/26/2018
JAMES SCOTT
597994
2.00
41.50
5.50
115.49
7/30/2018
KEVIN ANNAS BOGO
597995
8.00
49.50
22.00
137.49
7/30/2018
US LAWNS
597996
1.00
50.50
2.75
140.24
7/31/2018
SOIL SUPPLY @ 1.50
71800
161.00
211.50
442.75
582.99
7/31/2018
NATURE'S EDGE
71801
188.00
399.50
517.00
1099.99
7/31/2018
INGLE AND SON
71802
65.00
464.50
178.75
1278.74
7/31/2018
LT LINGLE @ 2.53
71803
34.00
498.50
93.50
1372.24
7/31/2018
SIGMON'S @2.53
71804
180.00
678.50
495.00
1867.24
8/1/2018
PERENNIAL GROVES 5
597997
10.00
688.50
27.50
1894.74
8/3/2018
US LAWNS
597998
2.00
690.50
5.50
1900.24
8/6/2018
CHONG MOUA
597999
0.50
691.00
1.83
1902.07
8/6/2018
ARMANDT BOONSTRA
597800
2.00
693.00
5.50
1907.57
8/6/2018
LUE YANG
804001
0.50
693.50
1.83
1909.40
8/7/2018
US LAWNS
804002
2.00
695.50
5.50
1914.90
8/8/2018
LAKE NORMAN
804003
10.00
705.50
27.50
1942.40
8/8/2018
LAKE NORMAN
804004
5.00
710.50
13.75
1956.15
8/10/2018
JOUA HER
804005
0.50
711.00
1.83
1957.98

8/10/2018
MAO XIONG
804006
1.00
712.00
2.75
1960.73
8/14/2018
PAUL ELLER
804007
1.00
713.00
2.75
1963.48
8/15/2018
ARMANDT BOONSTRA
804008
2.00
715.00
5.50
1968.98
8/17/2018
NENG YANG
804009
0.50
715.50
1.83
1970.81
8/17/2018
CE VANG
804010
0.50
716.00
1.83
1972.64
8/20/2018
JOUA HER
804011
0.50
716.50
1.83
1974.47
8/22/2018
PERENNIAL GROVES 5
804012
10.00
726.50
27.50
2001.97
8/24/2018
BLIA XIONG
804013
0.50
727.00
1.83
2003.80
8/24/2018
WESSON
804014
6.00
733.00
16.50
2020.30
8/28/2018
ARMANDT BOONSTRA
8040151
2.00
735.00
5.50
2025.80
8/31/2018
ARMANDT BOONSTRA
804016
2.00
737.00
5.50
2031.30
8/31/2018
ROCK BRANCH
804017
24.00
761.00
66.00
2097.30
8/20/2018
TB YANG
804030
1.00
762.00
2.75
2100.05
8/31/2018
INGLE AND SON
925864
74.00
836.00
203.50
2303.55
8/31/2018
SIGMON'S @2.53
925865
100.00
936.00
275.00
2578.55
8/31/2018
US LAWNS 925868
925866
35.00
971.00
96.25
2674.80
8/31/2018
SOIL SUPPLY @ 1.50
925867
9.00
980.00
24.75
2699.55
8/31/2018
CREATIVE
925869
5.00
985.00
13.75
2713.30
8/31/2018
M&M BARK
925859
324.00
1309.00
891.00
3604.30
9/4/2018
JOHN LENTZ
804018
1.00
1310.00
2.75
3607.05
9/5/2018
JOHN LENTZ
804019
1.00
1311.00
2.75
3609.80
9/5/2018
PERENNIAL GROVES 5
804020
10.00
1321.00
27.50
3637.30
9/6/2018
RAY FRANKLIN
804021
0.50
1321.50
1.83
3639.13
9/7/2018
RAY FRANKLIN
804022
0.50
1322.00
1.83
3640.96
9/13/2018
RAUL DURAN
804023
3.00
1325.00
8.25
3649.21
9/14/2018
DENVER LANDSCAPE
804024
4.00
1329.00
11.00
3660.21
9/19/2018
KHANG CHOU VUE
804025
0.50
1329.50
1.83
3662.04
9/20/2018
RAUL DURAN
804026
2.00
1331.50
5.50
3667.54
9/20/2018
RAUL DURAN
804027
6.00
1337.50
16.50
3684.04
9/20/2018
KEVIN ANNAS BOGO
804028
4.00
1341.50
11.00
3695.04
9/20/2018
KEVIN ANNAS BOGO
804029
4.00
1345.50
11.00
3706.04
9/21/2018
LAKE NORMAN
804030
5.00
1350.50
13.75
3719.79
9/21/2018
LAKE NORMAN
804030
5.00
1355.50
13.75
3733.54
DELLINGER GRADING
804031
6.00
1361.50
16.50
3750.04
DENVER LANDSCAPE
804032
4.00
1365.50
11.00
3761.04
K
MAI MOUA
804033
0.50
1366.00
1.83
3762.87
INGLE AND SON
925870
53.00
1419.00
145.75
3908.62
9/28/2018
LT LINGLE @ 2.53
925872
30.00
1449.00
82.50
3991.12
10/2/2018
RAUL DURAN
804034
6.00
1455.00
16.50
4007.62
10/4/2018
NELSON CANIPE
804035
5.00
1460.00
13.75
4021.37
10/4/2018
US LAWNS
804036
2.00
1462.00
5.50
4026.87
10/5/2018
CHARLES YODER
804037
0.50
1462.50
1.83
4028.70
10/8/2018
PEGGY GRANT
804038
6.00
1468.50
16.50
4045.20
10/8/2018
DEWEY GRANT
804039
4.00
1472.50
11.00
4056.20
10/8/2018
PEGGY GRANT
804040
6.00
1478.50
16.50
4072.70
10/8/2018
LAKE NORMAN
804041
5.00
1483.50
13.75
4086.45
10/9/2018
PAUL CAMPBELL
804042
2.00
1 1485.50
5.50
4091.95

10/12/2018
JAMES SCOTT
804043
2.00
1487.50
5.50
4097.45
10/15/2018
DENVER LANDSCAPE
804044
4.00
1491.50
11.00
4108.45
10/15/2018
PEGGY GRANT
804045
6.00
1497.50
16.50
4124.95
10/15/2018
JIMMY HEDRICK
804046
2.00
1499.50
5.50
4130.45
10/17/2018
JAMES SCOTT
804047
2.00
1501.50
5.50
4135.95
10/19/2018
JAMES SCOTT
804048
2.00
1503.50
5.50
4141.45
10/19/2018
KHANG CHOU VUE
804049
0.50
1504.00
1.83
4143.28
10/19/2018
JAMES SCOTT
804050
2.00
1506.00
5.50
4148.78
10/19/2018
JAMES SCOTT
804051
2.00
1508.00
5.50
4154.28
10/22/2018
DUAN FARMS
804052
4.00
1512.00
11.00
4165.28
10/22/2018
RAUL DURAN
804053
1.00
1513.00
2.75
4168.03
10/29/2018
LAKE NORMAN
804054
15.00
1528.00
41.25
4209.28
10/31/2018
RAUL DURAN
804055
1.00
1529.00
2.75
4212.03
10/31/2018
LT LINGLE @ 2.53
925873
44.00
1573.00
132.00
4344.03
10/31/2018
SIGMON'S @2.53 925879
925876
140.00
1713.00
420.00
4764.03
10/31/2018
INGLE AND SON
925877
43.00
1756.00
118.25
4882.28
10/31/2018
DICKINSON TO LANDFILL
925878
460.50
2216.50
1381.50
6263.78
11/1/2018
RAUL DURAN
804057
1.00
2217.50
2.75
6266.53
11/1/2018
LAKE NORMAN
804058
5.00
2222.50
13.75
6280.28
11/7/2018
LAKE NORMAN
804059
5.00
2227.50
13.75
6294.03
11/7/2018
ARMANDT BOONSTRA
804056
2.00
2229.50
5.50
6299.53
11/16/2018
RAUL DURAN
804060
1.00
2230.50
2.75
6302.28
11 / 1912018
KEVI N AN NAS
804061
2.00
2232.50
5.50
6307.78
11/23/2018
KEVIN ANNAS
804062
2.00
2234.50
5.50
6313.28
11/30/2018
DANNY MEDLOCK
804063
4.00
2238.50
11.00
6324.28
11/30/2018
SOIL SUPPLY @ 1.50
925880
54.00
2292.50
134.00
6458.28
11/30/2018
SIGMON'S @ 2.53
925881
20.00
2312.50
60.00
6518.28
11/30/2018
INGLE AND SON
925882
15.00
2327.50
41.25
6559.53
11/30/2018
DICKINSON TO LANDFILL
925883
216.00
2543.50
648.00
7207.53
11/30/2018
LT LINGLE @ 2.53
925884
12.00
2555.50
36.00
7243.53
11/30/2018
LT LINGLE @ 2.53
925873
0.00
2556.50
0.00
7243.53
12/19/2018
CONLEY HALL
804064
1.00
2556.50
2.75
7246.28
12/27/2018
LAKE NORMAN
804065
5.00
2561.50
13.75
7260.03
12/31/2018
LT LINGLE @ 2.53
925885
45.00
2606.50
123.75
7383.78
12/31/201,8
SOIL SUPPLY @ 1.50
925886
43.00
2649.50
118.25
7502.03
12/31/2018
SIGMON'S @ 2.53
925887
15.00
2664.50
41.25
7543.28
12/31/2018
MURRAY'S HATCHERY
925888
2.00
2666.50
5.50
7548.78
12/31/2018
INGLE AND SON
925889
8.50
2675.00
23.38
7572.16
2675.00
7572.16

•
]EXHIBIT 2
Operations Data and Performance Summary Tables
20

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC VEOLIA WATER NORTH AR
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY - 2018
page 1
BIOSOLIDS RECEIVING
HICKORY - HENRY FORK
HICKORY - NORTHEAST
HICKORY- CATAWBA
MONTH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
No.
gallons
% TS
DT
s.0
Is
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
s.0
Jan.
I 111
721,500
3.93
118.3
5.6
i 79
513,500
3.21
69.7
6.2
0
0
0.0
Feb.
102
663,000
4.04
111.8
5.7
66
429,000
3.73
66.9
6.0
0
0
0.0
Mar.
107
695,500
4.45
129.6
5.3
65
422,500
3.61
64.5
6.1
0
0
0.0
Apr.
113
734,500
4.54
138.7
5.2
60
390,000
3.82
62.1
6.1
0
0
0.0
May
95
617,500
4.37
113.5
5.3
59
383,500
4.24
67.8
6.1
0
0
0.0
Jun.
104
676,000
3.56
100.7
5.3
56
364,000
3.99
60.9
6.2
i 0
0
0.0
Jul.
114
741,000
3.35
102.9
4.9
61
396,500
3.70
61.8
6.2
0
0
0.0
Aug.
112
728,000
3.18
96.67
5.2
62
403,000
4.26
71.3
6.2
0
0
0.0
Sept.
98
637,000
3.67
80.44
5.7
57
370,500
3.94
61.0
6.3
0
0
0.0
Oct.
124
806,000
2.40
81.1
6.1
76
494,000
3.87
80.4
6.3
0
0
0.0
Nov.
104
676,000
3.02
85.2
5.5
67
435,500
4.19
76.4
6.3
1
6,500
2.83
1.5
6.5
Dec.
37
240,500
4.27
42.0
5.3
24
156,000
3.94
26.0
6.3
0
0
0.0
TOTAL
I 1,221
7,936,500
1,201
732
4,758,000
768.7
1
6,500
1.5
AVG.
102
661,375
3.68
100.1
5.4
1 61
396,500
3.88
64.1
6.2
1 0
540
2.83
0.1
6.5
0.00
BIOSOLIDS RECEIVING
CONOVER-NORTHEAST
CONOVER-NEWTON
NEWTON
MONTH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
N
gallons
% S
DT
s.0
No.
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
s.0
Jan.
25
150,000
3.74
23.2
6.2
10
60,000
2.33
5.3
7.7
0
0
0.0
Feb.
21
126,000
3.99
20.8
6.4
1 7
42,000
8.86
15.5
7.5
0
0
0.0
Mar.
24
144,000
4.08
24.5
6.1
13
78,000
7.08
23.1
6.8
0
0
0.0
Apr.
21
126,000
3.44
18.2
6.1
10
60,000
6.79
17.0
7.0
i 0
0
0.0
May
14
84,000
3.44
12.2
6.2
12
72,000
4.76
14.4
7.0
0
0
0.0
Jun.
14
84,000
3.85
13.9
6.3
9
54,000
3.17
7.4
7.0
0
0
0.0
Jul.
17
102,000
2.98
13.2
7.1
2
12,000
3.76
1.9
7.4
1 0
0
0.0
Aug.
12
72,000
3.32
10.0
0.5
16
96,000
4.60
18.6
7.8
0
0
0.0
Sept.
13
78,000
3.U5
10.5
7.1
14
84,000
2.83
10.2
7.5
0
0
0.0
Oct.
18
108,000
3.40
15.6
6.7
10
60,000
4.53
11.4
1.0
1 0
0
0.0
Nov.
15
90,000
3.42
12.9
6.5
12
72,000
2,95
8.4
7.5
1 0
0
0.0
Dec.
4
24,000
3.99
4.0
6.3
5
30,000
6.71
8.1
6.9
0
0
0.0
TOTAL:
198
1,188,000
178.9
120
720,000
141.1
0
0
0.0
AVG.
16.5
99,000
3.57
14.9
6.0
10
60,000
4.86
11.8
7.2
0
0
0.0

AERICA C
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY- 2018
page 2
BIOSOLIDS RECEIVING
CITY OF HICKORY WATER PLANT
CATAWBA COUNTY SEPTAGE
CATAWBA COUNTY- CLAREMONT - NORTH
DATE
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
No.
gallons
% TS
DT
s.0
No,
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
s.0
Jan.
0
0
0.00
0
0 0.00
4
18,400
2.51
2.01
6.5
Feb.
0
0
0.00
0
0 0.00
2
9,200
2.70
1.04
6.4
Mar.
0
0
0.00
0
0 0.00
3
12,600
2.48
1.26
6.0
Apr.
0
0
0.00
0
0 0.00
3
11,500
3.19
1.58
5.9
May
? 0
0
0.00
0
0 0.00
2
9,000
0.88
0.33
6.7
Jun.
0
0
0.00
0
0 0.00
3
9,500
2.87
1.11
6.9
Jul.
1 0
0
0.00
0
0 0.00
0
0
0.00
Aug.
0
0
0.00
0
0 0.00
3
10,500
2.22
1.22
6.8
Sept.
0
0
0.00
0
0 0.00
2
7,000
2.61
0.76
6.8
Oct.
0
0
0.00
0
0 0.00
3
10,500
2.82
1.27
5.8
Nov.
0
0
0.00
0
0 0.00
0
0
0.00
Dec.
0
0
0.00
0
0 0.00
2
7,000
3.74
1.09
6.9
TOTAL
€ 0
0
0.0
0
0 0.00
27
105,200
11.67
AVG.
2
8,765
2.60
0.97
6.4
BIOSOLIDS RECEIVING
CATAWBA COUNTY - CLAREMONT - MCLIN
CATAWBA COUNTY - MAIDEN
CATAWBA COUNTY -TOTAL
DATE
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
No.
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
SM.
No.
gallons
% TS
DT
S.0
Jan.
0
0
0.00
7
42,000
2.42
4.27
7.0
11
60,400
2.46
6.29
6.7
Feb.
5
32,500
3.53
4.73
6.8
4
24,000
2.96
2.94
6.7
11
65,700
3.13
8.71
6.5
Mar.
7
43,000
2.39
5.15
6.6
13
78,000
2.65
8.74
6.8
23
133,600
2.42
15.15
6.6
Apr.
3
11,500
3.19
1.58
5.9
2
12,000
2.20
1.10
6.7
5
23,500
2.50
2.68
6.2
May
2
13,000
2.79
1.51
7.2
4
24,000
2.22
2.23
7.3
8
46,000
2.03
4.07
7.1
Jun.
3
19,500
1.97
1.59
6.6
0
0
0.00
6
29,000
2.33
2.71
6.7
Jul.
3
19,500
2.59
2.10
6.5
1
6,000
1.68
0.42
7.2
4
25,500
2.36
2.52
6.7
Aug.
0
0
0.00
4
24,000
1.62
1.62
7.0
7
34,500
1.92
2.84
7.0
Sept.
4
26,000
1.82
1.97
6.3
2
12,000
2.89
1.45
7.0
8
45,000
2.44
4.18
6.7
Oct.
0
0
0.00
0
0
0.00
3
10,500
2.82
1.27
5.8
Nov. 1
2
13,000
4.37
2.37
6.4
5
30,000
3.18
4.08
7.1
7
43,000
3.48
6.45
6.9
Dec. 1
0
0
0.00
0
0
0.00
2
7,000
3.74
1.09
6.9
TOTAL
29
178,000
21.0
42
252,000
26.9
95
523,700
58.0
AVG.
2
14,835
2.83
1.8
6.5
3.5
21,000
2.42
2.2
7.0
8
43,642
2.64
4.8
6.7
4

VEOLIA !HATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY- 2013
page 3
BIOSOLIDS RECEIVING
CONOVER TOTAL
HICKORY TOTAL
PROJECT TOTAL
DATE
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
TRUCK
VOLUME
SOLIDS
MASS
pH
No.
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
s.0
No.
gallons
% TS
DT
s.0
Jan.
35
210,000
3.24
28.5
6.7
190
1,235,000
3.58
188.0
5.9
240
1,505,400
3.50
222.8
6.2
Feb.
28
168,000
5,05
36.3
6.6
168
1,092,000
3.92
178.7
5.8
209
1,325,700
4.07
223.7
6.1
Mar.
37
222,000
4.99
47.6
6.3
172
1,118,000
4.12
194.1
5.7
235
1,473,600
4.13
256.9
6.0
Apr.
31
186,000
4.35
35.1
6.3
173
1,124,500
4.28
200.8
5.6
212
1,334,000
4.27
238.6
5.8
May
26
156,000
4.01
26.6
6.5
154
1,001,000
4.30
181.3
5.7
190
1,203,000
4.19
211.9
6.0
Jun.
23
138,000
3.63
21.3
6.6
160
1,040,000
3.71
161.4
5.8
192
1,207,000
3.66
185.4
6.0
Jul.
19
114,000
3.03
15.1
7.1
182
1,183,000
3.45
169.6
5.6
205
1,322,500
3.40
187.2
5.9
Aug.
28
168,000
3.96
28.6
7.2
174
1,131,000
3.59
168.0
5.7
212
1,333,600
3.62
199.4
6.1
Sept. t
27
162,000
3.05
20.7
7.2
155
1,007,500
3.35
141.4
5.9
192
1,214,600
3.26
166.3
6.3
Oct.
28
168,000
3.84
27.0
6.8
201
1,306,500
2.94
162.3
6.2
235
1,485,000
3.05
190.5
6.3
Nov.
27
162,000
3.22
21.3
7.0
173
1,124,500
3.45
163.2
5.8
207
1,329,500
3.44
190.9
6.2
Dec.
9
54,000
5.35
12:0
6.6
i 61
396,500
4.11
68.0
5.8
1 74
457,500
5.28
81.1
7.0
TOTAL i
318
1,908,000
320,0
1963
12,759,500
1,977
2,403
15,191,200
2,355
AVG.
27
159,000
3.94
26.7
6.7
163.6
1,063,290
3.73
164.7
5.8
200
1,265,931
3.82
196.2
6.2
AMENDMENT HANDLING
WOOD AMENDMENTS
DRYING AGENT
AMENDMENT RECIPE
DATE
TRUCKS
MASS
SOLIDS
DENSITY
VOLUME
TRUCKS
MASS
SOLIDS
DENSITY
VOLUME
DISCHARGE
MASS
SOLIDS
DENSITY
VOLUME
No.
WT
%TS
Ib/ft3
yd3
I No.
WT
I %TS
Ib/ft3
yd3
hours
DT
%TS
Ib/ft3
yd3
Jan.
19
433.9
63.2
15.4
2,097
0
0.0
0
156
344
60.0
15.8
2,689
Feb.
16
368.6
60.6
18.4
1,491
0
0.0
0
135
337
55.9
19.1
2,350
Mar.
21
523.6
60.2
17.8
2,182
0
0.0
0
150
406
57.7
18.8
2,799
Apr.
21
214.0
58.5
18.8
837
0
0.0
0
169
403
57.5
18.9
2,798
May
26
387.2
61.3
17.9
1,645
0
0.0
0
229
402
59.2
17.8
2,890
Jun.
26
420.9
59.0
17.9
1,731
0
0.0
0
230
343
55.7
18.3
2,520
Jul.
26
617.6
58.9
18.1
2,548
0
0.0
0
232
387
60.4
17.3
2,783
Aug.
36
847.4
57.9
16.3
3,950
0
0.0
0
199
365
58.8
17.0
2,784
Sept.
28
673.1 1
55.3
16.4
3,051
0
0.0
0
173
290
57.4
16.7
2,293
Oct.
42
1,014.8
58.9
15.5
4,916
0
0.0
0
162
296
54.9
17.4
2,354
Nov.
18
452.3
56.5
17.4
1,966
0
0.0
0
121
296
54.1
19.4
2,108
Dec.
7
172.3
61.0
14.8
867
0
0.0
0
25
69
51.0
18.0
587
TOTAL 1
286
6,126
27,281
0
0
0
1,981
3,938
28,955
AVG.
24
510.5
59.3
17.1
2,273
165
328
56.9
17.9
2,413

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY- 2018
page 4
BIOSOLIDS DEWATERING
BLENDED BIOSOLIDS
CENTRIFUGE
DEWATERED SOLIDS
DATE
FEED
SOLIDS
MASS
MASS
AMENDMENT SERVICE
POLYMER
POLYMER
DOSAGE
COST
CTR.FUGEI
BFP2CAKE
I AVG. CAKE
I CENTRATE1
CAPTURE
g d
%TS
DT
WT
yd3
hours
gals
Ibs
lb/DT
$DT
CAKE %TS
%TS
I %TS
I Mg/L
I %
Jan.
2,054,795
3.09
264.3
8,568
0
156
50,703
4,541
19.4
$20.7
22.4
22.4
0.34
90.1
Feb.
1,736,090
3.63
262.7
7,239
0
136
49,553
4,326
20.5
$18.1
! 24.3
24.3
0.27
93.6
Mar.
1,970,431
3.78
312.3
8,217
0
150
44,774
5,342
19.2
$16.8
25.3
25.3
0.31
92.8
Apr.
1,900,518
3.91
311.0
7,925
0
169
60,406
4,428
17.8
$15.6
23.5
24.1
0.33
92.6
May
1,836,466
3.99
311.7
7,775
0
222
108,629
5,472
19.1
$16.0
22.3
26.6
26.1
0.19
95.8
Jun.
1,730,234
3.66
263.5
7,215
0
230
111,995
5,169
20.6
$17.5
31.6
23.9
24.7
0.17
96.1
Jul.
2,042,709
3.57
304.7
8,518
0
232
61,016
3,682
10.5
$13.9
i
23.6
23.6
0.18
95.7
Aug.
1,815,978
3.72
280.4
7,573
0
187
54,550
1,365
4.8
$6.8
i 23.0
25.0
24.6
0.20
95.4
Sept.
1,591,406
3.37
223.1
6,636
0
173
46,000
2,300
10.3
$14.6
21.8
21.8
0.14
96.6
Oct.
1,894,844
2.91
227.9
7,901
0
162
38,527
1,646
7.8
$11.1
i 24.4
19.1
21.6
0.13
96.2
Nov.
1,726,175
3.16
228.5
7,198
0
121
30,380
760
4.3
$6.2
24.1
24.1
0.20
94.3
Dec.
332,222
3.79
52.7
1,385
0
25
5,218
197
4.7
$6.6
24.8
24.8
0.32
92.6
TOTAL
20,631,868
3,043
86,150
0
': 1,962
661,751
39,228
AVG.
1,719,322
3.55
253.6
7,179
0
164
55,146
3,269
13.3
$13.7
24.6
23.3
24.0
0.23
94.3
AMENDMENT / BIOSOLIDS BLEND
BLENDED AMENDMENT
CENTRIFUGE CAKE
AMENDMENT/BIOSOLIDS
DATE
DOSAGE
MASS
SOLIDS
DENSITY
VOLUME
DOSAGE
MASS
SOLIDS
DENSITY
VOLUME
DOSAGE
MASS
VOLUME
A/B RATIO
AB RATIO
yd3/DT
DT
%TS
Ib/ft3
yd3
d3/DT
WT
%TS
Ib/ft3
yd31DT
WT
yd3
Ib/lb
yd3lyd3
Jan.
0.0
0.0
0
10.3
1,176
22.4
31.8
2,799
10.3
1,750
5,488
0.49
1.0
Feb.
0.0
0.0
0
9.0
1,081
24.3
30.6
2,677
9.0
1,684
5,027
0.56
0.9
Mar.
0.0
0.0
0
9.0
1,238
25.3
32.1
2,904 1
9.0
1,945
5,703
0.57
1.0
Apr.
0.0
0.0
0
8.9
1,306
24.1
35.0
2,797 's
8.9
2,011
5,595
0.54
1.0
May
0.0
0.0
0
9.3
1,196
26.2
34.3
2,608
9.3
1,880
5,498
0.57
1.1
Jun.
0.0
0.0
0
9.5
1,071
24.7
35.3
2,263 €
9.5
1,690
4,782
0.58
1.1
Jul.
0.0
0.0
0
9.2
1,303
23.6
36.7
2,629
9.2
1,955
5,412
0.51
1.1
Aug.
0.0
0.0
0
9.8
1,175
24.6
34.0
2,609
9.8
1,804
5,393
0.55
1.1
Sept.
0.0
0.0
0
10.2
1,040
21.8
32.3
2,395 ?
10.2
1,551
4,688
0.50
1.0
Oct.
0.0
0.0
0
10.3
1,057
21.6
35.5
2,210
10.3
1,605
4,564
0.52
1.1
Nov.
0.0
0.0
0
9.2
954
24.1
37.4
1,900
9.2
1,506
4,008
0.58
1.1
Dec.
0.0
0.0
0
10.6
210
24.8
41.0
376
10.6
357
964
0.65
1.5
TOTAL
0.0
0.0
0
12,807
28,167 1
19,738
57,122
AVG.
9.6
1,067
24.0
34.7
2,347
9.6
1,645
4,760
0.55
1.1

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY - 2018
page 5
IN -FEED COMPOST MIXTURE
INFEED MIXING
INLET
RAM FEED PITS
JOUTLET I
TIME AND TEMPERATURE
DATE
RUN TIME
MASS
SOLIDS
DENSITY
VOLUME
VOLUME
SERVICE
PUSHES
PUSH
VOLUME
L SRT
UC SRT
AC SRT
PFRP
VAR
hours
WT
%TS
Ib/0
yd3
yd3
No.
No.
inches
yd3,
days
I days
days
deg. C
deg. C
Jan.
156.0
1,820
43.0
24.6
5,488
6,068
4
232
16
2,697 ?
26.2
23.8
21.8
67.5
64.4
Feb.
134.0
1,649
42.8
24.3
5,027 i
5,615
4
199
16
2,496 i
27.2
23.3
21.3
66.6
65.2
Mar.
150.0
1,844
43.9
24.0
5,703
6,197
4
229
16
2,754
25.2
23.3
21.3
68.5
66.6
Apr.
i 169.0
1,795
46.1
23.8
5,695 's
6,248
4
236
16
2,777 €
27.3
25.5
23.3
69.1
66.2
May
i 222.0
1,688
43.5
22.7
5,498
5,829
4
230
16
2,591
24.4
23.8
21.8
68.0
65.3
Jun.
`: 230.0
1,458
44.9
22.4
4,782 i
5,037
4
235
16
2,239 i
23.6
26.8
24.6
66.7
65.2
Jul.
'. 232.0
1,608
45.6
21.9
5,412
5,926
4
265
16
2,634
21.9
23.3
21.3
69.0
66.4
Aug.
190.0
1,754
41.8
24.0
5,393 i
5,393
4
222
16
2,397
28.9
30.2
27.6
68.9
66.1
Sept.
173.0
1,378
43.1
21.7
4,688
5,050
4
254
16
2,245 s
21.3
26.5
24.2
67.7
65.4
Oct.
! 162.0
1,389
42.2
22.5
4,564 !
4,932
4
255
16
2,192
20.4
22.4
20.5
62.9
55.1
Nov.
121.0
1,431
40.0
26.4
4,008
4,304
4
163
16
1,913 (
32.1
29.5
27.0
67.2
63.0
Dec.
25.0
332
39.4
25.1
964
995
4
39
16
442 1
75.9
87.7
80.3
61.3
60.2
TOTAL
1,964
18,146
57,122 1
61,594
2,559
27,377
AVG.
163.7
1512
43.0
23.6
4,760 i
5,133
4
213
16
2,281 €
29.5
30.5
27.9
67.0
64.1
IN -VESSEL BIOSOLIDS COMPOSTING
TUNNEL REACTOR NO.1
DATE
PUSHES
SRT
AIRFLOW1
TEMP 1
I TEMP 2
1 TEMP 3
1 TEMP 4
1 TEMP 5
1 TEMP 6
1 TEMP 7
1 TEMP AVG
PFRP
VAR
DISCHRG
SOLIDS
No.
days
clm
deg. C
deg. C
deg. C
deg. C
deg. C
deg. C
deg. C
deg. C
deg. C
deg. C
yd3
%TS
Jan.
58
23.6
4,180
64.4
67.6
65.5
66.6
61.1
57.9
47.6
62.6
65.9
63.9
609
51.6
Feb.
51
21.6
3,515
61.9
63.0
59.6
66.9
67.4
59.5
53.1
62.0
61.5
63.0
536
50.4
Mar.
57
22.2
4,114
67.6
68.3
67.6
64A
65.6
60.7
53.8
64.8
67.8
65.7
599
49.0
Apr.
59
24.4
3,364 €
73.0
70.8
68.7
66.4
64.4
49.2
56.2
64.8
70.8
65.4
620
54.7
May
57
22.5
4,036
68.5
67.6
66.4
68.2
64.5
55.4
51.3
64.1
67.5
65.1
599
56.6
Jun.
58
25.3
3,752
61.0
65.9
61.9
63.6
66.4
55.8
45.5
62.0
62.9
62.4
609
55.6
Jul.
67
20.7
4,127
70.4
70.8
70.6
68.6
66.5
66.0
62.1
68.4
70.6
68.8
704
53.4
Aug.
55
30.1
4,277 i
72.0
69.0
70.2
68.9
65.8
61.6
62.6
67.4
70.4
67.9
578
54.0
Sept.
63
26.0
4,047
70.4
65.2
72.7
65.6
66.6
62.1
63.4
66.6
69.4
67.1
662
51.4
Oct.
64
24.2
4,289 i
69.6
66.3
65.3
65.9
67.9
62.3
65.4
66.1
67.1
66.2
672
52.0
Nov. j
37
28.9
4,788
61.6
60.0
62.6
65.4
64.7
62.4
50.3
62.4
61.4
62.8
389
53.6
Dec.
2
19.3
4,303
47.2
49.4
62.0
58.9
62.2
67.9
52.0
66.5
52.9
56.7
21
49.6
TOTAL `:
628
6,598
AVG. s
52
24.1
4,066
65.6
65.3
66.1
65.8
65.3
60.1
55.3
64.0
65.7
64.6
550
52.7

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY- 2018
page 8
ODOR CONTROL SYSTEMS
DUALLSCRUBBERS
TRAIN NO.1
TRAIN N0.2
DATE
1A-pH
1B-pH
113-ORP
113-TCR
1C-pH
1C-ORP
1C-TCR
2A-pH
28-pH
2B-ORP
28-TCR
2C-pH
2C-ORP
2C-TCR
S.0
s.0
my
mgA
SA
I S.0
I my
mg/I
sm
s.0
I my
mg
s.0
my
m A
Jan.
7,73
3.16
162
8.14
633
146
7.89
3.05
311
7.95
496
146
Feb.
7.82
2.85
137
8.37
653
78 !
8.02
2.84
281
7.90
515
44
Mar.
6.89
2.91
144
8.19
678
111
7.54
2.96
280
7.76
568
90
Apr.
7.43
2.94
108
7.91
666
101 ':
6.49
2.92
248
8.07
555
88
May
6.72
2.92
86
7.83
603
121
6.48
2.94
214
7.74
528
62
Jun.
3.45
6.82
242
7.60
468
245
6.52
2.96
225
8.04
491
39
Jul.
5.63
3.92
191
7.36
414
31
6.61
3.19
241
7.40
412
27
Aug.
6.39
2.85
186
8.16
497
51
2.97
7.98
371
8.03
348
28
Sept. i
6.82
2.90
149
8.46
625
87
6.44
2.94
307
7.92
481
13
Oct.
5.18
5.12
219
485
8.43
604
105
7.21
2.94
263
7.76
517
29
Nov.
4.18
7.14
323
235
7.09
551
135 €
7.80
2.92
289
8.19
524
217
Dec.
7.15
2.85
249
8.31
655
232
7.84
2.92
323
8.40
577
358
TOTAL
AVG.
6.28
3.87
183
360
7.99
687
120
6.82
3.38
279
7.93
501
95
ODOR SCRUBBING PERFORMANCE
DUALL INLET CONDITIONS
DUALL OUTLET CONDITIONS
REMOVAL EFFICIENCY
DATE
NH3
R-NH2
H28
CH3-SH
DMS
NH3
R-NH2
H25
CH3-SH
DMS
NH3
R-NH2
H2S
CH3-SH
DMS
m
pm
m
p m
m
PPM
ppm
ppm
ppm
DDM
%
%
%
Jan.
15
58
N/D
N/D
N/D i
N/D
N/D
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
Feb.
16
69
N/D
NID
N/D
N/D
NID
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
Mar.
14
73
N/D
NID
N/D
N/D
N/D
N/D
NID
N/D
>99%
>99%
>991/.
>99%
>99%
Apr.
19
83
N/D
NID
N/D
N/D
N/D
NID
N/D
N/D
>99%
>99%
>99%
>99%
>99%
May
14
66
N/D
NID
N/D i
N/D
N/D
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
Jun.
13
65
NID
N/D
N/D
N/D
N/D
N/D
N/D
NID
>99%
>99%
>99%
>99%
>99%
Jul.
14
58
N/D
N/D
N/D
N/D
N/D
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
Aug.
9
46
N/D
N/D
N/D
N/D
N!D
N/D
N/D
NID
>99%
>99%
>99%
>99%
>99%
Sept.
11
55
N/D
N/D
N/D i
N/D
N/D
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
Oct.
10
50
N/D
NID
NID
NID
N/D
N/D
N/D
NID
>99%
>99%
>99%
>99%
>99%
Nov.
11
42
N/D
N/D
NID
N/D
N/D
NID
NID
N/D
>99%
>99%
>99%
>99%
>99%
Dec.
13
48
N/D
N/D
N/D
NID
N/D
N/D
N/D
N/D
>99%
>99%
>99%
>99%
>99%
TOTAL
AVG. €
13
59
N/D
N/D
NID
NID
N/D
N/D
NID
N/D
>99.0
>99.0
>99.0
>99.0
>99.0

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY • 2018
page 9
ODOR CONTROL SYSTEMS
DUALL SCRUBBERS
MAPCO SCRUBBERS
OUTLET CONDITIONS
DATE
CL2
ACID
BLEACH
CAUSTIC
CHEMICALS
CHEMICALS
A -pH
B-pH
B-ORP
NH3
R-NH2
H2S
CH3-SH
DMS
CL2
ppm
qpd
gpd
gpd
$/dy
$/DT
s.0
S.0
my
ppm
ppm
Ppm
ppm
ppm
ppm
Jan. €
0.5
29.0
31.0
0.0
$97.00
$8.50
8.31 281
N/D
N/D
N/D
N/D
NID
0.5
Feb. I
0.5
26.8
29.0
0.0
$90.00
$7.16
8.23
103
NID
N/D
NID
N/D
NID
0.5
Mar.
0.8
24.4
50.4
0.0
$99.00
$6.98
7.80
95
N/D
N/D
N/D
NID
N/D
0.8
Apr. €
0.5
31.6
40.0
0.0
$110.00
$8.76
7.75
80
N/D
N/D
N/D
N/D
NID
0.9
May
0.3
23.0
30.3
0.0
$81.00
$5.78
7.73
30
N/D
NID
N/D
NID
WD
1
Jun.
ND
22.5
62.0
0.0
$102.00
$8.36
8.47
45
NID
N/D
NID
NID
N/D
0.6
Jul.
ND
12.9
20.2
0.0
$48.00
$3.46
8.72
25
N/D
NID
N/D
N/D
N/D
1.0
Aug.
0.4
7.1
50.0
0.0
$54.00
$4.74
8.33
44
N/D
N/D
N/D
N/D
N/D
1.0
Sept.
0.6
22.5
31.0
0.0
$80.00
$7.45
7.98
31
NID
N/D
N/D
NID
N/D
1.0
Oct. i
0.9
19.8
41.0
0.0
$80.00
$7.31
7.98
56
N/D
N/D
N/D
N/D
N/D
0.6
Nov. i
1
0.9
36.6
40.0
0.0
1 $123.00
$10.57
7.93
48
N/D
N/D
NID
NID
N/D
0.6
Dec.
1.0
3.2
51.0
0.0
$45.00
$10.82
7.73
25
N/D
N/D
N/D
NID
N/D
1.0
TOTAL
AVG. €
0.6
21.6
39.7
0.0
8.06
8.31 72
NID
NID
N/D
N/D
NID
0.8
ODOR CONTROL SYSTEMS
MAPCO SCRUBBERS
TOTAL SCRUBBERS
PRETREATMENT
DATE
ACID
BLEACH
CAUSTIC
CHEMICALS
CHEMICALS
ACID
BLEACH
CAUSTIC
CHEMICALS
CHEMICALS
FLOW
pH
RAINFALL
gpd
gpd
gpd
$/d
$/DT
gpd
gpd
I gpd
$/dy
$!DT
gpd
I s.0
I inches
Jan.
0.0
23.0
0.0
$16.40
$2.21
29.0
54.0
0.0
$113.00
$10.64
50,787
7.35
2.25
Feb. ?
0.0
13.0
0.0
$9.30
$0.83
26.8
42.0
0.0
$99.00
$7.80
53,446
7.47
4.06
Mar.
0.0
22.0
0.0
$15.70
$1.28
24.4
72.4
0.0
$114.00
$7.37
55,806
7.37
5.23
Apr. ':.
0.0
18.6
0.0
$13.30
$1.67
31.6
58.6
0.0
$123.00
$7.09
60,930
7.40
8.00
May 's
0.0
15.6
0.0
$11.10
$1.10 1
23.0
45.9
0.0
$92.00
$6.36
126,578
7.29
7.50
Jun.
0.0
34.3
0.0
$24.50
$2.77
22.5
96.3
0.0
$127.00
$11.49
131,677
7.26
2.63
Jul.
0.0
18.0
0.0
$12.80
$1.44
12.9
38.2
0.0
$61.00
$4.67
122,913
7.25
3.06
Aug.
0.0
34.0
0.0
$24.30
$2.55
7.1
84.0
0.0
$78.00
$7.50
93,865
7.31
10.44
Sept. !
0.0
22.0
0.0
$15.70
$1.79
22.5
53.0
0.0
$96.00
$9.45
110,630
7.12
9.06
Oct. i
0.0
25.0
0.0
$17.80
$2.15
19.8
66.0
0.0
$98.00
$7.95
76,165
7.27
6.44
Nov. ':
0.0
29.0
0.0
$20.70
$2.17
36.6
69.0
0.0
$144.00
$12.01
56,140
7.31
8.00
Dec.
0.0
11.4
0.0
$8.10
$0.70
3.2
62.4
0.0
$53.00
$7.40
33,197
6.82
7.34
TOTAL
74.0
AVG.
0.0
22.2
0.0
21.6
61.8
0.0
81,003
7.27
6.17

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC
REGIONAL COMPOST FACILITY - HICKORY, NC
OPERATIONS SUMMARY- 2018
page 10
CONSORTIUM OWNERSHIP & UTILIZATION
CITY OF HICKORY
CITY OF NEWTON
CITY OF CONOVER
DATE
OWNERSHIP
CAPACITY
LOADING
USAGE
CAPACITY OWNERSHIP
CAPACITY
LOADING
USAGE
CAPACITY
OWNERSHIP
CAPACITY
LOADING
USAGE
CAPACITY
%
DT/d
DT/dy
%
%
%
DT/dy
%
%
%
DT/dy
DT/dy
%
%
Jan.
66.0%
13.20
8.54
64.7%
42.7%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.30
41.9%
6.5%
Feb.
66.0%
13.20
8.93
67.7%
44.7%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.82
58.6%
9.1 %
Mar.
66.0%
13.20
9.24
70.0%
46.2%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
2.27
73,1%
11.3%
Apr.
66.0%
13.20
9.56
72.5%
47.8%
0.0%
0.00
0.00
0.0%
0.0%
15.6%
3.10
1.67
53.9%
8.4 %
May
66.0%
13.20
8.24
62.4%
41.2%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.21
39.0%
6.0%
Jun.
66.0%
13.20
7.69
58.2%
38.4%
0.0%
0.00
0.00
0.0%
0.0% 1
15.5%
3.10
1.01
32.7%
5.1%
Jul.
66.0%
13.20
7.71
58.4%
38.6%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
0.68
22.1%
3.4%
Aug.
66.0%
13.20
7.30
55.3%
36.5%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.24
40.1%
6.2%
Sept.
66.0%
13.20
7.44
56.4%
37.2%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.09
35.2%
5.5%
Oct.
66.0%
13.20
7.05
53.4%
35.3%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.17
37.8%
5.9%
Nov.
66.0%
13,20
9.26
58.9%
38.9%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.01
32.7%
5.1%
Dec.
66.0%
13.20
3.40
25.7%
17.0%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
0.60
19.4%
3.0%
TOTAL
AVG.
66.0%
13.20
7.86
69.6%
39.3%
0.0%
0.00
0.00
0.0%
0.0%
15.5%
3.10
1.26
40.5%
6.3%
CONSORTIUM UTILIZATION & COSTS
CATAWBA COUNTY
CONSORTIUM
DATE
OWNERSHIP
CAPACITY
LOADING
USAGE
CAPACITY
VOLUME
UNIT COST
MASS
UNIT COSTI OWNERSHIP
CAPACITY
LOADING
USAGE
CAPACITY
%
DT/dy
I
%
%
GAL
$/Gal
D Tons
$/DT
%
DT/
DT/dy
%
%
Jan.
18.5%
3.70
0.29
7.7%
1.4%
€ 2,054,795
$0.045
222.8
$659.13
100.0%
20.0
11.14
38.1%
55.7%
Feb.
18.5%
3.70
0.44
11.8%
2.2%
€ 1,736,090
$0.048
223.7
$439.32
100.0%
20.0
11.19
46.0%
56.0%
Mar.
18.5%
3.70
0.66
17.8%
3.3%
€ 1,970,431
$0.044
256.9
$363.09
100.0%
20.0
12.23
53.6%
61.2%
Apr.
18.5%
3.70
0.13
3.4%
6.0%
11,900,518
$0.051
238.6
$418.83
100.0%
20.0
11.36
43.3%
56.8%
May
18.5%
3.70
0.18
5.0%
9.0%
1,836,466
$0.047
211.9
$444.19
100.0%
20.0
9.63
35.5%
48.2%
Jun.
18Z%
3.70
0.13
3.5%
6.0%
': 1,730,234
$0.050
185.4
$583.18
100.0%
20.0
8.83
31.5%
44.2%
Jul.
18.5%
3.70
0.12
3.2%
6.00%
€ 2,042,709
$0.043
187.2
$469.45
100.0%
20.0
8.92
27.9%
44.6%
Aug.
18.5%
3.70
0.12
3.3%
6.00%
i 1,815,978
$0.055
199.4
$482.68
100.0%
20.0
9.49
32.9%
47.5%
Sept.
18.5%
3.70
0.22
5.9%
1.10%
1,591,406
$0.052
166.3
$514.78
100.0%
20.0
8.75
32.5%
43.8%
Oct.
18.5%
3.70
0.06
1.5%
0.30%
! 1,894,844
$0.045
190.5
$516.44
100.0%
20.0
8.28
30.9%
41.4%
Nov.
18.5%
3.70
0.32
8.7%
1.60%
1,726,175
$0.045
190.9
$488.82
100.0%
20.0
9.55
33.4%
47.8%
Dec.
18.5%
3,70
0.05
1.4%
0.30%
332,222
$0.156
81.1
$365.67
100.0%
20.0
11.59
15.5%
58.0%
TOTAL
€
i 20,631,868
2,355
AVG.
18.5%
3.70
0.23
6.1%
1.1%
1,719,322
$0.057
196.2
$478.80
1 100.0%
20.0
10.08
50.4%
50.4%

EXHIBIT 3
Bi-Monthly Laboratory Reports and Analytical Data
21

Bi - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of January and February 2018. This shows compliance with Alternative A5
of 40 CFR Part 503.32, 40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
Pathogen -Reduction ]ire ui>reme>lnts - Allternative A5 (Pl RP1
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 67.05 deg.0 for 3.07 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN DILL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — NA Dry Weight Basis. Fecal Coliform Results - <34.4
(MPN/g)_ (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Unde ed,
AW/ --f L�—
Paul Spencer
Vector Attraction Reduction - Option 5
TIME & TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 64.80deg. C for approximately 21.55days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Undersi ed.
Paul Spencer
PFRP Certification Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Undersi ed,
Paul Spencer
Project Manager
Veolia Water North America
Regional Compost Facility-
3200 20th Ave., SE
Newton NC 28658
Date Signed:
7,a 77W

(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.
IN

,��Ila'rceAnaljftal
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February 02, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Compost Metals
Pace Project No.: 92370821
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 25, 2018:
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cq*o(�
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
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Project: Compost Metals
Pace Project No.: 92370821
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification M 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13

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SAMPLE ANALYTE COUNT
Project: Compost Metals
Pace Project No.: 92370821
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92370821001 Compost Metals EPA6010 SH1 8 PASI-A
EPA7471 WAB 1 PASI-A
92370821002 Compost Moisture SM 254OG KDF 1 PASI-C
ASTM D2974-87 KDF 1 PASI-C
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Compost Metals
Pace Project No.: 92370821
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Compost Metals Lab ID: 92370821001
Results reported on a "wet -weight" basis
Parameters Results Units
Collected: 01/25/18 07:40
Report Limit DF
Received: 01/25/18 09:42 Matrix: Solid
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
0.95
mg/kg
0.93
1
01/31/18 01:00
02/01/18 07:48
7440-38-2
Cadmium
0.29
mg/kg
0.093
1
01/31/18 01:00
02/01/18 07:48
7440-43-9
Copper
132
mg/kg
0.46
1
01/31/18 01:00
02/01/18 07:48
7440-50-8
Lead
9.8
mg/kg
0.46
1
01/31/18 01:00
02/01/18 07:48
7439-92-1
Molybdenum
2.6
mg/kg
0.46
1
01/31/18 01:00
02/01/18 07:48
7439-98-7
Nickel
9.0
mg/kg
0.46
1
01/31/18 01:00
02/01/18 07:48
7440-02-0
Selenium
2.2
mg/kg
0.93
1
01/31/18 01:00
02/01/18 07:48
7782-49-2
Zinc
629
mg/kg
0.93
1
01/31/18 01:00
02/01/18 07:48
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.28
mg/kg
0.026
5
01/28/1819:37
02/01/1817:53
7439-97-6
REPORT OF LABORATORY ANALYSIS
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Date: 02/02/2018 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 13

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ANALYTICAL RESULTS
Project: Compost Metals
Pace Project No.: 92370821
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Compost Moisture Lab ID: 92370821002 Collected: 01/25/18 07:35 Received: 01/25/18 09:42 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
254OG Total Percent Solids Analytical Method: SM 254OG
Total Solids
Percent Moisture
Percent Moisture
Date: 02/02/2018 12:18 PM
59.3 %
Analytical Method: ASTM D2974-87
40.7 %
0.000010 1
0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
01 /26/18 12:23
01 /29/18 11:27
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QUALITY CONTROL DATA
Project: Compost Metals
Pace Project No.: 92370821
QC Batch: 395793 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92370821001
METHOD BLANK: 2194132
Associated Lab Samples: 92370821001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2194133
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 02/01/1815:56
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.083 0.079 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2194134 2194135
MS MSD
92370766001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND .061 .061 0.037 0.041 60 68 75-125 12 M1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/02/2018 12:18 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: Compost Metals
Pace Project No.: 92370821
QC Batch: 396104 Analysis Method: EPA 6010
QC Batch Method: EPA3050 Analysis Description: 6010 MET
Associated Lab Samples: 92370821001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2195989
Matrix:
Solid
Associated Lab Samples: 92370821001
Blank
Reporting
Parameter
Units
Result
. Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
1.0
02/01/18 07:10
Cadmium
mg/kg
ND
0.10
02/01/18 07:10
Copper
mg/kg
ND
0.50
02/01/18 07:10
Lead
mg/kg
ND
0.50
02/01/18 07:10
Molybdenum
mg/kg
ND
0.50
02/01/18 07:10
Nickel
mg/kg
ND
0.50
02/01/18 07:10
Selenium
mg/kg
ND
1.0
02/01/18 07:10
Zinc
mg/kg
ND
1.0
02/01/18 07:10
LABORATORY CONTROL SAMPLE:
2195990
Spike
LCS
LCS %
Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Arsenic
mg/kg
50
45.8
92
80-120
Cadmium
mg/kg
50
49.0
98
80-120
Copper
mg/kg
50
50.9
102
80-120
Lead
mg/kg
50
47.7
95
80-120
Molybdenum
mg/kg
50
51.8
104
80-120
Nickel
mg/kg
50
49.6
99
80-120
Selenium
mg/kg
50
44.4
89
80-120
Zinc
mg/kg
50
46.6
93
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2195991
2195992
MS
MSD
92371140001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
Arsenic
mg/kg
1.9
30.9
42.4
21.6
31.9
64
71
75-125
38 M1,R1
Cadmium
mg/kg a
ND
30.9
42.4
21.7
32.4
70
76
75-125
40 M1,R1
Copper
mg/kg
28.8
30.9
42.4
47.2
57.7
60
68
75-125
20 M1
Lead
mg/kg
14.3
30.9
42.4
32.2
41.8
58
65
75-125
26 M1,R1
Molybdenum
mg/kg
ND
30.9
42.4
19.5
30.0
62
70
75-125
43 M1,R1
Nickel
mg/kg
21.8
30.9
42.4
39.8
50.1
58
67
75-125
23 M1,R1
Selenium
mg/kg
2.4
30.9
42.4
21.5
32.0
62
70
75-125
39 M1,R1
Zinc
mg/kg
57.5
30.9
42.4
75.1
91.5
57
80
75-125
20 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/02/2018 12:18 PM without the written consent of Pace Analytical Services, LLC.
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Project: Compost Metals
Pace Project No.: 92370821
QC Batch: 395665
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92370821002
SAMPLE DUPLICATE: 2193394
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2193395
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92370955004 Dup
Units Result Result RPD Qualifiers
63.6 61.0 4
92370821002 Dup
Units Result Result RPD Qualifiers
% 40.7 37.2 9
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: Compost Metals
Pace Project No.: 92370821
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/0212018 12:18 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13

W
aceAnalytical oD
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Compost Metals
Pace Project No.: 92370821
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92370821001
Compost Metals
EPA 3050
396104 EPA 6010
396155
92370821001
Compost Metals
EPA 7471
395793 EPA 7471
395813
92370821002
Compost Moisture
SM 2540G
395861
92370821002
Compost Moisture
ASTM D2974-87
395665
Date: 02/02/2018 12:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 13

Document Name: 1 Document Revised: August 4, 2017
aceAnaVieai
Sample Condition Upon Recelpt(SCUR) { Page 1 of 2
Document No.: fi Issuing Authority_
F-CAR•CS-033-Rev.04 ? Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[ -] Greenwood❑ Huntersville�i' Raleigh❑ Mechanicsville[]
Client Name: WO# • 92370821
-
Courier: ❑Fed,Ex ❑UPS ❑USPS []Client
❑ 1111111 II 11111111111111
Commercial �1 a e ❑Other:
92370821
Custody Seal Present? ❑Yes P No Seals Intact? ❑Yes (]No rL
Date/lnitlalsPerson Examining Contents: pZ"S��
Packing Material: ❑Bubble Wrap .©Bubble Bags ❑None
Thermometer: tI]VJet
[I IR Gun ID: L �(� Type of Ice:
Correction factor: Cooler Temp Corrected (°C). 7,
❑ Other Biological Tissue Frozen?
[]Yes 2© o ❑N/A
❑Blue ❑None
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (A, water sample)
Did samples originat in a quarantine zone within the United States: CA, NY, or SC (check maps)?
177, nN7
Did samples originate from a foreign source (internationally,
Comments/Discrepancy: —
Chain of Custody Present?
f
Yes ❑No
[I N/A
1.
Samples Arrived within Hold Time?
Yes .[]No
❑N/A
2.
Short Hold Time Analysis (c72 hr.)?
[]Yes -06
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes ❑NO-'-" ❑N/A
4.
Sufficient Volume?
DYe > -ONo
❑N/A
S.
Correct Containers Used?
Die - ❑No
❑ N/A
6.
-Pace Containers Used?
,�-
QYes/ No
[]N/A
Containers Intact?
Ves ❑N�o✓
. N/A
7.
Dissolved analysis: Samples Field Filtered?
Qye -- ©rfo
❑N/A
S.
Sample Labels Match COC?
t Yes []No
❑N/A
9.
-includes Date/Time/ID/Analysis Matrix:
) L
/
Headspace in VOA Vials (>5-6mm)?
❑Yes ❑No/ ©NIA
10.
Trip Blank Present?
❑Yes aao
[]N/A
11.
Trip Blank Custody Seals Present?
[]Yes []NO
(]Nin
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot 10 of split containers:
Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: (aDate:
Project Manager SRF Review: C) Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 11 of 13

f•
u
Document Name:
Document Revised: August 4, 2017
105a�
02ceAnalyticaI
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Issuing Authority:
It/
Document No.:
F-CAR-CS-033•Rev.04
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
Project 0
WO# : 9237®321
is verified and within the acceptance
range
for
preservation samples.
PM:
AM9 Due Date: 02/08/18
**Bottom half of box is to list number of bottles
CLIENT: 92—Veol to Wa
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Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Page 12 of 13

CHAIN -OF -CUSTODY t Analytical Request Document
faeeAnalXieal The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. O
M
O)
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page: of ��
1111
f
Company: Veolia Water North America, Report To: Paul" Spencer Attention: Paul Spencer
Address: 3200 20th Ave SE copy
TO: Christopher Johnson Sr
Company Name:
REGULATORY AGENCY
Newton, NC 28658
Address:
r NPDES F GROUND WATER DRINKING WATE
i UST RCRA OTMER 503
R
Email To: [e-mail] Purchase
Order No.: CC on file
Pace Quote
Reference:
----
Phone: [phone]
Fax: Project
Name: Compost Metals
Pace Pro)oct Angela Baioni
Site Location
- 4 V
Manager:
STATE:
NC
- t
}
Requested Due Date/TAT: STD Project
Number:
Paco Profile 0:
Requested
Analysis
Filtered
(Y(N)
-
Section D Matrix Valid Codes
a
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ATRI
Roqulred Client Information cooE
COLLECTED
Preservatives
ORR1I' WATER DINy
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COMPOSITE
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Sample IDS MUST BE UNIQUE TISSUE Ts
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DATE
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OT
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ADDITIONAL COMMENTS
RELINQUISHED BY 1 AFFILIATION
DATE
TIME
ACCEPTED BY 1 AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
Metal; 4rsnn+:, Cadmium. Copper, Molybdenum, Nickel,
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SAMPLER NAME AND SIGNATURE
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SIGNATURE of SAMPLER"-` rt d 3 DATE Signed
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cananl Nola: By signing this form you are accepting Pace's NI? 30 day payment terms and agreeing to late charges of 1,S°6 per month for any invoices not paid within 30 days. F-ALL-Q-020rev.07, 15-Feb-2007

/.,,,raceAnaly ica!
—pa-14bs.com
i
I
February 22, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Compost Fecal
Pace Project No.: 92372042
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 06, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 5

V
Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 02/06/2018
Reported: 0212=018
For:
Comments:
Sample Number
Parameter
Sample ID
Result
Unit Method
Analyzed
Analyst
180206-11-01
Fecal Coliforms
Comp
<34.4
MPN/g sm922'cE-200e
.02/0612018
WC
180206-11-01
Percent Solids
Comp
58.2
% SM2540e-1997
02106/2018
WC
Respectfully submitted,
r0s.-*/O(lj1%�{A`'
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 o 704/872/4697
Page 1 of Sage 3 of 5

► kceAnalyfical - CD
nrv.:nuue:ah! cunr
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT, All refervant fields must he Completed atourately.
Section A section B Section C P.B.- t of 1.
Requirad Client Information: Required Project information: Invoice Information:
Company: Veol)a Water Report To: Paul Spencer Attention: Christopher Johnson
Addross: 3200 20 Avenue SE Copy To: Company Name: Veolia Water l" NPDES I GROUND WATER -' DRINKING WATER
NWdOn, Na 2swe 3200 20th Avenue SE NevaonMC 28668 UST I' RCRA :?(OTHER E03 Slosdids
,
Erne" T0; Pernhuee CC on file Pace ouele RMow= N wl X NC
OMer No.; GA - IL
Phone: [phone] PMOCI Name: Grnpostfeeal Paee Prl ewmc aaar; Angela 13910hl OH SC t ' NI OTHER
Req-4tod std PfolsotNumeec Pace Profile A: 2816, 2 FlRered pIN)
Duo 0MIT T:
Soction D V010 Wbft 00'f
ornrem"fn MATH 9201
m�•nw.ro+ av
SAMPLE ID "�
sr (A-Z. 49I r) me w
Sample IDa MUST 9E UNIQUE
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ENumue
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-
Preservatves
1otl
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DATE
TIME
DATE
TIME
Fecal
OT
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PRINT Name of
SAMPLER:
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SIGNATURE of SAMPLE
rO� sw-Hera on'irn: 2/6/1ti
e-Fite(ALL002orev.4,2gMor06)22Jun2006
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'aceAnalytical
www.pacelabs.com
February 27, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 06, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mr. Paul Spencer, Veolia Water North America
P«RF�
i
I N Ttea.
-eORA'�O
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

W
AceAnalytical
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I
CERTIFICATIONS
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 ICncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19

�aceAnalytical o
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Solids, Metals, Nitrate
92372065
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92372065001
Nitrate, Metals, Solids
EPA6010
SER
10
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
ECH
1
PASI-A
SM 2710B
EWS
1
PASI-A
TKN+NO3+NO2 Calculation
DMN
1
PASI-A
EPA 350.1 1993 Rev 2.0
AES2
1
PASI-A
EPA 351.2
AES2
1
PASI-A
EPA353.2
DMN
3
PASI-A
EPA 365.1
AES2
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Sample: Nitrate, Metals, Solids
Lab ID: 92372065001 Collected:
02/06/18 09:02
Received: 02/06/18 09:15 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
1410 mg/kg
8.9
1
02/17/18 02:05
02/18/18 05:34
7429-90-5
Arsenic
ND mg/kg
0.89
1
02/17/18 02:05
02/18/18 05:34
7440-38-2
Cadmium
0.15 mg/kg
0.089
1
02/17/18 02:05
02/18/18 05:34
744043-9
Copper
55.7 mg/kg
0.45
1
02/17/18 02:05
02/18/18 05:34
7440-50-8
Lead
3.8 mg/kg
0.45
1
02/17/18 02:05
02/18/18 05:34
7439-92-1
Molybdenum
1.2 mg/kg
0.45
1
02/17/18 02:05
02/18/18 05:34
7439-98-7
Nickel
3.2 mg/kg
0.45
1
02/17/18 02:05
02/18/18 05:34
7440-02-0
Potassium
689 mg/kg
446
1
02/17/18 02:05
02/18/18 05:34
7440-09-7
Selenium
1.1 mg/kg
0.89
1
02/17/18 02:05
02/18/18 05:34
7782-49-2
Zinc
291 mg/kg
0.89
1
02/17/18 02:05
02/18/18 05:34
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.074 mg/kg
0.0033
1
02/11/18 16:45
02/11/18 21:57
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
55.9 %
0.10
1
02/07/18 12:12
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.4 Std. Units
0.10
1
02/16/18 13:40
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
4080 mg/kg
0.12
1
02/27/18 16:48
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
11700 mg/kg
40.0
1
02/21/18 09:43
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
2810 mg/kg
106
10
02/24/18 15:10
7664-41-7 M6
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
11700 mg/kg
400
10
02/16/18 17:39
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA353.2
Nitrogen, Nitrate
ND mg/kg
1.9
1
02/20/18 14:46
Nitrogen, Nitrite
3.1 mg/kg
0.94
1
02/20/18 14:46
Nitrogen, NO2 plus NO3
3.6 mg/kg
1.9
1
02/20/18 14:46
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
3390 mg/kg
89.3
50
02/07/18 13.53
7723-14-0
Date: 02/27/2018 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

aceAnalj cal
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QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 397011 Analysis Method: EPA7471
QC Batch Method: EPA7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92372065001
METHOD BLANK: 2201421 Matrix: Solid
Associated Lab Samples: 92372065001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 02/11/18 20:51
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2201422
Spike
LCS
LCS
% Rec
Parameter Units
Conc.
Result
% Rec
Limits Qualifiers
Mercury mg/kg
.083
0.078
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2201423
2201424
MS
MSD
92371903001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Conc.
Conc. Result
Result
% Rec % Rec Limits RPD Qual
Mercury mg/kg 0.035
.084
.074 0.096
0.082
72 64 75-125 15 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19

aceAnalytical"
www.pacelabs.com
Pace Analytical Services, LLC W
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 398326 Analysis Method: EPA 6010
QC Batch Method: EPA3050 Analysis Description: 6010 MET
Associated Lab Samples: 92372065001
METHOD BLANK: 2209424
Associated Lab Samples: 92372065001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
02/18/18 05:15
Arsenic
mg/kg
ND
1.0
02/18/18 05:15
Cadmium
mg/kg
ND
0.10
02/18/18 05:15
Copper
mg/kg
ND
0.50
02/18/18 05:15
Lead
mg/kg
ND
0.50
02/18/18 05:15
Molybdenum
mg/kg
ND
0.50
02/18/18 05:15
Nickel
mg/kg
ND
0.50
02/18/18 05:15
Potassium
mg/kg
ND
500
02/18/18 05:15
Selenium
mg/kg
ND
1.0
02/18/18 05:15
Zinc
mg/kg
ND
1.0
02/18/18 05:15
LABORATORY CONTROL SAMPLE:
Parameter
2209425
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
500
478
96
80-120
Arsenic
mg/kg
50
44.7
89
80-120
Cadmium
mg/kg
50
45.6
91
80-120
Copper
mg/kg
50
48.2
96
80-120
Lead
mg/kg
50
45.9
92
80-120
Molybdenum
mg/kg
50
49.8
100
80-120
Nickel
mg/kg
50
46.5
93
80-120
Potassium
mg/kg
500
ND
94
80-120
Selenium
mg/kg
50
41.8
84
80-120
Zinc
mg/kg
50
44.8
90
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2209426
2209427
MS �
MSD
92371424001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
mg/kg
10700
287
347
11200
11500
173
240
75-125
3 E
Arsenic
mg/kg
0.95
28.7
34.7
26.6
35.5
89
99
75-125
29 R1
Cadmium
mg/kg
ND
28.7
34.7
26.1
32.0
91
92
75-125
20
Copper
mg/kg
0.95
28.7
34.7
28.9
35.4
97
99
75-125
20
Lead
mg/kg
6.8
28.7
34.7
35.5
39.4
100
94
75-125
10
Molybdenum
mg/kg
ND
28.7
34.7
26.4
45.3
91
130
75-125
53 M1,R1
Nickel
mg/kg
0.39
28.7
34.7
25.2
31.1
86
88
75-125
21 R1
Potassium
mg/kg
ND
287
347
499
557
150
141
75-125
11 M1
Selenium
mg/kg
ND
28.7
34.7
24.2
30.1
83
86
75-125
22 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aceAnaljd cal
www.pacelaftcom
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2209426 2209427
MS MSD
92371424001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[
Zinc mg/kg 3.5 28.7 34.7 29.5 34.4 91 89 75-125 15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

aceAnalytical
% wwpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 396942
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92372065001
SAMPLE DUPLICATE: 2201137
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2201138
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92371943001 Dup
Units Result Result
% 23.2 23.0
92372065001 Dup
Units Result Result
% 55.9 54.5
RPD Qualifiers
1
RPD Qualifiers
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

jl
�acmnalyiical
www.pacelabs.com
i
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 398365
QC Batch Method: EPA 9045
Associated Lab Samples: 92372065001
SAMPLE DUPLICATE: 2209531
Parameter Units
pH at 25 Degrees C Std. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
92372065001 Dup
Result Result RPD
8.4 8.4
0
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

1
aceAnalytical
www,pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 399595
QC Batch Method: EPA 350.1 1993 Rev 2.0
Associated Lab Samples: 92372065001
METHOD BLANK: 2216506
Associated Lab Samples: 92372065001
Parameter Units
Nitrogen, Ammonia mg/kg
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Solid
EPA 350.1 1993 Rev 2.0
350.1 Ammonia
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 02124/1815:08
LABORATORY CONTROL SAMPLE: 2216507
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 500 494 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2216508 2216509
MS MSD
92373244001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua)
Nitrogen, Ammonia mglkg ND 564 586 542 565 96 97 90-110 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2216510 2216511
MS MSD
92372065001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Ammonia mg/kg 2810 1230 1210 8520 8900 175 210 90-110 4 M6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

aceAna Xical
www.pacelabs.com
' I
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
QC Batch: 398303 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92372065001
METHOD BLANK: 2209342 Matrix: Solid
Associated Lab Samples: 92372065001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg ND 50.0 02/16/18 17:38
LABORATORY CONTROL SAMPLE: 2209343
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1000 918 92 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2209344 2209345
MS MSD
92372600010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 49600 148000 120000 197000 185000 100 113 90-110 6 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2209346 2209347
MS MSD
261498009 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 1070 588 667 1940 1390 147 48 90-110 33 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

raceAnalyfical"
www.pacelabs.com
1
i
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Pace Analytical Services, LLC NW
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 398288
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92372065001
METHOD BLANK: 2209302
Matrix: Solid
Associated Lab Samples: 92372065001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 2.0
02/20/18 14:33
Nitrogen, Nitrite
mg/kg
ND 1.0
02/20/18 14:33
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
02/20/18 14:33
LABORATORY CONTROL SAMPLE: 2209303
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
25
24.6
98 90-110
Nitrogen, Nitrite
mg/kg
10
9.9
99 90-110
Nitrogen, NO2 plus NO3
mg/kg
25
24.6
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2209304
2209305
MS
MSD
92372600009
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Cone.
Cone. Result
Result % Rec % Rec
Limits RPD Qual
Nitrogen, Nitrate mg/kg
ND
499
499 180
180 34 34
90-110 0 M1
Nitrogen, Nitrite mg/kg
23.3
200
200 85.0
84.5 31 31
90-110 1 M1
Nitrogen, NO2 plus NO3 mg/kg
ND
499
499 180
180 29 30
90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2209306
2209307
MS
MSD
92373244008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
32.7
32.7
34.0
34.1
103
103
90-110
0
Nitrogen, Nitrite
mg/kg
ND
13.5
13.5
13.7
13.7
101
101
90-110
0
Nitrogen, NO2 plus NO3
mg/kg
ND
32.7
32.7
34.0
34.1
103
103
90-110
0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

r
'aceAnalXical o
www.pacelabs.com
I
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 397029
Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92372065001
METHOD BLANK: 2201469
Matrix: Solid
Associated Lab Samples: 92372065001
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Phosphorus mg/kg
ND 2.0 02/07/1813:40
LABORATORY CONTROL SAMPLE: 2201470
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg
50 53.2 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2201471 2201472
MS MSD
92371291001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 133
88 86.3 241 219 123 100 90-110 10 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

Pace Analytical Services, LLC
aceAnalytical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
I
QUALIFIERS
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/27/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

RaceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Solids, Metals, Nitrate
Pace Project No.: 92372065
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92372065001
Nitrate, Metals, Solids
EPA 3050
398326
92372065001
Nitrate, Metals, Solids
EPA 7471
397011
92372065001
Nitrate, Metals, Solids
ASTM D2974-87
396942
92372065001
Nitrate, Metals, Solids
EPA 9045
398365
92372065001
Nitrate, Metals, Solids
SM 2710B
399947
92372065001
Nitrate, Metals, Solids
TKN+NO3+NO2
399044
Calculation
92372065001
Nitrate, Metals, Solids
EPA 350.1 1993 Rev 2.0
399595
92372065001
Nitrate, Metals, Solids
EPA351.2
398303
92372065001
Nitrate, Metals, Solids
EPA 353.2
398288
92372065001
Nitrate, Metals, Solids
EPA 365.1
397029
Date: 02/27/2018 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA 6010 398531
EPA 7471 397181
Page 15 of 19

V
Document Name: Document Revised: January 24, 2018
15 „ Sample Condition Upon Recelpt(SCUR) Page 1 of 2
aceAnapicai Document No.: Issuing Authority:
F-CAR-CS-033-Rev.05 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville[]/ Raleigh❑ Mechanicsville[]
Client Name: Project #: WO# : 92372065
`/ 1
V Q-0,1 6-\
Courier: ❑Fed Ex ❑UPS ❑USPS []ClientII I II' I II I I �I II I II I �II
❑ Commercial 0Pa-ce ❑Other: 92372068
Custody Seal Present? []Yes ,Zlllo Seals Intact? ❑Yes ❑Nt>�
Packing Material: ❑Bubble Wrap ; _439-ubble Bags ❑None ❑ Other
Thermometer: Type of Ice:
❑IRGunID: [2136 W/et ❑Blue
Cooler Temp (°C): Correction Factor: Add/Subtract (°C) • 0.1
Cooler Temp Corrected ('C): L
USDA Regulated Soil- N/A, water sample)
Did samples origin to In a quarantine zone within the United States: CA, NY, or SC (check maps)?
pate/Initials Person Examining Contents.-Z— I J
Biological Tissue Frozen?
❑YES--BNii ~❑ N/A
❑ None
Temp should be above freezing to 6°C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
__i...r:.... a —11 —1 Doom- Pl—)? f—IYP9 MNo-'�
LJ
Comments/Discrepancy
Chain of Custody Present?
/
Yef ❑No
❑N/A
1.
Samples Arrived within Hold Time?
es ❑No
QN/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes ISO/
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes iTo
❑N/A
4.
Sufficient Volume?
' Yes No
❑NX
5.
Correct Containers Used?
� es •❑No
❑N/A
6.
-Pace Con taine rs Used?
es ❑No
❑N/A
Containers Intact?
❑Y•es--ONo
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Y No ❑N/A
8.
Sample Labels Match COC?
r5es ❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
45`'
Headspace in VOA Vials (>5-6mm)?
❑Yes ONO
/
/
10.
Trip Blank Present?
Oyes ❑
❑N/A
11.
Trip Blank Custody Seals Present?
❑Yes ❑No
❑ A'
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Field Data Required? []Yes ❑No
Project Manager SCURF Review:
Date:
Project Manager SRF Review: 1f {�7 Date:
Page 16 of 19

FaceAnalyiical
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B Section C Page: 1 Of 1
Required Client Information: Required Project Information; Invoice Information:
company: Veolia Water Report To: Paul Spencer Attention: Christopher Johnson
REGULATORY
Address: 3200 20th Avenue SE Copy To: Christopher Johnson Company Name: Veolia Water t NPDES GROUND WATER DRINKING WATER
Newton, NC 28658 3200 20th Avenue SE Newton,NC 28658 UST ' RCRA XOTHER 503 B(osolids
Email To: Purcnaso CC on file Pace Quote Reference:
Order No.: GA IL N Lit X NC
Phone: [phone] Fax Project Name: Solids, Metals, Nitrate Pace Project Manager; Angela Baloni • W OH SC I NI OTHER
Requested Std Project Number. Pace Profile #: 2816, 2
Due DatefTAT: Filtered (YIN)
Section D Hoqurred valid Maui. eedea
ATRQP
Information
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DATE
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Metals- Al, As, Ca, Cd, Cu, Pb, Mg, Mo, Ni, K, Se, Na,
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Document Name:
Document Revised: January 24, 2018
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
Issuing Authority:
iceAnalytical'
f-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # I WO# : 92372®65
PM: AMB Due Date: 02/20/18
CLIENT: 9246011a Wa
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot k
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Outof hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 19
n

� 1
Page: 1 of 1
Report Number: 18-039-0205
Account Number: 05734 Waypoint(2)
ANALYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project : 92372065
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
Lab Number: 58516
Sample Id : Nitrate, Metals, Solids
REPORT OF ANALYSIS
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Date Sampled: 2/6/2018 09:02:00
Date Received: 02/08/2018 00:00
Date Reported: 02/15/2018
iotai 5oiias _ 33.53 335300 100.0 JM 02/08/2018 15:30 SM-2540G
Moisture * 66.46 100.0 JM 02/08/2018 15:30 SM-2540G
Total Calcium 0.78 7840 100 MOS 02/14/2018 16:29 6010C
Total Magnesium 0.12 1160 100 MOS 02/13/2018 18:21 6010C
Total Sodium 0.05 532 100 MOS 02/13/2018 18:21 6010C
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Oigrel)orts -and letters :,re for the exclusive and confidential use of our clients, and may not be reproduced in whole or part; nor may any reference be made
the company in any advertising, news release, or other public announcernenis without obtaining our prior written authorization.
0
Pauric McGroary
Agronomist

Ili - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of March and April 2018. This shows compliance with Alternative A5 of 40
CFR Part 503.32, 40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
]Pathogen Redtuetion Requirements - Alternative A5 FRP)
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 68.8 deg.0 for 3.18 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN KI1LL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — NA Dry Weight Basis. Fecal Coliform Results - <32
MPN/ (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Undersigned,
Paul Spencer
Vector Attraction Reduction - Option 5
TIME & TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 66.40deg. C for approximately 22.30days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Undersigned.
A�d
Paul Spencer
PFRP Certification Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Undersjgned,
Paul Spencer
Project Manager
Veolia Water North America
Regional Compost Facility
3200 20th Ave., SE
Newton NC 28658
Date Signed:
� %� � -aal

V
(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.

_ ace . napieal
wwwpacelabs.c=
May 07, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Compost Fecal
Pace Project No.: 92381640
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on April 17, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
01*0_1 -hl - -Ibaoru
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mir. Paul Spencer, Veolla Water North America
pcc
This report shall not be reproduced except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 3

qw
Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 04/17/2018
Reported: 05/07/2018
For:
Comments:
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
180417-28-01
Fecal Coliforms
Fecal
<32
MPN/g
sneMIM-2006
04/18/2018
WC
180417-28-01
Percent Solids
Fecal
61.6
%
SWO54OB-1997
04/18/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 © 704/872/4697
Page 1 of 4ge 3 of 3

77
�,. ceAnZfj cal
Section A
aaaulm' d f_ILmt trMirmiltictV
CHAIN -OF -(CUSTODY I Analyticai Request Document
The Choln-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Roouirod Proud Infoltin2 loin: Imnle4 lydorrnatlan:
Pam: 1 at 1
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Company: tfoolia Water
Repoli To: Paul Spencer
Attention: Christopher Johnson
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Company Noma: VeOIra Water
Hcw.nn, NC 2assa
3200 20th.Avenue'SE Newton,NC 28658
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��auceaAnalytical
www.pacelabs.com
March 15, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Compost Metals March
Pace Project No.: 92376141
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on March 08, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mr. Paul Spencer, Veolia Water North America
pCC4,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, LLC.
Page 1 of 12

e
jaceAnalytical G
winvpacelabs.com
CERTIFICATIONS
Project: Compost Metals March
Pace Project No.: 92376141
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 12

Pace Analytical Services, LLC
aceAnalytleal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
SAMPLE ANALYTE COUNT
Project: Compost Metals March
Pace Project No.: 92376141
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92376141001 Compost Metals & Moisture EPA 6010 SER 8 PASI-A
EPA 7471 SER 1 PASI-A
SM 2540G KDF 1 PASI-C
ASTM D2974-87 KDF 1 PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

aceAnaljftal
wvnvpacelabs.com
ANALYTICAL RESULTS
Project: Compost Metals March
Pace Project No.: 92376141
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Compost Metals &
Lab ID: 92376141001 Collected:
03/08/18 08:55
Received: 03/08/18 10:32 Matrix: Solid
Moisture
Results reported on a "wet -weight" basis
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
0.78 mg/kg
0.75
1
03/10/18 02:10
03/14/18 18:39
7440-38-2
Cadmium
0.40 mg/kg
0.075
1
03/10/18 02:10
03/14/18 18:39
7440-43-9
Copper
125 mg/kg
0.37
1
03/10/18 02:10
03/14/18 18:39
7440-50-8
Lead
7.7 mg/kg
0.37
1
03/10/18 02:10
03/14/18 18:39
7439-92-1
Molybdenum
2.5 mg/kg
0.37
1
03/10/18 02:10
03/14/18 18:39
7439-98-7
Nickel
8.3 mg/kg
0.37
1
03/10/18 02:10
03/14/18 18:39
7440-02-0
Selenium
2.1 mg/kg
0.75
1
03/10/18 02:10
03/14/18 18:39
7782-49-2
Zinc
652 mg/kg
0.75
1
03/10/18 02:10
03/14/18 18:39
7440-66-6
7471 Mercury
Analytical Method: EPA7471 Preparation Method: EPA7471
Mercury
0.12 mg/kg
0.0053
1
03/11/1814:50
03/12/1814:18
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
58.3 % 0.000010
1
03/08/18 17:25
Percent Moisture
Analytical Method: ASTM•D2974-87
Percent Moisture
41.7 %
0.10
1
03/09/18 13:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 12:05 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 12

�Pace,MalXical
www.pacelabs.com
Project: Compost Metals March
Pace Project No.: 92376141
QC Batch: 401504
QC Batch Method: EPA 7471
Associated Lab Samples: 92376141001
METHOD BLANK: 2227136
Associated Lab Samples: 92376141001
Parameter
Mercury
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/kg ND 0.0060 03/12/1812:44
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville,' NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2227137
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.090 108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2227138 2227139
MS MSD
92376142001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND .051 .046 0.017 0.016 32 33 75-125 6 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 12:05 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 12

lacieAnalyfical"
www.pacelabsxom
QUALITY CONTROL DATA
Project: Compost Metals March
Pace Project No.: 92376141
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
U
QC Batch: 401383
Analysis Method:
EPA 6010
QC Batch Method: EPA 3050
Analysis Description: 6010
MET
Associated Lab Samples: 92376141001
METHOD BLANK: 2226425
Matrix: Solid
Associated Lab Samples: 92376141001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
03/12/1819:48
Cadmium
mg/kg
ND
0.10
03112/1819:48
Copper
mg/kg
ND
0.50
03/12/1819:48
Lead
mg/kg
ND
0.50
03/1211819:48
Molybdenum
mg/kg
ND
0.50
03/12/1819:48
Nickel
mg/kg
ND
0.50
03/1211819:48
Selenium
mg/kg
ND
1.0
03/1211819:48
Zinc
mg/kg
ND
1.0
03112/1819:48
LABORATORY CONTROL SAMPLE:
2226426
Spike
LCS
LIDS % Rec
Parameter
Units
Cone.
Result
% Rec Limits
Qualifiers
Arsenic
mg/kg
50
50.5
101 80-120
-
Cadmium
mg/kg
50
51.2
102 80-120
Copper
mg/kg
50
53.3
107 80-120
Lead
mg/kg
50
51.3
103 80-120
Molybdenum
mg/kg
50
56.0
112 80-120
Nickel
mg/kg
50
52.3
105 80-120
Selenium
mg/kg
50
48.9
98 80-120
Zinc
mg/kg
50
51.4
103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2226427
2226428
MS
MSD
92376142001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits
RPD Qua[
Arsenic
mg/kg
ND
27.2
28.7
ND
ND 0
0
75-125
M1
Cadmium
mg/kg
ND
27.2
28.7
48.6
39.9 179
139
75-125
20 M1
Copper
mg/kg
912
27.2
28.7
1300
1050 1420
479
75-125
21 M6,R1
ug/g
Lead
mg/kg
11.3
27.2
28.7
162
57.0 554
159
75-125
96 M1,R1
ug/g
Molybdenum
mg/kg
824
27.2
28.7
1170
907 1280
288
75-125
25 M6, R1
ug/g
Nickel
mg/kg
21500
27.2
28.7
30600
21800 33500
1020
75-125
34 M6,R1
ug/g
Selenium
mg/kg
ND
27.2
28.7
14.8
26.3 55
92
75-125
56 M1,R1
Zinc
mg/kg
976
27.2
28.7
882
1450 -342
1640
75-125
48 M6, R1
ug/g
Results presented on this page are In the units Indicated -by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 12:05 PM without the written consent of Pace Analytical Services, LLC.
Page 6of12

acemalXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Compost Metals March
Pace Project No.: 92376141
QC Batch: 401264 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92376141001
SAMPLE DUPLICATE: 2225766
92376189003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Percent Moisture
%
15.6
15.4 1
SAMPLE DUPLICATE: 2225767
92376141001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Percent Moisture
%
41.7
38.9 7
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Unds" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 12:05 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12

W
'aceAnaljftal"
wrnxpacelabs.com
QUALIFIERS
Project: Compost Metals March
Pace Project No.: 92376141
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/15/2018 12:05 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 12

laceAnalyfical
www.pacelibs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Compost Metals March
Pace Project No.: 92376141
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Analytical
Batch
92376141001
Compost Metals & Moisture
EPA 3050
401383 EPA 6010
401484
92376141001
Compost Metals, & Moisture
EPA 7471
401504 EPA 7471
401539
92376141001
Compost Metals & Moisture
SM 254OG
401755
92376141001
Compost Metals & Moisture
ASTM D2974-87
401264
Date: 03/15/2018 12:05 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 12

W
Document Name:
Document Revised: February 7, 2018
011
aceAnalytical u
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR•CS-033•Rev,06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Courier:
❑ Commercial
Custody Seal Present?
Packing Material:
® Client Name:
Project 4:
❑F 6--, []UPS ❑LISPS ❑Client
' Pace ' ❑Qther:
❑Yes "'ZNo Sealsintact? ❑Yes r No
❑Bubble Wrap 'ZoBubble Bags ❑None ❑, Other
Thermometer: Type of Ice: [{Wet 091ue
❑IR Gun ID: 92T036 r✓
Cooler Temp (°Q: __.j i Correction Factor: Add/Subtract (°C) f0,1
Cooler Temp Corrected {°C): '
USDA Regulated Soil_ N/A, water sample)
rr Did samples originate a quarantine zone within the United States: CA, NY, or SC (check maps)?
r" t_ M
w0 •92376 1,41
i II
�II II' � fI II• II I I�III I
92376141
Date/Initials Person Examining Contents: -
Biological Tissue Frozen?
[]yes No [-]N/A
❑None
Temp should be above freezing to VC
❑samples out of temp criteria. Samples an ice, cooling process
has begun
Did samples originate from a foreign source tinatronally,
ter
inrhidlna Rawall and Puerto Ricol? MYes No
Comm ents/Dlscrepancy/
Chain of Custody Present?
Oqes ❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes ON.
- - N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes No
)]N/A
3.
Rush Turn Around Time Requested?
❑Yes No
❑N/A
•4.
Sufficient Volume?
Yes No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
ryKibNo
❑No
❑N/A
❑N/A
Containers intact?
Yes ONo
N/A
7.
Dissolved analysis: Samples Field Filtered? ❑Yes -[Sl<o
❑NIA
8.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis
_ores ❑No
Matrix:
❑N/A
I
9.
I,/
Headspace in VOA Vials (>S-6mm)?
[]yes CIO o
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes eE]Na
❑Yes ❑No
NjA
tl/A
11.
COMMENTS/SAMPLE DISCREPANCY
_ Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
, Fleld Data Required? []Yes ❑No
Person contacted: Date/Time:
Project Manager SCURF Review: 11 Date:
Project Manager SRF Review:` Date: �I �-
Page 10 of 12

7%
0
N
- ceAnalytical "
wrnv ycnLths r.Nn
i
CHAT -OF-CUSTODY / Analytical Bequest Document
The Chai ol-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section B
Section C Patio: j of
Required CI-1 Infonnalion: Required Project Information.
Invoice Information: 1
Attention; Paul Spencer
Company: Veolia Water North America Report
To: Paul Spencer
Address: 3200 20th Ave SE Copy
To; Christopher Johnson Sr
Company Name: Veolia
REGULATORY AGENCY
Newton, NC 28658
address:
r— INrt7Ee (-Gxcn:NUN+A'ITix (-)xtnxtvcttrATrt:
( I'Sr 1-RCPA FOTIIEI: 503
Email To: [e-mail] Purchase
Order No,: CConfile
P.OOele
P.ekrcncc
Phone: [phone] Fax. Project
Name: Compost Metals March
Pace P`etea1 Angela Baioni
Site Location
MannBcr
STATE:
\C
Requested Duo DateRAT: 5T0 Project
Number.
Pace Pynwe a: 2816,2
Requested
Analysis
Filtered
(YIN)
Section D Valid Matrix Codes
a
Required Clime lnlormalinn MATRIX CODe
-
°'
COLLECTED
Preservatives
>
,, nlr*fnT F! vi tki
„r.n..
ill
nnitMtNe Mir H D, 15
4." 1'
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Pace Project No./ Lab I.D.
1
Compost Metals
or,
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318118
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7
e
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10
11
12
ADDITIONAL COMMENTS
RELINQUISHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY/AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
Metals; Arsenic, Cadmium, Copper, Lead. Mercury.
/ 1 �
I
T .
R � .r
3/8/18
lG�-�Z
3/8118
V1,6e1. \inlYhlcneni, Selenium. 7anc,
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SAMPLER NAME
NO SIGNATURE
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SIGNATU Ili
E of SAMP [[[
DATE Signed
I.

Document Name:
Document Revised: February 7, 2018
g
aceAnalyfidal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, C.6lifarm, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # � .WOW' 9237.6141
PM:'RMB Due'Dite: 03/22/18
CLIENT': 92—Veol is Wa.
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pH Adjustment
Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy or tors form wnl be sent to the North Carouna DEHNR emus uncuuvss . il- ii—
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 11 of 12
Ak

1��aceAnaljftal@
www.pacelabs.com
I
April 30, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on April 17, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Christopher Johnson, Veolia Water
Mr. Paul Spencer, Veolia Water North America
pCCRF�.
•eORA"C�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aceAnalytical
wmupacelabs.com
CERTIFICATIONS
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028 Fiorida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648. South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19

aceAnaljftal
www.pacelabs.com
i
SAMPLE ANALYTE COUNT
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Pace Analytical Services, LLC
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
Reported
Laboratory
92381194001 Nitrate, Metals EPA6010
SH1
13
PASI-A
EPA 7471
JMW1
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
RLO
1
PASI-A
SM 2710B
EWS
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 1993 Rev 2.0
BRJ
1
PASI-A
EPA 351.2
CJH1
1
PASI-A
EPA353.2
CJH1
3
PASI-A
EPA 365.1
AES2
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 19

U
aceAna1j6ca1
www.pacelabs.com
ANALYTICAL RESULTS
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Nitrate, Metals
Lab ID: 92381194001 Collected:
04/17/1814:15
Received: 04/17/18 14:23 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
1970 mg/kg
7.7
1
04/26/18 23:55
04/27/18 21:46
7429-90-5
Arsenic
ND mg/kg
0.77
1
04/26/18 23:55
04/27/18 21:46
7440-38-2
Cadmium
0.26 mg/kg
0.077
1
04/26/18 23:55
04/27/18 21:46
7440-43-9
Calcium
4370 mg/kg
7.7
1
04/26/18 23:55
04/27/18 21:46
7440-70-2
Copper
77.8 mg/kg
0.38
1
04/26/18 23:55
04/27/18 21:46
7440-50-8
Lead
4.8 mg/kg
0.38
1
04/26/18 23:55
04/27/18 21:46
7439-92-1
Magnesium
712 mg/kg
7.7
1
04/26/18 23:55
04/27/18 21:46
7439-95-4
Molybdenum
2.0 mg/kg
0.38
1
04/26/18 23:55
04/27/18 21:46
7439-98-7
Nickel
5.1 mg/kg
0.38
1
04/26/18 23:55
04/27/18 21:46
7440-02-0
Potassium
1210 mg/kg
385
1
04/26/18 23:55
04/27/18 21:46
7440-09-7
Selenium
1.8 mg/kg
0.77
1
04/26/18 23:55
04/27/18 21:46
7782-49-2
Sodium
ND mg/kg
385
1
04/26/18 23:55
04/27/18 21:46
7440-23-5
Zinc
400 mg/kg
0.77
1
04/26/18 23:55
04/27/18 21:46
7440-66-6
7471 Mercury
Analytical Method: EPA7471 Preparation Method: EPA7471
Mercury
ND mg/kg
0.0047
1
04/26/18 02:55
04/27/18 08:29
7439-97-6
M1,R1
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
40.6 %
0.10
1
04/18/18 11:10
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.1 Std. Units
0.10
1
04/19/18 05:22
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
5120 mg/kg
0.12
1
04/30/18 14:21
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
13800 mg/kg
40.0
1
04/3011814:18
7727-37-9
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
4890 mg/kg
90.9
10
04/25/18 00:03
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
13800 mg/kg
1000
20
04/26/18 05:56
7727-37-9
353.2 Nitrogen, NO2IN03
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mglkg
20.0
10
04/25118 01:30
D3
Nitrogen, Nitrite
ND mg/kg
10.0
10
04/25/18 01:30
D3
Nitrogen, NO2 plus NO3
ND mg/kg
20.0
10
04/25/18 01:30
D3
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
4770 mg/kg
192
100
04/21/1814:53
7723-14-0
Date: 04/30/2018 02:23 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

�aceAnalyttcal
www.pacelabs.com
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 407975
QC Batch Method: EPA 7471
Associated Lab Samples: 92381194001
METHOD BLANK: 2263620
Associated Lab Samples: 92381194001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2263621
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 0.0060 04/27/18 08:21
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.083 0.073 87 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2263622 2263623
MS MSD
92381194001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND 11 .11 0.035 0.022 32 20 75-125 45 M1,R1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19

U
aceAnalyticaI
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Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 408151
QC Batch Method: EPA 3050
Associated Lab Samples: 92381194001
METHOD BLANK: 2264765
Associated Lab Samples: 92381194001
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
2-264766
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET
Matrix: Solid
Blank
Result
Spike
Cone.
500
50
50
500
50
50
500
50
50
500
50
500
50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
10.0
04/27/18 21:31
1.0
04/27/18 21:31
0.10
04/27/18 21:31
10.0
04/27/18 21:34
0.50
04/27/18 21:31
0.50
04/27/18 21:31
%0
04/27/18 21:31
0.50
04/27/18 21:31
0.50
04/27/18 21:31
500
04/27/18 21:31
1.0
04/27/18 21:31
500
04/27/18 21:31
1.0
04/27/18 21:34
LCS
Result
471
46.3
45.5
493
47.9
45.4
432
48.6
45.9
ND
44.5
444J
45.4
LCS
% Rec
94
93
91
99
96
91
86
97
92
92
89
89
91
Qualifiers
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Pace Analytical Services, LLC
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2264767
2264768
MS
MSD
92381747003 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result Cone.
Cone.
Result
Result
% Rec
% Rec
Limits RPD Qual
Aluminum mg/kg
4610 430
471
9060
11200
1030
1400
75-125 21 M1,R1
Arsenic mg/kg
2.2 43
47.1
39.8
43.0
87
87
75-125 8
Cadmium mg/kg
0.10 43
47.1
38.5
42.0
89
89
75-125 8
Results presented on this page are In
the units indicated by the
"UnW column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2264767
MS
92381747003 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
2264768
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
23400
430
471
26700
30400
775
1500
75-125
13 M1
Copper
mg/kg
2.5
43
47.1
44.9
49.1
98
99
75-125
9
Lead
mg/kg
8.9
43
47.1
45.8
51.9
86
91
75-125
12
Magnesium
mg/kg
286
430
471
729
797
103
109
75-125
9
Molybdenum
mg/kg
1.2
43
47.1
39.3
42.8
88
88
75-125
9
Nickel
mg/kg
2.6
43
47.1
39.9
43.6
87
87
75-125
9
Potassium
mg/kg
ND
430
471
541
586
103
104
75-125
8
Selenium
mg/kg
0.62J
43
47.1
36.6
39.8
84
83
75-125
8
Sodium
mg/kg
ND
430
471
561
605
96
97
75-125
8
Zinc
mg/kg
26.7
43
47.1
67.0
69.7
93
91
75-125
4
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

Pace Analytical Services, LLC
aceAnalytical®
9800 Kincey Ave. Suite 100
Fluntersville, NC 28078
www.pacelabs.com
i
[phone]
QUALITY CONTROL DATA
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 406669
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92381194001
SAMPLE DUPLICATE: 2256361
92380749003 Dup
Parameter
Units
Result Result RPD Qualifiers
Percent Moisture
%
16.6 16.6 0
SAMPLE DUPLICATE: 2256362
92381203001 Dup
Parameter
Units
Result Result RPD Qualifiers
Percent Moisture
%
53.6 50.2 6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

�- aceAnalytical
wvnvpacelabs.com
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 406893
QC Batch Method: EPA 9045
Associated Lab Samples: 92381194001
SAMPLE DUPLICATE: 2257616
Parameter Units
pH at 25 Degrees C Sid. Units
QUALITY CONTROL DATA
Analysis Method: - EPA 9045
Analysis Description: 9045 pH
92381216012 Dup
Result Result RPD
5.1 5.1
Qualifiers
0
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
i Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the resuR.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

U
a/
aceAnalytical
wvmpacelabs com
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 407571
QC Batch Method: EPA 350.1 1993 Rev 2.0
Associated Lab Samples: 92381194001
METHOD BLANK 2261435
Associated Lab Samples: 92381194001
Parameter Units
Nitrogen, Ammonia mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 1993 Rev 2.0
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 04/24/18 23:48
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2261436
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 500 505 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2261437 2261438
MS MSD
92381414001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 8970 2420 2420 11400 11500 100 103 90-110 0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

'aceAnaljftal ®
www.pacelabs.com
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 407574
QC Batch Method: EPA 351.2
Associated Lab Samples: 92381194001
METHOD BLANK: 2261451
Associated Lab Samples: 92381194001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 351.2
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 04/26/18 04:39
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2261452
-
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Nitrogen, Kjeldahl, Total
mg/kg
1000
962
96
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2261453
2261454
MS
MSD
92381414001
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total
mg/kg 84500
8330
8330
70800
84800
-165 4 90-110 18 M6,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 19

W
� raaceAnalXical
www.pacelabs.cum
I
i
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 407762
QC Batch Method: EPA 353.2
Associated Lab Samples: 92381194001
METHOD BLANK: 2262506
Associated Lab Samples: 92381194001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 04/25/18 01:17
ND 1.0 04/25/18 01:17
ND 2.0 04/25/18 01:17
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2262507
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 25 24.2 97 90-110
Nitrogen, Nitrite mg/kg 10 10.0 100 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 24.2 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2262508
2262509
MS
MSD
92381414001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Nitrogen, Nitrate
mg/kg
ND
195
195
186
184
95
94
90-110
1
Nitrogen, Nitrite
mg/kg
20.3
78.3
78.3
88.4
76.7
87
72
90-110
14 M1,R1
Nitrogen, NO2 plus NO3
mg/kg
ND
195
195
186
184
88
88
90-110
1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 19

acmnalXical
www.pacelabs.com
i
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
QC Batch: 406869
QC Batch Method: EPA 365.1
Associated Lab Samples: 92381194001
METHOD BLANK: 2257439
Associated Lab Samples: 92381194001
Parameter
Phosphorus
QUALITY CONTROL DATA
Analysis Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/kg ND 2.0 04/21/1811:20
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2257440
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 52.1 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2257441 2257442
MS MSD
92381143001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Phosphorus mg/kg 114 89.6 91.4 288 233 194 130 90-110 21 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

u
aceAnaljftal o
www.pacefab&coin
QUALIFIERS
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
DEFINITIONS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL- Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5,is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OP LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/30/2018 02:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19

aceAnalyiical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Solids, Metals, Nitrate
Pace Project No.: 92381194
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92381194001
Nitrate, Metals
EPA 3050
408151 EPA 6010
408237
92381194001
Nitrate, Metals
EPA 7471
407975 EPA 7471
408045
92381194001
Nitrate, Metals
ASTM D2974-87
406669
92381194001
Nitrate, Metals
EPA 9045
406893
92381194001
Nitrate, Metals
SM 2710B
408546
92381194001
Nitrate, Metals
TKN+NO3+NO2
408544
Calculation
92381194001
Nitrate, Metals
EPA 350.1 1993 Rev 2.0
407571
92381194001
Nitrate, Metals
EPA 351.2
407574
92381194001
Nitrate, Metals
EPA 353.2
407762
92381194001
Nitrate, Metals
EPA 365.1
406869
Date: 04/30/2018 02:23 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 19

qW
Document Name:
Document Revised: February 7, 2018
a
aceAnaocal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
issuing Authority:
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersvill Raleigh[] Mechanicsville❑
Clle -Name:Project q: W04 : 92381194
1
Courier: (:ed Ex []UPS LISPS []Qther: .❑Client
❑ II'II' I I II 110 I'll I I'll
Commercial pft e'
92
Custody Seal Present? ❑Yes Z No Seals Intact?
❑YesJNo''�
Packing Material: ❑bubble Wrap 2 bu ble Bags ❑None ❑ Other
Thermometer:
922TO36 TYPe of ice: -- []BlueCooler Temp ('C): Correction Factor, Add/Subtract (°C) +0,1
Cooler Temp Corrected (°C): 1
USDA Regulated Soil water sample)
Did samples orlginaSoa 'a quarantine zone within the United States: CA, NY, or SC (check maps)?
Mva. r7eT.-
383194
Date/InitialsPersonExaminingContents: in
Biological Tissue Frozen?
❑Yes []No gN/A`i
❑None
Temp should be above freezing to 6'C
[]Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
indnriina Hawaii and Puerto Ricol? 11Yes --P o
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑No
❑NIA
1.
Samples Arrived within Hold Time?
es
ONo
N/A
2.
Short Hold Time Analysis (<72 fir.)?
❑Yes
9-0—
ON/A
3.
Rush Turn Around Time Requested?
[--]Yes
jQNT
[]NIA
4.
Sufficient Volume?
YTS_
QN0
(]NIA
S.
Correct Containers Used?
-Pace Containers Used?
,j3r
es
ONo
[]No
[]N/A
[]NIA
6.
Containers Intact?
s
QNo
N/A
7.
Dissolved analysis: Samples Field Filtered?
0Yes
[]No
N/A
8.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
__--MYes
[]No
[]N/A
9.
Headspace in VOA Vials (>S•6mm)?
[]Yes
[]No
/�I A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[jYes
Oyes
(]No
❑No
.);� /A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Date Required? []Yes (]No
Person contacted: Date/Time:
Project Manager SCURF Review:�1 V Date:
Project Manager SRF Review: r� Date:
Page 16 of 19

aceAna1y6ca1 u F
tarty pacerabs cem
Section A
Required Client Information:
CHAIN-®F-CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately,
Section S Section C
Required Project Information: Invoice Information:
Page: 1 of 1
rn
CID
N
cc
a
Company: Veolia Water
Report To: Paul Spencer
Attention: Christopher Johnson
REGULATORY
17- NPOES C� GROUND WATER f DRINKING WATER
f UST (- RCRA RDTHER 503 Biosolids
Address: 3200 20th Avenue SE
Copy To: Christopher Johnson
Company Name: Veolia Water
Newton, NC 28658
3200 20th Avenue SE Newton,NC 28658
Email To: paui.soencerc(Dveolia. Corn
Purchase CC on file
order No.:
Pace Quote Reference:
GA I! IL r N r W I5Z NC
LOCATION F OH F SC f" NI h OTHER
Phone: [phone]
Fax:
Project Name: Solids, Metals, Nitrate
Pace Project Manager. Angela Baioni'
Requested std
Duo DateffAT:
Project Number:
Pace Profile #: 2816, 2
Filtered (YIN)
Section D Required VaI'd Matra Cod.
Ceent lnfarmotion MATRIX eGo2
«e�5v.na
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W Q. 0
COLLECTED
_
Q
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Preservatives
Requested
15'AaiFYarFS Y:N
SAMPLE 00 �. p
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COMPOSITE
START
COAPOSITE
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W Sample IDS MUST BE UNIQUE o o
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DATE TIME
DATE TIME
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SAMPLE CONDITIONS
Metals' AI(As, Ca, Cd, Cu, Pb, Mg, Mo, Ni, K; Se, Na,
Zn, H
•
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SIGNATURE of : SAMPLER ° " t {r (J \
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e-File(ALLQ020rev.4,29M2r06)22Jun2005

Document Name:
Document Revised: February 7, 2018
5
aceAnalytica!
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033•Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TdC, Oil and Grease, DRO/8015 (water) DOC, LLHS
"Bottom half of box Is to list number of bottle
Project t# -W0# ; 92381194
Due Date: 05/01/18
CLIENT: 92-Veolia Wa
PM: AMB
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pH Adjustment Log for Preseftfed Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of preservative
added
Lot N
Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a Copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 17 of 19
Ak

Page: i of 1
Report Number: 18-109-0206
Account Number: 05734 WaypRint.(2)
AYTICAL
Send To: PACE ANALYTICAL SVCS INC (for Angela Baioni) Project: SAR
ANGELA BAIONI
9800 KINCEYAVENUE
SUITE 100
HUNTERSVILLE , NC 28078
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS Date Sampled: 4/17/2018 14:15:00
Lab Number: 59846 Date Received: 04/19/2018 00:00
Sample Id : SAR/92381194002 Date Reported: 04/30/2018
NULM QUIlUb
bu.u4
bUU4UU
1U0.0
JM
04/19/2018 15:45
Moisture *
39.95
100.0
JM
04/19/2018 15:45
Total Calcium
0.90
9030
100
SMC
04/23/2018 15:05
Total Magnesium
0.15
1470
100
SMC
04/23/2018 15:05
Total Sodium
0.06
610
100
SMC
04/23/2018 15:05
Sodium Absorption Ratio *
1.60
Comments:
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
01reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole ur part, not may any reference be made
to u•grt, (h- —mule w the company irr any advertising. news release. or other public announcements without obtaining our prior written authorization.
SM-254OG
SM-254OG
6010C
6010C
6010C
CALCULATION
rofcr� #1 1041r1f
Pauric McGroary
Agronomist

Bi - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of Mav and ,tune 2018. This shows compliance with Alternative A5 of 40
CFR Part 503.32, 40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
Pathogen Reduction Reguirements - Alternative A5 (EFR1P)
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 67.35 deg.0 for 3.31 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN KILL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — NA Dry Weight Basis. Fecal Coliform Results - <31.5
(MPN/g) (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the, pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Unde ' ed,
Paul Spencer
Vector Attraction Reduction - Option 5
TIME & TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 65.25deg. C for approximately 23 20days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Unders' ed.
��J�J
Paul Spencer
PFRP Certification Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Under�igned,
Paill Spencer V
Project Manager
Veolia Water North America
Regional Compost Facility
3200 20th Ave., SE
Newton NC 28658
Date Signed:
I- V "2 -zZ&

MW
(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.

��'auc-,UeAnalytical
www.pacelabs.com
June 07, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Compost Metals May
Pace Project No.: 92386072
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 24, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 12

�PaceAnalytical
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I
CERTIFICATIONS
Project: Compost Metals May
Pace Project No.: 92386072
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 12

501
�acema0cal.®
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: Compost Metals May
Pace Project No.: 92386072
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92386072001 Compost EPA6010
SH1
8
PASI-A
EPA 7471
JMW1
1
PASI-A
SM 2540G
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

k—J
� aceAnalytical
mapacelabs.com
r
ANALYTICAL RESULTS
Project: Compost Metals May
Pace Project No.: 92386072
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Compost Lab ID: 92386072001 Collected: 05/24/18 09:00 Received: 05/24/18 10:20 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND mg/kg
0.91
1
06/05/18 02:30
06/05/18 22:01
7440-38-2
Cadmium
0.31 mg/kg
0.091
1
06/05/18 02:30
06/05/18 22:01
7440-43-9
Copper
92.1 mg/kg
0.45
1
06/05/18 02:30
06/05/18 22:01
7440-50-8
Lead
5.1 mg/kg
0.45
1
06/05/18 02:30
06/05/18 22:01
7439-92-1
Molybdenum
2.0 mg/kg
0.45
1
06/05/18 02:30
06/05/18 22:01
7439-98-7
Nickel
5.8 mg/kg
0.45
1
06/05/18 02:30
06/05/18 22:01
7440-02-0
Selenium
1.6 mg/kg
0.91
1
06/05/18 02:30
06/05/18 22:01
7782-49-2
Zinc
406 mg/kg
0.91
1
06/05/18 02:30
06/05/18 22:01
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.12 mg/kg
0.0064
2
06/0511812:10
06/05/1815:29
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G
Total Solids
53.6 %
0.000010
1
05/24/18 17:14
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
46.4 %
0.10
1
05/25/18 11:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2018 10:07 AM without the written consent of Pace Analytical Services, LLC.
Page 4 of 12

C.MnalXical
wmvpacelabs.com
QUALITY CONTROL DATA
Project: Compost Metals May
Pace Project No.: 92386072
QC Batch: 413355 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92386072001
METHOD BLANK: 2292390 Matrix: Solid
Associated Lab Samples: 92386072001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 06/05/1814:30
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL. SAMPLE: 2292391
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.072 86 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2292392 2292393
MS MSD
92385890001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND .043 .043 0.040 0.036 92 83 75-125 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2018 10:07 AM without the written consent of Pace Analytical Services, LLC.
Page 5 of 12

W
61011
AaceAnalyficai'
www.pacelabs.com
QUALITY CONTROL DATA
Project: Compost Metals May
Pace Project No.: 92386072
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 413736
Analysis Method:
EPA 6010
QC Batch Method: EPA 3050
Analysis Description:
6010 MET
Associated Lab Samples: 92386072001
METHOD BLANK: 2294315
Matrix: Solid
Associated Lab Samples: 92386072001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Arsenic
mg/kg
ND
1.0
06/06/18 21:49
Cadmium
mglkg
ND
0.10
06/06/18 21:49
Copper
mg/kg
ND
0.50
06/06/18 21:49
Lead
mg/kg
ND
0.50
06/06/18 21:49
Molybdenum
mg/kg
ND
0.50
06/06/18 21:49
Nickel
mg/kg
ND
0.50
06/06/18 21:49
Selenium
mg/kg
ND
1.0
06/06/18 21:49
Zinc
mg/kg
ND
1.0
06/06/18 21:49
LABORATORY CONTROL SAMPLE:
2294316
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits
Qualifiers
Arsenic
mg/kg
50
46.5
93
80-120
Cadmium
mg/kg
50
47.1
94
80-120
Copper
mg/kg
50
49.5
99
80-120
Lead
mg/kg
50
47.1
94
80-120
Molybdenum
mg/kg
50
50.6
101
80-120
Nickel
mg/kg
50
48.2
96
80-120
Selenium
mg/kg
50
45.1
90
80-120
Zinc
mg/kg
50
46.8
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2294317
2294318
MS
MSD
92384292019
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
2.3
33.7
33.3
28.7
31.5
79
88
75-125
9
Cadmium
mg/kg
ND
33.7
33.3
30.0
29.3
89
88
75-125
.2
Copper
mg/kg
4.0
33.7
33.3
37.9
37.0 101
99
75-125
2
Lead
mg/kg
4.2
33.7
33.3
33.7
35.7
88
95
75-125
6
Molybdenum
mg/kg
0.52
33.7
33.3
29.6
29.5
86
87
75-125
0
Nickel
mg/kg
3.2
33.7
33.3
35.0
34.6
95
94
75-125
1
Selenium
mg/kg
0.86
33.7
33.3
25.8
26.4
74
77
75-125
2 M1
Zinc
mg/kg
4.9
33.7
33.3
36.7
35.6
94
92
75-125
3
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2018 10:07 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 12
•

vcmnalytical
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I
QUALITY CONTROL DATA
Project: Compost Metals May
Pace Project No.: 92386072
QC Batch: 412318 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry WeightlPercent Moisture
Associated Lab Samples: 92386072001
SAMPLE DUPLICATE: 2287321
92386023011 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 28.0 27.5 2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2018 10:07 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 12

aceAnalytical
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i
QUALIFIERS
Project: Compost Metals May
Pace Project No.: 92386072
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration. _
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2018 10:07 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12

aceAn 1y�c i al
a
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I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Compost Metals May
Pace Project No.: 92386072
Pace Analytical Services, LLC
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92386072001
Compost
EPA 3050
413736 EPA 6010
413863
92386072001
Compost
EPA 7471
413355 EPA 7471
413843
92386072001
Compost
SM 2540G
412461
92386072001
Compost
ASTM D2974-87
412318
Date: 06/07/2018 10:07 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 12

1 aceAn L'�j� Sample Condition Upon Receipt SOUR) Page 1 or
Document No.: Issuing Authority:
! F CAR -CS 033 Rev 06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvillga Raleigh❑ Mechanicsville❑
Client Name: W®# : 92386®72
Courier: [-]Fed Ex ❑UPS ❑USPS ❑Gient 11111111 All111111 Ili
❑ Commercial ace ❑0ther:_ 92386072
Custody Seal Present? []Yes -EyNo Seals Intact? ❑Yes [>e L S�(
Date/Initials Person Examining Contents: / �J
Packing Material: ❑Bubble Wrap ❑Bubble Bags one ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes []No 0111A
❑IaGunlO: 92TO40 Type oflce: []Wet ❑Blue ❑tlene
Cooler Temp ('C): 5 0 Correction Factor: Add/Subtract (°C) t0.4
Tam
pshould 6e shove freezing to VC
Cooler Temp Corrected('CJ: 3, a ❑Samples out of tamp Criteria. samples on ice, cooling process
hasbegun
USDA Regulated Soil (T3—N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Cld samples originate from a foreign source (inNmatiomily,
Comments/Disttepancy:
Chain of Custody Present?
(21T.—
ON. ❑N/A
1.
Samples Arrived within Hold Time?
�
[IN. ❑NIA
2.
Short Hold Time Analysis [72 hr.)?
❑yes
OAd' EINIA
3.
Rush TemAround Time Requested?
❑yesOHS-
[]NIA
4•
Suffident Volume?
.87—.
EIN. ❑N/A
S.
CorrectCmtainers Used?
S!
❑t.
❑N/A
Containers Intact?
6Prs
[IN. ❑tl/A
7.
Dissolved analysis: Samples Field Filtered?
Y.
9. ❑N/A
8.
Sample Labels Match COC?
-Includes Date/Tme/tD/Analysis Matrix:
/ cs
i�✓
❑Na ❑N/A
9.
Headspace in VOA Wals (>5-6mm)7
❑Yet •
On EJ 1/A
10.
Trio Blank Present?
np ant—'k'cst� eas reseni7—-"Byes—[-1ua—�:+rA
❑Yes
❑❑_t o---❑ON/.A/
11•
--
COMMENT=/SAMPLe DISCREPANCY Field Data Required? ❑Yes ❑Na
:a s
Lot ID crimilt containers:
CUENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
17
Project Manager SCURF Review: (, Date: �,, r) 4-1 r` am' f�
Project Manager SRF Review: ��1�7 Date: � r1 -m -i n
Page 10 of 12

PaceAnaljdical
Section A Section B
Regw— C4enl Inrammlibn. Rcgeirod ft,- We.ev-
CHAIN-OF-CUSTODY / Analytical Request Document
The Chaia.bl-C-161( Is a LEGAL DOCUMENT. All retevael flelds must be completed accurelely.
Section C
ompany. Veotia
rtHughesweoLa.mm
_... _.__...._... ._
ananubm Logan Hughes
1
Addx,c- 3200 201h Ave SE
Spencerweolia.com
company Nama:REGULATORY
AGENCY
Newton, NC 28658AComsz
Emau To Logan.H0ghe5Qd veolia.comb.:
=—Lo,.n,.1H�1h�@1eoIja.wm
PRUST
— NPOES GROUNDWATER DRINKING WATER
Pnonp: 8289657401 Fan 8264656557
Compost Metals May
PacePmpd Angela Baioni
'- RCRA OTHER
Site LocatiovPmfJett NC
STATE:
Requested
Analysis
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(YIN)
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ADDITONAL COMMENTS
RELINQWSHED BVIAFFILIATION
DATE
TIME
ACCEPTED or AFRUATION
DATE
TIME
SAMPLECONDITIONS
METALS: Anv— CadmJ,Jm, Coppet. M,Plybden=, N--L
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5/?4/18
salana,m. _md. Hereon. Lead
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SAMPLER NAME AND SIGNATURE
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/JPafeflnalytrca( Document No.: Issuing Autlsorar.
F-CAR-CS-033•Rev O6 Pate Carolinas quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptlans; VOA, Caliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project 8'_ 1-1® ; 92336®72 _
Pit- RMB - Due DaLe: '06/06/1B
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Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
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added
Lots
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Out of hold, incorrect praservative, out of temp, incorrect containers.
Page 11 of 12

,�aleAnalytical@
www.pacelabs.com
June 29, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: June Fecal
Pace Project No.: 92390157
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most .
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in'the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Eaioni
[e-mail]
[phone] .
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
�Q404-
r
9e�RA'�0�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 5

r.
8C Anal ka
wvnvpacelaDs.eam
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. AN relevant fields must be completed accurately.
VaW." { is
Required Client Information:
Section B
Required Project informa90
Section C
: Invoice Inforrnalion:
Attentlon: Paul Spencer
veolla Company Name:
Address:
Pace Quote Reference
Paea Project Manager. Angela Baloni
Pace Profile 8
Page: 1 of 1
i NPDES I-' GROUND WATER r DRINKING WATER
(- UST I"" RCRA St OTHER IUP
r GA r IL r IN F MI K NC
dH f SC r tM r oTHER
Filtered (Y!N)
777777777
'CompanyVeolla Water
Report Ta: Pout Spencer
Addresss-
3200 2tNh Avenue BE
Copy To; Lo an.Hu h
Newton,
Newton,
, NC 28858
EmaN To; paULspencerC�yealia.com
PurchaseCC on file
Order No.:SITE
Phone: [phone] Fac 8284WMI
Project Name: ,tune Pecs
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Analytical e,=l e.x _ y
Pace Anal"ca9
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 06/28/2018
Reported: 06/29/2018 .
For: Veolia Water
Comments:
Sample Number Parameter Sample ID Result Unit Method
180628-13-01 Fecal Coliforms Fecal
180628-13-01 Percent Solids Fecal
Respectfully submitted,
r'Qp Vv ` —n)' " -)
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
<31.5 MPN/g SM92210E-2006
63.5 % SM25408-1997
Analyzed Analyst
06/28/2018 WC
06/28/2018 WC
PO Box 228 o Statesville, NC 28687 o 704/872/4697
Page 1 of Page 3 of 5

w
Condition of Receipt
Sample Number 180628-13-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, IBC 28687 • 704/872/4697
Page 2 of hge 4 of 5

FaceAnaly ical
CHAIN -OF -CUSTODY i Analytical Request Document
The Cham-c -Custody is a LEGAL DOCUMENT All relevant Gelds must !se compfe7M accuretefy
Section A
Required Client Intormatran
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Section C
im�Te fMarmalron
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aceAnalytical
www.pacelabs.com
July 10, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: June All Metals
Pace Project No.: 92389324
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 21, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
01*c " , �=Nu
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
pCGRF
O A'�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

�aceAnalj&al
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: June All Metals
Pace Project No.: 92389324
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

1I;acce Analytica
l
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SAMPLE ANALYTE COUNT
Project: June All Metals
Pace Project No.: 92389324
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92389324001 Comp EPA6010
SH1
13
PASI-A
EPA 7471
JMW1
1
PASI-A
SM 2540G
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045
ECH
1
PASI-A
SM 2710B
EWS
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 1993 Rev 2.0
CJH1
1
PASI-A
EPA351.2
BRJ
1
PASI-A
EPA353.2
DMN
3
PASI-A
EPA 365.1
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 92

aceAnalydical
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ANALYTICAL RESULTS
Project: June All Metals
Pace Project No.: 92389324
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Comp Lab ID: 92389324001 Collected: 06/21/18 08:05
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF
Received: 06/21/18 09:51 Matrix: Solid
Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
2840 mg/kg
8.3
1
06/22/18 14:15
06/26/18 01:52
7429-90-5
Arsenic
ND mglkg
0.83
1
06/22/18 14:15
06/26/18 01:52
7440-38-2
Cadmium
0.30 mg/kg
0.083
1
06/22/1814:15
06/26/18 01:52
7440-43-9
Calcium
5710 mg/kg
8.3
1
06/22/18 14:15
06/26/18 01:52
7440-70-2
Copper
90.5 mg/kg
0.42
1
06/22/18 14:15
06/26/18 01:52
7440-50-8
Lead
5.8 mg/kg
0.42
1
06/22/18 14:15
06/26/18 01:52
7439-92-1
Magnesium
882 mg/kg
8.3
1
06/22/18 14:15
06/26/18 01:52
7439-95-4
Molybdenum
2.1 mg/kg
0.42
1
06/22/18 14:15
06/26/18 01:52
7439-98-7
Nickel
6.5 mg/kg
0.42
1
06/22/18 14:15
06/26/18 01:52
7440-02-0
Potassium
1210 mg/kg
417
1
06/22/18 14:15
06/26/18 01:52
7440-09-7
Selenium
1.7 mg/kg
0.83
1
06/22/18 14:15
06/26/18 01:52
7782-49-2
Sodium
ND mglkg
417
1
06/22/18 14:15
06/26/18 01:52
7440-23-5
Zinc
480 mg/kg
0.83
1
06/22/18 14:15
06/26/18 01:52
7440-66-6
7471 Mercury
Analytical Method: EPA7471 Preparation Method: EPA7471
Mercury
0.069 mg/kg
0.015
5
06/2611816:30
06127/1814:32
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG
Total Solids
54.8 % 0.000010
1
06/21/18 15:06
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
45.2 %
0.10
1
06/22/18 11:55
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
7.8 Std. Units
0.10
1
06/28/18 12:36
Plant Available Nitrogen
Analytical Method: SM 2710B
Plant Available Nitrogen
9040 mg/kg
0.12
1
07/06/18 16:56
N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
25700 mg/kg
40.0
1
0710211815:33
7727-37-9
350.1 Ammonia
Analytical Method:, EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
6630 mg/kg
137
20
07/06/18 12:45
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
25700 mg/kg
952
20
06/29/18 03:53
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
2.0
1
06/22/18 12:36
Nitrogen, Nitrite
3.7 mglkg
0.99
1
06/22/18 12:36
Nitrogen, NO2 plus NO3
3.3 mg/kg
2.0
1
06/22/18 12:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 22

�aCeAnalytical
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i
ANALYTICAL RESULTS
Project: June All Metals
Pace Project No.: 92389324
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Comp Lab ID: 92389324001 Collected: 06/21/18 08:05 Received: 06/21/18 09:51 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 4340 mg/kg 185 100 06/25/18 20:16 7723-14-0
Date: 07/10/2018 08:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

u
_ f �aceAnaljftal
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Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416321
QC Batch Method: EPA 7471
Associated Lab Samples: 92389324001
METHOD BLANK: 2308561
Associated Lab Samples: 92389324001
Parameter Units
Mercury mglkg
LABORATORY CONTROL SAMPLE: 2308562
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 06/27/1814:04
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.083 0.072 86 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2308563 2308564
MS MSD
92389280001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.10 .17 .17 0.088 0.082 -7 -11 75-125 8 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 22

�aceAna lytical
www.pacelabs.com
Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416313
QC Batch Method: EPA 3050
Associated Lab Samples: 92389324001
METHOD BLANK: 2308494
Associated Lab Samples: 92389324001
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
2308495
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET
Matrix: Solid
Blank
Result
Spike
Conc.
500
50
50
500
50
50
500
50
50
500
50
500
50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
Qualifiers
10.0
06/26/18 01:15
1.0
06/26/18 01:15
0.10
06/26/18 01:15
10.0
06/26/18 01:15
0.50
06/26/18 01:15
0.50
06/26/18 01:15
10.0
06/26/18 01:15
0.50
06/26/18 01:15
0.50
06/26/18 01:16
500
06/26/18 01:15
1.0
06/26/18 01:15
500
06/26/18 01:15
1.0
06/26/18 01:15
LCS
Result
477
44.5
46.0
495
47.9
45.7
469
49.6
47.0
ND
43.3
491J
46.0
LCS
% Rec
95
89
92
99
96
91
94
99
94
97
87
98
92
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2308496
2308497
MS
MSD
92389280001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum mg/kg
42600
1700
1790
42900
43300
16
39
75-125
1 E,M1
Arsenic mg/kg
ND
170
179
154
163
90
91
75-125
6
Cadmium mg/kg
0.77
170
179
158
169
92
94
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

W
aceAnaij4ical
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QUALITY CONTROL DATA
Project: June All Metals
Pace Project No.: 92389324
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2308496
MS
92389280001
Spike
Parameter
Units
Result
Cone.
Calcium
mg/kg
25800
1700
Copper
mg/kg
279
170
Lead
mg/kg
7.2
170
Magnesium
mg/kg
2640
1700
Molybdenum
mg/kg
11.7
170
Nickel
mg/kg
12.0
170
Potassium
mg/kg
ND
1700
Selenium
mg/kg
7.6
170
Sodium
mg/kg
ND
1700
Zinc
mg/kg
677
170
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
2308497
MSD
Spike
MS
MSD
MS
MSD
% Rec
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
1790
26800
26500
60
37
75-125
1 M1
179
431
438
89
88
75-125
2
179
158
169
89
90
75-125
6
1790
4160
4340
89
95
75-125
4
179
175
187
96
98
75-125
7
179
165
177
90
92
75-125
7
1790
2750
2950
94
101
75-125
7
179
153
165
85
88
75-125
7
1790
2300
2430
97
100
75-125
6
179
808
826
77
83
75-125
2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 22

1�acaeAnalytical
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I
QUALITY CONTROL DATA
Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416139 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92389324001
SAMPLE DUPLICATE: 2307750
92389266001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 23.7 26.2 10
SAMPLE DUPLICATE: 2307751
92389324001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 45.2 45.1 0
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

aceAnalytical
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QUALITY CONTROL DATA
Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416995 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92389324001
SAMPLE DUPLICATE: 2312210
92389410001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 7.7 7.7 0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
VO4)875-9092
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

aceAnalytical
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Project: June All Metals
Pace Project No.: 92389324
QC Batch: 417837
QC Batch Method: EPA 350.1 1993 Rev 2.0
Associated Lab Samples: 92389324001
METHOD BLANK: 2316634
Associated Lab Samples: 92389324001
Parameter Units
Nitrogen, Ammonia mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 1993 Rev 2.0
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 07106/1811:40
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2316635
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 500 479 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2316636 2316637
MS MSD
92389421010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg ND 384 384 370 375 96 97 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 11 of 22

41(1
�Analytical @
WV".Pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
June All Metals
Pace Project No.:
92389324
QC Batch:
417088 Analysis Method: EPA 351.2
QC Batch Method:
EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: . 92389324001
METHOD BLANK: 2312974
Associated Lab Samples: 92389324001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2312975
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 06/29/18 03:44
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1000 995 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2312976 2312977
MS MSD
92389588001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 7350 1850 2120 16700 19100 57 165 90-110 14 M6, R1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22
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QUALITY CONTROL DATA
Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416270 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92389324001
METHOD BLANK: 2308310
Associated Lab Samples: 92389324001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 06/22/1812:21
ND 1.0 06/22/1812:21
ND 2.0 06/22/1812:21
Qualifiers
Pace Analytical Services, LLC
9800 KnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2308311
Spike LCS LCS % Rec
Parameter Units Conc_ Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 25 24.9 100 90-110
Nitrogen, Nitrite mg/kg 10 10 100 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 24.9 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2308312
2308313
MS
MSD
92388701001 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result Conc.
Conc. '
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Nitrogen, Nitrate
mg/kg
ND 128
128
122
122
94
94
90-110
0
Nitrogen, Nitrite
mg/kg
ND 51
51
48.0
47.5
94
93
90-110
1
Nitrogen, NO2 plus NO3
mg/kg
ND 128
128
122
122
94
94
90-110
0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: June All Metals
Pace Project No.: 92389324
QC Batch: 416359 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92389324001
METHOD BLANK: 2308849
Associated Lab Samples: 92389324001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 2308850
Parameter Units
Phosphorus mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 06/25/18 20:1'
Spike LCS LCS
Conc. Result % Rec
47.2 49.1 104
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
% Rec
Limits Qualifiers
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2308851 2308852
MS MSD
92388863001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 287 139 136 449 408 117 89 90-110 10 M6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/10/2018 08:55 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 22

Pace Analytical Services, LLC
` �aceAnalical 9800
PQncey Ave. te 100
Hunte sville, NC128078
wmxpacelabsxom [phone]
QUALIFIERS
Project: June All Metals
Pace Project No.: 92389324
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: June All Metals
Pace Project No.: 92389324
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92389324001
Comp
EPA 3050
416313 EPA 6010
416402
92389324001
Comp
EPA 7471
416321 EPA 7471
416405
92389324001
Comp
SM 254OG
416100
92389324001
Comp
ASTM D2974-87
416139
92389324001
Comp
EPA 9045
416995
92389324001
Comp
SM 2710B
418091
92389324001
Comp
TKN+NO3+NO2
417514
Calculation
92389324001
Comp
EPA 350.1 1993 Rev 2.0
417837
92389324001
Comp
EPA 351.2
417088
92389324001
Comp
EPA 353.2
416270
92389324001
Comp
EPA 365.1
416359
Date: 07/10/2018 08:55 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

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Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 06/21/2018
Reported: 06/22/2018
For: Veolia Water
Comments:
Sample Number
Parameter
Sample ID
Result
unit
Method
Analyzed
Analyst
180621-13-01
Fecal Coliforms
V. Water
>2552
MPN/g
SM92210E-2006
06/21/2018
WC
180621-13-01
Percent Solids
V. Water
62.7
%
SM254OB-1997
06/21/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 © Statesville, NC 28687 • 704/872/4697
Page 1 Rae 20 of 22

Condition of Receipt
Sample Number 180621-13-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 o Statesville, NC 28687 o 704/872/4697
Page 2 Kage 21 of 22

P
FaceAnalytical -
CHAIN -OF -CUSTODY I Analytical Request Document
The Cham-ot-Cus•,ody Is a LEGAL DOCUMENT AU relevant Fields must t> completed accurataly
Section A Section B Section C Pafls; 1 of 1
Roquffed Cdent info mmlion Requimd Plopct InfonnW.n Invoice lwomut:en
C«nPr Y Veolia Water Repo( To Paul Spencer Attention Paul Spencer REGULATORY
Address 32M 20M Averato SE Copy To [.r ,an Ali y'='_-_;dipas)r� Comprny Name '- NPDES { GROUND VVATER DRINKINGWATER
Na ,Iw, NC 286545 Address UST ( RCRA X 01 HER—IUP—
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Bi - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of ,lulu and Angust 2018.The August Fecal and Metal results were
conducted on September 13th of 2018. This shows compliance with Alternative A5 of 40 CFR Part 503.32,
40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
Pathloendrtetio» Re anire>r>tnents - Ai�ezrunsa>E�a= AS (��7R�i
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 68.95 deg.0 for 3.49 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN RILL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — NA Dry Weight Basis. Fecal Coliform Results - <51.9
MPN/ (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Under s' ed,
Paul Spencer
Vector Attraction Reduction - Option 5
TEME & TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 66.25deg. C for approximately 24.45 days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Unders' ed.
ea4le
Paul Spencer
PFRP Certification Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Undersigned,
Paul Spencer
Project Manager
Veolia Water North America
Regional Compost Facility
3200 20th Ave., SE
Date Signed:
a 7 - aod

Newton NC 28658
(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.

acmnalytical
www.pacelabs.com
July 23, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: July Metals SAR +
Pace Project No.: 92391774
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on July 12, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted, outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
L ", 1-�=n1
Angela Saioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
A�CR,tc
geORAro�.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pagel of 27

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CERTIFICATIONS
Project: July Metals SAR +
Pace Project No.: 92399774
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
Missouri Certification #: 235
ANAB DOD-ELAP Rad Accreditation #: L2417
Montana Certification #: Cert0082
Alabama Certification #: 41590
Nebraska Certification #: NE-OS-29-14
Arizona Certification* AZ0734
Nevada Certification M PA014572018-1
Arkansas Certification
New Hampshire/TNI Certification #: 297617
California Certification #: 04222CA
New Jersey/TNI Certification #: PA051
Colorado Certification #: PA01547
New Mexico Certification M PA01457
Connecticut Certification #: PH-0694
New York/TNI Certification #: 10888
Delaware Certification
North Carolina Certification * 42706
EPA Region 4 DW Rad
North Dakota Certification #: R-190
FloridarTNI Certification #: E87683
Ohio EPA Rad Approval: #41249
Georgia Certification * C040
OregonlrNI Certification* PA200002-010
Guam Certification
Pennsylvania/TNI Certification #: 65-00282
Hawaii Certification
Puerto Rico Certification #: PA01457
Idaho Certification
Rhode Island Certification #: 65-00282
Illinois Certification
South Dakota Certification
Indiana Certification
Tennessee Certification #: 02867
Iowa Certification M 391
Texas/TNI Certification #: T104704188-17-3
Kansas/TNI Certification * E-10358
Utah/TNI Certification #: PA014572017-9
Kentucky Certification * KY90133
USDA Soil Permit #: P330-17-00091
KY WW Permit #: KY0098221
Vermont Dept. of Health: ID# V17-0282
KY WW Permit #: KY0000221
Virgin Island/PADEP Certification
Louisiana DHH/TNI Certification #: LA180012
VirginiaNELAP Certification #: 9526
Louisiana DEQ/TNI Certification #: 4086
Washington Certification #: C868
Maine Certification #: 2017020
West Virginia DEP Certification #: 143
Maryland Certification #: 308
West Virginia DHHR Certification * 9964C
Massachusetts Certification #: M-PA1457
Wisconsin Approve List for Rad
Michigan/PADEP Certification #: 9991
Wyoming Certification #:8TMS-L
^u_
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification * 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: July Metals SAR +
Pace Project No.: 92391774
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92391774001 Comp EPA6010D
SH1
13
PASI-A
EPA 7471B
JMW1
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 1010A
ECH
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM4500S2F-00
PAS
1
PASI-PA
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: July Metals SAR +
Pace Project No.: 92391774
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Comp Lab ID: 92391774001 Collected: 07/12/18 07:45 Received: 07/12/18 09:45 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050E
Aluminum
3000 mg/kg
8.2
1
07/13/18 10:30
07/16/18 00:52
7429-90-5
Arsenic
ND mg/kg
0.82
1
07/13/18 10:30
07/16/18 00:52
7440-38-2
Cadmium
0.35 mg/kg
0.082
1
07/13/18 10:30
07/16/18 00:52
7440-43-9
Calcium
5430 mg/kg
8.2
1
07/13/18 10:30
07/16/18 00:52
7440-70-2
Copper
98.3 mg/kg
0.41
1
07/13/18 10:30
07/16/18 00:52
7440-50-8
Lead
6.2 mg/kg
0.41
1
07/13/18 10:30
07/16/18 00:52
7439-92-1
Magnesium
937 mg/kg
8.2
1
07/13/18 10:30
07/16/18 00:52
7439-95-4
Molybdenum
2.6 mg/kg
0.41
1
07/13/18 10:30
07/16/18 00:52
7439-98-7
Nickel
6.7 mg/kg
0.41
1
07/13/18 10:30
07/16/18 00:52
7440-02-0
Potassium
1520 mg/kg
410
1
07/13/18 10:30
07/16/18 00:52
7440-09-7
Selenium
1.6 mg/kg
0.82
1
07/13/18 10:30
07/16/18 00:52
7782-49-2
Sodium
444 mg/kg
410
1
07/13/18 10:30
07/16/18 00:52
7440-23-5
Zinc
496 mg/kg
0.82
1
07/13/18 10:30
07/16/18 00:52
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
0.068 mg/kg
0.0045
1
0711611812:36
07/16/1815:38
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 2540G-2011
Total Solids
63.2 %
0.000010
1
07/12/18 17:56
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
36.8 %
0.10
1
07/13/18 11:58
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200.0 deg F
70.0
1
07/17/18 10:00
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method:
SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg
0.99
1
07/19/18 22:13
07/20/18 02:17
734S Reactive Sulfide
Analytical Method: SM4500S2F-00
Preparation Method:
SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg
9.9
1
07/19/18 22:13
07/19/18 22:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 27

'acmnalytical
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I
i
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 419067
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92391774001
METHOD BLANK: 2322930
Associated Lab Samples: 92391774001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2322931
Parameter Units
Mercury mglkg
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 07116/1814:32
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.083 0.082 98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2322932 2322933
MS MSD
35403561001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0067 .074 .074 0.079 0.082 98 102 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 27

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_ aceAnalytical
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QUALITY CONTROL DATA
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 419005 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92391774001
METHOD BLANK: 2322572
Associated Lab Samples: 92391774001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Aluminum
mg/kg
ND
10.0
07/15/18 23:54
Arsenic
mg/kg
ND
1.0
07/15/18 23:54
Cadmium
mg/kg
ND
0.10
07/15/18 23:54
Calcium
mg/kg
ND
10.0
07/15/18 23:54
Copper
mg/kg
ND
0.50
07/15/18 23:54
Lead
mg/kg
ND
0.50
07/15/18 23:54
Magnesium
mg/kg
ND
10.0
07/15/18 23:54
Molybdenum
mg/kg
ND
0.50
07/15/18 23:54
Nickel
mg/kg
ND
0.50
07/15/18 23:54
Potassium
mg/kg
ND
500
07/15/18 23:54
Selenium
mg/kg
ND
1.0
07/15/18 23:54
Sodium
mg/kg
ND
500
07/15/18 23:54
Zinc
mg/kg
ND
1.0
07/15/18 23:54
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2322573
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
506
101
80-120
Arsenic
mg/kg
50
47.0
94
80-120
Cadmium
mg/kg
50
48.0
96
80-120
Calcium
mg/kg
500
505
101
80-120
Copper
mg/kg
50
50.2
100
80-120
Lead
mg/kg
50
47.8
96
80-120
Magnesium
mg/kg
500
488
98
80-120
Molybdenum
mg/kg
50
51.8
104
80-120
Nickel
mg/kg
50
48.9
98
80-120
Potassium
mg/kg
500
508
102
80-120
Selenium
mg/kg
50
45.7
91
80-120
Sodium
mg/kg
500
527
105
80-120
Zinc
mg/kg
50
47.1
94
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2322574
2322575
MS
MSD
92391621001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum mg/kg
3920
385
366
6310
6790
619
783
75-125
7 M1
Arsenic mg/kg
1.4
38.5
36.6
34.3
32.2
85
84
75-125
6
Cadmium mg/kg
0.22
38.5
36.6
34.5
32.7
89
89
75-125
5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 27

,�Iac'eAnaljdical"
www.pacelabs.com
QUALITY CONTROL DATA
Project: July Metals SAR +
Pace Project No.: 92391774
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2322574
2322575
MS
MSD
92391621001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
1440
385
366
2110
2640
175
329
75-125
22 M1,R1
Copper
mg/kg
5.5
38.5
36.6
74.1
40.8
178
96
75-125
58 M1,R1
Lead
mg/kg
64.2
38.5
36.6
106
94.7
109
83
75=125
11
Magnesium
mg/kg
469
385
366
888
728
109
71
75-125
20 M1
Molybdenum
mg/kg
ND
38.5
36.6
35.0
33.2
90
90
75-125
5
Nickel
mg/kg
1.8
38.5
36.6
36.7
35.2
91
91
75-125
4
Potassium
mg/kg
ND
385
366
633
623
114
117
75-125
2
Selenium
mg/kg
ND
38.5
36.6
32.3
30.4
84
83
75-125
6
Sodium
mg/kg
ND
385
366
413
388
95
93
75-125
6
Zinc
mg/kg
48.0
38.5
36.6
87.0
81.4
101
91
75-125
7
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 27

e/
aceAnaljftal o
vnvwpacolabs.com
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 418938
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92391774001
SAMPLE DUPLICATE: 2322330
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2322331
Parameter
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92391652003
Dup
Units
Result
Result
%
13.6
12.9
92391774001
Dup
Units
Result
Result
36.8
36.8
RPD Qualifiers
5
RPD Qualifiers
0
s
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 27

�aceAnaIXical
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I
QUALITY CONTROL DATA
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 419296 Analysis Method: EPA 1010A
QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92391774001
SAMPLE DUPLICATE: 2324124
92391921001 Dup
Parameter Units Result Result
Flashpoint deg F 57.8 69.6
RPD Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 27

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�%eAnalyfical
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I
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 306475
QC Batch Method: SW-846 7.3.3.2
Associated Lab Samples: 92391774001
METHOD BLANK: 1498249
Associated Lab Samples: 92391774001
Parameter Units
Cyanide, Reactive mg/kg
LABORATORY CONTROL SAMPLE: 1498250
Parameter Units
Cyanide, Reactive mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 9014
Analysis Description: 733C Reactive Cyanide
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.99 07/20/18 01:59
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
100 ND 0 0-8
SAMPLE DUPLICATE: 1498251
30259253001 Dup
Parameter Units Result Result
Cyanide, Reactive mg/kg ND ND
RPD Qualifiers
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 27

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: July Metals SAR +
Pace Project No.: 92391774
QC Batch: 306473
Analysis Method:
SM4500S2F-00
QC Batch Method: SW-846 7.3.4.2
Analysis Description:
734S Reactive Sulfide
Associated Lab Samples: 92391774001
METHOD BLANK: 1498246
Matrix: Solid
Associated Lab Samples: 92391774001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfide, Reactive
mg/kg
ND
9.9 07/19/18 22:16
LABORATORY CONTROL SAMPLE: 1498247
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Sulfide, Reactive
mg/kg
199 39.7
20 0-52
SAMPLE DUPLICATE: 1498248
30259253001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Sulfide, Reactive
mg/kg
ND
ND ,
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 27

MW
aceAnalytical
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I
QUALIFIERS
Project: July Metals SAR +
Pace Project No.: 92391774
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/23/2018 02:27 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 27

�aceAr�a/yticai
��
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: July Metals SAR +
Pace Project No.: 92391774
Lab ID
Sample ID
QC Batch Method
92391774001
Comp
EPA 3050B
92391774001
Comp
EPA 7471 B
92391774001
Comp
SM 254OG-2011
92391774001
Comp
ASTM D2974-87
92391774001
Comp
EPA 1010A
92391774001
Comp
SW-846 7.3.3.2
92391774001
Comp
SW-846 7.3.4.2
Date: 07/23/2018 02:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch
Analytical Method
Batch
419005
EPA 601OD
419194
419067
EPA 7471B
419197
419289
418938
419296
306475
EPA 9014
306524
306473
SM4500S2F-00
306523
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 27

U
Document Name:
Document Revised: February 7, 2018
m
80-AllalAcal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
F•CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples: r
Asheville ❑ Eden❑ Greenwood ❑ Huntersville /❑ Raleigh[] Mechanicsville❑
Client Name:
'Upon Receipt
Project u:
Courier: []Fed Ex ❑UPS ❑LISPS ❑Ciient
❑ Commercial /QPace ❑Other:
Custody Seal Present? ❑Yes [�No Seals Intact? []Yes ZNo
WO 92391774
II � III II r IN
s it i s ail
92391774
Date/initials Person Examining Contents:
Packing Material: ❑Bubble Wrap []Bubble Sags ❑None ❑ Other Blologlcal Tissue Frozen?
Thermome,�r: Type of Ice: *et ❑slue None
[]Yes []No UN/A
1'_.IIR Gun ID: 92TO40
Cooler Temp ` '~
p (°Cj; ,.„1_ C.? Correction Factor: Add/Subtract ("C) +0.4 Tempshould be above freezing to 6'C
Cooler Temp Corrected (°C): S • 5/ {]Samples out of temp criteria. samples on Ice, cooling process
has begun
USDA Regulated Soil (1 N/A, water sample)
Did samples originate irf a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (Inter ationally,
r—i.._ _ ill.._ .nrL.din° Hawaii and Pnrrto Rlcol? MYes RNo
Comments/Discrepancy: '
Chain of Custody Present?
EjYes
©No
(]N/A
1.
Samples Arrived within Hold Time?
� r
MYes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
byes
Efft
ON/A
3.
Rush Turn Around Time Requested?
OYes
i No
[]N/A
4.
Sufficient Volume?
E Yes
ONo
[]N/A
5.
Correct Containers Used?
❑No
[]N/A
6.
-Pace Containers Used?
by-esYcs
[3No
j]N/A
Containers Intact?
i Yes
ONo
)]N/A
7.
Dissolved analysis: Samples Field Filtered?
I]Yes
[]No
i N/A
8.
Sample Labels Match COO
[]No
[:]N/A
9.
�[Ycs
-includes Date/Time/ID/Analysis Matrix:
Headspace in VOA % lals (>5-6mm)7
OYes
ONo
•r
/ N/A
10,
1p 131155K Presentes
o
Trip Blank Custody Seals Present?
OYes
No
i
QN/A
COMMENTS/SAMPLE DISCREPANCY
Lot iD of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted,
Date/Time:
Field Date Required? []Yes ONO
r
Project Manager SCURF Review; % ems' Date: r r�
Project Manager SRF Review: Date: ­ t''l
Page 14 of 27

WPW
CHAIN -OF -CUSTODY J Anatlytacal Request Document
o
KaceAnalytiealThe Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields m st be completed accurately. CD
tV—V ABCe'a D5 COITI
t0
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Section A Section B Section C Page: of
Required Client Information: Required Project Information: Invoice Information:
company: Veolia Water Report
To: Paul Spencer
Attention: Paul Spencer
F NPD
r US
REGULATORY
S i GROUNDWATER F DRINKING WATER
RCRA i OTHER_X ^_
Address: 320020th Avenue SE COPY
TO: Loaan.Huahes(cDveolia
Company Name:
Newton, NC 28658
Address:
EmaIITo: pau1.spencerPveeh2.Cam Purchase
CC on file
Pace Quote Reference:
r r
r GA r IL IN MI NC X
Order
No.:
Filtered
, I
• r— OH r SC WI F OTHER
IN)
Phone: 828A65-1401
Fax Project
Name: July Metals SAR +
Pace Project Manager. Angela Beoni
Requosted Std Project
Due DaterrAT'
Number:
Pace Profile'#: 2816, 1
Section D VnGd Matrtr Codc
Raquimd Client lnlmmatton AAI AT I CO-
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Document Name:
Document Revised: February 7, 2018
�r aceAnalytrcal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project a
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box Is to list number of bottle
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pH Adjustment
Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Oate preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Loth
Note: Whenever there Is a discrepancy affecting North Carolina compaance sampies, a copy or this rorm wm ue sera to u,n ivur M �WQl i„a,UG-11,
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 15 of 27

JaceAnalytical® ANALYTICAL REPORT
National Canter !or Testing 6 Innova
don July 23, 2018
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1009775
Samples Received: 07/17/2018
Project Number: 92391774
Description: July Metals SAR +
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By: � �k L-0�
Nancy McLain
Project Manager
Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
4y,

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Tc: Table of Contents
2
LP
Ss: Sample Summary
3
E
Cn: Case narrative
Sr: Sample Results
5
3SS
COMP L1009775-01
5
4Cn
Qc: Quality Control Summary
6
Total Solids by Method 2540 G-2011
6
Er
Metals (ICP) by Method 6010D
7
GI: Glossary of 'Terms
8
EC
Al: Accreditations & Locations
9
Sc: Sample Chain of Custody
10
E'l
Page 18 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92391774 L1009775 07/23/1810:00 2 of 11

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
COMP L1009775-01 Solid
07/12/1807:45
07/17/1808:45
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Calculated Results
WG1138391
1 07118/1810:48
07/21/1813:08
CCE
Total Solids by Method 2540 G-2011
WG1139810
1 07/19/1814:25
07/19/1814:36
KS
Metals (ICP) by Method 6010D
WG1140041
1 07/18/18 22:05
07/19/1813:23
CCE
Page 19 of 27
ACCOUNT:
PROJECT:
SDG:
DATErfIME:
PAGE:
Pace Analytical - Huntersville, NC
92391774
L1009775
07/23/18 10:00
3 of 11

CASE NARRATIVE ONE LAB. NATIONWIDE. e
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All radiochemical sample results for
solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet
weight was requested by the client. All Method and Batch Quality Control are within established
criteria except where addressed in this case narrative, a non-conformance form or properly qualified
within the sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
Nancy McLain
Project Manager
Page 20 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92391774 L1009775 07/23/1810:00 4 of 11

COMP SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 07/12/18 07:45 L1009775
Calculated Results
CAD
Result Qualifier
Dilution
Analysis
Batch
Analyte
Sodium Adsorption Ratio 1.19
1
date / time
07/21/201813:08
WG1138391
E
Total Solids by Method 2540 G-2011
3
Ss '
Result Qualifier
Dilution
Analysis
Batch
Analyte %
date / time
a
Total Solids 38.1
1
07/19/201814:36
WG1139810
Cn
Metals (ICP) by Method 6010D
Result (dry) Qualifier
Analyte mg/kg
RDL (dry) Dilution
mg/kg
Analysis Batch
date / time
6 Qc
Calcium 11000
263
1
07/19/201813:23 WG1140041
Magnesium 1530
263
1
07/19/201813:23 WG1140041
�GI
Sodium 650 B
263
1
07/19/201813:23 WG114004'i
yAl
9
Sc
Page 21 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92391774 L1009775 07/23/18 10:00 5 of 11

WG1139810
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3327125-1 07/19/1814:36
MB Result MB Qualifier MB MDL MB RDL
Analyte % % %
Total Solids 0.00100
L1009766-01 Original Sample (OS) ® Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1009775-01
(OS) L1009766-01 07/19/1814:36 • (DUP) R3327125-3 07/19/1814:36
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte % % % %
Total Solids 97.4 96.9 1 0.446 5
Laboratory Control Sample (LCS)
(LCS) R3327125-2 07/19/1814:36
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte % % % %
Total Solids 50.0 50.0 100 85.0-115
ACCOUNT: PROJECT: SDG:
DATE/TIME:
-,3— "):—
ONE LAB. NATIONWIDE.
Page 22 of 27
PAGE:
r of"

1
x7 ■ o a a 0 a■■IL
WG1140041 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Metals (ICP) by Method 6010D L1009775-01
Method Blank (MB)
(Mb) H3326896-1 07/19/18 12:50
MB Result
Analyte
mg/kg
Calcium
5.41
Magnesium
1.41
Sodium
55.7
MB Qualifier
MB MDL
MB RDL
mg/kg
mg/kg
J
4.63
100
J
1.11
100
J
9.85
100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3326896-2 07/19/1812:53 > (LCSD) R3326896-3 07/19/1812:55
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte mg/kg mg/kg mg/kg
%
%
%
%
%
Calcium 1000 1070 1030
107
103
80.0-120
3.82
20
Magnesium 1000 1040 1010
104
101
80.0-120
2.53
20
Sodium 1000 1050 998
105
99.8
80.0-120
4.78
20
L1O1O19O-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1010190-01 07/19/1812:58 • (MS) R3326896-6 07/19/1813:06 • (MSD) R3326896-7 07/19/1813:09
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
Calcium
1000
84300
100000
169000
1590
8420
1 75.0-125
Magnesium
1000
31700
36500
84100
484
5240
1 75.0-125
Sodium
1000
260
1320 `
1350
106
109
1 75.0-125
MS Qualifier MSD Qualifier RPD RPD Limits
E V E J3 V 50.8 20
V J3 V 78.9 20
2.21 20
ACCOUNT:
Pace AnaMical - Huntersville. NC
PROJECT: SDG:
92391774 1 inn4,77s
DATE/TIME:
mnono 1—n
Page 23 of 27
PAGE:

GLOSSARY OF TERMS ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry) Results are reported based on the dry weight of the sample. (this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
RDL
Reported Detection Limit.
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used In the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
E
The analyze concentration exceeds the upper limit of the calibration range of the Instrument established by the initial
calibration (ICAL).
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
V
The sample concentration is too high to evaluate accurate spike recoveries.
ICE
E�C
Fs
En,
s '
Sr
i
F
R
El
9
Sc
Page 24 of 27
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - I-Iunlersville, NC 92391774 L1009775 ' 07/23/18 10:00 8 of 11

ACCREDITATIONS &
LOCATIONS
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
�®
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample Integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
{t
' Not all certifications held by the laboratory are applicable to the results reported In the attached report.
_
' Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
E
State Accreditations
Alabama
40660
Nebraska
NE-OS-15-05
F
Alaska
17-026
Nevada
TN-03-2002-34
Ariza
on
AZO612
New Hampshire
2975
Arkansas
88-0469
NewJersey—NELAP
TN002
En
California
2932
New Mexico'
n/a
Colorado
Connecticut
TN00003
PH-0197
New York
North Carolina
11742
Env375
F
Flar(da
E87487North
Carolina'
DW21704
Georgia
NELAP
North Carolina 3
41
Georgia
923
North Dakota
R-140
GQC j
Idaho
TN00003
Ohio—VAP
CL0069
Illinols
Indiana
200_008
C-TN-01
Oklahoma
Oregon
9915
TN200002
E
Iowa
364
Pennsylvania
68-02979
Kansas
Kentucky' 6
E-10277
90010
Rhode Island
South Carolina
LA000356
84004
1�1
Kentucky'
16
South Dakota
nla
Louisiana
A130792
Tennessee' °
2006
Louisiana'
LA180010
Texas
T104704245-17-14
95C
Maine
TN0002
Texas'
LAB0152
Maryland
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
Vi2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Thiid Party Federal Accreditations
A2LA — ISO 17025
1461.01
AIHA--LAP,LLC EMLAP
100789
A2LA — ISO 17025 6
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water ' Underground Storage Tanks
3 Aquatic Toxicity "Chemical/Microbiological s Mold 6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
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ACCOUNT: PROJECT: SDG:
Pace Analytical - Huntersville, NC 92391774 L1009775
7 1.1E
NY
PA
FL
VJV VA�,t�
T�.
L r
Page 25 of 27
DATEffIME: PAGE:
07/23/1810:00 9 of 11

Chain of Custody
laceAnalXical
H089
W­t'-Mew- OTIC11774 Wnf*nrdpr Name.- Julv Metals SAIR + Results Requestedl3y- 7/2612018
_.W_Nfw'Oc ad
I�dA
Angela Sajoni
Pace Analytical Charlotte P.O.'
9800 Kjpcey Ave. Suite 100
-fluntersville, NC 26078
Phone (7041j875-9092
Emil: angelg.bi3ionigpacelabs.com--"-
NC
ake of samole Origin,- ow -
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LAB USE ONLY
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Cooler Temgerature on ReceiptSeal
Y or N Receivedonlee Y or N
SamplesIntact Y or N
50dav
., JuLy 13,2018 2:55:16 PM
Page 4642'i

Pace Anal a National Center for
ReceiptCooler
Client:
i Innovation
N117 7
Cooler Received/Opened Can: 71 1't PIS
Lure:
Temperature:
Received By: C:hrysfian Lyle
Signature:
Receipt Check List
IMP
Yes
No
COC Seal Present f intact?
COC-Sighed / Accurate?
Bottles arrive intact?
Correct bottles used?
Sufficient volume sent?
VOA Zero headspace?
Peeser�tati�an:`�or- ectaf ., - -
Page 27 of 27'.

-acmnalXical
www.pacelabs.com
September 18, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: August Fecal
Pace Project No.: 92399358
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless othenlvise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 5

U)
CHAIN -OF -CUSTODY / Analytical Request Document o
�l GlCefil%aIICaI The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately. 0)
CC
n v.:s paC?�abs.cbttt
Section A Section B Section C Page: 1 of 1
Required Client Information: Required Project Information: Invoice Information:
Company: Veolla Water
Report To: Paul Spencer
Attention: Paul Spencer
e REGOLATRYAGENCY
r- NPDES I--' GROUND WATER F DRINKING WATER
i UST i RCRA X OTHER_IUP_
Address: 3200 20th Avenue SE
Copy To: Logan. Huohes cDyeolla
Company Name:
Newton, NC 26656
Address:
Email To: paul.sDencer(@veolia.com
Purchase CC on file
Order Na.; I
Pace Quote Reference:
1— GA r- IL F IN MI X NC
--
a fa i OH I SC WI I OTHER_
Filtered (YIN)
Phone: [phone]
F . 22/14656551
Project Name: August Fecal
Pace Project 6lanager. Angela Baioni
Roquestod std
Due DaterrAT'
Project Number.
Pace Profile :
Section D v,se rn's+`c°a"
Raquirod Mom lnformlodon r.1ATRnC CODE
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Analytical Results _ ISTATEMLLE
ANAL MAL
Pace Analytical C
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 09/13/2018
Reported: 09/14/2018
For:
Comments:
Sample Number Parameter Sample ID Result
180913-15-01 Fecal Coliforms Fecal <51.9
180913-15-01 Percent Solids Fecal 38.5
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Unit Method Analyzed Analyst
MPN/9 SM92210E-2006 09/13/2018 WC
SM2540B 2011 09/13/2018 WC
PO Box 228 m Statesville, NC 28687 a 704/872/4697
Page 1 of Oage 3 of 5

LJ
Condition of Receipt
Sample Number 180913-15-01 Temp on Arrival: 3.2
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 v Statesville, NC 28687 o 704/872/4697
Page 2 of kge 4 of 5

acaAnalytical
CHAIN -OF -CUSTODY / Analytical Request Document
The Chaln-OLCuatody is o LEGAL DOCUMENT All refevsnt hells must be compleled accumtely
Section A Section B Section C
Required client IMtxma;wn Required Pro)ecl htfurmalrcm 1m,Olce fnlonnation
Page; i of t
a•
comoarly Veofia Water
Repon To Paul Spencer
Attention Paul Spencer
AAdress. ZWO 2Mh Avenue. SE
COPY To L4gpn Fiufjll-,_ Z yeG'ta
- -- - -
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1laceAnalytical
www.pacelabs.com
September 27, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: June all metals - in September
Pace Project No.: 92399421
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Paul Spencer:
Enclosed are the analytical results for sample(s) received by the laboratory on September 13, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LA136RATORY ANALYSIS
�eORATO�
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
U
Project: June all metals - in September
Pace Project No.: 92399421
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
North Carolina Wastewater Certification M 12
Asheville Certification IDS
CERTIFICATIONS
South Carolina Certification M 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification M 99030001
Massachusetts Certification M M-NC030 Virginia/VELAP Certification M 460222
North Carolina Drinking Water Certification M 37712
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: June all metals - in September
Pace Project No.: 92399421
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample 10 Method
Analysts
Analytes
Reported
Laboratory
92399421001 June all metals EPA6010D
SH1
13
PASI-A
EPA 7471 B
SER
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271OB-2011
EWS
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
CJH1
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
CJH1
3
PASI-A
EPA 365.1 Rev 2.0 1993
BRJ
1
PASI-A
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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: June all metals - in September
Pace Project No.: 92399421
Sample: June all metals
Lab ID: 92399421001
Collected: 09/13/18 08:05
Received: 09/13/18 08:52 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601OD Preparation Method: EPA 3050B
Aluminum
3210
mg/kg
7.8
1
09/14/18 13:14
09/15/18 09:36
7429-90-5
Arsenic
ND
mg/kg
0.78
1
09/14/18 13:14
09/15/18 09:36
7440-38-2
Cadmium
0.27
mg/kg
0.078
1
09/14/18 13:14
09/15/18 09:36
7440-43-9
Calcium
2980
mg/kg
7.8
1
09/14/18 13:14
09/15/18 09:36
7440-70-2
Copper
77.4
mg/kg
0.39
1
09/14/18 13:14
09/15/18 09:36
7440-50-8
Lead
5.3
mg/kg
0.39
1
09/14/18 13:14
09/15/18 09:36
7439-92-1
Magnesium
588
mg/kg
7.8
1
09/14/18 13:14
09/15/18 09:36
7439-95-4
Molybdenum
1.8
mg/kg
0.39
1
09/14/18 13:14
09/15/18 09:36
7439-98-7
Nickel
6.7
mg/kg
0.39
1
09/14/18 13:14
09/15/18 09:36
7440-02-0
Potassium
785
mg/kg
391
1
09/14/18 13:14
09/15/18 09:36
7440-09-7
Selenium
1.1
mg/kg
0.78
1
09/14/18 13:14
09/15/18 09:36
7782-49-2
Sodium
ND
mg/kg
391
1
09/14/18 13:14
09/15/18 09:36
7440-23-5
Zinc
389
mg/kg
0.78
1
09/14/18 13:14
09/15/18 09:36
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
0.36 mg/kg 0.029
5 09/15/18 21:02
09/18/18 16:29 7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
;
Total Solids
34.8 % 0.000010
1
09/13/18 18:18
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
65.2 % 0.10
1
09/13/18 18:12
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
7.0 Std. Units 0.10
1
09/16/18 15:39 H6
Plant Available Nitrogen
Analytical Method: SM 271 OB-2011
Plant Available Nitrogen
3090 mg/kg 0.12
1
09/26/18 16:21 N2
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2IN03
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 09/27/2018 08:50 AM
9570 mg/kg 40.0 1 09/21/1815:55 7727-37-9
Analytical Method: EPA 350.1 Rev 2.01993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
985 mg/kg 78.1 10 09/22/1816:30 09/22/1817:45 7664-41-7 M6
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
9540 mg/kg 476 10 09/20/18 14:22 09/21/18 05:58 7727-37-9
Analytical Method: EPA 353.2 Rev 2.01993 Preparation Method: EPA 353.2 Rev 2.0 1993
27.8 mg/kg 2.0 1 09116/1812:03 09/16/1819:00
24A mg/kg 2.0 1 09/16/1812:03 09/16/1819:00 14797-55-8
3A mg/kg 0.99 1 09/16/1812:03 09/16/1819:00 14797-65-0
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: June all metals - in September
Pace Project No.: 92399421
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: June all metals Lab ID: 92399421001 Collected: 09113/18 08:05 Received: 09/13/18 08:52 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus 2190 mg/kg 94.3 50 09/17/18 23:51 09/20/18 02:30 7723-14-0
Date: 09/27/2018 08:50 AM
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 430846
Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471B
Analysis Description: 7471 Mercury
Associated Lab Samples: 92399421001
METHOD BLANK: 2376873
Matrix: Solid
Associated Lab Samples: 92399421001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0060
09/18/1815:32
LABORATORY CONTROL SAMPLE: 2376874
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
.083 0.089
107 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2376875 2376876
MS MSD
92399293005
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.025
.085 .088 0.13
0.13 121 121 75-125 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY, CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 430767 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Associated Lab Samples: 92399421001
METHOD BLANK: 2376416 Matrix: Solid
Associated Lab Samples: 92399421001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
10.0
09/15/18 08:48
Arsenic
mg/kg
ND
1.0
09/15/18 08:48
Cadmium
mg/kg
ND
0.10
09/15/18 08:48
Calcium
mg/kg
ND
10.0
09/15/18 08:48
Copper
mg/kg
ND
0.50
09/15/18 08:48
Lead
mg/kg
ND
0.50
09/15/18 08:48
Magnesium
mg/kg
ND
10.0
09/15/18 08:48
Molybdenum
mg/kg
ND
0.50
09/15/18 08:48
Nickel
mg/kg
ND
0.50
09/15/18 08:48
Potassium
mg/kg
ND
500
09/15/18 08:48
Selenium
mg/kg
ND
1.0
09/15/18 08:48
Sodium
mg/kg
ND
500
09/15/18 08:48
Zinc
mg/kg
ND
1.0
09/15/18 08:48
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2376417
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
500
482
96
80-120
Arsenic
mg/kg
50
45.8
92
80-120
Cadmium
mg/kg
50
45.9
92
80-120
Calcium
mg/kg
500
478
96
80-120
Copper
mg/kg
50
48.3
97
80-120
Lead
mg/kg
50
45.9
92
80-120
Magnesium
mg/kg
500
466
93
80-120
Molybdenum
mg/kg
50
49.4
99
80-120
Nickel
mg/kg
50
46.8
94
80-120
Potassium
mg/kg
500
ND
95
80-120
Selenium
mg/kg
50
43.7
87
80-120
Sodium
mg/kg
500
478J
96
80-120
Zinc
mg/kg
50
45.4
91
80-120
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2376593
2376594
MS
MSD
92399293005 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum mg/kg
40400 430
458
46700
43700
1450
720
75-125
6 M1
Arsenic mg/kg
4.5 43
45.8
31.5
34.9
63
66
75-125
10 M1
Cadmium mg/kg
0.071J 43
45.8
27.9
31.5
65
69
75-125
12 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/27/2018 08:50 AM without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
11
QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2376593
MS
92399293005 Spike
Parameter Units Result Cone.
MSD
Spike
Cone.
2376594
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
61.3
430
458
357
387
69
71
75-125
8 M1
Copper
mg/kg
29.8
43
45.8
66.5
72.5
85
93
75-125
9
Lead
mg/kg
12.5
43
45.8
37.6
45.1
58
71
75-125
18 M1
Magnesium
mg/kg
6120
430
458
8180
7920
479
394
75-125
3 MI1
Molybdenum
mg/kg
0.62
43
45.8
24.9
28.5
56
61
75-125
14 M1
Nickel
mg/kg
30.3
43
45.8
63.5
64.3
77
74
75-125
1 M1
Potassium
mg/kg
7000
430
458
11700
9130
1090
467
75-125
24 M1,R1
Selenium
mg/kg
ND
43
45.8
28.2
26.0
66
57
75-125
8 M1
Sodium
mg/kg
ND
430
458
364J
3911
70
72
75-125
M1
Zinc
mg/kg
110
43
45.8
158
158
111
103
75-125
0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/27/2018 08:50 AM without the written consent of Pace Analytical Services, LLC.
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Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 430694
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92399421001
SAMPLE DUPLICATE: 2376238
Parameter Units
Percent Moisture
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
92399301001 Dup
Result Result RPD Qualifiers
73.2 72.6 1
SAMPLE DUPLICATE: 2376239
92399421001 Dup
Parameter Units Result Result
Percent Moisture % 65.2 62.4
RPD Qualifiers
4
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 09/27/2018 08:50 AM without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 430907 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92399421001
SAMPLE DUPLICATE: 2377025
92398932001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.4 8.3 1 H6
SAMPLE DUPLICATE: 2377026
92399425003 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.9 8.8 2 D6,H6
r"
i.
Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 432155 Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod. Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92399421001
METHOD BLANK: 2382409 .
Associated Lab Samples: 92399421001
Parameter Units
Nitrogen, Ammonia mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 09/22/1817:20
Pace Analytical Services, LLC
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LABORATORY CONTROL SAMPLE: 2382410
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 500 516 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2382411 2382412
MS MSD
92399421001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 985 1140 1140 3080 3180 22 31 90-110 3 M6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 431660
Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Associated Lab Samples: 92399421001
METHOD BLANK: 2380005
Matrix: Solid
Associated Lab Samples: 92399421001
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
ND 41.7
09/21/18 05:48
LABORATORY CONTROL SAMPLE: 2380006
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/kg
1000 990
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2380007 2380008
MS MSD
92399549001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 33700
3790 3790 39000
38200 138 118 90-110 2 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
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QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 430901
Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Associated Lab Samples: 92399421001
METHOD BLANK: 2376999
Matrix: Solid
Associated Lab Samples: 92399421001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/kg
ND 2.0
09/16/18 18:42
Nitrogen, Nitrite
mg/kg
ND 0.99
09/16/18 18:42
Nitrogen, NO2 plus NO3
mg/kg
ND 2.0
09/16/18 18:42
LABORATORY CONTROL SAMPLE: 2377000
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/kg
15 15.1
101 90-110
Nitrogen, Nitrite
mg/kg
10 10.4
104 90-110
Nitrogen, NO2 plus NO3
mg/kg
25 25.5
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2377001 2377002
MS MSD
92398932001
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units
Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qua[
Nitrogen, Nitrate mg/kg
ND
54 53.6 43.9
40.6 81 76
90-110 8
Nitrogen, Nitrite mg/kg
ND
36.2 35.9 17.1
15.5 39 35
90-110 10
Nitrogen, NO2 plus NO3 mg/kg
ND
90.2 89.5 61.0
56.1 65 60
90-110 8
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: June all metals - in September
Pace Project No.: 92399421
QC Batch: 431057 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92399421001
METHOD BLANK: 2377478
Matrix: Solid
Associated Lab Samples: 92399421001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/kg
ND 2.0
09/20/18 01:48
LABORATORY CONTROL SAMPLE:
2377479
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/kg
50
54.5
109 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2377480
2377481
MS
MSD
92398932001
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus
mg/kg 29100
165
159 21700
17300 -4500 -7470 90-110 23 M6,R1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
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(,QUALIFIERS
Project: June all metals - in September
Pace Project No.: 92399421
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up .
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
Date: 09/27/2018 08:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 19

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Icncey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: June all metals - in September
Pace Project No.: 92399421
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92399421001
June all metals
EPA 3050B
430767
EPA 601 OD
430843
92399421001
June all metals
EPA 7471 B
430846
EPA 7471 B
431140
92399421001
June all metals
SM 2540G-2011
430792
92399421001
June all metals
ASTM D2974-87
430694
92399421001
June all metals
EPA 9045D
430907
92399421001
June all metals
SM 271OB-2011
432867
92399421001
June all metals
TKN+NO3+NO2
432036
Calculation
92399421001
June all metals
EPA 350.1 Rev 2.0 1993
432155
EPA 350.1 Rev 2.0 1993
432156
Mod.
Mad.
92399421001
June all metals
EPA 351.2 Rev 2.0 1993
431660
EPA 351.2 Rev 2.0 1993
43.1871
92399421001
June all metals
EPA 353.2 Rev 2.0 1993
430901
EPA 353.2 Rev 2.0 1993
430912
92399421001
June all metals
EPA 365.1 Rev 2.0 1993
431057
EPA 365.1 Rev 2.0 1993
431071
Date: 09/27/2018 08:50 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 19 �_

.1101
Document Name:
Document Revised: February 7, 2018
d
ace Analytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
l
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [ Ralelgh❑ MechanicsvilleQ
ConditionSample Client Name: + �� U "39942 ,
• Project #+:
•�G� Ili '
❑ tCourier: -]Fed Ex []UPS ❑Clen
Commercial Pe ❑Other:
92399421
(-'--
Custody Seal Present? Dyes ®No Seals Intact? []Yes EJho Cn / �
Date/Initlols Person Examining Contents:1 l 1
Packing Material: []Bubble Wrap ElBubbie Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: []Yes E]No ❑N/A
RR Gun ID: 92T0¢5 Type of Ice: wet ❑Blue ❑None
Cooler Temp (°C): Z,0 Correction Factor: Add/Subtract (°C) -0.1
Cooler Temp Corrected ('CI: ''i Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Soll (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source iinternationally,
FlYes PNo inrlurldna Hawaii and P—rfn Al-17 MVoc i- and
Comments/Discrepancy:
Chain of Custody Present?
)i]'Fes
[]NO
❑N/A
1.
Samples Arrived within Hold Time?
E fives
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
QYes
ffNo
❑N/A
4.
Sufficient Volume?
OVes
ONO
❑N/A
S.
Correct Containers Used?
Pace Containers Used?
Mies
(2res
[:]No
[]No
❑N/A
❑N/A
6.
Containers Intact?
®Yes
[]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
la /A
a.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
)B-Yes
[]No
[]N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
BTA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
[]Yes__
C—No
ONo
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
'}}8
Date/Time:
Field Data Required? []Yes ❑No
Date:t�
Date:
Page 17 of 19

Document Name:
Document Revised: February 7, 2018
a
�Ace
Sample Condition Upon Recel t(SCUR)
Pagel of 2
Analyi`ical
Document No.:
Issuing Authority:
r
f•CAR•CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coiiform, MC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # j WOW 9239 4221' .
i PM: 'AMB" .' ' : Due° Plate,:• 09/27/18
1' CLIENT: 92=VeaIia.Wa
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy or this corm will uesent ru Lilt:] -Oiur LaM, ,a „� ...
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 18 of 19

r
CHAIN -OF -CUSTODY / Analytical Request Document
aceAnalytical The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
,� Ivr.spaxrabs corn
Section A
Section B
Section C
Required Client Information:
Required Project Information:
Invoice Information:
Company: Veolia Water
Report To: Paul Spencer
Attention:
Paul Spencer
Address: 3200201hAvenue SE
Copy To: Lo41n.Hu q heS
p veoIia
Company Name:
Newton, NC 28658
Address:
Email To; paul.SDencef4Ey? LO1I@.g0M
Purchase CC on file
Pace Quote Reference;
Ortlor No,:
Phone: [phone]
Pex: 8284656551
Project Name: June all metals
Paco Project Manager.
Angela Baioni
Requested stCl
'Duo DatorrAT.
ProjeclNumber,
Pace Profile #:
Section D VoLd Matrix cod-.
Roquimd Client informnuon MATRIX CODE
d
COLLECTED
¢
P,
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wain
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COMPOSITE
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SAMPLE
SAMPLE ID cr.,ryq,o
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START
ENDIGRAa
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Sample IDS MUST BE UNIQUE of
m
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y
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it
DATE
TIME
DATE
TIME
j
=
Nitrate, Metals
SL
C
9/13118
B:OOAM
9/13118
8:05AM
,1
1
Solids
SL
C
9113/16
B:OOAM
9113/18
8:05AM
1
+f+
Ni,K,Se,Na,Zn,Hg,
we-,
of
8 f 8.' gz
Page: 1 of 1 1
i NPDES r GROUND WATER i DRINKING WATER
i UST (— RCRA IX OTHER—IUP—
SITE
GA I—' IL F 1N F MI X NC
LOCATION r OH r Sc i— WI F OTHER
Itered (YIN)
�\V
Paco Project Nt
Lab 1.0
X) 1
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• ' SAMPLE CONDITIONS
9/13/18J�
Z Z
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C m U
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Signed m C] m E
cDrvrj: 9/13/18 _ rmn cn
e-File(ALLQ020rev.4,29Mar06)22Jun2005
rn
0
N
07
f0
ll

Bi - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of September and October 201.S.The August Fecal and Metal results were
conducted on September l3a' of 2018. This shows compliance with Alternative A5 of 40 CFR Part 503.32,
40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
)Pathogen Reduction Reguiirements - Alternative A5 ()�'I RPi
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 67.85 deg.0 for 3.45 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN KILL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — NA Dry Weight Basis. Fecal Coliform Results - <36
MPN/ — (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Under* ed,
Paul Spencer
Vector Attraction Deduction - OiDtion 5
TIME &s TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 65.1deg. C for approximately 24.2 days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Undersigned.
Paul Spencer
PFRP Cer ifleation Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Unders' ed,
Paul Spencer
Project Manager
Veolia Water North America
Regional Compost Facility
3200 20th Ave., SE
Date Signned: Q

Newton NC 28658
(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.

4,,PkeAnalXical
ww .pacelabs.com
October 15, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: October Fecal
Pace Project No.: 92402745
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 09, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNIINELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia water North America
REPORT OF LABORATORY ANALYSOS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 5

Mr
Analytica� Results STATE- 8V LE
ANALYMAL
Pace Analytical ;..._:
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 10/09/2018
Reported: 10/12/2018
For: Veolia Water
Comments:
Sample Number
Parameter
Sample ID
Result
Unit Method
Analyzed
Analyst
181009-30-01
Fecal Coliforms
Fecal
<36
MPN/g SM92210E-2006
10/09/2018
WC
181009-30-01
Percent Solids
Fecal
55
% SM25408-2011
10/09/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 o 704/872/4697
Page 1 of Page 3 of 5

Chain of Custody
Workorder. 92402746
MA na4dical
rvww.paiaelabscanr
Workorder Name: October Fecal
Results Requested By' 10/23/2018
Re ' ark`f7nvoice'•To'`:
- - > •-• • _
,� �
,"Re"�ue`sYeil,Anal sisa;•:�;�
�r*�=�.':`:'�:'^
.,:,.,r:=�':c•:
Angela Baioni
Pace Analytical Charlotte
C}t1 P.O.
9800 Kincey Ave. Suite 100
Wunters'ville, NC 28078
Phone [phone]
Email: angela.baioni@pacelab
s.com
v
u
State of Sample Origin: N
v
Preserved:Coritainei;,.�;.:
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LAB USE ONLY
1
Feral
10/9/2018.08:05
'92402745001
Solid
t
X
2
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`
Transfers
Released By
Date/Time
Received By
DatefTime
1
2
j
3
.Co(ilerTemperatureqnRiceipt
°C Custod Seal Y or N I Received on Ice Y or N Samples Inftact Y or H
Wednesday, October 10, 2018 2:{19:18 PM FMT-ALL-C-002rev.00 24N arc=09 Page 1 of 1
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1_-AaueAna1yAca10
1 www.pacelabs.com
October 19, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: October All Metals
Pace Project No.: 92402226
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

R
� sacmnalj&al"
www.pacelabs.com
CERTIFICATIONS
Project: October All Metals
Pace Project No.: 92402226
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342 VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19

aceAnal ical
www.pas.com
SAMPLE ANALYTE COUNT
Project: October All Metals
Pace Project No.: 92402226
Pace Analytical Services, LLC
9800 iGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92402226001 Comp EPA 6010D
DS
13
PASI-A
EPA 7471B
JMW7
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA9045D
ECH
1
PASI-A
SM 271OB-2011
DMN
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
DMN
3
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 19

�acmnalXicalo
www.#acelabs.com
ANALYTICAL RESULTS
Project: October All Metals
Pace Project No.: 92402226
Pace Analytical Services, LLC
9800 Kinoey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Comp
Lab ID: 92402226001 Collected:
10/04/18 08:05
Received: 10/04/1814:25 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Aluminum
2660
mg/kg
7.0
1
10/08/1811:23
10/09/1816:30
7429-90-5
Arsenic
ND
mg/kg
0.70
1
10/08/1811:23
10/09/1816:30
7440-38-2
Cadmium
0.22
mg/kg
0.070
1
10/08/1811:23
10/09/1816:30
7440-43-9
Calcium
3040
mg/kg
7.0
1
10/08/1811:23
10/09/1816:30
7440-70-2
Copper
60.1
mg/kg
0.35
1
10/08/1811:23
10/09/1816:30
7440-50-8
Lead
4.3
mg/kg
0.36
1
10/08/1811:23
10/09/1816:30
7439-92-1
Magnesium
512
mg/kg
7.0
1
10/08/1811:23
10/09/1816:30
7439-95-4
Molybdenum
1.3
mg/kg
0.35
1
10108/1811:23
10/09/1816:30
7439-98-7
Nickel
4.1
mg/kg
0.35
1
10/0811811:23
10109/1816:30
7440-02-0
Potassium
620
mg/kg
352
1
10108/1811:23
10/09/1816:30
7440-09-7
Selenium
ND
mg/kg
0.70
1
10/08/1811:23
10/0911816:30
7782-49-2
Sodium
ND
mg/kg
352
1
10/08/1811:23
10/09/1816:30
7440-23-5
Zinc
302_
mg/kg
0.70
1
10/08/1811:23
10/09/1816:30
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
0.15
mg/kg
0.012
2
10/06/18 20:34
10/09/18 11:12
7439-97-6
254OG Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
39.0
% 0.000010
1
10/04/18 17:54
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
60.9
%
0.10
1
10/04/18 17:48
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 10/19/2018 03:30 PM
Analytical Method: EPA 9045D
7.6 Std. Units 0.10
1
10/05/18 13:19 H6
Analytical Method: SM 271 OB-2011
1860 mg/kg 0.12
1
10/19/1815:27 N2
Analytical Method: TKN+NO3+NO2 Calculation
8950 mg/kg 40.0
1
10/10/1814:49 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
2410 mg/kg 102.
10
10/1611814:29 10/17/1814:53 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
8960 mg/kg 455
10
10/09/18 09:57 10/10/18 00:18 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
2.9 mg/kg 2.0
1
10/08/1817:20 10/09/1811:42
ND mg/kg 2.0
1
10/0811817:20 10/0911811:42 14797-55-8
5.2 mg/kg 0.98
1
10/08/1817:20 10/0911811:42 14797-65-0
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: October All Metals
Pace Project No.: 92402226
Pace Analytical Services, LLC
9800 MnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Comp Lab ID: 92402226001 Collected: 10/04/18 08:05 Received: 10/04/18 14:25 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus - 3060 mg/kg 192 100 10/05/18 21:34 10/06/18 00:09 7723-14-0
Date: 10/19/2018 03:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

(�IaceAnalytical
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Project: October All Metals
Pace Project No.: 92402226
QC Batch: 434887
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92402226001
METHOD BLANK: 2394436
Associated Lab Samples: 92402226001
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 0.0060 10/09/18 09:41
Qualifiers
U
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)87&9092
LABORATORY CONTROL SAMPLE: 2394437
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.075 90 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2394438 2394439
MS MSD
92401660001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.15 .31 .3 1.1 0.93 293 258 75-125 13 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19

II
ceAnalytical
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QUALITY CONTROL DATA
Project: October All Metals
Pace Project No.: 92402226
QC Batch: 434941 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92402226001
METHOD BLANK: 2394537
Associated Lab Samples: 92402226001
Parameter
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed Qualifiers
Aluminum
mg/kg
ND
10.0
10/09/1816:12
Arsenic
mg/kg
ND
1.0
10/09/1816:12
Cadmium
mg/kg
ND
0.10
10/09/1816:12
Calcium
mg/kg
ND
10.0
10/09/1816:12
Copper
mg/kg
ND
0.50
10/09/1816:12
Lead
mg/kg
ND
0.50
10/09/1816:12
Magnesium
mg/kg
ND
10.0
10/0911816:12
Molybdenum
mg/kg
ND
0.50
10/09/1816:12
Nickel
mg/kg
ND
0.50
10/0911816:12
Potassium
mg/kg
ND
500
10/09/1816:12
Selenium
mg/kg
ND
1.0
10/09/1816:12
Sodium
mg/kg
ND
500
10/09/1816:12
Zinc
mg/kg
ND
1.0
10/0911816:12
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
® Parameter
2394538
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
481
475
99
80-120
Arsenic
mg/kg
48.1
45.6
95
80-120
Cadmium
mg/kg
48.1
46.2
96
80-120
Calcium
mg/kg
481
473
98
80-120
Copper
mg/kg
48.1
48.2
100
80-120
Lead
mg/kg
48.1
45.8
95
80-120
Magnesium
mg/kg
481
458
95
80-120
Molybdenum
mg/kg
48.1
49.3
103
80-120
Nickel
mg/kg
48.1
46.5
97
80-120
Potassium
mg/kg
481
ND
98
80-120
Selenium
mg/kg
48.1
44.4
92
80-120
Sodium
mg/kg
481
477J
99
80-120
Zinc
mg/kg
48.1
45.2
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2394539
2394540
MS
MSD
92401901001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qua]
Aluminum mg/kg
10700
9530
9910
21800
22200
117
117
75-125 2
Arsenic mg/kg
ND
953
991
892
930
93
94
75-125 4
Cadmium mg/kg
ND
953
991
894
935
94
94
75-125 4
Results presented on this page are In
the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 19

U
acmnalytical
www.pacetabs.com
QUALITY CONTROL DATA
Project: October All Metals
Pace Project No.: 92402226
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2394539
MS
92401901001
Spike
Parameter
Units
Result
Conc.
Calcium
mg/kg
121000
9530
Copper
mg/kg
252
953
Lead
mg/kg
24.0
953
Magnesium
mg/kg
5060
9530
Molybdenum
mg/kg
ND
953
Nickel
mg/kg
10.7
953
Potassium
mg/kg
ND
9530
Selenium
mg/kg
ND
953
Sodium
mg/kg
ND
9530
Zinc
mg/kg
810
953
Pace Analytical Services; LLC
9800 IGncey Ave. Suite 100
Huntersville, NC 28078
[phone]
2394540
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
9910
129000
129000
88
83
75-125
0
991
1200
1240
99
100
75-125
3
991
894
930
91
91
75-125
4
9910
14000
14400
94
94
75-125
2
091
948
991
99
100
75-125
4
991
893
931
93
93
75-125
4
9910
13200
13500
99
99
75-125
3
991
842
877
88
88
75-125
4
9910
11300
11700
96
97
75-125
4
991
1650
1680
88
88
75-125
2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 8 of 19

°acmnalyiical
www.pacelabs.com
t
QUALITY CONTROL DATA
Project: October All Metals
Pace Project No.: 92402226
QC Batch: 434451 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92402226001
SAMPLE DUPLICATE: 2392451
92402083001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Percent Moisture
%
23.6
23.5 1
SAMPLE DUPLICATE: 2392924
92402201001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Percent Moisture
%
17.3
18.0 4
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19

W
aceAnalyticai
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Project: October All Metals
Pace Project No.: 92402226
QC Batch: 434620
QC Batch Method: EPA 9045D
Associated Lab Samples: 92402226001
SAMPLE DUPLICATE: 2393164
Parameter Units
pH at 25 Degrees C Sid. Units
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92401650001 Dup
Result Result RPD Qualifiers
7.8 7.8 0 H6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

�PaceAnalXical
www.pacelabs.com
i
t
Project: October All Metals
Pace Project No.: 92402226
QC Batch: 436438
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92402226001
METHOD BLANK: 2401307
Associated Lab Samples: 92402226001
Parameter Units
Nitrogen, Ammonia mg/kg
LABORATORY CONTROL SAMPLE: 2401308
Parameter Units
Nitrogen, Ammonia mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 9.1 10/17/18 13:51
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
472 509 108 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2401309 2401310
MS MSD
92399753001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/kg 165 431 481 653 684 113 108 90-110 5 H1,M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

u
�aceAnalX cal
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Project: October All Metals
Pace Project No.: 92402226
QC Batch: 435126
QC Batch Method: EPA 351.2 Rev 2.0 1993
Associated Lab Samples: 92402226001
METHOD BLANK: 2395326
Associated Lab Samples: 92402226001
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
LABORATORY CONTROL SAMPLE: 2395327
Parameter Units
Nitrogen, Kjeldahl, Total mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 351.2 Rev 2.0 1993
Analysis Description: 351.2 TKN
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 10/09/18 23:53
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
769 726 94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2395328 2395329
MS MSD
92402339001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Kjeldahl, Total mglkg 437 1170 1170 444 510 1 6 90-110 14 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 19

11
��a-'ceAnalXicalo
wv=pacelabs.com
Project: October All Metals
Pace Project No.: 92402226
QC Batch: 435003
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92402226001
METHOD BLANK: 2394847
Associated Lab Samples: 92402226001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description. 353.2 Nitrate + Nitrite
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 10/09/1811:28
ND 1.0 10/0911811:28
ND 2.0 10109/1811:28
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2394848
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 15.2 101 90-110
Nitrogen, Nitrite mg/kg 10 10.2 102 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 25.4 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2394849
2394850
MS
MSD
92402339001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
18.8
18.9
10.0
10.5
54
56
90-110
5
Nitrogen, Nitrite
mg/kg
5.4
12.5
12.6
8.7
6.9
27
12
90-110
24 M1,R1
Nitrogen, NO2 plus NO3
mg/kg
5.2
31.3
31.6
18.8
17.4
43
39
90-110
8 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/19/2018 03:30 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

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awAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: October All Metals
Pace Project No.: 92402226
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92402226001
Comp
EPA 3050E
434941
EPA 601OD
435067
92402226001
Comp
EPA 7471E
434887
EPA 7471B
434897
92402226001
Comp
SM 254OG-2011
434973
92402226001
Comp
ASTM D2974-87
434451
92402226001
Comp
EPA 9045D
434620
92402226001
Comp
SM 271OB-2011
437018
92402226001
Comp
TKN+NO3+NO2
435490
Calculation
92402226001
Comp
EPA 350.1 Rev 2.0 1993
436438
EPA 350.1 Rev 2.0 1993
436462
Mod.
Mod.
92402226001
Comp
EPA 351.2 Rev 2.0 1993
435126
EPA 351.2 Rev 2.0 1993
435316
92402226001
Comp
EPA 353.2 Rev 2.0 1993
435003
EPA 353.2 Rev 2.0 1993
435069
92402226001
Comp
EPA 365.1 Rev 2.0 1993
434753
EPA 365.1 Rev 2.0 1993
434793
Date: 10/19/2018 03:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 19

a
Document Name: Document Revised: February7, 2018
g Sample Condition Upon Receipt(SCUR) Page 1 of 2
ceARc?&tal Document No.: Issuing Authority:
F•CAR-CS-033•Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvllle Raleigh❑ Mechanicsville❑
ConditionSaniplL
Client Name: O� �' �� ,.
Upon Receipt�f Project
V � �7� rr�. UIJJ -�tj
Courier: ❑F d Ex ❑UPS ❑ ❑Client i �I �I
❑ Commercial v Pace , []Other: / 92402226
Custody Seal Present? ❑Yes [DNo Seals intact?0 ❑Yes ❑NQ
Date/Initials Person Examining Contents:— �
Packing Material: ❑Bubble Wrap ,08ubble Bags ❑Non % ❑ Other
Thermometer. 92T045 Type of Ice: -(wet []Blue
'QIR Gun ID:
Cooler Temp (°C): Correction Factor: Add/Subtract (°C)
Cooler Temp Corrected ('`C): '
f
USDA Regulated Soil N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Biological Tissue Pozen?
❑Yes ❑No
❑None
Temp should be above freezing to 6'C
[-]Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
U--ii god pnorto Rirnl? MYes ❑NO
❑Yes ❑No
Comments/Olscrepancy:
I.
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)?
//
i❑Yes []No
l Yes []No
❑Yes EA
[]N/A
❑N/A
❑N/A
2.
3.
4.
Rush Turn Around Time Requested? Dyes Z No ❑NIA
Sufficient Volume? �fYes ❑No
Correct Containers Used? Yes No
-Pace Containers Used? 13Yes ❑No
Containers Intact? Yes ON.
Dissolved analysis: Samples Field Filtered? ❑yes []No
Sample Labels Match COC? Yes ON.
{
rAq-Includes
❑N/A
❑N/A
[]N/A
❑N/A
❑NIA
❑N/A
5.
6.
7.
B.
9.
Date/Time/ID/Analysis
Neadspace in VOA Vials (>5-6mm)?
.Trip Blank Present?
Trip Blank Custody Seals Present?
Matrix:
[]Yes []No._L\ N A
[]yes ❑No Q /A
❑Yas [:]No N/A
10.
11.
Field Data Required? UYes No
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Q�i Date:
Project Manager SRF Review:
Date:
Page 17 of 19

W
Document Name:
Sample Condition Upon Recell
Analytical' Document No::
F•CAR•CS•033•Rev.06
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease„DRO/@015 (water) DOC, LLHS
**Bottom half of box Is to list number of bottle
Document Revised: February 7, 2018
Page 1 of 2
issuing Authority:
Carolinas Quality Office
Project t# I W0 19 ;402226
( PM: AMB, Due Date: 10/18/18
CLIENT: 92-Veo,r 1a. IJa .
I
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4
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6
7
8
9
10
11
12
PH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount added DfPreservauve Lot �i
adjusted
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, in preservative, out of temp, incorrect containers.
Page 18 of 19

/ = aceAnalyical "
CHAIN -OF -CUSTODY I Analyfta6 Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
o)
0
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a>
m
D_
Section A
Required Client Information:
Section B Section C Page: 1 of 1
Required Project Information: Invoice Information:
Report To: Paul Spencer Attention: Paul Spencer . • kY AGENCY
I Copy To: Looan.Hughes(cDveolia Company Name: r NPDES r GROUND WATER r DRINKING WATER
Address: f US7 r RCRA 5C OTHER_(UP_
Purchase CC On file Pace Quote Reference: r GA r IL r IN r -MIX t
Order No,: SITE
Project Name: October all metals Pace Project Manager, Angela Baioni LOCATION f OH r SC r WI r OTHER
k Project Number: Pace Profile #: Filtered YIN
j _/7777777777///
Company: Veolia Water
Address: 3200 201h Avenue SE
Newton, NC 28658
Email To: _Daul.spencer(cDyeolia.com
Phone: [phone]
Fax: [phone]
Requested std
Duo Data/TAT:
Section D V.Dd MnbU Codas
Required Cfi nt Information ''-'"n"n • i cooE
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DATE
TIME
DATE
TIME
Nitrate, Metals
SL
C
1014118
8:00AM
1014118
1 8:05AM
1
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X
X
X
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Solids !
'SL
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1014118
8:00AM
10/4118
8:05AM
1
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ADDITIONALCOMMENTS
metals:
AI,As,Ca,Cd,Cu,Pb,Mg,Mo,Ni,K,Se,Na,Zn,H
91
RELINQUISHED BY •
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10/4/18
/ BY I AFFILIAT I"ONDATE
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1014/18
tiME,SAMPLE
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PRINT Name of SAMPLER:
Lo an Hu hes
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SIGNATURE of SAMPLER: f
DATE Signed
(MMIDDIYY): 10/4/18
U
e-File (AL LQ 020rev.4, 29Mar06)22Jun2005

Bi - MONTHLY CERTIFICATION STATEMENTS
The Regional Compost Facility is a "Process to Further Reduce Pathogens" (PFRP) system for
treatment of and beneficial use of dewatered biosolids. This section states that VWNAOS and the
Consortium have utilized Class A Pathogen Reduction using Alternative A5 - PFRP via Composting to
display compliance with 40 CFR Part 503.32 (a)(7) and in continuity with 40 CFR Part 503.33(b)(5).
Based upon site specific monitoring and operation data of the biosolids VWNAOS submits the following
information for the months of November and Dececnberber 2018. This shows compliance with
Alternative A5 of 40 CFR Part 503.32, 40 CFR Part 503.32(a)(7), and 40 CFR Part 503.33(b)(5).
Pathogen Reduction Rea ui>remrnents - Alternative A5 (P1FRP
TIME & TEMPERATURE - 40 CFR Part 503.32 Minimum - 55 deg. for 3 consecutive days.
Regional Compost Facility — 64.25 deg.0 for 7.66 consecutive days. (Please See Operation Summary
Report page 9).
PATHOGEN )KILLL - 40 CFR Part 503.32(a)(7) — Fecal Limit 1000 (MPN/g) .
Regional Compost Facility Salmonella — I+iA Dry Weight Basis. Fecal Colifonn Results - 697
MPN/ (Please See Report of Analysis for lab data).
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A pathogen requirements in 40 CFR Part
503.32(a)(7) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Under ' ed,
Paul Spencer
Vector Attraction Deduction - Option 5
TIME & TEMPERATURE - 40 CFR Part 503.33(b)(5) Minimum - 14 days above 40 deg. C and the
average temperature at or above 45 deg. C.
Regional Compost Facility - 61.6 deg. C for approximately 53.65 days. (Please see Operation Summary
Report, page 8)
CERTIFICATION STATEMENT - `I certify under penalty of law, that the Class A Vector Attraction requirements in 40 CFR Part
503.33(b)(5) have been met. This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment. "
Undersi ed.
Z�
9-x �
Paul Spencer
PF" Certification Statement
"I certify under penalty of law that this document and all attachments were prepared under my direction and supervision in
accordance with the system designed that qualified personnel properly gather and evaluate the information submitted. Based upon my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the available information
the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties
for submitting false information, including the possibility of fine and imprisonment for knowing violation."
Undersigned,
A� C'�
Paul Spencer
Project Manager
Veolia Water North America
Regional Compost Facility
3200 20th Ave., SE
Newton NC 28658
Date Signed: /

V
(828) 465 - 1401
Took average PFRP for January and February. Also got average ACSRT for both months and divided by
14. Use VAR. average for both months and ACSRT. Average for both months.

�aceAnalytical
www.pacelabs.com
November 21, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: November All Metals
Pace Project No.: 92406666
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

aceAnalytical
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Project: November All Metals
Pace Project No.: 92406666
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19

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aceAnalX cal
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SAMPLE ANALYTE COUNT
Project: November All Metals
Pace Project No.: 92406666
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytts
Reported
Laboratory
92406666001 nitrate, Metals, Solids EPA 601 OD
IDS
13
PAST -A
EPA 7471B
JMW1
1
PASI-A
SM 254OG-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
SM 271OB-2011
EWS
1
PASI-A
TKN+NO3+NO2 Calculation
EWS
1
PASI-A
EPA 350.1 Rev 2.0 1993 Mod.
NAL
1
PASI-A
EPA 351.2 Rev 2.0 1993
DMN
1
PASI-A
EPA 353.2 Rev 2.0 1993
DMN
3
PASI-A
EPA 365.1 Rev 2.0 1993
GC
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

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ANALYTICAL RESULTS
Project: NovemberAll Metals
Pace Project No.: 92406666
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: nitrate, Metals, Solids
Lab ID: 92406666001
Collected: 11/08/18 08:05
Received: 11/08/18 13:20 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3050B
Aluminum
2610
mg/kg
8.2
1
11/09/18 12:22
11/10/18 04:12
7429-90-5
Arsenic
ND
mg/kg
0.82
1
11/09/18 12:22
11/10/18 04:12
7440-38-2
Cadmium
0.15
mglkg
0.082
1
11/09/18 12:22
11/10/18 04:12
7440-43-9
Calcium
3360
mg/kg
8.2
1
11/09/18 12:22
11/10/18 04:12
7440-70-2
Copper
41.0
mg/kg
0.41
1
11/09/18 12:22
11/10/18 04:12
7440-50-8
Lead
3.1
mg/kg
0.41
1
11/09/18 12:22
11/10/18 04:12
7439-92-1
Magnesium
479
mg/kg
8.2
1
11/09/18 12:22
11/10/18 04:12
7439-95-4
Molybdenum
0.71
mg/kg
0.41
1
11/09/18 12:22
11/10/18 04:12
7439-98-7
Nickel
3.1
mg/kg
0.41
1
11/09/18 12:22
11/10/18 04:12
7440-02-0
Potassium
448
mg/kg
410
1
11/09/18 12:22
11/10/18 04:12
7440-09-7
Selenium
ND
mg/kg
0.82
1
11/09/18 12:22
11/10/18 04:12
7782-49-2
Sodium
ND
mg/kg
410
1
11/09/18 12:22
11/10/18 04:12
7440-23-5
Zinc
249
mg/kg
0.82
1
11/09/18 12:22
11/10/18 04:12
7440-66-6
7471 Mercury
Mercury
254OG Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
9045 pH Soil
pH at 25 Degrees C
Plant Available Nitrogen
Plant Available Nitrogen
Total Nitrogen Calculation
Nitrogen
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, N021NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Date: 11/21/2018 04:37 PM
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
0.060 mg/kg 0.0044 1 11/19/1816:55
11/20/18 12 :01 7439-97-6 M1,R1
Analytical Method: SM 254OG-2011
44.2 % 0.000010 1
11/09/1814:28
Analytical Method: ASTM D2974-87
55.8 % 0.10 1
11109/1814:20
Analytical Method: EPA 9045D
7.6 Std. Units 0.10 1
11/12/18 12:16 H3
Analytical Method: SM 271OB-2011
2210 mg/kg 0.12 1
11/20/1814:44 N2
Analytical Method: TKN+NO3+NO2 Calculation
6850 mg/kg 40.0 1
11/19/18 09:54 7727-37-9
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method:
EPA 350.1 Rev 2.0 1993 Mod.
763 mg/kg 10.0 1 11/14/1817:40
11/15/1816:35 7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
6850 mg/kg 250 5 11/14/18 01:17
11/14/18 13:38 7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
4.7 mg/kg 2.0 1 11/09/18 02:38
11/09/18 13:16
ND mg/kg 2.0 1 11/09/18 02:38
11/09/18 13:16 14797-55-8
3.8 mg/kg 0.99 1 11/09/18 02:38
11/09/18 13:16 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

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ANALYTICAL RESULTS
Project: November All Metals
Pace Project No.: 92406666
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: nitrate, Metals, Solids Lab ID: 92406666001 Collected: 11/08/18 08:05 Received: 11/08/18 13:20 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus 2170 mg/kg 92.6 50 11/12/18 20:01 11/13/18 23:01 7723-14-0
Date: 11/21/2018 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

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I
QUALITY CONTROL DATA
Project: NovemberAll Metals
Pace Project No.: 92406666
QC Batch: 443240 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92406666001
METHOD BLANK: 2432218
Associated Lab Samples: 92406666001
Matrix: Solid
Blank Reporting
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter
Units
Result
Limit
Analyzed Qualifiers
Mercury
mg/kg
ND 0.0060
11/20/1811:56
LABORATORY CONTROL SAMPLE:
2432219
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Mercury
mg/kg
.083
0.085
102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2432220
2432221
MS
MSD
92406666001
Spike
Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc.
Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury
mg/kg 0.060
.13
.14 0.19
0.13 44 -6 75-125 40 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2018 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19

)V-7
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QUALITY CONTROL DATA
Project: November All Metals
Pace Project No.: 92406666
QC Batch: 441349 Analysis Method: EPA 6010D
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Associated Lab Samples: 92406666001
METHOD BLANK: 2423629
Associated Lab Samples: 92406666001
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
LABORATORY CONTROL SAMPLE:
2423630
Parameter
Units
Aluminum
mg/kg
Arsenic
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Copper
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result
Spike
Conc.
490
49
49
490
49
49
490
49
49
490
49
490
49
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Reporting
Limit Analyzed
Qualifiers
9.8
11/10/18 02:31
0.98
11/10/18 02:31
0.098
11/10/18 02:31
9.8
11/10/18 20:19
0.49
11/10/18 02:31
0.49
11/10/18 02:31
9.8
11/10/18 02:31
0.49
11/10/18 02:31
0.49
11/10/18 02:31
490
11/10/18 02:31
0.98
11/10/18 02:31
490
11/10/18 02:31
0.98
11/10/18 02:31
LCS
Result
467
46.1
45.7
474
48.0
46.1
461
50.0
46.7
ND
43.9
468J
46.5
LCS
% Rec
95
94
93
97
98
94
94
102
95
94
90
96
95
% Rec
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2423631
2423632
MS
MSD
92406465008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
Aluminum mg/kg
511
481
490
1120
1130
127
126
75-125 1 M1
Arsenic mg/kg
ND
48.1
49
45.5
46.2
94
94
75-125 1
Cadmium mg/kg
ND
48.1
49
45.0
45.9
94
94
75-125 2
Results presented on this page are In
the units indicated by the
"Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

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qC1
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1
QUALITY CONTROL DATA
Project: NovemberAll Metals
Pace Project No.: 92406666
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2423631
2423632
MS
MSD
92406465008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Calcium
mg/kg
1120
481
490
1590
1570
99
93
75-125
1
Copper
mg/kg
11.7
48.1
49
59.4
61.3
99
101
75-125
3
Lead
mg/kg
2.6
48.1
49
46.6
47.3
91
91
75-125
1
Magnesium
mg/kg
236
481
490
663
630
89
80
75-125
5
Molybdenum
mg/kg
0.54
48.1
49
49.5
50.4
102
102
75-125
2
Nickel
mg/kg
1.4
48.1
49
47.6
48.0
96
95
75-125
1
Potassium
mg/kg
ND
481
490
683
692
96
95
75-125
1
Selenium
mg/kg
ND
48.1
49
42.0
43.3
87
88
75-125
3
Sodium
mg/kg
ND
481
490
532
538
96
95
75-125
1
Zinc
mg/kg
38.1
48.1
49
84.6
83.3
97
92
75-125
2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/21/2018 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19

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Project: November All Metals
Pace Project No.: 92406666
QC Batch: 441406
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 92406666001
SAMPLE DUPLICATE: 2423990
Parameter
Percent Moisture
SAMPLE DUPLICATE: 2424091
Parameter
Percent Moisture
(QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
2611144001 Dup
Units Result Result RPD Qualifiers
% 50.2 48.3 4
92406737001 Dup
Units Result Result RPD Qualifiers
% 19.0 18.1 5
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: NovemberAll Metals
Pace Project No.: 92406666
QC Batch: 441716 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92406666001
SAMPLE DUPLICATE: 2425304
Parameter
pH at 25 Degrees C
92406635001 Dup
Units Result Result RPD Qualifiers
Std_ Units 7.4 7.5 1 H3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

50
� aceAnaly ical
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Project: November All Metals
Pace Project No.: 92406666
QC Batch: 442330
QC Batch Method: EPA 350.1 Rev 2.0 1993 Mod.
Associated Lab Samples: 92406666001
METHOD BLANK: 2428012
Associated Lab Samples: 92406666001
Parameter Units
Nitrogen, Ammonia mg/kg
(QUALITY CONTROL DATA
Analysis Method: EPA 350.1 Rev 2.0 1993 Mod.
Analysis Description: 350.1 Ammonia
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 10.0 11/15/1816:22
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2428013
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/kg 490 518 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2428014 2428015
MS MSD
92406196001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia mg/kg 2260 472 490 1990 2350 -58 18 90-110 17 M1,R1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 19

�aceAnaRical
www.pacelabscom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: November All Metals
Pace Project No.: 92406666
QC Batch: 442120 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: , EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN
Associated Lab Samples: 92406666001
METHOD BLANK: 2427144
Associated Lab Samples: 92406666001
Parameter
Units
Nitrogen, Kjeldahl, Total
mg/kg
LABORATORY CONTROL SAMPLE: 2427145
Parameter
Units
Nitrogen, Kjeldahl, Total
mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 50.0 11/1411813:08
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1000 988 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2427146 2427147
MS MSD
92406735001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/kg 56300 4410 4010 60400 56900 94 16 90-110 6 M6
Results presented on this page am In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2018 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19

�a-eAnalX cal
www.pacelabs.com
i
Project: November All Metals
Pace Project No.: 92406666
QC Batch: 441309
QC Batch Method: EPA 353.2 Rev 2.0 1993
Associated Lab Samples: 92406666001
METHOD BLANK: 2423453
Associated Lab Samples: 92406666001
Parameter
Units
Nitrogen, Nitrate
mg/kg
Nitrogen, Nitrite
mg/kg
Nitrogen, NO2 plus NO3
mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 353.2 Rev 2.0 1993
Analysis Description: 353.2 Nitrate + Nitrite
Matrix: Solid
Blank Reporting
Result Limit Analyzed
ND 2.0 11/09/1813:03
ND 1.0 11/09/1813:03
ND 2.0 11/09/1813:03
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2423454
Spike LQS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/kg 15 14.5 97 90-110
Nitrogen, Nitrite mg/kg 10 10 100 90-110
Nitrogen, NO2 plus NO3 mg/kg 25 24.5 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2423455
2423456
MS
MSD
92405407001
Spike
Spike
MS
MSD
MS
MSD % Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec Limits
RPD Qual
Nitrogen, Nitrate
mg/kg
ND
29.3
29.3
14.5
ND
49
0 90-110
M1,R1
Nitrogen, Nitrite
mg/kg
2.4
19.7
19.5
14.0
8.7
48
21 90-110
47 M1,R1
Nitrogen, NO2 plus NO3
mg/kg
2.0
49
49
28.5
8.1
50
8 90-110
112 M1,R1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21/2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

J
-aceAna1j4ka(
wvmpacelabs.com
QUALITY CONTROL DATA
Project: November All Metals
Pace Project No.: 92406666
QC Batch: 441810 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92406666001
METHOD BLANK: 2425931
Associated Lab Samples: 92406666001
Parameter Units
Phosphorus mg/kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 11/13/18 22:54
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2425932
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 52.5 105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2425933 2425934
MS MSD
92406807002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 16000 2370 2750 17200 20100 49 146 90-110 15 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /21 /2018 04:37 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 19

Pace Analytical Services, LLC
acel® 9800 IGnceyAve, Suite 100
Arialytiea
/ Huntersville, NC 28078
www.pacelabs.com
[phone]
QUALIFIERS
Project: November All Metals
Pace Project No.: 92406666
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,. except in full,
Date: 11/21/2018 04:37 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 19

U
f
/7aicoAnalj&a(
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NovemberAll Metals
Pace Project No.: 92406666
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92406666001
nitrate, Metals, Solids
EPA 3050E
441349
EPA 601 OD
441493
92406666001
nitrate, Metals, Solids
EPA 7471 B
443240
EPA 7471 B
443274
92406666001
nitrate, Metals, Solids
SM 254OG-2011
441984
92406666001
nitrate, Metals, Solids
ASTM D2974-87
441406
92406666001
nitrate, Metals, Solids
EPA 9045D
441716
92406666001
nitrate, Metals, Solids
SM 271OB-2011
443438
92406666001
nitrate, Metals, Solids
TKN+NO3+NO2
443121
Calculation
92406666001
nitrate, Metals, Solids
EPA 350.1 Rev 2.0 1993
442330
EPA 350.1 Rev 2.0 1993
442423
Mod.
Mod.
92406666001
nitrate, Metals, Solids
EPA 351.2 Rev 2.0 1993
442120
EPA 351.2 Rev 2.0 1993
442261
92406666001
nitrate, Metals, Solids
EPA 353.2 Rev 2.0 1993
441309
EPA 353.2 Rev 2.0 1993
441310
92406666001
nitrate, Metals, Solids
EPA 365.1 Rev 2.0 1993
441810
EPA 365.1 Rev 2.0 1993
441865
Date: 11/21/2018 04:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 19

Document Name:
Document Revised: February 7, 2018
dCeAnalytlCai
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑
Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[]
Alb
'SampleCondition Client Na
Upon Receipt rlt
e: Project: ��"• �����
A'/ /
f
Courier:rci 1 ❑PFa .Ex UPS ❑USPS❑Client II I III I II I I`
e a II I II IB III
❑ 0 ce ❑Other . 92406666
Custody Seat Present? ❑Yes ❑Seals Intact? ❑Yes ❑No
Date/InitlelsPersenEaaminingContents:•"�
Packing Material: [-]Bubble Wrap QBubb el Bags ❑None ❑ Other Biological Tissue Frozen?
Thermomete r92TO45 Type of ice: Q❑8[]None
None ❑Yes ❑No ; QN%A "
Gun 1D: �
LJ IR Gun
Cooler Temp (•C): Correction Factor: Add/Subtract ('C) _0,1
Temp should be above freezing to 6°C
Cooler Temp Corrected ('C):_ 05amples out of temp criteria. Samples on ice, cooling process
hashegun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
i—IYes F-IN-n inrludinn HAwaii and Puarrn Rirnl? MYPS nkn
Comments/Discrepancy:
Chain of Custody Present?
jr]Yes
QN0
❑N/A
1.
Samples Arrived within Hold Time?
!:]No
❑N/A
2.
Short bold Time Analysis 1e72 hr.)?
❑Yes
❑No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑No
❑N/A
4.
Sufficient Volume?
Q<-
❑No
❑N/A
5.
Correct Containers Used?
❑>—
❑No
[]NIA
6.
-Pace Containers Used?
j]Yes
[]No
[-]N/A
Containers Intact?
Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field filtered?
❑Yes
No
❑N'/A
8.
Sample Labels Match COC?
QYes
[]No
[]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
r_) �-
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
EN/A
10.
Trip Blank Present?
[]Yes
❑No—
❑N/A
11.
Trip Blank Custody Seals Present?
[]Yes
❑No
❑Nla
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review: W
Project Manager SRF Review:L,-
Date/Time:
Field Data Required? ❑Yes ❑No
Date: �i-�-1'�
Date: 11 L-12 g
Page 17 of 19

MV
aceAnaljdical w
r
Document Name:
Sample Condition Upon Recet t(SCUR)
Document Revised: February 7, 2018
Pagel of 2
Document No;:
F•CAR-CS-033-Rev.06
issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO18015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project# I W F21406666��
PM`: Ab' Due• Date: 11/26%18
CLIENT: 92-Vell l I a• War
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot #
Note: Whenever there is -a discrepancy attecting North Carolina compliance samples, a copy or this Corm will oe sent to the Norrn larollna UtHIVK Lercincauon vmce (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 18 of 19

- !�O aceAnalXical "
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
N
(0
EL
Section A
Section B
Section C
Page: 1
of
1
Required Client Information:
Required Project Information;
Invoice Information:
Company: Veolia Water
Report To: Paul Spencer
Attention: Paul SpencerREGULATORY
Address: 32002othAvenue SE
Copy To: Logan.Hughes(a7veolia Company Name;
NPDES I GROUNDWATER i DRINKING WATER
Newton, NC 28658
Address:
i
UST i RCRA
X OTHER_IUP_
Email To: Daul.SDencCrt5veolia.com
Purchase CC On file
Pace Quote Reference:
I— GA i— IL F F MI
X NC
Order No.:
iN
Phone: [phone] Fax: [phone]
Project Name: November all metals Pace Project Manager.
Angela Saioni
• • C— OH i SC F WI OTHER_,_ _
Requested std
Due DaterrAT:
Project Number.
Pace Profile 41.
Filtored Y!N
(YIN)
Section D W9dr..a c*dC
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_�aceAnalytical
www.pacelabs.com
December 20, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: December Fecal
Pace Project No.: 92411191
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 lGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
pCCQEr
Ae�A�Q,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 5

.,P ceAnalylical "
.:.•rr na^�+ads ca•n
Section A
Gnn.d—d CauN ,nrnnnaenro
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Reouired Pmlxt Information: Invnl— ,nFnrmaltnn•
Page: 1 of 1
Company: Veolia Water
Report To: Paul Spencer
Attention: Paul Speticer
D'RY AGENCY
r— NPDES F GROUNDWATER i DRINKING WATER
r UST F RCRA X OTHER_IUP_,
Address: 3200 20th Avenue.SE
copy To: Loaan.Hughes veolia
Company Name:
Newton, NC 28658
Address:
Email To: [e-mail]'1
Purchase CC on file
Order No.:
Pace Quote Reference:SITE
fGA i IL F IN MI X NC
_
LOCATION r OH i -SC r WI .t OTHER_
Filtered (riN)
Phone: [phone]
Fax [phone]
Project Name: December Fecal
Pace Project Manager, Angela Baioni
Requested Std
Duo Data1TAT:
Project Number
Pace Prbhle k:
ik
F
Section D v°'d Maa+t tee'
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Required client information M
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Analytical Results
Pace Anal"ciail
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 12/18/2018
Reported: 12/19/2018
For:
Comments:
r ANALY A
Sample Number
Parameter
Sample ID
Result
Unit Method
Analyzed
Analyst
181218-19-01
Fecal Coliforms
Veolia Water
697
MPN/g SM92210E-2006
12/18/2018
WC
181218-19-01
Percent Solids
Veolia Water
33
% SM254OB-2011
12/18/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 o Statesville, NC 28687 o 704/872/4697
Page 1 of sage 3 of 5

Condition of Receipt
Sample Number 181218-19-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
pH on Arrival: <2 Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 o Statesville, NC 28687 m 704/872/4697
Page 2 of kge 4 of 5

RaceAnaljAical -
CHAIN -OF -CUSTODY / Analytical Request Document
The Chamt+t-Cuslcdy Is a LEGAL DOCUMENT All ieievant fields mini be completed accost
Section A Section B Section C Pago: 1 of f
Requlrod Cixnt Informalbn Raqulr-d Pr ,; cl Irdernvation lmorce Iruormahen
ComPany Veolia Water Report To Paul Spencer Attention Paul Spencer REGULATORY
Address 3200 201h Avrnu-3 SE Cepy To - 5:I ;n HUgh-qs,^v Ccmparry Nama -
-- NPDES GROUND WA ER DRINKINGWATER
Ne+4an, NC 25w Address r
- UST RCRA X OTHER —rUP —
Emil To y:r:,.- , ._t,
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�aceAnalytical
www.pacelabs.com
December 26, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: December Metals
Pace Project No.: 92411199
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 18, 2018.
The results relate only to the samples included in this report, Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�
�,xglo, W1, �G Qt1i
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 12

W
AaceAnalydcal o
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I
CERTIFICATIONS
Project: December Metals
Pace Project No.: 92411199
Pace Analytical Services, LLC
9800 incey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 12

aceAnalytical"
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SAMPLE ANALYTE COUNT
Project: December Metals
Pace Project No.: 92411199
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analyses
Lab ID Sample ID Method
Analysts
Reported
Laboratory
92411199001 Metals/Solids EPA 6010D
SER
8
PASI-A
EPA 7471B
JMW1
1
PASI-A
SM 2540G-2011
KDF
1
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

1laceAnalXica(
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i
ANALYTICAL RESULTS
Project: December Metals
Pace Project No.: 92411199
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Metals/Solids
Lab ID: 92411199001
Collected: 12/18/18 07:20
Received: 12118/18 09:12 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA6010D Preparation Method: EPA 3050B
Arsenic
ND
mg/kg
0.81
1
12121/18 17:51
12/24/18 00:24
7440-38-2
Cadmium
0.22
mg/kg
0.081
1
12/21/18 17:51
12/24/18 00:24
7440-43-9
Copper
61.1
mg/kg
0.40
1
12/21/18 17:51
12/24/18 00:24
7440-50-8
Lead
3.7
mg/kg
0.40
1
12/21/18 17:51
12/24/18 00:24
7439-92-1
Molybdenum
2.8
mg/kg
0.40
1
12/21/18 17:51
12/24/18 00:24
7439-98-7
Nickel
4.1
mg/kg
0.40
1
12/21/18 17:51
12/24/18 00:24
7440-02-0
Selenium
1.1
mg/kg
0.81
1
12/21/18 17:51
12/24/18 00:24
7782-49-2
Zinc
308
mg/kg
0.81
1
12/21/18 17:51
12/24/18 00:24
7440-66-6
7471 Mercury
Mercury
2540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
Date: 12/26/2018 01:42 PM
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
0.096 mg/kg 0.0053 1 12119/1819:13 12/20/1812:29 7439-97-6
Analytical Method: SM 2540G-2011
48.2 % 0.000010 1
Analytical Method: ASTM D2974-87
51.8 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/18/18 17:34
12/18/18 17:24
Page 4 of 12
U

�aceAnalytical
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Project: December Metals
Pace Project No.: 92411199
QC Batch: 448621
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92411199001
METHOD BLANK: 2457205
Associated Lab Samples: 92411199001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 2457206
Parameter Units
Mercury mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 12/20/1811:47
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
0.083 0.074 88 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2457207 2457208
MS MSD
35437634001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.0089 0.096 0.09 0.11 0.092 108 92 75-125 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/26/2018 01:42 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 12

VaceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: December Metals
Pace Project No.: 92411199
QC Batch: 449177 Analysis Method: EPA 6010D
QC Batch Method: EPA3050B Analysis Description: 6010 MET
Associated Lab Samples: 92411199001
METHOD BLANK: 2459836 Matrix: Solid
Associated Lab Samples: 92411199001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
12/23/18 23:10
Cadmium
mg/kg
ND
0.10
12/23/18 23:10
Copper
mg/kg
ND
0.50
12/23/18 23:10
Lead
mg/kg
ND
0.50
12/23/18 23:10
Molybdenum
mg/kg
ND
0.50
12/23/18 23:10
Nickel
mg/kg
ND
0.50
12/23/18 23:10
Selenium
mg/kg
ND
1.0
12/23/18 23:10
Zinc
mg/kg
ND
1.0
12/23/18 23:10
LABORATORY CONTROL SAMPLE:
Parameter
2459837
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.0
94
80-120
Cadmium
mg/kg
50
46.7
93
80-120
Copper
mg/kg
50
49.0
98
80-120
Lead
mg/kg
50
47.3
95
80-120
Molybdenum
mg/kg
50
50.4
101
80-120
Nickel
mglkg
50
47.6
95
80-120
Selenium
mg/kg
50
44.8
90
80-120
Zinc
mg/kg
50
48.0
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2459838
2459839
MS
MSD
92411236001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
31.2
31.2
29.4
29.6
94
95
75-125
0
Cadmium
mg/kg
ND
31.2
31.2
29.9
30.0
96
96
75-125
0
Copper
mg/kg
11.8
31.2
31.2
43.4
43.6
101
102
75-125
1
Lead
mg/kg
3.6
31.2
31.2
33.4
33.3
95
95
75-125
0
Molybdenum
mg/kg
1.0
31.2
31.2
32.0
32.0
99
99
75-125
0
Nickel
mg/kg
1.9
31.2
31.2
32.0
32.1
96
96
75-125
0
Selenium
mg/kg
ND
31.2
31.2
29.0
29.3
92
93
75-125
1
Zinc
mg/kg
289
31.2
31.2
296
293
20
12
75-125
1 M1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/26/2018 01:42 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 12

�aceAnaly`ical
www.pacelabs.com
QUALITY CONTROL DATA
Project: December Metals
Pace Project No.: 92411199
QC Batch: 448347 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92411199001
SAMPLE DUPLICATE: 2455873
92411060010 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 26.9 25.9 4
SAMPLE DUPLICATE: 2455977
92411221001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 69.7 69.8 0
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/26/2018 01:42 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 12

4 5rz
� PaceAnalytical
www,pecelabs.com
QUALIFIERS
Project: December Metals
Pace Project No.: 92411199
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited -analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
W
This report shall not be reproduced, except in full,
Date: 12/26/2018 01:42 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 12

�aceAnalj&al
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: December Metals
Pace Project No.: 92411199
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92411199001
Metals/Solids
EPA 3050B
449177 EPA 601 OD
449275
92411199001
Metals/Solids
EPA 7471 B
448621 EPA 7471 B
448676
92411199001
Metals/Solids
SM 2540G-2011
448813
92411199001
Metals/Solids
ASTM D2974-87
448347
Date: 12/26/2018 01:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 12

Document Name: Document Revised: February 7, 2018
m Sample Condition Upon Receipt(SCUR)Page 1 of 2
aceAnalyilsal: Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples: Mechanicsville❑
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [ Raleigh❑
client Name. W( A . 9�2r �il i�J"1
� Project #:
.. VPr)11'CA wcuCourier: ❑Fed Ex ❑UPS ❑LISPS []Client
❑ Commercial [DPfe []Other: . 92411199
Custody Seal Present? []Yes ❑No Seals Intact? []Yes []No S^ fr `�
pate/Initials Person Examining Contents:
Packing Material: []Bubble Wrap []Bubble Bags []None ❑ Other Biological Tissue Frozen?.
❑Yes 3-No ❑N/A
Thermometer: Type of Ice: j]4Vet ❑Blue ❑None
.glf Gun IB: 92T046
Cooler Temp (°C): Correction Factor: Add/Subtract (°C) 0.0
Temp should be above freezing to 6'C
Cooler Temp Corrected (°C): []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ([Z N/A, water sample}
Did samples originate from a foreign source (internationally,
Did samples originate in a quarantine zone within the United States: CA NY, or SC (check maps)?
r--i.. _ _ ram:. _ - including Hawaii and Puerto Rico)? ❑Yes ❑No
Chain of Custody Present?
[2'1 s
[]NO
❑N/A
1•
Samples Arrived within Hold Time?
[]�fes
[]NO
❑N/A
2.
3.
Short Hold TimeAnalysis (Q2 hr.)? ❑Ycs []IGo ❑N/A
Rush Turn Around Time Requested?
❑Yes
[390
[]N/A
4-
S.
SufficientVolume? ]]Yes []No ❑N/A
Correct Containers Used?
O Yes
[_—]No
❑N/A
6•
-Pace Containers Used?
�Yrs
❑No
❑N/A
7.
8-
9.
Containers Intact? i Yes ❑No ❑N/A.
Dissolved analysis: Samples Field Filtered? []Y. ❑No (3N/A
Sam pl e Lab elsMatch COC? 21G ❑No ❑N/A
Headspace in VOA Vials (>5-6mm)? (JYes LINO WN/A LV•
Trip Blank Present? ❑Yes No ❑N/A 11.
Trio Blank Custodv Seals Present? ❑Yes []No DN/A
Field Data Required? []Yes ❑No
COMMENTS/SAMPLE DISCREPANCY
,Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/iime:
r1
Date: i�i�
Project Manager SCURF Review: i�"`I r
Project Manager SRF Review: t?> Date:
W
Page 10 of 12

.�aceAnalytical -
•
Section A
Required Client Information:
CHAIN -OF -CUSTODY / Analy$uca0 Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Required Project Information: Invoice Information:
s
N
C71
l0
Page: of
Company: Veolia Water
Report To: Paul Spencer
Attention: Paul Spencer
a -
r NPDES GROUND WATER i DRINKING WATER
-
UST (- RCRA f OTHER_X_
Address: 3200201h Avenue SE
Copy To: Logan Huohes(d_)veolia
Company Name:
Newton, NC 28658
Address:
Email To: Daui.spenCE![Q rEOlia.COM
Purchase CC on file
,Order No,:
Pace Quote Reference;
GA r IL (- IN (- MI I NC.X
• • OH f SC F WI r OTHER
Filtered (YIN)
Phone: [phone]
Fax:
Project Name: DECEMBER METALS
Pace Project Manager. Angela Beoni
Requestod std
Due DateITATC
Project Number:
Pace Profile #: 2816, 1
7t
W
Section D Vad6labuOnd—
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Required CEent information
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Metals -Arsenic, Lead, Cadmium, Copper,
Molybdenum, Nickel, Selenium, Zino and Mercury
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e-File(ALLQ020rev.4, 29Mar06)22J un20o5

Document Name:
londition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project # W "W Q; "'a411 1
verified and within the acceptance range for preservation — — �-
samples. Pill AMB _ Due Date: 01/03/19
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 92--Veo i i a Wa
**Bottom half of box is to list number of bottle
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1
2
I
3
4
5
6
7
\
\
8
9
iD
it
12
pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount added of Preservative Lot It
a cnnv of
this form will to sent to the North Carolina DEHNR Certification -office (i.e.
Note: whenever mere is a aiscrepaucy aucunig �� �� - Out of hold, incorrect preservative, out of temp, incorrect containers.
Ah
Page 11 of 12

EXHIBIT 4
Annual TCLP Laboratory Report and Analytical Data
22

a/
_,,r�lac'eAnalyticalo
www.pacelabs.com
October 22, 2018
Paul Spencer
Veolia Water North America
3200 20th Ave SE
Newton, NC 28658
RE: Project: Full TCLP October
Pace Project No.: 92402231
Dear Paul Spencer:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Paul Spencer, Veolia Water North America
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 40

'aceAna1j4ical
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Project: Full TCLP October
Pace Project No.: 92402231
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
ANAB DOD-ELAP Rad Accreditation #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification #: PA01547
Connecticut Certification #: PH-0694
Delaware Certification
EPA Region 4 DW Rad
Flodda/TNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: KY90133
KY WW Permit #: KY0098221
KY WW Permit #: KY0000221
Louisiana DHH/TNI Certification #: LA180012
Louisiana DEQ/TNI Certification #: 4086
Maine Certification #: 2017020
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification #: 9991
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Missouri Certification #: 235
Montana Certification #: Cert0082
Nebraska Certification #: NE-OS-29-14
Nevada Certification #: PA014572018-1
New Hampshire/TNI Certification #: 297617
New Jersey/TNI Certification #: PA051
New Mexico Certification #: PA01457
New York/TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Ohio EPA Rad Approval: #41249
OregonlTNI Certification #: PA200002-010
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PAO1457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: 02867
Texas/TNI Certification #: T104704188-17-3
Utah/TNI Certification #: PA014572017-9
USDA Soil Permit #: P330-17-00091
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 9526
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Approve List for Rad
Wyoming Certification #: 8TMS-L
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 40

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SAMPLE ANALYTE COUNT
Project: Full TCLP October
Pace Project No.: 92402231
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92402231001 Full TCLP & CRI October EPA 8081 B
SEM
9
PASI-C
EPA6010D
IDS
7
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA8270D
RES
18
PASI-C
EPA 8260E
GAW
14
PASI-C
ASTM D2974-87
AK1
1
PASI-PA
EPA 1010A
SMK
1
PASI-A
EPA9045D
ECH
1
PASI-A
EPA9014
PAS
1
PASI-PA
SM4500S2F-00
PAS
1
PASI-PA
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 40

MW
all
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ANALYTICAL RESULTS
Project: Full TCLP October
Pace Project No.: 92402231
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: Full TCLP & CRI October Lab ID: 92402231001 Collected: 10/04/18 07:30 Received: 10/04/18 12:35 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 10/08/18 14:20 Initial pH: 4.24; Final
pH: 5
gamma-BHC (Lindane)
ND
ug/L
0.50 1
10/09/18 07:48
10/09/18 17:39
58-89-9
Chlordane (Technical)
ND
ug/L
3.0 1
10/09/18 07:48
10/09/18 17:39
57-74-9
Endrin
ND
ug/L
0.50 1
10/09/18 07:48
10/09/18 17:39
72-20-8
Heptachlor
ND
ug/L
0.50 1
10/09/18 07:48
10/09/18 17:39
76-44-8
Heptachlor epoxide
ND
ug/L
0.50 1
10/09/18 07:48
10/09/18 17:39
1024-57-3
Methoxychlor
ND
ug/L
1000 1
10/09/18 07:48
10/09/18 17:39
72-43-5
Toxaphene
ND
ug/L
3.0 1
10/09/18 07:48
10/09/18 17:39
8001-35-2
Surrogates
Decachlorobiphenyl (S)
74
%
10-138 1
10/09/18 07:48
10/09/18 17:39
2051-24-3
Tetrachloro-m-xylene (S)
72
%
10-110 1
10/09/18 07:48
10/09/18 17:39
877-09-8
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD
Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 10/05/18 22:19 Initial pH: 7.05; Final
pH: 5
Arsenic
ND
mg/L
0.050 1
10/06/1817:56
1010811813:51
7440-38-2
Barium
ND
mg/L
0.25 1
10/06/1817:56
10/0811813:51
7440-39-3
Cadmium
ND
mg/L
0.0050 1
10/0611817:56
10/08/1813:51
7440-43-9
Chromium
ND
mg/L
0.050 1
10106/1817:56
10/08/1813:51
7440-47-3
Lead
ND
mg/L
0.025 1
10/06/1817:56
10108/1813:51
7439-92-1
Selenium
ND
mg/L
0.10 1
10/06/1817:56
1010811813:51
7782-49-2
Silver
ND
mg/L
0.025 1
10/06/1817:56
10/08/1813:51
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311;
10/05/18 22:19 Initial pH: 7.05; Final
pH: 5
Mercury
ND
mg/L
0.00020 1
10/06/18 19:30
10/09/18 09:38
7439-97-6
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270D Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311;
10/08/18 14:20 Initial
pH: 4.24; Final pH: 5
1,4-Dichlorobenzene
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
106-46-7
2,4-Dinitrotoluene
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
121-14-2
Hexachloro-1,3-butadiene
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
87-68-3
Hexachlorobenzene
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
118-74-1
Hexachloroethane
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
67-72-1
2-Methylphenol(o-Cresol)
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
95-48-7
3&4-Methylphenol(m&p Cresol)
72.9
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
15831-10-4
Nitrobenzene
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
98-95-3
Pentachlorophenol
ND
ug/L
100 1
10/11/18 09:39
10/11/18 20:23
87-86-5
Pyridine
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
110-86-1
2,4,5-Trichlorophenol
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
50.0 1
10/11/18 09:39
10/11/18 20:23
88-06-2
Surrogates
Nitrobenzene-d5 (S)
36
%
12-102 1
10/11/18 09:39
10/11/18 20:23
4165-60-0
2-Fluorobiphenyl (S)
35
%
13-107 1
10/11/18 09:39
10/11/18 20:23
321-60-8
Terphenyl-d14 (S)
55
%
21-132 1
10/11/18 09:39
10/11/18 20:23
1718-51-0
Phenol-d6 (S)
17
%
10-110 1
10/11/18 09:39
10/11/18 20:23
13127-88-3
2-Fluorophenol (S)
23
%
10-110 1
10/11/18 09:39
10/11/18 20:23
367-12-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except
in full,
Date: 10/22/2018 04:41 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 40

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ANALYTICAL RESULTS
Project: Full TCLP October
Pace Project No.: 92402231
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(7,04)875-9092
Sample: Full TCLP & CRI October Lab ID: 92402231001 Collected: 10/04/18 07:30 Received: 10/04/18 12:35 Matrix: Solid
Results reported on a "wet -weight" Basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270D Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 10/08/18 14:20 Initial pH: 4.24; Final pH: 5
Surrogates
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
1010 Flashpoint,Closed Cup
Flashpoint
9045 pH Soil
pH at 25 Degrees C
733C S Reactive Cyanide
Cyanide, Reactive
734S Reactive Sulfide
Sulfide, Reactive
Date: 10/22/2018 04:41 PM
59 % 27-108 1 10/11/18 09:39 10/11/18 20:23 118-79-6
Analytical Method: EPA8260B Leachate Method/Date: EPA1311; 10/05/18 17:00
ND ug/L
100
20
10/0911818:05
71-43-2
ND ug/L
200
20
10109/1818:05
78-93-3
ND ug/L
100
20
10/09/1818:05
56-23-5
ND ug/L
100
20
10/09/1818:05
108-90-7
ND ug/L
100
20
10/09/1818:05
67-66-3
ND ug/L
100
20
10/09/1818:05
106-46-7
ND ug/L
100
20
10/09/1818:05
107-06-2
ND ug/L
100
20
10/09/1818:05
75-35-4
ND ug/L
100
20
10109/1818:05
127-18-4
ND ug/L
100
20
10/09/1818:05
79-01-6
ND ug/L
100
20
10/0911818:05
75-01-4
104 %
70-130
20
10/09/1818:05
17060-07-0
110 %
67-135
20
10109/1818:05
2037-26-5
107 %
70-130
20
10/09/1818:05
460-00-4
Analytical Method: ASTM D2974-87
63.2 %
0.10
1
10/16/1810:53
Analytical Method: EPA 1010A
>200 deg F
70.0
1
10/14/18 14:43
Analytical Method: EPA 9045D
6.8 Std. Units
0.10
1
10/05/18 13:13
H6
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
ND mg/kg
0.99
1 10/11/18 22:38
10/11/18 23:39
Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
ND mg/kg
9.9
1 10/11/18 22:38
10/11/18 22:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 40

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dlr
�.. lac'eAnaIX caI
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t
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 434885
QC Batch Method: EPA 7470A
Associated Lab Samples: 92402231001
METHOD BLANK: 2393655
Associated Lab Samples: 92402231001
Parameter
Units
Mercury
mg/L
METHOD BLANK: 2394104
Associated Lab Samples: 92402231001
Parameter
Units
Mercury
mg/L
METHOD BLANK: 2394120
Associated Lab Samples: 92402231001
Parameter Units
Mercury
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2394427
Units
Mercury
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2394428
Units
Mercury
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2394429
Units
Mercury
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method:
EPA 7470A
Analysis Description:
7470 Mercury TCLP
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
ND 0.00020 10108/1811:17
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
ND 0.00020 10/0811811:22
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.00020 10108/1811:27
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.0025 0.0025 100 80-120
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.0025 0.0025 100 80-120
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
.0025 0.0025 101 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 40

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QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2394430
2394431
MS
MSD
92402098001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Cone.
Cone.
Result
Result % Rec % Rec Limits RPD Qua[
Mercury mg/L ND .0025
.0025
0.00068
0.00089 25 33 75-125 26 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 40

u
AV11:-,7
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I
QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 434884
QC Batch Method: EPA 3010A
Associated Lab Samples: 92402231001
Analysis Method:
Analysis Description:
EPA 6010D
6010 MET TCLP
METHOD BLANK: 2393655
Matrix: Water
Associated Lab Samples: 92402231001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
10/08/1812:19
Barium
mg/L
ND
0.25
10/08/1812:19
Cadmium
mg/L
ND
0.0050
10/0811812:19
Chromium
mg/L
ND
0.050
10/08/1812:19
Lead
mg/L
ND
0.025
10/08/1812:19
Selenium
mg/L
ND
0.10
10/0811812:19
Silver
mg/L
ND
0.025
10/08/1812:19
METHOD BLANK: 2394104
Matrix: Water
Associated Lab Samples: 92402231001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
10/08/1812:26
Barium
mg/L
ND
0.25
10/08/1812:26
Cadmium
mg/L
ND
0.0050
10/08/1812:26
Chromium
mg/L
ND
0.050
10/08/1812:26
Lead
mg/L
ND
0.025
10/08/1812:26
Selenium
mg/L
ND
0.10
10/0811812:26
Silver
mg/L
ND
0.025
10/08/1812:26
METHOD BLANK: 2394120
Matrix: Water
Associated Lab Samples: 92402231001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
10/0811812:32
Barium
mg/L
ND
0.25
10/08/1812:32
Cadmium
mg/L
ND
0.0050
10108/1812:32
Chromium
mg/L
ND
0.050
10/0811812:32
Lead
mg/L
ND
0.025
10/08/1812:32
Selenium
mg/L
ND
0.10
10/08/1812:32
Silver
mg/L
ND
0.025
10/08/1812:32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2394422
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Arsenic mg/L 2.5 2.4 97 80-120
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Full TCLP October
Pace Project No.: 92402231
LABORATORY CONTROL SAMPLE:
2394422
Parameter
Units
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
LABORATORY CONTROL SAMPLE:
Parameter
2394423
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, LLC
9800 KinceyAve. Suite 10o
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Spike
LCS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.4
95
80-120
2.5
2.4
96
80-120
2.5
2.4
95
80-120
2.5
2.3
90
80-120
2.5
2.5
98
80-120
1.2
1.2
98
80-120
Spike
LCS
LCS
% Rec
Cone.
Result
% Rec
Limits Qualifiers
2.5
2.4
95
80-120
2.5
2.5
100
80-120
2.5
2.4
97
80-120
2.5
2.4
97
80-120
2.5
2.3
94
80-120
2.5
2.5
98
80-120
1.2
1.2
98
80-120
LABORATORY CONTROL SAMPLE:
Parameter
2394424
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/L
2.5
2.4
96
80-120
Barium
mg/L
2.5
2.4
96
80-120
Cadmium
mg/L
2.5
2.4
96
80-120
Chromium
mg/L
2.5
2.4
95
80-120
Lead
mg/L
2.5
2.2
90
80-120
Selenium
mg/L
2.5
2.5
98
80-120
Silver
mg/L
1.2
1.2
97
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2394425
2394426
MS
MSD
92401464002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.4
2.5
94
100
75-125
6
Barium
mg/L
0.35
2.5
2.5
2.8
2.9
99
102
75-125
2
Cadmium
mg/L
0.073
2.5
2.5
2.4
2.5
95
99
75-125
4
Chromium
mg/L
0.033J
2.5
2.5
2.4
2.5
96
99
75-125
3
Lead
mg/L
8.2
2.5
2.5
11.4
11.4
128
128
75-125
0 M1
Selenium
mg/L
ND
2.5
2.5
2.4
2.5
96
100
75-125
4
Silver
mg/L
ND
1.2
1.2
1.2
1.3
96
101
75-125
' 4
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 40

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50
�RaceAnalytical
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QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 435182 Analysis Method: EPA 8260E
QC Batch Method: EPA 8260B Analysis Description: 8260 MSV TCLP
Associated Lab Samples: 92402231001
METHOD BLANK: 2393834 Matrix: Water
Associated Lab Samples: 92402231001
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
1,1-Dichloroethene
ug/L
ND
5.0
10/09/18 16:40
1,2-Dichloroethane
ug/L
ND
5.0
1010911816:40
1,4-Dichlorobenzene
ug/L
ND
5.0
10/09/18 16:40
2-Butanone (MEK)
ug/L
ND
10.0
10/09/18 16:40
Benzene
ug/L
ND
5.0
10/09/18 16:40
Carbon tetrachloride
ug/L
ND
5.0
10/09/18 16:40
Chlorobenzene
ug/L
ND
5.0
10/0911816:40
Chloroform
ug/L
ND
5.0
10/09/18 16:40
Tetrachloroethene
ug/L
ND
5.0
10/09/18 16:40
Trichloroethene
ug/L
ND
5.0
10/09/18 16:40
Vinyl chloride
ug/L
ND
5.0
10/09/18 16:40
1,2-Dichloroethane-d4 (S)
%
109
70-130
10/09/18 16:40
4-Bromofluorobenzene (S)
%
104
70-130
10/09/18 16:40
Toluene-d8 (S)
%
106
67-135
10/09/18 16:40
LABORATORY CONTROL SAMPLE:
2395614
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1-Dichloroethene
ug/L
50
61.0
122
66-135
1,2-Dichloroethane
ug/L
50
54.8
110
67-128
1,4-Dichlorobenzene
ug/L
50
48.4
97
78-130
2-Butanone (MEK)
ug/L
100
118
118
61-144
Benzene
ug/L
50
53.8
108
80-125
Carbon tetrachloride
ug/L
50
54.2
108
69-131
Chlorobenzene
ug/L
50
49.0
98
81-122
Chloroform
ug/L
50
58.2
116
73-127
Tetrachloroethene
ug/L
50
50.7
101
78-122
Trichloroethene
ug/L
50
52.8
106
78-122
Vinyl chloride
ug/L
50
61.5
123
58-137
1,2-Dichloroethane-d4 (S)
%
110
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
96
67-135
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2395615
2395616
MS
MSD
92402279001
Spike
Spike
MS
MSD MS
MSD % Rec
Parameter
Units Result
Conc.
Conc.
Result
Result % Rec % Rec Limits RPD Qua]
1,1-Dichloroethene
ug/L ND
20
20
25.1
22.8 126 114 70-150 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No_: 92402231
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2395615
MS
92402279001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2395616
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qua[
1,2-Dichloroethane
ug/L
ND
20
20
24.2
23.0
121
115
70-150
5
1,4-Dichlorobenzene
ug/L
ND
20
20
23.0
23.0
115
115
70-150
0
2-Butanone (MEK)
ug/L
ND
40
40
52.9
52.5
125
124
70-150
1
Benzene
ug/L
ND
20
20
24.5
23.5
123
118
70-150
4
Carbon tetrachloride
ug/L
ND
20
20
22.7
22.4
113
112
70-150
1
Chlorobenzene
ug/L
ND
20
20
23.7
23.2
119
116
70-150
2
Chloroform
ug/L
ND
20
20
22.2
21.5
111
107
70-150
3
Tetrachloroethene
ug/L
ND
20
20
22.7
22.8
113
114
70-150
1
Trichloroethene
ug/L
ND
20
20
23.5
23.8
118
119
70-150
1
Vinyl chloride
ug/L
ND
20
20
24.9
24.2
125
121
70-150
3
1,2-Dichloroethane-d4 (S)
%
97
94
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8 (S)
%
97
96
67-135
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 40

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Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 435104
QC Batch Method: EPA 3510C
Associated Lab Samples: 92402231001
METHOD BLANK: 2394987
Associated Lab Samples: 92402231001
Parameter
Chlordane (Technical)
Endrin
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
QUALITY CONTROL DATA
Analysis Method: EPA 8081B
Analysis Description: 8081 TCLP Pesticides RV
Matrix: Water
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
ug/L
ND
3.0
10/09/1818:17
ug/L
ND
0.50
10/09/1818:17
ug/L
ND
0.50
10/0911818:17
ug/L
ND
0.50
10/09/1818:17
ug/L
ND
0.50
10/09/1818:17
ug/L
ND
1000
10/09/1818:17
ug/L
ND
3.0
10/0911818:17
%
113
10-138
10/09/18 18:17
%
99
10-110
10/09/18 18:17
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2395221
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Endrin
ug/L
1.2
1.1
89
20-134
gamma-BHC (Lindane)
ug/L
1.2
1.1
91
20-118
Heptachlor
ug/L
1.2
1.7
137
20-142
Heptachlor epoxide
ug/L
1.2
1.2
99
22-133
Methoxychlor
ug/L
3.8
ND
111
44-150
Decachlorobiphenyl (S)
%
138
10-138
Tetrachloro-m-xylene (S)
%
129
10-110 SO
MATRIX SPIKE SAMPLE:
Parameter
2395220
Units
92400969001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Endrin
ug/L
ND
1.2
1.1
87
21-133
gamma-BHC (Lindane)
ug/L
ND
1.2
1.1
88
24-119
Heptachlor
ug/L
ND
1.2
1.2
97
16-128
Heptachlor epoxide
ug/L
ND
1.2
1.3
101
50-150
Methoxychlor
ug/L
ND
3.8
ND
107
50-150
Decachlorobiphenyl (S)
%
91
10-138
Tetrachloro-m-xylene (S)
%
100
10-110
SAMPLE DUPLICATE: 2395222
92402231001 Dup
Parameter Units Result Result RPD Qualifiers
Chlordane (Technical) ug/L ND ND
Endrin ug/L ND ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Full TCLP October
Pace Project No.: 92402231
SAMPLE DUPLICATE: 2395222
Parameter
gamma-BHC (Lindane)
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
QUALITY CONTROL DATA
Units
92402231001
Result
Dup
Result
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
ug/L
ND
ND
%
74
61
%
72
58
RPD Qualifiers
20
21
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 40

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I
QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 435661 Analysis Method: EPA 8270D
QC Batch Method: EPA 3510C Analysis Description: 8270D TCLP MSSV
Associated Lab Samples: 92402231001
METHOD BLANK: 2394987
Associated Lab Samples: 92402231001
Parameter
Units
1,4-Dichlorobenzene
ug/L
2,4,5-Trichlorophenol
ug/L
2,4,6-Trichlorophenol
ug/L
2,4-Dinitrotoluene
ug/L
2-Methylphenol(o-Cresol)
ug/L
3&4-Methylphenol(m&p Cresol)
ug/L
Hexachloro-1,3-butadiene
ug/L
Hexachlorobenzene
ug/L
Hexachloroethane
ug/L
Nitrobenzene
ug/L
Pentachlorophenol
ug/L
Pyridine
ug/L
2,4,6-Tribromophenol (S)
%
2-Fluorobiphenyl (S)
%
2-Fluorophenol (S)
%
Nitrobenzene-d5 (S)
%
Phenol-d6 (S)
%
Terphenyl-d14 (S)
%
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
50.0
10111/1815:36
ND
50.0
10/11/1815:36
ND
50.0
10/11/1815:36
ND
50.0
10/11/1815:36
ND
50.0
10/1111815:36
ND
50.0
10111/1815:36
ND
50.0
10/1111815:36
ND
50.0
10/11/1815:36
ND
50.0
10/11/1816:36
ND
50.0
10/11/1815:36
ND
100
10/11/1815:36
ND
50.0
10/11/1815:36
79
27-108
10/1111815:36
70
13-107
10/11 /18 15:36
51
10-110
10/11/18 15:36
67
12-102
10111 /18 15:36
36
10-110
10/11 /18 15:36
101
21-132
10/11 / 18 15:36
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2397656
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,4-Dichlorobenzene
ug/L
500
341
68
10-110
2,4,5-Trichlorophenol
ug/L
500
437
87
39-108
2,4,6-Trichlorophenol
ug/L
500
459
92
40-104
2,4-Dinitrotoluene
ug/L
500
476
95
42-109
2-Methylphenol(o-Cresol)
ug/L
500
363
73
31-110
3&4-Methylphenol(m&p Cresol)
ug/L
500
317
63
30-110
Hexachloro-1,3-butadiene
ug/L
500
323
65
10-110
Hexachlorobenzene
ug/L
500
425
85
39-121
Hexachloroethane
ug/L
500
312
62
10-110
Nitrobenzene
ug/L
500
448
90
32-101
Pentachlorophenol
ug/L
1000
756
76
18-108
Pyridine
ug/L
500
211
42
10-110
2,4,6-Tribromophenol (S)
%
87
27-108
2-Fluorobiphenyl (S)
%
88
13-107
2-Fluorophenol (S)
%
53
10-110
Nitrobenzene-d5 (S)
%
84
12-102
Phenol-d6 (S)
%
35
10-110
Terphenyl-d14 (S)
%
96
21-132
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units Indicated by the " Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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PaceAnalgical ® 9800 Kinney Ave. Suite100
Huntersville, NC 28078078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
MATRIX SPIKE SAMPLE: 2397657
92402279001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
1,4-Dichlorobenzene ug/L ND 500 323 65 30-150
2,4,5-Trichlorophenol ug/L ND 500 371 74 30-150
2,4,6-Trichlorophenol ug/L ND 500 390 78 30-150
2,4-Dinitrotoluene ug/L ND 500 404 81 30-150
2-Methylphenol(o-Cresol) ug/L ND 500 374 75 30-160
3&4-Methylphenol(m&p Cresol) ug/L ND 500 342 68 30-150
Hexachloro-1,3-butadiene ug/L ND 500 303 61 30-150
Hexachlorobenzene ug/L ND 500 404 81 30-150
Hexachloroethane ug/L ND 500 318 64 30-150
Nitrobenzene ug/L ND 500 413 83 30-150
Pentachlorophenol ug/L ND 1000 664 66 30-150
Pyridine ug/L ND 500 237 47 30-150
2,4,6-Tribromophenol (S) % 85 27-108
2-Fluorobiphenyl (S) % 74 13-107
2-Fluorophenol (S) % 49 10-110
Nitrobenzene-d5 (S) % 77 12-102
Phenol-d6 (S) % 35 10-110
Terphenyl-d14 (S) % 91 21-132
SAMPLE DUPLICATE: 2397658
92402328001 Dup
Parameter Units Result Result RPD Qualifiers
1,4-Dichlorobenzene ug/L ND ND
2,4,5-Trichlorophenol ug/L ND ND
2,4,6-Trichlorophenol ug/L ND ND
2,4-Dinitrotoluene ug/L ND ND
2-Methylphenol(o-Cresol) ug/L ND ND
3&4-Methylphenol(m&p Cresol) ug/L ND ND
Hexachloro-1,3-butadiene ug/L ND ND
Hexachlorobenzene ug/L ND ND
Hexachloroethane ug/L ND ND
Nitrobenzene ug/L ND ND
Pentachlorophenol ug/L ND ND
Pyridine ug/L ND .ND
2,4,6-Tribromophenol (S) % 84 87 3
2-Fluorobiphenyl (S) % 51 51 0
2-Fluorophenol(S) % 32 35 10
Nitrobenzene-d5 (S) % 55 57 2
Phenol-d6 (S) % 24 25 6
Terphenyl-d14 (S) % 82 96 16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 316809 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92402231001
SAMPLE DUPLICATE: 1545835
30267424001 Dup
Parameter Units Result 'Result RPD Qualifiers
Percent Moisture % 0.36 0.23 44 D6
SAMPLE DUPLICATE: 1545836
30267340002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 3.1 2.9 9
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC.
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Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 436150
QC Batch Method: EPA 1010A
Associated Lab Samples: 92402231001
SAMPLE DUPLICATE: 2399888
Parameter
Flashpoint
QUALITY CONTROL DATA
Analysis Method: EPA 1010A
Analysis Description: 1010 Flash Point, Closed Cup
2610179001 Dup
Units Result Result RPD Qualifiers
deg F >200 >200
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 434620 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92402231001
SAMPLE DUPLICATE: 2393164
Parameter
pH at 25 Degrees C
92401650001 Dup
Units Result Result RPD Qualifiers
Std. Units 7.8 7.8 0 H6
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 316374
QC Batch Method: SW-846 7.3.3.2
Associated Lab Samples: 92402231001
METHOD BLANK: 1543844
Associated Lab Samples: 92402231001
Parameter
Cyanide, Reactive
QUALITY CONTROL DATA
Analysis Method: EPA 9014
Analysis Description: 733C Reactive Cyanide
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/kg ND 1.0 10/11/18 23:18
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1543845
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide, Reactive mg/kg 99.3 ND 0 0-8
SAMPLE DUPLICATE: 1543846
30267429001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg ND ND
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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/Jr ..
�aCum AnalyticaI
www.pacelabs.com
Project: Full TCLP October
Pace Project No.: 92402231
QC Batch: 316373
QC Batch Method: SW-846 7.3.4.2
Associated Lab Samples: 92402231001
METHOD BLANK: 1543839
Associated Lab Samples: 92402231001
Parameter
Sulfide, Reactive
QUALITY CONTROL DATA
Analysis Method: SM4500S2F-00
Analysis Description: 734S Reactive Sulfide
Matrix: Solid
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/kg ND 10 10/11/18 22:41
LABORATORY CONTROL SAMPLE: 1543840
Parameter Units
Sulfide, Reactive mg/kg
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 43.7 22 0-52
SAMPLE DUPLICATE: 1543841
30267429001 Dup
Parameter Units Result Result
Sulfide, Reactive mg/kg ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALIFIERS
Project: Full TCLP October
Pace Project No.: 92402231
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at, or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H6 Analysis initiated outside of the 15 minute EPA required holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/22/2018 04:41 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 40

Pace Analytical Services, LLC
m 9800 Kincey Ave. Suite 100
aceAnalyical Huntersville, NC 28078
www.pacelabs.com [phone]
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Full TCLP October
Pace Project No.: 92402231
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92402231001
Full TCLP & CRI October
EPA 3510C
435104
EPA 8081 B
435353
92402231001
Full TCLP & CRI October
EPA 3010A
434884
EPA 601 OD
434972
92402231001
Full TCLP & CRI October
EPA 7470A
434885
EPA 7470A
434895
92402231001
Full TCLP & CRI October
EPA 3510C
435661
EPA 8270D
435792
92402231001
Full TCLP & CRI October
EPA 8260B
435182
92402231001
Full TCLP & CRI October
ASTM D2974-87
316809
92402231001
Full TCLP & CRI October
EPA 1010A
436150
92402231001
Full TCLP & CRI October
EPA 9045D
434620
92402231001
Full TCLP & CRI October
SW-846 7.3.3.2
316374
EPA 9014
316408
92402231001
Full TCLP & CRI October
SW-846 7.3.4.2
316373
SM4500S2F-00
316407
Date: 10/22/2018 04:41 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 40

Document Name:
Document Revised: February 7, 2018
�.�aceklalytkal-
Sample Condition Upon Receipt(SCUR)
Pagel oft
Document No,:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilleoi' Raleigh❑ Mechanicsville❑
ConditionClient Name:
tr Project# ' Imo®# ' 924 1
'
Courier: ❑F� d Ex ❑UPS ❑USPS ❑Client
❑ Commercial peace ❑Other:
'92402231
—•Custedy-Se"resent?—❑Yes C2o----3ealsIntact?---Dyes - -12No ! jI
Date/initials Person Examining Contents:'
Packing Material: ❑Bubble Wrap ©Bubble Bags ' []None ❑ Other
Thermometer
�J Gun ID:
92 TO45 Type of ice: det ❑Blue
Cooler Temp (`C): (;> . Z Correction Factor: Add/5ubtract (°C)
Cooler Temp Corrected (•C):
USDA Regulated Soil (MN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
FlyPs r—INn
Biological Tissue Frozen?
❑None ❑Yes ❑No MN/A
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source (internationally,
Comm ents/Dlscrepancy:
Chain of Custody Present?
❑No
❑N/A
1.
�,[�
Samples Arrived within Hold Time?
I,tlYes
❑No
❑N/A
2.
Short Hold Time Analysis (e72 hr.)?
[]Yes
(]No
❑N/A
3.
Rush Turn Around Time Requested?
❑yes
No
❑N/A
4.
Sufficient Volume?
Yes
[]No
[]N/A
S.
Correct Containers Used?
y/e33
❑No
❑N/A
6.
-Pace Containers Used?
G es
❑No
❑N/A
Containers intact?
0 es
[]NO
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑yes
[]No
/A
8.
Sample Labels Match COC?
��es
[]No
❑N/A
9.
-includes Date/Time/ID/Analysis Matrix:
c�
Headspace in VOA Vials (>5-6mm)?
❑Yes
[]NO
�-
©N/A
10.
Trip Blank Present?
❑Yes
❑No
�WA
11.
Trip Blank Custody Seals Present?
❑Yes
❑No
❑ /A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Field Data Required? ❑Yes []NO
Project Manager SCURF Review: Al Date:
Project Manager SRF Review: Y'l1 1' I VD Date: I )
Page 23 of 40

Document Name:
Document Revised: February 7, 2018
a
.� aeeAnaiyfieal
Sample Condition Upon Recel t(SLUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev,06
Pace Carolinas QualRy Office
*Check mark top half of box if pH and/or dechlorination is project #j ` W�4022
verified and within the acceptance range for preservation tiT'
samples. it PM: AMB Due Date:,,' 10%18/,18
Exceptions: VOA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, U.Hg CLIENT: 92—Veo 1 i a- WA
**Bottom half of box is to list number of bottle
V
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification t)mce ii.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 24 of 40

-aceAnalytical
ANALYTICAL REPORT
National Center for Testing & Innovation October 22, 2018
Pace Analocal - Huntersvllle, NC
Sample Delivery Group: L1032792
Samples Received: 10/09/2018
Project Number: 92402231
Description: FULL TCLP OCTOBER
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By: J �
Nancy McLain
Project Manager
Results relate only to the Items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
Is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
,
N

P
'aceAnalytical "
Section A
i g
Required Client Information:
Re
Company: Veolia Water
Re
Address; 3200 20th Avenue SE
I Cc
Newton, NC 28658
mail To; Daui sDencet-6yeolia com
Pu
I Ord
?hone: 828-465-1401
Fax [phone]
Pro
Requested Std
Prdj
)ua DaterrAT: I
Section D va:d M.tr, Cad,-
Required Criant Intarination /.I TRIX
I
40DE
SAMPLE ID �m
r
(A-z, as 1,)
4
w
Sample IDS MUST BE UNIQUEA
Compost full TCLP
S.A.R.
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
ection B Section C
quired Project Information: Invoice Information:
port To: Paul Spencer Attention: Paul Spencer
PyTo: Leaan HuchesOveolia Company Name:
Address:
CC On file Pace Quote Reference:
er No.:
jeet Name: Full TCLP October Pace Project Manager. Angela Bz
a COLLECTED - W
o n>o az uw
L; ul © coMPo51TE CCLIG SITE W OU .��.
¢ a ¢ START ENDIGRAB 2 J U
s w UK N O
DATE TIME DATE TIME
SL C 10/4118 7:30ALI 10/4118 7:30AM 7 rI'
41 10/4118 7:30AM 10/4/18 7:30AM 3 /
1014118 7:30AM 1(Y4/18 7:30AM ✓ /
Page: 1 of j
e-
NPDES F GROUND WATER F DRINKING WATER
I UST I- RCRA X OTHER IUP
GA i IL r IN I MI X NC
c e F- OH f SC r WI I- OTHER
Itered (YIN)
An;
W ti �' •� b 4a Eg S �' �U C
v, a
c.1
0 Pace Protect No.
r Lab LD,
• SAMPLE CONDITIONS
1014118 .2 3 r } y
z z z
3;1371
z z z
} > y
01-7
C � �
O p
PRINT Name of SAMPLER: V o c
ICt7R NUL KGS CL u a
SIGNATURE of SAMPLER: C.-TE signed U w fi
✓ I _ / Do l rrJ; 10/4/18 W
e-File(ALLQ020rev.4, 29 Mar06) 22J u n 2005
0
LO
C4
0)
CA
f9
0_
a COLLECTED - W
o n>o az uw
L; ul © coMPo51TE CCLIG SITE W OU .��.
¢ a ¢ START ENDIGRAB 2 J U
s w UK N O
DATE TIME DATE TIME
SL C 10/4118 7:30ALI 10/4118 7:30AM 7 rI'
41 10/4118 7:30AM 10/4/18 7:30AM 3 /
1014118 7:30AM 1(Y4/18 7:30AM ✓ /
Page: 1 of j
e-
NPDES F GROUND WATER F DRINKING WATER
I UST I- RCRA X OTHER IUP
GA i IL r IN I MI X NC
c e F- OH f SC r WI I- OTHER
Itered (YIN)
An;
W ti �' •� b 4a Eg S �' �U C
v, a
c.1
0 Pace Protect No.
r Lab LD,
• SAMPLE CONDITIONS
1014118 .2 3 r } y
z z z
3;1371
z z z
} > y
01-7
C � �
O p
PRINT Name of SAMPLER: V o c
ICt7R NUL KGS CL u a
SIGNATURE of SAMPLER: C.-TE signed U w fi
✓ I _ / Do l rrJ; 10/4/18 W
e-File(ALLQ020rev.4, 29 Mar06) 22J u n 2005
0
LO
C4
0)
CA
f9
0_
Page: 1 of j
e-
NPDES F GROUND WATER F DRINKING WATER
I UST I- RCRA X OTHER IUP
GA i IL r IN I MI X NC
c e F- OH f SC r WI I- OTHER
Itered (YIN)
An;
W ti �' •� b 4a Eg S �' �U C
v, a
c.1
0 Pace Protect No.
r Lab LD,
• SAMPLE CONDITIONS
1014118 .2 3 r } y
z z z
3;1371
z z z
} > y
01-7
C � �
O p
PRINT Name of SAMPLER: V o c
ICt7R NUL KGS CL u a
SIGNATURE of SAMPLER: C.-TE signed U w fi
✓ I _ / Do l rrJ; 10/4/18 W
e-File(ALLQ020rev.4, 29 Mar06) 22J u n 2005
0
LO
C4
0)
CA
f9
0_
0
LO
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0)
CA
f9
0_

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
I
Tc: Table of Contents
2
FID
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
E
FULL TCLP & CRI OCTOBER 1-1032792-01
5
FULL TCLP & CRI OCTOBER L1032792-02
6
[En
Qc: Quality Control Summary
7
F
Total Solids by Method 2540 G-2011
7
Metals (ICP) by Method 6010D
8
QC
Chlorinated Acid Herbicides (GC) by Method 8151A
9
Gl: Glossary of Terms
10
E
AI: Accreditations & Locations
11
rAl
Sc: Sample Chain of Custody
12
177-1
I-sc I
L---j
Page 27 of 40
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
Pace Analytical - Huntersville. NC 92402231 L1032792
10/22/18 09:30 2 of'15

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
cj
Collected by
Collected date/time
Received date/time
FULL TCLP & CRI OCTOBER L1032792-01
Solid
10/04/1807:30
10/09/1808:45
C
Method
Batch
Dilution
Preparation
Analysis
Analyst
date/time
dateltime
1177-1
'TC
Calculated Results
WG1181232
1
10/1511815:07
10/16/18 09:03
TRB
Total Solids by Method 2540 G-2011
WG1179545
1
10/12/1813:33
10/12/1813:41
KDW
Metals (ICP) by Method 6010D
WG1178849
1
10/10/1818:40
10/11/1819:40
ST
Collected by
Collected date/time
Received date/time
a
Cn
FULL TCLP & CRI OCTOBER L1032792-02
Waste
10/0411807:30
10/09/1808:45
Analyst
FMethod
Batch
Dilution
Preparation
Analysis
date/time
dateltime
Preparation b Method 1311
WG1181637
1
10/16/1814:01
10/16/1814:01
TM
_
e
E�ct
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1182653
1
10/18/1810:11
10/18/18 21:47
KLM
Page 28 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Hunlersville, NC 92402231 L1032792 10/22/18 09:30 3 of 15

CASE NARRATIVE ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
c1�
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
EChave
been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
E
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
F
bt La
F
Nancy McLain
Project Manager
El:
E
Sample Handling and Receiving
Sample quantity was not sufficient to complete analysis per recommended method guidelines for the following samples.
Lab Sample ID Project Sample ID Method
L1032792-02 FULL TCLP & CRI OCTOBER 1311
Page 29 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME:
PAGE:
Pace Analytical - Hunlersville, NC 92402231 L1032792 10/22/18 09:30
4 of 15

FULL TCLP & CRI OCTOBER
SAMPLE RESULTS -
01
ONE LAB. NATIONWIDE.
Collected date/time: 10/04/18 07:30
L1032792
Calculated Results
Result Qualifier
Dilution
Analysis
Batch
C
Analyte
date / time
z
Sodium Adsorption Ratio 1.27
1
10/16/2018 09:03
WG1181232
TC
Total Solids by Method 2540 G-2011
FsResult
Qualifier
Dilution
Analysis
Batch
Analyte %
date/time
a
Cn
Total Solids 43.4
1
10/12/201813:41
WG1179545
Metals (ICP) by Method 6010D
Result (dry) Qualifier
MDL (dry) RDL (dry)
Dilution
Analysis
Batch
F
Analyte mg/kg
mglkg
mg/kg
date / time
QC
Calcium 10300
10.7
230
1
10/11/201819:40
WG1178849
Magnesium 1670
2.56
230
1
10/111201819:40
WG1178849
FGI
Sodium 522 B
22.7
230
1
10/11/201819:40
WG1178849
Page 30 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville. NC 92402231 L1032792 10/22/18 09:30 5 of 15

N
FULL TCLP & CRI OCTOBER SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 10/04/18 07:30 L1032792
Preparation by Method 1311
Result
Qualifier Prep
Batch
Cp
Analyte
TCLP Extraction -
date / time
10116/2018 2:01:53 PM
WG1181637
Ec
Fluid 1
10/16/2018 2:01:53 PM
WG1181637
Initial pH 8.06
10/1612018 2:01:53 PM
WG1181637
s
Final pH 5.14
10/16/2018 2:01:53 PM
WG1181637
SS
Chlorinated Acid Herbicides (GC) by Method 8151A
F
Result
Qualifier RDL Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I mg/1
date / time
2,4,5-TP (Silvex) ND
0.00200 1
1
10/18/2018 21:47
WG1182653
2,4-D ND
0.00200 10
1
10/18/2018 21:47
WG1182653
(S)2,4-DichlorophenylAcetic Acid 62.4
14.0-158
10/18/201821:47
WG1182653
Fc
�GI
�AI
Fc
Page 31 of 40
ACCOUNT: PROJECT: SDG: DATEMME: PAGE:
Pace Analytical - Huntersvllle, NC 92402231 L1032792 10/22/18 09:30 6 of 15

WG1179545
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3350311-1 10/12/1813:41
MB Result
Analyte %
Total Solids 0.000
MB Qualifier MB MDL MB RDL
L1032919-01 Original Sample (OS) e Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1032792-01
(OS) L1032919-01 10/12/1813:41 • (DUP) R3350311-3 10/12/1813:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limts
Analyte % % % %
Total Solids 81.0 80.9 1 0.150 10
Laboratory Control Sample (LCS)
(LCS) R3350311-2 10/12/1813:41
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte % % % %
Total Solids 50.0 50.0 100 85.0-115
ACCOUNT: PROJECT: SDG:
i 1i I- r! - I ---1C --- I L.---7"
DATEITIME:
ONE LAB. NATIONWIDE.
Page 32 of 40
PAGE:
7 ^f l�

WG1178849
Metals (ICP) by Method 6010D
Method Blank (MB)
(Mb) H3349963-1 10/11/18 19:03
MB Result
Analyte
mg/kg
Calcium
U
Magnesium
1.41
Sodium
25.5
o ® . . ® w w m a a m m w ® _ m .- a__ --,1 0 6 F1 0 ® G G G ■ ■ ■ ■
QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
1,1032792.01
MB Qualifier MB MDL
MB RDL
mg/kg
mg/kg
4.63
100
J 1.11
100
J 9.85
100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3349963-2 10/11/1819:05 • (LCSD) R3349963-3 10/11/1819:08
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
Calcium
1000
983
1020
98.3
102
80.0-120
Magnesium
1000
1000
1040
100
104
80.0-120
Sodium
1000
990
1020
99.0
102
80.0-120
LCS Qualifier LCSD Qualifier RPD RPD Limits
3.54 20
3.88 20
3.33 20
L1O329O7-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1032907-14 10/11/1819:10 • (MS) R3349963-6 10/11/1819:18 • (MSD) R3349963-7 10/11/1819:21
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
Calcium
1000
458
1800
1670
134
121
1 75.0-125
Magnesium
1000
427
1860
1680
143
125
1 75.0-125
Sodium
1000
57.1
1040
958
98.8
90.1
1 75.0-125
MS Qualifier MSD Qualifier RPD RPD Limits
J5 7.55 20
J5 10.0 20
8.65 20
Page 33 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 1 tn21)70� -- _ _._

WG1182653
Chlorinated Acid Herbicides (GC)
by Method 8151A
Method Blank (M13)
(MB) R3352283-1 10/18/18 20:52
MB Result
MB Qualifier MB MDL
Analyte mgll
mg/I
2,4-D U
0.000667
2,4,5-TP (Silvex) U
0.000667
(S) 2,4-Dichlorophenyl Acetic 58.0
Acid
QUALITY CONTROL SUMMARY
L1032792-02
MB RDL
mg/I
0.00200
0.00200
14.0-158
Laboratory Control Sample (LCS) o Laboratory Control Sample Duplicate (LCSD)
(LCS) R3352283-2 10/18/18 21:19 - (LCSD) R3352283-3 10/18/18 21:33
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/1
%
%
%
2,4-D
0.0500
0.0394
0.0385
78.8
77.0
50.0-120
2,4,5-TP (Silvex)
0.0500
0.0378
0.0364
75.6
72.8
50.0-125
(S) 2,4-Dichlorophenyl Acetic
75.8
68.4
14.0-158
Acid
LCS Qualifier LCSD Qualifier RPD
2.31
3.77
L1033739-01 Original Sample (OS) • Matrix Spike (MS) , Matrix Spike Duplicate (MSD)
(OS) L1033739-01 10/18/18 22:41 • (MS) R3352283-4 10/18/18 22:14 • (MSD) R3352283-5 10/18/18 22:27
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/1
mg/1
mg/l
mg/l
%
%
%
2,4-D
0.0500
ND
0.0766
0.0697
153
139
1 50.0-120
2,4,5-TP (Silvex)
0.0500
ND
0.0424
0.0337
84.8
67.4
1 50.0-125
(S) 2,4-Dichlorophenyl Acetic
88.2
80.8
14.0-158
Acid
ACCOUNT: PROJECT: SDG:
i A Iii 1 's r- -- p---I 1 1-- -7P'
RPD Limits
20
20
MS Qualifier MSD Qualifier RPD
J5 P J5 P 9.43
J3 22.9
DATF/TIME:
1-1/10 -:?v
ONE LAB. NATIONWIDE. *
RPD Limits
o�
20
20
Page 34 of 40
PAGE:
o ..v1q

GLOSSARY OF TERMS ONE LAB, NATIONWIDE. L
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit
MDL (dry) Method Detection Limit
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
u
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier Is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or'BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J3 The associated batch QC was outside the established quality control range for precision.
J5 The sample matrix interfered with the ability to make any accurate determination; spike value is high.
P RPD between the primary and confirmatory analysis exceeded 40%.
Page 35 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92402231 L1032792 10/22/18 09:30 10 of 15

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capabilityfrom our single location laboratoryis comparable to the collective totals of the network
laboratories in our Industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report-
" Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Acci editations
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZ0612
New_Hampshlre
2975
Arkansas
88-0469
New_J_ersey—NE_LAP
TNO02
California
2932
New Mexico'
—
n/a
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
EB7487
North Carolina'
DW21704_
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohlo—VW
CL0069
Illinois
200008
Oklahoma
9915
Indiana_
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68_-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky"
90010
South Carolina
84004
Kentucky
16
South Dakota
nla
Louisiana
A130792
Tennessee14
2006
Louisiana'
LA180010
Texas
T 104704245-1.7_-14
_
Maine
TN0002
_
Texas'
LABO152
Maryland
324
Utah
TN00003_
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN000_0.3_
West Virginia_
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
Third Party Federal Accreditations
A2LA_— ISO _17025 1461:01 AIHA-LAP,LLC EM_LAP 100789
A2LA— I_SO.1702_5' 1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA—Crypto TN00003
' Drinking Water I Underground Storage Tanks 'Aquatic Toxicity 4 ChemicaUMicrobiological 'Mold 'Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
NI E
MT ND
OR
IN
J
SD WI J ( �r, NY�
` . OH
IT
VA
1 OA \` _ KS r�t0 -'�KY
1 4,
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l AL GA
{ I
TX t LA
AK
FL
HI\
Page 36 of 40
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville. NC 92402231 L1032792 10/22/18 09:30 11 of 15

Grain of Custody F050
�AaceAnaocal
p
Workorder: 92402231 Worltorder dame: Full TCLP October
-
#; c _ - - - - St+hc�.tiftrct�Tia".-= -- - - - �:-•,
-_,,-^i
ry
--s
-
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Angela Baioni
•tau
face -Analytical Charlotte Rb ` lll•
9800 Kincey Ave. Suite 100
Hunlersville,NC 28078
Phone [phone]
Email: angeia.baionl(gpaceiabs.com Y AAA - , ,-f; + 3-11 2 ,
1—n—)
t, ci-� 1 �
State of Sample Origin: NC p'cesrvoCtz7itatiHf :.i
"'tt�{rt.
•sW.� t�'�iJ 1 - -
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10Idf2018 07:30
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Recei/vieved y �DatelTtme
�yt�.,� ,,-�/
2
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7
1 Cooler Temperature on Receipt °C Custod Seal Y or r
Received on Ice or N
Samples Intact
11 or N
RIND SCREEN' <0.5 MPJhr
FMay. OcItobw 05. ,'.+,) ;3 1.04;32 I'M FMT-ALL-C-002rev.00 ?_ brch?009 Page 37j of,40

sting
PaceAnalytical National r
L Innovation
Cooler Receipt Form
:t�uler Received/Opened On: 10/ 41 ! t $
Temperature:
Received By: Alemandrt lvlurt.augh
_- -
Signature: �A-V�' /,Y°
_
-- --
Receipt Check list
NP Yes No
COC Seal Present / Intact?
r
COC Signed / Accurate?
Bottles arrive intact?
Correct: bottles used?
�
Sufficient volume sent?
if Applicable
VOA Zero headspace?
Page 38 of 40

Chain of Custody
ce
'v1ww4*wIsb&=ff
Workorder: 92402231 Workorder Name: Full TCLP October Results Requested By: 10/1.8/2018
Angela Mont
PaceA:n'alytical,Charlotte
P.O. Pwb II-;-;T-GI-,-I'
9406 Kincey Ave. Suite 100
Huntersville, NC 28078
= =
(D
CC
-2
'Phone [phone]
Email; angela.balonigpacelabs.
6 I-TI-) 3-1 122-
State of Sample Origin: NC
resbNed.,Con 'kekg�,
I
ci
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Item
'AFampte 16
130F
LAB USE ONLY
1
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1
10/4/2018 07:30
92402231001
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2
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Transfers
Released By
I
DateMme
Received By
Date/Time
2
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Cooler Temperature an RecVjpt
a T - -,c
custody Seal Y or (N'
Received an Ice or N
Samples lhtact or N
PAD SCREEN: <0.5 mR/hr
Friday, October 05, 2018 1:04:32 P FMT-ALL-"02rev.00 24lvIarch2009 Page 1 of 1
11 Page 39 of 40

Pace A-halytical National
CoolerReceiptForm
Client:Z�
Center fo
SDG#
Cooler Received/Opened On: 1044�18
Temperature:
Received By: malik tisdale
Signature: %y
Receipt Check List
NP
Yes
No
COC Seal Present / Intact?
r
COC Signed / Accurate?
Bottles arrive intact?
Correct bottles used?
t
Sufficient volume sent?
If Applicable=
VOA Zero headspace?
Preservation Correct IMe&Wl-:
Page 40 of 40

EXHIBIT 5
NC State Laboratory Certification
23

Certificate No. 5466
STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
LABORATORY CERTIFICATION BRANCH
In accordance with the provisions of N.C.G.S. 143-215.3 (a) (1), 143-215.3 (a)(10) and NCAC 2H.0800:
Hickory Regional Compost Facility
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DEQ for'
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations,
By reference 15A NCA C 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,.
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until 12/31/2018
Dana B. Satterwhiteti _w,1

Cure Pad 'Temperatures
23

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
Cure Pile Temperatures - January 2018
COMPOST CURING - PILE TEMPERATURES
ROW 1
ROW 2
ROW 3
ROW 4
ROW 6
ROW 6
DATE
Cure Row Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Row
4 -East 4 West
Cure Row Cure Row
5 East 5 West
Cure Row Cure Row
6 -East 6 -West
January
U E, - F '
;A B ; .G ':`M E =. F
A . B .. G _ ' D; . E- ,'F'•
A - B C ; ,D- E: F
A _ B C D_ E : F
A B C ':•-, D --E - F,,
01/01/18
01/02/18
67
64
62 ; 65
68
64
57
62
61 61
62
59
01/03/18
61
65
64 ; 68
71
70
58
61
60 61
62
60
01/04/18
•.
66
63
65 62
68
70
56
57
61 63
62
57
01/05/18
58
61
641 65
67
64
F
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01106/18
01/07/18
01/08/18
61
64
61 61
61
58
01/09/18
64
68
61 62
61
62
01/10/18
65
68
66 ; 63
68
62
01/11/18
64
66
60 66
63
62
01/12/18
01/13/18
01/14/18
s
66
67
64 ; 66
65
65
I
01/15/18
69
66
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62
66
01/16/18
66
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69
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01l17/18
68
66
66 67
65
65
01/18/18
68
67
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01/19/18
'•
69
67
64 ; 66
67
69
01/20/18
-
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01/21/18
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01/22/18
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01/23/18
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01/25/18
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01/26/18
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01/28/18-
01/29/18
70
76
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01/30/18
70
74
72 73
58
01/31/181
1
174
75
70 73
70

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
Cure Pile Temperatures - January 2018
COMPOST CURING - PILE TEMPERATURES
ROW 7
ROW 8
ROW 9
ROW 10
ROW 11
ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
Cure Row Cure Row
8 -East 8 -West
Cure Row Cure Row
9 -East 9 -West
Cure Row Cure Row
10 -East 10 -West
Cure Row Cure Row
11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
January
A B C D E', F.
A B C- -D E F
A B C D E F
A B C D E F
A B, �C- D E F
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01/01/18
01/02/18
74
70
71 67
01/03/18
!
70
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69 1 71
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01/04/18
72
70
70 1 74
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01/05/18
57
70
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69 73
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01/06/18
01 /07118
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01 /08118
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60 61
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01/09/18
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01/10/18
66
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01/11/18
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01 /12/18
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01 /13/18
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01/15/18
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01/16/18
47
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01/17/18
42 51
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01/18/18
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01/23/18
79
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01/24/18
78
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01/25/18
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01/27/18
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01/28/18
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01/29/18
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01/30/18
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01/31/18
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1 71
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1 68
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71

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures - February 2018
COMPOST CURING - PILE TEMPERATURES
ROW 1
ROW 2
ROW 3
ROW 4
ROW 6
ROW 6
DATE
Cure Row Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East T 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure! Row Cure Row
4 -East 4 -West
Cure Row Cure Row
5 -East 5 -West
Cure Row Cure Row
6 -East 6 -West
February
A: E�­'6
A B d D E
%,;B --E
C r';*_'D�' F:
A B_ J�D, Ef
,:B' C D
z,E
02/01/18
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70
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02/02/18
57
55 1
76
75
73 2
75
73
02/03/18
0 2/04/18
02/05118
75 76 74 70
71
74
72 69
74
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02/06/18
40
45
75773
70 1 71
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69
71
69
67 67
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02/07/18
74
75 1
77
78
76 73
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66 1 64
73
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02/08/18
64
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02/09/18
76 74 65 60
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02/11/18
02/12/18
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02/13/18
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02/14/18
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02/15/18
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02/16/18
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02/17/18
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02/20/18
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02/21/18
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02/26/18
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75
76
66
64
77
69
65
71 70 74
70 f 71 74
68 73 74
72
65
73
74
F
70
I
69 170
N I
69
S
67
H
73
F
75
I
71 70
N l I
70
S
68
H
02/28118

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
r"— oila rA ar9/Ilrac - FahmAry 2018
COMPOST CURING - PILE TEMPERATURES
ROW 7
ROW 8
ROW 9
ROW 10
ROW 11
ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
Cure Row Cure Row
8 -East 8 -West
Cure Row Cure Row
9 -East 9 -West
Cure Row Cure Row
10 -East 10 -West
Cure Row Cure Row
11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
February.
A B C D: `_E F ,
A B- -C_ D ,_ E F.
A B- -C D- - E F
A- B C--€ M - _,E F-
._ A - B C• , D E :F
�A__ .B,- -, C ° _D --E_ _F.
02/01/18
71
70 71 :`' 67
71
73
63
69
64 68
72
69
02/02/18
71
73 i 76 67
70
72
69 ,
67
64 65
69
70
02/03/18
F-
1
N 1
S
H
I
I
I
I
02/04/18
_
02/05/18
60
66 69 68
72
70
02/06/18
70
73 69 1 68
71
67
02/07/18
66
63 65 69
72
70
02/08/18
70
72 69 73
71
68
02/09/18
67
70 69 ' 67
71
69
02/10/18
02/11/18
02/12/18
63
65 68 62
64
65
02/13/18
73
70 69 € 68
65
65
02/14/18
02/15/16
F
I N I
S
H
02/16/18
02/17/18
I
02/18/18
02/19/18
02/20/18
02/21/18
02/22/18
02/23/18
02/24/18
I
02/25/18
I
1
I
EE
02/26/18
-
02/27/18
02/28/18

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
Cure Pile Temperatures - March 2018
COMPOST CURING - PILE TEMPERATURES
ROW 1
ROW 2
ROW 3
ROW 4
ROW 5
ROW 6
DATE
Cure ROW Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Row
4 -East 4 -West
Cure Row Cure Row
5 -East 5 -West
Cure Row Cure Row
6 -East 6 -West
March
A B C' D E F..
A B C `� D E- F,
A -B , C D: �' E F'
A -• B C D E F
A' B C `:. � D E' `F
A B 'C ':- D_ E- F
03/01/18
75
71
73 60
73
75
71 72
77
74
69
65
63 1 69 69
71
03/02/18
73
75
72 '•. 51
45
75
78
72 73
79
71
70
69
66 1 69 72
67
03/03/18
F
1
N I S
H
_
03/04/18
03/05/18
77
75
73 69
75
71
75
--A
72 70
74
68
03/06/18
73
75
71 . 74
73
69
73
70 70
73
71
03/07/18
70
77
71 70
76
]73
65
67
68 62
67
62
03/08/18
67
73
70 71
73
64
72
70 69
73
70
03/09/18
63
74
71 ' 73
74
72
63
71
70 69
74
72
'
03/10/18
—^�-
03/11/18
03/12/18
66
69
67 7576
74
62
68
69 67
69
68
03/13/18
63
68
66 76
79
71
66
66
70 i 65
66
64
03/14/18
61
64
62 69
73
71
67
71 63
62
6403/15/18
71
77
72 71
74
76
r6l
I
N I
S
H
03/16/18
69
73 °
70 73
74
71
03/17/18
03/18/18
I
—
03/19/18
63
67
66 73
70
69
03/20/18
62
66
61 1 74
71
67
03/21/18
63
68
62 77
73
72
03/22/18
61
64
61 72
74
70
03/23/18
60
65
63 [ 72
71
70
03/24/18
�J
F
I
N 1
S
H
03/25/18
03/26/18
03/27/18
03/28/18
03/29/18
03/30/18
03/31/18
—��—
I
f
�
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��
I
I
I
I
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I
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I

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
t,_. oa- m.—h gniR
DATE
Cure Row Cure Row
7 -D 7 -West
Cure Row Cure Row
Cure Row
8 -East 8 -West
8 -East
. Cure Row Cure Row
9 -East 9 -West
Cure
Cure Row Cure Row
10 -East 0 -West
Cure Row Cure Row
. 11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
March
�A B C, D E F
C
A 13 C D E F
AF13
A B C D E F
A B C F EY -E F
A B C D E F-
A B C D E F
03/01/18
03/02/18
03/03/18
03/04/18
F`
03/05/18
73
03/06/18
70
03/07/18
60
78
03/08/18
45
72
74 44
03/09/18
72
75
79 50
03110/18
03/11118
03/12/18
76
78
73 77
72
03/13118
40
77
75
74 77
78
65
03/14/18
51
75
76
73 78
77
75
03/15118
53
72
76
79
74 76
77
73
03/16/18
59
72
77
78
74 77
76
74
03/17/18
— —
------------------
03/18/18
03/19/18
67
70
71
73
75 72
74
75
03/20/18
45
66
61
69
70
76 70
76
71
03/21/18
68
73
71 44
71
73
70 71
72
74
03/22118
70
72
75 68
72
71
68 1 70
73
72
03/23/18
72
73
71 62
45
72
71
70 69
73
71
03/24/18
03/25/18
03/26/18
68
70
73
69 71
74
70
69
72
6
70 8
70
72
03/27/18
65
70
74
72 71
70
73
68
75
69 67
69
70
03/28/18
63
69
75
71 68
72
74
67
70
71 65
71
69
03/29/18[±50
73
71
74
72 74
77
72
66
70
68 70
73
68
03/30/18
03/31/18

VEOLIA WATER.NO.RTH AMERICA OPERATING-BERVICES, INC...
REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures - April 2018
COMPOST CURING ;PILE TEMPERATURES
ROW I
ROW 2
ROW 3
ROW 4
ROW 5
ROW 6
Cure Row I Cure Row
I -East I -West
Cure Row Cure Row
2 -East 2 -West
R Cure
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Row
4 -East 4 -West
Cure Row Me Row
5 -East Cure
5t-West
Cure—Ro—w—F.—Cure Row
6 -East 6 -West
[-AtB
April
A B C D7 It' 'F
-A B C E' F,
A B C D E F-
'--A Ei-- C D E F
:A B C D E F
C
C D- E 0
04/01118—
T
04102/18
04/03/18
04/04/18
04/05118
-
- - ---------
04/06/18
04/07/18,
04/08/18
04/09/18
70
04/10/18
04/11/18
45
70
04/12/18
41
72
04/13/18
65
77
79 56
04114/18
---------------
04/,5/,8
04/16118
63
71
74 73
75
1
04117/18
72
74
71 78
75
04/18/18
1
40
73
74 77
73
67
04/19118
74
75 1
71
71
7 78
75
75
04/20/18
70.
73
70
70
76 75
74
70
04/21/18
04/22118
04/23118,
75
73
70 77
76
74
75
73 75
72
75
04/24/18
78
76
78
75
70 75
78
76
71
76
70 73
70
76
04/25/18,
65
71
76
73
71 77
76
74
.70
74
71 74
72
75
04/26/18
04/27118
60
55
58
7.2
70
171
73
73
74
70 74
65 = 74
72
75
75
*73
72
70
73
75
72 72
71 73
74
71
71
71
0 4/28118
04/29/18
04/30/18
-75
72
77 80 72
69
71
70 77
70
69
68
69
70 K 73
65
73
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715 11 73
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VEOLU9a_ ATE MORTH AMERICA OPERATING SERVICES, INC;
REGIONAL COMPOST FACILITY - HICKORY, NC
Cure Pile Temperatures.- May 2018
COMPOST CURING. PPLE TE PERATURES
ROW I
_R=1
ROW 2
ROW 3
ROW 4
ROIN 6
ROW 6
DATE
Cure Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row
4 -East
4 -We
Cure RJFA
ure Row
-East
Cure Row
5 -West
Cure Row
6 -East
Cure Row
6 -West
May
A B C D E F
A B:-C D E F
A B C D E F
A B C'
D E
B
C
':. -D
E F
A
B
C
D
"E F
05/01/18
I
74
74
75
71 7368
66
':71
64
70
60
65
70
73
65
69
05/02/18
75
71
73
75
71
72 7670
69
70
69
71
64
67
71
70
66
70
05/03/18
78
76
74
77
72
75 7968
66
70
60
66
68
60
65
72
68
65
05l04l18
73
75
69
70
71 ':.
75 74
77
70
67
65
76
58
174
68
63
72
70
65
69
05/05/18
05/06/18
i
I
05l07/18
78
76
80 59
70
76
81 74 76
73
68
65
66 7770
70
66
73 69
67
70
05/08l18
67
75
71 70
66
73
72 7475
71
65
69
65 7369
[14651
65
66
73 70
68
71
05/09/18
I
65
75
73 78
65
73
72 75 73
69
63
70
60 7063
63
65
70 i 72
68
69
u5/10/18
05/11/18
;
78
75
76
75
75 80
77 81
78
76
74
69
70
75
73
74 ':. 76 73
75 74 75
74
73
60
58
L63
F62
1 58 ; 64
F591 60
57
65
65
72
F
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S
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05/12/18
i
05/13/18
'
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06/14/18
55
58
169 `
70
75
73 70
73
1751
64
74
72 ' 72 70
75
70
64
68 61
59
60
05/15/18
69
71
73 58
51
73
74
76 s 72
76
74
59
71
68 74 71
77
60
59
62 68
61
62
05/16/18
68
72
73 70
71
69
70
71
70 70
74
71
62
73
70 ' 71 73
72
F
I
N I
S
H
05/17/18
69
71
70 71
72
74
70
73
74 72
73
70
67
74
71 73 71
70
05/18/18
68
67
F72 ' 70
68
69
70
74
74 73
71
69
68
71
70 72 71
72
_
05/19/18
05/20/18
05/21/18
73
80
72 70
75 1
71
71
72
70 73
77
72
67
70
68 1 72 71
69
05/22/18
72
81
74 73
74
70
73
74
71 72
75
74
68
69
71 70 73
74
05/23/18
71
80
75 75
73
71
70
72
76 1 76
71
74
F
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N I S
H
05/24/18
68
77
78 73
75
70
73
76
77 74
73
70
05/25/184
70
75
77 70
71
73
70
76
79 71
74
69
05/26/18
05/27/18-
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05l28/18
05/29/18
66
70
74 1 64
69
70
68
70
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05/30/18
68
73
62 67
69
72
70
71
72 73
05/31/18
••
70
73
68 70
73
71
65
69
70 75
I

VEOUA WATER NORTH AMERICA OPERATING SERVICES, INC.
-REGIONAL-•COMPOST FACILITY --HICKORY, NC -
Cure Pile Temperatures e May 2018
COMPOST CURING - PILE TEMPERATURES
NINE
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VEOLIA WATER WORTH AMERICA. OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, NC
Cure Pile Temperatures - June 2018
ROW I
`—Cure
WINFUUT GURIJVU:-
PILE TEMPERATURES
ROW 2
ROW 3
ROW 3
ROW 4
ROW 5
ROW 8
DOE—
Row Cure Row
1 -East I -West
Cure' Cure Row
2 -East 2 -West
ow Cure Row
'w
Cum -East _T 3-West
3 -Ea' t
Cure Row Cure Row
Cure ow
4 -East 4 -West
-West
Cure I
Cure Row
5 -East Me Row
5 -West
rA
Cure Row Cure ow
6 -East 6 -West
June
06/01/18
E' Fj
B `E F
6 6
66 74 65 75 75 74.
C
A B C I D E F
D E F�
64 66 69 78 70 63
9
6 . 8 70 63
A F
A 8 C 0 E' F'
B
A B C,,f, D 9,_ F
— A �B C 0 E
06/02il8
06/03/18
[69
06/04/18
9
69
72
76 i 74
72
69
66
69
69 75
74
69
06105118
0
70
7b
72 75
71
70
67
70
72 1 72
74
71
06/06/18
70
71 73
74
73
F
I
N I I
S
H
06/07/18
74
70
67 73
74
70
6/08/18 0
60
68
61 68
72
71
06/09/18
F
I
N 1
S
H
06/10/18
06/11118
06/12/18
06/13/18
06114/18
06/15118
06/16/18
06/17/18
06/18/18
06/19/18
06120/18
06/21/18
061221T8
06/23118
06124/18
06/25/18
06/26/18
06/27/18
I
II
06/28/18
06/29/18
06/30/18

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-

VEOLIA WATER WORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures:- July 2018
COMPOST CURING - PILE TEMPERATURES
11
ROW I ROW 2 ROMIR nnifil d -
DATE
Cure Row Cure Row
Cure Row Cure —Ro W
Cure Row Cure
Cure Row Cure _W0_w
Cure Row Cur Row
Cure Row`vyY Cure Row
I -East I -West
2 -East 2 -West
3 -East
4 -East 4 -West
5 5 -West
6 -West
July
A B C D E F
A`:'B C D E F
A B C D E F
- 7D
�A' B C D E F'
A B C­-D E V
A 8 C
A R C D' E F
0 0 01
7/ /18 7/01/18
07/02/18
53
52
53 58
56
59
74
07/03/18
55
56
57 1 58
56
58
71
74
07/04/18
07/05/18
56
59
61 57
60
59
73
76
07/0 6/18
55
56
53 55
54
51
80
8
07/07/18
07/08118
07/09/18
53
51
49 47
53
52
76
79
80 65
07110/18
F
I
N I I
S
H
78
80
77 75
70
07/11/18
R
E
S T
A
K
81
85
84 80
72
0711211
82
83
81 78
79
63
07/13/18
I
I
59
70
73
77 74
73
78
07/14/18
07/15/18
07/16/18
77
76
71
78 78
83
81
07/17/18
70
80
74
73
75 71
80
78
07/18/18
i
65
70
73
71
70
74 75
76
75
07/19/18
67
63
75 1 60
70
71
77 73
78
75
07/20/18
50
74
76
79 77
80
76
71
71
77 71
77
76
07/21118
07/22/18
07/23/18+
49
76 1
72
71
79 73
78
72
73
74
74 74
69
75
07/24/18
46
751
79 1
76
71
77 76
81
70
76
81 78
72
70
07/25/18
73
73
79 60
77
79
76 78
80
H77
70
0
5
75
76 74
69
74
07/26/18
75
77
75 6
73
71
76 72
77
8
78
75
71
74 1 7.5
76
71
07/27/18
55 1 I
77
74,1
74 s. 69- 55
57
75
77
74 1 75
78
76
73
70
75 74
73
72
07/28/18
07/29/18
07/30/18
----------
71
81
.80 65
73.1
75 1
78 76� 79-
.71
I 72
75
70 77
74
71
70
75
71 70 1
72 1
731
07/31/18
r:
73
80
79 76
74
0
76 1
77
L8 =j73 80
75
77
75
71
73
70 1
73 1
70 74
76 1
73

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
"REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures f. July 2018
COMPOST CURING = PILE TEMPERATURES.
ROUV 7
ROW 8
ROW 9
ROIN 10
ROW 11
ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
Cure Row Cure Row
8 -East 1 8 -West
Cure Row Cure Row
9 -East 9 -West
Cure Row Cure Row
10 -East 10 -West
Cure Row Cure Row
11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
Jul
A B -C D E F
A B C j D E F
A B C D E F
A E F
A B G D El F.
A B' F
07/01/18
07102/18
76
77
81 75
73
79
70
74
73 78 1
73 1
721
1
07/03/18
73
68
72 70
76
69
65
69
71 67
67
71
07/04/18
7j//18
0 /0 5
76
79
68 77
73
78
68
64
6 65
66
67
7/ 6/ 8
0 /0 /1
74
76
73 70
61
75
71
73
69 72
70
0
64
64
07/07/18
07/08/18
07109/18
71
77
73 75
70
740
69
71
73 71
7674
76
0
70
07110/18
73
76 1
72 1 7
73
76
70
74
71 71
74
76
07/11/18
74
75
77 79
70
80
3
70
72 69
73
76
07/1-2/18
71
77
79 1 77
71
80
:7 0
71
72 70
167
69
07/13/18
71
68
64 71
71
72
07/14/18
07/15118
07/16/18
70
69
77 77
72
75
07/17/18
71
68
70 73
74
71
07/18/18
69
71
65 71
72
74
07/19118
71
70
73 75
73
77
07/20118
69
72
73 72
71
74
07/21/18
07/22/18
07/23/18
i4l07/24/18
07/25/18
07/26/18
07/27118
07/28/18
F

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REMONAL COM069T FAdlLi-Ty, i idkdRv, mC
Cure Pile Temperatures - August 2018
COMPOST CUR/A!G a PILE TEMPERATURES
ROW 1 ROW 2
ROW 3
ROW 4
ROW 5
R®!ftl 6
DATE
Cure Row Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row '
3 -East 3 -West
Cure Row Cure Row .
4 -East 1 4 -West
Cure Row Cure Row r
5 -East 1 5 -West :
Cure Row Cure Row
6 -East 6 -West
August
A 8 C D E F'
A 8- C ':. D` _ E F i'
A B CD E F 7
A B_ C D. E F)
A B C; D E- F?
A B C D E Ft
08/01/18
47 '
70
78
77 71
79
77'
74
76
70 •`. 71 77
78
71
76
74 80
74
69'
68
66
71 70
71
69
08/02118
50
55
59 ; 55
73
77
79 70
71
69'
70
71
70 69 75
78'
71
69
64 77
74
1 67
71
68
69 71
75
75'
08/03/18
08/04/18
08/05/16
08/06/18
67
70
72 67
71
69:
71
75
73 73
76
70,1
70
70
74 '• 68 71
73.
71
69
70 72
74
69
08/07/18
69
72
71-1 70
69
71'
70
73
69 72
71
M
73
71
67 71 66
70
71
73
K
69 70
72
71
08/08/18
:.
72
70
71 69
70
73:.
74
72
68 71
69
72
70
73
71 68 70
69:
71
67
70 72
75
71.
08/09/18
72
70
67 ; 69
71
73'
70
71
70 '72
69
72:
67
66
69 E 74 72
70
69
70
71 73
70
71 ,
08/10/18
71
74
70 ; 69
72
73
69
72
74 70
73
70i
70
75
73 € 68 71
71
69
71
72 € 69
72
74:
08/11/18
08/12/18
08/13/18
71
70
73 69
70
72
72
74
71 72
73
70'
73
72
70 67 70
71
72
1 73
70 68
72
71
08/14/18
71
74
76 70
69
70
70
73
72 1 71
66
69
74
71
74 € 72 68
70
69
70
71 72
68
70
08/15/18
74
72
70 1 69
71
67
73
71
75 i 70
67
69
72
70
71 67 69
66
71
74
72 66
69
68
08/16/18
68
66
69 72
72
70
70
65
68 70
67
70'
68
1 67
1 66 = 69 66
67
68
66
66 66
68
70,
08/17/18
69
70
71 66
69
70'.
71
70
69 71
66
69
69
66
64 71 70
69
69
70
1 71 66
71
65
08/18/18
08/19/18
08/20/18
70
69
71 65
67
68
66
65
67 70
71
69
67
66
69 70 71
70
66
65
66 60
1 70
70
08/21/18
71
70
69 ` 69
66
67
67
68
70 69
68
70'
68
68
70 71 69
68
69
67
69 67
69
66
08/22/18
'•
69
68
67 69
70
71
66
67
71 '•. 68
67
70
69
70
71 67 68
67
70
69
71 69
67
70!
'
08/23/18
08/24/18
68
72
65 60
67
70
08/25/18
08/26/18
08/27/18
65
68
70 1 62
65
67
08/28/18
66
66
F68 65
65
70
•.
`
i
08/29/18
70
68
65 ; 71
68
66
08/30/18
t
08/3/18
�.
i::

V(E®LIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, WC
'. tl . 10.1- - e..w o 9n4fi
m, r COMPOST CURING -. PILE TEMPERATURES
ROW 7
ROW 8 ROW 9
ROW 10
ROW 11
ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
Cure Row Cure Row
8 -East 8 -West
Cure Row Cure Row
9 -East 9 -West
Cure Row Cure Row
10 -East 10 -West
Cure Row Cure Row
11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
August
A B C `•. D. E F,
A B C D E F
A B C D E F
A B C D E F
A B C s D E F'
A B C D E F
08/01/18
I
08/02/18
111
08/03/18
08/04/18
I
I
I
•. I
I
€ I
I
08/05I18
08/06/18
.
08/07/18
:
i
08/08/18
'•
08/09/18
.
`
08/10/181
70
72
70
I
08/11/18
08/12/18
:
08/13l18
•
:66
70
68
08/14/18
70
69
66
08/15/18
'
'. 70
68
72 66
69
68
08/16/18
-
68
65
67 69
66
68
F
OBl17/18
:
70
71
67 's 66
69
72
08/18/18
I
I
I
I
I
I
••
08/19/18
0$/20/18
70-171
65
66
68
08/21/1
.
70
68 69
68
70
08/22/18
[69'
64
66 64
70
68
08/23/18
71
69 69
75
64
i
08/24/18
•`:
:68
71
75 60
73
70
08/25/18
I
I
I
-
08/26/18
I.I
L
08/27/18
.
:64
155
67 = 65
72
71
.66
.70 >.
66 64
70
72
08/28l18
I
_
66
77
65 '•' ,71
72
71
72
72
73 72
73
70
08/29/18
?
72
75
74 70
70
73
75
70.1
68 77
- 75
71
I
08/30/18
i
71
69
65 `•: 67
63
70
68
72
75 69
70
68
i
08/31/18
i

VEOLIAVATER NORTH AMERICA OPERATING SERVICES, INC.-
REGIOtZAL COMPOST FACILITY - HICKORY, MC
Cure Pite Temperatures - September 2018
COMPOST CURING- PILE TEMPERATURES
ROW I
ROW 2
ROW 3
ROW 4
ROW 5
ROW 6
ffA_TE,
Cure Row Cure Row
1 -East I -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Mow—
4 -East 4 -West
Cure Row Cure Row
5 -East 1 5 -West
Cure Row Cure Row
6 -East 6 -West
September
A B C D ---E' 'F
:A B E
D F
A B C D E Fj
A B"' C _D E Fi
A B C i D E Fj
A 6 D E F ,
09/oi/16
�Cf
09/02/18
09/03118
09104/18
0910511b
09106/18
09/07/18
91
59
66
64
-09108/18
09/09/18
0 10/18
66
69
71 1 64
65
'09111/18
69
71
68 1 70
•
67
64
09/12/18
1
61
59
61
65
62
67 64
68
66
09/13/18
64
61
63
66
67
63 68
70
66
09114/18
58
56
61
60
71
68 58
63
64'
09/15/18
09/16/18
09117/18
59
63
61
63
[6
66
61 i 64
67
62
09/18/18
69
71
72 69
72
69
6,
69
69
68 65
70
69
09/19/18
45
74
71
65 1 71
71
1 69
67
68
65 68
68
65
9/20/18 0
58
55
54
76
76
75 69
71
75
70
68
65 i 67
68
71
09/21/18
61
74
78
g 70
76
77 70
72
77,
67
68
68 66
69
70
09/22/18
09123118
09/24116
68
62
64 1
59
6 1
66 63
60
64
61
66
63 1 65
62
60
09/25/18
60
64
61 1
62
66
651 59
63
61
59
1.62
61 1 64
61
63
09/26/18
09/27/18
62
62
60-
61
64
59 64 60
63
61
60.
63
-64
67 64
61 61
62'
'64
63
60
64
58
61
63
59 62
61 1 59
60,
62
59
61
09/28/18
63
62 60 1
64
7 1
-0i'll 68
_6
71
62'
-60
61 59
62
637'
09129"8
09/ 30/18

VEOLIA WATER WORTH AMERICA OPERATING SERVICES, INC.
Rg IOWALd6MO6ST-FACiLIT-Y-hidkdRfkd
Cure Pile Temperatures - September 2018
ROW 7 11 ROW 8 11 ROW 9 11 , ROIN 10 11 ROW 11 11 ROW 12
DATE
Cure Row Cu Row
8 -East' 8 -West
e Row
Cure Row Cure ]
9 -East 9 -West
Cure Row Cure Row"
16 -West
-Cure' Row Cure' Row
11 -East 11 -West
Cure Row Cure Row
12 -East 12 -West
Cure Row Cure Row
7 -East 7 -West
ber
Se tj
A B C D E F
A B C D E F
A B C D7E F
A e c D r= F
A B C 1 D E V
A B C D E F
09/01118
09102/18
09/03/18
09/04/18
09/05/18
60
70
71 60
71
66
70
69
70 1 63
72
69
70
69
72 67
69
67
09/06/18
66
72
70 68
71
67
69
71
67 70
68
70
70
68
71 69
71
66
09/07/18
69
72
67 68
67
65
68
71
66 1 64
62
64
.71
67
70 70
69
70
09/08/18
09/09/18
09/10/18
71
68
72 69
66
70
69
68
68 73
70 1
681
67 1
68
1 66 71
67
70
09111/18
64
67
63 68
65
69
67
63
681 66
61
67
63
67
651 67
64
68
09112/18,
63
69
65 67
64
69
'62
66
641. 68
70
66
F
I
N I
S
H
09/13/18
.62
66
68 66
61
67
-65
69
66 66
70
64
09/14/181
59
68
68 59
59
62
68
66
61 67
65
59
09/15/18
09/16/18
09/17/18
59
65
66 68
63
67
62
68
64 63
66
69
09118/18
62
64
68 157
66
68
'63
65
63 63
60
65
09/19/18
58
60
66 70
64
65
65
64
66 67
64
63
09/20/18
68
69
69 66
68
71
60
64
65 65
65
68
09/21/18
62
64
68 1 63
69
70
F
I
N 1 1
S
H
09/i2h8
09/23118
09/24/18
60
64
631 61
60
59
09/26/18
63
61'
64 1. 62
66
60
09/26/18
60
66
621 61
66
62
09/27/18
62
61
`6 ,,.63
66
63
0
71 1 69
70
67
09/29/18
09/3 11 0/18
d

VEOLIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures -'.October 2018
COMPOST CURING.- PILE TEMPERATURES - -
ROW 1
ROW 2
ROW 3
ROW 4
ROW 5
ROW 6
DATE
Cure Row Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Row
4 -East 4 -West
Cure Row Cure Row
5 -East 5 -West
Cure Row Cure Row
6 -East 6 -West
October
A B_ C D E F f
A_ B C `- D E F;
A __ : 8_ -C € D- E F!
-A B C ': D E F`
A t3 C D E F r
A B C •:' D E F
10/01/18
61
64
60 63 61
64
63
66
61 ' 61
63
65
66
63
62 60
64
62
10l02/1t3
61
64
63 ':
66
68
65 67 65
67
70
72
70 `•. 71
72
71 •
64
62
61 65
63
65
10/03/18
55
60
64
67
66
67 68 72
70'
65
67
66 62
66
69
62
60
59 61
58
60.
10/04/18
71
69
68 65
62
59'
64
68
69 70 71
68
68
65
621 65
68
64`
59
61
60 62
65
60
10/05/18
74
74
74 58
63
59
68
67
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REGIONAL COMPOST FACILITY - HICKORY, NC
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,REGIONAL COMPOST FACILITY HICKORY,-=
Cure Pile Temperatures - November 2018
COMPOST CURING!- PILE TEMPERATURES
ROW 1
ROW 2
ROW 3
ROW 4
ROW 5
ROW 6
DATE
Cure Row Cure Raw
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Raw
4 -East 4 -West
Cure Row Cure Row
5 -East 5 -West
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November
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11/61/18
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11/02/18
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11/03/18
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11/10/18
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11/12/18
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11/13/18
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11/14/18
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VEOLIA WATER WORTH AMERICA OPERATING SERVICES, INC.
'REGIONAL COMPOST FACILITY = HICKORY, MC
Cure Pile TemDeratures - November 2018
ROW 7 —IF— ROW a 11 ROW 9 11 ROW 10 11 ROW li H ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
Cure Row Cure Row
8 -East 8 -West
Cure Row Cure Row
9 -East 9 -West
Cure Row Cure Row
10 -East 10 -West
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11/08/18
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VEO.LIA WATER NORTH AMERICA OPERATING SERVICES, INC.
REGIONAL COMPOST FACILITY - HICKORY, MC
Cure Pile Temperatures - December 2018
COMPOST CURING o PILE TEMPERATURcs
ROW 7
ROW 8
ROW 9
ROW 10
ROUW 11 ROW 12
DATE
Cure Row Cure Row
7 -East 7 -West
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8 -East 8 -West
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ure'Row Cure Row
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rA
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12/13/18
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12/14/18
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REGIONAL COMPOST FACILIV - HICKORY, NC 9
Cure Pile Temperatures - bacember 2018
COMPOST CURING:- PILE TEMPERATURES
ROW 1
ROW 2
ROW 3
ROW 4
ROttlf 5
ROW 6
DATE .
Cure Raw Cure Row
1 -East 1 -West
Cure Row Cure Row
2 -East 2 -West
Cure Row Cure Row
3 -East 3 -West
Cure Row Cure Row
4 -East 4 -West
Cure Row Cure Row
5 -East 5 -West
Cure Row Cure Row
6 -East 6 -West
December
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12/04/18
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63
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70
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72 ` 70
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12/06/18
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62
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12/07/18
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65 71
70
60
1 62
64 = 62
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12/08/18
12/09/18
12/10/18
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12/11l18
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12/12/18
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12/13/98
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12/14/18
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12/18/18
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12l19/98
60
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61
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12/20/98
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12/21/18
60
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