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HomeMy WebLinkAboutWQ0001048_Annual Report_20190304Y• CMSD f POST OFFICE BOX 477 GRIFTON, NORTH CAROLINA 28530 CHARLES M. SMITHWICK, JR. DISTRICT MANAGER Mr. Daryl Merritt DENR/DWR/Water Quality Section Non -Discharge Compliance/Enforcement Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: Contentnea MSD Land Application Permit #WQ0001048 2018 Annual Report Dear Mr. Merritt, February 26, 2019 MAR 0 201� RECEIVEDNOEQ/DVIIR MAR - 4 2019 Non -Discharge Permitting Unit Please find enclosed three (3) copies of the above referenced annual sludge land application program report for the Contentnea Metropolitan Sewerage District (CMSD), Permit Number WQ0001048, for your review. If you should need any additional information please contact me at (252)524-5584. Sincerely, 1 Renee Smith Land Application ORC Enclosure ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001048 County: Facility Name (as shown on permit): Land Application Operator: Pitt Year: 2018 Contentnea MSD Renee Smith Phone: 252-524-5584 Land application of residuals as allowed by the permit occurred during the past calendar year? a ++ Yes ❑ ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled.RECEIVED/NcDEr-)t^), PR Part A - Residuals Application Summary. R„ „ Total number of application fields in the ermit: 2 e Total number of fields utilized for land application during the year: lNon- ' Total amount of dry tons applied during the year for all application sites: 69. 6#rM QJQ Unit Total number of acres utilizes for land application during the year: 52.17 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13. below) issued by the Division of Water Resources.. ❑ Yes No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was' adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified. in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three'(3) copies of certified laboratory results are attached.' 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) t copies of certified laboratory results are attached. ' 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant w Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: - ' "I certify, under penalty of law, that the above information is, to the best of my knowledge. and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Charles M. Smithwick, Jr./District Manager x�ermittee Name and Title (type or print) Signature of Permittee Date r Signature of Preparer* Date (if different from Permittee) * Preparer is defiried in 40 CFR Part 503.9 (r) and 15A NCAC 02T Signature of Land Applier Date (if different from P.ermittee and Preparer) .1102 (26) DENR FORM ACF (12/2006) EXPLANATIONS FOR DEVIATIONS FOR THE 2018 ANNUAL SLUDGE LAND APPLICATION, REPORT 2-20-18 Monitoring Well #10 Chromium 0:015 mg/L 6-20-18 Monitoring Well #9 Total Organic Carbon 10.27 mg/L Monitoring Well #10 Chromium 0.016 mg/L Monitoring Well #15 Total Organic Carbon 11.92 mg/L 10-11-17 Monitoring Well #9 Total Organic Carbon 17.06 mg/L Monitoring Well #10 Chromium 0.014 mg/L All of the above violations were reported to NC Department of Environment and Natural Resources -Washington Regional Office. We are currently working with NCDENR-WRO in an effort to address the Chromium issues. We believe this is an issue that is. occurring in the groundwater prior to our land application. In the past three years we have significantly decreased our land application practices due to the use of our screw press. All of the sludge that is processed through the screw press is hauled off site to a compost facility. r l 4 CLASS A Ai..,1gVAL DISTRIBUTION AND MARKETING/ SURFAu:1' DISPOSAL CERTIFICATION AND SUMMARY FORM. WQ PERMIT #: WQ0001048 FACILITY NAME: Contentnea MSD PHONE: 252-524-5584 COUNTY: Pitt OPERATOR: Renee Smith FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) ❑ Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes ® No ❑ --► If No skip parts A, B, C and certify form below Part A*: Part B": Month Sources sinclude NPDES # if () ( applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January February March April May June CMSD WWTP NCO032077 21.151 July CMSD'WWTP NCO032077 `26.304 August CMSD WWTP NCO032077 20.524 September CMSD WWTP NCO032077 1.082 October November December Total from FORM DMSDF sub, of , g< d ?m zx s.f:; .t,:: , Totals: Annual (dry tonsi- "..„. 'fi? . -^ ' .. ii-111 �iki" 'i'.Et<... rvt Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) Part C: Facility was compliant during the past calendar year with all conditions of the land application permit ❑ Yes (including but not limited to items 1-3 below) issued by the Division of Water Resources: ❑ No -► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." . (%t P/ j;�l 2 2 �Jci I , �k Signature of Permittee Date Signature of Preparer** (if different from Permittee) **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Z�al-e Date DENR FORM DMSDF (12/2006) AND ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001048 Laboratory:, 1) Environment I, Inc. Facility Name: Contentnea MSD 2) Residual Source WQ # or NCO032077 3) NPDES #: 4) WWTP Name: Contentnea MSD 5) %-Qirinal Analvaic Dnfn Parameter (mg/kg) Conc. Limit m a Sample or Composite Date 4-10-18 5-10-18 Percent Solids (%) NA 1.73% Arsenic 75 <2.5 Cadmium 85 1.1 Copper 4,300 .247 Chromium NA 13 Lead 840 18 Mercury 57 0.49 Molybdenum 75 <5.0 Nickel 420 13 Selenium 100 <5.0 Zinc 7,500 651 Total Phosphorus NA 27260 TKN NA 43740 Ammonia -Nitrogen NA 788 Nitrate and Nitrite NA 12951 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Preparer * ZZ6 t01 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) Enw,nRE&M % hw @Tml@d r.O. BOX 7085, 114 OAKMONT GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sludge Analysis Method PARAMETERS Sample Date Analyst Code PH (not to be used for reporting) 3.9 04/10/18 JTH 4500HB-11 Aluminum, (dry wt. basis), mg/kg 17916 04/16/18 LFJ EPA200.7 Arsenic (dry wt. basis), mg/kg <2.5 04/18/18 MTM 3113B-04 Calcium (dry wt. basis), mg/kg 16099 04/16/18 LFJ EPA200.7 "admium (dry wt. basis), mg/kg 1.1 04/23/18 MTM 3113B-04 opper (dry wt. basis), mg/kg 247 04/16/18 LFJ EPA200.7 chromium, T.(dry wt. basis),mg/kg 13 04/16/18 LFJ EPA200.7 Lead (dry weight basis), mg/kg 18 04/20/18 MTM 3113B-04 Magnesium (dry wt. basis), mg/kg 4632 04/16/18 LFJ EPA200.7 Mercury (dry wt. basis), mg/kg 0.49 04/17/18 MTM EPA7471B Nickel (dry wt. basis), mg/kg 13 04/16/18 LFJ EPA200.7 Potassium (dry wt. basis), mg/kg 7225 04/16/18 LFJ EPA200.7 Selenium (dry wt. basis), mg/kg <5.0 04/19/18 MTM 311313-04 Sodium (dry wt. basis), mg/kg 3163 04/17/18 ONS 3111B-11 Zinc (dry wt. basis), mg/kg 651 04/16/18 LFJ EPA200.7 Total Nitrogen, mg/kg (calc) Lab Error Total Solids, % 1.73 04/10/18 KDS 2540G-11 TKN (dry wt.), mg/kg c 39930 04/13/18 DTL 351.2 112-93 Ammonia Nitrogen (dry wt.),mg/kg c 788.0 04/26/18 MF 350.1 R2-93 Nitrate Nitrogen(dry wt.), mg/kg Lab Error Nitrite Nitrogen(dry wt.), mg/kg c 1.00 05/04/18 CLO 353.2 112-93 Phosphorus, T. (dry wt.), mg/kg c 27260 04/13/18 CLO 365.4-74 Molybdenum (dry wt. basis), mg/kg <5.0 04/16/18 LFJ EPA200.7 DNE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 04/10/18 DATE REPORTED : 05/10/18 REVIEWED BY: c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. Enwokummid % hw Tmhd GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Nitrogen, mg/kg (calc) TKN (dry wt.), mg/kg Nitrate Nitrogen(dry wt.), mg/kg Nitrite Nitrogen(dry wt.), mg/kg Sludge Analysis Method Sample Date Analyst Code 56691 06/04/18 SEJ c 43740 05/15/18 TLH 351.2 R2-93 c 12950 05/31/18 CLO 353.2 112-93 c 0.98 05/14/18 CLO 353.2 R2-93 nking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 Y DATE COLLECTED: 05/10/18 DATE REPORTED : 06/04/18 REVIEWED BY: 6 c Uncertified data. DWR does not offer non -aqueous certification for this analytical procedure. TC L P LAB REPORTS __ .j 1i'.c`;T" v• £4ubi'Fr�,;f',•'�MFX.� �" 'U•`Si�< �S?CNm *A i fiw Orland The results set forth herein are provided by SGS North America Inc. Technical;Report for Environment 1, Inc Contentnea Metro Sewage District; Grifton, NC 416 SGS Job Number: FA53172 Sampling Date: 04/04/18 Report to: Environment 1, Inc PO Box 7085 Greenville, NC 27835 dwoolard@environmentlinc.com ATTN: Deedee Woolard Total number of pages in report: 14 Autornated Report A O Test results contained within this data package meet the requirements Caitlin Brice, M.S. General Manager of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Jean Dent -Smith 407-425-6700 Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001) DoD ELAP(ANAB L2229), AZ(AZO806), CA(2937),'TX(T104704404), PA(68-03573), VA(460177), AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707 SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about Unauthorized modification of this report is strictly prohibited. how we can serve you better at: _ Review standard terms at: http://w+vw.sgs.com/en/terms-and-conditions EHS.US.CustonierCare@sgs.coni 1 of 14 FA53172 Table of Content Sections: -1- Section1: Sample Summary................................................................................................... 3 Section2: Summary of Hits.................................................................................................... 4 r Section 3: Sample Results ....... 5 3.1.: FA53172-1: SLUDGE SAMPLE.................................................................................. 6 Section4: Misc. Forms............................................................................................................ 12 4.1: Chain of Custody........................................................................................................... 13 I 2of14 FAS3172 SGS North America Inc. Sample Summary Environment 1, Inc Job No: FA53172 Contentnea Metro Sewage District; Grifton, NC Project No: 416 Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID FA53112=i : ;', 04/04/18 09:15 KH 04/07/18 SO Sludge SLUDGE SAMPLE""',-,..''. Soil samples reported on a dry weight basis unless otherwise indicated on result page. F", 3oi14 FA53172 Summary of Hits Job Number: FA53172 Account: Environment 1, Inc Project: Contentnea Metro Sewage District; Grifton, NC Collected: 04/04/18 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA53172-1 SLUDGE SAMPLE Corrosivity as pH 4.9' su SW846 CHAP? Ignitability (Flashpoint) a "> 200;, ":: Deg. F SW846 1010 Benzene 0:0032 J;' ,.t . 0.010 0.0031 mg/1 SW846 8260B Tetrachloroethylene 0.0235 0.010 0.0022 mg/1 SW846 8260B (a) Not ignitable. Page 1 of 1 4of14 FA63172 ' — ___ � .,.-?S;^.l4gis3':1':71: �T..„'�^�+";^� y•'�^,,"S T•*bv' ,,. z:;.t+`i'W'i d ?, 4 • d M� 'kY ��>#�b{�rvt .�3r.+� 'b„'i tlk�" Yi"'r k� �g�' 'YFr � ` ..r i+X N� .�L.-;�e..s�%.� Tx�ia r.� 5'Y .•.� �. i'''f °-,x'�i....$>}�,o`.n7E s�y"7^ .tfti"-W,r�S:';'}�z'.#ei y.}�, n`u�tt„?N v•t'. �i�. �'. c. Sample Results Report of Analysis Section 3 IM 5of14 _G_ FA53172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8260B SW846 1311 Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1' File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 M0102391.1) 10 04/11/18 17:40 MM 04/09/18 13:45 OP69516 VM4409 Run #2 Purge Volume .un #1 5.0 ml :un #2 VOA TCLP List TCLP Leachate method SW846 1311 CAS No. Compound . Result HW# MCL RL MDL Units Q 71-43-2 Benzene 0.50 0.010 0.0031 mg/1 J 78-93-3 2-Butanone (MEK) : NDr ;.E D035 200 0.050 0.020 mg/1 56-23-5 Carbon Tetrachloride ND°:? ; '.'; , = D019 0.50 0.010 0.0036 mg/1 108-90-7 Chlorobenzene ; ND ` _ ;.: >; D021 100 0.010 0.0020 mg/1 67-66-3 Chloroform ND'a'>`_ D022 6.0 0.010 0.0030 mg/1 106-46-7 1,4-Dichlorobenzene ND„,':': D027 7.5 0.010 0.0026 mg/1 107-06-2 1,2-Dichloroethane Np'_' ,. ; . D028 0.50 0.010 0.0031 mg/1 75-35-4 1,1-Dichloroethylene ND.., ,, ;; ,v„ �,,.' D029 0.70 0.010 0.0032 mg/1 127-18-4 Tetrachloroethylene ;., .., .w: 0:0235:.'-''...,''':, D039 0.70 0.010 0.0022 mg/1 79-01-6 Trichloroethylene ;Nb .''i',-''. `: D040 0.50 0.010 0.0035 mg/1 75-01-4 Vinyl Chloride °NDr=y' ;°°` D043 0.20 0.010 0.0041 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 .Limits 1868-53-7 Dibromofluoromethane 6 '102% ` -::: 83-118% 17060-07-0 1,2-Dichloroethane-D4 .;. -10.4% fi :.m, 79-125% 2037-26-5 Toluene-D8 101% '' 85-112% 460-00-4 4-Bromofluorobenzene 99%:'::°.; 83-118% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 6of14 FA53172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8270D SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 9I000906.1) 1 04/12/18 09:22 MV 04/11/18 13:00 OP69573 S9134 Run #2 Initial Volume Final Volume 'un #1 100 ml 1.0 ml 'un #2 ABN TCLP List CAS No. Compound 95-48-7 2-Methylphenol 3 &4-Methylphenol 87-86-5 Pentachlorophenol 95-95-4 2,4,5-Trichlorophenol 88-06-2 2,4,6-Trichlorophenol 106-46-7 1,4-Dichlorobenzene 121-14-2 2,4-Dinitrotoluene 118-74-1 Hexachlorobenzene 87-68-3 Hexachlorobutadiene 67-72-1 Hexachloroethane 98-95-3 Nitrobenzene 110-86-1 Pyridine CAS No. Surrogate Recoveries 367-12-4 2-Fluorophenol 4165-62-2 Phenol-d5 118-79-6 2,4,6-Tribromophenol 4165-60-0 Nitrobenzene-d5 321-60-8 2-Fluorobiphenyl 1718-51-0 Terphenyl-dl4 Result HW# MCL RL NI)_ ::.::,•; D023 200 0.050 D024 200 0.050 100 0.25 D041 400 0.050 NDt- ` D042 2.0 0.050 rND=' D027 7.5 0.050 D030 0.13 0.050 D032 0.13 0.050 D033 0.50 0.050 D034 3.0 0.050 D036 2.0 0.050 D038 5.0 0.10 Run# 1 Run# 2 Limits 33418% 42-108% 39-121% TCLP Leachate method SW846 1311 MDL Units Q 0.0056 mg/1 0.0098 mg/l 0.050 mg/1 0.0074 mg/I 0.0075 mg/1 0.0050 mg/1 0.0081 mg/1 0.0069 mg/1 0.0050 mg/1 0.016 mg/1 0.0093 mg/1 0.020 mg/1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 7of14 1 FA53172 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:. SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8151A SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 CC057863.1) 1 04/12/18 22:06 NJ 04/11/18 12:15 OP69575 GCC1276 Run #2 Initial Volume Final Volume Run #1 10.0 ml 5.0 ml Run #2 Herbicide TCLP Leachate TCLP Leachate method SW846 1311 CAS No. Compound Result HW# MCL RL MDL Units Q 94-75-7 - 2,4-D Np.;`:','' D016 10 0.050 0.017 mg/1 93-72-1 2,4,5-TP (Silvex) ND:: ,:.'.. _ . _: D017 1.0 0.0050 0.0013 mg/1 CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits - 19719-28-9 2,4-DCAA 132J1''_. 39-135% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 8of14 FA53172 SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Method: SW846 8081B SW846 3510C Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 File ID DF Analyzed IBy Prep Date Prep Batch Analytical Batch Run #1 TT387928.1) 1 04/12/18 15:16 KL 04/11/18 13:00 OP69574 GTT2128. Run #2 Initial Volume Final Volume :un #1 100 ml 5.0 nil :un #2 Pesticide TCLP Leachate CAS No. Compound 58-89-9 gamma-BHC (Lindane) 12789-03-6 Chlordane 72-20-8 Endrin 76-44-8 Heptachlor 1024-57-3 Heptachlor epoxide 72-43-5 Methoxychlor 8001-35-2 Toxaphene CAS No. Surrogate Recoveries 877-09-8 Tetrachloro-m-xylene 2051-24-3 Decachlorobiphenyl TCLP Leachate method SW846 1311 Result HW# MCL RL MDL Units Q D013 0.40 0.00010 0.000022 mg/1 D020 0.030 0.0010 0.00038 mg/1 0:020 0.00020 0.000021 mg/1 D031 0.0080 0.00010 0.000026 mg/1 D031 0.0080 0.00010 0.000020 mg/1 nNDd ` . D014 10 0.00020 0.000050 mg/I 0.50 0.0050 0.0021 mg/1 Run# 1 Run# 2 Limits ,7 89/c 42-127% 890 , 27-127% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value MCL = Maximum Contamination Level (40 CFR 261 7/1/11) B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound SGS North America Inc. Report of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC Page 1 of 1 Metals Analysis, TCLP Leachate SW846 1311 Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method Arsenic :410 " D004 5.0 0.10 mg/1 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 1'1Barium <_2;:0 : ; :: D005 100 2.0 mg/1 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Cadmium D006 1.0 0.050 mg/1 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Chromium 5D007 5.0 0.10 mg/1 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 .0.10:" . Lead <0:050 "._, D008 5.0' 0.050 mg/1 1 04/12/18 04/12/18 LM SW846 6010C 2 SW846 3010A 3 Mercury �,<0:0050I D009 0.20 0.0050 mg/l 1 04/12/18 04/12/18 LM SW846 7470A 1 SW846 7470A 4 Selenium < 0.:1'0; '::''". D010 1.0 0.10 mg/1 1 04/12/18 04/12/18 LM SW846 6010C Z SW846 3010A 3 Silver < 0 `10 -.. - : ;,." D0l l 5.0 0.10 mg/1 1 04/12/1-8 04/12/18 LM SW846 6010C 2 SW846 3010A 3 (1) Instrument QC Batch: MA14817 (2) Instrument QC Batch: MA14818 (3) Prep QC Batch: MP33585 (4) Prep QC Batch: MP33587 RL = Reporting Limit MCL = Maximum Contamination Level (40 CFR 261 7/1/11) 10 of 14 FAS3'172 SGS North America Inc. Deport of Analysis Client Sample ID: SLUDGE SAMPLE Lab Sample ID: FA53172-1 Date Sampled: 04/04/18 Matrix: SO - Sludge Date Received: 04/07/18 Percent Solids: 1.7 Project: Contentnea Metro Sewage District; Grifton, NC General Chemistry Analyte Corrosivity as pH Cyanide Reactivity Ignitability (Flashpoint) a Solids, Percent Sulfide Reactivity (a) Not ignitable. RL = Reporting Limit Result RL Units DF su 1 87 mg/kg 1 >200;_: Deg. F 1 L '. % 1 <;2900=- 2900 mg/kg 1 Page 1 of 1 Analyzed By Method 04/09/18 12:15 BR - SW846 CHAP7 04/19/18 18:36 JK SW846 CHAP7 04/23/1816:20 BW SW8461010 04/12/18 16:00 AG SM19 2540G 04/14/18 10:55 BW SW846 CHAP7 11 of 14 FA53972 S- - ,'�ii.^a:17'si ��,�'-,�A E.�'r gv�;;,�.�71,'v �y,€,r�;;,o�.�+Pi�'' 7��',+�s�.'+� 4x •"-i„r,;4«k"�'e '�°�, �,} ,�.+ �" ',�:•''��'"`�'i { ^,.;ham '�, ``t'': r, a vJ € �M ,y, —S. Gs—'� Orland �1Vlisc: Foriris� Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 0 �r 12 of 14 FA53172 CHAIN OF CUSTODY DY RF.COR�.® CHAIN P.O. BOX 7085, 114 Oakmont Dr. __ v v ✓ _ 1 Page 1 of 1 Greenville, NC 27858 DISINFECTION environmentl inc.com CHLORINE NEUTRALIZED AT COLLECTION ?hone (252) 756-6208 • Fax (252) 756-0633 ry CHLORINE pHCHECK (LAB) MIENT:416 Week:8 UV P P P G G G G G CONTAINERTYPE,PIG "MSD (SLUDGE & WELLS ACCT)NONE �ONTENTNEA METRO. SEWAGE DIST. 4S. RENEE PRIDGEN A A A A A 'A A A CHEMICALPRESERVATION .O. BOX 477 7.RIFfONNC28530 w A -NONE D-NAOH aao '252) 524-5584 . 1 s o w ¢ In w z > rn is •� ° w B-HNO, E-HCL o= C - HzSO, F -ZINC ACETATE/NA0H COLLECTION ¢ o a a 8 a b0 Q E. a p a E. F E+ G-NATHIOSULFATE a SAMPLELOCATION DATE TIME � CLASSIFICATION: Mudge� S WASTEWATER(NPDES) DRINKINGWATER DWO/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURI NG�S}I I PMENTIDELIVERY UY N SAMPLES COLLECTED BY: (Please Print) 1 SAMPLES RECEIVED IN LABAT(5-3 °C RELIN UISHEDBY(SIG.)(SAMPLER) DATUTIME a:s3 REG E BY( � ATE TIME y COMMENTS: y-Li�» LI EDB ) DATNTME REC ED ATEITIME RELINQUISH B DATE/TIME CEIVED (SIG.) 0,17 DATEMME k(22dwf u I PLEASE READ Instructions for eompletingAi4rm opAhe reverse si 4 Saup ur must piece a L, for composite sample or a G far Ff1RM &S �. ,� � g 915— Grab sample in the blocks above for each parameter reouested. NO i A 17 A 1 k A53172: Chain of Custody Page I of 2 I 13 of 14 —SG — FA53172 SGS Sample Receipt Summary Job Number: FA53172 Client: ENVA Project: CMSD Date / Time Received: 4/7/2018 9:15:00 AM Delivery Method: FED EX Airbill Ws: 771940436480 - Therm ID: IR 1; Therm CF: 0.4; # of Coolers: 1 Cooler Temps (Raw Measured) °C: Cooler 1: (4.2); Cooler Temps (Corrected) °C: Cooler 1: (4.6); Cooler Information Y or N Sample Information Y or N NIA 1. Custody Seals Present 2 ❑ 1. Sample labels present on bottles Rl ❑ 2. Custody Seals Intact ❑� ❑ 2. Samples preserved properly ❑Q ❑ 3. Temp criteria achieved ❑� ❑ 3. Sufficient volume/containers recvd for analysis: 0 ❑ 4. Cooler temp verification IR Gun 4. Condition of sample Intac 5. Cooler media Ice(Ban) 5. Sample recvd within HT 2 ❑ 6. Datesfrimes/IDs on CDC match Sample Label ❑ Trip Blank Information Y or N N/A 7. VOCs have headspace ❑ ❑ ❑� 1. Trip Blank present / cooler ❑ ❑ R 8. Bottles received for unspecified tests ❑ ❑./ 2. Trip Blank listed on CDC ❑ ❑ © 9. Compositing instructions clear ❑ ❑ ❑d 10. Voa Soil Kits/Jars received past 48hrs? ❑ ❑ R1 W or S N/A 11. % Solids Jar received? ❑ ❑ 3. Type Of TB Received El ❑ 12. Residual Chlorine Present? ❑ ❑ 10 Misc. Information Number of Encores: 25-Gram 5-Gram Number of 5035 Field Kits: Number of Lab Filtered Metals: Test Strip Lot #s: pH 0-3 230315 pH 10-12 219813A Other: (Specify) Residual Chlorine Test Strip Lot #: Comments SM001 Technician: SHAYLAP Date: 4/7/2018 9:15:00 AM Reviewer: SP Date: 4/7/2018 Rev. Dale 05/24/17 FA-53172: Chain of Custody page 2 ®f Z 14off4 FA53172 Environment 1, T- CHAIN OF CUS- _ DY RECORD P.O. Box 7085,1 ikmont Dr. Page 1 of 1 C,rPPnvi11P NC 2, , °nvironment1dnc.con DISINFECTION CHLORINE NEUTRALIZED AT COLLECTION Phone (252) 756-6208 o Fax (252) 756-0633 Ij CHLORINE CLIENT: 416 Week: 8 uv pH CHECK (LAB) CONTAINER TYPE, P/G ;MSD (SLUDGE & WELLS ACCT) NONE p p p I G G I G IG G :ONTENTNEA METRO. SEWAGE DIST. CHEMICALPRESERVATION CIS. RENEE PRIDGEN JA '.O. BOX 477 A A A A A A A m zo TRIFTON NC 28530 A - NONE D - NAOH E� w Uj v zo cc c b w C B- HNO E- HCL a 252) 524-5584 o z y w c (w c x w C- HZSO, F- ZINC ACETATE/NAOH COLLECTION Q w ��.• o P. Pa. A. a LL a G NATHIOSULFATE 2 o Ujo `W a o ry 44 U F EUa EU H F °¢ SAMPLE LOCATION DATE TIME 5 . — �� =<:';::> `> :>? >; :>::;;::: CLASSIFICATION: Ij WASTEWATER (NPDES) DRINKING WATER DWO/GW SOLID WASTE SECTION CHAIN OF CUSTODY (SEAL) MAINTAINED DURING IPMENT/DELIVERY Y N SAMPLES COLLECTED BY: (Please Print) (� SAMPLES RECEIVED IN LAB AT Q °C RELINQUISHED BY (SIG.) (SAMPLER) DATE/TIME REC BY ( ATEMME COMMENTS: RELI ED B .) / DATEMME RECEIVED B (' DATE/TIME RELINQUISH B DATE/TIME RECEIVED BY (SIG.) DATEMME Sampler must place a "C for composite sample or a "G" for PLEASE READ Instructions for completing this form on the reverse side. FORM #5 Grab sample in the blocks above for each parameter requested. N 0 _ 343741 LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �n N4) 0-K15D WQ Permit #: t> GIoLg Field #: Land Owner: CO-)ift4neA 1(b-D Annual Dry Tons Applied: 6•"7Cr-) Site #: Operator: Predominant Soil Series: -i6r%nrfr�, Crop 1 Name: (' aq ctajffkjd - Crop 1 Max. PAN: ��(�, Crop 2 Name: Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Z.IgQ Z. I� q/ 0-5 ° y ° ° Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal. Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Hrs. inches > o w a. o w N' * o' T w `, - * TKN mg/kg Z a �o o w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 - D- 37Z galZWED N 0C> , 437)4 i6g Zq-D, 'J. (o bey 3 CLAD IV,, 6AP6 3z017 Q 5 0-5 0. 30 ,3(vZ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTAL As Cd Cu Cr Pb HR Mo Ni Se Zn P Z3•GIZ Lime Applied Annual lbs/acre ,Ot .I(o-) O,C62 ,M-5 roo2 O.C2-Q O• Z o.0 - Z .-ntv ......:::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac • : 4q-3 o,5 ,:::::::::::::: 34, ,l I U, 31-I 7, G4is I ' °lv -- (,a 1 O. lv ,31vS 15 cl L•4�3 — 9,1444a 7• ZQ 37Ci Oa G,� >io 3 Z� IIZ 21gi ZUq'9 :::::::::: :::::::::::::::: :::::.:............. . Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop I "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier -1=Z6-1 C� Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: 0( n+,ffN-1'1'C'a_M6D Total Dry Tons Applied (Annual): 6„_)09 P -mit Cation Exchange Capacity (non 503 only): .S gyrator: -_)�i Owner: U(,.l)tfn44 0 -mb� Predominant Soil Series: Acres Used: Z. S L/ Acres Permitted: Z. Iq L/ Site #: Field #: i Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): I posite Date E non Non Total Phos- rus ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total App- Event iiii�iiii�■ 1 Total Phos- phorusmMENEENEENEENc. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i sonment for knowing violations". 4AW"It)L_ Z 26-10 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �bn*6* 06D WQ Permit #: V_)Q0D0J04q Field #: Land Owner: Cjj.�n+er)+n' Q 1) Annual Dry Tons Applied: 3 (" Site #: Operator:'?)gnee6m r� Predominant Soil Series: Crop 1 Name: Crop 1 Max. PAN: I-gO Crop 2 Name: Z Acres Utilized: Z . 6V Z B Acres Permitted: Z , & Z Cation Exchange Capacity (non 503): q- 5 Crop 2 Max. PAN: o ° ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond.'Cl (Dry, Moist Precip. Past 24 Hrs. inches a co � a w o o %`� w 7y w ; w * N' w 0 TKN mg/kg Z a o El uq o P. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 12-iQ "Llwo ). .ZI I >` cccroan df o 5 O, 5 0,30 43-140 az9 530 f =Z1 1 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: i-140D0 : As Cd Cu Cr Pb Hg Mo Ni Se Zn P W63D Lime Applied Annuallbs/acre 0-.00(F O.CQ3 $ 1 O.OI-A O-CO) O•UIZ O. 1 ,0tZ i. o-) -•D :<:: :::.....:::::::: »>: >: Date lbs/ac Prior Years Cumulative lbs/ac p.IoZ1;, 6.0�2 -)Q.5 r 34.Zl5 10,0(o L362 -0.q55 ZGl.5Q"l Current Cumulative lbs/ac I 0- (e4-L 5.065 4C14 ,RZ44 .p D ,3W3 ZA65 q,4 5 O, -) Permitted C. P. L. R.**** 3 (e 3(-I i3 - Z(j) 15 — 3-)y �G ZsiGg Permit PAN Limit 2 1 t s/ndCro p O "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation Z� **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: COr iff1 0e0_n1�17 Total Dry Tons Applied (Annual): 3. I-)Cf p^-mit #: LL�Qccploug Cation Exchange Capacity (non 503 only): 4.5 :rator: R� ,eeOwner: (`1(i-)+ef- nfS)_rf)b_D Predominant Soil Series:-R�C4pjUt Acres Used: Z, ie z Acres Permitted: Z & Z, Site 1b Field #: Z Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date I 1 LI-10-1$ 2 3 4 5 61 L 7 8 91 10 11 12 % Solids 1-)3% Arsenic CZ6 Cadmium i. l Copper Zy1 Chromium 1-5 Lead i g Mercury 0,L4cj Molyb- denum CS,p Nickel 13 Selenium <5.0 Zinc (' 6 i Total Phos- rus 27 k, O ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9j 10 11 12 DT/Ac./ '7-1Z-lg App. Event Arsenic ©, pp(, p: OCR . Cadmium .CO3 ,-5 Copper p, 5C1� D T1B Chromium 0.O31 o p31 Lead (),044 U4 Mercury C>: Gn 1 Molyb- denum o,D1Z C. iZ Nickel () , p3 i I Selenium ©, pi Z I Z Zinc i .577 1. �7 Total Phos- phorus 1v.02-1+ tG b•b�U "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I nm aware that there are significant penalties for submitting false information, including the possibility of fines and i �sonment for knowing violations". InL - 01- a6v && I Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Linn I fa (Yl b_D WQ Permit #: 00CWJ04S Field #: Land Owner:{- (� �� Annual Dry Tons Applied:flif43xsr,Nti Site #: Operator: I�Lh Predominant Soil Series:_fbr46m0U_+h Crop 1 Name: Crop 1 Max. PAN: 1-) U Crop 2 Name: 9 Acres Utilized: Z,'7 Z i� Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Z'� Z L/. 5 Volume applied Volume Residual Sources Soil Cond. Precip. Y t' o 9 7J � Z4 Nitrate PAN Applied Name of Crop Type (enter one) Solids/ % Applied per (NPDES #, WQ#, Past 24 co '`� w �, TKN o and (lbs/acre) Receiving Residual f, o Liquid Solids Acre Fert., Animal (Dry, Hrs. 6 a w - � N � • Nitrite Application - Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist inches * � o p mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 L'zwo J 1; 13`�ch +; :a �`'. �;' `:�i` J.�� 9CCGa.Z0__) � 0.5 35 �! tJv —A-0 h:V -g �y �j /Z'7�a'�D - � Z 'S Ct�U ^3y, ; J� 55:;= Rcoc3' 0 0,'5 0,30 t43 Y6g 1295r % wr'I:Cl7 5. v brx _61 '�,'}h.4,Mp, 4�* jS�L?�°i�' a�F"tA+R•t:^�ety„';"y?4,""�,�' <t'�"+�$�l'.s���.i�r;. $•J,,'f�ir{`��1�w,d':s�'�i'��, • +£;,'r`hY..'=`'.e+';,`:a7 V ��r�dy�i,�m.�'M(�,(''•���y;wv,4 Y6 iz-sy�,�fi".F„{�}�'rv`�.6��£R '�rM4y'.'� Y; n�,!c�.:�':'� .. .,��f^"��7��,N,J.{�,�,f�'�i3,�ir4 �-ey r`'e•'wF"$^,�ry��.,,5� t«•CJ.�.s0411 ??�h �r'_�tk:N rS�g�y. At MUM . x s �+"-. a",SY'J.. etAm'E iil4; .». ,aa,?j;'Jt7ts Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):.g `i+�wi.'!K. '=rf" r$h "r"2llwnFl „` TOTALS .r ; , br ; ::::::::... As Cd Cu Cr Pb Hg Mo Ni Se Zn P I23Z<s3:,. _ Lime Applied Annual lbs/acre !f.'dNG +... F' aY 77' x ,ro.IZ� 3/ `' �r> ;D�,L � {Rw4}rE.,� �1. 1:'b�l F�,.t��,�+:... o�6 y , ijd:#r oV,+(,6� V d `i ..Ob2 Tr4 '.fit a "' ,/.? :p k Y4" s , �« � a� ale, "N4 , .. � '^� ' :.05�� `t .T `r' IZ` .I ::::::::::::::::::.:::::::::::::::: ................. Date lbs/ac Prior Years Cumulativelbs/ac 0, 'P .Z3Z gZ."X�41. ZD .ZR 0,32 1 ••'1� fO,367 , 1P I-61�14 - Current Cumulative lbs/ac /,.,,Tyr:K ":9"s .;7,. Dr*, rlt'' {:+., n k~�P"kY' r. 23.i; 100, ,t""' k,' 3`.'N i=►.. yFi %:�.� ° !y d..a", SN •• - - -'(� ,y (�3 .r mot'. �j�/G/' el; . l �,U�I� yYn �G't�C�3f�53 Permitted C. P. L. R.**** 3 3t-1 133E Zl;i 15 — 374 ZUR ermit PA t 1st/2nd Crop PN Limit "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the• information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Bate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: C'yy�l BCLf-fi6D Total Dry Tons Applied (Annual): (v,�iZ " mit #:CCpj( Cation Exchange Capacity (non 503 only): erator: �i1 ��f1i�Y1 Owner: Cc{-*lp_� j{lD Predominant Soil Series:t� Acres Used: Z,7Z Acres Permitted: Site #: 13 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 4o-1-9 21 f {ao +4 3 4 5 6 7 8 _9j 10 11 12 % Solids 1.73'-U Arsenic C Z. 'D- < Z. Cadmium 1.1 1- 1 Copper 247 Chromium 13 Lead 1g II Mercury D, ie p. Liq Molyb- C 5 O ��. V Nickel 13 13 Selenium C 5.O <$. D Zinc ( f (061 Total Phos- )rus 7ZG2 D '1Z4.O ival Heavv Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 �7_l I - ►� /, 0 2j -Z�s-� OA 6� 3 4 v 5 6 j 7 8 9 Lj 11 J 12 y 1n L7. 350 Arsenic G, Cps C. 0.,01Z Cadmium G : CG3 D CO Z CC5 Copper D. b39 D.L177L !. Chromium C,C3 - 0;O 5 O-C(G Lead o.C6C D.C3t-1 '.4 Mercury C, , CC, 1 t COI &C&z Molyb- denumv.oi io u Nickel p, C3b D,GLS Selenium D;Cit-I C:GIO Zinc Wg I l0 1.2t 13 U `� Total Phos- phorusiZ,91 I ZL "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 7 --„ aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Signature of Land Applier 2 Zb-I Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FI-LLD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Ca)+et)�lto- m6D WQ Permit #: L,,_�CCDD!C�Ag Field #: Land Owner: (1) Annual Dry Tons Applied: 3.333 Site #: Operator:'--J�er)6e,-tM1V-) Predominant Soil Series: Crop 1 Name: Cca01aR�0n-udo - Crop 1 Max. PAN: j Qp Crop 2 Name: L4 Acres Utilized: 3.34 Acres Permitted: 3.3U Cation Exchange Capacity (non 503): 44`5 Crop 2 Max. PAN: ° y ° Q4 Volume applied (enter one) Solids/ Li uid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist Precip. Past 24 Hrs. inches Y co '� o w CL o o o N' * � o 4. :n � w �J TKN mg/kg Z a � El o � cra o c' ° W mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 �-� Wo-760 ).--)3b O-qQS NCC�-: Z17 ) dN Q S 10,5 0.38 -3W 01 1695z.: S� D•CP43 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: As Cd Cu Cr Pb Hg Mo Ni Se Zn P J-5-Z,3%-,1 Lime Applied Annual lbs/acre p.CD 0 •CCO .u93 0,024a 0.031.> -6o l O• i0 ,ot . i 6 l4-Li I I :::::: :::::::::::::. ::: ............................ Date lbs/ac Prior Years Cumulative lbs/ac p.-)3 4•G5Z 30.3Z1 '.)43 Q,►-X, C1.6CP 0.q7t) ZC6,39 Current Cumulative lbs/ac C)")41 I.9 •,SZ.y .3U -) .'1,1 0,177 Z.-AG a• 6- 3 0,qzo lib: Permitted C. P. L. R.**** 1 3 4 1 1339 1— Z.(�7 1 �J � 3A 1 Sq I Zvi mit 1 t Permit PAN Li 2nd Crop d "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation o **Volatilization Rate: Surface - 0.5. Iniection/Incoraoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Lanid-AeR-rf{ 'P Total Dry Tons Applied (Annual): a333 mit #: t,JQ 000fOU$ Cation Exchange Capacity (non 503 only): 45 ,rator: �j� `j(31111l1 Owner: �M40 1 17 Predominant Soil Series:'17 ��U� Acres Used: 3, 3A Acres Permitted: '3 Z14 Site #: {�j Field #: L� Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 Cmc_ -ig 2 3 4 5 6 7 81 91 10 11 12 % Solids ' '7 `7 Arsenic Q. 6 Cadmium i . I Copper ZLO Chromium 13 Lead j 00 MercuryL14q Molyb- NickelSeleniumZinc Total Phos- ,rus APO ival Heavv Metal Field Loadings (Calculated in lbs/acre): Total DT/Ac./ App. Event 1 n-Is , qGlg 2 3 L 4 v 5 6 7 8 _qj Loj 11 J 12 y Arsenic C),CffD Cadmium p,gD2 [:UZ Copper ,f4C(3 6 4 C13 Chromium CZI -, C , U z_L- Lead C),(Z(, C.G � Mercury C) ; CX) I D • CO l Molyb- denum O1 10 U.Ut(� Nickel G•GZI: D Selenium p:DIC) 01010 Zinc l ,Zgci A1 • GG Total Phos- phorus 5u •t-I 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. T nm aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Z--Zb-hi Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: rpn+e-)4� M61) Land Owner: a�-D Operator:F51 j Crop 1 Name:y,L WQ Permit #: V ICt4,q Field #: Annual Dry Tons Applied: 5.41 1 Site #: 5 Acres Utilized: Acres Permitted: Predominant Soil Series: ?gC-bIU5 Cation Exchange Capacity (non 503): Crop 1 Max. PAN: i Crop 2 Name: Crop 2 Max. PAN: C Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moist) Precip. past 24 Hrs. inches Y o w o o' o ?: 'Y N' w�, w * N TKN mg/kg Z 'D o ao o w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 32UX-, I2A 0.1oi MC Zv`i_) &4 © 5 1 0,.15 C),30 14-a-)40 1Zc1,f0(g ' Z3LS3 Z 1aL45= 7 ZCf W_CC37C;-J-) &[4 Q J 0-5 G. 2, 0?VP9 r ► 1 .l. 4(p Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: ) :::::::::::::: As Cd Cu CrVPb H Mo Ni Se Zn P '15,S Lime Applied Annual lbs/acre ©. O,C43 0,-)15 DTD• 5 O. 1 Z • 36 :: :::: :::::::::::::Permitted :::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0,905 44: I 0 7I 'mac 4 .1 4 .G -) M.QZZCurrent Cumulative lbs/ac ©. I (-I>I ' AY) b•544 .2,9(- •191 G• Z ,ctg i C. P. L. R.****t 3L4 13 g —16 1 3-YI ICI ZUci�' Permit PAN Limit 1 st/2nd Crop I O "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 Date ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Total Dry Tons Applied (Annual): 6 Li I J mit #: Cation Exchange Capacity (non 503 only): q.15 gyrator: Owner: Predominant Soil Series:-PCC-biU5 Acres Used:,Acres Permitted: 6 )l4 Site Field #: rj Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 61 711111 8 L9 10 111 12 % Solids i•�� �c 3`�y Arsenic <2.5 C2.5 Cadmium 1- J 1. I Copper r-4-) Chromium 1 13 Lead 1 14 Mercury O,Lrl O Molyb- <56 <denum , j Cj Nickel 13 Selenium <6. O <,j',(> Zinc iG51� Total Phos- rus ____ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Event Total Phos- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I -- aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Z-Z 6A� Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ffUp Land Owner: Cf)+6-4�cLn-0 Operator: i)ff)eebm&n Crop 1 Name: Cbc--yd 6e m 6o- WQ Permit #: c',_'QCCCIG4q Field #: {? Acres Utilized: Annual Dry Tons Applied: 15. OZO Site #: G l (ckCJ:ff Acres Permitted: Cation Exchange Capacity (non 503): Predominant Soil Series: Mrinil , Crop 1 Max. PAN n Z Crop 2 Name: Crop 2 Max. PAN: 1). 73 e1.5 ° ° r ° QWet,a Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Moist)inches Precip. Past 24 Hrs. Y -2 o w * o � w _ N' o. w =° CD w N * TKN mg/kg Z a El o � ao o w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 9-6 ZUu j.�3v :"7Zo t�C' 7b�� r xc,5,+ Q 0•5 C93 D 75� z �f 77Z arcs -I� U . o, ,W mo, C�•� o, 50 43-X+0 d . Z N CCCtW2 , 5 3U -rr� rsxic x- �3 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: As Cd Cu Cr Pb H Mo Ni Se Zn P l 31 Lime A lied Annual lbs/acre , D C• oCy5- G•Ci(oo (�,O'5C> O,6)b O.Co2 D.U9 3.050 Q,0lq Z- 3D I . 3Z ::'::::::::::::::......... :::: ......................... ......:...... ............................ Date lbs/ac Prior Years Cumulative lbs/ac O,(�(7(-I i•�Iv7 5,•25 1 Z5-bc�-1 .W(4 b•I Z Lo 5 .25g5 Z l�•G57 Current Cumulativelbs/ac ©-.h1 I �7Z Ju• I Z5-� �5•3,N pal Permitted C. P. L. R.**** 3 3 (-I f3 — Zb7 1 3-714 2nd r i PAN Limit 1st/ Crop Permit p Z "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier _2t Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorooration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: &)iTt ND M_D Total Dry Tons Applied (Annual): 1.QZD P—mit #: L;QLOQ cog Cation Exchange Capacity (non 503 only): 4. 5 -rator: " 131 ,e.C.t6 w-) Owner: rn,� DI Predominant Soil Series: Acres Used: % 7 Acres Permitted: �.7 Site #: CTrctC,Pff Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): 61FRUPTNIMON Corn- posite Date NEEMENNO MENOMONEE ual Heavy Metal Field Loadings (Calculated in lbs/acre): TotalN r 1WENEEMENEEMEN � • • TotalEvent Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Land Owner: eip` Ij Operator:'}�en-o-, �Man Crop 1 Name: M-6ff WQ Permit #: (, DO0IW9 Field #: q Annual Dry Tons Applied: 7.—�bZ Site #: Predominant Soil Series: A Iac1C�. Crop 1 Max. PAN: 1-)Z Crop 2 Name: Acres Utilized: C-TractF Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: �5•15 ° � ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources PDES #, W # Q ' Fert., Animal Waste, etc) Soil Cond. (Dry' Moist Precip. Past 24 Hrs. inches a b c 'cl o w * -� o ? ° N' m =° N * TKN mg/kg z a o El �. mgikg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 1 I 370-) rrxddi- G S O. 5 0.30 0 �Aq Zcl-SDCq , Wit - Ig Z 000 1-VIO 0.3 3 7D N664- 0 `7qg -XC4 , . ? I.Lf�ji Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: Ic✓appu :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P �It -Oc I Lime Applied Annual lbs/acre U.COs C .CD-3 0:-?Z0 C"C6Z owl �31 .035' 0.01 l 3( .......... :::::: .................. ........................... : »»>::::::::::'>:::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0,45QQ j. I .C42 ' Dq 1 5.4(,:P 0,1 0 Z,1 Z 5 Z - 8 Current Cumulativelbs/ac 0.65' --04 64- Z Zl,,•(3lC1 5.57,1 ©.N Z, 7V 5-W5 0.1666 6.-D Permitted C. P. L. R.**** 1-3 ZO 15 — 3-Y4 qC11 1 V-0 Permit PAN Limit lst/2nd Crop t Z "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier _ Z Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incort)oration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: �� �1�� (O�J� Total Dry Tons Applied (Annual): 1.1jOZ, Permit #: i,40CQI 041 Cation Exchange Capacity (non 503 only): 4. rj rator: 2) entt6-i�iOwner: (_Cll-�-� (f)�D Predominant Soil Series: �, Acres Used: 5. I ' j Acres Permitted: 6, I fj Site #: Lycacva Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 14-ID-Iq 2 LI-10-9 3 4 5 6 7j 8 9 10 11 12 % Solids I.�'��Ip i,�Y)o Arsenic Cadmium Copper ZL7 Z47 Chromium j 13 Lead I S' I q Mercury p,LCi Q,LiC Molyb- dennm <5.0 <5.0 Nickel 13 j3 Selenium <5.0 <50 Zinc Total Phos- rus o o ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total a B D MMEMEMENEEM Em no - •. Event Totalp. h .. �, "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". 6, i - a °Sj- Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION I IELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Lf)46,4� N)D WQ Permit #: IyQCptM Field #: Land Owner: e Annual Dry Tons Applied: Z. a2, Site #: Operator: ( Predominant Soil Series: Oci l ICL Crop 1 Name: C0066arben-LCk)k- Crop 1 Max. PAN: 1 (o Crop 2 Name: 13 Acres Utilized: 3, Zo —TFQCP- Acres Permitted: Cation Exchange Capacity (non 503): �, 5 Crop 2 Max. PAN: o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Co it (Dry' Moist Precip. Past 24 Hrs. inches �Y a 't? w o o w �, w CCD , �, w * w ] TKN mg/kg Z > o Q w o w mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 3E 1,%/00 1"WI , 5 dru n0.5 0,ao ,q lzq��a .(� 51� 15DUC) `7 p.3 iXC03715» D S O 5 0.30 4 i#v `?� z95� 0. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 30 As Cd Cu Cr Pb Hg Mo Ni Se Zn P Lime Applied Annuallbs/acre O• Z •33Z O.01Q zo a-Wo .0 ©. Z.: .... ..... .... ..... Date lbs/ac Prior Years Cumulative lbs/ac 03 ► ©• i 13.145 -?� Z. DC) . 0�3 i . OL)C1, ".c6cl L.N3 Zt b Current Cumulative lbs/ac o -'alo 0,-)�Fi 13.LO) Z-). ►11 333 0,p-)3 1.0 . --n q Z Permitted C. P. L. R.**** 3 3L4 i 5 — 3- I G Z Permit PAN Limit 1st/2nd Crop P I I "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation Zoo—� **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: 'C n+en nea_ty1,.� 7 Total Dry Tons Applied (Annual): Z. ZZZ 'P- -mit #: k�GCCDI DL4 Cation Exchange Capacity (non 503 only): 4'S gyrator: }henec 6mO) Owner: COnlerk(n N)Q Predominant Soil Series: Acres Used: 3.-60 Acres Permitted: 3,3.E Site #: C.'�'j��-� Field #: (� Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 2 g 3 j4 5 6 7 181 9 10 11 12 % Solids Arsenic Cz . <Z 5 Cadmium 1 . Copper ZLf-) �,W7 Chromium 1-3 Lead I (� 1 1 Mercury 0, W4 0 .L4q Molyb- < Nickel 13 13 Selenium < 5. (� <� • (� Zinc 6 I I Total Phos- 'rus Z(QU JZ(¢ 0 [ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total© D p. Event , L © © 0 - r Total Phos- • ,! • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Signature of Land Applier I,-( Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: �cr�fen4(o,rfb-0 Land Owner: , Operator,, Crop 1 Name: � Ibarq l PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: 4mcnaIoL9 Field #: 1,j Acres Utilized: Z.3-9 Annual Dry Tons Applied: A, U,3 Site #: -D Acres Permitted: Z, 3 R Predominant Soil Series: 'k(+6m� Cation Exchange Capacity (non 503): Cam- Crop 1 Max. PAN: I) (o Crop 2 Name: Crop 2 Max. PAN: 1U.5 ° y °) o M Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D ( ry' Wet' Moist Precip. Past 24 Hrs. inches a 5 �' o a? o 7y w ; N' o' o w N w TKN mg/kg Z > o on ° mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 1 3LKW I. 05ZCM 0.6 ,6 74D /)19 o bsr -lg ©DO • 3 NC� clr 5 4'g ,')2� Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS: U :: :::: As Cd Cu Cr Pb H g Mo Ni Se Zn P / .113 Lime Applied Annual lbs/acre 1 LZ47 I ,bqq ©,�3 ,022 ( 7 „5 (IU ,� ::. ...... .... ..... . Date lbs/ac Prior Years Cumulative lbs/ac Z 040 I 7. p , 2 7 g I t (_ Iri Current Cumulative lbs/ac 0. V4Z Q ; Ul 0 61 O •12 n - C6 5 L9 511 •17 Permitted C. P. L. R.**** I, r Z 7 15 Permit PAN Limit lst/2nd Crop t"1 Lo "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incoraoration - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: /f I7 Total Dry Tons Applied (Annual): (o,(. q3 permit #: k)( j=1p()-1 Cation Exchange Capacity (non 503 only): 0.15 ,rator: ?)aneubm g-k Owner: LaLea P1�0 Predominant Soil Series Acres Used: Z. 3g Acres Permitted: 2 3g Site #: T Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft Sample or Com- posite Date 1 2 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic < 2.5 <z . rj Cadmium 1. 1 1 Copper Chromium 13 13 Lead I I N Mercury C) • LJCl 0 .Lf Molyb- deniim C 6.-D Nickel I __� !3 Selenium <6. p < 5. D Zinc 661 Total Phos- rus I Z MeD I Z12LRO ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total D MENEEMEEMB - • •• Event:NMEM MRIMM� • __________ • r Total ' • • • • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". Luw Z-2 b-1 ci Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION I m .D SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: �O11t644)en- rl1 WQ Permit #: r oocopl c�4 Field #: Land Owner: �j T a F`(l�l Annual Dry Tons Applied: 6-U 0 Site #: Operator: �Ofwf 6-oi�Lh Predominant Soil Series: McQa, Crop 1 Name: CCX % i Crop 1 Max. PAN: 11Z Crop 2 Name: Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Z9Q Z.r'/25 �• 5 o � ° ° Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, Moist Precip. Past 24 Hrs. inches a 4 '� F '� o cw �. o' ° o 7* ` N' 4. � w CD w * N TKN mg/kg Z a 3 o a oe o w. mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 17 Crop 2 Crop 1 Crop 2 4�Ccxj r)3`7c) C). 0, 0 36U r I (QZ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: U ::: As Cd Cu Cr Pb H.21 Mo Ni Se Zn P Lime Applied Annual lbs/acre 0.00(v 0-00 0.614 O.Cbb 0.04Z 0• OD 10,D)Z O•Ca0 O.OIZ ::::::::...... .................. ::::::::::::::::::::::::::: ........................... ::::::::::::::::::::::::::::::::::::::::.: :::::::: : Date lbs/ac Prior Years Cumulative lbs/ac 0,76Z 7G ,14q 7g� Z•141a ,03Z O-602 -Q-9 0.3�� f 1 (o Current Cumulative lbs/ac . Z6 0 - -b s .b4Z .49 1-) Z • lO o..033 •6ILI Z. SI Z .t-Ia 1 ,.:::<::::' Permitted C. P. L. R.**** U t3' 7 t �.. qS S Permit PAN Limit t 2 1 s / nd Crop n Z "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant LoadinL3 Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name:Total Dry Tons Applied (Annual): 3_063 Do-mit #: Cation Exchange Capacity (non 503 only): q- •5 ;rator: Its Owner: C)C n� en�eD (fl _D Predominant Soil Series: k1 gL2Ck, Acres Used: Z,CI g Acres Permitted: i_q g Site #: 7 Field #: 1 C, Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 81 9 10 11 12 % Solids Arsenic Cadmium . Copper IC�7 Chromium )3 Lead 110 Mercury 0, LP Molyb- denurn <5. a Nickel 13 Selenium <� Zinc 1 Total Phos- rus I MOO ual Heavy Metal Field Loadings (Calculated in lbs/acre): TotalMoon D .,p o© o 0 0 0 - OEM TotalEvent Phos- __phorusW,EEEEEEEEEEEN "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i sonment for knowing violations". Signature of Land Applier z--Z10- 1 q Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION F MILD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ocnfff *,a,)— ftD WQ Permit #: N)()0jlCJR Field #: Land Owner: 1 Annual D Tons Applied: zk` Y" �i"� N-f' 1 °1`Q. (/l�� Dry PP • ix. �.�. r.��1���ln:'�>�; Site #: Operator:--Rene—�&njsh Predominant Soil Series: Crop 1 Name: Oaic&r ilk Crop 1 Max. PAN: 1/)�& Crop 2 Name: 17 Acres Utilized: j7 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Volume applied . Volume Residual Sources Soil Precip. o Z Nitrate PAN Applied Name of Crop Type 0 9.1(enter one) Solids/ % Applied per (NPDES #, WQ# Cond. Past 24 a '� w w' w TKN -+ o and Receiving Residual ° Liquid Solids Acre Fert., Animal (Dry, Hrs. o� w ; cc ?j * N' o� $ w• Nitrite (lbs/acre) Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet' Moist inches o p 10 * o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2 -14 &OD6 o A<<`' NCC03W-1 moil I Q 5 0.'5 O•ZO RFD 95D-GS :` .. 3 I-Z370 --pt) ' - 4 7 car&+ Cx,5 0,30 JZMQS y m WIN,s/Kz't ''x Ati}Fdl,"Lf`j ^arl>b �>.ai,•j+*a'x/`!" .,}� i'�w`�;�EJrM1S°t'�'t•s,+'T�`�'a� h ! � ;Tif' 3'S:? P R��r"„1r k�'+7 on � 3��X;"+S;wyf :;"i'Jf'�;'. t ' Y.'.` s?,j'�'�":c;�`"y"a;'a�r'�: >b,%.'4�;'s:%,G. �f �:=�'.,�•J�t�`�e,'3X: ti/a:,j.r -- .........`.aRs'zinrv'�rk : �p�',Qe�� a';kys',i.,.y>tu'!. ��5,;, � ,r - � ..::::::::::. T4"ea.'F ., �, ..I;. (} ,;_ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): r�i y..� `61^t.� �>''iv'ds-i<Y`.�,`E� v � s f ,�a� �, . .:::...........=»: : TOTALS: $- ; ' ".F ., , As Cd Cu Cr Pb Hg Mo Ni Se Zn P <) . ' `' x; Lime A lied Annual lbs/acre ,vlyic�' p ,,t.ilx.7.xr Yr' •ey ?3 5i;-+• } _^}�"t Yt ,O�-'i'i�^` r ":�Xx.i,'lr;�"•Yo!Os �:n, ": y.^i"^` .- r( - . ,. 3,'€:..a ) $f il :> *; ? Sjzf:a''"'x'I` 'fi,�.'i Date lbs/ac Prior Years Cumulative lbs/ac ,-'626 D.Lni 46•l tI•g iq Z• 41 DIC4Z (o &20S 0.61516g. Current Cumulative lbs/ac m I 0.::.,'Z,r:t3c. 7 1.:1..$5..t�Z. 3c`i9.�l�kOx ,.e.. ;. ,.{',•.+' :'f' 21.,ZU:S.O.3DI►co�.- .�" .t3k ;.arx'r'^>`a`v .r, 1,_. ,a,..,,...:<an> i� Permitted C. P. L. R.**** %3L � — 'UeQ t G Z 't Permit PAN Lima lst/2nd Crop P :.. ,p.,:4.-SW „, �. v , l F kt r �f ✓u . .Z , x. . �,:' �.. F�r. "ff C'` ±.r.l "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: 1f n tmSD Total Dry Tons Applied (Annual): 5, IP4 permit #: Cation Exchange Capacity (non 503 only): q. 6 :rator: Owner: Off-Apra-ntc,_rfXili Predominant Soil Series: 4 ICkoa- Acres Used: 3.1Q2 Acres Permitted: 3,102 Site #: Field #: 1) Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 q_,C�_) g 2 ig 3 4 51 6 7 81 9 10 11 12 % Solids Arsenic <Z.5 <2.5 Cadmium I,1 1.1 Copper Chromium 13 I Lead Mercury . Qq Molyb- denum Nickel I Selenium <5.D <5.p Zinc 1061 1 Total Phos- rus i 2721bb ual Heavy Metal Field Loadings (Calculated in lbs/acre): •. o © © o © on m • iv . We To al Phos- phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and it sonment for knowing violations". " -_ ""Wuk- _ 242_166l Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION HELD. SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: 02n�� WQ Permit #: �� j ( g Field #: Ce�� enApplied: Land Owner: K),6 l Annual Dry Tons `r, l Cf s''`'u' k `' "`' Site #: Operator:'`�o-)& 6m4k) Predominant Soil Series: Crop 1 Name: Crop 1 Max. PAN: hZ Crop 2 Name: 1 q Acres Utilized: C`('rccj-ff Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Volume applied pp Volume Residual Sources Soil Precip. Y 2. o Z Y Nitrate PAN Applied Name of Crop Type o � (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 � � a 5 7y w 7y � P �, TKN � � o and Receiving Residual ° ° Liquid Solids Acre Fert., Animal wry' Hrs. a w o Nitrite (lbs/acre) Application Q Waste, etc) Wet, 0 o R. Cu. Yds Gallons (Dry Tons/Ac) Moist inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 -413 ,6�0 1.-W tIcoo3Zo---) di O S 06 D-b 74 •S.r* ; S: �.:.tYagP..yb ;�,"�.{"y'i S'�S+'C,"; ',h .:.f c��:�;K�j!,:�. c�!:i,�.i1�:f'T�`i.i°,^e✓I%' `a';.,i:;Li°a. �'^.it',�� ,t .`:" -''fin. Y,,'d,'�f.`"rc-b`•T*i", i. N�3�":,u`•"y,> .x ":?.'.:.r;:,F:%� 'l `t':.:'il �.`;i.?r:, ��4 ' ,��� iM�ria;�,„5rj:;"^vwYy�r� �r.�:;:`;�`r'(� _-•�:rj€�?a„'? rk'+,a-w °,�r-u?:.l:'s,r;4z,+kt .�,2�a4,�.+.u�a ' '. '. '%i �` y:"itt C., FSo - p.4 x''4 Residuals Applications totals on FORM FSF supp (attach FORM FSF su to this form):-1 .t;� sT.£5 �'rt `r' w ;r , "�•" ^`,"::,F"",... '.,,,-t:.� . ppp ,.rig., aN TOTALS: Wt.�1_ F6,1`566% As Cd Cu Cr Pb H Mo Ni Se Zn P P `+.. I.rc R;ff� _„ Lime A lied : F.,:c , Annual lbs/acre ;a:i ( vZ. C? w1.;3 -•'-. i ° 17 F ! G i , - -. Date lbs/ac Prior Years Cumulative lbs/ac 3L,, 1 34 I. 36 m" Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop % r^. .,: "I certify, under.penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation Z&7'1 **Volatilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (1212006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Oc�nI-d-4flffuTOP Total Dry Tons Applied (Annual): L/, )L41? permit #: tJQOC9b1Q 1 Cation Exchange Capacity (non 503 only): U_ rj gyrator: Owner: Or f ety�( ' Predominant Soil Series: A �aC Acres Used: 1I,-5 Acres Permitted: Site #: CTraC47L Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 8 9 10 11 12 % Solids Arsenic <1-115 Cadmium 1, 1 Copper � Chromium 1 'j Lead le Mercury p,Lp Molyb- denum <5. n Nickel -5 Selenium <5. p Zinc 61 Total Phos- rus Z7�C7 ual Heavy Metal Field Loadings (Calculated in lbs/acre): Total I 1 2 3 5 6 7 8 9 10 11 12 _4j y DT/Ac./ g Zq-Ig C y App. Event o, 26-3 35 Arsenic YJZ Z Cadmium C), CC I I Copper 0, Chromium Lead , O13 O • v13 Mercury ©, CC>O O , 00c) Molyb- OoC04 0 cc" Nickel p, (,.GYM/ Selenium ©, C L p , Zinc C.L41VO 10 4 Total Phos- phorus . ZU icl. Cn "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and i isonment for knowing violations". zz%orJF Signature of Land Applier Date DENR FORM MFLSF (12/2006) PATHOGEN AND VECTOR l_ ATTRACTION REDUCTION FORM ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Contentnea MSD WWTP Name: Contentnea MSD Monitoring Period: i From 1/1/2018 To WQ Permit Number: NPDES Number: 12/31/2018 WQ0001048 NCO032077 ,(, c A nrr A P n2T 11061 _ Plense indicate level achieved and alternative performed: Yi11IlO�C11 1<CUUGUVu Class A: `1JA 1\t.L1v vr, a •_+��� Alt. A (time/temp) ❑ - ------------- Alt B (Alk Treatment) ❑ - Alt. C (Prior Testing)❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ElHeat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density .0 1 Alt. (2) Process to Significantly Reduce Pathogens ❑....77 If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": .S Lime Stabilization ❑ Air Drying [3 Composting ❑ Aerobic Digestion Anaerobic Digestion ' i es i n [Ig If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Number of Analytical Allowable Level Pathogen Density Frequency Sample � Parameter Excee- of Analysis Type Tech - in Sludge Minimum Geo. Mean Maxi Units 2x10tothe MPN <11 117 MPK�1420 .� 0 7 Grab f�� ►> -a, 6th power per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight)t v ector titu-ac11U11 XXUUUW.ilVu Alt.l (VS reduction) ❑ `iJ -1 -1-- Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) [3Alt. 4 (Spec. Oz uptake) 0 Alt. 5 (14-Day Aerobic) [3Alt. 6 (Alk. Stabilization [3Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Inj ection) � [3 Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed [3 CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Renee Smith/Land Application ORC Renee Smith/Land Application ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Y�l Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) EWOmEHM % hm * ^ P O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 TOW CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Sample Analysis Method //1 Date Analyst Code Total Residue, mg/1 17520 04/02/18 KDS 2540B-11 Fecal Coliform (MPH /gram Solids 451 04/02/18 KDS 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 FAX (252) 756 0633 ID#: 416 A DATE COLLECTED: 04/02/18 DATE REPORTED : 04/03/18 REVIEWED BY: EnAmNE&W % hw P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 TOW CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method ##2 Date Analyst Code 17680 04/03/18 JMT 2540B-11 130 04/05/18 JMT 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/03/18 DATE REPORTED : 04/06/18 REVIEWED BY: ., ., - n n - -- - — A — -fl GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPH /gram Solids Sample Analysis Method #3 Date Analyst Code 17220 04/04/18 AKS 2540B-11 64 04/04/18 AKS 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/04/18 DATE REPORTED : 04/09/18 REVIEWED BY: ElMommmo % hCupund P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/1 Fecal Coliform (MPN), /gram Solids Sample Analysis Method ##4 Date Analyst Code 16900 04/09/18 KDS 2540B-11 77 04/09/18 KDS 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/09/18 DATE REPORTED : 04/12/18 REVIEWED BY: ��dor�o��c��� Flo D��oQpor�a�c�d P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (MPN), /gram Solids Sample Analysis Method #5 Date Analyst Code 16580 04/10/18 JMT 2540B-11 66 04/12/18 JMT 9221E-06 Drinking Water ID: 37715 Wastewater ID: 10 U N E (252) 756 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/10/18 DATE REPORTED : 04/12/18 REVIEWED BY: poQ��c�d P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Total Residue, mg/l Fecal Coliform (M N), /gram Solids Sample Analysis Method #6 Date Analyst Code 16880 04/11/18 KDS 2540B-11 1420 04/11/18 KDS 9221E-06 Drinking Water in: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/11/18 DATE REPORTED : 04/16/18 REVIEWED BY: EWOTummid alp hcqwpowm%d P.O. BOX 7085, 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Sample Analysis Method PARAMETERS #7 Date Analyst Code Total Residue, mg/1 16780 04/16/18 KDS 2540B-11 Fecal Coliform (MPN), /gram Solids <11 04/16/18 KDS 9221E-06 " Drinking Water ID: 37715 Wastewater ID: 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 A DATE COLLECTED: 04/16/18 DATE REPORTED : 04/18/18 REVIEWED BY: Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: CMSD Biosolids Permit Number: WO00 Date: Digester Temperature: Sampling Date/Time: 4-2-18 Sampled By: Andre Analysis Date/Time: 4-2-1 E Analyzed By: Windy Sample Volume: Total Solids: Beginning Temperature'. End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 1' 131 ✓ Edwards '1322 Sammond 000 milliliters 1.88 % Dry Solids 19 degrees Celsius 21 degrees Celsius 0.1 8.5 1.0 4.49 mg Oxygen/hr 0.24 mg Oxygen/g/hr 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Rate:r 0.24 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically y =-0.0749x + 8.621 Oxygen Uptake Rate Chart 8.8 I 8.6 8.4 8.2 a� 8 7.8 x O -a 7.6 cn 0uw 7.4 7.2 7 i 6.8 6.6 1 2 3 4 5 6 7 g g 10 11 12 13 14 15 16 Time (minutes) Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: CMSD Biosolids Permit Number: WQ00 Date: Digester Temperature: Sampling Date/Time: 4-3-1 E Sampled By: Andre Analysis Date/Time: 4-3-1 f Analyzed By: Windy Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: Sam 000 milliliters 1.82 % Dry Solids 19 degrees Celsius 20 degrees Celsius 0.1 8.6 1.0 4.64 mg Oxygen/hr 0.26 mg Oxygen/g/hr 20 degrees Celsius 1 Temperature Corrected Specific Oxygen Uptake Ratel 0.0 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. y =-0.0774x + 8.6615 Oxygen Uptake Rate Chart 8.8 8.6 8.4 - -- 8.2 a� 8 E c 7.8 T X 0 -a 7.6 a� 0 N 7.4 0 7.2 7 6.8 6.6 3 4 5 6 7 8 g 10 11 12 13 14 15 16 1 2 4 Time (minutes) Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: CMSD WQ0001 4 4-4- And 4-4- Biosolids Permit Number: 048 Date: /4/2018 Digester Temperature: 18 Sampling Date/Time: 18/1312 Sampled By: rew Edwards Analysis Date/Time: 18/1319 Analyzed By: Windy Sammond Sample Volume: 1000 milliliters Total Solids: 1.8 % Dry Solids Beginning Temperature: 20 degrees Celsius End Temperature: 21 degrees Celsius Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: 0.1 8.2 1.0 Oxygen Uptake Rate: 5.14 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.29 mg Oxygen/g/hr Average Temperature: 21 degrees Celsius Temperature Correction Factor: 0.952380952 Temperature Corrected Specific Oxygen Uptake Rate:j 0.27 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 0 8.5 a Oxygen Uptake Rate Chart 1 2 3 4 5 6 / b 0 Time (minutes) y =-0.0857x + 8.2493 Time (minutes) 0 1 2 3 4 5 6 7 8 .g 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level . Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0001048 rew 1000 milliliters 1.8 % Dry Solids 18 degrees Celsius 18 degrees Celsius 0.1 8.6 1.0 3.28 mg Oxygen/hr 0.18 mg Oxygen/g/hr 18 degrees Celsius 1.1449 Temperature Corrected Specific Oxygen Uptake Rate: 0.21 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. M F.M. 8.4 a 8.2 E O m 0 N 7.8 0 W. 7.L 7.: Oxygen Uptake Rate Chart 1 2 3 4 5 6 0 V l„ - Time (minutes) y =-0.0546x + 8.6653 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: . Total Solids: Beginning Temperature: End Temperature Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: Q0001048 4/16/201 119 16-18/ idrew 16A 8 enee milliliters % Dry Solids degrees Celsius degrees Celsius Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 0.1 7.0 1.0 4.70 mg Oxygen/hr 0.27 mg Oxygen/g/hr 19 degrees Celsius 1.07 Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 13 7 I a 5 E Oxygen Uptake Rate Chart 1 2 3 4 5 6 a v (- Time (minutes) y =-0.0784x + 7.0935 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: CMSD Biosolids Permit Number: WQ0001048 nnta 4/17/201 Digester Temperature: Sampling Date/Time: 4-17-18/1020 Sampled By: Kyle Huggins Analysis Date/Time: 4-17-18/103C Analyzed By: Renee Smith Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 1000 milliliters 1.8 % Dry Solids 17 degrees Celsius 19 degrees Celsius Slope: 0.1 Intercept: 7.9 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 3.48 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.19 mg Oxygen/g/hr Average Temperature: 18 degrees Celsius Temperature Correction Factor: 1.1449 Temperature Corrected Specific Oxygen Uptake Ratei u mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 7.8 7.6 "a 7.4 E 6.E M, l Oxygen Uptake Rate Chart 2 3 4 5 6 o C, ,- Time (minutes) y =-0.058x + 7.9402 . Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: CMSU Biosolids Permit Number: WQ0001048 Date: 4/18/201 Digester Temperature: 1 Sampling Date/Time: 4-18-18/1035 Sampled By: Andrew Edwards Analysis Date/Time: 4-18-18/1045 Analyzed By: Renee Smith Sample Volume: 10( Total Solids: 1 Beginning Temperature: End Temperature: Dissolved Oxygen Level milliliters % Dry Solids degrees Celsius rIParees Celsius Slope:. 0.1 Intercept: 7.7 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 4.48 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 0.25 mg Oxygen/g/hr Average Temperature: 19 degrees Celsius Temperature Correction Factor: 1.07 Temperature Corrected Specific Oxygen Uptake Ratel 0.27 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation.and the Spreadsheet execute automatically. ►M 7.6 7.4 7.2 0 E m 7 a� X 0 6.8 0 N N a, on Oxygen Uptake Rate Chart 1 2 3 4 5 6 / 0 Z7 1, " Time (minutes) y =-0.0747x + 7.7778 GROUNDWATER MONITORING LAB REPORTS. GW-59•A COMPLIANCE REPORT FORM Permit 9000ODIC Z (Submit one each nionitorinb period with GJV-59 for•nis.) Enter date monitoring results were due. (,3-�1-I� ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? Was any required information missing on the GW-59 report forms? YES 2 IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information, 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missiieg cap, missing I YES I NO identification plate, area overgrown, ete.)? If the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YJS NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: �j211 � ►O C�romiurn t�uq IL 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO , skip to section 8. ce provided below, each well with constituents) exceeding If the answer to question 5 is "YES", list in the spa standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). oell-010 ChfD3niulm 14ug1(- (p-Z�-11 tt}211 -I-10 a-)rcv) i Li.i) 15LIg l C ��-II-i� I.�-en Flo Ci,fcm�urn t��tg1L Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES I N If the answer is "YES', a groundwater quality problem may be occurring. CONTACT THE REGIONAL is "NO", monitoring wells may be.improperly OFFICE IMMEDIATELY FOR GUIDANCE. if the answer located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. "NO", the Regional Office within 90 days an evaluation maybe If the answer to question 7 is contact ad to determine the impact the waste disposal system is having at the review and compliance re uir boundaries s urrounding this facility. Failure to do so ma subject the permittee to a Notice of Violation fines and/or penalties. , -hern4C, r )C0 '1 Cr 011Ci- eN CJU(l f The completing this portion (GW-59A) of the monitoring report should sign below and submit this g person form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. ..Fr��u...-•- • �"" - '"`nwas�evaluateii=sand-tiie�nfo�mation_subm�tted;�n4this,�:,: Lheretyacknowledg%:thatthe above informatio�,�§,�,;,, �eport'(C"oinp nc R`eport:GW59A)`st�ue;and;complete:toahe:best_of=my.:knowledge p lsk-- Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YEL­..'APER ONLY OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES DEPARTMENT INFORMATION PROCESSING UNIT GROUNDWATER QUALITY MONITORING: 1617 MAIL SERVICE CENTER, RALEIGH, NC 2768,Phone: 919.607-6306 COMPLIANCE REPORT FORM Please Print Clearly or Type PERMIT Number: Expiration Date: 1-ZD70 FACILITY INFORMATION Non -Discharge i.JQ�[O!-I�� UIC (-���� ^„ �-� Facility Name: I` �'� N PDES j--! CLY��-Z(S� Other Permit Name (if different): rn� I�I�L ��� TYPE OF PERMITTED OPERATION BEING MONITORED (�.' Facility Address: C(c)O L+�i�"C=PC �(i�t� strZ 530 County Lagoon ❑ Remediation: Infiltration Gallery ,;,,,,;, ,.... ❑ Spray Field ❑ Remediation: ,,, iv. �en ��ml Telephone#: Z�Z�7s� LI ❑ Rotary Distributor Land Application of Sludge Contact Person: Name: ' 2CC D��[Q�li �( - f wells to be sampled: 6 No. owe ❑ Water Source Heat Pump Other: Well Location/Site (from Permit) If WELL SAMPLING INFORMATION WELL ID NUMBER (from Permit): G Date sample collected: z"ZD I�i FIELD ANALYSES: WAS ooaoo: L CJC_i units Temp. 00010: I os -C DRY at Well Depth: �ft. Well Diameter: Z in. Screened Interval: 3 ft. to �ft. pH . time of ��, rµMhos Spec. Cond. 00094: sampling, Depth to Water Level 82546: � ft. below measuring point ft. Odor 00085: nont check Measuring Point is Z.'7 ft. above land surface Relative M.P. Elevation: Appearance here: El Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: [)I YES ❑ NO and field acidified: ®YES ❑ No LABORATORY INFORMATION Name: 1�11(C(�i n�+1 �" Certification No. 10 Date sample analyzed: 7-Zb-1 Laboratory J� PARAMETERS NOTE: Values should reflect dissolved and colloidal. concentrations. mg/L Pb - Lead D1051 ug/L COD 00335 mg/L Coliform: MF Fecal 31616 C ` /100mL Nitrite (NO2) as N OD615 Nitrate (NO3) as N 00620 Q•�o mg/L Zn -Zinc o10s2 mglL Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 O mg/L mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 a . issolved Solids:Total 70300 �?(.v mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 . t4q units Ba - Barium 01007 ug/L TOC 006Bo mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 CD,Q[Q mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 mg/L ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L Fe - Iron 01045 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L Hg - Mercury 71900 mg/L VOC 7873 method # pecific Conductance Doo95 �Q,Fj tLMhos Total Ammonia 00610 O, Ym9 /L K - Potassium 00937 Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese olo5s ug/L , method # N 5 mall_ Ni - Nickel 01067 ug/L method # TKN as oos2 For Remediation Systems Only (Attach Lab Reports) Influent Total VOCS: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORI Facility Name: Permit Name (if di Facility Address: T Please Print Clearly or Type e Ij 1p, :_Ip, SUBMIT FORM ON YEL 3APER ONLY Contact Person: iL°� (�li Telephone#: Zd2-57-LE Well Location/Site Name: '_� O l e� (_ No. of wells to be sampled: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV.OF WATER-REsuurcct_: INFORMATION PROCESSINGUNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919.007.6306 PERMIT Number: Expiration Date: I-a(-ZOZD Non -Discharge WQ 0001 OC-I- UIC NPDES 1_1CCC)a20-)7 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): I � Date sample collected: Z-Zv--19 Well Depth: Qft. Well Diameter: z in. Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: Z ft. to ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samoles for metals were collected unfiltered: [2 YES ❑ NO and field acidified: ®YES ❑ NO If WELL FIELD ANALYSES: WAS PH 00400: L. C 1 units Temp. 00010: 1,5 oC DRY at time of Spec. Cond. 000sa: 7. y µMhos sampling, Odor 00085: n check Appearance here:❑ LABORATORY INFORMATION Date sample analyzed: Z Zo--I Laboratory Name: ( --�j wf) 6)enj / PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb - Lead 01051 COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 C /100mL Nitrate (NO3) as N 00620 % Q mg/L Zn - Zinc 01092 Coliform: MF Total 31504 /1r%n I Phosphorus: Total as P 00665 mg/L MPIN method for highly turbid samples) O tho hos hate 70507 �, G3 mg/L Other (Specify Compounds and Concentration Units): (Note. use roml r p p issolved Solids:Total 70300 59 mg/L Al - Aluminum 01105 mg/L PH (Lab) 00403 G-0 units Ba - Barium 01007 ug/L TOC 00680 3 . �j��j mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Ch i m Total0103a l5 ug/L Certification No. I0 ug/L mg/L Arsenic 01002 ug/L mg/L Cu - Copper 01042 �O,OCD mg/L - ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L Fe - Iron 01045 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L Hg - Mercury 71900 mg/L VOC 7873 method # pecific Conductance 00095 �1 •u µMhos K - Potassium 00937 Total Ammonia 00610 <O. 0LA mg/L Mg - Magnesium 00927 mg/L method # method # (Ammonia Nitrogen: NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Effluent Total VOCs: mg/L VOC Removal% Influent Total VOCs: mg/L Permittee (or Authorized Agent) Name ana i uic - rnca— N...., rN GW-59 Rev.3-1-2016 SUBMIT FORM ON YEL__ 'APER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM - __ _ .. Please Print Clearly or Type Facility Name: Permit Name (if di Facility Address: 1® Contact Person: -P) e n-e 6r^fl l Telephone#: ZFJZ �ZLI- �u Well Location/Site Name: 6 C5+1 Nay No. of wells to be sampled: 5 (from Permit) DEPARTMENT OF ENVIRONMENTAL QUAY - DIW OF WATER: RESOURCES INFORMATION PROCESSING UNIT. 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 'Phone:919-807-6306 PERMIT Number: Expiration Date: Non -Discharge )C)1_0� UIC NPDES pC0037_o�-) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery I ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): i A Date sample collected: 2 Z . Well Depth: �ft. Well Diameter: Z in. Depth to Water Level 82546: [C), I-j ft. below measuring point Screened Interval: ft, to ft. Measuring Point is Z. ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: ®YES El NO FIELD ANALYSES: WAS 1 pH ooaoo: y �j units Temp. 00010: °C DRY at time of Spec. Cond. 00094: 10Z1 µMhos sampling, Odor 00085: ncn-5— check Appearance C) f here:❑ LABORATORY INFORMATION Laboratory Name: & Date sample analyzed: 2-zC3 1 �5� iTll (C�lfilC'1�� PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. /L Pb - Lead o1051 COD 00335 mg/L Nitrite (NO2) as N 00615 m9 Coliform: MF Fecal 31616 < ! /100mL Nitrate (NO3) as N 00620 3.L( p mg/L Zn -Zinc o1os2 /L Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) solved Solids:Total 70300 L4—) mg/L pH (Lab) 00403 4 -G 5 units TOC 00680 } . U (p mg/L Chloride 00940 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L )ecific Conductance 00095 �Z,(� ILMhos Total Ammonia oo610 �U• �U mg/L (Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total) TKN as N 00625 mg/L Phosphorus: Total as P 00665 mg Orthophosphate 70507 mg/L AI - Aluminum 01105 mg/L Ba - Barium 01007 ug/L Ca - Calcium oo916 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 '� ug/L Cu - Copper 01042 CG, OIL mg/L Fe - Iron 01045 ug/L Hg - Mercury 71900 ug/L K - Potassium 00937 mg/L Mg - Magnesium 00927 mg/L Mn - Manganese o1o55 ug/L Ni - Nickel 01067 ug/L For Remediation Systems Only (Attach Lab Reports):. Influent Total VOCs Certification No. I D ug/L mg/L Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # and that the laboratory analytical data ility of fines and imprisonment for knc JEWIF' 1 mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title - Please print or type - GW-59 Rev.3-1-2016 SUBMIT FORM ON YEL_ - 'APER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM _. _.. Please Print Clearly or Type Facility Name: Permit Name (if di Facility Address: ontact Person: Telephone#: fell Location/Site Name: iil-4e(6(' J iCi)u2lGlu V�21Gi0 No. of wells to be sampled: 5 (from Permit) DEPARTMENT OF ENVIRONMENTAL QUALITY- DIV. OF WATER RE5UUKct INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH,NC 27699-1617 Phone: 919-807-6306 PERMIT Number: Expiration Date: 1 31- L)L0 _ Non -Discharge L600000U06 UIC NPDES pCoCa2o— �D Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMAL IUN WELL ID NUMBER (from Permit):. 15 Date sample collected: -Z(} la, ft. Well Diameter: Z in. Well Depth: Depth to Water Level 62546: Le ft. below measuring point Screened Interval: J ft. to ft. Measuring Point is Z . 5 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samoles for metals were collected unfiltered: ® YES ❑ NO and field acidified: ©YES El NO If WELL FIELD ANALYSES: WAS pH 00400: 49 units Temp. 00010: 'C DRY at time of Spec. Cond. 00094: ��.ej µMhos u� t g sampling, Odol' 00085:'� check Appearance c� (�i here:11 LABORATORY INFORMATION Laboratory Name: F-mi tcnment TI lr. l� Date sample analyzed: 7= Z�" - PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb - Lead olos1 COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N ooszo D �2 mg/L Zn - Zinc 01092 T t I P 00665 mg/L s Certification No. _ k) ug/L mg/L Coliform: MF Total 31504 /100mL Phosphorus. o a a b d les) h h t 7oso7 d - GZ mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly tur i samp Orthop osp a e issolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 (� Ct units Ba - Barium 01007 ug/L TOC 00680 . �j� mg/L Ca - Calcium 00816 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L T t 1 --A 4 ug/L Arsenic 01002 ug/L Chromium. o a Cu - Copper 01042 <p.0 i O mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils m /L 9 uglL (Specify test and method #. ATTACH LAB REPORT.) 32730 Phenol 273o uglL Fe -Iron oloas ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L Hg - Mercury 71900 mg/L VOC 7873 method # pecific Conductance 000ss '%�h (� ItMhos K - Potassium 00937 # Total Ammonia 00610 D.ZS mg/L Mg - Magnesium 00927 mg/L ,method method # (Ammonia Nitrogen; NH, as N: Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , m /L Ni - Nickel 01067 ug/L method # TKN as N 00625 g For Remediation Systems Only (Attach Lab Reports) Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.3-1-2016 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORI Facility Name: Permit Name (if di Facility Address: Print Clearly or Type SUBMIT FORM ON YELL_ 'APER ONLY tact Person: �} Pf j� I Telephone#: �Z-1Zu- I Location/Site Name: 0 ©-�- 21 E'_ 1 Ch i 13 No. of wells to be sampled: DEPARTMENT OF ENVIRON MENTAL. QUALITY- DIWOF WATER RF=UUUKets INFORMATION PROCESSING`UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617Phone: 919-807=6306 _. PERMIT Number: Expiration Date: I-r�il-7U7C7 Non -Discharge lJ0QCGI0Q.' UIC NPDES zlnf ) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ® Land Application of Sludge ❑ Water Source Heat Pump 0 Other: SAMPLING INFORMA I IUN WELL ID NUMBER (from Permit): 1 Date sample collected: 7- /�-I Well Depth: }(D ft. Well Diameter: z in. Depth to Water Level 82546: °) ft. below measuring point Screened Interval: �J ft. to 10 ft. Measuring Point is -_ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 15 gallons Samoles for metals were collected unfiltered: Q YES El NO and field acidified: ®YES El NO If WELL FIELD ANALYSES: WAS oC DRY at pH ooaoo: , units Temp. 00010: time of Spec. Cond. 00094: LP µMhos sampling, P 9, Odor OD085: none- check Appearance u P cd here: ❑ LABORATORY INFORMATION � 2U-� � Laboratory Name: I (On��� j T I , nC. Certification No. )� Date sample analyzed: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb - Lead 01051 ug/L COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Zn - Zinc 01092 mg/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 6 . (� 1 mg/L I issolved Solids:Total 70300 aq mg/L AI - Aluminum 01105 mg/L (Lab) 00403 IWO units Ba - Barium 01007 ug/L pH TOC omm mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L ug/L Chromium: Total 01034 (-P ug/L Arsenic 01002 mg/L Cu - Copper 01042 40.CU1c> mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L Fe - Iron 01045 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L Hg - Mercury 7190D mg/L VOC 7873 method # pecific Conductance 00095 FLMhos K - Potassium 00937 Total Ammonia ooslo O.OIv m9 /L Mg - Magnesium 00927 mg/L method # method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L , TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports; --,I)e fLA- �I4-h (sand Rcn Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 Influent Total VOCs: mg/L Effluent Total VOCS: mg/L VOC Removal% EWMENUMIMI� Flo hwPOTMd tk P.O. BOX 7085; 114 OAKMONT DRIVE GREENVILLE, N.C. 27835-7085 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 02/20/18 DATE REPORTED : 03/08/18 REVIEWED BY: Well Well Well Well Well Analysis Method PARAMETERS #9 #10 #14 #15 #18 Date Analyst Code < 1 < 1 < 1 < 1 < 1 02/20/18 KAC 9222D-97 Fecal Coliform (MF), /100 Mls <0.04 <0.04 0.25 0.06 03/06/18 MF 350.1 R2-93 Ammonia Nitrogen as N, mg/1 0.37 0.28 0.46 0.52 0.04 02/28/18 DTL 353.2 R2-93 Nitrate Nitrogen as N, mg/l 0.06 3.59 1.46 9.58 6.75 02/21/18 SEJ 531OC-11 Total Organic Carbon, mg/l 8.82 47 95 129 02/22/18 KAC 2540C-11 'otal Dissolved Residue, mg/l 76 54 8 6 02/26/18 LFJ EPA200.7 .'otal Chromium, ug/l 9 15 < 10 7 < 10 < 10 < 10 02/26/18 LFJ EPA200.7 Copper, ug/l < 10 80.5 57.4 62.4 78.0 149 02/26/18 JTH 251OB-11 Conductivity (at 25c), uMhos/cm 0.02 0.02 0.01 02/21/18 SEJ 450OPE-11 Total Ortho-Phosphate as P, mg/l 0.02 0.03 GW-59A COMPLIANCE REPORT FORM Permit # I ') O20 U'2 (Submit one each monitoring period with GW-59 fnrms.) Enter date monitoring results were due. ( )Will this monitoring report (GW-59 and GW-59A) YES NO V be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing is "Yes", contact the Regional Office for guidance. YES NO x identification plate, area overgrown, etc.)? If the answer 4 Are any monitored constituents equal to or above the established standards? YTS NO X If the answer to question 4 is "NO , skip to section 8. /f fhe answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrafion(s) exceeding standards in ,the space, provided below: 6,?(�11 _oG io•��1� � GG CI-a2 11L Weil -A-10 Chrorn►uin Ilou IL For the constituents identified in question 4 above, have standards been exceeded previously for the YE$ NO \i/ 5 same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO'; skip to section 8. If the answer to question 5 is "YES" list in the space provided below, each well with constifuent(s) exceeding date for each occurrence (for the fast two years). standards, concentrations) reported, and sample collection P31)Zn-q1L i-29-1t.' eq � S G lo,lt�l, r lc. -il�-icy oel)-woomNl r\ 15+0 'f GG ta.50K-q/L o-31-A0 IL I I t 0 ChrOm um I U u� I L "L-ZZ-�% Z Zo I 16c, V,4 C)rom'lum it- -1•C'�C, �lz-IZrs�gl� � zN� C�ram��r'� Are the monitoring wells listed in section 5 located at or beyond the freview:boundary? YES N( �( 6 If the answer is "YES"; a groundwater quality problem may be occurring. CONTACT THE REGIONAL FOR GUIDANCE. If the answer is "NO'; monitoring wells may be improperly OFFICE IMMEDIATELY located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. onmaVb If the answer to question 7 is "NO'; contact the Replona+.m,a ► nv nice on at the review and codays; an evaluarmp a cee ies and/orpenalfies. a(,ee �6n� �3cp'-ojwiz-oaeo iba��°fallViOlc cnS arm oc � n mm i4ef ( metal ua-W- ct 11 1 5-J-L` 6 . 8 The person completing this portion (GW--59A) of fhe monitoring report should sign below and submit th form with GW-59 forms for required wells fo the address provided of the top of the current GW-59 form. r Signature of Permittee (or Authorized Agent) Date G9V-59A 12/8/2003 SUBMIT FORM ON YELI 'APER ONLY GROUNDWATER QUALITY MONITORING: INFrtr@M• • • COMPLIANCE REPORT FORM Please Print CteadyorType PERMIT Number: Expiration Date: I-ZI-ZOZQ FACILITY INFORMATION UIC Non -Discharge t,JQOC1'�lC�-I Facility Name: oo NPDES tiIOther Permit Name (if different): �GZ-fYlS� -� TYPE OF PERMITTED OPERATION BEING MONITORED Q� Facility Address: I� e �rl (���Ct� (street) Z 3p County �1 _ El Lagoon ❑Remediation: Infiltration Gallery (City) (Slate) (Zip) ❑Spray Field ❑ Remediation: !� Tele hone#: Z-�Z�55gu El Rotary Distributor Land Application of Sludge Contact Person: ►� ) ��� 61-y*Ltrl p ❑Water Source Heat Pump El Other: Well Location/Site Name:,6LO 06 QL (� Qn P �%1+� No. of wells to be sampled: (from Permit) I If WI 3AMPLING INFORMATION Date sample collected: J'_-Za-rq FIELD ANALYSES: NELL ID NUMBER (from Permit): q Well Diameter: Z in. pH ooaoo: 4.C1 units Temp. 00010: ZS �C Nell Depth: ft. Screened Interval: 3 ft. to ft. Spec. Cond. 0009a: („5 D µ Mhos Lhere'D Depth to Water Level 825a6: t�.5 ft. below measuring point ft. Odor 000as: (10(� Measuring Point is Z. 5 ft. above land surface Relative M.P. Elevation: Appearance �OUd Volume of water pumped/bailed before sampling: �j gallons c.... ^Ime, fnr mataic were collected unfiltered: ® YES El NO and field acidified: ®YES ❑ NO Date sample analyzed: 0-ZO'I PARAMETERS NOTE: Values should reflect dissolved COD 00335 mg/L Coliform: MF Fecal 31616 >; /100mL Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) issolved Solids:Total 70300 /)3 mg/L pH (Lab) 00403 4.c1 units TOC 00680 1012�) mg/L Chloride 00940 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L pecific Conductance oo095 &6, D µMhos Total Ammonia 00610 C)•Iu mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports): ILL.. Lv --u -"-.... n- . ------ GW-59 Rev.3-1-2016 l `DNllt �) n C Certification No. ►(�_ Laboratory Name: u 1V _ and colloidal concentrations. mg/L Pb -Lead o1os1 ug/L Nitrite (NO2) as N 00M Nitrate (NO3) as N 00620 ©.c)15 mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P 00665 mg/L �• 1 O mg/L Other (Specify Compounds and Concentration Units): Orthophosphate 70507 Al -Aluminum 01105 mg/L Ba - Barium 01007 ug/L Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 <Q .OI © mg/L ORGANICS: (by GC, GC/MS, HPLC) ug/L (Specify test and method #. ATTACH LAB REPORT.) Fe - Iron 01045 Hg - Mercury 71900 ug/L Lab Report Attached.) ❑ Yes (1) ❑ No (0) K - Potassium 00937 mg/L VOC 7873 method # Mg - Magnesium 00927 mg/L method # Mn - Manganese 01055 ug/L method # Ni - Nickel 01067 ug/L method # Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON YELI APER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): Facilitv Address: na or Type County Contact Person: 1' )�L°� l Telephone#: 7h7 57 U��t Well Location/Site Name: Jl C l� FI t°16 tLl No. of wells to be sampled: �_ (from Permit) PERMIT Number: Expiration Date: f-,-51= L/Z/_/ E Non -Discharge ia UIC NPDES HCOC,-�,76a Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor [�Z Land Application of Sludge SAMPLING INFORMATION WELL ID NUMBER (from Permit): � ('} Date sample collected: lo-ZU'� Well Depth: 19ft• Well Diameter: Z ft. Screened Interval: Z ft. to ft. Depth to Water Level szsas: 3, �7 ft. below measuring point — Measuring Point is __3_ft. above land surface Relative M.P. Elevation: ft• Volume of water pumped/bailed before sampling: 5 gallons Samnles for metals were collected unfiltered: m YES ❑ NO and field acidified: YES ❑ NO ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 00400:6.0 units Temp. 000lo: Zip °C Spec. Cond. 00094: Jrl• µMhos Odor 000e5: r1Cr>-e_ Appearance GOCIC� LABORATORY INFORMATION I � Laboratory Name: r-twimn rri I>e._-+ 1 Date sample analyzed: o D- PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. m /L Pb - Lead o1051 COD 00335 mg/L Nitrite (NO2) as N 00615 9 Coliform: MF Fecal 31616C /100mL Nitrate (NO3) as N 00620 ©� (P mg/L Zn - Zinc olosz T tal as P 00665 mg/L Certification No. ld ug/L mg/L Coliform: MF Total 31504 /100mL Phosphorus. o t rb'd sam les) Orth h s hate 70507 O . I Lp mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly u i p OF O p issolved Solids:Total 70300 l-) mg/L Al - Aluminum 01105 mg/L 00403 5 IC1 units Ba - Barium 01007 ug/L pH (Lab) TOC ooseo tkLi mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 T tai 01034 ug/L tip ug/L DRY at time of check here: ❑ Arsenic 01002 ug/L Chromium. o <p (,1© mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils o0552 m /L g Cu - Copper 01042 • ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L Fe - Iron 01045 ug/L Lab Report Attached? ❑ Yes (1) El No (0) Sulfate 00945 5 � mg/L µMhos Hg - Mercury 71900 K Potassium 00937 - mg/L VOC 7873 method # pacific Conductance 000ss • �C- ©L` mg/L Mg - Magnesium 00927 mg/L ,method # Total Ammonia 00610 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # • N' El o1os7 ug/L method # TKN as N 00625 mg/L NI - Ic e For Remediation Systems Only (Attach Lab Reports) Influent Total VOCs: mg/L Lo [ t-� cz(. Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON YELI APER ONLY GROUNDWATER QUALITY MONITORING: owmars Kffp•y• COMPLIANCE REPORT FORM-31-Z02C� FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: anieAneo-m�- Non -Discharge 1��QOC�I�-�� UIC Facility Name: l.C1 1 ' '- NPDES i�IC003Zo�� Other Permit Name (if different): er�t.r�ea_ YYI�� �� TYPE OF PERMITTED OPERATION BEING MONITORED Facility Address: I�� Q:��In (Street C Z 3Q County QI ❑Lagoon ❑Remediation: Infiltration Gallery (City) (State) (Z'N) ElSpray Field ❑Remediation: 1101-) Telephone#:57-5Zu-55��F ❑ Rotary Distributor Land Application of Sludge Contact Person: cnfe (� No. of wells to be sampled: ` El Source Heat Pump ❑ Other: Well Location/Site Name: b (J' { f �� (rr°m Perm;c If WE SAMPLING INFORMATION I U Date sample collected: �i�- ZD— I� FIELD ANALYSES: WAS ° DRY at WELL ID NUMBER (from Permit): ft• Well Diameter: 7_in. pH ooaoo;5.05 units Temp. 000io L3 C time M os hell Depth: to Water Level 82546: below measuring point Screened Interval: ft. Spec. Cond. 000aa: �C�. li µ sampling, Depth _ft. Measuring Point is Z ft. above land surface ft. Relative M.P. Elevation: ft. Odor 000es: ndn check here:❑ Volume of water pumped/bailed before sampling: 5 gallons Appearance Samples for metals were collected unfiltered: N YES ❑ NO and field acidified: J4 YES ❑ NO LABORATORY INFORMATION (p- I�"1q Laboratory Name: �nV I(�(lh(1P�� � t `(�' Certification No. I Q Date sample analyzed: _ PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. mg/L Pb - Lead 01051 ug/L COD 00335 mg/L Coliform: MF Fecal 31616 �L 1100ML Nitrite (NO2) as N 00615 Nitrate (NO3) as N ooszo d ,-) Q mg/L Zn - Zinc o1os2 mg/L Coliform: MF Total 31504 /100mL highly turbid samples) Phosphorus: Total as P 00665 mg/L Orthophosphate 70507 p , C�4 mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for issolved Solids:Total 70300 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 5. () units Ba - Barium 01007 ug/L TOG Z �J � ('rig/L TOG oosao Ca - Calcium 00916 mg/L Chloride oosao mg/L Cd - Cadmium 01027 ug/L _ ug/L Chromium: Total 01034 _uglL Arsenic 01002 Cu - Copper 01042 CO, DI0 mg/L ORGANICS: (by GC, GC/MS, HPLC) m /L Grease and Oils 9 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 273o ug/L 32730 Fe -Iron oloas ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L �' µMhos Hg - Mercury 71900 K Potassium 00937 mg/L - VOC 7873 method # pecific Conductance 00095 Total Ammonia 00610 <Q .Q� mg/L Mg -Magnesium oos27 mg/L method # # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese o1055 ug/L ,method TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # Only (Attach Lab Reports): Influent Total VOCs: m g /L Effluent Total VOCs: mg/L VOC Removal% For Remediation Systems t en�e�rn Land A pP� t C��tcyl OfiZC_ 2d� Signaure of Permittee (or ittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 SUBMIT FORM ON YEL 3APER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print CleadV or Facility Name: V )W ILam'-' , 11'� Permit Name (if different): 14 1� �0 Facility Address: Q�PJi) I ��� a6n� (Street) i4c Z6-y-) County l (City) (Slate) (zip) Telephone#: Z�24 _ Contact Person: I'1>�.�.m(� - Well Location/Site Name:,, njef682'k�'2((4lu- eL�} e1q (O No, of wells to be sampled: 5 (from Permit) PERMIT Number: Expiration Date: I rw LU Non -Discharge LOQ'DC) jOlk(9 UIC NPDES )3Z6� ) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Ed Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION Date sample collected: (o-ZU-I ,HELL ID NUMBER (from Permit): � Nell Depth: ft. Well Diameter: �L in. lj ft. below measurin oint Screened Interval: 3 ft. to ft. Depth to Water Level s2sas: �. ,_ g p Measuring Point is 7.5 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: ® YES ❑ No and field acidified: C.YES ❑ NO FIELD ANALYSES: pH 00400:6.0 units Temp. 00010: Z5 °C Spec. Cond. 00094: 1)3.(4 µMhos Odor 00085: n On Appearance ClIeD( LABORATORY INFORMATION ZOJI/Laboratory Name: 2 Date sample analyzed:_ 2' ZS ) PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. mg/L Pb - Lead 01051 COD 00335 mg/L Nitrite (NOZ) as N oos15 Coliform: MF Fecal 31s1s r /100mL Nitrate (NO3) as N o062o p,� mg/L Zn -Zinc o1os2 P ss5 mg/L Certification No. L© ug/L mg/L Coliform: MF Total 31504 /100ml- Phosphorus. Total as o0 507 ©,O"7 mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbld samples) Orthophosphate , issolved Solids:Total 70300 i (0 mg/L Al -Aluminum 01105 mg/L ug/L pH (Lab) 00403 5,13 units Ba - Barium 01007 TOC 00680 14Z mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 uglL Ch mium: Total 01034 ug/L DRY at time of check here: ❑ Arsenic a1002 ug/L ro <O.OI © mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 mg/L Cu - Copper oloaz ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L Fe - Iron 010a5 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 009a5 mg/L H Mercury 7190o g ry m /L g VOC 7873 method # pecific Conductance 00095 03 • U ItMhos K - Potassium 00937 mg/L ,method # Total Ammonia oosso ©• '? mg/L Mg -Magnesium oo9z7 ug/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 IL ,method # TKN as N 00525 mg/L Ni - Nickel 01067 ug For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.3-1-2016 SUBMIT FORM ON YELL, %PER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Facility Name: Permit Name (if di Facility Address: r% - r t _ (Stale) or o0.'N�u 16'l Telephone#: (;`j/� M-4 —r� act Person: � lea I��, r r,... ir(` ri el W i3 No. of wells to be sampled: Location/Site Name: „�,� , - PERMIT Number: Expiration Date: 1 ^^ S )1_0 Non -Discharge (�iji(Qj_ UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION Date sample collected: (, - D--I ,NELL ID NUMBER (from Permit): _ � � Well Diameter: �_ in. Nell Depth: -0ft. Screened Interval: ft. to l O ft. Depth to Water Level 82546:�_ft. below measuring point ft — Measuring Point is _�_ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: gallons Ilected unfiltered: JW YES ❑ NO and field acidified: YES ❑ NO FIELD ANALYSES: DRY at PH 00400: t units Temp. 0001o: � �C time of Spec. Cond. 000sa: ) (2) µMhos sampling, Odor 00085: rune- check Appearance here:❑ Samples for metals were co _ LABORATORY INFORMATION Laboratory Name: Date sample analyzed: �'717'I�b PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. m /L Pb - Lead o1051 COD 00335 mg/L Nitrite (NOZ) as N 00615 9 Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 ©, C3 (� mg/L Zn - Zinc 01092 P 5 mg/L Certification No. �C) ug/L mg/L Coliform: MF Total 3t5oa /100ml- Phosphorus: Total as ooss 7 © ©2, mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for highly turbid samples) Orthophosphate — mg/L issolved Solids:Total 70300 1 b mg/L Al - Aluminum 01105 PH (Lab) 00403 � • � units Ba - Barium 01007 ug1L TOC 00680 (o.�) mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 < �j.(� ug/L Arsenic 01D02 ug/L <0.0 io mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 m /L g Cu - Copper 01042 /L u 9 (Specify test and method #. ATTACH LAB REPORT.) ( p Phenol 32730 ug/L Fe - Iron oloas ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L H Mercury 7isoo g ry m /L 9 VOC 7B73 method # pecific Conductance 00095 1101 µMhos K - Potassium 00937 mg/L method # Total Ammonia oosso 0. 0�11 mg/L Mg - Magnesium 00927 ug/L method # (Ammonia Nitrogen: NH, as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 /L method # TKN as N 00626 mg/L Ni - Nickel 01067 ug For Remediation Systems Only (Attach Lab Reports): ittee (or Authorized Agent) Nr ame and Title - P14a' a print or type GW-59 Rev.3-1-2016 Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Enwkumm[ „.,= ;'� Drinking Wate_ ..�D377L.,. s - Wastewater I7): 19 O. BOX 7085, 114 OAKMONT DRIVE PHONE (252) 756-6208 GREENVILLE, N.C. 27835-7085 FAX (252) 756-0633 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 PARAMETERS Fecal Coliform (MF), /100 Mls Ammonia Nitrogen as N, mg/l Ammonia Nitrogen as N, mg/l Nitrate Nitrogen as N, mg/l Total Organic Carbon, mg/l Uotal Dissolved Residue, mg/l Total Chromium, ug/l Copper, ug/l Conductivity (at 25c), uMhos/cm Total Ortho-Phosphate as P, mg/l Well Well Well #9 #10 #14 ID#: 416 DATE COLLECTED: 06/20/18 DATE REPORTED : 07/11/18 REVIEWED BY: Well Well Analysis Method #15 #18 Date Analyst Code <1 <1 <1 1 <1 0.74 < 0.04 < 0.04 0.28 0.09 0.05 0.76 0.78 0.07 0.06 10.27 5.44 2.39 11.92 6.81 73 48 37 100 118 8 16 8 7 <5.0 <10 <10 <10 <10 <10 65.0 51.8 50.9 73.4 161 0.10 0.16 0.04 0.07 0.02 06/20/18 JMH 9222D-06 06/26/18 TLH 350.1 112-93 06/28/18 DTL 350.1 R2-93 07/10/18 CLO 353.2 R2-93 06/28/18 SEJ 531OC-11 06/21/18 JMT 2540C-11 06/27/18 LFJ EPA200.7 06/27/18 LFJ EPA200.7 06/25/18 HMM 251OB-11 06/20/18 SEJ 450OPE-11 GW-59A COMPLIANCE REPORT FORM Permit (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. (113b-1 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? . V 2 Was any required information missing on the GW-59 report forms? YES N IF the answer to question 1 or 2 is 'YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing "Yes", YES NO identification plate, area overgrown, etc.)? If the answer is contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YRS NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: oe-I I ip TccG tve11 *10 Chtcsniwm 14UgfC- �� �t5 �eca(Coit�arr� 511�� 1 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? Y If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection date for each occurrence (for the last two years). tell G 10G iD-3i-IG� to•ho l� i�11� I© G�tcrnicam Z ZZ-0 BLIu Z-211--11) i1Z_1IQn-%l- ;p-BI_I IQ L41 1/16Q, , ZZ/ tQ_2v �S 10, Z- ry)g/L to- 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES �TQ X If the answer is "YES" a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation, fines and/or penalties. HCuE. (Z-'DL0V_-lJa20 1,5 au�Qri and ►�haveb�n 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I�-`,'�e�eby�ac no`�iyledge that*the�afiove i"�nf�o��m,?,���evaluad a�ndthe`form �submltted ��t s p(Cov„m�pliance�tep�„GV1/�59Q) isttrue�`and comple'�e�tothe�bes��fmv�.`-�kr�owledg�{._ �_��.� N�.,�=�1 Signature of Permittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YE I PAPER ONLY mg/L Effluent Total VOCs: mg/L VOC Removal% GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: WI Permit Name (if different): Facility Address: Gu Please Pnnt c)eany or (State) (zip) County act Person: -?�Cnei /Yll _Telephone#: Z%­:!�lu, Location/Site Name�,`lt) CLig No. of wells to be sampled: �AMrl INU NELL ID NUMBER (from Permit): Nell Depth: Qft. Depth to Water Level 82546: L4 ft. below measuring point Measuring Point is Z• 15 ft. above land surface Volume of water pumped/bailed before sampling: Gambles for metals were collected unfiltered: N YES ❑ PERMIT Numbe'r:�cYExpiration Date: j-�1-11>LV Non -Discharge >,Y�i� UIC NPDESCOC)3Zv27 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor X Land. Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: FIELD ANALYSES: Well Diameter: Z in. pH 00400:4.2 units Temp. 00010: ZI °C Screened Interval: ft. to �? ft. Spec. Cond. 000ea: 105 µMhos Relative M.P. Elevation: ft. Odor 00085: Appearance dew NO and field acidified: ❑ YES LJ NO t,BORATORY INFORMATION ��) f��m��+= ate sample analyzed: I p-ZU-I Laboratory Name: t kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. /L Pb _Lead o1051 COD 00335 mg/L Nitrite (NO2) as N o0615 m 9 Coliform: MF Fecal 31616 < /100mL Nitrate (NO,) as N 00620 <C), mg/L Zn - Zinc 01092 mg/L Certification No. 10 ug/L mg/L Coliform: MF Total 31504 /100ml- Phosphorus. Total as P ooss5 d les) h h to 70507 Q t�n mg/L Other (Specify Compounds and Concentration Units): (Note: Use MPN method for higfily turbi ;amp Orthop osp a ;solved Solids:Total 70300 Cj C) mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 C1,Z units Ba - Barium 01007 ug/L TOC oosso I'1.00 mg/L Ca - Calcium 00916 mg/L Chloride 00940mg/L Cd - Cadmium 01027 ug/L Total 01034 ug/L If WELL WAS DRY at time of check here:0 Arsenic 01002 ug/L Chromium. Cu - Copper 01042 <G, � mg/L ORGANICS: (by GC, GC/MS, HPLC) m /L Grease and Oils 00552 9 ug/L (Specify test and method #. ATTACH LAB REPORT. Phenol 32730 ug/L Fe -Iron 01045 ug/L Yes (1) ❑ Lab Report Attached? IQ Yes (0) Sulfate oosa5 mg/L Hg -Mercury 71soo m /L g ,method # ip2Ll�� f` VOC 7873 � µMhos pecific Conductance 00095 1 o K -Potassium oos37 method # _ Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L _ method # (Ammonia Nitrogen; NHaas N; Ammonia Nitrogen, Total) Mn - Manganese 01055 uglL u /L ,method # TKN as N 00525 mg/L Ni - Nickel 01067 g For Remediation Systems Only (Attach Lab Reports): GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Facility Name: Permit Name (if di Facility Address: SUBMIT FORM ON YL___.V PAPER ONLY ontact Person: Eenepbm I Telephone#: Z�Z-�Zu-55�� 1 /ell Location/Site Name: 6 C'� RI eld # 0 No. of wells to be sampled: (O {from Permit) PERMIT Number: Expiration Date: j-6) _DC_G Non -Discharge I�Ccx- i/og UIC NPDES N�7p77 Other TYPE OF PERMITTED OPERATION BEING MONITORED El Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field El Remediation: El Rotary Distributor ® Land Application of Sludge El Water Source Heat Pump El Other: If WELL SAMPLING INFORMATION JVELL ID NUMBER (from Permit): � � Date sample collected: 1CYZt-i'I 9 FIELD ANALYSES: aC WAS DRY at Afell Depth: ft. Well Diameter: Z in. pH ooaoo: units Temp. 00010: ZZ time of Depth to Water Level s2sasft. below measuring point Screened Interval: Z ft. to ft. Sec. Cond. 0009a: ,$0 • `) µMhos p sampling, Measuring Point is ft. above land surface 5 Relative M.P. Elevation: ft. Odor 00085: r_lcn e Appearance /^i ( ldsl check here: ❑ Volume of water pumped/bailed before sampling: gallons Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: g YES ❑ NO kBORATORY INFORMATION �(j�Z4 I� Laboratory Name: F(NI(Onment1l I irr Certification No. 10 ate sample analyzed: kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb -Lead o1051 ug/L COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 C /100mL Nitrate (NO3) as N 00620 o, Iq mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 (Note: Use MPN method for highly turbid samples) /100mL Phosphorus: Total as P 00665 mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total70300 (5 mg/L Al -Aluminum o1105 mg/L pH (Lab) 00403 (). lv units Ba - Barium 01007 ug/L TOC 00680 4.45 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium olo27 ug/L Arsenic01002 ug/L Chromium: Total01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method{#. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? �EJ Yes (1) El No (0) VOC method # 67-4)0 -- pecific Conductance 00095 µMhos K - Potassium 00937 mg/L 7873 Total Ammonia omio mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.3-1-2016 CI IRMIT Pr1RM ON YF J PAPFR ONLY (GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if di Facility Address: (City) Print Clearly or (State) (zip) act Person:Telephone#: 4,57 6Z4_ JJg U_ Location/Site Name: ,� CL j-i-(. N ( Jq No. of wells to be sampled: PERMIT Number: Expiration Date: Non -Discharge k4cmi(((D UIC NPDES W(j3-2C7� Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor i?Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL WELL ID NUMBER (from Permit): IZ I Date sample collected: ZU�)g FIELD ANALYSES: DRY DRY Well Depth: 1-3 ft. Well Diameter: in. pH ooaoo:�/. (o units Temp. 00010: � �C at time of Depth to Water Level 62546: Q.15 ft. below measuring point Screened Interval: _ft. to 13 ft. Spec. Cond. 00094: -,)) _ 0 µMhos sampling, Measuring Point is Z ft. above land surface Relative M.P. Elevation: ft. Odor 00085: f1Cn-if check Volume of water pumped/bailed before sampling: gallons Appearance GQC1C here: El SamDles for metals were collected unfiltered: [N YES ❑ NO and field acidified: [N YES ❑ NO LAt3VKAI UKT INN-UKRRA I IVIM I&_2L► 19 Laboratory Name:((j(lf lld'`t } _T) I(yC• _ Certification No. 10 Date sample analyzed: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb -Lead o1051 ug/L Coliform: MF Fecal 31616 �� /100mL Nitrate (NO3) as N 00620 Z� mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 ©, i:73 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 5C mg/L AI - Aluminum o1105 mg/L pH (Lab) 00403 L4- Lo units Ba - Barium 01007 ug/L TOC 00680 3. Lj2- mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 <5 .0 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 <(j, Cl © mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? V Yes (1) ❑ No (0) Specific Conductance 00095 !. 0 µMhos K - Potassium 00937 mg/L VOC 7673 method # &WCC I i Total Ammonia 00610 O •-ZkO mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH,as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L t muent Iota1 vets: IltyrL_ Lood A-RpI ► Cr im Ca. Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 of Permittee (or Authorized Agent) VAVLK VNLT GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: _ I Permit Name (if different): Facility Address: o h( (Street) (city) (Stale) or Type SUBMIT FORM ON County Contact Person: 0 Telephone#: Z62 J5N_ Well Location/Site Name: it rfe FCC ICn ,_� AIU d-62_ i A I o No. of wells to be sampled: PERMIT Number: ,/'/� Expiration Date: r=-LDl1� Non -Discharge wimpTow UIC NPDES LI('hCi,3Zb77 Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor [M Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): 15 Date sample collected: 10-7-4-)Q Well Depth: 9 ft. Well Diameter: Z in. Depth to Water Level 82546: Lj ft. below measuring point Screened Interval: 3 ft. to CZ ft. Measuring Point is Z - S ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons Samples for metals were collected unfiltered: [N YES ❑ NO and field acidified: ® YES ❑ NO FIELD ANALYSES: vv"" pH 00400: L ,2 units Temp. 000lo: ZC) °C DRY at µMhos time of Spec. Cond. 00094: / Zci sampling, Odor 00085: 1 ont check Appearance Gar here: LABORATORY INFORMATION 0-LU-12 Laboratory Name: r/1Vl (C f) f -Ti I,I r c Certification No. 13 Date sample analyzed: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00336 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 ©, )Z mg/L Zn -Zinc olosz mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 (j , 63 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 15 mg/L Al -Aluminum oil o5 mg/L pH (Lab) o04o3 4 Z units Ba - Barium 01007 ug/L TOC 00680 P J L4 mg/L Ca -Calcium oosls mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 �] ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 CD. DIO mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? V Yes (1) ❑ No (0) Specific Conductance 00095 17q µMhos K - Potassium 00937 mg/L VOC 7873 method # /pZC1QC- Total Ammonia 00610 0- QZ mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # _roe For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mgn- tmuent i otal vvL,s. '�P� �•I� L,4oDli C�-l�ic� Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 Of Agent) (Date) .........— — -1.... __ onor=o nnn v GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM �., ...�...... Please Facility Name: ( 0 Permit Name (if different): Facility Address: qCD or Type County (City) (State) (LIP) act Person: ��� 6MIO-) Telephone#: Location/Site Name: t ( C(()'f ( ©- No. of wells to be sampled PERMIT Number: Expiration Date: ► ;tU- nt, O Non -Discharge UIC NPDES �f(�7i�� Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor CA Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFURMA I IUN WELL ID NUMBER (from Permit): I Date sample collected: ICrZU'1 AZ- FIELD ANALYSES: o DRY at Z(7 C Well Depth: �ft• Well Diameter: Z in. pH ooaoo: 1� units Temp. 00010: Spec. Cond. 00094: v (p µMhos time of Depth to Water Level 82546:_ ft, below measuring point Screened Interval: Z ft. to _ft. sampling, Measuring Point is Z. ;-3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: U) check here:❑ Volume of water pumped/bailed before sampling: 5 gallons Appearance Samples for metals were collected unfiltered: MI YES ❑ NO and field acidified: `X. YES ❑ NO LABORATORY INFORMATION 1 (7 �i�lg Laboratory Name: Env (�(��i� �1 �ic' Certification No. 10 Date sample analyzed: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. Pb - Lead wom ug/L COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Zinc mg/L Coliform: MF Fecal 31616 G /100mL Nitrate (NO3) as N 00620 ©.Zlo mg/L Zn - 01092 Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) Phosphorus: Total as P 00665 mg/L Orthophosphate 70507 Q , I mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 59 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 4.11 units Ba - Barium 01007 ug/L TOC 00680 (p• 1 5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium o1o27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 C) mg/L ORGANICS: (by GC, GC/MS, HPLC) ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 15 Yes (1) ❑ No (0) VOC method # �p71xiG—� pecific Conductance 00095 L/ (a. iv µMhos K - Potassium 00937 mg/L 7873 Total Ammonia 0061a Q - 13 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N o0625 mg/L Ni - Nickel 01067 ug/L method # — __. T_...i I moll VOC Removal% GW-59 Rev.3-1-2016 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if di Facility Address: (cityi Print Clearly or (Zip) SUBMIT FORM ON YELLuvv PAPER ONLY act Person: ���I D l I Telephone#: Location/Site Name: PI N1 d *I­5 No. of wells to be sampled: PERMIT Number: Expiration Date: Non -Discharge (•t)CXDC�04-9 UIC NPDES HCQ570-)_) Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor MI -and Application of Sludge ❑ Water Source Heat Pump ❑ Other: IIf WELL SAMPLING INt-UKMA I IUN WELL ID NUMBER (from Permit): 1 g Date sample collected: Well Depth: 10 ft. Well Diameter: Z in. Depth to Water Level 82546: Ly ft. below measuring point Screened Interval: S ft. to ft. Measuring Point is 7 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5 gallons SamDles for metals were collected unfiltered: ® YES ❑ NO and field acidified: C9 YES ❑ NO FIELD ANALYSES: pH ooaoo: c4:3 units Temp. 00010: Z °C Spec. Cond. 00094: / o ) _µMhos Odor o0065: n of.) Appearance Clea LABORATORY INFOKMA I IUN Date sample analyzed: 1C�-Laboratory Name: PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 Coliform: MF Fecal 31616 C l /100mL Nitrate (NO3) as N 00620 07 mg/L Zn - Zinc 01092 Coliform: MF Total 315oa /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 O.O 1 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 1 t4,5 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 Ll•3 units Ba - Barium 01007 ug/L TOC oomo 1) . j�)5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L IL Chromium: Total 01034 5 ug/L Certification No. 10 ug/L mg/L DRY at time of sampling, here: ❑ Arsenic 01002 Oils ug mg/L Cu - Copper 01042 4C)� pl C) mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and 00552 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? C9 Yes (1) ❑ No (0) # Conductance 00095 1 O µMhos K - Potassium 00937 mg/L VOC 7873 method pecific Total Ammonia 00610 D - Z mg/L Mg - Magnesium oo927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese olo55 ug/L , method # N' k 1 u /L method # TKN as N 00625 mg/L NI - lc a o1os7 9 For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.3-1-2016 Of Permittee (or Authorized Agent) mg/L VOC Removal% Emmkgovo % hCopumW 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 �.. vPa�t�Matar.ID� 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/24/18 DATE REPORTED : 11/15/18 REVIEWED BY: Well Well Well Well PARAMETERS #9 #10 #14 #15 Fecal Coliform (MF), /100 Mls <1 <1 <1 5 Ammonia Nitrogen as N, mg/1 0.83 0.10 0.26 0.82 Nitrate Nitrogen as N, mg/l <0.04 0.19 1.29 0.12 Total Organic Carbon, mg/1 17.06 4.45 3.42 9.74 Total Dissolved Residue, mg/l 90 45 50 125 Total Chromium, ug/1 8 14 <5.0 7 Copper, ug/l < 10 < 10 < 10 < 10 Conductivity (at 25c), uMhos/cm 105 50.7 71.0 129 Total Ortho-Phosphate as P, mg/1 0.09 0.08 0.03 0.03 Well Analysis Method #17 Date Analyst Code <1 10/24/18 JMT 9222D-06 0.13 10/29/18 DTL 350.1 112-93 0.26 10/26/18 DTL 353.2 112-93 6.15 10/24/18 SEJ 531OC-11 59 10/25/18 JTH 254OC-11 7 10/26/18 LFJ EPA200.7 < 10 10/26/18 LFJ EPA200.7 46.6 10/29/18 JMS 251OB-11 0.10 10/24/18 SEJ 450OPE-11 Eawn[MUM&M % hC0TP@TMW 114 OAKMONT DRIVE GREENVILLE, N.G. 27858 CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON ,NC 28530 Well Analysis Method PARAMETERS #18 Date Analyst Code Fecal Coliform Off), /100 Mls < 1 10/24/18 JMT 9222D-06 Ammonia Nitrogen as N, mg/l 0.24 10/29/18 DTL 350.1 R2-93 Nitrate Nitrogen as N, mg/1 0.07 10/26/18 DTL 353.2 R2-93 Total Organic Carbon, mg/l 7.05 10/24/18 SEJ 531OC-11 Total Dissolved Residue, mg/1 145 10/25/18 JTH 2540C-11 Total Chromium, ug/l 5 10/26/18 LFJ EPA200.7 <10 10/26/18 LFJ EPA200.7 Copper, ug/1 Conductivity (at 25c), uMhos/cm 107 10/29/18 JMS 251OB-11 Total Ortho-Phosphate as P, mg/l 0.01 10/24/18 SEJ 450OPE-11 WaotoWater IDa _..,0_.. PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 416 DATE COLLECTED: 10/24/18 DATE REPORTED : 11/15/18 REVIEWED BY: EmwonnEWC3 Flo hCOTPOTMI 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 FAX (252) 756-0633 CLIENT: CMSD (SLUDGE & WELLS ACCT) CLIENT ID: 416 CONTENTNEA METRO. SEWAGE DIST. KPG MS. RENEE PRIDGEN ANALYST: DATE COLLECTED: 10/24/18 Page: 1 P.O. BOX 477 DATE REPORTED: 11/15/18 GRIFTON, NC 28530 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 6200C-3.1 Date Analyzed: 10/26/18 1100//2 /18 10/27/18 10/27/18 Well 10/27/18 eIl /18 Well #10 Well #14 #15 #17 PARAMETERS, ug/l #9 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1. 2. Benzene Bromobenzene <0.50 < 0.50 <0.50 < 0.50 <0.50 < 0.50 < 0.50 < 0.50 3. Bromochloromethane < 0.50 < 0.50 <0.50 < 0.50 < 0.50 4. Bromodichloromethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 5. Bromoform < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 6. Bromomethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 7. N-Butylbenzene <0.50 < 0.50 < 0.50 < 0.50 < 0.50 8. Sec-Butylbenzene < 0.50 < 0.50 <.0.50 < 0.50 < 0.50 9. Tert-Butylbenzene < 0.50 < 0.50 < 0.50 < 0.50 0.50 10. Carbon Tetrachloride <0.50 < 0.50 < 0.50 < 0.50 < 11. Chlorobenzene <0.50 < 0.50 < 0.50 < 0.50 < 0.50 <0.50 12. Chloroethane <0.50 <0.50 <0.50 <0.50 <0.50 13. 14. Chloroform Chloromethane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 15. 2-Chlorotoluene <0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 16. 4-Chlorotoluene < 0.50 <0.50 < 0.50 < 0.50 < 0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <0.50 <0.50 18. 1,2-Dibromo-3-Chloropropane <0.50 <0.50 <0.50 <0.50 <0.50 19. 1,2-Dibromoethane < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 20. Dibromomethane <0.50 < 0.50 < 0.50 < 0.50 < 0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 23. 1,4-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 <0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 <0.50 <0.50 25. 1,1-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 26. 1,2-Dichloroethane <0.50 <0.50 <0.50 <0.50 <0.50 27. 1,1-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 28. Cis-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 29. trans-1,2-Dichloroethene <0.50 <0.50 <0.50 <0.50 <0.50 30. 1,2-Dichloropropane < 0.50 < 0.50 < 0.50 <0.50 < 0.50 31. 1,3-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 32. 2,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 33. 1,1-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 34. Cis-1,3-Dichloropropene <0.50 <0.50 <0.50 <0.50 <0.50 35. trans-1,3-Dichloropropene < 0.50 <0.50 < 0.50 < 0.50 <0.50 36. 37. Ethylbenzene Hexachlorobutadiene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 38. Isopropylbenzene < 0.50 <0.50 <0.50 <0.50 <0.50 <0.50 39. 4-Isopropyltoluene < 0.50 < 0.50 < 0.50 < 0.50 <0.50 < 0.50 40. Methylene Chloride < 0.50 <0.50 < 0.50 <0.50 < 0.50 41. Naphthalene < 0.50 < 0.50 < 0.50 <0.50 < 0.50 < 0.50 42. Propylbenzene < 0.50 < 0.50 < 0.50 < 0.50 <0.50 43. 44. Styrene 1,1,1,2-Tetrach1oroethane < 0.50 < 0.50 <0.50 < 0.50 <0.50 <0.50 <0.50 45. 1,1,2,2-Tetrachloroethane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 46. Tetrachloroethene < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 47. Toluene F�rnnnnmrnrnr �lnrn 0 � kh (f,-,nn f�f'o1nli`�o�ft1o..1 114 OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NCO28530 REVIEWED BY: PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/24/18 DATE REPORTED: 11/15/18 VOLATILE ORGANICS STD, METHODS 620OC-11 Date Analyzed: Well /18 WeIl /18 PARAMETERS, ug/l #9 #10 < 0.50 < 0.50 48. 1,2,3-Trichlorobenzene < 0.50 < 0.50 49. 1,2,4-Trichlorobenzene < 0.50 < 0.50 50. 1,1,1-Trichloroethane <0.50 <0.50 51. 1,1,2-Trichloroethane <0.50 <0.50 52. Trichloroethene < 0.50 < 0.50 53. Trichlorofluoromethane <0.50 <0.50 54. 1,2,3-Trichloropropane <0.50 <0.50 55. 1,2,4-Trimethylbenzene < 0.50 < 0.50 56. 1,3,5-Trimethylbenzene <0.50 <0.50 57. Vinyl Chloride < 1.00 < 1.00 58. Total Xylenes < 1.00 < 1.00 59. Methyl Tert Butyl Ether 10/27/18 Well #14 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 1.00 < 1.00 10/27/18 Well #15 < 0.50 < 0.50 < 0.50 <0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 1.00 < 1.00 Page: 2 10/27/18 Well #17 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 1.00 < 1.00 EOUT(BIMEW % hmpTOW 114.OAKMONT DRIVE GREENVILLE, N.C. 27858 CLIENT: CMSD (SLUDGE & WELLS ACCT) CONTENTNEA METRO. SEWAGE DIST. MS. RENEE PRIDGEN P.O. BOX 477 GRIFTON, NC 28530 REVIEWED BY: VOLATILE ORGANICS YNE (252) 756-6208 FAX (252) 756-0633 CLIENT ID: 416 ANALYST: KPG DATE COLLECTED: 10/24/18 Page: 3 DATE REPORTED: 11/15/18 STD. METHODS 620OC-11 Date Analyzed: 10/27/18 Well PARAMETERS, ug/1 #18 < 0.50 1. Benzene <0.50 2. Bromobenzene <0.50 3. Bromochloromethane < 0.50 4. Bromodichloromethane <0.50 5. Bromoform <0.50 6. Bromomethane <0.50 7. N-Butylbenzene <0.50 8. Sec-Butylbenzene <0.50 9. Tert-Butylbenzene < 0.50 10. Carbon Tetrachloride < 0.50 11. Chlorobenzene < 0.50 12. Chloroethane < 0.50 13. Chloroform < 0.50 14. Chloromethane <0.50 15. 2-Chlorotoluene <0.50 16. 4-Chlorotoluene < 0.50 17. Dibromochloromethane <0.50 18. 1,2-Dibromo-3-Chloropropane < 0.50 19. 1,2-Dibromoethane < 0.50 20. Dibromomethane < 0.50 21. 1,2-Dichlorobenzene < 0.50 22. 1,3-Dichlorobenzene < 0.50 23. 1,4-Dichlorobenzene < 0.50 24. Dichlorodifluoromethane <0.50 25. 1,1-Dichloroethane < 0.50 26. 1,2-Dichloroethane < 0.50 27. 1,1-Dichloroethene < 0.50 28. Cis-1,2-Dichloroethene <0.50 29. trans-1,2-Dichloroethene < 0.50 30. 1,2-Dichloropropane < 0.50 31. 1,3-Dichloropropane < 0.50 32. 2,2-Dichloropropane < 0.50 33. 1,1-Dichloropropene < 0.50 34. Cis,I,3-Dichloropropene <0.50 35. trans-1,3-Dichloropropene < 0.50 36. Ethlbenzene < 0.50 37. Hexachlorobutadiene < 0.50 38. Isopropylbenzene < 0.50 39. 4-Isopropyltoluene < 0.50 40. Methylene Chloride < 0.50 41. Naphthalene < 0.50 42. Propylbenzene < 0.50 43. Styrene 44. 1,191,2-Tetrachloroethane < 0.50 < 0.50 45. 1,1,2,2-Tetrachloroethane < 0.50 46. Tetrachloroethene <0.50 47. Toluene Enw'MRHM� % �NC@TP@T@"4 114 OAKMONT DRIVE GREENVILLE, N,C. 27858 PHONE (252) 756-6208 FAX (252) 756-0633 CLIENT: CMSD (SLUDGE & WELLS ACCT) CLIENT ID: 416 CONTENTNEA METRO. SEWAGE DIST. KPG MS. RENEE PRIDGEN ANALYST: DATE COLLECTED: 10/24/18 47 P.O.BOX 477 P.O. BOX DATE REPORTED: 11/15/18 GRIF28530 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 620OC-11 7/18 l PARAMETERS, ug/l 7#018 48. 1,2,3-Trichlorobenzene049. 1,2,4-Trichlorobenzene050. 1,1,1-Trichloroethane5051. 1,1,2-Trichloroethane5052. Trichloroethene5053. Trichlorofluoromethane5054. 1,2,3-Trichloropropane5055. 1,2,4-Trimethylbenzene .50 < 0.50 56. 1,3,5-Trimethylbenzene < 0.50 57. Vinyl Chloride < 1.00 58. Total Xylenes < 1.00 59. Methyl Tert Butyl Ether Page: 4 SOILS ANALYSIS LAB REPORTS LIME APPLICATION NCDA&CS Agronomic Division Phone: I G¢ICULTUgF�N Predictive a 2o�A cO p . N Soil Report o S Links to Helpful Information Farm: Not Provided 19) 733-2655 Website: www.neagr.gov/agronomi/ Client: CMSD PO Box 477 Mehlich-3 Extraction Griffon, NC 28530 Sampled: 10/18/2018 Received: 10/25/2018 Completed: 11 /06/2018 Sampled County : Pitt Client ID: 147385 Report No. FY19-SL009950 Advisor: Chris Whitehurst Ayden Nitrogen P.O. Box 7 Ayden, NC 28513 Advisor ID: 490477 Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where they become toxic to crops arown on a field. Nutrients (lb/acre) More Sample ID: 1 Recommendations: Lime S Mn Zn Cu B Information Crop (tons/acre) N P2O5 K2O Mg Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 0 pH$ Z Q 0 Note: 12 Note: 2-Bermuda hay/past., M 0.0 180-220 0 100 0 0 pH$ Z c Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg1dm3]: HM% WN ' CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.76 0.99 17.1 93 1.1 6.5 817 58 70 22 Sample ID: 2 Recommendations: Lime Crop (tons/acre) N P2O5 Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 2-Bermuda hay/past., M 0.0 180-220 0 Test Results [units - W/V in g/cnr3; CEC and Na in meq/100 cm3; NO3-N in mg1dm3]: HM% W/v CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.71 0.84 . 18.9 88 2.3 6.1 881 64 64 22 North Carolina Tobacco Trust Fund Commission Soil Class: Mineral S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 7F 134 90 90 2884 2884 904 0.2 1 Nutrients (Ib/acre) More K2O Mg S Mn Zn Cu B Information 20 0 0 0 Z 0 0 Note: 12 Note: 80 0 0 0 Z 0 0 Note: 12 Note: Soil Class: ' Mineral S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 82 107 79 79 3202 3202 1296 0.2 1 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.goviagronomi/ No. FYI--i .'J09950 Page 2 of 3 More Sample ID: 3 Lime History: Recommendations: Lime Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 -Bermuda hay/past., M 0.0 180-220 0 K2O 70 160 Mg 0 0 `'"' S 0 0 Mn pH$ pH$ Zn Z Z Cu 0 0 B 0 0 Information Note: 12 Note: Note: 12 Note: Test Results [units - WN in g/crrr3; CEC and Na in meg1100 cnr3; NO3-N in mg/drrr3]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.76 1.08 19.2 98 0.4 6.9 893 32 75 22 S-I 69 Mn-I 89 K2O 70 160 Soil Class: -Mineral Mn-All Mn-AI2 Zn-I Zn-AI Nutrient (lb/acre) 069 3069 S Mn Zn Mg Z 0 pH$ 0 0 pH$ Z 0 Cu-I 1045 Cu _ 0 0 Na 0.2 B 0 0 ESP SS-1 NO3-N 1 More Information Note: 12 Note: Note. 12 Note: Sample ID: 4 Lime History: Recommendations: Lime Crop (tons/acre) N P2O5 1 -Bermuda hay/past., E 0.0 60-80 0 2 -Bermuda hay/past., M 0.0 180-220 0 Test Results [units - WN in glcm3; CEC and Na iri meg/100 crrr3; NO3-N in mg/dr&]: HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0.66 0.90 20.7 93 1.5 6.5 1036 32 73 19 S-1 93 Mn-I 106 Mn-All 73 Soil Class: Mn-AI2 73 Mineral Zn-I Zn-AI 4403 4403 Cu-I 1295 Na 0.2 ESP SS-1 NO3-N 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at time, even if the report recommends more. You can apply the rest in similar increments every six months until the full i is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer . Recommendations for field crops or other large areas are listed separately for each nutrient (i be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special'attention to micronutrient levels. If $, pH$,. $pH, C or Z notations appear on the soil report, refer to $Note: econdary Nutrients and Micronutrients In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm.. Recommendations for small areas, such as home lawns/gardens, are listed in units of lb/1000 sq ft . If you cannot find www ncaar aov/agronomi/obpart4.htn&ffind information that the exact fertilizer grade recommended on the report, visit A Homeowners Guide to Ferti/izei may help you choose a comparable alternate. For more information, read Test Results Report Abbreviations Ac B BS% Ca% CEC Cu-1 ESP HM% K-1 K20 Mg% MIN Mn Mn-All Mn-AI2 Mn-1 M-O N Na NO3-N ORG pH P-1 P205 S-1 The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, WAR Zn-I, Zn-Al, Cu-1, S-I, SS-I,.Na, ESP, SS -I, NO3-N (not routinely available)] indicate. levels of plant nutrients or other fertility measurement. Visit www ncaar aov/aaronomi/uvrst hfm SS-1 WN Zn-AI Zn-I No. FY19-SL009950 Page 3 of 3 exchangeable acidity boron • CEC occupied by basic cations • CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent humic matter potassium index potash % CEC occupied by magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index mineral -organic soil class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index . weight per volume zinc availability index zinc index NCDA&CS Agronomic Division Phone: (919) 733-2655 G V ULTUJ�^No Predictive pkA CO Soil Report p �c Links to Helpful Information FUNDED \8�I Farm: Not Provided Website: www.ncagr.gov/agronomi/ Client: CMSD PO Box 477 Mehlich-3 Extraction Grifton, NC 28530 Sampled: 10/18/2018. Received: 10/25/2018 Completed: 11/06/2018 Sampled County: Pitt Client ID: 147385 No. FY1y=6Lv09902 Advisor: Chris Whitehurst Ayden Nitrogen P.O. Box 7 Ayden, NC 28513 Advisor ID: 490477 Agronomist's Comments: ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is designed to be a "trigger" that allows enough time. to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by ed. The CTL for copper and zinc was set to prevent levels from accumulating to the point where DENR as a benchmark to determine when application of waste products should be stopp they become toxic to crops rown on a field. Nutrients (fib/acre) More Sample ID: 5 Recommendations: Lime S Mn Zn Cu B Information Crop (tons/acre) N P2O5 K2O 0 p 0 Z 0 0 Note: 12 Note: Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 0 0 2 - 0.0 Test Results [units - W/V in g/cnt3; CEC and Na in meq/100-cnr3; NO3-N in mg/dO]: HM%p W/V CEC BS%p Ac pH P-1 K-1 Ca%p Mg°/ 0.66 0.74 21.0 87 2.8 6.0 930 83 63 22 Sample ID: 6 Recommendations: Lime Crop (tons/acre) N Lime History: 1 -Bermuda hay/past., E 0.0 60-80 2 - 0.0 Soil Class: Mineral p S-1 -Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 102 89 70 3974 3974 1314 0.3 1 Nutrients (Ib/acre) More P2O6 K2O Mg S Mn Zn Cu. B Information 0 20 0 0 0 Z 0 0 Note: 12 Note: Test Results [units - WN in glca; CEC and Na in meq/100 crr�; NO3-N in mg/dr&]: Soil Class: Mineral HM%p WN CEC BS%p Ac pH P-1 K-1 Ca%p Mg%p S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3=N 0.66 0.77 22.3 88 2.7 6.1 912 65 65 21 102 , 102 77 5253 5253 1490 0.4 2 North Carolina 'Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr. Report No. FY19-SL009902 Page 2 of 11 More Sample ID: 7 Recommendations: Lime K2O `' ­ -' Mg S Mn Zn Cu B Information Crop (tons/acre) N P2O5 0 . Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 pH$ 2 _ 0.0 WN in CEC and Na in meq/100 cnr3; NO3-N in mgldrr ]: Soil Class: Mineral Test Results [units - glcd; Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-1 Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 2403 2403 5 2 180 0. 0.76 1.02 16.8 96 0.7 6.9 815 56 72 22 57 138 86 Nutrients (Ib/acre)Mn More Sample ID: 8 Recommendations: Lime, K2O M9 S Zn Cu B Information Crop (tons/acre) N P2O5 0 Z 0 0 Note: 12 Note: Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 50 0 pH$ 2 _ 0.0 WN in CEC and Na in meg1100 cd; NO37N in mgldd]: Soil Class: Mineral Test Results [units - g/cO Ca% Mg% S-1 Mn-I Mn-Ali Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC 13S% Ac pH P-1 K-1 2859 2859 749 0.2 1 0.76 0.98 17.4 '95 0.9 6.8 '885 43 71 22 65 118 76 Nutrients (lb/acre) More Sample ID: 9 Recommendations:_ Lime K2O Mg S Mn Zn Cu B Information Crop (tons/acre) N P2O5 0 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 60 0 pH$ 2 - 0.0 WN in CEC and Na in meg1100 crrr3; NO3-N in mgldnft Soil Class: Mineral Test Results [units - g/cO; Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 2087 2087 630 2 1 0. 0.76 0.96 17.0 96 * 0.6 7.0 699 38 74 22 . 72 103 64 Nutrients (lb/acre) More Sample ID: 10 Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop (tonslacre) N P2O5 0 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 30 0 pH$ 2 _ 0.0 WN in CEC and Na in meq/100 crrr3; NO3-N in mgldO]: Soil Class: Mineral Test Results [units - glcrrr3; K-1 Ca% Mg% S-1 Mn-I . Mn-All Mn-AI2 Zn-I Zn-AI Cu-1. Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 86 3259 3259 803 0.2 1 0.56 0.99 16.6 92 1.3 6.7 793 61 67 23 59 131 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www. Page 3 of 11 More. Sample ID: 11 Recommendations: Lime K2O M9 S Mn Zn Cu B Information Crop (tons/acre) N PzOS 0' Z 0 0 Note: 12 Note: Lime History: 1 _Bermuda hay/past., E 0.0 60-80 0 0 0 pH$ 2 - 0.0 WN in CEC and Na in'meg1100 crrr�; NO3-N in mg/drrr3]: Soil Class: Mineral Test Results [units - g/curl; Mn-I Mrr-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 1 0.46 0.83 23.4 94 1.4 6.7 829 81 69 24 74 124 5985 5985 1700 0.3 More Nutrients (lb/acre) Sample ID: 12 Recommendations: Lime K2O M9 S Mn Zn Cu. B Information Crop (tons/acre) N _ P2O5 0 Z 0 0 Note: 12 Note: Lime History: 1 _Bermuda hay/past., E 0.0 60-80 0 50 0 pH$ 2 - 0.0 • WN in CEC and Na in meq/100 cm3; NO3-N in mgldrrr3]:. Soil Class: Mineral Test Results [units - g/cO; S-i Mn-I Mn-All Mn-AI2 Zn-I Zn-Al. Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 0. 2 2 0.71 1.15 12.8 93 0.9 6.7 741 45 71 21 57 152 98 2401 Nutrients (lb/acre) 2401 603 More Sample -ID: 13. Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop . (tons/acre) N P2O6 0 Z 0 p Note: 12 Note: Lime History: 1 =Bermuda hay/past., E 0.0 60-80 0 10 0 pH$ 2 - - 0.0 WN in CEC and Na in meg1100 crrr�; NO3-N in mgldr&]: Soil Class: Mineral Test Results [units - glcrr$; S-1 Mn-1 Mn-All Mn-AI2 Zn-I � Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN _ CEC BS% Ac pH P-I K-I Ca% Mg% 1 0.51 0.97 20.3 94 1.2 6.7 874 77 70 - 22 -67 149 4883 Nutrients (Ib/acre,) 4883 1197 0.2 More Sample ID: 14 Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop (tonslacre) N PzOs 0 Z 0 0 Note: 12 Note: Lime History: 1 -.Bermuda haylpast., E 0.0 . 60-80 0 10 0 pH$ 2 _ 0.0 WN in CEC and Na in meq/100 curl; NO3-N in mg/dm3]: Soil Class: Mineral Test Results [units - g/cO; S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 1 0.60 0.93 19.9 93 1.4 6.7 817 78 70 21 67 144 93 4791 4791 1171 0.2 _ NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FYIb-oCZ09902 Page 4 of 11 Nutrients (Ib/a(-re) More Sample ID: 15 Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop (tons/acre) N P2O5 0 0 0 0 0 Note: Note: 12 - Lime History:. 1-Bermuda hay/past., E 0.0 60-80 0 70 pH$ 2-0.0 WN in CEC and Na in meg1100 crrmt ; NO3-N in mgldrrr3]: Soil Class: Mineral Test Results [units - glcd; Ca% Mg% S-1 Mn-I Mir -All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 - K-1 697 133 2 2 0. 1.37 1.13 10.8 95 0.6 6.9 154 36 69 24 60 86 55 697 Nutrients (Ib/acre) More Sample ID:16 Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop (tons/acre) N P2O6 0 0 0 • 0 0 Note: 12 - Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 . 0 2- 0.0 - WN iti glcO; CEC and Na in meg1100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral Test Results [units K-1 Ca% Mg% S-I Mn-I Mri-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 883 883 268. 2 02 .� 1.02 1.12 8.9 87 1.1 6.4 362 36 65 21 51 84 62 Nutrients is (Ib/acre) More Sample ID: 17 Recommendations: Lime K2O Mg 15 Mn Zn Cu B Information Crop (tonslacre) N P2O6 0 0 0 0 0 Note: 12 Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 80 0 2- 0.0 WN in CEC and Na in meq/100 crrr3; NO3-N in mgldrft Soil Class: Mineral - Test Results [units'- g/ca; Ca% Mg% S-1 Mn-I Mn-AI1 Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N HM% WN CEC BS% Ac pH P-1 K-1. 487 487 112 ' 0.2 3 1.25 1.16 8.0 86 1.1 6.2 176 31 65 19 51 73 58 Nutrients (lb/acre) More Sample ID: 18 Recommendations: Lime K2O M9 g Mn Zn Cu B Information Crop (tons/acre) N P2O6 0 0 0 0 Note: 12 Note: Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 70 0 pH$ 2- 0.0 c WN in CEC and Na in meg1100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral Test Results [units - glcrrr3; Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 969 969 237 0.2 2 0.81 1.09. 10.0 92 0.8 6.7 442 33 66 25 60 83 57 1 Y� NCDA8,CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.govlagronomi/ �t Report No. FY19-SL009902 Page 5 of 11 More Sample -ID- 19 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tons/acre) N P206 0 Z 0 0 Note: 12 Note: 1 -Bermuda hay/past., E 1.1 - 60-80 0 70. 0 0 Lime History: , 0.0 2- in CEC and Na in meq/100 cO; NO3-N in mgldrr$]: Soil Class: Mineral Test Results [units - WN' glcd; Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% . S-1 Mn-I � 0.2 2 0.60 0.99 10.3 77 2.4 5.5 953 36 57 18 78 98 2053 Nutrients (Ib/acre) 2053 619 More Sample ID: 20 Recommendations: Lime (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Note: 12 Note: Crop 1 _Bermuda hay/past., E 0.0 60-80 0 80 0 0 pH$ 0 0 0 Lime History: 0.0 2_ in CEC and Na in meq/100 cm3; NO3-N in mgldrrti3]: Soil Class: Mineral Test Results [units - WN glcrrr3; Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 1687 1687 424 0.2 2 0.97 1.04 12.1 91 1.1 ' 6.6 754 29 66 24 64 84 58 Nutrients (lb/acre) More More Sample ID: 21 Recommendations: Lime K20 Mg S Mn Zn Cu B Crop (tons/acre) N P205 0 0 0 0 0 Note: 12 1 -Bermuda hay/past., E 1.1 60-80 0 60 0 Lime History: 0.0 2 - in CEC and Na in meq'/100 cd; NO3-N in mg1drri3]: Soil Class: Mineral Test Results [units.- WN glcr&; S-1 Mn-1 Mn-Ali Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% � 0.3 3 1.25 -0.92 11.6 77 2.7 5.6 875 38- 56 19 90 87 1667 (Ib/acre) 1667 582 More Sample ID: 22 Recommendations: Lime K20 Mn Mg S Mn Zn Cu B Information Crop (tonslacre) N P205 0 0 0 0 0 Note: 12 Lime History: 1 -Bermuda hay/past., E 1.0 60-80 0 60 0 2- 0.0 W/V in CEC and Na in meg1100 cd; NO3-N in mg1drrr3]: Soil Class: Mineral Test Results [units - g/cm3; Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S-1 0.2 2 0.60 0.98 11.9 78 2.6 5.6 962 40 57 20 80 83 67 1567 1567 651 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: 11 w/agronomil Report No. FY19-SL009902 Page 6 of 11 Nutrients (Ib/acre) More . Sample ID: 23 Recommendations: Lime K2O M9 S Mn Zn Cu B Information Crop (tonslacre) N P2O5 0 0 0 0 Note: 12 Note: Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 .80 0 pH$ 2- 0.0 in CEC and Na in meg1100 crn3; NO3-N in mg/dO]: • Soil Class:. Mineral Test Results [units - WN g/cd; Mn-I Mn-AI1 Mn-Al2 Zn-1 Zn-Al Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-I K-I Ca% Mg % S-1 0.2 2 0.81 1.08 11.0 98 0.2 7.2 344 29 71 26 64 111 65 715 715 Nutrients (lb/acre) 236 More Sample ID: 24 Recommendations: Lime K2O Mg g Mn Zn Cu B Information Crop (tonslacre) N P2O5 0 0 0 0 0 Note:12 Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 50 0 2- 0.0 in CEC and Na in meq/100 cnr3; NO3-N in m9ldm3]: Soil Class: Mineral Test Results [units - WN gled; S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% 1103 386 0.2 2 0.66 1.05 10.1 89 1.1 6.5 562 ' 43 68 19 .55 100 1103 Nutrients (Ib/acre) More Sample ID: 25 Recommendations: Lime K2O Mg g Mn Zn Cu B Information Crop (tonslacre) N P2O5 0 0 0 0 0 Note:12 1 -Bermuda hay/past., E 1.1 60-80 0 50 0 Lime History: 0.0 2- in CEC and Na in meg1100 crrr3; NO3-N in mg/drift Soil Class: Mineral_ Test Results [units - WN g/crrP; S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 Ca% - Mg% 0.2 2 1.25 0.99 9.9 76 2.4 5.5 716 45 59 15 71 110 1645 1645 Nutrients (lb/acre) 596 More Sample ID: 26 Recommendations: Lime K2O Mg S Mn Zn Cu B Information Crop (tons/acre) N P2O5 0 0 0 0 0 Note:12 Lime History: 1 -Bermuda hay/past., E 0.5 , 60-80 0 50 0 2- 0.0 in CEC and Na in meq/100 cnr3; NO3-N in mgldnr3]: Soil Class:. Mineral Test Results [units - WN g/cO; S-I.. Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN � CEC BS% Ac pH P-I K-I Ca% Mg% . 0.2 2 1.43 1.05 9.5 80 1.9 5.8 570 ' 47 63 15 64 83 67 1336 1336 353 Re ort No FY19-SL009902 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr-govlagronomi/ P Page 7 of 11 Nutrients (lb/acre) More Sample ID: 27 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tonslacre) N P20s 0 0 0 0 0 Note:12 Lime History: 1-Bermuda hay/past., E 0.0 60-80 0 60 0 ' 2- 0.0 WN in CEC and Na in meq/100 cd; NO3-N in mg/dm3]: Soil Class: Mineral Test Results [units - glcd; Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 , K-1 Ca% Mg% S-1 1.406 382 0.2 2 2.84 1.00 11.6 85 1.7 6.1 456, 41 66 18 58 80 1406 Nutrients (Ib/acre) More Sample ID: 28 Recommendations: Lime K20 M9 S Mn Zn Cu B Information Crop. (tons/acre) N P205 0 0 0 0 0 Note:12 Lime History: 1 -Bermuda hay/past., E 0.3 60-80 0 50 0 2- 0.0 in CEC and Na in meq/100 GO; NO3-N in mgldd]:Soil Class: Mineral Test7Resuultsnits-WN g/crrr�; S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS -I NO3-N HMCEC BS% Ac pH P-1 K-1 Ca% Mg% 0.2 2 -3.19 '0.96 12.4 81 2.4 5.9 708 47 61 18 60 81 66 1887 Nutrients (Ib/acre) 1887 542 More Sample ID: 29 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tons/acre) N P205 0 0 0 0 Note:12 1-Bermuda hay/past., E 0.0 60-80 0 40 0 .0 Lime History: 0.0 2- WN in CEC and Na-in meq/100 ctrr3; NO3-N in mg/dd]: Soil Class: Mineral Test Results [units - g/cO; Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS%° Ac pH P-1 K-1 Ca% Mg% S-1 416 0.2 2 1.87 0.98 11.8 85 1.7 6.1 670 53 65 18 57 83 65 1601 Nutrients (Ib/acre) 1601 . More Sample ID: 30 Recommendations: j Lime K20 Mg S Mn Zn Cu B Information Crop (tonslacre) N P206 0 Z 0 0 Note: 12 Note: Lime History: 1 - Bermuda hay/past., E 0.0 60-80 0 30 0 0 2- 0.0 in CEC and Na in meq/100 crrr�; NO3-N in mgldrrr�]: Soil Class: Mineral Test Results [units - WN g/cd; Mn Mn Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-I K-I Ca% Mg% S-1 1 2.15 0.93 13.9 86 2.0 6.0 715 61 69 15 60 85 68 2654 2654 705 0.2 NCDA&CS Agronomic Division Phone:. (919) 733-2655 Website: www.ncagr.goviagronomil No. FY1y:�LW0990Z Page 8 of 11 More Sample ID: 31 Recommendations: Lime K20 "" `.-. �-' -' Mg S Mn Zn Cu B Information Crop (tonslacre) N P205 0 Z 0 0 Note: 1Note: Lime History: 1 -Bermuda hay/past., E 0.3 60-80 0 40 0 0 2 - 0.0 WN in CEC and Na in meg1100 crrr3; NO3-N in mgldO]: Soil Class: Mineral Test Results [units - g/crrr3; Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac' pH P-1 K-1 • 0.2 1 1.80 r 0.90 13.6 84 2.2 5.9 808 51 67 15 60 88 3555 Nutrients (Ib/acre) 3555 890 More Sample ID: 32 Recommendations: Lime K20 M9 S Mn Zn Cu B Information Crop (tons/acre) N PzOs 0 Z 0 0 Note: 12 Note: Lime History: 1-Bermuda haylpast., E 0.0 60-80 0 40 0 pH$ 2 - 0.0 WN in CEC and Na in me4/100 cnr3; NO3-N in mg/drr$]: Soil Class: Mineral Test Results [units - glcrrr3; K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 3018 3018 749 0.2 1 1.25 1.06 13.6 • . 91 1.2 6.5 846 49 70 19 47 63 47 Nutrients (lb/acre) More Sample ID: 33 Recommendations: Lime K20 Mg S Mn Cu B Information Crop (tonslacre) N P206 0 0 0 0 0- 0 Note: 12 Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 70 0 2 - 0.0 WN in CEC and Na in meg1100 cO; NO3-N in mgldrrr3]: Soil Class: Mineral Test Results [units - g1crrr3; S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 . Ca% Mg% 0.51 1.08 10.4 89 1.1 6.4 558 36 64 23 46 80 59 .1499 Nutrients (Ib/acre) 1499 368 0.1 1 More Sample ID: 34 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tons/acre) N P206 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.6 60-80 0 60 0 0 •p 2 - 0.0 WN in CEC and Na in meg1100 crrr3; NO3-N in mg/drrr3]: Soil Class: Mineral Test Results [units - glcnr3; Ca% Mg% S-I Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 2545 2545 774 0.2 2 0.46 0.96 13.0 81 2.5 5.8 951 39 59 21 72 85 68 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/a No. FY19-SL009902 Page 9 of 11 More Sample ID: 35 Recommendations: Lime K20 "' 1­_- -' Mg S Mn Zn Cu B Information Crop (tons/acre) N P206 0 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 20 0 0 2- 0.0 WN in GEC and Na in meg1100 cd; NO3-N in mg1dm3]: Soil Class: Mineral Test Results [units - g1c0; Ca% M9% S-1 MiA Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 0.51 0.90 .17.9 86 2.5 6.0 1056 62 62 22 93 76 63 4172 4172 1074 - 0.3 2 More Nutrients (Ib/acre)Mn Sample ID: 36 Recommendations: Lime K20 Mg S Zn Cu B Information Crop (tons/acre) N P205 0 0 Z 0 0 Note: 12 Note: Lime History: Bermuda hay/past., E 0.0 60-80 0 1 -. 40 pH$ 2- 0.0 WN in CEC and Na in meq/100 crrr3; NO3-N in mgldrrr3]: Soil Class: , Mineral Test Results [units - g/crif; K-1 Ca% Mg% S-1 Mn-I Mn.-All Mn-AI2 Zn-I Zn-AI Cu-I ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 2 1.02 0.93 18.2 92 1.4 6.6 888 48 67 24 75 94 825 Nutrients (lb/acre) 2825 •686 .3 0.3 More• Sample ID: 37 Recommendations: Lime K20 M9 g Mn Zn Cu B Information Crop (tons/acre) N P206 0 0 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.0 60-80 0 50 0 pH$ 2- 0.0 WN in CEC and Na in meq/100 cnr3; NO3-N in mgldnr3]: Soil Class: Mineral Test Results [units - g/cm3; Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 0.51 1.21 7.4 94 0.4 6.9 302 42 68 23 30 100 64 711 157 0.1 1 More Nutrients (Ib/acre)711 Sample ID: 38 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop(tons/acre) N P206 0 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 0.3 60-80 0 30 0 0 2- 0.0 WN in CEC and Na in megI100 crrr3; NO3-N in mg/dnf]: Soil Class: Mineral , Test Results [units - glcrrr3; K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N HM% - WN WN CEC BS% Ac pH P-1 . 2 0.60 1.02 13.1 82 2.4 5.9 865 , 57 59 21 74 75 62 2.269 2269 718 0.2 Report No: FY1y-bL_u09902 NCDA&CS Agronomic Division Phone: (919) 733-2666 Website: www.ncagr.goviagronomil Page 10 of 11 Nutrients (lb/acre) More Sample ID: 39 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tons/acre) N P205 0 Z 0 0 Note: 12 Note: Lime History: Bermuda ha / ast., E 0.0 1 - y p 60-80 0 50 0 0 2 - 0.0 WN in CEC and Na in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral Test Results [units - g/cO; P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH 1 0.51 0.89 16.1 86 2.3 6.1 957 42 62 23 69 52 47 3745 3745 896 0.2 More Nutrients (Ib/acre) Sample ID: 40 Recommendations: Lime K20 Mg S Mn Zn Cu B Information Crop (tons/acre) N P205 0 Z 0 0 Note: 12 Note: Lime History: 1 -Bermuda hay/past., E 1.8 60-80 0 70 0 0 2 - 0.0 WN in CEC and Na in meq/100 cO; NO3-N in mg/dm3]: Soil Class: Mineral Test Results [units - g/cr&; Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N HM% WN CEC BS% Ac pH P-1 K-1 0.51 0.90 11.7 71 3A 5.3 950 36 54 16 72 72 60 3001 3001 920 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 to (50 Ib/1000 sq ft) at time, even if the report recommends more. You. can apply the rest in similar increments every six months until the full i is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. if Mg 'is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS -I levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note Secondary Nutrients and Micronutrients In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.gov/agronomi/pubs.htm. Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit www ncagr goylegronomi/Oboart4.htmVffsfind information that A Homeowner's Guide to Fertilizes may help you choose a comparable alternate. For more information, read No. FY19=5GiU9902 Page 11 of 11 Report Abbreviations Ac B BS% Ca% CEC Cu-I ESP HM% K-1 K20 Mg% MIN Mn Mn-All Mn-AI2 Mn-1 M-O N Na NO3-N ORG pH P-1 P205 S-1 SS-1 Test Results WN Zn-AI The first seven values [soil class, HM%, WN, CEC, BS%, Ac and pH] describe the soil and its degree o�facidity. The Zn-I remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-AI1, Mn-AI2, Zn-I, Zn-Al, Cu-1, S-I, SS -I, Na, ESP, SS-1, N3-N (not routine)available)] indicate levels of plant nutrients or other fertility measurement. Visit wwwrncaar gov noMi/uyrst.htm exchangeable acidity boron %•CEC occupied by basic cations % CEC occupied by calcium cation exchange capacity copper index exchangeable sodium percent percent Humic matter potassium index potash % CEC occupied by magnesium mineral soil class manganese Mn-availability index for crop 1 Mn-availability index for crop 2 manganese index mineral -organic soil class nitrogen sodium nitrate nitrogen organic soil class current soil pH phosphorus index phosphate sulfur index soluble salt index weight per volume zinc availability index zinc index <55� Statement Page: 1 Ayden Nitrogen 4728 Old NC 11 / P.O. Box 7 Ayden, NC 28513 Phone 252-746-2152 Conteritnea Metro Sewage Dist Po Box 477 Grifton, NC 28530 Date Number Description / Detail Balance Forward PaVments 01/22/2019 1004981 Regular Payment / Cash Payment 01/29/2019 1014967 Charge Invoice'- Due 02/28/2019 GPS Fees Dolomitic Lime - Bulk App Fees Materials Current 1,858.96 Ayden Nitrogen Statement Date: 01/31/2019 ID: 010202 Total Balance: $1,858.96 s Amount Remitted: Terms: Unless otherwise agreed in writing by Harvey Fertilizer & Gas Co, interest will accrue at a periodic rate of 1.5% per month. To avoid additional finance charges, payments must be in office by last day of month. .i-------- Your Share --------- i Quantity Price/Unit Extension / Prepaid Regular n nn 8.00 73.620 Acre 20.326 Tons 20.320 Each 1 - 30 31 - 60 61 - 90 Over 90 0.00 0.00 0.00 0.00 8.00 -8.00 Payment Total 8.00 0.00 -8.00 8.000 /Acre 588.96 588.96 49.000 !Tons 995.68 995.68 13.500 /Each 274.32 274.32 Invoice Total 1,858.96 0.00 1,858.96 Ending Total Balances 0.00 1,858.96 Unapplied Budget Billing Prepay Overall 0.00 0.00 0.00 1,858.96 19�r C ju Zvi awe d Zo l 9 I Date: 01/31/2019 Contentnea Metro Sewage Dist FIR /Ll,��/ .�+� •� "airy_„' K•. • :l w v 13n -:tsyi cross tic. ter, . Legend 4.07ItedPic. Monitor Well The Compliance Boundary shall be House located 50 feet within the property line-0 ' Stream `- or 250 feet from the edge of the r disposal area, whichever is closer to the — —► Ditch source. The Review Boundary shall be �NetArea located halfway in between the property rF line and the Compliance Boundary. ® Buffer G_ Field Boundary '0 150 300 600 � Pond Feet Scale: I inch = 300 feet SOIL PLUS BUFFER MAP 19 & 20 FIGURE CMSD CLASS B LAND APPLICATION Drawn By: CSC - 1 Class B Permit WQ0001048 Reviewed By: Soil Plus Project # 200710.A10 Date: June'18 �- I E I i