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WQ0035595_Modification_20190321
INITIAL REVIEW Reviewer Thornburg, Nathaniel Project Number* WQ0035595 SUBMITTAL DATED: 3/21/2019 Project Contact Information Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Drew Matthews Email Address* dmatthews@soilplus.net Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater r Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number WQ0035595 currently has project Permittee* Granville Farms, Inc. Facility Name * Granville Farms RLAP Phone Number* 2528839301 r Modification (Major or Minor) r Additional Information r Other r High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Hc.) GFI WQ0035595 Modification March 19.pdf 34.49MB Wload only 1 RDF document. NUltiple documents rust be corrtined into one RDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature iar_?A 2 Submission Date 3/21/2019 GRANVILLE FARMS, INC. PERMIT MODIFICATION CLASS B PROGRAM WQ0035595 Submitted by: Soil Plus PO Box 1396 Oxford, North Carolina 27565 March 2019 50IL PLUS SOIL PLUS March 19, 2019 NCDEQ-DWR Aquifer Protection Section Land Application Unit 1636 Mail Service Center Raleigh, North Carolina 27699-1636 Attention: Mr. Nathaniel Thornburg Reference: PERMIT MODIFICATION Granville Farms, Inc. Residual Biosolids "Class B" Program Permit WQ0035595 Soil Plus Project No. 200705.D10 Mr. Thornburg: Soil Plus, LLC (Soil Plus) is submitting one paper copy and one electronic copy of this permit modification application package for Granville Farms, Inc. (WQ0035595). This package includes: 1. Completed Residual Land Application Program Application 2. Completed Residual Source Certification Attachment a. Sunset WTP (New) b. Tar River Regional WWTP (New) c. Tar River WTP WWTP (New) d. Hominy Creek WRF (Modified) 3. Completed Land Application Site Certification Attachment a. Site T1 (Transfer from WQ0002047) b. Site T6 (Transfer from WQ0002047) This package is designed to add (3) new facilities, increase the permitted dry tonnage for (1) facility, and transfer (2) farms from permit WQ0002047 totaling approximately 153 acres. A check for $395 is enclosed with this package per the Division of Water Resources Land Application Unit's fee schedule for a major modification to a major non -discharge permit. Soil Plus will be responsible for completing this permit application for the Granville Farms, Inc. If there is any further information required or questions regarding this permit application, please do not hesitate to contact me for assistance. Respectfully, PO Box 1396 Z/)t"f _ {'e t (.C%LQ.1Ud1 Oxford, NC 27565 Drew Matthews, Soil Plus (252) 883-9301 dmatthews@soilplus.net Jason Smith, Granville Farms, Inc. www.soilplus.net Granville Farms, Inc. Permit Modification WQ0035595 Edgecombe County, NC Residual Land Application Program Application Weighted Source PAN Calculations Revised O&M Plan Residual Source Certification Attachment Sunset WTP Analytical/Field Loading Calculations Residual Source Certification Attachment Tar River Regional W WTP Analytical/Field Loading Calculations Residual Source Certification Attachment Tar River WTP Analytical/Field Loading Calculations Residual Source Certification Attachment Hominy Creek WRF Analytical/Field Loading Calculations Site T1 Land Owner Agreement Form Maps Biosolid Utilization CPLR Update Site T6 Land Owner Agreement Form Maps Biosolid Utilization CPLR Update Current Permit APPENDIX 1 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Land Application Program Application RLAP Weighted Source PAN Calculations Revised O&M Plan State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water Resources 15A NCAC 02T.1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 03-15 I. APPLICANT INFORMATION: 1. Applicant's name: tranville Farms, Inc. Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Jason Smith Title: Vice President Applicant's mailing address: P.O. Box 1396 City: Oxford State: NC Zip: 27565-__� Telephone number: (919) 690-8000 Email Address: jsmithkgranvillefarmsinc.com 2. Consultant's name: Drew Matthews License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: Soil Plus, LLC) Consultant's mailing address: PO Box 1396 City: Oxford State: NC Zip: 27565 - Telephone number: (252) 883-9301 Email Address: dmatthewsgsoilplus.net 3. Agronomist's name: License Number: Affiliation: ❑ N/A ❑ On Staff ❑ Retained (Firm: ) Agronomist's mailing address: City: State: Zip: W__ -M Telephone number: (_) = Email Address: In - 4. Soil Scientist's name: License Number: Affiliation: ❑ N/A ❑ On Staff Retained (Firm: ) Soil Scientist's mailing address: City: I State: j—_ Zip: W__ Telephone number: (_�) I - Email Address: 5. Fee submitted: $395.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: WQ0035595 Date of most -recently issued permit: 10/10/2016 Date of most -recently certified Attachment A (if different than the permit): 9/17/2018 Date of most -recently certified Attachment B (if different than the permit): 9/17/2018 FORM: RLAP 03-15 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: NA City: State: Zip: Coordinates: Latitude: _° Longitude: Datum: —M Level of accuracy: Method of measurement: County where residuals land application program is headquartered: _ 1. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Jason Smith Granville Farms, Inc. 13266 Back -Up ORC Bryan A. Smith Granville Farms, Inc. 13265 Additional Back -Up ORCs if applicable) 50.81 62.52 402,695 If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 2. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 7,926 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 35.8 51.47 283,724 407,919 Five -Year Maximum Adjusted 50.81 62.52 402,695 495,535 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation Row Crops 400.33 Hay 127.85 Pasture Total: 528.18 Methods Surface 528.18 Incorporation or Injection Total: 528.18 FORM: RLAP 03-15 Page 2 of 4 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac-yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 5,674.49 8,158.38 8,053.90 9,913.31 100 2,837.24 4,079.19 4,026.95 4,955.35 150 1,891.50 2,719.46 2,684.63 3,303.56 200 1,418.62 2,039.59 2,010.69 2,477.67 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.): Many of these sources will also maintain their current land application program coniunction with this one. Basicallv for most sources this hermit will not serve as an exclusive land annlication moeram. but rather as a supplement. 7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): ❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; � ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. Land Application Siite Certification.doc FORM: RLAP 03-15 Page 3 of Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T.0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T.0105. 0 Yes d No, Explain; I, Jason Smith Vice President (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Granville Farms Inc. (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes §143-215.6A and §143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. Signature: J 0,06" Date: 3-1,9-1 FORM: RLAP 03-15 Page 4 of 4 Q a 0 0 I s i a b I N 0 I i O11 O O 11 N a wM N N W a W r N* O'' a S W& r F 0 1, b O W M W g N a N a 0 M W 0 r?� M 1 N g W" O ? I a a M 9 A M? 4 vMi a c M OM N M a a c M r M M N� .� a .� M� M M W •� a0 vi O M vii .� �� r N O M� O� M� M O r C` O a f vi N N� o N W M q CO N O NN aO0N� NO Nr ? Q. .• O r O � c0 w N N � i L � u C N w% N or a O r I oI M N 1 �9" p a o N 1 m 114! o 115 w v I A N N a 14 04 NN Na - --- N M- r N N� N " N N N - N - ti N N ti - ti N N N N- - ti N ti N N� 'V M .+ M - N- ti a N1 2O N rcrrt O NN mS MM �W .-N a -NN N O :D� aa !2 Ma CNr Em o r O /Cay E N O O O 1111 E M M M E N 1115 ti OO5 O N N O W 1 1 O E 0 ti 115 15 3 N N 0 0 0 0 c'i O C o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o S Q r E x. C q° ,� o• a x u h 'rte c:JCg c� o m Cj > $ > v aj .c $ 3 a 2 x H H w a v o 00 0 0 a ��N GRANVILLE FARMS, INC. OPERATION AND MAINTENANCE PLAN LAND APPLICATION OF CLASS B RESIDUAL BIOSIOLIDS WQ#0035595 Revised March 2019 1.0 SUMMARY Granville Farms, Inc. (GFI) is a privately owned company that is contracted to haul and land apply nutrient enriched by-products such as Biosolids from Wastewater Treatment Plants, Residuals from Water Treatment Plants, Animal Waste from Animal Production Facilities, and certain Construction Debris from Road Work (i.e. slurry water from diamond cutting of concrete). GFI is unique in that it does not participate in the generation or treatment of the by- products generated by any of the source types listed above. At times GFI is requested to provide lime stabilization of Biosolids by smaller operating facilities, but this quantity is normally very small. GFI's main role is to provide transportation and operational equipment to spread the nutrient enriched by-products listed above. Another unique characteristic about GFI is that it owns and maintains permits to land apply these by-products. Given that most generators are issued their own land application permit, they have direct oversight of the preparation, removal, and application of their by-products. This creates some operational and permit challenges for GFI since standard, state issued permits are typically issued to generators not land application companies. This Operation and Maintenance Plan (O&M) addresses how GFI is able to manage by-products produced by multiple, independent generators and land applies under their own land application permit. Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN SAMPLING & ANALYTICAL 2.0 ANALYTICAL REQUIREMENTS Prior to the hauling and land application event being schedule the generator must provide analytical results documenting that all parameters listed in Condition IV. 2 — 4 and at the frequency listed in most recent copy of this permit. If GFI does not collect the sample then it DOES NOT own the responsibility of the integrity of the sample and the method it was collected, transported, submitted, and analyzed. Should the generating source elect to have GFI collect the sample prior to land application, then it will be done in the following manner: Four factors that may ultimately affect the integrity of reported data include: 1) obtaining a representative sample, 2) preventing contamination of the sample, 3) providing legal documentation of the sampling event, and 4) protecting the sample from chemical, physical or biological change prior to analysis. A sample will be collected according to the schedule provided in the most recent copy of the Attachment of this permit and prior to land application one composite sample should be pulled from a designated location from the generating source. GFI has identified Meritech, Inc. out of Reidsville, NC to be used as the Certified Laboratory. The composite sample should be analyzed for: • % Solids, • Nitrogen Series (TKN, Ammonia, Nitrate, Nitrite, and Organic Nitrogen), • Phosphorus, • Potassium, • Sulfur, • Calcium, • Magnesium, • Sodium, • Iron, • Aluminum, • Manganese, • Copper, • Zinc, • and Remaining 503 Metals (i.e. Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium) Approximately 2 quarts of residual should be collected. The sample containers should be clean and sterile. They should also be labeled so that they are easily identifiable in the lab. The samples should be pulled using the method listed below: ❖ Collect one sample from each digester(s) from which the material will be land applied using a "swing sampler" o The swing sampler must be used with a sterile, plastic 960 ml container ❖ Combine each sample in a stainless steel bucket ❖ Mix thoroughly using a fiberglass rod ❖ Collect each sample from the top of the access point at each digester. This access point is obtained by climbing the installed ladder on the side of the digester. Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan Once the sample is pulled, it should be placed in medium size cooler packed with ice. The sample should be collected with an enough time so that it can be delivered to the laboratory. Once per calendar year (if applicable) a sample should be collected and submitted to Meritech, Inc. in Reidsville, NC. This sample should be analyzed for: • Full TCLP • Ignitability, Corrositivity, and Reactivity • Requires 5 Liters (In Opac Glass Bottles) If required, a third should be submitted to Meritech, Inc. for a 30 -Day Scale Bench test and Fecal Colifom Density. The 30 -Day Scale Bench Test also requires 1 quart of "clear" water from the Clarifier for Dilution if necessary. This sample would be analyzed for: • 30 -Day Scale Bench Test (4 Quarts of Residuals and 1 Quart of Clarifier water) • Fecal Coliform Density Test (seven pint samples) The contact information for the lab is: Mailing Address Meritech, Inc. 642 Tamco Rd Reidsville, NC 27320 (336) 342-4748 Sampling frequency will be conducted in accordance with the Table listed in the most recent Attachment A of this permit. The sample will be collected by a representative of Soil Plus, LLC. For further information please contact: Drew Matthews PO Box 1396 Oxford, NC 27565 252-883-9301 Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN OPERATION, SPILL CONTROLL, & TRAINING 3.0 BIOSOLIDS REMOVAL, TRANSPORT, AND APPLICATION Biosolids will be transported from the generators to suitable, permitted land application sites. Transport equipment will be inspected, licensed and appropriately marked, as required, for the purpose of transporting biosolids. Biosolids will be delivered to the application sites between sunrise to sunset. Both liquid and dewatered biosolids distribution on the land application sites will be uniform throughout the application area. To ensure adequate control of the application rate for each site, the equipment used for spreading the sludge will be calibrated by measuring the amount handled on a known square footage. While the rate of discharge from the application vehicle is fixed, the speed of the equipment can be adjusted to maintain the flow rate needed to achieve specific application rates. Spreading operations will be discontinued during periods of inclement weather and will not be resumed until sufficient drying of the fields has occurred. This allows equipment access without causing excessive soil compaction or rutting. To prevent adherence of the biosolids, transport vehicles will be equipped with rear mud flaps, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. Examples of our application tracking and summary form/reports can be provided upon request. 4.0 SITE OPERATION Biosolids will be surface applied at the properly -calculated agronomic rate and in strict accordance with any state and federal regulations for the land application of the biosolids. Buffer zone distances will be observed in accordance with applicable state and federal regulations. Buffer zones will be flagged and no biosolids will be applied within those areas. The most restrictive buffer will apply in combined situations. Operational provisions will be taken to prevent soil loss through erosion. Provisions will include contour application and avoidance of areas where surface drainage patterns result in concentrated flow of runoff from rainfall. In accordance with sound, industry standard agronomic practice, areas which are unseasonably wet (and would produce rutting or damage to the field) will not be utilized for biosolids application operations during those periods. Operations will be discontinued when soils are saturated and will not be resumed until the field has sufficient dried. The amount of biosolids applied will not exceed the hydraulic capacity of the soil at the time of each application. If a subsequent pass across a field is necessary to achieve the desired application rate, sufficient drying time will be allowed between passes. 5.0 PROJECT CONTROL To ensure biosolids are continuously applied at the correct application rate and in a manner consistent with the Operations Plan, a GFI Project/Field Manager will be in direct charge of the field operations, controlling the amount of biosolids delivered to each field, and conducting daily field inspections. Field inspections will include ensuring that flags are in place, biosolids are applied uniformly at the designated application rate, setbacks are observed, trucks are unloading at best location, trucks are not driving over biosolids, trucks are cleaned before leaving the field and the land application equipment is maintained in working condition. 6.0 TRANSPORTATION SYSTEM ROUTING Per the specifications, GFI transportation vehicles will be equipped with GPS devices that will guide drivers to the land application sites. Transportation routes will follow primary highways and avoid residential areas where possible. Designated routes are followed unless a detour is specified. In the event of a detour route, it shall be taken as specified by the detour authority. There shall be no unscheduled stops when loaded. Transportation vehicles will be inspected, licensed and appropriately marked as required with identification numbers for the purpose of this contract. All units will be equipped with spill guards and full mud flaps. This will prevent the biosolids from adhering to the tires and undercarriage of the transport vehicle, thereby preventing biosolids from being tracked onto roadways. Biosolids adhering to the mud flap will be scraped off in the field before the truck returns to the roadway. All federal OSHA Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan and DOT laws and regulations are complied with for the protection of our clients, the community and our drivers. Examples of vehicle and driver transportation logs and inspection forms can be provided upon request. 7.0 DEWATERED BIOSOLIDS Dewatered biosolids will be transported in standard end dump trailers with a capacity of 22 wet tons. The tankers will be loaded per the generator's specifications and standard protocols. The aluminum dump trailers used for transportation of dewatered cake biosolids will be equipped with sealed tailgates and will be completely sealed to prevent leakage. All trucks will be fully covered and will be fitted with positive lock tailgates. 8.0 LIQUID BIOSOLIDS Liquid biosolids will be transported using 6,500 gallon capacity liquid tankers, pulled by standard road tractors, for liquid biosolids transportation. The tankers will be loaded per the generator's specifications and standard protocols. The tractor/tanker unit will transport its load to a designated staging area inside the buffered area of a permitted land application site. 9.0 APPLICATION (SPREADING) — DEWATERED BIOSOLIDS At the staging area each load will be unloaded in.a designated area within the land application site. Biosolids will be loaded into our Side Slinger cake box by a GFI employee using a front-end loader. This unit is capable of delivering an accurate, calibrated application of dewatered biosolids over the application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual PAN requirement. 10.0 APPLICATION (SPREADING) — LIQUID BIOSOLIDS At the staging area each load will be transferred into a 4,000 gallon capacity pull behind subsequent land application. This unit is capable of delivering an accurate, calibrated application of liquid biosolids over the application site. The uniform spread pattern ensures that biosolids are applied at proper agronomic (nutrient) and hydraulic loading rates. The application rates for each site, and its corresponding crop, will be determined based on the Plant Available Nitrogen (PAN) content of the biosolids, or other limiting factors. Typical applications will deliver between 75 and 100 percent of a crop's annual PAN requirement. 11.0 SPILL AND EMERGENCY RESPONSE PROGRAM In the unlikely event of a spill, GFI will take the following actions immediately. • Halt Source of Spill. Use of any leaking or damaged unit which is causing the spill will cease immediately. The unit will be repaired before resuming its use. • Contain Spill. In the event large quantities of biosolids have been spilled, straw bales will be used where available and as necessary to either form a barrier or absorb biosolids. • Clean -Up. Depending on the type and amount of biosolids spilled, a variety of equipment may be used to remove the biosolids: front-end loader, shovels and brooms and vacuum equipment of a liquid biosolids applicator. Any biosolids removed from the spill site will be spread on an approved application site, returned to the WWTP, or disposed of in an approved landfill. Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan • Final Clean -Up. Flush roadways with water or sweep as necessary to clean. Allow to dry and incorporate if spill occurs on non -paved and tillable area. In the event a spill occurs on private property, final clean-up should be completed immediately to the satisfaction of the owner. • Management of Clean -Up Efforts. The Operations Manager will take immediate charge and initiate clean-up activities. GFI labor will be used, with additional labor secured as needed. The Operations Manager will also communicate with the public on the scene, answering questions and advising of clean-up activities. • Reporting. All spills will be reported immediately to GFI offices and the client. State and local agencies will be notified in accordance with their notification requirements. Within 24 hours of the spill, the Operations Manager will send GFI office a written report detailing how the spill occurred and remedial action taken. This report will be provided using the enclosed Spill Report form. • Spill Prevention. The Operations Manager will implement the following spill prevention measures: o Ensure truck drivers watch trailer while loading and do not overload; o Ensure trailer hatches are closed and latched while transporting; o Ensure trailer seals are inspected on a daily basis and replaced as necessary; and o Ensure unloading operations in the field are conducted to minimize any potential runoff or tracking. All employees receive safety and spill response training as part to their new hire training and thereafter participate in our monthly safety and spill response training program. In addition to our internal training and protocols, we also contract with a regional emergency response firm - HEPACO - available to respond to an incident in the Central and Eastern North Carolina area within two hours. A copy of our agreement with HEPACO can be provided upon request. Names and Titles of Inspection Personnel Andy Smith, Area Supervisor Jason Smith, Area Supervisor JT Bryant, Regional Supervisor Jay Bryant, Project Supervisor Matt Foster Project Supervisor BJ Bryant, Field operator Jeff Bumpass, Field operator Tammy Walston, Field operator 12.0 PREVENTION The goal of a compliance assurance system is to prevent compliance issues from occurring. Prevention involves: • Ensuring personnel understand their role in assuring compliance; • Identifying compliance requirements at the federal, state and local levels; • Implementing a system where compliance tasks are scheduled, assigned and tracked to completion; • Developing standard operating procedures where appropriate; and • Reviewing the compliance task list and standard operating procedures on an ongoing basis and modifying them as appropriate to account for changes in regulations/requirements and operating methods, and to address compliance deficiencies. Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan GFI ensures employees understand their role in assuring compliance through new employee orientation programs and on the job training. 13.0 Standard Operating Procedures (SOP's) GFI develops and implements SOPs to ensure compliance tasks are completed consistently across the company. The SOP provides standard forms to use, approved biosolids analytical methods, frequency of monitoring information, etc. Another key SOP relative to preventing compliance issues from occurring is the use of a "Pre - Operating and Buffer Checklist". The Pre -Operating and Buffer Checklist ensures federal, state and local regulations and permit requirements are met prior to initiating biosolids applications at field sites. Compliance items on the Checklist include: • The field is permitted and suitable for the biosolids/residuals type being applied; • Pre -application requirements are met; • Farmer and landowner agreements are current and the crop to be grown has been verified; • The field is flagged to prevent applications in buffer zones and restricted areas; • The appropriate application rate and field capacity is calculated; and • Any special permit or local requirements are met. • A listing of the buffer zones and restricted areas where biosolids/residuals cannot be applied • A listing of operating requirements including notification requirements, • application method requirements, and inclement weather operating requirements 14.0 ASSESMENT To help ensure compliance requirements are being met and the compliance assurance system is implemented and working, periodic, consistent, objective and documented assessments of a project/ facility's compliance status are conducted. GFI personnel have clearly-defined compliance assessment responsibilities and time to conduct such assessments. GFI conducts informal site inspections and formal audits on an ongoing basis. 15.0 CORRECTIVE ACTION Once compliance issues have been identified during the course of day to day business and through internal audits and inspections a system must be in place which ensures that appropriate and timely corrective action is taken, the cause of the compliance issue is identified and actions are taken to prevent recurrence of the issue. GFI's goal is to have no instances of non-compliance. However, issues and incidents may occur and when this happens employees work to correct the incident in a timely and thorough manner. When compliance issues are identified, the situation is examined to determine the root cause of the problem and the corrective and preventive action that must be taken. The preventive action must address the root cause with the goal of preventing a recurrence. Depending on the nature of the compliance issue, it is assigned to one or more responsible parties to ensure that the corrective and preventive actions are implemented. A deadline for completion of the task is assigned and the issue is tracked to completion by regional and corporate compliance personnel. 16.0 TRAINING An effective compliance training program involves: • Identifying training needs and requirements; Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan • Assigning personnel to provide training and providing them the resources they need to conduct training; • Documenting and tracking that mandatory t raining has occurred; and • An employee's training needs and requirements, as well as their training responsibilities, are based on his/her position within the company. Revised 03/19 ©Granville Farms, Inc. Operation and Maintenance Plan GRANVILLE FARMS O&M PLAN PROCESS FLOW DIAGRAM GRANVILLE FARMS CLASS B WWTP SOURCES Ahoskie WWTP Amherst WWTP Ashley Hills WWTP Avocet Barclay Downs WWTP Beachwood WWTP Briar Chapel WWTP Briarwood Farms WWTP Carolina Meadows WWTP Cole Park Plaza Colvard Farms Contentnea MSD Crooked Creek WWTP Cross Creek WWTP Deerchase WWTP Govenor's Club WWTP Hasentree Golf Community Hawthorn Subdivision WWTP Hominy Creek WRF Kenly Regional WWTP Kings Grant Subdivision Knightdale Mobile Home Park Lake Ridge WWTP Legacy at Jordan Lake Mallard Crossing WWTP Nature Trails MHP WWTP Neuse Colony WWTP Neuse River Resource Recovery Facility Neuse River Village Perdue WWTP Pikeville WTF Plymouth WWTP Preserve at Jordan Lake River Mill WWTP Robersonville WWTP Rock Bridge WWTP Snow Hill WWTP Stantonsburg WWTP Tar River Regional WWTP Tarboro WWTP Tradewinds WWTP Westfall WWTP Williamston WWTP Whippoorwill Valley WWTP Wildwood Green WWTP Willowbrook WWTP These sources coorespond to the attached flow diagram provided below. m L co U U Ln a 0) LU N 2 L ot V N = Y� L! yn Cr LL b J � L Q (D � L co Q o U J Q a Lu c 0 Un a � Uod abpnlS palenllOV ua nja�{ cu mL W Q a ) Q �.± O O J od N Q 40 LU J Y L LE a a J �y J O V X O m C O C GRANVILLE FARMS CLASS B WTP SOURCES Martin County WTP Sunset WTP Tar River WTP These sources coorespond to the attached flow diagram provided below. 70 0- --0-.Q) m 1 i i2 Q Q)_ Q U) c a •� W co CO 0 V 2 o O �_ (0 r � J LL J •i� r'n C U) >m _0 O E cu 0 i) a) U) 0 N m o o U) 0 J � a U � U N 0 O c0 LL 0) V/ cu U � �y O m N a N H c ii = � o JFL V N--V,l/11i a/ U a E L W U J J_ Z (D C7 � cu a� U 0 cu 3 c0 GRANVILLE FARMS O&M PLAN MAXIMUM PRODUCTION QUANTIFICATION & JUSTIFICATION 35,316,544 4,677 AVERAGE #of Forecasted Requested Gallons Dry Tons W Years Counted Production DT 1,257,257 177.12 Ahoskie WWTP 7 Ahoskie 354.24 280 40,686 2.50 Amherst WWTP 7 Amherst WWTP 5.00 10.00 - - Ashley Hills WWTP 1 Ashley Hills WWTP 0.00 20.00 97,900 8.35 Avocet 1 Avocet 16.71 10.00 21,614 0.53 Barclay Downs WWTP 7 Barclay Downs WWTP 1.07 10.00 21,360 1.52 Beachwood WWTP 5 Beachwood WWTP 3.04 10.00 119,575 10.55 Briar Chapel Development 2 Briar Chapel Development 21.10 30.00 71,756 4.50 Briarwood Farms WWTP 8 Briarwood Farms WWTP 9.01 30.00 354,481 32.38 Carolina Meadows WWTP 8 Carolina Meadows WWTP 64.76 50.00 63,969 5.68 Cole Park Plaza 8 Cole Park Plaza 11.37 10.00 8,981 0.42 Colvard Farms 8 Colvard Farms 0.85 10.00 205,800 20.98 CMSD 5 CMSD 41.96 319.00 115,150 10.30 Crooked Creek WWTP 8 Crooked Creek WWTP 20.60 25.00 45,613 1.83 Cross Creek Mobile Estates 8 Cross Creek Mobile Estates 3.67 10.00 68,263 3.01 Deerchase WWTP 8 Deerchase WWTP 6.02 10.00 167,443 7.61 Govenor's Club WWTP 7 Govenor's Club WWTP 15.23 20.00 40,050 3.91 Hasentree Golf Community 1 Hasentree Golf Community 7.82 30.00 266,388 22.94 Hawthorne Subdivision WWTP 8 Hawthorne Subdivision WWTP 45.88 100.00 1,241 327.50 Hominy Creek WRF 3 Hominy Creek WRF 654.99 1000.00 937,350 80.15 Kenly Regional WWTP 8 Kenly Regional WWTP 160.29 318.00 28,925 1.59 Kings Grant Subdivision 8 Kings Grant Subdivision 3.19 10.00 67,306 5.67 Knightdale Mobile Home Park 8 Knightdale Mobile Home Park 11.35 15.00 20,025 1.73 Lake Ridge WWTP 6 Lake Ridge WWTP 3.45 10.00 - - Legacy at Jordan Lake 1 Legacy at Jordan Lake 0.00 20.00 79,544 6.18 Mallard Crossing WWTP 8 Mallard Crossing WWTP 12.36 15.00 288,167 18.44 Martin County WTP 3 Martin County WTP 36.87 319.00 137,950 5.75 Nature Trails MHP WWTP 7 Nature Trails MHP WWTP 11.50 20.00 886,571 62.25 Neuse Colony WWTP 7 Neuse Colony WWTP 124.49 100.00 77,319 3.79 Neuse River Village 8 Neuse River Village 7.58 15.00 4,324,622 619.60 Neuse River WWTP 6 Neuse River WWTP 1239.20 1500.00 1,215,350 246.09 Perdue WWTP 4 Perdue WWTP 492.17 600.00 53,625 6.23 Pikeville WTF 4 Pikeville WTF 12.46 75.00 441,875 41.05 Plymouth WWTP 8 Plymouth WWTP 82.11 85.00 116,400 5.97 Preserve at Jordan Lake 2 Preserve at Jordan Lake 11.94 20.00 - - River Mill WWTP 1 River Mill WWTP 0.00 10.00 369,080 59.93 Robersonville WWTP 5 Robersonville WWTP 119.87 80.00 46,725 3.12 Rock Bridge WWTP 4 Rockbridge WWTP 6.24 10.00 224,725 29.28 Snow Hill WWTP 6 Snow Hill WWTP 58.56 50.00 110,600 10.40 Stantonsburg WWTP 5 Stantonsburg WWTP 20.81 50.00 2,627,333 418.47 Sunset WTP 3 Sunset WTP 836.94 318.00 12,373,833 1,152.88 Tar River Regional WWTP 3 Tar River Regional WWTP 2305.76 800.00 4,627,000 654.11 Tar River WTP 3 Tar River WTP 1308.21 318.00 2,445,625 516.80 Tarboro WWTP 8 Tarboro WWTP 1033.61 829.00 79,656 3.88 Tradewinds WWTP 8 Tradewinds WWTP 7.76 10.00 13,350 0.81 Westfall WWTP 1 Westfall WWTP 1.62 10.00 43,706 1.94 Whippoorwill Valley WWTP 8 Whippoorwill Valley WWTP 3.88 10.00 75,413 6.08 Wildwood Green WWTP 8 Wildwood Green WWTP 12.15 15.00 567,014 70.26 Williamston WWTP 7 Williamston WWTP 140.51 300.00 69,929 3.18 Willowbrook WWTP 7 Willowbrook WWTP 6.36 10.00 9,354.54 7,926.00 35,316,544 4,677 GRANVILLE FARMS O&M PLAN SOURCE VICINITY MAPS SOURCE FIGURE Ahoskie WWTP 1 Amherst WWTP 2 Ashley Hills WWTP 30 Avocet 3 Barclay Downs WWTP 4 Beachwood WWTP 4 Briar Chapel Development 7 Briarwood Farms WWTP 5 Carolina Meadows WWTP 6 Cole Park Plaza 7 Colvard Farms 8 Contentnea MSD 9 Crooked Creek WWTP 2 Cross Creek WWTP 4 Deerchase WWTP 10 Governor's Club 6 Hasentree Golf Community 11 Hawthorne Subdivision WWTP 12 Hominy Creek WRF 13 Kenly Regional WWTP 31 Kings Grant Subdivision 14 Knightdale Mobile Home Park 4 Lake Ridge WWTP 15 Legacy at Jordan Lake 16 Mallard Crossing WWTP 17 Martin County WTP 26 Nature Trails MHP WWTP 6 Neuse Colony WWTP 18 Neuse River RRF 14 Neuse River Village 4 Perdue WWTP 29 Pikeville WTF 19 Plymouth WWTP 20 Preserve at Jordan Lake 16 River Mill WWTP 21 Robersonville WWTP 22 Rock Bridge WWTP 14 Snow Hill WWTP 23 Stantonsburg WWTP 24 Sunset WTP 33 Tar River Regional WWTP 34 Tar River WTP 35 Tarboro WWTP 25 Tradewinds WWTP 10 Westfall WWTP 32 Williamston WWTP 26 Whippoorwill WWTP 27 Wildwood Green WWTP 12 Willowbrook WWTP 28 N W E S 2 �G�j 4 Pinewood Manor Rest Home Ahoskie WWTP HERTFORD .I Ahoskier3 Legend ❑ NC Sources — Road ❑ County Boundary BERTIE ❑ Municipal Boundary ❑ River Ahoskie 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Ahoskie, North Carolina 1 Date: January '17 Soil Plus Project # 200705.C10 � N / SR- CAW Ei083 SR - 4i r SR - Cary a Springs IX"N 1568 FSR - SR `N� w A� SszO FUgOU 7SR-3942 CSR' -1467 SR�1391 �j � m N SR-1Sp3 I l v � � SR -1504 7 o c +.� � ti JIQ g uquay- SR -473; SR-39� 2811 I � I dle o iSg� NP Cr eek SR -2724 M SR -5006 -"733F-1 ( JJ r Fuquay-Varina SR -3952 �s SR '1595t' �1� 2393 Fuquay-VaAna S SR 39 � c� M SR -3959 m r SR_4038� � v � Boa Oti it �5� N SR -2752 S Fuquay-Varina Legend I SR -3730 Source Location Terrible Creek Fuquay-Varina — Road s�R,-356 s' R-315, Stream sR-41615 County F L_JounY Boundar Y SR -4813 L Municipal Boundary N 0.5 0.25 0 0.5 39 Miles SA 4881 Scale: 1 inch = 0.5 miles SOIL PLUS LOCATION MAP Figure 2 Drawn by: CSC GFI Land Application Permit (WQ0035595) Reviewed by: CSC Fuquay-Varina, North Carolina Date: Sept 16 Soil Plus Project # 200705.G10 Y N L a) W E S Y O S -P Y — v a) a> U Y a3 o'o Shearon Ha ris uclear Power Plant( S-� 1 27 a W wee o I 12 �J 115 1394 Q I� K 17 Ott o i s TP 1395 1123 1174 4 4024 1104 1 96 s Q �~ 1 01 1103 1126 IQ 1113 7274 n 1122 ei o 1 11 v 111,2S 1112 Twin L ke T o I. N 242 25 24 a 1 J 1110 c� II 2Q Q I 1123 1104 N Q 1103 IQ JIJB 7274 n 1122 /L Jl � 0 22 � CHATHAM 191 s tip° 1120 o t �ti ti J 140 � ~ 1 14 c w 1451 Legend 68 0 Source ee �5 Water — Stream Road e� Gte �eC� Sent rs t o 0 =County Boundary �� 0 Municipal Boundary , Ago 1 0.5 0 1 141a Miles 141 Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838) Reviewed by: Holly Springs, North Carolina 3 Date: Nov'17 Soil Plus Project # 200705.D10 N W E S 6 SR -2680 SR -2625 a �P A WAKE Raleigh Carolina Lak 0 1Wvvu L/ �\ h U' US 64 BUS SR -2946 NSrl:2s9� M � S y �5 � SR 2592 k, D 11 SR -416 SR -2593 ;l c, `SR -4188 Knightdale SR -4102 SR SR -2671 N Q S� 2608 6,31 < Neuse River Village j °K-1007 Knightdale MHP Cross Creek 0 Legend Source Location h 6 — Road • Stream J, IL _J County Boundary SR -2678 L Municipal Boundary 0.5 0.25 0 0.5 Miles r3, Scale: 1 inch = 0.5 miles SOIL PLUS LOCATION MAP Figure 4 Drawn by: CSC GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina Date: Sept 16 Soil Plus Project # 200705.G10 N \W E S � Cary V a SR -1010 Cam � co n � �ra�cli SR -so ^MO � SR -1448 542q v. SR SR -5098 WAKE s� ti p' SR -4017 Briarwood SR -5845 ❑ SR -4797 1 C� Sk3939 SR -3951 SR -3934 � m I �o SR -I172 0� SR_ 5832 SR -3937 5830 n u w \S AC)" J SR -1484 fir, N Legend .Source Location Holly Springs Sti53 s — Road r Stream Sg9 I SR -1390 aCounty Boundary F-1municipalBoundary o 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Cary, North Carolina 5 Date: Sept 16 Soil Plus Project # 200705.G10 N VV E Ste" ORANGE S --------------- <---- ---- SR-2001 Sg,1'116 S-1811 SR 1832 SR S� CHATHAM Morgan Creek N r Trail Morgan O� y Chatham WRF of Jordan Lake Legend SR -1753 Source Location — Road New Hope Rv Arm of B. Everett Jord Stream New Hope River Arm of B. Everett J [--_]County Boundary L Municipal Boundary c r Surface Water 40.5 0.25 0 0.5 Miles It Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Durham, North Carolina 6 Date: Sept 16 Soil Plus Project # 200705.G10 va N Q 1602 ^�0� 1575 ~ W ELn ` ►�` Cole Park Plaza _I a 1532 ell tih4i r13g� � .� I � 15800 Ln 4 �' IgGs 0 o 1530 ON M~ 1�� a 1721 o ti� `� cn 1606 Briar Chapel Development D 0 1634 r 1719 Dogwood Veterinary Hospital CHATHAM 1717 Legend 1618 E) NC Sources~ 3 ��T �� Fearrington Village — Stream 1❑ NN 1 , 1�6� 1779 — Road � 1803 4^ 9 NHDWaterbody ❑ <all other values> o 1 �. � 1805 I8 1718 q Oq FType 16 1802 ���157 0 1836 ❑ Estuary X11 ti ❑ Ice Mass ❑ LakePond ❑ Playa ❑ Reservoir 0 ❑ SwampMarsh 0 j J! CountyBoundary ❑ MunicipalBoundaries_polys 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn hy: CSC SOIL PL Us GFI Land Application Permit (WQ000838) Reviewed hy: CSC Chapel Hill, North Carolina 7 Date: April '17 Soil Plus Project # 200705.G10 DURHAM Colvard Farms 0 1103 Durham Durh IDurham SR,7 XI Legend Cary 8c, ❑Source Location — Road Cary Stream aCounty Boundary Northeast Creek F-1municipalBoundary 7"1 �_ - - M rgan C►reek Arm o New Hope River Arm of B. Everett Jo:0.5 0.25 0 0.5 Surface Water _ ^ � I I Milest y Morgan ree me u ing the Morgan Creek Arm of New Hope River Arm of B. Everett Jordan Lake Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595 Reviewed by: CSC Durham, North Carolina 8 Date: Sept 16 Soil Plus Project # 200705.G10 N �W E 1801 lJ r. Contentnea 190 1911 PITT 19og 1910 District WWTP LENOIR District WWTP Legend Neuse Rive_ ' ' Neuse River NC Sources-� — Road ❑ County Boundary CRAVEN Municipal Boundary ❑ River 0.5 0.25 0 0.5 Jas Miles 5 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WGrifton, North Carolina 9 Date: January Soil Plus Project # 200705.C10 N \ Wake Forest] W E / S Wake Forest o� v �Sl� SR\2045 I v Wake Forest SR -2043 Forest Deer Chase Me Forest ' s 5R-3564 T� Creek Raleigh SR -3509 Raleigh 4 SR -44601 Legend 11�\ Source Location SR -2930 Q SR -2982 — Road Stream County Boundary tititi� 54���� Municipal Boundary 54 0.5 0.25 0 0.5 Surface Water sR 2223 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Wake Forest, North Carolina 10 Date: Sept 16 Soil Plus Project # 200705.G10 N U1 N [� � N W E S � r J � M A 00 N 1909 x N Neuse River (Falls Lake below normal pool elevation) �I8 7t O N X21 Phase 1 & 2A Hasentree Golf N N � WAKE 98 V \Io 451 Legend \ 'l `--� / � NC Sources River (Falls/Lake below normal pool elevation) c N — Road County Boundary Raleigh I Municipal Boundary 0.5 0.25 0 0.5 River Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Wake Forest, North Carolina 11 Date: January '17 Soil Plus Project # 200705.C10 ^N / 3J SR -4281 s,�c Jf�cs/ SR -4633 J¢A J� J�g2 JR.1g4 SR -4230 VV E SR 1899 � 4 00 I s V1S� s� SR -4483 SR 4984 S , s� et •N � sR,s � �' SR -4976 n 5619 M Ak P SR r SR 66R� Cn sf A�n SR 4689 Sg s� SR -5686 oo X� T awt ornu • vis e Ln .Source Location s -4989 SR — RoadM) SR -49 90 / 69 �0 SR -1 \rI2 SR -3382 of SR -3305 SSD OCounty Boundary SSS g9�J GAG M F-1municipalBoundary —M 8 SR 3452 t� �scp3 v S CP n N N MSR -3286 1 y SR -3591 SR -3. W CP00 C SR -469$ 4�ofi Cn �ro 3379 w lL.�r, J �,�;• c SR -1839 � Raleigh s cc SR -1898 �2 I-540 5� SR 3354 SR -4276 RMP4201 SR -1830 41�9a SR -3225 S�p2° 0$ WildWo— d- reen � SR -3447 1540 Raleigh S4 . �M SR -3445 s� Raleigh N M 4209 SR 1 SR -3289 No Raleigh sR 1s29 S4 5^ s cJ ?R 3236 SR—_3221 00 ~� c cP� S � SR -3450 Sh, SR -3256 � . N R '•'>M 7 �(� SR -3241 Legend .Source Location — RoadM) �� y Raleigh — Stream �� of SR -3305 OCounty Boundary SR-3363SR-3303 F-1municipalBoundary Raleigh o'�� Surface Water lei g h p M 0.5 0.25 0 0.5 ��54 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina 12 Date: Sept 16 rS0i;lus Project # 200705.G10 N S �c 264 1613 1695 1615 1614 264 `0C ~� 2G57 ti 301 167 5 1607 �� Wilson, NG -Processing Facility E3 1608 Wilson Reclaimed Water -Distribution System 4692 Wilson WWTP WILSON 413 1696 1697 Legend 1616 . NC Sources Road 1617 16233 ❑ County Boundary ❑Municipal Boundary �titi Black Creek 0.5 0.25 0 0.5 ❑ River q— _,Jack Creek 0 Miles 7 22 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Wilson, North Carolina 13 Date: January '17 Soil Plus Project # 200705.C10 114 SR,4j 11 SR -21 Rock Bridge 's SR -2511 WAKE " s � 0 Neuse River 0 Y Kings/ Grant SR -4198 13p 5230 SR -524 N � SR - N iw SR -2507 SR -2508 01' �� Legend EDSource Location — Road Stream — Count Boundar %� JOHNSTON Clayton �_J Y Y L Municipal Boundary 1�rE Usk 0.5 0.25 0 0.5 Surface Water R Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Clayton, North Carolina 14 Date: Sept 16 Soil Plus Project # 200705.G10 N W E S M O V rC, Cn Cn C Cn SR_1g1 SR1 SNS 1 S� ��3� s� I�8 8 ja�tbe^xee�"' WE s�S03 ory SR -1214214 pool e le �7va attion) AKEEV Legend • �/ `� Source Location — Road SR -1895 Stream s� N QCounty Boundary ❑ Municipal Boundary �a c SR-1893� F Surface Water 0.5 0.25 0 0.5 ur am Miles u'rham Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Durham, North Carolina 15 Date: Sept 16 Soil Plus Project # 200705.G10 N Ne Hope River Arm of W E \S 1782 Legend NC Sources — Road County Boundary Municipal Boundary F River The Preserve at E) / The Legacy af J New Hope Rv New 8544 Lake Park � 85 L749 8,584 ja�2 40.5 0.25 0 0.5 Miles - Y V I .• 1 / ti Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Chapel Hill, North Carolina 16 Date: January '17 Soil Plus Project # 200705.C10 N �j � /W E0 SR -4657 SA4-62 S Raleigh Raleigh N N 0 , 2224 14 � N iA 'W-2982 SR -2223 S. SR 295 SR 4 08 SR-2296Od�.es � SR,3g M\ Creek S9,2958 Mallard Raleigh 1 LJ 43g0 SR/ SR -4313 \x Raleigh SR -2217 0N 0 N I N P4 Legend �V Source Location — Road Stream r i_J County Boundary Municipal Boundary Rr Surface Water 0.5 0.25 0 0.5 ti Miles ightdale nnigntaate Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Raleigh, North Carolina 17 Date: Sept 16 Soil Plus Project # 200705.G10 N SR -2641 VV E Archer Lodge o i S Sj� 323 SR=2693 c w 4 ti� SR'3215 SR 2669�'~� cG �� Clayton Clayton o o MND N � S zG s A9 Clayton 2670 �! N SR 5� x NC -42 w� Neuse-9-- Clayton JOHNSTON \2g2G Clayton `, 903 Legend 1NIZ Source Location R�0�Road laytonStream o r J County Boundary o o SR -1913 p� L Municipal Boundary Surface Water 0.5 0.25 0 0.5 � X003 Miles -0 US -70 R� Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Clayton, North Carolina 1 g Date: Sept 16 Soil Plus Project # 200705.G10 M ' r N /W E S 1363 v 1� Ss. cc C\1 `PS L Ln en 00 ss�s 1002 U` _J Pikcv ills 1322 1-542 1,534 Pikeville Wastewater Treatment WANE 1'4 Legend 2304 NC Sources — Road County Boundary ❑ Municipal Boundary River 0.5 0.25 0 0.5 1614 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC s o IL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Pikeville, North Carolina 19 Date: January '17 Soil Plus Project # 200705.C10 N W E S River R auth WWTP WASHINGTO rrs 13�� 1328 "s Legend 1325 NC Sources �J Road Plymouth w I County Boundary ❑ Municipal Boundary -' 0.5 0.25 0 0.5 River Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Plymouth, North Carolina 20 Date: January '17 Soil Plus Project # 200705.C10 V (N W E S O N SR -362'4 Neuse River S� 1 ennys M �i I River' Mill nal pool elevation) v v /110 o � U WAKE Raleigh Wake Forest NC -98 n—� i �3 M � O Wake1Forest Sl2 SR -5107 n S�, SR -2045 230 21 JS 2 � ti 5�-3691, Legend Source Location Wake Forest — Road Stream [_-_–],County Boundary L Municipal Boundary 0.5 0.25 0 0.5 Surface Water Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC4949swpw— Raleigh, North Carolina 21 Date: Sept 16 1 Soil Plus Project # 200705.G10 N / S 64 l/ / MARTIN 118 Robersonville WWTP )1438 � 1145 r A3 a A3 I SSI 1148 Legend NC Sources PITT — Road County Boundary Municipal Boundary River 0.5 0.25 0 0.5 zls� Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WRobersonville, North Carolina 22 Date: January Soil Plus Project # 200705.C10 N S 1247 1�Hill I 11 I ti Snow Hill WWTP 903 Legend v NC Sources — Road County Boundary a ~ do I Municipal Boundary ti~ I�3 s8 0.5 0.25 0 0.5 River IIo� Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC Snow Hill, North Carolina 23 Date: January'17 Soil Plus Project # 200705.C10 N W E ,G dl JG V- 1ti% WILSON Stantonsburg WWTP GREENE 1235 1230 1232 N� Legend ❑ NC Sources JA223 Road County Boundary F-1Municipal Boundary��❑ River 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 44owrs tantonsburg, North Carolina 24 Date: January'17 oil Plus Project # 200705.C10 —W E �J 9 iZ1� 1212 �1 J, 1� Orp Tarboro 1Z2 1351 12'9 !�19g! A�� 1344 10i 25S 'I'ar.River. P-rinc.vi e 111 oro WWTP E 1539 M \ 1020 45- JN tK Legend NC Sources — Road County Boundary ❑ Municipal Boundary River 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442spw- Tarboro, North Carolina 25 Date: January Soil Plus Project # 200705.C10 N W E S ROANOf RIVER BERTIE 1450 ~ Williamston WWTP tih 1581 Williamston b, 1 ti� 1 u 1598 1� c 37 O J 1123 M C ~ b ti ti Martin County WTP MARTIN 1124 1208 N 119a 0 ti moo° 454 0 7125 465-5zi Legend ❑ NC Sources — Road ❑ County Boundary ❑ Municipal Boundary jr ❑ River 1118 1501 0.5 0.25 0 � 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS Granville Farms, Inc. Class B (WQ0035595) Reviewed by: CSC 442WFso illiamston, North Carolina 26 Date: January '177 il Plus Project # 200705.C10 i N S 1a1a00 W E 19 8 1 co SR -1715 J S4/ FRANKLIN Sg SR_2447 �9I y SR -1724 SR,23�1 WAKE SR -2313 W O Legend Source Location 125 Sg — Road Stream N �e SR -2309 ce, J County Boundary 9�k L Municipal Boundary r 0.5 0.25 0 0.5 Surface Water Miles SR -2315 Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Zebulon, North Carolina 27 Date: Sept 16 Soil Plus Project # 200705.G10 \ N. W E S N � N G � ^� N 0 SR -4178 ' tihh� � N SR -52041 ,ela Gtieek '" n -265g Beadin� M WAKE W N N SR -1771 N SR -3224 Willowbrook w N� _10 SR SR-1779 ti JOHI S NN �0, s U SR -1615 SR -1639 MSR -1677 Clayton � SR -1632 Legend Cn w P Source Location N o� — Road s�'ssJ Stream SR -1550 r �_J County Boundary s L Municipal Boundary r hN Surface Water 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Garner, North Carolina 28 Date: Sept 16 Soil Plus Project # 200705.G10 1 N ( W E S HALIFAX _ SR -1 SR�1 Perdue WWTP S¢i Lewiston -'Woodville WWTP ,2 0 11 �J ti~ o BERNIE SR 1 �Wlston W00 'He SR1119- l� z� 1108 Legend 0 Sources Stream Road 0 County Boundary 0.95 0.475 0 0.95 N Municipal Boundary Miles z Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SDIL PLUS WQ0035595 O&M PLAN Reviewed by: Lewiston -Woodville, North Carolina 29 Date: Aug'17 Soil Plus Project # 200705.C10 N W E S WAKE Knig le e Cottonwood/Baywood 0 Ashley Hills WWTP Wendell Legend I e Sources — Road 0 County Boundary 0.5 0.25 0 0.5 Municipal Boundary Kings Gra Subdivision W Miles Scale: 1 inch = 1 milesSOURCE LOCATION MAP Drawn by: DM ;OIL PU GFI Land Application Permit (WQ0035595) Figure Reviewed by: Knightdale, North Carolina 30 Date: June'18 Soil Plus Project # 200705.D10 N 2�qS S� _W E SR -2147 S S aC � v '''o U 0 w w SR -2146 N z 4 / v NI Kenly 52143 Mill Creek S4 Kenly Kenly S� N SR -2343 1b Sg� r �R�2385 Legend �„�'�`� 7Source Location SR -2341 a — Road Qofi Stream ���� SR -2414 County Boundary S4 s� L Municipal Boundary Surface Water 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ000838) Reviewed by: CSC Kenly, North Carolina 31 Date: Sept 16 Soil Plus Project # 200705.G10 p W EV $ Gv XAGE f 198 CHA tfall WWTP n I m 1753 r, c 1795 F°lk Gr ner ce' e 1� C Creek Iia. 1740 41 N 1801 Legend 1j49 1 C, L . Source m� 761 m 2 Water �� m 1 0 — Stream 1,4 L 1WAKE Road Y' o p� Q County Boundary � D 1 0.5 0 1 Municipal Boundary Miles n 174 Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SOIL PL. Us GFI Land Application Permit (WQ0035595) Reviewed by: Chapel Hill, North Carolina 32 Date: Nov'17 Soil Plus Project # 200705.D10 N N DURHAM CD o n 1103 h N `°° O N N 1 C o ' a Meado s WW a k Nature Trail obile Home Par WWTP 1 6 l 1832 1 eiCc � Y n U tfall WWTP n I m 1753 r, c 1795 F°lk Gr ner ce' e 1� C Creek Iia. 1740 41 N 1801 Legend 1j49 1 C, L . Source m� 761 m 2 Water �� m 1 0 — Stream 1,4 L 1WAKE Road Y' o p� Q County Boundary � D 1 0.5 0 1 Municipal Boundary Miles n 174 Scale: 1 inch = 1 miles SOURCE LOCATION MAP Figure Drawn by: CSC SOIL PL. Us GFI Land Application Permit (WQ0035595) Reviewed by: Chapel Hill, North Carolina 32 Date: Nov'17 Soil Plus Project # 200705.D10 N VV \ter RMP -172 T H Rocky Mount Maple CreeJ M sR Horn B 1 S� SR -1599 v� p1 SR;1542 tiS3 O� o, G„ LO -915 y US -64P_1 WTP � o O U O \�f RUP_16j O G� L C G � Lc end LOC -914 cq C) Source Location — Road M Swami' Stream 1,;ttle C°key [_JCounty Boundary L Municipal Boundary SR -1'z7 0.5 0.25 0 0.5 Surface Water Miles u Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PLUS GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 33 Date: Sept 16 Soil Plus Project # 200705.G10 N W E S SR -1404 00 Rocky Mount Legend Source Location — Road Stream _IR J County Boundary L Municipal Boundary Surface Water N 0 Tar River U i �ek WWTP SR -1414 0.5 0.25 0 0.5 Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 34 Date: Sept 16 Soil Plus Project # 200705.G10 Z1707��t 460 CIOard SR -1710 rad � SR -1709 c!l a Tar River WTP S u SR -1749f NASH 1 Sg ranch 233` Rocky wK sR,l N� 8G3 1 �0 SR -1733 I V � Legend G - .Source Location — Road 7� Stream QCounty Boundary ❑ Municipal Boundary s�I��o 0.5 0.25 0 0.5 Surface Water Miles Scale: 1 inch = 0.5 miles LOCATION MAP Figure Drawn by: CSC SOIL PL Us GFI Land Application Permit (WQ0035595) Reviewed by: CSC Rocky Mount, North Carolina 35 Date: Sept 16 Soil Plus Project # 200705.G10 APPENDIX 2 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RSCA Sunset WTP Analytical Field Loading Calculations 4 c. oo O O oo Op O � p M M 00 m M .--i C. O H Lir Q p � O O O O p U s. ZN O N M E U U U U z z z z a a� w FL Z H � � � o x U U U P64 U U U o z z z v� U cu x c 3 State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Sunset WTP 2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private. Facility permit issued by: ❑ Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Jim Connolly, Superintendent Complete mailing address: PO Box 1180 City: Rocky Mount State: NC Zip: 27802- Telephone number: (252) 972-1293 E-mail address: Jim.Connolly�u rockymountnc.gov 4. Facility physical address: 1660 Sunset Avenue City: Rocky Mount State: NC Zip: 27804- Coordinates: Latitude: 35° 57'05" Longitude: 77° 49'05" Datum: NAD 83 Level of accuracy: Sub-Meter Method of measurement: GIS 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ® treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes ® No 7. Facility permitted/design flow: 18.0 MGD and facility average daily flow: a MGD 8. Average amount of residuals being generated at this facility 419 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Conventional Treatment (Caustic, Ferric, Carbon, Polymer, & Chlorine) Type and volume of residuals storage (i.e., outside of residuals treatment units): (2) 162,900 Gallon Above Ground Open Tanks and (2) 20,000 Gallon Vertical Silos: 365,800 Total Gallons II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ❑ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological 2 Non -Biological FORM: RSC 11-13 Page 1 of5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: M yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Meritech, Inc. and Date of analysis: 6/18/18 Passed corrosivity test: ® yes no. pH: 61 s.u. (2 < pH < 12.5) Passed ignitability test: ® yes no. Flashpoint: >140 OF (> 140°F) Passed reactivity test: ®yes Inno. HCN: m<T7 mg/kg (<250) & HzS: 10.0 mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 < 0.100 Hexachlorobenzene 0.13 < 0.100 Barium 100.0 0.093 Hexachloro-1,3-Butadiene 0.5 < 0.100 Benzene 0.5 < 0.0100 Hexachloroethane 3.0 < 0.100 Cadmium 1.0 0.049 Lead 5.0 < 0.100 Carbon Tetrachloride 0.5 < 0.0100 Lindane 0.4 < 0.040 Chlordane 0.03 < 0.003 Mercury 0.2 < 0.02 Chlorobenzene 100.0 < 0.0100 Methoxychlor 10.0 < 1.00 Chloroform 6.0 < 0.0100 Methyl Ethyl Ketone 200.0 < 0.100 Chromium 5.0 < 0.050 Nitrobenzene 2.0 < 0.100 m -Cresol 200.0 < 0.200 Pentachlorophenol 100.0 < 0.500 o -Cresol 200.0 < 0.100 Pyridine 5.0 < 0.100 p -Cresol 200.0 < 0.200 Selenium 1.0 < 0.100 Cresol 200.0 < 0.300 Silver 5.0 < 0.050 2,4-D 10.0 < 1.00 Tetrachloroethylene 0.7 < 0.0100 1,4 -Dichlorobenzene 7.5 < 0.100 Toxaphene 0.5 < 0.05 1,2-Dichloroethane 0.5 < 0.0100 Trichloroethylene 0.5 < 0.0100 1, 1 -Dichloroethylene 0.7 < 0.0100 214,5 -Trichlorophenol 400.0 < 0.100 2,4-Dinitrotoluene 0.13 < 0.100 2,4,6 -Trichlorophenol 2.0 < 0.100 Endrin 0.02 < 0.002 2,4,5 -TP (Silvex) 1.0 < 0.100 Heptachlor and its Hydroxide 0.008 < 0.005 Vinyl Chloride 0.2 < 0.0200 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Meritech, Inc. and Date of analysis: 12/4/18 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 20.6 Cadmium 85 39 2.10 Copper 4,300 1,500 33.70 Lead 840 300 22.10 Mercury 57 17 0.160 Molybdenum 75 n/a 10.300 Nickel 420 420 21.70 Selenium 100 100 20.6 Zinc 7,500 2,800 20.6 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/w 0 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 3.00 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech, Inc. / City of Rocky Mount and Date of analysis: 12/4/18 Parameter Result (mg1kg) Aluminum 11,300 Ammonia -Nitrogen 343 Calcium 3,090 Magnesium 514 Nitrate -Nitrite Nitrogen 65.90 pH (Standard Unit) 6.31 Phosphorus 1,587 Potassium 10,300 Sodium 10,300 Total Kjeldahl Nitrogen 7,433 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 7.81 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (Is) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg1kg) Surface 237 237 Injection/Incorporation 409 409 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None Known 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, ❑ air drying, ❑ anaerobic digestion, composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1 106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40 -Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30 -Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [ 15A NCAC 02T. 1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14 -Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [ 15A NCAC 02T. 1 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. Facility Sunset WTP FIELD LOADING ESTIMATES Sampling Date 12/4/2018 % Solids 3 Mineralization Rate 0 Gallons per DT 7,993.61 pH 6.31 Sodium Absorpotion 7.81 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 7,433 lbs./1,000 gal 1.86 Ammonia Nitrogen (mg/Kg) 343.00 lbs./1,000 gal 0.09 Nitrate -Nitrite (mg/Kg) 65.90 lbs./1,000 gal 0.02 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 237 lbs./1,000 gal 0.06 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 409 lbs./1,000 gal 0.10 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 2.58 Phosphorus lbs./1,000 gal 0.40 Calcium lbs./1,000 gal 0.77 Magnesium lbs./1,000 gal 0.13 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 20.60 Arsenic lbs./1,000 gal 0.01 Cadmium (mg/Kg) 2.10 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 33.70 Copper lbs./1,000 gal 0.01 Lead (mg/Kg) 22.10 Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 0.16 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 21.70 Nickel lbs./1,000 gal 0.01 Selenium (mg/Kg) 20.60 Selenium lbs./1,000 gal 0.01 Zinc (mg/Kg) 20.60 Zinc lbs./1,000 gal 0.01 RESIDUAL NITROGEN CALCULATION 7,196 Total 237 0.47 Total 409 0.82 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Surface Application Injection/ Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 7,433 237 0.47 7,196 7,433 409 0.82 7,024 7,196 0 0.00 7,196 7,024 0 0.00 7,024 7,196 0 0.00 7,196 7,024 0 0.00 7,024 7,196 0 0.00 7,196 7,024 0 0.00 7,024 7,196 0 0.00 7,196 7,024 0 0.00 7,024 Total 237 0.47 Total 409 0.82 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) O O M N O O a r 71 U\ t, O O O eC Q O 0 O O• ,cl o O M O O O O O O C O O O� cMr1 M Q1 rn O CG O rl M °OcimNo�NNC,M�oo�nr- n 0 o C p� t/'� O M M S O M �O M Q1 V1 N DD v1 O Q O N C O tO N M n1 N N a1 o0 0 o° in V'7 N N O N in N v7 N M in OA _ •-• O C 'n O N r- ON N 'n C14 M '-' M M oCo,n .-, .--i C 0 o � O d• r-- � V d- Q1 in N d• � DD O � o0 r�!? O 00 op 00 O O 00 •--i O M N '- 00 U O _ Vl O [� V) O O Cl O Q Q Q Q Q Q Q Q Q Q Q Q o�q � � � tr- co � � v� t� � • C14 ti ci Z zN a H o o n ap U Q° n U con M. Q U\ t, O O O eC Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 1jr—ECEIVE B:Y� � Y Q �-. Page 3 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 Meritech Work Order # 061918123 Sample: SAPSL 0618 Grab 6/18/18 1311 - TCLP Metals Parameters Result Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Barium 0.093 mg/L 6/26/18 0.050 100.0 EPA 200.7 Cadmium 0.049 mg/L 6/26/18 0.020 1.0 EPA 200.7 Chromium <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 6/26/18 0.02 0.2 EPA 245.1 Selenium <0.100 mg/L 6/26/18 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 TCLP Organics Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 6/27/18 - 8260 Semi Vol. 8270 Attached 7/5/18 - 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method Cyanide, total <0.5 mg/kg 6/20/18 0.5 mg/kg EPA 335.4 lgnitability (flashpoint) >140 °F 6/28/18 - EPA 1030 pH 6.1 S.U. 7/2/18 1.0-14.0 S.U. SM 4500 HB Sulfide, total <10.0 mg/kg 6/21/18 10.0 mg/kg SM 4500 SD 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Meritech Work Order # 061918122 Sample: SAPSL 0618 Grab Page 4 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 1311 - TCLP Pesticides & Herbicides Pesticide - SW -846 8081A Parameter Results Analysis Date Endrin <0.002 mg/L 7/3/18 Chlordane <0.003 mg/L 7/3/18 Toxaphene <0.05 mg/L 7/3/18 Methoxychlor <1.00 mg/L 7/3/18 Heptachlor <0.0005 mg/L 7/3/18 Lindane <0.040 mg/L 7/3/18 Herbicides - SW -846 8151A 6/18/18 Det. Limit Reg. Limit Dilution Factor 0.002 0.02 1 0.003 0.03 1 0.05 0.5 1 1.00 10.0 1 0.0005 0.008 1 0.040 0.4 1 Parameter Results Analysis Date Det. Limit Reg. Limit Dilution Factor 2,4-D <1.00 mg/L 7/3/18 1.00 10.0 1 2,4,5 -TP (Silvex) <0.100 mg/L 7/3/18 0.100 1.0 1 I hereby certify that I have reviewed and approve these data. �)Z66 Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. ►� ,,d, Environmental Laboratories A Division of Water Technology and Controls, Inc. Client: City of Rocky Mount Project: TCLP Client Sample ID: SAPSL0618 Sample Collection: 06/18/18 Meritech Sample ID: 061918123 1311 - TCLP Oraanics Volatiles: SW -846 8260 Analysis: 06/27/18 Date Extracted: 06/20/18 Analyst: VWV Parameter Result Units Det. Limit Ree. Limit Dilution Factor Benzene < 0.0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride < 0.0100 mg/L 0.0100 0.50 10 Chlorobenzene < 0.0100 mg/L 0.0100 100 10 Chloroform < 0.0100 mg/L 0.0100 6.0 10 1,2-Dichloroethane < 0.0100 mg/L 0.0100 0.50 10 1,1-Dichloroethene <0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone < 0.100 mg/L 0.100 200 10 Tetrachloroethylene < 0.0100 mg/L 0.0100 0.70 10 Trichloroethene < 0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride < 0.0200 mg/L 0.020 0.20 10 Semi -Volatiles: SW -846 8270 Extraction: 06/25/18 Analysis: 07/05/18 Analyst: PM Parameter Result Units Det. Limit Rer. Limit Dilution Factor 1,4 -Dichlorobenzene <0.100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o -cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5 -Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6 -Trichlorophenol <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. 6' �. (/ Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 3424748 Ph * (336) 342-1522 Fax f0 u o C a ^ 0 O !Z U rr a 0 * v fQ E O ) N L N H .Q C LQ O U z C O Q tD a c I i 3 E P E P E p •° Y S z a Ln o o No* LU o Join t � O L O •� _ E Z a LL w a a. 07 v N X �I u Q L LL n O41 V1 1 Q ✓ O Q 7 � Jo r o AQ 4-J va o CL �2J c c U o m W -� a � 11Q" > s Y E f _TJ ) Q rl O V _ T 0 E Ln �' Q N K W d K bZ ° o N_ C: .- �F a� v ¢ i7 4-`, Q oo V V r cz L a z'' \19 s v �(1 E i= � v ce cu v u } w O E W N 0 1 1 E N O UJ my Y Q m m `^ +' o V o C) m O m m a ro v c i O 0 = N �_ E a o --k U O ( ) vim/ J v c "'r O X +' L OJ u Vj •Q ~ 4 ' Ln y�1 o e" V. O on 0/ UJ C m LL -c M L L Z W @i O m N - ° O IN v - +' m {. W N 25 cr U ro E v a1 oLU o i Z ° » �. O It ai t aj c c � 3 (u C: @ C C 6 C V C CT C U c O � ^ J Ucc o01c ' • O V) V J O-0 CU X i •> L 1 e p1 Q °L 0 APPENDIX 3 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RSCA Tar River Regional WWTP Analytical Field Loading Calculations 4 c. oo O O oo Op O � p M M 00 m M .--i C. O H Lir Q p � O O O O p U s. ZN O N M E U U U U z z z z a a� w FL Z H � � � o x U U U P64 U U U o z z z v� U cu x c 3 State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Tar River Regional WWTP 2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private. Facility permit issued by: ❑ Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Darrell Highsmith, Chief Operator Complete mailing address: PO Box 1180 City: Rocky Mount State: NC Zip: 27802 - Telephone number: (252) 972-1406 E-mail address: darrell.highsmithgrockymountnc.gov 4. Facility physical address: 3031 Treatment Plant Road City: Rocky Mount State: NC Zip: 27801 - Coordinates: Latitude: 35° 59'24.14" Longitude: 77° 43'53.36" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: GIS 5. Purpose of the facility: ® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes ❑ No 7. Facility permitted/design flow: 21.0 MGD and facility average daily flow: 15.0 MGD 8. Average amount of residuals being generated at this facility 1,153 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 4.3 MG Extended Aeration Type and volume of residuals storage (i.e., outside of residuals treatment units): 6.0 MG Digester II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological N Non -Biological FORM: RSC 11-13 Page lof5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: M yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Meritech, Inc. and Date of analysis: 6/14/18 Passed corrosivity test: ® yes no. pH: 7.2 s.u. (2 < pH < 12.5) Passed ignitability test: ® yes no. Flashpoint: >140 OF (> 140°F) Passed reactivity test: ®yes Inno. HCN: m<T7 mg/kg (<250) & HzS: 10.0 mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 < 0.100 Hexachlorobenzene 0.13 < 0.100 Barium 100.0 0.123 Hexachloro-1,3-Butadiene 0.5 < 0.100 Benzene 0.5 < 0.0100 Hexachloroethane 3.0 < 0.100 Cadmium 1.0 < 0.020 Lead 5.0 < 0.100 Carbon Tetrachloride 0.5 < 0.0100 Lindane 0.4 < 0.040 Chlordane 0.03 < 0.003 Mercury 0.2 < 0.02 Chlorobenzene 100.0 < 0.0100 Methoxychlor 10.0 < 1.0 Chloroform 6.0 < 0.0100 Methyl Ethyl Ketone 200.0 < 0.100 Chromium 5.0 < 0.050 Nitrobenzene 2.0 < 0.100 m -Cresol 200.0 < 0.200 Pentachlorophenol 100.0 < 0.500 o -Cresol 200.0 < 0.100 Pyridine 5.0 < 0.100 p -Cresol 200.0 < 0.200 Selenium 1.0 < 0.100 Cresol 200.0 < 0.300 Silver 5.0 < 0.050 2,4-D 10.0 < 1.0 Tetrachloroethylene 0.7 < 0.0100 1,4 -Dichlorobenzene 7.5 < 0.100 Toxaphene 0.5 < 0.05 1,2-Dichloroethane 0.5 < 0.0100 Trichloroethylene 0.5 < 0.0100 1, 1 -Dichloroethylene 0.7 < 0.0100 2,4,5 -Trichlorophenol 400.0 < 0.100 2,4-Dinitrotoluene 0.13 < 0.100 2,4,6 -Trichlorophenol 2.0 < 0.100 Endrin 0.02 < 0.002 2,4,5 -TP (Silvex) 1.0 < 0.100 Heptachlor and its Hydroxide 0.008 < 0.005 Vinyl Chloride 0.2 < 0.0200 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Meritech, Inc. and Date of analysis: 11/29/18 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 55.90 Cadmium 85 39 5.60 Copper 4,300 1,500 307 Lead 840 300 29.2 Mercury 57 17 1.100 Molybdenum 75 n/a 28.0 Nickel 420 420 28.0 Selenium 100 100 55.90 Zinc 7,500 2,800 290 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/w 0 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 1.20 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech, Inc. / City of Rocky Mount and Date of analysis: 11/29/18 Parameter Result (mg1kg) Aluminum 7,330 Ammonia -Nitrogen 87,333 Calcium 6,760 Magnesium 1,870 Nitrate -Nitrite Nitrogen 4 pH (Standard Unit) 7.3 Phosphorus 57,167 Potassium 28,000 Sodium 28,000 Total Kjeldahl Nitrogen 118,250 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 8.49 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: This rate is a (check one): JW default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (Is) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg1kg) Surface 52,946 69,757 Injection/Incorporation 96,612 102,182 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None Known 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ® Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ® aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1 106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ® Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40 -Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30 -Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [ 15A NCAC 02T. 1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14 -Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [ 15A NCAC 02T. 1 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. Facility Tar River Regional WWTP Sampling Date 11/29/2018 % Solids 1.2 Mineralization Rate 0.3 Gallons per DT 19,984.01 pH 7.3 FIELD LOADING ESTIMATES Sodium Absorpotion 8.49 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 118,250 lbs./1,000 gal 11.83 Ammonia Nitrogen (mg/Kg) 87,333.00 lbs./1,000 gal 8.74 Nitrate -Nitrite (mg/Kg) 4.00 lbs./1,000 gal 0.00 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 52,946 lbs./1,000 gal 5.30 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 96,612 lbs./1,000 gal 9.67 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 2.80 Phosphorus lbs./1,000 gal 5.72 Calcium lbs./1,000 gal 0.68 Magnesium lbs./1,000 gal 0.19 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 55.90 Arsenic lbs./1,000 gal 0.01 Cadmium (mg/Kg) 5.60 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 307.00 Copper lbs./1,000 gal 0.03 Lead (mg/Kg) 29.20 Lead lbs./1,000 gal 0.00 Mercury (mg/Kg) 1.10 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 28.00 Nickel lbs./1,000 gal 0.00 Selenium (mg/Kg) 55.90 Selenium lbs./1,000 gal 0.01 Zinc (mg/Kg) 290.00 Zinc lbs./1,000 gal 0.03 RESIDUAL NITROGEN CALCULATION 65,304 Total 69,757 139.51 Total 102,182 204.36 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Surface Application Injection/ Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 118,250 52,946 105.89 65,304 118,250 96,612 193.22 21,638 65,304 9,796 19.59 55,509 21,638 3,246 6.49 18,392 55,509 4,163 8.33 51,346 18,392 1,379 2.76 17,013 51,346 1,925 3.85 49,420 17,013 638 1.28 16,375 49,420 927 1.85 48,493 16,375 307 0.61 16,068 Total 69,757 139.51 Total 102,182 204.36 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) h M 0 O O a/' 01 M O o O M 01 h0 225 °` O N M 'cl' O O Oh Z O M V N (�l \D h h m mvhi °\ 00 00 m N N a0 M 00 N o V1 O \OMmOh� CI O O O �n O O N M 'o h R M �--' O.-�� h �n .N -i ct �bOO�� M in cq 'r VOiN 00 o VOj .-' 'r M .�-i VO°'� .�-i 00 00 DD o m N O v1 O 00 O O M \O N h 'o 00 n oo m N 0 n N ao in M d N h M N .N -i '. M , M ..; O Net -� 00 d0-' 0 h co cn O _ 7 c:- 0�1 h M O 00�+ C Ohl O M N lO h.-�cV h�YDOI`, .-+�n In BOOM in �t h M to ,-�O�NO o M m n Cl �' .-+ OMO.--i00MOlO h V� C V' 7 �° BOOM Mit Oho OOM N �° I�N�Op�, 'cf' (V O �--� N m .--� .M-+ V 0�0 N _ 'o o In 0G h^'���� _ON vihr�� h�hONoa �M C) N - G N l° M N m M Oho M "" N M .--r O�0 Oo O o O N h M m M W h 0 h h 00 N h O t- pp M O S ~ N Q\ � h -Ood-O d'M-v1 Oh ma,Op��,--i 7 N O N h N N DO m o Mme.-- h<rl 0N0 �m hlN-000�a, 5 hMN.h� h N �o h O1 O h d' O p N d" N m M W M N 1O 017 7 01 M t0+1 M ^ O\ M .-. m N N\ O O Oh � p h�pO_pQO N om0 g go, t- -� � O\ O1 r hO\00 00 000 C. 0 N Op 0V Cl p� �o MM O� M N h N moi' I . h O N•r °O7 C> It cV �cM+l n h7 .--a �N N^'m 00 N c�+l O � ZZ �� pp Z a '^In ZZZZz '� \/ N w N ° k o +3 :o V] V On w) o rn �" a bA Q a Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 Meritech Work Order # 061918120 Sample: BF 0614 Grab 6/14/18 Parameter Results Analysis Date Reporting Limit Method % Total Solids 1,24 % 6/19/18 0-100 % SM 2540B Aluminum, total 10,000 mg/kg (27 6/22/18 2.50 mg/kg EPA 200.7 Arsenic, total <4.03 mg/kg46,6 � 6/22/18 4.03 mg/kg EPA 200.7 Cadmium, total 1.86 mg/kg 0.6�3b 6/22/18 0.376 mg/kg EPA 200.7 Calcium, total 14600 mg/kgN .0 6/22/18 10.0 mg/kg EPA 200.7 Copper, total 783 mg/kg0 6/22/18 1.00 mg/kg EPA 200.7 Lead, total 51.2 mg/kg Q 63 6/22/18 2.56 mg/kg EPA 200.7 Magnesium, total 4,620 mg/kg 6/22/18 10.0 mg/kg EPA 200.7 Mercury, total 0.081 mg/kg ��p0'i f 6/26/18 0.010 mg/kg EPA 245.1 Molybdenum, total 13 mg/kg 0.1612 6/22/18 0.100 mg/kg EPA 200.7 Nickel, total 43.7 mg/kg 6/22/18 0.5 mg/kg EPA 200.7 Potassium, total d'S`���� 16,300 mg/kg D 6/22/18 20.0 mg/kg EPA 200.7 Selenium, total <4.03 mg/kgs 2 `� 6/22/18 4.03 mg/kg EPA 200.7 Silver, total <2.02 mg/kg(� 0L6/22/18 2.02 mg/kg EPA 200.7 Sodium, total 5,475 mg/kg 6?, 6/22/18 20.0 mg/kg EPA 200.7 Zinc, total 660 mg/kg g 6/22/18 0.500 mg/kg EPA 200.7 Meritech Work Order # 061918121 Sample: BF 0614 Grab 6/14/18 1311 - TCLP Metals Parameters Result Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Barium 0.123 mg/L 6/26/18 0.050 100.0 EPA 200.7 Cadmium <0.020 mg/L 6/26/18 0.020 1.0 EPA 200.7 Chromium <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 6/26/18 0.02 0.2 EPA 245.1 Selenium <0.100 mg/L 6/26/18 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Aw iL Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 Meritech Work Order # 061918121 Sample: BF 0619 Grab Results 6/14/18 Endrin <0.002 mg/L TCLP Organics Chlordane <0.003 mg/L Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 6/27/18 - 8260 Semi Vol. 8270 Attached 7/5/18 - 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method Cyanide, total <0.5 mg/kg 6/20/18 0.5 mg/kg EPA 335.4 Ignitability (flashpoint) >140 "F 6/28/18 - EPA 1030 pH 7.2 S.U. 7/2/18 1.0-14.0 S.U. SM 4500 HB Sulfide, total <10.0 mg/kg 6/21/18 10.0 mg/kg SM 4500 SD 1311 - TCLP Pesticides & Herbicides Pesticide - SW -846 8081A Parameter Results Analysis Date Endrin <0.002 mg/L 7/3/18 Chlordane <0.003 mg/L 7/3/18 Toxaphene <0.05 mg/L 7/3/18 Methoxychlor <1.0 mg/L 7/3/18 Heptachlor <0.0005 mg/L 7/3/18 Lindane <0.040 mg/L 7/3/18 Herbicides - SW -846 8151A Parameter Results 2,4-D 2,4,5 -TP (Silvex) <1.0 mg/L <0.100 mg/L Det. Limit Reg. Limit Dilution Factor 0.002 0.02 1 0.003 0.03 1 0.05 0.5 1 1.0 10.0 1 0.0005 0.008 1 0.040 0.4 1 Analysis Date Det. Limit Reg. Limit Dilution Factor 7/3/18 1.0 7/3/18 0.100 I hereby certify that I have reviewed and approve these data. 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 10.0 1 1.0 1 Client: Project: Client Sample ID: Sample Collection: Meritech Sample ID: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. City of Rocky Mount TCLP BF0614 06/14/18 061918121 1311 - TCLP Organics Volatiles: SW -846 8260 Result Units Det. Limit Reg. Limit Dilution Factor Analysis: 06/27/18 <0.100 Date Extracted: 0.100 06/20/18 10 Analyst: VWV <0.100 mg/L 0.100 0.13 10 Parameter Result Units Det. Limit Ree. Limit Dilution Factor Hexachloroethane Benzene < 0.0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride < 0.0100 mg/L 0.0100 0.50 10 Chlorobenzene < 0.0100 mg/L 0.0100 100 10 Chloroform < 0.0100 mg/L 0.0100 6.0 10 1,2-Dichloroethane < 0.0100 mg/L 0.0100 0.50 10 1, 1 -Dichloroethene <0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone < 0.100 mg/L 0.100 200 10 Tetrachloroethylene < 0.0100 mg/L 0.0100 0.70 10 Trichloroethene < 0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride < 0.0200 mg/L 0.020 0.20 10 Semi -Volatiles: SW -846 8270 Extraction: 06/25/18 Analysis: 07/05/18 Analyst: PM Parameter Result Units Det. Limit Reg. Limit Dilution Factor 1,4 -Dichlorobenzene <0.100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o -cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5 -Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6 -Trichlorophenol <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. "/ Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax s M1' M1• O o- e O Q O * Q N a QI Ea I- m m NH L N J J J v >- C Orl. t0 CJ z N O a -3 7 J 7 N J O v _ E O y y cY O F U H r F- 0 3 °e v Ln M -' m E * -OLJv 5- Ln LU a �� E z a r LL E w O d O a d 4-1 o Ln U- 4.1 � 4.1 � LL O 4. 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CA LO � � I -T 't v INT v IT v v� O O O O O O O O O O CO CO CO 0 CO 0 co CO CO CD N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N u LMc) LMn 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 01 0 0 0 0 0 0 LO 0 o o 0 0 0 O O O O O O 0 0 M4L69990000000000 CO 0 (D CO CD O O O 0 r N M� LO 0 r- 00 6 O r N M It Ln CO t` CO 6 O r N M Ln 00 00 a0 00 M M M M M M 00 00 O c0 ONr O r O) 00 00 00 W W O M M 00 N 00 �h 00 r r f` r r r r r r r r r O r r O �- N M 4O CO ti 00 CA O M r'0 It� Op 00 0 0 1� N c6 Ln co P, O6 O r O C7 M M M M M M m M m v m N r 0 0 0 00 00 00 00 O0 00 00 00 00 00 00 r 00 r r r r r r r r r r r r r r r r 1 � CC 00 00 00 00 00 O CO 00 00 r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 G 0 0 0 m c 00 O O O O O O O N N N N N N N N N N N N N N N N N N N N N \\\\\\\\\ 00 (� O r N M C1 O CO CA O r N M� 0 CO t` O O r r r r � r r r r r r N N N N N N N N N N N N CO \ '\^ ,\^ ,\^ ,\^ ,\^ ,\^ '\^ , 5 \ '\^ ZZ5 ' 5 \ \ \ \ \ \ \ \ � ib \ � 1 \ \ \ \ I it Cn � ti ti > i QT NN Cm Cm Cm _M N O I ►� ti O CD N CD 00 CD O M 00 O O O r ti O O O LO Co O Nql� CO 00 O O M Nt CO r` 00 g O N O r• ti 00 O N M CO 00 00 00 O 00 0 0 0 0 0 0 O O O O O O O r N N N N N N N N N N N N N N M m M M M M M N N O It O N N N� M O N r` r• r` O co O� O CD Co Cn O r Cl) O CD CO CO CO Cn O CO It O O O (O 00 00 0 0 0 0 0 e- r r r r r r r r N N N N N N N O r• Cr) M M M M m M M Cl M M M M M CM C'M M M M M Cl) M N h LO Cq I i I CO) N r ! II N O O O ICO 00 00 O CO O M O O O O r` O O N COO O N M q1t Ln (0 CO CO co r• CD r• t` CO 00 00 q q N r N M04 0 0 0 0 0 O O O O C O O G C O O O r r r r M M M co M co co M M M M M M M co co M co M M M M 06 N NL� � m 00 N r M ONO COD co M coC I CN7 I CN7 M M M N N N LO co LO N O r r co CA N OI N O Nr Nt r` N r LO O O N O O O N. O O O O 0) O 0 r O 4 00 4 6 N � O O O CA r` 00 I- 00 co r` O ` co N M M M' O N I I O O O O O O O O O O O O O O O O O O O O O 0 0 0 0 0 0 0 0 0 O O N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N f` N O O N M et LO CD ti 00 O O N M It O CO N- 00 O O r N M 0 In CO t` 00 M CA ti CD 00 00 O M O M 00 O O O O O O O O O O O O O O O O O O i �t ct I et �t �t et d at d rt et O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O O C r N M 4 O 0 00 O C r N M 4 O CO r-2 6 O O r CV m 4 O CD r-. Co. CA LO � � I -T 't v INT v IT v v� O O O O O O O O O O CO CO CO 0 CO 0 co CO CO CD N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N u LMc) LMn 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 01 0 0 0 0 0 0 LO 0 o o 0 0 0 O O O O O O 0 0 M4L69990000000000 CO 0 (D CO CD O O O 0 r N M� LO 0 r- 00 6 O r N M It Ln CO t` CO 6 O r N M Ln 00 00 a0 00 M M M M M M 00 00 O c0 ONr O r O) 00 00 00 W W O M M 00 N 00 �h 00 r r f` r r r r r r r r r O r r O �- N M 4O CO ti 00 CA O M r'0 It� Op 00 0 0 1� N c6 Ln co P, O6 O r O C7 M M M M M M m M m v m N r 0 0 0 00 00 00 00 O0 00 00 00 00 00 00 r 00 r r r r r r r r r r r r r r r r 1 � CC 00 00 00 00 00 O CO 00 00 r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 G 0 0 0 m c 00 O O O O O O O N N N N N N N N N N N N N N N N N N N N N \\\\\\\\\ 00 (� O r N M C1 O CO CA O r N M� 0 CO t` O O r r r r � r r r r r r N N N N N N N N N N N N CO \ '\^ ,\^ ,\^ ,\^ ,\^ ,\^ '\^ , 5 \ '\^ ZZ5 ' 5 \ \ \ \ \ \ \ \ � ib \ � 1 \ \ \ \ 1 V d L N A �i O le A OA O M A co t/J C E L Cr li N M M 0 LO C O Nd li II I I III N Co lqr M N O O O O O CO CO 1- O r M N M ti W r'qr r m.;r to O r` r` co O N't M N M"T CO CO 0 0 0 O N N M N N N N N N N M m M M M M M of M M M v 14 v v v M M M M M M M M M M M M M M M M M M M M M M M i j I I r 00 �q't"t CD ti N N M M M ti O O O M M M M N N r CO O O O O N t M M !M M M M m M N M M mICM M M M M MM M M M M M M M M M I M M M M U 0 r Mlqr r 0 0'ltr O CO W M O M O r N N N M sf IT� d of r r N N N NN NN N N N N co, co CM M co C'M M co M M M co cM i N U T t` t` O co N lqr M � ti CD O r N r r r r r N N N G M M M M M M M M N N I I I 7 R L� M N O r r r r 00 M O r M0 M M M G. M N M M M M M M M W NCA M M M M M M M M O M CA O 1 r of M M M M M M M 'Q:� d N N N N I i N N N N N N N N N N N N N cM M M M M M M M cM M M m M co M M M M CM II I I III N Co lqr M N O O O O O CO CO 1- O r M N M ti W r'qr r m.;r to O r` r` co O N't M N M"T CO CO 0 0 0 O N N M N N N N N N N M m M M M M M of M M M v 14 v v v M M M M M M M M M M M M M M M M M M M M M M M i j I I r 00 �q't"t CD ti N N M M M ti O O O M M M M N N r CO O O O O N t M M !M M M M m M N M M mICM M M M M MM M M M M M M M M M I M M M M U 0 r Mlqr r 0 0'ltr O CO W M O M O r N N N M sf IT� d of r r N N N NN NN N N N N co, co CM M co C'M M co M M M co cM i N U :w COO, O r- N �M 't O O O O O O O O O O O O O O 0 0 0 0 0 0 0 O 0 0 0 0 410000 0 0 0 0 N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N m O 6 r N M 4 to CO ti 00 O O T N M 4 6 CO ;` CO 6 Or N M 4 O CO 11- Co 6 O T r r r r r r r r r N N N N N N N N N N M M M M M M M co co co r r r T r r r r r r r r r r r r r r r r r r r r r r r r r r r i + d O r N M"t M CO ti 00 O O r N CM r to CO 1-- 0 0 0 r N M -t 0 0 1-- w 6 O N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N m I I 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 CO to v r` r� to Co � r• ti ti 1` r - O O O O O O O O O O O O O O O O M O Nlo: M O Ot. to to . to Un [h 66 ti C10 6 O r N CM to CO ti M CA Ni O) to 4 M N r O W N M 't 00 � N N N N N N M M M M M c) M M m c) N N N N N N N N N N N N N N I I I 00 00 M M 00 00 00 CO 00 Co 00 00 00 00 M 00 O 00 00 OO OO 00 00 00 00 00 00 00 CO CO 00 � r r r r r r r r r r r rr r r r r r r r r r r r r r r r r r r C) N M 't to CO ti O O O- N M't O CO CO O O N M to CO ti ao CA O Q O O CA CA CA O O CA CA CA 0 0 0 0 0 0. O O O O r r• r r r r r r r r N r r r r r r r r r r r r r r r r r r r r r I I I i I 00 CJD 00 C>D 00 CO 00 00 00 00 00 00 00 M OO 00 00 0p M 00 O Co rte+ O CD 00 00 Co M 00 M 00 r r r r r T r r r r r r r r r r r r r r r r CO r r r r r r r r r 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 a O O O O O O O O O N N N N N N N N N N N N N N N N N N N N N N r, N N N N N N N N N� — � _ — O T N CO «i CO 1- CSD O O kcq M to COlA COOrrrr r r r r r r N N N N N N N N N M Me � 2z — ti ti ti ti 1` r` ti I• ti ti r- r` ti'' r` 1` ti t\ 1`� iz 1` t z iz 1` iz iz iz 1` iz N O M M M C14 N co C'7 N M M O CA N W co N N rn 0) M O M M 0) 0 M M N N r T to U) M co N O CA M M M � CA N O T r O O co O N N M � N N N 00. M r O N m E A E Q '� ti W N N O 1- r O M 0 M M W NCA Cn O O M CA O 1 r of M M M M M M M 'Q:� O ti OiO N N N N N N N N N N N N N N N N N cM M M M M M M M cM M M m M co M M M M CM COO. � N O CA qt :w COO, O r- N �M 't O O O O O O O O O O O O O O 0 0 0 0 0 0 0 O 0 0 0 0 410000 0 0 0 0 N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N m O 6 r N M 4 to CO ti 00 O O T N M 4 6 CO ;` CO 6 Or N M 4 O CO 11- Co 6 O T r r r r r r r r r N N N N N N N N N N M M M M M M M co co co r r r T r r r r r r r r r r r r r r r r r r r r r r r r r r r i + d O r N M"t M CO ti 00 O O r N CM r to CO 1-- 0 0 0 r N M -t 0 0 1-- w 6 O N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N m I I 1 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 CO to v r` r� to Co � r• ti ti 1` r - O O O O O O O O O O O O O O O O M O Nlo: M O Ot. to to . to Un [h 66 ti C10 6 O r N CM to CO ti M CA Ni O) to 4 M N r O W N M 't 00 � N N N N N N M M M M M c) M M m c) N N N N N N N N N N N N N N I I I 00 00 M M 00 00 00 CO 00 Co 00 00 00 00 M 00 O 00 00 OO OO 00 00 00 00 00 00 00 CO CO 00 � r r r r r r r r r r r rr r r r r r r r r r r r r r r r r r r C) N M 't to CO ti O O O- N M't O CO CO O O N M to CO ti ao CA O Q O O CA CA CA O O CA CA CA 0 0 0 0 0 0. O O O O r r• r r r r r r r r N r r r r r r r r r r r r r r r r r r r r r I I I i I 00 CJD 00 C>D 00 CO 00 00 00 00 00 00 00 M OO 00 00 0p M 00 O Co rte+ O CD 00 00 Co M 00 M 00 r r r r r T r r r r r r r r r r r r r r r r CO r r r r r r r r r 0 0 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 a O O O O O O O O O N N N N N N N N N N N N N N N N N N N N N N r, N N N N N N N N N� — � _ — O T N CO «i CO 1- CSD O O kcq M to COlA COOrrrr r r r r r r N N N N N N N N N M Me � 2z — ti ti ti ti 1` r` ti I• ti ti r- r` ti'' r` 1` ti t\ 1`� iz 1` t z iz 1` iz iz iz 1` iz N O M M M C14 N co C'7 N M M O CA N W co N N rn 0) M O M M 0) 0 M M N N r T to U) M co N O CA M M M � CA N O T r O O co O N N M � N N N 00. 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(WQ0035595) Residual Source Certification Attachment RSCA Tar River WTP Analytical Field Loading Calculations 4 c. oo O O oo Op O � p M M 00 m M .--i C. O H Lir Q p � O O O O p U s. ZN O N M E U U U U z z z z a a� w FL Z H � � � o x U U U P64 U U U o z z z v� U cu x c 3 State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Tar River WTP 2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private. Facility permit issued by: ❑ Div. of Water Resources, Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Jim Connolly, Superintendent Complete mailing address: PO Box 1180 City: Rocky Mount State: NC Zip: 27802 - Telephone number: (252) 972-1292 E-mail address: Jim. Connollygrockymountnc.gov 4. Facility physical address: 4400 Leaston Road City: Rocky Mount State: NC Zip: 27803 Coordinates: Latitude: 35° 54'22.37" Longitude: 77° 53' 14.72" Datum: NAD 83 Level of accuracy: Sub -Meter Method of measurement: GIS 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ® treatment of potable water, ❑ treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and % domestic) other (explain: ). 6. Does the facility have an approved pretreatment program: Yes ® No 7. Facility permitted/design flow: 12.0 MGD and facility average daily flow: a MGD 8. Average amount of residuals being generated at this facility 655 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Conventional Treatment (Gravity Settling and Decanting) Type and volume of residuals storage (i.e., outside of residuals treatment units): (2) 298,300 Gallon In -Ground Open Tanks and (2) 20,000 Gallon Vertical Silos: 636,600 Total Gallons II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ❑ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological [D Non -Biological FORM: RSC 11-13 Page lof 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: M yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Meritech, Inc. and Date of analysis: 6/18/18 Passed corrosivity test: ® yes no. pH: 62 s.u. (2 < pH < 12.5) Passed ignitability test: ® yes no. Flashpoint: >140 OF (> 140°F) Passed reactivity test: ®yes Inno. HCN: "U.7 mg/kg (<250) & HzS: 10.0 mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) Arsenic 5.0 < 0.100 Hexachlorobenzene 0.13 < 0.100 Barium 100.0 0.055 Hexachloro-1,3-Butadiene 0.5 < 0.100 Benzene 0.5 < 0.0100 Hexachloroethane 3.0 < 0.100 Cadmium 1.0 < 0.020 Lead 5.0 < 0.100 Carbon Tetrachloride 0.5 < 0.0100 Lindane 0.4 < 0.040 Chlordane 0.03 < 0.003 Mercury 0.2 < 0.02 Chlorobenzene 100.0 < 0.0100 Methoxychlor 10.0 < 1.00 Chloroform 6.0 < 0.0100 Methyl Ethyl Ketone 200.0 < 0.100 Chromium 5.0 < 0.050 Nitrobenzene 2.0 < 0.100 m -Cresol 200.0 < 0.200 Pentachlorophenol 100.0 < 0.500 o -Cresol 200.0 < 0.100 Pyridine 5.0 < 0.100 p -Cresol 200.0 < 0.200 Selenium 1.0 < 0.100 Cresol 200.0 < 0.300 Silver 5.0 < 0.050 2,4-D 10.0 < 1.00 Tetrachloroethylene 0.7 < 0.0100 1,4 -Dichlorobenzene 7.5 < 0.100 Toxaphene 0.5 < 0.05 1,2-Dichloroethane 0.5 < 0.0100 Trichloroethylene 0.5 < 0.0100 1, 1 -Dichloroethylene 0.7 < 0.0100 214,5 -Trichlorophenol 400.0 < 0.100 2,4-Dinitrotoluene 0.13 < 0.100 2,4,6 -Trichlorophenol 2.0 < 0.100 Endrin 0.02 < 0.002 2,4,5 -TP (Silvex) 1.0 < 0.100 Heptachlor and its Hydroxide 0.008 < 0.0005 Vinyl Chloride 0.2 < 0.0200 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Meritech, Inc. and Date of analysis: 12/4/18 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 12.8 Cadmium 85 39 1.30 Copper 4,300 1,500 36.2 Lead 840 300 16.9 Mercury 57 17 0.085 Molybdenum 75 n/a 6.4 Nickel 420 420 38.3 Selenium 100 100 12.8 Zinc 7,500 2,800 30.6 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/w 0 > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 5.4 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Meritech, Inc. / City of Rocky Mount and Date of analysis: 12/4/18 Parameter Result (mg1kg) Aluminum 15,200 Ammonia -Nitrogen 167 Calcium 1,560 Magnesium 658 Nitrate -Nitrite Nitrogen 36.20 pH (Standard Unit) 5.6 Phosphorus 1,240.7 Potassium 6,380 Sodium 6,380 Total Kjeldahl Nitrogen 6,556 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 7.91 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (Is) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg1kg) Surface 120 120 Injection/Incorporation 203 203 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None Known 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: aerobic digestion, ❑ air drying, ❑ anaerobic digestion, composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1 106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40 -Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30 -Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [ 15A NCAC 02T. 1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14 -Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [ 15A NCAC 02T. 1 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. Facility Tar River WTP FIELD LOADING ESTIMATES Sampling Date 12/4/2018 % Solids 5.4 Mineralization Rate 0 Gallons per DT 4,440.89 pH 5.6 Sodium Absorpotion 7.91 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio NITROGEN APPLICATION TKN (mg/Kg) 6,556 lbs./1,000 gal 2.95 Ammonia Nitrogen (mg/Kg) 167.00 lbs./1,000 gal 0.08 Nitrate -Nitrite (mg/Kg) 36.20 lbs./1,000 gal 0.02 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 120 lbs./1,000 gal 0.05 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 203 lbs./1,000 gal 0.09 Volatization Rate= 0.5 Surface Application 1.0 Injection/Incorporation EPA METAL LIMITS Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./1,000 gal 2.87 Phosphorus lbs./1,000 gal 0.56 Calcium lbs./1,000 gal 0.70 Magnesium lbs./1,000 gal 0.30 Manganese lbs./1,000 gal Sulfur lbs./1,000 gal Molybdenum lbs./1,000 gal 0.00 HEAVY METAL LOADING Arsenic (mg/Kg) 12.80 Arsenic lbs./1,000 gal 0.01 Cadmium (mg/Kg) 1.30 Cadmium lbs./1,000 gal 0.00 Copper (mg/Kg) 36.20 Copper lbs./1,000 gal 0.02 Lead (mg/Kg) 16.90 Lead lbs./1,000 gal 0.01 Mercury (mg/Kg) 0.09 Mercury lbs./1,000 gal 0.00 Nickel (mg/Kg) 38.30 Nickel lbs./1,000 gal 0.02 Selenium (mg/Kg) 12.80 Selenium lbs./1,000 gal 0.01 Zinc (mg/Kg) 30.60 Zinc lbs./1,000 gal 0.01 RESIDUAL NITROGEN CALCULATION 6,436 Total 120 0.24 Total 203 0.41 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) Surface Application Injection/ Incorporation Application Remaining Remaining Organic Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (mg/Kg) TKN (mg/kg) (lbs/DT) (mg/Kg) 6,556 120 0.24 6,436 6,556 203 0.41 6,353 6,436 0 0.00 6,436 6,353 0 0.00 6,353 6,436 0 0.00 6,436 6,353 0 0.00 6,353 6,436 0 0.00 6,436 6,353 0 0.00 6,353 6,436 0 0.00 6,436 6,353 0 0.00 6,353 Total 120 0.24 Total 203 0.41 Equations 1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Ig)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MIR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16) al —INI i I a G oc 7 c OC OC O M N 01 l O In N O 00 O 00 OC, \O Ooc -+O Tld N MO 'n N VjM CC NC cr CC O� O N C 01 t nDD �.,.� C7,C,N C l- M N N Op O p� "t O t� M O 01 O O O C O" M d' O, M 00 V OIcrq O in v1 0 oc F \ O 7 O h V' M M \D O O DD M M M M V1 M `D \O r - O O - M O N C N O GD 00 v'� OC r3. N O OCC O- Ic N � C � �p 00 N M N O O � N oo �O C � V' � h oo ,-• O [� N M 01 � OC ""' r-� � Oo � � C O _ u.x v �noo�v 000QQQQdQQQQQQQQ c a °' oo kn z z'z zz 44 z z z z z z N «7 by r1l N ^ bo CC G' fy O C) Y. r O" N SU- U y I.Ty U "'� ItTll l U Q a, x I a G Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 Meritech Work Order # 061918120 Sample: BF 0614 Grab 6/14/18 Parameter Results Analysis Date Reporting Limit Method % Total Solids 1,24 % 6/19/18 0-100 % SM 2540B Aluminum, total 10,000 mg/kg (27 6/22/18 2.50 mg/kg EPA 200.7 Arsenic, total <4.03 mg/kg46,6 � 6/22/18 4.03 mg/kg EPA 200.7 Cadmium, total 1.86 mg/kg 0.6�3b 6/22/18 0.376 mg/kg EPA 200.7 Calcium, total 14600 mg/kgN .0 6/22/18 10.0 mg/kg EPA 200.7 Copper, total 783 mg/kg0 6/22/18 1.00 mg/kg EPA 200.7 Lead, total 51.2 mg/kg Q 63 6/22/18 2.56 mg/kg EPA 200.7 Magnesium, total 4,620 mg/kg 6/22/18 10.0 mg/kg EPA 200.7 Mercury, total 0.081 mg/kg ��p0'i f 6/26/18 0.010 mg/kg EPA 245.1 Molybdenum, total 13 mg/kg 0.1612 6/22/18 0.100 mg/kg EPA 200.7 Nickel, total 43.7 mg/kg 6/22/18 0.5 mg/kg EPA 200.7 Potassium, total d'S`���� 16,300 mg/kg D 6/22/18 20.0 mg/kg EPA 200.7 Selenium, total <4.03 mg/kgs 2 `� 6/22/18 4.03 mg/kg EPA 200.7 Silver, total <2.02 mg/kg(� 0L6/22/18 2.02 mg/kg EPA 200.7 Sodium, total 5,475 mg/kg 6?, 6/22/18 20.0 mg/kg EPA 200.7 Zinc, total 660 mg/kg g 6/22/18 0.500 mg/kg EPA 200.7 Meritech Work Order # 061918121 Sample: BF 0614 Grab 6/14/18 1311 - TCLP Metals Parameters Result Analysis Date Det. Limit Reg. Limit Method Arsenic <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Barium 0.123 mg/L 6/26/18 0.050 100.0 EPA 200.7 Cadmium <0.020 mg/L 6/26/18 0.020 1.0 EPA 200.7 Chromium <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 Lead <0.100 mg/L 6/26/18 0.100 5.0 EPA 200.7 Mercury <0.02 mg/L 6/26/18 0.02 0.2 EPA 245.1 Selenium <0.100 mg/L 6/26/18 0.100 1.0 EPA 200.7 Silver <0.050 mg/L 6/26/18 0.050 5.0 EPA 200.7 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Aw iL Contact: Patrick Bone Client: Rocky Mount, City of PO Box 1180 Rocky Mount, NC 27802 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Report Date: 7/9/2018 Date Sample Rcvd: 6/19/2018 Meritech Work Order # 061918121 Sample: BF 0619 Grab Results 6/14/18 Endrin <0.002 mg/L TCLP Organics Chlordane <0.003 mg/L Parameter Results Analysis Date Reporting Limit Method Volatiles 8260 Attached 6/27/18 - 8260 Semi Vol. 8270 Attached 7/5/18 - 8270 Other Tests Parameter Results Analysis Date Reporting Limit Method Cyanide, total <0.5 mg/kg 6/20/18 0.5 mg/kg EPA 335.4 Ignitability (flashpoint) >140 "F 6/28/18 - EPA 1030 pH 7.2 S.U. 7/2/18 1.0-14.0 S.U. SM 4500 HB Sulfide, total <10.0 mg/kg 6/21/18 10.0 mg/kg SM 4500 SD 1311 - TCLP Pesticides & Herbicides Pesticide - SW -846 8081A Parameter Results Analysis Date Endrin <0.002 mg/L 7/3/18 Chlordane <0.003 mg/L 7/3/18 Toxaphene <0.05 mg/L 7/3/18 Methoxychlor <1.0 mg/L 7/3/18 Heptachlor <0.0005 mg/L 7/3/18 Lindane <0.040 mg/L 7/3/18 Herbicides - SW -846 8151A Parameter Results 2,4-D 2,4,5 -TP (Silvex) <1.0 mg/L <0.100 mg/L Det. Limit Reg. Limit Dilution Factor 0.002 0.02 1 0.003 0.03 1 0.05 0.5 1 1.0 10.0 1 0.0005 0.008 1 0.040 0.4 1 Analysis Date Det. Limit Reg. Limit Dilution Factor 7/3/18 1.0 7/3/18 0.100 I hereby certify that I have reviewed and approve these data. 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 10.0 1 1.0 1 Client: Project: Client Sample ID: Sample Collection: Meritech Sample ID: MERITECH, INC. Environmental Laboratories A Division of Water Technology and Controls, Inc. City of Rocky Mount TCLP BF0614 06/14/18 061918121 1311 - TCLP Organics Volatiles: SW -846 8260 Result Units Det. Limit Reg. Limit Dilution Factor Analysis: 06/27/18 <0.100 Date Extracted: 0.100 06/20/18 10 Analyst: VWV <0.100 mg/L 0.100 0.13 10 Parameter Result Units Det. Limit Ree. Limit Dilution Factor Hexachloroethane Benzene < 0.0100 mg/L 0.0100 0.50 10 Carbon Tetrachloride < 0.0100 mg/L 0.0100 0.50 10 Chlorobenzene < 0.0100 mg/L 0.0100 100 10 Chloroform < 0.0100 mg/L 0.0100 6.0 10 1,2-Dichloroethane < 0.0100 mg/L 0.0100 0.50 10 1, 1 -Dichloroethene <0.0100 mg/L 0.0100 0.70 10 Methyl Ethyl Ketone < 0.100 mg/L 0.100 200 10 Tetrachloroethylene < 0.0100 mg/L 0.0100 0.70 10 Trichloroethene < 0.0100 mg/L 0.0100 0.50 10 Vinyl Chloride < 0.0200 mg/L 0.020 0.20 10 Semi -Volatiles: SW -846 8270 Extraction: 06/25/18 Analysis: 07/05/18 Analyst: PM Parameter Result Units Det. Limit Reg. Limit Dilution Factor 1,4 -Dichlorobenzene <0.100 mg/L 0.100 7.5 10 Hexachlorobenzene <0.100 mg/L 0.100 0.13 10 Hexachloro-1,3-butadiene <0.100 mg/L 0.100 0.5 10 Hexachloroethane <0.100 mg/L 0.100 3.00 10 o -cresol <0.100 mg/L 0.100 200 10 m&p-cresol <0.200 mg/L 0.200 200 10 Total cresols <0.300 mg/L 0.300 200 10 Nitrobenzene <0.100 mg/L 0.100 2.00 10 Pentachlorophenol <0.500 mg/L 0.500 100 10 Pyridine <0.100 mg/L 0.100 5.0 10 2,4,5 -Trichlorophenol <0.100 mg/L 0.100 400 10 2,4,6 -Trichlorophenol <0.100 mg/L 0.100 2.00 10 2,4-Dinitrotoluene <0.100 mg/L 0.100 0.13 10 I hereby certify that I have reviewed and approve these data. "/ Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * (336) 342-1522 Fax s M1' M1• O o- e O Q O * Q N a QI Ea I- m m NH L N J J J v >- C Orl. t0 CJ z N O a -3 7 J 7 N J O v _ E O y y cY O F U H r F- 0 3 °e v Ln M -' m E * -OLJv 5- Ln LU a �� E z a r LL E w O d O a d 4-1 o Ln U- 4.1 � 4.1 � LL O 4. L O CL N ( ^ v lam/ o Q -s ai L o QJ L CL 0 01 J D __ p a a Q °a L •� > (J` p ar l E ai u � u u � = A I Q is a U ULA M Z Y °' t - J V) �1 E M v v i= !� E v ~ w U w w N ~ v otn v - p� +, 0 p of E 0O m o�,� o N N O Gi m � m '^ Q o Q L n 0 � -04..#f� l0 LO m i C m v 0 dA a) �® m m 0. Q 2 UO i Q J = 'L ~ \ O GO .i ULAJ -J O•Q y 40- a ii EE N V =0 0 Z @ _ m �— w O s N O s o m U s OC Cie0 N f0 U E C'-- V N N v oZ g LU N W m Q U > Ln N Q Lo cu O ai U r O cu E 7 7 Ln 7 C C C C V C U z ovc O ;F, a v o v OL O t CL LL = O ca L _ APPENDIX 5 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Residual Source Certification Attachment RSCA Hominy Creek WRF Analytical Field Loading Calculations 4 c. oo O O oo Op O � p M M 00 m M .--i C. O H Lir Q p � O O O O p U s. ZN O N M E U U U U z z z z a a� w FL Z H � � � o x U U U P64 U U U o z z z v� U cu x c 3 State of North Carolina DWR Department of Environment and Natural Resources Division of Water Resources Division of Water ResoUKes RESIDUALS SOURCE CERTIFICATION FORM: RSC 11-13 I. RESIDUALS SOURCE-GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Hominy Creek WWTP 2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or ❑ Private. Facility permit issued by: ■ Div. of Water Resources, Div. of Environmental Health, or j Other (explain: �. 3. Facility contact person and title: IlEmy Pridgen Complete mailing address: PO Box 10 City: Wilson State: NC Zip: 27894-0010 Telephone number: (252) 399-2491 E-mail address: jprid en e wilsonnc.org 4. Facility physical address: 3100 Old Stantonsburg Rd] City: Wilson State: E Zip: _-F— Coordinates: Latitude: 35° 41' 15.4" Longitude: M° L3'40.3 Datum: NAD 83 Level of accuracy: Sub-Meter Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, treatment of 100% domestic wastewater, treatment of potable water, treatment of 100% industrial wastewater, treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: _ % industrial and _ % domestic) other (explain: _ ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: E MGD and facility average daily flow: M MGD 8. Average amount of residuals being generated at this facility = dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type an volume of residuals treatment: conventional activated sludge with biological nutrient removal and tertiarX treatment Type and volume of residuals storage (i.e., outside of residuals treatment units): 4 anaerobic digesters with a total volume of 2,346,500; belt press with a covered 32,000 square ft storage pad holding approximately 216,000 cubic ft II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 0 40 CFR Part 503 or 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: 0 Biological 0 Non -Biological FORM: RSC 11-13 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no. If yes, list the number(s): _ b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: M yes 0 no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Wherican Testing Technoloeies, Inc. and Date of analysis: 2/7/18 Passed corrosivity test: ® yes ❑ no. pH: 6.8 s_u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: _ OF (> 140°F) Passed reactivity test: JU yes Ono. HCN: k 0.5 mg/kg (<250) & HZS: M mg/kg (<500) TCLP Parameter Limit (Mg/1) Result (Mg/1) TCLP Parameter Limit (mg/l) Result (Mg/1) Arsenic 5.0 < 1.0 Hexachlorobenzene 0.13 < 0.05 Barium 100.0 < 10 Hexachloro-1,3-Butadiene 0.5 < 0.05 Benzene 0.5 < 0.1 Hexachloroethane 3.0 < 0.05 Cadmium 1.0 < 0.5 Lead 5.0 < 1.0 Carbon Tetrachloride 0.5 < 0.1 Lindane 0.4 < 0.005 Chlordane 0.03 < 0.005 Mercury 0.2 < 0.02 Chlorobenzene 100.0 < 0.1 Methoxychlor 10.0 < 0.1 Chloroform 6.0 < 0.1 Methyl Ethyl Ketone 200.0 < 2.0 Chromium 5.0 < 1.0 Nitrobenzene 2.0 < 0.05 m -Cresol 200.0 < 0.5 Pentachlorophenol 100.0 < 0.5 o -Cresol 200.0 < 0.5 Pyridine 5.0 < 0.05 p -Cresol 200.0 < 0.5 Selenium 1.0 < 0.5 Cresol 200.0 < 0.5 Silver 5.0 < 1.0 2,4-D 10.0 < 1.0 Tetrachloroethylene 0.7 < 0.1 1,4 -Dichlorobenzene 7.5 < 0.05 Toxaphene 0.5 < 0.1 1,2-Dichloroethane 0.5 < 0.1 Trichloroethylene 0.5 < 0.1 1, 1 -Dichloroethylene 0.7 < 0.1 2,4,5 -Trichlorophenol 400.0 < 0.5 2,4-Dinitrotoluene 0.13 < 0.05 2,4,6 -Trichlorophenol 2.0 < 0.5 Endrin 0.02 < 0.005 2,4,5 -TP (Silvex) 1.0 < 1.0 Heptachlor and its Hydroxide 0.008 < 0.005 Vinyl Chloride 0.2 < 0.2 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory:aypom na sca and Date of analysis: 12/3/18 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 9.52 Cadmium 85 39 2.01 Copper 4,300 1,500 171 Lead 840 300 19.4 Mercury 57 17 0.047 Molybdenum 75 n/a 9.95 Nickel 420 420 21.4 Selenium 100 100 < 5.0 Zinc 7,500 2,800 781 b. For Surface Disposal Unit (landrill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: _ and Date of analysis: _ Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) > 0 but < 25 30 200 210 0 > 25 but < 50 34 220 240 > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 > 100 but < 125 53 360 390 > 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: a%. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: 6YMoint Analytical and Date of analysis: _ Parameter Result (mg/kg) Aluminum 5,970 Ammonia -Nitrogen 6,020 Calcium 7,970 Magnesium 1,080 Nitrate -Nitrite Nitrogen < 17.66 pH (Standard Unit) 5.2 Phosphorus 19,900 Potassium 653 Sodium 487 Total Kjeldahl Nitrogen 5,710 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): - [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: ii e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 2,966 3,451 Injection/Incorporation 5,976 5,929 6. Other Pollutants Determination: S eci whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): 0 Alternative 1 [15A NCAC 02T. I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.1106(b)(3)(B)] - Alkaline Treatment. ❑I Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. J Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 5 [15A NCAC 02T.1106b (3)(E) -(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: E7 composting, i heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: 0 Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. Alternative 2 [15A NCAC 02T.I 106(c)(2 - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, air drying, ❑ anaerobic digestion, ❑ composting, oi I lime stabilization. c. For Surface Disposal: Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [ 15A NCAC 02T.1 106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40 -Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30 -Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14 -Day Aerobic Processes. ❑ Alternative 6 [ 15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. 0 Alternative 8 [ 15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.1107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. NGMAN FIELD LOADING ESTIMATES Facility Hominy Creek WRF Sampling Date 12/3/2018 % Solids 26.1 Mineralization Rate 0.20 Wet Tons per DT 3.83 PH 5.2 Sodium Absorpotion 0.69 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply Ratio Class B Ceiling NITROGEN APPLICATION Limits (mg/Kg) TKN (mg/Kg) 5,710 lbs./WT 2.98 Ammonia Nitrogen (mg/Kg) 6,020.00 lbs./WT 3.14 Nitrate -Nitrite (mg/Kg) 17.66 lbs./WT 0.01 PLANT AVAILABLE NITROGEN SURFACE APPLIED PAN (mg/Kg) 2,966 lbs./WT 1.55 PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED PAN (mg/Kg) 5,976 lbs./WT 3.12 Volatization Rate= 0.5 Surface Application 2,800 1.0 Injection/Incorporation Nitrogen EPA METAL LIMITS PAN PAN Class A Ceiling Class B Ceiling Limits (mg/Kg) Limits (mg/Kg) 41 75 39 85 1,500 4,300 300 840 17 57 420 420 100 100 2,800 7,500 1 st Year 2nd Year 3rd Year 4th Year 5th Year HEAVY METAL CONCENTRATION NUTRIENT APPLICATION Potassium lbs./WT 0.34 Phosphorus lbs./WT 10.39 Calcium lbs./WT 4.16 Magnesium lbs./WT 0.56 Manganese lbs./WT 0.30 Sulfur lbs./WT 10.13 Molybdenum lbs./WT 0.01 HEAVY METAL LOADING Arsenic (mg/Kg) 9.52 Cadmium (mg/Kg) 2.01 Copper (mg/Kg) 171.00 Lead (mg/Kg) 19.40 Mercury (mg/Kg) 0.05 Nickel (mg/Kg) 21.40 Selenium (mg/Kg) 5.00 Zinc (mg/Kg) 781.00 RESIDUAL NITROGEN CALCULATION Total 3,451 6.90 Total 5,929 11.86 Arsenic lbs./WT Surface Application Injection/Incorporation Application 0.00 Copper lbs./WT 0.09 Remaining 0.01 Mercury lbs./WT Remaining Nickel lbs./WT 0.01 Selenium lbs./WT Organic Zinc lbs./WT 0.33 Organic PAN PAN Nitrogen PAN PAN Nitrogen TKN (mg/kg) (lbs/DT) (M9 Y_-) TKN (mg/kg) (lbs/DT) (mg/Kg) 5,710 2,966 5.93 2,744 5,710 5,976 11.95 -266 2,744 274 0.55 2,470 -266 -27 -0.05 -239 2,470 123 0.25 2,346 -239 -12 -0.02 -227 2,346 59 0.12 2,288 -227 -6 -0.01 -221 2,288 29 0.06 2,259 -221 -3 -0.01 -219 Total 3,451 6.90 Total 5,929 11.86 Arsenic lbs./WT 0.00 Cadmium lbs./WT 0.00 Copper lbs./WT 0.09 Lead lbs./WT 0.01 Mercury lbs./WT 0.00 Nickel lbs./WT 0.01 Selenium lbs./WT 0.00 Zinc lbs./WT 0.33 Equations 1 st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx 2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2) 3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4) 4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8) 5th Yr PAN (mg/Kg)= 5th Yr. 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O559 00 O 00 O 00 O 00 00 00 O 00 00 w a) =j 4 W O O O O O O O O O O O O N M WN N N N N N N N N N N N 'O O co O O O —co O O O CD O Y O N N N N N N N N N N N N a) ui r — — — r a) .> U d T � c O � = y L Y Y Y Y Y Y Y Y LQ .- co v Co � d J CL z �a J Q Q • � V LL O Lo OLo O O O OLO p OLq O ON N C''5 6 O 6 N N N �OJ O a �z a • Q 11' O N 0 O O O O 6 � O Lo I O O O Lq O LU N — N 65 LC)V O C) % V O A 00 2 M O M (6 O O O � LLCA Q O Y m 00 O a) Cl) C.OO N c U 00 05 0 U —_ — O Z 00 T c U M 0 L L d X O CoLm O O= E U Lm E U C) 0_ E :a Z = m c � 7 z O V Q V O O "EO OL Y _0 a) i N * O N c E > d V o' Q � f6 (a U L U O a) E Z J Q a) a) U) = O O_ 2 L U >, E U) U o U 00 2 M O M (6 02/28/2018 American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Report No.: 021318-0204 Enclosed are the results of the sample(s) submitted to our laboratory on 02/13/2018. All analyses were performed according to our laboratory's quality assurance program. All sample results are reported on an "as -received" wet basis unless otherwise noted. The test results meet requirements of the NELAP standards for methods listed on the laboratory's current fields of accreditation (EPA 8260, 8082, 8081, 8151, 8270, 6010, 6020, 1010, 9045, 7471, 1010, 1311, 150.1, 200.7, 200.8, and 245.1) except as noted. Results apply only to the items submitted to the laboratory for analysis. Pursuant to NELAP, this report may not be reproduced except in full, and with written approval from the laboratory. If you have any questions please contact the laboratory manager at 330-634-9906 or via email at samy@atnericantestinptechnolo2ies.com nager ATT is NELAP-accredited by the State of Florida, #E871084. Other state accreditations include: North Carolina, #670; Pennsylvania #68-05167; West Virginia, #372. The results relate only to the items tested. ATT shall have no liability to the client or client's customer with respect to decisions or recommendations made, actions taken or courses of conduct implemented by either the client or the client's customer as a result of or based upon the Test Results. In no event shall ATT's liability with respect to the Test Results exceed the amount paid to ATT by the client therefor. 1350 Home Avenue Akron, OH 44310 Page 1 of 19 Toll Free: 877-634-9906 Phone: (330) 6349906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/08/2018 Time Collected: 12:23 Client ID #: 58575 Laboratory ID #: 021318-03 Date of Analysis: 02/15/2018 Certificate of Analysis Metals-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Arsenic <1.0 mg/L 5.0 6010C Barium <10 mg/L 100.0 6010C Cadmium <0.5 mg/L 1.0 6010C Chromium <1.0 mg/L 5.0 6010C Lead <1.0 mg/L 5.0 6010C Mercury <0.02 mg/L 0.2 7470A Selenium <0.5 mg/L 1.0 6010C Silver <1.0 mg/L 5.0 6010C 1350 Home Avenue Akron, OH 44310 Page 14 of 19 Toll Free: 877-634-9906 Phone: (330) 634.9906 Fax: (330) 634-9907 Website: www.AmericarTestin,- echnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/16/2018 Certificate of Analysis Volatiles-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Benzene <0.1 mg/L 0.5 8260B Carbon tetrachloride <0.1 mg/L 0.5 8260B Chlorobenzene <0.1 mg/L 100 8260B Chloroform <0.1 mg/L 6.0 8260B 1,2-Dichloroethane <0.1 mg/L 0.5 8260B 1,1-Dichloroethene <0.1 mg/L 0.7 8260B Methyl ethyl ketone <2.0 mg/L 200 8260B Tetrachloroethene <0.1 mg/L 0.7 8260B Trichloroethene <0.1 mg/L 0.5 8260B Vinyl chloride <0.2 mg/L 0.2 8260B Page 15 of 19 1350 Home Avenue Akron. OH 44310 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.AmericanTestingTechnologies.com Amerls n Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/17/2018 Certificate of Analysis BNA-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 1,4 -Dichlorobenzene <0.05 mg/L 7.5 8270C 2,4-Dinitrotoluene <0.05 mg/L 0.13 8270C Hexachlorobenzene <0.05 mg/L 0.13 8270C Hexachlorobutadiene <0.05 mg/L 0.5 8270C Hexachloroethane <0.05 mg/L 3.0 8270C Nitrobenzene <0.05 mg/L 2.0 8270C Pyridine <0.05 mg/L 5.0 8270C o -Cresol <0.5 mg/L 200 8270C m,p-Cresol <0.5 mg/L 200 8270C Pentachlorophenol <0.5 mg/L 100 8270C 2,4,5 -Trichlorophenol <0.5 mg/L 400 8270C 2,4,6 -Trichlorophenol <0.5 mg/L 2.0 8270C .1350 Home Avencae Akron, OH 44310 Page 16 of 19 Tall Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 6349907 Website: ww v.AmericanTestingTechnologies.com American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/17/2018 Certiff'icate of Analysis Pesticides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number Chlordane <0.005 mg/L 0.03 8081B Endrin <0.005 mg/L 0.02 8081B Heptachlor <0.005 mg/L 0.008 8081B Heptacblor epoxide <0.005 mg/L 0.008 8081B Lindane <0.005 mg/L 0.4 8081B Methoxychlor <0.1 mg/L 10.0 8081B Toxaphene <0.1 mg/L 0:5 8081B 1350 Home Avenue Akron, OH 44310 Page 17 of 19 Toll Free; 877-634-9906 Phone: (330) 634-9906 Fax (330) 634-9907 Website: wv✓w.AmericanTestingTechnologies.com s American Testing Technologies, Inc. WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58514 Laboratory ID #: 021318-04 Date of Analysis: 02/27/2018 Certificate of Analvsis Herbicides-TCLP (EPA 1311) Parameter Results Units Regulatory Method Limits Number 2,4-D <1.0 mg/L 10.0 8151A 2,4,5 -TP (Silvex) <1.0 mg/L 1.0 8151A reviewed by: Manager 1350 Hame Avenue Akron,OH 44310 Page 18 of 19 Toll Free: 877-634-9906 Phone: (330) 634-9906 Fax: (330) 634-9907 4vebsite: www.AmericanTestingTechnologies.com WayPoint Analytical 7621 Whitepine Rd Richmond, VA 23237 Date Received: 02/13/2018 Date Reported: 02/28/2018 Date Collected: 02/07/2018 Time Collected: 11:57 Client ID #: 58513 Laboratory ID #: 021318-04 American Testing Technologies, Inc. Certificate of Analysis Parameter Results Unfits Method Date of Number Analvsis Reactive Cyanides <0.5 mg/kg 7.3.3.2 02/23/2018 Reactive Sulfides <25 mg/kg 7.3.4.1 02/23/2018 pH (Lab) 6.80 S.U. 9045D 02/13/2018 Flashpoint >140 °F 1010A 02/16/2018 Toll Free: 877-634-9906 1350 Home Avenue Akron, OH 44310 Page 19of19 Phone: (330) 634-9906 Fax: (330) 634-9907 Website: www.ArnericarTestingTechnologies.com M C N �9 O C O Q E v T CL IV t - O U N F - O Z O v � U U10 C: V X M r 3 m C O as O oto N N N O �ON r WTO N p t O M c C Q _ a O U c y LL � � t r 3 r ,c —sem ~ � c c m e o O N �9 O C _ Q w v C IV t - O N F - O Z r+ � v � U U10 C: y N X M iu 3 m (0 N N CL O Q > m Y N X tJ O M c Q LL a O U c y a) O U X 3 LU X c m ,n U O N �9 O C U C C IV Cf' O N F - U10 C: X iu 3 m c (L) CL m N 1 tJ O c — a O U c y a) O o 3 C) X c m 0 O m f0 E U a3 ,7 0 ) z `n is m C C U)- J Q E E m o m �1 � � C Y U Ln NW X a E N N � �0 O Q m c O J O _ CD m E E N X (n0 N 00- o J 2 U) aci u m CL -0a cu E -E 0 m E aE ns o w C L CL IT C7U C7U (7U c O m o to O c _ J >N X O N Z a) c' ` T > a� m N o c :3 ..+ N C .l N C T.0 Ut Z o a o 0 I `' a ' E .n -0 Q'o �_ L) o E O O Y I I I� I� co v Y �F @ 0 C: JL U) p U N U U) N U N U T &-c a) m@ Jl m 0 u) inn T ca N N R r� 4 C3 T C7 a C5 a 00- CD a m Y N a U a) U N N � � (n J � c _ o _ � to a� N C Wil_ p (D Q C d OE ` U) a1 `C1 -C (a O p Lq _ � 0 d N o z o i0- N �9 O C U C C IV Cf' C: iu 3 m E F- m N 1 tJ a c — a O U c y o E c m 0 O m f0 E U a3 ,7 0 is m C C Q E E m o m �1 � � C Y U — a E N N �0 O Q m c O J O _ m — E (n0 N 00- J 2 E aci u m CL -0a cu E -E 0 m E aE ns �E fl C L CL IT C7U C7U (7U CSU m o to O O a N Z a) c' ` T aci a� m N o c :3 Z E Ut Z =3d ' E .n -0 Q'o �_ L) o E mco J J Y F, CJ �Z co N U C: JL U) H = J n1 T E m (D 3 C3 m Y N a U a) U N O u U (n J � c 3 _ � to N �9 O C U C C IV C: iu m LL m 0 U a a O U °0' a0i E c m 0 m cci m m E E m � � C Y U cn E Z N �0 O Q m c O J O _ m — E (n0 Z 2 E aci u O fl C L CL o m m m o to 0 O N Z a) c' aci a� m N o c Y Z E Ut E =3d ' E o m �_ L) o E Y F, CJ Q co N U C: U) H = J n1 E C3 m Y N a U a) U O U H � c 3 _ � to a� N C Wil_ p (D Q 61 d U) a1 � 0 N f6 o i0- m CY0 CV � p Ul oLO Z B Waypoint- ANALYTICAL 02/08/2018 14:17:20 Export Batch Report Export Batch Id : 1987EXP To: I American Testing Technologies 1350 Hone Ave. Akron, CH 44310 330-634-9906 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypoi nta n a lytica l.com Page 1 of 1 Created: 2/8/2018 14:16:56 Computer: RVADESK001 User: Morgan Tichacek From: Waypoint Analytical Virginia, Inc. 7621 Whitepine Rd. Richmond, VA 23237 804-743-9401 Report No Sample Date Rush Lab No Method No Fee Code Description 18-039-0203 02/07/2018 11:57 Z 58513 ASTM D93-80 Ignitability/Flashpoint (ASTM HTime Re mquished By (s n) sign) D93-80) 18-039-0203 02/07/2018 11:57 58513 SW -7.3.3 Cyanide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW -7.3.4 Sulfide Reactivity 18-039-0203 02/07/2018 11:57 58513 SW -9045C Corrosivity (pH) 18-039-0203 02/07/2018 11:57 58514 SW -1311 TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW -1311 (ZHE) TCLP Extraction Method 1311 18-039-0203 02/07/2018 11:57 58514 SW -6010C (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW -7470A (TCLP) TCLP Metals (8 RCRA Metals) 18-039-0203 02/07/2018 11:57 58514 SW -8081A (TCLP) TCLP Pesticides (Pest) 18-039-0203 02/07/2018 11:57 58514 SW -8151A (TCLP) TCLP Herbicides (Herbs) 18-039-0203 02/07/2018 11:57 58514 SW -8260B (TCLP) TCLP 'VOCs (Volatiles) 18-039-0203 02/07/2018.11:57 58514 SW -82700 (TCLP) TCLP SVOCs (BNAs) Sampled By Method of Shipment Blank / Cooler Temp. t C Remarks Relinquished By (sign) TimeEReceiv (sign) Date / Timei Z ' l�f�®;3t HTime Re mquished By (s n) sign) Dpte / Ti 0 i (31 t3'_c % Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 1 Contact: Jimmy Pridgen Report Date: 12/13/2018 Client: City of Wilson Project: Hominy Creek Class B Sludge 3100 Old Stantonsburg Rd Project: AM12042018 Wilson, NC 27893 Date Sample Rcvd: 12/4/2018 Meritech Work Order # 120418117 Sample: Hominy Creek Class B (A-791-1) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 46.0 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 21,739 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D Meritech Work Order # 120418118 Sample: Hominy Creek Class B (A-791-2) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 28.6 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 129,371 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D Meritech Work Order # 120418119 Sample: Hominy Creek Class B (A-791-3) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 35.7 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 81,232 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D Meritech Work Order # 120418120 Sample: Hominy Creek Class B (A-791-4) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 29.6 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 60,811 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D Meritech Work Order # 120418121 Sample: Hominy Creek Class B (A-791-5) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 54.3 % 12/5/18 0400 % SM 2540B Fecal Coliform (Sludge) 502 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 Page 2 Contact: Jimmy Pridgen Report Date: 12/13/2018 Client: City of Wilson Project: Hominy Creek Class B Sludge 3100 Old Stantonsburg Rd Project: AM12042018 Wilson, NC 27893 Date Sample Rcvd: 12/4/2018 Meritech Work Order # 120418122 Sample: Hominy Creek Class B (A-791-6) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method % Total Solids 54.3 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 18,416 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D Meritech Work Order # 120418123 Sample: Hominy Creek Class B (A-791-7) Grab 12/4/18 Parameters Results Analysis Date Reporting Limit Method %Total Solids 36.1 % 12/5/18 0-100 % SM 2540B Fecal Coliform (Sludge) 22,161 col/g dry wt 12/4/18 382 col/g dry wt SM 9222D I hereby certify that I have reviewed and approve these data. .. Q _ (` Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 _ O O 0 0 V1 ¢ it vEl Z .- NO J .. 16 O n .. H U � E £ � N O E o �o m a z N N c -I s 1- U - ` O N N V 3 0 .-. C) ❑,, rn 3 tiO oU o o £ o o E M1 O x cr a H W o c o Y1v N a � U V U U � V U V5. O n '��1L LL LL W LL `� tL Yom. V — N ca q{ 40 OBJ ca Q{ cac O y0 N 1' E a � m N O O O O O O O a 'p �, Q N V) H N H V/ h �� O N m a am+ m m Im m m m J Q Z c 0 �' F- F FF F F• F• E Y E. o m x o H V y y I 8 v a E D c7 Q Q I C o o. a E E O ❑: F EA LA a N N ~ WV �I W n 0 O H .. r Zid N N O O o n m m a 41 E 6Ci r a m n' m U U ® T m aj 0 OJ 'Si. % ni E `O O i ) Ua 0 0005 £ O 9 9 O — R �J - �? 0 x '— o— ^t ai �Q i= v Q a LL� Q O o v v Z @J of o 0 WWc O O S H Y _ T G ^ C = 3 O O w U 'm W £ > W as `+- W w E y t� H N .Q ri ri rl rl rl H Q R V m r� t� t� t� t� t� t` N U m m O R1 Ci GC q P7 C7 FA U O v U U U U U U U O +' > X c e e o e n a N S S x 0 1:111 El El � P A AIF;Z PROM PT-ACCURATE- RELIAOLE LABORATORIES, INC WWW.PARLABS.COM REPORT OF ANALYSES Attn: ANDREW MLOT CITY OF WILSON PO BOX 10 WILSON, NC 27894-0010 PROJECT NAME: DEC IS r;A.TE: 01/23/19 SAMPLE NUMBER- 134235 SAMPLE ID- HOMINY CREEK A-789 "CLASS B" SAMPLE MATRIX- SO DATE SAMPLED-- 12/03/18 TIME SAMPLED- 1040 DATE RECEIVED- 12/04/18 SAMPLER- NH RECEIVED BY- DJ TIME RECEIVED- 0925 DELIVERED BY- FEDEX TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 40 DAY BENCHTOP DIGESTION EPA62SR 12/04/18 1350 RE 3.56 % LABORATORY DIRECTOR 2217 Graham Park Drive • Charlotte, NC 28273 Phone: (704) 588-8333 • Fax: (704) 588-8335 FR.- A. INC 40 Day Bench Scale Extended Aeration Test for Anearobically Digested Solids Percent Volatile Solids Reduction Day6 - Stallof Yest Raremnoa or CalcWa6on De -don Dish Wil RepBcate #1 25 0067 Re irate $2 21 5553 Replicate 93 20 6�8 R 4'4 205241 Re e5 AVERAGE 24.3091 22.3705 8 mmmEm In'rSal Sam WI+Em Dish M34,1953 Empty 00 Wt 29.9283 3148,24 3C 3341 34.7372 32-1171 C Dried Sam WI+Em DM WI 26.1120 24.2399 240694 237510 27.62e6 256044 D Ached Bu eD Sample M - Dish 4Vt Jill 26,3750 22.8977 21 9794 2t 9343 258528 23.7876 L= &A Uquid Sludge M 9.1288 0.2410 11,1256 9.5094 10.4281 9.7485 5 = (C -A) Dried Slud a Wt i 3-0453 2.8536 3.7226 3.2263 3.5195 3.2335 V • C-13 Volotle Solids Wt 1 17370 1.5412 2.1100 1.8167 1.4758 18361 F - (D -A) Fued Solids W1 11083 11124 15126 14088 1.5437 1.3973 VIA • (\0S), 100 OWN""Sdide % 57.039 56-080 56.681 56.309 56.139 56.&196 - 1L Mass Fraction of Volatile Sd�tls in a u1d (Feadi Slud a at Start Of Test 0.1902811 0.1870161 0-11511 0.1 e51999 0.1894688 0.1883 • F!L Mase Ftacton o1 Fued SOYds'st UqUd (Feed) bMill at Slart 01 Test 0.1433188 1 0-1349638 I 0.1449450 I 5.1436968 1 8,1460327 1 0.1430 Day 20 - Mid -Pohl! of Test (OC Check! Ratan- or Cnlwledon D"cVfiov Rel 01 Rai 82 ReOcai Replicalt Ifo Replicate *3 AVERAGE A Empty 00 Wt 21.5167 227089 21 0359 18.3051 = 21,6717 f 6 Inilial Sample Vit + EmDish Wl 304142 32.3221 26.5060 24.7205 30.56615 28.3161 C Dried SamicW1+Empty Dish Wt 244124 25.5576 235185 211178 24.7416 23.8292 D Ached &mad Sample WI+Dish Wt 22.8166 24.OB80 2214% 20.1050 23.154? 22-4633 L - B -A) - wd sludge 714 8.6853 B 6152 L5901 5.4154 8.5889 6.0290 5 = (C -A) Dived a WI 2.8937 3AWS 2AW7 1.8125 2,8699 2,8415 V = C -D Volatlle Solids Wt 1.59% 5.7598 1.3750 1 01 t6 1,5873 1.4659 F= D -A Fixed Solids Wt 1.2981 1.3911 1.1057 0.8008 12826 1,1757 V%= OlMriOQ Peroeld Volatile Solids ML 55.140 55.851 55.428 55.632 5$.309 559080 20 -V%(0) OC Check of Ana Is 20 da V% less than 0 da V%7 Yes Yas Yes Yes Yes re o es , n anal,o prw"aaa.9 --y _ a , ec r error. Day 40 - End of Test VSR (m0} - See Belov Fradionel Volatile Solids Reduction (Mass Balance Method) Average FVSR (mb) of all Valid replicate results Is Average FVSR (mb) less than or equal to 17%? *Calculation: FVSR (mb) _ y = mass fraction of volatile soiids In the liquid sludge x = mass fraction of fixed solids in the liquid sludge f = indicates feed sludge at start of the test b = indicates "bottoms" sludge at end of the test 5.21% •1,65% 2,55% 5,63% 6.08% 3.56°/D YES - Sample Passes Requirement [y(f) ` (1 - x(b))] - [Y(b) * (1-x(0)] [y(fl' (1-x(b)-y(b))] vo. a- 411483 • [.hit i- RC 75741-1+33 ehwa(9r ,W!1333era j'N).419+1135 h -v i'l. M PROMPT -ACLU RATE- RELIAOLC t,ABORATORIES, INC CHAIN OF CUSTODY Phone (704)588.8333 Fax (704) 588-8335 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241.1483 It Is essential that at] information be reeordad on this Chain of Custody document for acceptance by PAR Laboratories. Inc, and the North Carolina DenartmPnt of Environmental and Natural Rearourac Company Name (bitting) C.4 f W Lill Comments/ Special Instructions i d i t q p?' V S 20 i s Address — City, State fx zip code L'/-14 ciJ tQ Point of Contact 8 Telephone Number ��f�11u1 jqjotZS �� " 1YiV Sample AL, ,�( Taken By: SIGNATURE PRINTED NAME << -rim - ARE SAMPLES FOR STATE or EPA REPORTING? YES X NO `Sample Type: DW WW X GWVW Hw Sou Cather JC Sample Temp at time of sampling: ° C Sample Temp upon receipt: ° C "Field Preserved: YesTeflon Liner/Zero Headspace: Yes No n1a Residual Chlorine checked a tme of sampling (YIN): Dechlorination Necessary (YIN): Gent Sample 1,0, (Sample Location ! Number) Comp Grab 1 Set Up Preserv, i DaterTime Collection DaatelTlme Analyses RequestW 'JI ',,A -,I %1[tC ((A r, `7 l34ro(G �1 r I E I Relinauished Relinquished by DatelT me Recervea by: Received by. Datw7ime C=Composite G=Grab DW=Dnnking Water WW=Wastewater GWMW=Groundwater Monitoring Well I-W=Hazardous Waste APPENDIX 6 2019 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) LAS CA Site T1 Land Owner Agreement Form Maps Biosolid Utilization CPLR Update I� cd a � a D„ ou CA 0 0 0 0 0 0 0 0 0 0 0 0 0 z z 3 z z z z z z z z z z( -l)¢¢¢ o � o o � o o al 0 0 0 0 0 0 0 0 0 0 •b >, �, >, z z 3 z z z z z z z z z z¢¢ ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. a c7 c7 c7 U� c7 c7 cc U� c7 m c7 M U� c( c7 c7 M U� m(z c7 c7 M U� C7 o v 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 0 U 0 0 U N 0 N N 0 U N N U N N U N N 0 0 N 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 E 0 p N on N on N on N on N on N on N o4 N on N ou N on N on N on N o4 N on N on N on N cn U W W W W W W W W W W W W W W W W W i. en � O Vl � � M DD O M •--� 00 .�. N 00 l-� M 00 ,N -i Vl M (V N 00 00 01 L �• C7 C7 C7 C7 C7 C7 L7 C7 C7 C7 C7 C7 L7 C7 C7 L7 C7 � F�+ F�+ Ri �i F�+ �i Chi F�+ Ri Chi �i Rei 0.i Chi Rei Py CC ti ti ,� h ti h ti �O-, ra N Y Y Y Y Y Y Y Y Y Y N W W W W W N W W W W W W W W W W W W N w N w U w N w N w U w N w N w U w N w N w N w N w N w N w N w N w 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 F1 H H E-, H ^O O O O O O O O O0 N M -- H H— H H— H p H H H H H H H H H H H H H H H H H cd a State of North Carolina DWR Department of Environmental Quality Division of Water Resources DIvision of Water Resources 15A NCAC 02T.1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting nit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Granville Farms Inc. hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) Site T1 Fields 1-10 Yes Row Crop/Small Grains Animal Consumption No -Till The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. H. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12 -month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30 -day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30 -day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14 -month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20 -month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38 -month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12 -month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ® The land application field(s) ID: Site T1 Fields 1-10 is currently permitted under another residuals land application program; Permit Number WQ: 0002047 . The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; Granville Farms Inc. (WQ0035595) (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. I I ;') Land( Addr( City: State: V C . Zip: t�f�S L Phone: — ! ! E-mail addre s: Signature: `L- y ' Date: NORTH CAROLINA, Ghcc ni - I l e r I, the undersigned Notary Public do hereby certify that a S h l e6— _0, V l a i- personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the (� f' t dayof Decei,,h-er ,20 Signature and seal: &�te,` lJec. My commission expires: 7-3 Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby Lessee/operator name: I nc tAy to abide by the stipulations and restrictions as specified herein. Address: i 1� > f 31 ?5 City: a ����C: t State: Zip: Phone:.. (:. E-mail address: R Signature: vj�L") 1 Date: 12 ' 6 J �o%f Permittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing Signature: Date: i A/6 / o FORM: LOA 06-16 Page 3 of 3 . �N r S x W. [L Seaboard Coast Line (Railroad) 27.56 Gross Aeres 10.89 Gross Acres Field 1 Field 2 24.30 Net Acres 8.37 Net Acres m A . /A t� A r Vp 7y ;.aim c � G Legend f ■ House Structure 10.74 Gross Acres • Well Field 3 12.63 Gross Acres 7.56 Net Acres Field 5 —"'—'► Ditch 8.30 Net Acres Stream Buffer 4.68 Gross Acres Field 4 Field Boundary 3.75 Net Acres © Net Area ~ ♦ 28.10 Gross Acres Pond t Field 7 Property Boundary v 0 250 500 1,000 19.14 Net Acres Feet Scale: 1 inch = 500 feet so]L PLJ s BUFFER MAP - T1 FIELDS 1 - 2 FIGURE Drawn By: DM Granville Farms Class B Land Application Reviewed By: Class B Permit WQ0035595 Date: March '19 Soil Plus Project # 200705.C10 N S ♦ . 10:74 Gross Acres/ Field 3 7.56 Net Acres 4.68 Gross Acres Field 4 3.75 NetA� cress 16.48 Gross Acres Field 6 12.13 Net Acres 12.63 Gross Acre! Field 5 8.30 Net Acres 28.10 Gross Acres t Field 7 t 19.14 Net Acres t Field 9 i� 10.37 Gross Acres 355�Net Acres Field 8 5.90 Net Acres Legend ■ House �■ Structure 22.75 Gross Acres ■ Field 10 • Well ■ ■ ■ 14.29 Net Acres — — ► Ditch ■ Stream ■ Buffer ■ Field Boundary ■ © Net Area Pond Property Boundary 250 500 1,000 Feet Scale: 1 inch = 500 feet BUFFER MAP - T1 FIELDS 3 - 10 FIGURE Drawn By: DM Sol ILP J S Granville Farms Class B Land Application Reviewed By: Class B Permit WQ0035595 Date: March '19 Soil Plus Project # 200705.C10 07 M M G1 N 00 O 00 M M O r l� N O O N V' 00 r- to 00 i --i � N (V Ic �--i in N N V r- 00 l� Ln GJ N G� Gl l� V Gl M O uy Lr M M N r"o"o M r G\ N N O\ N ON V' O � F � U v �y \ N N(= N N N N N N N 7-i O O O O O O O O O O U HC�7HA MM 00 kn O N M O O � N M M U V V V V V V V V V V U N z M N I� m 00 l0 r� Ln M M ro Ln u) M r1i N O U `� I � O O "DL � N l0 � N O c -I � N O N Ln C7 GJ O O cl O O O O O O O p 4 44 �zz z z z z z z z N M "t u) V � 00 C, w w F F F F F F F F F F 9 0 c o O O O O O O O Cl O O O Cl O O O O Cl O Cl O O Cl O O O O O Cl Cl ClO O n H 'V N G\ M L N cc M O o0 O N I O M 00 00 ✓1 M N r- oo M �_ N O O 7 N 7 O O_ O O O O M _O O O O O O O O O O O O Cr O In cl O or0 M Qr� N V� �i Cl O O O O O O O O O O O O M N o0 N N N b r- M l - M O N O N O N Cl Cl O O O O O O O O O O O O O O O O O O O O O O O O O O Cl O O O O O O O O O O O O Cl Cl Cl Cl O O 7 V l- n N V 't co MV^ N r O O r Cl Cl O O O O O O O O O M ON 000 r GO c\ N O V' M lo O G1 M r - O O GDo O O O O cl d' W l- r- M M d' N L d' O O O O O 7 O O O O O O 7 O O 7 O O O O O O O O Cl Cl Cl Cl O O G1 W W cl t+'1 N M V V N M_ u1 O 7 C1 O C1 O W O M O N O cl O \0 G� O O O O O O O O O O O O O O N M 7 N V" n o m C, C, CN C, ol C', C', cam. V o0 . O O O O N O N N N N N N N o0 O O O O O O O O O O O O O O O O O O .--� m o M N 0 O 0 O 0 O 0 O 0 O 0 O 0 O Vr O C) M M N N N N N N N o0 O O O O O O O O O O M O O O O O O 7 O 7 O 7 O 7 O 7 O 7 O 7 7 O O O O O O O Cl Cl Cl O O N Gl M N N N N N N N o0 Ic 00 00 l� O O O O O O Cl Cl O Cl Cil O O O cl, 1� M N N `V d- Lf) O O O O O O O l� t� N O N O N O N O N O N O N O V o0 . O O O O O O Cl Cl O W Cf) C) N M 7 vn b n — APPENDIX 7 2018 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) LAS CA Site T6 Land Owner Agreement Form Maps Biosolid Utilization CPLR Update I� cd a � a D„ ou CA 0 0 0 0 0 0 0 0 0 0 0 0 0 z z 3 z z z z z z z z z z( -l)¢¢¢ o � o o � o o al 0 0 0 0 0 0 0 0 0 0 •b >, �, >, z z 3 z z z z z z z z z z¢¢ ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. ,-. a c7 c7 c7 U� c7 c7 cc U� c7 m c7 M U� c( c7 c7 M U� m(z c7 c7 M U� C7 o v 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 0 U 0 0 U N 0 N N 0 U N N U N N U N N 0 0 N 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 E 0 p N on N on N on N on N on N on N o4 N on N ou N on N on N on N o4 N on N on N on N cn U W W W W W W W W W W W W W W W W W i. en � O Vl � � M DD O M •--� 00 .�. N 00 l-� M 00 ,N -i Vl M (V N 00 00 01 L �• C7 C7 C7 C7 C7 C7 L7 C7 C7 C7 C7 C7 L7 C7 C7 L7 C7 � F�+ F�+ Ri �i F�+ �i Chi F�+ Ri Chi �i Rei 0.i Chi Rei Py CC ti ti ,� h ti h ti �O-, ra N Y Y Y Y Y Y Y Y Y Y N W W W W W N W W W W W W W W W W W W N w N w U w N w N w U w N w N w U w N w N w N w N w N w N w N w N w 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 F1 H H E-, H ^O O O O O O O O O0 N M -- H H— H H— H p H H H H H H H H H H H H H H H H H cd a State of North Carolina DWR Department of Environmental Quality Division of Water Resources DIvision of Water Resources 15A NCAC 02T.1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting nit. General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ® Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ® A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Granville Farms Inc. hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) Site T6 Fields 1-7 Yes Row Crop/Small Grains Animal Consumption No -Till The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 I. STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. H. RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12 -month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30 -day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30 -day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14 -month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20 -month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38 -month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12 -month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ® The land application field(s) ID: 51te T5 Fields 1-7 is currently permitted under another residuals land application program; Permit Number WQ: 0002047 The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; Granville Farms Inc. (WQ0035595) (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. I I ;') Land( Addr( City: State: V C . Zip: t�f�S L Phone: — ! ! E-mail addre s: Signature: `L- y ' Date: NORTH CAROLINA, Ghcc ni - I l e r I, the undersigned Notary Public do hereby certify that a S h l e6— _0, V l a i- personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the (� f' t dayof Decei,,h-er ,20 Signature and seal: &�te,` lJec. My commission expires: 7-3 Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby Lessee/operator name: I nc tAy to abide by the stipulations and restrictions as specified herein. Address: i 1� > f 31 ?5 City: a ����C: t State: Zip: Phone:.. (:. E-mail address: R Signature: vj�L") 1 Date: 12 ' 6 J �o%f Permittee's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing Signature: Date: i A/6 / o FORM: LOA 06-16 Page 3 of 3 iia: VV 0 ro� a. • Am � r 40 r - ■ • _ ■ VV a. Net Acres/ iA ■ Old -County -Home PV I � Field 6uut� /,141Gross Acres 24.72 GrossAcres A A Field.l A �i 13.58 Net Acres -- Field 3 2.08 Net I� l Field s Field 5 8.63 Net Ac gross Acres . 11.-_�.F� 11.71 G Field 6 8.17 Net A Legend \Y ' ' ' ' uross Acres '2!63'Net Acres ■ House Structure • Well — — ► Ditch I Stream , Buffer Field Boundary © Net Area Pond" Property Boundary o 250 500 1,000` - Feet i- 5' Scale: 1 inch = 500 feet BUFFER MAP -T6 FIELDS 1- 7 FIGURE Drawn By: DM SOIL PLt rs Granville Farms Class B Land Application EDavt EeM d By: J Class B Permit WQ0035595 rch'19 Soil Plus Project # 200705.C10 0 00 00 v o Ln "n 00 M M M O � H U V V V V V V V U 00 Ln m 00 N U z N N 00 00 Ql U p N N Ql m l0 N ci N � � l0 N C7 ��� O O O O O O u u u zzz���� w w H H H H H H H U U � o vHp+ FC7FA N l� 00 't N � � 't N N � M z 9 0 c o o m C, C, CN C, ol C', C', cam. V o0 . O O O O N O N N N N N N N o0 O O O O O O O O O O O O O O O O O O .--� m o M N 0 O 0 O 0 O 0 O 0 O 0 O 0 O Vr O C) M M N N N N N N N o0 O O O O O O O O O O M O O O O O O 7 O 7 O 7 O 7 O 7 O 7 O 7 7 O O O O O O O Cl Cl Cl O O N Gl M N N N N N N N o0 Ic 00 00 l� O O O O O O Cl Cl O Cl Cil O O O cl, 1� M N N `V d- Lf) O O O O O O O l� t� N O N O N O N O N O N O N O V o0 . O O O O O O Cl Cl O W Cf) C) N M 7 vn b n — APPENDIX 8 2018 PERMIT MODIFICATION Granville Farms, Inc. (WQ0035595) Current Permit I. NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH LAND APPLICATION OF CLASS B RESIDUALS PERMIT (NON -DEDICATED) In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations IS HEREBY GRANTED TO Granville Farms, Inc. Edgecombe County FOR THE continued operation of a residuals management program for Granville Farms, Inc. and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved sites listed in Attachment B with no discharge of wastes to surface waters, pursuant to the application received June 15, 2016, and subsequent additional information received by the Division of Water Resources, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from the date of issuance until September 30, 2021, shall void Permit No. WQ0035595 issued April 12, 2012, the most recent Attachment A certified July 23, 2014, and the most recent Attachment B certified August 17, 2012, and shall be subject to the following specified conditions and limitations: 1. No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. [15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T.01091 H. PERFORMANCE STANDARDS The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals to the site, contact the Raleigh Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.1] W00035595 Version 2.0 Shell Version 151201 Page 1 of 13 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [15A NCAC 02B .0200, 02L.0100] 3. Only those Class B residuals generated by the facilities listed in Attachment A are approved for land application in accordance with this permit. [G.S. 143-215.1] 4. Only the sites listed in Attachment B are approved for residuals land application. [G.S. 143-215.1] 5. Pollutant concentrations in residuals applied to land application sites listed in Attachment B shall not exceed the following Ceiling Concentrations (i.e., dry weight basis) or Cumulative Pollutant Loading Rates (CPLRs): Parameter Ceiling Concentration (milligrams per kilogram) CPLR (pounds per acre) Arsenic 75 36 Cadmium 85 34 Copper 4,300 1,338 Lead 840 267 Mercury 57 15 Molybdenum 75 n/a Nickel 420 374 Selenium 100 89 Zinc 7,500 2,498 The Permittee shall determine compliance with the CPLRs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application has not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. [15A NCAC 02T. 11051 6. Residuals that are land applied shall meet Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c). Exceptions to this requirement shall be specified in Attachment A. [ 15A NCAC 02T .1106] 7. Biological residuals (i.e. residuals generated during the treatment of domestic or animal processing wastewater, or the biological treatment of industrial wastewater, and as identified in Attachment A) that are land applied shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exceptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1107] WO0035595 Version 2.0 Shell Version 151201 Page 2 of 13 8. Setbacks for Class B land application sites shall be as follows: In accordance with the Setback Waiver Agreement (FORM: SWA), the setback requirement may be reduced to a minimum of 100 feet upon written consent of the owner of the property until September 30, 2021 or until the owner sells the property, whichever comes first. [15A NCAC 02T .1108] 9. Land application areas shall be clearly marked on each site prior to and during any residuals application event. [15ANCAC 02T .0108(b)(1)] WQ0035595 Version 2.0 Shell Version 151201 Page 3 of 13 Setback by application type (feet) Vehicular Irrigation Injection / Setback Description Surface Surface corporation Application Application Habitable residence or place of public assembly under separate ownership or not to be maintained as part of 400 400 200 the project site Habitable residence or places of public assembly owned by the Permittee, the owner of the land, or the 0 200 0 lessee/operator of the land to be maintained as part of the project site Property lines 50 150 50 Public right of way 50 50 50 Private or public water supply 100 100 100 Surface waters (streams — intermittent and perennial, 100 100 50 perennial waterbodies, and wetlands Surface water diversions (ephemeral streams, 25 100 25 waterways, ditches Groundwater lowering ditches (where the bottom of 25 100 25 the ditch intersects the SHWT) Subsurface groundwater lowering system 0 100 0 Wells with exception to monitoring wells 100 100 100 Bedrock outcrops 25 25 25 Top of slope of embankments or cuts of two feet or 15 15 15 more in vertical height Building foundations or basements 0 15 0 Water lines 0 10 0 Swimming pools 100 100 100 Nitrification fields 0 20 0 In accordance with the Setback Waiver Agreement (FORM: SWA), the setback requirement may be reduced to a minimum of 100 feet upon written consent of the owner of the property until September 30, 2021 or until the owner sells the property, whichever comes first. [15A NCAC 02T .1108] 9. Land application areas shall be clearly marked on each site prior to and during any residuals application event. [15ANCAC 02T .0108(b)(1)] WQ0035595 Version 2.0 Shell Version 151201 Page 3 of 13 10. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http://nutrients.soil.ncsu.edu/yields/index.phhpl. A copy shall be kept on file and reprinted every five years in accordance with Condition IV.S. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (htip://www.ncapr.gov/SWC/tech/documents/9th Guidance Doc 100109.pddfl. iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards (ftp://ftp-fc.se.egov.usda.eov/NHO/practice-standards/standards/590.12df). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [15A NCAC 02T . 1 109(b)(1)(k)] 11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25% in accordance with the USDA-NRCS 590 Nutrient Management Standards. [15A NCAC 02T .0108(b)(1)] 12. If land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer and rye grass in the winter with both crops to receive residuals), then the second crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A NCAC 02T .0108(b)(1)] 13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall maintain written records of these recommendations and details of their implementation. [15A NCAC 02T .0108(b)(1)] WQ0035595 Version 2.0 Shell Version 151201 Page 4 of 13 14. These residuals land application sites were individually permitted on or after December 30, 1983; therefore, the compliance boundary is established at either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. An exceedance of groundwater standards at or beyond the compliance boundary is subject to remediation action according to 15A NCAC 02L .0106(d)(2) as well as enforcement actions in accordance with North Carolina General Statute 143-215.6A through 143-215.6C. Any approved relocation of the COMPLIANCE BOUNDARY will be noted in Attachment B. [15A NCAC 02L .0107(a)] 15. The review boundary shall be established midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at the review boundary shall require action in accordance with 15A NCAC 02L.0106. [15A NCAC 02L .0108] III. OPERATION AND MAINTENANCE REQUIREMENTS The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [15A NCAC 02T .1110] 2. The Raleigh Regional Office, telephone number (919) 791-4200, and the appropriate local government official (i.e., county manager, city manager, or health director) shall be notified at least 48 hours prior to the initial residuals land application to any new land application site. Notification to the regional supervisor shall be made from 8:00 a.m. until 5:00 p.m. on Monday through Friday, excluding State Holidays. [15A NCAC 02T .0108(b)(1)] 3. The Raleigh Regional Office shall be notified via email or telephone, (919) 791-4200, at least 24 hours prior to conducting any land application activity not owned or leased by the Permittee. Such notification shall indicate, at a minimum, the anticipated application times, field IDs, and location of land application activities. If it becomes necessary to apply to additional fields due to unforeseen events, the Regional Office shall be notified prior to commencing the application to those fields. [15A NCAC 02T .0108(b)(1)] 4. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; c. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; W00035595 Version 2.0 Shell Version 151201 Page 5 of 13 iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [15A NCAC 02T.1 1001 5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition III.4.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement Branch at (919) 707-9105. [15A NCAC 02T .0117] 6. When the Permittee land applies bulk residuals, a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. [15A NCAC 02T .1110] 8. Class B residuals listed in the most recently approved Attachment A of this permit shall not be stored at any land application site, unless written approval has been requested and received from the Division. [G.S. 143-215.1] 9. When the Permittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.1] 10. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved by the Division. [15A NCAC 02T .1109(b)(1)] WO0035595 Version 2.0 Shell Version 151201 Page 6 of 13 11. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100 -year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. If the soil pH is not maintained at 6.0 or greater, unless sufficient amounts of lime are applied to achieve a final soil pH of at least 6.0, or if an agronomist provides information indicating that the PH of the soil, residuals and lime mixture is suitable for the specified crop. Any approved variations to the acceptable soil pH (6.0) will be noted in this permit; i. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a no -till program shall be exempted from meeting this vegetative cover requirement; j. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; k. If the vertical separation of bedrock and the depth of residuals application is less than one foot; 1. Application exceeds agronomic rates. [15A NCAC 02T. 1109] 12. The following public access restrictions apply to residual land application sites: a. Public access to public contact sites (e.g., golf courses, parks, ball fields, etc.) shall be restricted for 365 days after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event. [15A NCAC 02T. 1 109(b)(2)] 13. For any fields contained in Attachment B that are not fenced, public access controls shall include the posting of signs with a minimum area of 3 square feet (e.g., 1.5' x 2'). Each sign shall indicate the activities conducted at each site, permit number, and name and contact information, including the Permittee or applicator's telephone number. Signs shall be posted in a clearly visible and conspicuous manner at the entrance to each land application site during a land application event, and for as long as the public access restrictions required under Condition Ill. 12. apply. [15A NCAC 02T .0108(b)(1)] W00035595 Version 2.0 Shell Version 151201 Page 7 of 13 14. The following harvesting and grazing restrictions apply to residual land application sites after each land application event: Harvesting and Grazing Description Restricted Duration Animals shall not be allowed to graze during land application activities and restricted period. Sites that are to be used for grazing shall have fencing to 30 days prevent access after each land application event. Food crops, feed crops and fiber crops shall not be harvested for: 30 days Turf grown on land where residuals have been applied shall not be harvested for: 12 months Food crops with harvested parts that touch the residual/soil mixture and are totally above the land surface (e.g., tobacco, melons, cucumbers, squash, etc.) 14 months shall not be harvested for: When the residuals remain on the land surface for four months or longer prior to incorporation into the soil, food crops with harvested parts below the land 20 months surface (e.g., root crops such as potatoes, carrots, radishes, etc.) shall not be harvested for: When the residuals remain on the land surface for less than four months prior to incorporation into the soil, food crops with harvested parts below the land 38 months surface shall not be harvested for: [15A NCAC 02T. 1 109(b)(3)] 15. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (VI/UP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. [15A NCAC 02T .0108(b)(1), 02T .1104(c)(3)] 16. No residuals shall be land applied unless the submitted Land Owner Agreement Attachment (LOAA) between the Permittee and landowners or lessees/operators of the land application site is in full force and effect. These agreements shall be considered expired concurrent with the permit expiration date, and shall be renewed during the permit renewal process. [15A NCAC 02T .1104(c)(4)] WQ0035595 Version 2.0 Shell Version 151201 Page 8 of 13 Lut 1. Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)] 2. Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)] shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1,4 -Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1, 1 -Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Heptachlor (and its hydroxide) (0.008) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5 -Trichlorophenol (400.0) in -Cresol (200.0) Lead (5.0) 2,4,6 -Trichlorophenol (2.0) o -Cresol (200.0) Lindane (0.4) 2,4,5 -TP (Silvex) (1.0) p -Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. [15A NCAC 13A .0102(b), 02T.1101, 02T.11051 W00035595 Version 2.0 Shell Version 151201 Page 9 of 13 3. An analysis shall be conducted on residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) [15A NCAC 02T.11011 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (c) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [ 15A NCAC 02T .1106, 02T .1107, 02T .1111(c)] 5. An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B on which a residuals land application event will occur in the respective calendar year. This analysis shall be in accordance with the "Guidance on Soil Sampling" located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website (hU://www.ncagr.gov/a/agronomi/pubs.httn). The Permittee shall maintain these results and a description ofthe sampling methodologies used to determine soil fertility for a period of no less than five years, and shall be made available to the Division upon request. At a minimum, the Standard Soil Fertility Analysis shall include the following parameters: Acidity Exchangeable Sodium Percentage Phosphorus Base Saturation (by calculation) Magnesium Potassium Calcium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH [15A NCAC 02T.0 1 08(c), 15A NCAC 02T. 1111 (d)] 6. Laboratory parameter analyses shall be performed on the residuals as they are land applied, and shall be in accordance with the monitoring requirements in 15A NCAC 0213 .0505. [15A NCAC 02B .0505] WO0035595 Version 2.0 Shell Version 151201 Page 10 of 13 7. The Permittee shall maintain records tracking all residual land application events. At a minimum, these records shall include the following: a. Source of residuals; b. Date of land application; c. Location of land application (i.e., site, field, or zone number as listed in Attachment B); d. Approximate areas applied to (acres); e. Method of land application; f Weather conditions (e.g., sunny, cloudy, raining, etc.); g. Predominant Soil Mapping Unit (e.g., CbB2); h. Soil conditions (e.g., dry, wet, frozen, etc.); i. Type of crop or crops to be grown on field; j. Nitrogen Application Rate based on RYES (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years); k. Volume of residuals land applied in gallons per acre, cubic yard per acre, dry tons per acre, or wet ton per acre; 1. Volume of animal waste or other nutrient source applied in gallons per acre, dry ton per acre, or wet tons per acre; in. Volume of soil amendments (e.g., lime, gypsum, etc.) applied in gallons per acre, dry ton per acre, or wet tons per acre; and n. Annual and cumulative totals in dry tons per acre of residuals as well as animal waste and other sources of nutrients (e.g., if applicable), annual and cumulative pounds per acre of each heavy metal (e.g., shall include, but shall not be limited to, arsenic, cadmium, copper, lead, mercury, molybdenum, nickel, selenium, and zinc), annual pounds per acre of PAN, and annual pounds per acre of phosphorus applied to each field. [15A NCAC 02T .0109(a)] 8. Three copies of an annual report shall be submitted on or before March 111. The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reportin Forms. orms. Instructions for reporting and annual report forms are available at bqR://portal ncdenr or¢/web/wq/gps/lau/reportine, or can be obtained by contacting the Land Application Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [15A NCAC 02T .I I I I(a)] W00035595 Version 2.0 Shell Version 151201 Page 11 of 13 V. VI. 9. Noncompliance Notification The Permittee shall report by telephone to the Raleigh Regional Office, telephone number (919) 791- 4200, as soon as possible, but in no case more than 24 hours or on the next working day following first knowledge of the occurrence of any of the following: a. Land application of residuals abnormal in quantity or characteristic. b. Any failure of the land application program resulting in a release of material to surface waters. c. Any time self-monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)] IPECTIONS The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [15A NCAC 02T .0108(b)] 2. Prior to each bulk residuals land application event, the Permittee or his designee shall inspect the residuals transport and application sites and equipment that are part of the event to identify and repair malfunctions, facility deterioration and operator errors that could result in discharges to the environment, be a threat to human health or create a public nuisance. The Permittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the land application sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)] GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals land application events are not carried out in accordance with the conditions of this permit. [15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G. S. 143-215.1] W00035595 Version 2.0 Shell Version 151201 Page 12 of 13 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [15A NCAC 02T .0105(c)(6)] 5. In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60 -day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T.0 110. [ 15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). [15A NCAC 02T.0 120] 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .0105(e)(3)] Permit issued this the 10' day of October 2016 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION F. Jay Zimmerman, P.G., Director Division of Water Resources By Authority of the Environmental Management Commission Permit Number WQ0035595 W00035595 Version 2.0 Shell Version 151201 Page 13 of 13 THIS PAGE BLANK A ci M N G1 O O N a ' R •^ R M M M M M N M M M M M M M M M M M M M M M 0 0 0 0 6 6 0 0 0 6 0 6 0 6 0 0 o c o 0 0 d C FQ CQ �Q CG Q C 0�A + 7 O ro O O O p id O a O O - O id O 7 a O 7� O 78 O 79 7 O N :z : o o :z o CIO UO U� U N bA .w Q u •L �j � •L CC u R i p wz� C C � E [.Qr O �n N O 00 O O in vi O O O O O O O O •� � � N 00 M � vl -In 00 ,W). M N '� N in CO `� Q Q •� .i V] V] Q MMQ � 1+N 00 00 00 N It W. 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N O Q N YJ 00 N M .N -.i z o 3 3 y U bq � O R W m U UID 0.1 [ 0 60 0003 y GQ CQ 0A 0A A O 3 O o O O v y Q Q z z > > cq O O N � F [_+ bA a N W E S '4 -.22 Net 4.69 Grins 14.61 Gross - � 4 1 2.66%Net • A• M1 DRED BAPTIST C►HURC►H 2 L99 Net 23.81 Gross 11.60 Gross THOMAS, JENNIE EDWiARDS 12.83 Net 3 . 22.50 Net THOMAS, JENNIE EDWARDS ti 17:90 Net 6 �.` THOMAS, JENNIE EDWt1R2 s Gross 2.54 Net k� t `. 9 ` a 4.86tGross� Legend 6.02 Net ETHERIiDGE, H M pR ,� 7 ■ House 2.35 Net JBs Group, Well Gross `�•` r40m 10 15.3 _____ = Dirt Road //� � 3.78 Gross Ditch 1.47 _{ Stream 4.74 Net 07/� Buffer 819 17 2.9 Field Boundary Pond — 500 250 0 5+19 Gross 500 Net 2951 Net' Net Area4 F ' t , •. 11.36 Net Scale: 1 inch equals 500 feet BUFFER MAP - FIELDS 1-4,6-7,13 & 1 Figure Drawn by: CSC SOIL New GFI Land Application Permit 1 Reviewed by: PLUS Tarboro, North Carolina Date: November'11 1 Soil Plus Project # 200705.C10 i 8 11.3G Na 31.70 Net Group, LLC VV S .3 F- 32.45 17 21 21.03 Gross p u // 7.64 Gross 18 22 10.40 \ct 322� Legend 14.39 Gross +r Net �a ■ House u l • Well 1S S Dirt Road Ditch 15 7.61 Gross MANNING, Jo' Stream Buffer Buffer JIBS Group, LLC Field Boundary Pond 500 250 0 500 Net Area F Scale: 1 inch equals 500 feet 0054^BUFFER MAP - FIELDS 11, 15,18,18,20 & 32 Figure Drawn by: CSC SOIL New GFI Land Application Permit Reviewed by: PLUS Tarboro, North Carolina 3 Date: November'11 1 Soil Plus Project # 200705.C10 N W E S 16.21 Net Ac. 17.28 Gross Ac. 16.791 Field 2 HURTFORD .03 et BROWN, NELLIE B 3 BROWN, NELLIE B 7.89 N Field 5 i/11 Legend House Well Dirt Road Ditch X— Fence Stream Buffer Field Boundary Pond \ = Property Boundary 400 200 0 400 17 © Net Area Fee raj DD BEACH Scale: 1 inch equals 400 feet —00 BUFFER MAP - EB 1- 2 Figure Drawn by: CSC East GFI Land Application Permit (WQ0035595) Reviewed by:4 �� Oak City, North Carolina 4 Date: March'13 Soil Plus Project # 200705.C10 N B BROWN, NELLIE B 9.18 Net Field 5 12.76 Gross Ac. BEA'C►II, JOHN LEE SR Field 3 8.74 Net Ac. 16.79 Gross Ac. r 12.84 Gross Ac., Field 4 i i i i i i i i i i i i i i i i BEACH, JOHN LEE SR 400 200 0 400 Feet f Legend House Well Dirt Road © Net Area Ditch X— Fence --� Stream Buffer Field Boundary Pond 0 Property Boundary Scale: 1 inch equals 400 feet 0054^USDA BUFFER MAP - EB 3 - 5 Figure Drawn by: CSC SOIL East GFI Land Application Permit (WQ0035595) Reviewed by: PLUS Oak City, North Carolina 5 Date: March'13 1 Soil Plus Project # 200705.C10 N W E S 4 >� V BROWN HELL BUNTING T 400 200 0 400 F Scale: 1 inch equals 400 feet Drawn by: CSC Reviewed by: Date: Oct. '12 G �; ow' Legend House Well Ditch Dirt Road Stream Buffer . Field Boundary © Net Area -x Pond BUFFER MAP - EB 6 Figure East GFI Land Application Permit (WQ0035595) SOIL North Carolina 6 $LUS Speed, Soil Plus Project # 200705.C10 W E S Legend House • Well Ditch - Stream [Application Boundary FA Buffer Field Boundary F7 Pond F7 Property Boundary 0 0 jFie1 2 6.44 C3r,777,Ac. 4.45 Net�Ac.c, The Compliance Boundary shall be located 50 feet within the property line or 250 feet from the edge of the disposal area, whichever is closer to the source. The Review Boundary shall be located halfway in between the property line and the Compliance Boundary. 400 200 0 400 Fe Scale: 1 inch = 400 feet PLUS FIELDS 1 & 2 BUFFER MAP Figure Drawn by: DM SOIL PLUS GFI Land App Permit (WQ0035595) Reviewed by: CSC Oak City, North Carolina 7 Date: May'16 Soil Plus Project # 200705.C10 N W E S Legend QApplication Boundary Buffer Ditch Field Boundary House Pond ElProperty Boundary 11- Stream • Well The Compliance Boundary shall be located 50 feet within the property line or 250 feet from the edge of the disposal area, whichever is closer to the source. The Review Boundary shall be located halfway in between the property line and the Compliance Boundary. Scale: 1 inch = 400 feet PLUS FIELDS 1-2 BUFFER MAP Figure Drawn by: DM SOIL PLUS GFI Land App Permit (WQ0035595) Reviewed by: CSC Wilson, North Carolina 8 Date: April '18 Soil Plus Project # 200705.C10 State of North Carolina Department of Environment and Natural Resources Division of Water Quality SETBACK WAIVER AGREEMENT ATTACHMENT For Land Application of Residual Solids (FORM: SWAA 10-06) (THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL) The Division of Water Quality (Division) will not accept this attachment unless all the instructions are followed. Failure to submit all required items will lead to additional processing and review time. For more information, visit our web site at:htW:: 'h2o.enr.slate.nc.us:7au main. himl INSTRUCTIONS TO THE APPLICANT: A. Attachment Form: ✓ - Do not submit this attachment form for review without its corresponding residuals program application form (FORM: NDRLAP 10-06). ✓ Any changes to this attachment form will result in the application package being returned. B. Prepare a separate attachment form for each property from which a waiver from 15A NCAC 2T .1108(b)(2)(for habitable residences or place of public assembly) is being sought. ✓ Any other setbacks required by 15A NCAC 2T .1108, other than those referenced above, cannot be waived through execution of this attachment form. ✓ A copy of the completed and appropriately executed attachment form must be provided 'to the property owner. AGREEMENT TO WAIVE THE SETBACK REQUIRED BY 15A NCAC 2T. I 108(b)(2)(habitable residences) The undersigned property owner hereby permits: Applicant's name: Granville Farms, Inc Complete mailing address of applicant: P.O. Box 1396 City: Oxford State: North Carolina Zip: 27565 Telephone number: (919) 690-8000 Facsimile number: (919) 690-1157 E-mail address: hereinafter referred to as the Permittee, to land apply residuals within 100 feet (i.e., cannot be less than 100 feet) of the residence or place of public assembly located at the following: Location address of property: 2141 Cannon Road City: Hobgood State: North Carolina Zip: 27843 This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for the residuals land application program and shall be renewed each time this permit is renewed. In addition, this Agreement shall only remain in effect for as long as the undersigned property owner owns the property described herein. The undersigned property owner agrees to abide by this Agreement until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. ❑ I certify that I am a deeded property owner of above -referenced property and am authorized to make decisions regarding this property on behalf of other deeded property owners. Furthermore, I certify that I have read and understand this Agreement and do hereby grant permission to the Permittee to land apply residuals to land application site(s) as specified herein. 011✓ �I Property owner name: annon Signaturd: �— Date: FORM: SWAA 10-06 Page 1 of 1 Attachment Order 3-d