WQ0010689_Residual Annual Report 2018_20190305

2/27/2019
Division of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: 2018 Annual Ash Report
Permit No. WQ0010689
Wood Boiler —.North Cove, NC
RECEIVEDfNCDEOJD'NR
MAR 5 2019
Non -Discharge
Permitting
Enclosed is the 2018 Annual Ash Distribution Report using the forms provided by NCDEQ-
DWQ. Included in this report is the following information:
- Class A Annual DMSDF and Supplemental Information
- Annual Residual Sampling Summary Form and Form-B
- Ash Distribution Landowner Utilization Agreements
- Lab Sheets
There were no permit deviations noted during the 2018 Reporting Year.
If you have any questions or require additional information, please contact myself at 828-756-
6636.
Sincerely
e;� OZ5��
Corey Carpentier
Attachments: Annual Ash Report (3 copies)
Cc: Rickey Styles
MAR 0 5 2019
D NR qrl-(, �i'ON
i irOR IIATIW RROCESSUG UHT
i
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

.CLASS A ANNUAL:DISTR. BUTION. AND MARKETING/ SURFACE DISPOSAL: CERTIFICATION AND SUMMARY. FORM
WQ PERMIT #: WQ0010689 '.FACILITY NAME: Baxter Healthcare. Corporation North Cove Steam Generation Plant Ash
-PHONE:: [phone] CO.i7NTY:.. McDowell OPERATOR: Baxter Healthcare
FACILITY TYPE (please check one): 0. Surface Disposal (complete Part A (Source(s) and :"Residual In" Volume only) and Part C).
R : Distribution and -Marketing (complete Parts A, B, and,C)
Was;the facility in-overation durine the east calendar vear? Yes 0 No ® --�*-if No skin nnrts A: R: (" and eprtifv frirm hPlnw
Part A*:
- - Part B*:
Month
Sources s include NPDES #.if
�) (
applicable)
Volume (drytons)
:
Recipient.Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)' .
Volume (dry tons)
Intended uses)
January -
February. ..
March'
WQ0010689
.120
538.2.
658.2 .
See DMSDF Supp. Form
538.2
Land Application:
April.
May
......
June. . .
July
August:
WQ0010689
120
624.9
744.91
See DMSDF Supp: Form
624.0
Land Application
September
October
November
December
WQ00.1:0689'
. 120
250.8
370:8
See DMSDF-Supp: Form
250.8
Land Application
Total from -FORM DMSDF
. • .. . 360 `
=1413:9..
1'773:9
1413:9 : • . •
:::::::..:.:...:.:.:.:...: :
Totals.,
Annual (dry:tons):.
, :' 360
:•141'39 : ' •
:: 177,3:9 .: '
;;:::::c::::::: ::::::::::::::::: : ::::: °
.............
: :. ' 1413.9
:......:..: , :.::..:..
Amendments used: None Bulking Agents used: Dry Wood Chi s.
* If more space.is required, attach additional'information sheets (FORM DMSDF (supp)): Total'Number: of.Form DMSDF (Supp) 1
Part C:
Facility.was compliant, during the past calendar. year. With all -conditions of the land application permit -R Yes
(including.but not limited to items 1-3 below) issued by,the Division -of Water Quality: ® No I, If No, -Explain' -In Narritive
1. All monitoring Was done in accordance with the permit and -reported for the"year as required and three (3) copies of certified laboratory results are attached:
2: All operation -and maintenance requirements were compiled with or, in.the case of.a deviation, prior authorization was received; from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify; under penalty of law, that the above. information is, to the best of my knowledge and belief, true, accurate and complete..I am aware -that there are significant
penalties for submitting false information, including the possibility of fines and'.imprisonmentfor knowing violations:"
Z_-'76
Siquire of Permittee Date Signa a of eparer** Date.
(if different'from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r).and 15A NCAC 2T .1102 (26)

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM[
Supplemental Information _
WQ PERMIT #: WQ0010689 FACILITY NAME: 'i� ',r :'- Baxter;Healthcare Co oration North;Cove:-Sfeam'Geneiatiori:Plarit_Ash` '
PHONE:','829-756-6636, COUNTY:;: ',MV D6.welF, � OPERATOR•, .B'ax dr:�He'alth°care
FACILITY TYPE (please check one): ® Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only)
0 Distribution and Marketing (complete Parts A, and B)
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry
tons)
Intended use(s)
March
WQ0010689
120.00
538.20
658.20
Kenneth Hughes, Max Holland,
Mark Cole, Jeff Baiiks,and Jim
Phillips
538.20
Land Application
August
WQ0010689
120.00
624.90
744.90
Brian McKinney, Dean McClure,
Keith Collins
624.90
Land Application
December
WQ0010689
120.00
250.80
370.80
Max Holland
250.80
Land Application
IF
Totals:
Annual (dry tons
3:60 :...
4 l 139.
;;19739='''
Amendment(s used:
Bulking Agent(s) used: Dry Wood Chips
* TfmnrP crlarr is rannin-d nttnf-h ne1r1itinnn1 infnrmn*inn el,aa*e ICi—N blolonnl2l 'P-4--1 AT„« U-- .cam T,%RoriU io____lli

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0010689 Laboratory:
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash
Residual Source WQ # or WQ0010689
NPDES #:
W ffP Name:
Residual Analvsis Data
NA
1) Pace Analytical Services
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m a
Sample
SP12618A
SP12618B
NP71819A
NP71819B
SP122118A
SP122118B
Percent Moisture (%)
NA
54.4
53.9
39.9
47.5
57.5
57.7
Arsenic
75
2.9
3.3
3.6
2.9
ND
ND
Cadmium
85
1
1
1.8
1.2
1.5
1.8
Copper
4,300
55.9
56.8
78.5
92
58
467
Chromium
NA
16.9
17.4
19.2
24.7
16.9
18.5
Lead
840
18.6
18.9
23.3
15
17.7
21.0
Mercury
57
ND
ND
ND
ND
ND
ND
Molybdenum
75
ND
ND
1.3
1.5
0.83
ND
Nickel
420
19
20
21.2
31.9
18.9
21.6
Selenium
100
ND
ND
ND
ND
ND
ND
Zinc
7,500
153
154
188
147
129
247
Total Phosphorus
NA
1010
1080
784
827
2240
1930
Barium
NA
1510
1310
1590
2670
1490
1750
Calcium
NA
68600
66500
91100
137000
73300
87300
Iron
NA
8900
9120
10500
20700
10700
10600
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature
_Z lq
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
MKKM "�MKA --^- i.ni -n

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - E
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0010689 Laboratory: 1) Pace Analytical Services
Baxter Healthcare Corporation North Cove
Facility Name: Steam Generation Plant Ash 2)
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
WQ0010689
W
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
SP12618A
SP12618B
NP71819A
NP71819B
SP122118A
SP122118B
Magnesium
10400
10600
15200
23200
10200
13400
Manganese
2330
2280
3520
4930
3670
3220
pH
8.9
8.8
9.3
9.3
10.8
11.4
Potassium
8990
9010
18800
34700
9970
12900
Silver
ND
ND
ND
ND
ND
ND
Sodium
2790
2810
6310
11300
4340
5320
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to ­ f j1g Y (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). ;Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle_
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
r Application of bulk residuals shall not occur within 100 feet of a public or private water supply
• A «spy of this Utilization Agreement shall be maintained at the. land.. application site when bulk residuals are
being applied.,
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10•1 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): Ay J/0 AAW/ Date: � � - 49
Ash Recipient's Address: �� �' f �� t c s,C �l.q 0)4 4 ,i✓! 4-> NC. ZOO 761
Intended Use of Ash: /—,,., 6
Expected Qty/Yr: jO //-� fin. 4 (� c f Lan 3 6 5J
Baxter Representative Signature:
Page 2 e3
Updated: 10-22-14

Baxter Healthcare, Corp
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport. Adequate provisions shall be taken to ensure that the transportation ofash. does -not- cause nuisances and
hazards,to.public health and-safetyorotheiwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spin occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill Control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
be controlled. runoff However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runocannot
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land),..
Ash." not be stockpiled for wore than 60 days prior to land application
'Application of -bulk residuals shall not occur within 100 feet of a public or private water supply
'.. b SPY of title Utilization Agreement shall be maintained at the land application. site when bulk residuals are
btu applied .. .
. -.Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, . save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury. (including death) -or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of I a ash.
Signed (Ash Recipient): Date:
Ash Recipient's Address: ).Z? Q/W 'ioAij C,eret
Intended Use of Ash: .5 e y l t5f /,fin r e fm -A _/_
Expected Qty/Yr: _ �� Acres of Land:
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

•
Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare,Corp.,is the generator of the ash provided to j jam//,ek (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation ofash.does-not-cause nuisances and-
•
_ hazards:to_:public health and-safety or otherwtse cause'an adverse impact(e.g.,transport wet ash in leak-proof trucks
or cover dry ash). Any spill occurring while ash is in transport or on the application fields is the responsibility of the
transporter. The transporter must keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms, barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the liming requirements of the crops being grown on the land).
• Ash shall not be stockpiled for more than 60 days prior to land application
Application of.bulk residuals shall not occur within 100 feet of a public or private water supply
• A copy of this Utilization Agreement shall be maintained at the land application site when bulk residuals are
being applied.
s . -Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense(including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death)-or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of e ash.
Signed(Ash Recipient): 4Ce,1 Date: '-
Ash Recipient's Address: ..,7.? Old '/c.as Gene t' ,
Intended Use of Ash: .S e f l .4i11 ri-L r e
Expected Qty/Xr: 6 0 XV, Acres of Land:
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19),, Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to
Application of the aforementioned ash is prohibited except in accor c th the instructions on this sheet.
Recipient).
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Any spin Occuffin& while ash is in trap
ftMWVMW' The trMpotr mtest th sport or the application fields is the responsibility of the
keep spill control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically -justified (i.e., limited to that needed
' to meet the liming requirements of the crops being grown on the land).
aN".raoE.lpa.OQW*" for more than 60 days to land application
zls shall not ooanr within 100 feet of a public or private water supply
* A4VV oi'" LWOOM Apeem g Shall be maintained at the land I�lp application ate when bulls residuals are
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient):
Date:
Ash Recipient's Address:
f Ott'
Intended Use of Ash: /
Expected Qty/Yr:_16e�'_ ON
Acres of Land:
Baxter Representative Signature;_
Page 2 of 3
47 AW Ae ZC7.r
Updated: 11-07-14

- - Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to ,� (Recipient).
Application of the aforementioned ash is prohibited except in acco ce with the iffitructi on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dryash) . In transport or on the application fields is the re§0664006tlbe
ttanspt " 3 " Drier ell provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
:aka public or private water supply
ai =iaite when bulk dais are
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10' centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other }ise of the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr.Q� / 8/5 Acres of Land: / /©
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14
ON
13,61

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to AX 0 1 �/� ,ram
Application of the aforementioned ash is prohibited except in accordance with�tru� *instructions on �r Went).
Transport:' Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). Atit mill occptring while ash is in transport or on the application fields is the teV0rAibility of the
-k0M4WW. Tlw UADVMW WIM. keep Will control provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
not In.WWWW *we Oft 60 d"m prim to land appheation
i � s of is s l not occur within 100 feet of a public or private water supply
#��-W'" Wig Agmenam shall be maintained at the land application site when bulk residuals are
mod.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): ( rid P14A_(,!?,_� Date:
Ash Recipient's Address: (aW JJE(Q K AJ0 /3 � !�
Intended Use of Ash: &t_
Expected Qty/Yr: �� — 5cx� 4,r- 0tj Acres of Land: Q7
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to r i' &,10 M �yi /1 t i cY (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions onthis sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). transport or on the application fields is the rasp ate
160
. mum e1 provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
oii pftr. or private water supply
at 'site when bulk residuals are
Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
It I L V
Signed (Ash Recipient): i ' 1 = Date:_
Ash Recipient's Address: /1 %1,g�
Intended Use of Ash:
Expected Qty/Yr: J O �� `f on QGir Acres of Land:
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided tp Q-u i't'I G
Application of the aforementioned ash is prohibited except in accidacfce with the instruction s sheet.
Recipient).
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). opwxmg while ash is in Uwviport or on application fields is e
Mot *U cc of the of the
_
provisions on the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
. 40MAW 6 *3'6 PdOr to IWO Opplication
i�� i=VM of d 100 feet of a public or private water supply
Apoemt shedi be mawtamed at the land application site when bulk residuals are
lwii41d
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
Signed (Ash Recipient): ). - - Date: C
Ash Recipient's Addr
Intended Use of Ash:
Expected Qty/Yr: L-/ D Q Acres of Land: 6 0
Baxter Representative Signature:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare,Corp., is the generator of the ash provided to .F74>41A ( //,
Application of the aforementioned ash is prohibited except in accordance with the instructions onthis (Recipient).
sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact(e.g.,transport wet ash in leak-proof trucks
or cover dry ash). A cpig Occurring while ash is in transport or on the application fields is the
r The AnilkirefrOcr*pit p control provisions on the vehicle. responsibility of the
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land). _
a 4imin 60 days prior to land application
l not occur within 100 feet of a public or private water supply
• A n Agreement shall be maintained at the land application site when bulk residuals are
kilititateinit
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of the ash.
1
Signed(Ash Recipient): Date: S>- 3 - 18
1, t
Ash Recipient's Address: /2 CV e.--Oghs P414/7 Wets ',c e r7'7
Intended Use of Ash: 50, L ,-,if, tc-144 E„`(
Expected Qty/Yr: aS0 i (y jL Acres of Land: L C C.) o _
Baxter Representative Signature: 0
Page 2 of 3

U.
Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19) Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to ,'
Application of the aforementioned ash is prohibited except in accor c th the instructions on this sheeRecipient).
t.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact(e.g.,transport wet ash in leak-proof trucks
or cover dry ash). Any spill occurring while ash is in trap
!transporter must keep spill control transport the application fields is the responsibility of the
provisions onn the vehicle.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers, or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
*atikitatietbeitteeksiled for more than 60 days prior to laird application
A on of�.�
..:. not occur within 100 feet of a public private water supply
. op. nt shall be maintained at the.land
application site when bulb residuals are
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request. _
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of the ash.
Signed(Ash Recipient): S
Date: •- �"
Ash Recipient's Address:
idle- OW/WV Xe erxr,
Intended Use of Ash: + N 2 d c 4 <
Expected Qty/Yr: _ /O 2 FZ o._____^/
Acres of Land: A5/4"
Baxter Representative Signature; "'` 4 j�
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion,North Carolina 28752
Ash Distribution Utilization Agreement(Valid thru 11/30/19), Baxter Copy •
Baxter Healthcare,Corp.,is the generator of the ash provided to . /' (Recipient).
Application of the aforementioned ash is prohibited except in ce with the instructi - on this sheet.
Transport:Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact(e.g.,Jransport wet ash m leak-proof trucks
.R � _ _ ..�./..-. €.ST"-�,`.Sf�i3� ,�i�'J�, }'�,p� f4S5a.leak-proof
:_,+Ff Sr.
or cover ash). j (t;�'-or i�,p` YD +iO t i i t t 9 5 .:c,
. xf
'�1
... ::.,.-._.: ...Y vd51On9,:OI1� iVel11ae
-- _
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the liming requirements of the crops being grown on the land).
y ."+7 1 5 f t l 9 i. lsJ 1^(R L Y 0l]„#. ))9 tl Vn
.. yogis " '' - "'% {4 t�`°f5 fix) R.'SY4.•r%€ 4.; !.
7id.«3.-.a'- 4w �z 3..,,k 3t,. 1I4�.'� -i i .+,... .. .:s_ ... ...:.,. ....r...-n ...... '."vr^.u+Z
# tom..;�... r �.,.r v -. .. � ,
• •Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 104 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof Thereafter,Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third patty for any spill,.
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage,loss, cost,expense(including attorneys' fees),claim,demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp,by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other • of the ash.
_
Signed(Ash Recipient): A , ,: ,, ,.. .! . .,, -_, Date: j JI' J c
Ash Recipient's Address: /451 #01:2712'A4 /A/) _S�opvL p_ �n�. 4e 6,*
Intended Use of Ash: , 0;/ J 17? ,.i
Expected Qty/Yr. 3D Q 7145 Acres of Land: I/t
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752 .
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare,Corp.,is the generator of the ash provided to Ajeie 7%/y(5
Application of the aforementioned ash is prohibited except in accordance with the instructions on this s sheet.egpient).
Transport:'Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact(e.g.,transport wet ash in leak-:roof trucks
or cover ash), -•
dry ash). 4ny ?jp w nng while s_•th is>i ,transport.or.oin,the,.applic_ation Acids.is the. ; r
tbe
O* stilgltG011tOl YlslQns
P� on:the'.vehiale.
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply: •
• The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the i limng requirements of the crops beingthe 1
;�,..; ... . grown on and).
r,}.1�� 1 at on
�'�� �^' 'F'. t'f.. ,:�.. r.✓�.d'�.�^,s?;.:'�.'1`c-i71��'y`�..' '..:}:. .� r.rCYM;,!!ac+,✓fi
oc a.pub private water supply
. :r a rt3 �V :,•..,:::t Coif t�litl'1' 3, ee�iQ€' I.".Or
A M4;;; ,� "..._. _,_... lication site bulk
->y �t:s�itill,. �d4a�� d.� wlieii..^. residuals-are
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and oderlain by a
liner with a maximum hydraulic conductivity of 10 centimeters per second. If such a liner/cover i$provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense(including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of the ash.
Signed(Ash Recipient): U(lf Pott....L Date: 2/2 0/,24'
Ash Recipient's Address: Gustice Poo
Intended Use of Ash: A-6 e( CL4 L Ke
Expected Qty/Yr: /D0—50C) 17260 Acres of Land: et
Baxter Representative Signature:
Page 2 of 3
Updated: 11-07-14

•
Baxter Healthcare, Corp.
2859 Old Linville Road
Marion,North Carolina 28752
Ash Distribution Utilization Agreement(Valid thru 11/30/19), Baxter Copy
r G
Baxter Healthcare,Corp.,is the generator of the ash provided to $r-(oel (% i.n r1 (Recipient).
Application of the aforementioned ash is prohibited except in accordance with the instructions on This sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and or otherwise cause an adverse impact(e.g.,transport wet ash m leak a f trucks
or cover as ash 4 r a s f c a "u �r �a ... _ . .. c elds• s the i sr ,
$ OYEbToYLle ^FI �$Qn`fl ,
Y i „P ,z D t t:� 141E �y�v mops. pi we vemere ...
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,bathers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the liming requirements of the crops being grown on the land).
ads r a s x Leta t o t_c % 60 as�4 0.1:M ae Yin rhea ton
5e.' O 4 eAr i� lFs'F�' ..ap i! 7�.r'�r �b i F g� _4?'3 As 0 H i 1a
ss�te�� -VA
nl y G Tr
A: .a>s. .. .... tY i.r,7y rf'ate . .y
s�- e)i �ry
• 'Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare,Corp to Recipient upon delivery thereof Thereafter,Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,.
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability,damage, loss, cost,expense (including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
.bodily injury (including death) or damage to property, arising from or in connection with Recipient's,receipt,
transportation,handling or other use of the ash. •
Signed(Ash Recipient): pitiein1 H e. ��"� Date:
trVN���� ^ f
Ash Recipient's Address: C✓1//of) �d /Ott GY/)•
0
Intended Use of Ash: 60,! 6416i1 C.lle/
Expected Qty/Yr: I9C� i v() Rt yet/ Acres of Land: ( 00
Baxter Representative Signature:
Page 2 of 3
•
Updated: 11-07-14

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion,North Carolina 28752
Ash Distribution Utilization Agreement(Valid thru 11/30/19), Baxter Copy •
Baxter Healthcare,Corp., is the generator of the ash provided t ir11, (Recipient).
Application of the aforementioned ash is prohibited except in acco ce with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impr'ct(e.g.,transport wet ash in leak-proof trucks
or cover dry ash). r4 _:: g,K,} ash s '. port o n the a on flgilds is the
:- j �s r.o applic ti responsibility of
' 4_ n is i#1 pt►i p#.evisio is on_tli ,vdhicie.
•Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application:When using ash,the following shall apply:
• • The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the limingrequirements of the
, { _ce. equir the crops being grown on land). •
'` I,tsibi 1 $ lieation
aA`y!',Y`.,:i?, '•,{ q.;:-:F•'S.e.. +C+iF o
;:, •
, ._. t' `1OE••feat;of:•a;publte.orpriva • supply
7 .. .,� ,-rt ._.. tewSter
•
A o shall be•: ntained- Vtho•land'apphcatttm•site when' •° .
�i '�are
• Ash shall not be placed within one foot of the seasonal high water table.
•
•• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of le centimeters per second. If such a liner/cover is provided,
ash shall not be placed'within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter,Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of the ash.
Signed(Ash Recipient): � �wt��! -s— Date: i f / / /
Ash Recipient's Address: 7 3$ C.i.
Intended Use of Ash: , _
Expected Qty/Yr: D 0 Acres of Land: 20 0
Baxter Representative Signature:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road ,
Marion,North Carolina 28752
Ash Distribution Utilization Agreement(Valid thru 11/30/19), Baxter Copy
Baxter Healthcare,Corp., is the generator of the ash provided to 744t9 4 Ca//hi (Recipient). -
Application of the aforementioned ash is prohibited except in accor ce with the instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact(e.g.,transport wet ash in leak-proof trucks
or cover dry ash). '' ' �'� ' `- �� ' •
over i;,_ ;*`as sou transport°oron1. ,application fields is the responsibility-ofthe
'> ` = "` It tr00 s,o4`the lticle:
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However,berms,barriers,or tarps,may be necessary under windy or rainy conditions or if erosion or rtinoff cannot
be controlled.
Application:When using ash,the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified(i.e.,limited to that needed
to meet the liming requirements of the crops being grown on the�,$�.� �; land).
' €,' ; ,, , L u# ]q0 tet: ag c or.prvate Wine sppijft 1� _
If`a jw •^ 43 AA{��+,},�{{}yyj�'i�^ (3ri site i��y�rink}ps} [YIs alp
"�r � A.Fly?{P-'17Y�'avV►�.,vT�rw`:';fiF�V
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10"6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded,frozen,or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare,Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense(including attorneys' fees), claim, demand, suit, action,judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation,handling or other use of the ash.
Signed(Ash Recipient)` Date: F' 3 - 18
Ash Recipient's Address: /2 00 (.2-0 is P41 y Wete ive z r74/
Intended Use of Ash: 50, L .4, ,c144 E„Y
Expected Qty/Yr: )go T l y 1L Acres of Land: LC)C.) ,,�_ •
Baxter Representative Signature:
Page 2 of 3

Baxter Healthcare, Corp.
2859 Old Linville Road
Marion, North Carolina 28752
Ash Distribution Utilization Agreement (Valid thru 11/30/19), Baxter Copy
Baxter Healthcare, Corp., is the generator of the ash provided to �/� - ctJ fX
Application of the aforementioned ash is prohibited except in accordance with the instructions on this ss h sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and
hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leak -proof trucks
or cover dry ash). A py whine ash is in ftAnspoil or on tiro application fields is the
3*M poi provisions on the vehicle. responsibility of the
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any
surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions.
However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot
be controlled.
Application: When using ash, the following shall apply:
• The ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed
to meet the liming requirements of the crops being grown on the land).
'ik sty ti 60 days prior to land application
' a sal 10 occur within 100 feet of a public or private water supply
• A � 'U4 i of *istion meat shall be maintained at the l&ad applicarion site whey bulkresiduals are
Via•
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a
liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided,
ash shall not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results
are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter
Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for any spill,
misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being
delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore,
Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all
liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery
asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for
bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt,
transportation, handling or other use of the ash.
t -
Signed (Ash Recipient) Date: 0 - 3 - 1 S
Ash Recipient's Address: /,? OU ��'ns &M� y lVie�,►
Intended Use of Ash: $c , (_
Expected Qty/Yr: cJ IL Acres of Land: %c> c) At
Baxter Representative Signature:
Page 2 of 3

1aceAna1j&a(
wvvw.pace/aps.com
February 08, 2018
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
RECMM/NCCEQ0VM
MAR 0 4 2019
Water ci!,,Iity
Regional Operations Section
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on January 26, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
��Q pCtRF���cn
2 C
�'46nnst0�,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 29

acmflalytical
www.pacelabs.com
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L-A-B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification #: PH-0694
Delaware Certification
Florida/TNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DEQ/TNI Certification #: 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA110028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Montana Certification #: Cert 0082
Nebraska Certification #: NE-05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/TNI Certification M 2976
New Jersey/TNI Certification M PA 051
New Mexico Certification M PA01457
New York/TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
Pennsylvania/TNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/fNI Certification M T104704188-14-8
Utah/TNI Certification #: PA014572015-5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT-0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 460198
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification #: 8TMS-L
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification M 40
South Carolina Certification M 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 29

laneAnalytical
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite too
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Wood BoilerASh 1/25
92371068
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92371068001
SP12618A
EPA 6010
SH1
17
PASI-A
EPA 6010
SH1
7
PASI-A
EPA 7470
WAB
1
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 1010
ECH
1
PASI-A
EPA 9045
KMM
1
PASI-A
EPA 365.1
AES2
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM4500S2F-00
PAS
1
PAS[ -PA
92371068002
SP12618B
EPA 6010
SH1
17
PASI-A
EPA 6010
SH1
7
PASI-A
EPA 7470
WAB
1
PASI-A
EPA 7471
WAB
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 1010
ECH
1
PASI-A
EPA 9045
KMM
1
PASI-A
EPA 365.1
AES2
1
PASI-A
EPA 9014
PAS
1
PAS[ -PA
SM4500S2F-00
PAS
1
PAS[ -PA
92371068003
Test I
ASTM D2974-87
KDF
1
PASI-C
ASTM D5468-02
MJP
1
PASI-A
92371068004
Test 213
ASTM D2974-87
KDF
1
PASI-C
ASTM D5468-02
MJP
1
PASI-A
92371068005
Test 3C
ASTM D2974-87
KDF
1
PASI-C
ASTM D5468-02
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 29

aoeAnalytical
Wm..pacelabs.com
ANALYTICAL RESULTS
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP12618A Lab ID: 92371068001 Collected: 01/26/18 08:45 Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
2.9
mg/kg
2.2
1
02/01/18 02:15
02/07/18 13:19
7440-38-2
Barium
1270
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7440-39-3
Cadmium
1.0
mg/kg
0.22
1
02/01/18 02:15
02/07/18 01:35
7440-43-9
Calcium
68600
mg/kg
108
5
02/01/18 02:15
02/07/18 13:48
7440-70-2
Chromium
16.9
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7440-47-3
Copper
56.9
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7440-50-8
Iron
8900
mg/kg
21.5
1
02/01/18 02:15
02/07/18 13:19
7439-89-6
Lead
18.6
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7439-92-1
Magnesium
10400
mg/kg
21.5
1
02/01/18 02:15
02/07/18 01:35
7439-95-4
Manganese
2330
mg/kg
5.4
5
02/01/18 02:15
02/07/18 13:48
7439-96-5
Molybdenum
ND
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7439-98-7
Nickel
19.0
mg/kg
1.1
1
02/01/18 02:15
02/07/18 01:35
7440-02-0
Potassium
8990
mg/kg
1080
1
02/01/18 02:15
02/07/18 01:35
7440-09-7
Selenium
ND
mg/kg
2.2
1
02/01/18 02:15
02/07/18 01:35
7782-49-2
Silver
ND
mg/kg
1.1
1 ,
02/01/18 02:15
02/07/18 01:35
7440-22-4
Sodium
2190
mg/kg
1080
1
02/01/18 02:15
02/07/18 01:35
7440-23-5
Zinc
153
mg/kg
2.2
1
02/01/18 02:15
02/07/18 01:35
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method:
EPA 3010A
Leachate Method/Date:
EPA 1311; 01/27/18
16:30
Initial
pH: 9.5; Final pH: 6
Arsenic
ND
mg/L
0.050
1
01/28/1816:30
01/30/1816:52
7440-38-2
Barium
5.6
mg/L
0.25
1
01/28/1816:30
01/30/1816:52
7440-39-3
Cadmium
ND
mg/L
0.0050
1
01/28/1816:30
01/30/1816:52
7440-43-9
Chromium
ND
mg/L
0.050
1
01/28/1816:30
01/30/1816:52
7440-47-3
Lead
ND
mg/L
0.025
. 1
01/28/1816:30
01/30/1816:52
7439-92-1
Selenium
ND
mg/L
0.10
1
01/28/1816:30
01/30/1816:52
7782-49-2
Silver
ND
mg/L
0.025
1
01/28/1816:30
01/30/1816:52
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Leachate Method/Date: EPA 1311; 01/27/18
16:30
Initial pH: 9.5; Final pH: 6
Mercury
ND
mg/L
0.00020
1
01/28/1819:37
01/30/1816:31
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method:
EPA 7471
Mercury
ND
mg/kg
0.012
1
01/28/1819:37
02/01/1819:16
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
54.4
%
0.10
1
01/30/18 11:25
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200
deg F
70.0
1
01/29/18 09:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.9
Std. Units
0.10
1
01/27/18 03:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 4 of 29

I
aconAnalytical
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ANALYTICAL RESULTS
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP12618A Lab ID: 92371068001 Collected: 01/26/18 08:45 Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 1010 mg/kg 40.7 10 02/02/18 20:04 7723-14-0
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 2.2 1 02/01/18 20:02 02/02/18 02:03
734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 21.9 1 02/01/18 20:02 02/02/18 01:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 29

aceAnalj&oal
www.pacelabs.com
ANALYTICAL RESULTS
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
- [phone]
Sample: SP12618B Lab ID: 92371068002 Collected: 01/26/18 08:45 Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
3.3
mg/kg
1.9
1
02/01/18 02:15
02/07/18 13:22
7440-38-2
Barium
1310
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7440-39-3
Cadmium
1.0
mg/kg
0.19
1
02/01/18 02:15
02/07/18 01:51
7440-43-9
Calcium
66500
mg/kg
93.5
5
02/01/18.02:15
02/07/1813:51
7440-70-2
Chromium
17.4
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7440-47-3
Copper
66.8
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7440-50-8
Iron
9120
mg/kg
18.7
1
02/01/18 02:15
02/07/18 13:22
7439-89-6
Lead
18.9
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7439-92-1
Magnesium
10600
mg/kg
18.7
1
02/01/18 02:15
02/07/18 01:51
7439-95-4
Manganese
2280
mg/kg
4.7
5
02/01/18 02:15
02/07/18 13:51
7439-96-5
Molybdenum
ND
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7439-98-7
Nickel
20.0
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7440-02-0
Potassium
9010
mg/kg
935
1
02/01/18 02:15
02/07/18 01:51
7440-09-7
Selenium
ND
mg/kg
1.9
1
02/01/18 02:15
02/07/18 01:51
7782-49-2
Silver
ND
mg/kg
0.94
1
02/01/18 02:15
02/07/18 01:51
7440-22-4
Sodium
2810
mg/kg
935
1
02/01/18 02:15
02/07/18 01:51
7440-23-5
Zinc
154
mg/kg
1.9
1
02/01/18 02:15
02/07/18 01:51
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 'Preparation Method:
EPA 3010A
Leachate Method/Date: EPA 1311; 01/27/18 16:30
Initial
pH: 9.5; Final pH: 5.5
Arsenic
ND
mg/L
0.050
1
01/28/1816:30
01/30/1816:55
7440-38-2
Barium
5.2
mg/L
0.25
1
01/28/1816:30
01/30/1816:55
7440-39-3
Cadmium
ND
mg/L
0.0050
1
01/28/1816:30
01/30/1816:55
7440-43-9
Chromium
ND
mg/L
0.050
1
01/28/1816:30
01/30/1816:55
7440-47-3
Lead
ND
mg/L
0.025
1
01/28/1816:30
01/30/1816:55
7439-92-1
Selenium
ND
mg/L
0.10
1
01/28/1816:30
01/30/1816:55.
7782-49-2
Silver
ND
mg/L
0.025
1
01/28/1816:30
01/30/1816:55
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method:
EPA 7470
Leachate Method/Date: EPA 1311; 01/27/18 16:30
Initial
pH: 9.5; Final pH: 5.5
Mercury
ND
mg/L
0.00020
1
01/28/1819:37
01/30/1816:33
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method:
EPA 7471
Mercury
ND
mg/kg
0.011
1
01/28/1819:37
02/01/1819:18
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
53.9
%
0.10
1
01/30/18 11:37
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200
deg F
70.0
1
01/29/18 09:30
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
8.8
Std. Units
0.10
1
01/27/18 03:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 29

aceAnalytical
www.pacelabsmm
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Sample: SP12618B Lab ID: 92371068002 Collected: 01/26/18 08:45 Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
366.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus _ 1080 mg/kg 29.3 10 02/02/18 20:04 7723-14-0
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 2.2 1 02/01/18 20:02 02/02/18 02:03
734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 21.5 1 02/01/18 20:02 02/02/18 01:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 29

V aceAnalyiical
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ANALYTICAL RESULTS
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Test 1A
Lab ID: 92371068003 Collected: 01/25/18 15:00
Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
46.2 . % 0.10 1
01/30/18 11:37
ASTM D5468-02 BTU
Analytical Method: ASTM D5468-02
British Thermal Units
4310 BTU/lb 50.0 1
02/07/18 10:42 D6,N2
Date: 02/08/2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written'consent of Pace Analytical Services, LLC.
Page 8 of 29

aceAnalytical
'www.pacelabs.Com
ANALYTICAL RESULTS
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Test 2B Lab ID: 92371068004 Collected: 01/25/18 15:00 Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 46.4 % 0.10 1 01/30/18 11:37
ASTM D5468-02 BTU Analytical Method: ASTM D5468-02
British Thermal Units 4450 BTU/lb 50.0 1 02/07/18 10:42 N2
Date: 02/,08/2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 29

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Test 3C
Lab ID: 92371068005 Collected: 01/25/18 15:00
Received: 01/26/18 11:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF
Prepared Analyzed CAS No. Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
43.3 % 0.10 1
01/30/18 11:38
ASTM D5468-02 BTU
Analytical Method: ASTM D5468-02
British Thermal Units
6000 BTU/lb 50.0 1
02/07/18 10:42 N2
Date: 02/08/2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 29

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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 395790 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 2194122 Matrix: Water
Associated Lab Samples: 92371068001, 92371068002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 01/30/1814:27
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 10o
Huntersville, NC 28078
[phone]
METHOD BLANK: 2194124
Matrix: Water
Associated Lab Samples: 92371068001, 92371068002
Blank
Reporting
Parameter
Units
Result
Limit Analyzed Qualifiers
Mercury
mg/L
ND 0.00020 01/30/18.14:31
LABORATORY CONTROL SAMPLE:
2194123
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
Mercury
mg/L
.0025
0.0023 90 80-120
LABORATORY CONTROL SAMPLE: 2194125
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/L 0025 0.0024 98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2194126 2194127
MS MSD
92371098002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Mercury mg/L ND .0025 .0025 0.0025 0.0026 100 103 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 29

acmnalytical
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Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 395794
QC Batch Method: EPA 7471
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 2194136
Associated Lab Samples: 92371068001, 92371068002
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 02/01/1818:57
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2194137
Spike LCS LCS % Rec
Parameter Units Conc.. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.073 88 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2194138 2194139
MS MSD
92371076008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.028 .068 .068 0.068 0.091 59 94 75-125 30 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 396227 - Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 2196682
Associated Lab Samples: 92371068001, 92371068002
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result
Reporting
Limit
Analyzed
ND
1.0
02/07/1813:00
ND
0.50
02/07/18 01:17
ND
0.10
02/07/18 01:17
ND
10.0
02/07/1813:00
ND
0.50
02/07/18 01:17
ND
0.50
02/07/18 01:17
ND
10.0
02/07/1813:00
ND
0.50
02/07/18 01:17
ND
10.0
02/07/18 01:17
ND
0.50
02/07/18 01:17
ND
0.50
02/07/18 01:17
ND
0.50
02/07/18 01:17
ND
500
02/07/18 01:17
ND
1.0
02/07/18 01:17
ND
0.50
02/07/18 01:17
ND
500
02/07/18 01:17
ND
1.0
02/07/18 01:17
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2196683
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
48.5
97
80-120
Barium
mg/kg
50
51.7
103
80-120
Cadmium
mg/kg
50
45.9
92
80-120
Calcium
mg/kg
500
478
96
80-120
Chromium
mg/kg
50
46.9
94
80-120
Copper
mg/kg
50
47.6
95
80-120
Iron
mg/kg
500
473
95
80-120
Lead
mg/kg
50
43.6
87
80-120
Magnesium
mg/kg
500
451
90
80-120
Manganese
mg/kg
50
43.9
88
80-120
Molybdenum
mg/kg
50
47.5
95
80-120
Nickel
mg/kg
50
46.5
93
80-120
Potassium
mg/kg
500
ND
96
80-120
Selenium
mg/kg
50
41.6
83
80-120
Silver
mg/kg
25
23.0
92
80-120
Sodium
mg/kg
500
506
101
80-120
Zinc
mg/kg
50
42.4
85
80-120
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2196684
2196685
MS
MSD
92371024001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
<0.97
48.7
47.8
41.9
42.7
84
87
75-125
2
Barium
mg/kg
88.9
48.7
47.8
143
133
111
92
75-125
7
Cadmium
mg/kg
<0.097
48.7
47.8
40.4
41.1
83
86
75-125
2
Calcium
mg/kg
1620
487
478
2240
2030
127
86
75-125
10 M1
Chromium
mg/kg
18.5
48.7
47.8
65.9
64.3
97
96
75-125
2
Copper
mg/kg
16.4
48.7
47.8
67.6
62.3
105
96
75-125
8
Iron
mg/kg
16100
487
478
20300
16500
866
96
75-125
20 E,M1
Lead
mg/kg
5.2
48.7
47.8
41.0
43.4
73
80
75-125
6 M1
Magnesium
mg/kg
2090
487
478
2770
2330
140
50
75-125
17 M1
Manganese
mg/kg
86.8
48.7
47.8
142
145
114
123
75-125
2
Molybdenum
mg/kg
1.3
48.7
47.8
38.1
38.5
76
78
75-125
1
Nickel
mg/kg
8.3
48.7
47.8
50.9
49.4
88
86
75-125
3
Potassium
mg/kg
<486
487
478
710
695
96
95
75-125
2
Selenium
mg/kg
2.4
48.7
47.8
37.7
38.2
73
75
75-125
1 M1
Silver
mg/kg
<0.49
24.3
24
21.1
21.4
87
89
75-125
1
Sodium
mg/kg
<486
487
478
485J
494
92
96
75-125
Zinc
mg/kg
15.3
48.7
47.8
54.1
54.0
80
81
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
QC Batch: 395789 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92371068001, 92371068002
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 106
Huntersville, NC 28078
[phone]
METHOD BLANK: 2194116
Matrix: Water
Associated Lab Samples:
92371068001, 92371068002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/30/1815:41
Barium
mg/L
ND
0.25
01/30/1815:41
Cadmium
mg/L
ND
0.0050
01/30/1815:41
Chromium
mg/L
ND
0.050
01/30/1815:41
Lead
mg/L
ND
0.025
01/30/1815:41
Selenium
mg/L
ND
0.10
01/30/1815:41
Silver
mg/L
ND
0.025
01/30/1815:41
METHOD BLANK: 2194118
Matrix: Water
Associated Lab Samples:
92371068001, 92371068002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/30/1816:04
Barium
mg/L
ND
0.25
01/30/1816:04
Cadmium
mg/L
ND
0.0050
01/30/1816:04
Chromium
mg/L
ND
0.050
01/30/1816:04
Lead
mg/L
ND
0.025
01/30/1816:04
Selenium
mg/L
ND
0.10
01/30/1816:04
Silver
mg/L
ND
0.025
01/30/1816:04
LABORATORY CONTROL SAMPLE:
2194117
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2.5
2.5
100
80-120
2.5
2.3
93
80-120
2.5
2.4
97
80-120
2.5
2.4
98
80-120
2.5
2.3
92
80-120
2.5
2.5
99
80-120
1.2
1.2
99
80-120
Qualifiers
LABORATORY CONTROL SAMPLE: 2194119
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Arsenic mg/L 2.5 2.4 98 80-120
Barium mg/L 2.5 2.4 96 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
LABORATORY CONTROL SAMPLE:
2194119
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Cadmium
mg/L
2.5
2.4
97
80-120
Chromium
mg/L
2.5
2.4
98
80-120
Lead
mg/L
2.5
2.4
95
80-120
Selenium
mg/L
2.5
2.5
100
80-120
Silver
mg/L
1.2
1.2
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2194120
2194121
MS
MSD
92371098001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.4
2.4
97
97
75-125
1
Barium
mg/L
1.5
2.5
2.5
3.7
3.8
90
94
75-125
3
Cadmium
mg/L
ND
2.5
2.5
2.4
2.4
94
94
75-125
0
Chromium
mg/L
ND
2.5
2.5
2.4
2.4
95
95
75-125
0
Lead
mg/L
ND
2.5
2.5
2.2
2.2
89
89
75-125
0
Selenium
mg/L
ND
2.5
2.5
2.4
2.4
97
96
75-125
1
Silver
mg/L
ND
1.2
1.2
1.2
1.2
96
96
75-125
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 395862 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92371068001
SAMPLE DUPLICATE: 2194471
92371076003 Dup
Parameter Units Result Result
Percent Moisture % 14.5 14.6
SAMPLE DUPLICATE: 2194472
92371101001 Dup
Parameter Units Result Result
Percent Moisture % 18.8 19.7
RPD Qualifiers
1
RPD Qualifiers
5
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 29

aceAn4dkal
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QUALITY CONTROL DATA
Project: Wood Boiler ASh 1/25
Pace Project No.: , 92371068
QC Batch: 395901 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92371068002, 92371068003, 92371068004, 92371068005
SAMPLE DUPLICATE: 2194738
92371002001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 29.6 29.4 1
SAMPLE DUPLICATE: 2194739
92371068005 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 43.3 43.0 -1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
QC Batch: 395842 Analysis Method: EPA 1010
QC Batch Method: EPA 1010 Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92371068001, 92371068002
SAMPLE DUPLICATE: 2194276
92371068001 Dup
Parameter Units Result Result RPD Qualifiers
Flashpoint deg F >200 >200
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 395747 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92371068001, 92371068002
SAMPLE DUPLICATE: 2193930
92370428002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 13.2 13.3 0 E
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 397078 Analysis Method: ASTM D5468-02
QC Batch Method: ASTM D5468-02 Analysis Description: ASTM D5468-02 BTU
Associated Lab Samples: 92371068003, 92371068004, 92371068005
SAMPLE DUPLICATE: 2201882
92371068003 Dup
Parameter Units Result Result RPD Qualifiers
British Thermal Units BTU/Ib 4310 5170 18 D6,N2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 29

1-01
aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
QC Batch: 395774
Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 2194060
Matrix: Solid
Associated Lab Samples: 92371068001, 92371068002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 2.0
02/02/1815:41
LABORATORY CONTROL SAMPLE: 2194061
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
50 53.0
106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2194062 2194063
MS MSD
92370809001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 121
72.7 79.9 184
140 87 24 90-110 27 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 29

reAnalytical
www.pace/aftcorri
QUALITY CONTROL DATA
Project: Wood BoilerASh 1/25
Pace Project No.: 92371068
QC Batch: 286809 Analysis Method: EPA 9014
QC Batch Method: SW 846 7.3.3.2 Analysis Description: 733C Reactive Cyanide
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 1406433 Matrix: Solid
Associated Lab Samples: 92371068001, 92371068002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide, Reactive mg/kg ND 1.0 02/02/18 02:00
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1406434
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide, Reactive mg/kg 99.2 ND 0 0-8
SAMPLE DUPLICATE: 1406435
30242291001 Dup
Parameter Units Result Result RPD Qualifiers
Cyanide, Reactive mg/kg ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, I.I.C. Page 23 of 29

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 286808
Analysis Method:
SM4500S2F-00
QC Batch Method: SW 846 7.3.4.2
Analysis Description:
734S Reactive Sulfide
Associated Lab Samples: 92371068001, 92371068002
METHOD BLANK: 1406423
Matrix: Solid
Associated Lab Samples: 92371068001, 92371068002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Sulfide, Reactive
mg/kg
ND
10 02/02/18 01:52
LABORATORY CONTROL SAMPLE:
1406424
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Sulfide, Reactive
mg/kg
200 40.0
20 0-52
SAMPLE DUPLICATE: 1406426
30242291001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Sulfide, Reactive
mg/kg
410 386 6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/08/2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 29

aceAnalytical
www.pacelabs com
QUALIFIERS
Project: Wood Boiler ASh 1/25
Pace Project No.: 92371068
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
R1 RPD value was outside control limits.
Date: 02/08/2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 29

aceAnalytical e
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Wood Boiler ASh 1/25
92371068
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92371068001
SP12618A
EPA 3050
396227
EPA 6010
396288
92371068002
SP12618B
EPA 3050
396227
EPA 6010
396288
92371068001
SP12618A
EPA 3010A
395789
EPA 6010
395803
92371068002
SP12618B
EPA 3010A
395789
EPA 6010
395803
92371068001
SP12618A
EPA 7470
395790
EPA 7470
395812
92371068002
SP12618B
EPA 7470
395790
EPA 7470
395812
92371068001
SP12618A
EPA 7471
395794
EPA 7471
395814
92371068002
SP12618B
EPA 7471
395794
EPA 7471
395814
92371068001
SP12618A
ASTM D2974-87
395862
92371068002
SP12618B
ASTM D2974-87
395901
92371068003
Test 1A
ASTM D2974-87
395901
92371068004
Test2B
ASTM D2974-87
395901
92371068006
Test 3C
ASTM D2974-87
395901
92371068001
SP12618A
EPA1010
395842
92371068002
SP12618B
EPA1010
395842
92371068001
SP12618A
EPA 9045
395747
92371068002
SP12618B
EPA 9045
395747
92371068003
Test 1A
ASTM D5468-02
397078
92371068004
Test 2B
ASTM D5468-02
397078
92371068005
Test 3C
ASTM D5468-02
397078
92371068001
SP12618A
EPA 365.1
395774
92371068002
SP12618B
EPA 365.1
395774
92371068001
SP12618A
SW-846 7.3.3.2
286809
EPA 9014
286826
92371068002
SP12618B
SW-846 7.3.3.2
286809
EPA 9014
286826
92371068001
SP12618A
SW-846 7.3.4.2
286808
SM4500S2F-00
286827
92371068002
SP12618B
SW-846 7.3.4.2
286808
SM4500S2F-00
286827
Date: 02/08/2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 26 of 29

Document Name: Document Revised: January 24, 2018 0
r - m Sample Condition Upon Receipt(SCUR) Page 1 of 2
%,� aceAnalXical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.05 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville,] Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
• Cli tName-
MUM, WO## : 92371068
- . �O��p t � � Project h
Courier: ❑Fed Ex I "[ ❑UPS [-]LISPS �C4ient III III I II I I I I I I�I II �II
❑Commercial ❑Pace ❑Other: 92371068
Custody Seal Present? ❑Yes tti Seals Intact? Des -0N 5-'
Date/Initials Person . mining n nts:
Packing Material: ❑Bubble Wrap ❑Bubble bags None ❑ Other Biological Tissue Frroze-n?_
i hermometer: .� ❑Yes ❑No�] . /N A
❑ IR Gun ID: Type of Ice: ❑Wet E]Blue J one
Cooler Temp (°C): Correction Factor: Add/Subtract (°C)Vi 'T
(}�- Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): fT , []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil .(❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check Maps)? Did samples originate from a foreign source (intre-r�natio y,
I-1.,__ r"l../_ 1n�1� Aino Nawaii nnri Puprtn Rirnl? I�IYeS 1' 1 0
Comments/ Discrepancy:
Chain of Custody Present?
❑No ❑N/A
1.
Samples Arrived within Hold Time?
es
[]No []N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
©too ❑N/A
3.
Rush Turn Around Time Requested?
[]Yes _2N-b_'0N/A
4.
Sufficient Volume?
•-0a-s-
❑No ❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
es
❑Yes
❑No ❑N/A
❑Now []N/A
5.
Containers Intact?
-E eF s _-
❑No ❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
o ❑N/A
8.
Sample Labels Match C0C?
-Includes Date/Time/ID/Analysis Matrix:
` es
❑No ❑N/A
9.
Headspace in VOA Vials (>S-Gmm)?
[]Yes
❑No ON A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
❑Yes
'❑No [ A
[]No N A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes [-]No,
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:v
Project Manager SRF Review: Dater
Page 27 of 29

.
MAnalytica!
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: Januay 24, 2018
Page of 2
Document No::
r-CAR-0-033-Rev.05
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechiorination is
ve'rified'd d Within`the actepiance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box 'is to list number of bottle
Project ;9 ail®# : 92371068,
PM: C01 Due Date: 02/0.9/18
CLIENT: 92—Baxter
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1.2
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: wnenever tnere Is a aiscrepancy attecung Nortn t:arouna compnance sampies, a copy of uns IolIn wm uC 3rIIL L� Lli� l., - .,, --,-••.._ --• •.... --• --•_.. _...__
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 28 of 29

Baxter Biomass: -Wood Boiler Ash - Ricky :Styles
Please test the sample(8). forAhe _parameters as
listed below.
.Send original -results to: email:. [e-mail]
Send invoice and.copy of`results,to: email:, ricky- [e-mail]
Ricky Stylea
Baxter Biomass Purchase Order # 1.69803
2859 Old Linville.Rd.
Marlon, NC 28752
(828) '756-6650
aa�37�e�
r7C UUbLCU'IJUC
.Sample.#
VaLC. .V( IGlGV!, I
Sample
Sample•Date(s)'
Grab -or
Total Metals'-.
TCLP Metals.
Ignitability,
,pH
Total -Arsenic
Full TCLP'
Moisture.
BTU PER
Description
and time sample
Composite
As; Ba, Cd,
As,,Ba, Cd,
Reactivity
Corrosivity
Content
POUND
,collected
Ca, Cr,'Cu, Fe,
Cr, Pb, H-R,
Pb, Mg;, Hg,
Se,, Ag,
Mn, Mo, Ni, K,
Se, Ag, Na, Zn,
total
Phos horus
SP12618A
ASH
1126/18 8:45AM
COMPOSITE
'YES
YES
YES
'YES;
YES
SP126.186
ASH
1/26/18 8:45AM'
COMPOSITE,
YES
YES
YES
YES
YES
'Test 1A, Test
wood Fuel
1/25/2018-3:OOpm
COMPOSITE
YES
YES
28; Test�3C
Sample:sent to: Pace Analytical Services, Inc. Project Manager: Tom Williams
2225 Riverside Drive, 9800 KinceyAvenue',:Suite_ 1.00
Asheville, NC'28804 Huntersviile; NC 28078
828-254-7176' (704) 675 - 9092-ext. 233
Chain of Custody
4
G0

aceAnalytical
• wwwpacelabs.com
July 30, 2018
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood BoilerAsh 7/19
Pace Project No.: 92392663
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on July 19, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
'9enmtOQ`
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

(.�5aciekialytical
wwx:pace/ebs.com
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
ANAB DOD-ELAP Rad Accreditation M L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification #: PA01547
Connecticut Certification #: PH-0694
Delaware Certification
EPA Region 4 DW Rad
Florida/TNI Certification #: E87683
Georgia Certification #: C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification #: E-10358
Kentucky Certification #: KY90133
KY WW Permit #: KY0098221
KY WW Permit #: KY0000221
Louisiana DHH/TNI Certification #: LA180012
Louisiana DEQ/TNI Certification #: 4086
Maine Certification M 2017020
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification #: 9991
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Missouri Certification #: 235
Montana Certification #: Cert0082
Nebraska Certification #: NE-OS-29-14
Nevada Certification #: PA014572018-1
New Hampshire/fNI Certification #: 297617
New Jersey/TNI Certification #: PA051
New Mexico Certification #: PA01457
New York/TNI Certification #: 10888
North Carolina Certification #: 42706
North Dakota Certification #: R-190
Ohio EPA Rad Approval: #41249
Oregon/TNI Certification #: PA200002-010
Pennsylvania/fNI Certification #: 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: 02867
Texas/TNI Certification #: T104704188-17-3
Utah/TNI Certification #: PA014572017-9
USDA Soil Permit #: P330-17-00091
Vermont Dept. of Health: ID# VT 0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification #: 9526
Washington Certification #: C868
West Virginia DEP Certification #: 143
West Virginia DHHR Certification #: 9964C
Wisconsin Approve List for Rad
Wyoming Certification #: 8TMS-L
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 24

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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Wood Boiler Ash 7/19
92392663
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92392663001
NP71918A
EPA 601 OD
DS, SER
17
PASI-A
EPA 601 OD
DS
7
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 7471 B
JMW1
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 1010A
ECH
1
PASI-A
EPA 9045D
RLO
1
PASI-A
EPA 365.1 Rev 2.0 1993
BRJ
1
PASI-A
EPA 9014
PAS
1
PASI-PA
SM4500S2F-00
PAS
1
PASI-PA
92392663002
NP71918B
EPA 6010D
DS, SER
17
PASI-A
EPA 601 OD
DS
7
PASI-A
EPA 7470A
JMW1
1
PASI-A
EPA 7471 B
JMW1
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 1010A
ECH
1
PASI-A
EPA 9045D
RLO
1
PASI-A
EPA 365.1 Rev 2.0 1993
BRJ
1
PASI-A
EPA 9014
PAS
1
PAS[ -PA
SM4500S2F-00
PAS
1
PAS[ -PA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 24

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP71918A Lab ID: 92392663001 Collected: 07/19/18 09:45 Received: 07/19/18 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD
Preparation Method: EPA 3050B
Arsenic
3.6
mg/kg
1.2
1
07/21/18 11:16
07/23/18 03:48
7440-38-2
Barium
1590
mg/kg
5.9
10
07/21/18 11:16
07/23/18 21:05
7440-39-3
Cadmium
1.8
mg/kg
0.12
1
07/21/18 11:16
07/23/18 03:48
7440-43-9
Calcium
91100
mg/kg
117
10
07/21/18 11:16
07/23/18 21:05
7440-70-2
Chromium
19.2
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7440-47-3
Copper
78.5
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7440-50-8
Iron
10600
mg/kg
11.7
1
07/21/18 11:16
07/23/18 03:48
7439-89-6
Lead
23.3
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7439-92-1
Magnesium
15200
mg/kg
117
10
07/21/18 11:16
07/23/18 21:05
7439-95-4
Manganese
3520
mg/kg
5.9
10
07/21/18 11:16
07/23/18 21:05
7439=96-5
Molybdenum
1.3
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7439-98-7
Nickel
21.2
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7440-02-0
Potassium
18800
mg/kg
5860
10
07/21/18 11:16
07/23/18 21:05
7440-09-7
Selenium
ND
mg/kg
1.2
1
07/21/18 11:16
07/23/18 03:48
7782-49-2
Silver
ND
mg/kg
0.59
1
07/21/18 11:16
07/23/18 03:48
7440-22-4
Sodium
6310
mg/kg
586
1
07/21/18 11:16
07/23/18 03:48
7440-23-5
Zinc
188
mg/kg
1.2
1
07/21/18 11:16
07/23/18 03:48
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD
Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311;
07/20/18 18:15 Initial pH: 9.78; Final
pH: 5.5
Arsenic
ND
mg/L
0.050
1
07/21/1816:34
07/23/1819:24
7440-38-2
Barium
9.2
mg/L
0.25
1
07/21/1816:34
07/23/1819:24
7440-39-3
Cadmium
0.0080
mg/L
0.0050
1
07/21/1816:34
07/23/1819:24
7440-43-9
Chromium
ND
mg/L
0.050
1
07/21/1816:34
07/23/1819:24
7440-47-3
Lead
ND
mg/L
0.025
1
07/21/1816:34
07/23/1819:24
7439-92-1
Selenium
ND
mg/L
0.10
1
07/21/1816:34
07/23/1819:24
7782-49-2
Silver
ND
mg/L
0.025
1
07/21/1816:34
07/23/1819:24
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A
Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311;
07/20/18 18:15 Initial pH: 9.78; Final
pH: 4.5
Mercury
ND
mg/L
0.00020
1
07/24/1814:38
07/25/1810:16
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B
Preparation Method: EPA 7471 B
Mercury
ND
mg/kg
0.0058
1
07/19/1818:03
07/20/1810:48
7439-97-6 M1,R1
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
39.9
%
0.10
1
07/20/18 13:18
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200.0
deg F
70.0
1
07/30/18 17:43
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
9.3
Std. Units
0.10
1
07/20/18 08:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24

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ANALYTICAL RESULTS
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP71918A Lab ID: 92392663001 Collected: 07/19/18 09:45 Received: 07/19/18 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus 784 mg/kg 28.7 10 07/20/18 02:55 07/20/18 23:18 7723-14-0
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive ND mg/kg 1.7 1 07/26/18 20:12 07/26/18 21:01
734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive ND mg/kg 16.6 1 07/26/18 20:12 07/26/18 20:18
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 5 of 24

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP71918B Lab ID: 92392663002 Collected: 07/19/18 09:45 Received: 07/19/18 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050E
Arsenic
2.9
mg/kg
1.4
1
07/21/18 11:16
07/23/18 03:51
7440-38-2
Barium
2670
mg/kg
7.0
10
07/21/18 11:16
07/23/18 21:14
7440-39-3
Cadmium
1.2
mg/kg
0.14
1
07/21/18 11:16
07/23/18 03:51
7440-43-9
Calcium
137000
mg/kg
140
10
07/21/18 11:16
07/23/18 21:14
7440-70-2
Chromium
24.7
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7440-47-3
Copper
92.0
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7440-50-8
Iron
20700
mg/kg
140
10
07/21/18 11:16
07/23/18 21:14
7439-89-6
Lead
15.0
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7439-92-1
Magnesium
23200
mg/kg
140
10
07/21/18 11:16
07/23/18 21:14
7439-95-4
Manganese
4930
mg/kg
7.0
10
07/21/18 11:16
07/23/18 21:14
7439-96-5
Molybdenum
1.5
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7439-98-7
Nickel
31.9
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7440-02-0
Potassium
34700
mg/kg
7010
10
07/21/18 11:16
07/23/18 21:14
7440-09-7
Selenium
ND
mg/kg
1.4
1
07/21/18 11:16
07/23/18 03:51
7782-49-2
Silver
ND
mg/kg
0.70
1
07/21/18 11:16
07/23/18 03:51
7440-22-4
Sodium
11300
mg/kg
701
1
07/21/18 11:16
07/23/18 03:51
7440-23-5
Zinc
147
mg/kg
1.4
1
07/21/18 11:16
07/23/18 03:51
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 07/20/118 18:15
Initial pH: 9.72; Final
pH: 5
Arsenic
ND
mg/L
0.050
1
07/21/1816:34
07/23/1819:27
7440-38-2
Barium
9.3
mg/L
0.25
1
07/21/1816:34
07/23/1819:27
7440-39-3
Cadmium
0.0098
mg/L
0.0050
1
07/21/1816:34
07/23/1819:27
7440-43-9
Chromium
ND
mg/L
0.050
1
07/21/1816:34
07/23/1819:27
7440-47-3
Lead
ND
mg/L
0.025
1
07/21/1816:34
07/23/1819:27
7439-92-1
Selenium
ND
mg/L
0.10
1
07/21/1816:34
07/23/1819:27
7782-49-2
Silver
ND
mg/L
0.025
1
07/21/1816:34
07/23/1819:27
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 07/20/18 18:15
Initial pH: 9.72; Final
pH: 4.5
Mercury
ND
mg/L
0.00020
1
07/24/1814:38
07/25/1810:28
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
ND mg/kg
0.0065
1 07/19/1818:03
07/2011810:55 7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
47.5 %
0.10
1
07/20/18 13:19
1010 Flashpoint,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200.0 deg F
70.0
1
07/30/18 17:43
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
9.3 Std. Units
0.10
1
07/20/18 08:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, I.I.C.
Page 6 of 24

aceAnalytical
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: NP71918B
Lab ID: 92392663002 Collected: 07/19/18 09:45 Received: 07/19/18 11:50 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qua[
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus
827 mg/kg 35.3 10 07/20/18 02:55 07/20/18 23:19 7723-14-0
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2
Cyanide, Reactive
ND mg/kg 1.9 1 07/26/18 20:12 07/26/18 21:01
734S Reactive Sulfide
Analytical Method: SM4500S2F-00 Preparation Method: SW-846 7.3.4.2
Sulfide, Reactive
ND mg/kg 18.9 1 07/26/18 20:12 07/26/18 20:18
Date: 07/30/2018 08:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 24

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood BoilerAsh 7/19
Pace Project No.: 92392663
QC Batch: 420748 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 2330704 Matrix: Water
Associated Lab Samples: 92392663001, 92392663002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/L ND 0.00020 07/25/1810:11
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2330734
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/L .0025 0.0026 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2330735 2330736
MS MSD
92392663001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/L ND .0025 .0025 0.0026 0.0027 103 108 75-125 5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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aceAiialytical
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Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420143
QC Batch Method: EPA 7471 B
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 2327983
Associated Lab Samples: 92392663001, 92392663002
Parameter Units
Mercury mg/kg
QUALITY CONTROL DATA
Analysis Method: EPA 7471 B
Analysis Description: 7471 Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0060 07/20/1810:43
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2327984
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .083 0.070 84 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2327985 2327986
MS MSD
92392663001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND .08 .08 0.052 0.042 65 52 75-125 23 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420449 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3050B Analysis Description: 6010 MET
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 2329391
Associated Lab Samples: 92392663001, 92392663002
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Matrix: Solid
Blank
Result
Reporting
Limit
Analyzed
ND
1.0
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
0.10
07/23/18 03:02
ND
10.0
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
10.0
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
10.0
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
500
07/23/18 03:02
ND
1.0
07/23/18 03:02
ND
0.50
07/23/18 03:02
ND
500
07/23/18 03:02
ND
1.0
07/23/18 03:02
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2329392
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
45.5
91
80-120
Barium
mg/kg
50
48.1
96
80-120
Cadmium
mg/kg
50
46.1
92
80-120
Calcium
mg/kg
500
468
94
80-120
Chromium
mg/kg
50
47.7
95
80-120
Copper
mg/kg
50
48.8
98
80-120
Iron
mg/kg
500
474
95
80-120
Lead
mg/kg
50
45.7
91
80-120
Magnesium
mg/kg
500
453
91
80-120
Manganese
mg/kg
50
45.6
91
80-120
Molybdenum
mg/kg
50
49.8
100
80-120
Nickel
mg/kg
50
46.7
93
80-120
Potassium
mg/kg
500
ND
95
80-120
Selenium
mg/kg
50
44.1
88
80-120
Silver
mg/kg
25
23.8
95
80-120
Sodium
mg/kg
500
466J
93
80-120
Zinc
mg/kg
50
44.6
89
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 24

IneAnalyfical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
-9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2329303
2329394
MS
MSD
92392463009
Spike
Spike
IVIS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
0.95
47.2
48.1
42.9
43.5
89
88
75-125
1
Barium
mg/kg
8.2
47.2
48.1
62.1
56.1
114
100
75-125
10
Cadmium
mg/kg
ND
47.2
48.1
42.3
43.4
90
90
75-125
3
Calcium
mg/kg
112
472
- 481
595
628
102 ,
107
75-125
5
Chromium
mg/kg
9.8
47.2
48.1
82.9
53.3
155
90
75-125
43 M1,R1
Copper
mg/kg
1.3
47.2
48.1
47.5
50.1
98
101
75-125
5
Iron
mg/kg
4760
472
481
6900
6150
453
291
75-125
11 M1
Lead
mg/kg
2.0
47.2
48.1
43.4
43.9
88
87
75-125
1
Magnesium
mg/kg
181
472
481
897
679
152
104
75-125
28 M1,R1
Manganese
mg/kg
135
47.2
48.1
120
93.3
-31
-87
75-125
25 M1,R1
Molybdenum
mg/kg
ND
47.2
48.1
44.1
46.1
93
96
75-125
4
Nickel
mg/kg
0.86
47.2
48.1
44.3
44.6
92
91
75-125
1
Potassium
mg/kg
ND
472
481
1090
671
195
104
75-125
47 M1,R1
Selenium
mg/kg
ND
47.2
48.1
39.7
40.9
84
85
75-125
3
Silver
mg/kg
ND
23.6
24
21.7
22.4
92
93
75-125
3
Sodium
mg/kg
ND
472
481
443J
453J
92
93
75-125
Zinc
mg/kg
3.3
47.2
48.1
46.9
46.0
92
89
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 24

aL.MnalXical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420476 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 2329514
Matrix: Water
Associated Lab Samples:
92392663001, 92392663002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
07/23/1818:42
Barium
mg/L
ND
0.25
07/23/1818:42
Cadmium
mg/L
ND
0.0050
07/23/1818:42
Chromium
mg/L
ND
0.050
07/23/1818:42
Lead
mg/L
ND
0.025
07/23/1818:42
Selenium
mg/L
ND
0.10
07/23/1818:42
Silver
mg/L
ND
0.025
07/23/1818:42
METHOD BLANK: 2328612
Matrix: Water
Associated Lab Samples:
92392663001, 92392663002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
07/23/1818:36
Barium
mg/L
ND
0.25
07/23/1818:36
Cadmium
mg/L
ND
0.0050
07/23/1818:36
Chromium
mg/L
ND
0.050
07/23/1818:36
Lead
mg/L
ND
0.025
07/23/1818:36
Selenium
mg/L
ND
0.10
07/23/1818:36
Silver
mg/L
ND
0.025
07/23/1818:36
LABORATORY CONTROL SAMPLE:
2329513
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
2.5
2.5
99
80-120
2.5
2.2
89
80-120
2.5
2.4
94
80-120
2.5
2.3
94
80-120
2.5
2.3
90
80-120
2.5
2.5
100
80-120
1.2
1.2
97
80-120
LABORATORY CONTROL SAMPLE: 2329515
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Arsenic mg/L 2.5 2.4 98 80-120
Barium mg/L 2.5 2.3 93 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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ac"Analyical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2329515
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
mg/L
2.5
2.4
96
80-120
Chromium
mg/L
2.5
2.3
93
80-120
Lead
mg/L
2.5
2.3
94
80-120
Selenium
mg/L
2.5
2.5
100
80-120
Silver
mg/L
1.2
1.2
98
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2329528
2329629
MS
MSD
92392504002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.5
2.5
99
99
75-125
0
Barium
mg/L
1.1
2.5
2.5
3.4
3.4
94
94
75-125
0
Cadmium
mg/L
0.060
2.5
2.5
2.4
2.4
94
95
75-125.
1
Chromium
mg/L
ND
2.5
2.5
2.3
2.4
92
94
75-125
2
Lead
mg/L
0.19
2.5
2.5
2.4
2.4
89
89
75-1254
0
Selenium
mg/L
ND
2.5
2.5
2.5
2.5
99
100
75-125
1
Silver
mg/L
ND
1.2
1.2
1.2
1.2
97
99
75-125
2
Results presented on this page are in the, units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, L.L.C. Page 13 of 24

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QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420293 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92392663001, 92392663002
SAMPLE DUPLICATE: 2328571
92392662001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 12.1 1.2.5 3
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 2328572
92392663002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 47.5 48.3 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written.consent of Pace Analytical Services, LLC. Page 14 of 24

aucehialytical
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QUALITY CONTROL DATA
Project: Wood BoilerAsh 7/19
Pace Project No.: 92392663
QC Batch: 421849 Analysis Method: EPA 1010A
QC Batch Method: EPA 1010A Analysis Description: 1010 Flash Point, Closed Cup
Associated Lab Samples: 92392663001, 92392663002
SAMPLE DUPLICATE: 2335473
92392663001 Dup
Parameter Units Result Result
Flashpoint deg F >200.0 >200.0
RPD Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 24

?�IaaCeAnaljftal
ivww.pacelabs,cot#
QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420163 Analysis Method: EPA 9045D
QC Batch Method: EPA 9045D Analysis Description: 9045 pH
Associated Lab Samples: 92392663001, 92392663002
SAMPLE DUPLICATE: 2328043
92392663001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 9.3 9.3 0
SAMPLE DUPLICATE: 2328044
Parameter
pH at 25 Degrees C
92392663002 Dup
Units Result Result
Std. Units 9.3 9.2
RPD Qualifiers
0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
QC Batch: 420169
QC Batch Method: EPA 365.1 Rev 2.0 1993
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 2328063
Associated Lab Samples: 92392663001, 92392663002
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 2328064
Parameter Units
Phosphorus mg/kg
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Matrix: Solid
EPA 365.1 Rev 2.0 1993
365.1 Phosphorus, Total
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/20/18 21:50
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
50 52.1 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2328065 2328066
MS MSD
92392148001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 96.1 65.6 59.5 175 223 121 213 90-110 24 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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aWnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 307364
Analysis Method:
EPA 9014
QC Batch Method: SW-846 7.3.3.2
Analysis Description:
733C Reactive Cyanide
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 1502416
Matrix: Solid
Associated Lab Samples: 92392663001, 92392663002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cyanide, Reactive
mg/kg
ND
1.0 07/26/18 20:53
LABORATORY CONTROL SAMPLE:
1502417
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Cyanide, Reactive
mg/kg
99.2 ND
0 0-8
SAMPLE DUPLICATE: 1502418
30259867005 Dup
Parameter
Units
Result Result
RPD Qualifiers
Cyanide, Reactive
mg/kg
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 24

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QUALITY CONTROL DATA
Project: Wood BoilerAsh 7/19
Pace Project No.: 92392663
QC Batch: 307363 Analysis Method: SM4500S2F-00
QC Batch Method: SW-846 7.3.4.2 Analysis Description: 734S Reactive Sulfide
Associated Lab Samples: 92392663001, 92392663002
METHOD BLANK: 1502413 Matrix: Solid
Associated Lab Samples: 92392663001, 92392663002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide, Reactive mg/kg ND 10.0 07/26/18 20:18
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1502414 '
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide, Reactive mg/kg 200 48.0 24 0-52
SAMPLE DUPLICATE: 1502415
30259867005 Dup
Parameter Units Result Result
Sulfide, Reactive mg/kg ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: Wood Boiler Ash 7/19
Pace Project No.: 92392663
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 827b. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PAS[ -PA Pace Analytical Services - Greensburg
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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aceAnalytt+cal
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood BoilerAsh 7/19
Pace Project No.: 92392663
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92392663001
NP71918A
EPA 3050B
420449
EPA 6010D
420484
92392663002
NP71918B
EPA 3050B
420449
EPA 6010D
420484
92392663001
NP71918A
EPA 3010A
420476
EPA 6010D
420482
92392663002
NP71918B
EPA 3010A
420476
EPA 6010D
420482
92392663001
NP71918A
EPA 7470A
420748
EPA 7470A
420834
92392663002
NP71918B
EPA 7470A
420748
EPA 7470A
420834
92392663001
NP71918A
EPA 7471 B
420143
EPA 7471 B
420145
92392663002
NP71918B
EPA 7471E
420143
EPA 7471B
420145
92392663001
NP71918A
ASTM D2974-87
420293
92392663002
NP71918B
ASTM D2974-87
420293
92392663001
NP71918A
EPA 1010A
421849
92392663002
NP71918B
EPA 1010A
421849
92392663001
NP71918A
EPA 9045D
420163
92392663002
NP71918B
EPA 9045D
420163
92392663001
NP71918A
EPA 365.1 Rev 2.0 1993
420169
EPA 365.1 Rev 2.0 1993
420196
92392663002
NP71918B
EPA 365.1 Rev 2.0 1993
420169
EPA 365.1 Rev 2.0 1993
420196
92392663001
NP71918A
SW-846 7.3.3.2
307364
EPA 9014
307382
92392663002
NP71918B
SW-846 7.3.3.2
307364
EPA 9014
307382
92392663001
NP71918A
SW 846 7.3.4.2
307363
SM4500S2F-00
307381
92392663002
NP71918B
SW 846 7.3.4.2
307363
SM4500S2F-00
307381
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2018 08:46 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 24

aceAnalyrical
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Pagel of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality office
Laboratory receiving sam es:
Asheville Eden[]Greenwood ❑ Huntersville ❑ Raleigh[]Mechanicsville❑
Lff
SafnPClient Name:, �O : 9232663
. , � ` L (� � Project �
G� L III
Courier: []Fed ❑
Fed Ex Cli'ent I� II I I I III I IIII III
❑ Commercial ❑Pace ❑Other: p92392663
Custody Seal Present? [-]Yes [,JNo Seals Intact? ❑Yes [a ilFo j � A
Date/initials Person Examl i g t� ts:
Packing Material: ❑Bubble Wrap ❑Bubble Bags [�N no e ❑ Other Biological Tissue Frozen?
❑Yes ❑No 13N/-A
Thermometer: Type of Ice: []Wet []Blue r}NBne
❑ IR Gun ID:
Cooler Temp (°C):Correction Factor: Add/Subtract (°C) A 1 ! /Y
% Temp should be above freezing to 6°C
Cooler Temp Corrected (°C):. []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (` N/A, water sample)
Did samples originate in a quarantine tone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
r-i„__ r-i.._ inr4uainn Hawaii and Puerto Rico)? nYes []No
Comments/Discrepancy:
Chain of Custody Present?
,.�,,��
a2lres
[]No
❑N/A
1.
Samples Arrived within Hold Time?
Ely—
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
®N
❑N/A
3.
Rush Turn Around Time Requested?
Dyes
' No
❑N/A
4.
Sufficient Volume?
Ye-,
[]No❑N/A
5.
Correct Containers Used?
,..,
JI Yes
[:]No
❑N/A
6.
-Pace Containers Used?
Ores
[]No
❑N/A.
Containers Intact?
Ellre-5
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
®Nb
❑N/A
8:
Sample Labels Match COC?
es
[]No
[]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
a
(MN/A
10.
Trip Blank Present?
❑Yes
❑No
N/A
2N/A
11.
Trip Blank Custody Seals Present?
[]Yes
❑No
u
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Lot ID of split containers:
Field Data Required? []Yes [:]No
? Project Manager SCURF Review: /, Date: % 2 -
i
Project Manager SRF Review: Date:
i
Page 22 of 24

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Item#
Z'ZZZ
ZZZZAZ
BP4U-125 mL Plastic Unpreserved (N/A) (Cl-)
BP3U-250 mL Plastic Unpreserved (N/A)
BP2U-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
BRS-125 ml. Plastic H2SO4 (pH < 2) (Cl-)
BP3N-250 mL plastic HNO3 (pH <2)
BP4Z-125 mL Plastic ZN Acetate & NaOH (>9)
BP4C-125 mL Plastic NaOH (pH > 12) (CI-)
WGFU-Wide-mouthed Glass jar Unpreserved
AG1U-1 liter Amber Unpreserved (N/A) (Cl-)
AGiH-1 liter Amber HCI (pH <2)
AG31.1-250 i. Amber Unpreserved (N/A) (CI-)
AG1S-1 liter Amber H2SO4 (pH < 2)
AG3S-250 mL Amber H2SO4 (pH < 2)
AG3A(DG3A)-250 mLAmber NH4Cl (N/A)(CI-)
DG9H-40 mL VOA HCI (N/A)
VG9T-40 mL VOA Na2S2O3 (N/A)
VGOU-40 mL VOA Unp (N/Ai
OGSP-40'mL VOA HBP04 (N/A)
VOAK (6 vials per kit)-5035 kit (N/A)
V/GK (3 vials per kit)-VPH/Gas kit (N/A)
SP5T-125 mL Sterile Plastic (N/A — lab)
SP2T-250 mLSterilePlastic (N/A —lab)
-
BP3A-250 mL Plastic (NI.12)2SO4 (9.3-9.7)
AGOU-100 mL Amber Unpreserved vials (N/A)
VSGU-20 mLScintillation vials (N/A)
DG91.1-40 mLAmber Unpreserved vials (N/A)
V
A)
D
V
31
N

Baxter Biomass - Wood Boiler Ash - Ricky Styles
Please test the sample(s) for the parameters as
listed below.
Send original results to: email: [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Biomass Purchase Order # IN PROCESS
2859 Old Linville Rd.
Marion, NC 28752
[phone]
3-12-C63
He uestea uue
Sample #
vale: r7.5ucU io
Sample
Description
Sample Date(s)
and time sample
Grab or
Composite
•.•. ^-- _•� •
Total Metals -
As, BA, Cd,
—�
TCLP Metals
As, Ba, Cd,
Ignitability,
Reactivity,
pH
Corrosivity
Total -Arsenic
Full TCLP
Moisture
Content
BTU PER
POUND
collected
Ca, Cr, Cu, Fe,
Cr, Pb, Hg;
Pb, Mg, Hg,
Se, Ag
Mn, Mo, Ni, K,
Se, Ag, Na, Zn,
total
Phosphorus
NP71918A
ASH
7/19/18 9:45AM
COMPOSITE
YES
YES
YES
YES-
YES
YES
NP71918B
ASH
7/19/18 9:45AM
COMPOSITE
YES
YES
YES
YES
YES
YES
Sample sent.to: Pace Analytical Services, Inc. Project Manager: Tom Williams
2225 Riverside Drive 9800. Kincey Avenue, Suite 100
Asheville, NC 28804 Huntersville, NC 28078
828-254-7176. (704) 875 - 9092 ext. 233
Chain of Custody s\ �(1 \�)o
doe

aceAnalytical
www.pacelabs.com
January 08, 2019
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
RE: Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Dear Mr. Styles:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 19

laneAnalytical"
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
CERTIFICATIONS
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification M E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification M 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification M 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification M 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030
Virginia/VELAP Certification #: 460222
North Carolina Drinking Water Certification M 37712
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 19

aceAnalytical
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Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Lab ID Sample ID
92411973001 SP1221118A
92411973002 SP122118B
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 6010D
DS
17
PASI-A
EPA 6010D
KQ
7
PASI-A
EPA 7470A
RDT
1
PASI-A
EPA 7471B
JMW1
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
EPA 6010D
DS
17
PASI-A
EPA 6010D
KQ
7
PASI-A
EPA7470A
RDT
1
PASI-A
EPA 7471 B
JMW1
1
PASI-A
ASTM D2974-87
KDF
1
PASI-C
EPA 9045D
SMK
1
PASI-A
EPA 365.1 Rev 2.0 1993
MDW
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 19

5.aneAnalyfioal"
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ANALYTICAL RESULTS
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP1221118A Lab ID: 92411973001 Collected: 12/21/18 13:15 Received: 12/21/18 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Arsenic
ND
mg/kg
1.3
1
12/26/18 09:18
12/27/18 13:44
7440-38-2
Barium
1490
mg/kg
6.6
10
12/26/18 09:18
12/27/18 13:41
7440-39-3
Cadmium
1.5
mg/kg
0.13
1
12/26/18 09:18
12/27/18 13:44
7440-43-9
Calcium
73300
mg/kg
132
10
12/26/18 09:18
12/27/18 13:41
7440-70-2
Chromium
16.9
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7440-47-3
Copper
58.0
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7440-50-8
Iron
10700
mg/kg
13.2
1
12/26/18 09:18
12/27/18 13:44
7439-89-6
Lead
17.7
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7439-92-1
Magnesium
10200
mg/kg
13.2
1
12/26/18 09:18
12/27/18 13:44
7439-95-4
Manganese
2670
mg/kg
6.6
10
12/26/18 09:18
12/27/18 13:41
7439-96-5
Molybdenum
0.83
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7439-98-7
Nickel
18.9
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7440-02-0
Potassium
9970
mg/kg
661
1
12/26/18 09:18
12/27/18 13:44
7440-09-7
Selenium
ND
mg/kg
1.3
1
12/26/18 09:18
12/27/18 13:44
7782-49-2
Silver
ND
mg/kg
0.66
1
12/26/18 09:18
12/27/18 13:44
7440-22-4
Sodium
4340
mg/kg
661
1
12/26/18 09:18
12/27/18 13:44
7440-23-5
Zinc
129
mg/kg
1.3
1
12/26/18 09:18
12/27/18 13:44
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 01/03/19
20:03
Initial pH: 10.47; Final pH: 6
Arsenic
ND
mg/L
0.050
1
01/05/1915:32
01/07/1910:54
7440-38-2
Barium
6.4
mg/L
0.25
1
01/05/1915:32
01/07/1910:54
7440-39-3
Cadmium
ND
mg/L
0.0050
1
01/05/1915:32
01/07/1910:54
7440-43-9
Chromium
ND
mg/L
0.050
1
01/05/1915:32
01/07/1910:54
7440-47-3
Lead
ND
mg/L
0.025
1
01/05/1915:32
01/07/1910:54
7439-92-1
Selenium
ND
mg/L
0.10
1
01/05/1915:32
01/07/1910:54
7782-49-2
Silver
ND
mg/L
0.025
1
01/05/1915:32
01/07/1910:54
7440-22-4
7470 Mercury,, TCLP
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 01/03/19
20:03
Initial pH: 10.47; Final pH: 6
Mercury
ND
mg/L
0.00020
1
01/07/19 17:12
01/08/19 09:45
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
ND
mg/kg
0.0043
1
12/26/18 17:56
12/27/18 09:28
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
67.5
%
0.10
1
12/26/18 18:19
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
10.8
Std. Units
0.10
1
12/26/18 12:46
BC
H3
REPORT OF LABORATORY ANALYSIS
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Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 19

acekialXkal
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Wood BoilerAsh 12/21
Pace Project No.: 92411973
Sample: SP122118B
Lab ID: 92411973002 Collected: 12/21/18 13:15
Received: 12/21/18 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 OD
Preparation Method: EPA 3050B
Arsenic
ND
mg/kg
1.2
1
12/26/18 09:18
12/27/18 13:51
7440-38-2
Barium
1750
mg/kg
6.1
10
12/26/18 09:18
12/27/18 13:48
7440-39-3
Cadmium
1.8
mg/kg
0.12
1
12/26/18 09:18
12/27/18 13:51
7440-43-9
Calcium
87300
mg/kg
122
10
12/26/18 09:18
12/27/18 13:48
7440-70-2
Chromium
18.5
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7440-47-3
Copper
467
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7440-50-8
Iron
10600
mg/kg
12.2
1
12/26/18 09:18
12/27/18 13:51
7439-89-6
Lead
21.0
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7439-92-1
Magnesium
13400
mg/kg
122
10
12/26/18 09:18
12/27/18 13:48
7439-95-4
Manganese
3220
mg/kg
6.1
10
12/26/18 09:18
12/27/18 13:48
7439-96-5
Molybdenum
ND
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7439-98-7
Nickel
21.6
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7440-02-0
Potassium
12900
mg/kg
6090
10
12/26/18 09:18
12/27/18 13:48
7440-09-7
Selenium
ND
mg/kg
1.2
1
12/26/18 09:18
12/27/18 13:51
7782-49-2
Silver
ND
mg/kg
0.61
1
12/26/18 09:18
12/27/18 13:51
7440-22-4
Sodium
5320
mg/kg
609
1
12/26/18 09:18
12/27/18 13:51
7440-23-5
Zinc
247
mg/kg
1.2
1
12/26/18 09:18
12/27/18 13:51
7440-66-6 BC
6010 MET ICP, TCLP
Analytical Method: EPA 601 OD
Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311;
01/03/19 20:03
Initial pH: 10.46; Final pH: 6
Arsenic
ND
mg/L
0.050
1
01/0511915:32
01/07/1910:57
7440-38-2
Barium
7.0
mg/L
0.25
1
01/05/1915:32
01/07/1910:57
7440-39-3
Cadmium
0.0055
mg/L
0.0050
1
01/05/1915:32
01/07/1910:57
7440-43-9
Chromium
ND
mg/L
0.050
1
01/05/1915:32
01/07/1910:57
7440-47-3
Lead
ND
mg/L
0.025
1
01/05/1915:32
01/07/1910:57
7439-92-1
Selenium
ND
mg/L
0.10
1
01/05/1915:32
01/07/1910:57
7782-49-2
Silver
ND
mg/L
0.025
1
01/05/1915:32
01/07/1910:57
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A
Preparation Method: EPA 7470A
Leachate Method/Date:
EPA 1311;
01/03/19 20:03
Initial pH: 10.46; Final pH: 6
Mercury
ND
mg/L
0.00020
1
01/07/19 17:12
01/08/19 09:52
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B
Preparation Method: EPA 7471 B
Mercury
ND
mg/kg
0.0091
1
12/26/18 17:56
12/27/18 09:31
7439-97-6
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
57.7
- %
0.10
1
12/26/18 18:19
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
11.4
Std. Units
0.10
1
12/26/18 12:51
H3
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Phosphorus
1930
mg/kg
86.0
20
12/24/18 15:35
12/24/18 21:55
7723-14-0 M6, R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 19

'..aneAn91j&ca(
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 450873
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 92411973001, 92411973002
METHOD BLANK: 2465527
Matrix: Water
Associated Lab Samples: 92411973001,
92411973002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
01/08/19 09:31
METHOD BLANK: 2465706
Matrix: Water
Associated Lab Samples: 92411973001, 92411913002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
mg/L
ND 0.00020
01/08/19 09:38
LABORATORY CONTROL SAMPLE:
2466422
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0022
86 80-120
LABORATORY CONTROL SAMPLE:
2466661
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
mg/L
0.0025 0.0024
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2466423 2466424
MS MSD
92411973001
Spike Spike MS
MSD MS MSD % Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Mercury
mg/L ND
0.0025 0.0025 0.0022
0.0023 89 92 75-125 4
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 6 of 19

1tqCI
lytical
wwwpacelebs.m.
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
QC Batch: 449576 Analysis Method: EPA 7471 B
QC Batch Method: EPA 7471 B Analysis Description: 7471 Mercury
Associated Lab Samples: 92411973001, 92411973002
METHOD BLANK: 2461420 Matrix: Solid
Associated Lab Samples: 92411973001, 92411973002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0060 12/27/18 08:53
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2461421
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg 0.083 0.092 110 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2461422 2461423
MS MSD
92411686001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.72 1.7 1.6 1.8 1.8 64 72 75-125 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 19

lnaAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
QC Batch: 449472 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3050E Analysis Description: 6010 MET
Associated Lab Samples: 92411973001, 92411973002
METHOD BLANK: 2461079 Matrix: Solid
Associated Lab Samples: 92411973001, 92411973002
Parameter
Blank
Units Result
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/kg
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Reporting
Limit
Analyzed Qualifiers
ND
1.0
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
0.10
12/27/18 02:12
ND
10.0
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
10.0
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
10.0
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
500
12/27/18 02:12
ND
1.0
12/27/18 02:12
ND
0.50
12/27/18 02:12
ND
500
12/27/18 02:12
ND
1.0
12/27/1813:32 BC
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
2461080
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
48.8
98
80-120
Barium
mg/kg
50
50.0
100
80-120
Cadmium
mg/kg
50
48.6
97
80-120
Calcium
mg/kg
500
488
98
80-120
Chromium
mg/kg
50
49.9
100
80-120
Copper
mg/kg
50
51.9
104
80-120
Iron
mg/kg
500
502
100
80-120
Lead
mg/kg
50
49.0
98
80-120
Magnesium
mg/kg
500
478
96
80-120
Manganese
mg/kg
50
48.8
98
80-120
Molybdenum
mg/kg
50
52.9
106
80-120
Nickel
mg/kg
50
49.7
99
80-120
Potassium
mg/kg
500
ND
97
80-120
Selenium
mg/kg
50
47.7
95
80-120
Silver
mg/kg
25
25.2
101
80-120
Sodium
mg/kg
500
489J
98
80-120
Zinc
mg/kg
50
48.8
98
80-120 BC
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 19

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2461081
2461082
MS
MSD
92411221001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
106
99.3
101
96.3
96
97
75-125
5
Barium
mg/kg
400
106
99.3
530
535
123
136
75-125
1 M1
Cadmium
mg/kg
1.2
106
99.3
105
101
99
100
75-125
5
Calcium
mg/kg
16100
1060
993
18000
18300
180
222
75-125
2 M1
Chromium
mg/kg
22.1
106
99.3
128
124
100
103
75-125
3
Copper
mg/kg
493
106
99.3
632
641
132
149
75-125
1 M1
Iron
mg/kg
36200
1060
993
39400
40000
300
380
75-125
2 M1
Lead
mg/kg
17.9
106
99.3
119
114
96
97
75-125
4
Magnesium
mg/kg
3570
1060
993
4930
4990
129
143
75-125
1 M1
Manganese
mg/kg
151
106
99.3
262
261
105
111
75-125
0
Molybdenum
mg/kg
10.6
106
99.3
122
116
105
107
75-125
4
Nickel
mg/kg
20.0
106
99.3
124
120
98
100
75-125
4
Potassium
mg/kg
3200
1060
993
4650
4680
137
149
75-125
1 M1
Selenium
mg/kg
4.7
106
99.3
107
102
97
98
75-125
5
Silver
mg/kg
4.6
52.8
49.8
57.8
55.7
101
103
75-125
4
Sodium
mg/kg
ND
1060
993
1330
1290
99
102
75-125
3
Zinc
mg/kg
1730
106
99.3
1930
1950
187
223
75-125
1 BC,M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 9 of 19

aceAnalytical
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QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
QC Batch: 450872 Analysis Method: EPA 601 OD
QC Batch Method: EPA 3010A Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92411973001, 92411973002
METHOD BLANK: 2465527
Matrix:
Water
Associated Lab Samples:
92411973001, 92411973002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/07/1910:19
Barium
mg/L
ND
0.25
01/07/1910:19
Cadmium
mg/L
ND
0.0050
01107/1910:19
Chromium
mg/L
ND
0.050
01/07/1910:19
Lead
mg/L
ND
0.025
01/07/1910:19
Selenium
mg/L
ND
0.10
01/07/1910:19
Silver
mg/L
ND
0.025
01/07/1910:19
METHOD BLANK: 2465706
Matrix:
Water
Associated Lab Samples:
92411973001, 92411973002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/L
ND
0.050
01/07/1910:29
Barium
mg/L
ND
0.25
01/07/1910:29
Cadmium
mg/L
ND
0.0050
01/07/1910:29
Chromium
mg/L
ND
0.050
01/07/1910:29
Lead
mg/L
ND
0.025
01/07/1910:29
Selenium
mg/L
ND
0.10
01/07/1910:29
Silver
mg/L
ND
0.025
01/07/1910:29
LABORATORY CONTROL SAMPLE:
2466417
Parameter
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2.5
2.4
95
80-120
2.5
2.4
95
80-120
2.5
2.4
96
80-120
2.5
2.4
95
80-120
2.5
2.2
89
80-120
2.5
2.4
96
80-120
1.2
1.2
96
80-120
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
LABORATORY CONTROL SAMPLE: 2466418
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Arsenic mg/L 2.5 2.3 92 80-120
Barium mg/L 2.5 2.5 98 80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 19

lacieAnalyfical"D
Pace Analytical Services, LLC
te 100
Kincey Ave. 128078
9800Hunte
sv Ile, NC
wwwpaceiabs.com
[phone]
QUALITY CONTROL DATA
Project: Wood BoilerAsh
12/21
Pace Project No.: 92411973
LABORATORY CONTROL SAMPLE:
2466418
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Cadmium
mg/L
2.5
2.4
95
80-120
Chromium
mg/L
2.5
2.4
95
80-120
Lead
mg/L
2.5
2.3
93
80-120
Selenium
mg/L
2.5
2.4
96
80-120
Silver
mg/L
1.2
1.2
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2466419
2466420
MS
MSD
92411513001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
Arsenic
mg/L
ND
2.5
2.5
2.4
2.4
94
95
75-125
1
Barium
mg/L
0.55
2.5
2.5
3.0
3.0
97
97
75-125
0
Cadmium
mg/L
ND
2.5
2.5
2.4
2.4
96
97
75-125
1
Chromium
mg/L
ND
2.5
2.5
2.4
2.4
95
95
75-125
0
Lead
mg/L
ND
2.5
2.5
2.3
2.3
90
91
75-125
0
Selenium
mg/L
ND
2.5
2.5
2.4
2.4
96
96
75-125
1
Silver
mg/L
ND
1.2
1.2
1.2
1.2
96
96
75-125
0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 19

aceAnalydical
WWW.pace1863corn
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
QC Batch: 449628 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92411973001, 92411973002
SAMPLE DUPLICATE: 2461640
92412056001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 19.0 19.6 3
SAMPLE DUPLICATE: 2461690
92412018001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 0.76 0.74 3
Pace Analytical Services, LLC
-9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 19

aceAnalytical
www.pacelabs.com
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
QC Batch: 449382
QC Batch Method: EPA 9045D
Associated Lab Samples: 92411973001, 92411973002
SAMPLE DUPLICATE: 2460748
Parameter Units
pH at 25 Degrees C Std. Units
SAMPLE DUPLICATE: 2460749
Parameter
pH at 25 Degrees C
QUALITY CONTROL DATA
Analysis Method: EPA 9045D
Analysis Description: 9045 pH
92411543001 Dup
Result Result RPD Qualifiers
8.8 9.0 1 H3
92411555003 Dup
Units Result Result
Std. Units 6.8 6.8
RPD Qualifiers
0 H3
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 13 of 19

aceAnalytical
www.pacelaftcom
QUALITY CONTROL DATA
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 449426
Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92411973002
METHOD BLANK: 2460980
Matrix: Solid
Associated Lab Samples: 92411973002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Phosphorus mg/kg
ND 2.0
12/24/18 20:36
LABORATORY CONTROL SAMPLE: 2460981
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Phosphorus mg/kg
50 52.4
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2460982 2460983
MS MSD
92411973002
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result .
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 1930
114 118 2160
2470 204 454 90-110 13 M6, R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 19

aceAnalytical
www.pacelebupm
QUALIFIERS
Project: Wood Boiler Ash 12/21
Pace Project No.: 92411973
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
BC The same analyte was detected in an associated blank at a concentration above 1/2 the reporting limit but below the
laboratory reporting limit.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01/08/2019 11:58 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 19

aceAtialytical.
wviw.Pace'84pom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Wood BoilerAsh 12/21
Pace Project No.: 92411973
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92411973001
SP1221118A
EPA 3050B
449472
EPA 601OD
449601
92411973002
SP122118B
EPA 3050B
449472
EPA 601OD
449601
92411973001
SP1221118A
EPA 3010A
450872
EPA 601OD
450977
92411973002
SP122118B
EPA 3010A
450872
EPA 601OD
450977
92411973001
SP1221118A
EPA 7470A
450873
EPA 7470A
450906
92411973002
SP122118B
EPA 7470A
450873
EPA 7470A
450906
92411973001.
SP1221118A
EPA 7471B
449576
EPA 7471B
449674
92411973002
SP122118B
EPA 7471B
449576
EPA 7471B
449674
92411973001
SP1221118A
ASTM D2974-87
449628
92411973002
SP122118B
ASTM D2974-87
449628
92411973001
SP1221118A
EPA 9045D
449382
92411973002
SP122118B
EPA 9045D
449382
92411973002
SP122118B
EPA 365.1 Rev 2.0 1993
449426
EPA 365.1 Rev 2.0 1993
449453
Date: 01 /08/2019 11:58 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 19

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
PaceAnalyiical Document No.: Issuing Authority:
( F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ® Eden[] Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
Sm
Client Name: WO# : 92411973
Project #:
' Ilui r 91°>��ss IIIIIIIIIIIII IIIIII I Courier: []Fed Ex ❑UPS ❑USPs ®Clieht '
❑ Commercial ❑Pace ❑other: 92411973
Custody Seal Present? [:]Yes [ZNo Seals Intact? ❑Yes ®No I /)�
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap ❑Bubble Bags ®None ❑ Other Biological Tissue Frozen?
[]Yes []No NN/A
Thermometer: Type of Ice: ❑Wet []Blue[None
®IRGun ID. " i) c
Cooler Temp (°C): I • J V Correction Factor: Add/Subtract (°C)
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): / �, rl []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (® N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
.. _i..a:..,. U--i; —1 Dnortn Riml? f—IYeS MNo
L JYes JnNO.
- --
Comments/Discrepancy:
Chain of Custody Present?
Yes _
[:]No
❑N/A
1.
Samples Arrived within Hold Time?
Coyes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
MNo
[]N/A
4.
Sufficient Volume?
NYes
❑No
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
[[Yes
®Yes
❑No
❑No
[]N/A
❑N/A
6.
Containers Intact?
MYes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
®N/A
S.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
/ pyes
SZ_
❑Yes
[]No❑N/A
❑No
MN/A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
[]Yes
[]No
❑No
[VN/A
N/A
11.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
C—
Date/Time:
Field Data Required? [-]Yes ❑No
Lot ID of split containers:
Date:
Date: z
Page 17 of 19

Document Name:
Document Revised: February 7, 2018
e
2ceAnalyltical
Sample Condition Upon Receipt( CUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WO# ; 92411973
PM: CDl Due Date: 01/08/19
CLIENT: 92—Baxter
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there Is -a discrepancy affecting North Carolina compliance samples, a copy or this form will be sent to the North Cargmia u[nivn Ce unCeuvu W —
Out of hold, incorrect preservative, out of temp;incorrect containers.
Page 18 of 19

RE
O
W
Baxter Biomass - Wood .Boiler As,h - Ricky, Styles:
Please test the zample(s) for the parameters: as
]fisted below.,
Send original results -to: email: ricky_styles@baxter,com.
Send invoice and copy of •resultsto: email: [e-mail]
Ricky Styles -
Baxter Biomass Purchase .Order # 195461
2859-Old Linville Rd.
Marion, NC 28752
(828), 756-6650
q2-( r M 73'
. •V Sample #~�
Sample.
Descrlption
Sample Date(s)
and time:sample,
Grab or
Composite
Total Metals -'
.As, Ba.,.Cd,
TCLP Metals
As, Ba, Cd,
Ignitability,_
Reactivity
pH
Corrosivity,
Total=Arsenic
Full TCLP
Moisture-
Content
BTU.PER
POUND
collected
Ca,- C'r,, Cu, Fe,
Cr,; Pb, Hg;
Pb, Mg, Hg,
Se,.Ag
Mn,.Mo; Ni, K,.
Se, Ag,'Na, Zn;
total-
Phos horus
SP122118A
ASH
12/21/16-1:1'5pM
COMPOSITE_
YES
YES
YES:
SP12211.813
ASH.
'12/21/181:1;5pM
COMPOSITE
YES
YES
YES
Sample spent to: Pace Analytical Services, Inc:
2225 Riverside Drive
Asheville,-NC28804
828-254-7176
Chain of Custody
11
PrQject"Manager: Tom Williams
.9800 Kincey Avenue, Suite 1,00,
Huntersville; NC 28078
(704) 875, - 9092 ext. 233
1zy
)0 1