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HomeMy WebLinkAboutWQ0001346_Annual Report_20190227RFr.FR/l=D FEB 2 7 213119 DiM. KK i10l I 9Il, OR!jIATIOiNI PROCESSIiNIG U1 II T ' 'or 1lonroe North Carolina RESIDUALS LAND APPLICATION PROGRAM CITY OF MONROE ANNUAL REPORT 2018 PERMIT NUMBER W Q0001346 REGE �E82�2019 �on_plsch unit pe��tbn9 �I�I onroe North Carolina I City of Monroe Water & Wastewater Residuals Land Application Program 2018 Annual Report Table of Contents 1. Certification Form & Annual Operations Summary 2. Annual Residual Sampling Summary Forms & Biosolids Analysis 3. TCLP Analysis 4. Field Summary Forms 5. Pathogen Reduction & Vector Attraction Reduction 6. Soil Analysis ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001346 County: Facility Name (as shown on permit): Union Year: 2018 City of Monroe Land Application Operator: Steve Holden, Land Residual Coordinator Phone: Land application of residuals as allowed by the permit occurred during the past calendar year? 0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A -Residuals Application Summary: 704-282-4679 Total number of application fields in the ermit: 44 Total number of fields utilized for land application during the year: 18 Total amount of dry tons applied during the year for all application sites. 960 Total number of acres utilizes for land application during the year: 259.9 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 21 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH'of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received fi•om the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Russell Colbath, P.E., Water Res. Director 2^ lg -?q Permittee Name and Title (type or print) Signature of Permittee e Date )1�-' Sign ea ruru of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) Monroe North Carolina February 20, 2019 North Carolina Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: City of Monroe 2018 Land Application Annual Report Permit No: WQ00013463 City of Monroe personnel performed application events during 2018 on the permitted fields for the City of Monroe. A total of 5,488 Cubic Yards for a total of 960 dry tons of residual solids from the City of Monroe Wastewater and Water Treatment Facilities were land applied. If any further information is required regarding this land application report, please do not hesitate to contact Mr. Kyle Ketchum (704) 282-4612 or Steve Holden (704) 282-4679 with the City of Monroe. Sincerely, Russell Colbath, P.E. Director of Water Resources C: I: 8040 WWTP and Collection\ Land Application\2018\ correspondence CiLy of N/Ionroe + PO Box 69 + Monroe, NC 28111-0069 Tel: (704) 282-4500 + Fax: (704) 283-9098 www.iitoni,oeitc.org OPERATION SUMMARY Permit # W00001346 FIELDS USED IN 2018 NAME NO. GALS GALS YARDS YARDS Dry Tons DryTons (Ibs/ac) Calvin Morris 1 1 18-Apr 1 10.8 1 245 41.68 75. 03. Harry 1 8-Apr 35.5 00 5 .05 7. 5 Myers 25 5.18 1.50 NC-UN-18 278 47.29 25.90 2 34.2 225 34.10 10.84 240 40.83 23.21 245 41.69 23.69 117 26.40 12.11 7 4 5.4 75 11.43 55.94 5 Wayne ep 1 6.5 89 15.53 45.76 McBride 18 Sep 42 8.70 6.64 3 8- ep 1 14.155.3275. 4 Emerson I 18-Aug 18-Aug 15.4 5 56.72 94.87 McBride 84 17.4 6.41 NC-UN-26 2 18-Aug 6.1 125 21.81 92.12 3 18-Aug 10.5 203 35.42 86.91 4A 18-Aug 18-Aug 12.1 275 47.99 102.17 42 8.70 4.08 4B 18-Jul 12.7 1 175 30.54 61.95 18-Jul 1 50 10.35 4.63 6 18-Jul 14 289 50.43 1 .80 18-jul 4Z 3.b Leland 1 8- pr 13.4 225 3 . 7 55.5 Wolfe 18-Apr 50 10.40 7.95 - -7 2 8-un William 1 18-May 24.5 7.4 351 59.71 47.38 Griffin 3 18-Apr 145 24.66 64.81 NC-UN-29 18-Apr 50 10.39 14.39 4 18-Apr 7.2 78 13.27 35.83 g_ ay 5 .5 7 Tom 8- ay 3. 325 55.29 5 Appenzeller Totals 259.9 �0� 4,711 777 807.98 151.60 Total Gallons 0 Total Yards 5,g8g Total Dry Tons 960 WWTP- Metric Tons 732.84 WTP- Metric Tons 137.50 Total Metric Tons 870.34 ------ ---- - -- ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source WO # or 3) NPDES #: NC0024333 4) WWTP Name: Monroe WTP (cake) 5) A & L Eastern Lab. Inc. xesiauai Analysis Chia Ceiling Sample or Composite Date Parameter Conc. 3-20-18 6-11-18 7-9-18 10-1-18 (mg/kg) Limit Percent Solids (%) NA 17.99 24.68 24.59 26.8 Arsenic 75 4.25 20.1 17 45.2 Cadmium 85 33.5 2.7 2.62 3.11 Copper 4,300 374 499 542 612 Chromium NA inn 189 222 195 Lead 840 21.8 7.95 6.87 6.54 Mercury 57 0.0249 < 0.4 < 0.4 < .0151 Molybdenum 75 43.5 42.6 49 43.2 Nickel 420 21.2 37.8 35.3 1 35.2 Selenium 100 < 0.5 < 5.0 < 5.0 < 25 Zinc 7,500 97 390 201 368 Total Phosphorus NA 2970 6400 1980 4360 TKN NA 13200 12200 5770 19100 Ammonia -Nitrogen NA 1390 2270 1100 746 Nitrate and Nitrite NA 16.4 17.3 64.2 128 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nFNR pnRen RccF r����nnal ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00001346 Laboratory: 1) Facility Name: Residual Source NPDES # or WQ#: WWTP Name: T _ 1 City of Monroe NCO024333 Monroe WTP (cake) 2) -_ 3) _ 4) _ 5) nV5 U"U" jaaa Lana Sample or Composite Date 3-20-18 6-11-18 7-9-18 10-1-18 Parameter (mg/kg) Potassium 393 574 190 347 Sulfur 2670 4890 3040 3340 Calcium 1680 4770 1800 4680 Magnesium 490 770 318 635 Sodium 544 502 281 479 Iron 284000 279000 330000 306000 Aluminum 4980- 4160 2850 3350 Manganese 310 803 585 1250 Organic N 11810 9930 4670 18354 pH ( standard units) 5 6.5 5.9 6 Volitile,Solids % 35.33 44.08 37.23 31.4 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -Si—at4re of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) nr-nin Gnana Qccr - a ie)»nna% ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0001346 Laboratory: 1) Contract Labs Facility Name: City of Monroe 2) Residual Source WQ # or NCO024333 3) NPDES #: 4) WWTP Name: Monroe WWTP (cake) 5) Residual Analysis Data Ceiling Sample or Composite Date Parameter Conc. 3-20-18 6-11-18 7-9-18 10-1-18 (m&g) Limit -Percent Solids (%) NA 16.42 20.2 20.72 18.1 Arsenic 75 8.79 16.6 11.7 23.4 Cadmium 85 9.63 1.8 < 1.0 < 1.0 Copper 4,300 332 495 364 406 Chromium NA 118 167 112 117 Lead 840 15.3 11.8 13.5 12.9 Mercury 57 0.173 < 0A < 0.4 0.0472 Molybdenum 75 28 37 22.5 24.4 - Nickel 420 36.9 45.7 49.1 49.4 Selenium 100 I< 0.5 < 5.0 < 5.0 < 5.0 Zinc 7,500 587 601 738 867 Total Phosphorus NA 11200 11100. 14500 13900 TKN NA 34400 28200 28000 40700 Ammonia -Nitrogen NA 5110 6240 5740 4140 Nitrate and Nitrite NA 30.3 12.6 29 172 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference.the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ;001 1!6 1IN- Signature of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) rnCKID �rtone oeeC 14')M M ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00001346 Laboratory: 1) Facility Name: City of Monroe 2) Residual Source 3) NPDES # or WQ#: . NC0024333 4) WWTP Name: Monroe WWTP (cake) 5) Contract Labs Residual Analysis Data Parameter (mpg) Sample or Composite Date 3-20-18 6-11-18 7-9-18 10-1-18 Potassium 1040 886 983 918 Sulfur 6710 6670 7500 7970 7320 7510 10200 11300 .Calcium Magnesium 1220 669 1160 610 1340 599 1500 666 Sodium Iron 149000 220000 145000 147000 6110 5720 6410 6230 Aluminum Manganese 863 29290 6.6 53.28 1030 21960 7.3 48.31 1160 22260 7.5, 51.54 1440 36560 6.9 45.1 Organic N PH ( standard units) Volitile Solids % "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witn a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �11,G, �u-- �115119 * Date >ignature oreparer *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .l 102 (26) nFNR Fnpu RRCF - R t19nnw City of Monroe Reports of Lab Analysis 1st 90 Days Page: 1 of 1 Report Number: 18-080-0229 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 3/20/2018 10:00:00 Lab Number: 59302 Date Received: 03/21/2018 00:00 Sample Id: RAS Date Reported: 03/23/2018 e o oil 03/21/2018 14:00 SM-2540G Total Solids * 1.48 14800 100.0 BW1 Moisture * 98.52 100.0 BW1 03/21/2018 14:00 SM-254OG Total Volatile Solids 75.67 756700 100.0 BW1 03/21/2018 14:00 SM-254OG Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole orpart. nor may any reference he made to the worn. the results, orihe cotwany in any advertising, news release. or other public announcements without obtaining ourprior va'illen authorization. �W« m 60 Pauric McGroary Agronomist r 8-080-0229 m SAMPLE TRANSN ii�iiiiiiiiii�iiiiiiiiiiii�iiiii�i�iiiiiiiiiiriiiiiiiiiiii�iia�i�201r�20,8A&L F ci1VolMonrce ,2.?5:30 RAS 7621 White ine Office Information UU310rner 1111urr11ar1un Rept# Subrnitted'By Charge To; Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 isholden@monrociic.org Lab Number (Lab Use Only) Sample ID _; Container"T 'pe: . ;'.;; Sampled-D'ate: x - Za_ i Date Recd: RAS Glass (Yes or No) Same led Time:, vt0J Time Recd: Plastic (Yes or die) Sam' led 5g.-, Recd. B -, in uished' "'' (Signature) Date Time . Received 6' : (Sighature) Date Time 2,! Please -Place a "X" by Desired Tests Internal Lab code: `'` ' " M. f Z N�NO3=s ;Nlitl•/ N X t#M ti 0$ o? � ry one 0 'So ~L�F X ,..y. Ti11 - i .1: *'W �:"- : w tU': a "Be. F,�. .. �. ALK - SS - ¢ aAvaii,.Pi~"' Sol; 4 = `Cbni1 WIN i t SOL B,, #20; ;;Sieve#,80 S1eve#1,00 ASH"Eal7a;;' .6aCQ3,;i MgCO3', -,MdOs; C/N 7,:' +' ,'aT0`G°1=,;. ,Env, r ,�� 'L ,'..P205 ;;; i" i TOTAL'. n •" K20: �. �'' - - N4 � .� � ; TNT �' Y`'. .�', r, . n '� L :'fie t-TKNti'U;, _ "9' - jt 4. ' H. 1 __ _ ",� ti Y R O 3W a ��2•'".".�� a}`': �ORGN=W� �'C R SPA. E , T,; �h� Wit...... �;:�" >AZ'CERT __ ..1- .?u. ,' " '�BTU�: � �'- ;a;=. x` "'PGBS='�> �� :S sRE;4GT GN' ;�'..,., . — ..i •: F.E CAL::'. '?.�•..ar �,S• C L' ;.T P��' `.LCR State Certification, Needed: NORTH CAROLINA Special Instructions or Remafks Comments Page: 2 of 2 Report Number: 18-080-0227 Account Number: 46205 Submitted By. Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 REPORT OF ANALYSIS Lab Number: 59300 Sample Id: WWTP Cake Total Cadmium 9.63 Total Chromium 118 Total Nickel 36.9 Total Lead 15.3 Total Arsenic 8.79 Total Mercury 0.173 Total Selenium <0.500 pH * 6.6 Total Volatile Solids 53.28 532800 Total Molybdenum 28.0 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 3/20/2018 10:30:00 Date Received: 03/21/2018 00:00 Date Reported: 03/30/2018 0.100 JTR 03/28/2018 01:46 601 OC 0.250 JTR 03/28/2018 01:46 601 OC 0.250 JTR 03/28/2018 01:46 6010C 0.300 JTR 03/28/2018 01:46 6010C 1.00 JTR 03/28/2018 01:46 601 OC 0.0133 KKM 03/27/2018 12:42 7471 A 0.560 JTR 03/28/2018 01:46 6010C 1.0 JM 03/22/2018 08:15 9045D 100.0 BW1 03/21/201814:00 SM-2540G 0.250 JTR 03/28/2018 01:46 601 OC All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and contidenlial use or our clients. and may not be reproduced in whole or part nor may any reference be made to the uvot k, the results, or the company in any advedising, news release. or other public announcements without obtaining ourprior written authorization. ?ctW« me Gawr Pauric McGroary Agronomist Pace 3 of 3 Page: 1 of 2 Report Number: 18-080-0227 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 59300 Sample Id-: WWTP Cake Waypoint Project: WWTP Cake REPORT OF ANALYSIS VA 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 3/20/2018 10:30:00 Date Received: 03/21/2018 00:00 Date Reported: 03/30/2018 Total Solids" 16.42 164200 100.0 BW1 03/211201814:00 SM-2540G Moisture ` 83.57 100.0 BW1 03/21/2018 14:00 SM-254OG Total Kjeldahl Nitrogen 3.44 34400 50.0 JM 03/22/2018 08:15 SM-4500-NH3C-TKN Total Phosphorus 1.12 11200 5.00 JTR 03/28/2018 01:46 6010C Total Potassium 0.10 1040 50.0 BKN 03129/2018 13:15 6010C Total Sulfur 0.67 6710 5.00 JTR 03/28/2018 01:46 6010C Total Calcium 0.73 7320 5.00 JTR 03/28/2018 01:46 6010C Total Magnesium 0.12 1220 5.00 JTR 03/28/2018 01:46 6010C Total Sodium 0.07 669 25.0 JTR 03/28/2018 01:46 6010C Total Iron 149000 50.0 BKN 03/291201813:15 6010C Total Aluminum 6110 5.00 JTR 03/28/2018 01:46 6010C Total Manganese 863 0.500 JTR 03/28/2018 01:46 6010C Total Copper 332 0.250 JTR 03/28/2018 01:46 6010C Total Zinc 587 0.500 JTR 03/28/2018 01:46 6010C Ammonia Nitrogen 0.51 5110 50.0 R D 03/22/2018 08:15 SM-4500-NH3C Organic N 2.93 29290 50.0 03/22/2018 08:15 CALCULATION Nitrate+Nitrite-N 30.3 2.39 MMT 03/23/2018 09:07 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repoas and letters are for the exclusive and confidential use of our clients. and may not be reproduced in :whole or part. nor n7ay any reference he made to the +,vork. the results, or the rompany in any advortising, not -is release. or other public announcements without obtaining our prior written authorization. Pauric McGroary Agronomist Pace 2 of 3 SAMPLE TRANSMITTA 03 18' io'iii�iiiii�iii0iiiiiiiii�iiiii�iiiii�iiosii�ii A&L Easters C,N 111-1}a 11.34.51 HVWTP Cake Office Information ..�.��r���Go;;rnrorrnatlon Rept# 5utimitted;'By - IC To. Copy To Project Steve Holden City of Monroe Qccf# POB 69 Email .- 46205 Monroe NC 28111 sholden@monroene.or� Lab Nurribee,;(Lat U e;Only)'- ' Sample01D" : _ pet;_ Sampled;Date:,. - Date''Recd" W WTP Cake Glass (f or No) Sam"led .Time: v.'3 Tfine-Redd:. Plastic (Yes or+M} sbhipled•;B ' ' Recd.By.: - - Relin Date, Received;B :'(Signature)':' :'.'Date' ime Please Place a X by Desired Tests Internal Lab Code: SLMONR u . ., 'o ;Sl��li�ls,,fop:�:},.,TKN.�,: : :; tr • �: ,� Gt �ra�,. ';?� _tR��•�.0 na; �t�, .,K...:ir¢+: ,�. F• -->, _, S. x.• ,� ••.�., - .Gax ;: �~�.�` m ,.x •�h _i"� °'f,,.�1�19., s.- - tom:, Na'::;,;_`� ".� ': a c•-^{t; ' i, a.Y» F®:,,_ 'its 1.- t tr `::-; , i>. , _ „J 7.b., -��`.,AI, tl � :a; x `.A%:', �.Miibx�._. t,. , w,�..... �,C'u+�� .. i .,. , -'r ;.slZntx: r •.b` .�NHA.'s,1,d.,.,-.f�,O3;.N1.. 1' k :i x x x x x x x x x x x x x x x :tl :tl, c;+�;''r,.• 11 .i ., °bl a;-,. •.'art.] X r t"• ' i b$ '°� ^ cd, ,:i;z;,., -,§.; +rti" ; : ,i.0 �•'•.� .U''g i, 9:, i � i 1 A :iS} i�:lir 't. :i� rs.,, , - r' '!.ja;*.i 'ix. .�;,�}� . ��, ,t:+Sf t!y'Y. a •.1' "�F ". i?I�i•.i `T `LS •,.: .'a. .e �'_- >�4, _ ",. i4• �`�*•. .mot . `*tt : Pb1, k S':i' ,�� :C'--, .>,a i`"."x'' 'e -; i8e..,.k,"lu,Y•CF .#.y J..i t. w':>{ .r :.t 1.-, 1,. As.., n'*:,. r, r.^p nsT r�x�}f•a., t,:- .yi''..r;, ,... .:.}t�. � `-F=: x'.�i', .,..x. } k•^ v("5:.. , ti) x" ',Li" S � aPCk_�. ,yC.r.*..r.-,< t "}�. ' t Se._ :+t i`i ,E:�ri+:'' ",Y, ..� ,. x, :� .ux`�S'1-,1%'. nL• 11`. •„ r� .tom ,-6.p'GO ... i. w'�, ='i`• 3#" � x� i., ° _i.. 'it ,'Volatile ik+.giliLp..: �.. S�: z `0 J, 1;y;.a fr� ,x?t- )<a...J .'t . 2. .�.. .. tx...t +�, Y"ytrn;;.=, .:«t 's.t .. a, +4 .%e.., 9':. .,{". ^'•,v, .k t: i. .'°r*-t ".•,�',,. .�Y4i d..,, b}d 5 �., C, s^ °.t ^� G:3a {..f. �':w .}t Sri' •iii� "i :e+`ii" 1 _•�.i . .,� Ba xX. x x x x x x x x x x x 'r.-a, t.So?#raE.tAgir„Ic•i:,::3ii;S;=.. t • t;.t: �.. ri a.•t.' 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'".1deC N.1 a..:•",>is �,., `p::W'r�€';tY.x;. .'a:F rxx«^}'? v4a., u.,-"M';"'364<e 1 I.it,'„r ,t� .4'.° "tt' ',.','�•, � ;'"�_' �:,f1T:� R '} ':i`1.;,7:Y ,t �., ,+1 ' N'' ig to •7,, •T,CLPw ° rvt.,. ... ;R'Q'.: :��+:.••.:,. ',i� lCf2,r State CertifcatignsNeeded: NORTH CAROLINA S'=eeialInstnictloris;o Re'ma"ks: Comments 1 Page: 1 of 2 Report Number: 18-080-0228 Account Number: 46205. Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 59301 Sample id : WTP Ferric Cake Waypoint'-.0 ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 3/20/2018 10:15:00 Date Received: 03/21/2018 00:00 Date Reported: 04/03/2018 Total Solids ` 17.99 179900 100.0 BW1 03/21/2018 14:00 SM-2540G Moisture " 82.00 100.0 BW1 03l2112018 14:00 SM-2540G Total Kjeldahl Nitrogen 1.32 13200 50.0 JM 03/22/2018 08:15 SM-4500-NH3C-TKN Total Phosphorus 0.30 2970 5.00 JTR 03/28/2018 01:51 6010C Total Potassium 0.04 393 5.00 JTR 03/28/2018 01:51 6010C Total Sulfur . 0.27 2670 5.00 JTR 03/28/2018 01:51 6010C Total Calcium 0.17 1680 5.00 JTR 03/28/2018 01:51 6010C Total Magnesium 0.05 490 5.00 JTR 03/28/2018 01:51 6010C Total Sodium 0.05 544 26.0 JTR 03/28/2018 01:51 6010C Total Iron 284000 100 BKN 03/301201818:20 6010C Total Aluminum 4980 5.00 JTR 03/28/2018 01:51 6010C Total Manganese 310 0.500 JTR 03/28/2018 01:51 6010C Total Copper 374 0.250 JTR 03/28/2018 01:51 6010C Total Zinc 97.0 0.500 JTR 03/28/2018 01:51 6010C Ammonia Nitrogen 0.14 1390 50.0 R D 03/22/2018 08:15 SM-4500-NH3C Organic N 1.18 11810 50.0 03/22/2018 08:15 CALCULATION Nitrate+Nitrite-N 16.4 2.24 MMT 03/23/2018 09:08 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Pam« Ourreports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made to the work, the results, orthe company in any advertising, news release. orothar public announcemonts without obtaining ournrior wrillen authorization. Pauric McGroary Agronomist Paae 2 of 4 Page: 2 of 2 Report Number: 18-080-0228 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 59301 Sample Id : WTP Ferric Cake 0 V r, 0 0 �� u 7621 Whitepine Road, Richmond, VA 23237 VaypoMain 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 3/20/2018 10:15:00 Date Received: 03/21/2018 00:00 Date Reported: 04/03/2018 Total Cadmium 33.5 Total Chromium 199 Total Nickel 21.2 Total Lead 21.8 Total Arsenic 4.25 Total Mercury 0.0249 Total Selenium <0.500 pH * 5.0 Total Volatile Solids 35.33 353300 Total Molybdenum 43.5 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 0.100 JTR 03/28/2018 01:51 6010C 0.250 JTR 03/28/2018 01:51 6010C 0.250 JTR 03/28/2018 01:51 6010C 0.300 JTR 03/28/2018 01:51 6010C 1.00 JTR 03/28/2018 01:51 6010C 0.0133 KKM 03/27/2018 12:43 7471 A 0.500 JTR 03/28/2018 01:51 6010C 1.0 JM 03/22/2018 08:15 9045D 100.0 BW1 03/21/201814:00 SM-2540G 0.250 JTR 03/28/2018 01:51 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our repoas and fetters are for the exclusive and confidential use of'our clients. and may not be reproducad in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release, orotherpublic announcemenls without obtainlna ourprior vrritten authorization. ?of if- OF 60"tr Pauric McGroary Agronomist Paae 3 of 4 SAMPLE TRANSMITTAL City Of illMonroe 03llll!l1191�11181111111illillllllllllll161�IIIllll188 A&L Eastern . WTP Fertic Cake 12:21:49 g 71'mn71 Whito.,i.P P—d Ri,V1 V A 74 1 , , -_. ._.--- .-- Office Information _ . ° ' :Custoiier Infiarriiatimn ;- -Rept#: S'tilimittia&By.:,." `; ` ' Charge"1`o' Copy T6 Oct`Proj Steve Holden Ci of Monroe Acct #. POB 69 Email 46205 Monroe NC 28111 sholden(a).monroene.ore b+J.se,Only) -ConanerLab.Num6er-(L D6 Recd:D WTP Ferric Cake Glass Wee -or No) Sam'led-Time: Tiine:Recd:. Plastic (Yes or Ne)- Sam "led.B; ,,R" lin wished B Si' nature :", _ ,: " _ [J;atei Timer ': ; . . '_' ReeeivedB :. Signature) -'Date Time I ease,P'Iace , "X" 'by d@Sli`GCi , .a`2', TBStS Internal Lab Code:- SLMONR t t ..S..Oldit3.:to' Ira .'{v' j yy�x `i sri - .a• ''-$:;.., !$' ,c.. ii. P."..v,<.-...,"s,.�K`.:AF:t; + i`Y;:e �..•i-'^�n�: :`!y� 5 _..'`a.r `a• s., tet� 'y; ».:a'"�f A ,w ,-. d',^ wrj i'%; ti, '"'�y; a' ».w; "^,`,^. r x ... i t ..y+"w a °i .' "1 `I �'.:,:,-> ^•.,� �`.. : :: iiF., ..,Ay v; i;,�� .,,_ x.i.- o-L <= d°°tom_ f7n ) S. NH,4=N„ u> i:NO3- ci X x x x X X x X X x X x ;:•�F�'� '=ti ap .i�, € , c .+ 4 tl' +$q 'Y++v -. �'k _. `�:;• ac3+^'`i<` F .�yyy.,, .i: "" ��**..ryryrrf1 ppy•�..,.iyx` '": CXC .Y.4'6.,.4" 5;. v^. ,`e.;:` •"+ett"` 3a' % !,,. ¢,. ..• [;,',..%+ _z?i e .�.,a .6�d._ }}4'�X`1l:,a+� .` g ads 3 3�• ; (]{ r"eV..' • fnl �l�f. 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F _.��`Wilyt:�i s iP 4B:QL'Ni13&:®a iSP:C lS S x Slie#Yi s j_ iev ` .a` _(err €i 0 i M....COS'" l"t,,. �,.�I•..¢�a r.,u$wt.h?Atx3t�!2.a_L/.4�1• 1F'.'...a• "i:t i K�.aiI:,J�; �•i;' a,� }"4.:o"mob1 g",�'xa ».�j 4F°, ttN" i'.mot -;f�. 4 '.;��, ', '�.,:�,, p�,'i'�1t.:v. tN?R. , _ �•:""s' ,'w: 6 k.:. °E'AQ i`_ C�,► Ar'.»::'d "Sfafe`C6fflficatioh Ndddd d , NORTH CAROLINA ti Special Instiuctions-oi'Remp..s _�;;,: ;;. Comments G City of Monroe Reports of Lab Analysis 2nd 90 Days' Report Number: 18-164-0203 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 61166 Sample Id : RAS Total Solids Moisture Total Volatile Solids Comments: NC CERT#257 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 6/11/2018 06:30:00 Date Received: 06/13/2018 00:00 Date Reported: 06/1512018 PANALYSI!�'- ALOST •■ 0.95 9500 100.0 R D 06/13/2018 12:30 SM-2540G 99.04 100.0 R D 06/13/2018 12:30 SM-2540G 66.66 666600 100.0 R D 06/13/2018 12:30 SM-2540G All values are on a dry weight basis except as noted by asterisk. Detection limit -on all N series is on a wet basis. Cur reports and letters are for tire exclusiJe and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release. or other public announcements without obtaining our, prior written authorization. PW« m` Pauric McGroary . Agronomist Paqe 2 of 4 SAMPLE TRH( II AC IIIII�II�fIIIIIIII�I�III�II�IIIII��III�IIIf�II�III�III���IIIII��I 7621 W City of Monroe RAS Office Information Rept# Submitted By �nrarge f o rODY -- - - -_-- 06205 0203 ,3-25 1 D:37:25 j fig. Copy To Project Steve Holden City of Monroe Acct # POB 69 Einail 46205 Monroe NC 28111 sholdenil monroenc.ort� Lab Number (Lab Use Only) Sample ID Container Type Sampled Date: — J — Date Recd: �LQ RAS Glass (Fes or No) Sampled Time: Time Recd: Plastic (Yes orUG) Sampled By: Recd I3y: Reli'nquis ed B :'(Signature Date Time Received By: (Signature) Date Time Please Place a " " by Desired Tests Internal Lab Code: Gar Cu, :. :Zri'...'!NH4=N` NO3FN: x .:{` , " .a, _ tea. W �:2rc.ib zt 4 L'' 'Itn,i• ." 'mot rY `.x1 S, !fi : _ �\^ i :� _ t'ii _ -_> _ H. o. dIa 116 -o, _ td'� ., •rj r" ' 1 t X .1 'T".i .,:SO4a,° i•}. ;;4g;4. _ _,..y, Sti - _ ,.•�,.> '.Co: -,i �_.. $n .+:' .ti,,;, 's€=' T;f•:,- ° f"S.' 1>w:ll' =•U..,.... - ' Be:" .-t:'•^ tVO `k - ,!SS `r ; : Avai P ; r' 1. tin: Sol K; Cond' WIN : ' SOL:B ,SCQLa. ' , W 2i <+O& "..._..G" `SP:GR 1 .... a... . = .. TSS'+': Sie`ve#20 r :Sieve#80 sSleve#:1'00 ASH::- _Ga0'+="; CaGQ3 ` :_lU("CQ3:: 9 MgO: C/N:. ;.T,,OC.:+- ;Env TO, ;ALA °,���:F?2Q5'' r:k ' OTAL'" +! , .K2Q;';•f :�t. �;. _ - '7ias; �TKNW�:.�_;,N•H4W'.i;,..N.� t a . kc :+ "3 1N't::i -: :O G R N,W'`;PA„-E z` C � RT .+ +AZ•:CERT c:sU - ,8l'tJ:,� �:z,- r . ";P, B S _ RAT, E C ''s - `CN:.��;'S.��FE C`r' AL�' :i,•: Via, P.:»' T L�, �C' n :I C R State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments Nr 1 Report Number: 18-164-0202 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 a Way %Wo� in, ANALYTICAL Project: W WTP Cake 76211Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 6/11/2018 07:20:00 Lab Number: 61165 Date Received: 06/13/2018 00:00 Sample Id: WWTP Cake Date Reported: 06/22/2018 Total Solids" 20.20 zuzuuu -tuv.0 RLJ —.�,��. ,�•�� Moisture ` 79.80 100.0 R D 06/13/2018 12:30 Total Kjeldahl Nitrogen 2.82 28200 50.0 R D 06/14/2018 08:30 Phosphorus 1.11 11100 50.0 BKN 06/21/2018 01:47 Potassium 0.09 886 50.0 BKN 06/21/2018 01:47 Sulfur 0.67 6670 50.0 BKN 06/21/2018 01:47 Calcium 0.75 7510 50.0 BKN 06/21/2018 01:47 Magnesium 0.12 1160 50.0 BKN 06/21/2018 01:47 Sodium 0.06 610 250 BKN 06/21/2018 01:47 Iron 220000 500 BKN 06/221201813:53 Aluminum 5720 50.0 BKN 06/21/2018 01:47 Manganese 1030 5.00 BKN 06/21/2018 01:47 495 2.50 BKN 06/21/2018 01:47 Copper Zinc 601 5.00 BKN 06/21/2018 01:47 Ammonia Nitrogen 0.62 6240 50.0 R D 06/14/2018 08:30 Organic N 2.20 21960 50.0 06/14/2018 08:30 Nitrate+Nitrite-N 12.6 2.48 MMT 06/15/2018 09:13 k D t t' limit on all N series is on a wet basis. SM-2540G SM-4500-NH3C-TKN 6010D 601 OD 601 OD 6010D 601 OD 601 OD 601 OD 6010D 601 OD 601 OD 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 All values are on a dry weight basis except as noted by astens e ec ton 071 Our reports and t er are for the exclusive and confidential use of our clients. and may not be retxoduced in whole or part. nor may any reference be made V ett_ s to the : oix. tha results, or t17e cempary in any a<ivotttsiny, news release, er othe yx7btrc announcements mthout oblaininy Darr prior rrrittan autho zafion. Pauric McGroary Agronomist Page 4 of 7 Report Number: 18-164-0202 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 61165 Sample Id : WWTP Cake 9 t,� 7621 Whitepine Road, Richmond, VA 23237 WaypoinMain 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: W WTP Cake REPORT OF ANALYSIS Date Sampled: 6/11/2018 07:20:00 Date Received: 06/13/2018 00:00 Date Reported: 06/22/2018 Cadmium 1.80 Chromium 167 Nickel 45.7 Lead 11.8 Arsenic 16.6 Mercury <0.400 Selenium <5.00 pH * 7.3 Total Volatile Solids 48.31 483100 Molybdenum 37.0 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 1.00 BKN 06/21/2018 01:47 601OD 2.50 BKN 06/21/2018 01:47 6010D 2.50 BKN 06/21/2018 01:47 6010D 100 BKN 06/21/2018 01:47 601 OD 5.00 BKN 06/21/2018 01:47 601OD 0.400 SMC 06/14/2018 18:31 SW-7471 B 5.00 BKN 06/21/2018 01:47 6010D 1.0 R D 06/14/2018 08:30 9045D 100.0 R D 06/13/2018 12:30 SM-2540G 2.50 BKN 06/21/2018 01:47 601OD All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use or our clients. and may not be reproduced io wrote or parr. nor may any reverence be made to the work, tho results, or the company in any advanishV. news release. or other public announcements without obtaining our prior writton aulhorization. powf« Pauric McGroary Agronomist Page 5 of 7 . ,amm is_164-0202 SAMPLE TRANSIT I���`�A���������������I�����I�����0����I��O��li�llllllllllill ao206:;o,a T 52,� A&L L- Cily of Monroe: 14 ` WVVTP Cake ILEWhile inc Office Information Customer Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden@nipnroenc.org Lab Number (Lab Use Only) I Sample ID' Container -Type Sampled Date: -/ -/ Date'Reed: ���0� W WTP Cake Glass (lies or No) Sam led Time; %• 2a Time Recd: Plastic (Yes or Pie) Sampled B ; al ,� ',✓ Recd-By: Relin uishdd By-' (Signature) Date Time Received By: (Signature) Date Time i 7•'y Please Pla,}ce a ' " by Desired Tests Internal Lab Code: SLMONR . ir0 Soil ds. /o^ ;.ly .,. r., :rTKN tK.i., ti,R:, to % a.Pf..s' <K F: .[:.L'r.:ti S, :G" a's tl. `,1. ::Mg,..,. �`,t l'. Na:...r ;Fe:i 1 AI,; c; - 'Mn`l< ��:?: i:: .,Cu:,i • t ;<r L'I Zn_c NH, - ,., x x x x x x x x x x x x x x. x. �Is.p{r,rj,rxxyfi, .!w dt ,:�' 't 2i•f'• tit :3��` .'.?4i1i•=:,' '{" ,{�*. t i f .! _iF:•, :l•'y'r •.rx�"i:ti.'"t=ttz� f' rc.r- ..F r,.w',t._ ,'. •'>•i .'Y' ;a� .:_:i c:r; :'i��'�. .w: <.'• c,'°"s;a':'' - .,!• § :�'. - :; •€� I} i,; i�}^'� ;,i•.=u,,: ~a; H: - e(j C"• f � O . Il+ �:E o��_' :t ,f�.. - i.,' "•o' �� Solids••% +'ir1'.. •fit• :,Or :'4. :��':;' ^i• � •rd �•i ,Mo'''� s-.i:•, ,t t. ,i. I�� ;:t ,. :ty,_, ,.,. CL:=.:,a -- _ ., '�' - ,. v 1: r. '•ar' �=vi ,'j:!'�., x x x x x x x x x x x rC�!; rT irS��L;'J'a r' 'r•:::,' .ir j.arY^ ;i0' 4� '�t'.ix'a4.a',=.'.2: >:.'+'=rr „•i —':�.; - - �.':�SS;� ArcailfP";`;'';�WIPI;�=,.,.;SOL�Bi; •,;.Y 1. IS`IiNA;; j`Q'BiGi^"•'.';=SP:;GR:''s;:TrSS",`.'Siive#20S1e'e#t30''SieVe#1t)0 v._ 'WASH: s�: <c)Ga0' �.;_i , CaG.031? 9. CO3:x ' M"O`-' �. _ g .� , `° ._ I.;aC1Nk; DAi5L.. ,n.,. i' T`OK2T0A"L F+ .i!rxt. I. a.:�xi!:T.'� t T�11,: :,�r_'§ rp:T'r. yi'Kh1W,• r- N'; H.�,4`•F'y;;;Vi,,.l^ot, �..`f}103W"`• rt '`;fi?;ta "Vy1�1: .; QfG.N;;;PA:•'EFl ; Fg:?`; • rgZi,�Ci�"'E:a`:fi=�.�' T.•; ,.f C - - ¢af. `r -;`-9 FEG c7<;, TaGt, :s sR�a•1:.��, !•IG•� State Certification 'Neecled: NORTH CAROLINA Special Instructions or Remarks Comments 0 r a Report Number: 18-164-0201 Account Number: 46205 Waypoint 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 Submitted By: Steve Holden ANALYTICAL www.waypointanalytical.com Send To: City of Monroe Project NITP`Ferric Cake Steve Holden 775 Treeway Dr Monroe, NC 28110 REPORT OF ANALYSIS Date Sampled: 6/11/2018 07:15:00 Lab Number: 61164 Date Received: 06/13/2018 00:00 Sample Id WTP Ferric Cake Date Reported: 06/22/2018 nzzKE a oLST 00 e Total Solids ' 06/13/2018 12:30 SM-254OG 24.68 246800 100.0 R D Moisture ` 75.32 100.0 R D 06/13/2018 12:30 SM-2540G Total Kjeldahl Nitrogen . 1.22 12200 50.0 R D 06/14/2018 08:30 SM-4500-NH3C-TKN Phosphorus 0.64 6400 50.0 BKN 06/21/2018 01:42 601 OD Potassium 0.06 574 50.0 BKN 06/21/2018 01:42 601 OD Sulfur 0.49 4890 50.0 BKN 06/21/2018 01:42 601 OD Calcium 0.48 4770 50.0 BKN 06/21/2018 01:42 601 OD Magnesium 0.08 770 50.0 BKN 06/21/2018 01:42 601 OD Sodium 0.05 502 250 BKN 06/21/2018 01:42 601 OD Iron 279000 500 BKN 06/22/201813:48 6010D Aluminum 4160 50.0 BKN 06/21/2018 01:42 601 OD Manganese- 803 5.00 BKN 06/21/2018 01:42 6010D Copper 499 2.50 BKN 06/21/2018 01:42 6010D Zinc 390 5.00 BKN 06/21/2018 01:42 6010D Ammonia Nitrogen 0.23 2270 50.0 R D 06/14/2018 08:30 SM-4500-NH3C Organic N 0.99 9930 50.0 06/1412018 08:30 CALCULATION Nitrate+Nitrite-N 17.3 2.40 MMT 06/15/2018 09:12 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all ,N series is on a wet basis. our reports oad letters are for the exclusive and confidential use of our clients. and may not be reproduced in whote or part. nor may any reference be made to the wor '. the results, or the company in ary.adverbsing. news release, or other public announcements without obtaining our pnor ririlten authorization. Pauric McGroary Agronomist Perna d of 7 Report Number: 18-164-0201 Account Number: 46206 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 61164 Sample Id : WTP Ferric Cake Waypon-it IUDANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 * Fax 804-271-6446 www.waypointanalytical.com Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 6/11/2018 07:15:00 Date Received: 06/13/2018 00:00 Date Reported: 06/22/2018 Cadmium 2.70 Chromium 189 Nickel 37.8 Lead 7.95 Arsenic 20.1 Mercury <0.400 Selenium <5.00 pH * 6.5 Total Volatile Solids 44.08 440800 Molybdenum 42.6 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 1.00 BKN 06/21/2018 01:42 601OD 2.50 BKN 06/21/2018 01:42 601 OD 2.50 BKN 06/21/2018 01:42 601OD 3.00 BKN 06/21/2018 01:42 601OD 5.00 BKN 06/21/2018 01:42 601OD 0.400 SMC 06/14/201818:29 SW-7471B 5.00 BKN 06/21/2018 01:42 601OD 1.0 R D 06/14/2018 08:30 9045D 100.0 R D 06/13/2018 12:30 SM-2540G 2.50 BKN 06/21/2018 01:42 601OD All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may rot be reproduced in vvitole or part. nor may any refarence be made to the work, the results, or the company in any advenising, news release. or other public announcements without obtaining our prior written author.'ralion. Paunc McGroary Agronomist Pnnp ri of 7 I SAMPLE TRANSA IIIIIIIIIIIIIIIIIIIIIIIII�IIIIIIlIIIIlllllllllillllllllllllllll ps j�Q,g' A&L CiWofMonroe 10:26:24 WTP Femc Cake PTL 7621Whit e ini Office Information Customer Information le R—+lf u Q..K—;;4+-A•Rv I r'.hnrrio Tri I Cnnv To I Proiect Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden(a7monrocnc.org ti V aD M cz n City of Monroe Reports of Lab Analysis 3`a 90 Days Report Number: 18-191-0205 Account Number: 46205 Submitted By: Steve Hoiden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 61562 Sample Id : RAS t`0 Waypoint' ANALYTICAL Project: RAS REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 7/9/2018 08:55:00 Date Received: 07/10/2018 00:00 Date Reported: 07/15/2018 Total Solids * 1.00 10000 I uu.0 K v V r, 1 ul�v IV 1'... --- --- Moisture * 99.00 100.0 R D 07/10/201814:30 SM-254OG Total Volatile Solids 68.00 680000 100.0 R D 07/10/2018 14:30 SM-2540G Comments: NC CERT#257 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and fetters aro for the exClusive and confidential use or our clients, and may riot be reproduced irr whole or part. norway any reference be made to the work, the lesuffs, or the company in any advertising, ne:vs release, orotharpublic announcements without obtaining our pror vmtten authorization. 6wce- #1 607, Pauric McGroary Agronomist Page 2 of 4 SAMPLE TRANSM _ 18 191-0205 A&L E< I�I�I�I�����I� 00� 102018 CiN of Monroe 13:21:27 1 7621 Whitepine R RAS Office Information Rept# Submitted By Charge To, Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholdeliEynionroenc.org Lab Number (Lab Use Only) Sample ID lContainerType Sampled Date: •-—/ Date Recd: l(1 j�Q2 RAS Glass ( or No) Sampled Time: : S Time Recd: Plastic (Yes or" Sampled By: fEJf ., J Recd By: Relinquishe B : (Signature) Date I Time Received By: (Signature) Date Time v Please Place a "X" by Desired Tests Internal Lab Code: "Ca " Nig.. Na•... Fe., AI ,,. Mn Cu: Zn: :-NN4=N NO3'=N.. x Gd Cr NI,' Fti; As.;= "�:: _H `$e H E % 9• :3oltds %' ` A� =N+:, Mo CI. B. ea x =SC1.4.:' =A' g,; $6 k ;Co.:" "'Sni, r `,T:-' ,'.V. " :';Be- ALK: SSA• ``Avail'P: SoGK^:; '°`:GOiiCI P,. GR:, = " .: TSS;.::.' Siezie#20; Sieve#BO; .Sieve#100 `:'ASH ' CaO CaG03'' :-MgGQ3 ' MgQ ` ' C!N TOC': " Ehv ' "TOTAL', ;P205.``: :TOTAL . ' ',;K20•,r: ` .TtJ .-: _... ,. . _ TKN1N :"` - -- - NM4W' '• .,. ...._ • •- 'NO3W..` �rz -;,E - 'ORGN-1N _ . _ PA;CER t .. T. AZ'GER, T - - - = BTl1P1 . . ,. _ - '.PCBs: CN: • -, -. ; :FECAL T CLP: , _ IG R State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments 0 -7 Report Number: 18-191-0203 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 om' AlVaypoint. ANALYTICAL Project: WWTP Cake 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 7/9/2018 09:10:00 Lab Number: 61560 Date Received: 07/10/2018 00:00 Sample Id : WWTP Cake Date Reported: 07/17/2018 Total Solids * t 20.72 2u72uu I uu.0 r< t, V r t ; Vt�V '. ,-- Moisture * 79.28 100.0 R D 07/10/2018 14:30 Total Kjeldahl Nitrogen 2.80 28000 50.0 R D 07/11/2018 09:00 Phosphorus 1.45 14500 50.0 BKN 07/13/2018 23:35 Potassium 0.10 983 50.0 KKM 07/15/201814:22 Sulfur 0.75 7500 50.0 BKN 07/13/2018 23:35 Calcium 1.02 10200 50.0 KKM 07/13/2018 23:35 Magnesium 0.13 1340 50.0 KKM 07/13/2018 23:35 Sodium 0.06 599 250 BKN 07/13/2018 23:35 Iron 145000 500 KKM 07/15/201814:07 Aluminum 6410 50.0 BKN 07/13/2018 23:35 Manganese 1160 5.00 BKN 07/13/2018 23:35 Copper 364 2.50 BKN 07/13/2018 23:35 Zinc 738 5.00 BKN 07/13/2018 23:35 Ammonia Nitrogen 0.57 5740 50.0 R D 07/11/2018 09:00 Organic N 2.23 22260 50.0 07/11/2018 09:00 Nitrate+Nitrite-N 29.0 2.40 MMT 07/12/2018 09:09 d b terisk Detection limit on all N series is on a wet basis. SM-254OG SM-4500-NH3C-TKN 601 OD 601 OD 601 OD 6010D 6010D 601 OD 601 OD 601 OD 601 OD 6010D 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 All values are on a dry weight basis except as no e y as Our r' ports and letters are forth-, exckuire and ronik9pntial use a our clients. and tnav not be repredtrced in :, ircte or part. nor' n7ay arty. e;e ance i7e made �(M' �G fC e to the work. tha results. orlhe con�nany in ary advortisr7g, news release. crotherpublrc announcen7onls without obtaining ourprior uritlen authorization. Pauric McGroary Agronomist Paoe 4 of 7 Report Number: 18-191-0203 Account Number: 46205 Submitted By: Steve Holden Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 a -'1-9 Waypoint., ANALYTICAL Project: WWTP Cake 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 7/9/2018 09:10:00 Date Received: 07/10/2018 00:00 . Lab Number: 61560 Date Reported: 07/1712018 Sample Id: WWTP Cake Cadmium <1.00 Chromium 112 Nickel 49.1 Lead 13.5 Arsenic 11.7 Mercury <0.400 Selenium <5.00 pH • 7.5 Total Volatile Solids 51.54 515400 Molybdenum 22.5 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. 1.00 BKN 07/13/2018 23:35 601 OD 2.50 BKN 07/1312018 23:35. 601 OD 2.50 BKN 07/13/2018, 23:35 6010D 3.00 BKN 07/13/2018 23:35 601 OD 5.00 BKN 07/13/2018 23:35 6010D 0.400 SMC 07/16/2018 16:59 SW-7471 B 5.00 BKN 07/13/2018 23:35 601 OD 1.0 R D 07/11/2018 09:00 9045D 100.0 R D 07/10/2018 14:30 SM-2540G 2.50 BKN 07/13/2018 23:35 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our+eports and letters are for the exclusive and confidential use of ourclients anti may not be reproduced h; wbote or part. nor may any reference he ;rude to the Work, the results, or the company in any advc using, news ra/ease. orother public announcements without obtaining our anor writton authorization. PW�e, X 607 Pauric McGroary Agronomist Paqe 5 of 7 N SAMPLE TRANSMITTA II 11 18-191-0203 2018 gu 4 46205 A&L Easter Cily of Monroe 13:14:57 WWTP Cake 7621 White iuc Road Ric Office Information ���•�"'�' """""�""" Repttf Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # 46205 POB 69 Monroe NC 28111 Email sholdcn@monrocnc.ors1 Lab Number (Lab, Use Only) t ` R Sample ID WWTP Cake ContainerType- Glass (�& or No) Sampled Date: Sampled Time: 7 -/2r ^:/19 Date'Recd: Time Recd: Plastic (Yes or tdET) Sampled B : �-td� �, f Recd,By.: Relinquished By: ( igriature) Date Time Received By: (Signature) Date Time -/ : /D Please Place a "X" by Desired Tests ;, +�i':!' t; :'.4 ,; :} ;- FB;. 'i. 'AI•:` IVin ". i)fl9:',?'i Internal Lab Code: Cu:;;it t..,,Znl . i SLMONR :NH*N'.-:°='�NO3sfV;i C'' T'I"_C[lo:;' `1# Mt•'t,.,. yG '•t. it�:..ii,l`?:1:.'i�:i` •4ri° �i c.;1� � .-�- �i - 9..-��. ,r'�? •t _ 4caco& _qE . /.Yt,' Volatile" ; _ . ,9•, =: ;, 7 .#'` S,ai4,:,. r+ ,.�„r ;�. i, Agil' 1i' •y. :1. ,Sb iii,,: x .,�i ? �Coh�, x x x ..� 'Be'g'e.� 't F.. _ �1LK'.is x ,:7a; .;s w a. =,SBs,"°; x �- n Avail R� I. X :'� ,.$.oI K`c' , ! �.ls "�f 3': oriel ", . 1S;L7lziNAi 'a'• 0:&'Q °;�: <.SP:GR:=-,,:- ::"�'TSS'= ,,• Sieve#20 !Se"v"e#ii0� ( 0 'Sieve#I; d `p="ASH:-i E fCaOi;. i'CaC.03-.� fV C•Q3;; g.'.. M O:,s 1' g jC1N,;:`?,tt�!TOC;' :�'>E»v }! ;iTATAL • TOT A , •:�' l<2Q-,;;• i• !�;"<1`•N'.�`' i•'TKNUV�', Nki4NJ•,,; ,fir k•"�I�Q3W.: ' ;.i :Oi2'GM=1N; 7i" . s •'i iPA R ,AZ�.CERT • t3T�U • _ M,7,. S' .P. - - EC L :CLP' :rT G :1 R State Certification Needed: NORTH CAROLINA Special Instructions or Remafks Comments r� 0 Report Number: 18-191-0204 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 0 � � �M WayANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointa nalytica Isom Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 7/9/2018 09:05:00 Lab Number: 61561 Date Received: 07/10/2018 00:00 Sample Id : WTP Ferric Cake Date Reported: 07/17/2018 Total Solids * asterisk 24.59 24bUUU IUU.0 rX v "I' I— — '—'-- Moisture * 75.40 100.0 R D 07/10/2018 14:30 Total Kjeldahl Nitrogen 0.58 5770 50.0 R D 07/11/2018 09:00 Phosphorus 0.20 1980 50.0 BKN 07/13/2018 23:39 Potassium 0.02 190 50.0 KKM 07/15/201814:27 Sulfur 0.30 3040 50.0 BKN 07/13/2018 23:39 Calcium 0.18 1800 50.0 KKM 07/13/2018 23:39 Magnesium 0.03 318 50.0 KKM 07/1312018 23:39 Sodium 0.03 281 250 BKN 07/13/2018 23:39 Iron 330000 500 KKM 07/15/201814:32 Aluminum 2850 50.0 BKN 07/13/2018 23:39 Manganese 585 5.00 BKN 07/13/2018 23:39 Copper 542 2.50 BKN 07/13/2018 23:39 Zinc 201 5.00 BKN 07/13/2018 23:39 Ammonia Nitrogen 0.11 1100 50.0 R D 07/11/2018 09:00 Organic N 0.47 4670 50.0 07/11/2018 09:00 Nitrate+Nitrite-N 64.2 2.36 MMT 07/12/2018 09:10 t d b Detection limit on all N series is on a wet basis. SM-2540G SM-4500-NH3C-TKN 601 OD 601 OD 6010D 601 OD 6010D 601 OD 601 OD 601 OD 601 OD 6010D 6010D SM-4500-NH3C CALCULATION 4500NO3F-2011 All values are on a dry weight basis except as no e y / � m` �v Our reports and fetters are for the exclusive as?d cenfidenl`al arse ofour clients. and may r;ol be reUrocluced in whole orpa+'. rtor may' any reference be made `G to-tho work, the results, or the company in any advedising, nev:s release, or other pubirc announcemonts wilhoul obtaining our prior wrillen aulnorizalion. Pauric McGroary Agronomist Page 4 of 7 Report Number: 18-191-0204 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Wavpoinl..0 10. (a 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 7/9/2018 09:05:00 Lab Number: 61561 Date Received: 07/10/2018 00:00 Sample Id : WTP Ferric Cake Date Reported: 07/17/2018 CadmiumL.tiz Chromium 222 Nickel 35.3 Lead 6.87 Arsenic 17.0 Mercury <0.400 Selenium <5.00 pH * 5.9 Total Volatile Solids 37.23 372300 Molybdenum 49.0 Comments: NC CERT#257 SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. I.uu DMIM Vll 1J1-IV-./- 2.50 BKN 07/13/2018 23:39 601 OD 2.50 BKN 07/13/2018 23:39 6010D 3.00 BKN 07/13/2018 23:39 601 OD 5.00 BKN 07/13/2018 23:39 601 OD 0.400 SMC 07/16/201817:02 SW-7471B 5.00 BKN 07/13/2018 23:39 6010D 1.0 R D 07/11/2018 09:00 9045D 100.0 R D 07/10/2018 14:30 SM-254OG 2.50 BKN 07/13/2018 23:39 601 OD All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. our reports and letter's are for the exclusive and confidential use or our ctienls. and tnay not be reprodttcad in uvho!e or part. nor may any reference lie made to the work. tho resuns, orthe company in any advertising, news release. orotherpublic announcements without obtaining ourprior written authorization. Pauric McGroary Agronomist Paae 5 of 7 18-19 IIIIIIIIIIIIIIIIIIIIIIIIIIIIIIIiilllllllllllllllllllllllllllillll46205 1-0204 SAMPLE-TRANSIV ci,,.wonioe 0710-2018 N F VVTP Ferric Cake A&L 13:20:02 ATL 7621 Whitepine Road Richrnoll(l V Al.) -I.) I I r'. --- on Office Information Cu,morner intormation Projbct C'arge To copy To Rip-0 ��4brqftted'BV, Charge To: Cit of Monroe Steve Holden City of Monroe Email IM Acdt POB 69 sholden(&.monroenc.or C 46205 Monroe NC 28M 11 t Lab Number (Lab -Use Only) 'Sa(OplialD Contai.neir Type_ S*fioldd DafEi: Uate Recd: Time Redd: Glass (YesorIU) &6ftl6d.Time: ifE WTP Ferric Cake Plastic (Yin or No) Samoled'B: R6cd �y.: 11SIX I I';. - D a e, Rdceiv�: Signature) Date- Time Ri�jlfinqu'ishe'(J'By.W— a PQ U, Please Place a �'X- by Desired Tests V Internal Lab Code, SLIVIONR -Ap K N Kx a.0 4 - 11 N PZ-!U'- aK,* .7 x x x X -7, 7V v" P" 31 g,•n rd q ��Wi Nk— —T, L x x x X x X :—.-25:$K— ,S7 'IT L;_N Av 0j%GA! i, v TQ-I E K "i TpCL1T T 7 1 li:CK qERT p Statq C6rtifi&atip`h WiYde`&. NORTH CAROLINA SpeC1a17Ihsth[idti6n§- oc Remarks . Comments I rl- W a- City of Monroe Reports of Lab Analysis 4th 90 Days Report Number: 18-275-0205 Account Number: 46205 Send To: City of, Monroe Steve Holden 775 Treeway Dr Monroe , NC 28110 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: Lab Number: 62943 Date Received: 10/02/2018 00:00 Sample Id: RAS Date Reported: 10/08/2018 0 0 01 C Total Solids ` 1.24 12400 100.0 CJR 10/04/2018 15:29 SM-254OG Moisture ` 98.80 100.0 CJR 10/04/2018 15:29 SM-2540G Total Volatile Solids 68.10 681000 100.0 CJR 10/04/2018.15:29 SM-2540G Comments: All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B : Analyte detected in blank H - Beyond Holding Time our mports and letters ate for the exclusive and confidential use of our clients, anti may not be rapreduceid in whole or part no, may any,eference be made to ti;c :ve;ir, no results, nr''lie con;eany+n arry advertising. nc:.s release, orothor public announre:nants witi;out obtaining our prior mititlen 11;1h01iz,1ti00- Page 3 of 5 Pauric McGroary Agronomist SAMPLE TRANSN 18-275.0205 Y A&L F IIIIIIIIIIIIIIIIIIIIIIII�III�IIIIIIIII�IIIIIIIIIIIIII'IIIIIIIIIII 46205 aS2:2018 At City of Monroe 7621 Whitepine RAS I L Office Information Rept# Submitted By Charge To Copy To Project Steve Holden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 lsholden t monroenc.ora Lab Number (Lab Use Only) Sample ID Container Ty pe Sampled Date: p/-/ Date Recd: Cj 3 IAS Glass (a'as or No) Sampled Time: Time Recd: I Plastic (Yes or N&) Sampled By: Recd By: Relinquished By: (Signature) Date Time eceived By: (Signature) Date Time 2 ' Please Place a "X" by Desired Tests Internal Lab Code: r0 ;a;t.-f . ;;.t'� �; - ,f"sus' ..-a: ,17;c,:. - ct: M t; .:3.-,A • �:,d�ir; .Fd.;r: - - -{.� NH4=N NO3=N X t: -- .1' :b;,— 1. �L — '�;�:: •u=- Pb ',',' — ttt;. '^t% ti! i:4.;, ='t' t `, fG . e,•' _ 3•. H�''' aCO3%=. E o'" a 3 � of til 5 O � i' 'Sol ds-. .n; � � r.3:,... — �r'�, f' ..t dyer �•: i'.. x -ts, 'x; tZ •,SO�t, :4t•, Vie. .A ,i- _'f,- -'.i,Sb�'�' ,<tlM%75 ,+;Co, "'ri .Sn �,j_M. _ �`Ti=�'=':�' �M,.c "sU=;:•:>;c.�=""�Be'.`. _ u;«,-... ALff�� y, r..:... .�SS..� «,1> 4^ Avail'Pr,;''�:-Sol'K`�i� .^� - :Corid"`'`��• e.;„ .:WIN:: 'SO r.SOL•:NX` --%:O&G`�#2't)'.? SI0e00! Sieve#100 � i:ASHa�° ``a''Ca0'= �CaCO3� M"G.03=;' M" O'' C' N•= : TOC'' "• E' Y• ' 5 P20 ; ri-.. ,TOTAL '•K 2p: ,1: "S •,=ar' �T V k;. ..1. ;ct :++C`P'h i" � TKNW' ` _^. r_' a tt„ •J' • 4W.,`' ?=NH 1`.1. t��,Jro� O N 3UV'•F '•::F', - VS :O RGN=IN..RA.GERT ), .. ,it•`�x,-.-:. _ _,} _ �AZ•�GERT _ _ „-;, -. ,:p.. .,Y;;. 3, eke, :� .� EACT •E -t.,; .y",.,. -'•r; y�TGLR''� State Certification Needed: NORTH CAROLINA Special Instructions or Remarks Comments N,, 0 L^7 Report Number: 18-275-0204 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 62942 Sample Id : WWTP Cake Waypoint ANALYTICAL Project: WWTP Cake REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/1/2018 08:51:00 Date Received: 10/02/2018 00:00 Date Reported: 10/10/2018 Total Solids 18.10 181000 100.0 CJR 10/04/2018 15:29 Moisture'` 81.90 100.0 CJR 10/04/201815:29 Total Kjeldahl Nitrogen 4.07 40700 120 CLP 10/09/2018 13:30 Phosphorus 1.39 1.3900 50.0 BKN 10/05/2018 20:46 Potassium 0.09 918 50.0 BKN 10/05/2018 20:46 Sulfur 0.80 7970 50.0 BKN 10/05/2018 20:46 Calcium 1.13 11300 100 BKN 10/05/2018 20:46 Magnesium 0.15 1500 50.0 BKN 10/05/2018 20:46 Sodium 0.07 666 250 BKN 10/05/2018 20:46 Iron 147000 250 BKN 10/07/201816:29 Aluminum 6230 50.0 BKN 10/05/2018 20:46 Manganese 1440 5.00 BKN 10/05/2018 20:46 Copper 406 2.50 BKN 10/05/2018 20:46 Zinc 867 5.00 BKN 10/05/2018 20:46 Ammonia Nitrogen 0.41 4140 50.0 ZBD 10/08/201814:00 Organic N 3.66 36560 120 10/08/201814:00 Nitrate+Nitrite-N 172 4.78 ZBD 10/09/201815:42 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time Our reports and fetters are ;or tyre exclusive and confidential use of our clients, or part, nonnay any reference be matte te: the the rusuits, or the ccr•, pany rn any advertising. neR-i reloaso, or other p7blic atwounrcuie; is bvitl?out obtaining our pdor'wfilic:+ au?horizairen. SM-254OG SM-2540G SM-4500-NH3C-TKN 601 OD 6010D 6010D 601 OD 601 OD 6010D 6010D 6010D 601 OD 601 OD 601 OD SM-4500-NH3C CALCULATION 4500NO3F-2011 X 107,14" Pauric McGroary Agronomist Paae 5 of 8 Report Number: 18-275-0204 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 62942 Sample Id : WWTP Cake Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH Total Volatile Solids Molybdenum Comments: ., Ix e � ,O .W' ,Iyp: o � CF .oANALYTICAL Project: WWTP Cal REPORT OF ANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 10/1/2018 08:51:00 Date Received: 10/02/2018 00:00 Date Reported: 10/10/2018 <1.00 1.00 BKN 10/05/2018 20:46 601 OD 117 2.50 BKN 10/05/2018 20:46 601 OD 49.4 2.50 BKN 10/05/2018 20:46 601 OD 12.9 3.00 BKN 10/05/2018 20:46 601 OD 23.4 5.00 BKN 10/05/2018 20:46 601 OD 0.0472 0.0146 KKM 10/05/2018 12:54 SW-7471 B <5.00 5.00 BKN 10/05/2018 20:46 6010D 6.9 JSL 10/08/2018 08:50 9045D 45.10 451000 100.0 CJR 10/04/201815:29 SM-254OG 24.4 2.50 BKN 10/05/2018 20:46 601 OD All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Our'repo is and lettars are ran the exclusive and conlidertrat use of our clients. and may rqt be-rznrpJ�.cc�i-ir. ,v!1oJe o+' part. nor may arty reference be made -'Who :vonft. the ru'su!+S. or ir:e COUtpally w any adveriFsrng, nnvvs retaasc. Of' other public arnrnunr',ynarrts :without obtaining ou:'t.';ior twitFen au;ho:i a(iort. Paae 6 of 8 Pauric McGroary Agronomist SAMPLE TRANSIT A&L 7621 Whilepim 13-275-0204 norm)uJill 111111111111111111111111i111111111111l1i11111111146205 i2o1a ON of Monrne W WTP Cake 12:46:45 Office Information Customer Information Rept# Submitted By Charge To Copy To. Project Steve Hoiden City of Monroe Acct # POB 69 Email 46205 Monroe NC 28111 sholden@rnonroenc.orp, Lab Number (Lab Use Only) Sample ID ' Cbntainer-Type Sampled.Date: - - DbW'Recd: �`q, W WTP Cake Glass (V-ss or No) Sara Iedlirrle: Time Redd: Plastic (Yes or" Sampled By: Recd. By: Relinquished By! (Signature) Date Time. Received By: (Signature) Date Time tAgO 2 Please Place a "X" by Desired Tests Internal Lab Code: SLMONR .r.�J,..hO ? d 1 p`: o.0 'S S„M11.3:,•3TKN':1'.,: :•ATi - %) !1$l5_ ,,Y 2!}:t .�F t:,t,P,.r4.:2, ::Y•• a '.i'` - �t.� {.�L�' ?$i°,:.' "rv`;,' ,i. 'K'"E+'i'1? i�•i{ •;. it I�:ti.j i•`D' Yt _. 'S 3;. .Fe,<. "r' 'Ti" '.1. •Y,'V tiy. `).f... -17 x x x x x x x x x x x x x x .�;� S,t z'T�• sr`f., .aa=� -1 ,raz.•,.x., ,t'_St•�:U''4;P • C:' 1 • 'C t, n• �.s� sac ,..iz .ter 1: 2 „lt a\"^; nil"; @} '„�; � r... •�` �� ;,�` sy: :i:a:,- .a� �'r ,Y. gs.<..: „��+^}''..,. ..1 r:i7^1;^ rt t CaG,O.3'`� t. 4..Y '6 �i� .,t'/o_ �'Uolatile .t .. F��S ,StOhCts.•%' - 'Fi• -tif �:: �iO�gr:N.-, `rY .' -. +''1 'k; - . M,"o,,(;,; -,<c-<,}••s �1•'aa' �.: �a�.•C,L�a•:�: -.t^ - Riff is"•!i: r,tM;B. .F-:; `B f s x x x x x x x x x x x itaµip /� ,r^ q.1;t qq ,ar•,a"r4< G. °a'r s' +: tcn` ;sm.t:; t i"r4j:.i t };r `,°1'1•�• .4 _ ?- ;;t'. M, ,:1/;' �'n� r'7'^ 8e.. w�. _ :c �:ALK`i�•:.' a` i',' '$3:�::__ .a..� „, .Avaii�P::r =t: cir` tC:: ).,'; 'C'ojnil.w_ r+x.. f:.',r -{• r.SUL I tNA".1 ,..._r- ,._z,_ . _P__ . ,... , . _ _._•_ .. .....__. . _ .,. i.:..._...._ _.. v #1, .;'A H: Ca:O,,..�;',CaG�3M1: gCO3;!' 1ri.M O,zC PTO a � Y,� �t it . ,. 2 .5 • - .I, .TOTAL :�1�2 r.F !. � O .b: t ^,� C•^'t� §!w TN: 1. s _ _ ,�> �`.� t., •c. TKNlllt: i` _ ;"•`�tY;`-' :7 iVM41/V'�.�` l.t". .,,� +^+i:t •03VV"R� At. n':. �:r'k Jf. M1; r; ._4 i�� � T .4 ^,•; •AZ-CEj M1 R7;r t•;r+' •+$' .,� a" ;s` ` �'�., `; ;BT.U• •'!�` .;i: `4 U:i : ; CB;Sr t-. �+ ;I t REACT• :� :i.. ',in '` `4' 'FEGP,;L�, <:' • , n.*t4,'" zy :u �.r-:. } State Certification Needed: NORTH CAROLINA S' ecial Instructions or Remarks Comments 1 Q) 0) cu 0- 0 Report Number: 18-275-0203 0 � Account Number: 46205W7621 Whitepine Road, Richmond, VA 23237 j Main 804-743-9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 62941 Sample Id : WTP Ferric Cake Project: WTP Ferric Cake REPORT OFANALYSIS Date Sampled: 10/1/2018 08:46:00 Date Received: 10/02/2018 00:00 Date Reported: 10/10/2018 Total Solids 26.80 268000 100.0 CJR 10/04/2018 15:29 SM-2540G Moisture' 73.20 100.0 CJR 10/04/201815:29 SM-2540G Total Kjeldahl Nitrogen 1.91 19100 120 CLP 10/09/201813:30 SM-4500-NH3C-TKN Phosphorus 0.44 4360 50.0 BKN 10/05/2018 20:41 601 OD Potassium 0.03 _ 347 50.0 BKN 10/05/2018 20:41 601 OD Sulfur 0.33 3340 50.0 BKN 10/05/2018 20:41 601 OD Calcium 0.47 4680 100 BKN 10/05/2018 20:41 601 OD Magnesium 0.06 635 50.0 BKN 10/05/2018 20:41 601 OD Sodium 0.05 479 250 BKN 10/05/2018 20:41 601 OD Iron 306000 250 BKN 10/07/201816:19 601 OD Aluminum 3350 50.0 BKN 10/05/2018 20:41 6010D Manganese 1250 5.00 BKN 10/05/2018 20:41 6010D Copper 612 2.50 BKN 10/05/2018 20:41 6010D Zinc 368 5.00 BKN 10/05/2018 20:41 6010D Ammonia Nitrogen 0.07 746 50.0 ZBD 10/081201814:00 SM-4500-NI3C Organic N 1.84 18354 120 10/08/2018 14:00 CALCULATION Nitrate+Nitrite-N 128 4.82 ZBD 10/091201815:42 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B-Analyte detected in blank H - Beyond Holding Time PWt-a #1 &Wr our epe;ts andtellers are torthe exclusive and cart!,%danlial use of our clients, and may rgt ,rat roduced .%n s:!toie ortlart, rrar may any reference be rrrode Pauric McGroary .o tho :✓odr. L`c results. or the company yr eny advvrdsing. nows release, or alherpublic ar:nounroments vrr:;rool obtar: iing cur poor written aulhorrrat;on. Agronomist Page 5 of 8 I Report Number: 18-275-0203 Account Number: 46205 Send To: City of Monroe Steve Holden 775 Treeway Dr Monroe, NC 28110 Lab Number: 62941 Sample Id : WTP Ferric Cake Cadmium Chromium Nickel Lead Arsenic Mercury Selenium pH * Total Volatile Solids Molybdenum Comments: m Waypoint, 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 * Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project WTP Ferric Cake REPORT OF ANALYSIS Date Sampled: 10/1/2018 08:46:00 Date Received: 10/02/2018 00:00 Date Reported: 10/10/2018 3.11 1.00 BKN 10/05/2018 20:41 6010D 195 2.50 BKN 10/05/2018 20:41 6010D 35.2 2.50 BKN 10/05/2018 20:41 6010D 6.54 3.00 BKN 10/05/2018 20:41 6010D 45.2 5.00 BKN 10/05/2018 20:41 6010D <0.0151 0.0151 KKM 10/05/2018 12:53 SW-7471 B <25.0 25.0 BKN 10/07/201816:19 6010D 6.0 JSL 10/08/2018 08:50 9045D 31.40 314000 100.0 CJR 10/04/201815:29 SM-2540G 43.2 2.50 BKN 10/05/2018 20:41 6010D All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. B - Analyte detected in blank H - Beyond Holding Time Ow reports rind fellers ale for the excius:ve and confidential use oI our cliants, and Rtay nQt fJ6 !^(l:Q (IGB to whoie or part, nor inay any reference be trade to the >vnric the results. or the company in any advertising, oervs release, or otim public m;ounco nlcttta''"MhQut obtainhy cur prior md"ien a.rlhoriz, ion. Pape 6 of 8 P0f« XC 6047'1 Pauric McGroary Agronomist 18-27 SAMPLE TRANS] lot 11111111111111111111111111111111111111111111 I4620 N 5 5-0203 y Citv of Monroe 10-02-2018 A&L WTP Ferric Cake 12:45:20 QuOtbrhe'-r1hf6rination Office Information Rept# Charge To Copy To Project Steve Holden City of Monroe 'Acct # POB 69 Email 46205 Monroe NC 28111 sholden(Rmonrocne.org Lab NUaiber (Lab -Use Only) CotitainerTy0p 5dffip1601 QaW, /0-/ _/�' Date Repd- 2-CIL-1 WTP Ferric Cake Glass (W-" or S6*16d The: Time Redd: Plastic (Yes or -Mr..) Sbrhpled,B- _-, 1S4;L)j 14c)1,0�AJ R66d,13y: jith& 'Receiv6d.By: (Signature) Date Time LAP5 L017-1 ly Please' Pl.a-ce, -a "X4.." .by Desired Tests Internal Lab Code: SLMONR *i_I,dii_N, 30,14,10,;1"1 iR OW E 11'11VIM"'1311�"W F -A •-W, -to ir ili 6,Q '_NR41 x x x x x x x x x x x x x x x 5 a- x x x x x x x x x x x 77 —sc)474T, —S-,-, 11111 0 1, &f� -,A K_ :_ o'-.6ifV! ,SDE-Nk Al�� Tsfi— 'Slow-0015" H'77 OT _,�Ca CQ317", WC0011, QQ," '4_VZhfx 4'�;,T,, - JOTAL,- 14. -K-".N 40 GN�-'W� RT1. M T 'State e6ruflcatioh N64&& NORTH CAROLINA Sjj&_d1al_lhsftUcti66§ or-Rdrildrks, cbrrirri6hts II W 11, SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Monroe PO Box 69 Monroe, NC 28111 Attention: Steve Holden Project Name: Land Application Lot Number:TJ10098 Date Completed: 10/31/2018 10/31/2018 2:15 PM Approved and released by: Project Manager: Kelly M. Nance If6 •r_..t�� s'i AC CP E DI T ED eORQS�% p»nav The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 18 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Monroe Lot Number: TJ10098 i ( This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality _I Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or {— discussed below. Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" i qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. The pH analysis associated with the samples in this report were performed after the method �i recommended 15 minute holding time. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 1-8 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Monroe i Lot Number: TJ10098 Sample Number Sample ID Matrix Date Sampled Date Received 001 WWfP CAKE Solid 10/10/2018 0938 10/10/2018 002 WfP CAKE Solid 10/10/2018 0932 10/10/2018 (2 samples) ' I f Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 18 I Inorganic non-metals Client: City of Monroe Laboratory ID:TJ10098-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/10/2018 0938 % Solids: 14.6 1011212018 0202 Date Received:10110/2018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/23/2018 1747 KFE 87465 1 (pH) 9045D 1 10/12/2018 0024 SA1 86264 1 (Reactive Cya) 7.3.3 1 10/26/2018 1753 MSG 10/23/2018 1007 1 (Reactive Sul) 7.3.4 1 10/23/2018 2226 KFE 1012312018 1007 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 ° F 1 pH 9045D 7.4 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 110 50 mglkg 1 ' g LOQ = Limit of Quantilation B = Detected in the method blank E = Quantitalion of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 18 TCLP Volatiles Client: City of Monroe Laboratory ID:TJ10098-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/10/2018 0938 % Solids: 14.6 10112/2018 0202 Date Received:10/10/2018 Run Prep Method Analytical Method Dilutiom Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/50308 8260B 10 10/20/2018 0714 MINIS 87094 10/11/2018 2233 Parameter CAS Analytical Number Method Result Q LOQ Units Run Benzene 71-43-2 8260B ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260B ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260E ND 0.050 mg/L 1 Chloroform 67-66-3 8260B ND 0.050 mg/L 1 I 1,2-Dichloroethane 107-06-2 8260E ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260B ND 0.050 mg/L 1 i Trichloroethene 79-01-6 8260B ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260B ND 0.010 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 106 70-130 I Bromofluorobenzene 100 70-130 Toluene-d8 107 70-130 t t: - i l � { I I LOQ = Limit of Ouantitalion B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% • H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (B03) 791-9111 www.shealylab.com Page 5 of 18 I TCLP Semivolatiles Client: City of Monroe Laboratory ID:TJ10098-001 Description: WWTP CAKE Matrix: Solid Date Sampled:10110/2018 0938 % Solids: 14.6 10/12/2018 0202 Date Received: 1011012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10116/20181118 CMP2 10/12/20181658 86346 10/11/20182233 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270D ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270D ND 0.080 mg/L 1 Hexachlorobenzene 118-74-1 8270D ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270D ND 0.040 mg/L 1 I Hexachloroethane 67-72-1 8270D ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270D ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270D ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270D ND 0.040 mg/L 1 Pentachlorophenol 87-86-5 8270D ND 0.20 mg/L 1 Pyridine 110-86-1 8270D ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270D ND 0.040 mg/L 1 1 2,4,6-Trichlorophenol 88-06-2 8270D ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 67 37-129 2-Fluorophenoi 50 24-127 Nitrobenzene-d5 68 38-127 Phenol-d5 57 28-128 I Terphenyl-d14 99 10-148 f 2,4,6-Tribromophenol 65 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 18 TCLP Herbicides Client: City of Monroe Laboratory ID:TJ10098.001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/10/2018 0938 % Solids: 14.6 10/12/2018 0202 Date Received: 1011012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 131118151A 8151A 1 10/15/2018 1502 DAL1 10/12/2018 1948 86360 10/11/2018 2233 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg1L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 65 62-117 LOQ = Limit of Quanlitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 18 1 TCLP Pesticides Client: City of Monroe Laboratory ID:TJ10098.001 Description: WWTP CAKE Matrix: Solid Date Sampled:10/10/2018 0938 % Solids: 14.6 10/1212018 0202 Date Received: 10/1012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8081B 1 10/15/20181501 DAL1 10/12/20181658 86345 10/11/20182233 CAS Analytical Parameter Number Method Result Q LOQ Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081E ND 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Decachlorobiphenyl 1 69 20-131 Tetrachloro-m-xylene 77 26-132 LOQ = Limit of Quantilalion B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 18 TCLP Metals Client: City of Monroe Laboratory ID: TJ1 0098-001 Description:lNWTP CAKE Matrix: Solid Date Sampled:1Oil 0/2018 0938 % Solids: 14.6 10/12/2018 0202 Date Received:10/10/2018 Run Prep Method 1 1311/3010A 1 131117470A Analytical Method Dilution Analysis Date Analyst 601 OD 1 10/19/2018 1113 CJZ 7470A 1 10/16/2018 2011 JMH Prep Date Batch Leachate Date 10/17/2018 1632 86816 10/11/2018 2233 10/15/2018 1501 86429 10/11/2018 2233 CAS Analytical Parameter Number Method Result Q LOQ Units Run Arsenic 7440-38-2 601OD ND 0.15 mg/L 1 Barium 7440-39-3 6010D ND 0.25 mg/L 1 Cadmium 7440-43-9 601OD ND 0.050 mg/L 1 Chromium 7440-47-3 601OD ND 0.10 mg/L 1 Lead 7439-92-1 601OD ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 601OD ND 0.20 mg/L 1 Silver 7440-22-4 601OD ND 0.10 mg/L 1 iff 14 i� I i I� LOQ = Limit of Quanlitalion B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 18 Inorganic non-metals Client: City of Monroe Laboratory ID:TJ10098.002 Description: WTP CAKE Matrix: Solid Date Sampled:10/10/2018 0932 % Solids: 26.7 10/15/2018 2359 Date Received:1011012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Ignitability) 1010A 1 10/23/2018 1830 KFE 87465 1 (pH) 9045D 1 10/12/2018 0025 SA1 86264 1 (Reactive Cya) 7.3.3 1 10/26/2018 1753 MSG 10/23/2018 1007 1 (Reactive Sul) 7.3.4 1 10/23/2018 2226 KFE 10/23/2018 1007 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ignitability (Pensky-Martens Closed -Cup) 1010A >140 140 o F 1 pH 9045D 6.7 su 1 Reactive Cyanide 7.3.3 ND 50 mg/kg 1 Reactive Sulfide 7.3.4 ND 50 mg/kg 1 LOO = Limit of Quanlitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com j Page 10 of 18 TCLP Volatiles Client:City of Monroe Laboratory ID: TJ10098.002 Description: WTP CAKE Matrix: Solid Date Sampled:10/10/2018 0932 % Solids: 25.7 10/15/2018 2359 Date Received: 1011012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/5030B 8260E 10 10/20/20180651 MNS 87094 10/11/20182233 CAS Analytical Parameter Number Method Result Q LCIQ Units Run Benzene 71-43-2 8260B ND 0.050 mg/L 1 2-Butanone (MEK) 78-93-3 8260B ND 0.10 mg/L 1 Carbon tetrachloride 56-23-5 8260B ND 0.050 mg/L 1 Chlorobenzene 108-90-7 8260B ND 0.050 mg/L 1 Chloroform 67-66-3 8260B ND 0.050 mg/L 1 1,2-Dichloroethane 107-06-2 8260B ND 0.050 mg/L 1 1,1-Dichloroethene 75-35-4 8260B ND 0.050 mg/L 1 Tetrachloroethene 127-18-4 8260B ND 0.050 mg/L 1 Trichloroethene 79-01-6 8260B ND 0.050 mg/L 1 Vinyl chloride 75-01-4 8260B ND 0.010 mg/L 1 Run 1 Acceptance iSurrogate Q % Recovery Limits 1,2-Dichloroethane-d4 108 70-130 Bromofluorobenzene 100 70-130 Toluene-d8 109 70-130 LOQ = Limit of Quanlitation B = Detected in the method blank E = Quantilalion of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery Is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding lime W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 18 TCLP Semivolatiles Client: City of Monroe Laboratory ID:TJ10098-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/10/2018 0932 % Solids: 26.7 10/15/2018 2359 Date Received: 10/1012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/3520C 8270D 1 10/16/20181204 CMP2 10112/20181658 86346 10/11120182233 CAS Analytical Parameter Number Method Result Q LOQ Units Run 1,4-Dichlorobenzene 106-46-7 8270D ND 0.040 mg/L 1 2,4-Dinitrotoluene 121-14-2 8270D ND 0.080 mg/L 1 Hexachlorobenzene 118-74-1 8270D ND 0.040 mg/L 1 Hexachlorobutadiene 87-68-3 8270D ND 0.040 mg/L 1 Hexachloroethane 67-72-1 8270D ND 0.040 mg/L 1 2-Methylphenol 95-48-7 8270D ND 0.040 mg/L 1 3+4-Methylphenol 106-44-5 8270D ND 0.040 mg/L 1 Nitrobenzene 98-95-3 8270D ND 0.040 mg/L 1 j Pentachlorophenol 87-86-5 8270D ND 0.20 mg/L 1 Pyridine 110-86-1 8270D ND 0.040 mg/L 1 2,4,5-Trichlorophenol 95-95-4 8270D ND 0.040 mg/L 1 2,4,6-Trichlorophenol 88-06-2 8270D ND 0.040 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 74 37-129 j 2=Fluorophenol 55 24-127 Nitrobenzene-d5 71 38-127 Phenol-d5 76 28-128 ,Terphenyl-dl4 102 10-148 :.2•„4,6-Tribromophenol 73 41-144 rl, LOQ = Limit of Quantitallon B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 18 TCLP Herbicides Client: City of Monroe Laboratory ID:TJ10098-002 Description: WTP CAKE Matrix: Solid Date Sampled:10/1012018 0932 % Solids: 25.7 10/1512018 2359 Date Received: 10/1012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 1311/8151A 8151A 1 10/15120181548 DAL1 10112/20181948 86360 10/11/20182233 CAS Analytical Parameter Number Method Result Q LOCI Units Run 2,4-D 94-75-7 8151A ND 0.020 mg/L 1 2,4,5-TP (Silvex) 93-72-1 8151A ND 0.0050 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits DCAA 67 62-117 LOD = Limit of Quantilalion B = Detected in the method blank E = Ouantitation of compound exceeded the calibration range NO = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 18 TCLP Pesticides Client: City of Monroe Laboratory ID:TJ10098.002 Description: WTP CAKE Matrix: Solid Date Sampled:10/1012018 0932 % Solids: 25.7 1011512018 2359 )ate Received: 1011012018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date 1 131113520C 8081 B 1 10/15/2018 1516 DAL1 10/12/2018 1658 86345 10/11/2018 2233 CAS Analytical Parameter Number Method Result Q LOQ Units Run gamma-BHC (Lindane) 58-89-9 8081B ND 0.00040 mg/L 1 Chlordane 57-74-9 8081B ND 0.0040 mg/L 1 Endrin 72-20-8 8081B ND 0.00040 mg/L 1 Heptachlor 76-44-8 8081B ND 0.00040 mg/L 1 Heptachlor epoxide 1024-57-3 8081E ND 0.00040 mg/L 1 Methoxychlor 72-43-5 8081B ND 0.0016 mg/L 1 Toxaphene 8001-35-2 8081E ND 0.0080 mg/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits I Decachlorobiphenyl 91 20-131 Tetrachloro-m-xylene 82 26-132 l� I I i i I:r 1 I �. I • I I r� pli S �'t I -I LOQ = Limit of Quantitation B = Detected In the method blank E = Quanlitation of compound exceeded the calibration range NO = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on we[ weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 18 TCLP Metals Client: City of Monroe Laboratory ID:TJ10098.002 Description: WTP CAKE Matrix: Solid Date Sampled:10/10/2018 0932 % Solids: 25.7 10/16/2018 2359 Date Received: 10/1012018 Run Prep Method 1 1311/3010A 1 1311/7470A Analytical Method Dilution Analysis Date Analyst 601 DID 1 10/19/2018 1118 CJZ 7470A 1 10/16/20182013 JMH Prep Date Batch Leachate Date 10/17/2018 1632 86816 10/11/2018 2233 10115/20181501 86429 10111/20182233 CAS Analytical Parameter i Number Method Result Q LOQ Units Run C Arsenic 7440-38-2 6010D ND 0.15 mg/L 1 Barium 7440-39-3 601OD ND 0.25 mg/L 1 Cadmium 7440-43-9 6010D ND 0.050 mg/L 1 Chromium 7440-47-3 601OD ND 0.10 mg/L 1 Lead 7439-92-1 601OD ND 0.10 mg/L 1 Mercury 7439-97-6 7470A ND 0.0020 mg/L 1 Selenium 7782-49-2 601OD ND 0.20 mg/L 1 Silver I 7440-22-4 601OD ND 0.10 mg/L 1 I t I 1 I 1 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quanlitalion of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 18 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of I8 11'r04A / XdDILlb* ;Hs=AU1 E.F°lVIROMOSI N UiL-SERITCES, I,NG. n147, AL Sa>I5.:�s�� o ja�4:lrSl?`?rri��' �"aL:�'L�1Ji31 7.1 pphnna�Vo. (!l{?7) 7r91 �7C �il.Jtf;x!(J•u�i3031''31 ia. SC � 111 �LEE7I�3�i ! 6 � i Criev( Rc xlrf to Gbaf:f:f I?rfeao^rf= r5b, r�tz h1n � �rzr;i A Z� y7� •Jtvra i•Iv- '-- -0�-. r € --- a.rn•��y ssrr�ier aXazwe 1-: 4�: (3d7•^� it i — rity Sf:,lr. zip Lxr ?' _ r3rtu, .. (i7.1,.rJ1 A4a it oa: •e e�t18G. i5 n3e:437.J C 07if 1 i i J r .co At�rgc .aale!�Mramv, DG) cTn br. nxa PN'St'Fflydf!15 t��UI r�It TJ 10098 F.O. PAa ftb vj Tjr:b 4'r C!AM.allr:�%• % l fir' 2 A"st:r.-, ty�sc:.�vs�•- r:c � j � � i/ p,�c .�, �,' tiprS ID+.7d5Mfl4^A f �.�/ j6Y Y}•7 4 2rr-�'O If? , $d• ul G (aS - ��� �Qv [,r� ' y ") �f fi2�7tP.rY3i LC7io•! U. i{�rla''rzr<.4r<t�:.41hn�:='•41'!�c:^.'.6i'vd b1 :LL .1:di Y! - 1- —_ __ - -!'• ' I f fL7sa � ! � � ]�� � +� •x K +� t ripeA A Fran sixt Fk1sh FWA �ou•Ifinvne Trh:e rraqu7ed(ttivru �cY>,'capyr'g1.�'nCi�rr.+;rsvti•J T:T.! £arrair Gumc�rl QC RaSmiN�br�(s ;5}vLZ�y FnS-Lll a NazalCtz<SiA�`kc.6n•r C• •risfnnat a LSkq IrrPITt LIPa:01 .-1 hlkgnan ' LI h'cfrar.• ry Gricnr 1t'sgrsW 4}• i.ail �;r-tyJ� ,Srnaara _ 9w:b tSoerafy)•- f1:k: -rCCd� I.ii51'M�iSh '� fDaft Intl '-Ff6r-iui70 oY t ,may n r5ri ( C.vfo "ime Rb-ccivvd oy ^.. rl a�j � nj' ��t? C. urn � Gt>t'���` (Or'i o//If (t i-! �"�F��/..'�_-��;��i,�t`c-^=,>`.���- 7:rtr. ilT3 1 �'%,''Dji' 1 —2—•� ... oolir•f(lr: h:Yf 13��r,, ./ � Deco r1 n•r'• 3. pco-, Md by -- ::tc ?vl•5 �t — -- • -- - - r p.,r•:rpa:•z'x:n �.,. vary ,ne .. 1_u?a error I7e!tee' b r / { i 1`/ J ru�'-fL • �f3 � 7_ �,t(..� � Note: Pill SamNfes 4Ife ,'e,art RI frn• SiX Fvaaks frorn recaipi U.5 VSE C.MY Icepuk — f'1e �:r.: Two...ABf91K f-1 urfcssotf±eranagements?remade. I,u •„• �c„.c �;e), rlafear'b.•n: - nISTRIBUTION: M47Fr 8 Ye=Lti)4FRr..'r.r•, fc)ain.:^ifmy a!fr SI:rli;rti(r:J; F'!JK--� ie''.•utbnr G.py rvu:rvr..•a•! /.'anrLe.: F•:U-G3t �r!BC'I•�'-arc: ?-Gi-L15 SHEALY ENVIRONMENTAL SERVICES, INC. Sh=ly %m•irnpmN'4di :I v+ia�, ]iti. �-min--nt Alan: bar. hdE701 W-1 a { iient b`�l .t Al" r Pact 1 of I ;ample Receipt CheeWist (SAC) R.fferti•.r LtmC. Ft3+20I9 Onnl7.r tncnPAnrt hL:elate Pt .f') !'eho he r . ri. i''A11 A Y Means of receipt: Ta ..E5I ❑ Clicnl LIP'S [- FedEx D Oilier: ❑ Ycs �-n l Wra e ctutody seals present on the cooler? ._ Ycs D No h1A 'L. if cus ody seais wcre present, were they in [not and unbroken? plI Strip ID: C711orine Strip ID: _ Tested by: —� Or]ginul leriperaltir'e upon receipt! arived (!reeled) (emperalurc upon receipt: VaSolid Snap -Cup ID, k- rthod; i eanperatura 'lank.)=,Agabnst P3nules TR Gnu ID: �o TR Gun Correction Factor: e7 '(': I00thod of coolant: Wet Tut: ❑ Ice Packs L1 Dry ice i_ None 3. Iftcmperature ofany cook: exceeded 6-b°C, was Project VlanagerNotilied? D Yes ❑ Nu�'� I'N•I was Notified by: phone . email f Favu-to-face (circle one}. Cl Yes p r-3 No 2 ;NA d. Is the commercial courier's packing slip ariachcrl to this form? Yes D No S. tlrcrx proper custodypmcedultx (relhnquishud;rcccimel) followed? ices ❑ No 6. Were sample IDs lislud an the COM Z:yesl Nol 7. Wlsrr. sample IN listed on all sample containers? Ne S. Was coilection date &: time listed on the CO ? Yes CI No 9, Was collection ante.. R time listed on all sample container? Yes ❑ No 10. Did ull container label information (ID, date, lima) kigmc with the COC? [,Yes C T3o 1 I. Veic tests to be purfonnad lietcd on the COC? ❑ 1, es Vo 12. Did all .samples an'ive bi dwproper containers for each tes-, andlor !itgmid condition (unhmkcn, Jids lscs Gl N'ol 13. Was adequate sample volume avnailahle? es ❑ l�n { 1. Z:'Lzc all sarthples received within ii the holding time or48 knurl, whichever comes first? u Yes f^- rqo 1.,. wcrc any samples cuntalnUrS mtssingrexceat (ctrCJo one) <-arnples Not listed on COO, ❑ Yes ❑ No •rQ-F4A 16 For'v'OA and RSK-175 samples; were bubblcs present >"pea -sirs" (%"or 6nun is diameter) in _ nny of the \1OA vials? D 'Ye.; No A 17 'Worn all DROhnctolsfnuh•icni samples recPivcd at a p; i of •-:2? n Y'cs N7 L NA 18. A;7t:m all cyanide sate les received at a pl-i -> 12 and str fide. samples received at a pll ::, 9? D Y es C No E NA 19. VVt;rc all applicable TtiTl;rTK.I;,'c5aatidelphenol!ti25 1 0.5nig l.) mmpins aee of residual 01101-illZi . D Yes 0 Nn ONA 20, W'cre client remarks%Te.quests (i.e. requested dilutions, vIS.']VISD designations l caTeCtiy transcribed from. the COC into the comment section in LIMS? D Yes LEI No 21. Was the quote number listed on the container lubel? if yes, Ounte 4' _ Sample Presen•ation {Must be completed for any Snmp10(s) incorrectly preserved or, with headspacc.) Saluple(s) here received incorrectly preserved and were ndjusred acc-wdinely in sampic rccciving kvitln mL of circle one: 142SO4,1IN03,1101 NaOH using 5R 4 Time of preservation If more than one. preservative is needed, please note in rho comments below. Samples) _ werc received wit11 bubbles:,6 nnm in diameter. Samples(s) _., were received with TRC r 0.5 mg/L (If t119 is no) and were adjusted accordingiy in sampic receiving with soditan ltiosulfate (Na:S,(j;) v6th ShealyTD: f il SR harcode- labels applied by: f; ^ Date: ! 0 r Comments: pCL !i 6 L1 u !`:;+- i, - '� i r<t i !t/i lit �'r•r �t,l�ttfl -- l'1�`� 1'_, s, .., r, .� . Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 18 I ANNU- AL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 10.8 Land Owner: Calvin Morris Annual Dry Tons Applied: 41.6792 Site #: NC-AN-19 Acres Permitted: 10.8 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): NIA !-...... 1 XT-- r.PC-A (react ) rron 1 Max. PAN: 126 Crop 2 Name: Fescue (past.) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources S01I Precip. � 0 5 a Z P Nitrate PAN Applied Name of Crop Type o (enter one) Solids/ o /o A lied er pp p (NPDES #, WQ#, Cored. Past 24 a 't? '~ = CD w, TKN o B ao o and ( Ibs/acre) Receiving Residual o 0 Liquid Solids Acre Fert., Animal (Dry, Hrs. o N' N ' Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) inches 7 a mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 Apr 18 245 20.2 3.859 WWTPC D 0 S 0.5 0.3 28,200 6,240 12.6 75.027 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 ................... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): -......... TOTALS: 2451 As Cd Cu I Cr Pb Hg Mo Ni Se Zn P 75.027 0.000 Lime Applied Annual lbs/acre 0.128 0.014 3.820 1.289 0.091 0.003 0.286 0.353 0.039 4.639 85.670 :::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 1.312 0.214 15.106 23.123 2.92 0.091 2.392 4.427 0.501 84.153 Current Cumulative Ibs/ac 1.440 0.228 18.926 24.412 3.011 0.094 2.678 4.780 0.540 88.792 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit it PAN Limitlst/2n d Crop 126 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoruance warn a sysrem uesigueu w assu,-e LuaL qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Q *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, injection/Incorporation - 1.0 Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date - aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate Mr -KID c:rNo KA GCG tioignnAx ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 41.68 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Calvin Morris Owner: Same Predominant Soil Series: GOB-Goldston Acres Used: 10.8 Acres Permitted: 10.8 Site #: NC-AN-19 Field #: 1 Residual Analvsis Data (Heavy Metals and Total Phosphorus use me/ka. % Solids use Raw Percent #): Com- posite Date MENEM EM MEMEN Annual Heaw Metal Field LoadinLFs (Ualculated in lbs/acre): _Total 1 2 3 4 5 6j 71 81 9 LOJ 11 12 H �aDT/Ac:/ o (App, iEvent 3.86 Afsenic 0.000 0.000 1 0.000 0.000 0.000 0.128 0.000 0.000 0.000 0.000 0.000 0.000 1 0.128 Cadmium 0.000 0.000 0.000 0.000 0.000 0.014 0.000 0.000 . 0.000 0.000 0.000 0.000 j 0.014 .Copper 0.000 0.000 0.000 0.000 0.000 3.820 0.000 0.000 0.00.0 0.000 0.000 0.000 j 3.820 Chromium 0.000 0.000 0.000 0.000 0.000 1.289 0.000 0.000 0.000 0.000 0.000 0.000 1.289 ('MLpad 0.000 0.000 0.000 0.000 0.000 0.091 0.000 0.000 0.000 0.000 0.000 0.000 0.091 ':-Mercury 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.003 °lY b M; 0.000 0.000 0.000 0.000 0.000 0.286 0.000 0.000 0.000 0.000 0.000 � 0.000 ', 0.286 �, clenum :=Ticket 0.000 0.000 0.000 0.000 0.000 0.353 0.000 0.000 0.000 0.000 0.000 0.000 i, 0.353 I Selepium 0.000 0.000 0.000 0.000 0.000 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.039 ]'•Zinc 0.000 0.000 0.000 0.000 0.000 4.639 0.000 0.000 0.000 0.000 0.000 0.000 4.639 j Fie.T.otal V?40s 0.000 0.000 0.000 0.000 0.000 85.670 0.000 0.000 0.000 0.000 0.000 0.000 85.670 torus "l,certity, unuer penalty of law, tnat tnis aocument was prepareu unaer my uirecuUu or 5upe1_V151UU m AUUMUauco with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. )i+am aware that there are significant penalties for submitting false information, including the possibility of fines and frgprisonment for knowing violations". D'r/ a cp- ure of Land Applier 1 Date I DENR FORM MFLSF (12%2006),, ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 35.5 Land Owner: Harry Myers Annual Dry Tons Applied: 103.5250 Site #: NC-UN18 Acres Permitted: 35.5 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A !•..,., 1 TV-.- RPer"a (Pact 1 Crnn I Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources Soil Precip. Y C o z Y Nitrate PAN Applied Name of Crop Type o y (enter one) Solids/ o /o Applied per (NPDES #, WQ#, Cond. past 24 L? ;V = = a� 0 �, w TKN o o p and ( Ibs/acre) Receiving Residual 0 0 o Liquid Solids Acre Fert., Apimal D ( ry, Hrs. � �. o w c` « N N' N Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) inches c ° * * mglkg mg/kg mg/kg Crap I Crop 2 Crop I Crop 2 Apr 18 300 20.2 1.438 WWTPC D 0 S 0.5 1 0.3 28,200 6,240 1 12.6 27.949 NA Fescue Apr.18 25 24.68 0.146 WTPC D 0 S 0.5 0.4 12,200 21276 17 1.500 NA Fescue June 18 278 20.2 1.332 WWTPC D 0 S 0.5 0.3 28,200 6,240 12.6 25.900 NA Fescue 0.000 ' 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... :: ;:::::: Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... :: TOTALS: 603 0 ::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 55.349 0.000 Lime Applied Annuallbs/acre 0.098 0.011 2.888 0.980 0.068 0.002 0.217 0.264 0.029 3.443 63.363 :::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.956 0.113 14.297 14.812 1.935 0.034 0.726 2.358 0.123 46.226 Current Cumulative Ibs/ac 1.054 0.124 17.185 15.792 2.003 0.036 0.943 2.622 0.152 49.669 Permitted C. P. L. R.**** 36 1 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit 1 stl2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a system uesigneu Lv assu,-c LHUL qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Applier _ A __ Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land - _ _ - _- - - aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.. Cumulative Pollutant Loading Rate nFniR i:nRnn mcr: t19/9nnrn ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 103.52 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Harry Myers Owner: Same Predominant Soil Series: BdB2-Badin Acres Used: 35.5 Acres Permitted: 35.5 Site #: NC-UN18 Field #: 1 Residual Analvsis Data (Heavy Metals and Total Phosphorus use ms/k2, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6/11/18 6 6/11/18 71 8j 9 Lj 11j 12 % Solids 1 20.2 1 24.68 Arsenic 16.6 20.1 Cadmium 1.8 2.7 Copper 495 499 Chromium 167 189 Lead 11.8 7.95 Mercury 0.4 0.4 Molyb- denum 37 42.6 Nickel 45.7 37.8 Selenium 5 5 1"4aZinc 601 390 F, ;Total 1`l,Phos- P horus 11100 6400 Annual Heaw Metal Field Loadines (Calculated in lbs/acre): `!-.Vial 1 1 2j 31 4j 5 6 7 8 9 10 11 12 `D i,/Ac./ c App.in >v Event 2.77 0.15 ksenic 0.000 0.000 0.000 0.000 0.092 0.006 0.000 0.000 0.000 0.000 0.000 0.000 '. 0.098 Cadmium 0.000 0.000 0.000 0.000 0.010 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.000 .0.000 0.000 0.000 2.742 0.146 0.000 0.000 0.000 0.000 0.000 0.000 1888 Chromiu 0.000 0.000 0.000 0.000 0.925 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.980 (1ead 0.000 0.000 0.000 0.000 0.065 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.068 ::Mercury 0.000 0.000 0.000 0.000 0.002 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 ! 0.002. Nglyb '46num 0.000 0.000 0.000 0.000 0.205 0.012 0.000 0.000 0.000 0.000 0.000 0.000, 0.217 iNickel 0.000 0.000 0.000 0.000 0.253 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.264 Selenium 0.000 0.000 0.000 0.000 0.028 0.001 0:000 0.000 0.000 0.000 0.000 0.000 0.029 1,Z4ic 0.000 0.000 0.000 0.000 3.330 0.114 0.000 0.000 0.000 0.000 0.000 0.000 3.443 dTotal 0.000 0.000 0.000 0.000 61.494 1.869 0.000 0.000 0.000 0.000 0.000 0.000 63.363 h6rus "l`certiiy, unaer penalty of taw, that tms aocument was preparea unaer my airection or supervision in accoruance w,ith,a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Lam aware that there are significant penalties for submitting false information, including the possibility of fines and inip'risonment for knowing violations". PT of Land Applier Date DENR FORM MFLSF (12/20i.06) 4 - - ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. A Utilized• 34 2 Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Gres Land Owner: Harry Myers Annual Dry Tons Applied: 143.0040 Site #: NC-UN18 Acres Permitted: 34.2 Operator: Same Predominant Soil Series: GoB-Golston Cation Exchange Capacity (non 503): N/A /1...... 1 NT--.. P-- (PaQf 1 (`rnn 1 Max_ PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources Soil Cond. Precip. < o n X Y o Nitrate PAN Applied Name of Crop Type Receiving Residual o Y enter one Solids! ( ) o /o Applied per (NPDES #, WQ#, Past 24 cc 'o w ^ . TKN o and ( Ibs/acre) a� Liquid Solids Acre Fert., Animal D We ' Hrs. ' o * * n w Nitrite Application Crop 1 Crop 2 Crop l Crop 2 Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Moist) inches ° 0 c mg/kg mg/kg mg/kg Mar 18 225 17.99 0.997 WTPC D 0 S 0.5 0.4 13,200 1,390 16.4 10.836 NA Fescue May 18 240 20.2 1.194 WWTPC D 0 S 0.5 0.3 28,200 1 6,240 12.6 23.209 NA Fescue June 18 245 20.2 1.219 WWTPC D 0 S 0.5 0.3 28,200 6,240 12.6 23.693 NA Fescue Oct 18 117 26.8 0.772 WTPC D 0 S 0.5 0.4 19,100 746 128 12.111 NA Fescue 0.000 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... ::::::::::: ::::::::::::: Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): ...... :: ... . TOTALS: 827 0 ::::::.::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 69.849 O.000 Lime Applied Annuallbs/acre 0.158 0.080 4.080 1.504 0.111 0.002 0.332 0.317 0.064 3.662 66.223 :::::::::::::::::...:.:.:::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 4.527 0.362 21.72 17.44 4.983 1.437 3.297 4.238 2.229 58.325 Current Cumulative lbs/ac 4.685 0.442 25.800 18.944 5.094 1.439 3.629 4.555 2.293 61.987 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 ' 't 1st/ nd Crop Perm it PAN Limit 2 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accuraauce w1111 it 5ybao111 ucaigl,cu LU "00- �•...� qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of.Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate -_ nGnia r=nRnn FCF tiwinnm ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 143.02 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Hairy Myers Owner: Same Predominant Soil Series: GoB-Golston Acres Used: 34.2 Acres Permitted: 34.2 Site #: NC-UN18 Field #: 2 Residual Analvsis Data (Heave Metals and Total Phosphorus use me/ka. % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 3/20/18 4 5 6 6/11/18 7 81 91 10 10/1/18 11 12 % Solids 1 1 17.99 1 20.2 26.8 Arsenic 4.25 16.6 45.2 Cadmium 33.5 1.8 3.11 Copper 374 495 612 Chromium 199 1 167 195 Lead 21.8 11.8 6.54 Mercury 0.0249 0.4 0.02 Molyb- denum 43.5 37 43.2 Nickel 21.2 45.7 35.2 Selenium 0.5 5 25 ' i+'d! Ziric, 97 601 368 I�' oTotal (1 P;hos- n. phorus 2970 11100 4360 Annual Haaw Metal Viplrl 1 .natlinac it'alenlaten In Inginrre1: r' `Total 1 2 3 4 v 5 6 7 8 9 TO 11 12 H �DT/Ac./ !'App. ?Event 1.00 2.41 0.77 ' Air''§'enic 0.000 0.000 1 0.008 0.000 0.000 1 0.080 0.000 0.000 0.000 0.070 0.000 0.000 0.158 0,admium 0.000 0.000 0.067 0.000 0.000 1 0.009 0.000 0.000 0.000 0.005 0.000 0.000 0.080 j .;Copper 0.000 0.000 0.746 0.000 0.000 2.389 0.000 0.000 0.000 0.945 0.000 0.000 4.080 Chromium 0.000 0.000 0.397 0.000 0.000 0.806 0.000 0.000 0.000 0.301 0.000 0.000 f 1.504 ('Lead 0.000 0.000 0.043 0.000 0.000 0.057 0.000 0.000 0.000 0.010 0.000 0.000 ; 0.111 ::Mercury 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 I 0.002 j Nolyb- 0.000 0.000 0.087 0.000 0.000 0.179 0.000 0.000 0.000 0.067 0.000 0.000 0.332 r.denum �I ckel 0.000 0.000 0.042 0.000 0.000 0.221 0.000 0.000 0.000 0.054 0.000 0.000 0.317 I Selenium 0.000 0.000 1 0.001 0.000 0.000 0.024 0.000 0.000 0.000 0.039 0.000 0.000 0.064 INZinc 0.000 0.000 0.193 0.000 0.000 2.900 0.000 0.000 0.000 0.568 0.000 0.000 3.662 1 c.Total P4os- 0.000 0.000 5.922 0.000 0.000 53.569 0.000 0.000 0.000 6.732 0.000 0.000 66.22 -M 6rus y "tcertity, uncler penalty oI law, tnat tins aocumeni was prepareu unum- my LLlI V.-LIUJA V1 OUFVl ♦AORU- - aa.-uwaa.. with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. '!Team aware that there are significant penalties for submitting false information, including the possibility of fines and iinpi isonment for knowing violations". i S),pature of Land Applier Date ; _,...- DENR FORM MFLSF (12/2d06) "ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 7 Acres Utilized: 5.4 Land Owner: Harry Myers Annual Dry Tons Applied: 22.7176 Site #: NC-UN18 Acres Permitted: 5.4 Operator: Same Predominant Soil Series: CmB-Cid Cation Exchange Capacity (non 503): N/A r...,., 1 Nama• pPgnne (Past) Cron 1 Max. PAN: 141 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources Soil Precip. � < o g Z Y 5 Nitrate PAN Applied Name of Crop Type " one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 r; �'- ;0 W w _ ;i TKN, o � Go o and ( lbs/acre) Receiving Residual C .(enter Liquid Solids Acre Fert., Animal (Dry, Hrs. oa c * - * » CD o w Nitrite Application A Cu. Yds 'Gallons (Dry Tons/AC) Waste, etc) Wet Moist) inches o = mgtkg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 Oct 18 75 18.1 2.117 WWTPC D 0 S 1 0.5 0.3 40,700 4,140 172 55.935 NA Fescue Oct 18 50 26.8 2.090 WTPC D 0 S 0.5 0.4 19,100 746 128 32.780 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): :: :: :: . TOTALS: 125 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 88.714 0.000 Lime A lied Annuallbs/acre 0.288 0.017 4.277 1.310 0.082 0.000 0.284 0.356 0.126 5.209 77.077 Date lbs/ac Prior Years Cumulative lbs/ac 0.401 0.083 9.468 2.968 0.649 0.014 0.704 1.142 0.143 19.281 .:::....:: ::: Current Cumulative lbs/ac 0.689 0.100 13.745 4.278 0.731 0.014 0.988 1.498 . 0.269 24.490 Permitted C. P. L. R.**** 36 34 1 1338 X 267 15 1 X 1 374 89 2498 1 tJ2nd Cr Permit PAN Limit s op P 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance wire a sysrem aesigneu w assure tuaL qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibili of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land.Applier _ _ ._ _ Date aerobically digested -0.3, raw sludge -0.4 - _ ___ __ __ ________. _ - _______:_ d •__c. s= =__.__ ****C.P.L.R.: Cumulative Pollutant Loading Rate nGnta rnrnnn GeG /1010 AN ANNUAL METALS FIELD LOADING SUMMARY FORM* l•°�j ?!'"� ;;�"' itf� Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report;''Iil,,, 1+1a•�ility Name: City of Monroe Total Dry Tons Applied (Annual): l Pelr�mit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A I; Operator: Harry Myers Owner: Same Predominant Soil Series: CrnB=Cid ; 1 i. °Acres Used: 5! i .4 Acres Permitted: 5.4 Site #: NC-UN18 Field #: Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 3 4 5 6 7 8 9 10 11 12 •¢ 4t i' + ,� J ii +ill°� •li ra; i posite ,iiu,Date I, M1it 10/1/18 10/1/18 is 1!,;1 olids 18.1 1 26.8 Arsenic 23.4. 45.2 i Lead 1 ', !Mercur Wolyb- I denum P Nickel Annual in lbs/acre): 12.9 0.05 24.4 49.4 5 867 6.54 0.02 43.2 35.2 25 368 13900 1 4360 s ;.' _ Total _. 1 2 3 4 5 6 7 8 9 10 11 12 H SDi /Ac./ (;App. y !Event 2'.12 2.09 1 Ai"senic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099 0.189 0.000 0.288 Catllriium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 0.013 0.000 0.017 ,Copper 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.719 2.558 0.000 4.277 G;lir6mi 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.495 0.815 0.000 1,310 i'�1.4ead 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.055 0.027 0.000 !' 0.082 :'.Mercury 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 °'I 0.000 Molyb- p. denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.103.1 0.181 0.000 0.284 "jNickel 0.0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.209 0.147 0.0W 0.356 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 0.105 0.000 0.126 1,Zinc 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3..671 1.538 0.000 J 5.209 `-4,Ti otal I?lios- 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 58.853 18.225 0.000' 77.08 )iorus l:1certily, unaer penairy of iaw, inar ims aocument was prepareu unuer uiy uu-ecuuu �1 bupc, v,a,vi, m auw-u. U"11�c with a system. designed to assure that qualified personnel properly gathered and evaluated the information submitted. I!.a'pi' aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". + Signature of Land Applier Date ° DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: I Acres Utilized: 6.5 Land Owner: Wayne McBride Annual Dry Tons Applied: 24.2281 Site #: NC-UN25 Acres Permitted: 6.5 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A ram,..,., 1 wnmo• FP.Cf liP. (Pact) Cron 1 Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Volume applied Pp Volume Residual Sources Soil Precip. Y o 5 Z � Nitrate PAN Applied Name of Crop Type Y enter one Solids/ ( ) o /o A lted er PP P (NPDES #, WQ#, Cond. past 24 b °= _ w TKN o E3 and ( Ibs/acre) Receiving Residual +' o Liquid Q Solids Acre Fert., Animal D ( ry' Ham• �. o � n � w * N' o Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) inches o 0 mg/kg mglkg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 Sept 18 89 20.72 2.389 WWTPC D 0 S 0.5 0.3 28,000 5,740 1 29 45.764 NA Fescue Sept 18 42 24.591 1.338 WTPC D 0 S 0.5 0.4 5,770 1,100 64.2 6.643 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 1311 As Cd Cu C_r Pb Hg Mo Ni Se Zn P 52.407 1 0.0o0 Lime Applied Annuallbs/acre 0.101 0.012 3.190 1.129 0.083 0.003 0.239 0.329 0.037 4.064 74.579 :::::::::::::::::::::::::::::::: :: Date lbs/ac Prior Years Cumulative lbs/ac 0.947 0.109 15.68 12.582 1.483 0.04 1.77 2.092 0.096 35.732 :: July 18 2088 Current Cumulative lbs/ac 1.048 0.121 18.870 13.711 1.566 0.043 2.009 2.421 0.133 39.796 Permitted C. P. L. R.**** 36 34 1 1338 X 267 1 15 X 374 1 89 2498 Perm it PA N Limit is t/2nd Cro P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witn a system aestgneu to assure teat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includi g the possibili o tnes and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier_ _ _ _ Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, _ aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DFNR FORM FSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 24.23 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Wayne McBride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 6.5 Acres Permitted: 6.5 Site #: NC-UN25 Field #: 1 Residual Analvsis Data (Heaw Metals and Total Phosphorus use me/ke. % Solids use Raw Percent #): Com- posite Date Annual Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ti'yTotal 1 2 3 4 51 61 7 8 9 10 11 12 (App. m {Event 2.39 1.34 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.056 0.045 0.000 0.000 0.000 0.000 0.101 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.005 0.007 0.000 0.000 0.000 0.000 �: 0.012 :Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.739 1.450 0.000 0.000 0.000 0.000 3.190 Chromium0.000 0.000 0.000 0.000 0.000 0.000 0.535 0.594 0.000 0.000 0.000 0.000, 1.129 C,L^ead 0.000 0.000 0.000 0.000 0.000 0.000 0.065 0.018 0.000 0.000 0.000 0.000 0.083 ::Mercury. 0.000 0.000 0.000 0.000 0.000 1 0.000 0.002 0.001 0.000 0.000 0.000 0.000 0.003 Mplyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.108 0.131 0.000 0.000 0.000 0.000- 0.239 } d"e"num �,%hckel 0.000 0.000 0.000 0.000 0.000 0.000 0.235 0.094 0.000 0.000 0.000 0.000 0.329 $elepium 0.000 0.000 0.000 0.000 0.000 0.000 0.024 0.013 0.000 0.000 0.000 0.000 ; 0.037 'I4zin6 0.000 0.000 0.000 0.000 0.000 0.000 3.526 0.538 0.000 0.000 0.000 0.000 4.064 K3 oTotal Ehos- 0.000 0.000 0.000 0.000 0.000 0.000 69.281 5.298 0.000 0.000 0.000 0.000 74.579 " I•,certify, under penalty of law, that this document was prepared under my direction or supervision in accord 1 with a system designed to assure that qualified personnel properly gathered and evaluated the information su lam aware that there are significant penalties for submitting false information, including the possibility of fin imprisonment for knowing violations". ,p'l' s and , � Signature of Land Applier Date {. !!; !�„l DENR FORM MFLSF (12/2006 ) liri,,r.,, - _ ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized: 14.1 Land Owner: Wayne McBride Annual Dry Tons Applied: 55.3160 Site #: NC-UN25 Acres Permitted: 14.1 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A ('rnn 1 Namec Fescue (Past_1 Cron I Max. PAN: 137 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o Y 0 o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) precip. Past 24 Hrs. inches D o w _ * ° o _ * N' * � w * N' F o TKN mglkg Z 3 8 o C a �' mglkg Nitrate and Nitrite mglkg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 Sept 18 317 20.72 3.923 WWTPC D 0 S 0.5 0.3 28,000 5,740 29 1 75.143 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ....... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 317 0 :::::::::::::: As Cd Cu I Cr Pb Mo Ni Se Zn P 75.143 0.00o Lime A2plied Annual lbs/acre 0.092 0.008 2.856 I 0.879 0.106 -HE 0.003 0.177 0.385 0.039 5.790 113.767 :::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.966 0.138 15.546 13.857 1.449 0.036 1.773 2.214 0.223 38.911 :::.........:::::....:.:.::::::::::::::::::::: ................. Current Cumulative lbs/ac 1.058 0.146 18.402 14.736 1.555 0.039 1.950 2.599 0.262 44.701 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PAN Limit lsd2nd Crop 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system aeslgnea to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (� *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date - - -- --- - - aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nFNR FORM FRF (12(200M ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 55.31 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Wayne McBride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 14.1 Acres Permitted: 14.1 Site #: NC-UN25 Field #: 3 Residual Analvsis Data (Heavy Metals and Total Phosphorus use me/ke. % Solids use Raw Percent ft Com- posite Date Annual Annual Heavy Metal Field Loadings (Ualculated in lbs/acre): `Total "DT /Ac./ `APP• ;Event 1 2 3 4 5 6 7 3.92 8 9 10 11 12 H y Arsenic 0.000 0.000 0.000 0.000 0.000 0.000. 0.092 0.000 0.000 0.000 0.000 0.000 0.092 Cadrimium 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.000 0.000 0.000 0.000 0.000 j 0.008 ,Copper 0.000 0.000 0.000 0.000 0.00.0 0.000 2.856 0.000 0.000 0.000 0.000 0.000 j 2.856 cliflorriium 0.000 0.000 0.000 0.000 0.000 0.000 0.879 0.000 0.000 0.000 0.000 0.000 0.879 (:'.Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.106 0.000 0.000 1 0.000 0.000 0.000 0.106 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.003 1 0.000 0.000 0.000 1 0.000 0.000 ' 1 0.003 N�lolyb- ;, denum 0.000 0.000 0.000 0.000 0.000 0.000 0.177 0.000 0.000 0.000 0.000 0.000 0.177 Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.385 0.000 0.000 0.000 0.000 0.000 0.385 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.039 0.000 0.000 0.000 0.000 0.000 0.039 a,Zinc 0.000 0.000 0.000 0.000 0.000 0.000 5.790 0.000 0.000 1 0.000 0.000 0.000 5.790 ;ye�i,otal Pho"s- 0.000 0.000 0.000 0.000 0.000 0.000 113.767 0.000 0.000 1 0.000 0.000 0.000 113.70 "'I:certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". • 1X /' rI Signature of Land Applier Date DENR FORM MFLSF',(12120;06) j! C;ail, ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 15.4 Land Owner: Emerson McBride Annual Dry Tons Applied: 74.1075 Site #: NC-UN26 Acres Permitted: 15.4 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Cann 1 Nnme- Fescue Croo 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 Volume applied PP Volume Residual Sources Soil Precip. a n c �y 5 Z Y q B Nitrate PAN Applied Name of Crop Type 0 y (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 a °» ?, w TKN �o o and (Ibs/acre) Receiving Residual °0 o � Liquid Solids Acre Fert., Animal (Dry, Hrs. o w + N * `y a w Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet Moist) inches a o. � * R. o a * o' mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 - Crop 2 Aug 18 325 20.72 3.683 WWTPC D 0 S 1 0.3 0.5 28,000 1 5,740 29 94.871 NA Fescue Aug 18 84 24.59 1.130 WTPC D 0 S 0.4 0.5 5,770 1,100 64.2 6.414 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 4091 As Cd Cu Cr Pb 112 Mo Ni Se Zn J P 101.285 0.000 Lime Applied Annual lbs/acre 0.125 0.013 3.906 1.327 0.115 0.004 0.276 0.441 0.048 5.890 111.282 ::::::::::::::::::::::::::::::::::: :: Date lbs/ac Prior Years Cumulative lbs/ac 0.824 0.13 15.14 11.455 1.632 0.027 1.489 2.161 0.19 41.095 :: July 18 2088 Current Cumulative lbs/ac 0.949 - 0.143 19.046 12.782 1.747 0.031 1.765 2.602. 0.238 46.985 :::: Permitted C. P. L. R.**** 36 34 1338 1 X 267 15 X 374 89 2498 Permit PA N Limit lst/2nd C ro P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system aeslgnea to assure mat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation �- **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 .. *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land_Applier._ Date ------_= -. aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nFNR FnRnn F-qi= n9/9nnrn ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 74.12 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson Mcbride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 15.4 Acres Permitted: 15.4 Site #: NC-UN26 Field #: 1 Residual Analvsis Data (Heave Metals and Total Phosphorus use me/ke, % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6 7 j 7/9/18 8 7/9/18 91 10 11 12 % Solids 1 20.72 1 24.59 Arsenic 11.7 17 Cadmiumi 1 2.62 Copper 1 364 542 Chromium 112 222 Lead 13.5 6.87 Mercury 0.4 0.4 Molyb- denum 22.5 49 Nickel 49.1 35.3 Selenium 5 5 Fijz,7ric , 738 201 ,'� Total pAos-, ,, phorus 14500 1980 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): - _,Total 1 2 3 4 5 6 7 8 9 10 11 12 H "+DT/Ac./ C (A pp. Event 3.68 1.13 AFr'senic 0.000 0.000 0.000 0.000 0.000 0.000 0.086 0.038 0.000 0.000 0.000 0.000 0.125 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.006 0.000 0.000 0.000 0.000 0.613 ,Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.681 1.225 0.000 0.000 0.000 0.000 ! 3.906 qhr,9mium 0.000 0.000 0.000 0.000 0.000 0.000 0.825 0.502 0.000 0.000 0.000 0.000 1.327 (Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.099 0.016 0.000 1 0.000 0.000 0.0001 0.115 'Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.003 1 0.001 0.000 0.000 0.000 0.000 1 0.004 Molyb- 0.000 0.000 0.000 0.000 0.000 0.000 0.166 0.111 0.000 0.000 0.000 0.000.' 0.276 denum l k;Nckel 0.000 0.000 0.000 0.000 0.000 0.000 0.362 0.080 0.000 0.000 0.000 0.000-', 0.441 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.037 0.011 0.000 0.000 0.000 0.000 0.048 'Zinc 0.000 0.000 0.000 0.000 0.000 0.000 5.436 0.454 0.000 0.000 0.000 0.000 5.890 I ;gtal " Phos- 0.000 0.000 0.000 0.000 0.000 0.000 106.807 4.475 0.000 0.000 0.000 0.000' 111.282 11 Certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with;a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Ia am aware that there are significant penalties for submitting false information, including the possibility of fines and i prisonment for knowing violations". ,. nature of Land Applier Date DENR FORM MFLSF (12126,,06'' ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 6.1 Land Owner: Emerson McBride Annual Dry Tons Applied: 21.8123 Site #: NC-UN26 Acres Permitted: 6.1 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A rnn 1 Nnme! Fescue Cron I Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 Y °� o A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. We , Moist) Precip. Past 24 Hrs. inches a o ° C w * N � c� *w' * TKN mg/kg z a El 0o o 2. mg/kg Nitrate and Nitrite mglkg PAN Applied ( lbs/acre) Name of Crop Type' Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Aug 18 125 20.72 3.576 WWTPC D 0 S 0.3 0.5 28,000 5,740 29 92.119 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ............ TOTALS: 125 0 ::::::::::::: As Cd Cu Cr Pb Hg Mo Ni SeP43.454 P 92.119 0.000 Lime A lied Annuallbs/acre 0.084 0.007 2.603 0.801 0.097 0.003 0.161 0.351 0.036103.704::::::;::: :::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.733 0.112 14.664 10.19 1.729 0.027 1.349 2.21 0.184 ::Current Cumulative lbs/ac 0.817 0.119 17.267 10.991 1.826 0.030 1.510 2.561 0.220 Permitted C. P. L. R.**** 36 34 1338 X 1 267 15 1 X 1 374 89 1 2498 :: Permit PAN Limit is t/2nd Crop P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system uesignea to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possib'lity of fines and imprisonment for knowing violations." - *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 xx Mineralization Rates: Compost -0.1, anaerobially digested -0.2, ----- Signature of Land Applier= _ - _ _ Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nF=NR F:nRM FGF ii9i9nnnl ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 21.81 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: TaB2-Tatum Acres Used: 6.1 Acres Permitted: 6.1 Site #: NC-UN26 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use ma/ka. % Solids use Raw Percent #): Com- posite NEEME" MW on Non Date Annual Heavy Metal Field Loadings (Calculated in lbs/acre): O% Total mT/Ac./ (App• ;Event 1 _2j 31 41 51 6 7 3.58 8 9 LIIJ 12 i rt y Arsenic 0.000 0.000 .0.000 0.000 0.000 0.000 0.084 0.000 0.000 0.000 0.000 0.000 0.084 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.000 0.000 0.000 0.000 0.000 0.000 2.603 0.000 0.000 0.000 0.000 0.000 2.603 Chromiu 0.000 0.000 0.000 0.000 0.000 0.000 0.801 0.000 0.000 0.000 0.000 0.000 0.801 t:Lead 0.000 0.000 1 0.000 0.000 0.000 0.000 0.097 0.000 0.000 0.000 1 0.000 0.000 0.097 ,"-Mercury 0.000 0.000 0.000 0.000 0.000 '0.000 0.003 0.000 0.000 0.000 0.000 0.000 ! 0.003 Molyb- de'num 0.000 0.000 0.000 0.000 0.000 0.000 0.161 0.000 0.000 0.000 0.000 0.000... 0.161 -`i ckel 0.000 0.000 0.000 0.000 0.000 0.000 0.351 0.000 0.000 0.000 0.000 0.000.-' 0.351 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.036 0.000 0.000 0.000 0.000 0.000 0.036 1?-Zinc 0.000 0.000 0.000 0.000 0.000 0.000 5.278 0.000 0.000 0.000 0.000 0.000 5.278 Scrotal Plios- 0.000 0.000 0.000 0.000 0.000 0.000 103.704 0.000 0.00010 0.000 0.000 0.000 103.704 " '-horus "Il:cqtify, under penalty of law, that this document was prepared under my direction or supervision in accordance with;a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I 0,nm;aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". „" �gnature of Land Applier Date ! DENR FORM MFLSF (12/2006) E; 11 I ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: W00001346 Field #: 3 Acres Utilized: 10.5 Land Owner: Emerson McBride Annual Dry Tons Applied: 35.4232 Site #: NC-UN26 Acres Permitted: 10.5 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue Crop 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 a) V o A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons o/a Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NpDES # WQ#, Fert., Animal Waste, etc) Soil Cond. D ( ry, Moist) precip. pit 24 Hrs. inches Y b 0• o c� a P. * o w �» � _ * N' a w e * N' * * = TKN mg/kg z a o aD c g �. mg/kg Nitrate and Nitrite mglkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 Aug 18 203 20.72 3.374 W WTPC D 0 S 0.3 0.5 28,000 5,740 29 86.912 NA Fescue 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 203 As Cd Cu Cr Pb HR Mo I Ni Se I Zn P 86.912 0.000 Lime Applied Annual lbs/acre 0.079 0.905 0.984 36 0.007 0.147 0.154 34 2.456 18.364 20.820 1338 0.756 16.728 17.484 X 0.091 1.951 2.042 267 0.003 0.033 0.036 15 0.152 1.734 1.886 X 0.331 2.679 3.010 374 0.034 0.229 0.263 89 4.980 49.905 54.885 2498 97.846 ;:::::;:;:::::;:;::::::::::;: ::: Date lbs/ac Prior Years Cumulative lbs/ac July 18 2088 Current Cumulative lbs/ac Permitted C. P. L. R.**** d Crop e PAN Limit lsb2n C Permit A P 137 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includ'ng the possib'li of fines and imprisonment for knowing violations." --*Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applieri Date* Mineralization Rates: Compost -0.1, anaerobially digested -0.2, _ aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nGnin Gnnnn Gec fi wonnai ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 35.43 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 10.5 Acres Permitted: 10.5 Site #: NC-UN26 Field #: 3 Residual Analvsis Data (Heavy Metals and Total Phosphorus use ni&kg, % Solids use Raw Percent #): Com- posite Date Annual Annual Heavy Metal Field Loadings (Calculated in lbs/acre): '�tTotal !'aDT Ac./ I,/ 66 pp: ZEvent 1 _2j 31 4 5 6 71 3.37 8 9 10 11j 12 y Arsenic 0.000 0.000 1 0.000 0.000 0.000 0.000 0.079 0.000 0.000 0.000 0.000 0.000 s 0.079 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.000 0.000 0.000 0.000 ; 0.007 ;(Popper 0.000 0.000 0.000 0.000 0.000 0.000 2.456 0.000 0.000 0.000 0.000 0.000 .2.456 Chrbniium 0.000 0.000 0.000 0.000 0.000 0.000 0.756 0.000 0.000 . 0.000 0.000 0.000 0.756 QLead 0.000 0.600 0.000 0.000 0.000 0.000 0.091 0.000 0.000 0.000 0.000 0.000 1 0.091 ::Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 1 0.000 0.000 0.003 dT:".. , enum 0.000 0.000 0.000 0.000 0.000 0.000 0.152 0.000 0.000 0.000 0.000 0.000 0.152 1NciFe1 0.000 0.000 0.000 0.000 1 0.000 0.000 0.331 0.000 0.000 0.000 0.000 0.000, 0.331 Selenium 0.000 0.000 1 0.000 0.000 .000 0.000 0.034 0.000 0.000 0.000 0.000 0.000 0.034 j,Zinc 0.000 0.000 0.000 0.000000 H0. 0.000 4.980 0.000 0.000 0.000 1 0.000 0.000 4.980 ,;c}liotal -nI?hos- 0.000 0.000 0.000 0.000 0.000 0.000 97.846 0.000 0.000 0.000 0.000 0.000 97.846 _' "'brus ITI ertify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I�am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". v � I ature of Land Applier Date Id, i 1i t 1 f 1'�� ' DENR FORM MFLSF �'(1212006)', .' ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City Of Monroe WQ Permit #: WQ0001346 Field #: 4A Acres Utilized: 12.1 Land Owner: Emerson McBride Annual Dry Tons Applied: 56.6848 Site #: NC-UN26 Acres Permitted: 12.1 Operator: Same Predominant Soil Series: TaB-Tatum Cation Exchange Capacity (non 503): N/A rrnn 1 Name- Fescue Cron 1 Max. PAN: 137 Crop 2 Name: Fescue Crop 2 Max. PAN: QLiquid Volume applied (enter one) Solids/ Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil CDond. W Moist) Precip. Past 24 Hrs. inches a �' CL o * ° C o * 5 * TKN mglkg Z a @ • mglkg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 Aug 18 275 20.72 3.966 WWTPC D 0 S 0.3 0.5 28,000 5,740 29 102.169 NA Fescue Aug 18 42 24.59 0.719 WTPC D 0 S 0.4 0.5 5,770 1,100 64 4.082 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 317 0 ::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 106.251 0.000 Lime Applied Annuallbs/acre 0.117 0.012 3.667 1.208 0.117 0.004 0.249 0.440 0.047 6.143 117.861 ::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative Ibs/ac 0.925 0.142 19.107 12.202 2.025 0.033 1.79 2.64 0.235 49.511 ::: Current Cumulative lbs/ac 1.042 0.154 22.774 13.410 2.142 0.037 2.039 3.080 0.282 55.654 Permitted C. P. L. R.**** 36 34 1 1338 X 267 15 X 374 1 89 2498 ;: 2 Perm it PAN Limit 1st/ nd Crop P 137 50 0°I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system aesignea to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibili o nes and imprisonment for knowing violations." Q -*Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 _ = Signature of Land Applier_ . Date **x Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate n;=Kip Fr)phn GRF /19/9f nR\ ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 56.69 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson Me Bride Owner: Same Predominant Soil Series: TaB-Tatum Acres Used: 12.1 Acres Permitted: 12.1 Site #: NC-UN26 Field #: 4A Residual Analvsis Data (Heave Metals and Total Phosphorus use ma/ka. % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 41 5 6 7 7/9/18 8 7/9/18 9 10 11 12 % Solids 20.72 1 24.59 Arsenic 11.7 17 Cadmiumi 1 2.62 Copper 1 364 542 Chromium 112 222 Lead 13.5 6.87 Mercury 0.4 0.4 Molyb- denum 22.5 49 Nickel 49.1 35.3 Selenium 5 5 Vazinc 738 201 1��;Tota1 Pos- horus 14500 1980 ' Annual Heave Metal Field LoadinLFs (Ualculated in lbs/acre): 61�1Total 1 2 3 4 5 6 7 8 9 10 12 _... y ,BTi /Ac./ {Apo- r(0). 14 jEvent' 3.97 0.72 Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.093 0.024 0.000 0.000000 0.000 0.117 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.004 0.000 0.000 0.000 0.000 0.012 ,hopper 0.000 0.000 0.000 0.000 0.000 0.000 2.887 0.779 0.000 0.000 0.000 0.000 ; 3.667 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.888 0.319 0.000 0.000 0.000 0.000 1.208 CLead 0.000 0.000 0.000 0.000 0.000 0.000 0.107 1 0.010 0.000 0.000 0.000 0.000 0.117 ,;.1V4ercury 0.000 0.000 0.000 0.000 0.000 0.000 0.003 1 0.001 0.000 0.000 1 0.000 0.000 0.004 lolyb- 0.000 0.000 0.000 0.000 0.000 . 0.000 0.178 0.070 0.000 0.000 0.000 0.000. 0.249 '.-denum -Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.389 0.051 0.000 0.0.00 0.000 0.000 0.440 Selenium 0.000 0.000 0.000 0.000 0.000. 0.000 0.040 0.007 0.000 0.000 0.000 0.000 0.047 i Zinc 0.000 0.000 0.000 0.000 0.000 0.000 5.854 0.289 0.000 0.000 0.000 0.000 6.143 ,SeT;otal 1?lios- 0.000 0.000 0.000 0.000 0.000 0.000 115.014 2.847 0.000 0.000 0.000 0.000' 117.861 -_ hoi;us N "1i-,rtily, under penalty of law, tnat tnls document was prepareu unuer my airecuon or supervision in accoruance jj�ej h,a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Ikatn"aware that there are significant penalties for submitting false information, including the possibility of fines and ° im'p,risonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) fl�ITCYI p �' _______-ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 4B Acres Utilized: 12.7 Land Owner: Emerson McBride Annual Dry Tons Applied: 40.8917 Site #: NC-UN26 Acres Permitted: 12.7 Operator: Same Predominant Soil Series: CmB-CID Cation Exchange Capacity (non 503): N/A Cron 1 Name: Fescue Cron 1 Max. PAN: 141 Crop 2 Name: Fescue Crop 2 Max. PAN: 50 o .r �4 o Q Volume applied enter one Solids/ ( ) Liquid q Cu. Yds Gallons u /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. W , Moist) Preci P• Past 24 Hrs. inches Y � b 5 T3 0 o c �. ° = * » c°o w * * TKN mg/kg Z a 9 o 9 w O gam-,• mg/kg Nitrate and Nitrite mglkg 1 29 PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 July 18 175 20.72 2.405 WWTPC D 0 S 0.3 1 0.5 28,000 5,740 61.945 NA Fescue July 18 50 24.59 0.815 WTPC D 0 S 0.4 0.5 5,770 1,100 64.2 4.630 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 225 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 66.575 0.000 Lime A lied Annuallbs/acre 0.084 0.009 2.634 0.901 0.076 0.003 0.188 0.294 0.032 3.877 72.972 :::::::::::::::::::::::::::::::: Date Ibs/ac Prior Years Cumulative lbs/ac 0.71 0.123 13.697 10.755 1.697 0.03 1.278 2.159 0.172 42.207 Current Cumulative Ibs/ac 0.794 0.132 16.331 11.656 1.773 0.033 1.466 2.453 0.204 46.084 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 1 374 1 89 2498 i t/2nd Cr o Permit PAN Limit is P 141 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 - Signature of Land Applier; ,- _ Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nCn10 rnone COC i4o1')nnaX ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 40.89 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: CmB-Cid Acres Used: 12.7 Acres Permitted: 12.7 Site #: NC-UN26 Field #: 4B Residual Analvsis Data (Heavv Metals and Total Phosnhorus use mg/kg. % Solids use Raw Percent #): Sample or Com- posite Date 1 2 3 4 5 6j 7j 7/9/18 8 7/9/18 9 10 11 12 % Solids 20.72 1 24.59 Arsenic 11.7 17 Cadmium 1 2.62 Copper 364 542 Chromium 1 112 222 Lead 13.5 6.87 Mercury 0.4 0.4 Molyb- denum M5 49 Nickel 49.1 35.3 Selenium 5 5 V aZinc 738 201 a k r,J�ptal }jDpp- hors 14500 1980 Anneal Heaw Metnl Field l.nadinus lt.alculated in ins/acren a !"",Total 1 2j 3 4 5 6 7 8 9 10 11 12 y fA PP• 41Event 2.41 0.82 Arsenic 1 0.000 0.000 0.000 0.000 0.000 0.000 0.056 0.028 0.000 0.000 0.000 0.000 0.08.4 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.005 0.004 0.000 0.000 0.000 0.000111 0.009 ,Copper 0.000 0.000 0.000 0.000 0.000 0.000 1.751 0.883 0.000 0.000 0.000 0.000 2.634 Chromium 0.000 0.000 0.000 0.000 0.000 0.000 0.539 0.362 0.000 0.000 0.000 0.000 j 0.901 I Lead 0.000 ' 0.000 0.000 0.000 0.000 0.000 0.065 1 0.011 0.000 0.000 0.000 0.000 0.076 ::Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.002 0.001 0.000 0.000 0.000 0.000 I; 0.003 Molyb- "� 0.000 0.000 0.000 0.000 0.000 0.000 0.108 0.080 0.000 0.000 0.000 0.000.1i 0.188 denum iiN ckel 0.000 0.000 0.000 0.000 0.000 0.000 0.236 0.058 0.000 0.000 0.000 0.000' 11 0.294 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.024 0.008 0.000 0.000 0.000 0.000 j' 0.032 1*Zinc: 1 0.000 0.000 0.000 0.000 0.000 0.000 3.550 0.328 0.000 0.000 0.000 0.000 ;! 3.877 ( Total 0.000 0.000 0.0.00 0.000 0.000 0.000 69.745 3.227 0.000 0.000 0.000 0.000I 72.972 I '- horus "Iicertify, under penalty of law, that this document was prepared under my airecnon or supervision in acwruance w:in h a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. �aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" a 1)77'I ii f Signature of Land Applier Date DENR FORM MFLSF (1�2/2006J ,� ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 6 Acres Utilized: 14 Land Owner: Emerson McBride . Annual Dry Tons Applied: 59.1278 Site #: NC-UN26 Acres Permitted: 25.8 Operator: Same Predominant Soil Series: TaB2-Tatum Cation Exchange Capacity (non 503): N/A f'rnn t Name- Fescue (hav) CroD 1 Max. PAN: 137 Crop 2 Name: Fescue (hay) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources Soil Precip. Y C o Z a 51 Nitrate PAN Applied Name of Crop Type o (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 .'' w y w w TKN 00 o and ( Ibs/acme) Receiving Residual Solids Acre Fert.,.Animal (Dry, Hrs. 0 0 o� E # T --• fD ° o w Nitrite Application QLiquid Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet Moist) inches c � * 0 mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2 July 18 289 20.72 3.602 WWTPC D 0 S 0.3 0.5 28,000 5,740 29 92.798 NA Fescue July 18 42 24.59 0.621 WTPC D 0 S 0.4 0.5 5,770 1,100 64.2 3.528 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ......... .... TOTALS` 331 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 96.326 0.000 Lime Applied Annual lbs/acre 0.105 0.010 3.295 1.083 0.106 0.003 0.223 0.398 0.042 5.566 106.917 :::::::::::::::::::::::::::.: Date I lbs/ac Prior Years Cumulative Ibs/ac 0.412 0.068 11.865 4.041 0.952 0.013 0.993 1.22 0.144 20.364 Current Cumulative lbs/ac 0.517 1 0.078 15.160 5.124 1.058 0.016 1.216 1.618 0.186 25.930 Permitted C. P. L. R.**** 36 34 1 1338 1 X 267 15 X 374 1 89 2498 Permit PAN Limt i 1 st/2nd Crop 137 I 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witn a system aesignea to assure tuat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possi ility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation l "/9 **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier _ Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate mr-Kip G()PKA GCF !1g/7nrim r�P ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 59.12 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Emerson McBride Owner: Same Predominant Soil Series: TaB2-Tatum Acres Used: 14 Acres Permitted: 25.8 Site #: NC-UN-26 Field #: 6 Residual Analvsis Data (Heave Metals and Total Phosphorus use mii/ka, % Solids use Raw Percent #): Sample or Com- posite Date 11 21 3 4 5 6 7 7/9/18 8 7/9/18 9 10 11 12 % Solids 20.72 24.59 Arsenic 11.7 17 Cadmium 1 2.62 Copper 364 542 Chromium 112 1222 Lead 13.5 6.87 Mercury 0.4 0.4 Molyb- denum 22.5 49 Nickel 49.1 35.3 Selenium 5 5 F"IZihe 738 201 {[Wotal P,hos- �• horus 14500 1980 Anneal Heave Metal Vield I ,nodinuc (Calculated in Ills/acrel: 1 2j 3 4 v 51 61 7 _8j 91 LOJ 11 12 y (A y iE ent 3.60 0.62 Arsenic 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.084 0.021 0.000 0.000 0.0001 0.000 0.105 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.003 0.000 0.000 0.00.0 0.000 ; 0.010 ,Copper 0.000 0.000 0.000 0.000 0.000. 0.000 2.622 0.673 0.000 0.000 0.000 0.000 3.295 Chromium 0.000. 0.000 0.000 0.000 0.000 0.000 0.807 0.276 0.000 0.000 0.000 0.00011 1.083 (Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.097 0.009 0.000 0.000 0.000 0:000 ' 0.106 ,..Mercury 0.000 0.000 0.000 ' 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.003 lolyb- -denum 0.000 0.0.00 0.000 0.000 0.000 0.000 0.162 0.061 0.000 0.000 0.000 0.000 1, 0.223 `Nickel 0.000 0.000 0.000 0.000 0.000 0.000 0.354 0.044 0.000 0.000 0.000 0.000 0.398 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.036 0.006 0.000 0.000 0.000 0.000 f 0.042 Zinc 0.000 0.000 1 0.000 0.000 0.000 0.000 5.317 0.250 0.000 0.000 0.000 0.000 5.566 z, :Total 0.000 0.000 0.000 0.000 0.000 0.000 104.458 2.459 0.000 0.000 0.000 0.000" 106.9117 4J`1�'bi•us y " Vicertify, under penalty of law, that this document was prepares under my uirectlon or supervision in accuruance PIwith;a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I,am, aware that there are significant penalties for submitting false information, including the possibility of fines and ;''imprisonment for knowing violations". Signature of Land Applierrrr Date I DEN FORM MFLSF (12/2006) -ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 13.4 Land Owner: Leland Wolfe Annual Dry Tons Applied: 48.6692 Site #: NC-UN27 Acres Permitted: 13.4 Operator: Same Predominant Soil Series: G_sB-Goldston Cation Exchange Capacity (non 503): N/A 91- 1 Noma• FacnnP (Pact 1 Crnn 1 Max. PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 Volume applied Volume Residual Sources Soil Precip. • n G 2 a r S Z a Nitrate PAN Applied Name of Crop Type 34 (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 c 'b ;0m w TKN OQ o and ((bs/acre) Receiving Residual Liquid Solids Acre Fert., Animal (Drys Hrs. = c c * N - CD Z. �, Nitrite - Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet Moist) inches $ * mg/kg mglkg mg/kg Crop 1 Crop 2 Crop I Crop 2 Apr 18 225 20.2 2.856 WWTPC D 1 0 S 0.5 0.3 28,200 6,240 1 12.6 55.533 NA Fescue Apr 18 50 24.68 0.776 WTPC D 0 S 0.5 0.4 12,200 2,270 17.3 7.948 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this forEb.482 ................... TOTALS: 275 As Cd Cu Cr Pb H Mo Ni Se Zn 0.000 Lime Applied Annuallbs/acre 0.095 0.010 2.827 0.954 0.067 0.002 0.211 0.261 0.029 1 3.433 63.403 ::::::::::::::;:::;:;::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.36 0.065 9.695 3:174 0.876 0.012 0.711 1.154 - 0.134 20.539 Current Cumulative lbs/ac 0.455 0.075 12.522 4.128 0.943 0.014 0.922 1.415 0.163 23.972 Permitted C. P. L. R.**** 36 1 34 1338 X 267 15 X 374 89 2498 t it 1 st/2nd Cr Permit PAN Limiop P 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance wim a system aesignea to assure tuat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including t e possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Applier, _ _ _ _ - _ Mineralization Rates: Compost-0.1, anaerobially digested -0.2, Signature of.Land Date - - -_- -- _ aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.. Cumulative Pollutant Loading Rate --K1- r^-RA r fAn1nnnn% ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 38.27 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Leland Wolfe Owner: Same Predominant Soil Series: GsB-Golston Acres Used: 13.4 Acres Permitted: r 13.4 Site #: NC-UN27 Field #: 1 Residual Analvsis Data (Heavv Metals and Total Phosphorus use me/ka, % Solids use Raw Percent #): . .0 posite Date © © a © >0 f7 013 m � ,• . .. 11 .III Anni'inl Henw Metal Field Landin rs (Calculated in Ins/acre]: `=Total .- 1 2 3 4` 9 6 7 B 9 10 11 12 ; y 1JAc./ o y iEvent 2.86 Arsenic 0.000 0.000 1 0.000 0.000 0.095 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1, 0.095 Cadmium 0.000 0.000 0.000 0.000 0.010 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ; 0.010 Copper 0.000 0.000 0.000 0.000 2.827 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.827 Chrbroium 0.000 0.000 0.000 0.000 0.954 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.954 CLead 0.000 0.000 0.000 0.000 0.067 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.067 :1Vlercu y 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.000 0.000 0.000 0.000 0.211 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.211 denum `4,4,1ckel 0.000 0.000 0.000 0.000 0.261 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.261 Selenidm 0.000 0.000 0.000 0.000 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.029 l,zinc' 0.000 0.000 0.000 0.000 3.433 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.433 Sr?aotal Pl}os- 0.000 0.000 0.000 0.000 63.403 0.000 0.000 0.000 0.000 0.000 0.000 0.000 63.403 oborus ji" Ivertiiy, under penalty of law, that tors aocumentwas prepareu unuer iuy ulreAuUu yr suycrVs.Uu,n actinuai,co with,a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1r• :�. '; LqT, aware that there are significant penalties for submitting false information, including the possibility of fines and ri%prisonment for knowing violations". A` P"8",1', y ! S jnh6re of Land Applier Date }} - DENR FORM MFLSF (12/2006) , -- ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 2 Acres Utilized: 17 Land Owner: Leland Wolfe Annual Dry Tons Applied: 60.5624 Site #: NC-UN27 Acres Permitted: 17.0 Operator: Same Predominant Soil Series: GsB-Golston Cation Exchange Capacity (non 503): NIA d',.,,., , W.,...o. !Pact 1 1 rnn t Max_ PAN: 135 Crop 2 Name: Fescue (Past.) Crop 2 Max: PAN: 50 1 Volume applied Volume Residual Sources Soil - Precip. C o z Y • 5 Nitrate PAN Applied Name of Crop Type o (enter one) Solids/ % Applied per (NPDES #, WQ#, Cond. Past 24 n b w n TKN o as o and (lbs/acre) Receiving Residual o Liquid Solids Acre Fert., Animal (Dry, Hrs. � o' o * R CD * n Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet' Moist) inches * 0 o mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop I Crop 2 June 18 356 20.2 3.562 WWTPC D 0 S 0.5 0.3 28,200 6,240 12.6 69.259 NA Fescue 0.000 0.000 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ................... Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 356 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 69.259 0.000 Lime A lied Annuallbs/acre 0.118 0.013 3.526 1.190 0.084 0.003 0.264 0.326 0.036 4.282 79.076 :::::::::::::::::::::::::::;::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.388 0.092 11.358 3.63 0.898 0.0.15 0.862 1.313 0.163 24.465 =: Current Cumulative lbs/ac 0.506 0.105 14.884 4.820 0.982 0.018 1.126 1.639 0.199 28.747 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 ,Permit PAN Limit 1 sd2n d Crop 135 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accornance wim a system uesigneu w assure L1121l qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S -Surface, IN -Injection, INC -Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier_ _ = Date aerobically digested -0.3, raw sludge -0.4 _. _-___- ==-3_ ****C.P.L.R.: Cumulative Pollutant Loading Rate nGnin Gnaen GeG /4')/9nna% ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 60.55 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Leland Wolfe Owner: Same Predominant Soil Series: Gsl3-Go}ston Acres Used: 17 Acres Permitted: 17 Site #: NC-UN27 Field #: 2 Residual Analvsis Data (Heave Metals and Total Phosphorus use m0kLy. % Solids use Raw Percent ft N.Tp M Com- posite Date no Annual Heavy 1Vletal k1eld Loadings (Ualculated in Ws/acre): !I', Total 1 2 3 4 5 6 7 8 9 10 11 12 s '.D,T Ac./ o (App.Event R. 3.56 Arsenic 0.000 0.000 0.000 0.000 0.000 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Cadmium 0.000 0.000 0.000 0.000 0.000 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.013 ,Copper 0.000 0.000 0.000 0.000 0.000 3.526 0.000 0.000 0.000 0.000. 0.000 0.000 3.526 Chrbmium 0.000 0.000 0.000 1 0.000 0.000 1.190 0.000 0.000 0.000 0.000 0.000 0.000 1.190 ('bead 0.000 0.000 0.000 0.000 0.000 1 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.084 ['Mercury 0.000 0.000 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.003 lylolyb- i, " 0.000 0.000 0.000 0.000 0.000 0.264 0.000 0.000 0.000 0.000 0.000 0.000.. 0.264 ,,denum Nickel 0.000 0.000 0.000 0.000 0.000 0.326 0.000 0.000 0.000 0.000 0.000 0.000-- 0.326 Selenium 0.000 0.000 0.000 0.000 0.000 0.036 0.000 0.000 0.000 0.000 0.000 0.000 0.036 12in'c 0.000 0.000 0.000 0.000 0.000 1 4.282 0.000 0.000 1 0.000 1 0.000 0.000 0.000 1, 4.282 }'hqs- 10.000 10.000 10.000 10.000 10.000 179.076 10.000 10.000 10.000 10.000 10.000 1 0.000 ' 179.076 'Tcertify, under penalty of law, that this document was prepared under my direction or supervision in accordance with'a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. ., , I Team }aware that there are significant penalties for submitting false information, including the possibility of fineis and imprisonment for knowing violations". 1 SiW .. ure of Land Applier Date �w•. DENR FORM MFLSF (12/2006) .., -- ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 24.5 Land Owner: William Griffin Annual Dry Tons Applied: 59.7118 Site #: NC-UN29 Acres Permitted: 24.5 Operator: Same Predominant Soil Series: GoC-Golston Cation Exchange Capacity (non 503): N/A r....., 1 Nama• r.Pcn11P. (Pact 1 Cron 1 Max. PAN: 116 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 o Y 4 Q May 18 Volume applied PP (enter one) Solids/ Li uid a Cu. Yds Gallons 351 % Solids 20.2 Volume Applied per Acre (Dry Tons/Ac) 2.437 Residual Sources (NPDES #, WQ#, Fert. Animal Waste, etc) WWTPC Soil Cond. (Dry' Wet, Moist) D Precip. Past 24 Hrs. inches 0 Y "o a .a o a o ° S o w r N' ,� 1 0.5 5 w * N' * R, 0 0.3 TKN mg/kg 28,200 Z Y � o CD g °' mg/kg 6,240 Nitrate and Nitrite mg/kg 1 12.6 PAN Applied (]bs/acre) Name of Crop Type Receiving Residual Application Crop 1 47.382 Crop 2 NA Crop 1 Fescue Crop 2 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS 351 01. ::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 47.382 0.000 Lime Applied Annuallbs/acre 0.066 0.007 1.961 0.662 0.047 0.002 0.147 0.181 0.020 2.381 43.978 :::::::::::::::::::::::::::::::::::: Date lbs/ac Prior Years Cumulative lbs/ac 0.279 0,045 6.325 2.271 0.507 0.006 0.515 0.706 0.084 11.198 ':::::::::::::::::.::::::::::::::::::::::::::;:: Current Cumulative lbs/ac 0.345 0.052 8.286 2.933 0.554. 0.008 0.662 0.887 0.104 13.579 Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 Permit PA N Limit is t/Znd Cro P 116 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designee to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Q *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate MCI,= none cor /40/OnnG\ ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0003146 Cation Exchange Capacity (non 503 only): Operator: William Griffin Owner: Same Predominant Soil Series: Acres Used: 24.5 Acres Permitted: 24.5 Site #: NC-UN29 Field #: 48.53 N/A GoC-Golston 1 Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/kg. % Solids use Raw Percent #): Com- posite Date Annual Heavv Metal Field Loadings (Calculated in lbs/acre): t Total Annual Heavv Metal Field Loadings (Calculated in lbs/acre): t Total 1 2 3 4 5 6 7 8 9 10 11 12 H ` T/Acd , APp• tEyent 1.98 Arsenic 0.000 0.000 0.000 0.000 0.000 0.066 0.000 0.000 0.000 0.000 0.000 0.0.00 ' 0.066 Cadmium 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.007 ,Copper 0.000 0.000 0.000 0.000 0.000 1.961 0.000 0.000 0.000 0.000 0.000 0.000 1.961 Chromium 0.000 0.000 0.000 0.000 0.000 0.662 0.000 0.000 0.000 0.000 0.000 0.000 ; 0.662 1;L,e4d 0.000 0.000 0.000 0.000 0.000 0.047 0.000 0.000 0.000 0.000 1 0.000 0.000 ; 0.047 Mercury 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 1 0.000 0.000 f 0.002 M61yb- 0.000 0.000 0.000 0.000 0.000 0.147 0.000 0.000 0.000 0.000 0.000 0.000 0.147 A d6num 'j,Mickel 1 0.000 0.000 0.000 0.000 0.000 0.181 0.000 0.000 0.000 0.000 0.000 0.000, 0.181 Selenium 0.000 0.000 0.000 0.000 0.000 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Kzinc 0.000 0.000 0.000 0.000 0.000 2.381 0.000 0.000 0.000 0.000 0.000 0.000 2.381 c;t,Total - Phos- 0.000 0.000 0.000 0.000 0.000 43.978 0.000 0.000 0.000 0.000 0.000 0.000 43.97$ I ' _ ,hbrus "I'�certify, under penalty of law, that this aocument was prepares unaer my airecuon or supervision in accoraance I� I '+ 1 �Iwith?a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Lam, aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sis .:ignature of Land Applier Date DENR FORM MFLSF (12%2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 3 Acres Utilized. /A Land Owner: William Grim Annual Dry Tons Applied: 35.0597 Site #: NC-UN29 Acres Permitted: 7.4' Operator: Same Predominant Soil Series: BaB-Badin Cation Exchange Capacity (non 503): NIA rrnn 1 Nnmee Fescue (Past_) Cron 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 O °; o 18 Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (DryTons/Ac) Residual Sources (NpDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Precip. Past 24 Hrs. inches a v C " o w n g o °i * N' * °= � 5 w * N' * 7 TKN mglkg z a a o " mg/kg Nitrate and Nitrite mglkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop l Crop 2 Apr 18 145 20.2 3.333 WWTPC D 0 S 0.5 1 0.3 28,200 1 6,240 12.6 64.806 NA Fescue Apr 18 50 24.68 1.404 WTPC D 0 S 0.5 0.4 12,200 2270 17.3 14.393 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 1951 0 :::::::::::::: As Cd Cu Cr Pb Hg Mo Ni Se Zn P 79.198 0.000 Lime Applied Annuallbs/acre 0.167 0.020 4.701 1.644 0.101 0.004 0.366 0.411 0.047 5.101 91.964 ::::::::::::::::::::::::::::::::::: :::: >:*.* Date lbs/ac Prior Years Cumulative lbs/ac 0.448 0.081 11,671 4.502 0.787 0.015 1.021 1.324 0.692 18.109 ::::::?:`:?;::::::::::? Current Cumulative lbs/ac 0.615 0.101 16.372 6.146 0.888 0.019 1.387 1.735 0.739 23.210 Permitted C. P. L. R.**** 36 1 34 1338 X 267 15 X 374 89 2498 Permt tPAN Limit is t/2nd Crop 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accoraance witn a sysrem aesignea to assure [nai qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN -Injection, INC -Incorporation Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate nGnia cnann Ccr ia1)ronnaN ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): 35.05 Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: William Griffin Owner: Same Predominant Soil Series: BaB-Badin Acres Used: 7.4 Acres Permitted: 7.4 Site #: NC-UN29 Field #: 3 Residual Analvsis Data (Heavy Metals and Total Phosphorus use m0ke. % Solids use Raw Percent #): . . Com- posite Date i1 © © © MH d Em non Annual Heavv Metal Field Loadings (Ualculated in lbs/acrel: otal 1 2 3 4 5 6 7 8 9 10 11 12 ! c - DT/Ac./ (A pp. y ;Event 3.33 1.40 " Arsenic 0.000 0.000 0.000 0.000 0.111 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.167 Cadmium 0.000 . 0.000 0.000 0.000 0.012 0.008 0.000 0.000 0.000 0.000 0.000 j 0.000 0.020 Copper 0.000 0.000 0.000 0.000 3.300 1.401 0.000 0.000 0.000 0.000 0.000 0.000 4.701 Chr'.offi'iurn 0.000 0.000 0.000 0.000 1.113 0.531 0.000 0.000 0.000 0.000 0.000 0.000 1.644 Ctpad 0.000 0.000 0.000 0.000 0.079 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.101 :Mercury 0.006 0.000 0.000 0.000 0.003 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- -denum 0.600 0.000 0.000 0.000 0.247 0.120 0.000 0.000 0.000 0.000 0.000 0..000 0.366 �N;ickel 0.000 0.000 0.000 0.000 0.305 0.106 0.000 0.000 0.000 0.000 0.000 0.000 0.411 Selenium 0.000 0.000, 0.000 0.000 0.033 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.047 N, 4inc 1 0.000 0,000 0.000 0.000 4.006 1.095 0.000 0.000 0.000 0.000 0.000 0.000 5.101 �ii Total Plios- 0.000 0.000 0.000 0.000 73.993 17.971 0.000 0.000 0.000 0.000 0.000 0.000 91.964 ;horus i "I icertify, under penalty of law, that this document was prepared under my direction or supervision in accordance .,with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 'AmAiiaware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ;Signature of Land Applier Date DENR FORM MFLSF (12/2006) ,;' _ = = ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field M 4 Acres Utilized: 7_2 Land Owner: William Griffin Annual Dry Tons Applied: 21.7752 Site #: NC-UN29 Acres Permitted: 7.2 Operator: Same Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): NIA rrnn 1 Name: Fescue (Past.) Croo 1 Max. PAN: 122 Crop 2 Name:. Fescue (Past.) Crop 2 Max. PAN: 50 5 A Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, W #, Q Fert., Animal Waste, etc) Soil Cond. D W Moist) Preci . P Past 24 Hrs. inches a s oa o = o a °: n * $ 5 w =° �; * *.. ? TKN mg/kg Z Y R o o o �; mglkg Nitrate and Nitrite mglkg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 Apr 18 78 20.20 1.843 WWTPC D 0 S 0.5 0.3 28,200 1 6,240 12.6 35.829 NA Fescue May 18 50 20.2 1.181 WWTPC D 0 S 0.5 0.3 28200 6,240 12.6 22.967 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 128 0:::::::::::::: As Cd Cu Cr Pb I Hg Mo Ni Se Zn I P 58.797 1 0.000 Lime Applied Annuallbs/acre 0.100 0.011 2.994 1.010 0.071 0.002 0.224 0.276 0.030 3.635 67.133 :: :: Date lbs/ac Prior Years Cumulative lbs/ac 0.301 0.05 8.058 2.932 0.571 0.01 0.667 0.961 0.111 14.257 Current Cumulative Ibs/ac 0.401 0.061 11.052 3.942 0.642 0.012 0.891 1.237 0.141 17.892 .: Permitted C. P. L. R.**** 36 34 1338 X 267 15 X 374 89 2498 ,Permit PAN Limit 1st/ 2nd Cro P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land A lien Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, _ aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate riCP1113 CrNORA CQC /AO/Or\nC\ ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (Annual): Permit #: WQ0001346 Cation Exchange Capacity (non 503 only): Operator: William Griffin Owner: Same Predominant Soil Series: Acres Used: 7.2 Acres Permitted: 7.2 Site #: NC-UN29 Field #: 21.77 N/A BdB2-13ad,in 4 Residual Analvsis Data (Heavv Metals and Total Phosphorus use mg/ka. % Solids use Raw Percent ft ..-.a (om- posite Date © © © o no • . 11 Annual Heavv Metal Field Loadings (Ualculated in lbs/acre): Y` 'Total 1 2 3 4 5 6 7 8 9 10 11 12 rApp- �Evept 3.02 Arsenic 0.000 0.000 0.000 0.000 0.000 0.100 0.000 0.000 0.000 0.000 0.000 0.000 0.100 Cadmium 0.000 0.000 0.000 0.000 0.000 0.011 0.000 0.000 0.000 0.000 0.000 0.000] 0.011 .06pper 0.000 0.000 0.000 0.000 0.000 2.994 0.000 0.000 0.000 0.000 0.000 0.000 2.994 Philpmium 0.000 0.000 0.000 0.000 0.000 1.010 0.000 0.000 0.000 0.000 0.000 0.000 ' 1.010 t:;Lead 0.000 0.000 0.000 0.000 0.000 0.071 0.000 0.000 0:000 0.000 0.000 0.000' 0.071 :Mercury 0.000 0.000 0.000 0.000 0.000 0.002 0.000 0.000 0.000 0.000 1 0.000 0.000 0.002 1klolyb- 0.000 0.000 0.000 0.000 0.000 0.224 0.000 0.000 0.000 0.000 0.000 0.000.. 0.224 denum "(ckel 0.000 0.000 0.000 0.000 0.000 0.276 0.000' 0.000 0.000 0.000 0.000 0.000! 0.276 S,q'1enium 0.000 0.000 0.000 0.000 0.000 0.030 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.030 �7,,inc 0.000 0.000 0.000 0.000 0.000 3.635 0.000 0.000 0.000 0.000 0.000 0.000 3.635 Total Phbs- 0.000 0.000 0.000 0.000 0.000 67.133 0.000 0.000 0.000 0.000 0.000 0.000 67.133 `liorus WTI -.,�ertify, under penalty of law, that this document was prepared under my direction or supervision in accordance ,iih ,a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. h ;;*,aware that there are significant penalties for submitting false information, including the possibility of fines and A imOrisonment for knowing violations". { Al/z- ti Signature of Land Applier Date DENR FORM MFLSF (12/2006) , ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Monroe WQ Permit #: WQ0001346 Field #: 1 Acres Utilized: 13.1 Land Owner: Tom Appenzeller Annual Dry Tons Applied: 55.2887 Site #: UN-UN30 Acres Permitted: 13.1 Operator: William Griffin Predominant Soil Series: BdB2-Badin Cation Exchange Capacity (non 503): N/A Crop 1 Name: Fescue (Past.) Crop 1 Max. PAN: 122 Crop 2 Name: Fescue (Past.) Crop 2 Max. PAN: 50 S- c + O Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' Wet, t) Precip. Past 24 Hrs. inches > 'b a 'E o a ¢ c � � * � � � F w TKN mg/kg z Y 5 o � ac O Z. mglkg Nitrate and Nitrite mgtkg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 May 18 325 20.2 4.221 WWTPC D 0 S 0.5 0.3 28,200 6,240 12.6 82.052 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ................... TOTALS: 325 0 :::::::::::::: As Cd Cu Cr Pb H Mo Ni Se Zn P 82.052 0.000 Lime A lied Annuallbs/acre 0.140 0.424 0.564 36 0.015 0.07 0.085 34 4.179 11.262 15.441 1338 1.410 3.98 5.390 X 0.100 0.934 1.034 267 0.003 0.016 0.019 15 0.312 0.906 1.218 X 0.386 1.402 1.788 374 0.042 0.155 0.197 89 5.074 24.476 29.550 2498 93.706:::::::::::::::::::::::::::::::::::: .................. ........................... Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** PA Limit lst/2nd Crop Permit N P 122 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated -the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 _ Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate M=KIO =^MRA CoC 141)111nne% ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Monroe Total Dry Tons Applied (.Annual): 55.30 Permit #i WQ0001346 Cation Exchange Capacity (non 503 only): N/A Operator: Tom Appenzeller Owner: William Griffin Predominant Soil Series: BdB2-Badin Acres Used: 13.1 Acres Permitted: 13.1 Site #: NC-UN30 Field #: 1 Residual Analvsis Data (Heavy Metals and Total Phosphorus use mgALF. % Solids use Raw Percent #): Com- positeMR7NOW Date MEMEMEM13 a NEWMEN NONE Eff Annual Heavy Metal Field Loadings (Calculated in lbs/acre): ' btTotal 1 2 j 3 4 5 6j 71 8 91 10 11 1 12 3DT/Ac./ o pp, 1Event 4.22 Arsenic 0.000 0.000 0.000 0.000 0.000 0.140 0.000 0.000 0.000 0.000 0.000 0.000 0.140 r,aHminm 1 n nnn n nnn n nnn n nnn 1 n nnn n 015 n.nnn n-nnn 0-000 0.000 1 0.000 0-000 0.015 Copper 0.000 0.000 0.000 0.000 0.000 4.179 0.000 0.000 0.000 0.000 0.000 0.000 4.179 Clu-;omi 0.000 0.000 0.000 0.000 0.000 1.410 0.000 0.000 0.000 0.000 0.000 0.000 1.410 C:L'ead 0.000 0.000 1 0.000 0.000 0.000 1 0.100 u.uuu u.uuu I u.uuu u.uuu I u.uuu u.uuu U.1UU '.'.Mercury 0.000 0.000 1 0.000 0.000 0.000 0.003 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.003 Mplyb- denu,,. m 0.000 0.000 0.000 0.000 0.000 0.312 0.000 0.000 0.000 0.000 0.000 0.000 .., 0.312 'rNMekel 0.000 0.000 0.000 0.000 0.000 0.386 0.000 0.000 0.000 0.000 0.000 0.000 0.386 Selenium 0.000 F 6.000 0.000 0.000 0.000 0.042 0.000 0.000 0.000 0.000 0.000 0.000 11 0.042 ;'�tiinc 0.000 1 0.000 0.000 0.000 0.000 5.074 0.000 0.000 0.000 1 0.000 0.000 0.000 5.074 I'Moir - 10.000 10.000 10.000 10.000 10.000 193.706 10.000 10.000. 10.000 ,I 0.000 10.000 10.000 193.706 "'I�,certify, under penalty of law, that this document was prepared under my direction or supervision in accordance 'with,a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. laim,aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". gnature of Land Applier Date �, �'1 DENR FORM MFLSF (12/26,06)' .f r 'I Volatile Solids Reduction 2018 Van Kleek equation In (RAS) - Out (digested sludge) _ In (RAS) - (In * Out) (digested sludge) _ 1st 90 days RAS digested sludge IN- OUT 0.7567 0.5328 0.2239 IN- (IN -OUT) 63.33% 0.7567 0.40317 0.35353 2nd 90 days IN - OUT 0.6666 0.4831 0.1835 lReduction IN- (IN -OUT) 53.26% 0.6666 0.322034 0.344566 3rd 90 days IN - OUT 0.6800 0.5154 0.1646 Reduction IN- (IN -OUT) 49.95% 0.68 0.350472 0.329528 4th 90 days IN- OUT 0.6810 0.4510 0.23 lReduction IN- (IN -OUT) 1 61.520/6 0.681 0.307131 0.373869 0 PROMPT•A CCURATE •RELIABLE LABORATORIES) INC WWWPARLABS.COM REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: MAR 18 PO BOX 69 DATE: 04/05/18 MONROE, NC 28111- SAMPLE NUMBER- 130984 SAMPLE ID- MONROE WWTP SAMPLE MATRIX- SO DATE SAMPLED- 03/13/18 DATE RECEIVED- 03/13/18 SAMPLER- SH RECEIVED BY- DJ TIME RECEIVED- 1403 DELIVERED BY- SH TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 03/13/18 1500 RE 14,903 MPN/g i LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 m,e r"e:, PA CCURATE• RELIABLE LL�EOI2ATORIES� INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 • CITY OF MONROE MONROE WWTP • 03/13/18 FECAL COLIFORM, GEOMETRIC MEAN m SM 9221 E 1 3,599 16.82% 21,391.37 130984 2 1,519 16.03% 9,472.60 3 2,913 16.07% 18,131.89 4 1,317 16.45% 8,001.01 5 3,259 16.12% 20,217.50 6 2,695 15.70% 1 17,162.40 7 2,739 17.11 % 1 16,007.13 ,` FecalGollform Geomeinq'-Mean- CHAIN Ore CUSTOD Y �LASORA .rrrc. . PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 www.parfabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlo—ue, NC 28273 Charlotte, NC 28241-1483 is essen;ial ;hat all in;ormaaon be recorded cn ;his Chain o` Custody document for acceptance by PAR Laboratories. Inc. and the North Carolina Deoar,rnant o7 Environmental and Nacurai Resources_ Company Name (billing) Comments/ Special Instructions City oA Monroe Address PO Box 6Q 503 BZOSOLIDS Cry. Statc &zip coda Monroe" NC 28111 REPORTING Point of Contact & i ckphone-c___' Steve Holden ( 704) 282-4679 sholden@monroenc.ori a Sample Taken By: 5ill-)1 4CAd P-,13 IS THIS FOR STATE or EPA REPORTING? YES.—X—NO *Sample type: DW WW GWMW _ HW _ Soil _ other Sample Temp at time of sampling'./3 4!�°C Sample Temp upon receipt: -C Preserved: Yes No .X Teflon Liner/ Zero Headspace: Yes _ No N/A X Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested n I WWTP X NONE 3_ FECAL COLIFORM Y 2 WWTP X NONE 3, FECAL COLIFORM # 3 wxrrP X NONE 3- I g FECAL COLIFORM r 4 WWTP, - x NONE - i 3, 1 FECAL COLIFORM K 5 V✓WTP X NONE 3_ I g, FECAL COLIFORM 6 WWTP X NONE _ 13_ 1 g. FECAL COLIFORM 7 WWTP X NONE 3_ 3 _ t� FECAL COLIFORM Reli^qu' d by: Date/Time Rece'iv d by: Date/Time �i3 � �•d ,�-��-r �I/you relinquished by: Daterime Received by: Date/Tme C=Corinoosite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HIV=Hazardous Waste See Cther Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake Monitoring Period: From 1/1/2018 To WQ Permit Number: NPDES Number: 3/31/2018 WQ0001346 NCO024333 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ElProcess to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta B a Ra ❑ Y Gamma Ray ❑ Y Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion R1 Anaerobic Digestion ❑ If a plicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge in Pathogen Density Number ot Eencescee- Frequency of Analysis Sample Type Analytical Tech - MinimumGeo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8,001.01 14,903 21,391.37 MPN/g 0 quarterly grab sm922le CFU 1000 mpn per gram of total solid (dry weight) " Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) kV ectnr Attractinn Reduction (15A NUAl ULT .11U/ 1 - rlease lnuicaie alternative UerIormeQ: Alt.l (VS reduction) p Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake); ❑I Ali. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Ali. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed :' ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106' and the ' 4 vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .110,6 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." '(Plea's:e;note . if you check this statement attach an explanation why you have not met one or both of the f. requirements.) "This determination has been made under my direction and supervision in accordance with the system i designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." f Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type .or print) i Signature of Preparer* Date Signature of Land Applier (if applicable) Date. *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) ; DENR FORM PVRF 02T (12/2006) f• ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)"���" Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 1/1/2018 To 3/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alterative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ElAlternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray Y Gamma Ray Pasteur7zaf Class B: Alternative 1 R1 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Composting ❑ jAerobic, Digestion 21 El Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Sample Type Analytical Tech - Waue MinimumGeo. Mean MaximumUnitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 8,001.01 14,903 21,391.37 MGN/g 0 quarterly grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) 11yector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Mt.l (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. 02 uptake) : ' ❑ Aft. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Aft. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ' 0. ;CERTIFICATION STATEMENT (please check the appropriate statement) t] "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector' attraction reduction requirement in 40 CFR 503.33.have not been met." (Please note if you check'- this statement attach an explanation why you have not met one'for both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system ;designed to ensure that qualified personnel properly gather and evaluate the information used to determm that the pathogen and vector attraction reduction requirements have been met. I am aware that there are ;significant penalties for false certification including fine and imprisonment." jKyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator ! Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date 4 ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006),,,. P R C1 M RT- A, c c U R ATE• R E I- I A B LE I.AB013A`I"0RIES, INC WWNV.PARLABS.001N1 REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE, WASTEWATERPLANT PROJECT NAME: JUN 18 PO BOX 69 DATE: 06/22/18 j�j]j MONROE, NC 28111- SAMPLE NUMBER- 132015 SAMPLE ID- MONROE WWTP DATE SAMPLED- 06/18/'18 DATE RECEIVED- 06/18/18 SAMPLER- SH TIME RECEIVED- 0935 DELIVERED BY- SH Page I of 1 A fill SAMPLE MATRIX- WW TIME SAMPLED- 0825 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 06/18/18 1600 RE 17,006 MPN/g LABORATORY DIRECTOR c; init: P.O. Box 411483 - Charlotte, NC 28241-1483 Phone: (704) 588-8333 - Fax: (704) 588-8335 PA OOU RATE- RELIABLE LA.BOR..PiTORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 C, IENT� NA E� �" • - • SA`MPL'��ID^� ' ° ALl(sSlS • ' • e 4 1 a7. A�ALYSIS METFivO.D` • 132015 1 3,324 19.12% 17,389.06 2 3,303 18.47% 17,880.14 3 3,258 19.13% 17,027.80 4 2,891 19.44% 14,872.05 5 3,293 18.81 % 17,508.76 6 3,342 19.00% 17,587.70 7 3,175 18.71 % 16,963.58 t ar �e�c�l��oliform 11• CHAIN OF CUS TOD Y LASORaroRZS,INC. PAR Laboratories, Inc k Phone (704) 588-8333 Fax (704) 588-8335 yr w.parfabs.com Shippinc: Mailing: 2217 Graham Park Drive PO Box 411483 Charlo te, NC 28273 Charlotte, NC 28241-1483 it is essen;lal that ail intormaion be recorded on this Chain of Custody docurnent for acceptance by FAR Laboratories. Inc, and the NorTh Carolina Oeoartrnunt o7 Environmental and Natural Resources. - Ccnpany Name Ibillingl F Comments/ Special Instructions City o1 Monroe Address PO Box 69 503 B10SOLIDS City. Stale a Zip coda Monroe. NT 28I l I REP ORTNG Point of Contact a i cicphone"____""— - '- - - Steve Holden ( 704) 252-4679 sllolden@,ronrocne.ort), , Sample Taken By: s'�£ �'�y �() IS THIS FOR STATE or EPA REPORTING? YES NO ;Sample type_ DW __ WW Y GWMW _ HW _ Soil _ other Sample Temp at time of sampfrng3Z.ii IC Sample Temp upon receipt:°�C,r Preserved: Yes ^ No XTeflon Liner/ Zero Headspace: Yes No NIA .cam Client Sample I.D. (Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection I Date / Time Analyes Requested # 1 W' x NONE _ ,2 FECAL COLIFORM 2 WWTP X NONE - 9 � 1 25' FECAL COLIFORM r 3 WWTP X NONE - 2 S FECAL COLIFORM Y 4 WWIP - X NONE ��- I �s FECAL COLIFORM ! # 5 WWTp NONE le-1�' I� p D :2- FECAL COLIFORM P- 6 WWTP X NONE � L� FECAL COLIFORM wWTP X NONE 1 —� g: 2S FECAL COLIFORM i I r by: . w A 0 Date/rime Received UVA DatefFime by: by: �/ Date/Tirne C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well H'V=Hazardous Waste See 0-her Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: WWTP cake NPDES Number: NCO024333 Monitoring Period: From 4/l/2018 To 6/30/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Derformed: Class A: Alt. A (time/temp) ❑ Alt B-(Alk Treatment) [3 Alt. C (Prior Testing)❑.......... A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta RaY ❑ Gamma Ra ❑ Pasteurization ElY Class B: jAlt. (1) Fecal Density 21 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 0 Anaerobic Di estion g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number of Excee- denc Frequency of Analysis Y Sample Type a ytica Tech - njoue Minimum Geo. Mean Maximu Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 14,872.05 17,006 17,880.14 MPN/g 0 quarterly grab SM9221E CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) J Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Rl I Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ jAlt. 4 (Spec. 02 uptake) 0 Alt. 5 (14-Day Aerobic) ❑ JAR. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑; i CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the I j vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." I'❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the A vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please.note , if you check this statement attach an explanation why you have not met one or both of the requirements.) 'This determination has been made under my direction and supervision in accordance with the system :designed to ensure that qualified personnel properly gather and evaluate the information used to determine, that the pathogen and vector attraction reduction requirements have been met. I am aware that there are' significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Treparer Name and Title (type or print) Land Applier Name and Tjtle (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T'(12/2006) 11 , ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 4/1/201 To 6/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Therrnophilic ❑ Beta RayGamma Ray ❑ Pasteurization ❑ ❑ Y Class B: Alternative 1 21 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying[] Composting ❑ jAerobic Digestion 0 Anaeroe bic Digestion g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Allowable Level Pathogen Density Number of Frequency Sample Analytical Parameter Excee- Tech - in Sludge Minimum Geo. Mean Maximurr Units dences of Analysis Type woue 2 x 10 to the MPN 14,872.05 17,006 17,880.14 MGN/g 0 quarterly grab sm9221e 6th power per gram of CFU Fecal Coliform total solids 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry colifonn) weight) ,!Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.I (VS reduction) R1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ JAR. 4 (Spec. 02 uptake) ❑ Alt. 5 (14-Day Aerobic). ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ JAIt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ j CERTIFICATION STATEMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector !; attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system 1 :g designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are E significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator .Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 6 Signature of Preparer* Date ignature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (12/2006) PJ� A, R PROM PT•ACOURATE• RELIABLE LABORATORIES, INC WWWPARLABS.CO4 REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PROJECT NAME: JUL 18 PO BOX 69 DATE: 08/16/18 MONROE, NC 28111- SAMPLE NUMBER- 132286 SAMPLE ID- MONROE WWTP DATE SAMPLED- 07/09/18 DATE RECEIVED- 07/09/18 SAMPLER- SH TIME RECEIVED- 1030 DELIVERED BY- SH Page 1 of 1 SAMPLE MATRIX- WW TIME SAMPLED- 0920 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 07/09/18 1545 RE 16,312 MPN/g LABORATORY DIRECTOR P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 PRO MPT•ACCLI RATE• RELIABLE LABtJR�.TORZES� ZNC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 (:LIE � �T�NAME. ° SAMPLE ,IDr S"AMPLE ;DATE: AN4LYSIS P SA Et'OD • - • IIIET • - • . • • . • • 132286 1 2,858 18.91 % 15,118.47 2 3,091 19.30% 16,013.78 3 3,145 18.77% 16,755.73 4 3,115 19.17% 16,250.73 5 3,372 19.08% 17,670.57 6 2,988 18.69% 15,989.18 7 3.109 18.84% 16.501.64 eca�Co ifo�r`m�; C� oeirc'Me�anM 17 A CHAIN OF CUSTODY tpso�+ro�rEs.rrvc. PAR Laboratories, Inc . Phone (704) 588-8233 Fax (704) 588-8335 www.partabs.com com Shipping: Mailing: 22 i 7 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241-1483 il is essential that ail information be recorded on this Chain of Custody document for acceptance by PAR Laboratories. Inc. and the North Carolina l7eparimeni of Envimnmm;al and Natural Resources. Conpany Name (billing) ' City o,i MorLroe Comments/ Special instructions Address PQ Box 69 503 BZOSOLIDS CRy. Statc &zip coda REPORTTIG I Monroe: NNC 28111 Point of Contact & Telephone._ —" '- -! Steve Holden (704) 282-4C79 ;holden@nionroenc.or Sample Taken By: StULpl�� iS THIS FOR STATE or EPA REPORTING? YES NO '*Sample type: DW WW T GWMW HW _ Soil _ other —• y� Sample Temp at time of samprtng:��°C_ Sample Temp upon receipt: . % °-C�CLr Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes No N/A c?. 0 Client Sample I.D. Sample Location / Number) Comp Grab Preserv. Set Up Date / Time Collection Date I Time Analyes Requested I WVVTP X NONE ^9-�S : Zv FECAL COLIFORM 2 WW TP X NONE 7_ �, ; Zv FECAL COLIFORM 3 W"WTP X NONE i _10 FECAL COLIFORM Y 4 WWTP' - X NONE ' Zv FECAL COLIFORM # 5 VVtiVTP X NONE 7' g_ �. r) FECAL COLIFORM iu 6 WWTP X NONE 7 FECAL COLIFORM r 7 wwrn X NONE 7 _ : Zc� FECAL COLIFORM deli^ fished by: DatefrimReceived by, atemme �-9 reP rJ"I�� relinquished by: Dater me Received by: 1� DateMme C=Composite G=Crab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well H%V=Hazardous Waste See 0-her Side 1 I ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WQ Permit Number: WQOOO1346 WWTP Name: WWTP cake NPDES Number: NCO024333 Monitoring Period: From 7/1/2018 To 9/30/2018 Pathoeen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nerformed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thelmophilic ❑ Beta Ray❑ Gamma Ra ❑ Y 'Pasteurization ❑ Class B: Alt. (1) Fecal Density p Alt. (2) Process to Significantly Reduce Pathogens ❑ ............ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion 21 Anaerobic obi Digestion LJIf applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Number o Excee- Frequency Sample na ytica Tech - Minim- Geo. Mean Maxim- Unitsdences in Sludge of Analysis Type nioue 2 x 10 to the 6th power MPN 15,118.47 16,312 17,670.57 MPNIg 0 quarterly Grab SM9221E per gram of Fecal Coliform total solids CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) ;jVector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:. j Alt.l (VS reduction) 0 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) JAIt. 4 (Spec. 02 uptake) 0 Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable)' ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed '❑ CERTIFICATION STATEMENT (please check the appropriate statement) & 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." } ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 'and' the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please lnote d {y if you check this statement attach an explanation why you have not met one or both of 'the i requirements.) " "This determination has been made under my direction and supervision in accordance with the system°' !designed to ensure that qualified personnel properly gather and evaluate the information used to'deter'inine- that the pathogen and vector attraction reduction requirements have been met. I am aware that there are jsignificant penalties for false certification including fine and imprisonment." i ;4 Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator +�'Preparer Name and Title (type or print) - Land Applier Name and Title (if applicable)(type for print) k ojg110.1111V Ul 11V1JCL1V1 "CM, Ljlr11(1I.U1V VL L"Llll x-vFrJ11V1 `ll Glr./r.l11VUVIVy • LG1LV 1 *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) ! l p DENR FORM PVRF 02T (12/2006) . ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: Prom 7/1/2018 To 9/30/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alterative 1 ❑ Alternative 2 ❑ Alterative 3 ❑ Alterative 4 ❑ - Alterative 5 ❑ Alternative 6 ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alterative 1 21 Alterative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens' Lime Stabilization ❑ Air Drying❑ Composting ❑ lAerobic, Digestion R1 Digestion . ......... ......Anaerobic ............... . If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Pathogen Density Number ot Excee- Frequency Sample Analytical - Tech - Minim Geo. Mean Maximu Unitsence. in in Sludge of Analysis Y is Type n 2 x 10 to the 6th power MPN 15,118.47 16,312 17,670.57 MGN/g 0 quarterly grab sm9221 e per gram of Fecal Coliform total solids CFU 1000 mpn per gram ,.X. of total solid (dry i'• •4 " Salmonella bacterial 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform) weight) ,Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.1 (VS reduction) R1 Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ - lAlt. 4 (Spec. OZ uptake) El i Aft. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Ungtable) ❑ "Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were perfor n' 'ed " ❑: +CERTIFICATION STATEMENT (please check the appropriate statement) " l R1 "I certify, under penalty ty of law, that the pathogen requirements in 40 CFR 503.32 and tlie`vector attraction reduction requirement in 40 CFR 503.33 have been met." 9 i ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check j� this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system; . !designed to ensure that qualified personnel properly gather and evaluate the information used to'determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are ;significant penalties for false certification including fine and imprisonment." ;Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or -print) Signature of Preparer* Date Signature of Land Applier (if applicable) " Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) I DENR FORM PVRF 503 (12/200,6).,i ;! PROMPT -ACC ORATE -RELIABLE LABORATORIES, INC WWNV.PARLABS.001-I REPORT OF ANALYSES Attn: STEVE HOLDEN CITY OF MONROE WASTEWATERPLANT PO BOX 69 MONROE, NC 28111- PROJECT NAME: OCT 18 DATE: 11/08/18 SAMPLE NUMBER- 133542 SAMPLE ID- MONROE WWTP DATE SAMPLED- 10/01/18 DATE RECEIVED- 10/01/18 SAMPLER- SH TIME RECEIVED- 1020 DELIVERED BY- SH i Page 1 of 1 SAMPLE MATRIX- WW TIME SAMPLED- 08b4 RECEIVED BY- DJ TYPE SAMPLE- Grab ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 10/01/18 1630 RE 11,597 MPN/g LABORATORY DIP.ECTOR i P.O. Box 411483 • Charlotte, NC 28241-1483 Phone: (704) 588-8333 • Fax: (704) 588-8335 AIM PROMPT•ACCURATE• RELIABLE LABORATORIES, INC 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 CLIENT' NAME:' - "� SAMPLE`tID' AMPLE DATE: NALYSIS A� A Y�S1 `�M SHOD: • • - • • • • I 1011.1 A, Ke• • 133542 1 1,896 17.45% 10,862.87 2 1,910 16.98% 11,245.99 3 2,125 17.30% 12,284.84 4 1,939 17.41 % 11,135.05 5 1,981 16.88% 11,733.85 6 2,078 17.16% 12,110.25 7 2.083 17.53% 11.882.35 Fca��Cifb`rm� o et Mean r CHAIN OF CUSTODY U;SORA70RrES,INC. PAR Laboratories, Inc €_illi�ait1 Phone (704) 588-8333 Fax (704) 588-8335 wvrw.parfabs.com 5hippirtc: rdlailing: 2217 Graham Park Drive PO Box 411483 Chario7ze, NC 28273 Charlotte, NC 28241-1483 it :s e;sen;ial that all information be recorded on ,his Chain of Custody document for acceptance by ) AR Laboratories. Inc. and the North Carolina Deoariment of Environmental and Naurai Resources. Conpan•; Name lbiring) Comments/ Special Instructions City of Monroe Address PO Box 69 503 BXOSOLIDS C ty. State Fk Zip coda Moog �c zgx REPORTING Point of Contact a Yeiephont Steve Holden ( 704) 282-4679 sholden@monroenc.on) Sample Taken By:V I IS THIS FOR STATE or EPA REPORTING? YE_S.., NO *Sample type: DW WW GWMW�J_ HW _ Soil _ other Sample Temp at time of sa�mrpfng A� d °C Sample Temp upon receipt_ Z� °C '* Preserved: Yes _ No X Teflon Liner/ Zero Headspace: Yes _ No N/A X Client Sample I.D. ( Sample Location ! Number) Comp Grab Preserv. Set Up Date / Time Collection Date / Time Analyes Requested I WW X NONE 8 S; S#( FECAL COLIFORM Y 2 WWTP x NONE D ¢ �,. S FECAL COLIFORM # 3 VPWTP x NONE o FECAL COLIFORM r 4 WWTP ' - X NONE 0 S FECAL COLIFORM # 5 VVWTP X NONE ,. FECAL COLIFORM 9 6 WWTP X NONE SS- FECAL COLIFORM R 7 w)WlP NONE FECAL COLIFORM Jelin is ed by:001 Date/Time Recei by: Date/Time relinquished by: Dateri ime Received by: - l DatefTime C=Composite G=Grab DW=Dinking Water WW=Wastewa,er GWMW=Groundwater Monitoring Well H%V=Hazardous Waste See Other Side ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Monroe WWTP Name: WWTP cake WQ Permit Number: W00001346 NPDES Number: NCO024333 Monitoring Period: From 10/1/2018 To 12/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ElAlt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ElPasteurization Y ❑ Class B: Alt. (1) Fecal Density❑ Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Cl Air Drying ❑ Composting ❑ Aerobic Digestion Rl Anae robrc Dr esti on Elg ...........................................................................,....:.............................,.......................... I ... If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample Type Analytical Tech - n iaue Minim Goo. Mean aximu Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 10,862.87 11,597 12,284.84 MGN/g 0 quarterly grab sm9221 e CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.l (VS reduction) RI Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ I Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were,per'formed ❑ 'CERTIFICATION STATEMENT (please check the appropriate statement) Iii 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106, grid the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." i' U "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and ,the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Plea§e note if you check this statement attach an explanation why you have not met one or both of the i reauirements.) "This determination has been made under my direction and supervision in accordance with the system �' � ,' 's' �t designed to ensure that qualified personnel properly gather and evaluate the information used to determine -that the pathogen and vector attraction reduction requirements have been met. I am aware that there are i� significant penalties for false certification including fine and imprisonment." Kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator 4,' Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type,or print) Signature of Preparer* Date Signature of and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) . 1 _ ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules) Facility Name: City of Monroe WQ Permit Number: WQ0001346 j WWTP Name: Monroe WWTP cake NPDES Number: NCO024333 Monitoring Period: From 10/1/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 4 ❑ Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ra Y ❑ Gamma Ray ❑ Y a teu ' t' P s rrza ron ❑ Class B: Alternative 1 21 Alternative 2 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion R1 Anaerobic Digestion ................................................ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- dences Frequency of Analysis Sample 'Type Analytical Tech - W oue Minimum Geo. Mean Maximu I Units Fecal Coliform h 2 x 10 to the 6th power per gram of total solids MPN 10,862.87 11,597 12,284.84 MGN/g 0 quarterly grab sm922le CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry I weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Alt.l (VS reduction) RI Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec- OZ uptake). ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ ! Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ ERTIFICATION STATEMENT (please check the appropriate statement) " 0 "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." i f ❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you 'check,, I this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine , ; that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." kyle Ketchum, WWTP Superintendent Steve Holden, Residual Coordinator 44Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) ;i Signature of Preparer* Date Signature of Land Applier (if applicable) ' "'Date ' *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 503 (121200"6)1 i SodILIm % Solids, Na, Na, Calcium Magnesium Date/ Sample decimal mg/I<g mg/I Na, meq/L Ca, mg/I<g Ca, mg/I Ca, meq/L Mg, mg/kg Mg, mg/I Mg, meq/L SAR 60.10 1220I 200.324L16.42 0.77 WWTP 3/20/2018 0.1642 669 109.851 4.78 7320 1201.94 f WWTP 6/11/2018 I 0.2021 610 123.221 5.36 7510 1517.02 75.85 1160 234.32 19.21 0.78 WWTP 7/9/2018 0.2072 599 124.111 5.40 102001 2113.44 105.67 1340 277.648 22.76 0.67 WWTP 10/1/2018 0.181 666 120.551 5.24 11300 2045.3 102.27 1500 271.5 22.25 0.66 0 0.00 0 0.00 0 0.00 #DIV/0! 0 0.00 0 0.00 0 0.001 ##DIV/0! WTP 3/20/2018 0.1799 544 97.866 4.26 1680 302.232 15.11 ! 490 88.151( 7.23 1.27 WTP 6/11/2018 0.2468 502 123.89 5.39 4770 1177.24 58.861 770 190.036 15.58 0.88 WTP 7/9/2018 0.2459 281 69.098 3.00 1800 442.62 22.13 318 78.1962 6.41 0.80 WTP 10/1/2018 0.268 479 128.37 5.58 4680 1254.24 62.71 635 170.18 13.95 0.90 0 0.00 0 0.001 I 0 0.001 #DIV/0! 0 0.00 0 0.00 0 0.00 #DIV/0! 0 0.00 0 0.00 0 0.00 #DIV/0! 0 0.00 0 0.00 0 0.00 #DIV/0! Soil pH & Lime Application Records For all fields where pH was reported below a pH of 6.0 in accordance with NCDA&CS, fields will be limed prior to any land application in the year 2018. Any field that was below a pH of 6.0 was limed prior to any residual application during the year 2018. Myers field UN18-8 and Griffin field UN29-2 was limed during 2018 but was not applied to. Lime applied to these fields was 9.42 tons. The City of Monroe applied 33.83 tons of lime during the year 2018. The fields that had lime applied are recorded on the field sheets. Page 1 of 1 Report No: 19-029-0554 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Way oi n- ANALYTICAL Client: -Calvin Moms 554 Hasty Road Peachland NC 28133 7621 Whitepine Road, Richmond, VA 23237--- Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.corri - - Farm: ANA 9 Date Received: 01/29/2019 Date of Report: 01/31/2019 Lab No Field ID Sample ID Soil Class IiM% W/V pN Ac P-1 K-1 S-1 Mn_1 Zn-I Zn-Al Cu-1 CEC BS% Ca% Mg% ESP Na SS-/ A103 N 06929 NC 19-1 M-0 6.8 0.4 184 89 46 219 548 684 300 13.1 97 66 27 0.7 0.1 9 Crop Recommendations: 1- Lawn Rec Uom Lime (t(acre) Ib/1000 sf 0.0 N 4.0 P205 K20 0 0 S 0 Mn 0.10 Mn-AI 136 Zn 0 Cu 0 B 0 Mg Last Crop 0 Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed -in accordance within NCDA guidelines ,Analysis• -prepared by:.Waypoint Analytical Virginia, -Inc_ __ Page 1 of 1 Report No: 19-029-0555 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 I : q paw i Client: Harry Myers 2225 Olive Branch Road Monroe NC 28110 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 1 Fax 804-271-6446 www.waypointanalytical.com— Farm: Date Received: 01/29/2019 Date of Report: 01/31/2019 Lab No Field 1D Sample 10 Soil Class HM% WN pH Ac p-1 K-1 S-1 Mn-1 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N 06930 18-1 MIN 6.8 0.4 408 29 54 181 515 515 545 13.6 97 77 19 1.2 0.2 17 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (tlacre) 0.0 N 4.0 P205 0 K20 2.0 S 0 Mn 0.10 Mn-Al 113 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06931 18-2 MIN 6.8 0.4 432 35 48 181 530 530 560 13.6 97 76 19 1.2 0.2 22 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (tlacre) 0.0 N 4.0 P205 0 K20 1.0 S 0 Mn 0.10 Mn Al 113 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06933 18-7 MIN 6.8 0.4 432 32 56 194 538 538 575 14.5 97 76 18 1.3 0.2 18 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (tlacre) 0.0 N 4.0 P205 K20 0 1.0 S 0 Mn 0.10 Mn-Al 121 Zn 0 Cu 0 B 0 Mg 0 Last Crop Comment: Test result units = CEC and Na in megl100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations,shown,on lhis..report are performed,in accordance within-NCDAguidelines, Analysis -prepared by:.Waypoint Analytical Virginia;:lnc.- -- Page 1 of 1 Report No: 19-029-0558 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Waypomt,..011'-4�' ANALYTICAL Client: Wayne McBride 3303 Trinity Church Road Monroe NC 28112 7621 Whitepine Road; Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical:com _ Farm: UN-25 _ _ Date Received: 01129/2019 Date of Report: 01/31/2019 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-1 Zn-I Zn-Al Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N 06938 NC 25-1 MIN 6.0 0.9 150 13 33 163 445 445 395 6.0 85 63 19 1.3 0.1 8 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (tlacre) 0.0 N 4.0 P205 K2O 0 3.0 S 0 Mn 0.10 Mn AI 115 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06939 NC 25-3 MIN 6.1 0.8 145 13 27 175 410 410 410 6.0 87 65 19 1.4 0.1 8 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Vacre) 0.0 N 4.0 P205 K20 0 3.0 S 0.20 Mn 0.10 Mn Al 120 Zn 0 Cu 0 B 0 Mg 0 Last Crop Comment: Test result units = CEC and Na in meq/100cm3; NO N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations_shovm on thisLrreport,are pertarmed-in accordance_within NCDA_guidelines; Analysis_prepare_d_by Waypoint Analytical Virginia; Inc-_= Page 1 of 1 Report No: 19-029-0560 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 0 7621 Whitepine Road, -Richmond, VA 23237 Waypotnt. Main 804-743=9401 ° Fax 804-271-6446 ANALYTICAL www.waypointanalytical:com Client: -Emmerson McBride Farm: UN-26- 7210 Rocky-River•Rd South Monroe NC 28112 Date Received: 01/29/2019 Date of Report: 01/31/2019 Lab No Field ID Sample ID Soil Class HM% WN pH Ac P-1 K-1 S-1 Mn-I Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NOSIV 06942 NC 26-1 MIN 6.1 1.0 113 17 37 200 400 400 475 7.5 87 63 20 2.6 0.2 9 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Macre) 0.0 N 4.0 P205 K20 0 3.0 S 0 Mn 0.10 Mn-AI 135 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06944 NC 26-2 MIN 6.3 0.9 97 20 48 194 385 385 475 8.9 90 64 23 2.1 0.2 11 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Macre) 0.0 N 4.0 P205 K20 0 2.0 S 0 Mn 0.10 Mn-AI 129 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06945 NC 26-3 MIN 6.4 0.8 94 27 40 163 408 408 520 9.4 92 64 26 0.9 0.1 10 Crop Recommendations: 1- Lawn 06946 NC 26-4A Rec Uom Ib/1000 sf MIN Lime (Macre) 0.0 6.1 N 4.0 1.1 P205 K20 0 2.0 85 47 S 0 37 Mn 0.10 131 Mn-Al 109 370 Zn 0 370 Cu 0 520 B 0 8.0 Mg 0 87 62 21 Last Crop 0.7 0.1 10 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Macre) 0.0 N 4.0 P205 K20 0 1.0 S 0 Mn 0.10 Mn-AI 94 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06947 NC 26-4B MIN 6.2 1.0 96 53 40 131 425 425 560 8.5 89 63 21 1.0 0.1 9 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Macre) 0.0 N 4.0 P205 K20 0 1.0 S 0 Mn 0.10 Mn AI 92 Zn 0 Cu 0 B 0 Mg 0 Last Crop 06948 NC 26-6 MIN 6.1 1.2 96 50 35 138 413 413 540 8.5 86, 62 21 0.8 0.1 10 Crop Recommendations: 1- Lawn Rec Uom Ib/1000 sf Lime (Macre) 0.0 N 4.0 P205 K20 0 1.0 S 0 Mn 0.10 Mn-AI 98 Zn 0 Cu 0 B 0 Mg 0 Last Crop Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendalionsst�ovrnytkthisr_portafe pertormed-in accordance q_thimNCDAguidelines Analysis pNpared-by:=WaypointAnalytical Virginiajnc� Page 1 of 1 Report No: 19-029-0559 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 Comment: Client: Leland Wolfe 1805 Jack Davis Road Monroe NC 28112 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 = - www:waypointanalytical.com Farm: UN-27 Date Received: 01/29/2019 Date of Report: 01/31/2019 Test result units = CEC and Na in meq/100cm3: NO N in mg/dm3: WN in g/cm3 = North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations.shown on this-report.are performed in accordance, within;NCDA.guidelines, Analysis prepared=by: =Waypoint Analytical Virginia,_Inc._ Page 1 of 1 Report No: 19-029-0556 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 ° waypolnto-,.� ANALYTICAL Client: William Griffin 6705 Austin Grove Church Road Marshville NC 28103 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 '-Fax 804-271-6446 www.waypointanalytical.com Farm: UN-29 Date Received: 01/29/2019 Date of Report: 01/31/2019 Lab No Field ID Sample 1D Soil Class HM% WN pH Ac P-1 K-1 S4 Mn-1 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N 06934 29-1 MIN 6.3 1.1 307 37 50 181 320 320 775 10.4 89 64 22 1.7 0.2 14 Crop Recommendations: Rec Uom Lime (Vacre) N P205 K20 S Mn Mn-AI Zn Cu B Mg Last Crop 1- Lawn Ib/1000 sf 0.0 4.0 0 1.0 0 0.10 121 0 0 0 0 06935 29-3 M-0 6.4 1.1 212 95 60 313 435 544 830 12.6 91 61 25 1.5 0.2 17 Crop Recommendations: Rec Uom Lime (Vacre) N P205 K20 S Mn Mn-Al Zn Cu B Mg Last Crop 1- Lawn Ib/1000 sf 0.0 4.0 0 0 0 0.10 199 0 0 0 0 06936 29-4 MIN 5.9 1.5 165 37 67 175 343 343 680 8.8 83 61 18 1.3 0.1 16 Crop Recommendations: Rec Uom Lime (Vacre) N P205 K20 S Mn Mn Al Zn Cu B Mg Last Crop 1- Lawn Ib/1000 sf 0.0 4.0 0 1.0 0 0.10 123 0 0 0 0 Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed -in accordance.within-NCDA guidelines;=Analysis-prepared by: Waypoint Analytical Virginia; Inca_ Page 1 of 1 Report No: 19-029-0557 Account No: 46205 Advisor: City of Monroe Steve Holden 775 Treeway Dr Monroe NC 28110 a,o Waypoint ANALYTICAL Client: Tom Appenzeller 830 Clover -Road Marshville NC 28103 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271=6446 = - vdww.waypointanalytical.com Farm: UN-30 Date Received: 01/29/2019 Date of Report: 01/31/2019 Lab No Field ID Sample ID Soil Class HM% W/V pH Ac P-1 K-1 S-1 Mn-1 Zn-1 Zn-Al Cu4 CEC BS% Ca% Mg% ESP Na SS-1 NO3 N 06937 NC 30-1 MIN 5.9 1.5 158 41 79 169 323 323 710 8.8 83 60 19 1.3 0.1 28 Crop Recommendations: Rec Uom Lime (Vacre) N P205 K2 S Mn Mn-AI Zn Cu B Mg Last Crop 1- Lawn Ib/1000 sf 0.0 4.0 0 1.0 0 0.10 120 0 0 0 0 Comment: Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; WN in g/cm3 = North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations -shown on this -report are performed in.accordance-within'NCDA-guidelines,:Analysis_prepared byc_WaypointAnalytical Virginia;Jnc__ _.--_