WQ0012346_Residual Annual Report 2018_20190228

RECEIVEDINCDEQIDWR
FEB 2 8 2019
CLASS "A" WASTEWATER REDscharge
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ANNUAL APPLICATION REPORT
UNITED STATES
MARINE CORPS BASE
CAMP LEJEUNE, N. C.
PERMIT NO. WQ0012346

2018
ANNUAL REPORT ON
DISTRIBUTION OF CLASS "A"
WASTEWATER RESIDUALS
MARINE CORPS BASE
CAMP LEJEUNE
PERMIT NO. WQ0012346

2018 ANNUAL REPORT ON
DISTRIBUTION OF CLASS A
WASTEWATER RESIDUALS
MARINE CORPS BASE, CAMP LEJEUNE
PERMIT NO. WQ0012346
• Cover Letter..................................................................... SECTION 1
• Class A Annual Distribution and Marketing/Surface Disposal SECTION 2
Certification and Summary Form (Form DMSDF)........................
• Annual Residuals Sampling Summary Forms
SECTION
(Forms RSSF & RSSF-B)...................................................... 3
• Residuals Analysis Lab Sheets ................................................ SECTION 4
• TCLP Lab Sheets............................................................... SECTION 5
• Annual Pathogen & Vector Attraction Reduction Forms SECTION 6
(Form PVRF 503)............................................................
• Pathogen & Vector Attraction Reduction Lab Sheets/Records........... SECTION 7

Application to Forested Sites
Camp Lejeune Advanced Wastewater Treatment Plant
ATAD Facility
Application to TLZ Training Areas
Transferring Biosolids from Tanker to Applicator

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UNITED STATES MARINE CORPS
MARINE CORPS INSTALLATIONS EAST -MARINE CORPS BASE
PSC BOX 20005
CAMP LEJEUNE NC 28542-0005
5090.20.1
G-F/BEMD
FEB 2 6 2019
Mr. Nathaniel Thornburg
North Carolina Department of
Environmental Quality
Division of Water Resources
Non -Discharge Permitting Branch
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Dear Mr. Thornburg:
In accordance with requirements of 40 CFR Part 503, the
enclosure forwards Marine Corps Base Camp Lejeune's (MCB CAMLEJ)
Class "A" Wastewater Residuals Annual Application Report for the
Year 2018. For your awareness, our CROM tank mixer and rail
system failed in July 2018 and two sludge samples were unable to
be collected for fecal analyses between 7/24/18 - 8/17/18. To
resume operation, the rail system and mixer had to be
refabricated and reinstalled, and the motors rewound.
Additionally, impacts from Hurricane Florence temporarily closed
our laboratory, and prevented sludge sample collection for fecal
analysis between 9/11/18 - 9/25/18.
If you have any questions please contact Mr. Travis Voorhees,
Environmental Quality Branch, Environmental Management Division,
G-F, at [phone].
Sincerely,
• rn .6 ���.-c
v John R. Townson
Director, Environmental Management
By direction of
the Commanding General
Enclosure: MCB CAMLEJ's Class "A" Wastewater Residuals
Annual Application Report Year 2018 (3 copies)

SECTION 2
Class A Distribution & Marketing/Surface
Disposal Certification & Summary Forms
(Form DMSDF)

Reporting Period: 2018
CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: W00012346 FACILITY NAME: Camp Lejeune AWWTP
PHONE: [phone] COUNTY: Onslow OPERATOR: Charles Scozzari
FACILITY TYPE (please check one): Z Surface Disposal (complete Part A (Source(s) and 'Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? 0 Yes ❑No ---► If No skip parts A, B, C and certifv form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)'
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
Camp Lejeune AWWTP NCO063029
7.79
February
Camp Lejeune AWWTP NCO063029
31.15
March
Camp Lejeune AWWTP NCO063029
41.07
April
Camp Lejeune AWWTP NCO063029
26.20
May
Camp Lejeune AWWTP NCO063029
60.19
June
Camp Lejeune AWWTP NCO063029
76.47
July
Camp Lejeune AWWTP NCO063029
8.50
August
Camp Lejeune AWWTP NCO063029
0.00
September
Camp Lejeune AWWTP NCO063029
7.08
October
Camp Lejeune AWWTP NCO063029
0.00
November
Camp Lejeune AWWTP NCO063029
0.00
December ICamp
Lejeune AWWTP NCO063029
5.66
Total from FORM DMSDF (sup)
0
0
0
0
Totals: I Annual (dry tons):
0
264.11
0
0
Amendment(s) used:
Bulking A ent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp) 0
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit
(including but not limited to items 1-3 below) issued by the Division of Water Resources: No 0 If No, Explain in Narrative
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Resources.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitti a esp"tion, including the possibility of fines and imprisonment fgp4av)tviyg�vio)jations."
-/, S Ei
Date
J (if differen�'from Permittee)
is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
D to

BIODYNAMIC VOLATILITY ENHANCEMENT LOG
WT-310CS SWEET CANE SYRUP
(SUGAR WATER)
3 Jan 2018, 137 gallons were added to Train 3 Reactor A and 137
gallons were added to Train 3 Reactor B
10 Jan 2018, 275 gallons were added to Train 1 Reactor A
10 Jan 2018, 275 gallons were added to Train 3 Reactor A and 137
gallons were added to Train 3 Reactor B
8 Feb 2018, 137 gallons were added to Train 1 Reactor A and 137
gallons were added to Train 1 Reactor B
1 Oct 2018, 137 gallons were added to Train 3 Reactor A and 137 `
gallons were added to Train 3 Reactor B
14 Nov 2018, 275 gallons were added to Train 1 Reactor B
14 Nov 2018, 275 gallons were added to Train 2 Reactor A
19 Nov 2018, 275 gallons were added to Train 2 Reactor A
19 Nov 2018, 137 gallons were added to Train 3 Reactor A and 137
gallons were added to Train 3 Reactor B
20 Nov 2018, 550 gallons were added to Train 3 Reactor A and 550
gallons were added to Train 3 Reactor B
28 Nov 2018, 275 gallons were added to Train 3 Reactor A and 275
gallons were added to Train 3 Reactor B
29 Nov 2018, 275 gallons were added to Train 2 Reactor A
30 Nov 2018, 275 gallons were added to Train 3 Reactor B

18 Dec 2018, 275 gallons were added to Train 1 Reactor B
19 Dec 2018, 137 gallons were added to Train 3 Reactor A and 137
gallons were added to Train 3 Reactor B

SECTION 3
Annual Residuals Sampling Summary Forms
(Forms RSSF & RSSF-B)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0012346
Facility Name: Camp Lejeune AWWTP
Residual Source WQ # or NCO063029
NPDES #:
WWTP Name: Camp Lejeune AWWTP
Residual Analvsis Data
Laboratory:
1)
2)
3)
4)
5)
EMD,ELS
Environmental Chemists
Parameter
(mg/kg)
Cone.
Limit
(m )a
Sample or Composite Date
1/23/18
4/10/18
7/3/18
12/4/18
Percent Solids (%)
NA
2.81
2.46
2.11
4.39
Arsenic
75
1
20.7
23.8
25
Cadmium
85
1
20.7
23.8
11
Copper
4,300
312
303
155
349
Chromium
NA
1
23.6
23.8
40.8
Lead
840
1
20.7
23.8
20.7
-Mercury
57
0.002
0.766
0.766
0.541
Molybdenum
75
20.4
20.7
23.8
13.5
Nickel
420
28.8
26.4
23.8
32.2
Selenium
100
20.4
20.7
23.8
11
Zinc
7,500
1230
1400
919
1530
Total Phosphorus
NA
63700.
59900
51000
3480
TKN
NA
74400
87600
85200
52400
Ammonia -Nitrogen
NA
42000
50500
50900
14300
Nitrate and Nitrite
NA
79.9
83.9
162
107
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualifliedjptersonnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submi�king alseation, including the possibility of fines and imprisonment for knowing violations."
Signature of eparer ate
*PreparerTs defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed.
WQ Permit Number: WQOO12346
Facility Name: Camp Lcjeune AWWTP
Residual Source NPDES # or WQ#:
W WTP Name:
Residual Analvsis Data
NCO063029
AW WTI'
Laboratory: 1) EMD,ELS
2) Environmental Chemists
3)
4)
5)
Sample or Com osite Dale
Parameter (mg/I:g)
1/23/18
4/10/18
7123/18
12/4/18
SAR
4.27
150
5.81
5.85
Aluminum
70400
81700
39100
70600
Calcium
5860054800
55300
39900
4910
Magnesium
51504140
4130
3220
3470
Potassium
59806140
6550
10000
3830
Sodium
3860
3690
4490
12200
H
7.99
7.74
8.22
7.8
Plant Avaiable Nitrogen
11899
36400
26598
18687
"I certify, under penalty of law, that this
penalties for submitting false informptior
e
Signature nt Pwp— *
*Preparer is defined in 40 CPR ' S03.9(r) and I:
was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that ther
the possibility of fines and imprisonment for (mowing violations."
LD -q
Daw
DENR FORM RSSF - B (12/2006)

f
SECTION 4
residuals Analysis Labs Teets
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Environmental Chemists, Inc.
1 i 1 1 6602 Windmill V%�ay, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highwav, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(4!,environrncntalchemists.com
LISMC Camp Lejeune Date of Report: Feb 16, 2018
G-F/EMD/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2018-01197
Project ID: Crom Tank
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-02960 Site: CROM Tank 1/23/2018 7:30 AM Solid/Sludge Black
Test Method Results Date An
SAR
Calculation
4.27
02/16/2018
Nitrate Nitrogen (calc)
Nitrite Nitrogen
EPA353.2
38.0mg/kg
01/25/2018
Nitrate Nitrogen
Subtraction Method
41.7 mg/kg
02/14/2018
Sludge Residuals
Aluminum
EPA 2003
70400 mg/kg
02/13/2018
Arsenic
EPA 200.7
<20.4 mg/kg
02/13/2018
Cadmium
EPA 200.7
<20.4 mg/kg
02/12/2018
Calcium
EPA 200.7
54800 mg/kg
02/14/2018
Chromium
EPA 200.7
25.8 mg/kg
02/12/2018
Copper
EPA 200.7
312 mg/kg
02/12/2018
Lead
EPA 200.7
<20.4 mg/kg
02/12/2018
Magnesium
EPA 200.7
4140mg/kg
02/14/2018
Molybdenum
EPA 200.7
<20.4 mg/kg
02/12/2018
Nickel
EPA 200.7
26.8 mg/kg
02/12/2018
Potassium
EPA 200.7
6140 mg/kg
02/14/2018
Selenium
EPA 200.7
<20.4 mg/kg
02/13/2018
Sodium
EPA 200.7
3860 mg/kg
02/14/2018
Zinc
EPA 200.7
1230 mg/kg
02/12/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
79.7 mg/kg
02/06/2018
Total Solids (%)
SM 2540 B
2.80 %
01/29/2018
Ammonia Nitrogen
SM 4500 NH3 C
42000 mg/kg
01126/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
74400 mg/kg
01/30/2018
Total Phosphorus
SM 4500 P F
63700 mg/kg
01/30/2018
Mercury
SW846 74718
<0.643 mg/kg
02/11/2018
Report 0, 2018-01197 Page t of 2

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910-347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Comment: Results reported on a dry weight basis.
Reviewed by: 1. lUTAl p( ,D, 0N0JV-'
info(i;environmentalchemists.com
Date of Report: Feb 16, 2018
Customer PO #:
Customer ID: 12060026
Report #: 2018-01197
Project ID: Crom Tank
Report #. 2018-01197 Paoe 2 of 2

6602 Windmill Way
ngton
ENVIRONMENTAL CHEMISTS, INC OFFICE 9103 2-02231FtAX910-3 2� 4
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Commanding General
PROJECT NAME: Camp Lejeune MCB
REPORT NO:�-
ADDRESS: G-F/EMD/EQB/Environmental Laboratory
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper
PHONEIFAX: 910-451-0020 (fax) 910-451-7195
Camp Lejeune NC 28547
1 COPY TO:
- patncia.raper usmc.mil, [e-mail],
email: [e-mail]; lauren.acosta usmc.mil
Sampled BY: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
c d
s a
rn
2
a a
i� o f
°
d
e 0
o
m
C
s V
"
Q mm
m
g
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
_
_
o
_
g
_
c
o
,Ua
8
CROM TANK
SLUDGE—C
P
yf
X
luminum, Arsenic, Cadmiuil
G
agnesium, Molybdenum,
G
G
C
P
ickel, Potassium, Sodium,
�elenium, Zinc,
G
G
C
P
Mercury Sludge, Nitrite,
G
G
C
P
KN, Total Solids/Soils &
G
G
C
P
Studge, AmNionta,
Phosphorus, Calcium, SAR
G
G:
C
P
G
G
C
P
G
G
C
P
G
G
C
P.
G
G
Transfer
Relinquished By:
Datefri a
Received By:
Datefrime
1.
0 6
6%.
% i J t 23 r
%- L k- 0740
Temperature when Received:
v
Delivered By: l,/ Received By: Date: 1-L' -M5 '
Comments: �� TURNAROUND:

Date:
Client:
Date Collected:
Date Received:
Sample:
Analyte
% Solids
pH
Marine Corps Base
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
3/8/2018
FC Wastewater
1/23/2018
1/23/2018
Quarterly Sludge
Date
Results Units Analyzed Tech Method
2.81 % 1/23/2018 AYO SM 2540 G
7.99 SU 1/23/2018 DRS/AYO 4500H+ B - 2000
D BY:
LAUREN D. ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
I�`
d
Signature:
Date Collected:
Z
Time Coilected:
0 7
Location of sample:
Truck Loading Station
Comp/Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH "'
Report all results as mog dry wt.
Was sample dechlorinated?
n/a
Preservation:
Ice
Regulatory Sample:
Yes
Field
Comments:
Relinquished by:
Date
Time
Received by:
Date
T,iime
`t
p
�, �C]
0

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: ( 23 t TIME: p730 BY: 4c
DATE:
ANALYZED BY:
I --/-� /;-otg
TIME: 07�-Q
METHOD: 4500H+ B - 2000
TIME
TIME
VOLUME
%
SAMPLE
TEMP
pH (SU)
COLLECTED
ANALYZED
mLs
RECOVERY
BUFFER 4.00
60
0
BUFFER 10.00
Q
60
t 0' OCR
CHECK SUFFER 7.00
����.
60
CROM TANK
0 D
V-7+0
100
2-I
-7A�
i "-Ra
CROM TANK DUP
3
1
100
191
1D'0 I
CHECK BUFFER 7.004
604
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

envirochem
ANALYTICAL & CONSULTING CHEMISTS
F -.-7q9
FW'F-6
Environmental Chemists, Inc,
6602 Windmill Way, Wilmington, NC 25405 . 910.3920223 Iab . 910.392.4424 Fax
710 Bowwrtown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910 347.5843 Lab/ Fax
irtfo a em imnmentalchemists.com
USMC Camp Lejeune
Date of Report: Apr 30, 2018
G-FlEMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2018-05563
Project ID: Crom Tank
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
18-13770 Site: CROM Tank
4/10/2018
7:38 AM Solid/Sludge Acosta Julius
Test
Method
Results Date Analyzed
PAN
Calculation
36400 mg/kg
04/30/2018
SAR
Calculation
150
04/30/2018
Sludge Residuals
Aluminum
EPA 200 7
81700 mg/kg
04/19/2018
Arsenic
EPA 200 7
<20.7 mg/kg
04/19/2018
Cadmium
EPA 2007
<20.7 mg/kg
04/19/2018
Calcium
EPA 200 7
55300 mg/kg
04/16/2018
Chromium
EPA 2007
23.6 mglkg
04/19/2018
Copper
EPA 200 7
303 mg/kg
04117/2018
Lead
EPA 200 7
<20.7 mg/kg
0411912018
Magnesium
EPA 200 7
4130 mg/kg
04/16/2018
Molybdenum
EPA 200 7
<20.7 mglkg
04/19/2018
Nickel
EPA 200 7
26.4 mg/kg
04/19/2018
Potassium
EPA 2007
6550 mg/kg
04/16/2018
Selenium
EPA 200 7
<20.7 mg/kg
04/19/2018
Sodium
EPA 200 7
3690 mg/kg
04/16/2018
Zinc
EPA 200 7
1400 mg/kg
04/17/2018
Nitrate+ N itrite-N itrogen
EPA 353 2
83.9 mglkg
04/20/2018
Total Solids (%)
SM 2540 a
2.35 %
04/12/2018
PH
SM 4500 H 8
7.94 units
04/16/2018
Ammonia Nitrogen
SM 4500 NH3 C
50500 mg/kg
04/23/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 org a
87600 mg/kg
04/23/2018
Total Phosphorus
SM 4500 P F
59900 mg/kg
04/1612018
Mercury
Sw1146 7471s
<0.766 mg/kg
0412212018
Comment: Sludge residuals, except pH, reported on a dry
weight basis pH reported on an as received basis.
Reviewed by:
Report 9 2018.05563
Page 1 of t

4W
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 3T7n9
Cna I FCTION Awn CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910392-0223 FAX [phone]
[e-mail]
5
{
CLIENT:
PROJECT NAME: Camp Lejeune MCB
REPORT NO: i 43
ADDRESS: G-F/EMD/ECIB/Environmental Laboratory
CONTACT NAME: Alberta Y. Okamoto
1§
PO NO: 9
12 Post Lane
REPORT TO: Patricia H. Raper
PHONE/FAX: 910ASI-0020 (fax) 910A51-7195
Camp Le'eune NC 28547
COPY TO:
va raper ennui, a1Nna.MgW0VUVMt '
emall: mbert.a ,ar; . ="W
Sarnoled Bv: 71 cos a SAMPLE TYPE: I = Influent, E = Effluent: W = Well, ST = Stream, SO = Soil, SL = Sludge, Other. 9
-
Sample Identification
Collection
e
s
o
m_
9 o
o
a
a
C m
PRESERVATION
i
ANALYSIS REQUESTED
Date
Time
Tern
w
a
8
n
s
CROM TANK
Y
3LUD
E JZ
P
I� {�D
X
luminum, Arsenic, Cadmiu
i
G
P
agnesium, Molybdenum,
G
G
C
pSlickel,
Potassium, o ium
a
elenium, Zinc,
G
G
C
P
Mercury Sludge, Nitrite,
'
G
G
C
P
KN, Total Solids/Soils &I
i
G'
G
C
P
'
hosphorus, Calcium, SAR
G
G
C
P
?A9
G
G
C
P
G
G
C
P
i
t
G
G
C I
P
G
G
3
Transfer
Relinquished By:
DatelTime
Receive d B :
DateITime
19 071
T /0. IF 0745-i
0 . it
}
Temperature when
Delivered BY:�
W
to R qugsted: i
to ct Time:
TURNAROUND:
i

Date:
Client:
Date Collected:
Date Received:
Sample:
Analyte
% Solids
pH
Marine Corps Base
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
4/11/2018
FC Wastewater
4/10/2018
4/10/2018
Quarterly Sludge
Date
Results Units Analyzed Tech Method
2.46 % 4/11/2018 AYO SM 2540 G
7.74 SU 4/10/2018 DRS 4500H+ B - 2000
CERTIFIED
LAUREN D. ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected b :
A co-st a
Si natu
Date Collected:
Time Collected:
©? 3,9
Location of sample:
Truck Loading Station
Com /Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH
Report all results as mg/kgmg/kg dry wt.
Was sample dechlorinated?
n/a
Preservation:
Ice
Regulatory Sample:
Yes
IField
Comments:
Relinquished by:
Date
Time
Received by:
Date
Time
CcaS'� cZ
q -1c) / �
07q5
��
� � `�
C/WS

CAMP LEJ EU N E WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: to. IS TIME: BY:
DATE:
ANALYZED BY:
TIME:
METHOD: 4500H+ B - 2000
07-
TIME
TIME
VOLUME
%
SAMPLE
TEMP
pH (SU)
COLLECTED
ANALYZED
mLs
RECOVERY
BUFFER 4.00
R" ;�
60Le-
_
..
UALKSKATION
BUFFER 10.00
60
-
CHECK BUFFER 7.00
60��_
f
�. '79_:
CROM TANK
%3�
7�/9
100
CROM TANK DUP
100
CHECK BUFFER 7.00
1
1
60
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

Environmental Chemists, Inc®
6602 Windmill Wav, Wilmington, NC 28405 - 910.392.0223 Lab s 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 s 2.92.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
info(c�environnlentalcllemists.com
USMC Camp Lejeune Date of Report: Jul 30, 2018
G-F/EMD/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2018-10826
Project ID: Crom Tank
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-27315 Site: CROM Tank 7/3/2018 6:40 AM Solid/Sludge Black
Test Method Results Date Analyzed
SAR
calculation
5.81
07/25/2018
Nitrate Nitrogen (talc)
Nitrite Nitrogen
EPA 353.2
177 mg/kg
07/09/2018
Nitrate Nitrogen
Subtraction Method
<1.0 mg/kg
07119/2018
Sludge Residuals
Aluminum
EPA 200.7
39100 mg/kg
07/24/2018
Arsenic
EPA 200.7
<23.8 mg/kg
07/20/2018
Cadmium
EPA 200.7
<23.8 mg/kg
07/20/2018
Calcium
EPA 2007
39900 mg/kg
07/19/2018
Chromium
EPA 200.7
<23.8 mg/kg
07/20/2018
Copper
EPA 200.7
155 mg/kg
07/20/2018
Lead
EPA 200.7
<23.8 mg/kg
07/20/2018
Magnesium
EPA 200.7
3220 mg/kg
07/19/2018
Nickel
EPA 200.7
<23.8 mg/kg
07/20/2018
Potassium
EPA 2007.
10000 mg/kg
07/19/2018
Selenium
EPA 200.7
<23.8 mg/kg
07/20/2018
Sodium
EPA 200.7
4490 mg/kg
07/19/2018
Zinc
EPA 2007
919 mg/kg
07/20/2018
Molybdenum
EPA 200.8
<23.8 mg/kg
07/23/2018
Nitrate+Nitrite-Nitrogen
EPA 353.2
162 mg/kg
07/09/2018
Total Solids (%)
SM 2540 B
2.09 %
07/10/2018
pH
SM 4500 H B
8.47 units
07/10/2018
Ammonia Nitrogen
SM 4500 NH3 G
50900 mg/kg
07/13/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org B
85200 mg/kg
07/13/2018
Total Phosphorus
SM 4500 P F
51000 mg/kg
07/12/2018
Mercury
SW8467471B
<0.766 mg/kg
07/16/2018
Report #:: 2010-10826 Pane 1 of 2

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab $ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
USiiMC Camp Lejeune Date of Report: Jul 30, 2018
G-F/EIUI%/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 285447 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2018-10826
Project ID: Crom Tank
Comment: Results reported on al�d^ry weight basis. pH reported on an as received basis.
Reviewed by: ho'k ,;D z
ReGxA # 2018-10526 Pace 2 of 2

6602
Way
gton, NC
ENVIRONMENTAL CHEMISTS, INC OFFICE:9r101-392-0223F'AX910-3 2-442 45
Analytical & Consulting Chemists NCDENR. DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemists_com
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Commandina General
PROJECT NAME: Camp Lejeune MCB
REPORT NO:
ADDRESS: G-F/EMD/EQB/Environmental Laboratory
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper
PHONE/FAX: [phone] (fax) 910-451-7195
Cam Lejeune NC 28547
COPY TO:
palncia per@usmc mil. alberta okamoto@usmc mil
email: ra
roberta lowder@usmc and lauren acosta usmcmd
Sampled By: 1-5z-rj SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
01
R
r
o n
C v,^
c `o
m
c
W
m
gz
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
z
zz
�o
e
e
o
W
CROM TANK
7 j
ir.yD
LUD
E C
P
3+�
X
kluminum, Arsenic, Cadmiu
G
G
C
P
agnesium, Molybdenum,
G
G
C
P
I
\11ckei, Potassium, Sodium,
Pelenium, Zinc,
G
G
C
P
14ercury Sludge, Nitrite,
G
G
C
P
KN, Total Solids/Soils L
G
G
C
P
r Ammonia, Iota-1
Phosphorus, Calcium, SAR
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
2.
14—
7 3 (- V 7(,1
Ai;qc"144-
! k 0,703
Temperature w e . D Accepted:
Deliver d By: Received By:
Comments: —P
le eq ested• ,
Time:
TUR , R ND:
G�

Date:
Client:
Date Collected:
Date Received:
Sample:
Anaiyte
% Solids
pH
C
Marine Corps Base
G-F/E M D/EQB/E nviron mental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
7/30/2018 s
FC Wastewater
7/3/2018
7/3/2018
Quarterly Sludge
Date
Results Units Analyzed
2.11 % 7/5/2018
8.22 SU 7/3/2018
Tech
Method
AYO
SM 2540 G
DES
4500H+ B - 2000
CERTIF Y:
LAUREN D. ACOSTA

Chain of Custody Record
CLIENT: Commanding General
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
Attn: Alberta Y. Okamoto
(910) 451 - 0020
Collected by:
=-����- �� A JF L �
Si nature:
Date Collected:
,3 /
Time Collected:
iJ �t7
Location of sample:
Truck Loading Station
Comp/Grab:
Grab
Number of Containers:
2
Analyses Requested:
% Solids, pH
Report all results as mg/kg dry wt.
Was sample dechlorinated?
n/a
Preservation:
Ice
Regulatory Sample:
Yes
Field
CComments:
Relinquished by:
Date
Time
Received by:
Date
Time
�.
7/,3
0&'-r7
OW 3/4
a7aD

CONTINUATION CHAIN OF CUSTODY
DATE TIME RELINQUISHED BY RECEIVED BY

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: TIME: BY:
DATE: • 3
ANALYZED BY: �S
TIME:
METHOD: 4500H+ B - 2000
ot.0 -f-S`
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
RECOVERY
BUFFER 4.00
60
` O
BUFFER 10.00
60
CHECK BUFFER 7.00
60
;mil
CROM TANK
0�04_0
okVS 3
1003.
8 2 3-
CROM TANK DUP
ous-1"
100
'33
CHECK BUFFER 7.00
0
60
k
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab /Fax
[e-mail]
USMC Camp Lejeune Date of Report: Dec 31, 2018
G-F/EMD/ECB -12 Post Lane Customer PO #:
Camp Lejeune NC 28547 Customer ID: 12060026
Attention: Alberta Y. Okamoto Report #: 2018-20090
Project ID: T3B
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
18-50728 Site: T3B 12/4/2018 7:00 AM Solid/Sludge Black
Test Method Results Date Analyzed
SAR
calculation
5.85
12/31 /2018
Sludge Residuals
Aluminum
EPA 200.7
70600 mq/kg
12/16/2018
Arsenic
EPA 200.7
25.0 mg/kg
12/14/2018
Cadmium
EPA 200.7
<11.0mg/kg
12/14/2018
Calcium
EPA 200.7
4910 mg/kg
12/19/2018
Chromium
EPA 200.7
40.8 mg/kg
12/14/2018
Copper
EPA 200.7
349 mg/kg
12/14/2018
Lead
EPA 200.7
20.7 mg/kg
12/14/2018
Magnesium
EPA 200.7
3470 mg/kg
12/13/2018
Molybdenum
EPA 200.7
13.5 mg/kg
12/14/2018
Nickel
EPA 200.7
32.2 mg/kg
12/14/2018
Potassium
EPA 200.7
3830mg/kg
12/13/2018
Selenium
EPA 200.7
<11.0mg/kg
12/14/2018
Sodium
EPA 2007
2200 mg/kg
12/13/2018
Zinc
EPA 200.7
1530mg/kg
12/14/2018
Nitrate+Nitrite-Nitrogen
EPA 353.z
107 mg/kg
12/26/2018
Total Solids (%)
SM 2540 B
4.44 %
12/10/2018
pH
SM 4500 H B
8.23 units
12/12/2018
Ammonia Nitrogen
SM 4500 NH3 C
14300 mg/kg
12/27/2018
Total Kjeldahl Nitrogen (TKN)
SM 4500 org B
52400 mg/kg
12/18/2018
Total Phosphorus
SM 4500 P F
3480 mg/kg
12/19/2018
Mercury
SW8467471B
0.5410mg/kg
12/26/2018
Comment: Results reported on a
dry weight basis.
Reviewed by: C1�t1ti
/y��t�1 tr�1 C /1
Report #:. 2018-20090 Page 1 of 1

1 - 11
ENVIRONMENTAL CHEMISTS, INC OFFCE 910602 1-392-0223l Way FAX 910-3 2� 4ngton, NC 5
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: Commandina General
PROJECT NAME: Camp Lejeune MCB
REPORT NO: - cr&5 0
ADDRESS: G-F/EMD/EQB/Environmental Laboratory
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper
PHONE/FAX: [phone] (fax) 910-451-7195
Cam Lejeune NC 28547
COPY TO:
patr'cia raper@usmc md, alberta okamoto@usmc mil.
email: robertalowder@usmc mil lauren acosta usmc mil
Sampled Bv: *,--r, L-A c SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
_a
c
E �
rn ~
a
a
p
��
��
� o
O
_�
c
� �
V E
e�
m
mQ �
J=
Z
PRESERVATION
ANALYSIS REQUESTED
i
a
Time
Temp
Z
Z_2
oDa
^
o
0
Tl-ly
C
F�
E;LUD
E C
P
oI
X
luminum, Arsenic, Cadmiu
G
G
C
P
agnesium, Molybdenum,
G
G
C
P
qickei, Potassium, So ium,
3elenium, Zinc,
G
G
C
P
lercury Sludge, Nitrite,
G
G
C
P
KN, Total Solids/Soils &
G
G
C
P
o a
hosphorus, Calcium, SAR
G
G
C
P
G
G
C
P
G
G
C
P
G
G
-��
C
P
G
G
Transfer
Relinquished By:
Date/Time I
Received By: _
Daterrime
Temperature
Delivered By:
Comments:
pted: Resampl4Rq sted:Received By �. Date: 'dime:OUND:

Date:
Client:
Date Collected:
Date Received:
Sample:
Analyte
% Solids
pH
Marine Corps Base
G-F/EMD/EQB/Environmental Laboratory
12 Post Lane
Camp Lejeune, NC 28547
12/10/2018
FC Wastewater
12/4/2018
12/4/2018
Quarterly Sludge
Date
Results Units Analyzed Tech Method
4.39 % 12/6/2018 DRS SM 2540 G
7.80 SU 12/4/2018 AYO 4500H+ B - 2000
NOTE: Sample was from T3B since crom tank is down, waiting on mixers.
CERTIFIE
LAUREN D. ACOSTA

Chain of Custody'Rekord,
CLIENT. Commanding Gertoral,
G-REMD/EOR/Environmental., Laboratory
12.Post,Lane-
Camp Lejeune, NC 28547,
Attn:, Alber.ta,Y. Okamoto
(910)-451 --0020
Collected.by:
signature:
Date ' Collected:
TimwCollect6d-w
Location of'sample:
Comp/Grab.-
Grab
Number of Containers:
2
% Solids; pH
Analyses Requested-
Fleportall results :as,nq/kg dry wt.
Was sample-dechlorinatedl
n/a
Preservation:
Ice
RegulatorySample:
j Yes
Relinguished:,by:
Date
Time,
Receivedkw

CAMP LEJEUNE WWTP
pH READINGS FOR QUARTERLY SLUDGE SAMPLING
COLLECTED
DATE COLLECTED: i2 TIME: a 700 BY:
DATE:
ANALYZED BY:
TIME: 07►�
METHOD: 4500H+ B - 2000
SAMPLE
TIME
COLLECTED
TIME
ANALYZED
VOLUME
mLs
TEMP
pH (SU)
%
RECOVERY
BUFFER 4.00
60
4.01
BUFFER 10.00
60
0 n
CHECK BUFFER 7.00
60
-7.00
GRGiNA"kir
0100
0-1 c3
1 oo
4I-11
-7. �o
+c ou`
0`� i�-
100
�� I
1. 90
CHECK BUFFER 7.00
+�
60
-7- 00
FORM UPDATED: SEPTEMBER 2012 CHECKED BY:

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F7� —71 Environmental Chemists, Inc.
i 6602 Windmill Way, Wilmington, NC 28405 = 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(( environmentalchemists.com
USMC Camp Lejeune
Date of Report: Feb 20, 2018
G-F/EMD/ECB -12 Post Lane
Customer PO #:
Camp Lejeune NC 28547
Customer ID: 12060026
Attention: Alberta Y. Okamoto
Report #: 2018-01200
Project ID: Camp Lejeune MCB
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
18-02964 Site: CROM Tank
1/23/2018
7:30 AM Solid/Sludge Black
Test
Method
Results
Date Analyzed
Chlordane
SW 846 Method 80818/3510
<0.02 mg/L
02/07/2018
Endrin
SW 846 Method 8081B/3510
<0.0005 mg/L
02/07/2018
Heptachlor
SW 846 Method 8081B/3510
<0.0005 mg/L
02/07/2018
Heptachlor epoxide
SW 846 Method 8081B/3510
<0.0005 mg/L
02/07/2018
Lindane
SW 846 Method 8081B/3510
<0.0005 mg/L
02/07/2018
Methoxychlor
SW 846 Method 8081B/3510
<0.0005 mg/L
02/07/2018
Toxaphene
SW 846 Method 8081B/3510
<0.05 mg/L
02/07/2018
1,4-Dichlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
2,4,5-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
2,4,6-Trichlorophenol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
2,4-Dinitrotoluene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Hexachloro-1,3-butadiene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Hexachlorobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Hexachloroethane (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
m + p-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Nitrobenzene (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
o-Cresol (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
Pentachlorophenol (TCLP)
SW 846 method 8270/3510
<0.250 mg/L
02/12/2018
Pyridine (TCLP)
SW 846 method 8270/3510
<0.050 mg/L
02/12/2018
2,4,5-TP
SW846 Method 8151A
<0.003 mg/L
02/07/2018
2,4-D
SW846 Method 8151A
<0.003 mg/L
02/07/2018
1,1-Dichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
1,2-Dichloroethane
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Benzene
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Carbon Tetrachloride
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Report*: 2018-01200
pane 1 of 2

IL s o r
SM.
ANALYTICAL & CONSULTING CHEMISTS
USMC Camp Lejeune
G-F/EMD/ECB -12 Post Lane
Camp Lejeune NC 28547
Attention: Alberta Y. Okamoto
Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405 . 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(ci;environmentalchemists.com
Date of Report: Feb 20, 2018
Customer PO #:
Customer ID: 12060026
Report #: 2018-01200
Project ID: Camp Lejeune MCB
Chlorobenzene
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Chloroform
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Methyl ethyl ketone
SW846 Method 8260/5030
<0.05 mg/L
02/06/2018
Tetrachloroethylene
SW846 Method 826015030
<0.01 mg/L
02/06/2018
Trichloroethylene
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
Vinyl Chloride
SW846 Method 8260/5030
<0.01 mg/L
02/06/2018
RCI
Cyanide
EPA 335.4
<0.025 mg/kg
01/30/2018
pH
SM 4500 H B
7.85 units
01/30/2018
Sulfide
SM 4500 s o
2.09 mg/kg
01/29/2018
Ignitability
SW 846 method 1010
> 195 °F
02/02/2018
TCLP Metals
Arsenic
EPA 200.7
<1.0 mg/L
02/13/2018
Barium
EPA 200.7
<1.00 mg/L
02/12/2018
Cadmium
EPA 200.7
<1.00 mg/L
02/12/2018
Chromium
EPA 200.7
<1.00 mg/L
02/12/2018
Lead
EPA 200.7
<1.00 mg/L
02/12/2018
Selenium
EPA 200.7
<1.0 mg/L
02/13/2018
Silver
EPA 200.7
<1.00 mg/L
02/12/2018
Mercury
EPA 245.1
<0.0020 mg/L
02/11 /2018
Comment:
Reviewed by:
Report #:: 2018-01200 Page 2 of 2

ir -11P
NOW
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
CLIENT: C
PROJECT NAME: Camp Lejeune MCB
REPORT NO:
ADDRESS: I&E/EMD/EMEnvironmental Lab
CONTACT NAME: Alberta Y. Okamoto
PO NO:
12 Post Lane
REPORT TO: Patricia H. Raper
PHONE/FAX: [phone] (fax) 910-451-7195
Cam Lejeune NC 28547
COPY TO:
Patricia, raper@usme. mil,alberta. [e-mail],
email:
Sampled BY: SAMPLE TYPE:'I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other.
Sample Identification
Collection
to
a E
a o
d
e
o
tz
O m
m
5 z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
z__
.,
a
o
o
W
c
J
CROM TANK (�Z71
7
so
C
P
G
-`�9�Pesticides,
X
CLP - Volatile, Semi -volatile
Herbicides
G
G
C
P
RCRA (8 metals)
G
G
C
P
eactivity, Corrosivity,
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
C
P
G
G
Transfer
Relinquished By:
Date/Time
Received By:
Daterrime
1.
,E' av61 101,14401
D WO
2.
/ J'3 le. ojgL'
b 7q
Temperature when Received: Accepted:
Delivered By: Reci
Comments:

SECTION 6
Annual Pathogen & Vector Attraction
Reduction Forms
(Form PVRF 503)

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeune AWWTP NPDES Number: WQ0063029
Monitoring Period: From 1/1/2018 To 3/31/2018
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 0
Alternative 2
Alternative 3
Alternative 4
Alternative 5
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic r
Beta Ray
Gamma Ray
Pasteurization
Class B: Alternative I Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying I Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
Pathogen Density
Number of
Sxcee-
dences
Frequency
of Analysis
Sample
Type
Analytical
Tech -pique
Minimum
Geo. Mean
Maximu
Units
Fecal Coliform
2 x 10 to the
61h power
per grant of
total solids
MPN
CRJ
1000 ntpn per grant of total
solid (dry weight)
1
7.02
49.3
MPN/g
0
Weekly
Grab
SM9221 E
Salmonella bacteria (in
lieu of fecal coliform)
3 MPN per 4 grains total
solid (dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction)
All. 2 (40-day bench)
Alt. 3 (30-day bench) ]
Alt. 4 (Spec. 0, uptake)
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable)
I Alt. 8 (Drying - unstable)
Alt. 9 (Injection)
Alt. 10 (Incorporation)
No vector attraction reduction alternatives were perforated
CERTIFICATION STATEMENT (please check the appropriate statement)
o "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
O reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
`tThis determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment"
Charles J. Scozzari Charles J. Scozzari
Preparer Name and Title (typ or . t) Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* < Date Signature of Land Applier (if applicable) D• e
1
°Preparer t /dincd in 40 CFR Pan 503.9(r) and 15A NCAC 2T .1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejcune AWWTP WQ Permit Number: W00012346
WWTP Name: Camp Lejcune AWWTP NPDES Number: WQ0063029
Monitoring Period: From 4/1/2018 To 6/31/2018
Pathogen Reduction (40 CFR 50332) - Please indicate level achieved and alternative performed:
Class A:
Alternative I
Alternative 2
Alternative 3
Alternative 4
Alternative 5
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying Heat Treatment
Thermophilic Q
Beta Ray
Gamma Ray Pasteurization
Class B: Alternative 1 Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Puthogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the followingmonitorin
data:
Paramcler
Allowable Level to
Sludge
Pathogen Density
b y
Number of
Exc�w-
t1Cn[CS
Frequency
of Analysis
Sample
Type
Analytical
Technique
Minimum
Gen, Mean
Maximus
Units
Fecal Colifotm
2x10to
the 6th
Power per
grant of
Total solids
MPN
M
I OW mpo per grain of
total solid (dry
weight)
0.67
7.11
75.6
MPN/g
0
Weekly
Grub
SM9221 E
Salmonella bacteria (in
lieu of fecal coliform)
3 MPN per 4 grams
total solid (dry wcigho
Vector Attraction Reduction (44) CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction)
All 2 (40-day bench)
Alt 3 (30-day bench) Q
Alt. 4 (Spec. O_ uptake)
Alt. 5 (14-Day Aerobic)
Alt. 6 (Alk Stabilization
Alt 7 (Drying - Stable)
JAIt. 8 (Drying - Unstable)
Alt. 9 (injection)
Alt 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector attraction
El reduction requirement in 44) CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector attraction
O reduction requirement in 40 CFR 50333 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
Charles J. S ozza
Preparer Name and Ville (ty e ar rint)
1
Signature of
Charles J. Scozzari
Land Applier Name and Title (if applicable)(type or print)
Date Signature of L-and Applier (if applicable)
*Preparer is Wined in 40 CFR Pan 503.9rr) and 15A NCAC 2T .1 102 (26)
,z4
Dale

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp L:jcune AWWTP WQ Permit Number: WQ(1012346
WNVTP Name: Camp L:jeune AWWTP NPDES Number: WQ0063029
Monitoring Period: From 7/1P-018 To 9/302018
Pathogen Reduction (40 CFR $03.32) - Please indicate level achieved and alternative performed:
Class A: I
Alternative I O
Alternative 2
Alternative 3
Alternative 4
1 Alternative .5
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Heat Drying
Heat Treatment
Thermophilic []
Beta Ray
Gamma Ray
Pasteurization
Class B: Alternative I Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Patha ens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in Sludge
e.n
Pathogen
Density
y
Number of
6xcee
dences
Frequency
of Analysis
Sample
Type
Analytical
Ttch•niyuc
Minimum
Gco. Mean
Maxima
Units
Fecal Colifarm
2 x 10 to the 6th
power per gram of
total solids
MPN
CFU
lauo per gram total
solidlid (dry weight)
0.522
6.77
97.98
MPN/g
0
Weekly
Grab
SM922IE
Salmonella bacteria (in
lieu of fecal eoliform)
3 MPN per 4 grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 50333) - Please indicate option performed:
Ah.l (VS reduction) JAIt. 2 (40-Jay bench) Ali. 3 (30-day bench) Alt. 4 (Spero. 0; uptake)
Alt. 5 (14-Day Aerobic) Ah. 6 (Alk. Stabilization Alt 7 (Drying - Stable) JAR. 8 (Drying - Unstable)
Alt, 9 (Iniection) Alt 10 (Incorporation) lNo vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ `+I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332 and the vector attraction reduction
❑ requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. II um aware that there are significant penalties for false certification including fine and
imprisonment."
Charles J. Sco n
Preparer Name and Title { pe prin
Signature of Prepare Date
*Preparcr is dcfiffexl in 40 CFR Pan 503,9(r) and 15A NCAC 2T .1102 (26)
Charles J. Seozzari
Land Applier Name and Title (if applicable)(type or print)
� 9
Signature of Land Applier (if applicable) ste

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Camp Lejeune AWWTP WQ Permit Number: WQ0012346
WWTP Name: Camp Lejeunc AWWTP NPDES Number: WQ(x)63029
Monitoring Period: From 10/l/2018 To 12/31/2018
Pathogen Reduction (40 CFR 50332) - Please indicate level achieved and alternative performed:
Class A:
Alternative 10
Alternative 2
Alternative 3
Alternative 4
Alternative 5
Alternative 6
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens
Compost
Heat Drying
Heat Treatment
Thermophilic Q
Beta Ray
Gamma Ray
Pasteurization
Class B: Alternative I Alternative 2
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level in
Sludge
Pathogen
Density
Nut= of
Hxc" deuces
Frequency
of Analysis
Sample
'Type
Analytical
Tcch-nique
Minimum
Gco. Mean
Maximo
Units
Fecal Coliform
2x10to
the 61h
power per
grain of
total solids
MPN
CFU
I W0 mpn per gram of
total solid (dry
weight)
0.4
5.16
66.5
MPN/g
0
Weekly
Grab
SM9221 E
Salmonella bacteria (in
lieu of fecal Coliform)
3 MPN per 4 grams
total solid (dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
All t (VS reduction)
Alt. 2 (40-day bench)
Alt. 1 (30-day bench) 0
Alt. 4 (Spec. O, uptake)
Alt 5 (14-Day Aerobic)
jAft 6 (Alk Stabilization
Alt 7 (Drying - Stable)
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection)
jAh. 10 (Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
441 certify, under penalty or law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
reduction requirement in 40 CFR $03.33 have been met."
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction
O reduction requirement in 40 CFR 50333 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure
that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector
attraction reduction requirements have been met. I am aware that there are significant penalties for false certification
including fine and imprisonment."
Charles J. Sc cza Charles J. Scozzari
Preparer Name and Tit (ty e o ri Land Applier Name and Title (if applicable)(type or print)
Y Signature of r • arer• Date Signature of Land Applier (if applicable) 051/t
in 40 CFR Pan 503.9(r) and 15A NCAC 2T .1 102 (26)

SECTION 7
Pathogen & Vector Attraction Reduction
Lab Sheets/Records

2
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CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
1/1/2018
1/2/2018
1/3/2018
1/4/2018
1/5/2018
1/6/2018
1/7/2018
1/8/2018
1/9/2018
1/10/2018
60,000
21
1/11/2018
60,000
22
18.3
1/12/2018
25.7
25.5
1/13/2018
30.9
29.1
1/14/2018
37.1
32.1
1/15/2018
44.6
34.7
1/16/2018
52.7
38
1/17/2018
59.9
42.2
1/18/2018
59.8
45.4
1/19/2018
57
51.1
1/20/2018
55.3
53.8
1/21/2018
53.6
55.1
1/22/2018
18,000
47.7
54.3
1/23/2018
52.8
53.8
1/24/2018
13,500
53.2
53.1
1/25/2018
55.8
51.9
1/26/2018
55.4
50.2
1/27/2018
54.8
48.9
1/28/2018
53.5
48
1/29/2018
18,000
48.3
47.5
1/30/2018
135,000
48.7
47.7
20
1/31/2018
53.8
47.2
Total =
183,000
1,043.60
928
20
Ave=
8,318
47
44
20
Max=
60,000
59.9
55.1
20
Min=j
0
21
18.3
20

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
2/1/2018
54.8
46.4
2/2/2018
54
45.3
2/3/2018
52.5
43.9
2/4/2018
51.7
43.1
2/5/2018
18,000
49.4
44
2/6/2018
45.3
44.8
2/7/2018
46.6
44.7
2/8/2018
46.1
44.3
2/9/2018
44.4
44.5
2/10/2018
42.8
44.2
2/11/2018
41.5
43
2/12/2018
40.4
42
2/13/2018
2/14/2018
2/15/2018
2/16/2018
2/17/2018
2/18/2018
2/19/2018
2/20/2018
2/21/2018
2/22/2018
2/23/2018
2/24/2018
2/25/2018
2/26/2018
60,000
2/27/2018
38.7
2/28/2018
49.5
Total =
78,000
658
530
0
Ave=
2,786
47
44
0
Max=
60,000
54..8
46.4
0
Min=
0
40.4
42
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
3/1/2018
61.6
3/2/2018
60,000
50.9
45.1
3/3/2018
54
64
3/4/2018
65.5
65.2
3/5/2018
18,000
65
64.2
3/6/2018
67.2
61.9
3/7/2018
65
58.6
3/8/2018
18,000
58.9
56.2
3/9/2018
59.7
55.2
3/10/2018
59.2
54.4
3/11/2018
•59.1
53.9
3/12/2018
55.7
53.2
3/13/2018
18,000
55.8
52.4
0.6
3/14/2018
18,000
54.2
51.7
8/15/2018
57
51.1
3/16/2018
18,000
52.7
51.8
3/17/2018
56.6
51.8
3/18/2018
57.7
51.1
3/19/2018
56.1
50
3/20/2018
18,000
50.8
49.8
1.3
3/21/2018
53.3
49
-
3/22/2018
18,000
49.7
48.6
3/23/2018
53.4
48.3
3/24/2018
54.4
47.6
3/25/2018
53.2
47.7
3/26/2018
52
48.8
3/27/2018
50.5
44.9
3/28/2018
49
44.2
3/29/2018
47.5
43.4
3/30/2018
46
42.3
3/31/2018
44.2
39.8
Total =
186,000
1,716
1,542
2
Ave=
6,000
55.4
51
1
67.2
65.2
1.3
��Ma�x=60,000
Min=
0
44.2
39.8
0.06

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
1/1/2018
1/2/2018
1/3/2018
1/4/2018
1/5/2018
1/6/2018
1/7/2018
1/8/2018
1/9/2018
1/10/2018
1/11/2018
1/12/2018
1/13/2018
1/14/2018
1/15/2018
1/16/2018
60,000
1
1/17/2018
21.2
1/18/2018
24
1/19/2018
28.4
1/20/2018
30.3
1/21/2018
33.5
1/22/2018
38.6
1/23/2018
43.9
1/24/2018
49.1
1/25/2018
53.5
1/26/2018
55.5
1/27/2018
55.8
1/28/2018
57.8
1/29/2018
57.9
1/30/2018
55.8
1/31/2018
53.2
Total =
60,000
658.00
1
Ave=
3,750
44
1
Max=
60,000
57.8
1
Mil1=1
0
21.2
1

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
2/1/2018
51.1
2/2/2018
49.1
2/3/2018
46.7
2/4/2018
45.1
2/5/2018
2/6/2018
. 2/7/2018
2/8/2018
2/9/2018
2/10/2018
2/11/2018
2/12/2018
2/13/2018
2/14/2018
2/15/2018
2/16/2018
60,000
30.6
2/17/2018
37.2
2/18/2018
47:7
2/19/2018
61.5
2/20/2018
68
2/21/2018
60,000
56.9
37.6
2/22/2018
62.2
51.3
2/23/2018
66
60.7
2/24/2018
63.9
66.9
2/25/2018
61.8
66.1
2/26/2018
59.3
63.5
2/27/2018
'57
60.7
2/28/2018
55.2
58.6
Total =
120,000
919
465
Ave=
4,286
54
58
Max=
60,000
68
1 66.9
Min=
. 0
1 30.6
1 37.6

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
3/1/2018
53.8
.56.8
3/2/2018
52
54.8
3/3/2018
49.8
52.8
3/4/2018
48.3
51.7
3/5/2018
46.8
50.8
3/6/2018
45.3
50
3/7/2018
44.3
49
3/8/2018
42.7
48.2
3/9/2018
41.2
47
3/10/2018
40.1
45.7
3/11/2018
39.4.
44.8
3/12/2018
60,000
30.5
3/13/2018.
28.9
3/14/2018
31.6
3/15/2018
35.1
3/16/2018
40.5
3/17/2018
47.6
3/18/2018
56
3/19/2018
60.4
3/20/2018
60.3
3/21/2018
58.3
3/22/2018
56
3/23/2018
54.3
3/24/2018
52.2
3/25/2018
49.8
3/26/2018
47.8
3/27/2018
45.9
3/28/2018
44.3
3/29/2018
43.4
3/30/2018
32.7
3/31/2018
31.2
Total =
60,000
1,411
551
Ave=
1,935
45.5
50
Max=
60,000
60.4
56.8
Min=
0
28.9
44.8

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MP.N)
1/1/2018
--18,000--
56.7
1/2/2018
18,000
53.2
50.7
1
1/3/2018
56
51.4
1/4/2018
18,000
54.9
52.9
1/5/2018
13,500
52.7
52.2
1/6/2018
54
51.5
1/7/2018
54.6
50.2
1/8/2018
54.4.
49.2
1/9/2018
54.1
48.7
1
1/10/2018
54
48.8
1/11/2018
52.4
52.2
1/12/2018
55.1
51.8
1/13/2018
56.2
50.7
1/14/2018
55.3
49.3
1/15/2018
54
47.9
1/16/2018
53.2
47.9
1/17/2018
55.9
50.7
1/18/2018
53.9
49.2
1/19/2018
53
49.4
1/20/2018
55.2
52.1
. 1/21/2018
54.1.
51.3
1/22/2018
45.9
48.5
1/23/2018
18,000
45.9
48.5
1
1/24/2018
50.2
48.9
1/25/2018
13,500
54.6
52.2
1/26/2018
. 62.7
52.9
1/27/2018
18,000
60.9
53.7
1/28/2018
64.6
55.3
1/29/2018
69
54.4
1/30/2018
66.1
53.1
1/31/2018
62.3
52.3
Total =
117,000
1,725.10
1,579
1
Ave=
3,774
55
50
1
Max=
18,000
69
55
1
Min=
0
45.9
47.9
1

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
2/1/2018
13,500
58
56.4
2/2/2018
13,500
57.2
59.5
2/3/2018
59.4
59.9
2/4/2018
60.1
59.7
2/5/2018
18,000
56.1
59.2
2/6/2018
18,000
56.6
60
12.66
2/7/2018
18,000
58.98
62.2
2/8/2018
18,000
60.9
64.7
2/9/2018
68.9
66.8
2/10/2018
18,000
65.2
67.7
2/11/2018
18,000
64.2
69
2/12/2018
18,000
65
69.8
2/13/2018
18,000
70.2
63.7
6.65
2/14/2018
18,000
63.6
70.6
2/15/2018
13,500
62.1
69.9
2/16/2018
13,500
64.6
72.4
2/17/2018
71.3
73.2
2/18/2018
18,000
66
71.6
2/19/2018
71
71.2
2/20/2018
18,000
65.9
70.3
4.98
2/21/2018
66.5
70.5
2/22/2018
18,000
68.3
70.7
2/23/2018
71.3
71.5
2/24/2018
18,000
64.8
70.1
2/25/2018
69.5
69.8
2/26/2018
18,000
63.7
69
2/27/2018
18,000
62.1
68.9
6.01
2/28/2018
70.3
69.7
Total =
324,000
1,802
1,878
30
Ave=
11,571
64
67
8
Max=
18,000
71.3
73.2
12.66
Min=
0
56.1
56.4
4.98

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
-3/1/2018
-
- -71.9
68.9--
3/2/2018
68.1
67.7
3/3/2018
67.7
66.5
3/4/2018
66.6
65.8
3/5/2018
63.6
65..1
3/6/2018
18,000
59.8
64.1
4.05
3/7/2018
18,000
60.6
64.4
3/8/2018
18,000
63.9
66.2
3/9/2018
69.1
67.4
3/10/2018
69.1
67.3
3/11/2018,
67.3
67.2
3/12/2018
18,000
58.3
65.8
3/13/2018
57.1
66
3/14/2018
64.3
67.8
3/15/2018
15,000
66.2
68.3
3/16/2018
18,000
67.7
68.6
3/17/2018
66.8
67.1
3/18/2018
65.1
65.6
3/19/2018
18,000
60.1
64.4
3/20/2018
63.9
63.9
3/21/2018
18,000
59.3
63.5
3/22/2018
18,000
58.8
63.9
3/23/2018
65
66.5
3/24/2018
67.3
66.8
3/25/2018
65.3
66.1
3/26/2018
18,000
59.6
64.7
3/27/2018
18,000
59.1
65
0.67
3/28/2018
18,000
59.7
66.5
3/29/2018
18,000
60.6
67.2
3/30/2018
18,000
58.6
67.6
3/31/2018
64.2
67.5
Total =
247,500
1,974
2,054
.6
Ave=
7,984
63.7
66
2
Max=
18,000
71,9
68.9
4.05
Min=
0
57.1
63.5
0.67

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
1/1/2018
-
1/2/2018
1/3/2018
1/4/2018
1/5/2018
1/6/2018
1/7/2018
1/8/2018
1/9/2018
1/10/2018
1/11/2018
1/12/2018
1/13/2018
1/14/2018
'1/15/2018
1/16/2018
1/17/2018
1/18/2018
1/19/2018
1/20/2018
1/21/2018
1/22/2018
1/23/2018
1/24/2018
1/25/2018
1/26/2018
1/27/2018
1/28/2018
1/29/2018
1/30/2018
1/31/2018
Total =
Ave=
Max=
Min=

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(0C)
Temp
(oC)
Fecal
(MPN)
2/1/2018
-
-
2/2/2018
2/3/2018
2/4/2018
2/5/2018
2/6/2018
2/7/2018
2/8/2018
2/9/2018
2/10/2018
2/11/2018
2/12/2018
2/13/2018
2/14/2018
2/15/2018
2/16/2018
2/17/2018
2/18/2018
2/19/2018.
2/20/2018
2/21/2018
2/22/2018
2/23/2018
2/24/2018
2/25/2018
2/26/2018
2/27/2018
2/28/2018
Total =
Ave=
Max=
Min=

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
3/1/2018
3/2/2018
3/3/2018
3/4/2018
3/5/2018
3/6/2018
3/7/2018
3/8/2018
3/9/2018
3/10/2018
3/11/2018
3/12/2018
3/13/2018
3/14/2018
3/15/2018
3/16/2018
3/17/2018
3/18/2018
3/19/2018
3/20/2018
3/21/2018
3/22/2018
3/23/2018
-3/24/2018
3/25/2018
3/26/2018
3/27/2018
3/28/2018
3/29/2018
3/30/2018
3/31/2018
Total =
Ave=
Max=
Min=

CAMP LEIJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
CCS
DATE COLLECTED: ' TIME COLLECTED:(nq / COLLECTED BY: ,
RECEIVED BY: IDATE: . 2 . 1 TIME: i;)Ct Q
DATE ANALYZED: _ TIME: ANALYST:'
METHOD: .
3 HOURS at 35 * 0.51C in INCUBATOR
21 m 2 HOURS at 44.5 f 0.2'C In WATERBATH ,
SAMPLE LOCATION
10 mL
i mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
COMB. OF
POSMVES
MPNIM 00 mt.
MPNIGRAM
J
C!�
15 mL
O 15 mL
of 5 mL
O 15 mL
/ 5 mL
�� 15 mL
15 inl.
! 5 mL
�- C"
� , (223
/
DUP
lSmL
Q !l3mL
3 HOURS at 35 :L- 0.5°C in INCUBATOR
DATE IN INCUBATOR: )L
DATE OUT INCUBATOR: a- 1 U
21 x 2 HOURS at 44.5 s 0.2°C in WATERBATH
DATE IN WATERBATH: 'a, 1 g
DATE OUT WATERBATH: , 3-1 "f'
POSITIVE
CONTROL
NEGATIVE
CONTROL
13LANK
SS A 1 BROTH
\
N
I)S A•1 BROTH
FORM UPDATED: APRIL 2007
TIM.. , OQQ
CUSA70H:
TIME OUT �� OD
WUMATOR:
WATETITe 1 3 o t
MATH: 111
TIME ovT 9 c'
WATERAATH: � J
Mnw�rat
�erw�unwea 7
ro+wuiurea
uRrtwtec �.
�waw�nyro+ �„
3.1 % TOTAL SOLIDS
(ATAD SOLIDS ANALYSIS)
CALCULATION:
MPN Fecal ColifornVgram sludge
Largest volume x °% dry solids
CHECKED BY:
COPY MADE: ___�
FA

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: DATE RECEIVED: _ [? DATE ANALYZED:
TIME COLLECTED: O $ TIME RECEIVED: 0 qOD TIME ANALYZED: p 0 O
COLLECTED BY: ���� o �� RECEIVED BY: ANALYZED BY: l?4
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35+ 0.5'C IN INCUBATOR 1 21 + 2 HOURS AT 44.5+ 0.2-C IN WATERBATH
COMB. OF
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL I 1 mL I 0.10 mL 10.010 mL POSITIVES I MPN J mL' I MPN 1100 mL'I
f
M c�
O 15mL /5mL O /5mL 15mL O JSmL /5mL 15mL 15mL
i
DU P 15 mL 15 mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: _ DATE OUT INCUBATOR: 9.
TIME IN INCUBATOR: 3 TIME OUT INCUBATOR: 33
INCUBATOR TEMP: s— ° INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2'C IN WATERBATH
DATE IN WATERBATH: l , 9 . to DATE OUT WATERBATH
TIME IN WATERBATH: 1333 TIME OUT WATERBATH f23�
WATERBATH TEMP: s44 C— WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
-)
Vti
DS A-1 BROTH
N
FORM UPDATED: DECEMBER 2017
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN 1 100 mL 2 = (100)(MPN / ml-)
MPN J GRAMS
&- 17
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS) :
MPN / mL'
MPN/GRAMS=
g6 Tot. Solids'.
IlN�ti4
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: DATE RECEIVED: l • l4 - l8 DATE ANALYZED:
TIME COLLECTED: 7 �� TIME RECEIVED: O`'j�p TIME ANALYZED: Ov2S
COLLECTED BY: �Gr 1 RECEIVED BY: ANALYZED BY:��- '
METHOD: SM 9221C E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5•C IN INCUBATOR 21 ± 2 HOURS AT 44.5 + 0.rC IN WATERBATH
SAMPLE LOCATION 10 tOL I 1 mL 0.10 m! 0.010 mL 10 mL I 1 mL I 0.10 mL 10.010 mL I COMB. OF I POSITIVES MPN I ML' I MPN 1100 mL2
I ��n tA I 0 / 5 ml-I D 15 mLI E).15 and c 15 mLl 0 / 5 mLI d / 5 mLI 0 15 mLI O 15 mLl 0 " o ^ 0-,
[:1. ` � I /-) I
DUP
15
3 HOURS AT 35 + 0.5`C IN INCUBATOR
015
DATE IN INCUBATOR: 1 l ` a DATE OUT INCUBATOR:
TIME IN INCUBATOR: C7g?J2J TIME OUT INCUBATOR:
INCUBATOR TEMP: 3�—0 d c, INCUBATOR TEMP: 2js. D O CG
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: t _ l`C - e DATE OUT WATERBATH
TIME IN WATERBATH: "�j� TIME OUT WATERBATH
WATERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
?L->s
wfj>1
&16 ,
DS A-1 BROTH
t ` &j
FORM UPDATED' DECEMBER 2017
MPN Index Value
MPN/mL'=
Largest Sample Volume
MPN 1100 mL Z = (100)(MPN / mL)
MPN/GRAMS=
MPN IGRAM'
-1' 31
%, TOTAL SOLIDS
(ATAD SOLIDS
ANALY�,
QQSIS
I L/
MPN / mL'
% Tot. Solids 4 x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP _
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: / DATE RECEIVED: DATE ANALYZED:
TIME COLLECTED: C- / TIME RECEIVED: p'1 TIME ANALYZED:
COLLECTED BY: RECEIVED BY: ANALYZED BY: ell
METHOD: SM 9221C E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 1 21 ± 2 HOURS AT 44.5± 0.21C IN WATERBATH
SAMPLE LOCATION 1 10 mL I 1 mL - 1 0.10 mL 1 0.010 mL 1 10 mL 1 1 mL 1 0.10 mL 1 0.010 mL
j /5mL '� l5mL � /5mL -D 15mL � 15mL O /5mL �/5ml O 15mL
DUP 0 I.
i / 5mL 15 mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: _ 7 3,Q� �y DATE OUT INCUBATOR:
TIME IN INCUBATOR: oC(L#- TIME OUT INCUBATOR: t�
INCUBATOR TEMP: amINCUBATOR TEMP: �j 5
21 + 2 HOURS AT 44.5 + 0.20C IN WATERBATH
DATE IN WATERBATH: ,. T7, L% DATE OUT WATERBATH' , ' -n
TIME IN WATERBATH: TIME OUT WATERBATH O-1'-S
WATERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
�s
vw
VS A-1 BROTH
jpv5
vv
FORM UPDATED: DECEMBER 2017
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL z = (100)(MPN ! mL)
COMB. OF
POSITIVES MPN ! mL' MPN ! 100 mL'
o. 2-0
MPNIGRAM3
-7. t �L ,
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS�
MPN / mL'
MPNIGRAM3=
°k Tot. Solids, x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: i se)I DATE RECEIVED: I. '220 • DATE ANALYZED:
TIME COLLECTED: •7 2 & TIME RECEIVED: 0-1 5 j• j TIME ANALYZED:
COLLECTED BY: RECEIVED BY: aAlvANALYZED BY:
METHOD: SM 9221C E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 + 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL
i
Cji�-�/l \ /5mL O /5mL 0 I5mL O 15mL /5mL O /5mL O /5mL D I5mL
DU P (i
/6MLj 5mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: M . ' j(q. go `'�, DATE OUT INCUBATOR: • 30. a D
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP: INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: t • O • D-0 ( DATE OUT WATERBATH, �j.j • ��
TIME IN WATERBATH: I 0 S-10 TIME OUT WATERBATH �Sp
WATERBATH TEMP. A WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A4 BROTH
70
DS A-1 BROTH
p
I
FORM UPDATED: DECEMBER 2017
U U
MPN ImL'=
MPN Index Value
Largest Sample Volume
MPN 1100 mL Z = (100)(MPN i mt-)
COMB. OF MPN ! mL' MPN 1100
mL2
POSITIVES
1. o 0
MPN / GRAM3
MPNIGRAM3=
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)
;- V(Q
MPN / mL'
% Tot. Solids 4 x 100
CHECKED BY:
COPY MADE:

5
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
LP
{ DATE COLLECTED: 2 4 �� DATE RECEIVED: a , Lo / DATE ANALYZED:
TIME COLLECTED: TIME RECEIVED: QBQ�' TIME ANALYZED: ��3Q
i
COLLECTED BY: U%1 I RECEIVED BY: j ANALYZED BY: DES
9
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5•C IN INCUBATOR 21 + 2 HOURS AT 44.5 + 0.2•C IN WATERBATH
1 SAMPLE LOCATION 10 mL 1 mL r 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN I mL' MPN 1100 mO
r POSITIVES
('� 3
/5mL y /5mL Q 15mL 0 ISmL � fSmL 15mt t 15m! 1bmL
i Llll .1: -Ia-IY
DUP
1015
v 15 mL
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN INCUBATOR: DATE OUT INCUBATOR:
TIME IN INCUBATOR: !!� TIME OUT INCUBATOR: 14. s
INCUBATOR TEMP: S v OC INCUBATOR TEMP: 3S d cC
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
' DATE IN WATERBATH: ,;Z. l t� DATE OUT WATERBATH�
TIME IN WATERBATH: 114 (-P TIME OUT WATERBATH 3 3S`
WATERBATH TEMP: � 1 6 WATERBATH TEMP:
POSITIVE NEGATIVE BLANK MPN Index Value
CONTROL CONTROL MPNlmL'=
SS A-1 BROTH Largest Sample Volume
DS A-1 13ROTH �-
MPN / 100 mL2 = (100)(MPN / mL)
FORM UPDATED- DECEMBER 2017
MPN IGRAM3
%, TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS'
MPN / mL'
MPN/GRAM =
*A Tot. Solids" x 100
CHECKED BY: (,0,0-
COPY MADE; R b)k

k
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 2 . ! 8 DATE RECEIVED: '� �� DATE ANALYZED:
t
TIME COLLECTED: ? TIME RECEIVED: oe0o TIME ANALYZED: 0 /o-
COLLECTED BY: Cr0 RECEIVED BY: s ANALYZED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
1
3 HOURS AT 35 + 0.5'C IN INCUBATOR 21 + 2 HOURS AT 44.5 + 0.2'C IN WATERBATH
COMB. OF
1 SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL POSITIVES MPN/mL' MPN / 100 mLZ
{
C�oM o �2- c) U•�tc-3 4
a � /5mL �l5mL D/5mL 0/5mL � l5mL �lSmL /5mL 15mL
i
DUP /5mL y /5mL
MPN I GRAM'
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN INCUBATOR: 3 i D DATE OUT INCUBATOR: _) 3 , d LY • J
TIME IN INCUBATOR: C (2 - TIME OUT INCUBATOR: , L
INCUBATOR TEMP: L)INCUBATOR TEMP: 3�j , {� O� %TOTAL SOLIDS
�5 • C (ATAD SOLIDS
ANALYSIS t
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: • 13 , DATE OUT WATERBATH 2 1 . l , -1• 4 1
TIME IN WATERBATH: ` l3 TIME OUT WATERBATH Q C
WATERBATH TEMP: WATERBATH TEMP: 5
POSITIVE
NEGATIVE
BLANK MPN Index Value MPN / mL`
CONTROL
CONTROL
MPN ImL, = MPNIGRAM�=
SS A-1 BROTH �(�
i" {G��
Largest Sample Volume % Tot. Solids 4 x 100
DSA-1 BROTH
MPN / 100 mL 2 = (100)(MPN / mL)
FORM UPDATED: DECEMBER 2017
CHECKED BY; LDA•
COPY MADE: (AA

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: • � Z-0 � �, DATE RECEIVED: a 20 , /g
DATE ANALYZED:
TIME COLLECTED: j� TIME RECEIVED:b 73 TIME ANALYZED:
COLLECTED BY: wit rf RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0,5-C. IN INCUBATOR 21 ± 2 HOURS AT 44.5 + 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN ! mL' MPN 1100 mL
POSITNES
14
0 / 5mL �" (�}
f 5mL 0 /5mL O / 5mL � / 5mL t 5mL 15 mL O 15 mt
i
DUP 15 mL
F/5mL
MPN/GRAM
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: , l�J DATE OUT INCUBATOR:
TIME IN INCUBATOR, 110'7 TIME OUT INCUBATOR: 14o
INCUBATOR TEMP: 0 ' INCUBATOR TEMP; U b % TOTAL SOLIDS
(� (ATAD SOLIDS
ANALYSIS''
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH A 3
DATE IN WATERBATH: 9 . 3.a • 1 t' DATE OUT WATERBATH
TIME IN WATERBATH: l`{ L3 J TIME OUT WATERBATH n
WATERBATH TEMP: 4'{-. •� G. WATERBATH TEMP:. a G
POSITIVE
NEGATIVE
BLANK MPN Index Value
CONTROL
CONTROL
MPN /mL'=
SS A-1 BROTH PCs
U
Largest Sample Volume
DS A4 BROTH S
�'-
MPN / 100 ml-2 = (100)(MPN / mL)
MPN/GRAM'=
MPN / mL'
% Tot. Solids" (expressed as a decimal)
CHECKED BY: Lkw
FORM UPDATED: DECEMBER 2017 COPY MADE- w

0
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: DATE.RECEIVED: ��. 1 g DATE ANALYZED: 7.
TIME COLLECTED: O 3n TIME RECEIVED: (���� TIME ANALYZED: oo5q
COLLECTED BY: RECEIVED BY: 41 ANALYZED BY:
METHOD: SM 9221 C- E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2•C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSITIVES MPN/mL' MPN / 100 mLT
GRow, O /5mL l5mL v /5mL O /5mL Z4 /SmL /5mL /5mL ®/5mL
DUP
v /5mL 0I5mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR MPN/GRAM
DATE IN INCUBATOR: , ,� �(• (� DATE OUT INCUBATOR:
TIME IN INCUBATOR: TIME OUT INCUBATOR: 1
INCUBATOR TEMP: 35. 0 o� INCUBATOR TEMP: 3 J oc- %TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)4
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: . -a'� , `V DATE OUT WATERBAT 'j j
13
TIME IN WATERBATH: `�-`p TIME OUT WATERBATH Qcl2S!
WATERBATH TEMP: WATERBATH TEMP: 4¢ . 1
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
rr
DS A-1 BROTHS
FORM UPDATED: DECEMBER 2017
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN 1100 mL ` = (100)(MPN / mL)
MPN / mL'
MPN/GRAM3�
% Tot. Solids ° x 100
CHECKED BY: L,V"
COPY MADE: Lkw

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: ' • / DATE RECEIVED: 3. DATE ANALYZED: ->.,p _ t
TIME COLLECTED: Q� 9 TIME RECEIVED: --j 3 17 TIME ANALYZED: ! 0 Ll
COLLECTED BY: �cas {� RECEIVED BY: LOA ANALYZED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 21 +,2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL
C ko M
/5ml /5mL 15mL 15mL ` ]SmL G7 /SmL O /SmL � /5m
DUP
15mL O ]SmL
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN INCUBATOR: It, ,. ( DATE OUT INCUBATOR: 7j . (p . ( $
TIME IN INCUBATOR: p 5 TIME OUT INCUBATOR:
INCUBATOR TEMP: G INCUBATOR TEMP: 3 E-,
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: S,6.19 DATE OUT WATERBAT
TIME IN WATERBATH: I j TIME OUT WATERBATH oQ 3 S
WATERBATH TEMP: 3 G WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
P
�/
DS A-1 BROTH
FORM UPDATED: DECEMBER 2017
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mt 2 = (100)(MPN / mL)
COMB. OF MPN I mL' MPN 1100 me
POSITIVES
0.)AS I:2,0
MPN IGRAM"
0�>
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSISf
MPN / mL'
MPNIGRAM.3=
°•Tot. SolidS"x 100
CHECKED BY: (,0 )A
COPY MADE: _Up'n

CAMP LEJEUNE WWTP
ATAD SLUDGE -FECAL ANALYSIS
DATE COLLECTED: 3 ,) a DATE RECEIVED: .13 _ DATE ANALYZED: 3.
TIME COLLECTED: ) o U TIME RECEIVED: r 0 15 TIME ANALYZED: Q S
COLLECTED BY: A cost RECEIVED BY: LA)" ANALYZED BY: Lb A
METHOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5-C IN INCUBATOR 21 ± 2 HOURS -AT 44.5 ± 0.2-C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL �.vmo. WE- MPN/mL' MPN / 100 mL2
p� POSITIVES ` 3 I
0 /5mL � /5mL � /SmL © /5mL 0 15mL � /5mL ©5mL �/5mL O ~ o ~ O 0.O[�D` i • 803
DUP c )
/5mL 0. JSmL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: 3 13 �� DATE OUT INCUBATOR:
TIME IN INCUBATOR: C 0 JC s TIME OUT INCUBATOR: 3 j
INCUBATOR TEMP: 3 S • p " C INCUBATOR TEMP: s. G
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: _ `3� l� DATE OUT WATER13AT
TIME IN WATERBATH: ky�� TIME OUT WATERBATH 110
WATERBATH TEMP: C E _ WATERBATH TEMP:
POSITIVE
CONTROL
NEGATIVE
CONTROL
BLANK
MPN Index Value
MPN/mL'=
P
SS A-1 BROTH
Largest Sample Volume
DS A-1 BROTH
f
r/
j`1
MPN / 100 mL z = (100)(MPN / mL)
FORM UPDATED: DECEMBER 2017
MPN/GRAMS=
MPN/GRAM'
0. 6 / SY
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS�
,7 93
MPN / mL'
% Tot. Solids ° x 100
CHECKED BY: I�
COPY MADE: Id

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: limic.n=UruvQU: ------ .
TIME COLLECTED: px, L TIME RECEIVED: TIME ANALYZED: c)g SO
COLLECTED BY: Spa RECEIVED BY: ANALYZED BY:
METHOD: SM9221C_E-2006 (MULTIPLE TUBE FERMENTATION]
3 HOURS.AT 35±0.5'C IN INCUBATOR 21 ±2 HOURS AT 44.5± 0.2'C IN WATERBATH
COMB. OF
SAMPLE LOCATION 10 mL 1 mL 0.10 mL: 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL POSITIVES MPN ! mL' MPN / 100 mL'
% ^ �i'1 p .03 '�%
�12dM v /5mL 15ML /5mL 15ML 15ML " I5mL LJ /bmL l/ /smt `w� �i -3. 1
DUP i% IsmL
/5mL
MPN/GRAM'
3 HOURS AT 35 + 0.5"C IN INCUBATOR
DATE IN INCUBATOR: ?j— zQ (� DATE OUT INCUBATOR:
TIME IN INCUBATOR: 0 1 TIME OUT INCUBATOR: 1 -z
INCUBATOR TEMP: �j _ (� %TOTAL
SOLIDS
INCUBATOR TEMP: 3 � , !'� (ATAD SOLIDS
ANALYSIS ,
21 ± 2 HOURS AT 44.5 + 0.2°C IN WATERBATH Q./^
DATE IN WATERBATH: -3 - -21D` 1 Q DATE OUT WATERBATF
TIME IN WATERBATH: 2 TIME OUT WATERBATH c" Z
WATERBATH TEMP: WATERBATH TEMP: LA'A
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DSA-1 BROTH
Il�
MPN Index Value
MPN /mL'=
Largest Sample Volume
MPN / 100 mL 2 = (100)(MPN ! mL)
FORM UPDATED: DECEMBER 2017
MPN / GRAM
MPN/mL'
%Tot-Sollds' x 100
CHECKED BY: I+
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
Y
:i DATE COLLECTED: . Z DATE RECEIVED: �j . Z'j . ► $ DATE ANALYZED:
TIME COLLECTED: Z �} TIME RECEIVED: V -7 q cj TIME ANALYZED:
Lor ;.z7.la
I
,j COLLECTED BY: �3 RECEIVED BY: Leg ANALYZED BY:
METHOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 * 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 + 0.2-C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10•mL 0.010 mL COMB. OF MPN / mL' MPN / 100 mL!
{ POSITIVES
i
o o C� b
C•teo M /5mL 15mL 15mL /5mL /5mL /5mL /5mL /5mL
I
DUP
O 15mL /5mL
MPN/'GRAMS
3 HOURS AT 35 + 0.5°C IN INCUBATOR
Vl cow
DATE IN INCUBATOR: DATE OUT INCUBATOR: 3. 2'7, I
3- 71-7- 1$'�"'
TIME IN INCUBATOR: g ?�� TIME OUT INCUBATOR: Lf
INCUBATOR TEMP: ° INCUBATOR TEMP: %TOTAL SOLIDS
�j S , T) C (ATAD SOLIDS
ANALYSIS�
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: 3 , 2� I Q DATE OUT WATERBAT 3- 21'- I $
TIME IN WATERBATH: 11149 TIME OUT WATERBATH t t
WATERBATH TEMP: L f q 5 G WATERBATH TEMP: ------------
POSITIVE NEGATIVE BLANK MPN Index Value MPN / mL'
CONTROL CONTROL MPN /mL'= MPN/GRAMS=
SS A-1 BROTH Largest Sample Volume % Tot. SolldS ° x 100
DS A-1 BROTH N
MPN / 100 ml- s = (100)(MPN / mL) CHECKED BY:
COPY MADE:
FORM UPDATED: DECEMBER 2017 L1DN

CAMP LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALYSIS
TART -UP
ATE
1 /25/2018
A
B
C
D
E
F
G
H
I
J
TOTAL
VOLATILE
SOLIDS
ASH
SOLIDS
INHOUSE
WTOF
SAMPLE
WTOF
WEIGHT
%TOTAL
WTOF
WEIGHT
WEIGHT
%VOLATILE
%VOLATILE
SAMPLE
ATAD
WTOFDISH
DISH+WET
WEIGHT (g)
DISH+DRY
(g)
SOLIDS
DISH+ASH
(9)
(g)
SOLIDS
WEEKLY
SOLIDS
TEMP
DATE
DIGESTION
(g)
SOLIDS (g)
[H-A]
SOLIDS (g)
[D-A]
[(E/C)X100]
(g)
[G-A]
[E-H]
[(UE)X100]
AVERAGE
REDUCTION
0°C
1/26/2018 I.H. ATAD 74.3156 79.32 5.00 74.4111 0.0955 1.91 74.3618 0.0462 0.0493 51.62 51.74 13.3
DUP 49.6892 54.68 4.99 49.7837 0.0945 1.89 49.7347 0.0455. 0.049 51.85
2/2/2018
I.H. ATAD
49.6900
54.69
5.00
49.7805
0.0905
1.81
49.7329
0.0429
0.0476
52.60
52.46
-1.39
16.7
DUP 73.5929 78.59 5.00 73.6835 0.0906 1.81 73.6361 0.0432 0.0474 52.32
2/9/2018
I.H. ATAD
74.3185
79.32
1 5.00
74.4075
0.0890
1.78
74.361
0.0425
0.0465
52.25
51.29
2.23
21.5
DUP 74.6150' 79.62 5.01 74.7070 0.0920 1.84 74.6607 0.0457 0.0463 50.33
2/15/2018
I.H. ATAD
73.5931
78.59
5.00
73.6681
0.0750
1.50
73.6276
0.0345
0.0405
54.00
54.01
-5.30
23.3
DUP 73.2859 78.29 5.00 73.3607 0.0748 1.49 73.3203 0.0344 0.0404 54.01
2/23/2018
I.H. ATAD
72.3081
77.31
5.00
72.3757
0.0670
1.34
72.3407
0.032
0.035
52.24
52.23
3.29
23.6
.DUP 74.3169 79.32 5.00 74.3822 0.0653 1.31 74.3481 0.0312 0.0341 1999
3/2/2018
I.H. ATAD
72.3111
1 77.31
5.00 1
72.3805
1 0.0694
1 1.39 1
72.3446 1
0.0335
0.0359
51'.73
51.80
0.83
20.9
DUP
75.5263 1
80.53
5.00 1
75.5959
1 0.0696
1.39 1
75.5598
0.0335
0.0361
51.87.
i ..d..x•�. I
VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100
INITIAL VS. (VSR <15%)

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
4/1/2018
42
38.7
38
4/2/2018
60,000
41
37.9
4/3/2018
-
4/4/2018
4/5/2018
4/6/2018
4/7/2018
4/8/2018
4/9/2018
4/10/2018
4/11/2018
4/12/2018
4/13/2018
4/14/2018
4/15/2018
4/16/2018
4/17/2018
4/18/2018
4/19/2018
4/20/2017
4/21/2017
4/22/2017
4/23/2017
4/24/2017
29.7
4/25/2017
33.1
4/26/2017
37.2
4/27/2017
43.3
4/28/2017
50.5
4/29/2017
57
4/30/2017
51.6
39.3
Total =
60,000
385
116
0
Ave=
2,000
42.8
38.6
0
Max=
60,000
57
39.3
0
Min=j
0
29.7
37.9
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
.Fecal
(MPN)
5/1/2018
49.9
58.5
5/2/2018
60.2
61.3
5/3/2018
63.7
60.6
5/4/2018
61.5
59.2
5/5/2018
59.4
57.8
5/6/2018
57.9
56.4
5/7/2018
13,500
53.3
55.4
5/8/2018
57.5
54.4
5/9/2018
13,500
56.9
53.6
5/10/2018
58.9
52.6
5/11/2018
18,000
55.1
53
5/12/2018
59.8
53.3
5/13/2018
61.5
52.3
5/14/2018
60.2
51.2
5/15/2018
18,000
52.5
52.4
0.5
5/16/2018
58.6
53.8
5/17/2018
18,000
55.7
56.3
5/18/2018
57.2
57.4
5/19/2018
65.2
56.1
5/20/2018
64.6
54.8
5/21/2018
62.4
53.4
5/22/2018
18,000
59.4
53.3
5/23/2018
62.3
52.7
5/24/2018
18,000
58.8
53.3
5/25/2018
63.3
53.8
5/26/2018
63.9
53.4
5/27/2018
62.3
52.5
5/28/2018
60.2
51.3
5/29/2018
18,000
56.9
51.7
1.8
5/30/2018
18,000
59.6
52.9
5/31/2018
53.9
55.3
Total =
153,000
1,832
1,694
2
Ave=
4,935
59.1
54.6
1.2
Max=
18,000
65.2
61.3
1.8
Min=j
0
49.9
51.2
0.5

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
6/1/2018
58.2
57.7
6/2/2018
64.1
57.2
6/3/2018
64
56.2 ,
6/4/2018
18,000
59
56.7
6/5/2018
61.8
57
6/6/2018
18,000
59.5
57.8
6/7/2018
63.3
62.9
6/8/2018
63.8
56.6
6/9/2018
62.2
55.4
6/10/2018
60.2
54.2
6/11/2018
58.3
53.1
6/12/2018
56.9
51.5
6/13/2018
56
50.3
6/14/2018
55
49.3
6/15/2018
53.6
48.4 .
6/16/2018
52.5
47.5
6/17/2018
51.7
46.7
6/18/2018
51.1
46.2
6/19/2018
50.6
46
6/20/2018
50.2
46.1
6/21/2018
50.1
45.8
6/22/2018
49.4
45.6
6/23/2018
48.6
44.9
6/24/2018
47.7
45
6/25/2018
46.9
44.5
6/26/2018
45.7
43.9
6/27/2018
44.4
43.1
6/28/2018
43.4
42.3
6/29/2018
42.5
41.5
6/30/2018
41.8
40.8
Total =
36,000
1,613
1,494
0
Ave=
1,200
53.8
49.8
0
Max=
18,000
64.1
62.9
0
Min=j
0
41.8
40.8
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
4/1/2018
36.8
4/2/2018
60,000
45.9
4/3/2018
60.3
4/4/2018
66.5
4/5/2018
65.6
4/6/2018
67.7
4/7/2018
65.4
4/8/2018
62.2
4/9/2018
44.8
40
4/10/2018
18,000
43.5
60
4/11/2018
54.4
54.4
4/12/2018
63.5
65.3
4/13/2018
69.4
62.3
4/14/20181
69.2
61.6
4/15/2018
68.4
60.6
4/16/2018
65.2
59-
4/17/2018
61.3
58.2
4/18/2018
58.5
55.9
4/19/2018
57.3
54.7
4/20/2017
53.5
53.3
4/21/2017
53
51.9
4/22/20171
50.8
52
4/23/2017
49.9
51.4
4/24/2017
49
50
4/25/2017
48.7
48.7
4/26/20171
48.2
48
4/27/2017
47.5
47.3
4/28/2017
46.7
46.6
4/29/2017
45.7
45.8
4/30/20171
44.4
45.1
Total =
78,000
1,663
1,173
Ave=
2,600
55.4
53.3
Max=
1 60,000
69.4
65.3
Min=l
0
1 36.8
40

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
5/1/2018
43.5
44.6
5/2/2018
42.5
44
5/3/2018
5/4/2018
5/5/2018
5/6/2018
5/7/2018
29.5
5/8/2018
35
5/9/2018
43.6
5/10/2018
53.7
5/11/2018
64.3
5/12/2018
68.7
5/13/2018
69.8
5/14/2018
67.5
5/15/2018
66.o
5/16/2018
65.4
5/17/2018
63.1
5/18/2018
59.7
5/19/2018
57.4
5/20/2018
54.1
5/21/2018
51.3
5/22/2018
49.8
5/23/2018
49
5/24/2018
47.6
5/25/2018
46.3
5/26/2018
45.2
5/27/2018
44.4
5/28/2018
43.6
5/29/2018
42.8
5/30/2018'
60,000
42.1
5/31/2018
Total =
60,000
1,345
Ave=
1,935
51.7
89
Max=
60,000
69.8
44.3
Min=
0
29.5
44

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
6/1/2018
6/2/2018
6/3/2018
6/4/2018
6/5/2018
6/6/2018
6/7/2018
6/8/2018
32
6/9/2018
41
6/10/2018
51.5
6/11/2018
61.3
6/12/2018
61.9
6/13/2018
62.7
6/14/2018
60.2
6/15/2018
58.1 .
6/16/2018
56.6
6/17/2018
55.6
6/18/2018
45.8
44.6
6/19/2018
48.5
52.8
6/20/2018
57.7
53.3
6/21/2018
18,000
59.8
54.6
6/22/2018
18,000
60.3
57.2
6/23/2018
61.9
59.3
6/24/2018
61.6
58.5
6/25/2018
58.2
58.2
6/26/2018
18,000
58.2
58.8
1.2
6/27/2018
60.1
58.8
6/28/2018
46.9
51.7
6/29/2018
49.7
54.8
6/30/2018
57.5
55.8
Total =
54,000
1,267
718
1
Ave=
1,800
55.1
55.2
1.2
Max=
18,000
62.7
59.3
1.2
Min=
0
32
44.6
1.2

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
4/1/2018
67.7
66.2
4/2/2018
18,000
58.9
65.6
4/3/2018
18,000
59.7
66.5
0.67
4/4/2018
18,000
61.1
68.8
4/5/2018
18,000
61.2
69.9
4/6/2018
68
72.4
4/7/2018
71.3
70.5
4/8/2018
70.9
67.2
4/9/2018
18,000
67.1
65.1
4/10/2018
18,000
68
64.9
51.1
4/11/2018
18,000
67.3
65.2
4/12/2018
- 18,000
66
64.4
4/13/2018
18,000
65.4
68.2
4/14/2018
69.2
69.6
4/15/2018
68.2.
68.3
4/16/2018
18,000
60.1
66.1
4/17/2018
18,000
59.9
64.9
1.8
4/18/2018
18,000
60.7
66.2
4/19/2018
18,000
62.6
68.6
4/20/2018
68.1
69.1
4/21/2018
68.8
67.1
4/22/20181
67.4
65.1
4/23/2018
18,000
60
.64
4/24/2018
18,000
60.9
66.4
1.8
4/25/2018
18,000
60.4
67.6
4/26/2018
18,000
61.8
69
4/27/2018
18,000
62.4
71.2
4/28/2018
67.7
71.1
4/29/2018
69
68.7
4/30/2018
18,000
61.3
68.7
Total =
342,000
1,941
2,024
55
Ave=
111400
64.7
67.5
13.9
Max=
18,000
71.3
72.4
51.1
Min=j
0
58.9
64
0.67

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
5/1/2018
18,000
62.5
67.9
1.8
5/2/2018
18,000
64.7
69.7
5/3/2018
13,500
65.5
71
5/4/2018
70
71.3
5/5/2018
70.1
69
5/6/2018
69
66.2
5/7/2018
13,500
61.6
64.6
5/8/2018
68.7
65
1.8
5/9/2018
67.4
63.6
5/10/2018
13,500
62.7
63.1
5/11/2018
63.8
62.8
5/12/2018
61.8
61.9
5/13/2018
59.2
61.1
5/14/2018
18,000
54.8
60.4
5/15/2018
59.6
61.2
5/16/2018
'18,000
58.7
62.3
5/17/2018
63.5
63.3
5/18/2018
64.5
62.7
5/19/2018
63.1
61.4
5/20/2018
60.9
60
5/21/2018
18,000
56.1
59.6
5/22/2018
61.9
60.7
5/23/2018
18,000
50.7
61.8
5/24/2019
65.2
63
5/25/2018
18,000
61.8
64.1
5/26/2018
- 59.4
65.8
5/27/2018
59
65.1
5/28/2018
65.1-
63.8
5/29/2018
66.7
62.8
5/30/2018
62.4
63.5
5/31/2018
18,000
65.2
64.4
Total =
184,500
1,955
1,983
4
Ave=
5,952
63.1
64
1.8
Max=
18,000
70.1
71.3
1.8
Min=j
0
54.8
59.6
1.8

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
6/1/2018
66.1
64.9
6/2/2018
64.4
64.2
6/3/2018
62.5
62.9
6/4/2018
18,000
55.8
62.2
6/5/2018
18,000
558.8
63
1.18
6/6/2018
64.6
65
6/7/2018
18,000
64.7
64.6
6/8/2018
62.4
63.4
6/9/2018
63
62.1
6/10/2018
62.4
60.7
6/11/2018
62.3
59.6
6/12/2018
61.1
58.6
1.18
6/13/2018
59.
56.7
6/14/2018
57
55.3
6/15/2018
55.8
53.9
6/16/2018
54.7
52.8
6/17/2b18
53.8
52.1
6/18/2018
53.1
52.1
6/19/2018
54.7
52.4
1.4
6/20/2018
54.7
52.3
6/21/2018
53.6
51.7
6/22/2018
55.1
51.7
6/23/2018
56.7
51.8
-6/24/2018
56.7
51.6
6/25/2018
55.6
51.2
6/26/2018
55.1
51
6/27/2018
54.6
50.7
6/28/2018
60,000
59.3
57.7
6/29/2018
57.4
56.8
6/30/2018
55.5
56
Total =
114,000
1,750
1,709
5
Ave=
3,800
58.3
57
1.7
Max=
60,000
66.1
64.9
1.8
Mind
0
53.1
57.7
1.4

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
4/1/2018
4/2/2018
4/3/2018
4/4/2018
4/5/2018
4/6/2018
4/7/2018
4/8/2018
4/9/2018
4/10/2018
4/11/2018
4/12/2018
4/13/2018
4/14/2018
4/15/2018
4/16/2018
4/17/2018
4/18/2018
4/19/2018
4/20/2017
4/21/2017
4/22/2017
4/23/2017
4/24/2017
4/25/2017
4/26/2017
4/27/2017
4/28/2017
4/29/2017
4/30/2017
Total =
Ave=
Max=
Min=

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date - .
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
5/1/20.18
5/2/2018
5/3/2018
5/4/2018
5/5/2018
5/6/2018
5/7/2018
5/8/2018
5/9/2018
5/10/2018
5/11/2018
5/12'/2018
5/13/2018
5/14/2018
5/15/2018
5/16/2018
5/17/2018
5/18/2018
5/19/2018
5/20/2018
5/21/2018
5/22/2018
5/23/2018
5/24/2018
5/25/2018
5/26/2018
5/27/2018
5/28/2018
5/29/2018
5/30/2018
5/31/2018
Total =
'
Ave=
Max=
Min=

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
6/1/2018
6/2/2018
6/3/2018
6/4/2018
6/5/2018
6/6/2018
6/7/2018
6/8/2018
6/9/2018
6/10/2018
6/11/2018
6/12/2018
6/13/2018
6/14/2018
6/15/2018
6/16/2018
6/17/2018
6/18/2018
6/19/2018
6/20/2018
6/21/2018
6/22/2018
6/23/2018
6/24/2018
6/25/2018
6/26/2018
6/27/2018
6/28/2018
6/29/2018
6/30/2018
Total =
Ave=
Max=
Min=

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED; DATE RECEIVED: 4;-'�, { b DATE ANALYZED: 4 3• I
TIME COLLECTED: Ste- TIME RECEIVED: o aJ Lo TIME ANALYZED:
COLLECTED BY: RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2-C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL I 1 mL I 0.10 mL 10.010 mL pOSITI ES I COMB. OF MPN / mL1 I MPN / 100 mLzi
g C)IAI 0 / 5
DUP ID
/5
0 / 5 mLl D / 5 mLi . / 5 mLl O / 5 mLl 015
/ 5 rtiL
O15md v /5
3 HOURS AT 35 + 0.5*C IN INCUBATOR
DATE IN INCUBATOR: 4, '�. ( DATE OUT INCUBATOR:
TIME IN INCUBATOR: 06(`,'--TIME OUT INCUBATOR: l a`
INCUBATOR TEMP: INCUBATOR TEMP:-L7
21 ± 2 HOURS AT 44.5 +-0.2°C IN WATERBATH
DATE IN WATERBATH: .�f, t� DATE OUT WATERBAT
TIME IN WATERBATH: TIME OUT WATERBATH t7'YJ�
WATERBATH TEMP: L� _ WATERBATH TEMP:
POSITIVE
CONTROL
NEGATIVE
CONTROL
BLANK
MPN Index Value
MPN/mL'=
f SS A-1 BROTH
j
Largest Sample Volume
p C�
DS A-1 BROTH
j 1
t
FORM UPDATED: DECEMBER 2017
v v
MPN / 100 mL z = (100)(MPN / mL)
0. o. o f/- 0.1. e)o3 r .03
0. of 005
MPN / GRAM3
0 • tY
MPN/GRAMS
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS'
MPN / mL'
% Tot, Solids ° x 100
CHECKED BY: L171�
COPY MADE: (��

CAMP LEJEUNE WWTP
ATAC SLUDGE FECAL ANALYSIS
DATE COLLECTED: �/ , ! ,� C DATE RECEIVED:
TIME COLLECTED: 02 2.- S TIME RECEIVED: 075-0
COLLECTED BY: RECEIVED BY: Q,
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
DATE ANALYZED: 4 - W • L!
TIME ANALYZED:
ANALYZED BY:
3 HOURS AT 35 + 0,5•C IN INCUBATOR
21 + 2 HOURS AT 44.5 + 0.21C IN WATERBATH
SAMPLE LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
COMB. OF
MPN/mL'
MPN 1100 mL2
POSITIVES
CR-0
O
D
="' '
�}
�i
t� 0I
bp�
/5ml-
/5mL
l5ml.
15mL
15ml.
t5mL
15mL
Y tSmt-
DUP
f5mL
1
15mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: 10, (& DATE OUT INCUBATOR: L#.. j 0, t9
TIME IN INCUBATOR: 050b TIME OUT INCUBATOR: 1108
INCUBATOR TEMP: 13, v INCUBATOR TEMP: 3
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: 1 t 0 DATE OUT WATERBAT (`, t
TIME IN WATERBATH: TIME OUT WATERBATH
WATERBATH TEMP: �•I�'� - � WATERBATH TEMP: A-4.
POSITIVE
NEGATIVE
CONTROL
CONTROL
BLANK
SS A-1 BROTH
DS A-1 BROTH
L/ [%
FORM UPDATED: DECEMBER 2017
MPNImL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL 2 = (100)(MPN I mL)
MPN I GRAMS
01
`h TOTAL SOLIDS
(ATAD SOLIDS
ANALYSISf
MPN l mL'
MPNIGRAM3=
% Tot. Solids 4 x 100
CHECKED BY: GOP
COPY MADE: L1,0 IS

CAMP LEJEUNE WWTP -
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 7 I DATE RECEIVED: 4. [ _ t 0 -DATE ANALYZED:
. 1
TIME COLLECTED: (� TIME RECEIVED: p TIME ANALYZED:
COLLECTED BY: RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH I rSAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN / mL' MPN / 100 m!2
POSITIVES
cM D l 5 mL ! 5 mL 0 l 5-ml. / 5mL D 15mL "/ 5mL D 15 mL 0 f 5 mL
OUR 0-
J
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: �i, DATE OUT INCUBATOR:
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP: `�s.(� INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 +,0.20C IN WATERBATH
DATE IN WATERBATH:.. - �. DATE OUT WATERBAT
TIME IN WATERBATH: 1 Eros TIME OUT WATERBATH 0�
WATERBATH TEMP: 7 WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
�(�
DS A-1 BROTH
p [�
FORM UPDATED: DECEMBER 2017
MPN/mL'=
MPN Index Value
Largest Sample Volume
U U MPN / 100 ML2 = (100)(MPN / mL)
MPN/GRAM'
(ATAD SOLIDS
ANALYSIS14
�)L'-,qD
MPN /ML'
MPN/GRAM'=
Flo Tot. Solids ° x 100
CHECKED BY:
COPY MADE:
j

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE.COLLECTED: I j- Z �j . el9 DATE RECEIVED:
TIME COLLECTED: ) 610 TIME RECEIVED:
COLLECTED BY: S a RECEIVED BY:
y METHOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2•C IN WATERBATH
d
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL
0 /5mL /5mL /5mL O/5mL Q 15mL " /5mL 0 /5mL 15mL
I
DUP
/5mL /5mL
i
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: DATE OUT INCUBATOR:
TIME IN INCUBATOR: TIME OUT INCUBATOR: OCI
INCUBATOR TEMP: �j�j-(� INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2*C IN WATERBATH
DATE IN WATERBATH: ,'Y l DATE OUT WATERBAT J
TIME IN WATERBATH: C TIME OUT WATERBATH01l,�
WATERBATH TEMP: ,L� WATERBATH TEMP:
POSITIVE
CONTROL.
NEGATIVE
CONTROL
BLANK
SS A-1 BROTH
S
DS A-1 BROTH
US
v
FORM UPDATED: DECEMBER 2017
MPN / mL' =
MPN Index Value
Largest Sample Volume
MPN / 100 mL a = (I00)(MPN / mL)
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
COMB. OF MPN / mL' MPN / 10
POSITIVES
o- o
MPN/GRAM
a-$
(ATAD SOLIDS
ANALYSIS)4
MPN / ML'
MPN / GRAM 3 =
% Tot. Solids 4 x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: t DATE RECEIVED: Gj - 1 j DATE ANALYZED:
r8
TIME COLLECTED: 0 C TIME RECEIVED:_ �O� TIME ANALYZED:
COLLECTED BY: GtJ�Gt�t � RECEIVED BY:
ANALYZED BY:
METHOD: SM 9221C E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5•C IN INCUBATOR 21 + 2 HOURS AT 44.5+ 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN I mL' MPN 1100
POSITIVES
0 1 . 5mLl 015mL 0 /5mL Q /5mL � /5mL () 15mL D15ML, O /5mL �f O'C) � OD
DUP
1015
3 HOURS AT 35 + 0.5°C IN INCUBATOR
0 /5
DATE IN INCUBATOR:- ! . �j DATE OUT INCUBATOR:
{ TIME IN INCUBATOR: Q TIME OUT INCUBATOR: t
INCUBATOR TEMP. 3S. O INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: �, ! IS DATE OUT WATERBAT
TIME IN WATERBATH: l '3 3 TIME OUT WATERBATH t
WATERBATH TEMP: �- WATERBATH TEMP:
POSITIVE
CONTROL
NEGATIVE
CONTROL_
BLANK
SS A-1 BROTH
f�'&
DS A-1 BROTH
FORM UPDATED' DECEMBER 2017
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL' = (100)(MPN / mL)
0,01 g0'3
1ait S-71W
MPNIGRAM'
0• I
(ATAD SOLIDS
ANALYSISe
,�,.D9
MPN / mL'
MPNIGRAM'=
% Tot. Solids' x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 5 , 1 o DATE RECEIVED: S, 13 • 16 DATE ANALYZED: 5 - 6? • t U
TIME COLLECTED: ZS TIME RECEIVED: Q �j y TIME ANALYZED: 093o
COLLECTED BY: �U RECEIVED BY: ANALYZED BY: DES'
METHOD; SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5'C IN INCUBATOR 21 ± 2 HOURS AT ".5 + 0.21C IN WATERBATH
COMB. OF
SAMPLE LOCATION 10 mL 1 rnL 0.10 mL 0.010 mL 10 mL 1 mL 0.10, mL 0.010 mL POSITIVES MPN 1 mL° MPN / 100 mL2
015mL t 5ml /5 /5 mL 15 mL
D O 0 15mL 0 15mL v 15mL
r:L `
DUP 0 15 mL D 15 mL
MPN / GRAM3
3 HOURS AT 35 + 0.5°C IN INCUBATOR {
DATE IN INCUBATOR: �5 . 60. 19 DATE OUT INCUBATOR: �. Lq
TIME IN INCUBATOR: C)94� TIME OUT INCUBATOR: t 14 q
INCUBATOR TEMP: O INCUBATOR TEMP: - ;r ��- ` o/(ATAD SOL.IDSTOTAL S
ANALYSIS 4
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: 6 . C0 • 13 DATE OUT WATERBATH
TIME IN WATERBATH: TIME OUT WATERBATH 09
WATERBATH TEMP: 44WATERBATH TEMP: 1+4 . ,S
POSITIVE
CONTROL
NEGATIVE
CONTROL
BLANK
SS A-1 BROTH
N
DS A-1 BROTH
���j`r�
tQ
FORM UPDATED: DECEMBER 2017
MPN ImL1=
MPN Index Value
Largest Sample Volume
MPN 1100 mL2 = (100)(MPN I mL)
MPN / mL'
MPNIGRAM'=
% Tot. Solids ° x 100
CHECKED BY: _ /Hit
COPY MADE: 14611`

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: :5-(;-Wig DATE RECEIVED: 15 3 DATE ANALYZED: Ga. 1 S • 1 v
TIME COLLECTED: (9fz-0 TIME RECEIVED: TIMEANALYZED: O030
COLLECTED BY: tclll.�l9�rr RECEIVED BY:ANALYZED BY: •D v'
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5°C 1N INCUBATOR
DATE IN INCUBATOR:
TIME IN INCUBATOR:
INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH:
TIME IN WATERBATH:
WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
pNf6
...hjfK
FORM UPDATED: DECEMBER 2017
DATE OUT INCUBATOR:
TIME OUT INCUBATOR:
INCUBATOR TEMP:
DATE OUT WATERBA'
TIME OUT WATERBAI
WATERBATH TEMP:
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL 2 = (100)(MPN / ml-)
MPN 1100
o so
MPN/W
MPN/GRAM'=
% Tot. Solids 4 x 100
CHECKED BY: to
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: j L 1If DATE RECEIVED: . ZZ-lg DATE ANALYZED: 5 • Z7
TIME COLLECTED: -7 TIME RECEIVED: TIME ANALYZED:
COLLECTED BY: � � RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.51C IN INCUBATOR 21 + 2 HOURS AT 44.5 + 0.2•C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL POSITIVES
1 mL 0.10 mL 0.010 mL COMB. OF MPN I ML' MPN I i00 ML2
p 0 o O Q O ov.ut,9a3 I.fo?7
C Rory /5mL lSmL /5mL lSmL lSmL i5ml. lSmL rSmL
DUP pl5mL l5mL
MPNIGRAM3
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: S - Z 2 _ t 5 DATE OUT INCUBATOR: C.,y�� . ��
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP. INCUBATOR TEMP: LL-- - % tOTAL SOLIDS
3 7 -� (ATAD SOLIDS
ANALYSIS)
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH v�
DATE IN WATERBATH: DATE OUT WATERBATH 5. )'3 , t U
TIME IN WATERBATH: TIME OUT WATERBATH 00 3L
WATERBATH TEMP: 44 WATERBATH TEMP:
POSITIVE
CONTROL
NEGATIVE
CONTROL
BLANK
SS A-1 BROTH
-
\
�V
DS A-1 BROTH
��
FORM UPDATED: DECEMBER 2017
MPN Index Value
MPN /mL'=
Largest Sample Volume
MPN / 100 ML' = (100)(MPN / ml-)
MPN/GRAM'=
MPN / mL'
% Tat. Solids ° x 100
CHECKED BY: Ld W
COPY MADE. tAW

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: s Zq� a DATE RECEIVED: �. 2a . I 'c DATE ANALYZED: , �-ci . ( 6
TIME COLLECTED: 7 g TIME RECEIVED: U -7 S TIME ANALYZED: ( C)C-)U
COLLECTED BY: W IAs RECEIVED BY: OES ANALYZED BY.wf
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 + 0.5-C IN INCUBATOR 1 21 + 2 HOURS AT 44.5 + 0.2•C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN/mL' MPN/10
POSITIVES
GD�IM '�kt�l f� v — c)
O /5m! vDUP /5mL f5mL fSmL O l5mL O /SmL JSmL ISmL
l I C,
/5mL I /5mL
MPN/GRAM'
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: 5. �q , (`3 DATE OUT INCUBATOR:
TIME IN INCUBATOR: 1010 TIME OUT INCUBATOR:
INCUBATOR TEMP:' . ' G INCUBATOR TEMP: 1js , %TOTAL 54LIDS
(ATAD SOLIDS
ANALYSISI
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: DATE OUT WATERBATH
TIME IN WATERBATH: t l7 TIME OUT WATERBATH Q t7
WATERBATH TEMP: 44WATERBATH TEMP:
POSITIVE
CONTROL
NEGATIVE
CONTROL
BLANK
SS A-1 BROTH
oS
N 6
DS A-1 BROTH
Q 5
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL Z = (100)(MPN / mL)
MPN/GRAMM =
MPN / mL'
% Tot. Solids : x 100
CHECKED BY:
UA-
FORM UPDATED' DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: C,' ;K DATE RECEIVED: 6 / S//,5-- DATE ANALYZED:
TIME COLLECTED: S-D TIME RECEIVED: Ols/U TIME ANALYZED: 08jU
COLLECTED BY: ` RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C-E - 2006 (MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 1 21 ± 2 HOURS AT 44.5 ± 0.2•C IN WATERBATH
SAMPLE LOCATION I 10 mL :I 1 mL I 0.10 mL 10.010 mL 10 mL I 1 mL I 0.10 mL 10.010 mL POSITIVES
MB.OF I MPN / mL' { MPN / 10
0 /5mL4 C-D/5mLI OiSmLl 0 /51nj `s ;5
DUP 10 /5mLI I I 10 +5
0 i5md v 15md 0 /5mLI 6 -c — D
3 HOURS AT 35 + 0.5°C IN INCUBATOR,
DATE IN INCUBATOR: �y S - /� DATE OUT INCUBATOR:
TIME IN INCUBATOR: (.'t�`�� TIME OUT INCUBATOR: I �/
INCUBATOR TEMP: 3 (� INCUBATOR TEMP: :? I
21 + 2 HOURS AT 44.5 +•0.2°C IN WATERBATH
DATE IN WATERBATH: cJ — DATE OUT WATERBAT r
TIME IN WATERBATH: TIME OUT WATERBATH S 3
WATERBATH TEMP: 7 7 WATERBATH TEMP: (_
POSITIVE
NEGATIVE
CONTROL
CONTROL
BLANK
SS A-1 BROTH
n }
DS A-1 BROTH
P
FORM UPDATED: DECEMBER 2017
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL` = (100)(MPN / mL)
MPN / GRAM =
tM frN•11S I _t•R► 1
0.(ASD3 I•$c
MPN / GRAM'
IW
1.01
4i
(ATAD SOLIDS
ANALYSIS)'
MPN / mL'
% Tat. Solids" x 100
CHECKED BY: t4DYt
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: �, Z DATE RECEIVED: �, / DATE ANALYZED:
TIME COLLECTED: TIME RECEIVED:, p p TIME ANALYZED: �(�Q
COLLECTED BY: RECEIVED BY: ANALYZED BY:
METHOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± D•5•C IN INCUBATOR 21 -± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN / mL' MPN / 1Q0
POSITIVES
Dtrk/, I o;5md 111-)/5ind V.i5mLI 0 15mL, U /5mLl 015md c- /5inLl 0 /5
DUP 1 /// 5 mLl I I I v i 5
3 HOURS AT 35 + 0.5°C IN INCUBATOR
j DATE IN INCUBATOR: DATE OUT INCUBATOR: 4 �� Z
TIME IN INCUBATOR: TIME OUT INCUBATOR: 3 ; J�
INCUBATOR TEMP: J f�INCUBATOR TEMP:
j 21 + 2 HOURS AT 44.5 +•0.2°C IN WATERBATH
DATE IN WATERBATH: — j Z —/ DATE OUT WATERBAT
TIME IN WATERBATH: TIME OUT WATERBATH IL,91&
WATERBATH TEMP: yy `7 WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
fAj
DS A-1 BROTH
FORM UPDATED: DECEMBER 2017
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL2 = (100)(MPN / mL)
0
MPN/GRAMS=
MPN / GRAM'
�«r
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)°
/ Y/
MPN / mL'
% Tot. Solids'' x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: j DATE RECEIVED: �p " `� . Qj DATE ANALYZED:
TIME COLLECTED: TIME RECEIVED: Lr7 US TIME ANALYZED: Oelf)c-)
COLLECTED BY: RECEIVED BY: 'b�S ANALYZED BY:,
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5•C IN INCUBATOR
SAMPLE LOCATION 1 10 mL I 1 mL 1 0.10 mL 1 0.010 mL
0 15mL O ?5mL V r5mL Q 15
DUP D ,r5mL
21 ± 2 HOURS AT 44.5 ± 0.2•C IN WATERBATH
10 mL 1 mL 0.10 mL 0.010 mL COMB. OF
POSITIVES
r5mL 0/5mL D /5mL `' 15mL v 0' ✓
V
f5
3 HOURS AT 35 +0.5°C IN INCUBATOR
i
DATE IN INCUBATOR: l DATE OUT INCUBATOR;
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP: �s INCUBATOR TEMP: �� Q
21 + 2 HOURS AT 44.5 +-0.2°C IN WATERBATH "
DATE IN WATERBATH: 2-0 DATE OUT WATERBAT
TIME IN WATERBATH: t l7j' TIME OUT WATERBATH
WATERBATH TEMP:. WATERBATH TEMP: IT
POSITIVE
NEGATIVE
BLANK
CONTROL
SS A-1 BROTH
D5
,COONTROL
tom+
� -c
DS A-1 BROTH
Q'Ds
FORM UPDATED: DECEMBER 2017
MPN Index Value
MPN /ml-'= MPN/GRAM'=
Largest Sample Volume
MPN / 100 mL? = (100)(MPN / mL)
MPN/mL' I MPN / 101
MPN / GRAM
rA�
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)4
l�lY
MPN / mL'
% Tot. Solids 4 x 100
CHECKED BY:
COPY MADE:
l

DATE COLLECTED: Z tej
TIME COLLECTED: s-
COLLECTED BY: A
CAMP LEJEUNE VW TP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: (.- .1(e ,/ 9
TIME RECEIVED:
RECEIVED BY:
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
DATE ANALYZED:
TIME ANALYZED: ILI S0
ANALYZED BY:
3 HOURS AT 35 + 0,5'C IN INCUBATOR
21 +'2 HOURS AT 44.5 + 0.2•C IN WATERBATH
COMBINATION OF
POSITIVES
MPN / mL'
MPN 1100 MLz
SAMPLE LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL0.010
mL
C�
DUP
15 mL
C /5m!
L/ ! 5 mL
U 15 mL
15 mL
V 15 mL
15mL
6 15 mL
0 5 mL
L� 15 mL
U r CD
MPN TABLE VALUE
p
3 HOURS AT 35 + 0.5°C 1N INCUBATOR
DATE IN INCUBATOR: _ 1 1 DATE OUT INCUBATOR: _ �6
TIME IN INCUBATOR: 7—O TIME OUT INCUBATOR:
INCUBATOR TEMP: 3 Li _ c� . 'C INCUBATOR TEMP: 3 q •C
21 + 2 HOURS AT 44.5 + 0,2°C IN WATERBATH
DATE IN WATERBATH:
TIME IN WATERBATH: ye,
WATERBATH TEMP: 7 7 •C
POSITIVE
NEGATIVE
CONTROL
CONTROL
BLANK
SS A-1 BROTH
DS A-1 BROTH
FORM UPDATED: MARCH 2O18
DATE OUT WATERBAT _ 8
TIME OUT WATERBATH
WATERBATH TEMP: l7 {� J 'C
MPN/mL '=
MPN Index Value
Largest Sample Volume
MPN 1 100 mL 2 = (100)(MPN I ML)
MPN/GRAM
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS
S�
MPN / mL'
MPN I GRAM 3 = x 100
1% Tot. Solids`
CHECKED BY. L*
COPY MADE:

CAMP LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALYSIS
iTART-UP
)ATE
4/13/2018
A
B
C
D
E
F
G
H
1
J
TOTAL
VOLATILE
SOLIDS
ASH
SOLIDS
SAMPLE
DATE
INHOUSE
ATAD
DIGESTION
WTOFDISH
(g)
WT OF
DISH+WET
SOLIDS (g)
SAMPLE
WEIGHT (g)
[B-A]
WT OF
DISH+DRY
SOLIDS (9)
WEIGHT
(g)
[D-A]
%TOTAL
SOLIDS
[(E/C)X700]
WT OF
DISH+ASH
(g)
WEIGHT
(g)
[G-A]
WEIGHT
(g)
[E-H]
%VOLATILE
SOLIDS
[(I/E)X100]
WEEKLY
AVERAGE
% VOLATILE
SOLIDS
REDUCTION
TEMP
0°C
4/16/2018 I.H. ATAD 73.3383 78.34 5.00 73.4326 0.0943 1.89 73.3825 0.0442 0.0501 53.13 26.56 21.8
DUP 73.5963 78.60 5.00 73.6903 0.0940 1.88 73.6903 0.094 0 0.00
4/20/2018
I.H.. ATAD
49.69071
54.69
5.00
49.779
0.0883
1.77
49.7332
0.0425
0.0458
51.87
52.04
-95.90
20.4
DUP 74.6185 79.62 5.00 74.7068 0.0883 1.77 74.660.7 0.0422 0.0461 52.21 ,
4/27/2018
I.H. ATAD
88.6406
93.66
5.02
88.695
0.0544
1.08
88.6662
0.0256
0.0288
52.94
53.09
-2.03
23
DUP 72.3115 77.31 5.00 72.3654 0.0539 1.08 72.3367 0.0252 0.0287 53.25
5/4/2018
I.H. ATAD
88.3467
93.35
5.00
88.3991
0.0524
1.05
88.3719
0.0252
0.0272
51.91
51.77
2.50
22.7
DUP 88.6402 93.64 1 5.00 1 88.6925 1 0.0523 1 1.05 1 88.6655 1 0.0253 1 0.027 1 51.63
5/11/2018
I.H. ATAD
72.3153
77.32
5.00
72.3867
0.0714
1.43
72.3511
0.0358
0.0356
49.06
50.21
3.00
23.2
DUP 72.3131 77.31 5.00 72.3839 0.0708 1.42 72.3481 0.035 0.0358 50.56
5/18/2018
I.H. ATAD
74.3221
7 9. 32
5.00
74.3933
0.0712
1.42
74.3562
0.0341
0.0371
52.11
52.07
-3.71
24:9
DUP
74.6209
79.62
5.00
74.692
0.0711
1.42
74.655
0.0341
0.037
52.04 '
VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100
INITIAL. VS (VSR <15%)

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
7/1/2018
41.2
40.7
7/2/2018
40.7
39.8
7/3/2018
40.3
39.5
7/4/2018
39.9
39.1
7/5/2018
39.7
39.2
7/6/2018
39.5
38.4
7/7/2018
39.2
38.1
7/8/2018
38.5
37:4
7/9/2018
37.5
7/10/2018
39.4
7/11/2018
42.1
7/12/2018
45.3
7/13/2018
48.7
7/14/2018
52.6
7/15/2018
57.6
7/16/2018
61.6
7/17/2018
63.4
7/18/2018
62
7/19/2018
120,000
60.4
7/20/2018
59
7/21/2018
57
7/22/2018
56.1
7/23'/2018
47.2
36.6
7/24/2018
39.1
51.4
7/25/2018
42.6
52.5
7/26/2018
46.9
53
7/27/2018
53.2
52.2
7/28/2018
59.3
51.2
7/29/2018
62.3
50.1
7/30/2018
62.5
49.1
7/31/2018
60.8
48.3
Total =
120,000
1,536
757
0
Ave=
3,871
49.5
44.5
0
63.4
53
0
��Ma�x=120,000
Min=
0
37.5
36.6
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
8/1/2018
59.3
47.9
8/2/2018
58.3
47.4
8/3/2018
56.3
46.4
8/4/2018
54.6
45.6
8/5/2018
52.9
45.2
8/6/2018
51.5
44.9
8/7/2018
50.4
44.7
8/8/2018
49.3
44.4
8/9/2018
48.5
44.2
8/10/2018
48
44.1
8/11/2018
47.6
43.9
8/12/2018
47.3
43.6
8/13/2018
46.9
43.3
8/14/2018
46.5
43.
8/15/2018
46.1
42.7
8/16/2018
45.6
42.2
8/17/2018
44.9
41.7
8/18/2018
44.7
41.6
8/19/2018
44.1
41.4
8/20/2018
43.6
41.2
8/21/2018
43.2
41
.3.1
8/22/2018
42.2
40.8
8/23/2018
42.9
41.3
8/24/2018
44.4
41.7
8/25/2018
45.3
42
8/26/2018
46.2
42.3
8/27/2018
46.8
42.6
8/28/2018
46.7
42.6
8/29/20181
45.9
42.2
8/30/2018
45
41.9
8/31/2018
44.4
41.7
Total =
0
1,479
1,339
3.1
Ave=
0
47.7
43.2
3.1
Max=
0
59.3
47.9
3.1
Min=
0
42.2
40.8
3.1

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
9/1/2018
.43.9
41.4
9/2/2018
43.5
41
9/3/2018
43.2
40.8
9/4/2018
42.8
40.5
9/5/2018
41.8
39.7
9/6/2018
41.7
39.6
9/7/2018
41.4
39.3
9/8/2018
41.1
39.3
9/9/2018
40.9
39.7
9/10/2018
120,000
48.5
38.8
9/11/2018
34.7
35.5
9/12/2018
36.4
38.7
9/13/2018
39.1
43
9/14/2018
41.3
49.2
9/15/2018
44.8
49.2
9/16/2018
48.4
51
9/17/2018
51.3
51.5
9/18/2018
-
53.2
52.3
9/19/2018
54.2
.52.3
9/20/2018
53.7
51.5
9/21/2018
52.7
50.8
9/22/2018
51.7
49.9
9/23/2018
50.5
49.5
9/24/2018
18,000
42.7
48
9/25/2018
38.5
47.2
9/26/2018
41.7
50
9/27/2018
46.8
50.1
9/28/2018
50.7
49.8
9/29/2018
52.7
49.7
9/30/2018
53.4
48.9
Total =
138,000
1,367
1,317
0
Ave=
4,600
45.6
45.4
0
Max=
120,000
54.2
52.3
0
Min=
0
34.7
35.3
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
7/1/2018
53.5
55.2
,
7/2/2018
52.2
54.5
7/3/2018
60,000
46.5
53.3
0.9
7/4/2018
47.4
52.9
7/5/2018
54
52.7
7/6/2018
57.4
52.4
7/7/2018
59.6
51.9
7/8/2018
59
51.1
7/9/2018
57.2
50.3
7/10/2018
55.7
49.8
7/11/2018
54.4
49.5
7/12/2018
52.3
49.2
7/13/2018
49.8
48.5
7/14/2018
47.2
48
7/15/2018
46.3
47.5
7/16/2018
120,000
7/17/2018
7/18/2018
7/19/2018
7/20/2018
7/21/2018
7/22/2018
7/23/2018
7/24/2018
7/25/2018
7/26/2018
7/27/2018
7/28/2018
7/29/2018
7/30/2018
7/31/2018
Total =
180,000
825
767
1
Ave=
5,806
51.6
51.1
0.9
Max=
120,00
59.3
55.2
0.9.
Min=
0
33
47.5
0.9

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
8/1/2018
39.6
8/2/2018
43.7
8/3/2018
47.5
8/4/2018
49.8
8/5/2018
50.4
8/6/2018
50.1
8/7/2018
49.5
8/8/2018
48.8
8/9/2018
47.9
8/10/2018
60,000
43
39.9
8/11/2018
40.5
45.6
8/12/2018
39.5
47.3
8/13/2018
39.1
48.4
8/14/2018
52.5
49
8/15/2018
43.9
49.3
8/16/2018
44.7
49.5
8/17/2018
45.3
49.6
8/18/2018
45.2
49.6
8/19/2018
44.8
49.5
8/20/2018
44.5
49.4
8/21/2018
44
49.2
8/22/2018
8/23/2018
8/24/2018
8/25/2018
8/26/2018
8/27/2018
8/28/2018
35.3
8/29/2018
38.1
8/30/2018
38.1
39.9
8/31/2018
39.1
44.5
Total =
60,000
1,105
660
Ave=
1,935
44.2
47.2
Max=
60,000
52.5
49.6
Min=j
0
35.3
39.9

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
9/1/2018
42.2
47.7
9/2/2018
46.9
49.6
9/3/2018
49.7
50.4
9/4/2018
51.2
50.8
9/5/2018
51.6
51
9/6/2018
51.6
51
9/7/2018
51.2
51
9/8/2018
50.2
51
9/9/2018
49.3
50.9
9/10/2018
48.4
50.6
9/11/2018
47.3
50.5
1
9/12/2018
46.8
50.3
9/13/2018
46.7
49.8
9/14/2018
45.6
48.7
9/15/2018
45
47.7
9/16/2018
43.9
47
9/17/2018
43.1
46.8
9/18/2018
42.7
46.8
9/19/2018
42.8
46.7
9/20/2018
9/21/2018
120,000
31.7
9/22/2018
-34.9
9/23/2018
36.3
9/24/2018
38.1
9/25/2018
40.1
9/26/2018
43
9/27/2018
45.8
9/28/2018
40.6
39.4
9/29/2018
39.8
48.1
9/30/2018
42.8
53.8
Total =
120,000
1,290
1,079
1
Ave=
4,000
44.5
49.1
1
Max=
120,000
51.6
53.8
1
Min=j
0
31.1
39.4
1

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
7/1/2018
60.9
55.9
7/2/20181
18,000
58.2
56.8
7/3/2018
54.3
57.4
7/4/2018
55.9
56.9
7/5/2018
60.9
56.1
7/6/2018
18,000
57.9
56.9
7/7/2018
61
58
7/8/2018
,
62.7
57.4
7/9/2018
18,000
57.4
57.5
7/10/2018
18,000
50.1
57.8
1.8
7/11/2018
18,000-
47.1
57.3
7/12/2018
13,500
45.4
58.7
7/13/2018
49.9
63
7/14/2018
58.2
63.7
7/15/2018
65.7
63.3
7/16/2018
18,000
63
63.7
7/17/2018
18,000
61.7
65.4
428.9
7/18/2018
18,000
60.7
66.5
7/19/2018
13,500
63.3
66.3
7/20/2018
67
67.6
7/21/2018
65
66
7/22/2018
63.4
64.6
7/23/2018
61.6
63.5
7/24/2018
61.2
62.5
87.9
7/25/2018
61.2
61.2
7/26/2018
59.4
59.4
7/27/2018
58.6
58.1
7/28/2018
57.3
57.7
7/29/2018
55.7
55.7
7/30/2018
54.1
55.8
7/31/2018
51.7
54.5
Total =
171,000
1,810
1,865
519
Ave=
5,516
58.4
60.2
172.9
Max=
18,000
67
67.6
428.9
Min=j
0
45.4
54.5
1.8

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
8/1/2018
51.8
54.8
8/2/2018
52
54.3
8/3/2018
51.2
52.7
8/4/2018
50
51.4
8/5/2018
49
50.6
8/6%2018
48.2
50.1
8/7/2018
47.6
'49.5
8/8/2018
47.1
48.7
8/9/2018
46.7
48.1
8/10/2018
45.4
47.8
8/11/2018
47.5
47.3
8/12/2018
48.2
46.8
8/13/2018
49.1
46.6
8/14/2018
49.6
46.5
8/15/2018
50.6
46.3
8/16/2018
51.3
45.8
8/17/2018
45.2
45.2
8/18/2018
45.6
45.1
8/19/2018
45.6
44.7
8/20/2018
45.4
44.4
8/21/2018
45
44.2
8/22/2018
44.5
43.8
8/23/2018
44.6
43.5
8/24/2018
45.5
42.9
8/25/2018
45.6
42.5
8/26/2018
46.1
42.3
8/27/2018
46
42.2
8/28/2018
44.1
42.3
0.52
8/29/2018
43.5
42.4
8/30/2018
42.6
42.2
8/31/2018
41.7
41.9
Total =
0
1,456
1,437
0.52
Ave=
-0
47
46.3
0.52
Max=
0
52
54.8
0.52
Min=j
0
41.7
41.9
0.52

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
9/1/2018
41
41.6
9/2/2018
40.5
41.1
9/3/2018
40.3
40.8
9/4/2018
39.9
40.3
0.57
9/5/2018
38.5
9/6/2018
38.1
9/7/2018
39.2
9/8/2018
42.7
9/9/2018
46.6
9/10/2018
48.6
9/11/2018
50.7
9/12/2018
50.1
9/13/2018
50.9
9/14/2018
50.3
9/15/2018
49.1
9/16/2018
40.6
9/17/2018
35.3
9/18/2018
36.7
9/19/2018
36.7
9/20/2018
35.9
9/21/2018
35.8
9/22/2018
37.9
9/23/2018
40
9/24/2018
42
9/25/2018
43.5
9/26/2018
44.1
9/27/2018
44.3
9/28/2018
43.4
9/29/2018
44.2
9/30/2018
45.5
Total =
0
1,272
41.1
0.57
Ave=
0
42.4
41
0.57
Max=
0
50.9
41.6
0.57
Min=j
0
35.3
40.3
0.57

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
7/1/2018
7/2/2018
7/3/2018
7/4/2018
7/5/2018
7/6/2018
7/7/2018
7/8/2018
7/9/2018
7/10/2018
7/11/2018
7/12/2018
7/13/2018
7/14/2018
7/15/2018
7/16/2018
7/17/2018
7/18/2018
7/19/2018
7/20/2018
7/21/2018
7/22/2018
7/23/2018
7/24/2018
7/25/2018
7/26/2018
7/27/2018
7/28/2018
7/29/2018
7/30/2018
7/31/2018
Total =
Ave=
Max=
Min=

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(OC)
Temp
(oC)
Fecal
(MPN)
8/1/2018
8/2/2018
8/3/2018
8/4/2018
8/5/2018
8/6/2018
8/7/2018
8/8/2018
8/9/2018
8/10/2018
8/11/2018
8/12/2018
8/13/2018
8/14/2018
8/15/2018
8/16/2018
8/17/2018
8/18/2018
8/19/2018
8/20/2018
8/21/2018
8/22/2018
8/23/2018
8/24/2018
8/25/2018
8/26/2018
8/27/2018
8/28/2018
8/29/2018
8/30/2018
39.1
8/31/2018
41.4
Total =
81
Ave=
40.3
Max=
41.1
Min=I
39.1

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
9/1/2018
44.6
9/2/2018
47.6
9/3/2018
49.3
9/4/2018
50.4
9/5/2018
48.4
9/6/2018
47.6
9/7/2018
48.6
9/8/2018
50.7
9/9/2018
51.2
9/10/2018
51
9/11/2018
51.5
9/12/2018
51.6
9/13/2018
51.3
9/14/2018
51
9/15/2018
50.3
9/16/2018
45.9
9/17/2018
44
9/18/2018
45.5
9/19/2018
45.4
9/20/2018
46.5
9/21/2018
46.2
9/22/2018
46.7
9/23/2018
47.3
9/24/2018
47.3
9/25/2018
47.3
9/26/2018
9/27/2018
9/28/2018
9/29/2018
9/30/2018
Total =
1,207
Ave=
48.3
Max=
51.6
Min=
44

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
1TE COLLECTED: -7 3 DATE RECEIVED:
WE COLLECTED: p TIME RECEIVED:
)ELECTED BY: RECEIVED BY:
'HOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION] I
,MPLE LOCATION
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
121 ± 2 HOURS AT 44.5
± 0.2'C IN WATERBATH
10 mL
1 mL
0:1D mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
O1SmL
0 ,'5mL
0 15mL
0 15mL
J 15mi.
` 15mL
015mt.
15mL
D/SmL+SmL
OURS AT 35 + 0.5`C IN INCUBATOR
rE IN INCUBATOR: '1� l DATE OUT INCUBATOR: `? 3. 9-0 � d
IE IN INCUBATOR: 0145
TIME OUT INCUBATOR: O
UBATOR TEMP: `3) INCUBATOR TEMP:
4- 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
rE IN WATERBATH: ,'3 DATE OUT WATERBAT
E IN WATERBATH: TIME OUT WATERBATH
TERBATH TEMP: 4 "3 WATERBATH TEMP:-•
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
P
DS A4 BROTH
P
r/
MPN Index Value
MPN /mL'=
Largest Sample Volume
MPN / 100 mL2 = (100)(MPN / mL)
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
COMB. OF MPN / mL' MPN / 100 mL'
POSITIVES
cl -- tJ 40 OI�o3 i • {�a
MPN / GRAM =
MPN/GRAM'
00
(ATAD SOLIDS
2-` 1
MPN / mL'
%Tot. Solids 4 x 100
CHECKED BY: IA-
A UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
ATE COLLECTED: 7. /b- /y DATE RECEIVED: 7 ( 0. j
:ME COLLECTED: y --� TIME RECEIVED:
OLLECTED BY: t4c.G(� 3 RECEIVED BY:
THOD: SM 9221 C E - 2006 [MULTIPLE TUBE FERMENTATION]
AMPLE LOCATION
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
0 /5mL
O
15rnl-
D /5mL
15mL
/�)
t/ /5mL
rr
/5mL
%5mL
�
I M
0
15mL
15mL
-(OURS AT 35 + 0.5°C IN INCUBATOR
%TE IN INCUBATOR: DATE OUT INCUBATOR:
AE IN INCUBATOR: r!, TIME OUT INCUBATOR: 1 Q
,UBATOR TEMP: js.0 INCUBATOR TEMP:
+ 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
,TE IN WATERBATH: . 09- DATE OUT WATERBAT
AE IN WATERBATH: `1 �� TIME OUT WATERBATH ( 3
3TERBATH TEMP: *4 WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
4
DS A-1 BROTH
b-c
U (�
IM UPDATED: DECEMBER 2017
MPN / ML' =
MPN Index Value
Largest Sample Volume
MPN / 100 mL2 = (100)(MPN / ml-)
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
l o.
COMB. OF MPN/mL' MPN / 100 mL2
POSITIVES
0. o.c) oof l �03
MPN/GRAM'=
MPN/GRAM'
(' b
(ATAD SOLIDS
ANALYSIS)'
0.99
MPN/MC
% Tot. Solids ° x 100
CHECKED BY: IVY
COPY MADE: IY

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: . �� DATE RECEIVED:
TIME COLLECTED: A d 2 lie TIME RECEIVED:
COLLECTED BY: RECEIVED BY:
METHOD; F SM 9221C-E - 2006 [MULTIPLE TUBE FERMENTATION]
7. 1 7• IS' DATE ANALYZED: -'r. 177,
0000 TIME ANALYZED: j ©�
ANALYZED BY:
1
3'HOURS AT 35 ± 0.5•C IN INCUBATOR
21 + 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION
10 mL 1 mL 0.10 mL 0.010 mL
10 mL I 1 mL 0.10 mL 0.010 mL
�
15ML
v 15mt,
15mt.
015m!
J
5x5m!
D
15mt.
f5mL
15m
DUP
I
I l
15m! I
d5mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: ( DATE OUT INCUBATOR:
TIME IN INCUBATOR: tcL TIME OUT INCUBATOR: t
INCUBATOR TEMP: 3 5-0 INCUBATOR TEMP: 3� �
21 + 2 HOURS AT 44.5 +•0.2°C IN WATERBATH
DATE IN WATERBATH: `�. ��-1 DATE OUT WATERBAT
TIME IN WATERBATH: �'�'+�rj TIME OUT WATERBATH
WATERBATH TEMP: L,L� WATERBATH TEMP: 1 /mow
POSITIVE I NEGATIVE BLANK
CONTROL CONTROL
SS A-1 BROTH
DS A-1 BROTH
MPN Index Value
MPN /mL'=
Largest Sample Volume
COMB. OF
POSITIVES MPN / mL'
I MPN / 100 mL
19 -1-75 r�
MPN/GRAM'
F% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)°
;,11+
MPN / mL'
MPN / GRAM'
% Tat. Solids ° x 100
L MPN / 100 mL 2 = (100)(MPN / mL) CHECKED BY: L{�
FORM UPDATED: DECEMBER 2017
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: DATE RECEIVED:
TIME COLLECTED: S +) TIME RECEIVED:
COLLECTED BY: RECEIVED BY:
:910i$
DATE ANALYZED:
TIME ANALYZED: OGj
ANALYZED BY: a -4--R
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION] I -
3 HOURS AT 35 ± 0.5'C IN INCUBATOR - 21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OFPOSITIVES MPN/mL' MPN / 100 mL2
:'5mL '" /5mL © r5mt v :SmL 57 E5mL iSmL 15mL 15mL
DUP
SmL I � ;5mL
3 HOURS AT 35 + 0.5'C IN INCUBATOR MPN/GRAM'
DATE IN INCUBATOR: ;T DATE OUT INCUBATOR;
TIME IN INCUBATOR: , 00 {p TIME OUT INCUBATOR: ,O
-INCUBATOR TEMP: INCUBATOR TEMP: �j� -(� % TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)"
21 + 2 HOURS AT 44.5 + 0.2'C IN WATERBATH (�
DATE IN WATERBATH: 'Y2� �� DATE OUT WATERBAT
TIME IN WATERBATH: 171 p TIME OUT WATERBATH
WATERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
a
DS A-1 BROTH
u
FORM, UPDATED: DECEMBER 2017
V U
MPN /ML'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL z = (100)(MPN / mL)
MPN / mL'
MPN/GRAM'=
%Tot. SolIdS° x 100
CHECKED BY:
COPY MADE:

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY: 8t fC
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: _ } $ DATE ANALYZED: S .1'j ..I
TIME RECEIVED: ( TIME ANALYZED: D S q-5
RECEIVED BY: LIW ANALYZED BY: {'4�-
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION)
SAMPLE LOCATION
DUP
3 HOURS AT 35 ± 0.5•C IN INCUBATOR
21 + 2 HOURS AT 44.5 + 0.2•C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
© 15mL
0/5mL
�15rnL
D 15mL
o 15mt.
O 15mL
o 15mL
O 15rnL
/5 mL
O 15 mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: DATE OUT INCUBATOR:
TIME IN INCUBATOR: p p TIME OUT INCUBATOR:_
INCUBATOR TEMP: 3s- fl INCUBATOR TEMP: ?�
-21 + 2 HOURS AT 44.5 + OXC IN WATERBATH
DATE IN WATERBATH:
TIME IN WATERBATH: 1 [�
WATERBATH TEMP: C t1 11 1
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
1Q
DS A-1 BROTH
N
DATE OUT WATERBATH �? — is --'I ? -
TIME OUT WATERBATH d g z -z
WATERBATH TEMP:
MPNImL'-
MPN Index Value
Largest Sample Volume
MPN 1100 mL 2 = (100)(MPN / mL)
COMB. OF
POSITIVES MPN/mL' MPN 1100 mLZ
MPN/GRAM'
MPN/GRAM
rcGu r�
A-0 Sol r �S
5� S•
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
MPN / mL'
% Tat. Solids 4 x 100
CHECKED BY
FORM UPDATED, DECEM13ER 2017 COPY MADE

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: f 2 t If DATE RECEIVED:
TIME COLLECTED: 6 TIME RECEIVED:
COLLECTED BY., A 1,.i5' RECEIVED BY:
METHOD' SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
0.2-1 w I S DATE ANALYZED:
Clel- 00 TIME ANALYZED: d `
ANALYZED BY:
3 HOURS AT 35 + 0.5'C IN INCUBATOR
21 + 2 HOURS AT 44,5 ± 0.2'C IN WATERBATH
COMBINATION OF
POSITIVES
MPN ! mL'
MPN 1100 mL'
SAMPLE LOCATION
1`0 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
t�
V /5mL
O /5mL
/5mL
0 l5ml.
O /5mL
2-15mL
O l5mL
O /5mL
- G', g/
•"31
DUP
(�
15ml-
(dry/
/5mL
MPN TABLE VALUE
2
J�
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: �. �� DATE OUT INCUBATOR:
TIME IN INCUBATOR: TIME OUT INCUBATOR: t Z
INCUBATOR TEMP: `3� ,) 'C INCUBATOR TEMP: '35 ,0 C
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: DATE OUT WATERBAT
TIME IN WATERBATH: TIME OUT WATERBATH
WATERBATH TEMP: _ -C WATERBATH TEMP: Q�• 'C
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
QS
DS A-1 BROTH
p C�
MPN ImL'=
MPN Index Value
Largest Sample Volume
MPN 1100 mL 2 = (100)(MPN / mL)
MPN/GRAM
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
MPN I mL'
MPN/GRAM'= x100
% Tot. Solids'
CHECKED BY: Vq
FORM UPDATED' MARCH 2O18 COPY MADE:

DATE COLLECTED:
TIME COLLECTED: 02
COLLECTED BY: lGGr
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: s, 28 • DATE ANALYZED:
TIME RECEIVED: 00 TIME ANALYZED: L b 3O
RECEIVED BY: to:; ANALYZED BY: bP�
METHOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
SAMPLE LOCATION
f1 8
DUP
3 HOURS AT 35 ± 0,5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
10mL
1 mL
0.10mL
0.010mL
10mL
1 mL
0.10mL
0.010mL
i5mL
v i5mL
D i5mL
(" t5mL
O 5mL
Or5ml.
0:5mL
® 5mL
O ,5mL
O /SmL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: . Z Is DATE OUT INCUBATOR: 2
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP: 915. 0 INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: B - 2e, - V. -3
TIME IN WATERBATH:
WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
'ORM UPDATED: DECEMBER 2017
DATE OUT WATERBAT 2—q , T
TIME OUT WATERBATH O +
WATERBATH TEMP: .
MPN/mL'-
MPN Index Value
Largest Sample Volume
MPN / 100 mL 2 = (100)(MPN / mL)
COMB. OF MPN / mL' MPN / 100 mL
�
POSITIVES
o -
MPN/GRAM'
MPN/GRAM'
rPN / GRAM'
• .l �?-
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
3. q6
MPN / mL'
% Tot. Solids ° x 100
CHECKED BY:
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: � L/ • / �� DATE RECEIVED: �. Li . � � � DATE ANALYZED: � • jg
TIME COLLECTED: TIME RECEIVED: TIME ANALYZED: Q (3 1'
COLLECTED BY: c.C)E=t 7 RECEIVED BY: ANALYZED BY:
iAETHOD: SM 9221 C E - 2006 [MULTIPLE TUBE FERMENTATION]
SAMPLE LOCATION
DUP
3 HOURS AT 35 0.5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5
± 0.2'C IN WATERBATH
10 mL
1 mL
0/r.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
0 /5mL
/5mL
V /SmL
/5mL
0 /5mL
O 15mL
O J5mL
O J5mL
15mL
I
I
0 /5mL
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN INCUBATOR: rL . `3 DATE OUT INCUBATOR: r'(- W
TIME IN INCUBATOR: TIME OUT INCUBATOR:
INCUBATOR TEMP: INCUBATOR TEMP: 3S, CD
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: q , 4 _ 4 G DATE OUT WATERBAT '
TIME IN WATERBATH: L tZ L TIME OUT WATERBATH 0 �-�-
WATERBATH TEMP:, WATERBATH TEMP:,
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL- = (100)(MPN / mL)
COMB. OF MPN / mL' MPN / 100 mL2
POSITIVES
C)--o.oti8a3 y.8a3
MPN/GRAM'
Z O . S-7y z
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
-3. 1
MPN / mL'
MPN/GRAM'=
%Tot. Solids' x 100
CHECKED BY:
'ORM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE, FECAL ANALYSIS
DATE COLLECTED: _ /j _ / ¢ DATE RECEIVED: 9 , I _ I DATE ANALYZED:
TIME COLLECTED: S TIME RECEIVED: TIME ANALYZED: ,D S t-IJ
COLLECTED BY:RECEIVED BY: ANALYZED BY:
METHOD: F77SM9221C—E-2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN / mL' MPN / 100 ML'
POSITIVES
Q 0 O d 2 .O_Q 0.0 !
%ZB :5mL SmL /5mL O O /5mL /SmL SmL MIL O 5mL
DUP (9 /5mL O 15mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: [� , �l$ DATE OUT INCUBATOR:
TIME IN INCUBATOR: Cfl 5L) TIME OUT INCUBATOR: 1500
0
INCUBATOR TEMP: 5 C ]NCI IRATnP TEMP- 2 C ..
21 ±2 HOURS AT 44.5+0.2-C 1N WATERBATH
DATE IN WATERBATH: C1 DATE OUT WATERBAT
TIME IN WATERBATH: ,5 TIME OUT WATERBATH
WATERBATH TEMP: [�, JC WATERBATH TEMP: 44/
r
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A BROTH
'-t—
DS A-1 BROTH
4-
—^
MPN Index Value
MPN/mL'=
Largest Sample Volume
MPN / 100 mL' - (100)(MPN r'rnL)
MPNIGRAM'
MPN/GRAM
0 -0r](Q
%TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)4
q-? D
FORM UPDATED: DECEMBER 2017
,F 5 W&YY/ ( � Ivi '/5°(/ jto64APAc I -to
4v 44.5°(j Wkx Y LIA41')
MPNImL'
°b To1. Solid's ' x 100
CHECKED BY:
LA -
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 9 %, t� DATE RECEIVED:
TIME COLLECTED: 1 TIME RECEIVED:
COLLECTED BY: RECEIVED BY:
METHOD: SM 9221C._E - 2006 [MULTIPLE TUBE FERMENTATION]
SAMPLE LOCATION
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 + 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
/5mL
C-�/5mL
i
��/Sml
�'"/SmL
L�
1 ISmL
5 5rnL
Q 5mL
�''_.irL
0/5rid
10 /5m!
3 HOURS AT 35 + 0.5'C IN INCUBATOR
DATE IN INCUBATOR: Cl 2�� 1 l Q DATE OUT INCUBATOR: �s
TIME IN INCUBATOR: t aC TIME OUT INCUBATOR:
INCUBATOR TEMP: 3 S , D INCUBATOR TEMP: _
21 + 2 HOURS AT 44.5 + 0.2'C IN WATERBATH
DATE IN WATERBATH: q\-Zs \%
TIME IN WATERBATH: 3 v 3
WATERBATH TEMP: '-i
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
DATE OUT WATERBAT CTl .Z Qj
TIME OUT WATERBATH
WATERBATH TEMP:
MPN/mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL Z = (I00)(MPN / ml-)
DATE ANALYZED: -- kK
TIME ANALYZED: 9
ANALYZED BY:
COMB. OF MPN/mL' MPN / 100 mL2
POSITIVES
S - O - 2- 4 - Z`Z
`-i. ?--I
MPN/GRAM'
MPN/GRAM'
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
6•bS
MPN / mL'
% Tot. Solids ° x 100
CHECKED BY: w
=ORM UPDATED; DECEMBER 2017 COPY MADE:

CAMP LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALYSIS
START-UP
7/6/2018
A
B
C
D
E
F
G
H
I
J
DATE
WT OF
SAMPLE
WT OF
TOTAL
%
ASH
VOLATILE
°
/°
SAMPLE
IN-HOUSE
ATAD
WT OF DISH
DISH+WET
WEIGHT
DISH+DRY
SOLIDS
WEIGHT
TOTAL
WT OF
WEIGHT
SOLIDS
VOLATILE
WEEKLY
°� VOLATILE
TEMP
DATE
DIGESTION
SOLIDS
SOLIDS
SOLIDS
DISH+ASH
WEIGHT
SOLIDS
AVERAGE
SOLIDS
REDUCTION
0°C
(g)
(g)
(g)
(g)
(g)
(g)
[8 - A]
(g)
[D - A]
[E/C] X 100
(g)
[G - A]
(E - H]
[1/E] X 100
I.H. ATAD 49,6918 54.69 5.00 49.7426 0.0508 1.02 49.7125 0.0207 0.0301 59.25 59.68 21.2
7/10/2018 y
DUP 75.5328 80.53 5.00 75.5837 0.0509 1.02 75.5531 0.0203 0.0306 60.12
I.H. ATAD
88.3502
93.35
5.00
88.3984
0.0482
0.96
88.3695
0.0193
0.0289
59.96
58.03
-1.19
24.2
7/13/2018
DUP 74.3228 79.32 5.00 74.3704 0.0476 0.95 74.3437 0.0209 0.0267 56.09
I.H. ATAD
86.3942
91.39
5.00
86A414
0.0472
0.94
86.4129
0.0187
0.0285
60.38
59.17
-0.71
24.3
7/20/2018
DUP 49.6923 54.69 5.00 49.7401 0.0478 0.96 49.7124 0.0201 0.0277 57.95
I H. ATAD
73.6025
78.6
5.00
73.6509
0.0484
0.97
73.6215
0.019
0.0294
60.74
59.82
-0.60
26.0
7/27/2018
DUP 74.3236 79.32 5.00 74.3725 0.0489 0.98 74.3437 0.0201 0.0288 58.90
I.H. ATAD
73.6046
78.6
5.00
73.6498
0.0452
0.90
73.624
0.0194
0.0258
57.08
57.02
6.03
24.9
8/3/2018
DUP 88.6459 93.65 5.00 88.6905 0.0446 0.89 88.6651 0.0192 0.0254 56.95
I.H. ATAD
74.6252
79.62
4.99
74.6704
0.0452
0.90
74.6433
0.0181
0.0271
59.96
60.24
-5.04
24.8
8/ 10/2018
DUP 75.5349 80.53 5.00 75.58 0.0451 0.90 75.5527 0.0178 0.0273 60.53
VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100
INITIAL VS
(VSR < 15%)

,�"� � r
Z
d
f.
�fy � �
s„ i. ,. y?ie✓,F 1. .»r.n ... r

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(OC)
Temp
(oC)
Fecal
(MPN)
10/1/2018
53.1
48.3
10/2/2018
18,000
47.6
48.6
2.9
10/3/2018
48.6
49.6
10/4/2018
51.8
49.5
.10/5/2018
53.8
48
10/6/2018
53.8
47.7
10/7/2018
53
47
10/8/2018
52.2
46.6
10/9/2018
50.9
45.4
10/10/2018
49
44.4
10/11/2018
47.9
46.2
10/12/2018
46.5
42.8
10/13/2018
45.2
41.8
10/14/2018
44.3
41.1
10/15/2018
43.8
40.8
10/16/2018
43.2
40.5
10/17/2018
42.5
39.9
10/18/2018
41.5
39.1
10/19/2018
40.5
10/20/2018
39.9
10/21/2018
39.2
10/22/2018
38.3
10/23/2018
37.7
10/24/2018
37.2
10/25/2018
10/26/2018
10/27/2018
10/28/2018
23.9
10/29/2018
27.7
10/30/2018
27.2
26.9
10/31/2018
27.2
29.9
Total =
18,000
1,207
890
2.9
Ave=
581
43.1
42.4
2.9
Max=
18,000
53.8
49.6
2.9
Mln=j
0
23.9
26.1
2.9

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
11/1/2018
28.3
33.2
11/2/2018
29.9
35.7
11/3/2018
31.9
39.1
11/4/2018
33.1
39.1
11/5/2018
35.4
45.2
11/6/20181
37.8
48.8
11/7/2018
40.8
50.5
11/8/2018
46.4
50.8
11/9/2018
51
50.5
11/10/2018
54.4
50.3
11/11/2018
- 57.7
48.7
11/12/2018
58.4
47.5
11/13/2018
57.8
46.9
11/14/2018
56.2
46
11/15/2018
53.8
47.1
11/16/2018
51.1
45.9
11/17/2018
48.9
44.7
11/18/2018
47.2
44.1
11/19/2018
100,000
46
43.1
11/20/2018
45.3
42.3
11/21/2018
11/22/2018
11/23/2018
11/24/2018
11/25/2018
11/26/2018
11/27/2018
11/28/2018
11/29/2018
11/30/2018
Total =
100,000
911
899
0
Ave=
3,333
46
45
0
Max=
100,000
58.4
50.8
0
Min=
0
28.3
33.2
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 1 A
Train 1 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
12/1/2018
12/2/2018
12/3/2018
12/4/2018
12/5/2018
30.9
12/6/2018
32.1
12/7/2018
33.2
12/,8/2018
34.6
12/9/2018
36.6
12/10/2018
39.4
12/11/2018
42.8
12/12/2018
45.6
12/13/2018
47.5
12/14/2018
47.8
12/15/2018
47.2
12/16/2018
47.1
12/17/2018
39
28.1
12/18/2018
37.7
37.2
12/19/2018
42
39.5
12/20/2018
46.2
42.6
12/21/2018
49.6
46.4
12/22/2018
50.6
47.7
12/23/2018
49.6
47.4
12/24/2018
48.1,
46.7
12/25/2018
47.2
45.7
12/26/2018
46.3
43.3
12/27/2018
45.1
43.1
12/28/2018
44.2
42
12/29/2018
41.8
41
12/30/2018
42.6
41.4
12/31/2018
41.8
41
Total =
0
1,157
634
0
Ave=
0
42.8
42.3
0
Max=
0
50.6
47.7
0
Min=l
0
30.9
28.1
0

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
10/1/2018
47.6
10/2/2018
50.5
10/3/2018
60,000
46.5
10/4/2018
18,000
46
10/5/2018
18,000
48..3
10/6/2018
47.5
10/7/2018
46.9
10/8/2018
47.5
10/9/2018
18,000
49.9
0.4
10/10/2018
18,000
49.9
10/11/2018
18,000
48.4
10/12/2018
18,000
47.3
10/13/2018
49.2
10/14/2018
51.2
10/15/2018
18,000
49.6
10/16/2018
18,000
50.2
0.6
10/17/2018
18,000
48.6
10/18/2018
18,000
48.4
10/19/2018
18,000
51.1
10/20/2018
56
10/21/2018
55.9
10/22/2018
18,000
'52.7
10/23/2018
61.6
2.4
10/24/2018
18,000
61.7
10/25/2018
18,000
62.2
10/26/2018
18,000
65.8
10/27/2018
62.5
10/28/2018
71.4
10/29/2018
18,000
68.4
10/30/2018
18,000
39.2
1.6
10/31/2018
18,000
39.9
Total =
384,000
1,622
1,731
5
Ave=
12,387
52.3
55.8
1.2
Max=
60,00
71.4
58.5
2.4
Min=
0
39.2
52.4
0.4

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
11/1/2018
18,000
40.1
54.1
11/2/2018
18,000
39.8
54.6
11/3/2018
40.9
57.5
11/4/2018
43.2
59.2
11/5/2018
18,000
62.1
57.8
11/6/20181
18,000
71.1
57.9
2.2
11/7/2018
18,000
85.3
57.7
11/8/2018
18,000
93.5
58
11/9/2018
18',000
123.372.0
58
11/10/2018
54.2
59
11/11/2018
66.7
58.9
11/12/2018
81.8
58.2
11/13/2018
18,000
91
56
32.7
11/14/2018
18,000
114
53.8
11/15/2018
108.4
52.7
11/16/2018
1%000
107.8
52.4
11/17/2018
110.7
51.8
11/18/2018
110.4
51.2
11/19/2018
50.7
.11/20/2018
60,000
48.6
1.9
11/21/2018
42.3
11/22/2018
39.9
11/23/2018
42.9
11/24/2018
45.8
11/25/2018
49.1
11/26/2018
51.3
11/27/2018
18,000
52
2.4
11/28/2018
49.7
11/29/2018
51.3
11/30/2018
53.2
Total =
258,000
1,516
1,585
39
Ave=
8,600
79.8
52.8
9.8
Max=
60,000
123.3
59.2
32.7
Min=j
0
1 39.8
39.9
1.9

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 2 A
Train 2 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
12/1/2018
33.2
51.9
12/2/2018
34.7
54.6
12/3/2018
18,000
37.2
57
12/4/2018
35.8
54.1
9.4
12/5/2018
33.3
54
12/6/2018
33.4
57.5
12/7/2018
18,000
35.1
60.4
12/8/2018
34.6
58.1
12/9/2018
35.9
59.3
12/10/2018
18,000
37.5
59.2
12/11/2018
18,000
37
56.6
2.3
12/12/2018
18,000
34.6
�55.3`
12/13/2018
18,000
33
56.4
12/14/2018
18,000
31.4
57.6
12/15/2018
30.4
58.5
12/16/2018
30.2
53.4
12/17/2018
18,000
35.6
65.7
12/18/2018
18,000
35.3
61.8
66.6
12/19/2018
18,000
33.7
59.4
12/20/2018
18,000
34.2
54.7
12/21/2018
18,000
38.7
50.6
12/22/2018
39.5
51.3
12/23/2018
44.5
54.4
12/24/2018
52.9
60.6
12/25/2018
56.3
64
12/26/2018
59.2
65.6
7.2
12/27/2018
59.1
65.8
12/28/2018
58.4
64
12/29/2018
54.8
59.8
12/30/2018
56.6
71.7,
12/31/2018
18,000
54.8
59.8
Total =
234,000
1,263
1,814
85
Ave=
7,548
40.7
58.5
21.3
Max=
18,000
59.2
65.8
66.5
Min=
0
30.4
50.6
2.3

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date .
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
10/1/2018
46.6
10/2/2018
48.9
10/3/2018
48.9
10/4/2018
49.8
10/5/2018
49.6
10/6/2018
49.7
10/7/2018
49.8
10/8/2018
49.2
10/9/2018
48.3
10/10/2018
48.7
10/11/2018
47.9
10/12/2018
47.8
10/13/2018
47.9
10/14/2018
47.9
10/15/2018
47.4
10/16/2018
47.9
10/17/2018
48.2
10/18/2018
45.6
10/19/2018
43
10/20/2018
42.8
31
10/21/2018
42.6
32.9
10/22/2018
42.1
33.8
10/23/2018
40.4
34.7
10/24/2018
10/25/2018
10/26/2018
10/27/2018
10/28/2018
10/29/2018
10/30/2018
10/31/2018
Total =
0
1,081
132
Ave=
0
47
33.1
Max=
0
49.8
34.7
Min=
0
40.4
31

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
11/1/2018
11/2/2018
11/3/2018
11/4/2018
11/5/2018
11/6/2018
11/7/2018
11/8/2018
11/9/2018
11/10/2018
11/11/2018
11/12/2018
11/13/2018
11/14/2018
22.3
11/15/2018
24.7
11/16/2018
24.5
22.8
11/17/2018
25.7
25.8
11/18/2018
26.7
26.6
11/19/2018
28.1
27.6
11/20/2018
11/21/2018
11/22/2018
36.3
11/23/2018
38.1
11/24/2018
41
11/25/2018
44.3
11/26/2018
47.6
11/27/2018
49.9
37.2
11/28/2018
47.2
40
11/29/2018
50.3
41.2
11/30/2018
52.2
43.1
Total =1
0
559
264
Ave=
0
37.3
33
Max=
0
52.2
43.1
Min=
0
22.3
22.8

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 3 A
Train 3 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
12/1/2018
55.5
46.8
12/2/2018
54.4
52
12/3/2018
18,000
53.2
55.3
12/4/2018
50.6
54.7
12/5/2018
44.2
53.5
12/6/2018
18,000
49.2
54.7
12/7/2018
44.8
53
12/8/2018
48.5
53.5
12/9/2018
49.2
53.4
12/10/2018
18,000
48.1
52.5
12/11/2018
43.4
49.5
12/12/2018
46.3
49.8
12/13/2018
48.3
51
12/14/2018
18,000
48.9
52
12/15/2018
47.2
50.5
12/16/2018
46.6
50.6
12/17/2018
18,000
47.3
50.3
12/18/2018
42.3
47.7
12/19/2018
43.1
48.3
12/20/2018
46.6
49.4
12/21/2018
48.5
51.4
12/22/2018
49.5
50.4
12/23/2018
49.1
50.1
12/24/2018
48.3
49.6
12/25/2018
47.6
48.5
12/26/2018
46.5
47.3
12/27/2018
120,000
45.5
46.1
12/28/2018
35.1
40.3
12/29/2018
38.4
43.2
12/30/2018
35.1
42.3
12/31/2018
38.4
44.7
Total =
210,000
1,440
1,542
Ave=
6,774
46.4
49.7
Max=
120,000
55.5
55.3
Min=j
0
35.1
40.3

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
10/1/2018
10/2/2018
10/3/2018
10/4/2018
10/5/2018
10/6/2018
10/7/2018
10/8/2018
10/9/2018
10/10/2018
10/11/2018
10/12/2018
10/13/2018
10/14/2018
_
10/15/2018
10/16/2018
10/17/2018
10/18/2018
10/19/2018
10/20/2018
10/21/2018
10/22/2018
10/23/2018
10/24/2018
10/25/2018
10/26/2018
10/27/2018
10/28/2018
10/29/2018
10/30/2018
10/31/2018
Total =
Ave=
Max=
Min-

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
11/1/2018
11/2/2018
11/3/2018
11/4/2018
11/5/2018
11/6/2018
11/7/2018
11/8/2018
11/9/2018
11/10/2018
11/11/2018
11/12/2018
11/13/2018
11/14/2018
11/15/2018
11/16/2018
11/17/2018
11/18/2018
11/19/2018
11/20/2018
11/21/2018
11/22/2018
11/23/2018
11/24/2018
11/25/2018
11/26/2018
11/27/2018
11/28/2018
11/29/2018
11/30/2018
Total =
Ave=
Max=
Min --I

CAMP LEJEUNE,NC
2018 ATAD Performance Data
Date
ATAD Train 4 A
Train 4 B Coliform
Feed
(Gallons)
Temp
(oC)
Temp
(oC)
Fecal
(MPN)
12/1/2018
12/2/2018
12/3/2018
12/4/2018
12/5/2018
12/6/2018
12/7/2018
12/8/2018
12/9/2018
12/10/2018
12/11/2018
12/12/2018
12/13/2018
12/14/2018
12/15/2018
12/16/2018
12/17/2018
12/18/2018
12/19/2018
12/20/2018
12/21/2018
12/22/2018
12/23/2018
12/24/2018
12/25/2018
12/26/2018
12/27/2018
12/28/2018
12/29/2018
12/30/2018
12/31/2018
Total =
Ave=
Max=
Min=

CAMP LEJEUNE WWTP -
ATAD SLUDGE FECAL ANALYSIS
ATE COLLECTED: 1 n_ DATE RECEIVED: �.
IME COLLECTED: TIME RECEIVED: Q C�a C)
OLLECTED BY: ;S RECEIVED BY:
THOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
4MPLE LOCATION
cRor'l
1 *
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5
± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
/5mL
V /5mL
l5mL
D /5mL
/5mL
�- /5mL
O /SmL
?5mL
/5mL
/5mL
-IOURS AT 35 + 0.5°C IN INCUBATOR
ATE IN INCUBATOR: DATE OUT INCUBATOR: l 0.
OE IN INCUBATOR: 06j/ -5- TIME OUT INCUBATOR: r�
:UBATOR TEMP; INCUBATOR TEMP: '>7 -L
+ 2 HOURS AT 44.5 +-0.2'C IN WATERBATH
ATE IN WATERBATH: l .'� .'%� �D DATE OUT WATERBAT
AE IN WATERBATH: l-t TIME OUT WATERBATH 10g0
kTERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
+
--
DS A-1 BROTH
+-
r--
MPN /MLA=
MPN Index Value
Largest Sample Volume
MPN / 100 mLZ = (100)(MPN / ml-)
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
©10(",
COMB. OF POSITIVES MPN / mL' MPN / 100 mLz
�.. 5.0 0, r74 6 ` i
MPN/GRAM'
P.�71
% TOTAL SOLIDS
(ATAD SOLIDS
A 4
NALYSIS
VIC)p�
MPN / mL'
MPN / GRAM =
% Tot. Solids 4 x 100
CHECKED BY: `v
IM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
)ATE COLLECTED. D DATE RECEIVED: Q - 7.
'IME COLLECTED: O ? STIME RECEIVED: 09 to
:OLLECTED BY: c t a. RECEIVED BY:
'THOD: SM 9221 C_.E - 2006 (MULTIPLE TUBE FERMENTATION]
AMPLE LOCATION
Z /3
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS
AT 44.5 ± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
'0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
v /5mL
0/5mL
/5mL
—j
® /5mL
v `5mL
+5mL
0 /5mL
v /5mL
/5mL
HOURS AT 35 + 0.5°C IN INCUBATOR
4TE IN INCUBATOR: 1 d , 9_ .>-0 (� DATE OUT INCUBATOR:
ME IN INCUBATOR: (a ' —7 TIME OUT INCUBATOR: (3 7
CUBATOR TEMP: j'S-L) INCUBATOR TEMP:
1 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
4TE IN WATERBATH: D .6i, 1�101 DATE OUT WATERBAT `� , I?_ `? o
MEIN WATERBATH: )� � (337 TIME OUT WATERBATH1*4� �' c7O
ATERBATH TEMP: 44. WATERBATH TEMP: �� `I -
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DOS
DS A-1 BROTH
OS,
MPN /mL'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL 2 = (100)(MPN / mL)
DATE ANALYZED: 10. `. -?v o
TIME ANALYZED: 0 '� D
ANALYZED BY:
COMB. OF
POSITIVES MPN / mL' MPN 1100 mL2
MPN/GRAM'
MPN/GRAM'
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)
MPN / mL'
% Tot. Solids 4 x 100
CHECKED BY: v
IM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP .
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: /v / DATE RECEIVED:
TIME COLLECTED: �, S' TIME RECEIVED:
COLLECTED BY: COS RECEIVED BY:
ETHOD: SM 9221C E - 2006 (MULTIPLE TUBE FERMENTATION]
SAMPLE LOCATION
T2S
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS
AT 44.5
± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
/5mL
/5mL
�15mL
/5mL
v 15mL
15mL
0 15mL
0 15mL
v /5mL
O /5mL
I HOURS AT 35 + 0.5°C IN INCUBATOR
)ATE IN INCUBATOR: r,0. �V..�O �& DATE OUT INCUBATOR:
'IME IN INCUBATOR: TIME OUT INCUBATOR: 1 j rr7
NCUBATOR TEMP: 3►5 -D INCUBATOR TEMP:
H + 2 HOURS AT 44.5 +•0.2°C IN WATERBATH
)ATE IN WATERBATH: 4 0 ( (�
'IME IN WATERBATH: (�
VATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
1j00 S
U
DATE OUT WATERBAT .17. DrO I R
TIME OUT WATERBATH ! ';L
WATERBATH TEMP: 44. *-5
MPN IML'=
MPN Index Value
Largest Sample Volume
MPN / 100 mL2 = (100)(MPN / mL)
DATE ANALYZED: &, I& - 'PO4
TIME ANALYZED: (' o to
ANALYZED BY:
COMB. OF MPN / mL' MPN / 100 mL2
POSITIVES
0, D . D 0.0 I ku 3 (. 50 :5
MPN/GRAM'
�, 5�
(ATAD SOLIDS
MPN / mL'
MPN/GRAM =
% Tot. Solids 4 x 100
CHECKED BY: V'
)RM UPDATED: DECEMBER 2017 COPY MADE:

DATE COLLECTED: d 2 3 ,
TIME COLLECTED: a os
COLLECTED BY: c0 s `a
CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED: io . 3, k e DATE ANALYZED: � 0 - . �
TIME RECEIVED: 0-1l( C) TIME ANALYZED:
RECEIVED BY: ��� ANALYZED BY:�
ETHOD: F-SM9221C.-E-2006 [MULTIPLE TUBE FERMENTATION]
SAMPLE LOCATION
T— j— .
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5
± 0.2-C IN WATERBATH
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
/5mL
D 15mL
O /5mL
(0 15mL
V 15mL
i5mL
D 15mL
0 15mL
/S mLl
O /5mL
I HOURS AT 35 + 0.5°C IN INCUBATOR
)ATE IN INCUBATOR: l� , 9-3 , DATE OUT INCUBATOR: lQ . iL3
'IME IN INCUBATOR: TIME OUT INCUBATOR: t 3 l�
14CUBATOR TEMP: 3S , INCUBATOR TEMP S,
!1 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
)ATE IN WATERBATH: k(D . Z3 .
IME IN WATERBATH:
VATERBATH TEMP: G�
POSITIVE
NEGATIVE
CONTROL
CONTROL
BLANK
SS A-1 BROTH
�� 5
DS A-1 BROTHad
cy
DATE OUT WATERBAT 10 [ b
TIME OUT WATERBATH (�O
WATERBATH' TEMP:
MPN Index Value
MPN /mL'=
Largest Sample Volume
MPN / 100 mL z = (100)(MPN / mQ
COMB. OF
POSITIV S MPN ! mL' MPN / 100 mL2
IQ-Vy 0'
MPN/GRAMS
MPN/GRAM'
a, .�
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
MPN / mL'
% Tot. Solids 4 x 100
CHECKED BY: (I
IRM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
SATE COLLECTED: 113 - DATE RECEIVED: D. 30.14
IME COLLECTED: S TIME RECEIVED: p' ?.o
OLLECTED BY: RECEIVED BY:-
THOD: SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
AMPLE LOCATION
DUP
3 HOURS AT 35 ± 0.5'C IN INCUBATOR
21 ± 2 HOURS AT 44.5
± 0.2'C IN WATERBATH
10 mL
1 mL
0.10 mL
0,010 mL
10 mL
1 mL
0.10 mL
0:010 mL
O/5mL
15mL
l5ml-
/5mL
D l5mL
+ ;5mL
-0 5mL
;5mL
/5mL
I
D /5mL
HOURS AT 35 + 0.5°C IN INCUBATOR
1TE IN INCUBATOR: `(�.7J0 .�O` DATE OUT INCUBATOR: ' O /0
1AE IN INCUBATOR:% TIME OUT INCUBATOR:
CURATOR TEMP: `�fj .� INCUBATOR TEMP:
+ 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
►TE IN WATERBATH: �D .1JV DATE OUT WATERBAT
NE IN WATERBATH: TIME OUT WATERBATH
4TERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
S
DS A-1 BROTH
S
MPN / mL' =
MPN Index Value
Largest Sample Volume
MPN / 100 mL x = (100)(MPN / mL)
DATE ANALYZED: �' '-)Q,-XD 1 D
TIME ANALYZED: 0-14 j
ANALYZED BY: Elne
0. %,
COMB. OF MPN/mL' MPN / 100 mL2
POSITIVES
9,+0 0.o�5 7.
MPN/GRAM'
1-(ro
%TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)'
4,�V
MPN / mL'
MPN/GRAM =
% Tot. Solids" x 100
M
CHECKED BY: v
IM UPDATED: DECEMBER 2017 COPY MADE:.

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 6 / DATE RECEIVED: l DATE ANALYZED: l
TIME COLLECTED: c) L, L TIME RECEIVED: (D'l 00 TIME ANALYZED:
COLLECTED BY: rk LayRECEIVED BY: �' ANALYZED BY:
METHOD: SM 9221C. E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5'C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION I 10 mL 1 mL 0.10 mL 0.010 mL 10 mL 1 mCOMB. OF t 0.10 mL 0.010 mL POSITIVES MPN / mL' MPN / 100 m��
f 2,13 O i5ml. (D +5mL `✓ 'SmL (3 5mL � %5mL 4/5mL �15
DUP
l5mL l5mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: � � , � _ ` v DATE OUT INCUBATOR: `\ _ `P .
TIME IN INCUBATOR: 09 :?p 12)) TIME OUT INCUBATOR: -2, j0
INCUBATOR TEMP: �11?js C% INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2"C 1N WATERBATH
DATE IN WATERBATH: l ` _ ij DATE OUT WATERBAT
TIME IN WATERBATH: , y�j TIME OUT WATERBATH 0
WATERBATH TEMP: WATERBATH TEMP: -f4 _c
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
MPN/mL'=
MPN Index Value
Largesl Sample Volume
MPN / 100 mL" = I100]IMPN / mLI
0 1 t-4-n
/5mL
0- 1 0 5
MPN / GRAM'
,,2. ad-.
%TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS)4
v vlo,7-
MPN/ML'
MPN/GRAM'
,. Tot. Solids x 100
CHECKED BY' O
FORM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: (S DATE RECEIVED: B
TIME COLLECTED: TIME RECEIVED: oo
COLLECTED BY: RECEIVED BY:�
METHOD; SM 9221 C_E - 2006 [MULTIPLE TUBE FERMENTATION]
DATE ANALYZED:
TIME ANALYZED: Q� S
ANALYZED BY:�s
3 HOURS AT 35 t 0.5•C IN INCUBATOR 2112 HOURS AT 44.5 ± 0.2'C IN WATERBATHSAMPLE LOCATION 10 mL i mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF POSITIVES MPN / mL' MPN / 100 mLt
OJV "` /5mL `.J /5mL v I5mL O 15mL � 5
DUP CD l5mL ;5
3 HOURS AT 35 + 0.5°C IN INCUBATOR
45 t - 5 - v
+5mL T /V� ,SmL O+SmL
DATE IN INCUBATOR: _ lJ . '� G DATE OUT INCUBATOR: t l • `-3 . I
TIME IN INCUBATOR: TIME OUT INCUBATOR: `0 :3 l
INCUBATOR TEMP: 3S 0 INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH I
DATE IN WATERBATH: t 3 l J DATE OUT WATERBAT
TIME IN WATERBATH: `���, TIME OUT WATERBATH
WATERBATH TEMP: WATERBATH TEMP:
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
MPN / mL ' =
MPN Index Value
Largesl Sample Volume
MPN / 100 mL 2 = (100)(MPN / mL)
MPN/GRAM=
MPN / GRA__M
�9- btP
% TOTAL SOLIDS
(ATAO SOLIDS
ANALYSIS
+-
MPN /mL'
%P Tot. Solids 4 x 100
CHECKED BY:y
FORM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: 1-- do IO DATE RECEIVED: t ` Z CJ ( v
TIME COLLECTED: 3 TIME; RECEIVED:
COLLECTED BY: �� RECEIVED BY: I>
METHOD: SM 9221C_E - 2006 [MULTIPLE TUBE FERMENTATION]
DATE ANALYZED: l ` C) - I
TIME ANALYZED: v31D
ANALYZED BY:
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2•C IN WATERBATH
SAMPLE LOCATION lamL 1 mL 0.10 mL 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF MPN / mLr MPN ! 100 m12
POSITIVES
I �,�' 15mL/5ml v/5mL Y lSmt O 15mL 5 i5ml :5mL O 15mL 0~5 — O v� l " —
OUP 0 L
/5mL IS mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
MPN / GRAM'
DATE IN INCUBATOR: i t . ZD • 8 DATE OUT INCUBATOR:
TIME IN INCUBATOR: k ` 0 C a TIME OUT INCUBATOR:
INCUBATOR TEMP: �jS . C7 O G INCUBATOR TEMP: 25 v C� %TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS
21 + 2 HOURS AT 44.5 +•0.2°C IN WATERBATH
DATE IN WATERBATH: ` DATE OUT WATERBAT
TIME IN WATERBATH: k4` TIME OUT WATERBATH \bO
WATERBATH TEMP: 1 G WATERBATH TEMP: 4A A
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
k-IC61
DS A-1 BROTH
MPN / mL' =
MPN Index Value
Largest Sample Volume
MPN 1100 mL2 = (100)(MPN / mL)
MPN / mL'
MPN / GRAM =
% Tot. Solids ` x I OD
CHECKED BY: L
Ar
FORM UPDATED: DECEMBER 2017 COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE COLLECTED: / / • Z 7 19 DATE RECEIVED:
TIME COLLECTED: b 6 S G TIME RECEIVED:
COLLECTED BY: Ace f ci RECEIVED BY:
METHOD: I SM 9221C E-2006 [MULTIPLE TUBE FERMENTATION]
2.-7, w a DATE ANALYZED: Ir. 2'% 70 Is,
b 710-5 TIME ANALYZED: 0-1
an -
ANALYZED BY:
t
3 HOURS AT 35 ± 0.5•C IN INCUBATOR 21 ± 2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
SAMPLE LOCATION 10 mL 1 mL 0.10 mL 0.01D mL 10 mL 1 mL 0.10 mL 0.010 mL COMB. OF
POSITIVES
/ Z b D 15mL v 16ml. V 15
DUP D 15 mL
3 HOURS AT 35 + 0.5°C IN INCUBATOR
0 ,smLI O ,SmLl ` :Smj 015
V 15 mL
DATE IN INCUBATOR: `. W\ DATE OUT INCUBATOR: 1, -)/1. -n �D
TIME IN INCUBATOR: ot)u l TIME OUT INCUBATOR:
INCUBATOR TEMP: '75.0 INCUBATOR TEMP:
21 + 2 HOURS AT 44.5 + 0.2°C 1N WATERBATH G
DATE IN WATERBATH: XV t D DATE OUT WATERBAT t I . 2 0 , t v
TIME IN WATERBATH: 1�.Z/l• B �` TIME OUT WATERBATH 00 to
WATERBATH TEMP: WATERBATH TEMP: -t4 _
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A•1 BROTH
as
1 v
FORM UPDATED: DECEMBER 2017
MPN Index Value
MPN/ML'=
Largest Sample Volume
MPN / 100 mL? = (100)(MPN / ML)
005mLI ` - "- a
MPN/mL' I MPN / 100 mLz
0 vi,3' t-SD
MPN/GRAM'
a. I" -
%TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIISS� e
MPN I mL'
MPN/GRAM =
Tot. SoNd5 ` x 100
CHECKED BY: L14
COPY MADE:

CAMP LEJEUNE WWTP
ATAD SLUDGE FECAL ANALYSIS
PATE COLLECTED: L� DATE RECEIVED: { --�— DATE ANALYZED:
TIME COLLECTED: TIME RECEIVED: TIME ANALYZED: u j
COLLECTED BY: RECEIVED BY: ANALYZED BY:
METHOD: SM 9221C-,E - 2006 [MULTIPLE TUBE FERMENTATION]
3 HOURS AT 35 ± 0.5-C IN INCUBATOR 1 21 +2 HOURS AT 44.5 ± 0.2'C IN WATERBATH
COMB. OF
SAMPLE LOCATION 1 10 mL 1 1 mL 1 0.10 mL 1 0.010 mL 10 mL 1 mL 0.10 mL 0.010 mL POSITIVES MPN / mL' MPN 1100 mL2
0 15 mL U / 5 mL U 15 mL (D 15 mL 4 15 mL q 15 rnL 0 15 mL 0 15
DUP V /5nil- 0 1Sm:
3 HOURS AT 35 + 0.5°C IN INCUBATOR
DATE IN INCUBATOR: (Z - -A - , S DATE OUT INCUBATOR:
TIME IN INCUBATOR: q Z TI TIME OUT INCUBATOR:
INCUBATOR TEMP: 3 j, u INCUBATOR TEMP: j V
21 + 2 HOURS AT 44.5 + 0.2°C IN WATERBATH
DATE IN WATERBATH: 4 'Z- DATE OUT WATERBATH l - _"3-U `A,J
TIME IN WATERBATH: ` — 3 TIME OUT WATERBATH C o �f
WATERBATH TEMP; l l 1 `1 WATERBATH TEMP: 4/t
POSITIVE
NEGATIVE
BLANK
CONTROL
CONTROL
SS A-1 BROTH
DS A-1 BROTH
(y
Z
ya
V V
MPN Index Value
MPN) ML'a
Largest Sample Volume
MPN ! 100 mL' , (100)(MPN ! mL)
4,5.0 1 0`I-11 1 41.1
MPN/GRAM'
IR.3,
% TOTAL SOLIDS
(ATAD SOLIDS
ANALYSIS
4/. ,3
MPN / mL'
MPN/GRAM'=
%Tot. Solids'l x 100
CHECKED BY:
FORM UPDATED- DECEMBER 2017 COPY MADE:
M

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
IQ. II. It
0-703
W14LKJ;P
SM 8221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
I2.It . l8
0703
WQ12346
DATE ANALYZED: IQ. 0-I?
TIME ANALYZED: 08 ;Lb
ANALYZED BY: L-
Enclosure;
SAMPLE
LOCATION
3 HRS AT 35 + 0.5-C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2'C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN 1 mL'
10 mL
1 mL
0.10 mL _
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
T �- e
0 15
� 15
Q 15
O 15
� 15
t5
0 15
0
15
0-5 -- o
- D
a .q �f
o. O 9LI
DUP
D 15
1s
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
s nvurc� �► i oa
i�.{i•1$
O $3b
3 S.0 -c
c � : � nvurc� r� � a•r.�
l2•ll•1�
jl H�
-C
0.5°C IN INCUBA
DATE OUT
TIME OUT:
TEMP:
OR
113�
3s_ b -C
i + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
P
N
DS A-1 BROTH
1
N
1"
d8�{5
LtLf• -c
MPN I mL' = MPN Index Value
Largest Sample Volume
(from comb. of positives)
MPNIGRAM2
% TOTAL SOLIDS
14 . o -1
MPN/GRAM' MPN r mL
Total Solids
(expressed as a decimal)
CHECKED BY V
COPY MADE
FORM UPDATED OCTOBER 2018

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
�roSO
SM 9221C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO.
Ja rg.r8
D`7D0
L'
W012346
DATE ANALYZED:
TIME ANALYZED:
ANALYZED BY:
Enclosure
1--2 )8 18
0$ 50
--------------
3 HRS AT 35 + 0.5°C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2°C IN INCUBATOR
COMB. OF
MPN INDEX
MPN / mL'
SAMPLE
POSITIVES
VALUE
LOCATION
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.01110 mL
� �
Q 15
IS
Q 15
f5
15
15
0 15
V 15
�a..0
0
0'13
1
�.��
v
DUP
15
f5
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HOURS Al 35 +
1a.18•i$
U R a-G
S S .v •C
0.5°C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP: 3� ' •C
0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
lz-i9-It
049
4,a- 'C
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
DS A-1 BROTH
FORM UPDATED OCTOBER 2018
SPe-.Sa-mil` -
LAr•19.14
MPN / mL' = MPN Index Value
Largest Sample Volume
(from comb of posllives)
MPN/GRAM'
9'91
% TOTAL SOLIDS
MPN/GRAM = MPN / mL
CHECKED BY
COPY MADE
% Total Solids
(expressed as a decimal)
93

DATE COLLECTED:
TIME COLLECTED:
COLLECTED BY:
METHOD:
I Z 27- 0
o-720
li (C.- C
SM 9221 C E-2006
MCB CAMLEJ WWTP
ATAD SLUDGE FECAL ANALYSIS
DATE RECEIVED:
TIME RECEIVED:
RECEIVED BY:
PERMIT NO. I WQ12346
DATE ANALYZED: 2� I
TIME ANALYZED: C) 19 Is3Ile
ANALYZED BY:
Enclosure {
SAMPLE
LOCATION
3 HR5 AT 35 + 0.5•C IN INCUBATOR
21+2 HRS AT 44.5 + 0.2•C IN INCUBATOR
COMB. OF
POSITIVES
MPN INDEX
VALUE
MPN I mL r
10 mL
1 mL
0.10 mL
0.010 mL
10 mL
1 mL
0.10 mL
0.010 mL
P—U 6
0 15
15
f� 15
1s
15
E5 15
0 15
15
2r 5-U
DUP
O 15
k 15
DATE IN:
TIME IN:
TEMP:
DATE IN:
TIME IN:
TEMP:
3 HDUKb A I Jb +
�GpG
3�`. o •c
0.5°C IN INCUBATOR
DATE OUT:
TIME OUT:
TEMP:
71 + 2 14Cfl IRS AT 44.5 + 0.2°C IN WATER BATH
DATE OUT:
TIME OUT:
TEMP:
Z- S-1R
O oo
CONTROLS:
POSITIVE
NEGATIVE
BLANK
SS A-1 BROTH
�%
N
DS A-1 BROTH
T
N
QJ
MPN I mL' = MPN Index Value
Largest Sample Volume
(from comb. of positives)
MPN 1 GRAM=
TOTAL SOLIDS
MPN/GRAM? =
MPN ImL
% Total Solids
(expressed as a decimal)
CHECKED BY be
COPY MADE,
FORM UPDATED OCTOBER 2010

CAMP LEJEUNE BENCH SCALE ATAD VOLATILE SOLIDS REDUCTION ANALYSIS
START-UP 12/7/2018 A B C D E F G H I J
DATE
TOTAL VOLATILE
IN-HOUSE
WT OF
SAMPLE
WT OF
SOLIDS
° /°
WT OF
ASH
SOLIDS
%
%VOLATILE
SAMPLE
ATAD
WT OF DISH
DISH+WET
WEIGHT
DISH+DRY
WEIGHT
TOTAL
DISH+ASH
WEIGHT
WEIGHT
VOLATILE
WEEKLY
SOLIDS
TEMP
DATE
DIGESTION
SOLIDS
SOLIDS
SOLIDS
SOLIDS
AVERAGE
REDUCTION
0'C
(g)
(g)
(g)
(g)
(g)
(g)
[8-A]
(g)
[D-A]
(E/C]X100
(g)
[G-A]
[E -H]
[1/E]X100
I.H. ATAD 73.2911 78.31 5.02 73.3824 0.0913 1.82 73.3321 0.041 0.0503 55.09 55.17 21.8
12/10/2018
DUP 74.6251 79.63 5.00 74.7167 0.0916 1.83 74.6661 0.041 0.0506 55.24
I.H. ATAD
73.2933
79.29
6.00
73.3935
0.1002
1.67
73.3365
0.0432
0.0570
56.89
57.24
-3.25
21.8
12/14/2018
DUP.a 73.6043 78.6 5.00 73.688 0.0837 1.68 73.6398 0.0355 0.0482 57.59
u-
M
I.H. ATAD
86.3978
91.4
5.00
86A667
0.0689
1.38
86.4267
0.0289
0.0400
58.06
57.78
-2.05
26.1
12/21 /2018
DUP 75.5368 80.54 5.00 75.6055 0.0687 1.37 75.566 0.0292 0.0395 57.50
Sa,
1.H. ATAD
72,3196
77.32
5.00
72.4021
0.0825
1.65
72.358
0.0384
0.0441
53.45
53.51
7.92
25.0
12/28/2018
DUP 74.3219 79.32 5.00 74.4048 0.0829 1.66 74.3604 0.0385 0.0444 53.56
I.H. ATAD
74.3241
79.32
5.00
74.4258
1 0.1017
1 2.04
74.3717 1
0.0476 1
0.0541 1
53.20
53.18
1 0.48
20.4
1 /4/2019
DUP 74.6261 79.63 5.00 74.729 0.1029 2.06 74.6743 0.0482 0.0547 53.16
I.H. ATAD
86.3979
91.4
5.00
86.528
0.1301
2.60
86.4565
0.0586
0.0715
54.96
54.74
-3.31
15.9
1/11/2019
DUP 86.0365 91.04 5.00 86.1715 0.1350 2.70 86.0979 0.0614 0.0736 54.52
VOLATILE SOLIDS REDUCTION = INITIAL VS - FINAL VS X 100
INITIAL VS
(VSR < 15%)