NCS000030_MONITORING INFO_20181213

STORM WATER -DIVISION CODING -SHEET
PERMIT NO.
N cS Dioq
DOC TYPE
❑ FINAL PERMIT
K MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑
YYYYM M DD

.We, oe.)
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number NCS 000030
FACILITY NAME _Air Products and Chemicals Inc.
PERSON COLLECTING SAMPLE(S) _J. Powers
CERTIFIED LABORATORY(S) _PACE Analytical Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Rockingham
PHONE NO. (_336 ) 349-2962
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
Date
50050
00400
00556
00530
No.
Sample
Collected
Total
Flow if a
Total
Rainfall
pH
HEM Oil &
Grease
Total K,jeldahl
Nitrogen
Nitrogen,
NO2/NO3
Total Nitrogen
TSS
mo/dd/ r
MG
inches
m IL
in IL
m L
m /L
m /L
001
10/26/18
0.203861167
1.0
7.07
ND
ND
0.39
0.83
7.4
Mr
y
� v
CE
JTRAL FILES
DV
IR SECTION'
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _X_ yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/ddl r
MG
inches
m /l
m /l
unit
al/mo
001
10/26/18
0.203861167
1.0
NA
ND
7.4
7.07
75
Form SWU-247, last revised 21212012
Page I of 2

STORM EVENT CHARACTERISTICS:
Date _10/26/18
Total Event Precipitation (inches): _1.0
Event Duration (hours): _8 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable— see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
x - -- tag- (I2)
(Signature1of Per ittee) (Date)
SeA'.: A- C-,u'fir~'t�u T C�al�sf
Form SWU-247, last revised 21212012
Page 2 of 2

ceAnaocal'
YrMM.peL9fLDS.t?Pri!
November 12, 2018
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: STORMWATER
Pace Project No.: 92405137
Dear Mr. Owens:
(COPY
Pace knalytical Serviep, LLc
205 Es d [meadow Road - Stite A
Eden, NC 27PW
Enclosed are the analytical results for sample(s) received by the laboratory on October 29,
The results relate only to the samples included in this report. Results reported herein confor
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Man
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
Tlve report shalt not be reproduced, exospt in U,
vAum t the written earoent of Pace Artaly&W Services, i1C.
18.
to the
Pape 1 of 12

AlR L
PRODUM L—�
DELEGATION OF CORPORATE AUTHORITY TO NON -OFFICER POSITION'S
lz
1 jipE]
The undersigned, Geo_ffrev P. Wyatt, In my capacity as Vice President - Global Product Suooly. Gases and
Btauiament Group of Air Produgig find C emi is Inc., pursuant to resolutions of the Board of Directors, hereby
delegates authority as described herein below to the following non -officer posiUon(s):
POSMON Tr rU AND COMPANY
See attached Page 2 for list of position titles
MAYJM.UM VALUE
NIA
DESCR1P'nON OF AUTHaR1TY
Authority to execute permit applications, permit related submissions and documents, and all routine filings and
documents required by local, state, and federal regulatory agencies or authorities pertaining to environmental,
health and safety compliance for the APCI facilities.
❑ibis aulhorty may be subdelegated with the Mlowfng reaftt ons of aro:
This auftr ty may not be aubdel 4M&i
to take effect when countersigned by the Corporate Secretary or any Assistant Corporate Secretary and to continue
in effect for so long as the designated position title(s) remain unchanged, or until such authority shall be revised or
revoked by notice thereof by the undersigned, his or her successor in office, or the person to whom the designated
position(s) report.
✓ �f✓ &j
Sigmature Dark
Countersigned by:
carp �A�:�t ca��r� satza�.1;�t4

AIR L -
RELEGATION OF CORPORATE AUTHORITY TO NON -OFFICER POSITIONS
Page 2 Delegati® No.
Inc
POSITION TITLE AND COMPANY I (each 3�ra'nsactiMUM VALU tact}
PSO Global CPI Manager
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plat Superintendent
Construction Manager
Environmental Manager
EH&S Manager
Manager - Field EH&S
Regional EH&S Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
EH&S Specialist
Senior EH&S Specialist
Principal EH&S Specialist
Senior Principal EH&S Specialist
Lead EH&S Specialist
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmentai..Specialist
*In addition to the titles fisted above, the following individuals, who
may hold one of the titles listed above, should also be included:
Jeffrey L. Henninger
Joseph T. Succella
Keith B. Adams
Damian J. Maminek
Gerard P. Thompson
Michael R. Wambaugh
Farm 3999.2 ala'. 71961
NIA

AIR
FRODPM X=
Air Products and Chemicals, Inc.
2 Gulf States Utility Rd.
Baton Rouge, LA 70805
Telephone [phone]
Certified mail: return receipt requested
June 1, 2018
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NCS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320 RECEIVED
Dear Sir or Madam:
JUN 0 6 2018
CENTRAL FILES
DWR SECTION!
Enclosed please find one original and one copy of the Spring 2018 Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility. A copy of the cover page from the analytical
lab report is included to provide evidence the DMR is being submitted within the 30 day requirement.
If you have any questions regarding this submission or require additional information, please feel free to
contact me directly at [phone] x-11 or via email at [e-mail].
Sincerely,
A* oj'c't-_4�
Stephen Arceneaux
Sr. Environmental Specialist
Air Products and Chemicals, Inc.
Industrial Gas Organization
Baton Rouge, LA
Cc: Levi Owens —Air Products, Reidsville Site Supervisor

Permit Number NCS 000030
FACILITY NAME _Air Products and Chemicals INC.
PERSON COLLECTING SAMPLE(S) __J. Powers_
CERTIFIED LABORATORY(S)—PACE Analytical_
Part A: Specific Monitoring Requirements
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Lab #
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: 2018
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY Rockingham
PHONE NO. (_336) 349-2962
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
00400
00556
00530
Total
Flow if a
Total
Rainfall
pH
HEM Oil &
Grease
Total Kjeldahl
Nitrogen
Nitrogen,
NO2/NO3
Total Nitrogen
TSS
mo/ddl r
MG
inches
m IL
m /L
m /L
m IL
m /L
001
04/24/18
0.30579175
1.5
7.12
ND
ND
0.27
0.58
4.3
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _X_ yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
-
moldd/ r
MG
inches
m I
m I
unit
allmo
001
04/24/18
0.30579175
1.5
NA
ND
4.3
7.12
75
Form SWU-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date _4/24/18
Total Event Precipitation (inches): _1.5
Event Duration (hours): _6 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
' AW4, k GAtA.-5L2 4(((tB -
(Signaturi of Pe ittee) (Date)
S#_A► yX_ Er ,. at �0.t:a<i5{`
Form SWU-247, last revised 21212012
Page 2 of 2

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May 08, 2018
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: STORM WATER
Pace Project No.: 92382285
LUK
Pace =ee.LLC
205 East Meadow Road - Su1W A
Eden, NC 27=1
Dear Mr. Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on April 25, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNUNELAC standards and the laboratorys Quality Assurance Manuel, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
4
Clayton McCrickard
clayton.mcc [e-mail]
[phone]
Project Manager
Enaosurm
(0repOF LABORATORY ANALYSIS
otREPORT
This w s6 not be reprodmccL exoept in full,
*Mx t tha wAttan wownt of race An* tat Serrioes. LLC.
Pape 1 of 13

AIR
PRODUCTS Z=
Air Products and Chemicals, Inc.
2 Gulf States Utility Rd.
Baton Rouge, LA 70805
Telephone [phone]
Certified mail: return receipt requested
November 9, 2017
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RE: NCS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
Enclosed please find one original and one copy of the Fall 2017 Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility.
If you have any questions regarding this submission or require additional information, please feel free to
contact me directly at [phone] x-11 or via email at [e-mail].
Sincerely,
Stephen Arceneaux
Sr. Environmental Specialist a?
Air Products and Chemicals, Inc.F/��>>
Industrial Gas Organizationcr1 <F�
Baton Rouge, LA 0 l
Cc: Levi Owens — Air Products, Reidsville Site Supervisor

AN
Permit Number NCS 000030
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
FACILITY NAME _Air Products and Chemicals INC.
PERSON COLLECTING SAMPLE(S) _J. Powers
CERTIFIED LABORATORY(S) _PACE Analytical Lab # 460025_
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory_)
COUNTY Rockingham
PHONE NO. (_336) 349-2962
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
00400
00556
00530
Total
Flow if a
Total
Rainfall
pH
HEM Oil &
Grease
Total Kjeldahl
Nitrogen
Nitrogen,
NO2/NO3
Total Nitrogen
TSS
molddl r
MG
inches
m /L
m /L
m /L
m /L
m /L
001
10/16/17
0.203861167
1.0
7.05
ND
ND
0.33
0.77
17.1
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? X_ yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
molddl r
MG
inches
m /I
mg/1
unit
allmo
001
10/16/17
0.203861167
1.0
NA
ND
17.1
7.05
75
Form SWU-247, last revised 21212012
Page 1 of 2

r,0
STORM EVENT CHARACTERISTICS:
Date _10116/17
Total Event Precipitation (inches): _1.0
Event Duration (hours): _5 (only if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
r((a((-7
(Signatu a of Pef ittee) (Date)
5C._ 6^uV�onr.art�l �0ec.wa(is t'
Form S W U-247, last revised 21212012
Page 2 of 2

MODue 2L ODefspeHon ofA&gharffy to Mary-Gffkar PpwHIO s
r•Y M1�.f1��
The weasel Vied. Robert 0. t7rkrr_ in rsgr cap" as Vee Presrdant — Global t nan jadao of g: M,eu arid_
gbff**!L kr- pursueru b the Ddnau = of Aul<tprhy Pfl6Cy, hereby daWples atrthartfy as desciftd holes below to
the tdbM" non-owcer pwftn(s}.
FOWTW TMAM CflN: Wa U VALUE
Rh
See atUChed Fag= 2 for W at posman On WA
DISMIPftOrr OF AUTHOaW
Authority to e;ecule pendt appli<aftu. psr ra rotated svbrrMkm and dcownertts. and routine Mmgs and
downents required by twat, elate. and federal regulatory age or;aAhMTes pertairanp to enviro4trnenlat.
health, and safety corrtprlanm for the Wows Barre, Gsrdnsr, Criwan tdtary and Prom Mesnbranas f8c tes
OTtn My cm auoaafaparad w4h wa raaor+M fawrWOM br OMYI
W tM- err "M► not &W>x bdarasaua.
to take effect when courdetttlgtwa by Me Corporate Searelary or arty Assist'W Corporals Secretary and to cornir" to
effect far to " as the designated pasmon titta(sy ramain tr'TohsrMpd. or uM ouch atuMcrity shah be nrnxcd or
revoked by tctme thereof by flee undermigns a he or het st =Mor ei office. or RM p VWM to whm the de sled
poswgwgs) report.(/ 21,
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SWPA
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ll+w- .,v. ttniA�h t t rooma trrrrs.ur %nlc
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Paccu 7SAt/� 2L Detagation of Authority to Non4 ffreer Pasltio"s
Pr]snm TITLE
OperatW" manns-
LneAftmagw
She mvm% er
Assahm She Mir
We Suparvlsor
plane mmagor
As#bunt Plant Manager
Plant Ss�rhrtetrdsrt!
Cortshm4ion Manager
£e+Mrorrr�rr[ei Manager
Ernr=Wwtal Ett;hw
senior 6rwkOAnvneel Engineer
Principal Environmental Engh m
Settler Prtnoriral Errvirorrrrmrdm 6ngmaer
Load &wftmnimful EnWw r
EnWr4rmw tat SpecWbt
so=Envemmutw specia6at
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SQ*W Princtpat Envkcrtare nbW Spmaiia
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MIA

Permit Number NCS 000030
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
SAMPLES COLLECTED DURING CALENDAR YEAR: 2017
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
FACILITY NAME _Air Products and Chemicals INC. I1 ,ED
PERSON COLLECTING SAMPLE(S) _J. Powers V
CERTIFIED LABORATORY(S) _PACE Analytical Lab #�N 2011
Lab #
Part A: Specific Monitoring Requirements
CENTRAL FILES
DWR SECTION
COUNTY Rockingham
PHONE NO. (_336 ) 349-2962
SIGNATURE OF PERMITTEE OR DESIGNEE
REQUIRED ON PAGE 2.
Outfall
No.
Date
Sample
Collected
50050
00400
00556
00530
Total
Flow if a
Total
Rainfall
pH
HEM Oil &
Grease
Total Kjeldahl
Nitrogen
Nitrogen,
NO2/NO3
Total Nitrogen
TSS
mo/dd/ r
MG
inches
m IL
m IL
m IL
m L
m /L
001
05/23/17
0.407722333
2.0
7.10
ND
ND
0.22
0.28
11.0
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _X_ yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Acti ity MonitoringRe uirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total
Rainfall
Oil & Grease
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor
Oil Usage
mo/ddl r
MG
inches
m /I
m /l
unit
al/mo
001
05/23/17
0.407722333
2.0
NA
ND
11.0
7.10
75
Form S W U-247, last revised 21212012
Page 1 of 2

STORM EVENT CHARACTERISTICS:
Date _5/23/17
Total Event Precipitation (inches): —y if applicable — see permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
C �567
(Sig,A441nature of Permittee) (Date)
Form SWU-247, last revised 21212012
Page 2 of 2

ARM
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Authar0y to amaut+e pwn* appkarmu. pWMR mW tsd subattsisiora srxf dwAMUs, and rvuttnrt filings and
docaxmnts roquired by total, state. "federal rogutatory ap nchs or auth=Tm perkwwtg to environmentat
he8hh, and safetycarr>pbmofor the Wfts 8eme, Gardner, Cry"thiury and Pmm Meanbranas irraldws
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effect far so tong as ftte +yesi"ed ppSMM ftldep) remain w ch:rtged. or umd such autherlty 51=4 be nmoW Or
mvohed by mme IherW by the undarsWv4 to or hat sumn3or M off M or the p"m to whom me desrpr o*d
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Pace Anelytical SWVI W, LLC
• 205 Esst Meadow Read - Sutte A
e�0�
Eden, NC 27288-
[phone]
June 07, 2017
Mr_ Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project Stormwater
Pace Project No.: 92341712
Dear Mr. Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on May 24, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
pg--
Term Page for
Clayton McCrickard
clayton. [e-mail]
(336)62"921
Project Manager
Endoeums
REPORT OF LABORATORY ANALYSIS
This report dW not be reproduced, except in full,
wtthout the wittfen ooneent of Pace Analytical SeNces, LLC. Page 1 0113

�nrtpeoebb`oom
I
Project Stommater
Pace Project No.: 92341712
Paco Ana"cat Sorvieea, LLC
205 last Usadow Road - SufteA
Eden, NC 2rM'
(33eP23-6921
Charlotte CwWcadon IDs
9800 Klnoey Ave. Ste 100, HunWavtlle, NC 28M
North Carolina Drirddng Water Certification t. 37708
North Carolina Field Services Cer1iicabon ttl• 5342
North Carolina Wastewater rm fill-H' r #: 12
Asheville CwMCWon On
2225 Riverside Drive, Asheville, NC 28W
FloridalNF_LAP Certification d: E87848
Massechusetxs Certification f M-NCO30
North Carolina Drinking Water Co.fftatim * 37712
Eden Certification We
206 East Meadow Road Sults & Eden. NC 27288
North Carolina Drbdctng vwter Certification V. 37738
CERTIFICATIONS
South Carolina Carmen M 99006001
FloridaMELAP Certification 6: E87627
Kentucky UST Cerkfiration 0. 84
VirginialVi=L.AP C401cstW *. 46=1
North CamMa fstewater Certifim� Ilt: 40
South Carofhta Certiticatlon #. 99030001
VfrginkWELAP Caftitkatfon 460222
North Carolina Wastewater Cart kadon #
V40laNELAP Ca ltcWon V. 4WW5
REPORT OF LABORATORY ANALYSIS
This report Mall not be reproduced. except In U,
wtthout the wrHten O XMffE of Pane anat Cal Servtoes, L LC. Page 2 of 13

Pne Analytical GQrvicea, LLC
ne /j.�,� n� a 205 East Meadow Road- SUftA
LCX Ana4ft tl Eden, NC 27=
(338)5234M
SAMPLE ANALYTE COUNT
Project: swmnweb
Pace Project No.: 92341712
Lab 10 Sample ID Method
Armlysb
Arralhrtas
Deported
Laboratory
9=1712001 8tormwebw Outfall 1 SM 2540D
CHM
1
F ASi-E
EPA 16648
JMS
1
PASI-C
TKN+NO3+NO2 Calculation
EV4
1
PASI-A
EPA 3512
BRJ
1
PASI-A
EPA 353.2
AES2
1
PASI-A
REPORT OF LABORATORY ANALYSIS
Thts repon w w not be Mprodioed. axoept in 1A
wWoM ft written oonaent of Pace An*dcW semcm, LLC. Pape 3 of 13

(�Wcl WOWPKSMIGM
ANALYTICAL RESULTS
Project: Stormwater
Pans Project No.: 92341712
PeCoAnaly" t3sr km% LLC
206 East Meadow Road - Sults A
Eden. NC 27288-
M5)623-8921
Sample: St omwa ier OuIW 1
Lab 10: 92341712M Collected: 05=1714:10 Received:
05JAM 1
:10 Malriac VVMw
Parameters
Results Unb
Report Limit
DF Prepared
Ana
Vzod CAS No. Quaff
21140 Total Suspended Solids
Analytkal Method: SM 25M
Total Suspended Solids
11.0 M91L
2.5
1
05125M
7 10.03
HEK Oil and Orono
Anaykal Method: ERA 1664B
Oil and Grease
ND MOIL
5.0
1
05M
06:22
Total Nitrogen CatcutadYlon
AnalytUml Method: TKN+NO3+NO2 CalculMn
Total Nitrogen
0.26 rnglL
0.12
1
Ot3/06/1
7 18:43
351.2 Total Kodahl NitmW
Analytiral Method: ERA 351.2
Nitrogen, Neldahl, TOtai
ND mgR
0.50
1
05/31/1
02:49 7727-37-9
353.2 Nitrogen, M02MM pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NOS
0.22 MOIL
0.020
1
0610911
14:14
Data: 06/07/2017 07:37 AM
REPORT OF LABORATORY ANALYSIS
Ttft report shah rat be r OF m 111aI , 1-1; t In fun,
wMxM the wdW oaumarat of Peas AmMcal Services, iLC.
Page 4 of 13

/�ace,4nary6cai
QUALITY CONTROL DATA
Project stomtwater
Pace Projed No.: 92341712
QC Batch: 362153 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended SoWs
Aasoclated Lab Samples: =41712001
METHOD BLANK 2008245
AssodffW Lab Samples: 02341712001
Parameter Units
Total Suspended SoBds nv/L
Matft Water
Blank Reporting
Result L bm Analyzed
ND 2.5 05/25/17 WAS
LABORATORY CONTROL SAMPLE: 2008246
Spike LCS LCS % Reo
Parameter Urrlts Conn Rama % Rea Units
Total SumperKW SOlids mg/L 250 252 101 90-110
SAMPLE DUPLICATE: 2008247
92341521003 Dup
Parameter Urdta Result Result RPD Qualifiers
Total Suspended Sokis rng/L. 35.0 352 1
SAMPLE DUPLICATE 2008246
92341594002 Dup
Parwrieter Units Result Result RPD Qualifiers
Total Suspended Solids rng1L 43.3 25.8 51 D6
Rpanit pnogrod an aft pep aft In tier undo rodkand by tM 'UtAW oa{mm eecW wim m eRwmeet wi! ie preeaaLed 4o th
REPORT OF LABORATORY ANALYSIS
This report ahan not be reproduesd, except in nm,
Date: 08/07/2017 07:37 AM wwmd the wrtban oorment d Paoa Arraydt:al Services. LLC.
Pam AnBlpt Cd Serrlcea, LLC
205 East Meadaw Road - Sure A
Eden, NC 27288-
(=023-Ml
AOd� ar trr reetit.
Page 5 of 13

AncaP
i
QUALITY CONTROL DATA
Pmjeat Stormwater
Pace Project No.: 92341712
QC Batch: 363117
Analysis Method:
EPA IBM
QC Batch Method: EPA 188413
Analysis Dasczipdon:
1684 HEM, OR and Grease
Assodated Lab Samples: 92341712001
METHOD BLANK 2013158
Mavk Water
Assodatsd Lab Sampies: 9234m2001
Bku* ReporWV
Parameter
Units
Result Writ
Analyzed Qual>fie
Oil and Grease
MOIL
ND
5.0 05W17 05:08
LABORATORY CONTROL SAMPLE. 2013159
Spate LCS
LCS % Roe
Parameter
Units
Cont. Result
% Rec Ua is
O!l and Grease
MOIL
40 38.3
95 76-114
Pme Analyt I Semtaos, LLC
205 East Meadow Road - Sidle A
Eden, NC 27288'
[phone]
MATRIX SPIKE SAMPLE: 2013160
92341645004 Spare MS MS % Roe
Parameter Units Result Cont. Result % Roe Limits Qualifiers
Oil and Grease mWL ND 40 37.0 93 78-114
Rouib prMu - on Oda p W � rn &a rune brmc4ftd by do'SMder" oukarar aeoepe e 0 in eemrueme Ufa Is prrsu I es flr
REPORT OF LABORATORY ANALYSIS
Tft report OW not be repraduoed, a xoW In fu 1,
Date: DOM7=17 07,37 AM without the wrMten corawd of Pace An*dcw Seerioes, LLC.
i dgm den. rawrl
Paw 6 of 13

QUALITY CONTROL DATA
Project Stonymater
Pace Pm)W No.: 92341712
QC Batch: 3825% Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Pted Lab Samples: 92341712001
METMOD BLANK: 2010159
Associated Lab Samples: 92341712MI
Parameter Units
Nitrogen, Kjeidahl, Total mg&
Mabk 4Vhter
Blank Reporting
Result LLnitt Analysed
ND 0.50 05131n702:40
Pac* Anetytloal Sdf t ", LLC
205 East Meadow Road - Sutte A
Eden, KC 272W
(336)82343921
LABORATORY CONTROL SAMPLE: 2010160
Spike LCS LCS % Rea
Parameter Units Cont. Result % Roe Lonna Qualifiers
Nitrogen, Kjekfahl, Total mgA- 10 9.3 93 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2010151 2010152
MS MSD
92341958001 Spice Spike MS MSD M5 MSD % Rec
Parameter Units Result Cone. Cona Result Result % Rec % Raw, Lw to ftPD Qual
Nitrogen, IQeklahl, Total mg/L 1.1 10 10 9.5 9.7 83 86 900.110 2 M1
R WArs pnrwrerd on Ihr pop m in pn urft bxOcmd by On'UnW wham Iffm Ir t to Is P rlpfit of tm molt,
REPORT OF LABORATORY ANALYSIS
TMe report ehai not be reproduced, m=pt In IWI,
Otte: 08/072017 07:37 AM wWxxA the wr ftn oormwd of Pow Maly0cal Servims, LLC. Page 7 of 13

Poo AnaPyucal Sanlps, LLC
��Meadow �-��p
Cep!'
Eden, NC 27288
XM)t
QUALITY CONTROL DATA
Project: StonTrAr her
Pace Project No.: 92341712
QC Batch: 383292
AnaysisMebw& EPA353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, press
Associated Lab Samples: 92341712W1
METHOD BLANK 2014134
Matrix Water
Associated Lab SaMPISS: 92341712W1
Blank Reporfing
Parameter
Units Result Lin* Analyzed Qualms
ra
Nitrogen, NO2 plus NO3 mglL ND 0.020 0610311714:04
LABORATORY CONTROL SAMPLE
2014135
Spice LCS LCS % Roe
Panwwftr
Unite Conc. Result % Rec Lerfit8
Qualifiers
Nit ,open, NO2 plus NO3 MWL 2.5 2A 98 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 201413e 2014137
MS MSD
92342343004 Spice Spice MS MSD MS MSD
% Rex
Parameter
Units Result Conc. Conn Result Result % Rex % Red
Limits RPD Qual
Nitrogen, NO2 plus NO3
rnglL 0.061 2.5 2.5 1.8 1.7 64
64 75-125 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2014138 2014139
MS MSD
92341890001 Spice Spice MS MSD MS MSD
% Roe
Parameter
Units Result Canc. Conc. Result Result % Rec %
Limb RP0 Qua!
Nitrogen, NO2 plus NO3
M01L 10.0 2.5 2.6 13.5 12.4 141 1
lt5 75.125 9 M1
Raarr4 Prod an fdb pW main nM artlb m air mam urdt O pto am
rem of do ro uti
REPORT OF LABORATORY ANALYSIS
TW report mall not be rspoduMd, enoept In M,
)ate: 06J072017 07:37 AM
wlthaut ft wften oomerd of PaceArw*ftal Serrioe% LLC.
Page 8 of 13

QUALIFIERS
Project: Stomwmter
Pace Project No.: 92341712
DERNMONS
DF - Mution Factor. d repor6ad, represents the factor app0ed to the reported data due to daution of the sarnple
ND - Not Detected at or above edprstsd reporting Ihrct.
J - Estimated concentration above the adpAW method detection tirrdt and below the adjusted reporting tirnit.
MDL-Adjusted MoViod Detection UmiL
PQL- Practical Quantitation Umit
RL - Reporting U niL
S - Surrogate
1,2-1)iphenylhydmzlne daoornposes to and cannot be separated frimAzobenxene using Method SM. The resuR
a conftied concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to Calculate % reoovery and RI
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spke (Duplicate)
DUP - Semple Dupfieata
RPD - Relative Percent Dillarence
NC - Not Calculable.
SG - Sr'M= Gel - Clean -Up
U - Indicates the cornpound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 ChlomethyMnyl ether_
A separate vial preserved to a pH of 4-5 Is recommended In SW846 Chapter 4 for the analysis of Atxobin and
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphanytandne using Method WM. The
each analyte is a con nod concentration.
Pace Anst tic Is TNI acaedited. Contact your Pace PM for the current fist of accredited analyles.
TNI - The NELAC Institute.
LABORATORMS
PAST -A Pace Analytical Services -AshevMe
PASI-C PaceAnayticel Services- Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
DO The precision between the sarnple and sample duplicate exceeded laboratory control Amy.
M1 Matrix spike recovery exceeded OC Iirri ts. Batch accepted based on laboratory oontrol sarnimIe (LCS)
REPORT OF LABORATORY ANALYSIS
PWO Analytical SWVWSe, LLC
205 East Meadow Road - Suite A
Eden, NC Z72atl'
each anayte is
values.
MOO by EPA
reported for
TTds report shag not be repr0du04 ex0ept in h9l,
Date: 06107/2017 07:37 AM wM-A the wHsen oonsent of Pace Ana"wif Servioas, LLC. Page 9 of 13

SIG / U fM✓ ca
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pr*a StorT4tYrater
Pace Projed No.: 92341712
Lab 10
Sample ID
OC Batch Method
OC Batch
92341712001
sumnwater outlall 1
SM 2540D
362153
92341712001
Stonnwater OuftH 1
EPA 1684E
363117
923417120M
Stomwoater Ouftli 1
TKN+NO3+NM
383648
Calmmon
92341712M
Sto mvrat9r Outten 1
ERA 351.2
3525N
92341712M
Stormwaber Otrlfall 1
EPA 353.2
363292
Data: 0610712017 07:37 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reWoducad, a xcept in fun,
without the wrmen oomont of Pace Anarytieal Services, LLC.
Pace Areal dMd 8ervtaM t.LC
205 Teal Meadow Road - Suits A
Eden, NC 27288 '
(336)823-892i
Artaly0Cal
Batch
Page 10 of 13

/5a,CekWytk916
i
Document Name:
Document No.:
F-CAR-CS-033-Rev.01
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersviRe ❑
Document Revised: Sept. 21, 2016
P#fie 1 of 2
Issuing AudwrtW.
Pace Quaw Office
Client Name: O#
Rohl 1�, Project 0:
Courier: �Ex UPS USPS Client
❑ Commercial Jdra ❑Other 9234 1i
Custody Seal Present? ❑Yes P Seals Intact? ❑Yes ❑fro
Padd Materl�: Dat�tiah P
Pawns ❑Bubble Wrap ❑Bubble Bags one ❑Other.
Thermometer. ,., f
❑ lit Gun ID: � of I Ki []Blue []None
Correction Factor: Cooler Tamp Corrected ('Q. l � ' Biological Tissue Froi
Temp should be above freezing to 61C
USDA Regulated Soil (❑ NIA, water sample)
Did samples orlgtnate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples ortgloate
❑Yes ONO kmAtdtng Hawaii and I
Chain of Custody present?
Samples Arrived within Hold Time?
1.
2.
3.
Sufficient Volume? yes ❑No ❑N/A I S. t
Correct Containers Used? yes ❑No C3N/A I 6.
Mechanicsville[]
?341712
11111111
6aminft
Its on Ice, coo ft process has begun
❑Yes ❑No ❑NIA
a foreign source o ntematkma ft
Containers Intact?
yes
QN0
A
7.
Samples Field Filtered?
Yes
No
N A
L
Nate If sediment Is visible t
i therdlssolved container
Sample Labels Match COV
-includes meAQJAna
0/yes13No
❑WA
9.
S�+Nti�f�S
PA Y
Headspace In VOA Vials >5-6mm 7
13Yes
No
NIA
10.
Trip Blank Present?
TripBlank CustodySeals Present?
[]Yes
' ❑Yn
❑No
Na
11N/A
[ N/A
11.
Ctturr NuTiFiCAT1oN/RESO=oN
Fldii
Data Required'! ❑Yes ONO
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Project Manager SCURF Review: V— Date:
Project Manager SRF Review: _ Date:
Note: Whenever there is a discrepancy afkcting North Carolina compdanee samples, a Copy of this form will be sent to the North
Out of hold, incorrect preseiva0m out of temp, Incorrect containers)
OEHNR Certlf eRdon Office (i.e.
Page I I of 13

Document Dame;
Document Re sat Sept. 21, M6
.
2ceAn.?YW
Sant le Condition Upon Recei SCUR
P e 2 of 2
Document No.:
Issulnq Aut xwW.
F-CAR-CS-0334W.01
Pace anry Office
*thedc mark top half of box H pH and/or dechlorination
Is verified and within the acceptance range for
presentation samples.
"Bottom half of box Is to list number of mottles
project t
WO# : 92341 7 12
PM: am � Mn "tot MUM
CL.IMM : 83-41 Pro&
MOMMUMM
MOMERIEND
MOMMii��
��nui�aaaiie■=in""�i
1 pH Adjustment Log for Preserved Samples
Sample 10 Type of Prewrratke pH upon mceipt Date pnmrvation adjusted I Time preservation Aim Aim 6 of Preservative
adjastad added
Lot #
Page 12 of 13

PaceAnalytical'
wM.paatata.eam
Section A
Required CUM Information:
Company:
AddIpSS:
Emal!a omrrQ ape.,. te.
LZ 3 Faa:
Rarptestad Ow DamtrAT.
1L;r1A1N-u1--I;US I UVY 1 Analytical Request Document
The Chalnwf-Custody is a LEGAL DOCUMENT. AS relevant ffekds must be complelad accurately.
Seckhm a Socalm Cftquftd p:9e: of
Report Ta�� Infamaron: Invoice 2129701
Copy To: Camawy Name:
Name:
REGULJ1Tt7RY AGENCY
F NPDES F- GROUND WATER j" DRINKING WATER
i UST r RCRA i OTHER
SMe Location
STATE.
Requested Analysis Filtered (YIN)
section D Matrbt codes
wgw6w0 %tnronnaft M&= r cage
prinking Water DW
B
U
COLLECTED
Preservatives
z
a
Water WT
Waste Water WW
COTra'tl5[fE
C
V
Soiltsaw
u
SAMPLE ID oil L
3
{A-7. 0-9I:) Air AR
to
a
C
a
m
Semple Has MUST BE UNIQUE Toque TS
O
F
m
p
OEOT
x
Q
m
0
g
,
0
;
1
Z
DATE
TIME
DATE
TIME
�
�
2
g
O
c
m SAMPLER NAME AND MRATUFM
w t! I.+ I.al_ PRINT Nam. of SAMPLER:
W=KATURB of SAMPLER,
a
m
Pace Project NaJ Lab LD.
I-YA14111111111in'.--41111111111 1.hi
'tmp.nwu Note: By aignrq this ram you we a p" PamS NET 30 day payma d Weis ana agreeurg to late dmrgea d 1.5% per month fm any kNdces riot pa$d weMn 30 as"
F-ALL-0420rev.07. 15-Mav-2007

Pace Container Order #250324
Addresses
Order By:
Company Air Products
Contact Owens, Levi
Email powersnairproducts.corn
Address 226 Equity Road
Address 2
City ReldvAle
State NC Zip 27320
Phone [phone]
Info
Ship To :
Company Air Products
Contact Owens, Lavl
Email powers1f;Wrproducts.oDrn
Address 225 Equity Road
Address 2
City RaklW119
State NC Zip 27320
Phone [phone]
Project Name Storm water Due Date 05 2312017 Profile
Project AtWWW McOk wd. EM122 Ratum Carrier Courier
Return To:
Company Pace
Contact Mc o
E marl ctaytl
Address 205 E
Address 2 Sulte
City Edsn
State NC
Phone (33B)
Trip Blanks BotQe Labels Bottles
❑ Include Trip Blanks ❑ Blank ❑ Bay
o Pre-printed No Sample 02 ❑ Inds
❑ Pre -Printed With Sample IDs ❑ Gro
Return Shipping Labels MiSC
❑ No Shipper Number Sampling Instructions
❑ Nth Shipper Number ❑ Custody Seat
COC Options ❑ Temp. Blanks
❑❑ Number of Blanks El Coolers El
Syringes
❑ Pre -Printed
# of Samples Matrix Test Container Total # of t2C Lot #
lnafytical Eden I '
.kard, Clayton
IJn=[e-mail]
rat Meadow Road
27p 27288
Z38921
CNN"
cases
Lally Wrapped
ad By Sample
Ira Bubble Wrap
on HoldlRush Stickers
Water Effects)
'DA Regulated Solls
Lot Number
1
WT
Nitrate+NM% by 353.2
125'nL pissttc H2SO4
1
0
042217-4CGT
Lot Number
1
WT
TKN (total lgaidaN Nitrogen) by
1M,1 pb We H2SO4-
1
0
042217-4CGT
351.2
Lot Number
1
WT
00 and Grosse by 1 MK
1 1 L amber gkmO HU
1
0
040817-1 DAW
1
WT
TSS
t L ptastk unpres
1 10
042917-2APJ
Hazard Shipping Placard In Place: NO
'Sampe rece1vhV tours are Mon-Fd 8:00am-8:00pm and Sat via Fedex Daly unless spacial arrangements are made with your t
'Pace Analytical reserves the right to return hazardous, toxic, or radioactive samples to you.
'Pace Analytical reserves the right to charge for unused bottles, as well as cost associated with sample storage and disposal.
-Payment term are net 30 days.
'Please Include the proposal number on the chain of custody to insure proper billing.
Sample Notes
manager.
Date: 06l2212f117
W By: d plerce
d By:
Page 1 of 1
r9'9LL-WVva"ov,w, ,oypycv,v

�VMT S ,mow•
Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195-1501
Telephone [phone]
Via Certified mail: return receipt requested
February 27, 2017
NC DENR Division of Water Resources
450 W Hanes Mill Rd. Ste, 300
Winston-Salem, NC 27105
RE: NCS000030 Annual DMR Summary
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
NC Department of
Environmental Quality
Received
MAR 0 6 2017
Winston-Salem
Regional Office
Enclosed please find the Stormwater Discharge Monitoring Report Annual Summary for the Air
Products and Chemicals, Inc. Reidsvifle, NC Facility for calendar year 2016.
Please feel free to contact me with any questions or if you require additional information. I can be
reached at (22S) 355-4613, x-11 or arcenesF(@airproducts.com.
Sincerely,
Stephen Arceneaux
Sr. Environmental Specialist
Air Products and Chemicals, Inc.
Ofc [phone] x-11
Mobile [phone]
cc. Levi Owens —Air Products and Chemcials

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)1 SPPP Annual Update DATA REVIEW FORM
Calendar Year 2016
Individual NPDES Permit No.
Certificate of Coverage (COC) No
NCS❑O ❑O ❑o ❑O ❑3 ❑O or
NCG❑❑❑❑❑❑
This monitoring report summary of the calendar year should be kept on Me on -site with the facility SPPP.
Facility Name: Air Products and Chemicals_, Reidsville ASU
County: ,Rockingham
Phone Number: (336)_349-2962
Outfall No. )
Total no. of SDOs monitored 1
Is this outfall currently in Tier 2 (monitored monthly)?
Was this outfall ever in Tier 2 (monitored monthly) during the past year?
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities?
Yes ❑ No
Yes ❑ No
Yes ® No ❑
Parameter, (units)
Total
Rainfall,
inches
Flow, MGD
PH, standard
Total Nitrogen,
Oil & grease,
mglL
TSS, mg/L
New motor oil
usage, gal/mo
Benchmark
N/A
Date Sample
Collected,
mmlddlyy
5117/2016
1.5
0.30579175
7.05
0.51
ND
16.4
75
10110/2016
1.2
0.2446334
7.16
0.66
ND
24.7
75
F-
SWU-264 - Generic Annual DMR
Last revised S/17/2013

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Signs
Date
For questions, contact your local Regional Office:
DWQ Regional Office Contact Information:
SA HE_VILLE REGIONAL OFFICE
FAYETTEVILLE REGIONAL OFFICE
—
MOORESVILLE REGIONAL OFFICE
610 East Center Avenue/Suite 301
2090 US Highway 70
225 Green Street
Swannanoa, NC 28778
Systel Building Suite 714
Mooresville, NC 28115
[phone]
Fayetteville, NC 28301-5043
[phone]
[phone]
RALEIGH REGIONAL OFFICE
WASHINGTON REGIONAL OFFICE
_
WILMINGTON REGIONAL OFFICE.
127 Cardinal Drive Extension
3800 Barrett Drive
943 Washington Square Mall
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
[phone]
[phone]
[phone]
WINSTON-S_ALEM REGIONAL OFFICE
��—
CENTRALOFFICE
585 Waughtown Street
Winston-Salem, NC 27107
1617 Mail Service Center
Raleigh, NC 27699-1617
j "70 preserve protect
and enhance
[phone]
1 [phone]
North Carolina's water..."
SWU-264 - Generic Annual DMR
Last revised 511712013

PRVDCAN ;k.,�• Delegetfon of Authority to Man.Offkvr Posilfons
PY n�r.n. w
The undersigned. Sgban 2. Garrey: m my capewTy as Vre� idant — Giafsat Enoineerhro of 6jr EM"tn airs_
CUMN5818, WC.. pursuSM to the Delegattorts of Authonly Pt*cy, tsby deliagales authanty as described heron below to
the lattpwsig non-ol6cer poedlon(s).
POSMON TRTte ANo CCLWPJWY aIAJRMUM VALU[
feww,
See attached Page 2 for Of of position Iltias TWA
CHSCMMON OF AVTNOleTV
Authority to execute pemo appltastbris, garnO ■e4dW submissions and dacualents, and routine tidings and
documents required by Rocal, state. and federal regulatory agarrdes or awhadfin pertairxng to enviMnOlentai.
health. and safety compawme for the Woes Barre, Gardner. Cryornechinery and Prism Membranes laatrfies
OTna aunwty may arm aueestW WAh Iha 60*vj,, p Nalnei+ona dl tiny)
® ilex RMPOry n" rice to O'WahaMea
to lake affect when counlersfgned by the Corporate seertsfary or any Assistant Corporate Secretary and to etinifntre in
eftcl far so tang as the designated pusaion ttlte(s) rgrnain unchanged. w wud such i3LMwUy shalt be revised or
revoked by notice thereof by the urlde rilignsd, his or her successor M oNice. or the person to wh" the designated
position{s} repo6t. .�
Oro
J.-
(:auntersigntd by • � i '.�� `lL
t5.ryw�rr i t�n:A+a• it rparan- 0
tw y Ir�. I .M

PRODUCTS 'tom Delegation of Authority to Non -officer Positions
POSMON ME
Opem one Maneger
tine >wanager
Site Manager
Assmtaru Site Manager
site Supervisor
Pwd Manager
Assistant Plant Manager
Plant Superi tendeni
Ganslnrdion Manager
Envf ivnernal Manager
Envuommmial Engineer
Senior Emrlronrrmnlai Engmear
Principal tEnvtromm mW Erginaer
Senior PrOrWal E rvironmental F.ngnew
Lead EnvEnmranfai Er4rwer
Envfmnmental Speciagm
Semen Enwronrnentel SpecUffiat
Principal Envirc>nrnerda! SpeclOsl
Senior Poncfpat EnvkcnmeMel Specnaftal
"^MMUM VALUS
WA

'AIR ALIL
PRODUCTS
Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195-1501
Telephone [phone]
Via Fed Ex 7766 1392 6255
27 June 2016
NC DENR Division of Water Resources
450 W Hanes Mill Rd. Ste. 300
Winston-Salem, NC 27105
RE: NCS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
NC Department of
Environmental Quality
Received
JUN 2 S 2016
Winston-Salem
Regional Office
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility.
Please feel free to contact me with any questions or require additional information. I can be
reached at [phone] or creitzib@airl)roducts.com.
Sincerely,
e0reit
J nnifer B.Sr. Pr. Envirer
c. Coray Mitchell —Air Products

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 6 4000 Q or SAMPLES COLLECTED DURING CALENDAR YEAR: Z016
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
/ 1 the date the facility receives the sampling results from the laboratory.)
FACILITY NAME 1f �d�C 7j el0l; II I/t �SI epartment of COUNTY AOC&Afh41-7
PERSON COLLECTING SAMPLE S) mental Quality PHONE N t 6
CERTIFIED LABORATORY(5) Lab # Received
Lab # (40WUE OF PERMITTEE OR DESIGNEE)
~SUN 2 8 2016 By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A. Specific Monitoring Requirements Winston-Salem
No.
:Total
e
app.)
'
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? _yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total Rainfall
Oil & Greases
(if appl.)
Non -polar
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor Oil
Usage
motel yr
MG
inches
m
m
Units
aUmo
OVIVA,
G /
TT-
7- D
Form SWU-246-0623I0
Page 1 of 2

Certificate of Coverage No. NCG
(9odod.76
STOXMWATER DISCHARGE OVIVALL (SDO)
MONITORING REPORT
FACT M NAME l l f jSV IAt
PERSON COLLECTING SAI4IPLE(S)
CERTIFIED LA$ORATORY(S) t Lab #
..Lab # _
SAMPLES COLLECTED DURING CALENDAR YEAR: Zd��
('S his monitoring report shall be received by the Division no later than 30 days
AI from the date the facility receives the sampling results from the laboratory.)
�7fu COUNTY gi oc
PI30Ni� NO. 7 Ticz
(SIGN OF PERMIT= OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Vehicle Maintenance Activity Monitoring Requirements (only if, on average, more than 55 gallons per month of new motor oil is used)
Oatfall
No.
Date
Sample Collected,
molddlyr
TotalRainfall,
mcbes
New Motor OII iJsage,
Annual average
at/mo
00556
00530
OWN
Oil and Grease,
mgJL
Non -polar O&t (ITH
(Metbad 1664 SGT-HF, A
if a
Total Suspended Solids,
mg/L
pH,
Standard anus,
Benchmark
-
-
-
30
15
100
6.0 — 9.0
GL
Oft
Note; If you report a sampled value in excess of the benchmadc value, or outside the benchmark range for pH, you must implement Tier i or Tier 2 msponsm in the General Permit.
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this docament and all attachments were prepared antler my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person or persons who nmmge the system, or
those persons directly responsible for gathering a information, the information submitted is, to the best of my knowledge and belief, t me, accurate, and complete.
I am aware that there are signifipnt peodeAf9f submitting false information, including the possibility of fines and imprisonment for knowing violations."
Of
(Date
, 6�—j /. �—
Form SWU-254-062310
Page 1 of I

STORM EVENT CHARACTERISTICS:
Date 511; �—
Total Eve t Precipitation (inches): ,� 5
Event Duration (hours): �Z (only if applicable — see pemtit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable -- see pemut.)
Mail Original and one copy to.
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, tru accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibilit imprisonment for knowing violations."
—15-11 ;;1A
(Signs re o ermittee) (Date)
Form SWU-246-062310
Page 2 of 2

Outfall 001
Inches of Rain 1.5
Area Sq Ft Run Off Factor Ft of Rain Cubic Ft Gallons Million Gallons
Impervious Area 127000 0.9 0.125 14287.5 106870.5 0.1068705
Gravel 425500 0.5 0.125 26593.75 198921.3 0.19892125
Total 552500
Total Flow 0.30579175
Area x runoff factor x feet of rain = cubic ft of water runoff
Cubic feet x 7.48 = gallons

q !.
PRODUCTS Oefegetior, of AuthoNly to Hon -Officer Positions
:w
The uncerslgned. Robar jD. Conley. in my capacity asVice Prglidenl — Grobal Etolneerig of & Products A=
Chemic. Inc..IncInc.pursuant to the Delegations of Authority Policy, hereby delegates authority as described h&r&in below to
the following non -officer position(s),
POSITION TITLe AND COfI PANy MAi[IAIUMr VALUE
e.en 7ransVacdoniCentrael
See attached Page 2 for list of position tilt&& WA
DESCRIPTION OF AUTmOmTY
Authority to execute permit applications, permit related submissions and documents, and routine flings and
documents required by local, &rate, and federal regulatory agencies or aulhorities pertaining to environmenlat.
health, and safety compftance nor the Wilkes Barre, Gardner, Cryomachnery and Prism Membranes faclldlas
OTNI SwIftarlty May OC Sub0§189 1ld With the rO(W*PnQ MWncl*M 181 •ft)
® 003 ninew,ty may poi to wboshp ;&d.
la fake effect when counterslgneo by the Corporate Samfery or ariyAssislani Corporate Secretary and to continue In
affect for so tong as the designated position title(sj remain unchanged, or unid such authc9lity shall be revised or
revoked by notice lhareof by the undersigned, his or her successor in o tce. or the parson to whom the designated
posilion(s) report.
r
Countersigned by ' ,_ / I t
t,n,A•s»I�t1I [ �rport,W �n4'.r
Dole
Ier r ,1� � a, ✓ . r17' r��,r�n,w.�.+11 �4�

AfN /•
PrMDUCTS Delegation of Authority to Non -Officer Positions
12CSITM304 nTLE
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Silo Supervisor
Pisnt Manager
Assistant Plant Manager
Plant Superintendeni
Constnrclion Manager
Environmental Manager
Environmentat Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Sensor Principal Environmental Engineer
Lead Environmental Engineer
Environmental Speciefisi
Senior Envxonmental Specialisl
Principal Environmenlal Specialist
Senior Principal Environmental Speaabt
_..
MwwMUM VALUE
NIA

/��ac,-Analyfical*
www.psosrhs.can
June 03, 2016
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: STORMWATER
Pace Project No.: 92298242
Dear Mr. Owens:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pave Analytical Sorvlcea. Inc..
Page 1 of 8

aceAnaly cal
wwwPacetebscom
Project: STORMWATER
Pace Project No.: 92295242
Charlotte Certification 10s
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certificatlon #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Cert€licatlon M 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification lDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florlda/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VlrglnlaNELAP Certlticatton #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VlrginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virgin€aNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Ana"cal Services, Inc..
Pace Analytical 5ervlces, Inc,
205 East Meadow Road - Suite A
Eden, NC 27286
[phone]
Page 2 of 9

aceAnalytical
W WW.pmm4bs.com
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92298242
pace Analytical Services, Inc.
2u East Meadow Road - Suite A
Eden, NC 27288
[phone]
Sample: STORMWATER OUTFALL 1 Lab ID: 92298242001 Collected: 05/17/16 10:00 Received; 05/19/16 11:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qua[
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids
16.4 mg/L
2.6
1 05/19/10 14:18
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
NO mg/L
5.0
1 06/03/16 0a:52
Total Nitrogen Calculation
Analytical Method: TKN+NO3*NO2 Calculation
Total Nitrogen
0.51 mg/L
0.12
1 05/02/16 15.33
351.2 Total Kjeldahl Nitrogen
Analytioat Method: EPA 351.2
Nitrogen, Kjaidahl, Total
ND mg/L
0.50
1 05/28/16 00:56 7727-37-9
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.41 mg/L
0.020
1 06/01/16 22:16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full.
Date. 06/03/2016 01:02 PM without the written consent of Pace Anatytical Services. Inc.. Page 3 of 9

I t
aceAnalytical'
` � wt+wpaeefebamn
i
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project:
STORMWATER
Pace Project No.:
92298242
OC Batch:
EDEN122871 Analysis Method: SM 25400
QC Batch Method:
SM 2540D Analysis Description: 25401) Total Suspended Solids
Associated Lab Samples: 92298242001
METHOD BLANK: 1737550 Matrix Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.5 06/19/16 11:21
LABORATORY CONTROL SAMPLE: 1737551
Spike LCS LCS % Roe
Parameter Units Cone. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 256 102 90-110
SAMPLE DUPLICATE: 1738204
92297933003
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
159
200 23 06
SAMPLE DUPLICATE: 1738205
92297949001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
35.3
34.0 4
Results presented on this pago are In the units Ind lasted by the "Units" column exoopt where an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
r)atw nwn312016 01:02 PM without the written consent of Pace AnaMcal Services, Inc,.
Page 4 of 9

�-,;alaeAnalxical"
wMMcpecefabo.cam
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
QC Batch: GCSV125163 Analysis Method: EPA 1664E
QC Batch Method: EPA 16646 Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92298242001
METHOD BLANK: 1747600 Matrix: Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 06/03/16 08:45
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1747601
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Oil and Grease mg/L. 40 35.2 88 78-114
MATRIX SPIKE SAMPLE: 1747602
35246515001 Spike MS MS % Rec
Parameter Units Result Cone. Result % Roe Limits Qualifiers
Oil and Grease mg/L 3.4J 40 42.9 99 78-114
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 06/03/2016 01:02 PM without the written consent of Pace Ana4yticai Services, Inc.. Page 5 of 9

Analytical
WWW'Psoelab&XM
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
QC Batch: WETA127748 Analysis Method: EPA 351.2
OC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92298242001
METHOD BLANK: 1742451 Matrix: Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg1L ND 0,50 05/28/16 00:49
LABORATORY CONTROL SAMPLE: 1742452
Parameter
Nitrogen, Kjeldahl, Total
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Spike LCS LCS % Rac
Units Cone. Result % Rec Limits Qualifiers
mg/L 10 9.9 99 90-110
MATRIX SPiKE & MATRIX SPIKE DUPLICATE: 1742453 1742454
MS MSD
92298871001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 30.4 10 10 42.0 422 116 117 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1742455 1742456
MS MSD
92298756001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglL 20.2 10 10 30.8 30.7 105 105 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 01:02 PM without the written consent of Pace Analytical Services, Inc..
Page 6 of 9

aceAnaiytieai
www.pacalatw.00m
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
OC Batch: WETA127795 Analysis Method: EPA 353,2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92298242001
METHOD BLANK: 1746143 Matrix: Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifers
Nitrogen, NO2 plus NO3 mg/L ND 0.020 06101/16 22:06
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1746144
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1746145 1746146
MS MSD
92298219001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.68 2.5 2.5 3.1 3.0 95 95 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1746147 1746148
MS MSD
92298654002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0,28 2.5 2.5 2.6 1.9 94 66 75-125 31 M1,131
Results presented on this Page are In the units Indicated by the "Units" column except whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Dale: 06/0312016 01:02 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 9

_aceAnakical
� wwwpscaloifs.oam
QUALIFIERS
Project: STORMWATER
Pace Project No.: 92298242
DEFINITIONS
Pace Analytical Sorvlcoa, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection llmlt and below the adjusted reporting limit.
MD#_ - Adjusted Method Detection Limlt.
PQL • Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NEIAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/03/2016 01:02 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 9

�AceAnakicale
� .. wwirpscsfebs.eam
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER
Pace Project No.: 92298242
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 2728E
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92298242001
STORMWATER OUTFALL 1
SM 25400
EDEN122671
92298242001
STORMWATER OUTFALL 1
EPA 1664E
GCSV125163
92298242001
STORMWATER OUTFALL 1
TKN+NO3+NO2
WET145296
Calculation
92298242001
STORMWATER OUTFALL 1
EPA 351.2
WETA127748
92298242001
STORMWATER OUTFALL 1
EPA 353.2
WETA/27795
Date: 05/03/2016 01:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In V1,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 9

PaceAnalytical '
wmY_e lalu_mm
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain-ot-Custody is a LEGAL DOCLJUEN7. Ali relevant fields rtu,st be completed a=rately.
Page: of
Section A Section B Section C
Required Clie+d Irtfurnation: Required Project InforrnatioW Invoice Information:
C.omnany. Report To: Attention:
1 038706
ji • IF.
Ad mess: I
Copy To:
Company Name:
REGULATORY AGENCY
t -7'r '
i
Ad-areSS'
NPOES r GROUND WATER j - DRINKING WATER
!1, I
r UST RCRA ;.. OTHER
EraI To:
Purchase Omer No.:
paOe;_�'we
. r f ! •. 1 _ 1
Reference:
�t'wm
law:
Pm;eu Name:
Pace Project
Site Location
i f f,
6L�na�er.
STATE.
Requested Due CateNAT:
Pm,;ec1 Number:
Pam P;d"' °'
Requested
Anatysis
Fittered
(YIN)
Section D Matrix Codes
r
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RegvlredGien information MATRIX! CODE
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COLLECTED
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>`-
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ADDITIONAL COMMENTS
REUNQUiSNEO BY IAFFHJATIPN
DATE
r
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-ACCEPTED BYt AFFILIATION
i
DATE
TILME
SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE:
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SIGNATURE of SAMPLER:
DATE Sipped 1! rr, l , 1 f
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•Important Note: By sQnkV eft ram you arc aoccpeng Pares NET 30 day paymem teere a.¢ agreex,g to Tare charges of 1.5% per moon for try mwdces not raid Witt:. 30 days., F-ALL-0-020rev.07, 15-May-2DO7

PwAna44kaf '
www.pacerabs.com
Section A
Required Client IrdoPmadon:
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Required Project Information: Fnvcice Information:
Company: 'i Repm.
To:
r.;tnnfion:
I ,� h LJ
asdress: ? Copy
To:
Company Narre:
REGULATORY AGENCY
L'
Address.
NPDES I GROUND WATER I DRINKING WATER
I'
UST i RCRA F ' OTHER
E:naB To: r' +} �; Purchase
Order No.;
?ace Oome
f7c ? r r
atrer�r.�r:
Pt:one: , Fax: - or
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Name.
'race >argea
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Site LoWion
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STATE'
Requested Due 1LtelTAT: Project
Number.
Faca Profs =.
Requested
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RELINQUISHED BY IA AFFILIATION
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SIGNATURE of SAMPLER: .. =t✓ DATE Signed r r � I .
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'ImP BEN NOW P. ssgnng Ina Iran ;p. am accepting Pads NET 3D day paynumu hums ax agrarinp to We charges r,f 1.M, par moms for any in,�. is m ps-d wthin 30 days. F-ALL-0-020rev.07, 15-Vq,-2007

Reidsville NC Stormwater Sampling Checklist
Completed by: Item description
j Fr 1. Sample during representative* storm event at Outfall #1
*>0,1" rainfall, sampled within 30 minutes of start of event, and no other rainfall event >4.1" in
previous 72 hours
J 2. Spring sample between April V-June 30t or Fall sample between July
1st and December 315t
JV/ 1 3. At least 60 days has passed since last sample taken
CL 4. Sample refrigerated until lab pick-up
5. Calculate rain flow and print spreadsheet
6. Fill out SDO qualitative monitoring report for BOTH outfall 1 & 2.
J� Report any deviations to Site Manager
• NC State form SWU-242-XXXXXX
7. Fill out form B2 and C2, site inspection and summary
8. Fill out SDO monitoring report
• NC State form SWU-246-XXXXXX page 1
L L 9. Fill out Storm event characteristics form
• Nt Mate Corm SWU-146-XXXXXX page 2
10. After analysis is complete, check results against following benchmark
values. Report any deviations to the site manager
Total Nitrogen:
pH:
Oil and Grease:
Total Suspended Solids:
Benchmark
Result
30 mg/L
mg/L
6-9 su
7, .4 su
15 mg/L
41,!�' mg/L
100 mg/L
16-11 mg/L
J 11. Compile all documents listed above, together with analysis results,
scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12, Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR In
Reidsville share site

CALIBRATION AND SAMPLE ANALYSIS PROCEDURE
i
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
H analysis must be Performed within 30 minutes of sample collection.
1. Turn on pH meter
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
4. Rinse pH probe with deionized water and blot dry with a clean, soft cloth or tissue.
5. Place both the temperature probe and the pH probe in 7.01 pH buffer solution.
5. Shake the pH probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7. Record temperature and pH reading.
8. Press and hold the CAL button until "CAL" flashes on the screen.
9. Calibration will take approximately 30 seconds. When complete, record final pH reading.
10. Remove probes from 7.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
11. Repeat steps 5 through 9 using the 4.01 pH buffer solution
12. Remove probes from 4.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
13. Repeat steps 5 through 9 using the 10.01 pH buffer solution
14. Remove probes from 10.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
15. Insert both probes in the storm water sample, and stir the sample gently to ensure homogeneity
and minimize carbon dioxide entrainment.
15. Wait one minute for reading to stabilize.
17. Record temperature and pH reading.
18. Remove probes and rinse pH probe in deionized water. Blot dry with a clean, soft cloth or
tissue.
19. Dampen the inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace cap on probe.
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster-10 pH/mWTemperature Meter Serial Number 022055
pH 7.01 Buffer
pH 4.01 Buffer
pH 10.01 Buffer
Storm Sample
Da a
Temp I Initial
Final
Temp Initial Final
Temp Initial Final
Temp
pH
S l�
l (�.91
��u
Z3`lL 3�5.. .ol
ZyUC9. 3" MU2
Air Products Internal Use Only

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: http://112o.enr.state.ne,us/sulForms Doeuments.htm#miac-f9rms
Permit No.: &.0 Of 0 G / 0f 61116
Facility
c: t�r
County: Na
Inspector:
Date of Inspection: 117
Time of Inspection. 69-7
Total Event Precipitation (inches):
or Certificate of Coverage No.: �IJGGI�I 1_1_I_ I_I
I. s
No. '3 3 L 3P V 62-
Was this a Representative Storm Event? (See information below) $ Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that ~
is preceded by at least 72 howrs (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify At't�report is accurate and complete to the best of my knowledge:
JOB
(Signature ofInrpj or Designee)
1. Outfall Description: e
Outfall No. Struct 9 e. ditch, etc.)
C t
Receiving Stream: fw / /'�__
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: ► f' m"' ^
3. Odor: Describe any distinct odor • that the discharge may have (i.e., smells strongly of ail, weak
chlorine odor, etc.): d 0 a {
Page 1 of 2
SWU-242-112608

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
I 20 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where I is no solids annd� 5 is the surface covered with floating solids:
I /Z/ 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy;
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. is there an oil sheen in the stormwater discharge? Yes / N�
4. Is there evidence of erosion or deposition at the outfail? Yes o
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-112bos

Stormwater Discharge Outfali (SDO)
Qualitative Monitoring Report
For guidance on filling out thisform, please visit: http:/lh2o.enr.state.nc.us/su/Form5 D cuments.htm#miscfornis
Permit No.: ,N1011 QI d / dl 413/0/ or Certificate of Coverage No.: NIC/G/ I—I_ITl 1 I
Facility Name: ,1, J �7i; U
County:K6(Kf
Inspector:
Date of Inspection:
Time of Inspection:
ar
Total Event Precipitation (inches): I -
No.
Was this a Representative Storm Event? (See information below) Kyes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event' is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I cer�t this report is accurate and complete to the best of my knowledge;
(Signature�t`��:rniittee or Designee)
1- Out€allDescription-
Outfall No. Structure (pipe, ditch, etc.)
Receiving Stream: �T
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the
(light, medium, dark) as descriptors:
basic colors (red, brown, blue, etc.) and tint
3. Odor; Describe any distinct no�iors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /J f _
Page 1 of 2
5 WU-242-112608

,
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 7l 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 (2) 3 4 5
7. Is there any foam in the stormwater discharge? Yes o
8. Is there an oil sheen in the stormwater discharge? Yes /Nqj
9. Is there evidence of erosion or deposition at the outfall? Yes / io
10. Other Obvious Indicators of Stormwater Pollution:
List and describe / o
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242-1 l 26oa

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 6 00 0 0 � 6 or SAMPLES COLLECTED DURING CALENDAR YEAR: — Za 16
Certificate of Coverage Number: NCG (This monitoring report shall be received by the Division no later than 30 days from
/ J the date the facility receives the sampling results from the laboratory.)
FACILITY NAME f f !Z dLc 7f11 ft�SVl I,C S COUNTY 4G A'W h.
PERSON COLLECTING SAMPLE(S) PHONE N t &
CERTIFIED LABORATORY(S) Lab #f
Lab #1 ( -RE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Specific Monitoring Requirements
• :�
Total
r i
I�
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? .yes --_no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activit • Moniitorittg Requirements
Oetfall
No.
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total Ratnfall
Oil & Grease
(if appl.)
Non -polar
O&GITPH
(Method 1664
SGT-HEM), if
appl.
Total
Suspended
Solids
pH
New Motor Oil
Usage
mo/d4lyr,
MG
inches
m
Units
al/mo
I
7- 0
Form SWU-246-062310
Page 1 of 2

Certificate of Coverage No. NCG
Dodos'76
STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
FACILITY NAME
PERSON COLLECTING SAbIPLE(S) _ 3
CEIiTII'iED LABORATORY(S) Cti Lab #
Lob #.
SAMPLES COLLECT DURING CALENDAR YEAR Za/tit
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory-)
v COUNTY
PHONE NO. 9 L
(SIGN OF PFM TTTEE OR DESIGNEE)
By this signature, I certify that this report is accasate
complete to the best of my knowledge.
PartA: Vddde Maintenance Activity Monitoring RegUbtWentS (only if, on average, mare than S5 gallons per month of new motor oil is used)
Out12D
No.
Date
Sample CoDected,
nWddiyr
Total Rainfall
inches
New Motor 011 UsaM
Annual avezav
i OM56
0000
00400
07 and Grease,
mg1L
Noo-polar O&GnPH
(Method 1664 SGT-HEM),
da
Total Suspended Solids,
MA
PA
Standard units .
Benchmark
-
-
-
30
i5
100
6.0 — 9.0
G-
Nom If you report a sampled value in excess of the benclimadc value, or outside the benchmark range for pH, you must implement Tier I or Tier 2 responses in the General Pernik -
Mail Original and one copy to:
Division of Water Quality
Artru Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
'T certify, under penalty of law, that this document and ail attachments were prepared under m9 direction or supervision in accordance with a system dedgeted to
assare that gushed personnel properly gather and evaluate the information submitted. BaiW on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and be€ 4 true, accurate, and complete.
I am aware that there are signitiput pemdti, of submitting false information, including the possr-bility of 5nes and imprisonment for knowing riolatioas"
Mau) ---
Farm SWC-254-062310
Page 1 of 1

STORM EVENT CHARACTERISTICS:
Date
Total E�Princheseci Precipitation P (inches).
Event Duration (boars): �Z (only if applicable — see permit)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see penult.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, tru accurate, and complete- I am aware that there are significant penalties for submitting false information,
Including the possibility, d imprisonwnt for !mowing violations."
(Signae ormsttee) (Date)
Form SWU-246-062310
Page 2 of 2

Outfall 001
Inches of Rain 1.5
Area Sq Ft Run Off Factor Ft of Rain Cubic Ft Gallons Million Gallons
Impervious Area 127000 0.9 0.125 14287.5 106870.5 0,1068705
Grave! 425500 0.5 0.125 26593.75 198921.3 0.19892125
Total 552500
Total Flow 0.30579175
Area x runoff factor x feet of rain = cubic ft of water runoff
Cubic feet x 7.48 W gallons

AIR A
PRODUCTS 1.—. Delegation of Authority to Non -Officer Positions
�rEl
the unoersigned, rde , in my capacity as Vice Presi_ denj— GIQ,§al gniglneerino of air
Chj0*jpls_ fng., pursuant to the Delegations of Authorily Policy, hereby delegates aulhonty as described herein below to
the foliowing non officer poeitlon(s).
POSITION TIM Amu COmPANy MAmPAAUM VALUE
LFWF% Transacl,onrContracr
Sea attached Page 2 for list of position titlos NIA
DESCRIPTION OF AUTHOfaTY
Authority to execute permit applications, permit related submissions and documents. and routine filing$ and
documents required by local, stale, and federal regulatory agencies or authorities pertainng to envirOnmenlal,
heaflh, and safety compllence for the Wilkes Barre, Gardner, Cryornachinery and Prism Membranes facilities
13Tius a.,% niy may ba sut,dsiagnift wan irM lotlow,++g mWnCl%W* NI anti
0 Ms a,Wrwniy may na be subdatMpaiag,
to fake effect when countersfgneo by the Corporate Secretary or any Assistant Corporal* Secretary and to continue in
effect for ao tong as the designated pos(Wrl Iftia(s) remain unchang*d, or unid such authority shall be revised or
revoked by notice thereof by the undersigned, hIs or her successor in oflfce, or the person to wham the designaled
posftlor+(s) report.
t
Countersigned by
ty,rNwJtr:r t rn iA•in[�Ai ( rpOnr G'rrLrr r rill(&

Alf? A
PRODUCTS L= Delegation of Authority to Non -Officer Positions
POSITION nTLE
Operalions Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendeni
Construction Manager
Env'varrrental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialisl
Senior Principal Envinxii. entat Specialist
wad •.41,. ,.1a �., b0:,rn.,�,e.n,ili 1A
M"IMUM VALUE
WA

ace Analytical'
wwwpaoaMbo.00m
June 03, 2016
Mr, Levi Owens
Alr Products
225 Equity Road
Reidsville, NC 27320
RE: Project: STORMWATER
Pace Project No.: 92298242
Pace Analytical Services, Inc.
206 East Meadow Road • Suite A
Eden, NC 27288
[phone]
NC Department of
Enviro RmcelvelQuality
JUN282016
V1f inston-5aiem
R,eglo+)F-�l Otiice
Dear Mr, Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on May 19, 2016, The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,}
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
q without the wrillan consent of Pace Anetylical Services, Inc..
¢pRASO
Page 1 of 9

ac°eAn*tica!'
! www.pacelabscam
CERTIFICATIONS
Project: STORMWATER
Pace Protect No.: 92298242
Charlotte Certification IDS
9800 Klncey Ave. Ste 100, Huntersville, NC 28078
South Carolina Cartiricatlon #: 99006001
North Carolina Drinking Water Certification #: 37706
Florlda/NEL4P Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certlflcation #: 84
North Carolina Wastewater Certlflcation #: 12
VlrginlaNELAP Certlflcation #: 460221
Asheville Cartifleatlon IDS
2225 Riverside Drive, Asheville, NC 28804
North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648
South Carolina Certification #: 99030001
Massachusetts Certlflcation #: M-NCO30
VlrginlaNELAP Certlflcation #: 460222
North Carolina Drinking Water Certiflcatlon #: 37712
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633
North Carolina Drinking Water Certiricatlon #: 37738 VirginlafVELAP Certification #; 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 9

Analytical
wwwprcvirae.cnm
a
ANALYTICAL RESULTS
Project: STORMWATER
Pace project No.: 92298242
Pace Analytical Services, Inc.
205 East Meadow Road - Sul to A
Eden, NC 27288
t336 j623.8921
Sample: STORMWATER OUTFALL 1 Lab ID: 92298242001 Collected: 05/17/10 10:00 Received: 05/19/16 11:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No, Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids
16.4 mgtL
2.6 1
05119/1614:18
HEM, Oil and Grease
Analytical Method; EPA 1664B
Oil and Grease
NO mg/L
6.0 1
06/03/16 08:52
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Total Nitrogen
0.51 mg/L
0,12 1
06/02/16 15:33
351.2 Total KJeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, KJeldahl, Total
NO mg1L
0.50 1
05/28/16 00:56 7727-37-9
353.2 Nitrogen, NO2/NO3 pros,
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.41 mg/L
0.020 1
06/01/16 22:16
Bate: 06/03/2016 01:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 9

aCeAnalytical
*wwpasslabs.aam
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
QC Batch: EDENI22871 Analysts Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 25400 Total Suspended Solids
Associated Lab Samples: 92298242001
METHOD BLANK: 1737550 Matrix: Water
Associated Lab Samples: 92298242001
Parameter Units
Total Suspended Solids mg1L
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 06/19/1611:21
Paco Analytical Serviced, Inc,
205 East Meadow Road - SuRe A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1737551
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Suspended Solids mg1L 250 256 102 90.110
SAMPLE DUPLICATE: 1738204
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1738205
92297933003 Dup
Units Result Result RPD Qualiflers
mg/L 169 200 23 D6
92297949001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 35.3 34.0 4
Results pror'ented on this page are In the units Indicated by the "Units" column except where an alternate unit la presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
data. nRir m17016 01:02 PM without the written consent of Pace AnaMical Services, Inc..
Page 4 of 9

_ WeAnalX'lcal-
wwwPocolabt-com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
QC Batch: GCSV125163 Analysis Method: EPA 16648
QC Batch Method, EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92298242001
METHOD BLANK: 1747600 Matrix: Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Quallfiers
Oil and Grease mg/L NO 5.0 06/03/16 08:45
Pace Analytical Services, Ino.
206 East Meadow Road • Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE:
1747601
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil end Grease
mg/L
40 35.2
88
78-114
MATRIX SPIKE SAMPLE:
1747602
35240515001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Greaso
mg/L
3,4J 40
42.9
99
78-114
Results presented on this page are In the units indicated by the "Units" column maps whore an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, exceptin full,
Date: 06/0312015 01:02 PM without the written consent of Pace Analytical Services, inc.. Page 5 of 9

172ce Analytical
wKw,peaslaba,com
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92298242
QC Batch: WETA127748 Analysis Method: EPA 351.2
OC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92298242001
METHOD BLANK: 1742451 Matrix: Water
Associated Lab Samples: 92298242001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg1L ND 0.50 05/28/16 00:49
Pace Analytical Services, Inc.
205 East Meadow Road • $vile A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1742452
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L 10 9.9 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1742453 1742454
MS MSD
92298871001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone, Result Result % Rec % Rec Limits RFD Qual
Nitrogen, Kjeldahl, Total mglL 30.4 10 10 42.0 42.2 116 117 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1742465 1742456
MS MSD
92298756001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone, Cone, Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglL 20.2 10 10 30.8 30.7 105 105 90.110 0
Results presented on this page are in the unite indicated by The "Units" column oxcept whore an alternate unit Is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 06/03/2016 01:02 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 9

/7-pa"'Ce Ana 1ytical
www.psanlabs.com
QUALITY CONTROL DATA
Project: STORMWATE.R
Pace Project No.: 92298242
QC Batch: WETA/27795 Analysis Method: EPA 353.2
OC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92298242001
METHOD BLANK: 1746143
Associated lab Samples: 92298242001
Matrix: Water
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L ND 0,020 06/01/16 22:06
Pace Analytical Sorvloes, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
LABORATORY CONTROL SAMPLE: 1746144
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Quaiiners
Nitrogen, NO2 plus NO3 mg/L 2.5 2.4 96 9D-110
MATRIX SPIKE b MATRIX SPIKE DUPLICATE: 1746145 1746146
MS MSD
92298219001 Spike Spike MS MSD MS MS0 % Roe
Parameter Units Result Cone, Cone. Result Result % Rao % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg1L 0.68 2.5 2.5 3,1 3.0 95 95 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1746147 1746148
MS MSD
92298654002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone, Cones Result Result % Rae % Rec Llmits RPD Qua[
Nitrogen, NO2 plus NO3 mg1L 0.28 2.5 2.5 2.6 1.9 94 66 75-125 31 M1,R1
Roo ulls proxWed on thtc pogo pro In the units Ind lasted by tho "Units" column except whore an alternate unit Is prosonted to the right of the result.
REPORT OF LABORATORY ANALYSIS
This re port shalt not be reproduced, except In full,
Dale: 06/03/2016 01:02 PM without the written consent of Pace Analytical Services, Inc.,
Page 7 of 9

arcAnalkical
wwwpecefobt.tarr
QUALIFIERS
Project: STORMWATER
Paco Project No.: 92298242
DEFINITIONS
Face Analytical Services, Inc,
205 East Meadow Road - Sulle A
Eden, NC 27288
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MOIL - Adjusted Method Detection Limit.
PQL - Practical Quantltation Limit,
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte Is
a combined concentration,
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 Is recommended In SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260,
N-Nltrosodlphenylamine decomposes and cannot be separated from Dlphenylamine using Method 8270. The result reported for
each analyte Is a combined concentration.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except to full,
Date: 06/03/2016 01:02 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 9

-' aceAnalytkal'
wwwPeoMe6a.pom
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER
Pace Project No.: 92298242
Pace Analytical Services, Inc.
205 East Meadow Road • Suite A
Eden, NC 27288
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92298242001
STORMWATER
OUTFALL 1
SM 25400
EDEN/22871
92296242001
STORMWATER
OUTFALL 1
EPA 18648
GCSV/25163
92298242001
STORMWATER
OUTFALL 1
TKN+NO3+NO2
WET/45296
Calculation
92298242001
STORMWATER
OUTFALL i
EPA 3612
WETA/27748
92298242001
STORMWATER
OUTFALL i
EPA 353.2
WETA/27795
Date: 06/03/2010 01:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wtlhoul the written consent of Pace Analytical Services, Inc..
Page 9 of 9

010 ° CHAIN -OF -CUSTODY / Analytical Request Document
PaceAnalytical The Chairrof-Custody is a LEGAL DOCUMENT. A!(relevant fields must be completed accurately.
a .pates kxam
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. AV relevant fields must be completed amAat*.
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Invoice Information:
Section D Matrix Codes
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F-ALL-0-020rev.07, 15-May-2007

Reidsville NC Stormwater Sampling Checklist
Completed by-
Item description
1. Sample during representative* storm event at Outfall #1
*>0.1" rainfall, sampled within 30 minutes of start of event, and no other rainfall event >0.1" in
previous 12 hours
J 2. Spring sample between April 15t-June 30t or Fall sample between July
1" and December 31st
I )V/ 1 3. At least 60 days has passed since last sample taken
4, Sample refrigerated until lab pick-up
5. Calculate rain flow and print spreadsheet
6. Fill out SDO qualitative monitoring report for BOTH outfall 1 & 2.
Report any deviations to Site Manager
• NC State form SWU-242-XXXXXX
j -F)O 7. Fill out form B2 and C2, site inspection and summary
8. Fill out SDO monitoring report
• NC State form SWU-246-XXXXXX page 1
�__�___� 9. Fill out Storm event characteristics form
• IN(- Mate rorm JVVU-14b-XXXXXX page 2-
- 10. After analysis is complete, check results against following benchmark
values. Report any deviations to the site manager
Total Nitrogen:
pH:
Oil and Grease:
Total Suspended Solids
Benchmark
Result
30 mg/L
mg/L
6-9 su
.
7- su
15 mg/L
mg/L
100 mg/L
mg/L
1 11. Compile all documents listed above, together with analysis results,
J scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12, Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR in
Reidsville share site

CALIBRATION AND SAMPLE ANALYSIS PROCEDURE
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
H analysis must be 2erformed within 30 minutes of sample collection.
1. Turn on pH meter
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
4. Rinse pH probe with deionized water and blot dry with a clean, soft cloth or tissue.
5. Place both the temperature probe and the pH probe In 7.01 pH buffer solution.
6. Shake the pH probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7. Record temperature and pH reading.
8. Press and hold the CAL button until "CAL" flashes on the screen.
9. Calibration will take approximately 30 seconds. When complete, record final pH reading.
10. Remove probes from 7.01 buffer solution and rinse with delonized water and blot dry with a
clean, soft cloth or tissue,
11. Repeat steps 5 through 9 using the 4.01 pH buffer solution
12. Remove probes from 4.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
13. Repeat steps 5 through 9 using the 10.01 pH buffer solution
14. Remove probes from 10.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
15. Insert both probes in the storm water sample, and stir the sample gently to ensure homogeneity
and minimize carbon dioxide entrainment.
16. Wait one minute for reading to stabilize.
17. Record temperature and pH reading.
18. Remove probes and rinse pH probe in deionized water. Slot dry with a clean, soft cloth or
tissue.
19. Dampen the Inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace cap on probe.
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
PH 7,01 Buffer
pH 4.01 Buffer
pH 10.01 Buffer
Storm Sample
Da a
Temp
Initial I Final
Temp Initial Final
Temp Initial
Final
Temp pH
s 7
2V 36
G-
/0.02
Air Products Internal Use Only

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this fonn, please visit: Documents.htm#nii CffuLms
Permit No.: WC/ 010 6 41 613, G 1 or Certificate of Coverage No.: NJGGI�I
Facility Na106Wqh4*q
e:[�di -jiff - - - --
County: Phone No,
Inspector:5
Date of Inspection: -� /7 1-&
Time of Inspection: Q e;,
Total Event Precipitation (inches): I
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0,1 inches has
occurred. A single storm event may contain up to 10 consecutive flours of no precipi(ation.
By this signature, I certify t)-at''o
jr,-report is accurate and complete to the best of my knowledge:
JPM-<'rS
(Signature ofyCrn�tCcce; or Designee)
1. OutfaH Description:
Outfall No. - I- -- Struct �j(ipe, ditch, etc.) �t e_, ..._ ..._
Receiving Stream: �-' /t!6M ric---
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the disch
(light, medium, dark) as descriptors: •L r
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odor{• tlu t the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc,): d 0 d4(
Page I of 2
SWU-242-112608

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy;
] 20 3 4 S
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and
� S is the surface covered with floating solids:
1 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 6 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? YesN
9. Is there evidence of erosion or deposition at the outfall? Yes o
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Ala N)r
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-2a2-112608

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: jWp- lh'o.enr, state.nc uslsu11-orms Docuinems.htni#miscfornis
Permit No.: NIC/1I
Facility Name:
County: kf4lpl,
Inspector: --I
Date of Inspection:
Time of Inspection:
d l al d 134/ or Certificate of Coverage No.: NIC/Gl�hl_I 1_I_I
J<U 17i 71-0
0j
Total Event Precipitation (inches):
No.
Was this a Representative Storm Event? (See information below) Kyes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at Ieast 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I cer�at this report is accurate and complete to the best of my knowledge:
(Signaturel6!!6iittee or Designee)
I. Outfall Description:
Outfall No. — Z Structure (pipe, ditch, etc.) e ��
Receiving Stream:^�
Describe the industrial activities that occur within the outfall drainage area: _
2. Color: Describe the color of the discharge
(light, medium, dark) as descriptors: r llA
basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct
tnol ors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.):
Page 1 of 2
SWU-242-112608

10
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 3 4 5
b. Suspended Solids. Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 (2) 3 4 5
7. Is there any foam in the stormwater discharge? Yes o
8. Is there an oil sheen in the stormwater discharge? Yes JNgt}
9. Is there evidence of erosion or deposition at the outfall? Yes j 10
10. Other ObviousIndicators of stormwater Pollution:
List and describe ` / �
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242.112608

Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195-1501
Telephone [phone]
Via Fed Ex 7754 5918 7759
20 January 2016
NC DENR Division of Water Resources
450 W Hanes Mill Rd. Ste. 300
Winston-Salem, NC 27105
RE: NCS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
RECEIVED
N.C. Dept of ENR
JAN 2 5 2016
WINSTON-SALEM
REGIONAL OFFICE
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility.
Please feel free to contact me with any questions or require additional information. I can be
reached at [phone] or [e-mail].
Sincerely,
nnifer B. rei
r. Pr. Envir men al Engineer
c. Coray Mitchell —Air Products

�.
STORMAVA'i ER DISCHARGE OUTFALL (SDO)
\MONITORING REPOR"r
b6��
Permit Number: ND3o
CS or
Certificate of Coverage Number: NCG_
F:.CILITY NAME APe-/ (� ., JS, , I he
PERSON COLLECTING SAMPLE(S) rS
CERTIFIED LABORATORV(S) � G ce AnF+ t. g 1 Lab tr
Lab_._..
Part A: Specific Monitoring Requirements
SAIIPLI'S COLLI,CTED DURING CAI,I'NDAR YEAR: Zd/s—
(This monitoring report shall he received by the Division no later than 30 dal's from
the date the faeility receives the sampling result_, From the laboratory.)
COUNTY �CC Ki, n �.`' `•-A
rA y
ONE N""
(' .NATU F 14,1101 PTTEE OR DI-SIGNEE)
By this sicrnpull. I cer y that this report is accut•ate
complete to the best of my knowledge.
Outfall
Date
56050
No.
Sample
Collected
Total
Flow (if app.)
Total
Rainfall
�H
14 rM
pf�
f a� N
rig �vQ3
/
mo/d /vr
\4G
inches
.I7
Does 0iis facility perform VehiCie [Maintenance Activities using more than 55 gallons of new :ni►tor oil per mgnth" I yes _no
(if j'es, Completc Part B)
Part B: Vehicle Maintemince Arttvity Monitorinu Re►luiremenl�
Outf:ill
Date
50050
0I)S5(
00530
00400 i
!o.
Sample
Collected
Total Flow
(if al►plicabk)
Total Rainfall
Oil ct Gre.rse
(if appl.)
Nun -polar
O&C/TPIi
i'Medwd 1.664
if
appl.
Tota]
Suspended
Solids
pHI
New Motor Oil
U5:1ge
n►o/dd/vr
1I
inches
1112/1
mull
Units
t?al/mo
:L Zr IL
4 a
I
71
7
Form S %VU-246-0623 10
Page I ol• 2

STOWNI EVENT CIIA ACTE RISTICS:
Date 12 z, /r
Total Event Precipitation (incites): _ '
Event Duration (hours): 1. Sf (only if al)plicaLle — see permit.)
(if snore than omt storm cvew ova: sampl: d)
Date _
Total Event Precipitation (inches):
Event Duration (hoary): (only if applicable — see perrrtii.)
Mail Original and one copy to:
Division of Water Quality
Aan: Central Files
1617 Mail Service Censer
Raieijh. Nortb Carolina 27699-1617
"I certit;v. under penalty of how, that this document and a]I attucliments were prepared under my direction or supervision in accordance witli a
systent designed to assort: that qualified personnel properly Lather and evaluate the infornmlion submitted. Ilascd on my inquiry of the person
or persutis who innalge the systcin, or those. persons directly responsible for gathering the information, flit information submitted is', to the best
of my I,nowled-e and belief, trite, accurate, and complete. I ain aware that there are significant penalties for submitting false information,
including the possibility of lines and it)g)risunmenf for knowing violalions."
/ / .-6 Z�eI
(Signn 61
of Pcrinitl ei (Date)
Form SWU- 1ri_062310
Pars 2 of

STORAIWATER DISCHARGE ObTTALL (SDO)
MONITORING REPORT
Certiscate of Coverage No. NCG
F A C I'L ITY NXIN117 _ f# FL/ / fir CSvi Ile
PERSON COLL.ECTFI G SAMPL%S)
CE'RTIFEi D LABORUTORI- — 9Gt c ti Lab 4
Lab
SAMPLES COLLECTED DURP'G CALENWAR YEAR. Zo l-!�
('Phis monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling` results from the laboratory.)
C0UNITY � oCK�y icy
PHONE NO. 33G 3
(S ATUIRE O Y Al E, E OR IGNEE)
By this signatu I rtify that thus re ort is accurate
complete to the best of my lutowledge.
Part A: Vehicle Maintenance Activity Monitoring Requirements (only if, on average, more tban 55 gallons per month of new motor 00 is used)
outfall
'N0.
I
Date
# Sample Collected,
ma/ddAT
Total Rainfall,
inches
New Motor Oil Usage,
Annual average
ryat/mo
00S5f]
00530
60400
Oil and Greuse,
mg/L
Non -polar O&G/ITH
(Method 1664 SGT-HE2W,
if a2pl.
Total Suspended Solids,
mg/L
pH,
Stuudard units
Benchmark
-
30
15
100
6.0 — 9.0
Note: Ifyou report -a sampled valUe in excess ct the benchmark valoc, or outside- the cc:telutrark raanc for pal, you must implenicnt Tier l or'ficr 2 responses in the Gencral Fe -twit.
Mail Original and one copy to:
Division of Water Quality
A,= Central Piles
} 16l7 ?vSaii Service : enter
i Raleit h, N' orth Cara lL a' 27699-1617
"I certi y, under penalty of hare, that this document and all attactirnents.were prepared tinder my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the inforrtatioo, the imormation submitted is, to the best of my knowledge and belief, true, accurate, and complete.
l am awara that there are significant penalties for suhn0ving false information, including the possibility of fries and iniprisomnent for knowing violatinns."
a6��
(Date)
Fc;rs S%VU-254-062310
Page 1 of h

Outfall 001
Inches of Rain 0.5
Impervious Area
Gravel
Total
Area Sq Ft Run Off Factor Ft of Rain Cubic Ft
127000 0.9 0.0416667 4762.5
425500 0.5 0.0416667 8864.5833
552500
Area x runoff factor x feet of rain = cubic It of water runoff
Cubic feet x 7.48 = gallons
Gallons Million Gallons
35623.5 0.0356235
66307.08 0,066307083
Total Flow 0.101930583

Al am.'
/
PRODUCTS gDe/egafion of Authority to Non -Officer Positions
r .p 1tL-4•.[ .rrr w
.r G
The undersigned, Roort 12, C me , m my capacity as Vice President - Global Enameering of Au Products and
Chemicals- Inc., pursuant to the Delegations Of Authority Policy, hereby delegates auihonty as described harem below la
the follewmg non -officer posilion(s):
POSITION TITLE AND COMPANY MAXIMUM VALUE
Eoeh TransacswnrConXncX
See attached Page 2 for list of pos+IXon titles NIA
OESC011"ON OF AUTNOMTY
Aulhorily to execute permit applications. permit related submissions and documents. and routine filings and
documents required by local, state, and federal regulatory agencies or aulharilies pertaining to environmental•
health. and safety compliance for the WI)kes Barre. Gardner. Cryomachinery and Prism Membranes facilities
❑This BUMOMV may be UYbdelagatad wnlh the ronowmg rhlreclans fit any)
® Tits Aulhanry may not be subdah*ai&d,
to take effect when countersignso by the Corporate Secretary or any Assistant Corporate Secretary and to continue In
effect for so tong as the designated position tille(s) remain unchanged. or unld such authority shall be revised or
revoked by notice thereof by the undersigned. his or her successor In office, or the person to whom the designated
position(s) report.
Sepielurr / �{�
i
A �.
Countersigned by: ' ��� 1
Dole
l'uryur.r[r l in:.a.t��h74[ l rPn�a Xt �f'rrt Wr
I—, .IT-14. !Ni-rs.L...".-AI AA

AIR J*.
PRODUCTS 1= Delegation of Authority to Non -Officer Positions
POSITION TITLE
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmentai Engineer
Principal Environmental Engineer
Sensor Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmentai Specialist
Principal Environmental Specialisl
Senior Principal Environmental Specialist
Lead Environmental Seer:ialist
rrAxrMUM VALUE
TM!

ZO6 Eest Mea&w Road - Sulu A
Eden, NC Tras
December 30, 2015
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: Air Products
Pace Project No.: 92280296
Dear Mr. Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2015.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNi standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brittany Gibson
[e-mail]
Project Coordinator
Endusurea
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.,
Pagel W 9

_ �PfalJr��4>QU o
CERTIFICATIONS
Proleat Air Products
Pace Projed No.: 9228MG
Paaa MelyHra1 Series lnc.
205 East Meadow Road -Sub A
Eden, NC 2728tt
(33SAM I
Chariotta Cer0catton Ma
-
9800 Khoey Ave. Ste 100, Huntersvilla, NC 28078
Florida/NELAP Certificatton #: E87827
North Carolina Drinking Water Certifioetion #. 37708
Kentucky UST Certification #: 84
North Camfirta Reid Servloes Cartiftostion #: 6342
West VIM inia Certification M. 357
North Carolina Wastewater Certification 0:12
VhgintalVELAP Certification #: 460221
�South Carolina Certtficatton#:99008001_ �� _-- - _--_
. _�. �____ __ ---- ._._r .._____- _-- _ -.•-•
Asheville CeRttcation We
2225 Rlverside Drive, Ashaville, NC 28804
North CamU m Wastewater Certification M. 40
Florida/NELAP Certification #: E87648
South Camlirra Certlflcatlon M. 99030001
Massachusette Certification #: M-NC030
West Virginia Certification M 356
North Carolina Drinking Wafer Certification P. 37712
Vlrgi WVILAP Certification #: 480222
Eden CoM iceflon ID8
206 Ead Meadow Road Suite A. Eden, NC 27288
north Carolina Wastewater Certification #: 833
North Carolina Ddntdng Water Certification M. 37M
VirgtnialVELAP Certification #: 480026
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Servlcas, Inc.. Page 2 of 9

u� �e6al/YyA®nW„!/
ANALYTICAL RESULTS
Project Air Products
Pace Project No.: OM0296
Pace Ans"ael SerAces, Inc.
2D6 East M08daw Road • Sulte A
Eden, Nc 27m .
(338)6238921
Swnple: OUTFALL 1
Lab to: 9=0296001 Collected: 12116/16 08:05
Received: I?!17/1614.30 Matrix Water
Parameters
Results Units
Report Lfmtt
OF
Prepared ArtsWed CAS No. Qual .
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
10.0 mall.
2.6
1
12/17/1514:40
HEM, Oil and Grasso
Analytical Method: EPA 1664E
00 and Grease
NO mg/L
6.0
1
12129/15 05.11
Total Nitrogen Calculation
Anaklical Method: TKN4.NO3+1102 Ceic uldoti
Total Nitrogen
0.36 M91L .
.-0.12
1
12130/1510.45
351.2 Total Kleldehl Nitrogen
Analytical Method: EPA 3512
Nitrogen, I(jeldehl, Tonal
NO MOIL
0.60
1
12=1612:00 7727-37-9
353.21dltrogtiin, N07NO3 Ares.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.17 MOIL
0.020
1
12i2W616:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 12130/2015 04,46 PM wlttrout the written consent of Pace Analytical Services, Inc- Page 3 of 9

Peas Anafydt al 8eM=s, Inc.
2G8 Eset Meadow Road - Suite A
Eden, NC 27M
(8S8p3-i3M
QUALITY CONTROL DATA
Project: Air Products
Pace Pmjed No.: 92280296
QC Batas EDEN121140 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Anatysls Desedpilon: 25400 Total Suspended Solids
Associated Lab Samples: 92280296001
METHOD BLANK 1631717 Matrix Water
Associated Lab Samples: 922802s8009
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg1L ND 2.6 12117/1514:10
LABORATORY CONTROL SAMPLE: 1831718
Spike LCS LCS % Rao
Parameter Units Con& Result % Rao Limits Qualifiere
Total Suspended Solids m91L 250 256 1D2 00-110
•'s
SAMPLE DUPLICATE: 1831719
922802DO001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg1L 50.0 45.5 10 D6
SAMPLE DUPLICATE: 1631720
M80208001 Dup ti
Parameter linos Result Result RPD Qualifiers
Total Suspended Solids mglL 68A 68.2 3
Resulte presented on this page are in the units Indicated by the "Units" column except where an alterrwts unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1213012015 04:46 PM without the written consent of Pace Ana"cal Services, Inc.. Page 4 of 9

- _ . - - ---- - - - - - .17 PaaeAnatyHea! itentee, trta.
a 206 East Masdnw Road - Suite A
Eden. NC 2M8
�taaat (WSM348921
QUAL r Y CONTROL. DATA
Project: Air Products
Pace Project No.: 92280298
QC Batch: GCSV/23694 Analysis Method: EPA 1684B
QC Battle Method: EPA 1664E Analysis Descript)on: 1604 HEM, 00 and Grease
Associated Lob Samples: 92280296001
METHOD BLANK 1S38102 Matncc Water
Associated Lab Samples: 0280296001
Blank Reporting
Parameter Units Result Limit Analged Qualifiers
OII and Grease mg/L NO 6.0 12129M S 06:09
LABORATORY CONTROL SAMPLE:
1638103
ti•
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Umb
Qualifiers
OA and Grease
mg/L
40 34.e
66
78-114
MATRIX SPIKE SAMPLE:
108104
=80098004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Quellliere
Oq and Grease
mg/L
<6.0 40
37.9
96
78-114
Results prevented an this peg& are in the units Indicatod by the 'Units' column except where an alternate unit Is prevented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Th1s report shall not be reproduced, except In full,
Gate: 12/30/2015 04;46 PM without the written consent of pace Analytical Services, Inca
Page 6 of 8

"'�• ram:
QUALITY CONTROL DATA
Projeet: Air Products
Pace Project No.: M80298
Pen AnalAcat Services, Ina.
205 East Meadow Road - Scdto A
Eiden, NC 27M
(338W3- M1
QC Batch: WETA125930 Analyals Method: EPA 3512
QC Batch Method: EPA 3512 Analysis Description: 351.2 TKN
Associated Lab Samples: =80296001
METHOD BLANK: 1637562 Mavk Water
Associated Lab Samples: 92280296001
Blank Reporting
Parameter Units Result Limit Analyzed Qualltiara
Nitrogen, Kjeldehl, Total M91L NO 0.60 12129/1511:50
LABORATORY CONTROL SAMPLE: 16376S3
Spike
LCS
LCS
% Rae
Parameter
Units
Cana.
Result
% Roo
Llraila
Qualifiers
Nitrogen, Kjeldahl, Total
MA
10
10.0
106
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1637564
1637665
MS
MSD
8=80718001
Spike
Spike
MS
MSD
MS
MSD
% Rao
Parameter
Units Result
Cone.
Conn
Result
Result
% Rae
% Rao
Limits
RPD Qual
Nitrogen, Kjetdahl, Total
M91L 10.2
10
10
22.3
21.5
121
113
90"110
4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1637566
1837607
MS
MSD
92280376001
Spike
Spike
MS
MSD
MS
MSD
% Roe
Parameter
Units Result
Conc.
Cone.
Result
Result
% Rea
% Res
Limb
RPD Qual
Nitrogan, Neldshl, Total
mg/L IA
10
10
12.1
12.4
107
110
90-110
3
Results pressMod on this page are In the units Indicated by the "Units" column except whore an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 12/30/2015 04:46 PM without trio written consent of Pace Ana;yticel Services. Inc -
Page 6 of 8

`
- - -
Paco Annlytical BaMeea, Inc.
`
aEden,
2D5 East
Meadow Road - Suite A
cejt���
NC 27M
WWAFWBmb&O-
i336 21
QUALITY CONTROL DATA
Project: Air Products
Pace Project No.: 92280286
t,C Batch: WETA125902
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nttiita. preserved
Associated Lob Samples: OU80290001
METHOD BLANK 1638258
Matrix Water
Associated Lob Samples: 922802B$001
Blank Reporting
Parameter Units
Result Limit Analyzed Qua]lfiers
Nitrogen, NO2 plus NO3 mg1L
NO 0.020 1212311615-40
LABORATORY CONTROL SAMPLE: 1638259
Spike LCS LIDS % Rec
Parameter Units
Conc. Result % Rec Umits Qualt iers
Nitrogen, NO2 plus NO3 mg1L
2.6 2.4 B5 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 16=60 1636261
MS MSD
WM0087001
Spike Spike MS MSD MS MSD
% Rao
Parameter Unite Result
Conti. Conn Result Result % Rat: % Rec
Llmlis
RPD Qual
Nltmgen, NO2 plus NO3 mg1L NO
2.5 2.6 1.3 1.3 63 63
76-126
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1636282 16=83
MS MSD
92280376001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result
Conti. Conc. Result Result % Rec % Rea
Llmlts
RPD Qua]
Nitrogen, NO2 plus NO3 mglL 0.19
2.6 2.5 2.6 2.6 Be 96
75-125
0
Results presented on this page are in the units Indicated by the'Units" column except where an alternate unit is presented to the right of the reautt
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/30/2015 04:46 PM without the written consent of Pace Analytical Services, Inc..
Page 7 of 9

I_1'FkceArWcW o
meow
QUALIFIERS
Project" Air Products
Pace Project No.: 0=0208
DEFift MONS
Pace AnlU"C l Samtcee, Ins.
205 East Meadow Road - Butte A
Eden, NC zras
{33OWMeM
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentratlon above the adjusted method detection limit and below the adjusted reporting Ilmlt.
MDL - Adjusted Method Detection LlmIL
PQL - Practical Quantltation Limit.
RL - Reporting Limit
S - Surrogate
1,2-0Ipharrylhydrazine decomposes to and cannot be separated from Azoberaene using Method 8270. The result for each snalyte Is
a combined ooncerttradon.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Corftrol Sample (Duplicate)
MS(D) - Matrix Spike (Dupllasta)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SO - Sgico Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be approprlste for 2 Chloroethyivinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended In SW846 Chapter 4 for the analysis of Acroleln and Aeryionitrlle by EPA
Method 8260.
N-Nllrosodlphenylamine decomposes and cannot be separated from Diphanylemine using Method 8270. The result reported for
each anslyte Is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited enalytes.
TNI-The NELAC Institute.
ANALYTE QUALIFIERS
DO The relative percent diffarence (RPD) between the sample and sample duplicate exceeded laboratory control Ilmlte.
M1 Matrbc spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/30/2015 04:46 PM without the written consent of Pace Analytical Services, Inc.. Page a of 9

- _ — - Pace Analytical services, Ino. -
203 East Meadow Road - Sub A
Eden, NC 2nu
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project
Alf ProductB
Pace Project No.:
92280298
Analytical
Lab 10
Sample 10
QC Batch Method
QC Batch Analytical Method Batch
9Z280n8D01
OUTFALL 1
SM 2540D
EDEN121140
92260296001
OUTFALL 1
EPA 16848
OCSV123894
922 M6001
OUTFALL 1
TKN+NO3+NO2
WET142241 ".
Calt�latlon
-
92280288D01
OUTFALL 1
EPA 351.2
WETA125MO
92280296001
OUTFALL 1
EPA 3532
WETA125902
•
Date: 1213012015 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 9

Pacekialytical
. pace labs min
CHAIN -OF -CUSTODY ! Analytical Request Document
The Chain-aGCuslody is a LEGAL, DOCUMENT. All relevanl fields phist be completed accurately,
Section A Section a 5eetion C
Page: of s
Riccluired !;Bent Inlrrmaliom Required Project Informal ImJeicy Infolmatior.
Rev )rt To tnunr,en:
Y
194180
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Copy In-
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REGULATORY AGENCY
17r 4�SP J f/'���
Address
! NiGP.OUND WATER r • , D1�ItJK1tVG YJATER
j` LIST I7 RCRA r OTHER
r , ,3•/' h /�� l
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PaCO Qi101R
Duos:
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Ref
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Project Name:
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Site Location
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Llanarcr:
ST.A Tom'
Regrrested Dors Date1TAT:
Pro;ecl N,imb^.r:
Pace Pnrde 1),
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Reg6sted
Analysis
Flltered
(Y)N)
Section 13 Matrix Codes
Required Ix!nl Inf-,rrnalim IWJFIX r 001E
CGt,LECIED
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Waler INT
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• RELINQUISHED BY f AFFILIATION
DATE
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ACCEPTED BY I AFPILIATIO14
DATE
TIME
SAMPLE CONDITIONS
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'In-.pcdanl PoleFip signin3 phis icrm you we;rp�i Peos'e i{ET X day ❑aymenl rorms end agreel.'lq Ti late charges cf I, % j. Y mWiri far aay invoices not paid whin 30 days. F-ALL-0-020rev.07. 15-ly1ay-id♦77

ZarS
Reidsville NC Stormwater Sampling Checklist
Completed by�—
Item description
1. Sample during representative* storm event at Outfall #1
*>0.1" rainfall, sampled within 30 minutes of start of event, and no tither rainfall event >0.1" in
Previaris ii hours
J _ 2. Spring sample between April 1ST -June 30th or Fall sample between July
1" and December 315t
3. At feast 60 days has passed since last sample taken
I ) fy, 4. Sample refrigerated until lab pick-up
S. Calculate rain flow and print spreadsheet
Jr 6. Fill out SDO qualitative monitoring report for BOTH outfall 1 & 2.
Report any deviations to Site Manager
O NC State forrn SWU-242-XXXXXX
J� 7. Fill out form B2 and C2, site inspection and summary -1
8. Fill out S_DO monitoring report
NC State form SWU-246-XXXXXX page 1
j 9. Fill out Storm event characteristics form
o NC. State torn'l SWU-Lob-xxxxxx page 2 _
j !- 10. After analysis is complete, check results against following benchmark
values. Report any deviations to the site manager
Total Nitrogen:
pH:
Oil and Grease:
Total Suspended Solids:
Benchmark
Result
30 mg/L
()• 36 mg/L
6-9 su
7,11 _ su
15 mg/L
eJ0 rng/L
100 mg/L
/a. r, mg/L
�,/� 11. Compile all documents listed above, together with analysis results,
J i ( scan and send to Environmental Specialist and Site Manager. Store
_—__--Lhardcopy in Reidsville plant office
12. Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR in
Reidsville share site

CALIBRATION AND SAMPLE ANALYSIS PRO,
i
j
:EDURE;
EXTECH Oyster-10 pH/mV/Temperature Meter Seria) Numb& 022055
H analysis must be performed within 30 min
• Turn on pH meter
• Connect temperature and pH probes to meter
• Remove storage cap from pH probe
• Rinse pH probe with deionized water and blot dry wwith a lean, soft cloth or tissue.
• Place both the temperature prone and the pH probe in 7.101 pH buffer solution.
• Shake the pH probe gently to dislodge air bubbles and wa t one minute for reading to
stabilize.
• Record temperature and pH reading.
• Press and hold the CAL button until "CAL" flashes on the screen. i
• Calibration will take approximately 30 seconds. When complete, �recor inal pH
reading.
i
• Remove probes from 7.01 buffer solution and rinse with c eionized water and blot dry
with a clean, soft cloth or tissue.
i
• Repeat steps 5 through 9 using the 4.C1 pH buffer sclutio i
• Rerriove probes frain 4.01 Duffer solution and rinse with c eionized water and blot dry
with a clean, soft cloth or tissue.
• Repeat steps 5 through 9 using the 10.01 pH buffer solution
• Remove probes from 10.01 buffer solution and rinse with deionized water and bict dry
with a clean, soft cloth or tissue.
I -
!
• Insert both probes in the storrrr water sample, arid, stir thc sample gently to e11SUre
homogeneity and minimize carbon dioxide entrainment.
i'
• Wait one minute for reading to stabilize. '
4
I
I
7
I
t
S
i
`! r
1 €
3 ,

i
{
E
l
Record temperature and pH reading.
o Remove probes wid rinse l)H probe in deionized water. Blot dry with a clean, soft cloth
I
or tissue. I
E ;
f
o Dampen the inside of the pH storage cap with a small arty unt of pH 4.01 buffer solution
and replace cap on probe. i
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster-10 pH/mV/Temperature Meter erial Number 022055
pH 7.01 Buffer pig 4.01 Buffer pH 10.61 Buffer Storm Sample
Date Temp ! Initial Final Temp 1 Initial Firial T ip I lriitial I Final Temp I pH
I 73-_I 17, Xl 17. 01 7y 1 Ll 03 1 �Y(ol17s. S 1ia.oy /0-01 7 11
I

Stornmater Discharge Outfall (SDO)
Qualitative Monitoring; Report
Fua•tuirluat.rc un filliaahart 11ai.c�nrarr, Irle�a.vc visit: I�ttlralli"c}.rin.aatc.nc.us/sulhnr'uls Dc,c uincrrr;.lrrrndliFrsscfr,rrns
Permit No.: NICE J-410 W O 13 I U1 or• Ccrtiticme of Covcr,itc No.: NICIGI_l_l—/-1 I —I
p',rcifily N:rrne, 7e ��e j —
County: _ Km m Phone No.
InsIIL'cor: J dm*5
Z90
Date of Insliccaicrn: l Z /L 1.5-
--
`I'inic of lctshcction: .� 0'6d0 _
l nr;il F—vent PfeCilpit:ilion (incite;).
Was this a Repimsentative SLorin Event? (See infornunion belomo 19i Yes ❑ No
Plr.ra+',:' rh<,.k ynrrt �,crtttit tip r c rift/ rf'Qurrlitrrtive llfonitoring must he perlrwmed durh?g ci rcpresentative
stil1-01 CIT111 (reglarrt;11 ellr-F var.%')-
A-Rehi-e cniativc Storin went" is a sta ni evcrir that ineasures greater than (}- I inches of rahilldl and that.
is preceded by ;.it least 72 hours (3 days) in which no storm event ineasuring grciaer Ilan 0. i inches h:is
i ocon-red. A ste,rrn evCnt nra�arrrtain Lip to lf} consecutive hours of no precilritutiorr.
By Ibis mg al.urc. I Certify ih:st ii r-el,esrt is accost+~ find c0111I)letC to the f7est W' rtty knowledgc.:
( 15n:411F v or Nei- tty ; 1W nesi�^fwu) — -
1. G'utI';iEl f)iScr•iE�liur�:
Outfall No. Structarc; (Pipe, Glitch, eta:.)
1 1 t" e
Describe lire ilidusu-ial .ictivities lhat i?Ccur within the outf ilf drainaYe W'c,i:
2. 04or•: Dcscrihu tic Color of (lie di-cluti-e using basic colors (red, Drown, blue, etc.) and tint
(li�,ht, medium, dark-) as descr-iptc.lrs: 1,���_�i�131^rn -
3. Odor Describe .1ny distinct odors ih�it. the: discharge rn,iy have (i.c., smells stronbly of oil, walk
chlorine Woo etc.): �� ff�of - — -- ----
!OTC I OF?
swu MI MIS

a. Mrily: Choose the nunrber which hest WSW the clarity or•die clinch tile, where I is clear
and .5 is eery (Joudy:
1 0 4 5
S. Flolktrng Solids: Choosc: the. numhcr which best describes the amount of M acing sul N hi die
stormwatcr discharge. wl€ere I is no w lids and 5 is Ow sw1we covered wills rlomins. solids:
6 2 3 4 5
f. Sushenekrl Wids: Oumse the number which best descrihes the amount orsuspended solids in
the ti�rrnw:tter discharge, where I is "n solids and 5 is m r owly trtucicly-.
1 6 3 4 5
7
8.
y
Is there ally fnxlll in the slormwater discharge?
Yes 0
Is therc::rn oil sheen its the stonriwater dls0targe.' Yes
E; 11101c evidence Qf cry€sic►n 01- dcllUsitiutl at the qulrall? Yc 0()
11). 01hat' Obvious Indic.04orsol•Sformwilej-Y1llltltion:
List and describe
NQNc
Note: I_.ow e laxity, hi�tilt st)Iiels, astcE/or lhc. Prese ncc of ro,rnt. s>iE Sheen, or e r'n ic�rt/cic Itositiori may he
imucative of Ilollr Wla exp€.€sum. 'I'hcse condiiion,s warrant r€rrthel• investigalioll.
loge 2 of 2
SwwTv I I m's

r SrAr2'.
v� V
Stornnvater Dischareye Outi'all (SDO)
Qualitative Monitoring Report
1'r�r �rrirlrruC2' nrr Ifllirr;, out this fiorm, please visit: hllPa/h�t.t.utu'. lsfi_isc_ti�/�t1/1 ttnnc E)c t_tit�lcrtt.ti.hlrn4+'titi clF r�tss
Permit. No.: N/C/ 61 6/ 6/Q/6 / 3 l U/ or Certificate of Covera- No.- NICIGI�I_
Facility N.IrrQre:
CllltntV:
frttiP�.r:tor: �1 rW1
Date of Inspwc 011:
.1'inle c,l` Inspeckoll:
Total Iyvent Preuipit.lticui {MC]ICS)
Phone No.
7
WIs this a Representative Sturm E:ve rit? (See information below) 8 Yes ❑ No
Please c;hi-.—ck yourp(,,rmil to f-rri/}, il'Qrrahieaive rl-lonitoriti.> Hurst be ltetji)rined during rr reprC.reWarive
:�'tnrrrr crrrrl {"rrt;lrrirr>rrrr:jrta• ti�rrta�j.
A ` Re jm%; c mauve Storm .EVe11t" is a storm event that trlecrsure.. LrC,Oel- thtln 0.1~1tIdICs of rfttnfitll :111d thslt
is prc,cc rdccl by pit Ic::1sr 72 holds (3 days) in which t10 S101111 CVCttt 11-1c:lsurinL� [hail 0.1 inches has i
I occurred. A sinI2IC S(c.tnrt CVCnt fnay' Cuntairl Ill) tO 10 COnSe:CutiVC hours of no precipitation.
Rv this si,.[ ItltI]T-0,.1 cati{*y-'II,'I retort is aCCU rate and conlpfe:te to the Itest of -my lrnow,Icloo:
(,SiL-mitlltc, or DcsiLzicc)
1. (?utl.tii �}c:tic:riEstic>'tt:
Owf"all No. 2 ` IRIC1,11V (PihC, dilclt, etc.)
Rccciviny Stream: 1✓w��eSG"''t C
Dc,SC6kC tite inclttS16,11 aC.tivities that oCCur within the ouff,111 drainage area: Vehide �r�/ITh CC
2. 'Color: Duscribe thL ceder€ of,1.hC GW
llr-c using basic colors (=de brawn, blue, etc:.) r lld tint
(light, medium, dark -) as descriptors: _ Y/ A,
_
3.
3. Qthw: Dc .,nhe any distinct odors that the clischar-C may have (ix- smells stron0y c& nil. wca€c
c:h lori ne odor, ctu.): —NaniC - _ - `-- — _— -- ---- -- '
pagc, 1 0,2
SWU- 242-1 12608

% 4p r
4. C hlrily: Choose the number \Bich best describes the clarity of the discharge, where I is clear"
1-111d 5 is very cloudy:
i 2 3 4 5
5. hlo:rtinw SO NIIs: Choose 1J7e nu111lter which hest describes the amount of floating solids in the
stornmater discharge, where 1 is no solids mid 5 is the surface covered with floatim, solids:
1 2 4 5
6. Suspended Solids: Choose the; number which best describes the amount of suspended solids in
the siorinwater dischar,,e, where I is no solids and 5 is extremely muddy:
4 5
7. I.s there :n:y Imull in the stornnvater discharge? Yes f\'u
8. Is there lrl oil screen in the stornrwater discharge? Yes /N
9. Is tht.re CVide:riCC Of'erosiOr: (rr del)ositiun at then outfirll? Yes ONo
10. Other Obvious Indicators t►t' Sturmwater Pollution:
List irnd dcacribc 0506
Note: i_,uw cla3 ity, Iii��h Solitf5, .rncllor the I�resenec of foam. oil sheen, or erasion/depositiorl may ha
iric.iie;tlive of l}ollutantezf�csstirc. 'These Conditions wsrrmifftrtl.e.r irivesti�oation.

4
AIR A,
PRODUCYSZ
Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195-1501
Telephone [phone]
Via Fed Ex 7754 5918 7759
20 January 2016
NC DENR Division of Water Resources
450 W Hanes Mill Rd. Ste. 300
Winston-Saiem, NC 27105
RE: NCS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
` RECEIVED
N.C. Dept of ENR
JAN 2 5 2016
WINSTON-SALEM
REGIONAL OFFICE
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility.
Please feel free to contact me with any questions or require additional information. I can be
reached at [phone] or [e-mail].
Sincerely,
nnifer B. rei
r. Pr. Envira mental Engineer
c. Coray Mitchell —Air Products

STOR,MINTATE• R DISCHARGE OUTF_1LL SDO)
ViONITORING REPORT
p6�o
Permit umber: NCS o3aor
Certificate of Coverage Number: NCG
FACILITY NAME APO t;�-e,
PERSON COLLECTING SAMPLE(S)
CERTIFIED LABORATORY(S) _{Gr ce ffnN )l c L.�b
Lab
Part A. Specific \Monitoring Requirements
SA_IiPLES COLLECTED DURING CALENDAR YEAR: 2,015—
('This nioniioring report shall be received by the Division no later- than 30 days from
the date the facility receives flip sampling results front the laboratory.)
COUNTY
ONE \
($J41NATU1ffk0F 11,E1b T l'EE OR DESIGNEE)
BY this sign re. I certttfy that this report is accurate
complete to the best of my knowled("e.
Otttfall
Date
5 005; 0
I
No.
i
Sample
Collected
Total
Flow (if app.)
Total
Rainfall
7
�
� � �
OfCr
(OT �
f
mold /vr
!MG
inches
I
I
#
I
1
i
f
1�
_
k
�
i
Doe_ ti-is facility perform more Onan 55 gallons of new;nater oii per rtonTh'' � yes _no
corr131"l-w Part B)
Part B: Vehicle Maintenance Activity \ionitorin+= Regmirements
Ootfall
Date
so0.-�0
00556
00530
00400
No.
I
�
Sample
Collected
i
Total Flow
i if ;applicahle)
Total Rainfall
I
Oil fi. Grease
(if appl.)
Non -polar
O&Gf-rPH
(Method 1.664
SC"f-Filrllt, if
a p1.
Total
Suspended
Solids
pH I ?yetis. rlotor Oil
Usa c
'
mo/dd/yr
l \(G
inches
nmA
mRl
Units
6 Oil
I -
i N0
I -6
I
I
l
For!]1 SW"kj-'7i6-t 6=0
pads I cif 2

STORA•I EVENT CHARACTERISTICS -
Date S
Dale !Z11v -
Total Event Precipit:!tlon finches):
Event Duration (hours): r 5� (�nl;r it ril��iicnb —see permit.}
(if amorc rhaii one storm CVCIiT was ;srnpl xi)
Date
Total !went Precipitation (inches):
Event I3ua-a1ion (hours): (only if aappiicabie — _ee pennit.)
flail Original .and one copy to:
Divi_rx! of Water Qu3sity
AMP: C2rltra! ryes
1.617 Nlail. Service Center
Ra1ei?h. t\Nartil C'aralins 276,9;-1.617
"I certifc', under penalty of la%v, that this document and all attachments were prepared tinder my direction or supervisicm in accordance will! :a
system designed to assure that qualified pi:rsonnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who anana,e the. system, or those persons directly responsible for gathering the information. the information submitted is. to the best
of m ,- l;nowledoc and belief. true. accurate, and complete. I am aware that there are significant penalties for submitting false in]Qrn7ation.
including the possihilily of fines and in for knowing violations."
n W,)L, ) I.11
(Sign O of Perinift�e� (Date')
Fo,nt) SW UT -2 46- 06 2.i 1 i�

STORAIWATER DISCHARGE OIJiTALL (SDO)
1•IOYITORLNG RE -PORT
Certificate of Cove .g:: No. NCG
FACiLnYNA_ IE t4Pe/ 1" fie« /le
PERSON` C0LLECTLtiG SAMPL%(S) Cr
CERTIFITO LABOPLATORY(S) l?Cif [ 4 / Lab;
- - — --..Lab =% -
SA-'IeIPLFz COLLECTED DF,;-rta'G CALE\TDAR YEA. :
(This monitoring report shall be received by the Division no later than =0 drys
from the date the facihty receives the sampling result; from the Iabomtaryj
PHOi4M NO. r 334
(S , ATURE O I'13hZMI=E OR SIGNC'EE}
By this signa-m f rtify that tiffs report is accurate
complete to t1he best of my hmowledg.
Fart A: Vehicle 1NIainten2pce Activity Monitoring RegWremeuts (ordy if, on ayerage. more than SS gallons per month of new motor oil is used)
Outfsll I Date
Ito. f Sample Collected,
rno/ddiyr
!
Total %ainfall,
inebes
New Motor Oil Usage,
Aarual azeraae
4at/mo
005545
!
D0530
60400
Oil and Grease,
1339/L
Ncn-polar O&Gf PH
C-Method _ W4 SGT-BI. Tj,
if a �i.
' Total Saspended Solids,
mg./i
pH,
Standard emits
Benchmark
-
3Q
Wo
rz a1
7S-
j Al
�
f}
1
f
N1:o: li yQ_ repo, a ship rd value in excess c the ban:. Mark v:L'uc. or Cutslli: did bczub,% 21--+ 71:1-'•C for Fi,i, yo-L! F3 usl iiriip!cnacnt Tip. 3 o: Mir 2 respwis�s in t_he Gumeral
Mail Ori-Lual and one copy to:
Div!S:CB of Water Qua ty
i 1617 Mail Scrvicn Center i
Rele:an, Ncrth CarolLna 27599-1617 l
:I cer i fy, under persalty of iziw, that this dccumment and alI tine nluiens.ivere prt Pared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properly gather aad evaivate the imformat:on submitted- Based on my inqui ry of the person or persons who :rmna e the System, or
tI]CSs �r: �Jn�� dire^.t ;i r _aon,ible eor �a=liiI n� the infor a',sa!jou tba huror7a?icn subrnHed is, to the best of my Imo'ttledne and Relief, true, accurate, and complete.
i am .Var- that there lie sigi0leant pettal";es fa: su,Ct*.ii tic' a false _ u`oi motion, including the posAAl3tr of i7?es and iA]*t]rLioament ft]r lcacn'in.- violalrioas."
.77 ...7n S �� �l- 062Z id
Page 1 e= 1

Outfaff 001
Inches of Rain 0.5
Area Sq Ft Run Off Factor Ft of Rain Cubic Ft Gallons Million Gallons
Imperviaus Area 127000 0.9 0.0416667 4762.5 35623.5 0.0356235
Gravel 425500 0.5 0.0416667 8864.5833 66307.08 0.066307083
Total 552500
Total Flow 0,101930583
Area x runoff !actor x feet of raid = cubic ft of water runoff
Cubic feet x 7.48 = gallons

A� /.
PRODUC 2 .: Delegation of Authority to Non -Officer Positions
The undersigned, Robert Q, fonley, to my capacity as Vice P(eligent _Glgbal ling mo eerin9 of Au Producls-m-nrL
Chemicals Inc., pursuant to the Delegations of Authorily Policy, hereby delegates auihonly as described herein below to
the following non -officer positions);
POSMON TITLE AND COMPANY MAXIMUM VALUE
Eaen TrsnurnanrCantnet
See attached Page 2 far list of position lilies NIA
DESCRIPTION OF AUINC)PJTY
Authority to execute permll applications, permit related submissions and documents, and routine filings and
documents required by local, slate. and federal regulatory agencies or aulhorilies pertaining to environmental•
health, and safety compliance for the Wilkes Barre, Gardner, Cryomachinery and Prism Membranes facilities
❑True aulharHy may be subdetegatad wart the totteov-no mllirictons ht anyI
® Trus ruttwrty may noI be aubdelegeted,
to lake effect when countersigned by the Corporate secretary or any Assistant Corporate Secretary and to continue in
effect for so long as the designated position lille(s) remain unchanged, or unlit such authority shall be revised or
revoked by notice thereof by the undersigned, his or her successor to office, of fhe person to wham the designated
position(s) report,
Iirlfwturr ♦ I nnlr
OA
Countersigned by- r,,lt,•
Ca. W1 lLP Ne t IrT i,3.A+I�at L rperH t!• tirtrr N� r

Aff? i.
PRODUCTS L= Delegation of Authority to Non -officer Positions
POSITION TITLE
operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmentat Specialist
Lead Environmental Specialist
I... r'.IM.IJ•n.I:Mrl.nnrnMeA.,J 14A
C 1, ♦ r41., .�.Y., nY
MAXIMUM VALUE
NIA

^�. k ,"' �,�- -�y :-err--• -n. 3`�. �`.r� t T - - - - - - -- "-- - -
Paco MalyYfsal BeMCsa, lno.
jt r,i n
^Af Q 7 205 East Msadaw Road •Sufte A
Edar NC 27288
December 30, 2015
' Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NO 27320
RE: Project: Air Products
Pace Project No.: 92.280298
Dear.Mr. Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on December 17, 2015.
The results relate only to the samples Included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance.Manual, where applicable, unless
otherwise' noted in the body of the report.
Analyses were performed at the Pace Analytical Services location Indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
TWO report shall not be ►eproduced, except in full,
without the written consant of Pace AnalyticaI Services, lnc.,
Page 1 of 9

. � C�B�dTidly�CRI o -
CERTIFICATIONS
Project Alr Products
Pace Project No.: 02280288
. Paca Arielyticai Barrlcea, Ins. _ - _ .
295 Feet Meadow Road • Sub A
Eden, NC 27288
(338)t1734e11121
Charlotte Certification IDs
8800 Klncey Ave. Ste 100, HunterevIlle, NC 28078
FloridalNELAP Certificatlon #: E87627
North Carolina Drinking Water Certlflcatlon #. 37705
Kentucky LIST Certification #: 84
North Carollna Field Services Certification #: 6342
West VIrglnia Certification #: 357
North Caroline Wastewater Certificatlon #:12
Vtrginta/VELAP Certificatlon #: 480221
South Carolina Certification # 90008001
Asheville Certlflcation IDs
2225 Riverslde Drive, Asheville, NC 28804
North Carolina Wastewater CeMcatlon #: 40
FlorldalNELAP Certification # E8760
South Carolina Certificatlon #: 88030001
Massachusetts Certification #: M-NC030
West Virginia Certiflcstlon #: 356
North Carolina Drinking Water Certlflcaticn #: 37712
Vlrpinh V`L!LAP Certiflcatlon #: 480222
Eden Certification We
205 East Meadow Road Suite A, Eden, NC 27288
North CamUns Wastewater Cartifioation
North Carolina Drinking Water Certification #: 37738
Vlrglnia[VELAP Certiflcatlon # 480025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the wvltten consent of Pace Analytical Services, Inc..
Page 2 of 9

PSce ArrBlyttaa168Mcoo, Inc-.
-p 20b Easi Meadow Road-'Sufte A
Arr h k _ en, NC 27M
Ed
+o mm i336jB,29-W21 '
ANALYTICAL RESULTS
Project: Air Products
Pace Project No.: 9228D296
Sample: QUTFALL 1 _
Lab ID: 922BD206001 Collected: 12/16/15 08:05
Recelved: 12117/1514:30 Matrix Watar
Parameters
Results. Untts
Report Llmft
OF
Prepared AnsWad CAS No. Qual
y 2540D Total Suspended Solids
Analytical Method: SM 25400
Total Suspended Solids
10.6 mg&
2.6
1
12/1711514:48
HEM, Oil and Grease
Analytical Method: EPA 16648
OD and Grease
NO mg/L
6.0
1
12/29/15 05:11
Tate# Nltrogsn Calculation
AneNllcal Method: TKN4-NO3+NO2
Calculstloir
_
Total Nitrogen
0.36 mg/L
.' 0.12
1
12130/15 19.45
351.2 Total 4Qeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, KJeldahl, Total
NO mg/L
0.60
1
12129/1612:00 7727-37-9
353.2 Nitrogen, NO2IN03 prey.
Anslyttcal Method: EPA 363.2
Nitrogen, NO2 plus NO3
0.17 mg/L
0.020
1
12/23/1516,04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in lull.
Date: i2J3012016 04:46 PM without the written consent nI Pace Analytical Services, Inc,. Page 3 of 9

_ - Paine AnWAGel SsMw% Inc.'
.` a 205 EW Meadow Road - Suits A
Eden.
�NNCJJ 27288
'f PW A2�m
QUALITY CONTROL DATA
Project Alr Products
Pace Proud No.: 92280298
QC Batch: EDEhtl21140 Analysts Method: SM 2644D
QC Batch Method: SM 2540D Analysts Description: 2640D Total Suspended Solids
Associated Lab Samples: 9=80208001
METHOD BLANK: 1631717 Matrix Water
Associated Lab Samples: 922B0286DD1
Blank Reporting
Parameter Units Result Llmft Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 12/17/1514:10 ,
LABORATORY CONTROL SAMPLE:
1631718
Spike LC5 LCS
% Roe
Parameter
Units
Cana Result % Rec
Limits Qualifiers
Total Suspended Solids
mg/L
250 256 102
90-110
SAMPLE DUPLICATE: 1831719
92280206001 Dup
Parameter
Units
Result. Result RPD
Qualifiers
Total Suspended Solids
mglL
50.0 45.5
10 D6
SAMPLE DUPLICATE: 1631720
02280268001 Dup
Parameter Unft Result Result RPD Qualifiers
Total Suspended Solids molt. 68.4 66.2 3
Rosults presented on this page are In the units Indicated by the "UnIts" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2015 04:46 PM wlihoul the written consent of Pace Analytical Services, Inc.. Page 4 of 9

-
1 0 208 East Meadow Road-; Sub A
Eden, NC 2T2U
.1-' sarnpe�a9amom ; . - (398}B'29T8921
QUAfLiTY CONTROL DATA
PrcJea: Atr Products
Pace Project No.: 82280288 '
QC Batch: GCSV123884 Anatysls Method: EPA 18548
QC Batch Method: EPA 188413 Anafysls.06scrtptlon: 1884 HEM, 011 and Greasa
i Assocated Lab Samples: 92280298001
METHOD BLANK: 1638102 Matrtx Water
Associated Lab Samples: SUB0296001 ..
Blank Reporting
Parameter Unfts Result Umlt Anslyzed Quallflers
Ofl and Grease m81L ND 6.0 12/20/16 05:09
LABORATORY CONTROL SAMPLE; 1838i 03
Spike LCS LCS % Roe
Parameter Units Cane. Result' % Rec Limits QualHiere
09 and Grease mglL 40 34.0 , 86 78-114
MATRIX SPIKE SAMPLE: 1836104 '
- 9226na98oaa .
Parameter Units Result
O11 and Grease m91L a54
Spi
Con
ke Ms Ms
a Result % Rec
40 37.9 96
71; Roo
Limits Quallfiers
78-114
Resuna presented on this page are in the units Indicated by the "Units" column accept where an alternate unit Is prese+rted to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/30/2016 04:46 PM without the written consent of Pacej A atytical Services, lnc_
Page 5 of 9

"•r• rr:
Pace Ans"cal $erta om tne.
205 Eset Meadow Road- Sub A
Eden. NO 27288
QUALITY CONTROL DATA
Project: Air Products
Pace Project No.: =80298
QC Batch: WETA125930 Anatyats Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Descrlptlon: 351.2 TKN
Associated Lab Samples: =80296001
METHOD BLANK 1637582 Matrix: Water
Associated Lab Samples: 92280296001
Parameter Units
Nitrogen, Kjeldahi, Total mg&
LABORATORY CONTROL SAMPLE: 1837563
Blank Reporting
Result Llmlt Analyzed Qualifiers
ND 0.50 12/20/15 1 T:50
Spike
LCS
LCS
% Rao
Parameter
Units
Cana
Result
% Roe
Limits Qualmors
Nitrogen, Kjeldahl, Total
mg/L
10
10.0
106
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1637564
1837585
MS
MSD
OMS0718001
Spike
Spike MS
MSD
MS MSD % Roe
Parameter
Untfa Result
Conc.
Cone. Result
Result
% Rao % Rao Limits RPD Qual
Nitrogen, Kjeldahl, Total
mg/L 10.2
10
10 22.3
21.5
121 113 90-110 4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1637580 1637667- t.
MS MSD
92280376001 Spike Spice MS MSD MS MSD % Roo
Parameter Unite Result Cone. Conn • Result Rem" % Rec % Rao Llmlts RPD Qual
Nitrogen, Kjoldehl, Total mg/L 1.4 10 10 1211 12A 107 110 M110 3
Results presented on this papa ore In the unit@ Indicated by the "Units" column except whore an alternate unit Is presented to the right of the rssull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/30/2015 04:46 PM without Ind written consent of Pace Ana'.yticel Services. Inc- Page 6 of 9

.-•r.SYFY.9:'� �^Y'. r.` -`S vrr,.. _ r• .•.1-r •.• •.r-•..- � -•r.- S "T-'; ,Ca .w- _ ,�-•. .., _. ..: ..
Puce Analytical aa..tvtcas,_...
Ina._
CB `-�� 205 East Meadow Road •- S_ ulte A
��41,m••!t Eden, NC 277B8 .
{338}ti23-8 .
QUALITY CONTROL DATA
Pmlerb . Alr Products
Pace Project No.: 92280296
QC Batch: WETA126902 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 3532 Nitrate Nitrlta, preserved
Associated Lab Samples: 92280296001
METHOD BLANK 1030268 Matrix Water
Associated Lab Samples: 92280298001'
Blank Reporting
Parameter Units Result Limit Analyzed QualHlere
Nitrogen, NO2 plus NO3 mg1L ND 0.020 12/23/15 16:4A
LABORATORY CONTROL SAMPLE: 1030269
Spike
LCS
LCS
% Rea
Parameter Units
Conc.
Result
%Rea
Limits Qualifiers
Nitrogen, NO2 plus NO3 mg1L
2.5
2.4
95
90-110
MATRIX SPIKE 8t MATRIX SPIKE DUPLICATE: 1636280
1638261
MS
MSD
OM80087001
Spike
Spike MS
MSD
MS MSD % Ras
Parameter Unite Result
Cont.
Cones Result
Result
% Roo % Rea Limits RPD Qual
Nitrogen, NO2 plus NO3 mg1L ND
2.5
2.6 1.3
1.3
63 53 75-126 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1638262 1836283
MS MSD
92280376001 Spike Spike MS MSD MS MSO % Rae
Parameter Unite Result Cont. Conc. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, NO2 plus NO3 moll. 0.19 2.6 2.6 2.6 2.6 Be 98 76-125 0
Results presertted on this page are in the. unhs Indicated by the "Units" column kept where On ehornate unit Is presented to the rtght of the result.
REPORT OIL LABORATORY ANALYSIS
This report Shall not be reproduced. except In full,
Date: 12/3012015 04:46 PM without the written consent of Pace Me#ytical Services. Inu- Page 7 of 9

QUALIFIERS
Project: Air Products
Pace Project No.: =80298
qJJ I` �l • .F3
Pate Antatocal Be Woes, Inc.
205 East Meadow Road - SWW A
Eden, NC 27288
[phone]
DF - Dtlutlon Factor, If reported, represents the factor applied to the reported data due to dilution of the sample aliquot
ND - Not Detected at or above adjusted reporting [1mIL
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting IlmtL
MDL - Adjusted Method Detection Limit
PQL - Practical Quantltetlon Limit
RL - Reporting LWL
S - Surrogate
1,2-Dlphenylhydmzlne decomposes to and cannot be separated from Azobenzena using Method 8270. The result for each anatyte is
a combined concentration.
Conslatent with EPA guidelines, unroundad data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Semple (Duplicate)
MS(D) - Matt( Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SO - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroathylvinyl other, Styrene, and Vinyl chiorlde.
A separate vial preserved to a pH of 4-6 Is recommended In SW846 Chapter 4 for the analysis of Acroleln and Acrylonitrlle by EPA
Method 8260.
N-Nltrosodlphenylamine decomposes and cannot be separated from Dlphenylemine using Method 8270. The resultreported for
each analyte Is a combined concentration.
Pace Analytical Is TNI accredited. Contact your Pace PM for the current list of accredited onelytes.
TNI - The NELAC Institute.
AiNALY'TE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceaded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 12/30/2015 04:46 PM without the written consent of Pace Analytical Services. Inc- Page a of 9

r Pace Anelytical Ssrvlcas, Inm
r p 205 East Meadow. Road .,Suite A _
E-dan, NC i72aa
I33ON123.8921
QUALITY CONTROL. DATA CROSS REFERENCE TABLE
Project: - . Air Products
Pecs Project No.: =80298 _
Analytical
Lab 10
Sampta ID
QC Batch Method
QC Batch Analytical Method Batch
9=0206061.
OUTFALL 1
SM 25400
EDEN12114D '
02280200001
OUTFACE 1
EPA 1864E
GCSV 3s94
02280206001
OUTFALL 1
TKN+NO3+NO2
WETl42241
Calculation
9228M60D1
OUTFALL 1 .
EPA 361.2
WErAr25930
92280296001
OUTFALL 1
EPA 3533.2
WETAW902
REPORT OF LABORATORY ANALYSIS
Thla report shall not be reproduced, excapt in full,
Date: 12130/20-15 04:46 PM wllhout the written consent of Pace Analytical SeNces, Inc.- page 9 of 9

ce /1, na,�I!fical
CHAIN -OF -CUSTODY / Analytical Request Document
ile, ChcJn-rf,-1,5;Wy is a •_EC -AL 30CLIKIE H T. All elermri( fici.n alk,st IX- camp!ete;§ a
B Secticn C of
R,quirad 0 lrfcrwalf�::ti. Rnquirod 1:,f*J:m,-.jj:,n !1ANM1I:,.j1.
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R IF C Ij LA r(;S Y A' : F WC Y
OTHER
L
Site Loc3!;on
STATE:
Requesled Due DWeP I AT!
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Aiiaiysi%
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sactiorl, r) tlatfix ",-des
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Pace Project Nod Lab
3
4
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ADDITIONAL COMMENTS
RELINOUISHEl') GY I AFFILIATION
DATE
rjr.jr
_LL
ACCEPTED BY I AFFILIATION
DATE
TU.IF
SAMPLE CONDITIONS
ta
SAMPLER J%IAME AND SIGNATURF
Pr, 'INT Nima of SAMPLER:
Z
SIGNATLJRE cl SAMPLER; GATE Signed
E
L; -F
F
ch1V1E1rIYyj:
Xc-le, Sy nnn,I l7;.5 yn.0 zia a xttG­, F.,lm's 1qST 3.'.- Gay p2)"ne"I lvms 4la!e ;,` ,aee. or P-1 fur .1,y i 30 days FF.ALL-()-02".-v W. 17_-N1zy-2Z07

Reidsville NC Stormwater Sampling Checklist
-Completed by:
� item description --__
,)t
1. Sample during representative* storm event at Outfall 41
>0.1." rainfall, sampled withii7 30 minutes of start of event, and no other rainfall event >0j" if)
_ previous 72 haUrs _
R 2. Spring sample between April 1-t-June 30" or Fall sample between July
1st and December 31't
�3. At least 60 days has passed since last sample taken
4. Sample refrigerated until lab picl<-up — —�
5. Calculate rain flow and print spreadsheet
J f> 6. Fill out SDO qualitative monitoring report for BOI-11 outfall 1 & 2. —
Report any deviations to Site Manager
o NC State form SWU-242-XXXXXX_ _
7. Fill Out form B2 and C2, site inspection and summary
617—_ _ 8. Fill orit SDO monitoring report ^�
o NC State form SWU-246-XXXXXX page 1
9. Fill out Storm cver3t characteristics form J
NC State form SWU-246-XXXXXX page 2
JFP 10. After analysis is complete, check results against following benchmark
Values, Report any deviations to the site manager
Total Nitrogen:
pH:
Oil and Grease:
Total Suspended Solids:
Benchmark
Result
30 mg/L
().36
mg/L
6-9 su
7,11
Su
15 mg/L
mg/L
100 mg/L
n-ig/L
J m 11. Com
pile all docuents listed above, together with analysis results,
{" scan and send to Environmental Specialist and Site Manager, Store
har-dcopy in Reidsville plant office
�— 12. Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR in
Reidsville sham site

CALIBRATION AND SAMPLE ANALYSIS PRO EDLIRE'
EXTECH Oyster-:1.0 pH/n)V/Terlperature Meter Seria Numh& 022055
t
PH analvsis must be Performed within 30 m€ntrtes of ample collection
C Turn on pH meter
Y Connect temperature and pH probes to meter
O Remove storage cap from pH probe
Rinse pH probe with deionized water and blot dry w€th a lean, soft cloth or tissue
Place bath the terrrperature prole and the pH prof)e_ to 7. A. pH buffer SOILItlOi1.
III l
Shake the pH probe gently to dislodge air bubbles and wa t one niinute for reading; to
stabilize.
I;ecar[i temperature and pH reading, �
i
r
Press and hold the CAL button anti€ "CAL" flashes on the screeii. i
Calibration will take approximately 30 seconds. When co nplete, record final pH
reading;.
� I
Rerrrove probes from 7.01. buffer solution and rinsi? with c eionized water and blot dry
With a clean, soft cloth or tissue. } i
i
Repeat steps 5 through 9 using the 4.01 pH buffer sa€utio r
I I
Ren'iove probes fronr 4.01 buffer solution and rinsL with c eionizelf water and blot dry
with a clears, soft cloth or tissue. I
I
Repeat steps 5 through 9 using the 10.01 pH huffe�r soluti n
I
r
Remove probes from 10.01 buffer solution and rinse with deionize d water and blot dry
with a clean, soft cloth or tisscre. �
t
Insert both probes in the storm water samplrr, and,
, stir th sample gently to ensure
�
homogeneity and Minimize carbon dioxide entrain;nlerrt.
Wait one mirmte for reading to stabilize.
I

i
I f
i
o Record terr1perature and pl-i reading. 1
I i
I t
o Remove probes and rinse pH probe in deionized water. lot dry with a clean, soft eloth
I
or tiSSnc:.
I
o Dampen the inside of the pH storage cap with a siYiall am mint of pFl 4.01 buffer solution
and replace cap can probe.
r
CALIBRATION AND SAM.PLE RESULTS
EXTECH Oyster-10 pH/mV/Temperatrrre Meter erial Number 022055
j f
f t
pH 7.01 Buffer
Temp Initial Finial
pH 4.01 BufEFhijal
Temp InitialTemp
IIH 1-0.0). Buffer
Initial Final
Storm Saniple
Date
Ternlr
pH
173 1
7, 7_ 6
7q
03
14,01 17s_
z

Stor mwater Discharge ®utfall (SDO)
Qugalit7tive Monitorix)g Report
i>ur;'trirlrrr!r.r: on_Iillrrr?; ow [hisforarr, pkelsa visit: Iitll�all�"{1.c:n1:�t..StC.311:.11FItil]Il_ul:[IIs Ill!laIIilc ls.IIInIIII1134(:l'o_1I1�
Permit No.: Nl(,l 0I�0_l.0 10 /U 13 I0l car Ccrtif"icate of CoveraLzc: No,: NIGG_I
T�
i�;u;ilityNmuc: irrl5v�f�cP r�—Ll—
cownty: c3Gi{�t4 � — Phone No.
Dale ol, lnsllc(--tion: —1 Z /6 /.f ---- — - — --- —4�
ol,____----
total Pvc:ll_ Prec:ipil;1lion Onchcs)
11l:Is this a I ealrcAMMIive Slornl I7-vent? (Sec; tni'urmarion below) Yes ❑ No
Mer sc, dwi-.-k ,oil;— p'rmil to ve:ri& il'Quolilruive Mfwliloriu,l musl he he{/trrrrwd durilig (t rr:prr_scrrlrrlivc
.rlorm evcrrl vrrr+]).
;1 Storm f vent" is .1 Stol nt Cvtlrlt that nl[,asures greil(or than 0. f illch(s ul'rainEllf and tll:ll
k Ilta: crlud by is le:,lst 72 hours Q (lays) in which no storm event nlerlSI.Wirl" greater Iha[1 0. 1 inches IMS l
'I Occt1'1*t:(1. A sim-le morn event play contaill 1.11) to 10 Consecutive herons of'r10 precipitatioil.
13y this si!;nclture, I certify (11,11 hj.� repurl iS 'ICUIRL(C 111d complete t() the best (ifs my knmvledge.:
{S'ig1latrlrL: kA7 Po(
1. [;nlfafl I?irtic;ril�liun: p
Ourf'all Nu.
-- ! Strttcaurl.{pip(:, ditch, cti•.) -- -- _ --
Not:civing Slruatrl: rr,x'bleSe.+1e------
I?c;scrille lhc: indust.rial activities that Occur wilhin the; outl'all dr,tinaoe area:
2. Colru•: 1)CS(.I"ihc llle COI(W ok tlul: di.'c:h,lr��e using basic colors (reef, brown, blue, etc.) and tint
(li!:Ilt, 111c(limil, d;11,k) :I: cltacrilrttu'S: — !r
. (Jlit,r: distinct odor,~ th,t. t1w discharge may have. (i.c. smells strorr}gly of oil, Yvcnk
callorilic odor, ctc.: U ffc�0
P;1"'t, I of-2

4. Cluril : 01oosc; ill o nunll►c:r wlricII best describes [I EC cl,n-ity (It' Oh' diSGII;trgc, NVIILrc. 1 i5 GIc, u'
ilEttl ;1 IS VCr1' clQtfcly;
I 02 i 4 y
S. Floating Solids: Choosc: €Ile nurtthet• 1vlriclr hest.descrihes ilia wrim"O of t'IMAng MAN Al we
stunt►moer discharge:, whc:re: 1 is nn m lick am! 5 is €lre: sul'l:we coverecl with tln::l ke tiUlM:
r I) 2 31 4 5
6. Sr►slu:ruled Solids: Clunsc.• Ow rlun111cr which best.desra'ihcs the: amount 0l'susl1errdecl scllicls in
1lre s(.orniwawr clisc:har',_c:, whcrc: 1 is ncl solids crud 5 iti astre111ely tnudtly:
I a 3 4 5
7. Is tlte.rc arty foam io Ow storrnwater discharge? 1'cs
?i. Is Illerc an oil sltc•cn in €ire; Storinwatcr
9. Is tlrcrc ovidonce of crosit►n or deposition al tllc outfall'? Yc ss ,
I (). Other (?viola: Indir.ato►-ti of Ito► rniti°,ttc:r Yc►Ilrrtinn:
l_,iti[ :In(l ticsc:rihc
IZIOA)
Note: Low c;l,u-ily, high solids, ,Irtc or the: prawn e of Rmn; nil slwwq or nuty he
indic:irtive of poflu€"1111 c:.xl►0.SlH' :. 'flrest' c:nncliticrrrs warrant lttrtltczr inves€it_allon
s1wU-"bkalI wF

Storm water Discharge Outhall (SDO)
Qufalitative monitoring Report
1`or vIl7olllte,l.' oll lfl!'fnf( rlhlf fit is fi)r"Fll, PICI7SC 1 rISll: ISII]�_llli"_'t_,.�:11[',,t�F1i�I1L'.ilS/ ult�c)r[IIS 04IL1011IZ:11IS.1II1111.111im:ItII'll::;
Pc:rmil No.: N/iJ b/ a/� 0/ M 13 UI or Certificate of Covet-R-e No.: N/C/G/—/-- /--l—��l--/
Fact Illy 1\l une: T�Cldsvltj� �C P ___
Coun(y: lac r� �tlrru _ Phonc No.
Dille orJilsl)ectioll:Time ol' 1sIspeclion;
1'1�lal F vwlt Procipitalion (inc•hcs): `v "<
WV is Illis a R(:I)res<?ntsitivc Sulrll) I v nt? (See iilf'orn)at;olt below) O] Ycs ❑ No
I'Icrr.er. chi:ra,: yr w-pe"nnit Tn r-cri/ti' i '{hralitfflive Xlonitorht., must br paifr7nf ed rltcritig rr rrslneselftrrfive
rturrlr crr7t! ( re"quir-c'mcnic vary).
,� 'ltt l�rtacnl tliv(..SttTrm l vcnt" is ;) Storm (,Vc 111 thal. uie Islires treater (han 0.1 ilwhcs of rainf;111.:11al that i
is pi-cct dcA l.)y}tt I(':rst 72 h(ltlr, (3 LIZINIS) ill which (,Vent ll CkISnr-ill" g;J-C. IICT I.11:ktl 0, 1 inclleS Ilil,
oc.ciar•c.cl. A ,iW1IC StUi'nt CVellt rilaY corltn;n ut) to � �} CUllti(:elEl1VC l1011l'ti c)I' rl(T precil�iLttir)n_ -- -- --- ^•r
13)' this SII!Il:1tc11'('•, .1 cel-lifYfilat..lFfS report is aCC(lr;tI.0 allcl cotlll)ide to tlw, hest of my knowic(1ge:
(Si,_n:Fltir(; of �P -rillec or Designcc)
1. Oil fl':Elf Desc:ril Uml: :2
Uull,Ell No. —_ z Strts+`•ttrrL: (I)i1iu, (lit(;Il, etc.)etc.)— �9'_w—._---- w--
I�c:cc:i��iny---
D"SCI•i1)C Ill(: ilIdUS11.1.11 F1cliv'l.ies th:tl' oc utir wkhill tllc: oulf,111 drainage nrF.'
A
evGe
2. Cohw: I)cs(.rihc tilt, color ol'Ill (: iisdl tr,c/using basic Colors (rLll'. brown, Nuc, (Ac.) and lint
(light, nic(littm, (,ark) :is clesc,ril)lor,:__--
a. C)thW: ]�csl:rihr, ally (li,liuct odors (hal the dischar-ge Itl:l)' 11,1ve (i.U., snlcllti Strongly of Oil_ wt':lk
chlorine odor, oc. j:--N0pjG----
I-ago 1 ol'-'
Swt!-2'I:'-1 l"u)5

4. faarily': Choosu 1hc, nurnbur Wllicll !lust describes 111e clarity of tile. diseflat-p,c., tvllcrc; I is c:ieln•
:Ind > is vc:r'•y d0LJC1y:
I 7_ 3 4 5
-. Floatiiig 5,r1i115: Chorwo the nunl1mr which best cluscr•ibm the ,lnumnt or floating solids hi dic.
storimwiter discharge, where; f is no solids and 5 is the surface covered with flotahl ME
I (i)
3 d 5
6. Sllspelldetl Sullins: Cimsc solids in
the stornnvalter disc;lrirg, wliery I is iro solids wid 5 is (wremely muddy:
f � 2 : i �>• 5
7, is tllurc; ally !wall! ill the StOrInWalta discIlarg"e? Yes
8. Is there; ml oil sheen in 1110 s1c>rnlwatol. disclmrge? Yc, (N}�
{I. Is thurc, evidence; of crosioll or dellositioll at the ollt.1,1111? Yes 6()
10. 01.11c;1• Obviolls 111dicolor,S all still-111water 111111111ioll:
Us[ ;Ind do"C.ribe 4)150E
Not(": Low clarity, 11i"h Solids, candor 111C 17rtacnce ur 1•0:un_ coil sbCrn. dray I)C
inICIiVe 0 f po H Mmacgxmtlrc- 11wse conditions wan antRIrdwr investigation.
1ATv 2 or 2

• t
STORl4IWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 60000A0 or
Certificate of Coverage Number: NCG
FACILITY NAME 41i
PERSON COLLECTING SAA,IPLE(S) J
CERTIFIED LABORATORY(S) 4[ I4 Lab #
Part A: Specific Monitoring Requirements
SAIiPLES COLLECTED DURING CALENDAR YEAR: JgL4
(This monitoring report shall he received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY 11liZ Kl -Ifhalml
PHONE, N0_1,;1/) 3t14 Z:FG Z.
By this signature, I certify that this report is acettrate
complete to the best of my knowledge.
1
iSample
Date
11
Collected
K111141
Total,
Flow (if app.)
1
Ed
EPF& ZZIMi
A
idii
r -
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? ✓yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Renuirements
Outfall
Date
50050
00556
00530
00400
o.
Sample
Collected
Total Flow
(if applicable)
Total RainfallGrease
(if appl.)
Non -polar ar-Total
O&G/TPH
(Method 1664
SGT-HEM), if
appl.
Suspended
Solids
PH
New.Votor OF
Usage
nto/dd/ r
MG
inches
In
Units
al/mo
JV
2
-It.
7
Form SWU-246-062310
Page 1 of
I

STORMWATER DISCrL,RGE OUTFALL (SDO)
MONITORING REPORT
IVC.S
Certificate of Coverage No, NOW 06W30 SAMPLES COLLECTED DURING CALENDAR YEAR: z Of C.
(This monitoring report shall be received by the Division no later than 30 days
I ! from the date the facility receives the sampling results from the laboratory.)
FACILITYNAME A )r Prad`,-L Re{�y► lie Asv COUNTY _ �kUAs + 14 --
CERTIFIED LABORATORY(S) _ f laf 8 44eje4l Lab #
Lab # (SIGNAAVU OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Vehicle Maintenanee Activity Monitoring Requirements (only if, on average, more than 55 gallons per mouth of new motor oil is used)
Outfall
No.
Date
Sample Collected,,
molddiyr
Total Rainfall,
inches
New Motor Oil Usage,
Am mal average
afto
00556
00530
own
Oil and Grease,
mg/L
Non -polar O&GfTPH
(Method 1664 SGT-.REM),
if appl.
Total Suspended Solids,
M91L
pH,
Standard units
Benchmark
-
-
30
IS
100
6.0 — 9.0
►d 10 tit,
1-Z
7
nrD
ZN. 7
7.1G
Note: If you report a sampled value in excess of the bench=k value, or outside the benchmark range for pH, you must implement Tier 1 or Tier 2 responses in the General Permit.
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, underyenal!y of law. that this document Find Rif atfichments were prep red ienrl= my Air -action or- supop4sion In aecor-doaeo with --- rt� designed to
assure that qualified personnel properly gather and evaluate the information submitted, Based on my inquiry of the person or persons who manage the system, or
those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and hnprisoament for knowing violations."
-LiL Q-L,� �CW�6�2
NgnaturV Permittee) (Date) __-..
orra SWU-254062310
Page 1 of 1

PrOODU 21- Detegaffon of Authority to Nan-Qlfcer Positions
rY M1l.�.ww Irr
She UrtOerstpned, Rabart D. Ccrltev_ in my 03pacrty as V rt enl - 6fab I Ertosrfeerin0 Of
Q{sMO�Xs WS., pursuant 10 hDe1egaMm of AuOwhy Pofcy. hereby dsloples aul UMy as dnagwd heron below 10
the btbamg non -after posdl0n(s).
P0SM ON rirtrt ARM COWAAW Up-W MUM VALU9
See d Page 2 for tlst of pow4on liflea TWA
08SCMMCN OF AUTiits M
Ault>ertly to wwcute permit appkaran. per.. ralatad subrriftions and docarrrer>ts. and Muting M;ngs and
documents required by local, state. and federal regulatory agencies or crthwitias pertaimrtg 10 envi►onrrterttat
health. and safety compliance for the Wakes Barre. Gardner, Cryo rochlnery and Pnsrn Mea*nwms f40111e3
Or►ra wrnonty may On SUeerpI I Win ft forbv^V WWnelnru of •ny}
OTAq mUR.ry rnry nor de wbdohiiq a.
la lake effetl vrllen cowters(grza by the Gorp*Me Semlary or any Assislartt Cogwale Secrelery end to coniirwe in
effect for so " as the mated Pasoan 111WS) remain urrcharrged, or uMd slush aulhasRy fh" be revised or
revoked by notice lheM& by the undersigned. ht8 or her suctmor to QW.G. or the yer30n to whom the designated
pasition(s) raw. —is,;
ajL
ontor
C!Y
r
Cohn terWiped by } , "t r
�i.rywa9+. S iniA�fht f i t nsr 4rrr��r r Tq+rc
S+. r � �� •I..: yl41 • rnnwue.wal � •4t

AfR
OMODLICiS 'L Delegation of Authority to Non-Offeer Positivns
P44nmm rTu
Operabpns Manager
Lme
Site Allow w
Asastem Site Manager
Sue Supervisor
PI M Manager
Assistant Plant Manager
Plant &Vemlendenl
Canstrttc M Marmw
Ehviramnamal Manager
Enwarmanial Englnw
Senior Environrn mW Engmeer
Prfnclpal Environmental E-Ob"m
Senor Pdm pol Enviroamsnlat Engmeer
Load E nwimmmental Engineer
Emhmnrrumm Speclobt
Senior Env;mnrnentat SpecWsl
Prirt:ipW Ermkonnim" SpocUftl
Senbr PdrwjpW Enviromnwrtal Speaabt
FM I Spry W. 1.13w.InFTM11wI�M�11 it
NIA

AIR
ACTS�r
Air Products and Chemicals, Inc.
357 Marian Ave
Tamaqua, PA 18252
Telephone [phone]
June 18, 2014
Division of Water Quality
Attn Central Files
1617 Mail Service Center
Raleigh, NC 27600-1617
RE: NCSS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report for the Air
Products and Chemicals, Inc. Reidsville, NC Facility.
If you have any questions regaring this submission or require additional information, please feel free to
contact me directly at 570-467-4399.
Sincerely,
N
J seprnmental
a
En Specialist
Air Products and Chemicals, Inc.
Electronic Materials Organization
Tamaqua PA 18252
CERTIFIED MAIL: 7013 1090 0001 8611 4303
3t
C--
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@
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n
nn r:
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o
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9 i F
j

STORMW ATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
7 b
Permit Number: NC$ 0 a or
Certificate of Coverage Number: NCG
FACILITY NAME �� �," 't"'� ••�1VJ le-( ArLi
PERSON COLLECTING SAMPL
CERTIFIED LABORATORY(S) �CG Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: 7-"519
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
Wih1'M
PHONE O. (&&) y5 7196!z ..._
ATURE OF PERMYfTEE OR DESIGNEE)
By this signature, I certify that this report Is accurate
complete to the best of my knowledge.
I
111
1 1
I N
1 S 1 1
1
1 t
��
1 1 1 1•
1
R I I I
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? Dyes —no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Reouirements
Outfall
.No._..._...-.--
Date
-Sample---_. --- _----
Collected
56050
00555
00530
00400
_
.Total.Flow _---.......Total
(if applicable)
Rainfall_
-Off.&.Greco__
(if appl.)
.Non -polar--
O&GI"R
(Method I664
SGT-HEM), If
appl.
Total . .-
Suspended
Solids
.pH
New -Motor Ot7_
Usage
mo/dd/ r
MG
inches
Units
al/mo
1
r.( fib
7.
Form SNVII-246-062310
Page 1 of 2

STORMWATER DISCHARGE OUTF'ALL (SDO)
MONITORING REPORT
Certificate of Coverage No. NCG-lam,9y 3y
FACILITY NAME
PERSON COLLECTING SAMPLE(S) j
CERTiFtED LABORATORY(S) P Lab 4-
Lab 0
SAMPLES COLLECTED DURING CALENDAR YEAR:.201
(This monitoring report shall he received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
COUNTYjGlhlu r►•t
l�C��La�►i�air-C���'i�Lr�
(SIGMATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Vehicle Maintenance Activity Monitoring Requirements (only if, on average, more than 55 gallons per month of new motor ail is used)
Outfall
No.
Date
Sample Collected,
moldd/yr
Total Rainfall,
inches
New Motor Oil Usage,
Annual average
mo
00556
00530
00400
Oil and Grease,
mg/L
Non -polar O&G/TPH
(Method 1664 SGT-HErii),
if appL
Total Suspended Solids,
mg(L
pH.
Standard twits
Benchmark
-
-
-
30
15
100
6.0 — 9.0
r
P4 D7.
o
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must implement Tier l or Tier 2 responses in the General Permit.
Mail Original and one copy to:
Division of Water Quality
Attu: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty f Iaw, that this document and all attachments were prepared under my direction or supervision in accordance with a system ditigned to
--- -" assure that qualified pe ne l properly gat4�erariii evaiusite the in[armutian stihini#3et1 Rased an my inquiry of the person or gcrsot� whoitt�i3age the sysfem, ar
---
those persons directly res nsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true; accurate, and complete.
I um aNre that there are s gnificant penalties for submitting false information, including the possibility of iines and imprisonrnent for knowing violations."
GIlt�19
(Date)
Form SWU-254-062310
Page 1 of I

STORM EVENT CHA.RACI'ER1,STiCS:
Date /L I Y ,
Total Event Precipitation (inches): _ f
Event Duration (hours): -/ — (only if applicable - see pernvt.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable - seer permit)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who monageAtthe system, or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and b ief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
includinkthe possibility f fines and imprisonment for knowing violations."
61 1�� +y
(Date)
Form S WU-246-062310
Page 2 of 2

Outfall 001
Inches of Rain 1.1
Area Sq Ft
Impervious Area 127000
Gravel 425500
Total 552500
Run Off Factor Ft of Rain Cubic Ft Gall
0.9 0.0916667 10477.5 78371.
0.5 0.0916667 19502.083 145875.
Area x runoff factor x feet of rain = cubic ft of water runoff
Cubic feet x 7.48 = gallons
Million Gallons
0.0783717
0.145875583
Total Flow 0.224247283

A1R Z.
PRODUCTS *.` Delegation of Authority to Non -Officer Positions
The undersigned. Robert D. Conley, ,n my capacity as Vice Pfessdenl — Global Engineering of Air Produces and
Chemicals. InC.. pursuant to the Delegations of Authority Policy, hereby delegates authority as described herein below 40
the following non -officer posilion(s):
POSMON TITLE AN() COMPANY AAAXIMUm vALUE
Each TransachoNCOn"c+
See attached Page 2 for list of position lilles NIA
DESCRIPTION OF AUTHORITY
Authority to execute permit applications, permit related submissions and documents, and routine filings and
documents required by local, stale, and federal regulatory agencies or authorities pertaining to environmental.
health, and safety compliance for the Wilkes Barre, Gardner, Cryomachinery and Prism Membranes facilities
❑This aulnOnty may be subdelegaled w+lh the rOl[owing re5trrCl+onS ld any)
This Aulhonly may rTOi be subdelegaled.
to lake effect when countersigned by [he Corporate Secretary or any Assistant Corporate Secretary and to continue in
effect for so long as the designated position Gtie(s) remain unchanged, or until such authority shall be revised or
revoked by notice thereof by the undersigned, his or her successor in office. or the person to whom the designated
positions) report.
C --
r3Ntr
$IPlnlu+t /
Countersigned by: ti' -'-
n;+l.•
�'u ryu+:,b tir L.n�A..,�L flit (nrpora [[ err rrl.iy'
I—i. an, `.In..':nq t, —n „ —AI Dui

AIR -'•
PRovucTS 1= Delegation of Authority to Non -Officer Positions
El,rt.t u,.,., W.
I POSITION TITLE MAXIMUM VALUE
!i=arh T ran 5.KI,ofvC onvacl
I Operations Manager
j Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmental Soeciatist
NIA

aceAnalytical
r www.paoslab&cvm
May 30, 2014
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: Storm Water Testing WW
Pace Project No.: 92201685
Dear Mr. Owens:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on May 16, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Terri Page
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

aceAnaiXical
www.pacalaLaoom
CERTIFICATIONS
Project: Storm Water Testing WW
Pace Project No.: 92201685
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37705
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification M 12
VrginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
FloddalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VrginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, I nc. Page 2 of 13

Pace Analytical Services, Inc.
aceArralytica! 205 East Meadow Road - Suite A
Eden, NC 27288
wwwpaceJabs.com [phone]
SAMPLE ANALYTE COUNT
Project: Storm Water Testing WW
Pace Project No.: 92201685
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92201685001 OUTFALL 1 SPRING 2014 SM 2540D
CHM
1
PASI-E
EPA 1664B
CLW
1
PASI-C
EPA 351.2
JDA
1
PASI-A
EPA 353.2
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13

aceAnalXical
www.patalaUmm
f
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Storm Water Testing WW
Pace Project No.: 92201685
Sample: OUTFALL 1 SPRING 2014
Lab ID: 92201685001 Collected: 05/15/14 12:30
Received: 05/16/14 10:43 Matrix: Water
Parameters
Results Units
Report Limit DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
6.3 mg1L
2.6 1
05/19/14 12:30
HEM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg/L
5.0 1
05/20/14 14i56
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA351.2
Nitrogen, Kjeldahl, Total
0.68 mg/L
0.50 1
05/30/14 16:22 7727-37-9
353.2 Nitrogen, NO2IN03 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.55 mg1L
0.020 1
05/23/14 18:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13

aceAnalytical
wwwpaoel 4corn
i
i
Project: Storm Water Testing WW
Pace Project No.: 92201686
QC Batch: EDEN114592
OC Batch Method: SM 25400
Associated Lab Samples: 92201685001
METHOD BLANK: 1202007
Associated Lab Samples: 92201685001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1202008
Parameter Units
Total Suspended Solids n i
Pate Analytical Services, Inc.
205 East Meadow Road - Suite A
Edon, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 25400
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 05/19/14 12:24
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 238 95 80-120
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the written consent of Pace Analytical Services, Inc.
Page 5 of 13

1�55'&e Analytical
www.pacalabs.com
r
I
Project: Storm Water Testing WN!
Pace Project No.: 92201685
QC Batch: GCSV117663
QC Batch Method: EPA 1664B
Associated Lab Samples: 92201585001
METHOD BLANK: 1202826
Associated Lab Samples: 92201685001
Parameter Units
Oil and Grease mg/L
LABORATORY CONTROL SAMPLE: 1202827
Parameter Units
Oil and Grease mg1L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 05120/i414:51
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 37.5 94 78-114
MATRIX SPIKE SAMPLE: 1202828
92201875001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Oil and Grease mg1L ND 40 37,1 93 78-114
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the wntten consent of Pace Analytical Services, Inc.. Page 6 of 13

aceAnalytica!®
wwwpacehW.com
t
I
Project: Storm Water Testing WVV
Pace Project No.: 92201685
QC Batch: WETA119114
QC Batch Method: EPA 351.2
Associated Lab Samples: 92201685001
METHOD BLANK: 1207112
Associated Lab Samples: 92201685001
Parameter Units
Nitrogen, Kjeldahl, Total mg1L
LABORATORY CONTROL SAMPLE: 1207113
Parameter Units
Nitrogen, Kjeldahl, Total mg1L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336)62M921
QUALITY CONTROL DATA
Analysis Method: EPA 351.2
Analysis Description: 351.2 TKN
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 05130/1415:57
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
10 10.1 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1207114 1207115
MS MSD
92202287001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 6.5 10 10 17.9 16.6 114 101 90-110 7 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1207116 1207117
MS MSD
92201558001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 2.6 10 10 11.8 12.4 92 98 90-110 5
Results presented on this page are in the unite indicated by the "Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the written consent of Pace Analytical Services, Inc.,
Page 7of13

aceAnalytical
www.pacelabs.com
i
Project: Storm Water Testing WW
Pace Project No.: 92201685
QC Batch: WETA/19101
QC Batch Method: EPA 353.2
Associated Lab Samples: 92201685001
METHOD BLANK: 1206298
Associated Lab Samples: 92201685001
Parameter Units
Nitrogen, NO2 plus NO3 mg1L
LABORATORY CONTROL SAMPLE: 1206299
Parameter Units
Nitrogen, NO2 plus NO3 mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
(336 )623-8921
QUALITY CONTROL DATA
Analysis Method: EPA 353.2
Analysis Description; 353.2 Nitrate + Nitrite, preserved
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.020 05123/1418:05
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
2.5 2.5 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1206300 1206301
MS MSD
92201846001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, NO2 plus NO3 mg1L 0.039 2.5 2.5 2.4 2.4 95 94 75-125 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1206302 1206303
MS MSD
92201147001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, NO2 plus NO3 mg/L ND 2.5 2.5 2.3 2.3 94 93 75-125 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the written consent of Pace Analytical Services, tnc..
Page 8 of 13

aceAnalXical
www.pacslabs.00m
f
QUALIFIERS
Project: Storm Water Testing W11V
Pace Project No.: 92201685
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limil and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Se rvices- Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded OC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/30/2014 05:54 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 13

aceAnalytical
wwwpscebba.com
i
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Storm Water Testing WW
Pace Project No.: 92201685
Lab ID
Sample ID
QC Batch Method
QC Batch
92201685001
OUTFALL 1
SPRING
2014
SM 2540D
EDEN114592
92201685001
OUTFALL 1
SPRING
2014
EPA 1654B
GCSV117663
92201685001
OUTFALL 1
SPRING
2014
40CFR PART 432.2
WET131296
92201685001
OUTFALL 1
SPRING
2014
EPA 351.2
WETAl19114
92201686001
OUTFALL 1
SPRING
2014
EPA 353.2
WETA119101
Date: 05/30/2014 05:54 PM
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Analytical
Analytical Method Batch
Page 10 of 13

aceAnal ical'
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chainof-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page. of
Section A Section B Section C
Required Client Information: Required Project Inforratiom Invoice Information:
Company: ;P'R Repurt To: Attention:
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*Important Note: By Signing this farm you are amepfing Paco s NET 30 day payment terms and agreeing to late charges of 1.5% per month tDrany Invoices not paid wdNn 30 days. f F-ALL-Q-020rev,07, 15-May-2007

CHAIN -OF -CUSTODY,/ Ann loical Request Document
The Chain -of -Custody is a LEGAL DOCUMI,N7 All relevant fields must be completed accurately.
i aceArialytical' .
www.pacaiab®.com
Section A Section B S.4,169
Page: of
Required Client Infoprmatiion:- '/ 1 Required Projed Information: Invorce P ormatlon: 71 t/1
r, Company:��I'f/Lx741-�3df116 ���YtrGRI Report To: ,-'AtteMio :. - - ' 1 f. � 250:2.�"'
Address: - Copy.To: - - Company Name: REGULATORY �AGENCY
'" 6''77' Z r Address: r NPDES r . GROUNDWATER r : DRINKING WATER
Email To: - 1 Purchase Order No.: -=-+'--*+ Pace Quota '
crieAs�' %Y ,6e4C f �h+ x - - : - Reference: r UST r' RCRA r. ; OTHER
rR
Fa%: Project Named ' Pace Prgea.. A t
Z j Z X IS Manager- Site Location h r V
' Due DatafTAT: - - Project Number. .. ... Papa Prof" p, • f r '
. STATE Y .r
Requested Analysis uteied (Y/N
y - _
Section D Matrix Codes _ ^ _a z
Required Cpenf Information' - MATRIX hCODE $ g COLLECTED
. Drinking Water DW a .0 zz . .
Water- WT r,
WastoWater WW' - cc _coat SITE CNDIGP E -LU (I
Product P
Soil/Solid Si
SAMPLE ID.
oiI Ix
Wipe o U.,WP
{A-Z. 0-9 ! r} Air.' '. AR . a. z
Sample IDs MUST BE UNIQUE . Tissue TS • O : a � i
Other S OT - ) � ., Z o U '
r#u' co
a a d O G W lZ
F .. - • ¢ p e to Z U IOD N d7 C' . O
N DATE' '- TIME ., DATETIME �: S Z S Z Z O y 4 l,. Pace Project No./ Lab I.D.-
owl Ca
3:
:4:
7: ..
.10
21
12
-ADDITIONAL COMMENTS / RELINQUISHED BY f AFFILIATION DATE: TIME,;:" ACCE D BY A ILU13T0 PATE TIME SAMPLE CONDITIONS
_U .. u
pf SAMPLER NAME AND SIGNATURE' = - ' . C
m - - PRINT Name
. �
.'.DATE
SIGNATURE of SAMPLER;'-'2Y-", (M DDiiYY)tl ra
W „'Important Nate: By signing this form you are accepting Pace s NET?Aday peymant terms and agreeing to tote charge$ of 14% per month fu any invoices not paid within 3O days: - F-ALL-"20rov,07, 15-May=2007

Document Name: Sample Condition Upon
..Document Revised: March 13, 2013
�n�Aw
Recel t SCUR
P e i of 2
Document No.:
Issuing Authorities:
F-EDN-CS-003-rev.09
Pace Eden Quality Office
Client Name: .
Where Received: ❑ Huntersviille ❑ Asheville 2' Eden Raleigh
Courier (circle): Fed Ex TIPS USPS Client Commercial Pace Other
C�ist2slyS.ealarr.CoolerlB.oxPreserrt:_...[)yes_.....❑na..... Seals.intact:_...❑. -yes --.-❑-..no__.._.-----
Packing Material: [bubble Wrap []Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun E0007 Type of Ice: 81ue None . ,0 Samples on'ice, cooling process has begun
Temp Correction Factor: Add 1 Subtract _ C
Corrected Cooler Temp.: r O C
Temp should be above freezing to BBC .
Biological Tissue is Frozen: -Yes No r<uA
Comments:
Oafs and initials of person examining
Chain of Custody Present:
Wes ❑No
OWA
f . , -
Chain of Cu Filled Out:
WYes ❑No
❑NIA
2.
Chain of Oustxly Relinquished:
268 ❑Na
❑NM
3.
Sampler Name & SI nature on COO:
21%es- ONO.
❑wA
4.
Samples Arrived within Hold Time:
OYes ONO
I INIA
5.
Short Hold Time Anal is <72hr :.
Dyes Iallo
.13 NIA
6.
Rush Torn Around Time Requested:
G(Yes ❑No
❑ WA
7,
Sufficient Volume:
( Yes. ONO
❑wA
8, =
Correct Containers Used:
-Pace Containers Used:
UrYes ❑No
VYes ❑No
OWA
❑NIA
9.
Containers Intact:
InYes ❑No
, ❑NIA
10.
Filtered volume received, for Dissolved tests
tlYes ❑No
- VWA
11.
Sample Labels match COO:
-Includes date/timeAD/Anal)sis Matrix:
ElYes ❑No
OWA
12.
Alt containers needing preservation have been checked.
All containers needing preservation are found to be In
compliance with EPA recommendation.
exce irons: VOA, w9onn, TOC, 0&G, WI-10 water}
Yes ❑No
KY s ❑No
OYes ONO
❑NIA
ON/A
13.
(i
Inlltal when oom lend
Samples checked for dechlodnation:
4Yes 0No .
OWA
14.
Headspace In VOA Vials Amm :
❑Yes ONO
ZNNIA
15.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # If purchased):
❑Yes ❑No
[]Yes ❑No
WA
&A
16.
Client NotifieaVont Resolution: Feld Data Required? Y 1 N
- Person Contacted:. _. _... Datelrme:_----
Comments/ Resolution:
SCURF Review: is !jars: tA I V It 11 Place label here
SRF Review: L Date: I OR
Note. Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form vAl be sent to the North Carolina DEHNR
Certification Office (Le out of hold, incorrect preservative, out of temp, Handwrite project number
Incorrect containers) (If no label available)
e13of13

Reidsville NC Stormwater Sampling Checklist
Completed by:
Item description
D
1. Sample during representative* storm event at Outfalll#1
'>0.1" rainfall, sampled within 30 minutes of start of event, and no other rainfall event >0.1" in
previous 72 hours
.� 2. Spring sample between January 1s`-June 30t or Fall sample between
L July I" and December 31"
1 L7-0 1 3. At least 60 days has passed since last sample taken I 1
6. Fill out SDO qualitative monitoring report for BOTH o tfall 1 & 2.
Report any deviations to Site Manager ,
• NC State form SWU-242-XXXXXX
4�gt
7. Fill out form B2 and C2, site inspection and summary
rU
8. Fill out SDO monitoring report (DO NOT SIGN)
1
Y NC State form SWU-246-XXXXXX page 1
f�C,Tu
9. Fill out Storm event characteristics form (DO NOT SIGN)
o NC State form SWU-246-XXXXXX page 2 11
10. After analysis is complete, check results against following benchmark
' values. Report any deviations to the site manager
Benchmark I Result
Total Nitrogen: 30 mg/L 5. mg/L
pH: 6-9 su 7, YO1 su
Oil and Grease: 15 mg/L 'I mg/L
Total Suspended Solids: 100 mg/L b, 3 1 mg/L
11. Compile all documents listed above, together with analysis results,
scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12. Environmental Specialist signs form SWU-246-XXXX0 and sends to
NC State within 30 days of analysis results. Also places copy of all
communications with NC DENR in Reidsville share site

CALIBRATION AND SAMPLE ANALYSIS PROCEDURE
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
H analvsis mus
collection.
1. Turn on pH meter
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
4. Rinse pH probe with deionized water and blot dry with a clean, soft cloth or tissue.
5. Place both the temperature probe and the pH probe in 7.01 pH buffer solution.
6. Shake the pH probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7_ Record temperature and pH reading.
8. Press and hold the CAL button until "CAL" flashes or. the screen.
9. Calibration will take approximately 30 seconds. When complete, record final pH reading.
10. Remove probes from 7.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
11. Repeat steps 5 through 9 using the 4.01 pH buffer solution
12. Remove probes from'4.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
13. Reheat Steps 5 through 9 using the 10.01 pH buffer solution
14. Remove probes from 1.0.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
15. Insert both probes in the storm water sample, and stir the sample gently to ensure homogeneity
and minimize carbon dioxide entrainment.
:16. Walt one minute for reading to stabilize.
17. Record temperature and pH reading.
18. Remove probes and rinse pH probe in deionized water. Blot dry with a clean, soft cloth or
tissue.
19. Dampen the inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace cap on probe. jj
CALIBRATION AND SAMPLE RESULTS
EXTECH Ovster-10 off/mV/Temperature Meter Serial Number 022055
pH 7.01 Buffer
pH 4.01 Buffer pH 10.01 Buffer
Storm Sample
Date
Temp Initial Final
. Temp Initial Final Temp Initial Final
Temp pH
-7. &
77 7-Ile b 7 -7 �� �a.-s
1 `Z " 7,
Air Products lnternai Use Only

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: htti):Mo.cru.stntc.nc.us/su/Forms—Dr)cument.s.htmftmiscform.s
Permit No.: NfGol_Ql
Facility Name:
County: Lr
Inspector -14
Date of Inspection:
Time of inspection:
01.L2l6l„�l I or Certificate of Coverage No.: NIGGI !
c/Ctr� W 42!w4 I
Total Event Precipitation (inches):
Was this a Representative Storm Event? (See information below) `0] Yes E] No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary). I
A "Representative Storm Event" is a storm event that treasures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signature, I certify that this report is accurate and complete�o the best 4f my kn
(Signature of PerrniWee or Designee)
1. Outfall Description:
Outfall No. / Stnlcture (pipe, ditch, etc.) �� e
Receiving Stream: ! /C11.?6 / ('d ,ril- C g e
Describe the industrial activities that occur within the outfall drainage area:
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:._( t5�'i7Jl, _ — .--
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): A10 6yei--
Page 1 of 2
S WU-2a2-112608

4. Clarity: Choose the number which best describes the clarity of the discharge,
and 5 is very cloudy:
1 2 3 4 5
1 is clear
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating sots:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the storrnwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2! 3 4 5
� i
7. Is there any foam in the stormwater discharge? Yes
8. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes Ci
E
10. Other Obvious Indicators of Storrnwater Pollution:
List and describe tj bN
i
I
1
i
i
I
Note: Low clarity, high solids, andfor the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
i
Page 2 of 2
SWU-242.112608

Stormwater Discharge 4utfall (SDO)
Qualitative Monitoring Report
Forguidance onflling out thisfonn, please visit. htty /lh2y.cnr.state.nc.uslsu/Forms Documents htniftiscforms
Permit No.: N/Cll 0l �l (>I bl Ib I or Certificate of Coverage No.: JGGI IY%� I I I
Facility N a% V21
County: Phone No. ,fit 9 Z
Inspector:
Date of Inspection:
Time of Inspection: D
Total Event Precipitation (inches): A I
Was this a Representative Storm Event? (See information below) V Yes ❑ No
i
Please check your permit to verify if Qualitative Monitoring must be performed during a representati ve
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that i
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0. l inches has
joccurred. A single storm event may contain up to 10 consecutive hours of no prpcipitatiati.
By this signature, I certify that this report is accurate and
(Signature of Permittee
the best r knowledge:
1. Oatfall Description:
Outfall No. ?— Structure (pipe, ditch, etc.)
Receiving Stream: 6 Li v)nng cr&Q
Describe the industrial activities that occur within the outfall drainage area:
I�
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells
chlorine odor, etc.): WL%n t?
Page 1 of 2
SWU-242-112608
of oil, weak

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
L 20 3 4 5 `
i
5. Floating Solids: Choose the number which best describes the amount of floati . solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 L-- % 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy;
1( 22 3 4 5 1,
1
7. Is there any foam in the stormwater discharge? Yes No—
S.
9.
Is there an oil sheen in the stormwater discharge? Yes No
Is there evidence of erosion or deposition at the outfall? Yes Nq
10. Other Obvious Indicators of Storrnwater Pollution:
List and describe fjo
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/depo:
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
may be

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Permit Number: NCS 6000096 or
Certificate of Coverage Number: NCG
FACILITYNAME 11-PCt' P4e10JV"L►-E
PERSON COLLECTING SAIMPLE(S) LEb! 6�)! '
CERTIFIED LABORATORY(S) i <1 AN4L?1-)(eL, Lab #
Lab #
Part A: Specific Monitoring Requirements
SAMPLES COLLECTED DURING CALENDAR YEAR: T.0 f
LI
(This monitoring report shall be received by the Division no later than 30 days from
the date the facility receives the sampling results from the laboratory.)
COUNTY iwuu� 6 IpM
PHONE NO. (33 t, I Iq q- ZR W-
(SfGNATURE OF PERMITTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Does this facility perform Vehicle Maintenance Activities using more than 55 gallons of new motor oil per month? k yes _no
(if yes, complete Part B)
Part B: Vehicle Maintenance Activity Monitoring Requirements
Outfall
No:
Date
Sample
Collected
50050
00556
00530
00400
Total Flow
(if applicable)
Total Rainfall
OR & Grease
(if appl-)
Non -polar
O&GffPA
(Method 1664
SGT-HEM). 9
appi.
Total
Sugpended
Solids
pH
New Motor Oil
Usage
mdddl r
MG
inches
me
1110
Units
ii 25 r
, o0,
P4 L)
3.1
0
Farm SWU-246-062310
Page I of 2

STORMWATER DISCHARGE OUTFALL (SDO)
MONITORING REPORT
Certificate of Coverage No. NCG
FACILITY NAME ,&6,' , ra0 ( { E
PERSON COLLECTING SAMPLE(S) !r
CERTIFIED LAB 0 RATO RY(S) f?f Lab #
Lab #
SAMPLES COLLECTED DURING CALENDAR YEAR: zo l q
(This monitoring report shall be received by the Division no later than 30 days
from the date the facility receives the sampling results from the laboratory.)
COUNTY
PHONE NO. f33( 1 34 % - 2.q
(SIGN,IITURE OF PERMiTTEE OR DESIGNEE)
By this signature, I certify that this report is accurate
complete to the best of my knowledge.
Part A: Vehicle Maintenance Activity Monitoring Requirements (only if, on average, more than 55 gallons per month of new motor oil is used)
Ontfall
No.
Date
Sample Collected,
maidd/yr
'Total Rainfall,
inches
New Motor Oil Usage,
Amoral average
P—VBlq
00556
00530
00400
Oil and Grease,
mg/L
Non -polar O&G/rPH
(Method 1664 SGT-HEM),
if appl.
Total Suspended Solids,
mPJL
pH,
Standard units
Benchmark
-
-
30
15
100
6.0 - 9.0
-7
N -P
rr M
7. YO
Note: If you report a sampled value in excess of the benchmark value, or outside the benchmark range for pH, you must inipletnent Tier I or Tier 2 responses in the General Permit.
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Ralei t, North Carolina 27699-1617
"I certify, under penalty of In Mat this document and all attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified pFresj�gnlfl
roperly gather and evacuate the information submitted. Based on my inquiry of Me person or persons who manage the system, or
those persons directlyb a for gathering the information, the information submitted i s, to the but of my knowledge and belief, true, accurate, and complete.
I am awn hat there nt penalties for submitting false information, including the passibility of fines and imprisonment for knowing violations."
or
(Signature o P ttce) (Date)
Form SWU-254-062310
Page I of 1

STOILM EVENT CHARACTERISTICS:
Date tit 17,51lq
Total Event Precipitation (inches): — D
Event Duration (hours): _�___ __ _ (only if applicable —sec permit.)
(if more than one storm event was sampled)
Date
Total Event Precipitation (inches):
Event Duration (hours): (only if applicable — see permit.)
Mail Original and one copy to:
Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure qualified personnel properly gather and evaluate the information submitted. Based on my Inquiry of the person
or persons who manage the s em, or those persons directly responsible for gathering the information, the Information submitted Is, to the best
of my knowledge and belief. . accurate, and complete. I am aware that there are signiFcant penalties for submitting false information,
Including thVmibility of fin and Imprisonment for knowing violations."
IZ 4
(Date)
Form SWU-246-062310
Page 2 of 2

outfau 001
Inches of Rain 0.22
Area Sq Ft Run Off Factor Ft of Rain Cubic Ft Gallons Million Gallons
Impervious Area 127000 0.9 0.0183333 2095.5 15674.34 0.01567434
Gravel 425500 0.5 0,0183333 3900.4167 29175.12 0.029175117
Total 552500
Total Flow 0.044849457
Area x runoff factor x feet of rain = cubic ft of water runoff
Cubic feet x 7.48 = gallons

AIR /•
PRODUCTS fit-.- Delegation of Authority to Non -Officer Positions
E=
The undersigned. Robert Q, Conley. in my capacity as _Vice President — Global Eny,neerin of A!r Products and
Chemicals, lnc.. pursuant to the delegations of Authority Policy, hereby delegates authority as described herein below to
the following non officer position(s):
POSITION TITLE AND COMPANY MAXIMUM VALUE
Each TgnsaCkon/COnIraG
See attached Page 2 for list of position titles NIA
❑ESMPTION OF AUTHORITY
Authority to execute permit applications. permit related submissions and documents. and routine fifings and
documents required by local• state• and federal regulatory agencies or authorities pertaining fo environmental,
health, and safety compliance for the Wilkes Barre. Gardner, Cryomachinery and Prism Membranes facilities
❑This aulhordy may be subdelegaled with the forl",ng reslrrcl,pni lot any)
Q This aulhonly may not be subde+egated.
10 lake effect when countersigned by the Corporate Secretary or any Assistant Corporate Secretary and to continue in
effect for so Fong as the designated position tille(s) remain unchanged, or until such authority shall be reused or
revoked by notice thereof by the undersigned, his or her successor in office. or the person to whom the designated
posilion(s) report.
hH Ir
Se�snlirrt / I
f" f I L r^
Countersigned by f'
!•prw, �v tie t rn:>..,�l�6t [ �rpornw SrCrrt.n v (l: to

AIR A
Pf?ODUCTS I= Delegation of Authority to Non -Officer Positions
I POSITEON TITLE + MAXIMUM VALUE
!Farh Tt angad�orvC ont rar1
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistanl Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmental SOectalist
In. _ :I.-1J....,'011. n11 J..1
NIA

www.paoalabs.com
1
December 16, 2014
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
RE: Project: Air Products
Pace Project No.: 92227543
Dear Mr. Owens:
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on December 01, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brittany Gibson for
Terri Page
[e-mail]
Project Manager
Enclosures
OF LABORATORY ANALYSIS
L-J
This report shall not be reproduced, except in full,
ithout the written consent of Pace Analytical Services, Inc..
w
Page 1 of 12

72ceAnalytical
wxwpacefabaown
r
l
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Project: Air Products
Pace Project No.: 92227543
Charlotte Certification IUs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
North Carolina Drinking Water Certification #: 37712
Eden Certification ids
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
VirginiaNELAP Certification M 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 12

alceAnalytical
www.pscawbs.cm
1
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Project: Air Products
Pace Project No.: 92227543
Sample: OUTFALL 001 Lab ID: 92227543001 Collected: 11/25/14 07:30 Received: 12/01/14 14:22 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
3.1 mg/L
2.7 1
12/02/14 14:37
HEM, oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mgJL
5.0 1
12/05/14 13:28
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Total Nitrogen
0.14 mg/L
0.12 1
12/16/14 15:52
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
ND mg/L
0.50 1
12/12/14 14:30 7727-37-9
353.2 Nitrogen, N021NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.14 mg/L
0.020 1
12/10/14 19:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/16/2014 04:43 PM without the written consent of Pace Analytical Services, Inc..
Page 3 of 12

acemaIxical
www.pat we6s.com
f
Project: Air Products
Pace Project No.: 92227543
QC Batch: EDEN116554
QC Batch Method: SM 2540D
Associated Lab Samples: 92227543001
METHOD BLANK: 1341224
Associated Lab Samples: 92227543001
Parameter Units
Total Suspended Solids mg1L
LABORATORY CONTROL SAMPLE: 1341225
Parameter Units
Total Suspended Solids mg1L
SAMPLE DUPLICATE: 1341226
Parameter Units
Total Suspended Solids mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 12102M414:36
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 252 101 90-110
92227670001 Dup
Result Result RPD Qualifiers
78.0 73.5 6
Resuhs presented on tills page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the resutt.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/16/2014 04:43 PM without the written consent of PaceAnalytical Services, Inc..
Page 4 of 12

ceAnalytical.
www.pecembs.com
I
QUALITY CONTROL DATA
Project: Air Products
Pace Project No.: 92227543
QC Batch: GCSVI19698 Analysis Method: EPA 1664E
OC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92227543001
METHOD BLANK: 1344728
Associated Lab Samples: 92227543001
Parameter
Units
Oil and Grease
mg/L
LABORATORY CONTROL SAMPLE:
1344729
Parameter
Units
Oil and Grease
mg/L
MATRIX SPIKE SAMPLE:
1344730
Parameter
Units
Oil and Grease
mg&
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 12/05/14 13:20
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 35.8 90 78-114
92228007002 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 40 34.4 86 78-114
Results presented on this page are In the un@s Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1211612014 04:43 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 12

lnoAnalytical
www.pacebb3.cam
Project: Air Products
Pace Project No.: 92227543
QC Batch: WETA121195
QC Batch Method: EPA 351.2
Associated Lab Samples: 92227543001
METHOD BLANK: 1346568
Associated Lab Samples: 92227543001
Parameter Units
Nitrogen, Kjeldahl, Total mg1L
LABORATORY CONTROL SAMPLE: 1346569
Parameter Units
Nitrogen, Kjeldahl, Total mglL
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 351.2
Analysis Description: 351.2 TKN
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.50 12/12/1414:25
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
10 10.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1346570 1346571
MS MSD
92228319001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg1L 1360 1000 1000 2340 1990 98 63 90-110 16 M6,R1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1346572 1346573
MS MSD
92227544011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mglL 11.1 10 10 22.0 22.7 109 116 90-110 3 M1
Resuhs presented on this page are In the units indicated by the "Units" column except where en alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
Date: 12116/2014 04:43 PM without the written consent of Pace Analytical Services, Inc,.
Page 6 of 12

�Ice Analytical
www.pacelaha.com
Project: Air Products
Pace Project No.: 92227543
QC Batch: WETA121208
QC Batch Method: EPA 353.2
Associated Lab Samples: 92227543001
METHOD BLANK: 1347203
Associated Lab Samples: 92227543001
Parameter Units
Nitrogen, NO2 plus NO3 mg1L
LABORATORY CONTROL SAMPLE: 1347204
Parameter Units
Nitrogen, NO2 plus NO3 mg/L
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.020 12/1011419:13
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1347205 1347206
MS MSD
92227541002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 68.4 2.5 2.5 70.3 70.0 77 65 75-125 0 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1347207 1347208
MS MSD
92227984001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.057 2.5 2.5 2.6 2.6 101 100 75-125 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in fulti,
Date: 12/16/2014 04:43 PM without the written consent of Pace Analytical Services, Inc,.
Page 7 of 12

Pace Analytical Services, Inc.
s 265 East Meadow Road - Suite A
ceMalytical Eden. NC 27288
wxwpeae136s.0om [phone]
r
I
QUALIFIERS
Project: Air Products
Pace Project No.: 92227543
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/16/2014 04:43 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 12

aceAnalyhcalo
www.pacelBu =n
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Air Products
92227543
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method Batch
92227543001
OUTFALL 001
SM 2540D
EDEN116564
92227643001
OUTFALL 001
EPA 1664E
GCSVI19698
92227543001
OUTFALL 001
TKN+NO3+NO2
WET134799
Calculation
92227643001
OUTFALL 001
EPA 351.2
WETA121195
92227543001
OUTFALL 001
EPA 353.2
WETA121208
Date: 1211612014 04:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 12

aceAnalytical o
CHAIN -OF -CUSTODY 1 Analytical Request' Document
The Chain -at -Custody fs a LEGAL DOCUMENT. All relevant fields must be completed accurately.
..-.P..........:,:
Page: of
Section A Section B Section C
Required Client Information: Required Project Information: Invoice Information:
Company: Report To: Attenlloe:
O
Add
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Copy
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' -
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Pars ProteProtecte
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Manager:
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Project Number:
Pace Profiler:
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Section D Matrix Codes`
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Required Client information MATRIX !CODE
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U
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Waste Water WW
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DATE
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SAMPLER NAME'AND SIGNATURE
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PRINT Name of SAMPLER. �(���yyti,,L f`
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SIGNATURE of SAMPLER:
DMAMIro�igned / , !
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*Important Note; By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any'Involces not paid Wthdn 30 days. - F-ALL-0-020rev.07, 15-May-2007

/ PaceAnal ical'
www.pacalabs.com
Section A
Rnnulrad Client InfmmnnKnn-
;Section B
Raouired Protect Information:
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody Is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
I—i Infnrmntlnn'
.. Page: a?
Company: -
Report To:
Attention:
z I J LJ . I
Address:
7
Copy To:
an
Company Name:-
- ,r-
REGULi4T012Y
�Tt<�14; 2 ���O '
Address:
j— .; NPDES .: r' GROUND WATER r, . DRINKING WATER
� usr RCRp; .. . r OTHER
Email To: -
Purchase Order No.:
-
Quote Pam
Rom:
•
Phone:
'
Fax.
Project Name:
Pace Project.
!Site Location
2. Z �f
.
Manager.
;
Requested Due DateITAT:
Project Number:
Pace. PileSTATE:
Requested
Analysis
Filt
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Sactlon D Matrix Codes
Required Client lnforinadon MATRIX' I CODE
3
CO€.LECTEp -
Preservatives
. Drinking Water DW
'WT
O
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Waste water WW
U
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compos",
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w
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Sample IDs MUST BE UNIQUE Tissue TS
Other OT
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DATE:
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;-'' 'ACCEPTED BY! AFFILIATION
DATE
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SAMPLE CONDITIONS
Of PC15
- ... .: . _
SAMPLER N411AE AND SIGNATURE
m PRINT Name of SAMPLER.
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SIGNATURE of SAMPLER: 'DATE Signed
iMMID DlYY : tZ / /
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. ' N 'important Note: 4 signing this forth you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% par month for any Invoices not paid wkthin 30 days.._ FALL-Q-020rov.07, 15-May-2007

DoCument IVarne: SamplB; oneli fors; Upon°
b6wa ent Revised: Maroh 13, 2013 ,
At1�1 t(G1�.
Recei t SGUR 3.:
: _P e 1 of:2
`'":
Document No.:
lssuJng AuthoKes: '
P-DN-CS-OOS=rev aS :':
'; Pace Eden Quati Qice
C[lent -Name::' AR l' .
More Resetvad ❑ 46tersA116 ❑ Asheville Ed®n ❑ Ra]aigh
Courier (cede): Fed Ex .". -.UPS - USPS Client. Commercial )mac Other
Custody $eal `on CoaicdBok`Pre�ent:. ❑yee ❑ no Seals Intact ❑yes ❑ rio
Pac<dng Mateilal:. [bbfe Wrap, ❑Bubble Bao ❑ None'i
Other
Thermometer Used [R Gttn F`AOtl7 Tyjie of lc�� f3[ue f l�iohe /samples an �oe;,cooGn pkvoess has begun :
n r „+ r 5.
Temp Corle�on Fadak- Add
} <,
Car[edod Choler Temp:: 6, G �;ofaglcW TWW61s Mien.- Yes No .WA ' �d �o�f pet son eii�lning'
cnnk0w.
Temp•should be etiove freeing to 6'G. ' - Gommen
Chain of Present ldYss ONa C7N1A is -
Chaln.of Custo1{led Oetr fdYos' C1Na: ©WA 2:
Ghaln of Cu 13efin fished . -: t ftis Md -17WA 7
Sam erNarn6 & Sl re bn:COC: Vi6 taw QWA 4:
Sam 1esArFNedwithfn#ioid Ttttie:;:; Wes, OADI: ❑wn 6.
Short Hold Time Ana ' si§/2hr :�3Yes QiNo. = f7wA 6:"
Rush Turn Around Tung Rb' nested, . C7Y.0 too `I~IwA 7.
Correct QOlitalg9r8 9d :0.yes Oi4o • OwA 9::
-Pace Containers Efsed: ` : Yea: ONa- CIWA =
Containers Intact: 171ves-lrlNo'.,.[:]WA.10: _
:.
Entered volume received for Dlssolved tests .. OYes- l7No: QIN1A 11.
Sample Labels match oQC:: 2o ,QW .,OWA 12.. -- -
AD oonfdners needle nraiion� have been checked.
9 VfYes i7No ONZA 13:
All wtalnsrs needing preservation are found to'be to F<JYaa []Na OwA
oomprranceWOEPA rec=' enddon
.. ..T. -- _ .. ..... .. .. -
o VOA, oot€tomr, T(o, w1 DRO LIYe3. PNo . _ tnutal when cfta '
Samples checked for dechlognafron: ' C1v4 , f2. NQ ''Orin 14
iieadspaoe 1n VOA Vials'6UMt , :. [7Yes'ONo :I;INlA 15 '
Trip B"Present: E)Yea :ONO NIA 1$:
Trip Blank Custody Seas Preset C}Yes ENa^` dt�rq
Paw TrIp Wank Lot 9'f Odiafi;is6dYi _
Page 12 of 12

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. htM://h2o.enr.statr,nc.us/su/Fon-ns ocurnents.htm#miser rms
Permit No.: �VIG�l�f t3 /�1 b/, / / or Certificate of Coverage No.: N Cj01_J _j 1 I 1
Facility Name: RGlc15y//1e Ate/
County: ram" 1+ a r,n Phone No. C3 (1) 16 17- -
inspector: _ GeL 2We-P t f
Date of Inspection:
Time of Inspection: 673b — —,-•-- —,__,. _
Total Event Precipitation (inches): D • Z 2-
_
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
4 A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has 3
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. —
By this signature, I certify that this report is accurate and complete to the pot of my knowledge:
(Signature of Pierminee or Designee)
1. Outfall Description:
Outfall No. L_ Structure (pipe, ditch, etc.) lae
Receiving Stream: _ ^rrn-�.�Ir—rdY► r^i�e►�_ - -
Describe the industrial activities that occur within the outfatl drainage area: Ar
2. Color: Describe the color of the dlschar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: /7� r Arzs��
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): Sek anl2k---
Page 1 of 2
SWU-242-112608

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 0 3 4- 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solid
s and 5 is extremely muddy:.
1 3 4 . 5
7. Is there any foam in the stormwater discharge? Yes 6Nq/
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfali? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Alor?e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosiun/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S WU-242.112W

Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance orefilling out this form, please visit: http://h2o.enr state,nc.uslsu/Form-4 Doe umentG,htm#mi5crorms
Permit No.: NICJQI olv /U I U l�bl or Certificate of Coverage No.: JGGI 1 1 1 I 1 I
Facility Name:
County: jed c + "Sk Phone No. ge- Y
Inspector: 0),V-6 t '
Date of Inspection: 1 /4alY
Time of inspection: 6,�z30
Total Event Precipitation (inches):
Was this a Representative Storm Event? (See information below) ® Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must he performed during a representative
storm event (requirements vary).
A "Representative Sturm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no vrecivitatilM. #
By this signature, I certify that this report is accurate and complete to the best of my
(Signature of Permittee
1. Outfall Description:
Outfall No. _— Structure (pipe, ditch, etc.)
Receiving Stream: r vu /c-s'o'- e-c
Describe the industrial activities that occur within the outfall drainage area: t/ k. cfp cu'Tig..
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: /f b,-ww ,
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): _ IL Ode _ -- —
Page t of 2
SWU-242-112608

4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
0 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
0 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes Cp
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfail? Yes No
10. Other Obvious indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112609

Reidsville NC Stormwater Sampling Checklist
Completed by:
Item description
L.-Y-D
1. Sample during representative* storm event at Outfall #1
1>0.1" rainfall, sampled within 30 minutes of start of event, and no other rainfall event >0.1" in
previous 72 hours
2. Spring sample between January 1"-June 30t or Fall sample between
L� July 1" and December 31"
t~ 3. At least 60 days has passed since last sample taken
tau 4. Sample refrigerated until lab pick-up
S. Calculate rain flow and print spreadsheet
6. Fill out SDO qualitative monitoring report for BOTH outfall 1 & 2.
Report any deviations to Site Manager
* NC State form SWU-242-XXXXXX
LTU 7. Fill out form 82 and C2, site inspection and summary
8. Fill out SDO monitoring report (DO NOT SIGN)
a NC State form SWU-246-XXXXXX rwe 1
1 9. Fill out Storm event characteristics form (DO NOT SIGN)
i lvL dale Torm swu-<<+o-AAAAAA page z
10. After analysis is complete, check results against following benchmark
values. 'Report any deviations to the site manager
Benchmark Result
Total Nitrogen: 30 mg/L to -A - n.ky mg/L
pH: 6-9 su 7. U0 su
Oil and Grease: 15 mg/L W D mg/L
Total Suspended Solids: 100 mg/L 3,1 mg/L
11. Compile all documents listed above, together with analysis results,
scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12. Environmental Specialist signs form SWU-246-XXXXXX and sends to
NC State within 30 days of analysis results. Also places copy of all
communications with NC DENR in Reidsville share site

CALIBRATION AND SAMPLE ANALYSIS PROCEDURE
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
pH analysis must be performed within 30 minutes of sample collection.
1. Turn on pH meter
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
4. Rinse pH probe with deionized water and blot dry with a clean, soft cloth or tissue.
5. Place both the temperature probe and the pH probe in 7.01 pH buffer solution.
6. Shake the pH probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7. Record temperature and pH reading.
8. Press and hold the CAL button until "CAL" flashes on the screen.
9. Calibration will take approximately 30 seconds. When complete, record final pH reading.
10. Remove probes from 7.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
11. Repeat steps 5 through 9 using the 4.01 pH buffer solution
12. Remove probes from 4.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
13. Repeat steps 5 through 9 using the 10.01 pH buffer solution
14. Remove probes from 10.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
15. Insert both probes in the storm water sample, and stir the sample gently to ensure homogeneity
and minimize carbon dioxide entrainment.
16. Wait one minute for reading to stabilize.
17. Record temperature and pH reading.
18. Remove probes and rinse pH probe in deionized water. Blot dry with a clean, soft cloth or
tissue.
19. Dampen the inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace cap on probe.
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster•10 pH/mV/Temperature Meter Serial Number 022055
pH 7.01 Buffer pH 4.01 Buffer
pH 10.01 Buffer
Storm Sample
Date
Temp Initial
Final Temp Initial Final
Temp Initial Final
Temp pH
�r(zc:,liy
S.C. 6.90
7.�/ S5, 5 y
L, 1-02- I/O,c:r
55, Z 7Yb
Air Products Internal Use Only

I Facility: Reldsvllle NC
WORKSHEET B2 Rev.: B
INVENTORY OF SIGNIFICANT MATERIALS Date: 06126MI
{
INSTRUCTIONS Page 1 of 1
1. Make a copy of this worksheet to conduct an inspection of the potential pollutant sources listed In this
worksheet. Documented Inspections must be conducted at the frequency specified in Section 8.1.4
of this Plan.
2. Use the following criteria when conducting the inspection:
• Observe piping, hoses, valves, pumps and connections for leaks, excessive wear or potential
discharges.
• Observe process equipment, bulk storage containers, fuel islands, tractor/trailer parking areas,
coaling systems and materials storage areas for signs of a discharge.
• Observe drums and containers of hazardous wastes for signs of discharge, deterioration or
bulging due to corrosion or other factors. Drums or containers should be tightly sealed at all
times except when withdrawing or adding materials. Drums stored in a horizontal position should
have drip pans beneath dispensing areas. Replace leaking or damaged drums with good drums
and dispose of in a proper manner.
• Observe storm water and waste water management devices or structures such as oll/water
separators or storm water retention basins to ensure proper operation.
• Observe transformers for signs of discharge or an integrity problem that may lead to a discharge.
• Observe containment dikes, curbing, valves and blocked floor drains for discharges and structural
Integrity. Ensure containment area drainage valves are in the closed position and secure.
• Observe aboveground storage containers, tank supports, foundations and valves for signs of
corrosion, structural fatigue, leakage, general integrity and accumulation of product inside the
secondary containment areas.
• Observe spill kits to ensure that sufficient inventory is in stock.
3. Take appropriate corrective action for any deficiencies noted during the inspection_ In particular.
• Replace or repair any equipment for which an integrity problem is observed or suspected.
• Clean up all observed discharges promptly and report discharges to management.
• Restock facility and vehicle spill kits as needed. Ensure facility always has spare spill clean up
materials on hand.

Facility:
Reidsville NC
WORKSHEET B2
Inspected by:
Le,
Rev_:
6
INVENTORY OF SIGNIFICANT MATERIALS
Date:
it 12��/
Date:
06/28/11
Pae1ot
4
Rate of Flow, Maximum
Advanced Best Management
Location on Map
Potential Pollutant Sources
Material and Quantity
Amount That Could
Practices (Baseline BMPs not
Inspection Results
Discharge, Predicted
inciuded)
Direction 01 Flow
Underground Storage
Diesel Fuel
Seepage through
BMP 8.3.1 - Truck
Tanks
(2 @ 10,000 gal)
ground. 10,000 gal
Fuel/Heating Oil
1
Underground Storage Tank
S stem
Underground Storage
No. 2 Heating Oil
Seepage through
BMP 8.3.2 — Heating Oil
Tank
(2,500 gal)
ground 2, 500 gal
UST
2
Aboveground Storage
Used Oil (375 gal)
West, Catch Basin
BMP 8.3.5.1-- Shop
3
Tank
#10, 375 gal
Fabricated Tanks
Truck Fuel Dock
Motor Fuels (small
Oil/Water Separator
BMP 8.3.3 - Oily Water
1
fugitive amounts)
5 gal
Control System
4k-
Truck Wash Pad
Motor Oils and
Oil/Water Separator
BMP 8.3.3 - Oily Water
Motor Fuels (small
5 gal
Control System
4
fugitive amounts)
D
01.16 Main Air
Lube Oil (300 gal)
Oil/Water Separator
BMP 8.3.3 - Oily Water
Compressor
300 gal
Control System
d�
5
01.30 Nitrogen
Lube Oil (300 gal)
Oil/Water Separator
BMP 8.3.3 - Oily Water
Make -Up
300 gal
Control System
Ole-
6
Compressor

Facility:
Reidsville NC
WORK5HEET B2
inspected tay:f
Rev.:
6
INVENTORY OF SIGNIFICANT MATERIALS
Date:
/l
Date:
608/11
Page 2 of
4
Rate of Flow, Maximum
Advanced Best Management
Location on Map
Potential Pollutant Sources
Material and Quantity
Amount That Could
Practices (Baseline BMPs not
Inspection Results
Discharge, Predicted
included)
Direction of Flow
01.46 Recycle
Lube Oil (1,000
Oil/Water Separator
BMP 8.3.3 - Oily Water
7
Compressor
gal)
1000 gal
Control System
1 CP-K I II Main Air
Lube Oil (665 gal)
Oil/Water Separator
BMP 8.3.3 - Oily Water
21
Compressor
665 gal
Control System
vac
ICP-K301/321
Lube Oil (565 gal)
Oil/Water Separator
BMP 8.3.3 - Oily Water
22
Recycle Compressor
565 gal
Control System
b�
ICS-T361
Lube Oil (250 gal)
West, Catch Basin
23
Compander
#9.250 gal
Oil/Water Separator
Used Oil (2,500
Seepage through
BMP 8.3.3 - Oily Water
8
gal)
ground. 2,500 gal
Control System
b
01.14A Compander
Lube Oil (450 gal)
West, Catch Basin
9
Lube Oil Console
#9.450 gal
UDC
12.42 Instrument Air
Lube Oil (1.5 gal)
Southeast, Catch
10
Compressor Sump
Basin #9. 1.5 gal
Dim

Facility:
Reidsville NC
WORKSHEET B2
Inspected by:
bcw Ow NS
Rev_:
B
INVENTORY OF SIGNIFICANT MATERIALS
Date:
f
Date:
OIU28/11
Pa e3of
4
Rate of Flow, Maadmum
Advanced Best Management
Location on Map
Potential Pollutant Sources
Material and Quanffty
Amount That Could
Practices (Baseline gMPs not
Inspection Resuits
Discharge, Predicted
Included)
Direction of Flow
14.10 Gear Reducers
Lube Oil (3 @
Southwest, Catch
l l
3gal)
Basin Q. 3 gal
vim
Lube Oil Storage
Lube Oil (2 drums
South, Catch Basin
BMP 8.2.12 - Drum and
12
max @ 55 gal)
#11.55 gal
Container Storage Areas
Transformers
Mineral Oil L_ �,
Southwest, Catch
BMP 8.2.8 - Transformers
14
gal)
Basin #8. 5 gal
Truck Garage
Oils and
East, Catch Basins
BMP 8.2.5 - Vehicle
15
Lubricants, Parts
#13 & #14.5 gal
Maintenance and Repair
Washer
Truck Scale
Motor Oils and
To Scale Drain. 5
16
Motor Fuels (small
gal
fugitive amounts)
Tire and Drum
BUT 8.2.14 - Drum and
17
Storage Building
Container Storage Area
Water Treatment
Sulfuric Acid (105
To Floor Drain. 5
BMP 8.2.11- Chlorine
18
Area (Room,
gal max)
gal
Cylinders
Building)
Chlorine (450 lb
BMP 8.3.4 - Water Treatment
max)
Building

Facility:
Reidsvllle NC
WORKSHEET B2
Inspected by:
I t'L! Un�LS
Rev_:
6
INVENTORY OF SIGNIFICANT MATERIALS
Date:
/
Gate.
06128/11
Page 4 of
4
Hate of Flow, Maximum
Advanced Best Management
Location an Map
Potential Pollutant Sources
Material and nuanttty
Amount That Could
Prackes (Baseline SMPs not
Inspection Results
Discharge, Predlcted
Included)
Direction of Flow
LIN/LOX/L.AR
Motor Oils and
Southwest, Catch
19
Trailer Loading
Motor Fuels (small
Basin #12. 5 gal
ok
fugitive amounts)
LH2 Trailer Parking
Motor Oils and
Catch Basin # 15.5
20
Motor Fuels (small
fugitive
gal
OK
amounts)
LOX/LIN Trailer
Motor Oils and
North, Catch Basin
20
Parking
Motor Fuels (small
#14, 5 gal
6kk
fugitive amounts)
Urea solution
32% Urea Solution
700 gallons Oil
21
Vehicle Maintenance
Water Separator
6)12/_
Shop

Facility: Reidsville NC
WORKSHEET CZ Rev,: s
COMPREHENSIVE COMPLIANCE EVALUATION Date: 06128111
REPORT Page 1 of 3
Istructions:
1. Using a copy of Worksheet B2, conduct a Visual Site Inspection of potential pollution sources
Hated in Worksheet B2. When making the inspection look for evidence of the following:
• Evidence of pollutants entering the storm water drainage system
• Best Management Practices are adequate and properly implemented
• Storm water structural features and sediment controls are operating properly
• Spill response equipment is in proper working condition.
2. Summarize the results of the Inspection on Worksheet C2. Attach Worksheet 82 to Worksheet
C2 and Insert in Appendix C of this Plan for at least three (3) years from the date of the
Inspection.
3. Implement any corrective actions Identified In Worksheet CZ Based on the results of the
annual Inspection, necessary revisions to pollution prevention measures, controls, and the
SWPP Plan shall be Initiated within two (2) weeks of such Inspection. Revisions shall be
completed within 12 weeks of the Inspection.
4. The SWPP Plan shall be reviewed and the following sections updated, where necessary:
• Changes to the Pollution Prevention Team member roster (Worksheet B1)
• The inventory of significant materials and BMPs (Worksheet B2, Site and Drainage Map)
• The history of significant spills and leaks (Worksheet B3)
• For facilities subject "to special storm water requirements for SARA 313 water priority chemicals
(Section 10.5), the Plan shall be reviewed and certified by a Professional Engineer every three (3)
years.

€ Facility: Reidsville NC
WORKSHEET C2 Rev.: 6
COMPREHENSIVE COMPLIANCE EVALUATION Date: 06/28/11
REPORT Page 2 of 3
1. Scope of Visual Inspection
Date of Visual Inspection. ( 2S I
Inspection Conducted by:
2. Major Observations
As a result of this inspection, the following major observations were made (include written
documentation of the visual inspections for all outlalls):

Facility: Reidsville NC
WORKSHEET C2 Rev.: e
COMPREHENSIVE_ COMPLIANCE EVALUATION Date: OW28111
REPORT Page 3 of 3
3. Action Taken
The following actions were taken as a result of the major observations. This includes making
appropriate revisions to the SWPP Plan. These actions must begin within two (2) weeks of the
inspection. The action plan must allow for completion of the changes within 12 weeks.
N
4. Incidents of Non -Compliance
After reviewing the SWPP Plan and storm water permit conditions (Section 10), all incidents of non-
compliance are identified below:
Certification;
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision In accordance
with a system designed to assure that qualified personnel property gather and evaluate the Information submitted. Based on my
inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penaides for submitting false information, Including the possibility of fine and imprisonment for knowing violations.
Furthermore, when this report does not identify any incidents of non-compliance, l certify that the facility Is In compliance with the
storm water Pollution prevention plan SWPP and the storm walerpemtiL
A. Name (Type or Print)
B. Title
C. Signature
D. Date Signed

Pii�DUCTS �
Air Products and Chemicals, Inc.
357 Marian Ave
Tamaqua, PA 18252
Telephone [phone]
December 29, 2014
Division of Water Quality
Attn Central Files
1617 Mail Service Center
Raleigh, NC 27600-1617
RE: NCSS000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
RECEIVED
JAN a 6 2015
CENTRAL FILES
DWR SECTION
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report for the Air
Products and Chemicals, Inc. Reidsville, NC Facility.
If you have any questions regaring this submission or require additional information, please feel free to
contact me directly at 570-4674399.
Si erely,
Josep Sebia
Environmental Specialist
Air Products and Chemicals, Inc.
Electronic Materials Organization
Tamaqua PA 18252
CERTIFIED MAIL: 7010 0780 0000 8680 7239

AIR
PRODUCTS
Air Products and Chemicals, Inc.
357 Marian Ave
Tamaqua, PA 18252
Telephone [phone]
January 13, 2014
Division of Water Quality
Stormwater Division
585 Waughtown Street
Winston-Salem NC 27107
RE: NCS000030 Annual DMR Summary
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
RECEIVED
N.C. Dept of ENR
s ° JAN Z i ZW
REC-JONAL {OFFF C E
Enclosed please find Stormwater Discharge Monitoring Report Annual Summary for the Air Products and
Chemicals, Inc. Reidsville, NC Facility for calendar year 2013.
If you have any questions regaring this submission or require additional information, please feel free to
contact me directly at 570-467-4399.
Sincerely,
Joseph Sebia
Environmental Specialist
Air Products and Chemicals, Inc.
Electronic Materials Organization
Tamaqua PA 18252
CERTIFIED MAIL: 7013 1090 0001 8611 2552

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year z n 13
Individual NPDES Permit No. NCS©®©® 3❑ O❑ or
Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑
This monitoring report summary of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: A ,(l PAre3oC+ fV
Ct)C M.(, l's L (Vc (ZcZ05QN zt C-
County: R oc is "VC %4et�
Phone Number: (A3 �) 3 4 q - Z 9 4 L Total no. of SDOs monitored
Outfall No. i
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ® No ❑
Total
Rainfall,
inches
Parameter, units
P
N EM
Oy F
--rotm -.
rV 0mc,('r-mil
•T SS. .
tJa-L +
No3
Benchmark
N/A
G cl Sj
1 5 (L
30-4L
Date Sample
Collected,
mmlddlyy
oS C* o.
b.zv
(0,3
f110
ICI
0 V7
0,qC)
Z.z 1 is
0.3
(0 '9
N P
I • 4
0 tv
p - 33
SW U-264-Generic-i 3Dec2012

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the passibility of finks and imprisonment for knowing violations."
Signature _
Date 1 115
For questions, contact your local Regional Office:
DWO Regional Office Contact Information:
ASHEVILLE REGIONAL OFFICE
FAYETTEVILLE REGIONAL OFFICE
MOORFSVILLE REGIONAL OFFICE
225 Green Street
610 East Center Avenue/Suite 301
2090 US Highway 70
Swannanoa, NC 28778
Systel Building Suite 714
Mooresville, NC 28115
[phone]
Fayetteville, NC 28301-5043
[phone]
[phone]
RALEIGH REGIONAL OFFICE
LWASHINGTON REGIONAL OFFICE
WILMINGTON REGIONAL OFFICE
3800 Barrett Drive
943 Washington Square Mall
I
127 Cardinal Drive Extension
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
[phone]
[phone]
[phone]
WINSTON-SALEM.REGIONAL.. OFFICE
CENTRAL OFFICE
1617 Mail Service Center
Raleigh, NC 27699-1617
To preserve, protect
and enhanm
585 Waughtown Street
Winston-Salem, NC 27107
[phone]
[phone]
Norih Carolina's water..."
SW U-264-Generic-13Dec2012

AIR �•
PRODUCTS I: Delegation of Authority to Non -Officer Positions
F K.- T11.hr ,nnn Nu
The undersigned, Robert D. Conley, in my capacity as Vice President — Global Eagjneerinq of Air Produ is and
Chemicals, Inc., pursuant to the Delegations of Authority Policy, hereby delegates authority as described herein below to
the following non -officer posilion(s):
POSITION TITLE AND COMPANY MAXIMUM VALUE
Each Tran5achonlContracl
See attached Page 2 for list of position titles N/A
DESCRIPTION OF AUTHORITY
Authority to execute permit applications, permit related submissions and documents, and routine filings and
documents required by local, slate, and federal regulatory agencies or authorities pertaining to environmental,
health, and safety compliance for the Wilkes Barre, Gardner, Cryomachinery and Prism Membranes facilities.
❑This aulrlonty may be subdelegated with the lollowing resirlclionS (it any)
OThIs authority may not be subdelegaied.
to take effect when countersigned by the Corporate Secretary or any Assistant Corporate Secretary and to continue in
effect for so long as the designated position title(s) remain unchanged, or until such authority shall be revised or
revoked by notice thereof by the undersigned, his or her successor in office, or the person to whom the designated
position(s) report.
SltmnlueY � nnlr
I�
Countersigned by: itr' c��
('urpo.:ltr Fe rq'i ;nt�4t (nrporaiw ",etrrtary" n;tte
I—p'. Im-1•la._' M:'.r -,--A -A$ Jot

AIR A
PWL)UCTs * — . Delegation of Authority to Non -Officer Positions
POSITION TITLE
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmental Soecialist
H, ::tin., IJ.r i_1 2007. 1+11 Jai
lfnpbLal�un N
MAXIMUM VALUE
N/A

Kt UEIVED
N.C.Dept. of ENR
JUL 2 7 2015
F� _.
Air Products and Chemicals, Inc.
7201 Hamilton Boulevard
Allentown, PA 18195.1501
Telephone [phone]
Via Certified Mail 9414 7266 9904 2954 5257 19
20 July 2015
NC DENR Division of Water Resources
450 W Hanes Mill Rd. Ste. 300
Winston-Salem, INC 27105
RE: NC5000030 Stormwater Permit Monitoring
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
Winston-Salem
Regional Office
Enclosed please find one original and one copy of the Stormwater Discharge Monitoring Report
for the Air Products and Chemicals, Inc. Reidsville, NC Facility.
Please feel free to contact me with any questions or require additional information. I can be
reached at [phone] or creitzib(@airproducts.com.
Sincerely, t
Sincerely,
B r i z
Sr. Pr. En roaental Engineer
c. Coray Mitchell — Air Products
1

M]tMWATER DISCHARGE OUPFALL (SDD)
MONTTORING REPORT
Permit Number: NCS. 900�O or SAb9qFS COLLECPEDDURING CAI EMMRYLAH: ZO/�
Certificate of Coverage Number. NCG ('ibis monitoring repm t dmU be reedu d by the Divhdon no later titan 30 days from
dm date the fadI ty r ecelm the sampilag results L+tmt the lab mdoiy.)
FAcELMNAhM APB ofv�ct� A0e&,I1.6�,
PERSON COLLECTING SAMPLE(S) 19as 4 f #111111111111'
CERnFJED LABORATORY V �[,ab ..
Lab p "E=Z=
o ffi
By that Q t b aCCWz e
completkwnwle8ge.
Part A: Specific Monitoringequireournts
Does this facility perform Vehicle Maintenance Activities using mom then SS gallons of new motor oil per month?Ryes --no
(if yes, complete Pan B)
PaN S: Vehlr]e Maintennnm Aetivity MmIMAnv Rmmntrp~%Im
Otttfeil
No.
Date
Sample :
Coftcted
59WO
0 ...
OQ43Q
00400
Total Flow
(ifappliesbte)
i,
ToUd Rs&"
Ofl & Grime
(ftappL)
Num jpda r.
O&(xlllM,
(Me 9"
SGT-FM, It
SOL
Total
5 I
Sonde '
PH
Nevr A !"V oll
UStom
and r
MG
hU*M
EVA
Uvft
Z7 l
S4 9 4
Q Z
/• 4
`i•
Farm 5W[A7Ab OM10
Page I of 2

i
Certificate of Coverage No. NCG
STORMWATER DISCHARGE OUTFA11(SDO)
MONITORING aiEi?'ORT
IFAciurY NAME
PERSON COLLECTII1iG SANIFLE(S) � •�"' t
vw+rX
C3ERTI>fW LABORATORY(S)Aef ns to $
Lab #
SAMI'LW COLLECTED DURING CAIMNDAR YFARt ZOlS
('1'bia moaitorbtg report steal! be rwdved by the Division no later titan 30 days
from tie date the fact ity rwelv�eQeMe samp!results from the labatatory.)
CO
PHONE N G l z'➢�2
(SOMTURE OF PERNWI M OR DERGNM .
s By this d aatare, I that this report is accurate
complete to the best of nq knowledge.
Part A. Vehicle Maintenance Activity Monitoring Requirements (ordy if, on average, mere than 55 galim per mouth of new motor o0 is used)
Outisi!
No..
Date
Ssmpie CuffiwWd,
moldd/yr
Total R-h-
inches
New bintar 0fl Usage,
Aamita#'ate
00556 _u
00539
09M
DD and Gam;
u�ll:
Nuojnhtr0&&gTiq
I
if e
TOM Saflft
"V&
pH,
Sbutdad unbs
Benehmark,
30.,
in
6A- 9.0
tZ 7i5 ?
o_zs
MD
7_6
yam.
Nate: If you report a sampled value in excess of the bemburmi. valve, or outside the benchmark range far pH, you must implam ut Tier 1 ar Tier 2 responses in the Gaaeral ParndL
Mail OrWinal and one ropy to:
Division of Water Quality _
Attn: Central Files
1617 Mail Service Center
Ral_aigb, Ngth Caroline 27699-1617
r
"I certify, under penalty of law, that this document and aU attachments were prepared undermy direction or mgxrvlalon in accosdanca with a system designed to
assure that guailfied personnel properly gather and evaluate the hriarmation subu tb& Based on my htquiEy of the parson or persons who manage the q3tC1016 or
thane persons directly responsible for gathering the information, the Wor®fIon submitted is, to the beat of my knmdedge and belie!; trace, accurate, and. ci m fete.
I am aware that thew app4gntdcaut pdnaldes for submitting !blue Information, bt&dhrg the pass[bility of Buss and imprisonment for !mowing violations."
(Sigua of Permit E (Date
k i
Page I of I
F

STORM EVENT CHARACTERISTICS: 3
Date j Z if
Total Predplb" (Inches): 61 aS
Event flotation (hour's): I_ (a* if applicable — sec permit:)
(f more than one storm event was sampied)
Date
Told Event Precipitation (inches):
Mag Orlgtnal and one dopy to:
Melon of Water Quality
Ann: C.antml Flies
1617 Mag Service
Raleigh, North Carolina 27699-1617
Event Duration (hours): (only if applicable — see perinit.)
r
"I rerdo, under penalty of law, that this document and all atbacluawts wen prepared node= q direr or sapervfsian l® aerordenee with a .
system designed to sem that 4aali W pawnuel prWe * pthcr and evabno tbeWbrnmtlon eubsclied-' Based on nwmgntry of the person
or Persons who manage the syst=4 or than pe:sana dire* respoaslhie tar galb the Whnwtlam, the Wm=W subm Wed 1% to the lust
of my knowledge and belW, true, awe, and complete. I am aware that there are sigatHc®t peoaltles for sa>anittiag false bftrmstlon,
7
77=
for knowing violations."
(S' lure orper ttee)/ I (Da7-U te)
Fmm SW[7-246-OMIO
Pap 2 cf2

Outfall001
Inch of Rain
025
Area Sq Et
Run Off Factor Ft of Rain Cubic Ft Gallons
Million Gallons_,
Impervious Area
127000
0.9 0.0208333 2381.25' 17811.75
0,01781-175
Gravel
425500
0.5 0.0208333 4432.2917 33153.54
0.033153542
Total
552500
Total Flow
0.050965292
Area x runoff factor x feet of rain = cubic ft of water runoff
Cublc feet x 7.48 = gallons

A!R 4
PRODUCT'S — Delegation of Authority to Non -Officer Positions
G
The undersigned. Robert O. Conley, in my capacity as Vice President - Global Ert9meerin9 of Air Prodlu(:i5 and
Chemicals Inc., pursuant to the Delegations of Authority Policy, hereby delegates authority as described herein below to
the follomrig non -officer position(s):
POSITION TITLE ANO COMPANY MALximUM VALUE
Eacn Transaction/Caniracl
r.tilchdPage2 for list of position titles NIA
DESCRIPTION OF AUTHORITY
Authority to execute permit applications, permit related submissions and documents. and routine flings and
documents required by local, state, and federal regulatory agencies or authorities pertaining to environmental,
health, and safety compliance for the Wilkes Barre, Gardner, Cryomachinery and Prism Membranes faafihes
❑Tn,s aulhorvy may be SUMetegaled wtlh the fpllow,rg restndwns (d any)
0This tulhonfy may nol be subdelegaled.
to lake effect when counlersigned by the Corporate Secretary or any Assistant Corporate Secretary and 10 continue in
effect for so tong as the designated position tflle(s) remain unchanged, or until such authority shall be revisers or
revoked by notice thereof by the undersigned, his or her successor In office, or the person to whom the designated
position(s) report.
1 $r�flnlurc nh lr
Countersigned by'
l �nryu�.iv S.• lrnid•.r+l�6t[nrpar:r fr tirrrrl.rr r R,rl.•

AM /.
►NPODUCTS L= Delegation of Authority to Non -Officer Positions
7 POSITION TITLE { MAXIMUPA VALUE
I! !Each TfensacljorvConlraCI
Operations Manager
Line Manager
Site Manager
Assistant Site Manager
Site Supervisor
Plant Manager
Assistant Plant Manager
Plant Superintendent
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Senior Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmental Soectalist
Inca: tpn_�.}.n �_brtr �. n.ireen�rr��li J..�
WA

ceAn*fcal
i e�rw°°m
i
i
July 13, 2015
Mr. Levi Owens
Air Products
225 Equity Road
Reidsville, NC 27320
Pace Analytical Servlcas, I=
205 East Meadow Read - SuMsA
Edert, NC 27203
(33Bj8234M
RE: Project: WW TESTING
Pace Project No.: 92256414
Dear Mr. Owens:
Enclosed are the analytical results for sample(s) received by the laboratory on June 29, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless.
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
`&dta►j- of.. Cj
Brittany Gibson for
Terri Page
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This repon shall oct be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.,
Page i of 11

q
Pecs Anetyticai SoMooe, Ina
CZt�ril`II�i[,a1 S
205 East Meadow Road - SuftA
Eden, NC27288
w
(938}BZ9 8821
i
'
CER11FICATIONS
Project WW TESTING
Pace Project No.: 9=56414
Charlotte Certification 1Da
9800 10nceyAve. Ste 100, Huntersvflle, NC 28078
FloridalNEt_AP Certification E87527
North Carolina Drtnldng Water Certification M. 37706
Kentucky UST Certification 0: 84
Ngrth Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater CeAftallon M 12
VirgirdaAtELAP Certification * 46M1
South Carolina Certification #: 99DO8001
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 29804
North Carolina Wastewater Certification #: 40
RorldafNELAP Certification # E87848
South Carolina Certification #: 99030001
Massachusetts Certification # M-NCO30
West VlrgiNa Certification #: 356
North Carolina Drinking Water Certification #: 37712
VirglnialVELAP Certification #: 460M
Eden Certification IDS
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Wastewater Certification A: 633
North Carolina Drinking Water Certification #r: 37738
Vlrginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent o1 Pace Analytical Services, Inc-. Page 2 of 11

l�
cel4ira"cai e
. � wnrpaadatramm
ANALYTICAL RESULTS
Pace Analytical 8enrlcea, lna.
205 East Meadow Road - auha A
EdaN NC 27285
(33E)8234W
Project VWVTESTING
Pace Project No.: 92258414
Sampler OUTFALL 1
Lab iD: 92256414001 Collected: 08/27/15 20:30
Received: 08129/1514:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. QUO]
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
71.6 mg1L
4.5
1
00/30115 09:22
REM, Oil and Grease
Analytical Method: EPA 1664B
Oil and Grease
ND mg1L
5,0
1
07/10/15 10:46
Total Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Total Nitrogen
1.4 m9/L
0.12
1
07/W/15 17.19
351,2 Total Kjeldahi Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Noldahi, Total
0.80 mg/L
0.50
1
07/09/15 03:54 7727-37-9
363.2 Nitrogen, NO21NO3 pros.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.80 mg/L
0.020
1
07/05/15 14:19
REPORT OF LABORATORY ANALYSIS
This (enact shall net be reproduced, except in full,
Date: 07/1312015 08:36 AM wlthotd the written consent or Pace ArtalyuCal Services, Inc., Page 3 of 11

i.
1+ �,,,,J ,,,�( PaceAnal"cai t3enrlaee, Intl.
Ir�I"UlCfl f�Q1 a 205 East Meadow Roed-StftA
Eden. NC 2728a
1 ..
[phone]
' QUALITY CONTROL DATA
Pmject: VVW TESTING
Pace Project No.: 92256414
QC Batch EDEN119082
Analysis Method:
SM 2540D
QC Batch Method: SM 25400
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92256414001
METHOD BLANK: 1497870
Matrbc: Water
Associated Lab Samples: 92258414001
Blank Reporting
Parameter
Units
Result Unit
Analyzed Qual iers
Total Suspended Solids
mg1L
NO 2.5 011W15 09:15
LABORATORY CONTROL SAMPLE: 1497871
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits 4ualiflem
Total Suspended Solids
mg/L
250 256
102 90-110
Results presented cn this page are In the untts Indicated by the "Units' column except where an anernate unit Is presented to the right of the resuh.
REPORT OF LABORATORY ANALYSIS
This report shall not bo reproduced, except in full,
Date: 07/13/2015 08:36 AM without the written consent of Pace Analylical Services, Inc_
Page 4 of 11

Pace Anatytica! Services, Inm
205 Ent Meadow Rood -Sub A
J r'P`I`V Edo». NC s72atl
nrw.pansisDatnrtl ��gy�.t
QUALITY CONTROL DATA
Project WWTESTING
Pate Project No.: 92255414
QC Batch: GCSV/21905
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1684B
Analysis Descrlptlon:
1664 HEM, Oil and Grease
Assocated Lab Samples: 92256414001
METHOD BLANK- 1506287
Matrix: Water
Associated Lab Samples: 922584140()l
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
M91L
ND 5.0 07/10/15 10:37
LABORATORY CONTROL SAMPLE: 1506288
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mgrL
40 33.9
85 76.114
MATRIX SPIKE SAMPLE: 1506289
92257786002 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg/L
ND 40 35.8 90 78-114
Resutts presented on this page am In the units Indicated by the "Units" column except whom an alternate unit is presented to the right of the result:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full;
Date: 07113r2015 08:36 AM without the written consent of Face Anstrikal Services. !nc . Page 5 of 11

3
Pace Anatyttcal SerAM% Ina.
j w Road - &ft A
' CreMa"bar p 205 East MeadoEden. NC T/Zee .
t�wtrynoetf6acam (gge)e29.gg11
f-
.i -
QUALITY CONTROL DATA
Project YWYTESTING
Pace Project No.: 92256414
QC Bald: WETA/23612 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92255414001
METHOD BLANK: 1502746 Matrbt: Water
Associated Lab Samples: 92256414001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L ND 0.50 07/09/15 03:32
LABORATORY CONTROL SAMPLE: 1502747
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total MOIL 10 9.9 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1502748 1502749
MS MSD
92257133002 Spike Spike MS MSD MS • MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD ' Qual
Nitrogen, Kjeldahl, Total mg1L 22.7 10 10 • 35.2 35.7 125 130 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1502750 1502751
MS MSD
92256864005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec "A Rec Limits RPD Qual
Nitrogen, KJeldahs, Total. mglL 8810 500 500 630 608 109 104 90.110 4
Resuhs presented on this page are In the units Indicated by the "Units" carurnn except where an alternate unit is prosentad to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 0711312015 08136 AM without the written consent of Pace Analytical Services, Inc,. Page 6 of 11

aCeAna"cal
Project VWVTESTING
Pace Project No.: 92256414
QUALITY CONTROL DATA
QC Batch: VVETA123602 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate t Nitrite, preserved
Associated Lab Samples: 92256414001
Pace Analytical Servitee, tnc.,
205 East Meadow Road - Suft A
Edgit, NC 2T288
{S9B)e�s-89�1
METHOD 13LANK 1501941
Matrix: Water
Associated Lab Samples: 92256414001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3
mg1L
ND 0.020
07/06/15 14:14
LABORATORY CONTROL SAMPLE:
1501942
Spike
LCS
LCS % Rec
Parameter
units
Cone.
Result
% Rec Limits Qualifiers
Nitrogen, NO2 plus NO3
mg/L
2.5
2,4
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE, 1501943
1501944
MS
MSD
92256346003
Spike
Spike MS
MSD • MS MSD % Rec
Parameter
Units Result
Cone— ,
Cone. Result
Result % Rec % Rec Limits, RPD Qua]
Nitrogen, NO2 plus NO3
mg1L 7.4
2.5
2.5 9.9
9.6 100 90 75-125 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1501945 1501946
MS MSD
92258635001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, NO2 plus NO3 mg1L 39.2 2.5 2.5 41.4 41.6 B5 96 75-125 1
Results presented on this page are In the units indicated by the "Units" colurnn except whin an altercate unit Is Presented to the right of the resub.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, eKCetlt in full,
Date: 0711312015 08:36 AM without the written consent of Pace Analytical Services Inc.. Page 7 of 11

-ffl-0007
ceAnalyf cal
(
QUALIFIERS
Project WVVTESTING
Pace Project No.: 92258414
DEFINITIONS
Pace Analytical SerAces, Inc.
205 Fast Meadow Reed - 8t4te A
Eden, NC 27288
(338)025-t18x1
DF - Dilution Factor, If reported, represents the factor applied to the reported data due to dpuMon of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting Unit.
MDL-Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each anayte is
a combined concentration.
Consistent with EPA guidelines, tnrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Dtfference
NC - Not Calculable.
SG - Spica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyt ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosadlphenyiamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited anaytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
Date- 07/13/2015 0816 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc,.
Page 8 of 11

Pane Analytical SerAC626 ton. "-
�+�
11lQl isL[I•
205 East Megdow Road -SufeA
NV/
Eden. NC 272M
WWWPm lthamm
(3at;l s-sszl
QUALITY. CONTROL DATA CROSS REFERENCE TABLE
Project: WWTESTENG
Papa Project No.: M56414
Analytical .
Lab ID Sample ID
QC Batch Method
QC Balch Analytical Method Batch
92256414001 OUTFALL 1
SM 2540D
EDENl19082
r 92256414001 OUTFALL 1
EPA i664B
GCSVM905
92256414001 OUTFALL 1
TKN+NO3+NO2
WETIW731
Calculation
92258414001 OUTFALL 1
EPA 351.2
WETAr23612
92256414001 OUTFALL 1
EPA 353.2
WETAl23602
REPORT OF LABORATORY ANALYSES
This report shall not he reproduced, except in full,
Dow 07/ 13/2015 08:36 AM without the written consent of Pace Analytical Services, inc.. Page 9 of 11

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CHAIN "4F-CUSTODY I A alytical Request Document
The Ch &&rant* la a LEGAL DC+CUMOU. M mkvaM Qdde rr1W 4e cmrIlelsd axon Wy,
/=��aTOFZY
AGENCY
LIND WATER
UST RCRA OTHER
SAMPLE A
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•hnporemRNala8yjdynfnyIhl■1h�myoumaI�eA YPace!NET80derpWmmftWftImW 9tirlab:ohmpeiu[1�ILprrm fhAre mmlpelda�dn3odrys FALL-&020rm.07.15-May-2007

Reidsville NC Stormwater Sampling Checklist
completed by: Item description
iq= 1. Sample during representative* storm event at Outfall #1
S`FR
2015-
1>0.1" raintall, sampled within 30 minutes of start of event, and no other raintall event >0.1" in
previous 72 hours
2. Spring sample between April 1�'t-June 30t or Fall sample between July
V and December 31st
3. At least 60 days has passed since last sample taken
4. Sample refrigerated until lab pick-up
5. Calculate rain flow and print spreadsheet
it 6. Fill out SDO qualitative monitoring report for BOTH outfall 1 & 2.
1 ' Report any deviations to Site Manager
o NC State form SWU-242-XXXXXX
7. Fill out form 132 and C2, site inspection and summary
j S. Fill out SDO monitoring report
m NC State form SWU-246-XXXXXX page 1
9. Fill out Storm event characteristics form
o NC State form SWU-246-XXXXXX page 2
G,P 10. After analysis is complete, check results against following benchmark
values. Report any deviations to the site manager
Total Nitrogen:
pH:
Oil and Grease:
Total Suspended Solids:
Benchmark
Result
30 mg/L
1. mg/L
6-9 su
7 /s su
15 mg/L
Np mg/L
100 mg/L
7/. G mg/L
11. Compile all documents listed above, together with analysis results,
scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12. Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR in
Reidsville snare site

CALIBRATION AND SAMPLE ANALYSIS PROCEDURE
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
pH analysis must be performed within 30 minutes of sample collection.
1. Turn on pH meter
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
+ 4. Rinse pH probe with deionized water and blot dry with a clean, soft cloth or tissue.
5. Place both the temperature probe and the pH probe in 7.01 pH buffer solution.
6. Shake the pH probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7. Record temperature and pH reading.
8. Press and hold the CAL button until "CAL" flashes on the screen.
9. Calibration will take approximately 30 seconds. When complete, record final pH reading.
10. Remove probes from 7.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
11. Repeat steps 5 through 9 using the 4.01 pH buffer solution
12. Remove probes from 4.01 buffer solution and rinse with deionized water and blot dry with a
clean; soft cloth or tissue.
13. Repeat steps 5 through 9 using the 10.01 pH buffer solution
14. Remove probes from 10.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or tissue.
15. Insert both probes in the storm water sample, and stir the sample gently to ensure homogeneity
and minimize carbon dioxide entrainment.
16. Wait one minute for reading to stabilize.
17. Record temperature and pH reading.
18. Remove probes and rinse pH probe in deionized water. Blot dry with a clean, soft cloth or
tissue.
19. Dampen the inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace cap on probe.
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
pH 7.01 Buffer
pH 4.01 Buffer pH 10.01 Buffer
Storm Sample
Date
Temp Initial Final
Temp Initial Final Temp Initial Final
Temp
pH
z7 I5
7ic, 7-IV �4A
76.E V.a1 y.�+ 7'�j IQQZ )l� vp
V.Q
u
Air Products Internal Use Only

Stolrmwatelr Discharge OutffaH (SDO)
Ouafitative Monitoring Report
For guidance on filling out thisform, please visit: hU://h2o.enr-slate.nc,us/swForms Documents.htm#miscForrns
Permit No.: NIGA1410 / 0 / 017l 0 / or Certificate of Coverage No.: NIC_JGf
Facility Name•. tr v(j C 1-
County: __ o-mar&M _ Phone No. T334S JYf 4
Inspector:
Date of Inspection: Z7 /
Time of Inspection: 6
Total Event Precipitation (inches): 7
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary),
k A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that,
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event -may contain up to 10 consecutive hours of no precipitation.
By this signature, I certifj tog this report is accurate and complete to the best of my knowledge:
(Signature of PeWO6 or Designee)
I: Outfail Description:
Outfall No. � I Structure (pi e, ditch, etc.).
Receiving Stream:
Describe the industrial activities that occur within the outfall drainages area: 411 f 4,-Zc1
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:�j>!i?
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): IJ I d- ol- _
Page I of 2
swu-2,12•1120ox

4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
l (2J 3 4 5
5. Floating SoIids.-. Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 V 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 20 33 4 5
7. Is there any foam in the stormwater discharge? Yes X0)
S. Is there an oil sheen in the stormwater discharge? Yes /No/
9. Is there evidence of erosion or deposition at the outfali? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe NGN
Note: Low clarity, high solids, and/or the presence of foam, oil sheen; or erosion/deposition may be
indicative of ,pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
5 W U-242- t 12608

5t®rmwater Discharge Outfa.11 (SJ)0)
Qualitative Monitoring Report
For guidance on filling out this form. please visit: httpl/h2o.enr tate.nc—us/su/Eorms Documents.htm#miscforrn,,%
Permit No.: N/C/ 6A / Q / 0 / 417 / 0 / or Certificate of Coverage No.: JC/C�l I I 1 I I 1
Facility Name: If I u PC
County: G NMOA40 -_ Phone No. 36 Alf Z%2
Inspector: j iGuS
Date of Inspection: Z7
Time of Inspection:
Total Event Precipitation (inches): •- Z5'
Was this a Representative Storm Event? (See information below) A Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A ."Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may contain up to 10 consecutive hours of no precipitation_
By this signature, I certify, that this report is accurate and complete-tetithe *t of my knowledge:
(Signature ofJ t4.ttee or Designee) // f
1. OutfaB Description:— {/ O
Outfall No. Z Structure (pipe, ditch, etc.)
Receiving Stream: C ru
Describe the industrial activities that occur within the outfall drainage area: t
2. Color: Describe the color of th
(light, ntedium, dark) as descriptors: !
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any disti'}�t odors that the discharge may have 0,e., smells strongly of oil, weak
chlorine odor, etc.): Ad 's
Page 1 of 2
Swt 1-242• 1 12608

i
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
] 2 3 4 S
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where l is no solids and 5 is the surface covered with floating solids:
10 3 4 5
d. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes
No
S. Is there an oil sheen in the stormwater discharge? Yes
9. Is there evidence of erosion or deposition at the outfall? Yes
/Nd
10. Other Obvious Indicators of Stormwater Pollution:
List and describe 2 o.._ _ .... _.._.._.__
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SW11-242-112N $

1; Vol W 1
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Cerffwsde of Coverage Number: _. readwaf by theD,111,1314i i;ww ltills� 3#dW
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Certificate of Coverage No. NCG
MMMM COLLECTED DUMG GI�AR YEARS
(TIdB ;egart Qht+11 be reed b,- lljlt sin iQO later'. &n 30 �
' ' f� the -date the a+aoeivee tine tn�liog resplts #iro�m the labttrator!') r
.
FAC1LiT'Y NAME ppCl
COUN' , C►tKiivfrffifa+ Z. ,
P'RRSON couwnNG SAMPLUS} '"
o" 'wy 4 PBOItIN 336
CERTII M LABORATORY(5) [ ns
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6 � � TUBE O1O PBR tax DBSIGNE� ,k
By ft dimsbiv� I tit titrepagt � aaaarste
to the best of p� ftaavrkdge.;
h
Pact A: Vehicle Maintenance Acti ty Monftorlpg �,lo�]' it, am average, ietnra than 55 galiaae per munW of stew nmtor a le peed)
OutFatf
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a <i
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Nate: If you report a sampled value in c�oess of the boachmerlc valve, or otdside ttto beachnaedc for A you must impl=ma Tier
1 or Tarr 2 n: tha Gaacral i'anmt.
-Mall Or4AIM and =4 con tm,
Division of -Wales Quality;:
..Am- Central Fiics
1617 Mail Sm-Ace Cm = -
R4WA Nmth Carolina 27699-1617
�
"h certify, paler Penalty of lair, that this dacuumo and all attadummts was prelmrsd wtdex, tl+ won or ! fa acesmance wltl a systrm designed to
assure that qwdiftd personnel pro1erly pflm aad'evafoate the _ Based'o� may hgp*y of tide pe�t�sol er i who mattuV wr _
those persons direetfy reVonslble fur gathering ft.#nQormstfon; the ledbrmatie� snhm�ed �, to We bt t id�q imativledge and hnl� trtte;'iic�iistc, turd comp2ate. `
I am aware that there for ilea iuforniatioa, itdl�;the PO'adflnes and hnprinmant thr imowing viaaetionti.�
(Signs of Permit
r
,-

STORM EVENT CHARACTERISTICS: Mall OCighuNd and am copy to: `
F Dish dwarer �r
nate,T rf , >ntm: conriat�es > ., .
Total Predpliation (inches): O 1 S 1617 Mail SW&D
�C�eutar
Event Dmdon (hours): __ I (only. if applicable — see permit) , . Raleigh; Nortb Carolina 27699.1617 . .
(if mare than noe storm event was sampled)
Date
Total Event Precipitation (hu*q):
Event Duradon (hours): (only if applicable— see permit.)
E
2
" 1 certify, under penalty at law, that thls doeament and all attechwere prepared under aw di gdion ar soper9ldma In aecorde— wlth a
system deslgaed to aswre titiat gaali8ed 1>moaual gt+► aria evoioete m�" ' used on uq.,iagalry at tie person
w.. "
or permos who made the gab^ or theme !br the the lulimrnEetfpu sabaaalmied ie,` tD tha lust
t
of ay knowledge and >idld, tree: anonate, that ase far i!elei W cengplete. , slg�tEirnnt Aenatbior S' . aetiau+'
the pnssEWlity and for 1pmawhtg vieaotiuns." '
• � ao CIS~.
( at P (Date)
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. AIR A
PRODUCTS — Delegation of Authority to Non -Officer Positions
The undersigned. Robert 0. Conley. in my capacity as Vice President - QfgbalEngineering of Air Prnduci5 and
Chemicals. Inc.. pursuant to the Delegations of Authority Policy, hereby delegates aulhonly as described herein below to
the followeng non -officer poaition(s).
POSITION TITLE AND COMPANY MAXIMUM VALUE
Each Tmnsac1ianlG0ntr0C1
See attached Page 2 for list of position tilles NIA
DESCRtPTION OF AUTHORITY
Authority to execute permit applications, permit related submissions and documents. and routine filings and
documents required by local. state• and federal regulatory agencies or authorities pertaining to environmental.
health. and safely compliance for the Wilkes Barre. Gardner, Cryomachinery and Prism Membranes facilities
❑This authwiiy may be subdalegaled wish the lo"owing reslrmiWna tit any)
©This authority may not be subdelegiiiiiedr
to take effect when countersigned by the Corporate Secretary or any Assistanl Corporate secretary and to continue in
effect for so fong as the designated position tille(s) remain unchanged, or until such authority shall be revised or
revoked by notice thereof by the undersigned, his or her successor in office. or the person to whom the designate
position(s) report.
''siinrure D.
—�
Countersigned by:
hate
ryui!sr �.- i in�.j•a�IJbt r`{rpara le Srtrr l.u.r
In..t ilm-i •R. .-' _M:'.n.ir ir��n.wi.iti •Lit

AIR 4
PRODUCTS L: Delegation of Authority to Non -Officer Positions
POSITION TITLE
Operations Manager
Line Manager
Site Manager
ASSlslanl Site Manager
Site Supervisor
Plant Manager
AsSiSlanl Plant Manager
Plant Superintendenl
Construction Manager
Environmental Manager
Environmental Engineer
Senior Environmental Engineer
Principal Environmental Engineer
Sensor Principal Environmental Engineer
Lead Environmental Engineer
Environmental Specialist
Senior Environmental Specialist
Principal Environmental Specialist
Senior Principal Environmental Specialist
Lead Environmental Soeclalist
P.y• M1rIr1 .�..... l+r
MAXIMUM VALUE
NIA

- Paral Analytleal aervilcm Ina:
�, I1�)1lfj��1 • ZQS East Mew Road - Suite A
Ce/'V Iw.J N(,Lil Edon, Ne 71na
i f ,itrst!'A!ao�°°`A; 4 i?38i�-BeTt'"
J u1 :13 ,2015
y ,
aw; Mr. Levi O'"ens "
S i Air Products ;
226 Equity Road°
�.
Reidsville, NC 27320
`i RE: Project; WWTESTING
Pace Project No.: 92256414
Dear Mr. Owens: -
}: Enclosed are the analytical results for sample(s) received by the laboratory on June 29, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNl"standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report..
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted..
If you have any'questions concerning this report,' please feel free to contact me.
{ rd Sincerely, .
Brittany Gibson for
Terri Page
[e-mail]
Project Manager
Endosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reptadueed, except in full.
without the written consent of Pace Analytical Sei vices, Inc..
Page 1 of 11

Pace AnaEytlwi Sarvi4w, jap ,
205 East Meadow q Sutte A f
Lr I�IIIa
Elan Nt+'27Y8B`r"
CERTIFICATIONS
Protect i } WWTESTING
;F`aP'z aF .
PaCB Project
z
{"eta `='
! :•" < <:y's � £ �
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.. �
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Charlotte.CerliN[.attonlQar ,.. � w _n
"
ry
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,� yt`•
8800 fOrtcay Ave. Ste,100. Hullteravple NC 28078 <
FlorldalNE! AP CartMctation E87t327
s,
,. North Carollna DrfnkUlg:Wataf,CertMcation 0- 37706
Kentucky UST.Certiicatfon 84
Ngrth Caraitna Field ricets Sen.Certiffcalion 5342
'
letit
": WVirginia Cecatian 357
Nortt CarolinaWaatewatsi.Certlficationti:12
VlrglrtiaNNfl
ELAPCertiflmdon# 460221
South Caroma C&Mk2tion A 99006001—
AshtivlllaCeltteltaslon IDa%
2225 Riverside D6 . psherrEite. NC 28804
North Carotins Wislawater CerMcaton 0 40. .
2.
FlorldalNELAP, Certification * E87648
;.South Carolina Ceritflcatlon *',99030001;
Massachusetts Cer"catlon C M-NC030 . •
West Vlrgirfla CertHimlloil#1 3.% .. -
}
North Garonne Drtdking Water Certt16tlon * 37712 .:.. ;
VlrgirialVELAP Certification V 4W=
'
Edon Certllicatl n IQs - .
•
205 East Meedow Road Suite A, Eden, NC 27288
North Carollna Wastewater Ceritttcation 0- 833
-
North Carolina Drinking Water CeMl6atlon M. 37738
Vhgin%NELAP Certification A 460025 •' ..
REPORT OF LABORATORY ANALYSIS
Thi% report shall not be reproduced, except in full•
without the written consent of Pace Analytical Services. Inc . Page 2 of 11

pace Attalyllcal t3eitrlcttis, Inert: '
}
aceArialytica!
M EastM60dow >_� A.
Eden, NC 27280'
yrvtrpaeageecam.
(396eZ4e92!
ANALYTICAL RESULTS
'
.
:IT otet� �_; WWTESTINGJT
. rr
Pace, Project No .922R%14-
Samplin fOt1TFALL 1
Lab ID: 922MW14001 Collected. 0&27115 20-30
Ra mlved: 0=911514:10 Matrtc Water
.,Parnmetma,
Residtat> Units RepOA Lim!!''>; DF ,.
Ptepgred: „ Aiialyxed - CAS 'No gtml ^
21540D Total Suspended Soileta
Ans"cai Method: SM 2540D
Total Suspended Solids
71.6 r g& 4.5.- 1
08W15 09:22
HER; Oil and Grease:
Analytical Method: EPA 18848
011.and Grease
ND mglL 5,0 1
07110V15.10:4t3
r.,
Tots) Nitrogen Calculation
Analytical Method: TKN+NO3+NO2 Calculation
Total Nitrogen:.-,
1.4 mg1L 0.12 1
071{19l15 17:19 r
351.2 Total Igaldahi Nhrogon
Analytical Method: EPA 351.2
REPORT OF LABORATORY ANALYSIS
This repart shell not be reproduced, except in NJ,
Dale: 07113/2015 08:38 AM without the wntten consent of Pace Analytical Services, Inc.. page 3 of 11

l
Petra Anellq cal SeArtCea; Inc.'
ztis EaaehAeadaw Road-st,ttea-�
Eden: NC Tr1B8'`"
W.
QUALITY CONTROL DATA
f
'.^
WW-TASTING .
° r �`;
� �
�'�
d '� Pecs Project No 92258414 �
,� � • .
r t_ qC Batch EDENM9082
Analysis Method SM. 254013�.
QC Balch Method: : SM 2540D
Antllysts DescriP an ` '-2640D 7btal Suspended Solid9r
,a
Asaootated Lab Samples M58414001
"
v.' METHOD BUWK 1497870
Matrix Water
Associated Lab Samples:' 92258474001r.
Blank Reporting-
Parameter . units
Raw& . Lima., - -- Analyzed Qualftra
hotel Suspended Salida' mg/L
ND" " 2.5 06W15 09:15
LABORATORY CONTROL SAMPLE: 1497871 .
Spike LCS . LCS % Rea.
Parameter. Units
Cotyc "' :. Result ` . 96.Reo Limits . 4ualiffers
Total Susperided Solids-, mglL
250 25ti,. in9011D`
Results presgHed on this page art to the untts Indlcated by the "Units" Column except where an ahernsta unit la prasanted to the right of the resrrh.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in cult.
Date: 07/ 1312015 08:36 AM without the written consent of pace analytical Services, Inc.. Page 4 of 11

Pace Analytical9arlir a 1ttc.
/+� js
GeAW
205 Esal Meadow Road • 8u1t A
`
�.. -
Eder; NC 27288
wr"cpea ed°m
C338]MZ$4 s12'l. .
QUALITY CONTROL DATA
Pn4ectWUVTESTiNG.
s
PewP No: 92256414
is4y:
., °•., ' -
..
QC 8atd1. - GCW21905F
AnaNsls Method: EPA 1684E
h
QC Batrtl Method:, EPA 168413 - :
Analysis Destzipblxt: 1684 HEM, Oil and Grease
Aiiaodated Lad Samples:. 92258414001
`
-
MEtHdD BLANK.- ` 1508i67
Matu: Water
Associated Lab Samples: 922SU14001
Blank Reporting
Parameter,
Units,
Result Limit Analyzed Qualifiers
Oil and Grease
mglL
ND 5.0 07110/1510:37
LABORATORY CONTROL SAMPLE:
1506288
Spike LCS LCS % Rec
Parameter
units
Corwc Resul % Rec Limits
Qualifiers
OII and Grease
mg&
40 33.9. 85 78-114
MATRIX SPIKE SAMPLE:
150e289
92257768002 Spike MS MS
% Rec
Parameter
Units
Result .' Conc Resuil % Rec
Limits Qualifiers_
Oil and Grease'
lilglL
ND 40 35.8
90 78-114 `
Results presented an this page are In the units Indicated by the "units' column except when an 41ternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. et'wpt in full,
Dais: 07/13/2015 0& 38 AM without the written consent o1 Pace Analyt l Services. Inc . Page 5 of 11

Y��
J
Aata Aihah/11da1,t3�irlcme lnc.
e
n 1v
/+ MOO
205East MeadowRogd-SLIJWA-
t3C�!'UI✓ Lam!"
Eiert; NC 27M
A�e
-Yalfrl
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f,
-
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QUALITY CONTROL DATA
! �
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t
yy l,.Al .: per} /�,
k Projact I Y 4s -" 1, WtES IN1] `
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1 5Y.
# Peas.Project No.:.,92ZSl3414
r z..
yy
_
i sQC
t3att�i WE7A/238i 2 ' °
Anatys[s Mettlod w EPA 351.2
Y + 4
' QC Batik Method: �- £EPA351 2
'Analysts f]iaftdon 351 2TKN :
� -
3.-'-
Asibaited Lab Sampled 1 32258414001
r ?
x
N r
_3
METHOD BLANK 1502T48
Matrix Water
u Z'
r
AaaoGated Lati�Samplea: 9225t341400t
Blank Reporting
Parameter Units
Result. Llirdt Analyzed Qualifiers.
e
Total
mg/!,
`
.32Ni>rpg:n,t]edat,
-
21
Y - "
LABORATORY CONTROL SAMPLE: 1502747.
_
Spike LCS - LC3
% Rec
. Parameter . Units .
Conc. Result' % Rec
Limps Qualifiers
Nitrogen, Kjeklahl, Total . ' mg/L:
10 - 3.9 99'.
*110 . .
MATRtX SPIKE 8 MATRIX SPIKE DUPLICATE: 1502748 1501749 .
MS M5O
92257133002
Spike.- Splka MS MSD-
MS MSD % Rec
Parameter ' Units •- Result
Conc.- Cons " . Result-- Result-
'% Rec % Rec Limits
RPD • Quaff . :
Nltrcgen,K]eldatil.Total rng1L 22.7
10- 10• 35.2 35.7.
125 130 90110
1 Mi..:r• '`: ,
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: i502750 1502751
MS- MSD .
= 92256864005
Spike,. Spike MS MSD
MS MSD % Rec
Parameter Units Result
Cant: Conc- Result Result
% Rec 95 Rec - Limits
RPD Qual
Nitrogen, Kjeldahl, Total mg/L 86.0
- 500 600 630 608
109 104 90-110
4
Rewtts presented on this gage are In the units Indicated by me -lJrdW column aacapl where an altirmats unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full.
C7ate: 07/13/2015 08:36 AM without the written consent of Pace Analytical Services, Inc . Page 6 of 11

Pace Analytical it lwaOa. In*.,_
aceAWW
205 East Meeclow Road - Suite A
Edit, NC 27200
i -
awapa°talpDame-,
i33�5T.9-efi21.. '
QUALITY CONTROL DATA
Project = WWTESTING`
t
.Pace Project No.: 92258494'
QC Batch: WETA123602
Analysis Method: EPA 353.2
QC Batch Method: EPA353.2:',:.
Analysis Desa_iption: 353.2 Nitrate + Nitrite, preserved
'
Attsodated Lab Samples.' 92258414001
{
METHOD BLANK 1501941
Matnk- Water
Asaoclated Lab Samples: M56414001
Blank Reporting
:
Parameter Units
Result. Limit Analyzed Quailtlers
Nitrogen, NO2 plus NO3 mg/L.'
ND0.020 07/06/15 14:14
LABORATORY CONTROL SAMPLE: 1501942
o `
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualftrs
Nitrogen, NO2. plus NO3 M9fL
2A 2.4 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:'1601943 1501944
MS MSD
92256346003,
Spike Spike., _ MS MSD MS. MSD
96 Rea-
-z
f. Parameter -. Units'. Result
Conc:-' . Conc.' Result RestSt 96Rec' %'Rec
Limits RPD
`-
lVltrogeri NO2 plus NO3 mglL, 7.4'
2.5 2,$ 9.9 9.6 100 90
75-125 3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1501945 1501948
-
MS MSD.
„
92258835001
Spike Spike MS MSD MS MSD
% Rec
Parameter Units Result.
Conc. Conn Result. Result % Rec % Rec
is RPD Quat
'
Nlirogen, NO2 plus NO3 mg1L 39.2
2.5 2.5 41.4 41.6 85 98
75-125: 1 -
Reautts presented on this page are In the units Indicated by the "Elnite" column except when an attentete unit Is presented to the tight of the result.
REPORT OF LABORATORY ANALYSIS
This fepon shall not be reproduced, except in full.
DaW 07/ 1312015 08:38 AM without the written consent of Pace Analytical Services, Inc.. Page 7 of 11

k
at,e/`Ufalytrv[i!*
QUAE.IFIERS
"mot tiProjed F WW TESTING
'M= f Pace geCt No.
js'1� .4 �• 'l
Pace Anatytf6at 8eiviasar lea .
205 East Meadow Rued gytteeA,: .
Aden., ntc essay
(eyB2sae2, .
`tom
..PAl�'+.
I„.
--
r
dF D[lutl represents If reported reprasea the factor applied to the reported data due to dllution of the Bemplti aliquot
`n
`
NU Not Defected at cu above adjusted reporting AmIL
J - I59mated i onces<ration above the adjusted method detection Ilmil and belt It the adkusted reporting limit
_ F
"[uIDL -Ad fed Method Detection Llrrtit
t
PQ Practical Quantltatlon Urnit
RL Repotting Un
a`
S
r
far
5
; . i,2-DlptrerryUiydrszlne dec ornposes to and Cannot be separated from Azcbenzme using Method 8270. The result each anatyte is s
a
y a combined conCentratian.
Consistent wltft EPA guidelines, unfounded data are displayed and have been used to eak;ulate % recovery and RPfl values.
LCS(D) 'Lsborelory Canitroi Sample (Duplicate)
`
MS(D) Miatrtx Spike (�uplhate)
DUP Sample Duolkate
RPD - RetattVa Percent Difference
z -
NC - Not Cak�iable. -
-
SG - SMca Gel - Clew -Up...
1
U Indlcateo the caaipolutd~was analyzed for, but not detected.::
y '
=
Add prEservatlart may not be appropriate for 2 ChloraettrySvtny! ether Slyrerie, and Vinyl chloride. ^
A,separete'vlal'preasrved to a pH of 4-51a recommended In SWW Chapter 4 for the analysis of Acroletn and Acrytonitrile byEPA
r > .
Method 82150.1
N-Nltnosodfpharrylamine decomposes and cannot be separated from D1pt±enylamine using Method 82.70. The result reported for
each analyte la a combined concentration.
Peoe Analytical la TNI atxxedlted: Contact your Pace PM for the cement 113t of accredited analytes.
r _
TNI - The NELAC institute.
ANALYTH QUALIFIERS.
M1 Matrix spike recovery exceeded DC Iinrits. Bairn accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall nol be reproduced, except in full,
Date: 07/13/2015 08:36 AM without the written mneent of PaceAnalytiral Services. Inc., Page 6 of t i

Paco Ana "cal BeTvlaas. h10.
/y,, ,�,,+a
CZV,�./'1f. coca
205 East Meadow Road * $4ft A e
Edeti, NC zy=
QUALITY CONTROL DATA CROSS REFERENCE TABLE'
ProJeci WWTEST]NG
r'
'•
F.
9
Pare Prajecl,NO.: 92258414
Analytical
' Sa pie ID:..
QC Batch Meffi6d',•
QC Batch Analytical Method Hatch
t
92286414001 ` :. OUTFALL 1,
- SM 2540D
EDEN119082
922664140(M OUTFALi'I
EPA 16648
GCSV121308;
:�
,-
y
_
92286414001 OUTFALL 1
TKN+NO3+NO2
WET13B731
CaimdBlion
922564140D7 OUTFALLi
EPA351.2
WETAMS12
92258414001 OUTFALL 1;
EPA 353,2
WETAl23002
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 07113/2015 08:36 AM without the written consent of Pace Analytical Services, Inc., Page 9 of l I

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• ' ORIGINAL
t ' PRI4[T Ftmw of BAlePL� �, � , t . ,`
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ti� L'iBpaSntNo�9ldpoiVl�hlnlwwe�ae�QP�oraNETSQd�pgm�et��odvfnBel�admpadt6tiPrmm�A6r �ntpddsdhg7Bd�
. F,ALL-0.020sev.07, i�rMsy-200T

SDK �A� ,
Reidsville: NC Stormwater Sahnpling,Checkl st
20��
Completed by
Item description
' =
3
Sarimple during representative* stor, evetit:at0utfa1l
*>0.1" rainfall; sampfed.w�thin 3o minutes of start ofi:e�ent, and,hd'othei.rainfill event?o 1" in ;
previous 7Z hours:
2 Spring sample between April 1� June 30, or,Fali sample between July
�,
x;
1st
and Decernber3
�
At least fi0 days.has passe dsince last sample taken
4.. Sampl-:ref rigerated:until lab: ick-up
5.. punt spreadsheet
_Calculate_ran'flovu;arid
7. Fill out.form B2 jnd•'C2, site inspection and summary
j 8 Fill.out SDG monitoring report ,
a NC State form-SWU-246-XXXKXX page 1
9. Fill out Storm event.characteristics form
NC Sate form SWU�246-XxXKXX page;2
10: After"an*' sis s complete 'check results against following benchmark
values. Report any deviations to the site manager
_ Benchmark. Result
Total Nitrogen: 30 mg/L^ mg/L
pH: 6-9 su 7 /S su:
Oil and Grease: 15 mg/L N+o mg/L
Total Suspended Solids: 100 mg/L _71- G mg/L
11. Compile all documents listed above, together with analysis results,
scan and send to Environmental Specialist and Site Manager. Store
hardcopy in Reidsville plant office
12. Environmental Specialist sends to NC State within 30 days of analysis
results. Also places copy of all communications with NC DENR in
Reidsville share site

: CALIMRATidWAND SAMPLE ANALYSIS PROCEDURE
EXTECH Qyster-l0 pH/mV/Temperature Meter Serial Number 022055 .
pH a a sis ust be ;eiformed within 30 minutes of slam 'le collection.
Turn on pH meter ;
2. Connect temperature and pH probes to meter
3. Remove storage cap from pH probe
�+
4. Rinse.pH probe with deionized water and blot dry with a clean; soft cloth or tissue.
Y
S. Place both the temperature probe and the pH probe in 7.01 pH buffer solution.
6. Shake the pH. probe gently to dislodge air bubbles and wait one minute for reading to stabilize.
7. Record temperature and pH reading.
8. Press and hold the CAL button until "GAL" flashes on the screen.
a
9. Calibration will take approximately 30 seconds.. When complete, record final pH reading.
.�
10. Remove probes from 7.01 buffer solution and rinse with deionized water and blot dry with a
clean, soft cloth or. tissue:
11. Repeat steps 5 through 9 using the 4.01 pH buffer. solution. .
;zv<
12. Remove probes from 4.01 buffer solutlon and'rinse with deionized water and blot dry with a
clean, Soft cloth or tissue. '
13. Repeat: steps 5 through 9 using the 10.01 pH buffer solution .
14. Remove probes from 10.01 buffer solution and rinse with deionized water and blot dry with a
`
clean, soft cloth or tissue.. .
is. Irisert both probes in the storm water sample, and stir the sample gently to ensure homogeneity . `
and minimize, carbon dioxide entrainment.
16. Wait one minute for reading to stabilize. .
17. Record temperature and pH'reading.
18. Rernove-probes and rinse pH probe in'delonized water. Blot dry with a clean, soft cloth or
tissue:
19. Dampen the inside of the pH storage cap with a small amount of pH 4.01 buffer solution and
replace capon probe.
CALIBRATION AND SAMPLE RESULTS
EXTECH Oyster-10 pH/mV/Temperature Meter Serial Number 022055
pH 7.01 Buffer
pH 4.01 Buffer
pH 10.01 Buffer
Storm Sample
Date Temp Initial I Final
Temp Initial I Final
Temp Initial Final
Temp pH
74.3�* 4;.61
7S'q IaOZ )O,af
&r,o 7
r
Air Products Internal Use Only

St® r>lAwater DI9&irge ®utfail '(SD0)
�naliiat�ve 1Vo»tvring deport`
y
For guidance on filling 'out this farm, please visit huB //h2o ear state.nc us/sulForms Dcm; ments.httm#m_isc
rm�
Pernut No N/C/C 1 ! d / Q / Q 1 161' or Cer[ifcate of Coverage No NfC�GI
_
Factitty,Name ri �r [f
::
County, 14GtKnt trLs Phone No. 14-ZE
inspector:
Date of Inspeetiori: Z7 / _
Time of Inspection:
Total Event Precipitation (inches): • 7 5r
,
Was this a Representative Storm Event? (See information below} ' Yes
Please check your permit'ra verrfy if Qualitative Moni#oring ?mist be'performed diiring a representative
storm:event requirements vary).
2.
By this signature, I ce..' report is accurate and co to th best of r6y knowledge:
.. (Signature of P or Designee)
l: Outfaff Descriptioln:
Outfall Nb.. Structure (pi ,Glitch, etc.)
Receiving Stream:. mar. Ilw_
Describe the industrial activities that occur within the outfall drainage area: t/ a
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: /o47yem _
T
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): /(d d6r _
Page E of 2
0 W 1J-2,t2 -1 12601

I
4. G9ai ity:, Choose' the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy.
A
.4 .
S. Flosting"'Solidg -Choose the number which best describes the arriotint of floating solids an the �l t
storinwater discharge, where 1 is no'solids and.5 is'the surface covered with floating solids:
(2)
1 3 4, 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in..-,.-,' ."
the stormWater discharge, where 1 is no solids and 5 is extremely muddy:
. 1 C2) 3 4 5
7, Is there any foam in the stormwater. discharge? Yes
8. :1 there an oil sheen in the stormwater'discharge? Yes
9. islhere'evidence of erosion or deposition at the outfall? - Yes No
i
10. Other Obvious Indicators of Stormwater Pollution:
List and describe NGw
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
S W U-242-112606

Y'Q� 4[a'�
'. t... _i.
/[5�.. g
C`F�R
s40i����Y4' c_fl/YiS+ �� ®� � t1J�O
~'
S.
gutdance.on filling out this form, please visit ]Lt err state ncslsu/FormsJocsancois.htti!#;ntscfoljrlyg
Permit �"CtctoCoveag�iNo :NIC! JC/SSI7777
t
4"
Facility Name:
County. ' L ! Phone No. 'zuz
lnspzctoi: Gt�uf
Date of Inspections G zi
t '
Time of Inspection:' 76 36.
t
Total Event Precipitation (iriches)s
.'
Was this a Representative Storm Event. (See information below) .:Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed during
a representative
storm event (requirements vary),
A "Representative Storm Event" is,a storm event that measuies greater than 0.1 inches of rainfall and that,' " r
is preceded by at least 72 hours Q days) in which no storin event measuring greater than 0.1 inches has
occurred, A single storm event may contain up to 10 consecutive hours of no precipitation.
By this signatuim,_I certify. - that this report is accu te:and complet the t of my knowledge:
(Signature 6fJrm ttee;or Designee)
is outfali'Deserioiion: p
Outfall No.' Z Structure (pipe, ditch, etc.)
Receiving Stream: e• 1te
Describe the industrial activities that occur within the outfall drainage area: ele 1L4Attr&ee
2. Color- Describe the color of
(light, medium, dark) as descriptors: _
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Demribe any disti t odors that the discharge may have 0,e., smells strongly of oil, weak
chlorine odor, etc.): AG Q1/_ _
Page I of 2
Swl 1.242.1 12608

1
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear "
and 5 is very cloudy:
S. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater'discharge, where l is no solids and 5 is the surface covered with floating solids: .
tf t 'J
1 3 4 5
6, Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
] 2 3 4 5
7. Is there any foam in the stormwater discharge? Yes Na .
' x
8. Is there an oil sheen in the stormwater discharge? Yes
v
!-
9. Is there evidence of erosion or deposition at the outfall?. Yes /Nql :y
v
10. Other Obvious Indicators of Stormwater Pollution:
List and describe Ap
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosionldeposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
swi r-z42-11 mg

t
AIR
j
ROWDU
Air Products and Chemicals, Inc.
357 Marian Ave
Tamaqua, PA 18252
Telephone [phone]
February 27, 2013
Division of Water Quality
Stormwater Division
585 Waughtown Street
Winston-Salem NC 27107
RE: NCS000030 Annual DMR Summary
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
RECEIVED
N.G. Dept. of ENR
MAR 0 4 2011
Winston-Salem
Regional Office
Enclosed please find Stormwater Discharge Monitoring Report Annual Summary for the Air Products and
Chemicals, Inc. Reidsville, NC Facility for calendar year 2012.
If you have any questions regaring this submission or require additional information, please feel free to
contact me directly at 570-467-4399.
Sincerely,
Joseph Sebia
Environmental Specialist
Air Products and Chemicals, Inc.
Electronic Materials Organization
Tamaqua PA 18252
CERTIFIED MAIL: 7010 0780 0000 8680 9004

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year A O i Z
Individual NPDES Permit No. NCS❑O 0 O❑❑O 3❑ O or
Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑
This monitoring report summary.of the calendar year should be kept on file on -site with the facility SPPP.
Facility Name: P\ti Paooyc,}s 04f,M,c-rkt,.r, IIyG Rr�r�sv►L�4 NG r��-���Ty
County:
Phone Number: (!3(0 ) .3 `t 9 ~ Z q (6'Z Total no. of SDOs monitored i
Outfall No. b vi
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No j)9
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ' ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes'K No ❑
SW U-264-Generic-13Dec2012

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the
Signature _
Date a ! z7
lity of finest and imprisonment for knowing violations."
For questions, contact your local Regional Office:
DWQ Regional Office Contact Information:
ASHEVILLE REGIONAL OFFICE
FAYETTEVILLE REGIONAL OFFICE
MOORESVILLE REGIONAL OFFICE--
2090 US Highway 70
225 Green Street
610 East Center Avenue/Suite 301
Swannanoa, NC 28778
Systel Building Suite 714
Mooresville, NC 28115
[phone]
Fayetteville, NC 28301-5043
[phone]
[phone]
RALEIGH REGIONAL OFFICE
WASHINGTON:REGIONAL OFFIC9
WILMINGTON REGIONAL OFFICE
943 Washington Square Mall
127 Cardinal Drive Extension
3800 Barrett Drive
Raleigh, NC 27609
Washington, NC 27889
Wilmington, NC 28405-2845
[phone]
[phone]
[phone]
WINSTON-SALEM_REGIONA OFFICE
CENTRAL OFFICE
1617 Mail Service Center
Raleigh, NC 27699-1617
585 Waughtown Street
Winston-Salem, NC 27107
'To protect
Preserve, enhance
[phone]
[phone]
North Carolina's water
SW U-264-Generic-13Dec2012

" Ctz"
AIR
PRODUCTS
Air Products and Chemicals, Inc.
357 Marian Ave
Tamaqua, PA 18252
Telephone [phone]
March 8, 2012
Division of Water Quality
Stormwater Division
585 Waughtown Street
Winston-Salem NC 27107
RE: NCS000030 Annual DMR Summary
Air Products and Chemicals Inc.
225 Equity Road
Reidsville, NC 27320
Dear Sir or Madam:
��//N��QDept. of ENR
1�11 R 12 n411lZ
V tston-3aieno
Enclosed please find Stormwater Discharge Monitoring Report Annual Summary for the Air Products and
Chemicals, Inc. Reidsville, NC Facility for calendar year 2011.
If you have any questions regaring this submission or require additional information, please feel free to
contact me directly at 570-467-4399.
Sincerely,
1
Joseph Sebia
Environmental Specialist
Air Products and Chemicals, Inc.
Electronic Materials Organization
Tamaqua PA 18252
CERTIFIED MAIL: 7011 1150 0002 3820 3187

STORMWATER DISCHARGE OUTFALL (SDO)
ANNUAL SUMMARY DATA MONITORING REPORT (DMR)
Calendar Year R 01 1
Individual NPDES Permit No. NCS[JJ ®A[ []Jj0 or
Certificate of Coverage (COC) No. NCG❑❑❑❑❑❑
This monitoring report summary of the calendar year is due to the DWO Regional Office no later than March ys` of the following year.
Facility Name: AIR N-0100G'73 C+4Vj,c*(.,C -L/f G 0,C_y���t
County: R0C"c-''jC.,IjAA^
Phone Number: (5794 !g-7- 9 39 rl Total no. of SDOs monitored
Outfall No. 1
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes © No ❑
P4
Total
Rainfall,.
inches
Parameter, (units)
) O ,-.�
.Y /1 • i"r�
t
�
i ���
OU-M
wtG- L �:.
`%t N
C,FJL�
T KrV
�i"'4v�Ll
N NO W
�I/"+G(.
C O o
(a►G Z
Benchmark
—A
30
),D'ate;Sample
`'Collected, ,.
rmn/dd/yy. f
Z)
101`l3
N
-L
—L
it 17 11
0 ' N o 0o
A/ 0
rJ D
O I
SW U-264-Generic-25May2010

Additional Outfall Attachment
Outfall No. I
Is this outfall currently in Tier 2 (monitored monthly)? Yes ❑ No
Was this outfall ever in Tier 2 (monitored monthly) during the past year? Yes ❑ No
If this outfall was in Tier 2 last year, why was monthly monitoring discontinued?
Enough consecutive samples below benchmarks to decrease frequency ❑
Received approval from DWQ to reduce monitoring frequency ❑
Other ❑
Was this SDO monitored because of vehicle maintenance activities? Yes ® No ❑
Total
Rainfall
; inches
Benchmark
N/A
1 Date'Sarnple
Collected,',,
kv
mm/dd/yy'1`
NON Pow.,
Z
z 5. 7
N 0
N e w 0&bt
Orgy USA(- -
(«rL1 Ma)
C
Parameter
SW U-264-Generic-25May2010

I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person
or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possitfik of fines and) imprisonment for knowing violations."
Signature
Date :?
Mail Annual DMR Summary Reports to:
DWO Regional Office Contact Information:
SW U-264-Generic-25May2010

EN
i
' JUL 1 3 2005
. 1F it li
Michael F. Easley, Govemor
William G. Ross 3r., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P. E. Director
Division of Water Quality
Coleen H. Sullins, Deputy Director
Division of Water Quality
STAFF REVIEW AND EVALUATION WSRO
NPDES Stormwater Permit
Facility Name:
Air Products & Chemicals, Inc.
NPDES Permit Number:
NCS000030
Facility Location:
Reidsville, NC (Rockingham Co.)
Type of Activity:
Industrial —manufactures liquid oxygen, nitrogen, and argon.
SIC Code (if applicable):
2813 (Industrial gases)
f
Receiving Streams:
UT to Little Troublesome Creek (index no. 16-7) [Impaired]
River Basin:
Cape Fear River Basin, Sub -basin 03-06-01
Stream Classification:
C-NSW
Proposed Permit Requirements:
See attached draft permit.
Compliance Schedule:
N/A.
Basis for Monitoring:
See attached Monitoring Data Analysis. Removed TP and TSS
monitoring Kept COD monitoring for at least two more years;
footnote explains that if all values below 120 mg/l, site may
discontinue monitoring for remainder of the permit.
All monitoring has changed to Semi -Annual (spring and fall). This
change is based on the Division's revised strategy for stormwater
monitoring in renewal permits and makes stormwater discharge
sampling frequency consistent with qualitative monitoring. In
addition, DWQ has incorporated benchmark values into the permit.
These benchmarks are not permit limits but should be used as
guidelines for the facility's Stormwater Pollution Prevention Plan
(SPPP). New language specifies that if any measurements exceed
benchmark values, the facility should evaluate the effectiveness of its
BMPs, review and/or update its SPPP, and document any efforts to
address stormwater contamination (see Part 11, Sec. B & D).
Total Flow monitoring has been removed per DWQ revised strategy
(Total Rainfall and Event Duration parameters retained). Instead, Part
11. Sec. A clarifies that SPPP site map include drainage area for each
outfall in acres and percent impervious area in each drainage area
(should flow ever need to be estimated).
Basis for Other Requirements: TMDL language added in Part II, Section B—impaired stream
segment & upstream of Jordan Reservoir.
Response Requested by (Date): August 15, 2005
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [phone]
l
NLDENR
Customer Service
I-877-623-6748

NCS000030
Central Office Staff Contact: Bethany Georgoulias, [phone], ext. 529
DOCUMENTS REVIEWED
NPDES Stormwater Permit Application Materials
S/W Permit File
Analytical &Qualitative Monitoring Results summary
Cape Fear Basinwide Plan (rev. July 2000) & Draft Plan rev. March 2005, out for
Central Office Review Summary:
Since last renewal, the company has had no significant changes in industrial activities. This site compresses,
liquefies, and distills components of the incoming air stream into liquid nitrogen, oxygen, and argon.
Facility discharges stormwater into impaired waters. Little Troublesome Creek was added to the 303(d) list
because of impaired biological integrity (and further downstream of Reidsville WWTP, fecal coliform). The
potential sources noted are urban runoff and storm sewers. A fecal TMDL for Little Troublesome Creek was
approved in May 2002, but no loads were allocated to any permitted point source dischargers (would include
NPDES Stormwater discharges), and activities at this site should not be a significant source of the bacteria.
The Draft 2005 Cape Fear Basinwide Plan cites the November 2002 WARP Study that identified toxicity, organic
enrichment, and habitat degradation from impervious surface runoff, urban development, unpaved roads, road
construction, and cropland and streambank erosion as the biological community stressors in the stream. Also,
stormwater discharges throughout this sub -basin potentially contribute nutrients downstream to the Haw River
Arm of Jordan Lake Reservoir, impaired from chlorophyll a violations. The Jordan Reservoir and Haw River
Nutrient Sensitive Waters (NSW) Management Strategy and TMDL for the Upper New Hope Arm resulted in
nitrogen and phosphorus loading limits for the Reidsville WWTP wastewater discharge. Current recommendations
are also for all local governments in the Haw River Arm watershed to meet NPDES Phase II stormwater
requirements and to achieve stormwater TN & TP export performance goals for new and existing development.
This is important for the Air Products facility for two reasons: It is located in Reidsville, a municipality not
automatically designated in Phase II, but one that will probably be brought in as a result of NSW Management
Strategy requirements for the Cape Fear Basin; also, the activities at this site are a potential source of nitrogen.
Qualitative Monitoring Results: Permittee sent results from 1999-04. No problems observed.
Analytical Monitoring: See attached Monitoring Data Analysis. Permittee's outfall 001 was granted
representative status in 1995 (letter attached). Recommend removing TP (not a significant source of phosphorus)
but retaining TN monitoring (maximum close to benchmark of 30 mg/1) because of nutrient concerns in this
watershed. Also removed TSS monitoring because values were well below benchmark (1999 permit reviewer noted
more data needed to definitely rule out need for monitoring). Probably not necessary to include pH monitoring for
this site.
For this industry sector, the EPA Multi -Sector permit includes monitoring for total recoverable Aluminum and
Iron, but these are not pollutants of concern at this facility. Nitrate+nitrite monitoring would also not apply.
Monitoring frequency will increase to semi-annually. This change ensures at least nine data points are collected
through the permit term and makes monitoring frequency consistent with qualitative monitoring. Also, benchmark
values for all parameters have also been added to the permit as a guide for the permittee to check the effectiveness
of BMPs (and document efforts) when necessary. Because TN monitoring is based on a potential source, a
benchmark concentration for this nutrient is included (would not be if only monitoring to collect data).
COD levels decreased markedly since 1999 (from 142 to <25 mg/1). Facility has made significant efforts to
eliminate several chemicals on site and improved storage practices the past few years, though it's not certain if
anything specifically removed the source. Because quarterly monitoring during 2002-03 recorded four values,
reviewer recommends keeping COD monitoring (semi-annual) for at least two more years to collect four
additional data points. Site may discontinue monitoring if no values are above the benchmark.

NCS000030
Follow-up with the company contact (David Eberle, 336-342-2311) on 5/17/2005:
• There are vehicle maintenance activities at this site with oil usage exceeding 55 gal/mo. (tractor
maintenance); however, any spilled oil or other runoff in this area drains to the oil/water separator
and into the sanitary sewer. All used oil is collected by a vendor. No stormwater runoff contacts
residue from these activities.
• COD was in the I00s back in 1994 and 1999 (116 and 142 mg/l, resp.), but 2002-03 monitoring showed
substantial decrease (<30 mg/1). Any particular reason or different BMPs?
Not sure. ]Talked with Environmental Engineer for the site, Damian Marcinek (610-481-5766) on 5/17.
Company has been in the process of eliminating several chemicals on site and has re-examined its storage
practices the past few years. Probably no one particular change, but reinforcing BMPs already in place has
hopefully made the difference. Site was concerned when COD jumped up in 1999.]
• Any other chemicals stored outside besides diesel fuel and liquid NZ, OZ, and Ar?
No. All diesel fuel tanks are now underground and monitored around the clock.
Recommendation: Based on the documents reviewed, the application information submitted on October 22, 2004
is sufficient to issue an Individual Stormwater Permit.
Prepared by (Signature)
Stormwater Permitting Unit Supervisor
Concurrence by Regional
Water Quality Supervisor
Date J ZL�d
i
Tf
�E i, t
1 j
1I
k,k'
Date !
Date h 3
Date

NCS000030
Regional Office Staff Comments

Stormwater Monitoring Data Review - NCS000030 (2005 Renewal)
Permit: NCS000030
Facility: Air Products & Chemicals, Inc.
Reviewer: S. Georgoulias
Receiving Waters: UT to Little Troublesome Creek"
Classification: C-NSW
CMC = Criterion Maximum Concentration
FAV = Final Acute Value
*303(d) listed stream
Benchmarks last updated 5/4/2005 by B. Georgoulias & J. Wynn
Analysis Guidance:
Check for any measured values that equal or exceed benchmark concentration. (Check. maximum value)
Also consider.- are any borderline, or otherwise still considered a pollutant of concern (POQ? Use BPI.
Values are for Freshwater. Check criteria for Saltwater and Human Health Consumption (Lk/Wer Supply) when applicable,
to see if more stringent values are appropriate.
vY'r; �i<
�,3'�r
A�. "rr'_ •t1Et�J' �i 7�} 1�'•.7-
>}�J
i
1? r m
a a
'-r z
.� ';
��.'� �
.7'� a 7 �
ry
Benchmarks
k f i 3ia
,, Cone :
+(
youtfall x'
Y�
w
rjSi �'.
001= a
y
r Max,r
?' ,Y"
y5�
r.. �••
�'�'. aT:
i•. �, -,.+
- z,�, r.: h
�?k
,xUnits
�,� e',; :r• .:.y'.� �.5- G-""5:.;,3"iY...�,�F.rS.�,.. §. .M:' '-r��
g •' i s f ;?
{ ; � .� '1� � t rS No,}' �
-; ry'}. �` t . E�.. i t� .... r4. n•
( b[i. EA �t' "�1,�
w �!3`.N. 74,
4x7 �'� I - 7.<,', er �,. �.x�
t�Ly[,-g:.1 =;. 4*;,. �•,�s,��
. F��
COD
120
25
m I
BPJ, Generally found at levels 4 x (BOD5) in domestic wastewaters.
Nitrate + Nitrite (NO3+NO2)
10
-
mg/I
National Primary Drinking Water Regulation in 40 CFR 141.11 and
15A NCAC 2B for nitrate (Expressed in mg/I of N).
Nitrogen, Total (TN)
30
28.2
m I
TKN + Nitrate + Nitrite Benchmarks (Expressed in m I of N).
Oil and Grease
30
-
m I
BPJ, based on wastewater permit limits.
H (min, max)
6-9
su
Water Quality Standard (Except Sw waters can be as low as 4.3
Phosphorous, Total (TP)
2
0.5
m I
BPJ, based on wastewater permit limits for NSW waters.
TKN (Total K'eldahl Nitrogen)
20
-
m l
BPJ, based on approximate equivalency to secondary treatment of
wastewater. Expressed in m l of N.
TSS
1 100
27
m ]
BPJ, EPA Multi -Sector Permit
5/17/2005 Pagel

Cape Fear River Basin
The
proper technical
conditions do not yet exist to develop TMD7
Assessment
Year
Waterbody and Description Unit (AU)
Class
Subbasln
lmpalredUse
Listed Category and Reason for Listing
Potential Source(s) Miles Acres
Stump Sound (DEH Area) B9
SA ORW
1998
7
145.0
Overall
1, 1998
7
Shellfish harvesting closure:
1. Municipal Point Sources
Fecal Coliform
2, Onsite Wastewater Systems
(Septic Tanks)
Cape Fear River Basin
Waters with impaired biological integrity.
Assessment
Year
Waterbody and Description Unit (AU)
Class
Subbasin
lmpairedUse
Listed Category and Reason for Listing
Potential Source(s) Miles Acres
}law River 16-(1)a
C NSW
30601
2000
6
7.7
From source to SR 2109, Guilford
Overall
1, 2000
6
Impaired biological integrity:
1. Agriculture
stressors not identified
Haw River 16-(1)b
C NSW
30601
2000
6
20.1
From SR 2109 to SR 2426, Guilford
Overall
1. 2000
6
Impaired biological integrity:
1. Agriculture
stressors not identified
Troublesome Creek 16-6-(0,3)
WS-III NSW
30601
2000
6
15.6
From source to Rockingham County SR 2423
Overall
1. 2000
6
Impaired biological integrity:
l Agriculture
stressor study complete
Little Troublesome Creek 16-7a
C NSW
30601
2000
6
3.3
From source to Reidsville WWTP
Overall
1. 2000
6
Impaired biological integrity:
1. Urban Runoff/Storm Sewers
stressor study complete
Little Troublesome Creek 16-7b
C NSW
30601
1998
6
5.0
From Reidsville WWTP to Haw River
Overall
1. 1998
6
Impaired biological integrity:
1. Urban Runoff/Storm Sewers
stressor study complete
2. 1998
4a
Standard violation: Fecal
Coliform
Monday, April 26, 2004 North Carolina 303(d) Impaired Waters List-2004 River Basin: Cape Fear
Page 3 of 112

] _ r
r�/ '7
� 1
f
Name:
No.
Facility Location:
Staff Review and Evaluation
NPDES Stormwater Permit
Contact: Antonio Evans
Air Products and Chemicals
NCS0000030
Air Products and Chemicals
225 Equity Road
Reidsville, NC
Rockingham County
Type of Activity : SIC 2813, Industrial Gases
Receiving Stream Name and Classification: unnamed tributary to Little
Troublesome Creek, C NSW, B20SW _
Proposed Permit Requirements: See attached draft permit
Compliance Schedule: See Part 111, Section A of attached draft permit
Basis for Monitoring Requirements: Recommend continued monitoring for COD
because this parameter is above the cutoff concentration (120 ppm) for last year of
permit. Recommend monitoring for Total Nitrogen and Total Phosphorus because
the receiving stream is NSW. Recommend continued monitoring for TSS to obtain
additional data to definitively rule out future monitoring for this parameter.
Basis for Other Requirements.
NIA
Prepared B VA ,
(Sig ature) (date)
Permits and Engineering Supervisor: Bradley Bennett
(signature)
Response Requested Before:
(with attachments)
(date)
Page 1 of 2

SUMMARY OF MONITORING RESULTS, AIR PRODUCTS
PARAMETERS
UNITS
SAMPLE
DATE
12/17/1994
SAMPLE
DATE
02/17/1999
pH
std.
7.1
6.86
OIL & GREASE
m /l
< 5
8
TOTAL RECOVERABLE LEAD
U Lo
25
< i O
TOTAL SUSPENDED SOLIDS
m /I
12
38
DETERGENTS (MBAS)
m A
0.35
< 0.1
COD
m A
116
142
TOTAL RAINFALL
inches
0.2
0.6
EVENT DURATION
hours
5
22
New Motor oil Usage
al/month
129
72
Flow
MG
0.020386
0:122317
Flow Calculation
Total Runoff Volume (cu. ft.) =total rainfall (ft) x [ (paved area'.90) + (unpaved area x .50) )
"EPA Guidance Manual for the preparation of NPDES Permit Applications for Storm Water Discharges
Page 1

ducts and Chemicals, Inc.
/i,nto,wn,
Hamilton Boulevard
PA 18195-1501
Telephone [phone]
Individual Permit Renewal
Division of Water Quality I WQ Section
Stormwater and General Permits Unit
Post Office Box 29535
Raleigh, North Carolina, 27626-0535
Attn: Tony Evans
12 March 1999
Subject: Stormwater Permit Renewal, Air Products & Chemicals, Inc., Reidsville, NC,
Permit # NCS000030
Dear Mr. Evans;
Enclosed please find the stormw'ater permit renewal package for our facility at 225 Equity Road,
Reidsville, NC. There have not been any significant changes in the industrial activities at the site
since our previous permit application. One change that has occurred is that we no longer store or
use isulfuric acid for.,industrial-wateutreatment'at
The monitoring summary enclosed contains data from 2 monitoring events, the initial monitoring
conducted in 1994 and the recent monitoring in 1999. Our initial monitoring event met the
specified cutoff concentrations and no additional samples were taken until the current year. Also,
we were unable to locate the visual monitoring results for 1995, the results from the.other years are
included in the summary- The monitoring was conducted at outfall 001 as we were granted a
identical outfall exemption and were authorized to sample only that outfall as representative of4y*a
runoff at our site. A copy of that authorization letter is enclosed.=z
kxy
,.�7�cs^"��-._...,--., T=r„r. �-a4�Y?`•�1�
This application and the Stormwater Pollution Prevention Phan eert11716 ton�E been signed by our
Site Manager, David Eberle, as a delegated, authorized representative of the company relating to
the overall responsibility for environmental matters at the site. The Signature delegation was
previously sent to the NCDEHNR, a copy of the submission is enclosed.
If you should have any additional questions or require any additional information regarding this
application, please contact me at [phone] or contact our site manager, Mr. David Eberle at
[phone]. Thank you.
Sincerely,
Damian Marcinek
Environmental Coordinator
GEG Environment, Health & Safety

rth Caroiinc
nt of Environment,
nd Natural Resources
of Environmental Management
, hes B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
:'A. Preston Howard, Jr., P.E., Director
Air Products and Chemicals, Inc.
Attn: Francis-P. Rudy / MC W 1402
7201 Hamilton Blvd.
Allentown, PA 18195-1501
Dear Francis Rudy:
i .
IDEHNF
February 22, 1995
Subject: Request for Identical Outfall Exemption
NCS00030 -
Air Products and Chemicals, Inc.
Rockingham County
Your request to sample the stormwater discharge outfall 001 on your site for"purposes of NPDES
stormwater general permit monitoring requirements has been reviewed by members of the Water Quality
Section staff. Your request described two (2) outfalls of which are associated with substantially'identical
industrial activities and runoff from non -industrial areas.
Based upon staff review of your letter dated January 16, 1995, and attached site map, we have
concluded that the requested determination is warranted and in accordance with Chapter 40 of the Code of
Federal Regulation part 122.21 (g) (7). We authorize you to sample at outfall 001 as stormwater
discharges representative of the runoff from the Air Products and Chemicals, Inc., facility for your
NPDES stormwater general permit monitoring requirements.
If you have any questions concerning this authorization, please contact Steve Ulmer at (919) 733-
5083
cc: Winston-Salem Regional Office
Regional Offices
Sincerely, .
Coleen H. s, P.E.
Supervisor, Permits and Engineering
Asheville Fayetteville 'Mooresville' Raleigh Washington Wilmington Winston-Salem
704/251-6208 919/486-1541 704/663-1699 919n33-2314 919/946-6481 9191395-3900 919/896-7007
Pollution Prevention Pays
P.O. Sox 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

TO
REIDSVILLE FACILITY
►-1 .'
/ F 5T� y
OF ELxxRE A tNA k/TA 5 E APP ATP
P • • X
TORW TO STORM �
Ot< EPA TOR DRAIN
in n NA fiOAD • s i
AIR PRODUCTS GATE l` E SE P R 1
• f • X
• • PI R ER E QA NG •• t �
•
• • • • • • • • •• FIRE • • # � ��, • •
Impervious Su.r1faceS • •• • • DRIVER • HOUSE •
� • • • •
X PARKfdG • • STORK • To • x
Gravel Surfaces . ` • • • • ' ' . • ' •
r r
• • • • DRAIN
a • •• # • BLDG.
• RREIMI-E + • • •
• �r • I •
�R ARGON
• ` • • • • • • RECYCLE COLUMN • •
• • • I • ELEC. • CO►.tP • BOX • •.
o • SUE35TATIOU [� ELECTRt0 L BLDG I -CAT • • x
X * • • • I BLDG.- • EXCHANGER -
• • •• w • +• • M : ! a • ' IRE • •
• �, • ❑ HOUSE
•+ • • • I' AIH • • r • • J
I • • O COMP • AD•
• D-Nx
x ..« • • • �. • • • •
STORM •
• • • • • • • ® DRAIN • • • • + • • • • a
•VF'10RE ` + •• COOLING
.. 7QWERUSE •• A • • • •� r • _ - X
qb
• • • • • • k
x x x
GATE L\�
RT 97 BARNESA ST.
WIN
I

MW N Im
REIDSVILLE FACILITY
�002 Sanitary tool
x x TIRE Ar+i X x x X---x X�l�X X- X
DRUM
LTG -� . PARKING I GATE
8LflG. 7 TRUCK
K GARAGE'
SZORM
. � •� . ' � RAIN l.�X X-----
OI I FIRST AID OFFICE •
I BREAYHr46 AND
X FIRE DIESEL FLIEL APPARMUS SUPPLY 1� I/
I HOUSE TANK — �'
! UY.IP
To
A1R PRODUCTS��
RT W BARNE.5 5T.
F 1 STORM DRAIN TO ` STORM
OL SEPARATOR � � �} DRAIN
OIL /
SC�J,£ - (D, 5EPARA7OR
P17 ( TRAILER LOADING
CONI' AREA
uAINT
BLDG.
FIRE
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PAR"
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QL3Q
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ELEC. CI.Ip BOX
5L19STATION r ELECi[�tCALLDG 1-£AT
I BLDG.'I EXCHANGER LOX
FIRE
HOUSE
PL—&STORM
pG
RW
FIRE ® COOLING
``3 11OU5E TOWER
x —
1>vTFRNAL ROAD
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a
3
4
z
Or
LL'

PERMIT COVERAGE
�( RI NEAVAL APPLICATION FORM Permit Number
Natlonni Pollutant Dlsdiarbe Elimination System NCS000030
Storniwater Discharge Permit
TIIIS AI'PLICA,rION imus,r 1ST: SIGNED AND RETURNED ALONG WITH THE, REQUFSTE.1) 5UPPLEMENTM,
INFORMATION 'TO THE DIV. OF WATEIZ (ZUALITY IN ORDER FOR YOUR FACILITY TO QUALIFY FOR
RIENE«'AL OF YOUR STORNMATER PERMIT NC:S000030
'the followinL, is the information currently in our database fur your facility. Please review this information carefully
and make all corrections as necessary in the space provided to the right of the current information.
OWNER INFORMATION
Owner/Org. Name: AIR PRODUCTS & CHEWCALs tNC
Owner COnMW:
Mailing Address:
Phone NUrnber:
Fax Number
E mail address:
FACILITY INFORMATION
Facility Name. AIR PRODUCTS S CIIEMICALS INC
Facility Contact:
f=aciIiI), Address: 225 EQUITY RI)
REIDSVILLE, NC 27320
Phone Number:
Fax Number
E-mail address:
PERMIT INFORMATION
Permit Contact: DAVIT) V rIIERLE
Mailing Address: 225 EQUITY RD
REIDSVILLE, NC 27321)
Phone Number: 3363-122311
Fax Number:
E-mail address:
DISCHARGE INFORMATION
Discharge Receivin` Water: UT LI1 T'LE'rR()UBLES0NIE C'RELK
Stream Class: C NSW
Basin: CAPE FEAR
Sub -Basin #: 030001
Number of outfalls:
CERTIFICATION
_336-349-2962
_336-342-0408
[e-mail]
336-342--0408
[e-mail]
I certify that I atn familiar with the information contained in the application and that to the hest cif" my knowled!ae and
belief such information is trtte, comple e ind accurate.
0 Si21lalu1e Date October 15_, 2004
M e_V. (Renie) Stack gran Pr — F.H&S
Print or type name of person signing, above Title
Please return this completed renewal application Barra to,
Individual Pernik Renewal
Attn:
Slortnwater and Gencral Permits Unit
1617 Ma [I Service Center
r) I,,; - I, Nr t, f!,..-I',,:, '?7(,99- 1 () 17

STORMWATER POLLUTION PREVENTION PLAN
DEVELOPMENT AND IMPLEMENTATION
CERTIFICATION
N.C. Division of 14 aler Qrralir., Slorl icater and General Permits Umt
Facility Name: AIR PRODUCTS & CHEMICALS INC
Permit Number: NCS000030
Location Address: 225 EQUITY RD
REIDSVILLE. NC 27320
CUUMV: ROCKINGHAM
"1 certify, under penalty of law, that the Stormwater PrrllUtiOn Prevention Plan (SPPP) document and all attachments
were developed and implemented under my direction or Super-visicm in accordance with a system designed to assure
that qualified personnel properly gather and evalualc the information required by the SPPP. Based on my inquiryof
the person or persons who manage the system, or those persons directly responsible for gatherin, the information,
the information gathered is, to the best of my knowiedge and hclief, true, accurate, and complete"
"I certify that the SPPP has been developed, signed and retained at the facility location and the SPPP has been fully
implemented at the named facility location in accordance with the terms and conditions of the stormwater general
hermit."
"I am aware that there are significant penalties ror falsifying inl'()rmation, including the possibility of fines antl
imprisonment fos- knowing violntions"
Sign (according to permit signatory requirements) and return this Certification. DO NOT SENT) THE
S'rORMWATER POLLUTION PREVENTION PLAN ti5'I'I'hl THE CER'I'IIrICA'riON.
Signature
ie V. (Renie) Stack
Print or type name of person signing above
� 1 •.- 11
Manager — EH&S
Title
$ITP Certil-m::idon 2199

SUPPLEMENTAL INFORMATION REQI IREID FOR RENEWAL OF INDIVIDUAL NI'DES
S'C0RN,l11'ATER PERMIT
jjL , copies of each of'the following shall accompany this submittal in order for the application to be
considered complete:
(Do not submit the site S[ormwa(er Pollution Prevention Plan)
�Initial-,
YJ
/' + 1.
A current Site Map from the Stormwater Pollution Prevention Plan. The location Of
industrial activities (including storage of materials, disposal areas. process areas and
loading and unloading areas), drainage structures, drainage areas for each outfal], building
IJ
locations and imper'viuus surfaces should be clearly ne otd.
I
A summary -of Analytical Monitoring results during the term of the existing permit (it* your
hermit required analytical sampling). DO not submit individual lab reports. The summary
can consist of a table including st:ch items as outfall number, parnrrreters sampled, lab
results, date sampled, and storm event data. �r
��y]
'
/ / 3.
A summary of the Visual Monitoring results. Du riot submit individual monitoring= reports.
The summary can consist ol'a table includinb such items :as outf:all number, parasneiers
surveyed, observations, and elate monitoring cunductc;d.
Y
J a.
A summitry of (lie Best Management practices utilized at the permitted facility. Summitry
should consist of a short narrative description of each BMP's in place at the facility. If the
] C
implementation of any BMP's is planned, please include information on these BMP's.
5.
A short narrative describing tiny si1tinifscant chan4zes in industrial activities at the permitted
facility. Significant changes could include the addition or deletion of work processes,
changes in material handlings practices, changes in material storage practices, and/or
]�
changes in the raw materials used by the facility.
G.
Certification of the development and implementation of a Stormwater Pollution Prevention
Ilan for the permitted Facility (Sign and return attached form).
* If the final year analytical nio nitoring of the existing permit term has not been completed
prior to filinU the renewal submittal, then the last years monitoring results should be
submitted within 30 clays of receipt of the laboratory reports. (i.e. do not withhold renewal
submittal waitin�(I Oat lab results)
Representative storm sarnpling may noxv he conducted anytime during the year (the April to
November window has been eliminated} and the representative rainfall event is now
defined as a storm event that measures 4uremer- than 0.1 inches and is preceded by at least 72
hours in which 110 storm event nic.tsuring Urcater than 0.1 inches h,ts c}ccurred.

ask _•fir: } — i` i `��v•�` 1025
u,�„ ✓ .y{ t •r ''-�•/r / -wry
y - ~__�; � �02 �— "'} h A..�. / J W
tan q
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avB a 9T f �n �� i ✓ �� O' I.
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00
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774
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• Lam•■?^�'.q�� i � ��~ �� � _,.•�" �// 940000
�Q s �t° ti • \ FEET
4021
24
�` I' :.� mil- _ _ �. � % � � , �1 • � \I "
\ ---- Se r--
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-�:.- a -��/ _ ad�"�: ��-\ . 1 r.. - _ ..I�Ra>?e�of2_/.'� ., •� •��. l`��-� JLn

O D r. O
o (D G o
S J I 7]
Y _
(3
N
FLOW DIRECTION
C.B. CATCH AA$IN
M.N. MANHOLE
C.G. CLEANOOT
R.C.P. REINFORCED CONCRETE PIPE
V.C.P. VITRIFIED CLAY PIPE
C.M.P. CORRIGATEO METAL PIPE
CAST IRON SOIL PIPE
r111111111=Z STORM SEWER
E _ INOLISTRIAL WASTE & SANITARY SEWER
• 7 ■ MAFARI- SUB DRAINAGE
'SiGNiFICAUT maTERIALS' LISTED IN
WORASHFET B2 OF SPCC.SWP] ROAN
NOTE:
BASE MAP PROVIDED BY APCI
REFERENCE:
I�envlr.r �n r�eG CA S-1G^A-n(rrin OGr�r<rlr�r �` rrl_'�O_�]�
I SITE AND ORAINAGE MAP I
E-NC

Air Products and Chemicals; Inc.
225 Equity Road
Reidsvilie, NC 27320
Permit No.: NCS000030
Analytical Data
Outfall No.
Date Sample
Collected
Total Flow
Chemical
Oxygen
Demand
Total
Nitrogen
Total
Phosporus
Total
Suspended
Solids
001
11/11/2002
0.225
<20.0
0.6
0.17
27
001
2/4/2003
0.153
<20.0
28.2
0.1
15.9
001
5/21 /2003
0.1529
<20.0
3.7
0.5
5.3
001
9/4/2003
0.4077
25
0.9 j
0.1
25.5
Visual Monitoring Summary
Outfall No,
Date
Color
Odor
Clarit
Floating
Solids
Settled
Solids
Suspended
Solids
Foam
Oil Sheen
001
5/12/1999
Clear
None
Clear
None
None
None
None
No
001
4/9/2000
Clear
None
Clear
None
None
None
None
No
001
1218/2000
Clear
None
Clear
None
None
None
None
No
001
4/4/2001
Clear
None
Clear
None
None
None
None
No
001
1019I2001
Clear
None
Clear
None
None
None
None
No
001
4/10/2002
Clear
None
Clear
None
None
None
None
No
001
11/11/2002
Clear
None
Clear
None
None
None
None
No
001
5/12/2003
Clear
None
Clear
None
None
None
None
No
001
Fall 2003
No data in files
001
Sprinq 2004
No data in files
001
8/21/2004
Clear None
Clear
None
None
None
None
No

1.1 BASELINE BEST MANAGEMENT PRACTICES
Baseline BMPs are general practices that apply to most industrial sites, independent of the types
of materials used, processes employed, products manufactured, or site location. Baseline BMPs
are relatively simple, inexpensive, and cost-effective because they emphasize prevention of
pollution rather than treatment cf pollutants. The baseline BMPs listed in Section 8.1 are
employed across the entire facility and are not necessarily associated with any specific source of
significant materials listed in Worksheet B2 of Appendix B.
1.1.1 GOOD HOUSEKEEPING
Good housekeeping involves a common sense approach to improve and maintain a clean and
orderly work environment by implementing the following practices:
• Sweeping parking lots
• Storing chemicals in a neat and orderly manner
Clean up small spills promptly
Regular refuse pickup and disposal
• Good storage and material inventory practices, including labeling of all containers
• Schedule routine cleanup efforts
• Discuss and promote good housekeeping practices with employees
1.1.2 PREVENTIVE MAINTENANCE
A preventive maintenance program is an effective BMP for preventing surface or ground water
pollution. A preventive maintenance program should include:
• Timely inspection and maintenance of storm water management devices (e.g., cleaning
oil/water separators, catch basins, etc.)
Inspection and testing of facility equipment and systems to uncover conditions that could
cause breakdowns or failures resulting in discharges of pollutants to surface water and
ground water (including pipes, pumps, storage tanks and bins, pressure vessels, pressure
release valves, and process and material handling equipment)
• Proper maintenance of facility equipment and systems
1.1.3 RELEASE RESPONSE AND REPORTING PROCEDURES
Effective spill and release response and reporting procedures are important because they provide
for rapid response to mitigate the impact of the release. Release response and reporting
procedures for this facility are described in more detail in Section 9. These procedures describe
the following measures that will be implemented upon discovery of a significant release:
• Access the risk
• Control the release to the extent possible
• Report the release to management and government agencies
• Clean up the impacted area as soon as possible
• Follow up with preventive measures

1.1.4 INSPECTIONS
This facility is required to conduct a formal. documented inspection on a semiannual basis using
a copy of Worksheet B2. inspection criteria is listed in the instructions to Worksheet B2.
In addition to documented inspections, regular observations of process and material storage
areas are encouraged to ensure that spills are detected and responded to as in a timely manner.
Observations can be conducted during employees' regular "rounds" of the facility grounds and
need not be formally documented_
1.1.5 EMPLOYEE TRAINING
Pollution prevention training for employees should be held annually. Training should be
documented in the facility's training database or in employee records located at the facility.
Employees are trained in the following areas:
• Release Prevention, Reporting, and Response - a review of emergency procedures,
communications, reporting and cleanup techniques.
• Pollution Prevention - a review of the purpose and goal of this Plan, potential sources of storm
water pollution at the site, BMPs implemented at the site, and the role employees fulfill in
pollution prevention.
1.1.6 RECORDKEEPING AND INTERNAL REPORTING PROCEDURES
Good recordkeeping and reporting procedures help to identify and communicate information
about potential sources of surface water and ground water contamination and assure that
appropriate measures are taken_ This Plan includes procedures for recording indents, such as
spills or other discharges, along with other information describing the.quality and quantity of
potential pollution sources. Ail pertinent information regarding a spill will be documented and
records maintained for three years. Pollution prevention recordkeeping and reporting are
integrated into current management systems and include:
• The use of the RMS preventive maintenance system, or an equivalent system, for scheduling
applicable preventive maintenance tasks and inspections.
• Required reporting of spills and leaks to Line Management, Facility Environmental
Coordinator, and Corporate EH&S_
The periodic review of significant safety and environmental issues or incidents and corrective
action progress by a Line and Staff Management Safety Committee.
1.1.7 SPILL CLEANUP KITS AND MATERIALS
Spill cleanup kits are maintained at the facility. They are routinely inspected to keep them in good
workinc order. These kits are composed of absorbent sheets, pillows and booms, as appropriate_
In addition, sorbent materials such as oil -dry or vermiculite should be available at all times.
Alkaline neutralizing kits or materials such as soda ash or lime should also be available onsite
from a nearby chemical distributor, for those facilities that use sulfuric acid for cooling water
treatment. Spill cleanup kits or materials are typically maintained within a reasonable distance of
the following areas:
• Truck fueling area
• Truck terminal

• Air Separation Unit (ASU) compressor area/Air Separation Process
• Maintenance buildings or areas
• A dedicated spill kit on each truck tractor
1.1_8 SPILL CLEANUP CONTRACTORS
In the event of a spill, outside assistance for cleanup may be required. Worksheet B4 in Appendix
B lists emergency response contractors located within a reasonable response time from this
facility.
1.1.9 EMERGENCY PREPAREDNESS AND COMMUNICATIONS
This facility shall have a Site Emergency Plan prepared in accordance with GEG EH&S Procedure
01.08.02.A, "Site Emergency Planning". Additionally, GEG EH&S Procedures 01.08.05.A.M.,
"Crisis Management" and 01.08.16.A.M., `HAZWOPER" address emergency preparedness.
These procedures can be found in the GEG EH&S Manual.
1.1.10 SECURITY
This facility is completed surrounded by a security fence. Access to the site is controlled through
a main gate. Entry through this gate can be made only by a security access code or through
permission received from the Control Room. Storage tanks, secondary containment systems,
process areas and piping systems are confined within the fenceline_ The area is lighted and is
subject to typical facility security measures, including restricted vehicular traffic.
1.2 ADVANCED GENERIC BEST MANAGEMENT PRACTICES
Advanced generic BIv1Ps are generic measures or practices that are employed to address specific
sources, materials, or activities that may be present at the facility. They include generic
prevention, containment, and mitigation practices that can be applied to specific sources (e.g.,
fueling stations) commonly found at Air Products industrial gas facilities. Section 8.2 provides a
reference list of generic BMPs that may be used at industrial gas facilities. Those source -specific
BMPs that are actually implemented at this facility, and the locations where they are Implemented,
are listed in Worksheet B2 of Appendix B.
1.2.1 SECONDARY CONTAINMENT
Secondary containment systems are efle0ve in controlling spills. To be most effective,
secondary containment systems and diversionary structures should meet the following standards:
• The systems block possible routes by which spilled materials could reasonably be expected to
flow, migrate, or escape into surface waters or upon the land from within the containment
areas.
• The secondary containment systems have sufficient capacity to contain the largest probable
spill that could occur in the containment area plus an additional capacity to compensate for
anticipated normal accumulation of rainwater.
• The secondary containment system is sufficiently impermeable to contain spilled material for
a duration necessary for the cleanup or recovery of the spilled substance.
• The secondary containment system is routinely inspected for accumulated liquids, debris, or
incompatible materials.

• No transfer area, curbed storage area, or secondary containment system is drained into a
watercourse or public sewage treatment plant unless provision is made to retain, by valves or
other means, any accumulated rainwater until its condition can be determined.
• No incompatible materials are stored within the same containment area.
1.2.2 LOADING AND UNLOADING OPERATIONS
The following measures are key to preventing the release of significant materials during transfer
operations:
• Trainincq - Prevention of the release of materials during transfer operation is accomplished
through implementing procedures discussed during personnel training programs, regular
safety meetings, and briefings.
• Vehicle positioning - Whenever possible, vehicles should be positioned within spill
containment areas during transfer. Positioning near or over storm drains or sewer drains
should be avoided. Wheel blocks and emergency brakes should be used to avoid sudden
movement of the vehicle. if the vehicle is positioned near a traffic corridor, traffic barriers
should be placed to avoid collisions.
• Pre -positioning of spill kits, booms, or sewer block mats - If secondary containment is not
available during loading or unloading, spill mats or 'booms must be readily available or pre -
positioned to seal any nearby catch basins that could lead directly to surface water or sewer
systems.
• Pre -inspection of connections, fittings, and hoses - Prior to each unloading operation,
connections, hoses and fittings should be checked to maker sure they are in good working
condition. Unloading areas should be well illuminated if material transfer occurs at night.
• Dri_o pans - Drip pans or buckets should be used to catch small volume leakage from transfer
hoses or fittings during transfer operations. Captured materials should be reused or properly
disposed.
• Overfill prevention - during a delivery, tank truck operators should be instructed to remain with
the vehicle along with at least one qualified facility employee. Before a delivery, the liquid
level in the receiving tank is checked. Employee training procedures include instructing
operators not to leave the delivery area prior to checking and disconnecting the transfer line.
Prior to material transfer, qualified facility personnel and the driver are instructed to:
♦ Predetermine the maximum volume of material that can be transferred without overfilling
the tank.
♦ Check the liquid level in the tank(s) during transfer to avoid overfilling the tank.
1.2.3 ABOVEGROUND STORAGE TANKS
The following practices should be implemented for aboveground storage tanks:
• All pipes leading to and from aboveground storage tank(s) that enter the tank(s) below liquid
level are equipped with valves sufficiently close to the tank(s) so as to prevent the contents of
a tank from escaping the confines of the secondary containment area in the event of a pipe
rupture outside of the containment area. Any valves that permit the direct outward flow of
tank contents are kept in the closed position when in non -operating or standby status.

• In heavy traffic areas, protective guards should be placed around tanks and piping to prevent
vehicle or forklift damage.
• Tanks, associated valves and piping should be clearly labeled to reduce human error.
• Tanks and associated piping should be routinely inspected for integrity.
1.2.4 FUELING STATIONS
The following practices should be implemented at fueling stations:
• Avoid topping off - To minimize overfilling of truck fuel tanks, special fill procedures must be
followed to ensure that there is adequate room for expansion of cooler diesel fuel drawn from
underground tanks when it is placed in the truck saddle tanks and cryogenic delivery pump
engines- Hot summer weather greatly increases the potential for overflow of vehicle fuel
tanks that have been overfilled. To avoid this condition, the fuel tank should not be filled
above the neck on the fuel tank.
• Avoid unattended filling - When refueling vehicles, the driver should hold the fuel nozzle in
hand during the entire refueling operation, even if the fuel nozzle has an automatic shutoff
device.
• Avoid hosing down- Cleaning the fueling area with running water should be avoided because
the wash water will pick up fuel, oil and grease. Use dry clean-up methods whenever
possible. Control and clean up petroleum spills immediately.
• Keep spill kits accessible - An adequate supply of spill kit materials should be available before
fueling vehicle. Control, report and clean up petroleum spills immediately.
• Minimize storm water run-on - Minimize storm water run-on to the fueling area through flow
diversion around the fueling station and using roofs over the fueling area when feasible.
1.2.5 VEHICLE MAINTENANCE AND REPAIR
Many vehicle and equipment maintenance operations use materials that can be harmtr,l to the
environment. The following practices should be followed at vehicle and equipment maintenance
operations to reduce or eliminate potential sources of pollution:
• Parts washing - Clean without using liquids (e.g., scraper, wire brush) whenever possible. Do
all liquid cleaning at a centralized station so solvents and residues stay in one area.
• Use nontoxic or low toxicity solvents - Minimize the number and volume of hazardous
materials used. Avoid chlorinated solvents. Choose cleaning agents that can be recycled.
• Control leaks and drips - Collect leaking fluids in drip pans. Keep a drip pan under the vehicle
while unclipping hoses, unscrewing filters, or removing parts. Control leaks from wrecked or
damaged equipment that may be stored outdoors. Promptly transfer used fluids to proper
waste or recycling containers. Do not leave full drip pans lying around.
• Drain oil filters - Used oil fitters disposed of in trash cans can leak oil and contaminate surface
water. Place used oil filters in a funnel over the waste oil recycling or disposal collection tank
to drain excess oil before disposal. Whenever possible, crush and recycle oil filters.

Never pour licluid wastes into drains or onto the ground - Do not pour liquid waste to floor
drains, sinks, outdoor storm drains, or sewer connections_
• Recycle materials - Whenever possible, recycle degreasers, used oil and oil filters, antifreeze,
cleaning solutions, automotive batteries, hydraulic fluid and tires -
Segregate and label wastes - Separating wastes allows easier recycling and may reduce
treatment costs. Locate waste and recycling containers in clearly marked and controlled
areas.
1.2.6 VEHICLE AND EQUIPMENT WASHING
Washing vehicles and equipment outdoors or in areas where washwater can flow onto the ground
can pollute surface or ground waters. Washwater can contain high concentrations of oil and
grease, phosphates, and suspended solids. To reduce or eliminate these potential sources of
pollution_
• Use designated cleaning areas only. Washwater is regulated as a process wastewater. It
can only be discharged to a properly permitted sanitary sewer or process sewer line.
• If a permitted sewer line is not available, washwater should be collected in bermed areas or
sumps for offsite disposal.
• As an alternative, offsite commercial washing facilities can be used
1.2.7 WASTE MANAGEMENT AREAS
Wastes spilled, leaked or lost from waste management areas may build up in soils or be carried
away by rainfall. To reduce the potential for pollution, the following practices should be
implemented:
• Minimize the amount of waste managed on -site.
• Prevent run-off and run-on from contacting waste management areas.
• Keep waste containers closed or securely covered.
1.2.8 TRANSFORMERS
The following practices should be implemented in transformer yard areas:
• Transformers should be inspected periodically for evidence of leaks.
• Leaks should be cleaned up as soon as possible.
• Adequate spill kit materials should be available to prevent a leak from reaching a waterway.
1.2.9 OIIJWATER SEPARATORS
The following practices should be implemented to assure proper operation of an oil/water
separator unit:
• The level of oil captured in the unit should be routinely monitored and removed by a properly
permitted used oil vendor.
• Any associated oil skimmers should be checked for proper operation.

• The wastewater effluent from the unit should be routinely observed or monitored to determine
i# the unit is functioning properly.
• The unit should be periodically cleaned to remove accumulated solids on the bottom of the
unit and on any coalescing plates.
• Spills and leaks should be cleaned up as soon as possible.
• The discharge of solids and detergents to the oillwater separator should be minimized.
1.2.10 GREASE TRAPS AND GRIT CHAMBERS
The following practices should be implemented to assure proper operation of grease traps and grif
chambers:
• The levels of accumulated oil and solids should be routinely monitored and removed for
proper disposal.
• Any associated oil skimmers should be checked for proper operation.
• The wastewater effluent from the unit should be routinely observed or monitored to determine
if the unit is functioning properly.
• Spills and leaks should be cleaned up as soon as possible.
1.2.11 CHLORINE CYLINDERS
The chlorine handling practices and emergency response procedures found in the Site
Emergency flan should be followed.
1.2.12 DRUM AND CONTAINER STORAGE AREAS
The following practices should be implemented at drum and container ("drums") storage areas:
• The contents of alt drums should be properly identified by a label.
• Drums that are stored in a horizontal position must be tightly sealed to avoid seepage through
the bung. Drip pans should be placed beneath horizontal drums that have a dispensing valve
installed.
* Drums should be kept closed except when material is being added or withdrawn.
• For drums stored outdoors, drums caps should be used if accumulated rain water on the top
lip of the drum can cause contamination of the product. Outdoor drums should be stored off
of the ground to prevent bottom corrosion and possible leakage from the drum. Wooden
pallets may be used if an impervious surface is not available.
• Drums should be neatly stored with sufficient access and aisle space.
• Because empty drums often contain residual product, they should be managed according to
the practices listed above, uniess they have been thoroughly cleaned.

• Leaking drums should be immediately moved to a containment area, placed in a salvage
drum, plugged, or the contents transferred into another drum. Spilled product should be
cleaned up immediately.
1.2.13 SEDIMENT AND EROSION PREVENTION
The following practices should be implemented in areas of high soil erosion potential or during
construction periods:
• Preserve existing vegetation or revegetate disturbed soil areas.
• Stabilize stream banks.
• Install interceptor dikes and swales.
• Use fabric filter fences around disturbed areas.
• Maintain storm water retention/detention ponds in good operating condition.
1.2.14 SARA 313 WATER PRIORITY CHEMICALS
Facilities subject to reporting under SARA Section 313 for water priority chemicals may be
required to implement special BMPs for storm water pollution prevention. Any applicable, special
BMPs are further described in Sections 10.5.2 through 10.5.7. They must be implemented in
areas where storm water can come in contact with SARA Section 313 water priority chemicals.
1.3 ADVANCED SITE -SPECIFIC BEST MANAGEMENT PRACTICES
Advanced site -specific BMPs are measures or practices that are implemented at specific
locations at this facility, They include such BMPs as oiVwater separators or underground storage
tank leak detection monitoring. Site -specific BMPs implemented at this faciiity are described in
Section 8.3 and the locations where they are implemented are identified in Worksheet 132 of
Appendix B.
1.3.1 TRUCK FUEL/HEATING OIL UNDERGROUND STORAGE TANK SYSTEM;USED OIL
ABOVEGROUND STORAGE TANK
The truck fuel underground storage tank system consists of two 10,000-gallon diesel fuel
underground storage tanks (USTs), submersible pumps with underground pressurized piping,
leak detection system, spill and overfill prevention devices, and an associated fuel dispensing
island. The tanks were installed in 1992. The Heating oil tank was installed in 1992 and is a 2500
gallon UST with a submersible pump with pressurized piping.
Fuel releases to groundwater or surface waters may occur through the leaking of the underground
tanks or underground piping system, or during fuel transfer at the fuel island, and possibly during
fuel vendor deliveries. The underground tank system is equipped with the following features to
prevent such leaks or spills.
• Corrosion protection
• Leak detection for tank and piping
• Spill and overfill control
• Automatic line leak flow restrictor
The ATG is a Veeder-Root TLS-350 equipped with a continuous statistical leak detection (CSLD)
tank level monitoring system. The system includes a sensing probe in the tank and a remote

monitor with printer. The system provides continuous monitoring of product level, water level, and
product temperature. Whenever the fueling system is idle, the TLS-350 collects data and
performs a statistical analysis to detect leaks as small as 0.2 gallons per hour. There is no need
to shut down the fueling system for the leak detection test. Leak tests are constantly being
performed, and test results are automatically provided every 24-hour period, or on demand from
the console printer.
The red jacket pump for the diesel oil system is equipped with an automatic line leak detector flow
restrictor that dramatically cuts the flow through the piping when the unit senses a leak. The
double walled fiberglass piping has an interstitial leak detection monitor in the form of a piping
sensor_
To prevent surface spills and tank overfills, each tank is equipped with a catchment basin, overfill
alarm, and automatic shutoff device.
The catchment basin is an OPW 1 Spill Container with 5 gallons capacity. A manual drain in the
spill container can be used to drain spilled product back into the tank. tt water is present, the spill
container will be manually bailed out.in addition to serving as a leak detection device, the Veeder-
Root TLS-350 level monitor also serves as a high level alarm. A red alarm light is remotely
mounted at the fueling island to indicate an overfill condition.
An OPW 61-SO two -stage overfill prevention valve serves as both an overfill alarm and automatic
shutoff device. The first stage alerts the transfer cperator by reducing the flow rate to
approximately 2 to 5 gallons per minute through a bypass valve. The second stage will
completely cut off flow inlo the tank by closing the bypass valve if the level approaches a critical
overfill condition. The valve resets itself when the tank level drops below the critical level.
Any spills that occur on the concrete fueling station pad drain to the 14.50 Oil/Water Separator
where the spilled product is captured and can be removed.
The fuel dispenser is mounted on a Total Containment dispenser sump to coniain any spills or
leaks from the dispenser or associated piping. It serves as a termination point for the double -
walled fiberglass piping from the submersible sump pump to the fuel dispenser.
There is a 375 gallon double wall aboveground storage tank for temporary storage of used motor
oil from the rouline maintenance of the truck ileet. This tank is located outdoors at the west end
of truck garage bay. This tank was installed in 1992.
1.3.2 OILY WATER CONTROL SYSTEM
1.3.2.1 POLLUTANT SOURCES
Contaminated rainwater run-off from the foundations of the following equipment discharges to the
oil/water separator for treatment prior to discharge from the facility:
• Truck Fueling Station (See Section 8.3.1)
• 01,10 Main Air Compressor, Motor, Lube Oil System (600 gals.)
01.30 Nitrogen Make-up Compressor, Motor, Lube Oil Systern (300 gals.)
• 01,40 Nitrogen Recycle Compressor, Motor, Lube Oil System (1,200 gals.)
In addition, the washwater from the truck wash area (1,170 square feet) is collected and
discharges to the oil/water separator. Any oil or grease picked up by the washwater would be
removed in the oillwater separalor before discharging to the sanitary sewer for off -site
treatment.

1.3.2.2 01LAVATER SEPARATOR
The oillwater separator is designed to handle 100 gallons per minute (gpm) of wastewater
flow. The oil/water separator has a maximum oil storage capacity of 2,500 gallons and will act
as a containment device to capture accidental oil spills and/or leakage occurring at the
equipment. After oil is removed in the oil/water separator, the effluent is discharged to the
sanitary sewer,
The oil/water separator is installed underground inside a concrete vault. This vault serves as
a secondary containment device to capture any oil spill or leakage from the separator. Any
leakage from the unit is unlikely. In the event of a small leakage into the concrete vault,
sorbent materials shall be used to clean up the oil. The concrete vault should be monitored
weekly to check for any leakage of oil.
Oil will periodically be removed from the side -oil storage reservoir for proper disposal in
compliance with environmental regulations. Any small spills related to a waste oil vendor
pumping the stored oil from the oil/water separator would be cleaned up using sorbent
materials. A large spill could be prevented from reaching a storm drain through the use of oil
booms.
1.3.3 COOLING WATER TREATMENT BUILDING
A small building adjacent to the cooling tower houses a small tank and drums of water treatment
chemicals. Floor drains which lead to the sanitary sewer should be plugged under normal
conditions. Major spills of water treatment chemicals should be recovered and reused in the
cooling tower.

Air Products and Chemicals, Inc.
225 Equity Road
Rockingham. County
Reidsville, North Carolina 27320
NCS 000030
Air Products and Chemicals, Inc. (APCI) is a major international supplier of
industrial gases, chemicals and technology. The Reidsville, North Carolina
facility, consists of an air separation plant and a truck terminal that is located in
the Watlington Industrial Park on Equity Road in the City of Reidsville, NC. This
facility began operation in 1978 and today produces greater than 300 tons/day of
liquid nitrogen, oxygen and argon by separation of these gases from the
atmosphere.
The industrial gas manufacturing process includes compressing and liquefying the
incoming air stream, and then distilling the liquefied air into its principal
components: oxygen, nitrogen and argon. The equipment used in the air
separation process includes compressors and expanders, heat exchangers, a
distillation column (cold box), and other miscellaneous equipment.
There have been no significant changes to the plant or any changes in raw
materials used at this facility since the last permit submission.

NCS000030
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
ul
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by�he�North Carolina Environmental
Management Commission, and the Federal Water Pollution Control Act, as amended,
Air Products and':Chemicals, Incorporated
is hereby authorized to dischargestormwaterfrom a facility located at
19' and Chemicals, Incorporated
2`25 Equity Road
Reidsville, NC
Rockingham County
to receiving waters designated as an unnamed tributary (UT) to Little Troublesome Creek, a class
C-NSW stream in the Cape Fear River Basin, in accordance with the discharge limitations,
monitoring requirements, and other conditions set forth in Parts 1, 11, III, IV, V and VI hereof.
Note: Draft Permit Dates are Approximate
This permit shall become effective November 1, 2005.
This permit and the authorization to discharge shall expire at midnight on October 31, 2010.
Signed this day October 10, 2005.
for Alan W. Klimek, P.E., Director
Division of Water Quality
By the Authority of the Environmental Management Commission

Permit No. NCS000030
TABLE OF CONTENTS
PART I INTRODUCTION
Section A: Individual Permit Coverage
Section B: Permitted Activities
Section C
PART II
Section A
Section B
Section C
Section D:
PART III
Section A:
Location I
MONITORIN
DISCHARGE
Stormwate
Analytical
Qualitative
On -Site V,
STANDARD
Compliance and Liability
1. Compliance Schedule
2. Duty to Comply
3. Duty to Mitigate
4. Civil and Criminal Liability
5. Oil and Hazardous Substance Liability
6. Property Rights
7. Severability
8. Duty to Provide Information
9. Penalties for Tampering
10. Penalties for Falsification of Reports
Section B: General Conditions
1. Individual Permit Expiration
2. Transfers
PERMITTED

Permit No. NCS000030
3. Signatory Requirements
4. Individual Permit Modification, Revocation and Reissuance, or
Termination
5. Permit Actions
Section C: Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D: Monitoring and Records
1.
Representative Sampling
2.
Recording Results
3.
Flow Measurements -'
4.
Test Procedures
5.
Representative 0u fall '�.
b.
RecordsReten[1on
an try
7.
Inspectia +E
Section E: Reporting
Requirements
.If
L
Dis arge, Reports
2.
Submitting Reports
3.
Availability of Reports
4.
Non-Stormwater Discharges
5.
Planned Changes
G.
Anticipated Noncompliance
7.
Bypass
8.
Twenty-four Hour Reporting
9.
Other Noncompliance
10,
Other Information
PART IV LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
PART VI DEFINITIONS
11

Permit No. NCS000030
PART I INTRODUCTION
SECTION A: INDIVIDUAL PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified in this permit.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the
stormwater to the surface waters of North Carolina oy
been adequately treated and managed in accordance wi
individual permit. All discharges shall be in accordance
Any other point source discharge to surface
allowable non-stormwater discharge or is cc
errrutteeis authorized to discharge
pa at storm sewer system which has
,the emis•and conditions of this
r . N_
with the conditions of this permit.
t\
is prohibited unless it is an
permit, authorization or approval.
This permit does not relieve the permitteef,romirespronsibility for compliance with any other
applicable federal, state, or local,law, rule;j.standard, ordinance, order, judgment, or decree.
Part I Page I of 2

SECTION C: LOCATION MAP Permit No, NCS000030
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Latitude: 36'19'50" pp., 7mFV,-X
Longitude: 79'40'00" NCS000030 Facility a
County: Rockingham Air Products & Location
Stream Class: C-NSW Chemicals, Inc.
Receiving Stream: UT to Little Troublesome Creek P
Sub -basin: 03-06-01 (Cape Fear River Basin) rxottA ICALI 1:24,000
Part I Page 2 of 2

Permit No. NCS000030
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR
PERMITTED DISCHARGES
SECTION A: STORMWATER POLLUTION PREVENTION PLAN
The permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as
the Plan. This Plan shall be considered public information in accordance with Part III, Standard
Conditions, Section E, Paragraph 3 of this individual permit. The Plan shall include, at a
minimum, the following items:
Site Plan. The site plan shall provide a description of tth.S physical facility and the
potential pollutant sources which may be expected tocontribute to contamination of
stormwater discharges. The site plan shall contain the`following:
a. A general location map (USGS quadranglb,map or appropriately drafted
equivalent map), showing the facility's location in relation to transportation
411
routes and surface waters, the narne:of,the receiving water(s) to which the
stormwater outfall(s) discharge orb f`tie discharge is to a municipal separate
storm sewer system, the nam Yof�thelmunicipality and the ultimate receiving
waters; and accurate latitude andlonfgitude of the point(s) of discharge.
_u
b. A narrative descriptit0off stooge practices, loading and unloading activities,
outdoor process areas, dustjor particulate generating or control processes, and
waste disposal,rpractices
C. A site map drawn�to-§dale with the following items:
(1)
Distance legend and north arrow
(2)
Location of industrial activities (including storage of materials,
disposal areas, process areas and loading and unloading areas)
(3)
Drainage structures
(4)
Delineated drainage areas for each outfall
(5)
Drainage area for each outfall in acres and percentage of
each drainage area that is impervious
(b)
Building locations
(7)
Existing BMPs and impervious surfaces
(8)
For each outfall, a narrative description of the potential pollutants that
could be expected to be present in the stormwater discharge.
d. A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
C. Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part III, Standard Conditions, Section
B, Paragraph 3.
Part I1 Page I of 7

Permit No. NCS000030
2. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed which control or
minimize the exposure of significant materials to stormwater, including structural and
nonstructural measures. The stormwater management plan, at a minimum, shall
incorporate the following:
Feasibility Study. A review of the technical and economic feasibility of changing
the methods of operations and/or storage practices to eliminate or reduce exposure
of materials and processes to stormwater. Wherever practical, the permittee shall
prevent exposure of all storage areas, material handling operations, and
manufacturing or fueling operations. In areas where elimination of exposure is
not practical, the stormwater management plan hAl document the feasibility of
NY
diverting the stormwater runoff away from areas -of potential contamination.
b. Secondary Containment Schedule. A 'sdhd'dule to provide secondary containment
for bulk storage of liquid materials, storm of Section 313 of Title III of the
Superfund Amendments and Reauthgrizatibn Act (SARA) water priority
chemicals, or storage of hazardou s su Thnc s to prevent leaks and spills from
contaminating stormwater runoff. If thejsecondary containment devices are
Z.4 & d
connected directly to stormwater conveyance systems, the connection shall be
I #i Atg?
controlled by manually acti;vatedvalves or other similar devices [which shall be
�' 1 V2�1i � �A
secured with a locking,mechanism] and any stormwater that accumulates in the
Nl �
containment area shallxbe,at a runimum visually observed for color, foam, outfali
staining, visible sheens an&dry weather flow, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated by theAmaterial stored within the containment area. Records
documentingtth,�e �d viduai making the observation, the description of the
accumulated stormwater and the date and time of the release shall be kept for a
period of five years.
C. BMP Summary. A narrative description shall be provided of Best Management
Practices (BMPs) to be considered such as, but not limited to, oil and grease
separation, debris control, vegetative filter strips, infiltration and stormwater
detention or retention, where necessary. The need for structural BMPs shall be
based on the assessment of potential of sources to contribute significant quantities
of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or team) responsible for implementing the
SPRP shall be identified. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater runoff through spills or
exposure of materials associated with the facility operations. The SPRP must be site
stormwater specific. Therefore, a SPCC plan may be a component of the SPRP, but may
not be sufficient to completely address the stormwater aspects of the SPRP. The common
elements of the SPCC with the SPRP may be incorporated by reference into the SPRP.
Part It Page 2 of 7

Permit No. NCS000030
4. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance program shall be developed. The program shall document schedules of
inspections and maintenance activities of stormwater control systems, plant equipment
and systems. Inspection of material handling areas and regular cleaning schedules of
these areas shall be incorporated into the program.
5. Employee Training. Training schedules shall be developed and training provided at a
minimum on an annual basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
operations that have the potential to contaminate stormwater runoff. Facility personnel
(or team) responsible for implementing the training shall be identified.
6. Responsible Party. The Stormwater Pollution Pteventtlan shall identify a specific
position(s) responsible for the overall coordinationdevelopment, implementation, and
revision to the Plan. Responsibilities for all componentsof the Plan shall be documented
and position assignments provided.
7. Plan Amendment. The permittee shall amend the,Plan whenever there is a change in
design, construction, operation, or mai�enance which has a significant effect on the
Potential for the discharge of polluta is ta�surface waters. The Stormwater Pollution
Prevention Plan shall be reviewed�and uud`ai:ed on an annual basis.
The Director may notify th�eIt""— ' e when the Plan does not meet one or more of the
minimum requirements df the pehrmtt. Within 30 days of such notice, the permttee shall
submit a time scheduleto the Director for modifying the Plan to meet minimum
requirements. The permittee sliall provide certification in writing (in accordance with
t �,- -
Part III, Standard Cond tons, Section B, Paragraph 3) to the Director that the changes
have been made.
8. Facility Inspection Program. Facilities are required to inspect all stormwater systems on
at least a semiannual schedule, once in the fall (September -November) and once in the
spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date and time of inspection, individual(s)
making the inspection and a narrative description of the facility's stormwater control
systems, plant equipment and systems. Records of these inspections shall be
incorporated into the Stormwater Pollution Prevention Plan.
Stormwater discharge characteristic monitoring as required in Part I1 of this permit shall
be performed in addition to facility inspections.
9. Implementation. The pernttee shall document all monitoring, measurements,
inspections and maintenance activities and training provided to employees, including the
log of the sampling data and of activities taken to implement BMPs associated with the
industrial activities, including vehicle maintenance activities. Such documentation shall
be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
Part IL Page 3 of 7

Permit No. NCS000030
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater subject to the provisions of this permit.
Analytical monitoring of stormwater discharges shall be performed as specified below in Table
1.
All analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of nine analytical samplings being conducted over the term
of the permit at each stormwater discharge outfall (SDO). The permittee shall complete the
minimum nine analytical samplings in accordance with the schedule specified below in Table 2.
Monitoring results shall be compared to the benchmark vvalues,in�able 3. The benchmark
values in Table 3 are not permit limits but should be used aslguidelines,for the permittee's
Stormwater Pollution Prevention Plan (SPPP). The permittee slali;evaluate the sources of any
benchmark exceedances and evaluate the effectiveness- site BMPs. The permittee shall
review and/or update the SPPP and document any efforts%tdress stormwater contamination.
Table 1. Analytical Monitoring Requirements"rt
`= Discharge P
f�
m Measurement Ei'equeiicyl
SampleSample'
�
Cha>racteristicsTriits?
Location3
��;
: Typez
:_
Chemical Oxygen Demand
Semi-annuall y
Grab
SDO
Total Nitrogen
�j
Semi-annually
Grab
SDO
Total Rainfall
inched
Semi -Annually
Rainfall Event Duration
,minutes
Semi -Annually
Footnotes:
I Measurement Frequency: All analytical monitoring will be performed twice per year, once in the spring (April -
June) and once in the fall (September - November). See Table 2 for schedule of monitoring periods.
2 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. If the detention pond discharges only in response
to a storm event exceeding a ten year design storm, then no analytical monitoring is required and only qualitative
monitoring shall be performed.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative
outfall status has been granted.
4 If all COD values are below the benchmark value in Table 3 of this section after at least four samples have been
collected, the Permittee may discontinue monitoring for this parameter.
Part 11 Page 4 of 7

Permit No. NCS000030
Table 2. Monitoring Schedule
�ylVlonrtoring peiriod'
Sample:Number
Start;
Year 1 Fall. `�` �,
See Footnote 2
September 1,�2005
No embei 30, 2005
Year 1 — Spring
1
April 1, 2006
June 30, 2006
Year 2 — Fall
2
September 1, 2006
November 30, 2006
Year 2 — Spring
3
April 1, 2007
June 30, 2007
Year 3 — Fall
4
September 1, 2007
November 30, 2007
Year 3 — Spring
5
April 1, 2008
June 30, 2008
Year 4 — Fall
6
September 1, 2008
November 30, 2008
Year 4 — Spring
7
April 1, 2009,E
June 30, 2009
Year 5 — Fall
8
September fi',V 09
November 30, 2009
Year 5 —Spring
9
April 1,�2010
June 30, 2010
Footnotes:
1 Maintain semi-annual monitoring during permit renewal
2 If unable to sample a representative storm event prior to
following spring_ .z
Table 3. Benchmark Values for
Om
2005, may begin sampling schedule the
;Disci arge W- Aracterist cs
w4rY ` Un" is '
: r ` �Beiicti'mark
, Sr
Chemical Oxygen Demand
0 ;m 1v
120
Total Nitrogen
m /l
30
This site discharges to impaired waters experiencing problems with fecal coliform and unpaired
biological integrity, and to waters upstream of the Haw River Arm of the Jordan Reservoir,
experiencing problems with nutrients and chlorophyll a violations (indicative of excessive
nutrient loads). A Total Maximum Daily Load (TMDL) for fecal coliform was approved in May
2002 for Little Troublesome Creek, but the Permittee was not allocated a load for stormwater
discharge and is not required to monitor for fecal coliform at this time.
If additional TMDLs are approved for this segment of Little Troublesome Creek, the Permittee
may be required to monitor for the pollutant(s) of concern in the future and submit results to the
Division of Water Quality. The Division will consider the monitoring results in determining
whether additional BMPs are needed to control the pollutant(s) of concern to the maximum
extent practicable.
If additional BMPs are needed to achieve the required level of control, the Permittee will be
required to (1) develop a strategy for implementing appropriate BMPs, and (2) submit a
timetable for incorporation of those BMPs into the permitted Stormwater Pollution Prevention
Plan.
Part 11 Page 5 of 7

Permit No. NCS000030
SECTION C: QUALITATIVE MONITORING REQUIREMENTS
Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified below in Table 4. Qualitative
monitoring is for the purpose of evaluating the effectiveness of the Stormwater Pollution
Prevention Plan (SPPP) and assessing new sources of stormwater pollution. No analytical tests
are required. Qualitative monitoring of stormwater outfalls is performed when stormwater
discharge occurs but does not need to be performed during a representative storm event.
In the event an atypical condition is noted at a stormwater discharge outfall, the Perrnittee shall
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the Stormwater Pollution Prevention
Plan. A Z
All qualitative monitoring will be performed twice per year, once in -the spring (April - June) and
once in the fall (September - November).
v- 1%
Table 4. Qualitative Monitoring Requirements
Discharge Characteristics
_' �Frequency�,-,
Monitoring.
f1 y-�G A �"-� `?.
�- •y4
1 • #- to ..
I:ocationl
K..es
Color
Semi-annuall
SDO
Odor
5i "mtjannualr
SDO
.
Clarity
�Se fitially
SDO
-
Floating Solids
Semi -annuall
SDO
Suspended Solids
Semi annually
SDO
Foam
Semi-annually
SDO
Oil Sheen
Semi-annually
SDO
Other obvious indicators
SDO
m of stormwater pollution
Semi-annually
Footnotes:
I Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO)
regardless of representative outfall status.
SECTION D: ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
Facilities which have any vehicle maintenance activity occurring on -site which uses more than
55 gallons of new motor oil per month when averaged over the calendar year shall perform
analytical monitoring as specified below in Table 5. This monitoring shall be performed at all
outfalls which discharge stormwater runoff from vehicle maintenance areas.
All analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of nine analytical samplings being conducted over the term
of the permit at each stormwater discharge outfall (SDO) which discharges stormwater runoff
Part 11 Page 6 of 7

Permit No. NCS000030
from vehicle maintenance areas. The permittee shall complete the minimum nine analytical
samplings in accordance with the schedule specified in Table 2 (Section B).
Monitoring results shall be compared to the benchmark values in Table 6. The benchmark
values in Table 6 are not permit limits but should be used as guidelines for the permittee's
Stormwater Pollution Prevention Plan (SPPP). The permittee shall evaluate the sources of any
benchmark exceedances and evaluate the effectiveness of any site BMPs. The permittee shall
review and/or update the SPPP and document any efforts to address stormwater contamination.
Table 5. Analytical Monitoring Requirements for On -Site Vehicle Maintenance
Yy i r'
Discha((rge"Charla'cteristtcs
meµ. r_ i •r d.-�
'� Units'
'i Y "�?.,$3 T..+r -
' Measurement
l
Sample
a; ^ : 4�,
SaR�nple
�'"t In#:_Ri 31 yly a
FrequencY.]Location4.
3
_�'+sy, -.� ��.�
Q y � :
H
standard
Serniin -anua�.11y.,
Grab
SDO
Oil and Grease
mg/1
Semi-annualiy!Grab
awcw .ter
SDO
Total suspended Solids
m 1
Semr:=annually
Grab
SDO
New Motor Oil Usagegallons/month
Semi-annually
Estimate
-
Rainfall
inches
nnual]
Sa
YTotal
-
-
ae W'
Rainfall Event Duration
minutes
emt�annuaIly
Footnotes: � �: �-- 4..
1 Measurement Frequency: All analytical m'' �
onitoring wiII be performed twice per year, once in the spring (April -
'0_ -; - .
June) and once in the fall (September - November). See Table 2 (Section B) for schedule of monitoring periods.
2 If the stormwater runoff is con]
pond shall be collected within i
to a storm event exceeding a to
monitoring shall be performed.
by a 5formwater detention pond, a grab sample of the discharge from the
[_Amr inutes of discharge. If the detention pond discharges only in response
design storm, then no analytical monitoring is required and only qualitative
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle maintenance activities occur.
Table 6. Benchmark Values for Vehicle Maintenance Analytical Monitoring
nDtscharge_Characteristfcs
xev
,Unitsn'
Benchmark
Total Suspended Solids
mg/1
100
OiI and Grease
mg/1
30
PH
standard
6-9
Part II Page 7 of 7

Permit No. NCS0000 30
PART III STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented within
12 months of the effective date of the initial permit and updated thereafter on an annual basis. Secondary
containment, as specified in Part II, Section A, Paragraph 2(b) of this permit, shall be accomplished within
12 months of the effective date of the initial permit issuance. Aty
Proposed Facilities: The Stormwater Pollution Preveni
the beginning of discharges from the operation of the i
annual basis. Secondary containment, as specified in I
be accomplished prior to the beginning of discharges 1
2. Duty to Com Iv
tn`shall+be developed and implemented prior to
al activity-and5be updated thereafter on an
Section A Paragraph 2(b) of this permit shall
1;9peration of the industrial activity.
The permittee must comply with all conditions of this individual permit. Any permit noncompliance
it
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuanceZo�r,modiftcation; or denial of a permit upon renewal application.
a. The permittee shall comply" it standards or prohibitions established under section 307{a} of the
� - , �"-�.
Clean Water Act fo�toxic pollutants within the time provided in the regulations that establish these
standards or prohibitions, even if the permit has not yet been modified to incorporate the
requirement. t-1
b. The Clean Water`Act`pFovides that any person who violates a permit condition is subject to a civil
penalty not to exceed $27,500 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than 1 year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed an administrative penalty not to exceed $11,000 per violation with the maximum
amount not to exceed $137,500. [Ref: Section 309 of the Federal Act 33 USC 1319 and 40 CFR
122.41 (a).]
Under state law, a daily civil penalty of not more than twenty-five thousand dollars ($25,000) per
violation may be assessed against any person who violates or fails to act in accordance with the
terms, conditions, or requirements of a permit. [Ref: North Carolina General Statutes 143-
215.6A]
d. Any person may be assessed an administrative penalty by the Director for violating section 301,
302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing any
of such sections in a permit issued under section 402 of the Act. Administrative penalties for Class
I violations are not to exceed $11,000 per violation, with the maximum amount of any Class I
penalty assessed not to exceed $27,500. Penalties for Class II violations are not to exceed $11,000
per day for each day during which the violation continues, with the maximum amount of any Class
It penalty not to exceed $137,500.
Part III Page 1 of 8

Permit No. NCS000030
Duty to Miti agate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the environment.
4. Civil and Criminal Liability
Except as provided in Part III, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6A, 143-215.613, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to
the permittee from any responsibilities, liabilities, or p
under NCGS 143-215.75 et seq. or Section 311 of the I
6. Property Rights
e theiifistituOn of any legal action or relieve
to which=the permittee is or may be subject to
tct, 33 USC 1321.
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor do Aalthor`ize any injury to private property or any invasion of
personal rights, nor any infringement of Rderal., s0te or local laws or regulations.
�o
7. Severability_
Z
The provisions of this individual permit'dre severable, and if any provision of this individual permit, or the
Je
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other c_tances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall furnish to the Director, within a reasonable time, any information which the Director
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit. The
permittee shall also furnish to the Director upon request, copies of records required to be kept by this
individual permit.
Penalties for Tamperine
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate,
any monitoring device or method required to be maintained under this individual permit shall, upon
conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more
than two years per violation, or by both. If a conviction of a person is for a violation committed after a first
conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per day of
violation, or by imprisonment of not more than 4 years, or both.
to. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this individual
Part III Page 2 of 8

Permit No. NCS000030
permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years
per violation, or by both.
SECTION B: GENERAL CONDITIONS
Individual Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the permittee shall submit forms and fees as are
required by the agency authorized to issue permits no later than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at IeW 180 days prior to expiration, will be
subjected to enforcement procedures as provided in NCGS § 143�2153.6 and 33 USC 1251 et. seq.
2. Transfers
This permit is not transferable to any person except aftefriotice to and approval by the Director. The
Director may require modification or revocation and.reissuance,of.the permit to change the name and
incorporate such other requirements as may be necessai=y rind r-the Clean Water Act. Permittee is required
to notify the Division in writing in the event the$ceer"ittal,,fac lity is sold or closed.
Signatory Requirementsy/
t', YS
All applications, reports, or information submitted to the Director shall be signed and certified.
All applications to be'covered;under this individual permit shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
;,.
responsible, corporate officer means: (a) a president, secretary, treasurer or vice president
of the co poration in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the
manager of one or more manufacturing production or operating facilities employing more
than 250 persons or having gross annual sales or expenditures exceeding 25 million (in
second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
Part III Page 3 of 8

Permit No. NCS000030
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
Any person signing a document under paragraphs a. or b. of this'section shall make the following
certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties,for submitting false information,
including the possibility of fines and imprisonment for?ltrtowmg violations."
4. Individual Permit
The issuance of this individual permit does not prohibit,ifie Dirrecctor from reopening and modifying the
individual permit, revoking and reissuing the individual,permtt; or terminating the individual permit as
allowed by the laws, rules, and regulations contained,in Title 40, Cade of Federal Regulations, Parts 122
and 123; Title 15A of the North Carolina Admiiiistrative,Cod' Subchapter 2H .0100; and North Carolina
General Statute 143-215.1 et. al.
Permit Actions
The permit may be mo
changes or anticipated
SECTION C: OPERATION i
Proper Operation and Maintenance
issued, or terminated for cause. The notification of planned
not stay any individual permit condition.
ZCE OF POLLUTION CONTROLS
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the permittee to achieve compliance with
the conditions of this individual permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
2. Need to Halt or Reduce Not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this individual permit.
Bypassing, of Stormwater Control Facilities
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless:
a_ Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
Part III Page 4 of 8

Permit No. NCS000030
weather. This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
C. The permittee submitted notices as required under, Part I11, Section E of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may approve an
anticipated bypass after considering its adverse effects.
SECTION D: MONITORING AND RECORDS
Representative SampIin
Samples collected and measurements taken, as required h
nature of the permitted discharge. Analytical sampling st
event. Samples shall be taken on a day and time that is�l
taken before the discharge joins or is diluted by any other
Monitoring points as specified in this permit shall not be
the Director.
Recording Results
all%tie characteristic of the volume and
!F
rformed during a representative storm
stic'of;the,discharge. All samples shall be
rea n body of water, or substance.
without notification to and approval of
For each measurement, sample, inspectionfo"r maintenance activity performed or collected pursuant to the
mit h permittee shall record the following information: requirements of this individual'
a. The date, exact place, aadYtiiiieaof'sairipling, measurements, inspection or maintenance activity;
b. The individual(s)�who performed the sampling, measurements, inspection or maintenance activity;
C. The date(s) analyses,Nyer6performed,
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136.
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower reporting level of the procedure.
Part III Page 5 of 8

Permit No. NCS000030
Representative Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status. If it is
established that the stormwater discharges are substantially identical and the permittee is granted
representative outfall status, then sampling requirements may be performed at a reduced number of outfalls.
Records Retention
Visual monitoring shall be documented and records maintained at the facility along with the Stormwater
Pollution Prevention Plan. Copies of analytical monitoring results shall also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous monitoring instrumentation, and copies of all
reports required by this individual permit for a period of at least 5 years from the date of the sample,
AV
measurement, report or application. This period may be extended. by quest of the Director at any time.
Inspection and Entry
The permittee shall allow the Director, or an authorized.repiesentative (including an authorized contractor
+ ,e.: 1h
acting as a representative of the Director), or in the case of a`facility which discharges through a municipal
separate storm sewer system, an authorized represent at ive�of a,municipal operator or the separate storm
sewer system receiving the discharge, upon the,presen ation o credentials and other documents as may be
required by law, to;
a. Enter upon the permittee's premises where Vregulated facility or activity is located or conducted,
or where records must=be) ept undegthe conditions of this individual permit;
b. Have access to andlicopy, at eea�§onable times, any records that must be kept under the conditions of
this individual hermit;
C. Inspect at reasotial 6.times'any facilities, equipment (including monitoring and control equipment),
practices, or ope ations regulated or required under this individual pern*; and
d. Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
SECTION E: REPORTING REQUIREMENTS
Discharge Monitorinp, Reports
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be received by the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
2. Submitting Reports
Duplicate signed copies of all reports required herein, shall be submitted to the following address:
Division of Water Quality
Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Part III Page 6 of 8

Permit No. NCS000030
Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection
at the offices of the Division of Water Quality. As required by the Act, analytical data shall not be
considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.613 or in Section 309 of the Federal Act.
Non-Stormwater Discharzes
If the storm event monitored in accordance with this individual permit coincides with a non-stormwater
discharge, the permittee shall separately monitor all parameters as required under the non-stormwater
discharge permit and provide this information with the stormwater discharge monitoring report.
Planned Changes
The permittee shall give notice to the Director as soon as po
facility which could significantly alter the nature or quantity
requirement includes pollutants which are not specificallyili
notification requirements under 40 CFR Part 122.42 (a).
Anticipated Noncompliance
The permittee shall give notice to the I
facility which may result in no, cn ompli
Bvnass
a. Anticipated bypass If the
prior notice, if possible at
the anticipated qual�tyand
Aile6f,any.pl"anned changes at the permitted
L-I .Y
f pollutants discharged. This notification
!d in the individual permit or subject to
possible of any planned changes at the permitted
iduat permit requirements.
iittee knows in advance of the need for a bypass, it shall submit
ten days before the date of the bypass; including an evaluation of
I of the bypass.
Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass.
Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment_ Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been received
within 24 hours.
9. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
Part III Page 7 of 8

Permit No. NCS000030
L0. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in an application for an
individual permit or in any report to the Director, it shall promptly submit such facts or information.
Part III Page 8 of 8

NCS000030
PART IV LIMITATIONS REOPENER
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) (c), and (d), 304(b) (2) and
307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or approved:
a. Contains. different conditions or is otherwise more stringent than any effluent limitation in the individual
permit, or
b. Controls any pollutant not limited in the individual permit.
The individual permit as modified or reissued under this
Act then applicable.
PART V ADMINISTERING AND
REQUI R El
The permittee must pay the administering and
the Division. Failure to pay the f
Division to initiate action to revo
1. Act
See Clean Water Act.
2. Arithmetic Mean
3
rd
in
ny other requirements in the
MONITORING FEE
ing fee within 30 (thirty) days after being billed by
e with 15A NCAC 2H .0105(b)(4) may cause this
DEFINITIONS
The arithmetic mean of any set of values is the summation of the individual values divided by the number of
individual values.
Allowable Non-Stormwater Discharges
This permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) All other discharges that are authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant
flushings, water from footing drains, flows from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -fighting training.
Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure.
Parts IV, V and VI Page 1 of 5

Permit No. NCS000030 ,
5.
P
7
8
9
Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
Clean Water Act
The Federal Water Pollution Control Act, also known asithe C a—rh ater Act (CWA), as amended, 33
US 1251, et. seq.
Division or DWO
The Division of Water Quality, Department of Environment an 'Natural Resources.
Director
The Director of the Division
10. EMC
The North Carolina En
W
it issuing authority.
mm s
Grab Sample Q_ :_
An individual sample collected instantaneously. Grab samples that will be directly analyzed or qualitatively
monitored must be taken within the first 30 minutes of discharge.
12. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
B. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility or
a surface storage facility.
14. Municipal Separate Storm Sewer. S stem
A stormwater collection system within an incorporated area of local self-government such as a city or town.
15. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsoil or similar naturally -occurring surface materials that are not disturbed by mining operations.
Part VI Page 2 of 5 Pages

Permit No. NCS000030
16. Permittee
The owner or operator issued a permit pursuant to this individual permit.
17. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch,
channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to waters
of the state.
18. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours in which no
storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive
hours of no precipitation. For example, if it rains for 2 hours without producing any collectable discharge, and then
stops, a sample may be collected if a rain producing a dischar e=begins a ain within the next 10 hours.
P P Y P g g �r g g 3
19. Representative Outfall Status
When it is established that the discharge of stc
discharges at multiple outfalls, the DWQ may
status allows the permittee to perform analytic
20. Rinse Water Discharge
The discharge of rinse water f
waters from vehicle and equip
utilizing any type of detergent
21. Secondary Containment
f f o a single outfall is representative of the
ae outfall status. Representative outfall
at a reduced number of outfalls.
44-gg areas associated with industrial activity. Rinse
are process wastewaters and do not include washwaters
Spill containment for the`c6ntents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25` year. 24-hour storm event.
22. Section 313 Water Priority Chemical
A chemical or chemical category which:
Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right -
to -Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III, Section 313 reporting
requirements; and
That meet at least one of the following criteria:
(1) Is listed in Appendix D of 40 CFR part 122 on either Table II (organic priority
pollutants), Table III (certain metals, cyanides, and phenols) or Table IV (certain toxic
pollutants and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40
CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
Part VI Page 3 of 5 Pages

Permit No. NCS000030 . ,
23
24
Severe Property Dama e
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss caused
by delays in production.
Significant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or production;
hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required to
report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes,
slag and sludge that have the potential to be released with storm water„discharges.
25. Sit?nificant Spills
26.
27.
28
29
IN
Includes, but is not limited to: releases of oil or hazardo"ussiibstances iri-lexcess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CF�a1d .40 and CFR 117.21) or section 102 of
CERCLA (Ref: 40 CFR 302.4). ,, , ,ah
Stormwater Runoff
The flow of water which results from precipitatidr;.and;which occurs immediately following rainfall or as a
result of snowmelt. '�
Stormwater Associated with Industrlal�Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacttring, processing or raw material storage areas at an industrial site. Facilities
considered to be engagedin industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include dikharges from facilities or activities excluded from the NPDES program.
Stormwater Pollution Prevention Pian
A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution and
is based on an evaluation of the pollution potential of the site.
Ten Year Design Storm
The maximum 24 hour precipitation event expected to be equaled or exceeded on the average once in ten
years. Design storm information can be found in the State of North Carolina Erosion and Sediment Control
Planning and Design Manual,
Total Flow
The flow corresponding to the time period over which the entire storm event occurs. Total flow shall be
either; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event.
Part VI Page 4 of 5 Pages

Permit No. NCS000030
31. Total Maximum Daily Load (TMDL)
A TMDL is a calculation of the maximum amount of a pollutant that a waterbody can receive and still meet
water quality standards, and an allocation of that amount to the pollutant's sources. A TMDL is a detailed
water quality assessment that provides the scientific foundation for an implementation plan. The
implementation plan outlines the steps necessary to reduce pollutant loads in a certain body of water to
restore and maintain water quality standards in all seasons. The Clean Water Act, section 303, establishes
the water quality standards and TMDL programs.
32. Toxic Pollutant
33
34
35
36.
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
upset
Means an exceptional incident in which there is unint
technology based permit effluent limitations because
permittee. An upset does not include noncompliance
designed treatment or control facilities, inadequate tri
maintenance, or careless or improper operation. ,
Vehicle Maintenance Activity
nd temporarynoncompliance with
`beyond the -reasonable control of the
tent c used�by operational error, improperly
�r, control facilities, lack of preventive
Vehicle rehabilitation, mechanical repairs,!painting fueling, lubrication, vehicle cleaning operations, or
airport deicing operations. 2 'f
;4
Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or ice from its site of origin�'hich can be seen with the unaided eye.
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
Part VI Page 5 of 5 Pages