NCS000374_HISTORICAL WITH APPLICATION_20181127

---'STORMVNATER-DIVISION-CODING-SNEET -- ---�—
PERMIT NO.
N (�S QOcD ;�-7y
DOC TYPE
❑FINAL PERMIT
❑ MONITORING INFO
PPLICATION
COMPLIANCE
❑ OTHER
DOC DATE
ZOl g 11 a�
T YYYYMMDD

NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue
Governor
Mr. Charles P Oxendine
Buckeye Lumberton
1000 Noir St
Lumberton, NC 27894
Dear Mr. Oxendine:
Coleen H. Sullins Dee Freemari
Director Secretary
June 1, 2010 DENR.—FRO'
JUN 0 7 2010
DWQ
Subject: Draft NPDES Stormwater Permit
Permit No. NCS000374
Buckeye Lumberton
Robeson County
Enclosed with this Ietter is a copy of the draft stormwater permit for your facility. Please review the draft
very carefully to ensure thorough understanding of the conditions and requirements it contains.
The draft permit contains the following significant changes from this facility's current permit:
Analytical monitoring changes:
1. Analytical monitoring parameters, TSS and pH, have been maintained in this permit. Oil and Grease has
been removed from the monitoring because the 50 gallons drums of lubricate were moved offsite and the
results from all the previous analytical samples were under Elie benchmark.
2. All analytical monitoring remains at semi-annually during a representative storm event as defined in Part
II Section B. The permittee must also document the total precipitation for each event. If no discharge
occurs during the sampling period, the permittee must submit a monitoring report indicating "No Flow"
within 30 days of the end of the six-month sampling period. Additionally, samples must be taken a
minimum of 60 days apart, as specified in Table 2,
3. Exceedances of benchmark values require the permittee to increase monitoring, increase management
actions, increase record keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered
program. If the sampling results are above a benchmark value, or outside of the benchmark range, for
any parameter at any outfall then the facility shall follow the Tier 1 guidelines which require a facility
inspection within two weeks and implementation of a mitigation plan within two months. If during the
term of this permit, the sampling results are above the benchmark values, or outside of the benchmark
range, for any specific parameter at a specific discharge outfall two times in a row (consecutive), then the
facility shall follow the Tier 2 guidelines which require a repetition of the steps listed for Tier 1 and also
immediately institute monthly monitoring for all parameters at every outfall where a sampling result
exceeded the benchmark value for two consecutive samples.
4. You are required to collect all of the analytical and qualitative monitoring samples during representative
storm events as defined in Part II Section B. Qualitative monitoring is required regardless of
representative outfall status.
5. You are responsible for all monitoring until the renewal permit is issued. See Footnote 1 of Tables 1, 4,
and 5.
Wetlands and Stonmwater Branch One 1617 Mall Service Cenler, Raleigh, North Carolina 27699-1617 NOrthCarOhna
ne:
Location: 6N. Salisbury St. Raleigh, North Carolina 2604 Nat�lt'ally
Pho919-8-807-63001 FAX: [phone] Customer Service: 3� ervice: 1-877-62748
Internet: www.ncwaterquality.org
An Equal Opportunity 4Affirmative Action Employer

Mr. Charles P Oxendine
Buckeye Lumberton
Permit No. NCS000374
6. Vehicle maintenance monitoring has remained at semi-annually in order to coincide. with analytical and
qualitative monitoring. Monitoring for TPH has replaced Oil & Grease. This requirement appears in all
Individual Stormwater permits, however it only applies to facilities that do vehicle maintenance. If the
facility begins vehicle maintenance during the permitted timeframe then the requirements shaII apply.
Other permit changes:
1. Information regarding the No Exposure Exclusion has been added to this draft permit. If industrial
materi,, ;w and activities are not exposed to precipitation or runoff as described in 40 CFR §122.26(g), the
facility may qualify for a No Exposure Exclusion from NPDES stormwater discharge permit
requirements. Additional information is provided in Part I Section A.
2. In addition to submitting two signed copies of DMRs to Central Files, a separate signed Annual Summary
DMR copy irust be submitted to the local DWQ Regional Office by March 1 of each year.
Please submit any comments to me no later than thirty (30) days following your receipt of the draft.
Comments should be sent to the address Iisted at the bottom of this page. If no adverse comments are
received from the public or from you, this permit will likely be issued in about two months.
If you have any questions or comments concerning this draft permit, contact me at [phone] or
[e-mail]
cc: Fayetteville Regional Office
Stormwater Permitting Unit
Attachments: Draft Permit NCS000374
Sincerely,
Brian Lowther
Environmental Engineer
Stormwater Permitting Unit
2

Lawyer, Mike r
From: Lawyer, Mike
Sent: Monday, May 24, 2010 2:15 PM
To: Lowther, Brian
Subject: RE: Individual Renewal Staff Report for NCS000374
Attachments: Staff Report comments -Buckeye Lumberton-NCS000374.pdf
Brian,
See attached FRO comments for the subject permit renewal. Let me know if you need anything further on our end.
Thanks,
Mike
Michael Lawyer, CPSWQ
Environmental Specialist
NCDENR-Division of Water Quality
Surface Water Protection Section
Fayetteville Regional Office
Direct: [phone]
Main: [phone]
Fax: [phone]
e-mail: [e-mail] (please note my current e-mail address)
*E-mail correspondence to and from this address may be subject to the North Carolina Public Records Law and may be
disclosed to third parties.
From: Lowther, Brian
Sent: Monday, May 17, 2010 11:13 AM
To: Lawyer, Mike
Subject: Individual Renewal Staff Report for NCS000374
Mike,
FYI, I sent you the draft renewal package for the individual permit
NCS000374 for your review and comment. Thanks.
Brian
Brian C. Lowther
Environmental Engineer
NCDENR I DWQ I Stormwater Permitting Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
512 N. Salisbury St, Raleigh, NC 27604
Phone: [phone]
Email: brian.lowtheraa,ncdenr. og_v
Website: http_//h2o.enr.state.ne.us/su/stortnwater.htmi

NCS000374
Recommendations: Based on the documents reviewed, the application information submitted on March 16.2010
sufficient to issue an Individual Stormwater Permit.
Prepared by (Signature) _ �c-�� C Date V,71p
Stormwater Permitting Unit Supervisor 1 �f-c Date
for Bradley Bennett
Concurrence by Regional Offic c��J i�✓Q Date Z �_
RO Water Quality Supervisor ALV&9J:i Date 0
Regional Office Staff Comments (attach additional pages as necessary)
idxGr 'tW C,d1nn�I�*a-YiG� QV, // 7l1 %. Ax 1tv
(INK
/'��i' C r��r r ✓tom �. a 4 a¢c ,1',
cc �;,� ,�� f►;�ml YES c�
1�4 4 44-- 74,E 70�
tf TeC3 ,, , q/1�r� ►-LS Oh Prf�d-T'S ,t��.►�W' 124,46Iv:
b,/ cc`F �" d.�,rvh� `� (r 1 55`�?��e71 aT Mee'( VL 577�� a-•,� a[
J Ain,
c� HvZb-e-� 7Zo
40 is:tia,•G z d-� d,-.
Page 7 of 7

��A
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
May 17, 2010
Individual NPDES Stormwater Permit Renewal Transmittal Cover Page
To: Fayetteville Regional Office
Subject: NPDES Stormwater Permit No. NCS000374
Buckeye Lumberton
Lumberton, NC (Robeson County)
Attachment Description
® Staff Report
Draft Permit
® Renewal Application
DENR-FRO
MAY 19 2010
DWQ
Please provide comments on the facility, draft permit, and staff report and sign/return
if acceptable.
Return to Brian Lowther at the Central Office by June 17, 2010.
Brian Lowther
Division of Water Quality
Stormwater Permitting Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Wetlands and Stormwater Branch One L, 1 1617 Mail Service Center, Raleigh, north Carolina 27699-1617 NOl) i1C�O1111�
Location: 5-8 7 Salisbury : Raleigh, North Carolina r S604 �aturalC�
Phone: 9t9-807-630fl 1 FAX: [phone] Customer Service: 1-877-623-6748
Internet: www.ncwaterquality.org
An Equ6 Opportunity 1 Affirmative Actien Employer

Permit No, NCS000525
5. Bypass
A bypass,is the known diversion of stormwater from any portion of stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
6. Bulk Storage of Liquid Products
Liquid raw materials, manufactured. products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
7. Clean Water Act '
The Federal. Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, et. seq.
8.. Division orDWQ
The ]division of Water Qual ity,. partment of Environment an Natural Resources.
9. •Director .
The Director of the Division of Water Q lity, the permit ssuing authority.'.
10. EMC ;
The North Carolina Environmental Management o ission.
11. Grab Sample
An individual sample. collected instantaneous Grab s iples that will be directly analyzed or
qualitatively monitored must be taken with' the first 30 'nutes of discharge.
12.. Hazardous Substance ,
Any.substanee., designated under 40 FR Part 11.6 pursuant to S tion 311 of the Clean Water Act.
13. Landfill
A disposal facility or part /adisposal facility wherewaste is placed in or o and and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term'storage facility
or a surface storage•facility.
14, Municipal Separate Storm Sewer.Sxstem
A stormwater collection system within.an. incorporated area of local self-government such as a city or
Mown.
' 15. . No Exposure
A condition.ofno exposure means that all industrial materials and activities are protected by a storm
resistant shelter or acceptable storage containers to prevent exposure to rain, snow, snowmelt; or runoff.
Part VI Page 2 of Pages

NCS000374
'IV
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
STAFF REVIEW AND EVALUATION
NPDES Stormwater Permit
Dee Freeman
Secretary
Facility Name:
Buckeye Lumberton,
NPDES Permit Number:
NCS000374
Facility Location:
1000 Noir St, Lumberton, NC (Robeson County)
Type of Activity:
Industrial - Pulp Mill
SIC Code:
2611
Receiving Streams:
See Figure 1
River Basin:
Lumber River Basin, Sub -basin 03-07-51
DENR-FRO
Stream Classification:
C;Sw
Proposed Permit Requirements:
See attached draft permit.
MAY 19 2010
Monitoring Data:
See Table 1
�JYYD Y Y Q
Response Requested by (Date):
t'17-10
Central Office Star Contact:
Return to: Brian Lowther, [phone]
Special Issues:
Issue
Ratin Scale: 1 eas to 10 hard
Compliance history
6'
Benchmark exceedance
6
Location (TMDL, T&E
_species, etc
5
Other Challenges:
No File
7
Difficulty Rating:
24140
Special Issues Explanation:
• SW Permit File Missing
Description of Onsite Activities:
a Buckeye Lumberton entered the bleached cotton fiber market in September of 2001 with state of the art
equipment and technology utilizing a batch bleaching process to treat a variety of cotton fibers. Bleached
cotton fibers are used in personal care, cosmetic and pharmaceutical products around the world and arc
gaining acceptance in nonwoven applications. The Lumberton operation has the capacity to produce 8,000
metric tons of fiber annually and is currently operating at about 90% capacity with annual sales revenue of
approximately $14 million. http://www.fibre2fashion.com/news/fashion-
news/newsdetaiis.as x?news id=29549& a e=1
Page 1 of 7

NCS000374
Ate
Documents Reviewed:
• NPDES Stormwater Permit Application Materials
• National Heritage Program (NHP) Threatened and Endangered Species Database
• SPU File
• Central Files
• EPA Sector -Specific Permit, 2008
• 303(d) List, 2010 draft, 2008 final
• Lumber 1.3asinwide Plan
History:
• June 18, 1999: Date permit first issued.
• July 1, 2005: Date permit re -issued. Analytical monitoring included TSS, Oil&Grease and pH to be -
monitored semi-annually in the spring and fall. Benchmarks were included.
• March 16, 20f0: Date permittee submitted renewal application.
Page 2 of 7

NCS000374
NCS000374
Nip Scale 1: 24,000
Figure 1: Map of Facility
Facility Location
Page 3 of 7

NCS000374
Central Office Review Summary:
1. Owner's Other Permits: NPDES Non -Major NCG500638, Air 3715500004, WQ0022877 —.Gravity Sewer
Extension, Pump Stations, & Pressure Sewer Extensions, WQ0002932 - Land Application of Residual Solids
(503 exempt)
2. General Observations:
• Seven Outfalls total, 5 quantitative (2, 4, 6, 7 and 8).
• The pulp mill operation was shut down on August 27, 2003. The only operations left are the Fiberline
operation. The Fiberline process was started in August 2001. The Fiberline is a staple cotton bleaching
process that produces products used in cosmetic and absorbent applications and medical devices. The`.
Fiberline process is.located in the building at the Northwest end of the site. Fiberline utilizes the pre-
existing warehouse space for storage of raw materials and finished products.
• The wastewater treatment plant has been closed and there is no longer a direct discharge of wastewater..
to the Lumber River.
• The Fiberline Process discharges plant process waters to the City of Lumberton municipal treatment
system.
• The Fiberline process uses Hydrogen peroxide, Sodium hydroxide and Sulfuric acid as process
chemicals. No. 4 Fuel oil also continues to be used as a backup fuel source to natural gas in boiler
operations. The site no longer has Chlorine, Sodium Chlorite or Tall Oil.
• There are no cotton linter or denim raw materials in storage at the site. Staple fibers (i.e. virgin staple,
cardstrip, regins, comber) are the raw materials fibers used in the Fiberline process.
• Generation of used oils and lubricants has significantly decreased.
• Storage of fuels (diesel and gasoline) has been eliminated.
• The Fiberline typically operates a 12/2 work schedule (12 days up and 2 days shutdown) but may
operate 24/7 as required to meet business needs.
3. Impairment: The Lumber River 14-(13)a-f is on the 2008 303(d) list and impaired for fish consumption. The
parameter of interest is mercury. The Lumber River 14-(13) is not on the 2010 draft 303d list. Based on the
1003 Lumber Basinwide Plan all waters in the subbasin are considered Impaired on an evaluated basis because
of fish consumption advice.
4. Threatened and Endangered: Based on the Natural Heritage Virtual Workroom there is one Federal protected
species (T (SIA) — threatened due to similarity of appearance): Alligator mississippiensis
5. Location: C;Sw
6. Industrial Changes Since Previous Permit: None included in renewal application.
7. Analytical Monitoring: See Table 1.
The SIC code 2611 is covered by the EPA Multi Sector General Permit in Sector B Paper and Allied Products
and no specific monitoring is recommend Paper Mills.
Reviewer recommends retaining monitoring requirements for TSS and pH because many of the samples are
above the benchmark concentration. There were TSS exceedances at outfalls 2, 6, 7 and 8. pH was under the
benchmark range for samples from outfalls 2, 4, 7 and S.
Oil and Grease (O&G) was in the previous permit but no sample results are over the benchmark (30 mg/1).
There were multiple samples that show O&G are present as well as close to the current benchmark. However,
the permittee said that all of the 50 gallon drums on the site were removed from the site after the pulp mill closed
in 2003. All of the most recent Oil and Grease samples were less than 5 mg/l. The reviewer recommends
removing O&G.
8. Qualitative Monitoring Notes: Permittee sent results from 2005-09. Some suspended solids, as well as, a
decrease in clarity occasionally observed. Color varied from light tan to medium brown. .
Page 4 of 7

NCS000374
Table 1: Analytical Monitoring
Required
Sampling
Range
Sample Date
Tolial Flow
{MGD)
Precipitation
(In)
Duration
(hours)
T5S
08G
pH
Benchmark:
100 mg1L
Benchmark:
30 mg/L.
Benchmark:
6-9 su
Outfall 2
11 2005
0.0086
0.42
48
<6.3
7.51
6/12/2006
0.0203
1
3
29
WM Wd15
6/15/2007
0.0237
1.17
10.9
6.46
6.04
10/26/2007
0.0152
0.8
148
7.7
doom,8
512812008
0.0156
0.82
26.3
6.46
NOUL87
11I M008
0.0073
0.36
67.1
<5
5►7
4114/2009
0.002
0.1
8.69
<5
6.34
11/30/2009
0.002
0.1
8
<5
6.28
Outfa I14
11/21/2005
0.0358
0.42
19
<6.1
728
6/12/2006
0.0852
1
<.1
27.8
EW 5�
6/1512007
0.0997
1.17
6.81
<5
6.59
10/26/2007
0.064
0.6
12
6.3
6.7
5/28/2008
0.086
0.82
2.27
<5
6.86
11/312008
0.0307
0.36
2.78
<5
7,06
4/1412009
0.0085
0.1
7.8
<5
7
11/30/2009
0.0085
0.1
<2.6
<5
7.14
Outtall 6
11/21/2005
0.01391
.6
7.19
6/12/2006
0.0331
1
18
24.8
6.42
6/1512007
0.0387
1.17
39.3
<5
6.98
10/26/2007
0.0288
0.8
92
<5
7.9
5/28/2008
0.0295
0.82
37.3
<5
7.77
1113MOB
0.0119
0.36
96.4
<5
7.99
4/14/2009
0.003
0.1
R4
<5
6.43. ,
11/30/2009
0.0033
0.1
52.4
<5
8
Outfal1 7
11121/2005
0.0175
0.42
7
18.2
7.4
6/12/2006
0.0415
1
53
20.9
5&
6/15/2007
0.0486
1.17
75.6
<5
7.23
10/26/2007
0.0576
0.8
..7
5.2
7.2
5/28/2008
0.059
0.82
70.5
<5
4�45
1113/2008
0.0149
0.36
11Q
<5
7.01
4/14/2009
0.0042
0.1
5.6
<5
6.08
11/30/2009
0.0042
0.1
83.6
<5
7.42
Outfall 8
11/21/2005
0.0093
0.42
29
8.8
7.25
6/12/2006
0.0222
1
'46
23.4
6.39
6/1512007
0.026
1.17
50.2
<5
6.83
10126/2007
0.0168
0.8
jjjj145
12.6
8.4
5/28/2008
0.0172
0.82
45.5
<5
5.83
11/3/2008
0.008
0.36
1
<5
111FAim
4/14/2009
0.0022
0.1
22.6
<5
6.93
11/3012009
0.0022
0.1
5.97
<5
6.79
Over Current Benchmark
Data Not Collected
DENR-FRCS
MAY 19 2010
DWQ
Page 5 of 7

NCS000374
Revised Permit Recommendations: Analytical Monitoring:
1. Maintaining analytical monitoring requirements for TSS and pH.
2. All analytical monitoring remains at semi-annually during a representative storm event as defined in Part 11
Section B. The permittee must also document the total precipitation for each event. If no discharge occurs
during the sampling period, the permittee must submit a monitoring report indicating "No Flow" within 30 days
of the end of the six-month sampling period. Additionally, samples must be taken a minimum of 60 days apart,
as specified in Table 2.
3. Exceedances of benchmark values require the permittee to increase monitoring, increase management actions,
increase record keeping, and/or install stormwater Best Management Practices (BMPs) in a tiered program.
4. The permittee is required to collect all of the analytical and qualitative monitoring samples during representative
storm events as defined in Part 11 Section B. Qualitaiive monitoring is required regardless of representative
outfall status.
5. The permittee is responsible for all monitoring until the renewal permit is issued. See Footnote 1 of Tables 1, 4,
and 5.
6. Annual summary DMR will be due to RO in March of every year.
Discussions with permittee: Charles Oxendine, [phone], 5/12/10
1. Description of the onsite industrial activities. Cotton bleach and purification plant. They use hydrogen peroxide
to bleach the f bers. Sell fiber to other companies to make final products.
2. What oils or fuels are stored onsite? #4 f iel oil. Used for the back boiler. They usually use natural gas. The pulp
mill onsite closed in 2003. There are no more 50gallon drums of lubricate that used to be used for the pulp mill.
There are monitoring values over our benchmarks for TSS and under for pH. Do you have any ideas why this is the
case? Not sure about the pH. For the TSS, the permittee thinks there was plant debris because of the large storm
events.
4. Do you have any vehicle maintenance? No
Page 6 of 7

NCS000374
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
I ti�l -
��..,�. ,
In compliance with the provisions of North CarolinaGeneraI Statute 143-215:1, other lawful
standards and regulations promulgated and adopted by the.North Carolina Environmental
Management Commission, and the Federal Water Pollution -Control Act, as amended,
Buckeye Lumberton, Inc.
is hereby authorized,to..discharge stormwater from a facility located at
/Buckeye Lumberton
1000 Noir St
Lumberton, NC
Robeson County
to receiving waters designated as the Lumber River, a class 3 I stream in the *ftdkir, Pee
River Basin, in accordance with the discharge limitations, monitoring requirements, and other
conditions set forth in Parts I, II, III, IV, V and VI hereof.
Note; Draft Permit Dates are Approximate
This permit shall become effective August 1, 2010.
This permit and the authorization -to discharge shall expire at midnight on July 31, 2015.
Signed this day July 10, 2010.
for Coleen H. Sullins Director
Division of Water Quality
By the Authority of the Environmental Management Commission

Permit No. NCS000374
TABLE OF CONTENTS
PART I
INTRODUCTION
Section A:
Individual Permit Coverage
Section B:
Permitted Activities
Section C:
Location Map
PART 11
MONITORING, CONTROLS, AND LIMITATIONS FORPERMITTED
DISCHARGES
1,
Section A:
Stormwater Pollution Prevention Plan `
J"
Section B:
Analytical Monitoring Requirements
Section C:
Qualitative Monitoring Requirements
Section D:
On -Site Vehicle,Maintenance.Monitoring Requirements
PART III
STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL
PERMITS ' • V _f�' _--
Section A:
Compliance and Liability
l . Compliance Schedule
2. Duty to Comply
3. Duty to Mitigate
4. Civil and Criminal Liability
5. Oil and Hazardous Substance Liability
6. Property Rights
7. Severability
8. Duty to Provide Information
9. Penalties for Tampering
10. Penalties for Falsification of Reports
Section B: General Conditions
1. Individual Permit Expiration
2. Transfers
3. Signatory Requirements
t

Permit No. NCS000374
4. Individual Permit Modification, Revocation and Reissuance, or
Termination
5. Permit Actions
Section C: Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D: Monitoring and Records
1. Representative Sampling
2. Recording Results
3. Flow Measurements
4. Test Procedures
5. Representative Outfdll
6. Records Retention
7. Inspection and -,Entry
Section E: Reporting Requi`rdments'
1. Discharge Monitoring Reports
2. Submitting,Reports
3. Availability of Reports
4. Non-Stormwater Discharges
5. Planned Changes
6. Anticipated Noncompliance
7. Spills
8. Bypass
9. Twenty-four Hour Reporting
10. Other Noncompliance
11. Other Information
PART IV LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
•r
PART VI DEFINITIONS
ii

Permit No. NCS000374
PART I INTRODUCTION
SECTION A: INDIVIDUAL PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as sped . ed in this permit.
If industrial materials and activities are not exposed to precipitation or runoff as described in 40
CiW R § I22.26(g), the facility may qualify for a No Exposure Exclusion from NPDES stormwater
discharge permit requirements. Any owner or operator wishing'to obtain a No Exposure
Certification must submit a'No Exposure Certification`NOI form to the.Division; must receive
approval by the Division; must maintain no exposure conditions unless authorized to discharge
under a valid NPDES stormwater permit; and must reapply for the No Exposure Exclusion once
every five (5) years.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or 'revoked, the permittee is authorized to discharge
stormwater to the surface waters of North Carolina or separate storm sewer system that has been
adequately treated and managed§in accordance with the terms and conditions of this individual
permit. All stormwater discharges shall be in accordance with the conditions of this permit.
Any other point source discharge to surface waters of the state is prohibited unless it is an
allowable non-stormwater discharge or is covered by another permit, authorization, or approval.
The stormwater discharges allowed by this individual permit shall not cause or contribute to
violations of Water Quality Standards.
This permit does not relieve the permittee from responsibility for compliance with any other
applicable federal, state, or local law, rule, standard, ordinance, order, judgment, or decree.
Part I Page ] of 2

SECTION C: LOCATION MAP
Permit No. NCS000374
NCS000374
W Scale 1;24,000
Buckeye Lumberton
Lab tude:34036' 25"N
Longitude: 780 59' 50" W
County: Robeson
Recdving Stream: Lumber River
Strum Class: C;Sw
Sub -basin: 03-07-51 (Lumber River Basin)
Facility Location
Part I Page 2 of 2

Permit No. NCS000374
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR
PERMITTED DISCHARGES
SECTION A: STORMWATER POLLUTION PREVENTION PLAN
The Permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as
the Plan. This Plan shall be considered public information in accordance wi&Part III, Standard
Conditions, Section E, Paragraph 3 of this individual permit.. The Plan shall include, at a
minimum, the following items:
l . Site Plan. The site plan shall provide a description of the 'physical facility and the
potential pollutant sources which maybe expected to'contribute to contamination of
stormwater discharges. The site plan shall contain the %llowing:
(a) A general location map (USGS quadrangle, map or appropriately drafted
equivalent map), showing the facility's location in relation to transportation routes
and surface waters, the name of the''receiving water(s) to which the stormwater
outfall(s) discharges, or if the discharge is to a municipal separate storm sewer
system, the name of the municipality and the ultimate receiving waters, and
accurate latitude and longitude of the; point(s) of discharge. The general location
map (or alternatively the site map) `shall identify whether each receiving water is
impaired (on the s'tate`s 303(d) list of impaired waters) or is located in a
watershed for which -a TMDL has been established, and what the parameter(s)
of concern are'./�� �1
(b) A narrative description of storage practices, loading and unloadin' activities,
`._._
outdoor process areas, dust or particulate generating or control processes, and
waste disposal practices. A narrative description of the potential pollutants which
could be expected to be present in the stormwater discharge from each outfall.
(c) A site map drawn to scale (including a distance legend) showing: the site property
boundary, the stormwater discharge outfalls, all on -site and adjacent surface
waters and wetlands, industrial activity areas (including storage of materials,
disposal areas, process areas, loading and unloading areas, and haul roads), site
topography, all drainage features and structures, drainage areas for each outfall,
direction of flow in each drainage area, industrial activities occurring in each
drainage area, buildings, existing BMPs, and impervious surfaces. The site map
must indicate the percentage of each drainage area that is impervious.
(d) A list of significant spills or leaks of pollutants that have occurred at the facility
during the three (3) previous years and any corrective actions taken to mitigate
spill impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part 111, Standard Conditions, Section
Part It Page 1 of 9

Permit No. NCS000374
B, Paragraph 5. The permittee shall re -certify annually that the stormwater
outfalls have been evaluated for the presence of non-stormwater discharges.
2. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed which control or
minimize the exposure of significant materials to stormwater, including structural and
nonstructural measures, The stormwater management plan, at a minimum, shall
incorporate the following:
(a) Feasibility Study. A review of the technical and economic feasibility of changing
the methods of operations and/or storage practices to eliminate or reduce exposure
of•materials and processes to stormwater. Wherever practical, the permittee shall
prevent exposure of all storage areas, material^handling operations, and
manufacturing or fueling operations. In areas where elimination of exposure is
not practical, the stormwater management plan shall --document the feasibility of
diverting the stormwater runoff away frori ,areas ofpotential contamination.
(b) Secondary Containment Requiremerits'and'Records. Secondary containment is
required for: bulk storage,of IigLifd materials; storage in any amount of Section
313 of Title III of the Superfund Amendments and Reauthorization Act (SARA)
water priority chemicals; and storage in any amount of hazardous substances, in
� 4 i.f
spil order to prevent leaks and ls from contaminating stormwater runoff. A table
or summary of all such,tanks nd stored materials and their associated secondary
containment areas.shall be.main/tained. If the secondary containment devices are
connected to stormwate`r,coriveyance systems, the connection shall be controlled
by manually activated valves or other similar devices (which shall be secured
closed with a'locking'inechanism), and any,stormwater that accumulates in the
containment area shall be at a minimum visually observed for color, foam, outfall
staining, visible sheens and dry weather flow, prior to release of the accumulated
stormwater. Accumulated stormwater shall be released if found to be
uncontaminated by any material. Records documenting the individual making the
observation, the description of the accumulated stormwater, and the date and time
of the release shall be kept for a period of five years.
(c) BMP Summary. A listing of site structural and non-structural Best Management
Practices (BMP) shall be provided. The installation and implementation of BMPs
shall be based on the assessment of the potential for sources to contribute
significant quantities of pollutants to stormwater discharges and data collected
through monitoring of stormwater discharges. The BMP Summary shall include a
written record of the specific rationale for installation and implementation of the
selected site BMPs. The BMP Summary shall be reviewed and updated annually.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or the team) responsible for implementing the
SPRP shall be identified in a written list incorporated into the SPRP and signed and dated
by each individual acknowledging their responsibilities for the plan. A responsible
Part II Page 2 of 9

Permit No. NCS000374
person shall be on -site at all times during facility operations that have the potential to
contaminate stormwater runoff through spills or exposure of materials associated with the
facility operations. The SPRP must be site stormwater specific. Therefore, an oil Spill
Prevention Control and Countermeasure plan (SPCC) may be a component of the SPRP,
but may not be sufficient to completely address the stormwater aspects of the SPRP. The
common elements of the SPCC with the SPRP may be incorporated by reference into the
SPRP.
4. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance and good housekeeping program shall be developed. The program shall list
all stormwater control systems, stormwater discharge outfalls;;all on -site and adjacent
surface waters and Wetlands, industrial activity areas (including material storage areas,
material handling areas, disposal areas, process areas, loading and unloading areas, and
haul roads), all drainage features and structures, and existing structural BMPs. The
program shall establish schedules of inspections, maintenance;%and housekeeping
activitics of stormwater control systems, as well as facility cquipmcnt, facility areas, and
facility systems that present a potential for stormwater exposure or stormwater pollution.
Inspection of material handling areas and regular cleaning schedules of these areas shall
be incorporated into the program. Timely compliance with the established schedules for
inspections, maintenance, and housekeeping shall be recorded in writing and maintained
in the SPPP.
5. Employee Training. Training programs shall be developed and training provided at a
minimum on an annual basis for facility personnel with responsibilities for: spill response
and cleanup, preventative maintenance activities, and for any of the facility's operations
that have the potential to contaminate stormwater runoff. Facility personnel (or team)
responsible for implementing the training shall be identified, -and their annual training
shall be documented bythe signature of each employee trained.
6. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific
position(s) responsible for the overall coordination, development, implementation, and
revision to the Plan. Responsibilities for all components of the Plan shall be documented
and position assignments provided.
7. Plan Amendment. The permittee shall amend the Plan whenever there is a change in
design, construction, operation, or maintenance which has a significant effect on the
potential for the discharge of pollutants to surface waters. All aspects of the
Stormwater Pollution Prevention Plan shall be reviewed and updated on an annual
basis. The annual update shall include an updated list of significant spills or leaks of
pollutants for the previous three years, or the notation that no spills have occurred. The
annual update shall include written re -certification that the stonnwater outfalls have been
evaluated for the presence of non-stormwater discharges. Each annual update shall
include a documented re-evaluation of the effectiveness of the BMPs listed in the BMP
Summary of the Stormwater Management Plan.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requirements of the permit. Within 30 days of such notice, the permittee shall
Part II Page 3 of 9

Permit No. NCS000374
submit a time schedule to the Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with
Part III, Standard Conditions, Section B, Paragraph 5) to the Director that the changes
have been made.
8. Facility Inspections. Inspections of the facility and all stormwater systems shall occur as
part of the Preventative Maintenance and Good Housekeeping Program at a minimum on
a semi-annual schedule, once during the first half of the year (January to June), and once
during the second, hal f.(July to December), with at least 60 days separating inspection
dates (unless performed more frequently than semi-annually). These facility inspections
are different from,'and in addition'to, the stormwater discharge characteristic monitoring
required in Part II B and C of this permit.
9. Implementation. The permittee shall implement the P1ari.\�rnplementation of the Plan
shall include documentation of all monitoring; measurements;; nspections, maintenance
activities, and training provided to employees ,,including the'log of the sampling data and
of actions taken to implement BMPs associated`with,the industrial activities, including
vehicle maintenance activities. Such documentation' hall be kept on -site for a period of
five years and made available to the Directtrror the; Director's authorized representative
immediately upon request.
:1 'h,
Part II Page 4 of 9

Permit No. NCS000374
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
Analytical monitoring of stormwater discharges shall be performed as specified in Table 1. All
analytical monitoring shall be performed during a representative storm event. The required
monitoring will result in a minimum of ten analytical samplings being conducted over the term of
the permit at each stonnwater discharge outfall (SDO).
A representative storm event is a storm event that measures greater than 0.1 inches of rainfall. The time
between this storm event and the previous storm event measuring greater than 0.1 inches must be at least
72 hours. A single storm event may have a period of no precipitation of up to 10 hours. For example, if
it rains but stops before producing any collectable discharge, a sample may be collected if the next rain
producing a discharge begins within 10 hours.
Table 1. Analytical Monitoring Requirements , .
Discharge
Characteristics
Units
Measnrement Frequency)
Sample
TypC2
Sample
Location3
Total Suspended Solids
m L
,'semi-annual
Grab
SDO
H
standard
�1` ;semi-annual
Grab
SDO
Total Rainfal14
inches
, ., semi-annual
ain Gauge
1-
Footnotes:
1 Measurement Frequency: Twice per year during'a representative storm event.
2 Grab samples shall be collected within the First 30 minutes of discharge.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative outfall
status has been granted.
4 For each sampled representative stormevent the total precipitation must be recorded. An on -site rain gauge or local rain
gauge reading must be recorded.
The permittee shall complete the minimum ten analytical samplings in accordance with the
schedule specified below in Table 2. A minimum of 60 days must separate Period 1 and
Period 2 sample dates unless monthly monitoring has been instituted under a Tier Two
response.
Part It Page 5 of 9

Permit No. NCS000374
Table 2. Monitoring Schedule
Monitoring period t'2
Sample Number
Start ,
End
Year 1 — Period 1
1
August 1, 2010
December 31, 2010
Year 1 — Period 2
2
January 1, 2011
June 30, 2011
Year 2 — Period 1
3
July 1, 2011
December 31, 2011
Year 2 — Period 2
4
January 1, 2012
June 30, 2012
Year 3 — Period 1
5
July 1,3,012
December 31';'2012
Year 3 — Period 2
6
January 1,,2013
June 30, 26 3
Year 4 — Period 1
7
July 1, 2013
December 31, 2013
Year 4 — Period 2
S
January 1, 201;4.
June 3.0, 2014
Year 5 — Period 1
9
July 1, 2014'>
December 31, 2014
Year 5 — Period 2
10
January l; 2b15
, July 31, 2015
Footnotes:
1 Maintain semi-annual monitoring during permit renewal process. If at;the'expiration of the Individual
Permit, the permittee has submitted an application for renewal of coverage before the submittal deadline,
the permittee will be considered for renewed coverage. The applicant must continue semi-annual
monitoring until the renewed permit is issued. ,,,
2 If no discharge occurs during the sampling period he pgrrnittee must submit a monitoring report indicating
"No Flow" within 30 days of the end of the siz month s am pling period.
4
The permittee shall report the analytical 'results' from each sample within the monitoring period. The
permittee shall compare monitorindresults`to•the benchmark values -in Table 3. The benchmark
values in Table 3 are not permitrlimits bulshould he used as guidelines for the permittee's
Stormwater Pollution Prevention Plan (SPPP). Exceedences of benchmark values re4dite the
permittee to increase monitoring,.increase management actions, increase record keeping, and/or
m install storwater Best Management Practices (BMPs) in a tiered program. See below the
descriptions of Tier One and Tier Two.
Table 3. Benchmark Values for Analytical Monitoring
Discharge Characteristics
Units
Benchmark
Total Suspended Solids
mg/L
100
pH
standard
6-9
Part II Page 6 of 9

Permit No. NCS000374
Tier
IIf: The first valid sampling results are above a benchmark value, or outside of the benchmark range, for any I
parameter at anv outfall;
Then: The permittee shall
1. Conduct a stormwater management inspection of the facility within two weeks of receiving
4
sampling results.
2. Identify and evaluate possible causes of the benchmark value exceedence.
3. Identify potential and select the specific: source controls, operational controls, or physical
improvements to reduce concentrations. of the parameters of concern, or to bring concentrations
within the benchmark range.
4. Implement the selected actions within two months of the inspection.
5. Record each instance of a Tier One response in the Storm 'water Pollution Prevention Plan. Include
the date and value of the benchmark exceedence, the. inspection date the personnel conducting the
inspection, the selected actions, and the date the selected actions were implemented.
Tier Two
If: During the term of this permit, the first valid sampling results from two consecutive monitoring periods
are above the benchmark values, or outside of.the benchmark range, for any specific parameter at a
specific discharge outfall;
Then: The permittee shall:
1. Repeat all the required actions �outlined.above in Tier One.
2. Immediately institute monthly monitoring for all parameters at every outfall where a sampling result
exceeded the benchmark value for two consecutive samples. Monthly (analytical and qualitative)
monitoring shall continue.until three consecutive sample results are below the benchmark values or
within the benchmark range.
3. If no discharge occurs during the sampling period, the permittee is required to submit a monthly
monitoring report indicating "No Flow" to comply with reporting requirements.
4. Maintain a record of the Tier Two response in the Stormwater Pollution Prevention Plan.
During the term of this permit, if the valid sampling results required for the permit monitoring periods
exceed the benchmark value, or are outside the benchmark range, for any specific parameter at any specific
outfall on four occasions, the permittee shall notify the DWQ Regional Office Supervisor in writing within
30 days of receipt of the fourth analytical results. DWQ may but is not limited to:
• require that the permittee revise, increase, or decrease the monitoring frequency for the remainder
of the permit;
• require the permittee to install structural stormwater controls;
• require the permittee to implement other stormwater control measures; or
• require that the permittee implement site modifications to qualify for the No Exposure Exclusion.
Part II Page 7 of 9

Permit No. NCS000374
SECTION C: Qualitative Monitoring Requirements
Qualitative monitoring requires a visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified in Table 4, during the analytical
monitoring event. [If analytical monitoring is not -required, the permittee still must conduct semi-
annual qualitative monitoring.] Qualitative monitoring is for the purpose of evaluating the
effectiveness of the Stormwater Pollution Prevention Plan (SPPP) and assessing new sources of
stormwater pollution.
In the event an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the SPPP
Table 4. Qualitative Monitoring Re uiremento
Discharge Characteristics
Frequencyl
Monitoring
Location2
Color
semi-annual-';
\ -,SDO
Odor
semi-annual,
`� %SDO
Clarity
semi annual
i SDO
Floating Solids
semi-annual,'
SDO
Suspended Solids �, `\
>.. semi annual
SDO
Foam /,r
y semi annual
SDO
Oil Sheen
' semi-annual
SDO
Erosion or deposition at the butfall�
'semi-annual
SDO
Other obvious indicators -''
semi-annual
SDO
of stormwater pollution
Footnotes:
1 Measurement Frequency: Twice per year during a representative storm event, for each year until either another
permit is issued for this facility or until this permit is revoked or rescinded. If at the end of this permitting cycle
the permittee has submitted the appropriate paperwork for a renewal permit before the submittal deadline, the
permittee will be considered for a renewal application. The applicant must continue semi-annual monitoring until
the renewed permit is issued. See Table 2 for schedule of monitoring periods through the end of this permitting
cycle.
2 Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO)
regardless of representative outfall status.
SECTION D: ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
Facilities which have any vehicle maintenance activity occurring on -site which uses more than 55
gallons of new motor oil per month when averaged over the calendar year shall perform
analytical monitoring as specified below in Table 5. This monitoring shall be performed at all
stormwater discharge outfalls which discharge stormwater runoff from vehicle maintenance
i
Part II Page 8 of 9

Permit No. NCS000374
areas, and in accordance with the schedule presented in Table 2 (Section B). All analytical
monitoring shall be performed during a representative storm event.
Table 5. Analytical Monitoring Requirements for On -Site Vehicle Maintenance
Discharge Characteristics
Units
Measurement
Sample
Sample
Fre uenc 1
Typt2
Location3
H
standard
semi-annual
Grab
SDO
TPH�
mg/l
semi-annual
Grab
SDO
EPA Method 1664 (SGT-HEM
Total Suspended Solids
mg/1
semi-annual
Grab
SDO
Total Rainfal14
inches
semi-annual , '
Rain gaug6
-
New Motor Oil Usage
gallons/month
semi-annual
Estimate
-
Footnotes:
I Measurement Frequency: Twice per year during a representative storm event, for each year until either another
permit is issued for this facility or until this permit is revoked'or rescinded. If at the end of this permitting cycle
the permittee has submitted the appropriate paperwork for a renewal permit before the submittal deadline, the
permittee will be considered for a renewal application. The applicant must continue semi-annual monitoring until
the renewed permit is issued. See Table 2 for schedule,of monitoring periods through the end of this permitting
cycle. �. f
l'
2 If the stormwater runoff is controlled by a stormwater detention pond a grab sample of the discharge from the
pond shall be collected within the first.30 minutes of discharge from the pond.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle maintenance activities occur.
4 For each sampled representative 'storm event the total precipitation must be recorded. An on -site or local rain
gauge reading must he recorded.
Monitoring results shall be compared to the benchmark values in Table 6. The benchmark
values in Table 6 are not permit limits but should be used as guidelines for the permittee's
Stormwater Pollution Prevention Plan (SPPP). Exceedences of benchmark values require the
permittee to increase monitoring, increase management actions, increase record keeping, and/or
install stormwater Best Management Practices (BMPs), as provided in Part II Section B.
Table 6
Benchmark Values for Vehicle Maintenance Analytical Monitoring
..Discharge Characteristics
'Units
Benchmark
pH
standard
6-9
TPH
[EPA Method 1664 (SGT-HEM)]
mglL
15
Total Suspended Solids
mg/L
100
r
Part II Page 9 of 9

Permit No. NCS000374
PART III STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule: '
Existing Facilities already operating but applying for permit coverage for the first time: The Stormwater
Pollution Prevention Plan shall be developed and implemented within 12 months of the effective date of the
initial permit and updated thereafter on an annual basis,, -"Secondary containment, as specified in Part II,
Section A, Paragraph 2(b) of this permit, shall be accomplished within,12 months of the effective date of
the initial permit issuance.
New Facilities applying for coverage for the first time and existing -facilities previously permitted and
applying for.renewal under this permit: The Stormwater Pollution Prevention Plan shall be developed and
u�
implemented prior to the beginning of discharges from,the operation of the industrial activity and be
updated thereafter on an annual basis. Secondary containment, as specified in Part I1, Section A,'Paragraph
� I
2(b) of this permit shall be accomplished prior to,the beginning of discharges from the operation of the
industrial activity.
Duty to Comply
The permittee must comply with;all'coriditions of this individual permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit upon renewal application.
r +.jr
a. The permittee shall comply -with standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants within•the time provided in the regulations that establish these
standards or prohibitions, even if the permit has not yet been modified to incorporate the
requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $25,000 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to 25,000 per day of violation, or
imprisonment for not more than 1 year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed an administrative penalty not to exceed $10,000 per violation with the maximum
amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33 USC 1319 and 40 CFR
122.41(a).]
C. Under state law, a daily civil penalty of not more than ten thousand dollars ($10,000) per, violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: • NC General Statutes 143-215.6A].
d. Any person may be assessed an administrative penalty by the Director for violating section 301,
302, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any
of such sections in a permit issued under section 402 of the Act. Administrative penalties for Class
I violations are not to exceed $10,000 per violation, with the maximum amount of any Class I
penalty assessed not to exceed $25,000. Penalties for Class 11 violations are not to exceed
Part III Page I of 8

Permit No. NCS000374
$10,000 per day for each day during which the violation continues, with the maximum amount of
any Class II penalty not to exceed S 125,000.
3. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the environment.
4. Civil and Criminal Liability
Except as provided in Part III, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance purse«alit to NCGS 143-215.3, 143-215.6A, 143-215.613, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities,' r penalties to"which the permittee is or may be subject to
under NCGS 143-215.75 et seq. or Section 311,of the Federal Act, 33 USC 1321.
6. Property Rights
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
ederal, State or local laws or regulations: personal rights, nor any infringement of f
7. Severability /
The provisions of this individual permit are severable, and if any provision of this individual permit, or the
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall famish to the Director, within a reasonable time, any information which the Director
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit. The
permittee shall also furnish to the Director upon request, copies of records required to be kept by this
individual permit.
Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate,
any monitoring device or method required to be maintained under this individual permit shall, upon
conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more
than two years per violation, or by both. If a conviction of a person is for a violation committed after a first
conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per day of
violation, or by imprisonment of not more than 4 years, or both.
Part III Page 2 of 8

Permit No. NCS000374
10. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this individual
permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a fine of not more than $10,000 per violation, or by imprisonment'for not more than two years
per violation, or by both.
SECTION B: GENERAL CONDITIONS
Individual Permit Expiration ,
The permittee is not authorized to discharge after the expiration date. An order to receive automatic
authorization to discharge beyond the expiration date, the permittee'shall submit forms and fees as are
required by the agency authorized to issue permits no later than,l80 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at Ieast,180 days prior to expiration, will be
subjected to enforcement procedures as provided in NVGS § 143-215.36 and 33 USC 1251.et. seq.
ti
2. Transfers
This permit is not transferable to any person except after notice to and approval by the Director. The
Director may require modification or revocation and reissuance of the permit to change the name and
incorporate such other requirements as maybe necessary under the Clean Water Act. The Permittee is
required to notify the Division in writing in. the event the permitted facility is sold or closed.
3. Signatoly Requirements 'T
All applications, reports, or information submitted to the Director shall be signed and certified.
a. All applications to'be covered under this individual permit shall be signed as follows:
(1) In the case of a corporation: by a principal executive officer of at least the level of vice-
president, or his duly authorized representative, if such representative is responsible for
the overall operation of the facility from which the discharge described in the permit
application form originates;
(2) In the case of a partnership or limited partnership: by a general partner;
(3) In the case of a sole proprietorship: by the proprietor;
(4) In the case of a municipal, state, or other public entity: by a principal executive officer,
ranking elected official, or other duly authorized employee.
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
i
Part III Page 3 of 8

Permit No. NCS000374
responsibility, or an individual or position having overall responsibility for environmental
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
C. Any person signing a document under paragraphs a. or b. of this section shall make the following
certification:
"I ccrtify,•under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
4. Individual Permit Modification. Revocation and Reissuance: or Termination
The issuance of this individual permit does not prohibit the Director from reopening and modifying the
individual permit, revoking and reissuing the individual permit,•or terminating the individual permit as
allowed by the laws, rules, and regulations contained in Title.40, Code of Federal Regulations, Parts 122
and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North Carolina
General Statute 143-215.1 et al.
5. Permit Actions
J.
The permit may be modified„revoked and reissued, or terminated for cause. The notification of planned
changes or anticipated noncompliance.do/es not stay any individual permit condition.
! f
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
l . Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the-permittee to achieve compliance with
the conditions of this individual permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
Need to Halt or Reduce Not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order,to maintain compliance with the condition of this individual permit.
Bypassing of Stormwater Control Facilities
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless:
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
Part III Page 4 of 8

•S -
Permit No. NCS000374
b. " There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
weather. This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
C. The permittee submitted notices as required under, Part III, Section E of this permit,
If the Director determines that it will.nieet the three conditions listed above, the Director may approve an
i .;'anticipated bypass after considering it�,.adverse effects.
SECTION D: MONITORING AND RECORDS., '
X0 n
Representative Sampling
Samples collected and measurements taken, as required; herein; shall be' characteristic of the volume and
nature of the permitted discharge. Analytical samplingtishall be perf&'rmed during a representative storm
event. Samples shall be taken on a day and time that ischaracteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of water, or substance.
Monitoring points as specified in this permit shall -not be changed without notification to and approval of
the Director. _
Recording Results
For each measurement, sample, inspection of maintenance activity performed or collected pursuant to the
requirements of this individual permit; the permittee shall record the following information:
a. The date, exact place, and time.of sampling, measurements, inspection or maintenance activity;
c
b. The individuat(s) who pe rfornred the sampling, measurements, inspection or maintenance activity;
2.
C. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required„appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136.
PartIII Page 5 of 8

Permit No. NCS000374
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower.reporting level of the procedure.
Representative Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status. If it is
established that the stormwater discharges are substantially identical and the permittee is granted
representative outfall status, tl`,pn sampling requirements may be performed at a reduced number of outfalls.
6. Records Retention
Visual monitoring shall be documented and records maintained at the.facility along with the Stormwater
Pollution Prevention Plan. Copies of analytical monitoring results.shali also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous monitoring instrumentation, and copies of all
.reports required by this individual permit for a period of at least 5 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time.
7. Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director), or in the case"of a facility which discharges through a municipal
separate storm sewer system, an authorized representative of a municipal operator or the separate storm
sewer system receiving the discharge, upon the presentation of credentials and other documents as may be
required by law, to;
Enter upon the perniittec'apremises where a regulated facility or activity is located or conducted,
or where records must be kept under the conditions of this individual permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of
this individual permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),
practices, or operations regulated or required under this individual permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
SECTION E: REPORTING REQUIREMENTS
Discharge Monitoring Reports
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be delivered to the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
The permittee shall submit an Annual Summary Data Monitoring Report to the appropriate DWQ Regional
Office in February of each year. The submittal shall be on forms supplied by the Division.
Part III Page 6 of 8

Permit No. NCS000374
When no discharge has occurred from the facility during the report period, the permittee is required to
submit a discharge monitoring report, within 30 days of the end of the six-month sampling period, giving all
required information and indicating "NO FLOW" as per NCAC T15A 02B .0506.
The permittee shall record the required qualitative monitoring observations on the SDO Qualitative
Monitoring Report form provided by the Division, and shall retain the completed forms on site. Visual
monitoring results should not be submitted to the Division, except upon DWQ's specific requirement to do
SO.
2. Submitting Reports
Two signed copies of Discharge Monitoring Reports (DMRs) shall be submitted to:
Central Files
Division of Water Qualitytt
1617 Mail Service Center
Raleigh, North Carolinaf27699 161 t t
In addition, a separate signed Annual Summary DMR copy shalt be submitted to the local DWQ Regional
Office (RO) by March 1 of each year.
Addresses for each RO and the counties covered by each RO can be found here:
http://www.enr.state.ne.us/html/repionaloffices.htmt,�The permittee shall retain the completed originals
on site. Visual monitoring results should not be submitted to the Regional Offices or Central Files unless
specifically requested by DWQt� !,
3. Availability of Reports
Except for data determined to be confidential under NCGS 143=215.3(a)(2) or Section 308 of rho Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection
at the offices of the Division of Water Quality. As required by the Act, analytical data shall not -be
considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.613 or in Section 309 of the Federal Act.
Non-Stormwater Discharges
If the storm event monitored in accordance with this Individual Permit coincides with a non-stormwater
discharge, the permittee shall separately monitor all parameters as required under the non-stormwater
discharge permit and provide this information with the stormwater discharge monitoring report.
Planned Chances
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which could significantly alter the nature or quantity of pollutants discharged. This notification
requirement includes pollutants which are not specifically listed in the Individual Permit or subject to
notification requirements under 40 CFR Part 122.42 (a).
6. Anticipated Noncompliance
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which may result in noncompliance with the individual Permit requirements.
Part III Page 7 of 8

Permit No. NCS000374
The permittee shall report to the local DWQ Regional Office, within 24 hours, all significant spills as
defined in Part VI of this permit. Additionally, the permittee shall report spills including: any oil spill of 25
gallons or more, any spill regardless of amount that causes a sheen on surface waters, any oil spill
regardless of amount occurring within 100 feet of surface waters, and any oil spill less than 25 gallons that
cannot be cleaned up within 24 hours.
Bypass
a. Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit
prior notice, if possible at least ten days before the date of the bypass_ ; including an evaluation of
the anticipated quality and affect of the bypass.
b. Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass. ;
4. Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times; -and if the noncompliance has not been corrected, the
anticipated time compliance is'ckpected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance. ,.
The Director may waive the written report on a case -by -case basis if the oral report has been.received
within 24 hours.
10. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
Ill. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in a Notice of Intent to be
covered under this Individual Permit or in any report to the Director, it shall promptly submit such facts or
information.
Part III Page 8 of 8

NCS000374
PART IV LIMITATIONS REOPENER
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under provisions of the Clean Water Act, if the
effluent guideline or water quality standard so issued or approved:
a. Contains different conditions or is otherwise more stringent than any effluent limitation in the individual
permit; or
b. Controls any pollutant not -limited in the individual permit.
>� e
The individual permit as modified or reissued under this paragraph'shall also contain any other requirements in the
Act then applicable. - -
- S
PART ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed by
the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the.Individual Permit.
PART�VI DEFINITIONS
1. A&tr '
See Clean Water Act,
Allowable Non-Stormwater Discharges
This permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) All other discharges that are authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant
flushings, water from footing drains, flows from riparian habitats and wetlands.. .
(c) Discharges resulting from fire -fighting or fire -fighting training.
Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure. More information on BMPs can be found at:
http:/Ycfpub.epa.gov/npdes/stormwater/menuofbmps/index.cfm.
4. Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
Parts IV, V and VI Page 1 of

Permit No. NCS000374
6. Certificate of Coverage
The Certificate of Coverage (COC) is the cover sheet which accompanies the Individual Permit upon
issuance and lists the facility name, location, receiving stream, river basin, effective date of coverage under
the permit and is signed by the Director.
7. Clean Water Act
The Federal Water Pollution Control :act, also known as the Clean Water Act (CWA), as amended, 33 USC
1251, et. seq.
S. Division or DW
The Division of Water Quality, Departmient of Environment and Natural Resources.
r,
4. Director
The Director of the Division of Water Quality, the permit issuing authority.
10. EMC �r •.
The North Carolina Environmental Management Commission. `>
l l . Grab Sample
An individual sample collected instantaneously. Grab samples that will be analyzed (quantitatively or
t qualitatively) must be taken* within the first 30 minutes,of discharge.
12. Hazardous Substance 4
Any substance designated under 40 CFR Part:116 pursuant to Section 311 of the Clean Water Act.
13. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundmdat, an injection well, a hazardous waste long-term storage facility or
a surface storage facility. - "r
14. Municipal Separate Storm Sewer S stem
A stormwater collection system within an incorporated area of local self -government -such as a city or town.
15. No Exposure
A condition of no exposure means that all industrial materials and activities are protected by a storm
resistant shelter or acceptable storage containers to prevent exposure to rain, snow, snowmelt, or runoff.
Industrial materials or activities include, but are not limited to, material handling equipment or activities,
industrial machinery, raw materials, intermediate products, by-products, final products, or waste products.
DWQ may grant a No Exposure Exclusion from NPDES Stormwatcr Permitting requirements only if a
facility complies with the terms and conditions described in 40 CFR § 122.26(g)
16. Notice of Intent
The state application form which, when submitted to the Division, officially indicates the facility's notice of
intent to seek coverage under an Individual Permit.
17. Permittee
The owner or operator issued a certificate of coverage pursuant to this Individual Permit.
Part VI Page 2 of 4 Pages

Permit No. NCS000374
18. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch,
channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to waters
of the state.
19. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall. The time between this storm event and the previous
storm event measuring greater than 0.1 inches must be at least 72 hours. A single storm event may have a period of
no precipitation of up to 10 hours. For example, if it rains but,stops before producing,any collectable discharge, a
sample may be collected if the next rain producing a discharge begins within 10 hours
20. Representative Outfall_Status
When it is established that the discharge of stormwater-runoff from a single outfall is representative of the
discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall
status allows the permittee to perform analytical monitoring at a reduced number of outfalls.
21. Secondary Containment ' /�°'• - -!:
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year, 24-hour storm even,
22. Section 313 Water Priority Chemical
A chemical or chemical category which:
b n'
a. Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, alsojitled the'Emergency Planning and Community Right -
to -Know Act of 1986; 'J
b. Is present at or above'threshold-levels,at a facility subject to SARA title III, Section 313 reporting
requirements; and
C. Meets at least one ofthe following criteria:
(1) Is listed in appendix D of 40 CFR part 122 on Table II (organic priority.,pollutants), Table
III (certain metals,,cyanides, and phenols) or Table IV (certain toxic pollutants and
hazardous substances); . �.
(2) Is listehs'a•hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40,"_
CFR 1 16.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
23. Severe Property Damage
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss caused
by delays in production.
24. Sianificant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or production;
hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required to
report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes,
slag and sludge that have the potential to be released with stormwater discharges.
25. Significant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of
CERCLA (Ref: 40 CFR 302.4).
Part VI Page 3 of 4 Pages

Permit No. NCS000374
26. Stormwater Discharge Outfall (SDO)
The point of departure of stormwater from a discernible, confined, or discrete conveyance, including but not
limited to, storm sewer pipes, drainage ditches, channels, spillways, or channelized collection areas, from
which stormwater flows directly or indirectly into waters of the State of North Carolina.
27. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
28. Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacturing, processing or raw material storage arefirAt an industrial site. Facilities
considered to be engaged in "industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include discharges from facilities or activities excluded from the NPDES program.
29. Stormwater Pollution Prevention Plan .
A comprehensive site -specific plan which details measures and practices m to reduce stormwater pollution and
is based on an evaluation of the pollution potential of the site.
30. Total Maximum Daily Load (TMDL)
TMDLs are written plans for attaining and maintaining water quality standards, in all seasons, for a specific
water body and pollutant. (A list of approved TMDLs for the state of North Carolina can be found at
http://h2o.enr.state.ne.us/tmdl/)
31. Toxic Pollutant G
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
32.. Vehicle Maintenance Activity
Vehicle rehabilitation, ,mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or
airport deicing operations.
33. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or ice from its site of origin which can be seen with the unaided eye. . ,
34. .25-gear, 24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
PartV I Page 4 o f 4 Pages

STORMWATER POLLUTION PREVENTION PLAN
DEVELOPMENT AND IMPLEMENTATION
CERTIFICATION
North Carolina Division of Water Quality - Storm water Permitting Unit
Facility Name: Lumberton Mill
Permit Number: NCS000370
Location Address: 1000 E Noir St
Lumberton, NC 28359
County: Robeson
"I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all
attachments were developed and implemented under my direction or.supervision in accordance with a system
designed to assure that qualified personnel properly gather and evaluate the information required by the SPPP.
Based on my inquiry of the person or persons who manage the system, or.those persons directly responsible
for gathering the information, the information gathered is, to the best of my knowledge and belief, true,
accurate and complete."
And
"I certify. that the SPPP has been developed, signed and retained at the named facility location, and the SPPP
has been fully implemented at this facility location in accordance with the terms and conditions of the
stormwater discharge permit."
And
"I am aware that there are significant penalties for falsifying information, including the possibility of fines and
imprisonment for knowing violations."
Sign (according to permit signatory requirements) and return this Certification. DO NOT
SEND STORMWATER POLLUTION PREVENTION PLAN WITH THIS CERTIFICATION.
Signature
Print or type name of person signing above
Date _�111,120/O
91Mcss.,4,1,0 PIAvz:, &WfeX
Title
SPPP Certification 5/09

TABLE 3-1
GENERAL BEST MANAGEMENT PRACTICES
'Facility
Ogerahon°
`Best 1Vlanagement Prichce
x y
• Wherever practical, install.roofs over storage areas or the areas should be completely, enclosed.
Bulk Storage
. Divert off -site drainage aroundstorage areas.
• Make employees aware of the potential environmental problems caused when spilled products are not cleaned up immediately.
Drainage
• When oil or other pollutants are seen ponding in the secondary containment areas, remove and properly dispose of them to
Procedures
prevent pollutant discharge.
Transfer
• Train truck drivers and delivery personnel to comply with pollution prevention procedures and spill control measures.
Operations and
Perform vehicle and equipment maintenance indoors when possible. Use drip pans when changing fluids and immediately clean
In -Plant
any spillage.
Processes
• When feasible, protect loading and unloading areas with roofs over docks.
• Use berms or proper grading to divert stormwater from loading and unloading areas where spills are likely to occur.
Loading and
• Sweep loading areas to remove debris and other particulate contaminants.
Unloading
. Train truck drivers and delivery personnel on pollution prevention procedures.
• Prevent leaking trucks and railcars from entering or leaving the plant site until the leak is stopped.
• Place dumpsters under covered areas if possible. The area should be large enough to allow for emptying the dumpster without
exposing the contents to stormwater.
Waste Disposal
• If waste is stored outside, provide containers with tight fitting lids and keep them closed except when loading waste material
Practices
into the dumpster.
• Use compactors that are loaded from an end or from within a building as an alternative to dumpsters. (Stored waste materials
are less likely to come into contact with the rainfall.)
Spill Prevention
• Implement the Spill Prevention Policies and Procedures in Annex D of the One Plan.
48301SWP3 10 Buckeye Lumberton, Inc.
December 2003 One Plan - IV SWP3

Permit Coverage
I'C�I�lQ Renewal Application Form Permit Number
u.• National Pollutant Discharge Elimination System NCS000374
5tormwater Discharge Permit
The following is the information currently in our database for your facility. Please review this information_ carefully and
make all corrections/additions as necessary in the space provided to the right of the current information.
Owner Affiliation Information -Reissued Permit will ,be mailed to the owner address
Owner/ Organization Name: Bridgestone Americas Tire Operations LLCC((�uL,�
Owner Contact:
Mailing Address: 1000 E Noir St 1c�
Lumberton, NC 28359 L
Phone Number: [phone] 10 713 p
Fax Number:
E-mail address:
FacilitWPermit Contact Information
Facility Name:
Lumberton Mill
Facility Physical Address:
1000 E Noir St
Lumberton, NC 28359
Facility Contact:
Charles P Oxendine
Mailing Address:
PO Box 1139
Wilson, NC 27894-1139
Phone Number:
[phone]
Fax Number:
E-mail address:
Discharge Information
Receiving Stream Lumber River
i,
•
Stream Class: C;Sw
Basin: Lumber River Basins
Sub -Basin: 03-07-51
Number of Outfalls:u
7 -►vt�r
Impaired Waters/TMDL
Does this facility discharge to waters listed as impaired or waters with a finalized TMDL? 0 Yes ❑ No © Don't Know
( for information on these waters refer to http./lh2o.enr.state.nc.us/suilmpalred Waters TMULI )
CERTIFICATION
I certify that I am familiar with the information contained in the application and that to the best of my knowledge and
belief such information is true, complete and accurate.
Signature
/1�LEI ENL7iv
Print or type name of person signing above
Date
Title
Please return this completed renewal application form to: Stormwater Permitting Unit
Attn: Brian Lowther
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

5 Fall 11/21/05
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
2
clear
none
1
2
2
No
No
No
No
4
clear
none
1
2
2
No
No
No
No
6
clear
none
1
1
1
No
No
No
No
7
clear
none
1
2
2
No
No
No
No
8
clear
none
1
1
1
No
No
No
No
i Spring 6112/06
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
2
clear
none
1
1
2
No
No
No
No
4
clear
none
1
1
1
No
No
No
No
6
light brown
none
4
2
7
No
No
No
No
7
light brown
none
4
2
7
No
No
No
No
8
light brown
none
1 4
2
7
No
No
No
No
'Spring 6/15107
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
2
light tan brown
none
2
1
3
No
No
No
No
4
light tan brown
none
2
1
3
No
No
No
No
6
light brown
none
3
1
3
No
No
No
No
7
medium brown
I none
4
2
4
No
No
No
I Yes
8
medium brown
I none
4
2
1 4
No
No
No
I Yes
Deposition accounts for increased truck activity close
to the outfall. Truck activity increased due to removal of equipment from existing pulp mill facility.
7 Fall 10/26/07
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
1
none
none
1
1
1
No
No
No
No
2
light tan
none
2
1
3
No
No
No
No
4
none
none
2
1
1
No
No
No
No
5
li ht brown
none
1
1
1
No
No
No
No
6
light tan
none
2
1
2
No
No
No
No
7
light brown
none
2
2
3
No
No
No
No
8
light brown
none
3
2
2
No
No
No
No
clear and 5 is very cloudy
and 5 is surface covered with floating solids
I is no solids, 5 is extremely muddy

I Spring 5/28/08
Outfall No.
Color
Odor
Clarity
Floatin Solids
Sus ended Solids
Foam
Oil Sheen
Erosion
De osition
1
none
none
1
1
1
No
No
No
No
2
none
none
1
1
1
No
No
No
No
4
none
none
1
1
1
No
No
No
No
5
none
none
2
1
2
No
No
No
No
6
none
none
1
1
1
No
No
No
No
7
none
none
1
1
1
No
No
No
No
8
none
none
2
1
2
No
No
No
No
8 Fall 11/03/08
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
1
clear
none
1
1
1
No
No
No
No
2
light brown
none
1
2
3
No
No
No
No
4
medium brown
none
1
1
1
No
No
No
No
5
clear
none
1
1
1
No
No
No
No
6
light tan
none
2
1
3
No
No
No
No
7
light tan
none
1
1
1
1
No
No
No
No
8
medium brown
none
2
1
3
No
No
No
No
I Spring 4/14109
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
1
clear
none
1
1
1
No
No
No
No
2
clear
none
1
1
1
Yes
No
No
No
4
clear
none
1
3
1
Yes
No
No
No
5
li ht tan
none
2
3
1
No
No
No
No
6
medium brown
none
5
1
5
No
No
No
No
7
light tan
none
2
1
1
No
No
No
No
8
clear
none
3
1
3
No
No
No
No
Very small amount of foam present at the end of pipe line.
9 Fall 11/30/09
Outfall No.
Color
Odor
Clarity
Floating Solids
Suspended Solids
Foam
Oil Sheen
Erosion
Deposition
1
medium brown
none
2
1
2
No
No
No
No
2
light tan brown
none
1
1
1
No
No
No
No
4
light tan
none
1
1
1
No
No
No
No
5
light tan
none
1
1
1
No
No
No
No
6
light gray -green
none
2
1
2
No
No
No
No
7
light graUreen
none
3
2
3
No
No
No
No
8
light brown
none
2
1
1
No
No
No
No

Outfall
Flow
pH
TSS
Oil & Grease
Rainfall (in)
Outfall
Flow
pH
TSS
Oil & Grease
Rainfall (in)
Outfall
Flow
pH
TSS
Oil & Grease
Rainfall (in)
Outfall
Flow
pH
TSS
Oil & Grease
Rainfall (in)
Stormwater Data Table
2005 Fall 11/21/05 2006 Spring 6/12106
2 4 6 7 8 2 4 6
0.0086
1 0.0358
0.0139
0.0175
0.0093
7.51
7.28
7.19
7.4
7.25
48
19
41
7
29
<6.3
<6.1
<5.6
<18.2
<8.8
0.42
0.42
0.42
0.42
0.42
2007 Spring 6/15/07
2 4 6 7 8
0.0237
0.0997
0.0387
0.0486
0.0260
6.04
6.59
6.98
7.23
6.83
10.9
6.81
39.3
75.6
50.2
5.04
<5.00
<5.00
<5.00
<5.00
1.17
1.17
1.17
1.17
1.17
2008 Spring 5128108
2 4 6 7 8
0.0156
0.0660
0.0295
0.0590
0.0172
4.87
6.86
7.77
4.45
6.83
26.3
2.27
37.3
70.5
45.5
6.46
<5.00
<5.00
<5.00
<5.00
0.82
0.82
0.82
0.82
0.82
2009 Spring 4/14/09
2 4 6 7 8
0.0020
0.0085
0.0030
0.0042
1 0.0022
6.34
7
6.43
6.08
6.93
8.69
7.8
144
5.6
22.6
<5.00
<5.00
<5.00
<5.00
<5.00
0.1
0.1
0.1
0.1
0.1
7 8
0.0203
0.0852
0.0331
0.0415
0.0222
4.15
5.58
6.42
5.4
6.39
3
<0.1
118
153
146
29
27.8
24.8
20.9
23.4
1
1
1
1
1
2007 Fall 10/26/07
2 4 6 7 8
0.0152
0.0640
0.0288
0.0576
0.0168
5.8
6.7
7.9
7.2
8.4
148
1.2
92
127
145
7.7
6.3
<5.00
5.2
12.6
0.8
0.8
0.8
0.8
0.8
2008 Fall 11/03/08
2 4 6 7 8
0.0073
1 0.0307
0.0119
0.0149
0.0080
5.71
7.06
7.99
7.01
2.12
67.1
2.78
96.4
110
101
<5.00
<5.00
<5.00
<5.00
<5.00
0.36
0.36
0.36
1 0.36
1 0.36
2009 Fall 11/30/09
2 4 6 7 8
0.0020
0.0085
0.0033
0.0042
0.0022
6.28
7.14
8
7.42
6.79
8
<2.6
52.4
83.6
5.97
<5.00
<5.00
<5.00
<5.00
<5.00
0.1
0.1
0.1
0.1
1 0.1

i
May 18, 2004 3:34A psn.
Orawiq: 4VO M':.MfA7XYG
OFF SIZE
ST ORM,AIAai
WAIMLE O 5{'SG' .
/ OUTFALL 8
ca OUTFALL 7 LEGEND
W,FALL FMOM
ORSFIE IOCADON rt� ROOF ROOF ORYB
f)FW8 �
CWoP.{•T nAZARDDUIVAM E ' —x x— FENCE
^i. l'�An ACCUMAnONAlEA
METALC 2 OUTFALL 8 CAMERA
iRLLK OFF , M ryKl OA
=MEROON �> STAT STORAGE SURVEILLANCE
] `mR�uf OOO IOAOEA
POINT
aoRs oUTFALL9
0 3 =E
QUTFALL a O
co ROOF 7 1I RISK CONTROL
��.4�.}•
Ir coNc TROIIOR ioor 4
T Q ❑ Agry NOT f-GRA4BJ �,,. A�y{Tq�r - POINTS
'TTTT"• uSm FOFRE♦• Sly WPyF�,TaT4i'�
ROOF dyi�
"To � ,pApNG OOCX T9LOWOOM11d MRM
SLLOCE AAmC MALSIAl"MATBUtA � I
/ 7 m / '� iTPRAGEAI�A
OUTFALL2 [cowR. sTATK)N CO„Tr�aRMU p Q o / Q FIRE EXTINGUISHER
I � ® s o
BOCI(El E WM9ER,ON- WC ® �\\
FIRER!•NE STA5" �3-17 { I I
FIRE FI.Fp TA FROM" (`RElQ�A•L y`TAGING AST• NOTUSED R.FR I
HOUSE TAM AREA
❑ ❑ FORMER
' 3 © ROOF DM" o o O WASTE TREATMENT RANT /
AFAATIONF�OFO
�i��jL/ U
ICLOsr�OA'M • M� REERLINE OLA➢ 4uuu OFF�cE a1,ED.lO
I IEi) ]
. N3US
HOUS
E ouTFaLLi2 s QA:E
CANAL { CANAL ♦ ORMNAOErnAi LEORNFRE 4ENT 06puR.
NORTHOMM1J I SOUTH
ENMIO TRE - UM ENTRANCE - Dff
REFERENCE NOTE:
BASE MAP TAKEN FROM OVERALL LAYOUT MAP
PREPARED BY ANDERSON ENGINEERING & ASSOCIATES,
P.A. ANDERSON ENGINEERING PROJECT NUMBER 60-857,
DRANNG NUMBER 857—Li, DATED JULY 18, 2002.
SECURITY MAP
/ Q / BUCKEYE LUMBERTON, INC.
// // LUMBERTON, NORTH CAROLINA
SCALE r ' _ 20 APPROVED BY : C.Z.H. DRAWN BY: J.K.S.
DATESEPTEMBER 2003 DESIGNED BY : L.R.M. REVISED
PROJECT NUMBER DRAWING NO.
N 4 8 3— 0 3 �-J AiI KOM Nc 2527o FIGURE 3

I
I
R
W.'
':��y'
0.
,
s �p
,
' _ }p
r n
.::,�}
i �ti',
:1i
'y'
... I�";�
-.':1:
i•
i
� �.
I
Yqy
4.`-S�
...

12=��
NCDENR
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
December 7, 2009
Mr. Charles P Oxendine
Buckeye Lumberton,. Inc.
1000 E Noir St
Lumberton, NC 28358 '
Subject: NPDES Stormwater Permit Coverage Renewal
Lumberton Mill
Permit Number NCS000374
Robeson County
Dear Permittce:
Dee Freeman
Secretary
Your facility is currently covered for stormwater discharge under NPDES Permit NCS000374. This
permit expires on June 30, 2010. To assure consideration for continued coverage under your individual
permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit. Enclosed
you will find an individual permit Renewal Application Form, Supplemental Information request, and
Stormwater Pollution Prevention Plan Certification for your facility.
Filing the application form along with the requested supplemental information will constitute your
application for renewal of this permit. Until your permit renewal is completed and you receive a new
permit, please continue to comply with all conditions and monitoring requirements in your expired
NPDES stormwater permit.
The application and supplement must be completed and returned to DWQ by March 1, 2010. Failure to
request renewal within this time period will result in delay of your permit renewal and may result in a
civil assessment. Discharge of stormwater from your facility without coverage under a valid
stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and -could result in
assessments of civil penalties of up to $25,000 per day.
If you have any questions regarding permit renewal procedures please contact Brian Lowther of the
Stormwater Permitting Unit at (919)-807-6368 or [e-mail].
Cc: Central Files
SPU Files
Fayetteville Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617
Location: 512 N. Salisbury St. Raleigh, North Carolina 27604
Phone: [phone] FAX: [phone] Customer Service: 1-877.623-6748
Internet: www rimaterquality,org
An Equal Opportunity 1 Affirmalive Action Employer
Sincerely,
Bradley Bennett, Supervisor
Stormwater Permitting Unit
tick"',
DEC492;
6Eirl -' I i��>'�i�,:.. I�� .�l:l ���� t�l•ii�J�
One
NorthCaroliila
Naturalt,ff

Q�0FwArBq�o Permit Coverage
a Renewal Application Form
National Pollutant Discharge Elimination System Permit Number
Stormwater Discharge Permit NC5000374
The following is the information currently in our database for your facility. Please review this information carefully and
make all corrections/additions as necessary in the space provided to the right of the current information.
Owner Affiliation Information * Reissued Permit will be mailed to the owner address
Owner / Organization Name
Owner Contact:
Mailing Address:
Phone Number:
Fax Number:
E-mail address:
Bridgestone Americas Tire Operations LLC
1000 E Noir St
Lumberton, NC 28359
[phone]
Facilitv/Permit Contact Information
Facility Name: Lumberton Mill
Facility Physical Address: 1000 E Noir St'
Lumberton, NC 28359
Facility Contact: Charles P Oxendine
Mailing Address
Phone Number:
Fax Number:
E-mail address:
Discharge Information
Receiving Stream
Stream Class:
Basin:
Sub -Basin:
Number'of Outfalls:
PO Box 1139
Wilson, NC 27894-1139
[phone]
Lumber River
C;Sw,
Lumber River Basins
03-07-51
Impaired Waters/TMDL
Does this facility discharge to waters listed as impaired or waters with a finalized TMDL? ❑ Yes ❑ No, ❑ Don't Know
( for information on these waters refer to http://h2o. enr state. nc. us/su/Impaired Waters TMDL/ )
CERTIFICATION
I certify that I am familiar with the information contained in the application and that to the best of my knowledge and
belief such information is true, complete and accurate.
Signaturerrr c� '3 Date
Print or type name of person signing above
Title
Please return this completed renewal application form to: Stormwater Permitting Unit
Attn: Brian Lowther
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

�0F 1fV.4TLc�W
Mr. Charles Oxendine, Operations Manager
Buckeye Lumberton, Inc.
PO Box 1305
Lumberton, North Carolina 28359
Dear Mr. Oxendine:
Michael F. Easley, Governor
State of North Carolina
William G. Ross, Jr., Secretary
Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
April 21, 2005 "" =_v
APR 22 2005
DENR-FA2FT LLERSIO
NAL OFRCEE
Subject: Draft NPDES Stormwater Permit
Permit No. NCS000374
Buckeye Lumberton, Inc.
Robeson County
Enclosed with this letter is a copy of the draft stormwater permit for your facility. Please review the draft very
carefully to ensure thorough understanding of the conditions and requirements it contains.
The draft permit contains the following significant changes from this facility's current permit:
• In Part II, Sec. B, Fecal Coliform monitoring has been removed, and Oil and Grease monitoring has been
added.
• Total Flow monitoring has been removed. The permit still requires that Total Rainfall amount and Rainfall
Event Duration be recorded for each sampling event. This change is also based on the Division's revised
strategy for stormwater monitoring in renewal permits. Please note that the Stormwater Pollution
Prevention Plan (SPPP) site map must include drainage area for each outfall in acres and the
percentage of each drainage area that is impervious (see Part II, Sec. A).
• All analytical monitoring has changed from annual to semi-annual (once in the spring and once in the
fall). This change is based on the Division's revised strategy for stormwater monitoring in renewal permits
and makes stormwater discharge sampling frequency consistent with qualitative monitoring. Please note
that analytical monitoring must still be performed during a representative storm event (whereas qualitative
does not).
• Instead of "cut-off concentrations," the Division has incorporated benchmark values into the permit. These
benchmarks are not permit limits but should be used as guidelines for your facility's Stormwater Pollution
Prevention Plan (SPPP). If any measurements exceed benchmark values, your facility should evaluate the
effectiveness of its Best Management Practices (BMPs), review and/or update the SPPP, and document any
efforts to address stormwater contamination (see Part II, Sections B and D).
Please submit any comments to me no later than thirty (30) days following your receipt of the draft. Comments
should -be sent to the address listed at the bottom of this page. If no adverse comments are received from the public
or from you, this permit will likely be issued in about two months.
If you have any questions or comments concerning this draft permit, contact me at [phone] x 537 or
[e-mail].
Sincerely,
Jonathan A. Diggs
cc: Fayetteville Regional Office
Stormwater Permitting Unit
Attachments
North Carolina Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[phone]
FAX [phone]
On the Intemet at http://h2o.enr.state.nc.us/

NN A T, Michael F. Easley, Governor
10 60 RQG William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
1�-- Alan W. Klimek, R E. Director
> Division of Water Quality
Q Coleen Fl. Sullins, Deputy Director
Division of Water Quality
STAFF REVIEW AND EVALUATION FRO -
NPDES Stormwater Permit
Faciiity Name:
Buckeye Lumberton, Inc.
NPDES Permit Number:
NCS000374
Facility Location:
1000 East Noir Street, Lumberton, NC 28358 Robeson County
Type of Activity:
Pulp and paper manufacture
SIC Code (if applicable):
2611
Receiving Streams:
Lumber River
River Basin:
Lumber River Basin, subbasin 03-07-51
Stream Classification:
C SW
Proposed Permit Requirements:
See attached draft permit
Compliance Schedule:
See Part V, Section A of the attached draft permit
Basis for Monitoring:
See attached Monitoring Data Analysis. Removed fecal coliform
monitoring. There are no obvious sources of fecal coliform at the site,
and all but one of the samples were below the bechmark value. Oil and
grease monitoring added to address petroleum products stored onsite.
Basis for Other Requirements:
Monitoring frequency changed to semi-annually in years 1-5.
Benchmarks for analytical monitoring have been added to provide
incentive for facilities to incorporate BMPs to reduce pollutants that
exceed benchmark values. These benchmarks are not cut-off
concentrations for monitoring, nor are they permit limits.
Total Flow monitoring has been removed. The permit still requires
Total Rainfall amount and Rainfall Event Duration be recorded for each
sampling event. This change is also based on the Division's revised
strategy for stormwater monitoring in renewal permits. Please note that
the Stormwater Pollution Prevention Plan (SPPP) site map must include
drainage area for each outfall in acres and the percentage of each
drainage area that is impervious (see Part 11, Sec. A).
Response Requested by (Date): May 20, 2005
Central Office Staff Contact: Jonathan Diggs, [phone], ext. 537
DOCUMENTS REVIEWED
NPDES Stormwater Permit Application Materials
S/W Permit File
Analytical & Qualitative Monitoring Results summary
The NC Integrated Report [305(b) and 303(d) List] (2004 Draft)
2003 Lumber River Basinwide Water Quality Plan
N. C. Division of Water Quality 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [phone]
MENR
Customer Service
1-877-623-6748

NCS000370
Central Office Review Summary:
Since last renewal, the company has cleaned out and shut down their wastewater treatment plant. Since the WWTP
is no longer in operation, the site does not generate, store, or transport residual solids from the biological treatment
process. Generation of used oils and lubricants has significantly decreased. Storage of diesel and gasoline has been
eliminated.
Qualitative Monitoring Results: Permittee sent results from 2000-03. No observed problems, except in outfalls 6
and 7, where suspended solids were present on 11/21/2002. These solids were probably the result of construction
work to complete a new warehouse in the vicinity. Warehouse was to be completed in March 2003.
Analytical Monitoring: See attached Monitoring Data Analysis. Permittee reported that the following chemicals
were stored externally: propane, 70% hydrogen peroxide, #4 fuel oil, 93% sulfuric acid, BL-1544 blend of amines,
BL-110 chelant polymer solution, B-120, petroleum, oils, and lubricants. Oil and grease monitoring added to
address oil products stored onsite.
The facility drains to the Lumberton River, which currently has a TMDL for mercury. Mercury monitoring was not
added because of the difficulty of obtaining accurate measurements and because mercury contamination occurs from
atmospheric deposition. This strategy was approved by the TMDL unit in the Central Office (Michelle Woolfolk).
Total Flow monitoring has been removed. The permit still requires Total Rainfall amount and Rainfall Event
Duration be recorded for each sampling event. This change is also based on the Division's revised strategy for
stormwater monitoring in renewal permits. Please note that the Stormwater Pollution Prevention Plan (SPPP) site
map must include drainage area for each outfall in acres and the percentage of each drainage area that is impervious
(see Part 11, Sec. A).
Recommendation: Based on the documents reviewed, the application information submitted on January 30, 2004 is
sufficient to issue an Individual Stormwater Permit.
Prepared by (Signature)
Stormwater Permitting Unit Supervisor
Date
Date
Concurrence by Regional Office �1 Date
Water Quality Supervisor Date

NCS000370
Regional Office Staff Comments

Stormwater Analytical Sampling
611412000
fecal coliform
Monitor
Flow (MG)
TSS (mg/L)
pH
(col/100mL)
Outfall 1
now
0.024
-
-
-
Outfall 2
flow, TSS, pH,
0.008
56.8
6.1
-
Outfall 4
flow, TSS, pH, fecal coliform
0.034
1.6
6.4
5
Outfall 5
flow
0.012
-
-
-
Outfall 6
flow, TSS, pH, fecal coliform
0.013
13.6
6.9
773
Outfall 7
flow, TSS, pH, fecal coliform
0.017
17.6
7.1
1282
Outfall 8
flow, TSS, pH
0.009
0.8
7.8
1111912003
Outfall 2
flow, TSS, pH,
0.014
14.0
6.9
-
Outfall 4
flow, TSS, pH, fecal coliform
0.060
6.0
7.1
200.0
Outfall 6
flow, TSS, pH, fecal coliform
0.023
180.0
7.0
790.0
Outfall 7
flow, TSS, pH, fecal coliform
0.029
6.0
6.8
10.0
Outfall 8
flow, TSS, pH
0.016
7.5
7.1
-
Cutoff Concentrations 100 6.0 - 9.0

Buckeye Lumberton Inc.
Stormwater Permit No. NCS000374
Visual Monitoring Results
Outfall Number Parameters Surveved Observations Date Monitoring Conducted
Color, Odor, Clarity, Floating
Solids, Suspended Solids,
Foam, Oil Sheen, Other
1,2,4,5,6,7,8
Indicators of Pollution
Not Present
6/14/2000
1,2,4,5,6,7,8
Not Present
11/30/2000
1,2,4,5,6,7,8
Not Present 6/22/2001
1,2,4,5,6,7,8
Not Present 11/30/2001
1,2,4,5,6,7,8 Not Present 5/30/2002
1,2,4,5,*6,-7,8 Suspended Solids 11/21/2002
1,2,4,5,6,7,8
Not Present
4/812003
1,2,4,5,6,7,8
Not Present
9/23/2003
Comments: 11/21/02 sampling showed Suspended solids in outfalls 6 and 7 due to construction work going on to
build a new warehouse in the vicinity. Warehouse completion date and clean up targeted for March 2003.

NCS000374
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT NO. NCS000374
TO DISCHARGE STORMWATER UNDER THE
4
Incompliance with the provisions of North Carolina General Statute 443-215.1, other lawful
standards and regulations promulgated and adopted by the,North Carolina Environmental
Management Commission, and the Federal Water Poll1""M n Control Act, as amended,'
Buckeye umberton, Inc.
is hereby authorized to discharge=stormwater from a facility located at
Buckeye Lumberton Inc.
11600 East Noir Street
Lumberton, NC
Robeson County
to receiving waters designated as Lumber River, a class C Sw stream, in the Lumber River Basin
in accordance with the discharge limitations, monitoring requirements, and other conditions set
forth in Parts I, II, III, IV, V and VI hereof.
This permit shall become effective Month Day, 2005.
This permit and the authorization to discharge shall expire at midnight on Month Day, 2010.
Signed this day Month Day, 2005.
r
for Alan W. Klimek, P.E., Director.
Division of Water Quality
By the Authority of the Environmental Management Commission

Permit No. NCS000374
TABLE OF CONTENTS
PART I
INTRODUCTION
Section A:
Individual Permit Coverage
Section B:
Permitted Activities
Section C:
Location Map;
PART II
MONITORING, CONTROLS, AND LIMITATIONS
DISCHARGES
Section A:
Stormwater Pollution Prevention Plan';>
Section B:
Analytical Monitoring Re uirements
� 9
Section C:
Qualitative Monitorin*Reaquirements,
PERMITTED
Section D: On -Site Vehicle Maintepance Monitoring Requirements
PART III STANDARD CONDITIONS
Section A: Compliance
and Liability
1.
Compliance Schedule
2.
Duty to Comply
3.
Duty to Mitigate
4.
Civil and Criminal Liability
5.
Oil and Hazardous Substance Liability
6.
Property Rights
7.
Severability
8.
Duty to Provide Information
9.
Penalties for Tampering
10.
Penalties for Falsification of Reports
Section B: General Conditions .
1.
Individual Permit Expiration
2.
Transfers

Permit No. NCS000374
3. Signatory Requirements
4. Individual Permit Modification, Revocation and Reissuance, or
Termination
5. Permit Actions
Section C: Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D: Monitoring and Records
1. Representative Sampling
2. Recording Results
3. Flow Measurements
4. Test Procedures
5. Representative Outf all
6. Record`Retent'on
7. Inspect i Iandlntry
Section E: Reporting Req� uirements
1. DiscliargeD Monitoring Reports
2. Submi ' mg Reports
3. Availability of Reports
4. Non-Stormwater Discharges
5. Planned Changes
6. Anticipated Noncompliance
7. Bypass
8. Twenty-four Hour Reporting
9. Other Noncompliance
10..Other Information
PART IV - LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
PART VI DEFINITIONS
ii

Permit No. NCS000374 I `
PART I INTRODUCTION
SECTION A: INDIVIDUAL PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater associated with industrial activity. Such
discharges shall be controlled, limited and monitored as specified in this permit.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee s authorized to discharge
^ AQiV.,
stormwater to the surface waters of North Carolina or separatetorm sewer system which has
been adequately treated and managed in accordance wVe terms,and conditions of this
individual permit. All discharges shall be in accordancewith the conditions of this permit.
An other Dint source discharge to surface waters afthe state is prohibited unless it is an
allowable on-stormwater discharge or is coveted y ano#1 er permit, authorization or approval.
This permit does not relieve the permittee, o responsibility for compliance with any other
applicable federal, state, or local%w, rule,3s#andard, ordinance, order, judgment, or decree.
Part I Page I of 2

' SECTION C: LOCATION MAP
Permit No. NCS000374
Part I Page 2 of 2

Permit No. NCS000374
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR
PERMITTED DISCHARGES
SECTION A: STORMWATER POLLUTION PREVENTION PLAN
The permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as
the Plan. This Plan shall be considered public information in accordance with Part III, Standard
Conditions, Section E, Paragraph 3 of this individual permit. The Plan shall include, at a
minimum, the following items:
1. Site Plan. The site plan shall'provide a description of. the physical facility and the
potential pollutant sources which may be expected to/c\ontribute to contamination of
stormwater discharges. The site plan shall contain thefollowing:
a. A general location map (USGS quadranlemap or appropriately drafted
equivalent map), showing the facility's location in relation to transportation
routes and surface waters, the name:ofthe receiving water(s) to which the
stormwater outfall(s) discharges, o�'if'thdischarge is to a municipal separate
me storm sewer system, the naof the municipality and the ultimate receiving
waters; and accurate latitude an� gitude of the point(s) of discharge.
b. A narrative descripti6n;;of st6r ge practices, loading and unloading activities,
outdoor process area" sad, usVor particulate generating or control processes, and
waste disposal p actices. +
C. A site map dra mtlto scale with the following items:
(1) Distance legend and north arrow
(2) Location of industrial activities (including storage of materials,
disposal areas, process areas and loading and unloading areas)
(3) Drainage structures
(4) Delineated drainage areas for each outfall
(S) Drainage area for each outfall in acres and percentage of
each drainage area that is impervious
(6) Building locations
(7) Existing BMPs and impervious surfaces
(8) For each outfall, a narrative description of the potential pollutants that
could be expected to be present in the stormwater discharge.
d. A list of significant spills or leaks of pollutants that have occurred at the facility
during the 3 previous years and any corrective actions taken to mitigate spill
impacts.
e. Certification that the stormwater outfalls have been evaluated for the presence of
non-stormwater discharges. The certification statement will be signed in
accordance with the requirements found in Part III, Standard Conditions, Section
B, Paragraph 3.
Part 11 Page 1 of 7

Permit No. NCS000374
2. Stormwater Management Plan. The stormwater management plan shall contain a
narrative description of the materials management practices employed that control or
minimize the exposure of significant materials to stormwater, including structural and
nonstructural measures. The stormwater management plan, at a minimum, shall
incorporate the following:
a. Feasibility Study. A review of the technical and economic feasibility of changing
the methods of operations and/or storage practices to eliminate or reduce exposure
of materials and processes to stormwater. Wherever practical, the permittee shall
prevent exposure of all storage areas, material handling operations, and
manufacturing or fueling operations. In areas where elimination of exposure is
not practical, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from azeasFof potential contamination.
b. Secondary Containment Schedule. A schedule to provide secondary containment
for bulk storage of liquid materials, storag'df�Section 313 of Title III of the
Superfund Amendments and Reauthorizatioh'4 ct (SARA) water priority
chemicals, or storage of hazardous substances to prevent leaks and spills from
contaminating stormwater runoff. If thsecondary containment devices are
connected directly to stomp water conveyance systems, the connection shall be
controlled by manually acttvated4va1ves or other similar devices [which shall be
secured with a locking mechanism] and any stormwater that accumulates in the
containment area shallbe"at a minimum visually observed for color, foam, outfall
staining, visible sheens anddry weather flow, prior to release of the accumulated
stormwater. Accumul�ed stormwater shall be released if found to be
uncontaminatedibv the material stored within the containment area. Records
documenting th 4 dividual making the observation, the description of the
accumulated stormwater and the date and time of the release shall be kept for a
period of five years.
C. BMP Summary. A narrative description shall be provided of Best Management
Practices (BMPs) to be considered such as, but not limited to, oil and grease
separation, debris control, vegetative filter strips, infiltration and stormwater
detention or retention, where necessary. The need for structural BMPs shall be
based on the assessment of potential of sources to contribute significant quantities
of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP)
shall incorporate an assessment of potential pollutant sources based on a materials
inventory of the facility. Facility personnel (or team) responsible for implementing the
SPRP shall be identified. A responsible person shall be on -site at all times during facility
operations that have the potential to contaminate stormwater runoff through spills or
exposure of materials associated with the facility operations. The SPRP must be site
stormwater specific. Therefore, a SPCC plan may be a component of the SPRP, but may
Part 11 Page 2 of 7

Permit No. NCS000374
not be sufficient to completely address the stormwater aspects of the SPRP. The common
elements of the SPCC withthe SPRP may be incorporated by reference into the SPRP.
4. Preventative Maintenance and Good Housekeeping Program. A preventative
maintenance program shall be developed. The program shall document schedules of
inspections and maintenance activities of stormwater control systems, plant equipment
and systems. Inspection of 'material handling areas and regular cleaning schedules of
these areas shall be incorporated into the program.
S. Employee Training. Training schedules shall be developed and training provided at a
minimum on an annual Basis on proper spill response and cleanup procedures and
preventative maintenance activities for all personnel involved in any of the facility's
operations that have the potential to contaminate stormw ter runoff. Facility personnel
(or team) responsible for implementing the training shall,be identified.
6. Responsible Party. The Stormwater Poll
position(s) responsible for the overall co(
revision to the Plan. Responsibilities for
and position assignments provided.
7. Plan Amendment. The permittee
design, construction, operation,,o
potential for the discharge 6f poll
Prevention Plan shall be reviewer
ion`Pl'an shall identify a specific
v elopment, implementation, and
its of the Plan shall be documented
-nd1he Plan whenever there is a change in
lance which has a significant effect on the
surface waters. The Stormwater Pollution
ated on an annual basis.
The Director may notify the permittee when the Plan does not meet one or more of the
minimum requiremettsloLthhe ermit. Within 30 days of such notice, the permittee shall
submit a time schedule;t&tlie Director for modifying the Plan to meet minimum
requirements. The permittee shall provide certification in writing (in accordance with
Part III, Standard Conditions, Section B, Paragraph 3) to the Director that the changes
have been made.
8. Facility Inspection Program. Facilities are required to inspect all stormwater systems on
at least a semiannual schedule, once in the fall (September -November) and once in the
spring (April - June). The inspection and any subsequent maintenance activities
performed shall be documented, recording date and time of inspection, individual(s)
making the inspection and a narrative description of the facility's stormwater control .
systems, plant equipment and systems. Records of these inspections shall be incorporated
into the Stormwater Pollution Prevention Plan.
Stormwater discharge characteristic monitoring as required in Part H of this permit shall
be performed in addition to facility inspections.
9. Implementation. The permittee shall document all monitoring, measurements,
inspections and maintenance activities and training provided to employees, including the
log of the sampling data and of activities taken to implement BMPs associated with the
industrial activities, including vehicle maintenance activities. Such documentation shall
Part II Page 3 of 7

Permit No. NCS000374
be kept on -site for a period of five years and made available to the Director or his
authorized representative immediately upon request.
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
During the period beginning on the effective date of the permit and lasting until expiration, the
permittee is authorized to discharge stormwater subject to the provisions of this permit.
Analytical monitoring of stormwater discharges shall be performed as specified below in Table
All analytical monitoring shall be performed during a i
monitoring will result in a minimum of nine analytical
of the permit at stormwater discharge outfalls 2, 4, 6,
minimum nine analytical samplings in accordance wit]
Monitoring results shall be compared to the benchmaf.
values in Table 3 are not permit limits but shouldibe
Stormwater Pollution Prevention Plan (SPPP). e p`(`
benchmark exceedances and evaluate the effectiveness
review and/or update the SPPP and document any; f. c
Table 1. Analytical Mon
ts"
storm event. The required
ng conducted over the term
)er ittee shall complete the
specified below in Table 2.
flues in Table 3. The benchmark
l 4guidelines for the permittee's
i4e shall evaluate the sources of any
any site BMPs. The permittee shall
to address stormwater contamination.
Ydi i k 4i � 1 J r
D�schargel`f;,li� ;'
n I i
r'h:r'E'� 'i;'
i 'nMf i
'Measurement Frequency/;
'Sample
i4 Sample;'
rtiRr,�P
' ,rut
� ``,�r� ,r ,� ,�
2.
a:.
` 3
n
�iCbaracteristics ,.
r
=�E 6,
�u.;�r �F
.,�rT �..
oca;
..Ltio
Total Suspended Solids ;
,
Semi-annuall
Grab
SDO
Oil and Grease
m
Semi-annually
Grab
SDO
H
standard
Semi-annually
Grab
SDO
Total Rainfall
inches
Semi -Annually-
-
Rainfall Event Duration
minutes
I Semi -Annually-
-
Footnotes:
I Measurement Frequency: All analytical monitoring will be performed twice per year, once in the spring (April -
June) and once in the fall (September - November). See Table 2 for schedule of monitoring periods.
2 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. If the detention pond discharges only in response
to a storm event exceeding a ten-year design storm, then no analytical monitoring is required and only qualitative
monitoring shall be performed.
3 Sample Location: Samples shall be collected at stormwater discharge outfalls 2, 4, 6, 7, and 8.
Part II Page 4 of 7.

Permit No. NC5000374
Table 2. Monitoring Schedule
..", i-I - period;.
t
Number
A
Year I — Fall
I
September 1, 2005
November 30, 2005
Year 2 — Spring
2
April 1, 2006
June 30, 2006
Year 2 — Fall
3
September 1, 2006
November 30, 2006
Year 3 — Spring
4
April 1, 2007
June 30, 2007
Year 3 — Fall
5
September 1, 2007
November 30, 2007
Year 4 — Spring
6
April 1, 2008
June 30, 2008
Year 4 — Fall
7
September 1, 2008
November 30, 2008
Year 5 — Spring
8
April 1, 2009
June 30, 2009
Year 5 — Fall
9
September 1,20,Q9
November 30, 2009
Footnote
Maintain semi-annual monitoring during permit renewal process.
)kLi
Table 3., Benchmark Values for Analytical Monitoring
;.
"-7
M
nits
cnch"mar,;Digthir&,chafit
Total Suspended Solids
100
Oil and Grease
mg li.r
30
pH 11ZIN
NWO
d
t stanRd
6 -9
SECTION C: QUALITATIVE MONITORING REQUIREMENTS
Qualitative monitoring requirds,d visual inspection of each stormwater outfall regardless of
representative outfall status and shall be performed as specified below in Table 4. Qualitative
monitoring is for the purpose of evaluating the effectiveness of the Stormwater Pollution
Prevention Plan (SPPP) and assessing new sources of stormwater pollution. No analytical tests
are required. Qualitative monitoring of stormwater outfalls is performed when stormwater
discharge occurs but does not need to be performed during a representative storm event.
In the event an atypical condition is noted at a stormwater discharge outfall, the Permittee shall'
document the suspected cause of the condition and any actions taken in response to the
discovery. This documentation will be maintained with the Stormwater Pollution Prevention
Plan.
All qualitative monitoring will be performed twice per year, once in the spring (April - June) and
once in the fall (September - November).
Part 11 Page 5 of 7

Permit No. NCS000374
Table 4. Oualitative Monitoring Reauirements
Discharge`Charaete'ristics '
(i?
"A '; Frekquency' ���
``'Monitoring
rLocat�on,,��,' ,
Color
Semi -Annual
SDO
Odor
Semi -Annual
SDO
Clarity
Semi -Annual
SDO
Floating Solids
Semi -Annual
SDO
Suspended Solids
Semi -Annual
SDO
Foam
Semi -Annual
SDO
Oil Sheen
Semi -Annual
SDO
Other obvious indicators
of stormwater pollution
Semi -Annual
SD
Footnotes: R, .
l Monitoring Location: Qualitative monitoring shall be performed at'i'ach stormwater discharge outfall (SDO) .
regardless of representative outfall status.
SECTION D: ON -SITE VEHICLE M_ AINT'EN. CE MONITORING REQUIREMENTS
Facilities that have any vehicle ma tenance%ctivity occurring on -site that uses more than 55
gallons of new motor oil per month wheriaveraged over the calendar year shall perform
tom:
analytical monitoring as specified below xn Table 5. This monitoring shall be perfonned at all
outfalls that discharge stormwater runoff from vehicle maintenance areas.
All analytical monitoring shall"be performed during a representative storm event. The required
monitoring will result in a minimum of nine analytical samplings being conducted over the term
of the permit at each stormwater discharge outfall (SDO) that discharges stormwater runoff from
vehicle maintenance areas. The permittee shall complete the minimum nine analytical samplings
in accordance with the schedule specified in Table 2 (Section B).."
Monitoring results shall be compared to the benchmark values in Table 6. The benchmark
values in Table 6 are not permit limits but should be used as guidelines for the permittee's
Stormwater Pollution Prevention Plan ($PPP). The permittee shall evaluate the sources of any
benchmark exceedances and evaluate the effectiveness of any site BMPs. The permittee shall
review and/or update the SPPP and document any efforts to address stormwater contamination.
Part 11 Page 6 of 7

Permit No. NCS000374
Table 5. Analvtical Monitoring Reauirements for On -Site Vehicle Maintenance
Deschr a Cha�racter�stics
g
�,' .�ki .. � ', � " �,
rII` ',� Units`
3
�" �� � , i �
Measureme t
:. 'Fre uenc
_Sample 1'
t Z e2 �,
"
�fSample
3 .
L4Catlon ;
H
standard
Semi-annually
Grab
SDO
Oil and Grease
mg/1
Semi-annually
. Grab
SDO
Total suspended Solids
mo
Semi-annually
Grab
SDO
New Motor Oil Usagegallons/month
Semi-annually
Estimate
-
Total Rainfall
inches
Semi-annually
Rainfall Event Duration
minutes
Semi-annually
Footnotes:
l Measurement Frequency: All analytical monitoring will be pe ormed.,twice per year, once in the spring (April -.
June) and once in the fall (September - November). See Table 2 (Section B schedule of monitoring periods.
2 If the stormwater runoff is controlled by a stormwater detention -pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. if the`detention pond discharges only in response
/. ?*, .,,?. \ ✓
to a storm event exceeding a ten-year design storm, then>no.analyttical,monitoring is required and only qualitative
monitoring shall be performed.
3 Sample Location: Samples shall be collected at stormawater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle mamtenance activities occur.
Table 6. Benchmark Values'#oreVehicle Maintenance Analytical Monitoring
`
r Units ' "T
Benchmark
!„ ; gip,Cliaracteristus,�f s
ftit i
;,,��, , ,.
Total Suspended Solids ;+
mg/L
100
Oil and Grease
mg/L
30
pH
standard
6-9
Part iI Page 7.of 7

DRAFT Permit No. NCS000374
PART III STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
1. Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing Facilities: The Stormwater Pollution Prevention. Plan shall be developed and implemented within
12 months of the effective date of the initial permit and updated thereafter on an annual basis. Secondary
containment, as specified in Part 11, Section A, Paragraph 2(b) of this permit, shall be accomplished within
12 months of the effective date of the initial permit issuance.
Proposed Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented prior to
the beginning of discharges from the operation of the industrial activity and be updated thereafter on an
annual basis. Secondary containment, as specified in Part II, Section A, Paragraph 2(b) of this permit shall
be accomplished prior to the beginning of discharges from the operation of the industrial activity.
2. Duo to Comp
IY
The permittee must comply with all conditions of this individual permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit upon renewal application.
a. The permittee shall comply with standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants within the time provided in the regulations that establish these
standards or prohibitions, even if the permit has not yet been modified to incorporate the
requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $27,500 per day for each violation. Any person who negligently violates any
permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than I year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit condition
may be assessed anadministrative penalty not to exceed $11,000 per violation with the maximum
amount not to exceed $137,500. [Ref: Section 309 of the Federal Act 33 USC 1319 and 40 CFR
122.41(a).]
C. Under state law, a daily civil penalty of not more than twenty-five thousand dollars (525,000) per'
violation may be assessed against any person who violates or fails to act in accordance with the
terms, conditions, or requirements of a permit. [Ref. North Carolina General Statutes 143-
215.6A]
d. Any person may be assessed an administrative penalty by the Director for violating section 301, .
302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing any
of such sections in a permit issued under section 402 of the Act. Administrative penalties for Class
I violations are not to exceed $11,000 per violation, with the maximum amount of any Class I
penalty assessed not to exceed $27,500. Penalties for Class 1I violations are not to exceed $11,000
per day for each day during which the violation continues, with the maximum amount of any Class
I penalty not to exceed V 37,500.
Part III Page 1 of 8 Pages.

DRAFT Permit No. NCS000374
3. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the environment.
4. Civil and Criminal Liability
Except as provided in Part III, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215,3, I43-215.6A, 143-215.613, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be .
temporarily suspended.
5. Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permittee is or may be subject to
under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USC 1321.
6. Property Rights
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
7. Severabiliri
The provisions of this individual permit are severable, and if any provision of this individual permit, or the .
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall furnish to the Director, within a reasonable time, any information which the Director.
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit., The
permittee shall also furnish to the Director upon request, copies of records required to be kept by this.
individual permit..
9.. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate,
any monitoring device or method required to be maintained under this individual permit shall, upon
conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more
than two years per violation, or by both. If a conviction of a person is for a violation committed after a first
conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per day of
violation, or by imprisonment of not more than 4 years, or both.
10. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this individual
Part III Page 2 of 8 Pages

DRAFT Permit No. NCS000374
permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be
punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years
per violation, or by both. ,
SECTION B: GENERAL CONDITIONS
1. Individual Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the permittee shall submit forms and fees as are
required by the agency authorized to issue permits no later than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will be
subjected to enforcement procedures as provided in NCGS § 143-2153.6 and 33 USC 1251 et. seq.
2. Transfers
This permit is not transferable to any person except after notice to and approval by the Director. The .
Director may require modification or revocation and reissuance of the permit to change the name and
incorporate such other requirements as may be necessary under the Clean Water Act..Permittee is required
to notify the Division in writing in the event the permitted facility is sold or closed.
3. Signatory Requirements
All applications, reports, or information submitted to the Director shall be signed and certified.
a. All applications to be covered under this individual permit shall be signed as follows: ,
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the
manager of one or more manufacturing production or operating facilities employing more
than 250 persons or having gross annual sales or expenditures exceeding 25 million (in
second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official.
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if:
(1) The authorization is made in writing by a person described above;
.(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for environmental
Part Ill Page 3 of 8 Pages

DRAFT Permit No. NCS000374
matters for the company. (A duly authorized representative may thus be either a named
individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
C. Any person signing a document under paragraphs a. or b. of this section shall make the following
certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false. information,
including the possibility of fines and imprisonment for knowing violations."
4. Individual Permit Modification, Revocation and Reissuance, or Termination
The issuance of this individual permit does not prohibit the Director from reopening and modifying the
individual permit, revoking and reissuing the individual permit, or terminating the individual permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122
and 123; Title 15A of the North Carolina Administrative Code, Subchapter 21-1.0100; and North Carolina
General Statute 143-215.1 et. al.
5. Permit Actions
The permit may be modified, revoked and reissued, or terminated for cause. The notification of planned
changes or anticipated noncompliance does not stay any individual permit condition.
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
1. Pro er Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the permittee to achieve compliance with
the conditions of this individual permit, Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
2. Need to Halt or Reduce Not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this individual permit.
3. BvDassing of Stormwater Control Facilities
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless:
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
b. There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
Part III Page 4 of 8 Pages

DRAFT Permit No. NCS000374
weather, This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal
periods of equipment downtime or preventive maintenance; and
C. The permittee submitted notices as required under, Part III, Section E of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may approve an
anticipated bypass after considering its adverse effects.
SECTION D: MONITORING AND RECORDS
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and
nature of the permitted discharge. Analytical sampling shall be performed during a representative storm
event. Samples shall be taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of water, or substance.
Monitoring points as specified in this permit shall not be changed without notification to and approval of
the Director.
2. Recording Results
For each measurement, sample, inspection or maintenance activity performed or collected pursuant to the
requirements of this individual permit, the permittee shall record the following information:
a. The date, exact place, and time of sampling, measurements, inspection or maintenance activity;
b.. The individual(s) who performed the sampling, measurements, inspection or maintenance activity;
C. The date(s) analyses.were performed; .
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f. The results of such analyses.
3. Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136.
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower reporting level of the procedure.
Part III Page 5 of 8 Pages

DRAFT Permit No. NCS000374
5. Representative_Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status. If it is
established that the stonmwater discharges are substantially identical and the permittee is granted
representative outfall status, then sampling requirements may be performed at a reduced number of outfalls.
6. Records Retention
Visual monitoring shall be documented and records maintained at the facility along with the Stormwater
Pollution Prevention Plan. Copies of analytical monitoring results shall also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous monitoring instrumentation, and copies of all
reports required by this individual permit for a period of at least 5 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time.
7. Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director), or in the case of a facility which discharges through a municipal
separate storm sewer system, an authorized representative of a municipal operator or the separate storm
sewer system receiving the discharge, upon the presentation of credentials and other documents as may be
required by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or conducted,
or where records must be kept under the conditions of this individual permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of..
this individual permit;
C. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment),
practices, or operations regulated or required under this individual permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
SECTION E: REPORTING REQUIREMENTS
1. Discharge Monitoring Reports
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be received by the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
2. Submitting Reports
Duplicate signed copies of all reports required herein, shall be submitted to the following address:
Division of Water Quality
Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Part III Page 6 of 8 Pages

DRAFT Permit No. NCS000374
3. Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection
at the offices of the Division of Water Quality. As required by the Act, analytical data shall not be .
considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.6E or in Section 309 of the Federal Act.
4. Non-Stormwater Discharges
If the storm event monitored in accordance with this individual permit coincides with a non-stormwater
discharge, the perminee shall separately monitor all parameters as required under the non-stormwater,
discharge permit and provide this information with the stormwater discharge monitoring report.
5. Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which could significantly alter the nature or quantity of pollutants discharged. This notification
requirement includes pollutants which are not specifically listed in the individual permit or subject to
notification requirements under 40 CPR Part 122.42 (a).
6. Anticipated Noncompliance
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which may result in noncompliance with the individual permit requirements. .
7. Bypass
a. Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit
prior notice, if possible at least ten days before the date of the bypass; including an evaluation of
the anticipated quality and affect of the bypass.
b. Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass.
8. Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been received
.within 24 hours.
9. .-Other Noncompliance
The permittee shall report all instances of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
Part I Page 7 of 8 Pages

DRAFT Permit No. NCS000374

DRAFT Permit No. NCSOOOXXX
PART IV LIMITATIONS REOPENER
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) (c), and (d), 304(b) (2) and
307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or approved:
a.' Contains different conditions or is otherwise more stringent than any effluent limitation in the individual
permit; or
b. Controls any pollutant not limited in the individual permit.
The individual permit as modified or reissued under this paragraph shall also contain any other requirements in the .
Act then applicable.
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
.REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed by
the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause this
Division to initiate action to revoke the Individual Permit.
PART VI DEFINITIONS
1. Act
See Clean Water Act. '
2. Arithmetic Mean
The arithmetic mean of any set of values is the summation of the individual values divided by the number of
individual values.
3. Allowable Non-Stormwater Discharges
This permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) ' All other discharges that are authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant.
flushings, water from footing drains, flows from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -fighting training.
4. Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure.
Parts IV, V and VI Page l of 5

DRAFT Permit No. NCS000374
5 Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
6. Bulk Storage of Liquid Products
Liquid raw materials, manufactured products, waste materials or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons. .
7. Clean Water Act
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, et. seq.
$. Division or DWQ
The Division of Water Quality, Department of Environment and Natural Resources.
9. Director,
The Director of the Division of Water Quality, the permit issuing authority.
10. EMC
The North Carolina Environmental Management Commission.
11. Grab Sample
An individual sample collected instantaneously. Grab samples that will be directly analyzed or qualitatively
monitored must be taken within the first 30 minutes of discharge.
12. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the Clean Water Act.
13. Landfill ,
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility or.
a surface storage facility...
14. Municipal Separate Storm Sewer System
A stormwater collection system within an incorporated area of local self-government such as a city or town.
15. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsoil or similar naturally -occurring surface materials that are not disturbed by mining operations.
Part VI Page 2 of 5 Pages

' DRAFT Permit No. NCS000374
16. Permittee
The owner or operator issued a permit pursuant to this individual permit.
17. Point Source Discharge of Stormwater'
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe, ditch,
channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to waters
of the state.
18. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours in which no
storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive
hours of no precipitation. For example, if it rains for 2 hours without producing any collectable discharge, and then
stops, a sample. maybe collected if a rain producing a discharge begins again within the next 10 hours.
19. Representative Outfall Status
When it is established that the discharge of stormwater runoff from a single outfall is representative of the
discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall
status allows the permittee to perform analytical monitoring at a reduced number of outfalls.
20. Rinse Water Discharge
The discharge of rinse water from equipment cleaning areas associated with industrial activity. Rinse
waters from vehicle and equipment cleaning areas are process wastewaters and do not include washwaters
utilizing any type of detergent or cleaning agent.
21. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year, 24-hour storm event. .
22. Section_313 Water Priority Chemical
A chemical.or chemical category which:
a. .Is listed in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right -
to -Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title I1I, Section 313.reporting
requirements; and
C. That meet at least one of the following criteria:
(1) Is listed in Appendix D of 40 CFR part 122 on either Table II (organic priority
pollutants), Table III (certain metals, cyanides, and phenols) or Table IV (certain toxic
pollutants and hazardous substances); = :
(2) . Is listed as a hazardous substance pursuant to section 31 l(b)(2)(A) of the CWA at 40
CFR 116.4; or
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
Part VI . Page 3 of 5 Pages

DRAFT Permit No. NCS000374
23
24.
25.
Severe Prouerty Damaae
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production.
Sianificant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or production;
hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required to
report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as ashes,
slag and sludge that have the potential to be released with stormwater discharges..
Sianificant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section.102 of
CERCLA (Ref: 40 CFR 302; 4).
2b. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmelt.
27.Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacturing, processing or raw material storage areas at an industrial site. Facilities
considered to be engaged in "industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include discharges from facilities or activities excluded from the NPDES program.
28. Stormwater Pollution Prevention Plan
A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution and
is based on an evaluation of the pollution potential of the site.
20.: 'Ten Year Design Storm
The maximum 24 hour precipitation event expected to be equaled or exceeded on the average once in ten
years. Design storm information can be found in the State of North Carolina Erosion and Sediment Control
Planning and Design Manual.
30. Total Flow
The flow corresponding to the time period over which the entire storm event occurs. Total flow shall be
either; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event.,

'
DRAFT Permit No. NCS000374
31.
Total Maximum Daily Load (TMDL)
A TMDL is a calculation of the maximum amount of a pollutant that a waterbody can receive and still meet
water quality standards, and an allocation of that amount to the pollutant's sources. A TMDL is a detailed .
water quality assessment that provides the scientific foundation for an implementation plan. The.
implementation plan outlines the steps necessary to reduce pollutant loads in a certain body of water to
restore and maintain water quality standards in all seasons. The Clean Water Act, section 303, establishes
the water quality standards and TMDL programs.
32.
Toxic Pollutant
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
33.
Ups et
Means an exceptional incident in which there is unintentional and temporary noncompliance with
technology based permit effluent limitations because of factors beyond the reasonable control of the
permittee. An upset does not include noncompliance to the extent caused by operational error, improperly
designed treatment or control facilities, inadequate treatment or control facilities, lack of preventive
maintenance, or careless or improper operation.
34.
Vehicle Maintenance Activity
'
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or
airport deicing operations.
35.
Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or ice from its site of origin which can be seen with the unaided eye.
36.
25-year, 24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
Part VI Page 5 of 5 Pages

�Y

BUCKEYE
1000 EAST NOIR ST., P.O. BOX 1305
LUMBERTON, NORTH CAROLINA 28359
TEL [phone] FAX [phone]
``,'' rml
UI'%1y ID U
January 28, 2004
Individual Permit Renewal
Attn: Mr. Darren England
Stormwater and General Permits Unit
1617 Mail Service Center
Raleigh, N.C. 27699-1617
Re: Permit renewal information for permit number NCS000374
Mr. England,
Please find enclosed a completed permit renewal application form and the requested
supplemental information for Stormwater Discharge Permit number NCS000374.
Please note the mailing address change on the Permit Renewal Form.
If you have any additional information requests upon review of this submission please do not
hesitate to contact me at 910-737-3231.
Sincerely,
e4441 d � �� d�
Chuck Oxendine
Operations Manager
Buckeye Lumberton Inc.
BUCKEYE LUMBERTON INC.

PERMIT COVERAGE
RENEWAL APPLICATION FORM Permit Number
National Pollutant Discharge )Elimination System NCS000374
Stormwater Discharge Permit
TIIIS APPLICATION NIUST BE SIGNED AND RETURNED ALONG WIT14 TEM R QUESTED SUPPLEMENTAL
INFORMATION TO 171C DI'V. OF WATER QUALITY IN ORDER FOR YOUR F CILITY'TO QUALIFY FOR
RENEWAL OF YOUR STORMWATER PERMIT NCS00 374
The following is the information currently in our database for your facility. Please rc view this information carefully
and make all corrections as necessary in the space provided to the right of the current information,
OW R INFOR A I N
OwncrlOrg. Name: BUCKEYE LUMBBRTON INC
Owner Contact: 014UCK 0 k G-
Mailing Address; ILOQ E S &7-9CE7-
�Rtv� .C. 8
Phone Number: q10 -
Fax Number I 0 - S
E-mail address: .. OKt' d.ne nG l
F AC [L.ITY gmoand
, TA i4N.
Facility Name:
BUCKEYE LUMBERTON INCORPORATED
Facility Contact:
LM{�
Facility Address:
1000 EASTNOIR STREET
LUMBERTON, NC 25359
Phone Number:
Fax Number
E-mail address:
PEMjT'W0P'MATION
Permit Contact: CHUCK OXWDINE
Mailing Address; PO Box 1303
LUMBERTON. NC 28359
Phone Number: 9107373331
Fax Number: SAS AS
- &mail address: it
Dig CHARGE INPQRMATION
Discharge Receiving Water; LIT OF LUMBER RIVER
Stream Class: CSw
Basin: LUMBER
Sub -Basin if: .030131
Number of outfalls:
CERTIFICATION
I certify that i am familiar with the information contained in the application and that
belief such information is true, complete and accurate.
Signature Date _
ellUZt' QX &AI&AA
Print or type name of person signing Above Title
Please return this completed renewal application form to:
Individual Permit Renewal
Aun. Darren England
Stormwater and General Permits Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
the best of my knowledge and
/--2Q-
ONS /Y A1.46tt
fn"d rf":6 EOaz 6L sea 6t66EEL6l6:X2j A;Ilend jaleg 10 Ala

SUPPLEMENTAL WFORMATION REQUIRED FOR RENEWX L O INDIVIDUAL NPDES
STORMWATER PERMIT
"w copies of each of the following shall accompany this submittal in order fo the application to be
considered complete:
(Do not submit the site Stormwater Pollution Preventio Plan)
Initials
1. A current Site Map from the Stormwater Pollution Prevention I Ian. The location of
industrial activities (including storage of materials, disposal areas, process areas and
loading and unloading areas), drainage structures, drainage are s for each outfall, building
locations and impervious surfaces should be clearly noted,
2, A summary of Analytical Monitoring results during the term o the existing permit (if your
permit required analytical sampling). Do not submit individua lab reports. The summary
-can consist of a table including such items as outfall number, p ameters sampled, lab
results, date sampled, and storm event data. it
3. A summary of the Visual Monitoring results. Do not submit in fividual monitoring reports.
The summary can consist of a table including such items as out all number, parameters
surveyed, observations, and date monitoring conducted.
4. A summary of the Best Management Practices utilized at the permitted facility. Summary
should consist of a short narrative description of each BMP's in place at the facility. If the
��7 implementation of any BMP's is planned, please include info ation on these BMP's,
w 5. A short narrative describing any significant changes in industri ki activities at the permitted
facility. Significant changes could include the addition or dele ion of work processes,
changes in material handling practices, changes in material stoi age practices, and/or
changes in the raw materials used by the facility.
6. Certification of the development and implementation of a Ston awater Pollution Prevention
Plan for the permitted facility (Sign and return attached form).
�r If the final year analytical monitoring of the existing permit to has not been completed
prior to filing the renewal suhmitta.l,.then the last year$ monito ing results should be
submitted within 30 days of receipt of the laboratory reports, (.e. do not withhold renewal
submittal waiting on lab results)
Representative storm sampling may now be conducted anytime
November window has been eliminated) and the representative
defined as a storm event that measures greater than 0.1 inches
hours in which no storm event measuring greater than 0.1 inch
daring the year (the April to
rainfall event is now
nd is preceded by at least 12
s has occurred.
b0'd ££:6 E40Z 61. oea 6166£6L6l6txeJ h11len0 .re�eA }o Ala

STORMWATER POLLUTION P12EVE TIO1V PLAN
DEVELOPMENT AND IMPLEMENTATION
CERTIFICATION
N.C. Division of Water Quality, Srormwater and General hermits Unit
Pacili(y Name: BUCKEYE LUMBERTON TNCORPORATED
Permit Number: NCS000374
Location Address: 1000 EAST NOIR STREET
LUMBERTON, NC 28359
County: ROBESON
_ __::( certify_. under penalty of Iaw,.0gt tbf�SiQlrltwater Pollutij)II Pr=rEi0n,P1ag1,SPP )_docti nent.and all Atsacbments.
were developed and implemented under my direction or supervision in accordance with a system designed to Assure
that qualified personnel properly gather and evaluate, the information required by the SPPP. Based on my inquiry of
the person or persons who manage the system, or those persons directly responsible for gathering the information,
the information gathered is, to the best of my knowledge and belief, true, accurite, and complete"
" T certify that the SPPP has been developed, signed and retained at the facility locatilin and the SPPP has been fully
implemented at the named facility location in accordance with the terms and conditi ns of the stormwater general
permit."
" I am aware that there are significant penalties for falsifying information, including a possibility of fines and
imprisonment for knowing violations"
Sign (according to permit signatory requirements) and return this Certificat##'on. DO NOT SEND THE
STORMWATER POLLUTION PREVENTION PLAN WITH THE CERTIfMATION.
Signature _ Date
An e�1 -- 4 ea I C— iM ari 0. cr
Print or type na a of person signing Above Title
SPPP Certification 2M
Cn'a cc:R cnn7 Ai Sea 9I99i',f'/RIR:Xe4 Alilend joie,N 40 Aln

Stormwater Analytical Sampling
611412000
fecal coliform
Monitor
Flow (MG)
TSS (mg/L)
pH
(coll100mL)
Outfall 1
flow
0.024
-
-
-
Outfall 2
flow, TSS, pH,
0.008
56.8
6.1
-
Outfall 4
flow, TSS, pH, fecal coliform
0.034
1.6
6.4
5
Outfall 5
flow
0.012
-
-
-
Outfall 6
flow, TSS, pH, fecal coliform
0.013
13.6
6.9
773
Outfall7
flow, TSS, pH, fecal coliform
0.017
17.6
7.1
1282
Outfall 8
flow, TSS, pH
0.009
0.8
7.8
-
1111912003
Outfall 2
flow, TSS, pH,
0.014
14.0
6.9
-
Outfall 4
flow, TSS, pH, fecal coliform
0.060
6.0
7.1
200.0
Outfall 6
flow, TSS, pH, fecal coliform
0.023
180.0
7.0
790.0
Outfall 7
flow, TSS, pH, fecal coliform
0.029
6.0
6.8
10.0
Outfall8
flow, TSS, pH
0.016
7.5
7.1
-
Cutoff Concentrations 100 6.0 - 9.0

Buckeye Lumberton Inc.
Stormwater Permit No. NCS000374
Visual Monitoring Results
Outfall Number Parameters Surye ed Observations Date Monitorinq Conducted
Color, Odor, Clarity, Floating
Solids, Suspended Solids,
Foam, Oil Sheen, Other
1,2,4,5,6,7,8
Indicators of Pollution
Not Present
6/14/2000
1,2,4,5,6,7,8
1 Not Present
11/30/2000
1,2,4,5,6,7,8
Not Present 6/22/2001
1,2,4,5,6,7,8
Not Present 11/30/2001
1,2,4,5,6,7,8
Not Present
5/30/2002
1,2,4,5,-6,*7,8
Suspended Solids
11/21/2002
1,2,4,5,6,7,8
Not Present
4/8/2003
1,2,4,5,6,7,8 "
Not Present
9/23/2003
Comments: 11/21/02 sampling showed Suspended solids in outfalls 6 and 7 due to construction work going on to
build a new warehouse in the vicinity. Warehouse completion date and clean up targeted for March 2003.

BEST MANAGEMENT PRACTICES SUMMARY
_�+
ZF-
'
4
� Be t Mana eme t Practice ;
erahon
A� n -
•
Wherever practical, install roofs over storage areas or the areas should be completely enclosed.
Bulk Storage
•
Divert off -site drainage around storage areas.
•
Make employees aware of the potential environmental problems caused when spilled products are not cleaned up immediately.
Drainage
•
When oil or other pollutants are seen ponding in the secondary containment areas, remove and properly dispose of them to
Procedures
prevent pollutant discharge.
Transfer
*
Train truck drivers and delivery personnel to comply with pollution prevention procedures and spill control measures.
Operations and
*
Perform vehicle and equipment maintenance indoors when possible. Use drip pans when changing fluids and immediately clean
In -Plant
any spillage.
Processes
+
When feasible, protect loading and unloading areas with roofs over docks.
•
Use berms or proper grading to divert stormwater from loading and unloading areas where spills are likely to occur.
Loading and
.
Sweep loading areas to remove debris and other particulate contaminants.
Unloading
•
Train truck drivers and delivery personnel on pollution prevention procedures.
•
Prevent leaking trucks and railcars from entering or leaving the plant site until the leak is stopped.
•
Place dumpsters under covered areas if possible. The area should be large enough to allow for emptying the dumpster without
exposing the contents to stormwater.
Waste Disposal
•
If waste is stored outside, provide containers with tight fitting lids and keep them closed except when loading waste material
Practices
into the dumpster.
•
Use compactors that are loaded from an end or from within a building as an alternative to dumpsters. (Stored waste materials
are less likely to come into contact with the rainfall.)
Spill Prevention
•
Implement the Spill Prevention Policies and Procedures in Annex D of the One Plan.
48301 SWP3 1 Buckeye Lumberton, Inc.
December 2003 One Plan - IV SWP3

WRY
i

Subject: Narrative describing changes in industrial activity at the Buckeye Lumberton Inc.
facility.
There were three significant changes in industrial activities at the Buckeye Lumberton facility
during the terms of permit NCS000374.
A new process (Fiberline) was started up in August 2001, The Fiberline is a staple cotton bleaching
process that produces products used in cosmetic and absorbent applications and medical devices.
The Fiberline process is located in a new building located at the Northwest end of the facility. The
Fiberline utilizes the pre-existing warehouse space for storage of raw materials and finished
products.
The pulp mill operation was shut down on Wednesday, August 27, 2003. Prior to the closure of the
pulp mill, the denim cutting process, which supplied raw fiber material to the pulp mill process,
was shut down. The shutdown of the pulp mill and denim cutting operations left only the Fiberline
process in operation at the Lumberton site.
The pulp mill operation was started in 1968 and was the primary business unit at the site until the
Fiberline was constructed and started up in 2001. The pulp mill closure has resulted in several
significant changes:
• The wastewater treatment plant has been cleaned out and shut down. Buckeye Lumberton no
longer has a direct discharge of wastewater to the Lumber River.
• The Fiberline Process discharges plant process waters to the City of Lumberton municipal
treatment system. The typical flow to the City of Lumberton is — .250 MGD versus — 2.2 MGD
effluent discharge from Buckeye WWTP in the past.
• With the WWTP no longer in operation, the site does not generate, store or transport residual
solids from the biological treatment process.
• The overall consumption of manufacturing chemicals has decreased and several chemicals used
in the pulp mill are not required in the Fiberline process (i.e. Chlorine, Sodium Chlorite, Tall
Oil).
• The Fiberline continues to use Hydrogen peroxide, Sodium hydroxide and Sulfuric acid as
process chemicals. No. 4 Fuel oil also continues to be used as a backup fuel source to natural
gas in boiler operations.
• There are no cotton linter or denim raw materials in storage at the Lumberton facility. Staple
cotton fibers (i.e. virgin staple, cardstrip, regins, comber) are the raw material fibers used in the
Fiberline process.
• Generation of used oils and lubricants has significantly decreased.
• Waste streams (water, fibers, and general refuse) from the denim cutting and pulp mill
processes have been eliminated.
• Storage of fuels (diesel and gasoline) have been eliminated.
• The Fiberline typically operates a 12/2 work schedule (12 days up and 2 days shutdown) but
may operate 2417 as required to meet business needs.
Chuck Oxendine
January 27, 2004

Cf�OF \NAT E19 Michael F. Easley. Governor
rC7 William G. Ross Jr., Secretary North Carolina Department of Environment and Natural Resources
0 Alan W. Klimek, P.E. Director
Division of Water Quality
December 3, 2004 n-* f --� r_
Chuck Oxendine ��
Buckeye Lumberton, Inc. — 2094
1000 East Noir Street
Lumberton, NC 28358 �U14410
Subject: NPDES Permit Renewal Application
Permit Number NCS000374
Individual Stormwater Permit
Robeson County
Dear Mr. Oxendine:
The Division of Water Quality's Stormwater and General Permits Unit hereby acknowledges receipt of your renewal
application for coverage under NPDES Permit Number NCS000374 on January 30, 2004. The submitted renewal package
contained the following items:
➢ Signed application
➢ Site map
➢ Analytical monitoring results summary
➢ Visual monitoring results summary
➢ Best Management Practices summary
➢ Narrative describing significant changes at the permitted facility
➢ Signed Stormwater Pollution Prevention Plan certification
A preliminary review of the submitted renewal application package has been conducted, and it appears to be complete. No
further information is required at this time. If you have any questions about the renewal process or would like to discuss this
letter, please contact me at [phone], extension 537.
Sincerely,
Jo than A. Diggs
Environmental Engineer
cc: Fayetteville Regional Office
Stormwater Permitting Unit
Central Files
Nne
Carolina
AarAmally
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699.1617 Phone [phone] Customer Service
Internet h2o.enr.state.nc.us 512 N, Salisbury St. Raleigh, NC 27604 FAX [phone].623-6748
An Equal OpportunitylAtfirmative Action Employer- 50% Recycled110"k Post Consumer Paper

}
n
y
is F
=p
', 5-.',ii
�:.

State of North.Carolina
Department of Environment
and Natural Resources
Division of Water Quality ! O 2001
Michael F. Easley, Governor j
William G. Ross Jr., Secretary
Alan W. Klimek, P.E., Director
December 3, 2003
BUCKEYE LUMI3ERTON INCORPORATED
ATTN: CHUCK OXENDINE, OR SUCCESSOR
PO BOX 1305
LUMBERTON, NC 28359
Dear Perm ittee:
--.NCDENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND (NATURAL RESOURCES
Subject: NPDES Stormwater Permit Renewal
Buckeye Lumberton Incorporated
Permit Number NCS000374
Robeson County
Your facility is currently covered for stormwater discharge under NPDES Permit NCS000374. This permit expires
on July 31, 2004. North Carolina Administrative Code (l5A NCAC 2H.0105(e)) requires that un application for
permit renewal be filed at least t 80 days prior to expiration of the current permit. In orcler to assure your continued
coverage under your permit, you must apply to the Division of Water Quality (DWQ) for renewal of your permit.
To make this renewal process easier, we are informing you in advance that your permit will be expiring. Enclosed
you will find an individual permit renewal application form, supplemental information request, and Stormwater
Pollution Prevention Plan certification.
Filing the application form along with the requested supplimental information will constitute your application for
renewal of your permit. As stated above, the application farm must be completed and returned along with all
requested information by February 2, 2004 in order for- the permit to be renewed by July 31, 2004.
Failure to request renewal by February 2, 2004 may result in a civil assessment of at least $500.00. Larger
penalties may be assessed depending on the delinquency of the request. Discharge of stormwater from your facility
withOut Coverage Linder a valid Stormwater NPDES permit would constitute a violation of NCGS 143-215.1 and
could result in assessments of civil penalties of up to $25,000 per clay.
If you have any questions regarding the permit renewal procedures please contact Bill Mills of the Stormwater and
General Permits Unit at [phone], ext. 548.
Sincerely,
Bradley Bennett, Supervisor
Stormwater and General Permits Unit
cc: Central Files
Storniwaler and General Permits Unit Files
l"ayetteville Rcgicmal Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] Fax [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper

i .i
RECO16ED
Staff Review and Evaluation
NPDES Stormwater Permit
Contact: Darren England (919-733-5083, ext. 545)
4PR 61999
FAYMEVI LLE
REG. OFFICE
Facility Name:
Buckeye Lumberton, Inc.
NPDES Permit Number:
NCS000374
Facility Location:
1000 East Noir Street
Type of Activity:
Pulp Mill
SIC code (if applicable):
2611
Receiving Stream:
Ut of Lumber River, Lumber River Basin
Stream Classification:
C Sw
Proposed Permit Requirements:
See attached draft permit
Compliance Schedule:
See Part III, Section A of attached draft permit
Basis for monitoring
See attached Data Analysis Summary
Basis for other requirements:
NIA 1
L4 I &) 1 G9
Response requested by (date):
Regional Office Staff Comments:
�� �titi1

NCS000374
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
s
PERMIT
TO DISCHARGE STORMWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and
regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the
Federal Water Pollution Control Act, as amended,
Buckeye Lumberton, Inc.
is hereby authorized to discharge stormwater from a facility located at
1000 East Nair Street
Lumberton, North Carolina
Robeson County
to receiving waters designated as an unnamed tributary of Lumber River, a class C Sw stream in the Lumber River
Basin in accordance with the discharge limitations, monitoring requirements, and other conditions set forth in Parts
I, I1, III, IV, V and VI hereof.
This permit shall become effective .
This permit and the authorization to discharge shall expire at midnight on .
Signed this day
Kerr T. Stevens, Director
Division of Water Quality
By the Authority of the Environmental Management Commission

I
Permit No. NCS000374
TABLE OF CONTENTS
PART I INTRODUCTION
Section A: individual Permit Coverage
Section B: Permitted Activities
Section C: Location Map
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED DISCHARGES
Section A:
Stormwater Pollution Prevention Plan
Section B:
Analytical Monitoring Requirements
Section C:
QuaIitative Monitoring Requirements
Section D:
On -Site Vehicle Maintenance Monitoring Requirements
PART III
STANDARD CONDITIONS
Section A:
Compliance and Liability
I. Compliance Schedule
2. Duty to Comply
3. Duty to Mitigate
4. Civil and Criminal Liability
5. Oil and Hazardous Substance Liability
6. Property Rights
7. Severability
8. Duty to Provide Information
9. Penalties for Tampering
10. Penalties for Falsification of Reports
Section B:
General Conditions
1. Individual Permit Expiration
2. Transfers
3. Signatory Requirements
4. Individual Permit Modification, Revocation and Reissuance, or Termination
5. Permit Actions
Section C:
Operation and Maintenance of Pollution Controls
1. Proper Operation and Maintenance
2. Need to Halt or Reduce Not a Defense
3. Bypassing of Stormwater Control Facilities
Section D:
Monitoring and Records
1. Representative Sampling
2. ' Recording Results
3. Flow Measurements
4. Test Procedures
5. Representative Outfall
6. Records Retention
7. Inspection and Entry
1

Permit No. NCS000374
Section E: Reporting Requirements
L
Discharge Monitoring Reports
2.
Submitting Reports
3.
Availability of Reports
4.
Non-Stormwater Discharges
5.
Planned Changes
6.
Anticipated Noncompliance
7.
Bypass
8.
Twenty-four Hour Reporting
4.
Other Noncompliance
10.
Other Information
PART IV LIMITATIONS REOPENER
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE REQUIREMENTS
PART VI DEFINITIONS
ii

Permit No. NCS000374
PART I INTRODUCTION
SECTION A: INDIVIDUAL PERMIT COVERAGE
During the period beginning on the effective date of the permit and lasting until expiration, the permittee is
authorized to discharge stormwater associated with industrial activity. Such discharges shall be controlled, limited
and monitored as specified in this permit.
SECTION B: PERMITTED ACTIVITIES
Until this permit expires or is modified or revoked, the permittee is authorized to discharge stormwater to the
surface waters of North Carolina or separate storm sewer system which has been adequately treated and managed in
accordance with the terms and conditions of this individual permit. All discharges shall be in accordance with the
conditions of this permit.
Any other point source discharge to surface waters of the state is prohibited unless it is an allowable non-stormwater
discharge or is covered by another permit, authorization or approval.
This permit does not relieve the permittee from responsibility for compliance with any other applicable federal,
state, or local law, rule, standard, ordinance, order, judgment, or decree.
Part I Page 1 of 2

Permit No. NCS000374
SECTION C: LOCATION MAP
1 railer rarK
DWI T :� ,�.. !l NI
�)
Z�-'
M.F7�
�'Library Cem y
b� ` •:� ' •'`' M ainu �_ `� ernI _ ' Hyde Park
Ich
�� :� •r.�! ►�� `'1, p of
04,
ct:. a e Ind
toPds
Ois�a, I5 + • WT
V '.'� -• �' _ t'.` ',1r _ _ .mot
Traile
Hestertoam' �— \
i;adioSlatian
§ 1 iiadi Tgwero _ (WAGR� c - LU�1BE -
\���JJJ II I sr 106 x
\( kl
h• �� •I • Publi Rr Bmpadi0 • ,f 5
Ig}, n �~�Tower- 1
It
.108
Sew spose
Ponds
l � K
Part I Page 2 of 2

Permit No. NCS000374
PART II MONITORING, CONTROLS, AND LIMITATIONS FOR PERMITTED DISCHARGES
SECTION A: STORMWATER POLLUTION PREVENTION PLAN
The permittee shall develop a Stormwater Pollution Prevention Plan, herein after referred to as the Plan. This Plan
shall be considered public information in accordance with Part III, Standard Conditions, Section E, Paragraph 3 of
this individual permit. The Plan shall include, at a minimum, the following items;
Site Plan. The site plan shall provide a description of the physical facility and the potential pollutant
sources which may be expected to contribute to contamination of stormwater discharges. The site plan
shall contain the following:
(a) A general location map (USGS quadrangle map or appropriately drafted equivalent map),
showing the facility's location in relation to transportation routes and surface waters, the name of
the receiving water(s) to which the stormwater outfall(s) discharges, or if the discharge is to a
municipal separate storm sewer system, the name of the municipality and the ultimate receiving
waters; and accurate latitude and longitude of the point(s) of discharge.
(b) A narrative description of storage practices, loading and unloading activities, outdoor process
areas, dust or particulate generating or control processes, and waste disposal practices.
(c) A site map drawn to scale with the distance legend indicating location of industrial activities
(including storage of materials, disposal areas, process areas and loading and unloading areas),
drainage structures, drainage areas for each outfall and activities occurring in the drainage area,
building locations, existing BMPs and impervious surfaces, and the percentage of each drainage
area that is impervious. For each outfall, a narrative description of the potential pollutants which
could be expected to be present in the stormwater discharge.
(d) A list of significant spills or leaks of pollutants that have occurred at the facility during the 3
previous years and any corrective actions taken to mitigate spill impacts.
(e) Certification that the stormwater outfalls have been evaluated for the presence of non-stormwater
discharges. The certification statement will be signed in accordance with the requirements found
in Part III, Standard Conditions, Section B, Paragraph 3.
2. Stormwater Management Plan. The stormwater management plan shall contain a narrative description of
the materials management practices employed which control or minimize the exposure of significant
materials to stormwater, including structural and nonstructural measures. The stormwater management
plan, at a minimum, shall incorporate the following:
(a) Feasibility Study. A review of the technical and economic feasibility of changing the methods of
operations and/or storage practices to eliminate or reduce exposure of materials and processes to
stormwater. Wherever practical, the pennittee shall prevent exposure of all storage areas, material
handling operations, and manufacturing or fueling operations. In areas where elimination of
exposure is not practical, the stormwater management plan shall document the feasibility of
diverting the stormwater runoff away from areas of potential contamination.
(b) Secondary Containment Schedule. A schedule to provide secondary containment for bulk storage
of liquid materials, storage of Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) water priority chemicals, or storage of hazardous substances to
prevent leaks and spills from contaminating stormwater runoff. If the secondary containment
devices are connected directly to stormwater conveyance systems, the connection shall be
controlled by manually activated valves or other similar devices [which shall be secured with a
Part II Page i of 6

Permit No. NCS000374
locking mechanism] and any stormwater that accumulates in the containment area shall be at a
minimum visually observed for color, foam, outfall staining, visible sheens and dry weather flow,
prior to release of the accumulated stormwater. Accumulated stormwater shall be released if
found to be uncontaminated by the material stored within the containment area. Records
documenting the individual making the observation, the description of the accumulated
stormwater and the date and time of the release shall be kept for a period of five years.
(c) BMP Summary. A narrative description shall be provided of Best Management Practices (BMPs)
to be considered such as, but not limited to, oil and grease separation, debris control, vegetative
filter strips, infiltration and stormwater detention or retention, where necessary. The need for
structural BMPs shall be based on the assessment of potential of sources to contribute significant
quantities of pollutants to stormwater discharges and data collected through monitoring of
stormwater discharges.
3. Spill Prevention and Response Plan. The Spill Prevention and Response Plan (SPRP) shall incorporate an
assessment of potential pollutant sources based on a materials inventory of the facility. Facility personnel
(or team) responsible for implementing the SPRP shall be identified. A responsible person shall be on -site
at all times during facility operations that have the potential to contaminate stormwater runoff through
spills or exposure of materials associated with the facility operations. The SPRP must be site stormwater
specific. Therefore, a SPCC plan may be a component of the SPRP, but may not be sufficient to
completely address the stormwater aspects of the SPRP. The common elements of the SPCC with the
SPRP may be incorporated by reference into the SPRP.
4. Preventative Maintenance and Good Housekeeping Program. A preventative maintenance program shall
be developed. The program shall document schedules of inspections and maintenance activities of
stormwater control systems, plant equipment and systems. Inspection of material handling areas and
regular cleaning schedules of these areas shall be incorporated into the program.
5. Employee Training. Training schedules shall be developed and training provided at a minimum on an
annual basis on proper spill response and cleanup procedures and preventative maintenance activities for
all personnel involved in any of the facility's operations that have the potential to contaminate stormwater
runoff. Facility personnel (or team) responsible for implementing the training shall be identified.
6. Responsible Party. The Stormwater Pollution Prevention Plan shall identify a specific position(s)
responsible for the overall coordination, development, implementation, and revision to the Plan.
Responsibilities for all components of the Plan shall be documented and position assignments provided.
7. Plan Amendment. The permittee shall amend the Plan whenever there is a change in design, construction,
operation, or maintenance which has a significant effect on the potential for the discharge of pollutants to
surface waters. The Stormwater Pollution Prevention Plan shall be reviewed and updated on an annual
basis.
The Director may notify the permittee when the Plan does not meet one or more of the minimum
requirements of the permit. Within 30 days of such notice, the permittee shall submit a time schedule to
the Director for modifying the Plan to meet minimum requirements. The permittee shall provide
certification in writing (in accordance with Part III, Standard Conditions, Section B, Paragraph 3) to the
Director that the changes have been made.
8. Facility Inspection Program. Facilities are required to inspect all stormwater systems on at least a
semiannual schedule, once in the fall (September -November) and once in the spring (April - June). The
inspection and any subsequent maintenance activities performed shall be documented, recording date and
time of inspection, individual(s) making the inspection and a narrative description of the facility's
stormwater control systems, plant equipment and systems. Records of these inspections shall be
incorporated into the Stormwater Pollution Prevention Plan.
Part II Page 2 of 6

Permit No. NCS000374
Stormwater discharge characteristic monitoring as required in Part II of this permit shall be performed in
addition to facility inspections.
9. Implementation. The permittee shall document all monitoring, measurements, inspections and
maintenance activities and training provided to employees, including the log of the sampling data and of
activities taken to implement BMPs associated with the industrial activities, including vehicle maintenance
activities. Such documentation shall be kept on -site for a period of five years and made available to the
Director or his authorized representative immediately upon request.
SECTION B: ANALYTICAL MONITORING REQUIREMENTS
During the period beginning on the effective date of the permit and lasting until expiration, the permittee is
authorized to discharge stormwater subject to the provisions of this permit. Analytical monitoring of stormwater
discharges shall be performed as specified below in Table 1.
For each parameter, the arithmetic mean of all analytical sampling results collected during the term of the permit
shall be calculated for each individual outfall. The computed arithmetic mean is then compared to the cut-off
concentrations listed below in Table 2. If the arithmetic mean is less than the specified cut-off concentration for a
given parameter, then the facility is not required to continue annual analytical monitoring for that parameter (at that
outfall) during the' -remaining term of the permit unless a significant change in facility operations or configuration
occurs. if a cut-off concentration results in discontinued analytical monitoring at an individual discharge outfall, the
permittee is required to maintain facility operations that ensure the continuation of stormwater runoff quality.
The permittee must perform analytical sampling during the first and last year of the permit coverage regardless of
cut-off concentration conditions. Analytical results from sampling during the final year of the permit coverage must
be submitted with the permit renewal application. All analytical monitoring shall be performed during a
representative storm event.
The permittee has identified seven active stormwater discharge outfalls for this facility. The outfalls were
designated by the permittee as outfalls 1, 2, 4, 5, 6, 7, and 8..For the initial term of this permit, analytical sampling
at outfall l and outfall 5 is not required. The drainage areas for these two outfalls contain the same types of
potential pollutants as those'found in the drainage area for outfall 4, Therefore, sampling of outfall 4 will be
considered as representative of outfalls 1 and 5. Analytical sampling is required at outfalls 2, 4, 6, 7, and 8 unless
otherwise specified in Table 1.
Table 1. Analytical Monitoring Requirements
pt i'x' t i:`;D�scharge'`" a ,tE " rTT
�#�, �•a�1a ���
Cl►araeterist�cs u ort
-InF�} tw
M,Unitsa,_t t.
„�i Measurement
;.•:'.. _Fregquency;_,
,4�FSample "s
r..Type
r Ji Sample yl
Total Suspended Solids
mg/l
annually
Grab
SDO
Fecal Coliform'
col. / 100 ml
annually
Grab
SDO
pH
standard
annually
Grab
SDO
Total Rainfall
inches
annually
-
-
Event Duration
minutes
annually
-
-
Total Flow
MG
annually
-
SDO
Footnotes:
1 Measurement Frequency: Once per year during a representative storm event. A year is defined as the 12 month
period beginning on the month and day of issuance of the Permit.
Part II Page 3 of 6

Permit No. NCS000374
2 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. if the detention pond discharges only in
response to a storm event exceeding a ten year design storm, then no analytical monitoring is required and only
qualitative monitoring shall be performed.
3 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) unless representative
outfall status has been granted or unless otherwise specified.
4 Sampling for this parameter is required at outfalls 4, 6, and 7 only. After two rounds of sampling have been
completed at each outfall (for a total of six samples), the permittee may petition the Division to review the
requirement to sample for this parameter.
5 For each sampled representative storm event the total precipitation, storm duration, and total flow must be
monitored. Total flow shall be either; (a) measured continuously, (b) calculated based on the amount of area
draining to the outfall, the amount of built -upon (impervious) area, and the total amount of rainfall, or (c)
estimated by the measurement of flow at 20 minute intervals during the rainfall event.
Table 2. Cut-off Concentrations for Analytical Monitoring Requirements
cag'.°P...,,'
°. : .;'�
I r;DihrCcteristis,r `
s. �.:..,Cu='ofCanetriton°
Total Suspended Solids
100 mg/l
pH
within range 6.0 - 9.0
SECTION C: QUALITATIVE MONITORING REQUIREMENTS
Qualitative monitoring requires a visual inspection of each stormwater'outfall regardless of representative outfall
status and shall be performed as specified below in Table 3. Qualitative monitoring is for the purpose of evaluating
the effectiveness of the Stormwater Pollution Prevention Plan (SPPP) and assessing new sources of stormwater
pollution. No analytical tests are required. Qualitative monitoring of stormwater outfalls does not need to be
performed during a representative storm event.
The first qualitative monitoring event during the coverage of the permit must coincide with the initial analytical
monitoring event (regardless of the season). All other qualitative monitoring will be performed twice per year,
once in the spring (April - June) and once in the fall (September - November).
Table 3. Qualitative Monitoring Requirements
T;_Y. h€i "<dg r€.-
DischarQbe Character�sUcs
Y'xt![ �'Zjhf I�f 4F°I, tt'ly
uencr i
-7d,r.Sy,
Ci h N... IN im`� tN"� a'! ],aft
C �]VNonitormg Location, 4;.
Color
Semi -Annual
SDO
Odor
Semi -Annual
SDO
Clarity
Semi -Annual
SDO
Floating Solids
Semi -Annual
SDO
Suspended Solids
Semi -Annual
SDO
Foam
Semi -Annual
SDO
Oil Sheen
Semi -Annual
SDO
Other obvious indicators
of stormwater pollution
Semi -Annual
SDO
Footnotes:
1 Monitoring Location: Qualitative monitoring shall be performed at each stormwater discharge outfall (SDO)
regardless of representative outfall status.
Part II Page 4 of 6

Permit No. NCS000374
SECTION D: ON -SITE VEHICLE MAINTENANCE MONITORING REQUIREMENTS
Facilities which have any vehicle maintenance activity occurring on -site which uses more than 55 gallons of new
motor oil per month when averaged over the calendar year shall perform analytical monitoring as specified below in
Table 4. This monitoring shall be performed at all outfalls which discharge stormwater runoff from vehicle
maintenance areas.
For each parameter, the arithmetic mean of all analytical sampling results collected during the coverage of the
permit shall be calculated for each individual outfall. The computed arithmetic mean is then compared to the cut-
off concentrations listed below in Table 5. If the arithmetic mean is less than the specified cut-off concentration for
a given parameter, then the facility is not required to continue annual analytical monitoring for that parameter (at
that outfall) during the remaining coverage of the permit unless a significant change in facility operations or
configuration occurs. If a cut-off concentration results in discontinued analytical monitoring at an individual
discharge outfall, the permittee is required to maintain facility operations that ensure the continuation of stormwater
runoff quality.
The permittee must perform analytical sampling during the first and last year of the permit coverage regardless of
cut-off concentration conditions. Analytical results from sampling during the final year of the permit coverage must
be submitted with the permit renewal application. All analytical monitoring shall be performed during a
representative storm event.
Table 4. Analytical Monitoring Requirements for On -Site Vehicle Maintenance
Discharge,Charactsr'ist�cs , „y,
E, `, Unittls`� "{' ;<<{�
`wMeasur'ement� ,
; 4Sample
£Ir'.,ip
i,"�r� °E e;�`,.
yp
,-Sample,,,t
pH
standard
annually
Grab'
SDO
Oil and Grease
mg/l
annually
Grab
SDO
Total Suspended Solids
mg/l
annually
Grab
SDO
New Motor Oil Usage
gallons/month
annually
Estimate
-
Total Flow
MG
annually
Grab
SDO
Footnotes:
1 If the stormwater runoff is controlled by a stormwater detention pond, a grab sample of the discharge from the
pond shall be collected within the first 30 minutes of discharge. If the detention pond discharges only in
response to a storm event exceeding a ten year design storm, then no analytical monitoring is required and only
qualitative monitoring shall be performed.
2 Sample Location: Samples shall be collected at each stormwater discharge outfall (SDO) that discharges
stormwater runoff from area(s) where vehicle maintenance activities occur.
3 Total flow shall be; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall,
the amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the measurement
of flow at 20 minute intervals during the rainfall event. Total precipitation and duration of the rainfall event
measured shall result from the sampled representative storm event.
Part II Page 5 of 6

Permit No. NCS000374
Table 5. Cut-off Concentrations for On -Site Vehicle Maintenance Activities
�. a.;s"�?,Discha"rge Characteristics`ill T � ,1=" .
i', �€�9 �?�. , ` �' RCut offaConcentrat�on El ',..: :.��°'f`n3�3 E e[
pH'
Within range 6.0 - 9.0
Oil and Grease
30 mg/l
Total Suspended Solids
100 mg/l
Footnotes:
1 pH cannot be averaged due to the nature of the logarithmic pH scale, The most recent pH sample result shall be
used for cut-off concentration purposes.
m
Part II Page 6 of 6

Permit No. NCS000374
PART III STANDARD CONDITIONS FOR NPDES STORMWATER INDIVIDUAL PERMITS
SECTION A: COMPLIANCE AND LIABILITY
Compliance Schedule
The permittee shall comply with Limitations and Controls specified for stormwater discharges in
accordance with the following schedule:
Existing Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented within
12 months of the effective date of the initial permit and updated thereafter on an annual basis. Secondary
containment, as specified in Part II, Section A, Paragraph 2(b) of this permit, shall be accomplished within
12 months of the effective date of the initial permit issuance.
Proposed Facilities: The Stormwater Pollution Prevention Plan shall be developed and implemented prior
to the beginning of discharges from the operation of the industrial activity and be updated thereafter on an
annual basis. Secondary containment, as specified in Part 11, Section A, Paragraph 2(b) of this permit shall
be accomplished prior to the beginning of discharges from the operation of the industrial activity.
2. Duty to Comply
The permittee must comply with all conditions of this individual permit. Any permit noncompliance
constitutes a violation of the Clean Water Act and is grounds for enforcement action; for permit
termination, revocation and reissuance, or modification; or denial of a permit upon renewal application.
a. The permittee shall comply with standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants within the time provided in the regulations that establish
these standards or prohibitions, even if the perm it has not yet been modified to incorporate the
requirement.
b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil
penalty not to exceed $25,000 per day for each violation. Any person who negligently violates
any permit condition is subject to criminal penalties of $2,500 to $25,000 per day of violation, or
imprisonment for not more than 1 year, or both. Any person who knowingly violates permit
conditions is subject to criminal penalties of $5,000 to $50,000 per day of violation, or
imprisonment for not more than 3 years, or both. Also, any person who violates a permit
condition may be assessed an administrative penalty not to exceed $10,000 per violation with the
maximum amount not to exceed $125,000. [Ref: Section 309 of the Federal Act 33 USC 1319 and
40 CFR 122.4 ] (a).]
C. Under state law, a daily civil penalty of not more than ten thousand dollars ($10,000) per violation
may be assessed against any person who violates or fails to act in accordance with the terms,
conditions, or requirements of a permit. [Ref: North Carolina General Statutes 143-215.6A]
d. Any person may be assessed an administrative penalty by the Director for violating section 301,
302, 306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing
any of such sections in a permit issued under section 402 of the Act. Administrative penalties for
Class I violations are not to exceed $10,000 per violation, with the maximum amount of any Class
I penalty assessed not to exceed $25,000. Penalties for Class II violations are not to exceed
$10,000 per day for each day during which the violation continues, with the maximum amount of
any Class Il penalty not to exceed $125,000.
Part III Page 1 of 8 Pages

Permit No. NCS000374
3. Duty to Mitigate
The permittee shall take all reasonable steps to minimize or prevent any discharge in violation of this
individual permit which has a reasonable likelihood of adversely affecting human health or the
environment.
4. ' Civil and Criminal Liability
Except as provided in Part III, Section C of this permit regarding bypassing of stormwater control facilities,
nothing in this individual permit shall be construed to relieve the permittee from any responsibilities,
liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6A, 143-215.6B, 143-
215.6C or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Oil and Hazardous Substance Liability
Nothing in this individual permit shall be construed to preclude the institution of any legal action or relieve
the permittee from any responsibilities, liabilities, or penalties to which the permitter is or may be subject
to under NCGS 143-215.75 et seq. or Section 311 of the Federal Act, 33 USC 1321.
6. Property Rights
The issuance of this individual permit does not convey any property rights in either real or personal
property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of
personal rights, nor any infringement of Federal, State or local laws or regulations.
7. Severability
The provisions of this individual permit are severable, and if any provision of this individual permit, or the
application of any provision of this individual permit to any circumstances, is held invalid, the application
of such provision to other circumstances, and the remainder of this individual permit, shall not be affected
thereby.
8. Duty to Provide Information
The permittee shall furnish to the Director, within a reasonable time, any information which the Director
may request to determine whether cause exists for modifying, revoking and reissuing, or terminating the
permit issued pursuant to this individual permit or to determine compliance with this individual permit.
The permittee shall also furnish to the Director upon request, copies of records required to be kept by this
individual permit.
9. Penalties for Tampering
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders
inaccurate, any monitoring device or method required to be maintained under this individual permit shall,
upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not
more than two years per violation, or by both. If a conviction of a person is for a violation committed after
a first conviction of such person under this paragraph, punishment is a fine of not more that $20,000 per
day of violation, or by imprisonment of not more than 4 years, or both.
Part III Page 2 of 8 Pages

Permit No. NCS000374
10. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation,
or certification in any record or other document submitted or required to be maintained under this
individual permit, including monitoring reports or reports of compliance or noncompliance shall, upon
conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more
than two years per violation, or by both.
SECTION B: GENERAL CONDITIONS
Individual Permit Expiration
The permittee is not authorized to discharge after the expiration date. In order to receive automatic
authorization to discharge beyond the expiration date, the permittee shall submit forms and fees as are
required by the agency authorized to issue permits no Iaer than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not
have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will
be subjected to enforcement procedures as provided in NCGS §143-2153.6 and 33 USC 1251 et. seq.
2. Transfers
This permit is not transferable to any person except after notice to and approval by the Director. The
Director may require modification or revocation and reissuance of the permit to change the name and
incorporate such other requirements as may be necessary under the Clean Water Act.
3. Signatory Requirements
All applications, reports, or information submitted to the Director shall be signed and certified.
a. All applications to be covered under this individual permit shall be signed as follows:
(1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a
responsible corporate officer means: (a) a president, secretary, treasurer or vice president
of the corporation in charge of a principal business function, or any other person who
performs similar policy or decision making functions for the corporation, or (b) the
manager of one or more manufacturing production or operating facilities employing
more than 250 persons or having gross annual sales or expenditures exceeding 25 million
(in second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor,
respectively; or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive
officer or ranking elected official
b. All reports required by the individual permit and other information requested by the Director shall
be signed by a person described above or by a duly authorized representative of that person. A
person is a duly authorized representative only if.
(1) The authorization is made in writing by a person described above;
Part III Page 3 of 8 Pages

Permit No. NCS000374
(2) The authorization specified either an individual or a position having responsibility for the
overall operation of the regulated facility or activity, such as the position of plant
manager, operator of a well or well field, superintendent, a position of equivalent
responsibility, or an individual or position having overall responsibility for
environmental matters for the company. (A duly authorized representative may thus be
either a named individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Director.
C. Any person signing a document under paragraphs a. or b. of this section shall make the following
certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my
direction or supervision in accordance with a system designed to assure that qualified personnel
properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system, or those persons directly responsible for gathering the
information, the information submitted is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
4. Individual Permit Modification Revocation and Reissuance, or Termination
The issuance of this individual permit does not prohibit the Director from reopening and modifying the
individual permit, revoking and reissuing the individual permit, or terminating the individual permit as
allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122
and 123; Title 15A of the North Carolina Administrative Code, Subchapter 2H .0100; and North Carolina
General Statute 143-215.1 et, al.
After public notice and opportunity for a hearing, the individual permit may be terminated for cause. The
filing of a request for a individual permit modification, revocation and reissuance, or termination does not
stay any individual permit condition. The permit shall expire when the individual permit is terminated.
Permit Actions
The permit may be modified, revoked and reissued, or terminated for cause. The notification of planned
changes or anticipated noncompliance does not stay any individual permit condition.
SECTION C: OPERATION AND MAINTENANCE OF POLLUTION CONTROLS
1. 'Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and
control (and related appurtenances) which are installed or used by the permittee to achieve compliance with
the conditions of this individual permit. Proper operation and maintenance also includes adequate
laboratory controls and appropriate quality assurance procedures. This provision requires the operation of
back-up or auxiliary facilities or similar systems which are installed by a permittee only when the operation
is necessary to achieve compliance with the conditions of this individual permit.
2. Need to Halt or Reduce Not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt
or reduce the permitted activity in order to maintain compliance with the condition of this individual
permit.
Part III Page 4 of 8 Pages

Permit No. NCS000374
Bypassing of Stormwater Control Facilities
Bypass is prohibited and the Director may take enforcement action against a permittee for bypass unless:
a. Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; and
b. There were no feasible alternatives to the bypass, such as the use of auxiliary control facilities,
retention of stormwater or maintenance during normal periods of equipment downtime or dry
weather. This condition is not satisfied if adequate backup controls should have been installed in
the exercise of reasonable engineering judgment to prevent a bypass which occurred during
normal periods of equipment downtime or preventive maintenance; and
C. The permittee submitted notices as required under, Part 11I, Section E of this permit.
If the Director determines that it will meet the three conditions listed above, the Director may approve an
anticipated bypass after considering its adverse effects.
SECTION D: MONITORING AND RECORDS
1. Representative Sampling
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and
nature of the permitted discharge. Analytical sampling shall be performed during a representative storm
event. Samples shall be taken on a day and time that is characteristic of the discharge. All samples shall be
taken before the discharge joins or is diluted by any other waste stream, body of water, or substance.
Monitoring points as specified in this permit shall not be changed without notification to and approval of
the Director.
2. Recording Results
For each measurement, sample, inspection or maintenance activity performed or collected pursuant to the
requirements of this individual permit, the permittee shall record the following information:
a. The date, exact place, and time of sampling, measurements, inspection or maintenance activity;
b. The individual(s) who performed the sampling, measurements, inspection or maintenance activity;
C. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. . The analytical techniques or methods used; and
f. The results of such analyses.
Flow Measurements
Where required, appropriate flow measurement devices and methods consistent with accepted scientific
practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of
monitored discharges.
Part III Page 5 of 8 Pages

Permit No. NCS000374
4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the EMC regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant
to Section 304(g), 33 USC 1314, of the Federal Water Pollution Control Act, as Amended, and Regulation
40 CFR 136.
To meet the intent of the monitoring required by this individual permit, all test procedures must produce
minimum detection and reporting levels and all data generated must be reported down to the minimum
detection or lower reporting level of the procedure.
Representative Outfall
If a facility has multiple discharge locations with substantially identical stormwater discharges that are
required to be sampled, the permittee may petition the Director for representative outfall status. If it is
established that the stormwater discharges are substantially identical and the permittee is granted
representative outfalI status, then sampling requirements may be performed at a reduced number of
outfalls.
6. Records Retention
Visual monitoring shall be documented and records maintained at the facility along with the Stonnwater
Pollution Prevention Plan. Copies of analytical monitoring results shall also be maintained on -site. The
permittee shall retain records of all monitoring information, including all calibration and maintenance
records and all original strip chart recordings for continuous monitoring instrumentation, and copies of all
reports required by this individual permit for a period of at least 5 years from the date of the sample,
measurement, report or application. This period may be extended by request of the Director at any time.
7. Inspection and Entry
The permittee shall allow the Director, or an authorized representative (including an authorized contractor
acting as a representative of the Director), or in the case of a facility which discharges through a municipal
separate storm sewer system, an authorized representative of a municipal operator or the separate storm
sewer system receiving the discharge, upon the presentation of credentials and other documents as may be
required by law, to;
Enter upon the permittee's premises where a regulated facility or activity is located or conducted,
or where records must be kept under the conditions of this individual permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions
of this individual permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control
equipment), practices, or operations regulated or required under this individual permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring individual permit compliance
or as otherwise authorized by the Clean Water Act, any substances or parameters at any location.
Part III Page 6 of 8 Pages

Permit No. NCS000374
SECTION E: REPORTING REQUIREMENTS
1. Discharge Monitoring Reports
Samples analyzed in accordance with the terms of this permit shall be submitted to the Division on
Discharge Monitoring Report forms provided by the Director. Submittals shall be received by the Division
no later than 30 days from the date the facility receives the sampling results from the laboratory.
Documentation of the qualitative monitoring associated with the initial analytical monitoring event shall be
included with the required analytical monitoring submittal for the first year of the permit coverage.
Analytical results from sampling during the final year of the permit coverage shall be submitted with the
permit renewal application.
2. Submitting Reports
Duplicate signed copies of all reports required herein, shall be submitted to the following address:
Division of Water Quality
Water Quality Section
ATTENTION: Central Files
Post Office Box 29535
Raleigh, North Carolina 27626-0535
Availability of Reports
Except for data determined to be confidential under NCGS 143-215.3(a)(2) or Section 308 of the Federal
Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public
inspection at the offices of the Division of Water Quality. As required by the Act, analytical data shall not
be considered confidential. Knowingly making any false statement on any such report may result in the
imposition of criminal penalties as provided for in NCGS 143-215.6E or in Section 309 of the Federal Act.
4. Non-Stormwater Discharges
If the storm event monitored in accordance with this individual permit coincides with a non-stormwater
discharge, the permittee shall separately monitor all parameters as required under the non-stormwater
discharge permit and provide this information with the stormwater discharge monitoring report.
Planned Changes
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which could significantly alter the nature or quantity of pollutants discharged. This notification
requirement includes pollutants which are not specifically listed in the individual permit or subject to
notification requirements under 40 CFR Part 122.42 (a).
6. Anticipated Noncompliance
The permittee shall give notice to the Director as soon as possible of any planned changes at the permitted
facility which may result in noncompliance with the individual permit requirements.
Part III Page 7 of 8 Pages

Permit No. NCS000374
7. Bypass
a. Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit
prior notice, if possible at least ten days before the date of the bypass; including an evaluation of
the anticipated quality and affect of the bypass.
b. Unanticipated bypass. The permittee shall submit notice within 24 hours of becoming aware of an
unanticipated bypass.
I
8. Twenty-four Hour Reporting
The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from
the time the permittee became aware of the circumstances. A written submission shall also be provided
within 5 days of the time the permittee becomes aware of the circumstances.
The written submission shall contain a description of the noncompliance, and its causes; the period of
noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the
anticipated time compliance is expected to continue; and steps taken or planned to reduce, eliminate, and
prevent reoccurrence of the noncompliance.
The Director may waive the written report on a case -by -case basis if the oral report has been received
within 24 hours.
9. Other Noncompliance
The permittee shall report all instances of noncompliance not reported under 24 hour reporting at the time
monitoring reports are submitted.
10. Other Information
Where the permittee becomes aware that it failed to submit any relevant facts in an application for an
individual permit or in any report to the Director, it shall promptly submit such facts or information.
Part III Page 8 of 8 Pages

Permit No. NCS000374
PART IV LIMITATIONS REOPENER
This individual permit shall be modified or alternatively, revoked and reissued, to comply with any applicable
effluent guideline or water quality standard issued or approved under Sections 302(b) (2) (c), and (d), 304(b) (2)
and 307(a) of the Clean Water Act, if the effluent guideline or water quality standard so issued or approved:
a. Contains different conditions or is otherwise more stringent than any effluent limitation in the individual
permit; or
b. Controls any pollutant not limited in the individual permit.
The individual permit as modified or reissued under this paragraph shall also contain any other requirements in the
Act then applicable.
PART V ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
The permittee must pay the administering and compliance monitoring fee within 30 (thirty) days after being billed
by the Division. Failure to pay the fee in timely manner in accordance with 15A NCAC 2H .0105(b)(4) may cause
this Division to initiate action to revoke the Individual Permit.
PART VI DEFINITIONS
1. Act
See Clean Water Act.
2. Arithmetic Mean
The arithmetic mean of any set of values is the summation of the individual values divided by the number
of individual values.
3. Allowable Nan-Stormwater Discharges
This permit regulates stormwater discharges. Non-stormwater discharges which shall be allowed in the
stormwater conveyance system are:
(a) All other discharges that are authorized by a non-stormwater NPDES permit.
(b) Uncontaminated groundwater, foundation drains, air -conditioner condensate without added
chemicals, springs, discharges of uncontaminated potable water, waterline and fire hydrant
flushings, water from footing drains, flows from riparian habitats and wetlands.
(c) Discharges resulting from fire -fighting or fire -fighting training.
4. Best Management Practices (BMPs)
Measures or practices used to reduce the amount of pollution entering surface waters. BMPs may take the
form of a process, activity, or physical structure.
Parts IV, V and VI Page 1 of 5

T v 1
Permit No. NCS000374
5. Bypass
A bypass is the known diversion of stormwater from any portion of a stormwater control facility including
the collection system, which is not a designed or established operating mode for the facility.
6. Bulk Storage of Liquid Products i
Liquid raw materials, manufactured products, waste materials. or by-products with a single above ground
storage container having a capacity of greater than 660 gallons or with multiple above ground storage
containers located in close proximity to each other having a total combined storage capacity of greater than
1,320 gallons.
7. Clean Water Act
The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33
USC 1251, et, seq.
8. • Division or DWQ
The Division of Water Quality, Department of Environment and Natural Resources.
9. Director
The Director of the Division of Water Quality, the permit issuing authority.
10. EMC
The North Carolina Environmental Management Commission.
IL Grab Sample
An individual samples collected instantaneously. Grab samples that will be directly analyzed or
qualitatively monitored must be taken within the first 30 minutes of discharge.
12. Hazardous Substance
Any substance designated under 40 CFR Part 116 pursuant to Section 3 11 of the Clean Water Act.
13. Landfill
A disposal facility or part of a disposal facility where waste is placed in or on land and which is not a land
treatment facility, a surface impoundment, an injection well, a hazardous waste long-term storage facility
or a surface storage facility.
14. Municipal Separate Storm Sewer System
A stormwater collection system within an incorporated area of local self-government such as a pity or
town.
15. Overburden
Any material of any nature, consolidated or unconsolidated, that overlies a mineral deposit, excluding
topsoil or similar naturally -occurring surface materials that are not disturbed by mining operations.
Part VI Page 2 of 5 Pages

z Q I
Permit No. NCS000374
16. Permittee
The owner or operator issued a permit pursuant to this individual permit.
17. Point Source Discharge of Stormwater
Any discernible, confined and discrete conveyance including, but not specifically limited to, any pipe,
ditch, channel, tunnel, conduit, well, or discrete fissure from which stormwater is or may be discharged to
waters of the state.
18. Representative Storm Event
A storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours in
which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain
up to 10 consecutive hours of no precipitation. For example, if it rains for 2 hours without producing any
collectable discharge, and then stops, a sample may be collected if a rain producing a discharge begins
again within the next 10 hours.
19. Representative Outfall Status
When it is established that the discharge of stormwater runoff from a single outfall is representative of the
discharges at multiple outfalls, the DWQ may grant representative outfall status. Representative outfall
status allows the permittee to perform analytical monitoring at a reduced number of outfalls.
20. Rinse Water Discharge
The discharge of rinse water from equipment cleaning areas associated with industrial activity. Rinse
waters from vehicle and equipment cleaning areas are process wastewaters and do not include washwaters
utilizing any type of detergent or cleaning agent.
21. Secondary Containment
Spill containment for the contents of the single largest tank within the containment structure plus sufficient
freeboard to allow for the 25-year, 24-hour storm event.
22. Section 313 Water Priority Chemical
A chemical or chemical category which:
a. Is Iisted in 40 CFR 372.65 pursuant to Section 313 of Title III of the Superfund Amendments and
Reauthorization Act (SARA) of 1986, also titled the Emergency Planning and Community Right -
to -Know Act of 1986;
b. Is present at or above threshold levels at a facility subject to SARA title III, Section 313 reporting
requirements; and
That meet at least one of the following criteria:
(1) Is listed in Appendix D of 40 CFR part 122 on either Table II (organic priority
pollutants), Table III (certain metals, cyanides, and phenols) or Table IV (certain toxic
pollutants and hazardous substances);
(2) Is listed as a hazardous substance pursuant to section 311(b)(2)(A) of the CWA at 40
CFR 116.4; or
Part VI Page 3 of 5 Pages

f 4 1
Permit No. NCS000374
(3) Is a pollutant for which EPA has published acute or chronic water quality criteria.
23. Severe Property Damage
Means substantial physical damage to property, damage to the control facilities which causes them to
become inoperable, or substantial and permanent loss of natural resources which can reasonably be
expected to occur in the absence of a bypass. Severe property damage does not mean economic loss
caused by delays in production.
24. Si ificant Materials
Includes, but is not limited to: raw materials; fuels; materials such as solvents, detergents, and plastic
pellets; finished materials such as metallic products; raw materials used in food processing or production;
hazardous substances designated under section 101(14) of CERCLA; any chemical the facility is required
to report pursuant to section 313 of Title III of SARA; fertilizers; pesticides; and waste products such as
ashes, slag and sludge that have the potential to be released with stormwater discharges.
25. Significant Spills
Includes, but is not limited to: releases of oil or hazardous substances in excess of reportable quantities
under section 311 of the Clean Water Act (Ref: 40 CFR 110.10 and CFR 117.21) or section 102 of
CERCLA (Ref: 40 CFR 302A).
26. Stormwater Runoff
The flow of water which results from precipitation and which occurs immediately following rainfall or as a
result of snowmen.
27. Stormwater Associated with Industrial Activity
The discharge from any point source which is used for collecting and conveying stormwater and which is
directly related to manufacturing, processing or raw material storage areas at an industrial site. Facilities
considered to be engaged in "industrial activities" include those activities defined in 40 CFR 122.26(b)(14).
The term does not include discharges from facilities or activities excluded from the NPDES program.
28. Stormwater Pollution Prevention Plan
A comprehensive site -specific plan which details measures and practices to reduce stormwater pollution
and is based on an evaluation of the pollution potential of the site.
29. Ten Year Desi2 Storm
The maximum 24 hour precipitation event expected to be equaled or exceeded on the average once in ten
years. Design storm information can be found in the State of North Carolina Erosion and Sediment
Control Planning and Design Manual.
30. Total Flow
The flow corresponding to the time period over which the entire storm event occurs. Total flow shall be
either; (a) measured continuously, (b) calculated based on the amount of area draining to the outfall, the
amount of built -upon (impervious) area, and the total amount of rainfall, or (c) estimated by the
measurement of flow at 20 minute intervals during the rainfall event.
Part VI Page 4 of 5 Pages

Permit No. NCS000374
31. Toxic Pollutant
Any pollutant listed as toxic under Section 307(a)(1) of the Clean Water Act.
32. Upset
Means an exceptional incident in which there is unintentional and temporary noncompliance with
technology based permit effluent limitations because of factors beyond the reasonable control of the
permittee. An upset does not include noncompliance to the extent caused by operational error, improperly
designed treatment or control facilities, inadequate treatment or control facilities, lack of preventive
maintenance, or careless or improper operation.
33. Vehicle Maintenance Activity
Vehicle rehabilitation, mechanical repairs, painting, fueling, lubrication, vehicle cleaning operations, or
airport deicing operations.
34. Visible Sedimentation
Solid particulate matter, both mineral and organic, that has been or is being transported by water, air,
gravity, or iee from its site of origin which can be seen with the unaided eye.
35. 25-year, 24 hour storm event
The maximum 24-hour precipitation event expected to be equaled or exceeded, on the average, once in 25
years.
Part VI Page 5 of 5 Pages

KE"i
20emo RECEIVED
APR b 1999
FAYETTEVILLE
To: Ken Averitte REG. OFFICE
Fr: Darren England
,Re: Draft of NCS000374 for regional staff review
Date: 04/05/99
Attached you will find for your review and approval, a draft of an individual stormwater
permit for the Buckeye Lumberton, Inc. facility in Lumberton, N.C. The majority of the
permit is standard boilerplate, except for the pages dealing with analytical sample
requirements and representative outfall status (see flags). If you have any questions give
me a call. Thanks!

NPDES Stormwater Permit Application
Buckeye Lumberton, Incorporated
1000 East Noir Street
Lumberton, North Carolina
December 1998
Prepared by
ARCADIS Geraghty & Miller
2301 Rexwoods Drive
Raleigh, North Carolina 27607
Project Number 39781.0000

4
•
.•
TABLE OF CONTENTS
General Information Form - EPA Form 3510-1
Permit Application Forms - EPA Form 3510- 2F
Discharge Information Forms - EPA Form 3510 - 2F
Analytical Laboratory Reports
Calculations of Total Flow
Facility Drainage Map
REC�IVED
QPR 6 1999
RAG rLLE
OFFICE
Section I
Section II
Section III
Appendix A
Appendix B
Appendix C

_ -rA�rtiiL.i'a—•AC'Y:-'Cn ♦_['.-
-.EPA GENERAL INFORMATION
Car*solydeyd PerrnrCr Program
GENERAL �1 Rer l the "General lnsrruct", of/ore Irarrtnr .
I. EPA I.O. NUMBER
PAC\LITY NAME Buckeye Lumberton, Inc,
FACILITY 1000 East Noir Street
V. I\ II;NG AODRESS,, Lumberton, NC 28359
FACILITY ±
V!. LOCATION
I1. POLLUTANT CHARACTERISTICS
I, :?1 I,�, VI,IMiSER
GC`iCPAL INSTw UCTIpn3
If a preprinted lapel has been provided. affix
it In the designated space. Review the ,ntarm-
atiOn Carefutly: if any Of it is incorrect. Cross
through it and enter the enr"ct Oats in the
appropriate fill—in error below, Also, if any of
the preprinted data is absent (the area ro the
left of the label space Jim the iirFormarion
Gnat should appear), please provide it in vta
proper fill -min arse l below. It the label la
complete and correct, you need aoi eompiets
Items I. I I t, V, and V 1 fesemr Yl-8 aot is r
murr be completed rogordlessl, Complete sit
items if no label has been providad. paler to
the instructions for deuiled item deurip-
lions and for the legal authorisations under
which this data is Collernd.
INSTRUCTIONS: Complete A through J to determine whether you need -to submit.any permit Application farms to the EPA. It you answer "yes" to any
questions, you must submit this form and the supplementat form listed in the parent msis following the question, Marie ,Xr, in the box in the third column
if the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity
is excluded from permit requirements: sea Section C of the instructions, Sae also, Section 0 of the instructions for definitions of bold—faced terms.
MAR. Y
SPECIFIC OUCSTION5
A. Is this facll,ry a publicly owned treatment wosks
wn-cri results in a discharge to wtrtem of the U.S.?
(FORM 2A)
C. is trt;$ a facility wn-cn currentiy results In discharges
10 waters tsf the U.S. Other than those described in
A or 9 aoo.0 IFr]P. V1 2C1
E Cots or will this facility treat• store, or dispose of
hauaraous wastals? (FORM 3)
U. Ua you or will you In1eC: it M,S IaCillty any prOouccO
water or Other fluids which are brought to the surface
in connection with conventional oil or natural gas pro-
Sumion, inlect Huids used for enhanced recovery of
it or natural gas, or inlect fluids for storage of liquid
ydrocarbons? IF OR M 41
s tills au try s prop -sod strtionary source w i Is
one of the 28 industrial categories listed in the in.
structrons and which will potentially emit 100 tons
per year of any air' pollutant regulated under the
Clean Air Act and may affect are be loeetad in an
attainment areal (FORM 51
111, NAME OF FACILITY
c I I I
IV. FACILITY CONTACT
+,�y
wa VewY
••-r wci,�
�Xj
I�
X
I
s.
X
X
A. NAME ar TITLE (last. /lilt, et fiflel
SPECIFIC QW93TIONS
•ss I we Air �c.�iec
8. Does or will this facility (either errirring or Proposed!
include a eor+arstrrtad animal fmdin4 apeesrtion or
equrtic anirrsal production facithy which results in a
discharge to srstoo of the U.S,? (FORM 2B)
,X, „
let is a proposed taciirry o or than Mom Cemribeil
in A or B abovel which will rttsu(t in a dinctiorge to
Xj
sirseters of the US.? (FORM 201
i+ a• n
F, Do you or will you inject at this facility industrial or
;
municipal effluent below the lowermost stratum con-
I
raining, within one quarter mile of the well bore,
Xj
underground aourcas of drinking water? (FORM 41
M. Do you or will you inject at this facility fluids for spa-
cial processes such as mining of sulfur by the Frasch
X
process, Solution mining of minerals, in situ combus
tion of fossil fuel, or recovery of geothermal energy?
(FORM 4)
J. s this teality, a pr000sed tritardionary source whicrt 1I
NOT one of the 28 industrial categories listed in the
Instructions and which will potennially emit 250 torts
X
per year of any air pollutsrrt regulated under the Clean
Air Act and may affect or be located in an arttoinmertt
area? (FORM 5)
.s
..
.+
e. ►r+ON E farra code b no. r
I
2 ^.A bar s
'Bound. Plant Manager, f`r I I 1'llt_y—/_J—f Itll'
V. FACILITYMAILING"ADDRESS
A. STREET OR I.O. SOX
3 .East. offing LDp -
e. CITY OR TOWN IC.STATE; to III COOS 1
4 u 283 9
V1. FACILITY LOCATION
A. STREET. ROUTE NO. OR OTHER SPECIFIC 10£i4TIFiER
5: 1A00 East Noir Street I
e C'.SV NTY NAMC
obeson I
c =,TY OR TOwir 0.sT,•re: E. ZIP coot COUNTY
_ 'n
o Lumberton _ ! NC i 28358 f I
EPA Form 3570.1 IRay. 10-801
1-12
CONTINUE ON REVERSE

•
SECTION II, ITEM E.
Buckeye disposes of a very small quantity of hazardous waste through Safety Kleen,
Inc. The waste is from a parts washer in the maintenance area. Buckeye is a
conditionally exempt small quantity generator (CESQG).
Ll
C:

CONT;NUEO eROM THE a
V11• SIC CODES ia.dI In OrOer Of ohorrry,
A FIRST • SlC0N0
lrprc1l;' rr:rrlJ:•
Put M 7
C. THIwO
D FOURTH
liplrr%}'1 lfp rr,fV1
7
,f
viw OPERATOR INFORMATION
A. NAM E It the n•Flt• Hated In
It+rn VIII-A also me
c
ovint o 7
8 Lumberton Tnnnrpnrated a) YES = NO
•4
C. STATUS OF OPERATOR ,'Enter the appropriare lerrrrento the answer box, if"Other". specify.)
D. F..ONE larva cods 6 no.,
FEDERAL M • UBL! (other than federal orrtare)
ecs 1Y1
S - STATE 0 OTHER (opacity)
P
TIP.
A 910
737
3200
P -PRIVATE
„
. ,. ,.
,. i,
,� �,
K. STREET OR P.C. Box
1000 East Noir Street
F. CITy OR TOWN
r-.ST^TK
H• ZIP CODE
IX, INDIAN LANO
' ' 1 ' 'I I I
I
. I
It the faCillty 1005ted On IrI 121'1
B
Lumberton
NC
28349
= YES IZ; NO
s:
X. EXISTING ENVIRONMENTAL PERMIT5
A. N►ots /Discharges to Surface Water)
D, FSD (Air E•miszions from Proposed Sources).
e
9 P 583R8
e
P�9
N
NC 0005321
•'. U IC IL'ndersround fn)eerian of Fluids)
[. OTHER (specify)
c
9 U'
9 `
T
ea'ly1 (sp
c. wcwA (Ha.ardous Wastes)
K.0THEw fsprerfy)
RQISIU920143 (saecify)
9
WAP'
Attach to this application a topographic map of the area extending to at least one mile beyond property bounderies. The map must show
the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its hazardous waste
treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include ail springs,_rivers and other surface
water bodies in the map area. See instructions for precise requirements.
XI I. NATURE OF BUSINESS )provide -a brief destr)ptian
This facility manufactures cotton paper using cotton linters as a raw material. The
final product consists of card stock type paper that is bulk packaged and sold as
intermediate material to paper finishing manufacturers.
X1I1, CERTIFICATION (s•einsvixtiona)M
I certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this application and all
attachments and char, based on my inquiry of those persons immediately responsible for obtaining the information contained in the
application, 1 believe that the information is true, accurate and complete. I am aware that there are significant penalties for submitting
false information, including the possibility of fine and imprisonment.
A NAME • OFFICIAL TIT a_r: ,rype qr inn f: ■. SIGNATURE C, DATE SIGNED
Albert,A. Bounds, Plant Manager
ENTs FOR OFFICIAL USE ONLY
i i I I i 4 L I i I I I j
CI
EPA Form 3510.1 IR•v, 10-901 Ravens
1-13

L rrL� .--{1a�ri
` Fi� 1riiHr rf yr'�y
�}
�_�
�•1
�cyaa' .��•sF'?�,','.,IIC�7)��g
�I�C.a�LwaY�c�l7i f' lw �u rb �i i +•
'`-c; �,:✓ � � r 4 � Ir�e�+`—`,� 1 �ir'��� ''�i' ��I�'���f_aif�/
,.NOR ,�
L
j/
----� :.':.!ire• f :s a�k?. Iri '�PE
'"js�"•�'�` � � � � '1 � �r, �s'�r'n� s•C 1 fY F:,.S.,.e'S �� Fn . pig M'�� ,t~' �'• w� Mh It"�'.+�y� �..-_ \
An
/A� `, �,?C/.- � s y :Y�w A� f.l � M1 �.�! \�" •.w.r s.• � h� ` �`" �i)�
f I �
\ Y� �r''�4• '��C� + is Tr I 1 \ Jj r rY,
Lt-;
\llr"61fr1
'-f+S { =rl ,•'!•�.:�, _ S V�l ter., 'w i��5� \\1 `.. �� N
NLYW
} }� �� •�. �� au i �e� f•-�Y}—IJ In�� ) f �' �7, r .�1. ��'�`"/n.

Please print or type in the unshaded areas only
EPA ID Number (copy from Item ! of form 1J Form Approved. OMB No. 2040-0086
Approval expires 5-31-92
Form United States Environmental Protection Agency
Washington, DC X460
2Fl EPA
�er Application for Permit To Discharge Stormwater
PpEs t� Discharoes Associated with Industrial Activitv
Paperwork Reduction Act Notice
Public reporting burden for this application is estimated to average 28.6 hours per application, including time for reviewing instructions,
searching existing data sources, gathering and maintaining the data needed, and completing and reviewing the collection of information. Send
comments regarding the burden estimate, any other aspect of this collection of information, or suggestions for improving this form, including
suggestions which may increase or reduce this burden to: Chief, Information Policy Branch, PM-223, U.S. Environmental Protection Agency,
401 M St., SW. Washington, DC 20460, or Director, Office of Information and Regulatory Affairs, Office of Management and Budget,
Washington, DC 20503. ,
I. QUtfall Location
For each ouffall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receivino water.
D. Receiving
• •
e>A r.Rl�111IN111111
V_ .
_
0 Mom
NIP 1.11M.1
A. Are you now required by any Federal, State, or local authority to meet any implementation schedule for the construction, upgrading or
operation of wastewater treatment equipment or practices or any other environmental programs which may affect the discharges
described in this application? This includes, but is not limited to, permit conditions, administrative Or enforcement orders, enforcement
compliance schedule letters, stipulations, court orders, and grant or loan conditions,.
. I 1 f 4. Final
1, identification of Conditions, 2, Affected Outtalls
Anfeements. Etc. I number I source of disc)
Brief
a. req, I b,
B. You may attach additional sheets describing any additional water pollution (or other environmental projects which may affect your
discharges) you now have under way or which you plan, Indicate whether each program is now under way or planned, and indicate your
actual or planned schedules Ior construction.
III, Site Drai
Attach a site map showing topography (or indicating the outline of drainage areas served by the outfall(s) covered in the application it a
topographic map is unavailable) depicting the facility including: each of its intake anti discharge structures; the drainage area of each storm
water outfall; paved -areas and buildings within the drainage area of each storm water ouffall, each known past or present areas used for
outdoor storage or disposal of significant materials, each existing structural control measure to reduce pollutants in storm water runoff,
materials loading and access areas, areas where pesticides, herbicides, scil conditioners and fertilizers are applied; each of its hazardous
waste treatment, storage or disposal units (including each area not required to have a RCRA permit which is used for accumulating hazardous
waste under 40 CFR 262.34); each well where fluids from the facility are injected underground; springs, and other surface water bodies which
receive storm water discharges from the facility.
EPA Form 3510-2F (11-90) Page 1 of 3 Continue on Page 2
2F-1

Contlnued from the Front
4
r
A. For each outfall, provide an estimate of the area (include units) of impervious surfaces [including paved areas and building roofs♦ drained
to the outfall, and an estimate of the total surface area drained by the outfall.
utfafl
Area of Impervious Surface
Total Area Drained
Outfall
I Area of impervious Surface
Total Area Drained
J
i
;r
1
2.06 ac
2.75 ac
6
.073'ac
2.39 ac
2
.83 ac
:83-ac
7
1.7 ac
1.7 act
4
3.65 ac
..41 ad'
1 94
8
0.57 ac
1.17 ac'
S. Provide a narrative description of significant materials that are currently or in the past three years have been treated, stored or disposed in
a manner to allow exposure to storm water; method of treatment, storage, or disposal; past and present materials management practices
employed, in the last three years, to minimize contact by these materials with storm water runoff; materials loading and access areas; and
the location, manner, and frequency in which pesticides, herbicides, soil conditioners, and fertilizers are applied.
See attachments
C. For each outfall, provide the location and a description of existing structural and nonstructural control measures to reduce pollutants in
storm water runoff; and a description of the treatment the storm water receives, including the schedule and type of maintenance for control
Ultimate solid
Outfall
List Codes from
NWmbr,r
T
T 1 F•t
c
See attachments
V. Nonstormwater Discharges
A. I certify under penalty of law that the outfall(s) covered by this application have been teSted or evaluated for the presence .of
nonstormwater discharges, and that all nonstormwater discharges from these outfall(s) are identified in either an accompanying Form 2C
r Form 2E application for the outlall.
Name and Otficial Title (type orprint)
Signature��q�
Date Signed
Albert A. Bounds, Plant Manager
B. Provide a description of the method used, the date of any testing., and the onsite drainage points that were directly observed during a test.
See attached memos from ARCADIS Geraghty & Miller to Eric -Bolin.
VI. Significant Leaks or S ills
Provide existing information regarding the history of significant leaks or spills of toxic or hazardous pollutants at the facility in. the last three
years, including the approximate date and location of the spill or leak, and the type and amount of material released.
No record of spilled materials classified toxic or hazardous as listed in
Table 2F-3 or 2F"4: "'
EPA Form 3510.2F (11.90) Page 2 of 3
2F-2
Continue on Page 3

•
C,
•
IV. NARRATIVE DESCRIPTION OF POLLUTANT SOURCES
PARTS B. AND C.
Buckeye Lumberton, Inc. uses, produces, and stores a number of materials that are important to
the industrial process. The major raw materials used by the plant include cotton linters, sodium
hydroxide, chlorine, sodium chlorite, sodium hypochlorite, hydrogen peroxide, sulfuric acid, and
tall oil fatty acid. The plant uses these materials in the digestion process to produce cotton pulp.
Other materials which are necessary to the plant's operation include fuel for the boilers, boiler
treatment chemicals, wastewater treatment chemicals(phosphoric acid, ammonium nitrate,
coagulant, flocculant, defoamer) , oils and lubricants for equipment maintenance, general house
keeping supplies, and laboratory chemicals.
The table below is a listing of significant materials and current management and control measures
in each outfall drainage area. Each item is identified on the site map by key note.
Drainage Area ! Existing Management Practices and Control Measures
OUTFALL 001
Shipping Dock
• The finished products loading dock is such that trucks back under a
roof overhang to load. This minimizes stormwater contact with
finished materials. Finished materials consist of cotton paper stock.
Chemical Loading
• The area identified by keynote 13 on the site plan (attached)
includes five hose connections for loading sodium hypochlorite,
sodium chlorite, tall oil, caustic, and scale troll corrosion inhibitor.
These chemical are pumped pneumatically to storage tanks inside
the facility.
OUTFALL 002
Waste Compactor
* The paper waste compactor is located on a concrete pad
surrounded on three sides by containment curbing. There is a sump
and pump at the low corner of the pad to transfer leachate to the
wastewater treatment plant.
g:Wmm%397911app1, narrativcdoc
Page:
1/4

L`
•
•
Drainage Area
Existing Management Practices and Control Measures
Receiving Loading Dock
• Raw materials consisting of baled cotton linters are unloaded in this
area. The loading dock is covered by a permanent shelter to shield
materials during rain. The loading dock shelter is such that trucks .
can back up under the shelter out of the rain.
OUTFALL 004
Rail Car Unloading for
• The rail cars are located such that any spilled material drains to a
chemicals.
sump where a pump, transfers the material to the facility wastewater
treatment plant. Chemicals shipped by rail include chlorine and
sodium hydroxide. Baled cotton linters and finished cotton paper
stock are also shipped by rail.
Bale Wire Dumpster
• An open dumpster is located in this area for disposal of metal straps
from bales of cotton linters.
Digester Blow -Off Tank
• Prior to installation of a cap for the digester blow down tank, air -
born pollutants were subject to settle on the roof and possibly reach
the outfall during storm events. Installation of the cap for the blow
down tank has drastically reduced if not eliminated this pollution
potential. The area around the blow -down tank drains to a sump
and is pumped to the wastewater treatment plant. -
• Outfall 005 consists only of roof drainage and a small portion of the
OUTFALL 005
asphalt road that loops around the plant. Prior to installation of a
cap for the digester blow -off tank, air -born pollutants were subject
to settle on the roof and possibly reach the outfall during storm
events. Installation of the cap for the blowdown tank has drastically
reduced if not eliminated this pollution potential.
OUTFALL 006
Flammable Liquids Storage
• Flammable liquids such as lubricants are stored under a shelter on a
concrete pad. Containment curbing is installed around the pad to
isolate leaks and spills. Material containers consist of 55 gallon
drums. During the past three years all drums have not been stored
inside the containment curbing, however better management
Scrap Yard
practices are currently being implemented.
• The scrap yard consists of a- partially grassed, bare soil area where
scrap arts and equipment are stored until reused in the plant or
g.VmmU9791%@pp1. naaat",dac
Page:
2/4

•
•
•
Drainage Area
Existing Management Practices and Control Measures
sold as salvage.
OUTFALL 007
Hydrogen Peroxide Storage
* The Hydrogen Peroxide Tank is surrounded by a secondary
containment wall to prevent spills. There is also containment
curbing for the truck unloading the peroxide.
General Waste Dumpster
* The dumpster is located on a concrete pad and surrounded by
concrete curbing to prevent stormwater runoff. Any liquid collected
here is pumped to the wastewater treatment plant.
Stock Towers
* The stock towers contain digested cotton linters at various stages in
the refining process. The stock towers ,as indicated by key note on
the site plan, are surrounded by concrete containment curbing with
drains to the wastewater treatment plant to prevent contact with
stormwater.
OUTFALL 008
Primary Receiving Basin
• The primary receiving basin is where the entire plant process sewer
is discharged. There are two backup pumps in case the normal
pump fails or the flow is two great. The primary basin is also
equipped with an audible alarm to signal plant personnel if levels in
Coagulant Bulk Storage
the basin get too high.
• Bulk coagulant for the wastewater sludge processing is stored in
this area. The tank currently does not have secondary containment.
AREA WEST OF WWTP
Sludge Filter Press and
• The filter press and facilities are housed in a metal building to
Facilities
prevent contact with stormwater. Sludge is loaded into trailers
inside the building with curbing to capture any filtrate. Empty
sludge trailers are parked on a concrete pad where all stormwater is
captured in a sump and pumped to the wastewater treatment plant.
Thickened sludge is then trucked to the farm off site and land
applied.
Fuel Oil and Sulfuric Acid
• Both the bulk fuel oil and sulfuric acid storage tanks are equipped
Storage Tanks
with secondary containment walls to prevent leaks and spills.
Stormwater that collects in the secondary containment areas is
pumped to the wastewater treatment plant.
Ammonia and Phosphoric
• The ammonia and phosphoric acid storage tanks used for
Acid Storage Tanks
wastewater treatment are equipped with secondary containment
walls to prevent leaks and spills.
Defoamer Bulk Storage
e The defoamer storage tank is equipped with seconda containment.
9Uwm13479UappL ne"atNe.doc
Page:
3/4

•
•
•
Drainage Area I Existing Management Practices and Control Measures
GENERAL
All raw and finished materials are stored inside the facility warehouse
areas. The primary plant process is indoors and includes a plant process
sewer to which all floor drains and process wastewater discharge. The
plant sewer discharges to the primary receiving basin prior to being
pumped to the wastewater treatment plant.
Pesticides, Herbicides, and No fertilizers are currently used, however there is some use of
Fertilizers herbicides and pesticides. Herbicide (Rround-up) is applied on an as
needed basis to control vegitation around fences and other structures.
Buckeye also contracts with Orkin to spray for fire ants around the
facility as needed. Drexel Dimethoate 4EC is applies to the waste
sludge inside the sludge building before land application to reduce
vector attraction.
p4vwm1397915appl. narrative.do[
Page:
4/4

�J
MEMO
To: Copies:
Eric Bolin
Buckeye Lumberton
From: Date:
Whit Wheeler
Subject:
Outfall Certification
ARCADIS Geraghty & Miller, Inc.
2301 Rexwoods Drive
Suite 200
Raleigh
North Carolina 27607-3366
Tel [phone]
Fax [phone]
Water and Waste
Management
Following are the observations from the first outfall certification performed on June 23, 1998. Visual
monitoring was performed by Whit Wheeler of ARCADIS Geraghty & Miller while accompanied by Eddie •
Wilkerson of Buckeye Technologies.
Outfall #1
Small amount of flow observed entering the canal in front of the plant. No flow was observed in either of
the two yard inlets that drain to this outfall. The observed flow is believed to be groundwater seeping into
the concrete drainage piping.
Outfall #2
Small amount of flow was observed leaving the yard inlet that drains to this butfall. The outfall pipe itself
was submerged in the drainage canal. The flow appeared to be seeping up from the bottom of the inlet and
is believed to be groundwater. No drain piping entering the inlet was visible. No surface flow was observed
entering the inlet.
Outfall #3
No flow observed. This outfall has been abandoned in place by filling the inlet with concrete.
Outfall #4
No flow observed
•
our ref.:
39791.00001outf a I I.doc
Page:
1/2

• ARCADIS
Outfall #5
Some flow observed (approximately lgpm). No flow was observed in the yard inlet at the corner of the
building that is piped to this outfall. The source of the flow is believed to be groundwater or the remnant
from the fire sprinkler drains.
Outfall #6
The outfall pipe was not viewable due to excess vegetation. However, flow was observed in the yard inlet
located in the scrap yard. A stream of water (approximately 3 gpm) was observed to be entering this
drainage system from an off site source adjacent to two abandoned masonry manholes. Per discussion with
Mr. Eric Bolin of Buckeye, The City of Lumberton was contacted to investigate the source of flow.
Outfall # 7
Flow from the air conditioning cooling water was draining to this outfall. The ac was out of service and
• this was not a normal event. The water was reported to be non -contact cooling water by plant maintenance
personnel. The outfall pipe was not visible due to excessive vegetation.
•
Outfall #8
The outfall pipe is not visible due to excessive vegetation. However, the three yard inlets that drain to this
outfall were observed and found to be dry.
our ref.: Page:
39791.00001outfall.doc 2/2

•
MEMO
To: Copies:
Eric Bolin
Buckeye Lumberton
From: Date:
Whit Wheeler 15 October 1998
5 u6J ect:
Outfall Certification
ARCADIS Geraghty & Miller, Inc
2301 Rexwoods Drive
Suite 200
Raleigh
North Carolina 27607-3366
Tel [phone]
Fax [phone]
Water and Waste
Management
Following are the observations from the outfall certification performed on October 13, 1998. Visual
observations were performed by Whit Wheeler of Arcadis Geraghty & Miller while accompanied by Eric
Bolin of Buckeye, Technologies.
Outfall #1
Small amount of flow observed entering the canal in front of the plant. The outfall showed no obvious color
or odor. The yard inlets feeding this outfall were also observed. A Small trickle of clear water was observed
flowing to the inlet at the NW corner of the building. The flow was coming from water left standing in the
open drainage channel adjacent to the building. Water in the drainage channel was explained to be the
remnant of a routine fire hydrant blow -off by plant maintenance personnel. The other yard inlet just north
of the building did not. exhibit any flow.
Outfall #2
No flow observed entering the yard inlet near the loading dock. The outfall pipe itself was submerged in the
drainage canal.
Outfall #3
No flow observed. Pipe has be plugged with concrete at the inlet.
Outfall #4
• No flow observed.
Our ref.: Page:
39791.0000loutfall2.doc 1 /2

0 ARCADIS
Outfall #S
No flow observed.
Outfall #6
The outfall pipe was submerged in the canal. Inlets feeding this outfall were visually monitored. Inlet 1 had
no flow entering through the top grating. The bottom of the inlet was not visible due to standing water.
Inlet 2 had no flow entering through the top grating. The bottom of the inlet had standing water as well, but
the water appeared calm and non- flowing. Inlet 3 was observed with no inflow. This outfall is connected
to drainage piping that goes off the property site.
Outfall # 7
The outfall pipe was submerged in the canal. Inlets feeding this outfall were visually monitored. Both inlet
• 1 and 2 were observed to be without flow.
0
Outfall #S
No flow observed.
our ref.: Page:
3979t.00001autfa112.doc 2/2

EPA ID Number (copy from Rem l of Form 1)
Continued from Page 2
IC, & D: See instructions before proceeding, Complete one set of tables for each outfail. Annotate the outfall number in the space provided.
Tables Vli-A, VII•B, and VII-C are included on separate sheets numbered VII-1 and VII.2.
Potential discharges not covered by analysis • Is any pollutant listed in Table 2F-2 a substance or a component of a substance which you
currently use or manufacture as an intermediate or final product or byproduct?
R Yes (list all such llurants below)No a ib section !JC)
F
Chlorine
Phosphoric Acid
Ammonium -Nitrate - 40% solution
Sulfuric Acid
Jesting Ontp
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or
on a receiving water in relation to your discharge within the last 3 years?
Yes (list all such pollutants below) No o to Section W
Chronic toxicity is a quarterly monitoring parameter in the facility.
NPDES permit for the existing WWTP discharge to the Lumber River.
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
® Yes (list the name, address, and telephone number of, and pollutants No (go to Section A)
A. Name B. Address C. Area Code & Phone No. D. Pollutants Analyled
ARCADIS Geraghty & Miller 2301 Rexwoods Drive
[phone] None
Suite 200
Raleigh, NC 27607
1 certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and
belief, true, accurate, and complete. l am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
tCNae
m& Cflicial Title (type or print) B. Area Code and Phone No.
Albert A. Bounds, Plant Manager [phone]
Signature � � D. Date Signed
EPA Form 3510-2F (11.9o) Page 3 of 3
1) t- I

EPA tD Number (copy from item i of Form r)
Outfall 001
rorm Approved. OMB No, 2040.0p86
Approval expires 5-31-82
V11. discharge Information (Ccnrrnued from page 3 of Form 2F
Part A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each curtail. See
instructions for additional details.
Pollutant
and
CAS Number
frl available)
Maximum Values Average Values Number
I !include units) (include units) of
Storm
Taken During Flow -weighted Taken Curing Flow -weighted E'+ents
Grab Sample Grab SampleI'Samoted
First 30 First 30 '
Minutes Composite Minutes Composite
Sources of Pollutants
Oil and Grease
3.5 m /1
{I
� 1 I Asphalt road
Biological Oxygen
Demand (8005)
7.6 mg/1
1
Chemical Oxygen
Demand fCO❑I
.410 mg/1
I
I
I 1
Total Suspended
Solids (TSSI
9.5 mg/1
1
Total Keldahl
Nitrogen
<1.0 mg/1
1
Nitrate plus
Nitrite Nitrogen
0.31 mg/1
I
1 I
Total
Phosphorus
r ,02 mg/1
1
PH Minimum- -Maximum Minimum Maximum
Part 8 - List eacn pollutant that is limiteo in an ettluent guidetrne wnrcn ine laanty is suolect to or any pollutant listed in the lacrlity s NP❑Ea
permit for its process wastewater (if the facility is operating under an existing NPOES permrtl Complete one table for eacn outfail.
f
Pollutant
and
CAS Number
(if available)
Maximum Values # Average values Number
(include units) I{ (include units) of
Grab Sample Grab Sample Storm
Taken During Flow -weighted Taken During Flow -weighted Events
First 30 First 30
Minutes Composite Minutes Composite Sampled Sources of Pollutants
NH3-- N
NA I I
Dissolve Ox NA I I
I
Temp I NA
i.
Chronic Toxi
NA I
Resid. C19 I
NA I — I
IBleaching process
Conductivit
NA
Dioxin
NA
I IBy—product
Settleable
I
Solids
NA
Above parameters
are re uired to -be reported -by
he NPDES pehgit for the facility WWT
I
I
I
I
I
I
I
I
I
I
�
EPA Form 3510-2F (11-90) Page Vtl-t Continue on Reverse
7F_d

-^ ram- l—&d frorn the Front
4
Part C - List each pollutant shown in Tables 2F-2, 2F•3, and 2F-4 that you know of have reason to believe is present. See the instructions for
additional details and requirements. Complete one table for each outfalf.
Pollutant
and
CAS Number
(if available)
Maximum Values
(include units)
Average Values Number
(include units) of
Grab Sample Storm
Taken During Flow -weighted Events
First 3f]
Minutes Composite Sampled
Sources of Pollutants
Grab Sample
Taken During
Fiat 30
Minutes
Flow -weighted
Composite
Unknown
Ma
Unknown
Zinc
Unknown
Ti
Unknown
Barium
Part D - Provide data for the storm eventfsl which resulted in the maximum values for tha flow weighted comnosita samoie_ 1
1.
Date of
Storm
Event
2
Duration
of Storm
in minutes
3.
Total rainfall
during storm event
rn inches)
4.
Number of hours between
beginning of storm meas-
ured and end of previous
measurable rain event
5.
Maximum floe rate
during rain event
(gallons/minute or
spectly units
S.
Total flow from
rain event
(gallons or
ZeLcA units)
7.
Season
sample was
taken
.8.
Form of
Precipitation
(rainfall,
snowmelt)
I0/3/
8 270
0.5
>72 hrs.
90 gpm
534
Fall
rain
1 9. Provide a description of the method of flow measurement or estimate.
Total flow estimated based on.approximate drainage area and impervious surface in
drainage area. Flow rate was estimated visually by the individual taking the sample.
Calculation for total flow are attached.
EPA Form 3510-217 (11-90) Page VII.2
2F-5

EPA 10 Number (copy from r;em 1 01 Form r1 } rarm Approved. OM9 No. 2040..pagg
Outfall 002 I _ AVPmwa►expires 5,3t-92
n
Part A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See
instruction_ s for additional details.
Maximum Values Average Values Number
Pollutant I (include units) (include units) I at
and Grab Sample Grab Sample Storm
CAS Number Taken During Flow -weighted Taken During Flow -weighted Events
First 30 First 30 -
til available) Minutes Composite Minutes Composite Sampled Sources of Pollutants
I 1 1 i
and Grease I 2.6 mrr / 1
I I T.nadinc einrk
Biological Oxygen
I
Demand (8O05)
5 mg/1
1
Chemical Oxygen
Demand (COD)
17.6 mg/11
l
I
Total Suspended
Solids (TSSI
84 Mg/1
I
1
Total Wleldahl
1.0 mg/l
1
Nitrogen
Nitrate plus
Nitrite Nitro en
0.17 mg/ l
1
Total
Phosoharus
0.09 mg/1
1
pH !Minimum - Maximum !Minimum Maximum
Part B - List each pollutant that is limited in an effluent guideline wnicn the tacaity ,s sueleci to or any pollutant listed in the tacifity, s NPDES
permit for its process wastewater (it the lacrlity is operating under an exLsting NPOES permrt) Complete one table for each outtall.
r
Pollutant
and
CAS Number
(if available)
I Maximum Values
(include units)
Average Values Number
(include units) of
Grab Sample Storm
Taken fluting Flow -weighted Events
First 30
Minutes Composite Sampled
Sources of Pollutants
Grab Samosa
Taken Dunng
First 30
i Minutes
Flow -weighted
Composite
NH -- N
I
Dissolve. Og NAI
1
I
TemR N
Chronic Toxi
NA
I
Resid. C19
NA
I --
I
'
Conductivit
NA
I
Settleable
I
I
Solids
NA
Dioxin
NA
Above ar
I
I
I
f
I
I
I
I
I I
I
EPA Form 3510-2F (11-90) Page VII-t Continue on Reverse
71 _n

ConAnued from the Front
Part C - List each pollutant shown in Tables 2F-2, 2>=-3, and 2F4 that you know or have reason to believe is present. See the instructions for
additional details and requirements. Complete one table for each outfall,
Maximum values Average Values Number
Pollutant Cnclude units) (include units) of
and Grab Sample Grab Sample Storm
LCASber Taken Ounng Flow -weighted Taken Ouring Flow -weighted Events
First 30 First 30
ble) Minutes Composite Minutes Composite Sampled Sources of Pollutants
Tin
PartD - Provide data for the storm event(s) which resulted in the maximum values for the flow weighted composite sample.
1.
Oate of
Storm
Event
2.
Duration
of Storm
in minutes
3.
Total rainfall
during storm event
in inches)
4,
Number of hours between
beginning of storm meas-
ured and end of previous
measurable rain event
5.
Maximum floe rate
during rain event
(gallons/minute or
s units
B.
Total flow from
rain event
(gallons or
s units)
7,
Season
sample was
taken
8.
Form of
Precipitation
(rainfall,
snowmelt)
10/3/
8 270
0.5
-S- 72 hrs.
40 gpip
181.gallon3
Fall
rain
1 9. Provide a description of the method of flow measurement or estimate. I
Total flow estimated based on approximate drainage area and impervious surface in
drainage area. Flow rate was estimated visually by the individual taking the sample.
Calculations for total flow are attached.
EPA Form 3510-2F (11-90) Page Vli-2
2F-5

- EPA 10 Number (co0y tram rem r or Form r) I corm Approved. ONIS No. 2040-OC86
Outfall 004 l Appmval expires 5_31.92
Vil. Discharge Information fCorxinued from oa e 3 of Form 2F
Part A - You must provide the results of at least one analysis for every pollutant ,n trns iabte. Complete one table tar eacn outtall. See
instructiorts for additional details.
Pollutant
and
CAS Number
fif availaole)
Maximum Values
(include units)
Average Values Number
(include units) I of
Grab Sample Storm
Taken Curing
Taken
30 ' Flow -weighted Events
Minutes Composite Sampled
Sources of Pollutants
Grab Sample
Taken During
First 30
Minutes
Raw-weighted
Composite
Oil and Grease
'
5.8 m l
I
I
11 I Asphalt road
Biological Oxygen
Demand (SCOS)
4.0 Mg/1
1
Chemical Oxygen
Demand (COD)
I 15 mg/1
1
Total Suspended
Solids (TSS)
9.0 mg/1
I
I 1
Total Kieldahl
Nitrogen
L 1.0 mg/1
1
Nitrate plus
Nitrite Nitro en
0.79 mg/1 '
1
Total
Phasohorus
0.05 mg/1
\
1
PH Minimum '1aximum Minimum Maximum
Part H - List eacn pollutant that is limited ,n an ettluent guiaeime wnicn ine facility is sucleC: to or any pollutant IiSted ,n the tacitrty s NPDES
permit lot its process wastewater lit the facility is operating under an existing NPOES permit) Complete One table for each outfall.
See jr!iiinvirticligns for ngoitional details gag (e!�Wjrrnrfertt,3
Pollutant
and
CAS Number
fit availaole)
Maximum Values I Average Values i Number
(include units) (include units) at
Grab Sample Grab Sample Storm
Taken During Flow -weighted Taken During Flow -weighted Events
First 30 First 30
, Minutes Composite Minutes Composite Sampled
Sources of Pollutants
NH3-- NI
Dissolved
Temp
i
Chronic Tox ) NA
Resid. C1 NA
ConductiviviA
NA
I
Settleable
I I
Solids
NA
I
Dioxin
NA
Above param
tars are required
to be ieDorted
by the NP ES permit for
the facility WWTP-
I
i
!
i
I
I
I
I
i
I �
I
EPA Form 9510-2F (11-90) Page Vitt Continue on Reverse

— Con -hued Irom the Front
Part C . List each pollutant shown in Tables 2F-2, 2F•3, and 2F-4 that you know or have reason to believe is present. See the instructions for
additional details and requirements. Complete one table for each outfap.
Maximum Values Average Values Number
pollutant (include unifs) (include units) of
and Grab Sample Grab Sample Storm
CAS Number Taken Ouring plow -weighted Taken During Flow -weighted Events
'IAA 11 iM j niLm- n 1 r
First 30 Frst 30
(if available) Minutes Composite Minutes Composite Sampled Sources of Pollutants
I
1
1
1
.00035, m I 1
Part D - Provide data for the storm eventfsl which resulted in the maximum values for the flow weighted comoosite sample.
1.
Date of
Storm
Event_(In
2.
Ouration
of Storm
minutes
9.
Total rainfall
during storm event
in inches)
4.
Number of hours between
beginning of storm meas-
ured and and of previous
measurable rain event
5.
Maximum floe rate
during rain event
(gallons/minute or
s units
B.
Total flow from
rain event
(gallons or
s units)
7.
Season
sample was
taken
8.
Form of
Precipitation
(rainfall,
snowmelt)
10/3/
8 270
0.5
\ 72 hrs.
70 gpm
757 gal.
Fall
rain
1 9. Provide a description of the method of flow measurement or estimate.
Total flow estimated based on approximate drainage area and impervious surface in
drainage area. Flow rate was estimated visually by the individual taking the sample.
Calculations for total flow are attached.
EPA Form 3510-2F (il-90) P3geVII.2
2F-5

~ EPA l tvumoef (copy ero,n item 1 or corm rl rorm Approved. OMB No 2040-0086
Outfall 005 Approval expires 5-31-92
VIi. Discharge Information (C;ontinued from cage 3 of Form 2F
Part A - You must provide the results of at least one analysis for every pollutant in tms table. Complete one table for each outtall. See
instructions for additional details.
Maximum Values Average Values Number
Pollutant !include units) (include units) of
and Grab Sample Grab Sample Storm
Taken Outing Taken During
CAS Number First 30 Flow -weighted First 30 . Flow -weighted Events
(itavailaole) Minutes Composite Minutes Composite Sampled Sources of Pollutants
Oil and Grease 1
Biological Oxygen
Demand (BOOS)
9.1 MR/1
1
Chemical Oxygen
Oemand fCOO)
<10.0 Mg/1
o
I 1
Total Suspended
Solids (TSS)
4.0 m /l
I
1
Total Kieldahl
Nitrogen
1.2 mg/1
1
Nitrate plus
"
I
1
Nitrite Nitro en
0.14 mg/1
Total
1
Phosphorus
< .02 mg/1
PH Minimum" 'Maximum !Minimum Maximum
Part 8 - List eacn pollutant tnat is limited in an ettluent guideline wntc17 the lacslity is suelect ro or any pollutant listed in Me lacilhty s NPOES
permit for sts process wastewater (it the facility is operating under an existing NPOES permit! Complete one table for each outfall.
See ime instrLjrtFons 1
Pollutant
and
CAS Number
(if available)
Maximum Values Average Values Number
(include units) (include units) I of
Grab Sample Grab $ample Storm
Taken Outing Flow•weighted Taken Ourng Flow -weighted Events
First 30 First 30
Minutes Composite Minutes Composite Sampled Sources of Pollutants
_
I
I �
Chronic Tox.!
- NA
I
Resid. C12 i NA
I
Ccnductivit
NA
I
Settleable
Solids
NA
! I
Dioxin
I
Above Dara
eters are re
red to"
I
I
'
I
I
I
I
I
I
"
I
I
�
EPA Form 3510-21' (11-90) Page Vlt•t Continue on Reverse
,)F_Q

' — Co.-Anued from the Front
Part C - List each pollutant shown in Tables 2F•2, 2F.3, and 2F-4 that you know or have reason to believe is present. See the instructions Ier
additional details and requirements. Complete one table for each outfall.
Maximum Values Average Values Number
Pollutant {include units) (include units) of
and Grab Semple Grab Sample Storm
Taken Dunng d Taken During
[Flo-;lightedCAS Number First 30 Flow-weighteFirst Events
(ifavailacle) Minutes Composite Minutes Coosite Sampled Sources of Pollutants
1 Part D - Provida data for the storm Aventfsl which resulted in the marimum values for the flow wainhted nmmnesita samnla_ 1
1.
Date of
Storm
Event
2.
Duration
of Storm
in minutes
3.
Total rainfall
during storm event
in inches)
4.
Number of hours between
beginning of storm mess-
ured and end of previous
measurable rain avant
5.
Maximum floe rate
during rain event
(gallons/minute or
specify units
6.
Total flow from
rain event
(gallons or
Y units
specff
7.
Season
sample was'
taken
8.
Form of
Precipitation
(rainfall,
snowmelt)
10/3/
8 270
0.5
> 72 hrs.
100 gpm.
271 gal,
Fall
rain
9. Provide a descriotion of the method of flow measurement or estimate.
Total flow estimated based on approximate drainage area and impervious surface in
drainage.area. Flow rate was estimated visually by the individual taking the sample.
Calculations for total flow are attached.
EPA Form 3510-2F (11-90) Page VII2
2F-5

EPA 10 Number (copy lrom item r of i"orrn +) norm Approved. 0MB No. 2040-0086
Outfall 006 Approval expires 5,31-92
11,0ischarge information I'Conrinu_ed from page 3 of Form 2F) ^
Part A - You must provide the results of at least one analysis for every pollutant in this tatle. Complete one table for each ourtalt_ See
instructions for additional details.
Maximum Values Average Values Number
Pollutant I (include units) (include units) of
and Grab Sample Grab Sample Storm
CAS Number Taken During
Flow-weighted Taken During Pow -weighted Events
First 30 First 30
(if available) Minutes Composite Minutes I Composite Sampled Sources of Pollutants
Oil and Grease
1.3 mg/1
I
1 i
I
Biological Oxygen
6.8 mg/1
1
Demand (80051
Chemical Oxygen
'�10.0 mg/1
Demand (COON
❑
Total Suspended
50 mg/1
I
1
}
kl
Solids (TSS)
Total tCeidahl
1.1 mg/ l
1
Nitro en
Nitrate plus
0.73 mg/
1 l
Nitrite Nitrogen
I
Total
`I
0.09 Mg/1�
1
Phosphorus
rr
PH Minimum • :Maximum . Minimum Maximum
Part 9 - List each pollutant inat is limited ,n an effluent guideline which the tacii,ry is suolect to or any pollutant listed ,n the tacitity s NPOES
permit far its process wastewater (if the facility is operating under an existing NPOES permit} Complete one table for each outtall.
for ,and recuorcments,
Maximum Values I Average Values Number
Pollutant (include units) (include units) of
and Grab Sample Grab Sample Storm
CAS Number Taken During Flow -weighted Taken During Flow -weighted Events
First 30 First 30
(if ","la,
, Minutes Composite Minutes Composite Sampled Sources of Pollutants
i
i
Residualf
Cdndiint­lyi_L4 NA
I ,
Sol qri-q NA
i
I I
EPA Form 3510-2F (11-90) Page VII.1 Continue on Aeverse
9F_tl

"Cor.-.inued from the Front
Part C • Ust each pollutant shown in Tables 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for
additional details and requirements. Complete one table for each outfail.
Maximum Values Average.Values Number
Pollutant (include units) (include units) of
and Grab Sample Grab Sample Storm
CAS Number Taken During Flow -weighted Taken During Flow -weighted Events
First 30 First 30
(if available) Minutes Composite Minutes Composite Sampled Sources of Pollutants
Bar
Con
Titanium 0.078 m
Tin 0.71 mg/1
Zinc 0.34 MR/1
Endosulfur 0.061 m
Bis (2 eth lhexvl) nht alate
Part n - Penvirfa data for tha ctnrm nventrsl which resulted in the maximum value, far the flaw waiahted r_nmonsita samole 1
1.
Date of
Storm
Event
2.
duration
of Storm
in minutes
3.
Total rainfall
during storm event
in inches)
4.
Number of hours between
beginning of storm meas-
ured and end of previous
measurable rain event
5.
Maximum floe rate
during rain event
(gallons/minute or
,s units
6.
Totat flow from
rain event
(gallons or
s units)
7.
Season
sample was
taken
8.
Form of
Precipitation
(rainfall,
snowmelt)
270
0.5
> 72 hrs.
30 gpm
297 gal.
Fall
rain
1 9• Provide a description of the method of flow measurement or estimate.
Total flow estimated based on approximate drainage area and impervious surface in
drainage area. Flow rate was estimated visually by the individual taking the sample.
Calculations for total flow are attached.
EPA Form 3510-2F (11-90) Page Vu•2
2F-5

~
EPA IO Number (Copy tram item r of Form r)
rorm Approveo. OM8 No. 2040.Coas
Ou t; f al l 007
ApprovW expires 5-31-92
a Information (Continued from oa
e 3 of Form 2F
You must provide the results of at least one analysis far every pollutant in this table.
Complete one table for each cutfall. See
rVIIDischar
instructions for additional details.
Maximum Values
Average Values
Number
nt
(include units)
(include units)
of
and
Grab Sample
Grab Sample
Storm
CAS Number
Taken Curing
First 30
Flow -weighted
Taken Outing
First 30 '
Flow -weighted
Events
(if availale)
Minutes
Composite
Minutes
Composite
Sampled
Sources of Pollutants
Oil and Grease
1 9 Mg/1
I
1
Biological Oxygen
Oemand f80051
5.7 mg/1
1
Chemical Oxygen
1
Cemand fC001
C 10.0 mg/1
I j
Total Suspended
I
1
Solids (TSS)
62.5 mg/l
Total K-jeldaht
1
C 1 .0 mg / 1
Nitro en
Nitrate plus
0.36 mg/1
I
Nitrite Nitrogen
total
c0.02 mg/1
N
1
Phosaharus
pH
!Minimum• !Max.mum
!Minimum Maximum
Part B - first eacn pollutant inat is limited in an effluent guideline whicn the facility 15 suolect to or any peifutam listed in the facility s NPOES
permit
for ds process wastewater (if me.ta6ity is operating under an existing NPOES
permn) Complete one table for eacn outfalt.
h
i f
Maximum Values j
Average Values
Number
Pollutant
(include units) II
(include units)
of
and
Grab Sample
Grab Sample
Storm
CAS Number
Taken Cunn9
First 30
Flow -weighted
Taken During Flow -weighted
First 30
Events
(if available)
_
I
I
Minutes
Composite
Minutes Composite
Sampled
Sources of Pollutants
NA I
.
I
r i
NA
2glids
Above garaM
NA
I 1
I
I
I
Cow e,...., ac,n_'Y= r„-env
Paqe Vtl-1
Continue an Reverse
12C_a

— Co,-Anued from the Front
Part C - List each pollutant shown in Tables 2F-2, 2F-3, and 2F-4 that you know or have reason to believe is present. See the instructions for
I additional details and requirements. Complete one table for each outtall.
4
4
Pollutant
and
CAS Number
(if available)
Maximum Values
include units)
Average Values
(include units)
Number
of
Storm
Events
Sampled Sources of Pollutants
Grab Sample
Taken Dunng
First 30
Minutes
Flow -weighted
Composite
Grab Sample
Taken During flaw -weighted
First 30
Minutes Composite
Sulfate
3.5 1
1
Aluminum
2.52 m 1
1
Barium
0.038 mgj 1
1
Chromium
0.-006 m 1
1
Co er
0.022 mg/1
1
Magnesium
1.53 m 1
1 I
Titanium
0.26 mg/1
1
Tin
1.26 m /l
.
1
Zinc
2.41 m /1
1
I Part n . P—;,4A Hit. rAr 1ha t1Arm AVPAtItt whir_h mmidtAd In thA mnvimllm val..a4 tnr thA f1nw wainhtAd a mmnntifw eamntA I
1.
Date of
Storm
Event
1 2.
Duration
of Storm
in minutes
3.
Total rainfall
during storm event
On inches)
4.
Number of hours between
beginning of storm meas-
Ad and and of previous
measurable rain event
5.
Maximum floe rate
during rain event
(gallons/mfnute or
specify units
8.
Total flow from
rain event
(gallons or
s units)
7.
Season
sample was
taken
- 8.
Form of
Precipitation
(rainfall,
snowmelt)
10/3/
8 270
0.5
-\72 hrs.
130 gpm
.371 gal.
Fall
rain
1 S. Provide a description of the method of flow measurement or estimate. )
Total flow estimated based on approximate drainage area and impervious surface in
drainage area. Flow rate was estimated visually by the individual taking the sample.
Calculations for total flow are attached.
EPA Form 3510-2F (11-90) Page V11.2
2F--5

EPA ID Number (COPY from rrem 1 of roan rl -crm Approved. CM8 No, 2044-0086
Outfall 008 Approval expires 5-31.92
VII. Oischartae information (Continued from nacre 3 of Form 2F)
Part A - You must provide the results of at least one analysis for every pollutant in tnis table. Complete one table for earn autiall. See
instructions for additional details.
i I Maximum Values Average Values Numbef
Pollutant I(include units) (include units) of
and Grab Sarnot Grab Sample Storm
CAS Number Taken Ourin Flog., -weighted Taken Outing Flow -,,weighted Events
First 30 First 30 '
fit availacle) Minutes Composite Minutes Composite Sampled Sources al Pollutants
I
Oil and Grease 2.1 mg f ,1 I I ]
Biological oxygen
7.2 mg/l
I
I
I 1
Demand (8005)
Chemical Oxygen
4 10.0 Mel
1
Demand (CCD)
Total Suspended
78 mg/l
I
1
Solids (TSSI
Total Kefdahl
I
1
Nitro en
8.2 mg/1
Nitrate plus
1.0 mg/1Total
Nitrite Nitro en
{
0.03 mg/1
1
Phosphorus
pH Min]mum %laximum Minimum Maximum
Part 8 - List each pollutant trial is limited in an effluent guicleline wnicn the taclhty is suclect to or any pollutant listed to the tacdity s NPpES
permit for its process wastewater (it the facility is operating under an existing NPDES permit) Complete one table lot each outtall,
the inst uctigns f
Pollutant
and
CAS Number
(ifavailaale)
tH3issolved
Maximum Values
(include units)
Average Values
(include units)
Number
of
Slorm
Events
Sampled
Sources of Pollutants
Grab Sample
Taken During Flow -weighted
First 30
, Minutes Composite
Grab Sample
Taken During
First 30
Minutes
i
Flow -weighted
Composite 1
— N NA
OxL NA I
I
Chronic Tox.l NA
I
Residual C1 i NA
IBleachinp, process
C-onductivit NA I
I
I
Settleable
Solids
NA
I I
Toxin
NA
I
B -- roduct
Ahnup pprnmL�-
_tgj
hy
j-hp WPT)rq irip"it fir
fbp fninijilry WTP
I
I
I
I I
I
I
I I
I
-
I
I
I !
I
EPA Form 3510-2F (11-90) Page VII-1 Continue an Reverse
7F_fl

— Con-lnuad from the Front
j part C - List each pollutant shown in Tables 2F-2, 2F-3, and 2F-4 that you know or have reason to >zeiieve is present. See the instructions Icr
l additional details and requirements. Complete one table for each curtail.
Pollutant
and
CAS Number
(if available)
Maximum Values j
rinclude units) I
Grab Sempte
Taken Dunng Ftow-weighted
First 30
Minutes Composite
Average Values
(include units)
Grab Sample
Taken Curing Flow -weighted
First 30
Minutes Composite
Number
of
Storm
Events
Sampled
Sources of Pollutants
I
IT
1, 1 I I
I I
RArlitrn
n 7 IL Mer/1
I I
I I
ruppwr
I
I I
1
I I
I
II
n
I
I
I !
I
I I
#
I I
I I
I I
I I
I
I
1 Part r7 - Orn..irin rint�i Mr tho "nrm nuwnflel which rwuilterl in thw mavim.,m unllfwe Mr tho flnur woinhfnrf rmmnncitn "mnlo 1
1.
Date of
Storm
Event
2.
Duration
of Storm
rn minutes)
3.
Total rainfall
during storm event
ran inches)
4,
Number of hours between
beginning of storm meas-
ured and end of previous
measurable rain avant
• 5.
Maximum floe rate
during rain event
te
(gallons/minuor
specdy units
6.
Total Sow from
rain event
(gallons or
I mnU units)
7.
Season
sample was
taken
8.
Form of
Precipitation
(rainfall,
snowmelr)
10/3/
8 270
0.5.
>72 hrs.
130 gpm
202 gal.
Fall
rain
Provide a description of the method of flow measurement or estimate.
Total flow was estimated based on approximate drainage area and impervious surface in
the drainage area. Flow rate was estimated.visually by the individual taking the
sample. Calculations for total flow are attached.
EPA Form 3510-2F (11-40) Page V11•2
2F-5

m ri Test e ca
I N C 0 A P 0 A A T E �
RECEIVED
NOV 21998
ARCADIS Geraghty & Miller
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMWATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, NC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37589 SAMPLE ID- OUTFALL 01 SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1025
DATE RECEIVED- 09/30/98 SAMPLER- K. EMANUEL/F. MISHUE RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
• BIOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSW
7.6
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSW
< 10.0
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 160.2
09/30/98
KSW
9.5
MG/L
1.0
OIL A GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSW
3.5
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSW
58
COL/100
ML 1
LABORATORY DIRECTOR
SC
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX. [phone]

•
Testl�merica
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT HAKE: STORMWATER
P.O. BOX 1305 ' REPORT DATE: 10/22/98
LUMBERTON, HC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37590 SAMPLE ID- OUTFALL 02 SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1030
DATE RECEIVED- 09/30/98 SAMPLER- K. EMAHUEL/F. MISHUE RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
OBIOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSW
5.0
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSW
18.7
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 160.2
09/30/98
KSW
84.0
MG/L.
1.0
OIL & GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSW
2.6
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSW
> 3,600
COL/100 ML
1
LABORATORY DIRECTOR 4 )_LS7t7
NCDEETTR ryrr) #37
NCD ""7716
SC
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX: [phone]

TesU�merica
I N C 0 R P 0 a A T E 0
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMNATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, NC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37591 SAMPLE ID- OUTFALL 04 SAMPLE MATRIX- wM
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1035
DATE RECEIVED- 09/30/98 SAMPLER- K. EMANUEL/F. MISHUE RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
• BIOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSW
4.0
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSW
15.0
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 160.2
09/30/98
KSW
9.0
MG/L
1.0
OIL & GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSW
5.8
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSW
> 4,700
COL/100
ML 1
(i�LABORATORY DIRECTOR N )-b-d96=_
NCDENR DWQ #37
• NCB R DW-#37716
• SC DErIC #99037
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX. [phone]

TestAmerica
INC o R F OR ATE o
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMWATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, HC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37392 SAMPLE ID- OUTFALL 05 SAMPLE MATRIX WW
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1040
DATE RECEIVED- 09/30/98 SAMPLER- K. EMAHUEL/F, MISHUE RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
OBIOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSW
9.1
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSW
< 10.0
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 150.2
09/30/98
KSW
4.0
MG/L
1.0
OIL & GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSW
1.7
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSW
150
COL/100
ML i
LABORATORY DIRECTOR
NCDENR DWQ #37
t NCDrP:ll DW #377I6
SC DENC #99037
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX: [phone]

Testl�mericaP OR ATE 0
•
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMWATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, NC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37593 SAMPLE ID- OUTFALL 06 SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1045
DATE RECEIVED- 09/30/98 SAMPLER- K. EMANUEL/F. MISHU£ RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS DET.
ANALYSIS METHOD DATE BY RESULT UNITS LIMIT
• BIOCHEMICAL OXYGEN DEMAND EPA 405.1 10/01/98 KSW 6.9 MG/L 2.@
CHEMICAL OXYGEN DEMAND 410.4 10/09/98 KSW < 10.0 MG/L 10.0
TOTAL SUSPENDED SOLIDS EPA 160.2 09/30/98 KSW 50.0 MG/L 1.0
OIL A GREASE (GRAVIMETRIC) EPA 413.1 10/02/98 KSW 1.3 MG/L 1.0
FECAL COLIFORM-MEMBRANE FILTER 908C 09/30/98 KSW > 7,000 COL/100 ML 1
LABORATORY DIRECTOR- "
NCDEN7t DWQ #37
NCI)EI j" 7 #37716
` SC DEliC #99037
2003 N. PINE STREET / LUMBERTON. NC 28358 / 910-738-6190 / FAX: [phone]

TestAmerica
•
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMwATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, NC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37594 SAMPLE ID- OUTFALL 07 SAMPLE MATRIX- wK
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1050
DATE RECEIVED- 09/30/98 SAMPLER- K. EMANUEL/F. MISHU£ RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
&'IOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSw
5.7
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSw
< 10.0
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 160.2
09/30/98
KSw
62.5
MG/L
1.0
OIL i GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSw
1.9
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSw
560
COL/100
ML 1
LABORATORY DIRECTOR
NCDENR DW4 #37
�• NCDELTR D41 #37716
SC DEHC #99037
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX: [phone]

0
Test merioca
INC O R P OR ATE O
FINAL REPORT OF ANALYSES
BUCKEYE OF LUMBERTON PROJECT NAME: STORMWATER
P.O. BOX 1305 REPORT DATE: 10/22/98
LUMBERTON, NC 28359-
Attn: MR. ERIC BOLIN
SAMPLE NUMBER- 37595 SAMPLE ID- OUTFALL 08 SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98 TIME SAMPLED- 1055
DATE RECEIVED- 09/30/98 SAMPLER- K. EMANUEL/F. MISHUE RECEIVED BY- PSH
TIME RECEIVED- 1125 DELIVERED BY- CLIENT
Page 1 of 1
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
RESULT
UNITS
LIMIT
BIOCHEMICAL OXYGEN DEMAND
EPA 405.1
10/01/98
KSW
7.2
MG/L
2.0
CHEMICAL OXYGEN DEMAND
410.4
10/09/98
KSW
< 10.0
MG/L
10.0
TOTAL SUSPENDED SOLIDS
EPA 160.2
09/30/98
KSW
78.0
MG/L
1.0
OIL & GREASE (GRAVIMETRIC)
EPA 413.1
10/02/98
KSW
2.1
MG/L
1.0
FECAL COLIFORM-MEMBRANE FILTER
908C
09/30/98
KSW
360
COL/100 ML
1
LABORATORY DIRECTOR*
NCDENR DWQ #37
NCD , TR DW #37716
SC DET-3C #99037
2003 N. PINE STREET / LUMBERTON, NC 28358 / 910-738-6190 / FAX: [phone]

Chain of Ady Record HYDROWGIC, INC. -B L09 3018'
L7 Asheville, NC L7 Norcross, GA l3 Charluue. NC n Frankfurt KY i7 Morri,ville, NC
f828) 254-5161) � [phone] [phone] (5031 223-0251 t9l')t 1Mt1-ii69ti
L Lumtknon, NC Q Lexington, SC L! Brighton, CO I� Alacun. GA 1 Or)antlu, H.
[phone] [phone] [phone] 19121 737-081 1 (4W) s51-256( I
Client: m
Project No.:
REQUESTED
U Q
Dp
`�
"` III
PARAMETERS
LAI ('ODE 1.1);
a = a,he%i)le. NC
= Ch:trhxte, NC
f� D = Dom er, CO
F_ = 1-0\i1wiml. SC.
G = Aran k fort.
K = Frankfort. K1'
d'} L = Lumberlon. NC
\ A1= hlun'I,+i11e.N('
N = Norcrosss. 0A
FL
/V `{,) S = Subcontracted
ct
� S = 5uhcuntractctl
OV
Report Address: O, ( G
ll 30
InvoiceAddress: s(�
Ll "JC 2y3
[iii4+>
Attn: B� '�
AIM: ` o t
Phone No.: �-7 %— 3 2 Z (
J
Sampled By: e� /_, _ _
vet.+
Fax No.: �_ 3 Z
P.O. No:
SIacS:myrL�Culkcicd
TURNAROUNWriNi :
L1 24 hours' LI 48 Hours
0 5 Days 0 10 nays Date Needed:
Sample 11)
Dute
'line
Comp/
Grab
Matrix
Contain
E - i'reserv. REMARKS
Q D I
3o
O:z
�
•�.�
► ( ©
✓ ✓ ✓
Ir D
(�1s
0'�1 o
✓ r� t�
( o
�t Lab Use pn�3y,;`�rs*uy i ru ` )� f Citstudy Seal F L.1Yes L: rNn rr�IV►�1;
Ll
(tee. Lab temp
]nil Lab Temp.
COMMENTS:
Relinquished By-
Dale Tillie
Received By.
Date 1` le
Lab Use Only:
Relinquished *
'C]
I� ie
/
Received -By:
Date Time
Relinquished By:
Date Time
Received By:
Dale Time
Relinquislicd 11y: Date Time Received By: ]late Tiutc
1 t

TesU�merica
FINAL REPORT OF ANALYSES
HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attn: PAM HESTER
SAMPLE NUMBER- 128461 SAMPLE ID- OUTFA_LL 01
DATE SAMPLED- 09/30/98
DATE RECEIVED- 10/01/98 SAMPLER- KG/FM
TIME RECEIVED- 0920 DELIVERED BY- COURIER
Page 1 of 2
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE MATRIX- WW
TIME SAMPLED- 1025
RECEIVED BY- DHT
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
TOTAL
EPA 335.2
10/06/98-APT
<0.005
mg/l
0.005
*YANIDE,
UORIDE
EPA 340.2
10/08/98
DEP
<0.1
mg/l
0.10
AS
EPA 425.1
10/01/98
APT
0.17
mg/l
0.10
TOTAL KJELDAHL NITROGEN
EPA 351.3
10/14/98
APT
<1.0
mg/l
1.0
NITRATE/NITRITE
CALC
10/02/98
APT
0.31
mg/l
0.11
TOTAL PHOSPHORUS
EPA 365.2
10/16/98
APT
<0.02
mg/l
0.02
SULFATE
EPA 375.4
10/13/98
KHJ
41.0
mg/l
1.0
SULFIDE
EPA 376.1
10/07/98
APT
<1.0
mg/l
- 1.0
SULFITE
377.1
10/01/98
APT.
<2.0*
mg/l
2.0
PHENOL, TOTAL
420.1
10/05/98
APT
<5.0
ug/l
5.0
ARSENIC, TOTAL
206.2
10/03/98
LJP
10/12/98
LJP
<
0.003
mg/l
0.003
MERCURY, TOTAL
245.1
10/06/98
LJP
<
0.0002
mg/l
0.0002
SELENIUM, TOTAL
270.2
10/03/98
LJP
10/13/98
LJP
<
0.003
mg/l
0.003
THALLIUM, TOTAL
279.2
10/03/98
LJP
10/16/98
LJP
<
0.001
mg/l
0.001
ANTIMONY, TOTAL
204.2
10/03/98
LJP-10/16/98
LJP
<
0.003
mg/l
0.003
SILVER,TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
TOTAL, ALUMINUM
200.7
10/03/98
LJP
10/08/98
LJP
0.350
mg/l
0.025
BARIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.007
mg/l
0.005
BORON, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.100
mg/l
0.100
BERYLLIUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0,001
CADMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.001
mg/l
0.001
l•
NC DEHNR DEM #47
NC D)EHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

Testl.
merlca
I N C 0 R P 0 R A T E 0
•
Page 2 of 2
CONTINUATION OF DATA
FOR SAMPLE NUMBER
128461
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.005
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.220
mg/l
0.010
LEAD, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
MAGNESIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.170
mg/l
0.025
NICKEL, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
< 0.010
mg/l
0.010.
TIN, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.069
mg/l
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.210
mg/l
0.010
0
SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST. /
4
LABORATORY DIRECTOR
V '
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 2880 t / 828-254-5169 / FAX: [phone]

C,
HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attn: PAM HESTER
TestA.merica
i N C 0 Fl P 0 Fl A T 6 0
FINAL REPORT OF ANALYSES
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE NUMBER- 128462
SAMPLE ID- OUTFALL 02
SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98
TIME SAMPLED- 1030
DATE RECEIVED- 10/01/98
SAMPLER- KG/FM
RECEIVED BY-
DHT
TIME RECEIVED- 0920
DELIVERED BY- COURIER
Page 1 of 2
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
AIKYANIDE, TOTAL
EPA 335.2
10/06/98
APT
<0.005
mg/l
0.005
WB_UORIDE
EPA 340.2
10/08/98
DEP
<0.1
mg/1
0.10
MAS
EPA 425.1
10/01/98
APT
<0.10
mg/l
0.10
TOTAL KJELDAHL NITROGEN
EPA 351.3
10/14/98
APT
<1.0
mg/1
1.0
NITRATE/NITRITE
CALC
10/02/98
APT
0.17
mg/l
0.11
TOTAL PHOSPHORUS
EPA 365.2
10/16/98
APT
0.09
mg/l
0.02
SULFATE
EPA 375.4
10/13/98
KHJ
<1.0
mg/l
1.0
SULFIDE
EPA 376.1
10/07/98
APT
cl.0
mg/1-
1.0
SULFITE
377.1
10/01/98
APT
<2.0*
mg/l
2.0
PHENOL, TOTAL
420.1
10/05/98
APT
<5.0
ug/l
5.0
ARSENIC, TOTAL
206.2.
10/03/98
LJP
10/12/98
LJP
< 0.003
mg/l
0.003
MERCURY, TOTAL
245.1
10/06/98
LJP'<
0.0002
mg/l
0.0002
SELENIUM, TOTAL
270.2
10/03/98
LJP
10/13/98
LJP
c 0.003
mg/l
0.003
THALLIUM, TOTAL
279.2
10/03/98
LJP
10/16/98
LJP
< 0.001
mg/l
0.001
ANTIMONY, TOTAL
204.2
10/03/98
LJP-10/16/98
LJP
< 0.003
mg/l
0.003
SILVER,TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.001
mg/l
0-.001
TOTAL, ALUMINUM
200.7
10/03/98
LJP
10/08/98
LJP
1.580
mg/l
0.025
BARIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.030
mg/l
0.005
BORON, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.100
mg/l
0.100
BERYLLIUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.001
mg/l
0.001
CADMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.001
mg/l
0.001
0
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET/ ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

TestAmerica
i N 0 0 R P 0 R A T E 0
•
Page 2 of 2
CONTINUATION OF DATA
FOR SAMPLE NUMBER
128462
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/96
LJP
10/14/98
LJP
0.009
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
1.620
mg/l
0.010
LEAD, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.018
mg/l
0.010
MAGNESIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.440
mg/l
0.025
NICKEL, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
0.095
mg/1
0.010
TIN, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.480
mg/l.
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.540
mg/l
0.010
•
SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST. 41
LABORATORY DIRECTOR
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

6
TestAmerica
FINAL REPORT OF ANALYSES
HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attn: PAM HESTER
SAMPLE NUMBER- 128463 SAMPLE ID- OUTFALL 04
DATE SAMPLED- 09/30/98
DATE RECEIVED- 10/01/98 SAMPLER- KG/FM
TIME RECEIVED- 0920 DELIVERED BY- COURIER
Page 1 of 2
ANALYSIS
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE MATRIX- WW
TIME SAMPLED- 1035
RECEIVED BY- DHT
SAMPLE PREP ANALYSIS , DET.
METHOD DATE BY DATE BY RESULT UNITS LIMIT
TOTAL
EPA 335.2
10/14/98
APT
<0.005
mg/1
0.005
qYANIDE,
,UORIDE
EPA 340.2
10/08/98
DEP
<0.1
mg/1
0.10
MBAS
EPA 425.1
10/01/98
APT
<0.10
mg/l
0.10
TOTAL KJELDAHL NITROGEN
EPA 351.3
10/14/98
APT
<1.0
mg/1
1.0
NITRATE/NITRITE
CALC
10/02/98
APT
0:79
mg/l
0.11
TOTAL PHOSPHORUS
EPA 365.2
10/16/98
APT
0.05
mg/l
0.02
SULFATE
EPA 375.4
10/13/98
KHJ
1.90
mg/1
1.0
SULFIDE
EPA 376.1
10/07/98
APT
<1.or-mg/
1
1.0
SULFITE
377.1
10/01/98
APT
<2.0*
mg/l
2.0
PHENOL, TOTAL
420.1
10/05/98
APT
<5.0
ug/l
5.0
ARSENIC, TOTAL
206.2
10/03/98
LJP
10/12/98
LJP
<
0.003
mg/l
0.003
MERCURY, TOTAL
245.1
10/06/98
LJP
<
0.0002
mg/l
0.0002
SELENIUM, TOTAL
270.2
10/03/98
LJP
10/13/98
LJP
<
0.003
mg/l
0.003
THALLIUM, TOTAL
279.2
10/03/98
LJP
10/16/98
LJP
<
0.001
mg/l
0.001
ANTIMONY, TOTAL
204.2
10/03/98
LJP-10/16/98
LJP
<
0.003
mg/l
0.003
SILVER,TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
TOTAL, ALUMINUM
200.7
10/03/98
LJP
10/08/98
LJP
0.160
mg/l
0.025
BARIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.007
mg/l
0.005
BORON, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.100
mg/l
•0.100
BERYLLIUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
CADMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.001
mg/l
0.001
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-234-5169 / FAX: [phone]

TestAmerica
I N C 0 A P 0 R A T E 0
Page 2 of 2
CONTINUATION OF DATA FOR SAMPLE NUMBER 128463
ANALYSIS
CHROMIUM, TOTAL
COBALT, TOTAL
COPPER, TOTAL
IRON, TOTAL
LEAD, TOTAL
MAGNESIUM, TOTAL
NICKEL, TOTAL
MOLYBDENUM, TOTAL
TITANIUM, TOTAL
TIN, TOTAL
ZINC, TOTAL
(0
SAMPLE PREP
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
r
mg/1
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
200.7
10/03/98
LJP
10/08/98
LJP
0.240
mg/l
200.7
10/03/98
LJP
10/08/98
LJP
<
0.010
mg/l
200.7
10/03/98
LJP
10/14/98
LJP
0.230
mg/l
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
200.7
10/03/98
LJP
10/08/98
LJP
<
0.010
mg/l
200.7
10/03/98
LJP
10/19/98
LJP
<
0.010
mg/l
200.7
10/03/98
LJP
10/08198
LJP
0.097
mg/l
200.7
10/03/98
LJP
10/08/98
LJP
0.470
mg/l
SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST.
i
LABORATORY DIRECTOR z1alfl P/�"
NC DEENR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE. NC 28801 / 828-254-5169 / FAX. [phone]
DET.
LIMIT
0.005
0.005
0.005
0.010
0.010
0.025
0.005
0.010
0.010
0.050
0.010

HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28356-
Attn: PAM HESTER
Testjlmerica
FINAL REPORT OF ANALYSES
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE NUMBER- 128464 SAMPLE ID- OUTFALL 05
DATE SAMPLED- 09/30/98
DATE RECEIVED- 10/01/98 SAMPLER- KG/FM \
TIME RECEIVED- 0920 DELIVERED BY- COURIER
Page 1 at 2
SAMPLE PREP ANALYSIS
ANALYSIS METHOD DATE BY DATE BY
ANIDE, TOTAL
UORIDE
`•- r®AS
TOTAL KJELDAHL NITROGEN
NITRATE/NITRITE
TOTAL PHOSPHORUS
SULFATE
SULFIDE
SULFITE
PHENOL, TOTAL
ARSENIC, TOTAL
MERCURY, TOTAL
SELENIUM, TOTAL
THALLIUM, TOTAL
ANTIMONY, TOTAL
SILVER,TOTAL
TOTAL, ALUMINUM
BARIUM, TOTAL
BORON, TOTAL
BERYLLIUM, TOTAL
CADMIUM, TOTAL
SAMPLE MATRIX- WW
TIME SAMPLED- 1040
RECEIVED BY- DHT
RESULT UNITS
EPA 335.2
10/14/98
APT
<0.005
mg/l
EPA 340.2
10/08/98
DEP
<0.1
mg/l
EPA 425.1
10/01/98
APT
<0.10
mg/1
EPA 351.3
10/14/98
APT
1.2
mg/l
CALL
10/02/98
APT
0.14
mg/l
EPA 365.2
10/16/98
APT
<0.02
mg/l
EPA 375.4
10/13/98
KHJ
<1.0
mg/l
EPA 376.1
10/07/39-8
APT
<1.0
mg/l
377.1
10/01/98
APT
<2.0*
mg/l
420.1
10/05/98
APT
<5.0
ug/l
206.2
10/03/98
LJP 10/12/98
LJP
<
0.003
mg/l
245.1
10/06/98
LJP
<
0.0002
mg/l
270.2
10/03/98
LJP 10/13/98
LJP
<
0.003
mg/l
279.2
10/03/98
LJP 10/16/98
LJP
<
0.001
mg/l
204.2
10/03/98
LJP•10/16/98
LJP
<
0.003
mg/l
200.7
10/03/98
LJP 10/08/98
LJP
<
0.001
mg/l
200.7
10/03/98
LJP 10/08/98
LJP
0.083
mg/l
200.7
10/03/98
LJP 10/14/98
LJP
<
0.005
mg/l
200.7
10/03/98
LJP 10/14/98
LJP
<
0.100
mg/l
200.7
10/03/98
LJP 10/08/98
LJP
<
0.001
mg/l
200.7
10/03/96
LJP 10/14/58
LJP
<
0.001
mg/l
NC DEHNR DEM #47
NC DEHIVR DW #37717
SC DEHC #99015
DET.
LIMIT
0.005
0.10
0.10
1.0
0.11
0.02
1.0
1.0
2.0
5.0
0.003
0.0002
0.003
0.001
0.003
0.001
0.025
0.005
0.100
0.001
0.001
122 LYMAIY STREET / ASHEVILLE. NC 28801 / 828-254-5169 / FAX: [phone]

TestAmerica
NCO APO RATEO
Page 2 of 2
CONTINUATION OF DATA
FOR SAMPLE NUMBER
128464
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98.LJP
10/14/98
LJP
<
0.005
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.100
mg/l
0.010
LEAD, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.010
mg/l
0.010
MAGNESIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.082
mg/l
0.025
NICKEL, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
<
0.010
mg/l
0.010
TIN, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.050
mg/l
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.360
mg/l
0.01.0
*SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST.
i
LABORATORY DIRECTOR -r
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE. NC 28801 / 828-254-5169 / FAX: [phone]

HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attn: PAM HESTER
Testlimerica
FINAL REPORT OF ANALYSES
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE NUMBER- 128465
SAMPLE ID- OUTFALL 06
SAMPLE MATRIX- WW
DATE SAMPLED- 09/30/98
TIME SAMPLED-
1045
DATE RECEIVED- 10/01/98
SAMPLER- KG/FM
RECEIVED BY- DHT
TIME RECEIVED-' 0920
DELIVERED BY- COURIER
Page 1 of 2
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
YANIDE, TOTAL
EPA 335.2
10/14/98
APT
<0.005
mg/1
0.005
UORIDE
EPA 340.2
10/08/98
DEP
<0.1
mg/l
0.10
AS
EPA 425.1
10/01/98
APT
0.15
mg/l
0.10
TOTAL KJELDAHL NITROGEN
EPA 351.3
10/14/98
APT
1.1
mg/l
1.0
NITRATE/NITRITE
CALC
10/02/98
APT
0.73
mg/l
0.11
TOTAL PHOSPHORUS
EPA 365.2
10/16/98
APT
0.09
mg/l
0.02
SULFATE
EPA 375.4
10/13/98
KHJ
6.57
mg/l
1.0
SULFIDE
EPA 376.1
-1-0/07/98
APT
<1.0
mg/l
1.0
SULFITE
377.1
10/01/98
APT
<2.0*
mg/l
2.0
PHENOL, TOTAL
420.1
10/05/98
APT
<5.0
ug/l
5.0
ARSENIC, TOTAL
206.2
10/03/98
LJP
10/12/98
LJP
< 0.003
mg/l
0.003
MERCURY, TOTAL
245.1
"'".•10/06/98
LJP
< 0.0002
mg/l
0.0002
SELENIUM, TOTAL
270.2
10/03/98
LJP
10/13/98
LJP
< 0.003
mg/l.
0.003
THALLIUM, TOTAL
279.2
10/03/98
LJP
10/16/98
LJP
< 0.001
mg/l
0.001
ANTIMONY, TOTAL
204.2
10/03/98
LJP.10/16/98
LJP
< 0.003
mg/l
0.003
SILVER,TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.001
mg/l
0.001
TOTAL, ALUMINUM
200.7
10/03/98
LJP
10/08/98
LJP
1.260
mg/1
0.025
BARIUM, TOTAL
200.7
10/03/96
LJP
10/14/98
LJP
0.024
mg/l
0.005
BORON, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.100
mg/l
0.100
BERYLLIUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
c 0.001
mg/l
0.001
CADMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.001
mg/l
0.001
0
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

TestAmerica
0
Page 2 of 2
CONTINUATION OF DATA FOR SAMPLE NUMBER 128465
SAMPLE PREP
ANALYSIS
DET.'
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.057
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
2.450
mg/l
0.010
LEAD, TOTAL
200.7
.10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
MAGNESIUM, TOTAL
200.7
1'0/03/98
LJP
10/14/98
LJP
0.980
mg/l
0.025
NICKEL, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
0.078
mg/l
0.010
TIN, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.710
mg/l
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.340
mg/l
0.010
0 SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST.
r
LABORATORY DIRECTOR
1
r1
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

Testl�merica
INCO APO R A T E O
•
FINAL REPORT OF ANALYSES
HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attn: PAK HESTER
SAMPLE NUMBER- 128466 SAMPLE ID- OUTFALL 07
DATE SAMPLED- 09/30/98
DATE RECEIVED- 10/01/98 SAMPLER- KG/FM
TIME RECEIVED 0920 DELIVERED BY- COURIER
Page 1 of 2
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE MATRIX- WW
TIME SAMPLED- 1050
RECEIVED BY- DHT
SAMPLE PREP
ANALYSIS
.
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
YANIDE, TOTAL
EPA 335.2
10/14/98
APT
<0.005
mg/l
0.005
qWLUORIDE
EPA 340.2
10/08/98
DEP
<0.1
mg/l
0.10
MBAS
EPA 425.1
10/01/98
APT
<0.10
mg/l
0.10
TOTAL KJELDAHL NITROGEN
EPA 351.3
10/20/98
APT
<1.0
mg/l
1.0
NITRATE/NITRITE
CALC
10/02/98
APT
0.36
mg/l
0.11
TOTAL PHOSPHORUS
EPA 365.2
10/16/98
APT
<0.02
mg/l
6.02
SULFATE
EPA 375.4
10/13/98
KHJ
3.50
mg/l
1.0
SULFIDE
EPA 376.1
10/07/98
APT
<1.0
mg/l
1.0
SULFITE
377.1
10/01/98
APT
<2.0*
mg/l
2.0
PHENOL, TOTAL
420.1
10/05/98
APT
<5.0
ug/l
5.0
ARSENIC, TOTAL
206.2
10/03/98
LJP
10/12/98
LJP
<
0.003
mg/l
0.003
MERCURY, TOTAL
245.1
10/06/98
LJP
<
0.0002
mg/l
0.0002
SELENIUM, TOTAL
270.2
10/03/98
LJP
10/13/98
LJP
<
0.003
mg/l
0.003
THALLIUM, TOTAL
279.2
10/03/98
LJP
10/16/98
LJP
<
0.001
mg/l
0.001
ANTIMONY, TOTAL
204.2
10/03/98
LJP-10/16/98
LJP
<
0.003
mg/l
0.003
SILVER,TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
TOTAL, ALUMINUM
200.7
10/03/98
LJP
10/08/98
LJP
2.520
mg/l
0.025
J BARIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.038
mg/l
0.005
BORON, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.100
mg/l
0.100
BERYLLIUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
CADMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<
0.001
mg/1
0.001
0
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE. NC 28801 / 828-254-5169 / FAX: [phone]

TiLestL.�merica
•
Page 2 of 2
CONTINUATION OF DATA
FOR SAMPLE NUMBER
128466
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS'
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.006
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.022
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
2'.495
mg/l
0.010
LEAD, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
MAGNESIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
1.530
mg/l
0.025
NICKEL,'TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
0.260
mg/l
0.010
TIN, TOTAL
200.7
10/03/98
LJP
10/08/'98
LJP
1.260
mg/l
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
2.410
mg/l
0.010
SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST.
0
I
LABORATORY DIRECTOR
r
�J
NC DEHNR DEM # 47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

0
HYDROLOGIC, INC.-LUMBERTON
2003 N. PINE STREET
SUITE 2
LUMBERTON, NC 28358-
Attzi: PAM HESTER
TestAmerioca
I N C 0 R P 0 Fl A I E 0
FINAL REPORT OF ANALYSES
PROJECT NAME: BUCKEYE L'TON
REPORT DATE: 10/21/98
SAMPLE NUMBER- 128467 SAMPLE ID- OUTFALL 08
DATE SAMPLED- 09/30/98
DATE RECEIVED- 10/01/98 SAMPLER- KG/FM
TIME RECEIVED- 0920 DELIVERED BY- COURIER
Page 1 of 2
SAMPLE PREP ANALYSIS
ANALYSIS METHOD DATE BY DATE BY
ANIDE, TOTAL
UORIDE
MAS
TOTAL KJELDAHL NITROGEN
NITRATE/NITRITE
TOTAL PHOSPHORUS
SULFATE
SULFIDE
SULFITE
PHENOL, TOTAL
ARSENIC, TOTAL
MERCURY, TOTAL
SELENIUM, TOTAL
THALLIUM, TOTAL
ANTIMONY, TOTAL
SILVER,TOTAL
TOTAL, ALUMINUM
BARIUM, TOTAL
BORON, TOTAL
BERYLLIUM, TOTAL
CADMIUM, TOTAL
•
SAMPLE MATRIX- WW
TIME SAMPLED- 1055
RECEIVED BY- DHT
DET.
RESULT UNITS LIMIT
EPA 335.2
10/14/98
APT
<0.005
mg/l
0.005
EPA 340.2
10/08/98
DEP
<0.1
mg/l
0.10
EPA 425.1
10/01/98
APT
<0.10
mg/l
0.10
EPA 351.3
10/20/98
APT
8.2
mg/l
1.0
CALC
10/02/98
APT
1.00
mg/l
.0.11
EPA 365.2
10/16/98
APT
0.03
mg/l
0.02
EPA 375.4
10/13/98
KHJ
1.49
mg/l
1.0
EPA 376.1
--
10/07/98
APT
<1.0
mg/l
1.0
377.1
10/01/98
APT
<2.0*
mg/l
2.0
420.1
10/05/98
APT
<5.0
ug/l
5.0
206.2
10/03/98
LJP
10/12/98
LJP
<
0.003
mg/l
0.003
245.1
10/06/98
LJP
<
0.0002
mg/l
0.0002
270.2
10/03/98
LJP
10/13/98
LJP
<
0.003
mg/l
0.003
279.2
10/03/98
LJP
10/16/98
LJP
<
0.001
mg/l
0.001
204.2
10/03/98
LJP-10/16/98
LJP
<
0,003
mg/l
0.003
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0.001
200.7
10/03/98
LJP
10/08/98
LJP
1.435
mg/l
0.025
200.7
10/03/98
LJP
10/14/98
LJP
0.014
mg/l
0.005
200.7
10/03/98
LJP
10/14/98
LJP
<
0.100
mg/l
0.100
200.7
10/03/98
LJP
10/08/98
LJP
<
0.001
mg/l
0-.001
200.7
10/03/98
LJP
10/14/98
LJP
<
0.001
mg/l
0.001
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LYMAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

Test merica
I N C 0 R P 0 R A T H D
Page 2 of 2
CONTINUATION OF DATA
FOR SAMPLE NUMBER
128467
SAMPLE PREP
ANALYSIS
DET.
ANALYSIS
METHOD
DATE
BY
DATE
BY
RESULT
UNITS
LIMIT
CHROMIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COBALT, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
< 0.005
mg/l
0.005
COPPER, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.019
mg/l
0.005
IRON, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
1.550
mg/l
0.010
LEAD, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
< 0.0.10
mg/1
0.010
MAGNESIUM, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
0.500
mg/l
0.025
NICKEL, TOTAL
200.7
10/03/98
LJP
10/14/98
LJP
<'0.005
mg/l
0.005
MOLYBDENUM, TOTAL
200.7
10/03/98
LJP
10/08/98,LJP
< 0.010
mg/l
0.010
TITANIUM, TOTAL
200.7
10/03/98
LJP
10/19/98
LJP
0.063
mg/1
0.010
TIN, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.445
mg/l
0.050
ZINC, TOTAL
200.7
10/03/98
LJP
10/08/98
LJP
0.490
mg/l
0.010
SULFITE ANALYZED OUT OF PROTOCOL PER CLIENT'S REQUEST.
LABORATORY DIRECTOR
0
NC DEHNR DEM #47
NC DEHNR DW #37717
SC DEHC #99015
122 LY,%IAN STREET / ASHEVILLE, NC 28801 / 828-254-5169 / FAX: [phone]

Churn of Wdy Record
L7 Asheville, NC �^
[phone]
L l...libennn, NC
(9 10) 738-6190
HYDR
❑ Norcross, GA L7 Charlotte. NC
(770) 368-(1636 [phone]
❑ lAminglun, SC
(803)796.089
GIC, INC. 3L09 30TR %� k b 64 6-e
C3 Fruzi1:lnri KY 1 C) hlurri,ville. NC
15021 223-0251 [phone]
17 Biighlon, CO 1-1 hlacun, GA L1 (Maud+L, 1-1.
003) 659-0497 (9121 7]7-0811 (4071 s5l -25611
Of __
Client:
Project No.:
nEQurs•rED
of e �� Q
l7
`
�O
`J
PARAMETERS
j�
f� -y
1�
r
�J
LAH.001% 1.1).
A = Ashevil1e, NC
= Charltme, NC
D = Deaver, CO
E = Lexinglull, SC
= i�l:leL}n.GA
K = Frani.for1, KY
t_ = Lumberton. NC
r`1= 11111rrisville, NC
(�q!
�( � N = Norcross, GA
S = SLlhllnilrLLClL!d
OV
Repon Address: G
B 30
nv
lnice Address: ! ;(--e—
L�7►[J �i J ��-3
Al
Alm:Altlr:
L BJ
G
I'huuc No.:
Jn/G'� 37— SZZ�
Fax No.: %3 7- 3 Z
Sam �Ird li
I y .1„fJ
P.O. No:
Sl:uc Sant♦11e5 Crrlh clod
Tl11tNaR()IINI)'1'lAli.
1-1 24 114urs ❑ 48 I bars
11 S Days C1 10 Days Date Needed:
Saillple 11)
Dale
'lilue
C6'lllr/
G rub
hialrix
Clulluillel
l'reserr. REMARKS
oz
/o:,3W
.�.✓.✓
1 8
✓ ✓ �I
L-�O
/F d
Ct
✓
✓
`�
i r p .�
��;
ll
✓
✓
+: Lab Use Onty : ; :; .; Cua4ody Sealy ., : Yes ; - ��`lo: ;' �Pl/A
:.:
Rec. Lab Temp
Intl Lah Temp.
C()h1 h11iN'1'S:
'` S"
Relinquished ey:
S
Date Y R I :'I inu:
Received By.
Dal D ZT* le
Lab Use Only:
Relinquished
*
,C]
gDaIeL_ 13 na
Received By:
/Da _ aTime
Relinquished By:
Dale TLme
Received By:
i);ue Tillie
Relinquished By:
Dale rime
I
Received By:
I):ue Tiler
1

Aquatic Bioassay Testing - Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments - NPOES Testing
Reporting & Data Handling Services
RLINGTON 1302 Belmont Street • Burlington, NC 27215-6935 - Phone [phone] • Fax [phone]
SEARCH
ANALYTICAL REPORT
CUSTOMER: Hydrologic, Inc.
REPORT TO: Ms. Pamcla Hester
SAMPLE DESC: BCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810:25 SITE: Outfall01
WORK ORDER #:
8J020-001
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BL093098
PARAMETER DATE/TIME/ANALYST MOIL RESULT
Apparent Color Storet 00081 Started 10/02/98 08:42 5 25 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington
Bromide, Total for Liquids by IC Started 10/05/98 14:11 0.1 <0.10 mg/L
SM 4500-BR B Analyzed 10/06/98 by MTT at BRI - Burlington
MQL = Minimum Quantitation Limit
•
Water Environmental Services - Eden Water Environmental Services - Kinston
Division of Burlington Research, tnc. Page 1 Division of Burlington Research, Inc.
370 W. Meadow Road Eden. NC 27288 100 E. Gordon Street Kinston, NC 28501
Phone [phone] Fax [phone] Phone [phone] Fax [phone]
aa.2 3M

Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments - NPDES Testing
R 11 ED
Reporting & Data Handling Services
hLiNGTON 1302 Belmont Street • Burlington, NC 27215-6935 • Phone [phone] • Fax [phone]
SEARCH
ANALYTICAL REPORT
CUSTOMER: HydroLobic, Inc.
REPORT TO: Ms. Pamela Hester
SAMPLE DESC: BCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810:30 SITE: Outfall02
Ll
WORK ORDER #:
8JO20-002
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BL093098
PARAMETER DATE/TIME/ANALYST MOL RESULT
Apparent Color Storct 00081 Started 10/02/98 08:42 5 15 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington
Bromide, Total for Liquids by IC Started 10/05/98 14:11 0.1 <0.10 mg/L
SM 4500-BR B Analyzed 10/06/98 by MTT at BRI - Burlington
MQL = Minimum Quantitation Limit
Water Environmental Services - Eden Water Environmental Services - Kinston
Division of Burlington Research, Inc. Page 2 Division of Burlington Research, Inc.
370 W. Meadow Road Eden, NC 27288 100 E. Gordon Street Kinston, NC 28501
Phone [phone] Fax [phone] Phone [phone] Fax [phone]
gN•2 L9a

Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments • NPDES Testing
Ell
Reporting & Data Handling Services
bLINGTON 1302 Belmont Street • Burlington, NC 27215-6935 • Phone [phone] • Fax [phone]
SEARCH
ANALYTICAL REPORT
CUSTOMER: Hydi-oLogic, Inc.
REPORT TO: Ms. Panicla Hester
SAMPLE DESC: BCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810.35 SITE: Outfall04
WORK ORDER #:
8J020-003
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BL093098
PARAMETER DATE/TIME/ANALYST MOIL RESULT
APrarcm Color Storet 00081 Started 10/02/98 08:42 5 20 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington
l3romitic, Total for Liquids by IC Started 10/05/98 14:11 0.1 <0.10 mg/L
SM 4500-I3 R B Analyzed 10/06/98 by MTT at BRI - Burlington
MQL = Minimum Quantitation Limit
0'
Water Environmental Services - Eden Water Environmental Services - Kinston
Division of Burlington Research, Inc. Page 3 Division of Burlington Research, Inc.
370 W, Meadow Road Eden, NC 27288 100 E. Gordon Street Kinston, NC 28501
OR-2 39i7 Phone [phone] Fax [phone] Phone [phone] Fax [phone]

Aquatic 9ioassay Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments - NPOES Testing
Reporting & Data Handling Services
PSLEA
TON 1302 Belmont Street • Burlington, NC 27215-6935 - Phone [phone] + Fax [phone]
IHCH
ANALYTICAL REPORT
CUSTOMER: HydroLooic, Inc.
REPORT TO: Ms. Pantcla Hcstcr
SAMPLE DESC: SCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810:40 SITE: Outfall05
WORK ORDER #:
8JO20-004
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BLO93098
PARAMETER DATE/TIME/ANALYST MQL RESULT
Apparent Color Storct 00081 Started 10/02/98 08:42 5 5 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington.
Bromide:, Total for Liquids by 1C Started . 10/05/98 14:11 0.1 <0.10 mg/L
SM 4500-BR B Analyzed 10/06/98 by MTT at BRI - Burlington
MQL = Minimum Quantitation Limit
Water Environmental Services - Eden Water Environmental Services - Kinston
Division of Burlington Research, Inc. Page 4 Division of Burlington Research, Inc.
370 W. Meadow Road Eden, NC 27288 100 E. Gordon Street Kinston, NC 28501
Phone [phone] Fax [phone] Phone [phone] Fax [phone]
BR-Z 3M

Aquatic Bioassay Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments • NPDES Testing
ED11
Reporting & Data Handling Services
bLI NGTON 1302 Belmont Street • Burlington, NC 27215-6935 • Phone [phone] • Fax [phone]
SEARCH
ANALYTICAL REPORT
CUSTOMER: HydroLogic, Inc.
REPORT TO: Ms. Panicla Hcster
SAMPLE DESC: SCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810:45 SITE: Outfall06
WORK ORDER #:
8J020-005
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BL093098
PARAMETER DATE/TIME/ANALYST MOIL RESULT
Apparcnt Color Storet 00081 Started 10/02/98 08:42 5 50 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington
Bromidc, Total for Liquids by IC Started 10/05/98 14:11' 0.1 <0.10 mg/L
SM 4500-BR B Analyzed 10/06/98 by MTT at BRI - Burlington
MQL = Minimum Quantitation Limit
•
Water Environmental Services - Eden Water Environmental Services - Kinston
Division of Burlington Research, Inc. Page 3 Division of Burlington Research,. Inc.
370 W. Meadow Road Eden, NC 27288 100 E. Gordon Street Kinston, NC 28501
Phone [phone] Fax [phone] Phone [phone] Fax [phone]
ea•: sue

Aquatic Bioassay'Testing • Aquatic Toxicity Reduction Evaluations
Chemical Product Environmental Assessments - NPDES Testing
Reporting 8 Data Handling Services
LI N GTON 1302 Belmont Street • Burlington, NC 27215-6935 • Phone [phone] • Fax [phone]
,SEARCH
ANALYTICAL REPORT
CUSTOMER: HydroLogic, Inc.
REPORT TO: Ms. Pamela Hester
SAMPLE DESC: BCELLULOSE
SAMPLE TYPE: WASTEWATER, GRAB
COLLECTED: 09/30/9810:55 SITE: Outfall08
•
WORK ORDER #:
8J020-007
RECEIVED:
10/01/98
REPORTED:
10/07/98
PO NUMBER: BL093098
PARAMETER DATE/TIME/ANALYST MOIL RESULT
Apparent Color Storet 00081 Started 10/02/98 08:42 5 25 Color Units
EPA 110.2 Analyzed 10/02/98 by LMB at BRI - Burlington
Bromide, Total for Liquids by [C Started 10/05/98 14:11 0.1 <0.10 mg/L
SM 4500-BR B Analyzed 10/06/98 by MTT at. BRI - Burlington
MQL = Minimum Quantitation Limit
tifications:
111U - Burlington
NC Chemistry: #85, Biotnonitoring: #002, Drinking Water: #37743, Radiation License: #001-0904-OG
VA SWC13 I6: #000061, Drinking Water: #00018
SC Environmental: #00018
Ei'A Chemistry Lab ID: NCO0137, Bioassay Lab ID: NC2721500
Water Environmental Services - Eden
Division of Burlington Research, Inc.
370 W. Meadow Road Eden, NC 27288
Phone [phone] Fax [phone]
Page 7 Water Environmental Services - Kinston
Division of Burlington Research, Inc.
100 E. Gordon Street Kinston, NC 28501
Phone [phone] Fax [phone]
SR-2 3M

Chain of gldy Record
11 Asheville, NC
[phone]
L I-unlha:rlon, NC
[phone]
HYDRC49GIC, INC,_ 3L09�'1e
Norcross, GA IJ chadotle, NC
[phone] [phone]
L7 Lexiugwa. SC
(8113) 796.8989
L7 Pranl:forl KY
1502) 23 3-0211
11 1)righloll, CO 1-1 Macon. GA
[phone] (91 ? 1 737-081 1
STOAe of--
1-1 Murrisvillc, NC
19191 381)�9699
L7 Orlando, Ff.
1.07) 8]1-2560
Clicril;R(Lec ILL,m- L
ProjectNO,.
REQUESTED
jj L)
13kcu2 Aj - p
4/
��
/
PARANIffrrRS
��
1�
f�
.�
l'!`
411 Asheville.
� A = �hz�iller:, NC
.�
= Charloue, NC
17 = DeLlVCr, CO
L' = Lexington, SC
i� G = hI tcwI,C;A
� h = Frankfurt, KY
l_ = I-1111IN rtun, NC
Al = Mi rrisvi lle, NC:
Norcruas, GA
4
ReportAdJrcss: ((��
a• !�V 30
lnvoiceAddress:
�� ""�'
/ 3
�C
Awl: {� d �l
1..�
Atut: � o t
Phone No.:
/DIG �� 3 %— 3 ZZ•�
Sampled By:
�vtc �w
Fax Nu.: �7
I'.O. Nu:
Slide S atytics [ u!k sled
TURNAROUNDTI111)i
L1 'a 11aun
-
Days 1111e Needed:
t1 5 Days orm
Sample ID
Date
ItitlC
(,O11t1�
[.rab
AEulrix
CUrdahle
F— Pvtners.
REMARKS
)r p
o:c�p
►� �� �
d-C-0
✓
✓
�/ t�
' I D
Ib� .�
u
✓
✓
_ ab Usc poly' t' {� r i,a „ CIIslody Sealt Imo_ Yexi k No r 1_ rN1A
Al
Init Gab Temp.
Rec. Lab Temp i.
COMMENTS:
�ur� 1 ✓iq�
Relinquished 13y:
Date
Tllttc
RCL'CiVCd Ry.
17a1e T' to
Date I'in,c
I.ah Use Only,
Rclingoislted I *
'C]
�. Ite
Rrecivcd fly:
Relinquished ay:
Dare
'Iiute
Received Il
c
1)a - r 1'Irile
O 5
Relinquished BY:
Dale
lints
I
Rcccivell 11y:
I)me link
I

HYDRQLOGIC, INC. ,
1412 Oakbrook Drive ANALYTICAL
4 cite 105 REPORT
Korcross GA 30093
Phone [phone]
Fax [phone]
CLIENT: Ledger Number N803273
Hydrologic Inc.
P.O. Number
Pam Hester
Date Received
10/01/1998
2003 N. Pine Street
Time Received
10:00
Lumberton, NC 28358
Reporting Date
10/07/1998
P:910-738-6190 F:910-671-8837
Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfail 01
Sampling Date/Time 09/30/1900 10:25
Lab Sample ID N80327301
Prep/Method Dilution Analyst Date of
Analyte Result \ RL Units Factor Init. Prep Analysis
3610/8081 PESTIPCB'S LIQUID
Alpha-BHC
Beta-BHC
Delta-BHC
0ma-BHC(Lindane)
cachlor
Aldrin
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-DDE --
Endrin
Endosulfan II
4,4'-DDD
Endosulfan Sulfate
4,4'-DDT
Methoxychlor
Endrin Aldehyde
Chlordane
Toxaphene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
On Ketone
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02-/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
BelowRL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
BelowRL.
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
BelowRL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.50
ug/L,
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
5.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/0211998
Below RL
1.0
uglL
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/0211998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
.;510/8270 SEMI (GC/MS) LIQUID
Phenol Below RL
Bis(2-Chloroethyl) Ether Below RL
10 ug/L 1.0
10 ug/L 1.0
ML 10/02/1998 10/02/1998
NIL 10/02/1998 10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 1

ProjecLName Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 01
Sampling Date/Time 09/30/1900 10:25
Lab Sample ID N80327301
Method Dilution Analyst Date of
to Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GC/MS) LIQUID
2-Chlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,3-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,4-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-chlorcisopropyl) ether
Below RL
10
ug/L
1.0
ML
• 10/02/1998
10/02/1998
2-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodi-n- pro pylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloroethane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Nitrobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Isophorone
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitrophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dimethylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
8is(2-chloroethoxy)methane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2,4-Trichiarobenzene
Below RL
10
ug/L
1.0
ML
10102J1998
10/02/1998
Naphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chloroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
lahlorobutadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4Wora-3-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylnaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorocyclopentadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,6-Tdchlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,5-Tdchlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chloronaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
Dimethyl Phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
Acenaphthylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzofuran
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Diethyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4,6-Dinitro-2-methylphenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodiphenylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
femophenyl
achlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pe. ntachlorophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Phenanthrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
Hydrologic, Inc. Ledger N803273
PAGE
2

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outFall 01
Sampling DatelTime 09/30/1900 10:25
Lab Sample ID N80327301
6 (te
Method Dilution Analyst Date of
Resulf RL Units Factor Init. Prep Analysts
5030/8260 VOC (GCIMS) LIQUID
Bromodichloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Dibromomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
4-Methyl-2-Pentanone (MIRK)
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
2-Hexanone
Below RL
10
ug/L
1.0
KD
N/A
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KO
N/A
10/0211998
Toluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,12-Trichioroethane
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
1,3-Dichloropropane
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
Tetrachloroethene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
Chlorodibromomethane .
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dibromoethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Ethyibenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
Xylenes (Total)
Below RL
15
ug/L
1.0
KD
N/A
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
aftform
Below RL
5.0
ug/L
1.0
KO
NIA
1010211998
IW,2-Tetrachloroethane
Below RL
5.0
uglL
1.0
KD.
NIA
10/02/1998
1,2,3-Tdchloropropane
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
N-Propylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Bromobenzene
Below RL
5.0
ug/L
1.0
'KD
N/A
10/02/1998
1,3,5-Tdmethylbenzene
BelowRL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
4-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Tert-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
1010211998
1,2,4-Tdmethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
Sec-Butylbenzene
Below RL
5.0
uglL
1.0
KD
N/A
10/0211998
P-Isopropyltotuene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L..
1.0
KD
NIA
10/02/1998
1,4-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
1010211998
N-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dibromo-3-Chloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2,4-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Hexachlorobutadiene
Below RL
5.0.
ug/L
1.0
KD
N/A
10/02/1998
Naphthalene
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
1,2,3-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans-1,4-Dichloro-2-Butene
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
Acetone
Below RL
100
ug/L
1.0
KO
N/A
10/02/1998
�anone (MEK)
Below RL
5.0
ug/L
1.0
1.0
KD
KD
N/A
NIA
10/02/1998
10/02/1998
2.. Moroethylvinyl Ether
Below RL
5.0
ug/L
Acrolein
Below RL
100
ug/L
1.0
KD
N/A
10/02/1998
Methyl Methacrylate
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
HydroLogic, Inc. Ledger N803273
PAGE
4

Projecs Name Buckeye Lumberton
Client Site # SL093098
Client Sample # outfall 01
Sampling Date/Time 09/30/1900 10:25
Lab Sample ID N80327301
!Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GC/MS) LIQUID
lodomethane
Below RL
5.0
ug/L
1.0
KD NIA
10/02/1998
Vinyl Acetate
Below RL
50
ug/L
1.0
KD NIA
10/02/1998
Cis- 1,4-Dichloro-2-Butene
Below RL
5.0
ug/L
1.0
KD NIA
10/02/1998
Methyl Tert-Butyl Ether
Below RL
5.0
ug/L
1.0
KD N/A
10/02/1998
Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 02
Sampling DatelTime 09/30/1900 10:30
Lab Sample ID
N80327302
Prep/Method Dilution Analyst Date of
Analyte Result RL Units Factor Init. Prep Analysis
361018081 PESTIPCB'S LIQUID
Alpha-BHC
Beta-BHC
Delta-BHC
Gamma-8HC(Lind ane)
40chlor
Heptachlor Epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan 11
4,4'-DDD
Endosulfan Sulfate
4,4'-DDT
Methoxychlor
Endrin Aldehyde
Chlordane
Toxaphene
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Endrin Ketone
SEMI (GC/MS) LIQUID
Bis(2-Chloroethyl) Ether
2-Chlorophenoi
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0,050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
uglL
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ugll.
1.0
BG
10/02/1998
10/02/1998
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/0211998
Below RL
5.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger H803273 PAGE 5

Project, Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 02
Sampling Date/Time 09/30/1900 10:30
Lab Sample 1D N80327302
Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GC1MS) LIQUID
1,3-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,4-Dichloco benzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-chloroisopropyl) ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodi-n-propylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloroethane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Nitrobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Isophorone
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitrophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dimethylphenol
Below RL
10
ug/L -
1.0
ML
10/02/1998
10/02/1998
B is (2-chloroethoxy) methane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,24-Trichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Naphthalene
Below RL
10
ug1L
1.0
ML
10/02/1998
10/02/1998
4-Chloroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobutadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
r6-3-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
thylnaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorocyclopentadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,6-Trichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,5-Tdchlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chloronaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitroaniline
Below RL
10
ug1L
1.0
ML
10/0211998
101021199E
Dimethyl Phthalate
Below RL
10
ug/L
1.0
ML
10/0211998
10/02/1998
Acenaphthylene
Below RL
10
ug1L
.1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrophenoi
Below RL
50
ug/L -
1.0
ML
10/02/1998
10/02/1998
4-Nitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzofuran
Below RL
10
ug/L
1.0
ML
10102JI998
10/02/1998
2,4-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Diethyl phthalate
Below RL
10
ug/L
1.0 .
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniline
Below RL
10
ug/L
1.0
ML
10102/1998.1
0/0211998
4,6-Dinitro-2-methylphenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodiphenylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4- romophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
chlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
I, tachlorophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Phenanthrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 6

Project. Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 02
Sampling DatelTime 09/30/1900 10:30
Lab Sample ID N80327302
!Method Dilution Analyst Date of
t
yte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
Di-n-butyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Butyl benzyi phthalate
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
3,3'-Dichlorobenzidine
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(a)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-ethylhexyl) phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Chrysene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
Di-n-octyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
13enzo(b)fluoranth ene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(k)fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(a)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Indeno(1,2,3-cd)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzo(a,h)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(g,hJ)perylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Carbazole
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodimethylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzoic acid
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
I alcohol
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
idine
Below RL
80
ug/L
1.0
ML
10/02/1998
10/02/1998
5030/8260 VOC (GC/MS) LIQUID
Dichlorodifluoromethane
Below RL
10
uglL
1.0
KD
N/A
10/02/1998
Chloromethane
Below RL
10
ug/L
1.0
KD
N/A
10/02/1998
Vinyl Chloride
Below RL .
2.0
ug/L
1.0
KD
NIA
10/02/1998
Bromomethane
Below RL
10
ug/L
1.0
KD
N/A
10102 I998
Chloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trichlorofluoromethane
Below RL
5.0 ,
ug/L
1.0
KD
NIA
10/0211998
1,1-Dichloroethene
Below RL
5.0
uglL
1.0
KD
N/A
10/02/1998
Methylene Chloride
Belo wRL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Carbon Disulfide
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Acrylonitrile
Below RL
5.0
ug/L .
1.0
KD
NIA
10/02/1998
Trans-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0
KO
NIA
10/02/1998
M-Dichloroethane
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
2,2-Dichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
Cis-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0.
KD
N/A
10/02/1998
Chloroform
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
Bromochloromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,1-Trichloroethans
Below RL
5.0
ug/L
1.0
KO
NIA
10/02/1998
1,1-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Carbon Tetrachloride
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
Below RL
5.0
ug/l_
1.0
KDN/A
10/0211998
O-Dich'oroethane
ene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
loroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dichioropropane
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
Bromodichloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 7

Project -Name Buckeye Lumberton
Client Site # BL093098
Client Sample # outfall 02
Sampling Date/Time 09/30/1900 10:30
Lab Sample ID N80327302
!Method Dilution Anayyst Date of
yte Result RL Units Factor !nit Prep Analysts
503018260 VOC (GCIMS) LIQUID
Dibromomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
4-Methyl-2-Pentanone (MIBK)
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
2-Hexanone
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Toluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,2-Tdchloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3-Dichicropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Tetrachloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chlorodibromomethane
Below RL
5.0
ug/L
1.0
KD
N/A
10102 I998
1,2-Dibromoethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Chlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Ethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Xylenes (Total)
Below RL
15
uglL
1.0
KD
NIA
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Bromoform
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
2-Tetrachloroethane
0J-
Below RL
5.0
ugll-
1.0
KD
NIA
10I0211998
Trichioropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
N-Propylbenzene
Below RL
5.0 .
ug/L
1.0
KD
N/A
10/0211998
Bromobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3,5-Trimethyibenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
4-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Tert-Butylbenzene
Below RL
5.0
ug1L
1.0
KD
NIA
10/02/1998
1,2,4-Trimethyibenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Sec-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
P-Isopropyltoiuene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,4-Dichlorobenzene
Below RL
5.0
ug/L .
1.0
KD
N/A
10/02/1998
N-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dibromo-3-Chloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Tdchlorobenzens
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Hexachlorobutadiene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Naphthalene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2,3-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans-1,4-Dichloro-2-Butene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
Acetone
Below RL
100
uglL
1.0
KD
NIA
10/02/1998
- utanone (MEK)
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
lomethylvinyl Esther
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
-,,,Iein
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
Methyl Methacrylate
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
lodomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 8

Project,Name Buckeye Lumberton
Client Site # SLO93098
Client Sample # outfall 02
Sampling Date/Time 09/30/1900 10:30
Lab Sample ID N80327302
!Method Dilution Analyst Date of
y t a Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GCIMS) LIQUID
Vinyl Acetate Below RL 50 ug/L 1.0 KD NIA 10/02/1998
Cis-1,4-Dichloro-2-Butene Below RL 5.0 ug/L 1.0 KD N/A 10/02/1998
Methyl Tert-Butyl Ether Below RL 5.0 ug/L 1.0 KD N/A 10/02/1998
Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 04
Sampling DatelTime 09/30/1900 10:35 Lab Sample ID N80327303
Prep/Method Dilution Analyst Date of
Analyte Result RL Units Factor !nit. Prep Analysis
351018081 PEST/PCB'S LIQUID
Alpha-BHC
Below RL
0.050
ugll-
1.0
BG
10/02/1998
10/02/1998
Beta-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Delta-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Gamma-BHC(Lindane)
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Schlor Epoxide
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan I
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Dieldrin
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DDE
BelowRL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin
BelowRL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan 11
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DDD
Below RL
0.10
ug/L
1.0
BG
10/0211998
10/02/1998
Endosulfan Sulfate
Below RL
0.10
ug/L
1.0
SG
10/02/1998
10/02/1998
4,4'-DDT
Below RL
0.10
ug/L
1.0
eG
10/02/1998
10/02/1998
Methoxychlor
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Aldehyde
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Chlordane
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Toxaphene
Below RL
5.0
ug/L-
1.0
BG
10/02/1998
10/02/1998
Aroclor 1016
BelowRL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1221
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1232
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1242
Below RL
1.0
ug/L
1.0 •
BG
10/02/1998
10/02/1998
Aroclor 1248
Below RL
1.0
uglL
1.0
BG
10/02/1998
10/02/1998
Aroclor 1254
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1260
Below RL
1.0
ug/L
1.0
SG
10/02/1998
10/02/1998
Endrin Ketone
Below RL
0.10
ug/L
1.0
SG
10/02/1998
10/02/1998
3510/8270 SEMI (GC/MS) LIQUID
of
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
-Chloroethyl) Ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,3-Dichloro benzene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10102/1998
HydroLogic, Inc. Ledger N003273
PAGE
9

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 04
Sampling ❑atelTime 09/30/1900 10:35 Lab Sample ID N80327303
!Method Dilution Analyst Date of
vte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GC/MS) LIQUID
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Bis(2-chloroisopropyl) ether
2-Methylphenol
4-Methylphenol
N-Nitrosodi-n-propylamine
Hexachlorcethane
Nitrobenzene
Isophorone
2-Nitrophenoi
2,4-Dimethylphenol
Bis(2-chloroethoxy)methane
2,4-Dichlorophenol
1,2,4-Tdchlorobenzene
Naphthalene
4-Chloroaniline
Hexachlorobutadiene
4-Chloro-3-Methylphenol
*hylnaphthalene
chlorocyclopentadiene
2,4,6-Tdchlorophenol
2,4,5-Tdchlorophenoi
2-Chloronaphthalene
2-Nitroaniline
Dimethyl Phthalate
Acenaphthylene
2,6-Dinitrotoluene
3-Nitroaniline
Acenaphthene
2,4-Dinitrophenoi
4-Nitrophenoi
Dibenzofuran
2,4-Dinitrotoluene
Dlethyl phthalate
4-Chlorophenyl phenyl ether
Fluorene
4-Nitroaniline
4,6-Dinitro-2-methylphenol
N-Nitrosodiphenylamine
4-Bromophenyl phenyl ether
Hexachlorobenzene
chioropheno!
ianthrene
Anthracene
Di-n-butyl phthalate
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL.
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
Below RL
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
50
50
10
10
10
10
10
10
50
10
10
10
50
10
10
10
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
Mt_
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
uglL
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02-/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug1L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10102J1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
,10/02/1998
ug/L
1.0
ML
10102/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
" 10/02/1998
10/02/1998
ug/L .
1.0
' ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02J1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
ug/L
1.0
ML
10/02/1998
10/02/1998
RydroLogic, Inc. Ledger N603273 PACE 10

Project, Name Buckeye Lumberton
Client Site # SLO93098
Client Sample # outfall 04
Sampling OatelTime 09/30/1900 10.35
Lab Sample ID N80327303
/Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Butyl benzyl phthalate
Below RL
10
ugJL
1.0
ML
10/02/1998
10/0211998
3,3'-Oichlorobenzidine
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(a)anthracene
Below RL
10
ugJL
1.0
ML
10/02/1998
10/02/1998
Bis(2-ethylhexyl) phthalate
350
50
ugJL
5.0
ML
10102J1998
10102/1998'
Chrysene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-octyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Senzo(b)fluoranthene
Below RL
10
ugJL
1.0
ML
10/02/1998
10/02/1998
Benzo(k)fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Senzo(a)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Indeno(1,2,3-cd)pyrene
Below RL
10
ugJL
1.0.
ML
10/02/1898
10/02/1998
Dibenzo(a,h)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(g,h,i)perylene
Below RL
10
ug/L
1.0
ML
10/02/1998.10/02/1998
Carbazole
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodimethylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzoic acid
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzyl alcohol
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
�dine
Below RL
80
ug/L
1.0
ML
10/02/1998
10/02/1998
0/8260 VOC (GCIMS) LIQUID
Dichlorodifluoromethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Chloromethane
Below RL
10
ug/L
1.0
KD
NIA
10/0211998
Vinyl Chloride
Below RL
2.0
ugJL
1.0
KD
NIA
10/02/1998
Bromomethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Chloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trichlorofluoromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
1,1-Dichloroethene
Below RL
5.0
uglL
1.0
KD
NIA
10102/1998
Methylene Chloride
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
Carbon Disulfide
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acrylonitrile
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans-1,2-Dichloroethene
Below RL
5.0
ug/L •
1.0
KD
N/A
10102/1998
1,1-0ichloroethane
Below RL
5.0
ugJL
1.0
KD
NIA
10/0211998
2,2-Dichloropropane
Below RL
5.0
uglL
1.0
KD
N/A
10/02/1998
Cis-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Chloroform
Below RL
5.0
ug/L
1.0.
KD
N/A
10102/1998
i3romochloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,1-Trichloroethane
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
1,1-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Carbon Tetrachloride
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
1,2-❑ihloroethane
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
zene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
loroethene
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
,--Oichloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Bromodichloromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Dibromomethane
Below RL
5.0
ugJL
1.0
KD
NIA
10/02/1998
HydroLogic, Inc. Ledger N803273
PAGE
11

Project. Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 04
Sampling Date/Time 09/30/1900 10:35
Lab Sample ID
N80327303
!Method
Dilution
Analyst
Date of
yte
Result
RL
Units
Factor
[nit
Prep Analysis
5030/8260 VOC (GC/MS) LIQUID
4-Methyl-2-Pentanone (MIBK)
Below RL
10
ug1L
1.0
KD
NIA
10/02/1998
2-Hexanone
Below RL
10
ug/L
1.0
KD
N/A
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Toluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans- 1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,12-Trichloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3-Dichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Tetrachloroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Chlorodibromomethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dibromoethane
Below RL.
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Etylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Xylenes (Total)
Below RL
15
ug/L
1.0
KD
N/A
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Bromoform
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,2,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
'OTrichloropropane
pylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Bromobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3,5-T6methylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
4-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Tert-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Tdmethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Sec-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
P-Isopropyltoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,4-Dichlorobenzene
Below RL
5.0
ug/L.
1.0
KD
N/A
10/02/1998
N-Butylbenzene
Below RL
5.0
ug/L _
1.0
KD
NIA
10/02/1998
1,2-Dichlorobenzene
BelowRL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2-Dibromo-3-Chloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Hexachlorobutadiene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Naphthalene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,3-Tdchlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans- l,4-Dichloro-2-8utene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acetone
Below RL
100
ug/L
1.0
KD
N/A
10/02/1998
2-Butanone (MEK)
Below RL
5.0
uglL
1.0
KD
NIA
10/0211998
2-Chloroethylvinyl Ether
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Oein
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
lyi Methacrylate
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
lodomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Vinyl Acetate
Below RL
50
ug/L
1.0
KD
N/A
10/02/1998
HydroLogic, Inc. Ledger H803273
PACE
12

Project Name Buckeye Lumberton
Client Site # EL093098
Client Sample # outfall 04
Sampling Date/Time 09/30/1900 10:35
Lab Sample ID N80327303
(Method Dilution Analyst Date of
lyte Result RL Units Factor [nit. Prep Analysis
5030/8260 VOC (GC/MS) LIQUID
Cis-1,4-Dichloro-2-Butene Below RL 5.0 ug/L 1.0 KD NIA 101021199E
Methyl Tert-Butyl Ether Below RL 5.0 ug/L 1.0 KD NIA 101021199E
Project Name Buckeye Lumberton
Client Site # lBLO93098
Client Sample # outfall 05
Sampling Date/Time 09/30/1900 10:40 Lab Sample ID N80327304
Prep/Method Dilution Analyst Date of
Analyte Result RL Units Factor Init. Prep Analysis
3510/8081 PEST/PCS'S LIQUID.
Alpha-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Beta-BHC
Below RL
0,050
ug/L
1.0
BG
. 10/02/1998
10/02/1998
Delta-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Gamma-BHC(Lindane)
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Atdrin
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
chlor Epoxide
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
sulfan I
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Dieldrin
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-ODE
Below RL
0.10
ug/L
1.0
SG
10/02/1998
10/0211998
Endrin
Below RL
0.10
ug/L
1.0
- BG
10/02/1998
10/02/1998
Endosulfan 11
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DOD
Below RL
0.10
uglL
1.0
BG
10/02/1998
10/02/1998
Endosulfan Sulfate
Below RL
0.10
ug/L
1.0
BG,
10/02/1998
10/02/1998
4,4'-DDT
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Methoxychlor
BelowRL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Aldehyde
Below RL
0,10
ug/L
1.0
BG
10/02/1998
10/02/1998
Chlordane
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Toxaphene
Below RL
5.0
ug/L _
1.0
BG
10/02/1998
10/02/1998
Aroclor 1016
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1221
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1232
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1242
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1248
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1254
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1260
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Ketone
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
351018270 SEMI (GCIMS) LIQUID
Phenol
Below RL
10
ug/L
1,0
ML
10/02/1998
10/02/1998
4 Chioroethyl) Ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
- . dorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,3-Dichlorobenzene
BelowRL ,
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,4-Dichlorobenzene
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger N803273
PAGE
13

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 05
Sampling Date/Time 09/30/1900 10:40
Lab Sample ID N80327304
!Method Dilution Analyst Date of
F
yte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
1,2-Dichlorobenzene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-chloroisopropyl) ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Methylphenal
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodi-n-propylamine
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloroethane
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Nitrobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Isophorone
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitrophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dimethylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Sis(2-chioroethoxy)methane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2,4-Tdchlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Naphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chloroanitine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobutadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chloro-3-M ethyl phenol
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylnaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
0 chlorocyclopentadtene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
rTrichlorophenal
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,5-Trichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chloronaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dimethyi Phthalate
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3-Nitroaniline
Below RL
10
ug1L
1.0
ML
10/02/1998
10/02/1998
Acenaphthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitraphenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzofuran
Below RL
10
ug/L .
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Diethyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
4,6-Dinitro-2-methylphenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
N-N itrosodiphenyla mine
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Bromophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pentachlorophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Oranthrene
acene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-butyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
KydroLogic, Inc. Ledger N803273
PAGE
14

Project dame Buckeye Lumberton
Client Site # BLO93098
Client Sample 9 outfall 05
Sampling Date/Time 09/30/1900 10:40
Lab Sample ID N80327304
Method Dilution Analyst Date of
to Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
Pyrene
Butyl benzyl phthalate
3,3'-Dichlorobenzidine
Senzo(a)anthracene
Sis(2-ethylhexyl) phthalate
Chrysene
Di-n-octyl phthalate
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)pyrene
Dibenzo(a,h)anthracene
Benzo(g,h,i)perylene
Carbazole
N-Nitrosodimethylamine
Benzoic acid
Benzyl alcohol
Benzidine
VQC (GC1MS) LIQUID
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Tdchlorofluoromethane
1,1-Dichloroethene
Methylene Chloride
Carbon Disulfide
Acryionitrile
Trans-1,2-Dichloroethene
1,1-Dichloroethane
2,2-Dichloropropane
Cis-1,2-Dichloroethene
Chloroform
Bromochloromethane
1,1,1-Tdchlorcethan e
1,1-Dichloropropene
Carbon Tetrachloride
1,2-Dichloroethane
Benzene
Trichloroethene
chloropropane
,, odichloromethane
Dibromomethane
4-Methyl-2-Pentanone (MIBK)
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
` 10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
80
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
KD.
NIA
10/02/1998
Below RL
10
uglL
1.0
KD
N/A
10/02/1998
Below RL
2.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L .
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 15

Project Name Buckeye Lumberton
Client Site # SLO93098
Client Sample # outfall 05
Sampling Date/Time 09/30/1900 10:40
Lab Sample ID N80327304
9(Method Dilution Analyst Date of
Fl
�_
yte Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GCIMS) LIQUID
2-Hexanone
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Toluene
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
Trans- 1, 3-D ichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,2-Tdchloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
1, 3-Dichloropro pane
Below RL
5.0
ug/L
1.0
KO
N/A
10/02/1998
Tetrachloroelhene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chlorodibromo methane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dibromoethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Ethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Xylenes (Total)
Below RL
15
ug/L
1.0
KO
NIA
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Bromoform
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,2,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,3-Trichloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
0 pylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
iobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3,5-Tdmethylbenzene
Below RL
5.0
ug1L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ugll-
1.0
KD
N/A
10/02/1998
4-Chlorotoluene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
Tert-Butylbenzene
BelowRL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2,4-Trimethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Sec-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
P-lsopropyltolueneBelow
RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
1,4-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
N-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dichlorobenzene
Below RL
5.0
ug/L .
1.0
', KD
NIA
10/02/1998
1,2-Dibromo-3-Chloropropane
Below RL
5.0
ug/L
1.0
KD­
NIA
10/02/1998
1,2,4-Trichlorobenzene
Below RL
5.0
u91L
1.0
KD
NIA
10/02/1998
He xachlorobutadiene
Below RL
5.0
ug/L
1.0
KO
NIA
10/0211998
Naphthalene
Below RL
5.0
ug/L
1.0
KD
NIA
10I0211998
1,2,3-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KO
NIA
10/02/1998
Trans-1,4-Dichioro-2-Butene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acetone
Below RL
100
ug/L
1.0
KD
N/A
10/02/1998
2-Butanone (MEK)
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
2-Chloroethylvinyl Ether
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acrolein
Below RL
100
ug/L
1.0
KD
NIA
10102M 998
yl Methacrylate
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
19 methane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Vinyl Acetate
Below RL
50
ug/L
1.0
KD
NIA
10/02/1998
Cis-1,4-Dichloro-2-Butene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02-/1998
HydroLogic, Inc. Ledger N803273
PAGE
16

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 05
Sampling DatelTime 09/30/1900 10:40
Lab Sample ID N80327304
Method Dilution Analyst Date of
to Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GCIMS) LIQUID
Methyl Tert-Butyl Ether Below RL 5.0 ug/L 1.0 KD NIA 10/02/1998
Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 06
Sampling Date/Time 09/30/1900 10:45 Lab Sample ID N80327305
Prep/Method Dilution Analyst Date of
Analyte Result RL Units Factor Init. Prep Analysis
351018081 PESTIPCB'S LIQUID
Alpha-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Beta-BHC
Below RL
0,050
ug/L
1.0
BG
10/02/1998
10/02/1998
Delta-BHC
Below RL .
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Gamma-BHC(Lindane)
Below RL
0,050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Aldrin
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor Epoxide
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Wan 1
0.061
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
n
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DDE
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan 11
Below RL
0.10
ug/L
1.0
-BG
10/02/1998
10/02/1998
4,4'-DDD
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan Sulfate
Below RL
0.10
ug/L
1.0
BG
10/0211998
10/0211998._
4,4'-DDT
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Methoxychlor
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Aldehyde
Below RL
0.10
ug/L.
1.0
BG
10/02/1998
10/02/1998
Chlordane
Below RL
0.50
ug/L
1.0
8G
10/02/1998
10/02/1998
Toxaphene
Below RL
5.0
uglL
1.0
BG
10/02/1998
10/02/1998
Aroclor 1016
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1221
Below RL
1.0
ug/C
1.0
BG
10/02/1998
10/02/1998
Aroclor 1232
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1242
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1248
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1254
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1260
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Ketone
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
361018270 SEMI (GC/MS) LIQUID
Phenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-Chloroethyl) Ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
(Wrophenol
chlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,4-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hydro Logic, Inc. Ledger N803273 PAGE I7

Project Name Buckeye Lumberton
Client Site # SLO93098
Client Sample # outfal! 06
Sampling Date/Time 09/30/1900 10:45
Lab Sample ID N80327305
!Method Dilution Analyst Date of
Jyte Result RL Units - Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
8is(2-chloroisopropyl) ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Methylphenol
Below RL
10
ug/L
1.0
ML
110/02/1998
10/02/1998
N-Nitrosodi-n-propylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloroethane
Below RL
10
ug/L
1.0
ML
10/02/1998
10102/1998
Nitrobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Isophorone
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitrophenol
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dimethylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1996
Bis(2-chloroethoxy)methane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2,4-THchlorobenzene
Below RL
`. 10
ug/L
1.0
ML
10/02/1998
10/02/1998
Naphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chioroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998 "
Hexachlorobutadiene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chloro-3-M ethyl phenol
BelowRL
10
ug/L
1,0
ML
10/02/1998
10/02/1998
2-Methylnaphthalene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorocyclopentadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
07richlorophenol
Trichlorophenol
Below RL
10
ug/L
1,0
ML
10/02/1998
10/02/1998
2-Chloronaphthalene
BelowRL
10
ug/L
1.0
'ML
10/02/1998
10/02/1998
2-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dimethyl Phthalate
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3-Nitroaniline
BelowRL
10
ug/L
1,0
ML
10/02/1998
10/02/1998
Acenaphthene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzofuran
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrotoluene
BelowRL
10
ug/L..
1.0
ML
10/02/1998
10102JI998
Diethyl phthalate
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4,6-Dinitro-2-methylphenol
Below RL
50
uglL
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodiphenylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Bromophenyl phenyl ether
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pentachlorophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Phenanthrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
acene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
butyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
Pyrene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
RydroLogic, Inc. Ledger N803273
PAGE
18

Project,Name Buckeye Lumberton
Client Site # SLO93098
Client Sample # outfall 06
Sampling Daterrime 09/30/1900 10:45
Lab Sample ID N80327305
!Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GC1MS) LIQUID
Cis- 1, 3-Dichloropropene
Toluene
Trans-1,3-Dichloropropene
1,12-Trich loroetha n e
1,3-Dichloropropane
Tetrachloroethene
Chlorodibromomethane
1,2-Dibromoethane
Chlorobenzene
Ethylbenzene
1,1,1,2-Tetrach loroetha ne
Xylenes (Total)
Styrene
Isopropylbenzene
Bromoform
1,1,2,2-Tetrachloroeth ane
1,2,3-Trich lora propane
N-Propylbenzene
Mobenzene
Tdmethyl benzene
2-Chlorotoluene
4-Chlorotoluene
Tert-Butylbenzene
1,2,4-Tdmethylbenzene
Sec-Butylbenzene
P-Isopropyltoiuene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
N-Butylbenzene
1,2-Dichlorobenzene
1,2-D i b romo-3-Chloropropane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
1,2,3-Trichlorobenzene
Trans-1,4-Dichloro-2-Butene
Acetone
2-Butanone (MEK)
2-Chloroethylvinyl Ether
Acrolein
Methyl Methacrylate
ethane
Acetate
Cis-1,4-Dichloro-2-Butene
Methyl Tert-Butyl Ether
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
1010211998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
15
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/19988
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Below RL
5.0
ug1L
1.0
KD
NIA
10/0211998
Below RL
5.0
uglL
1.0
KD
N/A
1 OAW1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
i0/02/1998
BelowRL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L _
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
uglL
1.0
KD
NIA
10/0211998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998,
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Below RL
50
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug1L
1.0
KD
NIA
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 20

Project Name Buckeye Lumberton
Client Site # EL093098
Client Sample # outfall 07
Sampling Date/Time 09/30/1900 10:50
Lab Sample ID N80327306
!Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
351018270 SEMI (GC1MS) LIQUID
2,4-Dichlorophenal
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2,4-Tdchlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Naphthalene
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
4-Chloroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobutadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chloro-3-Methylphenal
Below RL
10
ug/L
1.,0
ML
10/02/1998
10/02/1998
2-Methyinaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorocyclopentadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,6-Trichlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,5-Trichlorophenol
BelowRL
10
ug/L
1,0
ML
10/02/1998
10/02/1998
2-Chioranaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dimethyl Phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
Below RL
10
ug/L
1.0
ML.
10/02/1998
10/02/1998
3-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
10nophenal
BelowRL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
zofuran
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Diethyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4,6-Dinitro-2-methyiphenol
BelowRL
50
ug/L
1.0
ML
10/02/1998
10102I998
N-Nitrosodiphenylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Bromophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorobenzene
BelowRL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pentachloropheno!
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Phenanthrene
Below RL
10
ug/L .
1.0
ML
10/02/1998
10/02/1998
Anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-butyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pyrene
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
Butyl benzyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3,3'-Dichlorobenzidine
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(a)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-ethylhexyi) phthalate
Below RL
10
ug/L
1.0
ML
10/0211998
10/02/1998
Chrysene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-octyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
0o(b)fiuoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
zo(k)fluoranthene
BelowRL-
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Senzo(a)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Indeno(1,2,3-cd)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger N803273
PAGE
22

Project Name Buckeye Lumberton
Client Site # BL093098
Client Sample # outfall 07
Sampling Date/Time 09/30/1900 10:50 Lab Sample ID N80327306
lMethod Dilution Analyst Date of
yte Result RL Units Factor Init Prep Analysis
3510/8270 SEMI (GClMS) LIQUID
Dibenzo(a,h)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(g,h,i)perylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Carbazole
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodimethylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzoic acid
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzyl alcohol
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzidine
Below RL
80
ug/L
1.0
ML
10/02/1998
10/02/1998
503018260 VOC (GC/MS) LIQUID
Dichlorodifluoromethane
Below RL
10
ug/L
1.0
KD
N/A
10/02/1998
Chioromethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Vinyl Chloride
Below RL
2.0
ug/L
1.0
KD
N/A
10/02/1998
Bromomethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Chloroelhane
BelowRL.
5.0
ug/L
1.0
KD
N/A
10/02/1998
Tdchlorofluoromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Methylene Chloride
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Carbon Disulfide
Below RL
5.0
uglL
1.0
KD
N/A
10/02/1998
Acrylonitrile
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
0 1,2-Dichloroethene
kchloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2,2-Dichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Cis-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Chloroform
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Bromochloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
1,1,1-Tdchloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
1,1-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Carbon Tetrachloride
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dichloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Benzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trichloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2-Dichloropropane
Below RL
5.0
ug/L •
1.0
KD
N/A
10/02/1998
Bromodichloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
Dibromomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
'4-Methyl-2-Pentanone (MIRK)
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
2-Hexanone
Below RL
10
ug/L
1.0.
KD
N/A
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Toluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,2-Trichloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3-Dichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
trachloroethene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
lT odibromometharie
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
)ibromoethane
Below RL
• 5.0
uglL
1.0
KD
NIA
10/02/1998
Chlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Ethylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
HydroLogic, Inc. Ledger N803273
PAGE
23 .

t rojectfName Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 07
Sampling DatelTime 09/30/1900 10:50
Lab Sample ID N80327306
(Method Dilution Analyst Date of
.81 yte Result RL Units Factor Init. Prep Analysis
503018260 VOC (GCIMS) LIQUID
1,1,1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Xyienes (Total)
Below RL
15
ug/L
1.0
KD
NIA
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Bromoform
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1,2,2-Tetrachioroethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,2,3-Trichloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
N-Propylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Bromobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,35-Trimethylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
4Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Tert-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Tdmethyibenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Sec-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
P-Isopropyltoluene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1',4-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Aftylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
ichlorobenzene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
1,2-Dib romo-3-Chlo ropro pane
Below RL
5.0
ug/L
1.0
K❑
N/A
10/02,/1998
1,2,4-Tdchlorobenzene
BelowRL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Hexachiambutadiene
Below RL
5.0
ug/L
1.0
- KD
NIA
10/02/1998
Naphthalene
Below RL
5.0
uglL
1.0
KD
N/A
10/02/1998
1,2,3-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Trans-1,4-Dichloro-2-13utene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acetone
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
2-Butanone (MEK)
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
2-Chloroethylvinyl Ether
Below RL
5.0
ugll-
1.0
KD
NIA
10/02/1998
Acroiein
Below RL
100
ug/L
1.0
KD
NIA
10/0211998
Methyl Methacrylate
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
lodomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Vinyl Acetate
Below RL
50
ug/L
1.0
KD
NIA
10/02/1998
Cis-1,4-Dichloro-2-Butene
Below RL.
5.0
ug/L
1.0
KD
N/A
10/02/1998
Methyl Tert-Butyl Ether
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
HydroLogic, Inc. Ledger N803273 PAGE 24

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfail 08
Sampling Date/Time 09/30/1900 10:55
Lab Sample ID N80327307
!Method Dilution Analyst Date of
to Result RL Units Factor Init. Prep Analysis
351018081 PEST/PCB'S LIQUID
Alpha-BHC
Below RL
0.050
ug/L
1.0
BG
• 10/02/1998
10/02/1998
Beta-BHC
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Delta-BHC
Below RL
0.050
ug/L
1.0
8G
10/02/1998
10/02/1998
Gamma-BHC(Lindane)
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Aldrin
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Heptachlor Epoxide
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan I
Below RL
0.050
ug/L
1.0
BG
10/02/1998
10/02/1998
Dieldrin
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DOE
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin
Below RL
0,10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan II
Below RL.
\0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DOD
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Endosulfan Sulfate
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
4,4'-DDT
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Methoxychlor
Below RL
0.50
ug1L
1.0
BG
10/02/1998
10/02/1998
Endrin Aldehyde
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
Chlordane
Below RL
0.50
ug/L
1.0
BG
10/02/1998
10/02/1998
hens
Below RL
5.0
ug/L
1.0
BG
10/02/1998
10/02/1998
or 1016
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1221
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1232
Below RL
• 1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1242
Below RL
1.0
ug/L
1.0
BG
10/02/1998
'10/02/1998
Aroclor 1248
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Aroclor 1254
Below RL
1.0
ug/L
1.0
BG
10/02/1998
1010211998
Aroclor 1260
Below RL
1.0
ug/L
1.0
BG
10/02/1998
10/02/1998
Endrin Ketone
Below RL
0.10
ug/L
1.0
BG
10/02/1998
10/02/1998
3510/8270 SEMI (GCIMS) LIQUID
Phenol
Below RL
10
ug/L
1.0
ML
10102/1998 -
10/02/1998
Bis(2-Chloroethyl) Ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chlorophenol
Below RL
10
ug/L -
1.0
ML
10/02/1998
10/02/1998
1,3-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,4-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
1,2-Dichlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Sis(2-chloroisopropyi) ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methylphenol
Below RL
10
ug/L
1.0
MI_
10/02/1998
10/02/1998
4-Methylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodi-n-propylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloroethane
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
Nitrobenzene
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
*Ohnoorone
phenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dmethylphenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-chloroethoxy)methane
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dichlorophenoi
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger N803273
PAGE
25

ProjectWarne Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfail 08
Sampling Date/Time 09/30/1900 10:55
Lab Sample ID N80327307
!Method Dilution Analyst Date of
yte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GCIMS) LIQUID
1,2,4-Tdchlorobenzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Naphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chioroaniline
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorabutadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/0211998
4-Ch loro-3-Methyl phenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Methyinaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachlorocyclopentadiene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,6-Tdchlorophenoi
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4,5-Tdchlorophenol
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Chloronaphthalene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2-Nitroaniiine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dimethyl Phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,6-Dinitrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
3-Nitroaniiine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Acenaphthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
2,4-Dinitrophenol
BelowRL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Nitrophenol
Below RL
50
ug/L
1.0
ML
10/02/1998
10/0211998
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
lazofuran
initrotoluene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Diethyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Chlorophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluorene
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
4-Nitroaniiine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4,6-Dinitro-2-methylphenoi
Below RL
50
ug/L
1.0
ML
10/02/1998
10/02/1998
N-Nitrosodiphenylamine
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
4-Bromophenyl phenyl ether
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Hexachloro benzene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pentachlorophenol
Below RL
50
uglL
1.0
ML
10/02/1998
10/02/1998
Phenanthrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-butyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Butyl benzyl phthalate
Below RL
10
ug/L
1.0 .
ML
10/02/1998
10/02/1998
3,3'-Dichlorobenzidine
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(a)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Bis(2-ethylhexyl) phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Chrysene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Di-n-octyl phthalate
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzo(b)fluoranthene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Below RL
10
ug/L
1.0
ML
1010211998
1010211998
q!o(k)fluoranthene
(a)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Indeno(1,2,3-cd)pyrene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Dibenzo(a,h)anthracene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
HydroLogic, Inc. Ledger N803273
PAGE
26

Project Name Buckeye Lumberton
Client Site # BLO93098
Client Sample # outfall 08
Sampling DateMme 09/30/1900 10:55
Lab Sample ID N80327307
/Method Dilution Analyst Date of
lyte Result RL Units Factor Init. Prep Analysis
3510/8270 SEMI (GC1MS) LIQUID
Benzo(g,h,i)perylene
Below RL
10
ug/L
1.0
ML
10/02/1998
10/02/1998
Carbazole
Below RL
10
ug/L
1.0
ML
10/02/1998
10102/1998
N-Nitrosodimethylamine
Below RL
10
uglL
1.0
ML
10/02/1998
10/02/1998
Benzoic acid
Below RL
50
ug/L
1.0
ML
10/0211.998
10/02/1998
Benzyl alcohol
Below RL
20
ug/L
1.0
ML
10/02/1998
10/02/1998
Benzidine
Below RL
80
ug/L
1.0
ML
10/02/1998
10/02/1998
503018260 VOC (GC/MS) LIQUID
Dichlorodifluoromethane
Below RL
10
ug/L
1.0
KD
N/A
10/02/1998
Chloromethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Vinyl Chloride
Below RL
2.0
ug/L
1.0
KD
NIA
10/02/1998
Bromomethane
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Chloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Tdchlorofluoromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,1-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Methylene Chloride
Below RL
5.0
uglL
1.0
KD
N/A
1010211998
Carbon Disulfide
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Acrylonitrile
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
0ahloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
)Ichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Cls-1,2-Dichloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Chloroform
Below RL
5.0
ug/L
1.0
KD
NIA
.10/0211998
Bromochloromethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1,1-Trichloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,1-Dichloropropene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
Carbon Tetrachloride
BelowRL
5.0
uglL
1.0
KD
N/A
10/02/1998
1,2-Dichloroethane
Below RL
5.0
ug/L
1.0
KD
N/A
1010211998
Benzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trichloroethene
Below RL
5.0
uglL
1.0
KD
NIA
10/02/1998
1,2-Dichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
Bromodichlaromethane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Dibromomethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
4-Methyl-2-Pentanone (MIBK)
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
2-Hexanone
Below RL
10
ug/L
1.0
KD
NIA
10/02/1998
Cis-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0.
KD
NIA
10/0211998
Toluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans-1,3-Dichloropropene
Below RL
5.0
ug/L
1.0
KD
N/A
10102/1998
1,1,2-Trichloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
1010211998
1,3-Dichloropropane
Below RL
5.0
uglL
1.0
KD
N/A
10/02/1998
Tetrachloroethene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Worodibromomethane
ibromoethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
c7_ .robenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Ethylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
1, 1, 1,2-Tetrachloroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10102/1998
HydroLogic, Inc. Ledger N803273
PAGE
27

Project Name Buckeye Lumberton
Client Site # BL093098
Client Sample # outfali 08
Sampling Date/Time 09/30/1900 10:55
Lab Sample ID N80327307
!Method Dilution Analyst Date of
to Result RL Units Factor Init. Prep Analysis
5030/8260 VOC (GC/MS) LIQUID
Xylenes (Total)
Below RL
15
ug/L
1.0
KD
NIA
10/02/1998
Styrene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Isopropylbenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Bromoform
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
1,1,2,2-Tetrachicroethane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,3-Trichloropropane
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
N-Propylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Bromobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3,5-Tdmethylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
4-Chlorotoluene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Tert-8 utyl benzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Trimethylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
Sec-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
P-Isopropyltoiuene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
1,3-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,4-Dichlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
N-Butylbenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
chlorobenzene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
ibromo-3-Chloropropane
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,4-Trichlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
1010211998
Hexachlorobutadiene
Below RL
5.0
ug/L
1.0
KD
NIA
10/0211998
Naphthalene
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
1,2,3-Tdchlorobenzene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Trans- l,4-Dichloro-2-8utene
Below RL
5.0
ug/L
1.0
KD
N/A
10/02119M
Acetone
Below RL
100
ug/L
1.0
KD
NIA
1010211998
2-Butanone (MEK)
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
2-Chicroethyivinyi Ether
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
Acrolein
Below RL
100
ug/L
1.0
KD
NIA
10/02/1998
Methyl Methacrylate
Below RL
5.0
ug/L
1.0
KD
N/A
10/02/1998
lodomethane
Below RL
5.0
ug/L..
1.0
KD
N/A
10/02/1998
Vinyl Acetate
BelowRL
50
ug/L
1.0
KD
N/A
10/02/1998
Cis-1,4-Dichloro-2-8utene
Below RL
5.0
ug/L
1.0
KD
N/A
10/0211998
Methyl Tert-Butyl Ether
Below RL
5.0
ug/L
1.0
KD
NIA
10/02/1998
(
RL = Reporting limit INIT. (•) Analysis performed by another Hydrologic laboratory, (1.1
l
alysis perff%ormed/b�ysubcontracted Laboratory.
! i'lgr`4. f i /�to ..+
)rganics and inorganics In Wastewater, Solids, and Wastes
NC-DEHNR 441, SC-OHEC 98013, GA-DNR-806 UT OOH E-229 (UST), FL-DEP 940134 HRS E87194 {Water} HRS 87368 (Drinking Water)A2tA:0594-01,
EPA ID EPA Reg Waste US Army Corps of
0033 GA-0001011006 Engineers Validation
6 resuigs) relate only to the itent(s) tested.
report shall not be reproduced, except in full, without the written approval of Hydrologic Inc.
HydroLogic, Inc. Ledger N803273 PAGE 28

Chain ()fc*—/Y Recant HYDROS ic, INC. -a�09 30 I � ,)f
171 Ahhcville, NC 17 Nurcrusx, GA L-1 Clt:rrluue, N(' ❑ Frrnkfurl KY l-1 A1oni;eillc. NC
(828) 25.1-5169 (710) J68-11636 {7{I413H2-1164 {SU2l 223-U351 {9191380-a1h9�)
L l_unrttcrlon, NC ❑ l.cxingutrr. SC 11 lirighpm, CO 1-1 hl:rcun, GA 1-1 Orlando, I`1_
(9111) 738-6190 (80.1) 796.8989 [phone] (912) 757.081 1 [phone]
Ciienl: "t101
roject No.: REQUESTED PARAMETERS
Report Address: O Gnvoice Addrcss: s(� n..�, ] A R ('ODE 1.11
�� A = Asheville. NC
ti/ ' = C'Itarlrtllc, NC
1) = Denver, CO
Ann: Aun: L o 1 p, 1; = LeXh%10n, SC
Phone No.: (7 /G �-7 3 7-- 2- TS 5amplcd By: / (� Q pl J� nr (7 = hl:rcrfon.
(�'�rR.•r.d L.e � _ a7 /� � iC = f�rankfnn, KY
Fax No.: l0 7- 3 Z P.U. No: }/ 1. = l.unttn:rlon, NC
1 L7 hl = Morrisville. NC
1'UItNAIt()t1N!)'1'Ihll: State Smnples(ldkcicd 1 `, , ��
N = Norcross, GA
L1 24 f lours ❑ 48 I lours {,� (3 = 01lando, FL
��yJ S = Suhcnnlracicli
o �4 v
1—)5 Days r-1 ltl Days Dale Needed: V \d
Sample 11) Dale Time 031111A/ hlalrlx Cagainc F Presers. REMARKS
Gras
rf
-Z �o: i ✓.✓
i O �a: �� ✓ ,✓ ✓
I
i
!{�a``I,tf` ����°�� �}�j 'ti111�L 1 r l +Y`i.��R - r � 1 � � ,, -. ' �5ry�:1'� a ��• • -'•;'�;� ,•N• _ ., A'.1.
�NIA" Ink Lab Temp. Rec. Lab Temp
COMMENTS:
Relinquished By: Date o q , �T'ir� Receiml l)YJj Daley Z11we Lab Ilse Qnly:
Reliuquishcd Received
Et.
ished By: Dale lime, 11cccivell 13y: Dale •liurr
ishcd ny: D:uc Tune Received lly: Dale [ime

•
•
I[]
CALCULATION OF TOTAL FLOW
Outfall 001
Total Area = 2.75 acres
Impervious = 2.06 acres
Pervious = 0.69 acres
Runoff Coeff
Pervious
Impervious
2.199 = 0.8
2.75
Rainfall = 0.5"
Total Flow =
Outfall 002
.69 acres x (0.5) = 0.345
- 2.06 acres x (0.9) — 1.854
2.199
(0.5")(1/12)(2.75)(43,5601(8)
7.481
534 gallons
Total Area — 0.83 acres
Impervious — 0.83 acres
Pervious — 0,00 acres
Runoff Coeff = 0.9
Rainfall = 0.5
Total Flow — 0.5" 1/12 0,83 43 560 0.9
7.481
— 181 gallons
Page:
1/4

• Outfa11004
Total Area W 3.65 acres
Impervious = 3.24 acres
Pervious = 0.41 acres
Runoff Coeff.
Pervious =
Impervious =
3.121 = 0.86
3.65
Rainfall = 0.5"
Total Flow =
0.41 acres x (0.5) = 0.205
3.24 acres x (0.9) — 2.916
3.121
(0.5 ")(1/ 12)(3.65)(43 s560)(.86)
7.481
757 gallons
Outfall 005
• Total Area = 1.24 acres
Impervious = 1.24 acres
Pervious = 0.00 acres
Runoff Coeff = 0.9
Rainfall = 0.5
Total Flow = (0.5")(1/12)(1.24),(43,560)(0.9)
7.481
C7
— 271 gallons
4
Page:
2/4

• Outfa11006
Total Area = 2.39 acres
Impervious = 2.317 acres
Pervious — 0.073 acres
Runoff Coeff.
Pervious = 2.317 acres x (0.5) _
Impervious — 0.073 acres x (0.9) —
1.2242 = 0.51
2.39
Rainfall = 0.5"
Total Flow -- 0.5' 1/12 2.39 43 560 0.51
7.481
= 297 gallons
Outfall 007
• Total Area — 1.7 acres
Impervious = 1.7 acres
Pervious = 0.00 acres
Runoff Coeff = 0.9
Rainfall = 0.5
Total Flow = 0.5" 1/12 1.7 43 560 0 9
7.481
371 gallons
•
1.1585
0.0659
1.2242
Page:
3/4

• Outfa11008
Total Area = 1.17 acres
Impervious = 0.57 acres
Pervious — 0.6 acres
Runoff Coeff.
Pervious =
Impervious =
0.825 = 0.71
1.17
Rainfall = 0.5"
0.57 acres x (0.5) = 0.285
0.6 acres x (0.9) = 0.540
0.825
Total Flow — (0.5" )(1/12)(1.17)(43,560)(0.71)
7.481
= 202 gallons
0
•
Page:
4/4

G�{��� '— iL� 'r�rr-1 ►'r�7
6�CZ Jig `Ko jL [. f�I CIA
S V'�I121 v` 1,1) v ej 1 V 2 (I A o d v ft
'V'661 3hf1r CINV 1661 ),dvna3-J 'Orfl,1 1 ins aNV! ,ll_SvI-J
�� // I r t: Q= E'l2JQJ21� 1 11�21r1S /W11dM1J NO 01SV0 HVId 311S ' l
:SILON
/�// VM3ddfl�lO
7
HUMS
11 .
I �
k-k k
/ -„ 3 J IIUSicI
f V Wi
-C.NJt\'MV.r1�t)J �2NUP.;?_�`IS�-11=liw2l0.1.S?I'i�lE!_1CI1\C)2T?dP�f=lo021CIn.l1
(S
cl
Dj',U 12I D LNIAINr\IVI.M):) -\' 1d,1A.SM1W1Cf
t_
I_N:-1I�.:�n•°ztic7o t-�l� crl�r,�:.�-r�� i:�� _]rw�lo.r.s ��1� Is ar��� :�l�l��_l�Ir�s
��
,i. FINI.NIN.L1`C5:3)i "Y Ic 21"_1VA1 ,-.1:f l
I
D.11fl MD t i�"_IfV vIV'.i. o:_) it\1 C1vIl f,Rf1'ri 21'-I 1IV21.1. tf`)(Il1'is
it
3JV21ol-I.K1%'1f1 7:701I
G1
1:�b'2TOI-S )I ifAl 1Av-1i�:-)v0-)
LI
;At 1()V110 J S N'1f Id A_I_\'ZI_i_IN, rv111.NOI,1,1 v CIC.V CI1JV SU lei
cl
(11115 .vA1 801 NISva A>Iv1VI�I:T
S
�I?Il1JV1�i1'�II�dI)ICI)f�h.)�I)1U�?"flo�1EI7Yi
�1
Z1'f 1`6 `S 5mf_I_I vo-1 v:=(xv I(Iv0,f "Iv-)IiN=II I)
C
�l')V2IC}_i.S>1"I?ff 1fD1011 1I(10S
.�
C3rIV S)1:•1h1Qf, >1701.5
(1
?1 NA1'A f fW),fff-) 1,W11003
:�iJV)Io.T'; `f`rllli �IrO "I"11�1.
ST.LS IVJ
�!
v��1v .:>�rnvo I 21V:�`Iiv21
�.
�IC)VN(7 L5 Yfnu Dn.SilvJ
:l'._til-ir1�105 �f_l_SZi.ti1 f��1 I'T}1 ,l':I.L1VS
�-
S_!.1�1�JIiiI:If3�1 CINV S-110V11111' NIVr\,l
432rc1J-1.h::II-JNIv_i_.�07 /A" KM]d "Iv.) SS _ SC11Ili l`f I`rF.1Vt 1' V"i_I
� I
\ lZll
\ J QNod N0HVkl3V
JNVId IN3Wld3M A1.SVM
:Too si t ... z
- (d1 ,.1) SNIVda W3.l s,1s dIIAHm iS '-1
�snari �liY(tJ-C�
.I:)VZIo15'ivlil:f LVI" (1"_IIISltll:! — l
�� r 111
.
CJ
arc 11vnr at ris - - rn
L !
>JfdVl NMO(]MO I�3-
/61 ' �l A
\ 773M i
J
>INV1 I10 f102 A �A��N
J �
J �0# RvAno —
g Ilvllno
(SV 1ZIV IdIG )? SSv21O) JOV._MIS ShOiAdId
0(_ i _iC)V2iU.l S Nr21=1 r Vlti hlV2i CINV LI"III ISIP!fl
� SZ
�.�nlxou��I
S4
V - I
Mo311&1�
lie
S01noll
lam
Z) \
/]
dV21�5
?J-al.11Zly-IO i�
��ollN w 0
HSvd IIOJ.'dJ o
S>1 vdl GV0Iv21
IN1 i 13N3
ONIAI Vc1 (INV C1v0d SS3OUv
--iWl 30vNIVM - —
-JVNvO
31,11� 13321.1S
S`1T.i.ON ,E7i 1