HomeMy WebLinkAboutNCS000330_Monitoring Reports_20140306STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
A)C SCXD6 Zj2j�
DOC TYPE
❑ FINAL PERMIT
MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ -Zb VA •
YYYYM M DD
February 28, 2014
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
RECEIVED
MAR 0 6 2014
OE(FILES
)\AtQlBOG
�/`1TI Allvac
P.O. Box 5030
2020 Asheraft Avenue
Monroe, NC 28111-5030
Phone: (704) 289-4511
Fax: (704)290-5194
Email: Joe. Hinkle@atimetals.com
Attached, please find stormwater monitoring data for Permit No NCS000330. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period Sample Number I Start I End
Year 5 — Period 1 9 1 September 1, 2013 1 February 28. 2014
Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
e Hinkle
EHS Manager
Sample Date:-
1 11!111
.13 �
Allvac - Monroe Plant IkATI Allvac
Stormwater Monitoring. Report Fonn
Sample Time: lcl�o
Wr—rawater Dischame Outfall #2
Drainage Area = 272,590sci. ft. = 6.25 acres
%Impervious = 36%
—T0---Mz27 Ll
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
41-a
30
COD
W,
120
TSS
100
Cadmium
Al
i)
0.001
Chromium, total recoverable
0, A)D6
I
Lead, total recoverable
NA
0.03
Nickel, total recoverable
0.26
Zinc, total recoverable
11ISS
0.067
Oil and Grease
SI/
30
pH
(std units)
6-9 (std units)
Storm Date: / IT Storm Duration: Mrs.) Inches of Rainfall: '50 ;I
Duration of time preceding rain event exceeding 0.1": 41 (Firs.)
Q = CIA
Q(Total) = Q(Pervious Area) + Q(Impervious Area)
Q(tot., cis) = (A x inches rain/I 2 inches/ft. x 6.25 acres x .64) + .9 x inches rain/] 2inches/ft. x 6.25 x .36)
Q(Total,cf§)=.l333x (Inches of rain) + .1688 x (Inches of rain)
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Qualitative Monitoring Report
For guidance on filling out this form, please visit: hqp://h2o.enr.state.nc.as/su/Forms Documents htm#miseforms
Permit No.: I !CJJ�lt� l I�3131. 1 /)/ or Certificate of Coverage No.: N/C/Cs/T/ / / / / /
Facility Name: — 7 — 1111V4 c
County:
Inspector: e e'
Date of Inspection: _ —13
Time of Inspection:
of
Total Event Precipitation (inches): d 56
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your permit to verify if Qualitative Monitoring must be performed daring a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
lis preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
j occurred. A single storm event may contain up to 10 consecutive hours of no rrrecioitation.
By this signature, I cefy that this report is accurate and complete to the best of my knowledge:
(Signature of Pee inittee or
Ontfalt Description:
Outfall No. i Sttuc tuie� (pipe, elite h, �Cc.) (, ��
ReucivingSlt=n: ft°.1'L8� 5'�� �(�t L
scribe the industrial activities that occur within the outfall drainage area:
u ' (fcc.f; err+.. ryi �,"�"�. �•���
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: _ r ; l
3. Odor: Describe any distinct odors that the discharge may have (i.e., ,_Hells strongly of oil, weak
chlorine odor, etc.): _ A A it
Page 1 of 2
SWU-2E2-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 2 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 62, 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 (4� 3 4 5
7. Is there any foam in the stormwater discharge? Yes oNo
8. Is there an oil sheen, in the stormwater discharge? Yes 60)
9. Is there evidence of erosion or deposition at the outfall? Yes 0
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SwU-242-112608
aau�
For guidance on filling out this form, please visit: htto:/lh2o.enr.state.ne.us/su/Forms Documents.htm#miscforms
PnnTdt No : N_/CS/d/.
Facility Name: �� O
County: dG r l
Inspector. esrt�! a
Date of Inspection: z
�2l -lal Gil or Certificate of Coverage No.: NIC/G/
Tine of Inspection: /4", /., - __
Total Event Precipitation (inches): O r t
No. lO V-
Was this a Representative Storm Event? (See information below) Yes ❑ No
Please check your pertnit to verify if Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
{ is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
i occ=ed. A single storm event may contain up to 10 consecutive hours of no nrecinitatinn.
By this signature, I certify th4 this report is accurate and complete to the best of my knowledge:
(Signature of Permitaor
I. Gut€al Description:
Outfali No. St<ujctult (Pipe, diLc;h, etc.)
Rec i viug 5ttealtt. o 0` i 2A Ce e e l
Describe theginduitrial_ act villa sdt ucc:u/ witluii LLIe uutl'all 1l iciage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and lint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): jJ0 /I e -
Page I of 2
S,WLt-242-112608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy: _
1 2 3 4 5
5. Floating solids: Choose the number which best describes the amount of floating solids in the
sto_rmwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 20 3 4 5
6. Suspended solids: Choose thee number which best describes the amount of suspended sol;cls ill
the stormwater discharge, where I is no solids and 5 is extremely muddy:
1 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes 60)
IQ. Other Obvious Indicators of Stormwater pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions wal-Tant further investigation.
Page 2 of 2
SWU-242-112608
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httu:/Ih2o,enr.state.nc.us/su/Forms Documents.htmilmiscforms
Permit No_: N_ICC45/
Facility Name:
County:
Inspector:
Date of Inspection:
Time, of Inspection:
/ or Certificate of Coverage No.: NIC/GI l l l l l l
Total Event Precipitation (inches): �6 /<
No.
Was this a Representative Storm Event? (See information below) Ej-,Yes ❑ No
Please check your permit to verify rf Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
i occurred. A single storm event may contain up to 10 consecutive hours of no nreciBitation. i
By this signature, I c�tify that this rTort is accurate and complete to the best of my knowledge:
(Signature of Permittee or
1. Out€all Description:
OutfaIl No. C�,') V �StLC Lae (pipe, clitcil, etc.} r �` t oe c t✓
_►Zeceiviag Sl�eaw: r'r�
Die ,cribe th®�Zndustrt}',a1_ activities that occur withip the outfall drainage at�ea: r^ ot,{ 5 'i (e r .
2. Comer: Describe the color of the disc arge usintr basic colors (red, brown, blue, etc.) and tint
(light, medium, dark:) as descriptors: I ® it' - � /'atzdt-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak -
chlorine odor, etc.): n V A r .
Page I of 2
SWU-242—I 12608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 3 4 5
C. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
l C 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
S. Is there an oil sheen in the stormwater discharge? yes oNo
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SwU-242-112608
QuaNtative Monitoring Report
For guidance on filling out this form, please visit: httn://h2.o.enr.state.nc.us/su/Forms Documants.htm#miscforms
Permit No.: N_/CLS_/
Facility Name:
County:
Inspector: 04
Date of Inspection: _
Time- of InspP.ctton:
or Certificate of Coverage No.: NIC/C-/ / / / / / /
at
Total Event Precipitation (inches): I o_
�KWIM
Was this a Representative Storm Event? (See information below) ages ❑ No
Please check your permit to verify rf Qualitative Monitoring roust be performed daring a representative
.storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.I inches has
j occurred. A single storm event may contain up to 10 consecutive hours of no oreciuitaiion. i
By this sign re, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permitta or
1. Gutfall Dese ' tion:
EDufall No. t StLuc;Lwe (pipe, BALL, etc.) a16k
Rtuci viug Stream: o
{
Detscrib[e� the industrial_ activities at occur within the outfal] d��aivage area:. - ;," , "A !{ ��
fi �,�.� IL. I C4 r 11 A0ra-q
0
2. Color: Describe the color of the disc arge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: lj'c jl C CA4
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak -
chlorine odor, etc.): A DA e .
Page I of 2
SWU-242-I 22608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very cloudy:
1 20 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
sto_rmwater discharge, where 1 is no solids and, 5 is the surface covered with floating solids:
te
1 3 4 5
6. ,Suspended Solids-, Choose the number which best describes the amount of susp--ade;d solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1(D 3 4 5
7. Is there any foam in the stormwater discharge?
Yes (Lo
8. Is there an oil sheen in the stormwater discharge?
Yes �o
9. Is there evidence of erosion or deposition at the outfail?
Yes hTo
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
au.K
QuaRtative
o, g Report
For guidance on filling out this form, please visit: httn://h2o.enr.state.nc.us/su/Forms Documents htmOmiscforms
PPamit No-: ItLcdf
Facility Name: _
County: G
Inspector.
Date of Inspection:
Time of 1nspPction:
HLI1
or Certificate of Covcrage Nu.. N/C/G/
ems' —
Total Event Precipitation (inches): . s4b
Nre��" '�'
Was this a Representative Storm Event? (See information below) ZYes ❑ No
.Please check your pennit to verify sf Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfaE and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
occurred. A single storm event may, contain up to 10 consecutive hours of no nrecinitatinn
By this signaturd, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of
1. Ontfall Description:
Outfall No. �� ~� Si1Lc Lie (pipe, ditch, etc.)
Rec;eivh g Stream:
Describe the industrial_ activities that oc ui within the outfall drainage area: �ih A'� f jr an M�, j,g
U- c
2. Color: Describe the color of the di ge using basic colors (red, brown blue etc.) and tint
(light, medium, dark) as descriptors: _f , rou)
3. Odor: Describe any distinct odors that the discharge .may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): ft,o,evc—
Page I of 2
S,wCT-2e2-I 22608
4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear
and 5 is very cloudy:
l 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 3 4 5
7. Is there any foam in the stormwater discharge?
Yes (DO
8. Is there an oil sheen in the stormwater discharge`?
Yes No
9. Is there evidence of erosion or deposition at the outfali?
Yes (No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242-112608
nAT
R
For guidance on filling out this form, please visit: htto://h2o.enr.state.nc.us/su/Forms Documents.htm-fmiscforms
Permit No.: NT/C!s/
Facility Name:
—
County: ;
Inspector. -
Date of Inspection:
Time of inspection:
d 101 31 ?101 or Certificate of Covcragc No.: NfC/G/
Total Event Precipitation (inches):
Was this a Representative Storm Event? (See information below) `— Cs ❑ No
Please check your permit to verify rf Qualitative Monitoring must be performed during a representative
storm event (requirements vary).
A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that
is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has
I occurred. A single storm event may contain up to 10 consecutive hours of no arecirfitation.
By this signa m, I certify tha� this report is accurate and complete to the best of my knowledge:
(Signature of
1. Gutfall Deseripfon: 1. 1 .f
Duffall No. �� St<UULUe (pipe, clAuli, eCc.)
Receiving Stream: i 7 . C / e- e—
Describe the industri 1 activities that occur with Clio uu(Sall drainage area:
2. Color-: Describe the color of the discphar e using b is colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: 'e� { T o z A_ _ I rkj
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak
chlorine odor, etc.): 1ADAC
Page I of 2
S,wII-2s2-II2608
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear
and 5 is very. cloudy:
1 20 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in the
stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of Suspended solids in
the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 1. n, 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes (DO
9. Is there evidence of erosion or deposition at the outfall? Yes �No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be
indicative of pollutant exposure. These conditions wa`-rant further investigation.
Page 2 of 2
SWU-242-112608
acmnalytical
www.pacelabs.com
February 11, 2014
Mr. Joe Hinkle
Allvac
RE: Project: MONROE S TORMWATER
Pace Project No.: 92188815
Dear Mr. Hinkle:
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
q1t;n M WaAzc
Erin Waters
erin waters@pacelabs.com
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13
Pace Analytical Services, Inc.
aeeAnalytical ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
wmpamlabs.com
(704)875-9092
CERTIFICATIONS
Project: MONROE S I ORMWATER
Pace Project No.: 92188815
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
Virginia/VELAP Certification #: 460221
Smith Carolina Certification #- 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 13
t
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
,�a'cmnalXicai
www.pwalabs.com
(704)875-9092
SAMPLE ANALYTE COUNT
Project: MONROE STORMWATER
Pace Project No.: 92188815
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92188815001 MONROE SW02
EPA 1664E
CLW
1 PASI-C
FPA 200 7
SH1
5 PASI-A
SM 2540D
WRC
1 PASI-A
SM 5210E
DAS
1 PASI-A
SM 5220D
EWS
1 PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13
aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: MONROE STORMWATER
Pace Project No.: 92188815
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MONROE SW02
Parameters
Lab ID: 92188815001 Collected: 02/04/14 13:20
Results Units Report Limit DF
Received: 02/05/14 17:00 Matrix: Water
Prepared Analyzed CAS No. Qual
HEM, Oil and Grease
Analytical Method: EPA 16648
Oil and Grease
5.1 mg/L
5.0
1
02/06/14 08:45
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200 7
Cadmium
ND ug/L
1.0
1
02/06/14 08:50
02/11/14 11:47
7440-43-9
Chromium
20.6 ug/L
5.0
1
02/06/14 08:50
02/09/14 16:46
7440-47-3
Lead
ND u0/L
6 0
1
02/06/14 08,60
02/09/14 10AG
74301 02 1
Nickol
98.9 ug/L
5.0
1
02/06/14 00:50
02/09/14 10:40
7440-02-0
Zino
155 ug/L
10.0
1
02/00/14 08:50
02/09/14 10.46
7440-66-6
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
44.3 mg/L
8.3
1
02/10/14 16:12
5210B BOD, 5 day
Analytical Method: SM 5210B
BOD, 5 day
25.0 mg/L
2.0
1
02/07/14 07:09
02/11/14 09:25
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
66.0 mg/L
2b.0
1
02/07/14 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02111 /2014 05:27 PM without the written consent of Pace Analytical Services, Inc..
Page 4 of 13
aceAnalytical
www.pacelahs.com
i
QUALITY CONTROL DATA
Project: MONROE S'IORMWATER
Pace Project No.: 92188815
QC Batch: GCSV/16595 Analysis Method: EPA 1664E
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92188815001
METHOD BLANK: 1133931
Associated Lab Samples: 92188815001
Parameter
Units
Oil and Grease
mg/L
LABORATORY CONTROL SAMPLE:
1133932
Parameter
Units
Oil and Grease
mg/L
MATRIX SPIKE SAMPLE:
1133933
Parameter
Units
Oil and Grease
mg/L
Date: 02/11/2014 05:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix- Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 02/06/14 08:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 37.6 94 78-114
92188301001 Spike MS MS
Result Conc. Result % Rec
ND 41.7 40.4 88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
% Rea
Limits Qualifiers
78-114
Page 5 of 13
aceAnalytical
www.pacelabs.corn
QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92188815
QC Batch: MPRP/15194 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92188815001
METHOD BLANK: 1133916
Associated Lab Samples: 92188815001
Parameter Units
Cadmium
Chromium
L Pad
Nickel
Zinc
ug/L
ug/L
ug/L
ug/L
ug/L
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
1.0
02/11/1411:25
NI)
50
0.2109/14 16-16
ND
5.0
02/00/1416:16
ND
6.0
02/09/1416:15
ND
10.0
02109/1416:15
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE:
1133917
Spike
LCS
LCS
% Rec
Parameter
Units
Cone.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
516
103
85-115
Chromium
ug/L
500
494
99
85-115
Lead
ug/L
500
602
100
85-115
Nickel
ug/L
500
504
101
85-115
Zinc
ug/L
500
489
98
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1133918
1133919
MS
MSD
92188808001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
ND
500
500
487
480
97
96
70-130
1
Chromium
ug/L
ND
500
500
480
486
95
96
70-130
1
Lead
ug/L
ND
500
500
466
4/2
93
94
70-130
1
Nickel
ug/L
7.9
500
500
480
488
94
96
70-130
2
Zinc,
utl/L
303
500
500
/ /6
184
96
06
7G 130
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1133920
1133921
MS
MSD
92188777001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD
Cadmium
ug/L
ND
500
500
516
514
103
103
70-130
1
Chromium
ug/L
0.53J
500
500
496
488
99
98
70-130
2
Lead
ug/L
5.7
500
500
501
495
99
98
70-130
1
Nickel
ug/L
ND
500
500
506
495
101
99
70-130
2
Zinc
ug/L
195
500
500
693
670
100
95
70-130
3
Date: 02/11/2014 05:27 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 6 of 13
acmnalytical
www.pecetabs.c=
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92188815
QC Batch: WET/29471 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92188815001
METHOD BLANK: 1136199
Associated Lab Samples: 92188815001
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE:
1136200
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1136201
Parameter
Total Suspended Solids
SAMPLE DUPLICATE: 1136202
Parameter
Total Suspended Solids
Date: 02/11/2014 05:27 PM
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 02/10/1416:08
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 248 99 80-120
92188644001 Dup
Units Result Result
mg/L 6.9 6.7
92188815001 Dup
Units Result Result
mg/L 44.3 45.3
RPD Qualifiers
3
RPD Qualifiers
2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 13
aceAnalytical
www.pacelabs.com
Project: MONROE STORMWATER
Pace Project No.: 92188815
QC Batch: WET/29408
QC Batch Method: SM 5210B
Associated Lab Samples: 92188815001
METHOD BLANK: 1133903
Associated Lab Samples: 92188815001
Parameter Units
BOD, 5 day mg/L
LABORATORY CONTROL SAMPLE: 1133904
Parameter Units
BOD, 5 day mg/L
SAMPLE DUPLICATE: 1133905
Parameter
BOD, 5 day
Date: 02/11/2014 05:27 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 52108 BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 02/11/14 09:25
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 173 87 84.5-115.4
92188706001 Dup
Units Result Result RPD Qualifiers
mg/L 378 339 11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 13
4
aceAnalytical
www.pacelabs.corn
Project: MONROE STORMWATER
Pace Project No.: 92188815
QC Batch: WETA/17985
QC Batch Method: SM 5220D
Associated Lab Samples: 92188815001
METHOD BLANK: 1134191
Associated Lab Samples: 92188815001
Parameter Units
Chemical Oxygen Demand mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5220D
Analysis Description: 5220D COD
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 02/07/1413:30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY CONTROL SAMPLE: 1134192
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 736 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134193 1134194
MS MS[)
92188713001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 461 750 750 1050 1060 79 80 75-125 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134195 1134196
MS MSD
92188710001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 2220 3000 3000 5100 5180 96 99 75-125 2
Date: 02/11/2014 05:27 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 13
aceAnalytical
wmpacelabs.com
QUALIFIERS
Project: MONROE STORMWATER
Pace Project No.: 92188815
DEFINITIONS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamino decompot:oe. and cannot bo soparatod from Diphonylamino using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/11/2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13
Pace Analytical Services, Inc.
®
9800Kincey te 100
Hunte svlle, NC'28078
��acmnalXical
www.pacelabs.com
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE
TABLE
Project: MONROE STORMWATER
Pace Project No.: 92188815
Analytical
Lab ID Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92188815001 MONROE SW02
EPA 1664E
GCSV/16595
92188816001 MONROE SW02
EPA 200.7
MPRP/15194 FPA 200 7
ICP/13792
92188815001 MONROE SW02
SM 2540D
WET/29471
92188815001 MONROE SW02
SM 5210B
WET/29408 SM 5210B
WET/29437
92188815001 MONROE SW02
SM 5220D
WETA/17985
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/11/2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13
/ P"7ceAnalyiiad
Page 1 of 2
Issuing Authority:
Pace Huntersville Quality Office
Client Name:
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other Optional
CustodySeal on Cooler/Box Present: ❑ Proj. Due Date:
yes ❑� Seals intact: ❑yes ❑ no
Proj. Name:
Packing Material: ❑ Bubble Wrap ❑ Bubble Bags []/None ElOther
Thermometer Used: IR Gun T1102 T1 0 Type of Ice:/ 1l1 t Blue None ElS�es on ice, cooling process has begun
Temp Correction Factor ,�T1102: No Correction T113011: No Correction
VWl ul 111. ll 1IQI 14-.
Condition Upon Recei
Document Number:
F-CHR-CS-03-rev.13
Corrected Cooler Temp.: 'G
Temp should be above freezing to 6°C
Chain of Custody Present:
Biological Tissue is Frozen: Yes No N/A Date and I 'tials of p� s xafnining
g contents:
Comments:
es ❑No ❑N/A 1.
Chain of Custody Filled Out:
es
❑No
❑N/A
2.
Chain of Custody R—e nquls e :
es
❑No 0NTA-—
Sampler Naive & Slgnalure on COC:
e
❑Nu
LJN/A
4.
5,
Sam loc Arrived within Hold Time: o ❑No
❑N/A
Short Hold Time Analysis (<72hr):
Yes
El No
❑N/A
6.
Rush Turn Around Time Requested:
❑Yes
7No
El N/A
7.
Sufficient Volume:
es
❑No
❑N/A
8.
Correct Containers Used:
-Pace Containers Used:
Yes
es
[]No
❑No
❑N/A
❑N/A
9.
Containers Intact
- Yes
UNo
LJPM
10
Filtered volume received for Dissolved tests
[]Yes ❑No
❑N/A
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
Cs
711
❑No
❑N/A
12.
All containers needing preservation have been checked.
All containers needing preservation are found to bo in
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
,I�Yes
Vd es
❑Y s
❑No
UNo
El No
❑N/A
UN/A
13.
Samples checked for dechlorination:
Yes
❑No
❑N/A
14,
I leadspace In VOA Vials (>(hnin).
❑Yes ❑No
LJ6A
*lb.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
❑Yes
❑Yes
❑No
❑No
❑N/A
El N/A
16.
Client Notification/ Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
SCURF Review: Date: c7� 04
SRF Review: qto Date: 1'9j15'[)qj
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office (Le out of hold, incorrect preservative, out of temp,
incorrect containers)
Field Data Required? Y / N
Place label here
WOi1:92188835
92188815
Page 12 of 13
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--
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3of13