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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20140306STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. A)C SCXD6 Zj2j� DOC TYPE ❑ FINAL PERMIT MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ -Zb VA • YYYYM M DD February 28, 2014 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED MAR 0 6 2014 OE(FILES )\AtQlBOG �/`1TI Allvac P.O. Box 5030 2020 Asheraft Avenue Monroe, NC 28111-5030 Phone: (704) 289-4511 Fax: (704)290-5194 Email: Joe. Hinkle@atimetals.com Attached, please find stormwater monitoring data for Permit No NCS000330. The originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number I Start I End Year 5 — Period 1 9 1 September 1, 2013 1 February 28. 2014 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, e Hinkle EHS Manager Sample Date:- 1 11!111 .13 � Allvac - Monroe Plant IkATI Allvac Stormwater Monitoring. Report Fonn Sample Time: lcl�o Wr—rawater Dischame Outfall #2 Drainage Area = 272,590sci. ft. = 6.25 acres %Impervious = 36% —T0---Mz27 Ll Parameter Results (mg/1) Benchmark Values (mg/1) BOD 41-a 30 COD W, 120 TSS 100 Cadmium Al i) 0.001 Chromium, total recoverable 0, A)D6 I Lead, total recoverable NA 0.03 Nickel, total recoverable 0.26 Zinc, total recoverable 11ISS 0.067 Oil and Grease SI/ 30 pH (std units) 6-9 (std units) Storm Date: / IT Storm Duration: Mrs.) Inches of Rainfall: '50 ;I Duration of time preceding rain event exceeding 0.1": 41 (Firs.) Q = CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cis) = (A x inches rain/I 2 inches/ft. x 6.25 acres x .64) + .9 x inches rain/] 2inches/ft. x 6.25 x .36) Q(Total,cf§)=.l333x (Inches of rain) + .1688 x (Inches of rain) cfs f zo g C O O m K a G1 � o i attics C � m i:+ t s f c y eOi- to t�D ow x !•r O � m o e' o° m th � A m tn E; on y O O � C dam �_ h IT o � 9 � At PD A C 'y, 0 A O ° O T H 0 b 3 I a 0 � � m Cc, y l�•r tD p" (t0 m � A d pet, -, � �• �, $CO as bd C IQ R y m CD G �.... �' N O `< O ON "O l° o S Cr C ON c A n e 'o tD tD K S. m Qualitative Monitoring Report For guidance on filling out this form, please visit: hqp://h2o.enr.state.nc.as/su/Forms Documents htm#miseforms Permit No.: I !CJJ�lt� l I�3131. 1 /)/ or Certificate of Coverage No.: N/C/Cs/T/ / / / / / Facility Name: — 7 — 1111V4 c County: Inspector: e e' Date of Inspection: _ —13 Time of Inspection: of Total Event Precipitation (inches): d 56 Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your permit to verify if Qualitative Monitoring must be performed daring a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that lis preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has j occurred. A single storm event may contain up to 10 consecutive hours of no rrrecioitation. By this signature, I cefy that this report is accurate and complete to the best of my knowledge: (Signature of Pee inittee or Ontfalt Description: Outfall No. i Sttuc tuie� (pipe, elite h, �Cc.) (, �� ReucivingSlt=n: ft°.1'L8� 5'�� �(�t L scribe the industrial activities that occur within the outfall drainage area: u ' (fcc.f; err+.. ryi �,"�"�. �•��� 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: _ r ; l 3. Odor: Describe any distinct odors that the discharge may have (i.e., ,_Hells strongly of oil, weak chlorine odor, etc.): _ A A it Page 1 of 2 SWU-2E2-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 62, 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (4� 3 4 5 7. Is there any foam in the stormwater discharge? Yes oNo 8. Is there an oil sheen, in the stormwater discharge? Yes 60) 9. Is there evidence of erosion or deposition at the outfall? Yes 0 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SwU-242-112608 aau� For guidance on filling out this form, please visit: htto:/lh2o.enr.state.ne.us/su/Forms Documents.htm#miscforms PnnTdt No : N_/CS/d/. Facility Name: �� O County: dG r l Inspector. esrt�! a Date of Inspection: z �2l -lal Gil or Certificate of Coverage No.: NIC/G/ Tine of Inspection: /4", /., - __ Total Event Precipitation (inches): O r t No. lO V- Was this a Representative Storm Event? (See information below) Yes ❑ No Please check your pertnit to verify if Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that { is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has i occ=ed. A single storm event may contain up to 10 consecutive hours of no nrecinitatinn. By this signature, I certify th4 this report is accurate and complete to the best of my knowledge: (Signature of Permitaor I. Gut€al Description: Outfali No. St<ujctult (Pipe, diLc;h, etc.) Rec i viug 5ttealtt. o 0` i 2A Ce e e l Describe theginduitrial_ act villa sdt ucc:u/ witluii LLIe uutl'all 1l iciage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and lint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): jJ0 /I e - Page I of 2 S,WLt-242-112608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: _ 1 2 3 4 5 5. Floating solids: Choose the number which best describes the amount of floating solids in the sto_rmwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 20 3 4 5 6. Suspended solids: Choose thee number which best describes the amount of suspended sol;cls ill the stormwater discharge, where I is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes 60) IQ. Other Obvious Indicators of Stormwater pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions wal-Tant further investigation. Page 2 of 2 SWU-242-112608 Qualitative Monitoring Report For guidance on filling out this form, please visit: httu:/Ih2o,enr.state.nc.us/su/Forms Documents.htmilmiscforms Permit No_: N_ICC45/ Facility Name: County: Inspector: Date of Inspection: Time, of Inspection: / or Certificate of Coverage No.: NIC/GI l l l l l l Total Event Precipitation (inches): �6 /< No. Was this a Representative Storm Event? (See information below) Ej-,Yes ❑ No Please check your permit to verify rf Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has i occurred. A single storm event may contain up to 10 consecutive hours of no nreciBitation. i By this signature, I c�tify that this rTort is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Out€all Description: OutfaIl No. C�,') V �StLC Lae (pipe, clitcil, etc.} r �` t oe c t✓ _►Zeceiviag Sl�eaw: r'r� Die ,cribe th®�Zndustrt}',a1_ activities that occur withip the outfall drainage at�ea: r^ ot,{ 5 'i (e r . 2. Comer: Describe the color of the disc arge usintr basic colors (red, brown, blue, etc.) and tint (light, medium, dark:) as descriptors: I ® it' - � /'atzdt- 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak - chlorine odor, etc.): n V A r . Page I of 2 SWU-242—I 12608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 C. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: l C 3 4 5 7. Is there any foam in the stormwater discharge? Yes No S. Is there an oil sheen in the stormwater discharge? yes oNo 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SwU-242-112608 QuaNtative Monitoring Report For guidance on filling out this form, please visit: httn://h2.o.enr.state.nc.us/su/Forms Documants.htm#miscforms Permit No.: N_/CLS_/ Facility Name: County: Inspector: 04 Date of Inspection: _ Time- of InspP.ctton: or Certificate of Coverage No.: NIC/C-/ / / / / / / at Total Event Precipitation (inches): I o_ �KWIM Was this a Representative Storm Event? (See information below) ages ❑ No Please check your permit to verify rf Qualitative Monitoring roust be performed daring a representative .storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.I inches has j occurred. A single storm event may contain up to 10 consecutive hours of no oreciuitaiion. i By this sign re, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permitta or 1. Gutfall Dese ' tion: EDufall No. t StLuc;Lwe (pipe, BALL, etc.) a16k Rtuci viug Stream: o { Detscrib[e� the industrial_ activities at occur within the outfal] d��aivage area:. - ;," , "A !{ �� fi �,�.� IL. I C4 r 11 A0ra-q 0 2. Color: Describe the color of the disc arge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: lj'c jl C CA4 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak - chlorine odor, etc.): A DA e . Page I of 2 SWU-242-I 22608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 20 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the sto_rmwater discharge, where 1 is no solids and, 5 is the surface covered with floating solids: te 1 3 4 5 6. ,Suspended Solids-, Choose the number which best describes the amount of susp--ade;d solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1(D 3 4 5 7. Is there any foam in the stormwater discharge? Yes (Lo 8. Is there an oil sheen in the stormwater discharge? Yes �o 9. Is there evidence of erosion or deposition at the outfail? Yes hTo 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition maybe indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 au.K QuaRtative o, g Report For guidance on filling out this form, please visit: httn://h2o.enr.state.nc.us/su/Forms Documents htmOmiscforms PPamit No-: ItLcdf Facility Name: _ County: G Inspector. Date of Inspection: Time of 1nspPction: HLI1 or Certificate of Covcrage Nu.. N/C/G/ ems' — Total Event Precipitation (inches): . s4b Nre��" '�' Was this a Representative Storm Event? (See information below) ZYes ❑ No .Please check your pennit to verify sf Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfaE and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may, contain up to 10 consecutive hours of no nrecinitatinn By this signaturd, I certify that this report is accurate and complete to the best of my knowledge: (Signature of 1. Ontfall Description: Outfall No. �� ~� Si1Lc Lie (pipe, ditch, etc.) Rec;eivh g Stream: Describe the industrial_ activities that oc ui within the outfall drainage area: �ih A'� f jr an M�, j,g U- c 2. Color: Describe the color of the di ge using basic colors (red, brown blue etc.) and tint (light, medium, dark) as descriptors: _f , rou) 3. Odor: Describe any distinct odors that the discharge .may have (i.e., smells strongly of oil, weak chlorine odor, etc.): ft,o,evc— Page I of 2 S,wCT-2e2-I 22608 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: l 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes (DO 8. Is there an oil sheen in the stormwater discharge`? Yes No 9. Is there evidence of erosion or deposition at the outfali? Yes (No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242-112608 nAT R For guidance on filling out this form, please visit: htto://h2o.enr.state.nc.us/su/Forms Documents.htm-fmiscforms Permit No.: NT/C!s/ Facility Name: — County: ; Inspector. - Date of Inspection: Time of inspection: d 101 31 ?101 or Certificate of Covcragc No.: NfC/G/ Total Event Precipitation (inches): Was this a Representative Storm Event? (See information below) `— Cs ❑ No Please check your permit to verify rf Qualitative Monitoring must be performed during a representative storm event (requirements vary). A "Representative Storm Event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has I occurred. A single storm event may contain up to 10 consecutive hours of no arecirfitation. By this signa m, I certify tha� this report is accurate and complete to the best of my knowledge: (Signature of 1. Gutfall Deseripfon: 1. 1 .f Duffall No. �� St<UULUe (pipe, clAuli, eCc.) Receiving Stream: i 7 . C / e- e— Describe the industri 1 activities that occur with Clio uu(Sall drainage area: 2. Color-: Describe the color of the discphar e using b is colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 'e� { T o z A_ _ I rkj 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 1ADAC Page I of 2 S,wII-2s2-II2608 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very. cloudy: 1 20 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of Suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 1. n, 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes (DO 9. Is there evidence of erosion or deposition at the outfall? Yes �No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions wa`-rant further investigation. Page 2 of 2 SWU-242-112608 acmnalytical www.pacelabs.com February 11, 2014 Mr. Joe Hinkle Allvac RE: Project: MONROE S TORMWATER Pace Project No.: 92188815 Dear Mr. Hinkle: Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on February 05, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, q1t;n M WaAzc Erin Waters erin waters@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 13 Pace Analytical Services, Inc. aeeAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 wmpamlabs.com (704)875-9092 CERTIFICATIONS Project: MONROE S I ORMWATER Pace Project No.: 92188815 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 West Virginia Certification #: 357 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Smith Carolina Certification #- 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 13 t Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 ,�a'cmnalXicai www.pwalabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: MONROE STORMWATER Pace Project No.: 92188815 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92188815001 MONROE SW02 EPA 1664E CLW 1 PASI-C FPA 200 7 SH1 5 PASI-A SM 2540D WRC 1 PASI-A SM 5210E DAS 1 PASI-A SM 5220D EWS 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 13 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: MONROE STORMWATER Pace Project No.: 92188815 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MONROE SW02 Parameters Lab ID: 92188815001 Collected: 02/04/14 13:20 Results Units Report Limit DF Received: 02/05/14 17:00 Matrix: Water Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 16648 Oil and Grease 5.1 mg/L 5.0 1 02/06/14 08:45 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200 7 Cadmium ND ug/L 1.0 1 02/06/14 08:50 02/11/14 11:47 7440-43-9 Chromium 20.6 ug/L 5.0 1 02/06/14 08:50 02/09/14 16:46 7440-47-3 Lead ND u0/L 6 0 1 02/06/14 08,60 02/09/14 10AG 74301 02 1 Nickol 98.9 ug/L 5.0 1 02/06/14 00:50 02/09/14 10:40 7440-02-0 Zino 155 ug/L 10.0 1 02/00/14 08:50 02/09/14 10.46 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 44.3 mg/L 8.3 1 02/10/14 16:12 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 25.0 mg/L 2.0 1 02/07/14 07:09 02/11/14 09:25 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 66.0 mg/L 2b.0 1 02/07/14 13:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02111 /2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 13 aceAnalytical www.pacelahs.com i QUALITY CONTROL DATA Project: MONROE S'IORMWATER Pace Project No.: 92188815 QC Batch: GCSV/16595 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92188815001 METHOD BLANK: 1133931 Associated Lab Samples: 92188815001 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 1133932 Parameter Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 1133933 Parameter Units Oil and Grease mg/L Date: 02/11/2014 05:27 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix- Water Blank Reporting Result Limit Analyzed Qualifiers ND 5.0 02/06/14 08:39 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 37.6 94 78-114 92188301001 Spike MS MS Result Conc. Result % Rec ND 41.7 40.4 88 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. % Rea Limits Qualifiers 78-114 Page 5 of 13 aceAnalytical www.pacelabs.corn QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92188815 QC Batch: MPRP/15194 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92188815001 METHOD BLANK: 1133916 Associated Lab Samples: 92188815001 Parameter Units Cadmium Chromium L Pad Nickel Zinc ug/L ug/L ug/L ug/L ug/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 02/11/1411:25 NI) 50 0.2109/14 16-16 ND 5.0 02/00/1416:16 ND 6.0 02/09/1416:15 ND 10.0 02109/1416:15 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1133917 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 516 103 85-115 Chromium ug/L 500 494 99 85-115 Lead ug/L 500 602 100 85-115 Nickel ug/L 500 504 101 85-115 Zinc ug/L 500 489 98 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133918 1133919 MS MSD 92188808001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 487 480 97 96 70-130 1 Chromium ug/L ND 500 500 480 486 95 96 70-130 1 Lead ug/L ND 500 500 466 4/2 93 94 70-130 1 Nickel ug/L 7.9 500 500 480 488 94 96 70-130 2 Zinc, utl/L 303 500 500 / /6 184 96 06 7G 130 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1133920 1133921 MS MSD 92188777001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Cadmium ug/L ND 500 500 516 514 103 103 70-130 1 Chromium ug/L 0.53J 500 500 496 488 99 98 70-130 2 Lead ug/L 5.7 500 500 501 495 99 98 70-130 1 Nickel ug/L ND 500 500 506 495 101 99 70-130 2 Zinc ug/L 195 500 500 693 670 100 95 70-130 3 Date: 02/11/2014 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Qual Page 6 of 13 acmnalytical www.pecetabs.c= Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92188815 QC Batch: WET/29471 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92188815001 METHOD BLANK: 1136199 Associated Lab Samples: 92188815001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1136200 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1136201 Parameter Total Suspended Solids SAMPLE DUPLICATE: 1136202 Parameter Total Suspended Solids Date: 02/11/2014 05:27 PM Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 02/10/1416:08 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 248 99 80-120 92188644001 Dup Units Result Result mg/L 6.9 6.7 92188815001 Dup Units Result Result mg/L 44.3 45.3 RPD Qualifiers 3 RPD Qualifiers 2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 13 aceAnalytical www.pacelabs.com Project: MONROE STORMWATER Pace Project No.: 92188815 QC Batch: WET/29408 QC Batch Method: SM 5210B Associated Lab Samples: 92188815001 METHOD BLANK: 1133903 Associated Lab Samples: 92188815001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 1133904 Parameter Units BOD, 5 day mg/L SAMPLE DUPLICATE: 1133905 Parameter BOD, 5 day Date: 02/11/2014 05:27 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 52108 BOD, 5 day Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 02/11/14 09:25 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 173 87 84.5-115.4 92188706001 Dup Units Result Result RPD Qualifiers mg/L 378 339 11 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 13 4 aceAnalytical www.pacelabs.corn Project: MONROE STORMWATER Pace Project No.: 92188815 QC Batch: WETA/17985 QC Batch Method: SM 5220D Associated Lab Samples: 92188815001 METHOD BLANK: 1134191 Associated Lab Samples: 92188815001 Parameter Units Chemical Oxygen Demand mg/L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 02/07/1413:30 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1134192 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 736 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134193 1134194 MS MS[) 92188713001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 461 750 750 1050 1060 79 80 75-125 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1134195 1134196 MS MSD 92188710001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 2220 3000 3000 5100 5180 96 99 75-125 2 Date: 02/11/2014 05:27 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 13 aceAnalytical wmpacelabs.com QUALIFIERS Project: MONROE STORMWATER Pace Project No.: 92188815 DEFINITIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamino decompot:oe. and cannot bo soparatod from Diphonylamino using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PAST-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11/2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13 Pace Analytical Services, Inc. ® 9800Kincey te 100 Hunte svlle, NC'28078 ��acmnalXical www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MONROE STORMWATER Pace Project No.: 92188815 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92188815001 MONROE SW02 EPA 1664E GCSV/16595 92188816001 MONROE SW02 EPA 200.7 MPRP/15194 FPA 200 7 ICP/13792 92188815001 MONROE SW02 SM 2540D WET/29471 92188815001 MONROE SW02 SM 5210B WET/29408 SM 5210B WET/29437 92188815001 MONROE SW02 SM 5220D WETA/17985 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/11/2014 05:27 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13 / P"7ceAnalyiiad Page 1 of 2 Issuing Authority: Pace Huntersville Quality Office Client Name: Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ Commercial Pace Other Optional CustodySeal on Cooler/Box Present: ❑ Proj. Due Date: yes ❑� Seals intact: ❑yes ❑ no Proj. Name: Packing Material: ❑ Bubble Wrap ❑ Bubble Bags []/None ElOther Thermometer Used: IR Gun T1102 T1 0 Type of Ice:/ 1l1 t Blue None ElS�es on ice, cooling process has begun Temp Correction Factor ,�T1102: No Correction T113011: No Correction VWl ul 111. ll 1IQI 14-. Condition Upon Recei Document Number: F-CHR-CS-03-rev.13 Corrected Cooler Temp.: 'G Temp should be above freezing to 6°C Chain of Custody Present: Biological Tissue is Frozen: Yes No N/A Date and I 'tials of p� s xafnining g contents: Comments: es ❑No ❑N/A 1. Chain of Custody Filled Out: es ❑No ❑N/A 2. Chain of Custody R—e nquls e : es ❑No 0NTA-— Sampler Naive & Slgnalure on COC: e ❑Nu LJN/A 4. 5, Sam loc Arrived within Hold Time: o ❑No ❑N/A Short Hold Time Analysis (<72hr): Yes El No ❑N/A 6. Rush Turn Around Time Requested: ❑Yes 7No El N/A 7. Sufficient Volume: es ❑No ❑N/A 8. Correct Containers Used: -Pace Containers Used: Yes es []No ❑No ❑N/A ❑N/A 9. Containers Intact - Yes UNo LJPM 10 Filtered volume received for Dissolved tests []Yes ❑No ❑N/A 11. Sample Labels match COC: -Includes date/time/ID/Analysis Matrix: Cs 711 ❑No ❑N/A 12. All containers needing preservation have been checked. All containers needing preservation are found to bo in compliance with EPA recommendation. exceptions: VOA, coliform, TOC, O&G, WI-DRO (water) ,I�Yes Vd es ❑Y s ❑No UNo El No ❑N/A UN/A 13. Samples checked for dechlorination: Yes ❑No ❑N/A 14, I leadspace In VOA Vials (>(hnin). ❑Yes ❑No LJ6A *lb. Trip Blank Present: Trip Blank Custody Seals Present Pace Trip Blank Lot # (if purchased): ❑Yes ❑Yes ❑No ❑No ❑N/A El N/A 16. Client Notification/ Resolution: Person Contacted: Comments/ Resolution: Date/Time: SCURF Review: Date: c7� 04 SRF Review: qto Date: 1'9j15'[)qj Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le out of hold, incorrect preservative, out of temp, incorrect containers) Field Data Required? Y / N Place label here WOi1:92188835 92188815 Page 12 of 13 0 1. wi ITEM # m 3 D o y e ap a �., o a W - in r, as r m In t0 n3 onFir @ X X l 0 O o o C ['� b v n �7 D a N v a m �-' -4WX �rr� �O N -i� v i c �; b c m N 0 4' W MATRIX CODE (see valid codes to left) m r R SAMPLE TYPE (G=GRAB C=COMP) ti 10 ° 0 0 m w� a • . y� 1^ in m " 1 \ A 1 m Z 3 !`a Z r— n m l `� - '�: a i 8 m m G1 y D i t` \ D m In 3 n m C p O SAMPLE TEMP AT COLLECTION m fl _ # OF CONTAINERS v ��U 3 ° n m c, o d m m- o � � � 5 a x X Unpreserved 2,>< H2SO4 d ° n HNO3 3 OF (� HCl m NaOH 0 Na2S203 N �1 �s 0 Methanol y o Other G S w jAnalysis Test j Y/ N x S` 3 m T ro F n (. ' i C- gap a 0, a C � ��• n `' W �1 y m t� y !?t mm O ~ a mm G) m Z o 1 pZ C Z Temp in Residual Chlorine (Y/N) y m m Received on Ice (Y/N) y w T In —. N °. Custody -- Sealed Cooler J z (D m w (YIN) o O Z z m 71 z Samples Intact m (YIN) a m C -1 0 m "a m o 00 Z c 0 N a � r (n m �v O m > z z = m m m 3 (D .0 i @ N 8 a E �v a o C N 3of13