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NCS000330_Monitoring Reports_20170321
STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. A)Cj'; %bo DOC TYPE ❑ FINAL PERMIT MONITORING REPURTS APPLICATION ❑ COMPLIANCE ❑ OTHER ❑ 20�� 07�_ DOC DATE YYYYM M DD March 16, 2017 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED MAR 2 1. 2017 CENTRAL FILES 0VVR SECTION P.O. Box 5030 2020 Asheraft Avenue Monroe, NC 28111-5030 Phone: (704) 289-4511 Fax: (704)290-5194 Email: Joe.Hinkle@atimetals.com Attached, please find stormwater monitoring data for Permit No NCS000330 The originals and one copy ate included. The mollitwhig data is for the following monitoring schedule: Monitoring Period Sample Number t Start End Year 8 — Period 1 15 September 1, 2016 February 28, 2017 Stoimwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, Joe Hinkle EHS Manager RECEIVED MAR 2 1 201? E -,rpA tPILES DWR Sc- . IeAnalyfical" www.pacelabs.00m i February 15, 2017 Mr. Joe Hinkle Allvac RE: Project: Monroe Stormwater Pace Project No.: 92329092 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on February 08, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 aceAnalj&al www.pacelabs.com I CERTIFICATIONS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Monroe Stormwater Pace Project No.: 92329092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Asheville Certl4lcatlon ll3s 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #- 40 Florida/NELAP Certification ✓ . E87648 South Carolina Certiflcalion M. 09030001 Massachusetts Certification #• M-NC030 Vir0iniaNEL AP Certification #- 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 aceAnalytical www.pacWabs.=n I SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Monroe Stormwater Pace Project No.: 92329092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92329092001 Monroe SW02 EPA 200.7 SER 5 PASI-A 92329092002 Monroe SW02 EPA 1664E JMS 1 PASI-C 92329092003 Monroe SW02 SM 2540D ALC 1 PASI-A 92329092004 Monroe SW02 SM 5220D MDW 1 PASI-A 9.232909.2005 Monroe GW02 SM 5210B CJH 1 I PASI A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.L.C. Page 3 of 18 1eAnalyticaloD wtivw.pacelabs.com ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92329092 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Monroe SW02 Parameters Lab ID: 92329092001 Results Units Collected: 02/08/17 01:15 Report Limit DF Received: 02/08/17 11:15 Matrix: Water Prepared Analyzed CAS No. Qua] 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 02/09/17 21:00 02/13/17 18:41 7440-43-9 Chromium 24.4 ug/L 5.0 1 02/09/17 21:00 02/13/17 18:41 7440-47-3 Lead ND ug/L 5.0 1 02/09/17 21:00 02/13/17 18:41 7439-92-1 Nickel 115 u0/L 50 1 02/09/17 21 00 02/13/17 18-41 7440-02-0 Linc 259 ug/L 10.0 1 02/09/ 17 2,1:00 02/13/17 18:41 7440-66-6 Date: 02/15/2017 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 18 Pace Analytical Services, LLC aceAnalytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92329092 Sample: Monroe SW02 Lab ID: 92329092002 Collected: 02/08/17 01:16 Received: 02/08/17 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 02/15/17 07:39 Date: 02/15/2017 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 18 IeAnalytical® wmpacelabs.com ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92329092 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Monroe SW02 Lab ID: 92329092003 Collected: 02/08/17 01:18 Received: 02/08/17 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 22.8 mg/L 2.5 1 02/10/17 14:37 Date: 02/15/2017 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 k aceAnalytical www.pacelabs=m ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92329092 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Monroe SW02 Lab ID: 92329092004 Collected: 02/08/17 01:20 Received: 02/08/17 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 38.0 mg/L 25.0 1 02/09/17 22:59 Date: 02/15/2017 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytical www.pacelabs.com i ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92329092 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Monroe SW02 Parameters Lab ID: 92329092005 Collected: 02/08/17 01:21 Results Units Report Limit DF Received: 02/08/17 11:15 Matrix: Water Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By DPJ 1 02/09/17 11:15 Collected Date 02/08/17 1 02/00/17 11:15 Collected Time 01:32 1 02/09/17 11:15 Field pH 71 Sid (snits 010 1 02/09/17 VIA 5 Field Temperature 15.8 deg C 0.50 1 02/09/17 11:15 521013 BOD, 5 day Analytical Method: SM 62106 BOD, 5 day 7.7 mg/L 2.0 1 02/09/17 03:25 02/13/17 23:40 Date: 02/15/2017 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 18 laneAnalj6calo www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92329092 QC Batch: 348256 QC Batch Method: EPA 1664B Associated Lab Samples: 92329092002 METHOD BLANK: 1932211 Associated Lab Samples: 92329092002 Parameter Units Oil and Grease mg/L LABORATORY CONTROL SAMPLE: 1932212 Parameter Units Oil and Grease mg/L MATRIX SPIKE SAMPLE: 1932213 Parameter Units Oil and Grease mg/L QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water Blank Reporting Rosult Limit Analysed Qualifiers ND 50 02/15/17 07.32 Spike LCS LCS Conc. Result % Rec 40 36.9 92 35293826002 Spike MS Result Conc. Result 1.1U 40 36.0 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 78-114 MS % Rec % Rec Limits Qualifiers 90 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/1512017 02:35 PM without the written consent of Pace Analytical Services, I.I.C. Page 9 of 18 aceAnalj6cal www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92329092 QC Batch: 347561 QC Batch Method: EPA200.7 Associated Lab Samples: 92329092001 Analysis Method: Analysis Description: EPA 200.7 200.7 MET METHOD BLANK: 1928155 Matrix: Water Associated Lab Samples: 92329092001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium (10/1. ND 10 02113/1717:01 Chromium up/L NI) 50 02/13/17 17.01 Lead ug/L ND 6.0 02/13/1717:01 Nickel ug/L ND 5.0 02/13/1717:01 Zinc ug/L ND 10.0 02/13/1717:01 LABORATORY CONTROL SAMPLE: 1928156 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Cadmium ug/L 500 556 111 85-115 Chrurnlurn ug/L b00 5b4 Ill 8b-I lb Lead ug/L 500 549 110 85-115 Nickel ug/L 500 547 109 85-115 Zinc ug/L 500 558 112 85-115 I Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928157 1928158 MS MSD 92329043019 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 537 540 107 108 70-130 1 Chromium ug/L ND b00 b00 b21 b38 104 108 /0-130 3 Lead ug/L ND 500 500 526 531 105 106 70-130 1 Nlckol ug/L ND 600 600 6118 6:28 '104 106 /O� 1'.10 7 Zinc ug/L ND 500 500 528 539 105 108 70-130 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928159 MS 92328962003 Spike Parameter Units Result Conc. MSD Spike Conc. 1928160 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 561 559 112 112 70-130 0 Chromium ug/L 0.013 500 500 552 544 108 106 70-130 2 mg/L Lead ug/L ND 500 500 534 527 107 105 70-130 1 Nickel ug/L 0.012 500 500 548 544 107 106 70-130 1 mg/L Zinc ug/L 0.085 500 500 634 621 110 107 70-130 2 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2017 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 aceAnalj&al www.pacelabs.corn Project: Monroe Stormwater Pace Project No.: 92329092 QC Batch: 347724 QC Batch Method: SM 2540D Associated Lab Samples: 92329092003 METHOD BLANK: 1929058 Associated Lab Samples: 92329092003 Parameter Units Total 91.1-SlV:ncle:d Solids mg/t LABORATORY CONTROL SAMPLE: 1929059 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 1929060 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2 5 02/10/17 14.18 Spike LCS Conc. Result 250 240 92328982003 Dup Result Result 14.5 13.8 SAMPLE DUPLICATE: 1929061 92329112001 Dup Parameter Units Result Result Total Suspended Solids mg/L ND ND LCS % Rec 96 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 90-110 fzPL1 Uualifiers 5 RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2017 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalXical www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92329092 QC Batch: 347491 QC Batch Method: SM 5210B Associated Lab Samples: 92329092005 METHOD BLANK: 1927949 Associated Lab Samples: 92329092005 rarameter Units ROE), 5 (lay Intl/1 LABORATORY CONTROL SAMPLE: 1927950 Parameter Units BOD, 5 day mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 5210B BOD, 5 day Matrix: Water Blank Reporting Result Limit Analyzed QUalifiel'i ND 2 0 0.2113/17 7140 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 170 86 84.6-115.4 SAMPLE DUPLICATE: 1927951 92329036001 Dup Parameter Units Result Result BOD, 5 day mg/L NO ND RPU (lualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/1512017 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92329092 QC Batch: 347683 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92329092004 METHOD BLANK: 1928918 Associated Lab Samples: 92329092004 Parameter Unit Ohemical Oxygen DomAnd mg/t LABORATORY CONTROL SAMPLE: 1928919 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzod Qualif]ors ND 25 0 02/09/17 22 59 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 754 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928920 1928921 MS MSD 92329195001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua] Chemical Oxygen Demand mg/L 2110 750 750 2600 2600 66 66 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1928922 1928923 MS MSD 92329088001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RND Qual Chemical Oxygen Demand mg/L 38.0 750 750 798 795 101 101 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2017 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical www.pacelabs.corn QUALIFIERS Project: Monroe Stormwater Pace Project No.: 92329092 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. III Reporting L imit Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - Surrogate 1,2 Diphonylhydrozino deoomposes to and cannot be separated from Azobenzene using Method 8270 The result for each analyte is a combined concentration Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up LI - Indicator the compound was analyzed for, but not dotoctod Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. L ASORATORIFS PASI-A Pace Analytical Services - Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2017 02:35 PM without the written consent of Pace Analytical Services, I.I.C. Page 14 of 18 Pace Analytical Services, LLC ® aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Monroe Stormwater Pace Project No.: 92329092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92329092005 Monroe SW02 92329092002 Monroe SW02 EPA 1664B 348256 92329092001 Monroe SW02 FPA 2007 347561 FPA 200 7 347718 92329092003 Monroe SW02 SM 2540D 347724 92329092005 Monroe SW02 SM 5210B 34/491 SM 5210B 341499 92329092004 Monroe SW02 SM 5220D 347683 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/15/2017 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 18 aceAnalyticai® Laboratory receiving samples: Asheville ❑ Eden❑ uucuruemc ivame: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ Huntersville Raleighn Mechanicsville❑ • -' ' ®• ° Client dame: W® • t+ /+ : Project # Courier: ❑Fed Ex ❑UPS ❑USPS [ lient II II fIl fiI I I IfI� Commercial El commercial ❑Other: 92329092 Custody Seal Present? ❑Yes [914o' Seals Intact? ❑Yes [3N/o Date/Initials Person Examining Contents:__` Packing Material: ❑Bubble Wrap Bubhie Bags ❑None ❑Other: Thermometer: �-- , IR Gun ID: Type of ice: pGyet ❑Blue ❑None lffsamples on Ice, cooling process has begun Correction Farttlr: Cooler temp Corrected (°C): t% Biological Tissue Frozen? ayes Pilo nN/A I ernp should be above freeing to 6'C USDA Regulated Soil ( [ I N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did iarripim arighmte frorn d foreign source (intern tionally, ❑Yes �io influrlino Nawnii 1 Dunrtn Rijn)? I—IVne .. ' Comments/Discrepancy: Chain of Custody Present? res ❑No ❑N/A 1. Samples Arrived within Hold Time? DY6, ❑No ❑N/A 2.6 Short Hold Time Analysis (<72 hr.)? es ®No ❑N/A 3. Rush Turn Around Time Requested? Sufficient Volume?' worrect Containers Used? -PaCE6Containers Used? ®Yes as es es ONO []NO [:]No [IN. ❑N/A ❑N/A ❑N/A ❑N/A 4. 5_ 6. :ontainers Intact? Oes ONO ❑N/A 7. ;amples Field Filtered? QYes []No A 8. Note if sediment is visible in the dissolved container w;ampleLab els Match COC? -Includes Date ime ID/ ttalysis Matrix: ieadspace in VOAVials (>5.6mm)? es V" ❑Yes �No QNo ❑N/A N 9. 10. 'rip Blank Present? 'rip Blank Custody Seals Present? ❑Yes ❑Yes ❑No [--]No NJQ+ iA 11. .. .4r. .fnsauwnu'v Field Data Required? HYes [ ,INo Person Contacted: Date/Time: Comments/Sample -- Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Date• .,._�� �`� � ` ;-- Date: C, ote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office:;_.e. ut of hold, incorrect preservative, out of temp, incorrect containers) ' Page 16 of 18 Document Name: Document Revised: Sept. 21, 2016 �,aceAnalyfical' Sample Condition Upon Receipt(SCUR) Page 2 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office *Check mark top half of box if pH and/or dechlorination Project #t is verified and within the acceptance range for preservation samples. PM: MWB Due Date: 02/17/17 **Bottom half of box is to list number of bottles CLIENT: 92—A1 lvae NC Z Z Z O (v1 v a Q Z a Z f0 n 67 2 V Z e21 N /V H ^ a C i^y V V Z m 7 m Q1 a OL O O Mu uU aOCL 2u o v O a1; O aN Z 1JN} � Z n a o �^ ?�C a uVtS O y 9N C C 0 aaU u Od NJ Z SQqJ1 J V N1 d A V w IL FL IL C Yu Gc 4 Cal AZ (�r� E V E E Ln (I E E F nl u`I J Q87 E e�i E i E > ro € E E E N 0) Q CL CL 0. IL IL N NIt (1') M M if) v) VQd N yr tYl g (Il 5 t71 IJt QI UI 4 0I UI < N M Y IL a a a a _ CO CO Co oo a m 0. a CO a CO3 (� a (o a t? a t9 a C7 a i'1 a C7 a (� > {� > to o 0 > \ > n, V) A. In m 3 U 1n Z > 17 1 2 3 4 NK s 6 7 R 9 10 it 12 pH Adjustment Log for Preserved Samples Sample ID I Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Page 17 of 18 0 cr 0) E Ix 0 M C.) (U z w 0in L) LL '0 9 Z 9 2 F- MIN, w soldweS Q) 0- Q 0 q7'— z 0 z o-. 2 0 (NIA) 0 0 0 u J910 Z) POILOS APOIsno d. cr- w w (NIA) &31 cc w uo PDA!31Da (N/,k) euijolqo lenp!saa :41 C), ut dwal —&—L— 0 z W z 0 c� (D X 71 all fy 0 U) I.J - E z 0 Ult Vj 0) m INS ,z I INIA t JSq.L SISAleuvt - - JqqjO w loueqievq -JZ, a HOEN JOH ONI I x E 'OS'H [XI pamasaidun X1 [XI J R- U, S2I3NIVIN00:J0 0 0 < w w N011391100 IV dNBI 31dNV5 0 0 w w 8 w z C) IZ I),( In -K �K Z w 0 :2 < tL F- (d[NOD=O BVIJE)=D) 3dU 31MVS -NJ z 3C1OOXlUiWN P 0 E E r 2 ir U) U) 0 3: < 0. --l(I H Mcno 8 uj 0 w w 0 E A EL ZZ) Cf) C) r lyN 2 a E -R, 0 E .6 F age 18 of 18 4, 0 (n () < E w aa: — I W� l C-� -i Allvac - Manrne.-Mmt ATIA11vac SIOEMML4—ter Monito-rine-Revoit Forni Sample Date: _.. c9 YZ_ Sample Time:_. Z- Sample Location: SLormwat-e-r Discharge Qutfall #2 Drainage Area = 272°590sq.A= �.25 acres % Impervious = 36% Person Collecting Samples: '1R. Laboratory Performing Analysis: Anstytical Techniques and Methods: 40. CFI J)Ut jj§ Results of Sample Anal sis: Parameter Results BOD COD TSS Cadmium Chromium , total recoverable Lead, total recoverable Nickel, total recoverable Zinc, total recoverable Oil and Grease pH Vol (std units) enchmark 30 120 100 0.001 1 0.03 0.26 0.067 30 6-9 (std units) St® Date: -5?LB--LZ St® Duration: (Hrs.) Inches of Rainfall: .�c9 Duration of time preceding rain event exceeding 0.111: Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area) Q(tot, cfs) = (A x inches rain/1 2 inches/ft. x 6.25 acres x 64) +.9 x inches rain/1 2inches/ft. x 6.25 x .36) Q(Total,cfs)=.l333x 0-52) (Inches of rain) +.1688 x..... 0..-00 _(Inches ofrain) = —.0 ./So efs R n d a, e e o . COi Jr' N R ' CYti� w n ° �� p e r0 aai � y ti 'O C O ^ j y W 0.0 d ppO R tv�M.,i p ab �0, a p. o py o o e a P. a Ix AFW AFW c y o o.? O O fV O O N 0 N � 6 AAA �MA� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, pleace visit- http://Vort.al,ncdenr.org/wtbL",q/iti�,v/,cu/npd tltab 9 Permit No.: IV/C/,'�/Q/Q/O/3/,�/Q/ or Certificate of Coverage No.: N/f/G/_/_/_/_/_/_1 Facility Name: _ /ITT A/1 Vac County: 4Gq;on Phone No. 7041 o289-yS// Inspector: �y aW oDe JR . Date of Inspection: o? -9 -17 Time of Inspection: _ / - 4a a». Total Event Precipitation (inches): Q - SO Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .............. _. I ...................... _..................... .......... _..... _- - - ..._. __._. -._...._.............. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm evert" od dut inn a "weasureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event' is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event' is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. Structure (pipe, ditch, etc.) Pip a Receiving Stream: �icti an Cre�jC --z— Describe the industrial activities that occur within the outfall drainage area: Ine4L/ 5f,*-'0- 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 'uA2� hl-JAIII ell 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Np l g 4. Clarity: Choose the number which best describes the clai Ity of the discharge, where 1 is clear and 5 is very cloudy: 1 (S 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: ® 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ® 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes to 8. Is there an oil sheen in the stormwater discharge? Yes Q�o 9. Is there evidence of erosion or deposition at the outfall? Yes 4� 10. Other Obvious Indicators of Stormwater Pollution: List and describe /Uyr1 e- Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SM-242, Last modified 10/25/2012 trl 4 INCDENi- Stormwater Discharge ®utfall (SDD) Qualitative Monitoring Report For guidance on filling out this form, please visit., jttp://portal ncdenr org/web/wq/ws/su/npdessw#tabA Permit No.: N/C/.4-'l or Certificate of Coverage No.: Facility Name: AT.r A//✓a-C County: 141ion Phone No. �Dy-a89-yS// Inspector: Aawid' f'D,ye Date of Inspection: Time of Inspection: Total Event Precipitation (inches): D . S'D Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) des ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .................... . Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. swots Structure (pipe, ditch, etc.) Receiving Stream: ��e_ha®a�.s�r, PeeK Describe the industrial activities that occur within the outfall drainage area: ReAl f Mz9 e 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: l-�Xf 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ AdwG 4. Clarity, Choose the number which crest describes the clarity of the discharge, where 1 is clear and S is very cloudy: 1 ® 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: d> 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 ® 3 4 5 7. Is there any foam in the stormwater discharge? Yes ®o 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 09 10. Other Obvious Indicators of Stormwater Pollutions List and describe /VDiJ e Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 �`AA WDENR Storrnwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit. ht-tp,//PQrta1,nc-le..[#r,QLr1wcb/wq/w5/su/npdessw#tab-4 Permit No.: N/C/,f/Q/ o/ o1.g1 1Q1 or Certificate of Coverage No.: Facility Name: _All 411.,k c County: 44yi3, Phone No. 70y o?89' Sys// Inspector: Aae& P Aope, .7R. Date of Inspection: oZ - 8'n Time of Inspection: /-,98A.,. Total Event Precipitation (inches): 0. SD Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) ['Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). _..._._............ ._._....... ..... I ......... _................. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be perfortrted during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: n ��; V I. Outfall Description: Outfall No. 0.3 Strt Receiving Stream: A16 Describe the industrial activities (pipe, ditch, etc.) —O/®e 1,04c-4 occur within the area: W 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): AW-e 4, Clarity: Choose the iruuibe" which Lest desci ibes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 tP 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0) 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. 8. 9. 10. © 2 3 4 5 Is there any foam in the stormwater discharge? Yes 0 Is there an oil sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Other Obvious Indicators of Stormwater Pollution: List and describe /!!D/7e- Yes Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SM-242, Last modified 10/25/2012 Page 2 of 2 `j ` * v� NEDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. lttR�/lpgrtat llcdenr,org/web/wq (ws sulnrldcss_w#tab-4 Permit No.: or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ Facility Name: fiT.z 41/r4G County: LGniorr Phone No. yDy-�89�ys// Inspector: VW/W &e- mg Date of Inspection: a? -8 -17 Time of Inspection: 4 Oa?a#., Total Event Precipitation (inches): D . Sa Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) E6Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: I. Outfall Description: Outfall No. - 'W©Y AStru Receiving Stream: Describe the industrial activities S/,ioyi�g s (pipe, ditch, etc.) occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ND�e 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ Am e 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: ® 2 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: d> 2 3 4 5 d. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ® 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 0. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes & 10. Other Obvious Indicators of Stormwater Pollution: List and describe ol? L Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SM-242, Last modified 10/25/2012 A NCDENR Stormwater Discharge ®utfall (SD®) Qualitative Monitoring Report Forguidanre on filling out this form, please visit- 4 Permit No.: N/C/S/O/O/O/,�/,g/Q/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ Facility Name: County: Inspector: owl 3R. Date of Inspection: ;Z -Sy 7 Time of Inspection: _ /- 6dz. Total Event Precipitation (inches): 0 - S'O Phone No. 701/aB9 --M/ Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be pet funned during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: ,41 � 1. Outfall Description: Outfall No. .ShI05' S r Receiving Stream: i Describe the industrial activitie: (pipe, ditch, etc.) �iCit SOr! �iIrCe— occur 2. Color: Describe the color of the disci: (light, medium, dark) as descriptors: the outfall drainage area: using basic colors (red, brown, blue, etc.) and tint 3. Odor. Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc) Non P 4, Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: & 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ® 2 3 4 5 Is there any foam in the stormwater discharge? Yes 6o Is there an oil sheen in the stormwater discharge? Yes Is there evidence of erosion or deposition at the outfall? Other Obvious Indicators of Stormwater Pollution: List and describe AlDn ,- Yes Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 �r NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please visit. http:1/12orW.ncdeni-.org/web/wqlws/su./iijidessw#Lat)-4 Permit No.: N/C/�'/ o / e / o%�/,�/Q/ or Certificate of Coverage No.: Facility Name: Alt'-//yaG County: Inspector: _A -;R Date of Inspection: Time of Inspection: Total Event Precipitation (inches): ©- SD Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [(Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. S Structure (pipe, ditch, etc.) . /29/ Receiving Stream: rr{+ o (��ee/C Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): A1d4e- 4. Clarity: Choose tlic- "U"Iber which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 ® 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ® 2 3 4 5 7. Is there any foam in the stormwater discharge? Yeso 8. Is there an oil sheen in the stormwater discharge? Yes �f 9. Is there evidence of erosion or deposition at the outfall? Yes 653) 10. Other Obvious Indicators of Stormwater Pollution: List and describe Ikon e Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SM-242, Last modified 10/25/2012 �, c a