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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20170811STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. DOC TYPE ❑ FINAL PERMIT K MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER ❑ Q ok-) • D% • �t DOC DATE YYYY M M D D August 8, 2017 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: RECEIVED 45� 11 2017 CENTRAL FILES DWR SECTION 3kATI P.O. Box 5030 2020 Ashcraft Avenue Monroe, NC 28111-5030 Phone: (704) 2894511 Fax: (704)290-5194 Email: Joe. Hinkle@atimetals.com Attached, please find stoiniwale;i inuuiluiing data foi Petinil No NCS000330. The origiiials and one copy are included. The monitoring data is for the following monitoring schedule-, Monitonng Period Sample Number I Start End Year 8 — Period 2 16 1 March 1, 2017 1 August 31, 2017 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, q0 (L t.4jL JoHinkle FHS Manager AllV fiATI Allvac Storinwater Monitoring ke-port Form Sample Date: 2-/7-17 Sample Time: 7" c 0 40M Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods SLo-nnwater Discharge Outfall #2 Drainage Area = 272,590sg. ft. = 6.25 acres % linpervious = 36% Parameter Results (mg/1) Benchmark Values (mg/1) BOD "a 6.9 30 COD lag 120 TSS 6. 100 0.001 Cadmium A/40 Chromium, total recoverable 0,6107 1 Lead, total recoverable AJD 0.03 Nickel, total recoverable 0 0 7 1/3 0.26 Zinc, total recoverable 0 - LIS � 0 0.067 Oil tuid Gicase NO 30 pH 7.3 (std units) 6-9 (std units) Storm Date: -7-/ 7-.1 *7 StormDuration: 0-7-4 (1-Irs.) Inches of Rainfall: 0-aO Duration of "e preceding rain event exceeding 0.1": / 6 0 Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x,64) +.9 x inches rain/12inches/ft. x 6.25 x.36) Q(Total, efs) =.1333 x -. 0 -,� C (Inches of rain) +.1688 x 6-;La (Inches of rain) �� 7 ® O tD A Ci. oil � � lh o 9 r m c 1 rj y M rt y y cr �. C froD O arm O p, � ►dip f�D rt M rD �' Yl o C p TJ O C a � w cm 8 R. G M rt 1A tz y aro C rt 1�py( C CL hod cr A n , M � � N d Wig o off' 'ti a� C e b K o a�. As V C CD a .6 A ~ Odd y A 'qm AT ,AA NEDENR St®rmwater Discharge ®utfall (SD®) Qualitative Monitoring Deport 11oi guidunce on filling out this fbi tit, pleuse visit: lily://jjui L d.ucdenu .ui g/web/wq/ws/su/npdessw#tab-4 Permit No.: N/( /.�/ (7/ C / C7/* /. / Cy/ or Certificate of Coverage No.: NXAi/_/_/_/_/_/_/ Facility Name: County: Inspector: Date of Inspection: % - oZ. 3 — 17 Time of Inspection: 6 : 3.5 OgM Total Event Precipitation (inches): /- 90 Phone No. _70 y- cZ $9' - 1f.51 Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) �es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatur , I certify that thi report is accurate and complete to the best of my knowledge: 6� 1. Outfall Description: Outfall No. L Structure (pipe, ditch, etc.) Receiving Stream: al cr- - — C Describe the industrial activities that occur within the outfall drainage area: /71G3�/�� !Gn,.,-fjA, 2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: //"QA �r'4 CA 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _ /t/'OAle 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 :3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 i. Is there any foam in the stormwater discharge? Yes o 0. Is there an oil sheen in the stormwater discharge? Yes de 9. Is there evidence of erosion or deposition at the outfall? es,> No 10. Other Obvious Indicators of Storinwater Pollution: List and describe J0P9'1 d F o ewe A0 be - Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Ferr pui�lnrtre oi� �illi�i alit this Fu r►, pleaw visit U Up://11ot Uil,twdtiutot g/wet)/VVti/w V's.U/11i1du' V#wb2- Pei inft Nu.. ui Cei bfic.ale of Cuvei age Nu.: Facility Name: County: Inspector:Z M Date of Inspection: 7 - of 3 — / 7 Time of Inspection: 6 : Y3 am 'total Event Precipitation((inches):. 1. 9 0 i Phone No. -7 0 -V — �2 99 - Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be pei fui hied dui ing a "i epi eseiaduve slui in eveiil" or during i "Ineasui eable slue in evenU' However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatur9/1 certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. W 0 Structure (pipe, ditch, etc.) Receiving Stream: r' h Ards 0,0 Cc - Describe the industr`a] activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: ^,Tz;� jFi^A 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): __/Vdlye 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Z 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Storinwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. 'These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 'j NCDENR Stormwater Discharge ®utfall (SD®) Qualitative Monitoring Report For guidance on filling out this form, please visit• hHp;(�/p Pei iriil No.. N/C/S/ P/ QI 3/3/ -C/ ui Cei lific.ale of Coverage No.: Facility Name: / c- County: LfA.1('©A." Phone No. Inspector: —1 r4/1?es cts !�2 Date of Inspection: 7- a 3 - / 7 Time of Inspection: 6 : Y C/fog M Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). QualiLaiivu irioiriloriug requirmtienb; vary. Motif periniLs require qualitative monitoring to be peiforiried during a "iepreseiilalive Aoiin eveiil" of during a "ineasuiedble slorin evens." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ...............__.................................................................................._................................_.........__............._......................._.................................................._..........................._................................................................................................................_._.._..._.--- By this signature/I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. W 03 Structure (pipe, ditch, etc.) ® 1 __ Receiving Stream: i G Nr t®A-1 Describe the industrial activities that occur 2. Color: Describe the color of the discharge (light, medium, dark) as descriptors: OWdt` outfall drainage area: basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.):.Al45,.�,E' 4. Clardy: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy° 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (0 3 4 5 i. Is there any foam in the stormwater discharge? Yes o B. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe _/ lolyeq Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 ALTT`�-YAA NCDENR St®rmwater Discharge ®utfall (SD®) Qualitative Monitoring Report Horguidance on filling out this form, please visit. http_/,/portal.ncdenr.off/wQ,(w5(5u,(nPd.e5 vy#tab-4 Permit No.: N/C/ Facility Name: County: (f1y D/Q1 O/3/9/ P1 or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ TX IVIVA c Inspector: _sAM6S / Jr (0-545 G Date of Inspection: .23 177 Time of Inspection: 7 : O Phone No. ,_704/- Total Event Precipitation (inches): D " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event"or "ineusuleuble storm event"(requirements vuty, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." IIowever, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, certify that this re ort is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. 3 W D Structure (pipe, ditch, etc.) %6 lall C Receiving Stream: f G Ar Sn Cr Describe the industrial activities that occur within the outfall drainage area: IDAdiAI[A S IT rva;cf'a ✓YID % cC 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: �04dia�43row,,y 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): lV ayVi! 4. Clarity: Choose the number which hest describes (lie clarity of the discharge, where 1 is clear and 5 is very cloudy. 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yes (J B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes o 10. Other Obvious Indicators of Stormwater Pollution: List and describe WON Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 A'Tt"A'A NCDENR St®rmwater Discharge ®utfall (SDD) Qualitative Monitoring Report Forguidance on tilling out this form, please visit. htt_P://pQrtal,ncdenr.Qrg/web/wq/ws/�u/npdessw#ltabA Permit No.: N/C/J/D/0/9/-1/3/ O/ or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ Facility Name: A T Z A /l ✓A G County: _ Inspector: 1Nr'oA✓ _ Phone No. 70 5/- oL$Q- Y5 /l Date of Inspection: 7 - of 3 - / 7 Time of Inspection: 6 : 30 aM Total Event Precipitation (inches): / - 9 D " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) [q"Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." Ilowever, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I Sgrtify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. (.� StructL (pipe, ditch, etc.) Receiving Stream: ��I'C- k tPrCS.eIGP'EE�C Describe the industrial activities that occur within the outfall drainage area: ,!�%fM1 4&22 s' f r" 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors:. zWedivr.-, 42r"awW 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _/t oA.,4 4. Clarity: Choose the number which best describes the clarity of the discharge, where "1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 7. 8. 9. 10. Is there any foam in the stormwater discharge? 4 5 Yes o Is there an oil sheen in the stormwater discharge? Yes o Is there evidence of erosion or deposition at the outfall? Yes Other Obvious Indicators of Stormwater Pollution: No List and describe el o c -49 RAC ,6� Any ,6 e e l f Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 AL7vt�"A` NCDENR Stormwater Discharge ®utfall (SD®) Qualitative Monitoring Report Yorguidance on filling out this form, please visit. hhtt pd//n r al n dent orp-/w wq/wsjsu npdessw#tab-4 Permit No.: N/C/„6/-0/O/V/3_ /3/Q/ or Certificate of Coverage No.: IV Facility Name: County: 0. Inspector: f r1o:jeEg Date of Inspection: T -d? 3 -17 Time of Inspection: (" :.S 6 OQM Phone No. 1041- cUq- 4,/s11 tl Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Y"Y"es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit. Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable sturin event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative stoma event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatu T, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: 1 / Outfall No. '5W 0 6 Structure (pipe, ditch, etc.) Receiving Stream: - Describe the industrial activities that occur within the outfall drainage area: ' YYl c`�R l {� ro9 0► c .�J,�-,� i" h �bf/ ®d�� 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /r e+A-- bre5 A., 3. Odor: Describe any distinct odors that Lhe discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4. Clarity: Choose the number which best describes the clarigr of the discharge, Where 1 is clear acid 5 is very cloudy: 1 Q 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes o B. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? Yes ) 10. Other Obvious Indicators of stormwater Pollution: List and describe WOA14F Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Allvac - Monroe Plant 'AI 1ivac Stormwater Monitoring, Deport Form r3 ,IL. 1. , .�. 1'. v= Person Collecting Samples: Analytical Techniques and Methods: Results of Sample Analysis: Stormwater Discharge Outfall #2 Drainage area = 272.590sg. ft. = 6.25 acres % impervious = 36% Parameter Results ( g/1) Benchmark values ( gll) BOO 30 COD 120 TSS 100 Cadmium 0.001 Chromium, total recoverable 1- Lead, total recoverable 0.03 0.26 Nickel, total recoverable a 7 Zinc, total recoverable Oil and Grease 0.067 30 pH 7. 3 (std units) 6-9 (std units) Duration of time preceding L 3 exceeding i ?�} r - I Q—CIA Q(Total) = Q(Pervious Area) + Q(Impervious Area.) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x ,64) + .9 x inches rain/12inches/fi. x 6.25 x .36) Q(Total, cfs) = .1333 x ®o (inches of rain) + .16$8 (Inches of rain) _ 0.060 cfs im 0 c o ro o o ro Forguidance on fllling out this form, please visit. httl2:1/portal.ncdenr.org/weblwg/ws/su,/nl2dessw#Lab-4 Permit No.: N/C/,�/ ®/ �/ ®/�3/.3/ ®/ or Certificate of Coverage No.: N Facility Name: County: Inspector: „yam Date of Inspection: '7 ® aq 3 — / 7 Time of inspection: 4 :.3 -6 AM Total Event Precipitation (inches): 1 a 7 ® ° r Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). .._........._._...._..-_._____..__.____ Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be i performed during a "representative storm event" or during a "measureable storm event" However, some permits do not have this requirement. Please refer to these definitions, if applicable. I A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall I and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the " permitted site outfall. The previous measurable storm event must have been at least 72 hours 1 prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter j interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office By this signature, I certify that thi report is accurate and complete to the best of my knowledge: t'• 1. Outfall Description: Outfall No. W 0 1 Structure (pipe, ditch, etc.) Receiving Stream: v ® c Describe the industrial activities that occur within the outfall drainage area: e 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: h t �'r",q LA 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): yowe 4. Clarity: Choose the dumber which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy- 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 h. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes o 8. Is there an oil sheen in the stormwater discharge? Yes o 9: Is there evidence of erosion or deposition at the outfall? y = No 10. Other Obvious Indicators of Stormwater Pollution: List and describe SOM I�- dre-d. Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 V. Forguidance on filling out this form, please visit,- http=J/portal,ncdCnr.orgJweb/wq/ws/su/nndessw#tab-4 Permit No.: IC/-,' Facility Name: A County: Inspector: Date of Inspection: Time of Inspection: 7- 23 `17 6 : q3 or Certificate of Coverage No.: N/C/fi/_/_/_/_/_/_/ Total Event Precipitation (inches): 1. 9 0 " Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature,/I certify that thi§ report is accurate and complete to the best of my knowledge: 1. Outfall Description. Outfall No. ILL9 -0& Structure (pipe, ditch, etc. Receiving Stream: i A SQA2 Describe the industrial activities that occur within the outfall drainage area: 2. Color; Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: tj 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): AAO 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy- 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 4 5 7. Is there any foam in the stormwater discharge? Yes 8. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the out fall? Yes 10. Other Obvious Indicators of Stormwater (pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/2S/2012 For guidance on filling out this form, please visit.: htm:Ilportal.ncdenr.org/eb w ws s u !nndessw#tab-4 Permit No.: or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ Facility Name: A County: I-1-1 I Inspector: ---S6.5 f r l 0-5 957 Date of Inspection: 7 - a 3 m / 7 Time of Inspection: 6 : Y .aM Total Event Precipitation (inches): / a f i Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ...... ... ... ...... _... --...-...__............_..................._..................... . Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatureri certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: ®utfall No. W Structure (pipe, ditch, etc. Receiving Stream: Describe the industrial activities that occur within the 2. Color: Describe the color of the discharge (light, medium, dark) as descriptors: ` basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): �.•e.✓�' 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 h. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 i. Is there any foam in the stormwater discharge? Yes o 8. Is there an oil sheen in the stormwater discharge? Yes o 9, Is there evidence of erosion or deposition at the out fall? Yes 60 10. Other Obvious Indicators of Stormwater Pollution. - List and describe NOW OWE Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 r Norguidance on filling out this form, please visit: http://portal.ncdenr.org/web/wg/ws/su/nndessw#tab-4 Permit No.: N/C/, Facility Name: r County: (flv or Certificate of Coverage No.: 7-x /qll L.-*C, Inspector: --I A M 6S f f (CZ5 C Date of Inspection: 7 —f 7 Time of Inspection: 7 ® O Y pin Phone No. %O Total Event Precipitation (inches): _/ , tl Was this a `Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Yes ❑ No Please verify whether Qualitative. Monitoring must he performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requireineiils vary. MoA permits require qualitative monitoring to be performed during d "re},resenlalive slorin event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, certify that this report is accurate and complete to the best of my knowledge: r 1. Outfall Description: Outfall No. ® Structure (pipe, ditch, etc.) / Receiving Stream: LW t G Describe the industrial activities that occur within the outfall drainage area: /0` -el< MA4 i;yim , t�(?1�e;c�® e'3 s-IA/ 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /roLjjw 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): AlQ&o` 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 i. Is there any foam in the stormwater discharge? Yes o 8. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the uulfailV Yes c 10. Other Obvious Indicators of Stormwater Pollution: List and describe W61V Dote: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. SWU-242, Last modified 10/25/2012 Page 2 of 2 I Forguftlance un filling out this form, please visit. http://12ortal.ncdenr.org/web/wQ/ws/su/npdessw#tab-4 Permit No.: N/C//®//®// 3/ / or Certificate of Coverage No.: Facility Name: ✓A G County: _ Inspector: Date of Inspection: 7 - - / 7 Time of Inspection: 6.30PM Total Event Precipitation (inches): /: q 0 °, Pho Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 2"'Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative moidLoi ing requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I c ify that this report is accurate and complete to the best of my knowledge: ec- /9 l-7 1. Outfall Description: Outfall No. 5 W C Structu e (pipe, ditch, etc.) Receiving Stream: s' 0'j r Describe the industrial activities that occur within the outfall drainage area: K-% 9® e^go 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: Por of -W 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): _A1 4. Clarity: Choose the number which best describes the clarity of the dischai ge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1QJ 3 4 5 7. Is there any foam in the stormwater discharge? Yes o 8. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? e No 10. Other Obvious Indicators of Stormwater Pollutions List • • • ` d'ues As,* G r/ i fir; Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 Forguidunce on filling out this form, please visit. http://12ortal.ncdenr.org/web/wq/ws/su./npdessw#tab-4 Permit No.: N/C/,1/-0/d/, Facility Name:t County: vsl✓s �� Inspector. Date of Inspection: Time of Inspection: 6 or Certificate of Coverage No.: Total Event Precipitation (inches): a 9 0 " Phone No. Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Eg"'Y'es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatur , I certify that this report is accurate and complete to the best of my knowledge: a 1. Outfall Description: 11 Outfall No. -5W 0 6 Structure (pipe, ditch, etc.) lTi Receiving Stream: Rl '-h14 4,0,1.r Describe the industrial activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: rT/� brows 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): d&AW 4. Clal•Ity: Choose Lhe number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 i. Is there any foam in the stormwater discharge? Yes 0. Is there an oil sheen in the stormwater discharge? Yes o 9. Is there evidence of erosion or deposition at the outfall? Yes c 10. Other Obvious Indicators of S'tormwater Pollution: List and describe VAI on sneen, or erosion/cleposition rinay be indicative of pollutant exposure. These conditionsinvestigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 a� acmnalXical www.pacelabs.com July 27, 2017 Mr. Joe Hinkle Allvac FEE. PiojecL Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applluable, unless utlleiwlse limed lit llte putty ur tiie iepurL. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)870-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnaIXical www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs ???5 Riverside [hive, Asheville, NO ?8804 f Inrida/NLLFU' (: ertifis,ntien tt: L-.8 /(:i48 Ma66atlweeUe co,tinoallun #: M NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #• 40 SMIth Cflrolina Certification M: 090,.t0001 Vlrginla/VELAh CertincaLlon #. 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 { aceAnalytical wwwpacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 Lab ID Sample ID 92348113001 MSW 02 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory EPA 1664E JMS 1 PASI-C EPA200.7 SER 5 PASI-A SM 2540D NAL 1 PASI-A SM 5210B ECH 1 PASI-A SM 5220D NAL 1 PASI A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 b Pace Analytical Services, LLC aceAna/ytical ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92348113 Sample: MSW 02 Lab ID: 92348113001 Collected: 07/17/17 07:00 Received: 07/18/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ Field Data Analytical Method: Collected By JM 1 07/17/17 07:02 Field lemperature 28.3 deg (: (1 110 1 U//11/17 (11-0? HFM, CAl and Crease Analytical Method. FPA 1604B Oil and oleaml ND ing/L 6.0 1 01/2b/1106.08 200 7 MFT ICP Analytical Method- l-PA?00 1 Preparation Method: FNA?00.1 Cadmium ND ug/L 1.0 1 07/19/17 15:30 07/23/17 08:14 7440-43-9 Chromium 10.7 ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-47-3 Lead ND ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7439-92-1 Nickel 74.8 ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-02-0 Zinc 459 ug/L 10.0 1 07/19/17 15:30 07/23/17 08:14 7440-66-6 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 26.2 mg/L 8.3 1 07/19/17 18:17 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 26.9 mg/L 2.0 1 07/19/17 06:30 07/24/17 09:13 D6 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 124 mg/L 25.0 1 07/20/1720:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 .g oo aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 370347 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92348113001 METHOD BLANK: 2052116 Matrix: Water Associated Lab Samples: 92348113001 Blank Reporling Parameter units Result Limit Analyzod Quullflurs Oil and Grease mg/L NU 5.0 0//25/17 06:07 LABORATORY CONTROL SAMPLE: 2052117 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 2052118 92348428001 Spike MS MS % Rec Praliarnctur Units Result Colic. Result % Rec Limits Ouall(Iers Oil and Grease mg/L ND 40 38.0 95 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical wwvw.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369581 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92348113001 METHOD BLANK: 2047905 Matrix: Water Associated Lab Samples: 02348113001 Blank Reporting Parameter (Inita ItoeLilt limit Annlyzod Cadrriluin ug/L ND 1.0 O7/23/17 07.03 Chromium ug/L ND 5.0 07/23/1707:03 Lead ug/L ND 6.0 07/23/ 17 07.03 Nickel tag/L ND 5.0 07/23/17 07:03 Zinc ug/L ND 10.0 07/23/17 07:03 01.11711ifiom A Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2047906 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 478 96 85-115 Chromium ug/L 500 470 94 85-115 Lead ug/L 500 468 94 85-115 Nickel ug/L 500 468 94 85-115 Zinc ug/L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047907 2047908 MS MSD 92347968019 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 482 471 96 94 70-130 2 Chromium ug/L NO 500 500 493 464 99 93 70-130 6 Lead ug/L ND 500 500 494 459 99 92 70-130 7 Niol(ol tlg/( ND b(1() b00 414 4(V 0b ()Y IO 1:i0 a Zinc ug/L ND 500 500 499 463 100 92. 70-130 8 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047909 2047910 MS MSD 92347941003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 453 465 91 93 70-130 2 Chromium ug/L ND 500 500 447 458 89 92 70-130 2 Lead ug/L ND 500 500 441 450 88 90 70-130 2 Nickel ug/L ND 500 500 442 453 88 90 70-130 2 Zinc ug/L ND 500 500 451 461 90 92 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 6 r aceAnaIX cal twiw.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369720 QC Batch Method: SM 2540D Associated Lab Samples: 92348113001 METHOD BLANK: 2048785 Associated Lab Samples: 92348113001 Parameter Unite 'futal Suspended Sulids ing/L LABUkA1 UPY CON I kOL SAMPLE: 2048786 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2048787 rt iameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2048788 Parameter Units Total Suspended Solids mg/L QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Dlank Reporting Rocult Limit Analyzed Qualifiers ND 2..5 07/19/17 -I8" 14 Spike LCS Conc. Result 250 248 92348128001 Dup Result Result ND NO 92348118001 Dup Result Result ND NO Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LCS % Rec % Rec Limits Qualifiers 99 90-110 f�('U Qualifiers RPD Qualifiers Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, L.L.C. Page 7 of 14 aceAnalXical www.pacelabs.com A Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369591 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92348113001 METHOD BLANK: 2047932 Associated Lab Samples: 02348113001 rarameter Unit, BOD, 5 day Ing/L LABORATORY CONTROL SAMPLE: 2047933 Parameter Units BOD, 5 day mg/L SAMPLE DUPLICATE: 2047934 Parameter Units BOD, 5 day mg/L 0 Matrix: Water Rlank Reportin0 ROMA I imit Anelyrod QLVI[ifiers ND 2.0 07/24/ 17 00.13 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 197 99 84.6-115.4 92348113001 Dup Result Result RPD Qualifiers 26.9 35.3 27 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 kd a aceAnalj6cal www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369924 QC Batch Method: SM 5220D Associated Lab Samples: 92348113001 METHOD BLANK: 2049917 Associated Lab Samples: 92348113001 Poromotor Units Chernlcal Oxygen Demand trig/L LABORATORY CONTROL SAMPLE: 20499,18 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Dlank Reporting Result Limit Analyre.d Qualifiers ND 25.0 011201-1120:39 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 773 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049919 2049920 MS MSD 92347277007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 31.0 750 750 813 808 104 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049921 2049922 MS MSD 92348319001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 642 750 750 1380 1360 98 96 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 9of14 Pace Analytical Services, LLC Kincey Ave. te 100 aceAnalytical � 9800Hunte sville, NC�28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: Monroe Stormwater Pace Project No.: 92348113 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Ouantitation Limit. RL - Reporting Limit. S - Surrogate 1,2 Diphonylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Ulean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services - Aslieviile PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The prooision between tho samplo and samplo duplicate exceeded laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 F aceAnaIXical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 I luntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92348113001 MSW 02 92348113001 MSW 02 EPA 1664B 370347 92348113001 MSW 02 EPA200.7 369581 FPA2007 37008.2 92348113001 MSW 02 SM 2640D 360720 92348113001 M8W 02 SM 5210E 369591 SM b210b 369608 02349113001 MSW 03 SM 5220D 360024 Date: 07/27/2017 05:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 a / aceAnalXical Laboratory receiving samples: Asheville ❑ Eden[—] Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: issuing Authority: F-CAR-CS•033-Rev.01 Pace Quality Office Greenwood ❑ HuntersvillieQom° Raleigh❑ Mechanicsville❑ Client Name: WO# 1 13 A923TV �j,T..�- Project #: • 'Courier: ❑Client []Fed Ex ❑UPS ❑LISPS Commercial r OPace ❑Other: 92348113 Custody Seal Present? ❑Yes QNo Seals intact? ❑Yes QNo Date/Initials Person Examining Contents: ii 7 7 I Packing Material: ❑Rubble Wrap ❑Bubble Bags [-]None QOther•�n(e C, Thermometer: �_- •- 'El IR Gun ID; -UQ '- - Type of Ieec aWet ❑Blue ❑None -[-]Samples on Ice, cooling process has begun Currectlon Factor: CoolerYampCorrected ('C)i. _- Biological flssue Frozen ❑Yes ❑Nv- ❑N/A Temp should be above freezing to 6*C USDA Regulated Soil ( [ --f •N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, nyes I71No' includine Hawaii and Puerto Rico)? I-lYes--..[-1No--- Comments/Discrepancy: Chain of Custody Present? --[-3Yes (_jNo E JN/A 1. Samples Arrived within Hold Time? EaYl?s [)No ❑N/A 2, Short Hold Time Analysis (<72 hr.)? _QYes []NO ❑N/A 3, Rush Turn Around Time Requested? Dyes J<No ❑N/A 4. SuffidontVolume?' ,[DI es []NO ❑N/A S. Correct Containers Used? -Pace Containers Used? (Yes eyes ❑No []No []NIA ❑N/A 6. Containers Intact? .ales []No ❑N/A 7. Samples field Filtered? ❑Yes ©go ❑N/A 8. Note if sediment is visible in the dissolved container . Sample Labels Match COC? -includes Date/Time/ID/Analysis -Dyes Matrix: \ i ❑No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? []Yes ❑No _.QN?K 10, Trip Blank Present? Trip Wnk Custody SOS Present? Des C-IYes ❑No ( vlNa DkIA n-t0 : 11. CIIENT NOTIFICATION/RESOLUTION Person Contacted: Comment;/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Field D3t2 Required? ❑Yet []No Date/Time: Rate: Date: Cl Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 12 of 14 Document Name: Document Revised: Sept. 21, 2016 ace _ Analytical Sample Condition Upon Receipt(SCUR) Page 2 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace quality Office *Check mark top half of box if pH and/or dechlorination Project # �� 2348 113 is verified and within the acceptance range for preservation samples. PM: MWB Due Date: 07/27/17 **Bottom half of box is to list number of bottles CLIENT: 92-A1lvae NC ^ a ^ x Z N y a ? ¢ ? Q Z \ Z A `—° ( n m r-1 A = 'O � a y x z a 2 z _ a '� z � Q a ,� :2 M z L1 O v a N H H d N d. di O }SLn G M ,M U a ,`,. c N L7 °N' n V x a vi � g a. d, `f .gU F ¢ k m 6 a z z Uer Y Ln z u 2 H N j C) > > •� (Cvry'y - i'u'a.�i�i 14i Fi U i� fQQ� t' 4 n,�i u U Ln �3-, 0 o' E E AC a 0 P to o u > > > > to w a a a a cna Z N a lJ a W. i7 T l7 iM7 Vt i? a tM 2 0 r (D C7 'G. C7 !G O SC f: a F: a a v� z CO CO m m m MM. CO m m 3 a a a a a a o>NN > 1 I 2 H\ 3 � - 4 I 5 6 \\N 7 N\N 1'* \N\N N\\ 9 N N\N \N 1p 11 \ 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot fi Page 13 of 14 w } pelul saldweS 4 .cc y / • w... U O O ' (NIA) Y tY _ Z v r _ CO z = r d r o pp U p u Jaloo0 paleas Rpolsn0 oLO L. L o a N >. (NIA) 001 �''` uo Panla38a w CU (N/%) BulJONO lenpisa�jo. o C�1 ul dwal aZ } 0 V. 1>1 - w r�l o } r o o ti w N 3. to 5-5 i cr t w u t ;sal sjSAjeuyt .� J9410 n°w LU Joue419N tOZSBEN a ) �1 @ HOeN q IOH 5 � � CD _ 'UNH 5< yC rOS H Panjesaddu0 �t X _ a 0 o o ' E Sa3NIV1N00 d0 # "� ... .. u 'o e ` E o = _ `` N0I10911001V dW3131dl'WS rV! Op w w a a_ J J QM IL Z w qo 4 ~ a N N V! h I ° O O _m G w cr p o oz W w t 1 t t t 1 w z F r a p F o a t t t 1 V X t� ........... ... O LL ryK IL � ,Q�x •' .- e c d a z ` (dW00=0 M16=9) 3dA131dWVS %b Alb V 0 1 z -a a � ul (p9j0)saP03Ppena8s) BaOC)XIid1VW m 0.0 m d 0 Lod F F m Z Z 3�--�.a����LtD:rnF- l� z !A K K U ('. 0 a o CL a 3 � � C .0 O d�t o3 ac9C) E0 r" .r w J w D Cf g � Q _ �, k ❑ Z V o � co Z oc- d m .J rn H 0. O } O r IEQ& C) _ Q L) p t 9 c E C9t ��\ �y y v 0 FO- I Pa e 14 of 14 # W311 N M 3 aceAnalytical www.pacelabs.com July 27, 2017 Mr. Joe Hinkle Allvac RF project: Monrue Sturrrlwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicabla, unless otherwise nuted in the burly u'r Lho rupurt. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainardLpacelabs.com (704)875-9092 Plujeut Managed Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 k acmnalytical www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/N€L.AP Ceitiflualiun #: E87618 MaRSachUg0. t4 Certification #- M-N('030 North Omoliur Dihiklntl Watei (e-ItlM oLlon # ITT 12 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina WaMewaler Certificaliul1 #. 40 South Carolina Cei tiflcatloii #: 00030001 Virginia/VFL AP Certification # 460222 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 Pace Analytical Services, LLC ® aceAnalXical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: Monroe Stormwater Pace Project No.: 92348113 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92348113001 MSW 02 EPA 1664B JMS 1 PASI-C EPA 200.7 SER 5 PASI-A SM 2540D NAL 1 PASI-A SM 521011 ECM 1 PASI-A SM 5220D NAL I PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 acmnalytical wtw.pacelabs.com ANALYTICAL RESULTS Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MSW 02 Lab ID: 92348113001 Collected: 07/17/17 07:00 Received: 07/18/17 11:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ Field Data Collected By Field Temperature HEM, Oil and Groaso Oil and Grease 200.7 MET ICP Cadmium Chromium Lead Nickel Zinc 2540D Total Suspended Solids Total Suspended Solids 5210E BOD, 5 day BOD, 5 day 5220D COD Chemical Oxygen Demand Date: 07/27/2017 05:03 PM Analytical Method: JM 1 07/17/17 07:02 28.3 deg C 0.60 1 07/17/17 07:02 Analytical Method: LPA 1664B NO m0/1 50 1 07/25/17 06-08 Analytical Method: EPA200.7 Preparation Method: EPA200.7 ND ug/L 1.0 1 07/19/17 15:30 07/23/17 08:14 7440-43-9 10.7 ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-47-3 ND ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7439-92-1 74.8 ug/L 5.0 1 07/19/17 15:30 07/23/17 08:14 7440-02-0 459 ug/L 10.0 1 07/19/17 15:30 07/23/17 08:14 7440-66-6 Analytical Method: SM 2540D 26.2 mg/L 8.3 1 07/19/1718:17 Analytical Method: SM 6210B 26.9 mg/L 2.0 1 07/19/17 06:30 07/24/17 09:13 Analytical Method: SM 5220D 124 mg/L 25.0 1 07/20/17 20:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D6 Page 4 of 14 acmnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 370347 Analysis Method: EPA 1664E QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92348113001 METI IOD DLANK: 2052116 Matrix. Water Associated Lab Samples: 92348113001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Groaso — rrl[j/l ND 5.0 07/25/17 06.07 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LAUORATORY CONTROL SAMPLE. Parameter 2052117 Units Spike LCS Conc. Result LCS % Rec % Rec Limits Qualifiers Oil and Grease mg/L 40 36.8 92 78-114 MATRIX SPIKE SAMPLE: 2052118 92348428001 Spike MS MS % Rec Parameter Units Result Conc Result % Rec t imits (lualifierF Oil and Grease mg/L ND 40 38.0 95 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 369581 QC Batch Method: EPA 200.7 Associated Lab Samples: 92348113001 Analysis Method: Analysis Description: EPA 200.7 200.7 MET METHOD BLANK: 2047905 Matrix: Water Associated Lab Samples: 92348113001 Blank Repulling Parameter Units Result t unit Analyied Qualifier, Cadmium ug/L NU 1.0 01/23/1101:03 Chiorriium up/L NO 6.0 07/23/1707.03 lead ug/t_ NU 5.0 01/23/1101:03 Nickel ug/L ND 5.0 07/23/17 07:03 Zinc ug/L NO 10.0 07/23/17 07:03 LABORATORY CONTROL SAMPLE: 2047906 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 478 96 85-115 Chromium ug/L 600 470 94 85115 Lead ug/L 500 468 94 85-115 Nickel ug/L 500 468 94 85-115 Zinc ug/L 500 476 95 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047907 2047908 MS MSD 92347968019 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 482 471 96 94 70-130 2 Chromium ug/L ND 500 500 493 464 99 93 70-130 6 Lead ug/L ND 500 500 494 459 99 92 70-130 7 Nlt:ke:l u(1/t ND 500 500 474 462 1)F 02 70.1,0 3 Zinc ug/L ND 500 50U 400 463 100 92 70-130 8 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2047909 2047910 MS MSD 92347941003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 453 465 91 93 70-130 2 Chromium ug/L ND 500 500 447 458 89 92 70-130 2 Lead ug/L ND 500 500 441 450 88 90 70-130 2 Nickel ug/L ND 500 500 442 453 88 90 70-130 2 Zinc ug/L ND 500 500 451 461 90 92 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 14 d aceAnalj6cal www.pacelabs.com QUALITY CONTROL DATA Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369720 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92348113001 METHOD BLANK: 2048785 Matrix: Water Associated Lab Samples: 92348113001 Blank Reporting Parameter - Units Result Limit Analyzed Qualifiers Total Susponded Sollda mg/1 NU 2.b 0//10/1118:14 LABURAIURY CON I ROL SAMPLL. 2048/86 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2048787 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2048788 Parameter Units Total Suspended Solids mg/L Spike LCS LCS Conc. Result % Rec 250 248 99 92348128001 Dup Result Result ND ND 92348118001 Dup Result Result ND ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 % Rec Limits Qualifiers 90-110 RPD Qualifiers RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 acmnalytical o www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369591 QC Batch Method: SM 5210B Associated Lab Samples: 92348113001 METHOD BLANK: 2047932 Associated Lab Samples: 92348113001 Parameter Units, HOD, h day m0/t LABORATORY CONTROL SAMPLE: 2047933 Parameter Units BOD, 5 day mg/L SAMPLE DUPLICATE: 2047934 Parameter Units BOD, 5 day mg/L QUALITY CONTROL DATA Analysis Method: SM 5210B Analysis Description: 5210E BOD, 5 day Matrix: Water Blank RepoiLing RP.Slllt limit Analyzed NU 20 01124/1109.13 Qualifiers a Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 197 99 84.6-115.4 92348113001 Dup Result Result RPD Qualifiers 26.9 35.3 27 D6 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 14 R acMnalj4ical www.pacelabs.com Project: Monroe Stormwater Pace Project No.: 92348113 QC Batch: 369924 QC Batch Method: SM 5220D Associated Lab Samples: 92348113001 METHOD BLANK: 2049917 Associated Lab Samples: 92348113001 Parwneter Unitc Chemical Oxyyun Durnund rnq/L I A130RATORY CONTROI ` AMPI E• 2040018 Parameter Units Chemical Oxygen Demand mg/L Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix Water Blank Reporting Result Limit Analyzed Qualifiers Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 750 773 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049919 2049920 MS MSD 92347277007 Spike Spike MS MSD MS MSD % Rec I'artameter Units Result Colic. Cuuu. Result Result % Rec % Rec Limits kNU Qual Chemical Oxygen Demand mg/L 31.0 750 750 813 808 104 104 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2049921 2049922 MS MSD 92348319001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 642 750 v750 1380 1360 98 96 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 91 aceAnalytical www.pacelabs.com QUALIFIERS Project: Monroe Stormwater Pace Project No.: 92348113 DEFINITIONS Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. POL- Practical Quantltation Limit. RL - Reporting Limit. S - Surroqate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene usinq Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANAIYTF C, tIAl IFIFRS U6 the precision between the sample and sample duplicate exceeded laboratory control Ilmlts. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 g Pace Analytical Services, LLC V aceAnalytical ® 9800 KinceyAve. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Monroe Stormwater Pace Project No.: 92348113 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92348113001 MSW 02 92348113001 MSW 02 EPA1664B 370347 92348113001 MSW 02 EPA200.7 369581 EPA200.7 370082 0234811300.1 M6W 02 5M zlb40U 009120 92348113001 MSW 02 SM 5210E 369591 SM 5210B 30R,08 92348113001 MSW 02 SM 52?01) 369924 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/27/2017 05:03 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 14 aceAna1Xica1 Laboratory receiving samples: Asheville ❑ Eden❑ Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.01 Pace Quality Office Greenwood ❑ HuntersvilleE]— Raleigh❑ Mechanicsville[] Client N'�amej:: WO# 923481 13 : Project #: 'Courier: I �. ❑Client ❑Fed Ex []UPS [:]LISPS ❑ Commercial .Pace ❑Other: 92348113 ' 11 Custody Seal Present? ❑Yes QNo Seals Intact? []Yes •- 17No Date/Initials Person Examining Contents:T % 7 Packing Material: ❑Bubble Wrap ❑Bubble Bags [-]None -❑Other:...--7-�� C / Thermometer: ,-,; --`U m Gun ID: �1 43Wet ❑Blue Type of Ice: []None' -Samples on Ice, cooling process has begun Correction rector: Cooler Tetnp C.utre<ded (°C): '2 �L _. -_ .-. _, Blulugical Tissue Frmen? ❑Yea F�No ❑N/A I emp should be above freezing to 6°C USDA Regulated.Soil ([,I,N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, nYes MNo includine Hawaii and Puerto Rico)? I -!Yes-_IrINo-- Comments/Discrepancy: Chain of Custody Present? _..-[jam ❑No ❑N/A 1. Samples Arrived within Hold Time? [DNts [:]No ❑N/A 2. Short !-told Time Analysis (a72 hr.)? _QYhs ❑No ❑N/A 3. Rush Turn Around Time Requested? Sufficient Volume?' Correct Containers Used? -Pace Containers Used? (•-)Yes .[, (es QYes -fires _. Na ]NO ❑No [--]No nN/A N/A ❑N/A [I N/A 4. 5. 6. Containers Intact? QYes ❑No ❑N/A 7. Samples Field Filtered? []Yes 4D90 ❑N/A 8. Note if sediment is visible in the dissolved container •. . Sample Labels Match COC? -Includes Date/Time/ID/Analysis / -QYes Matrix:__ ❑No ❑N/A 9. Headspace in VOA Vials (>5-6mm)? []Yes ❑No --QN%A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes []Yes [-]No []No QW/A ❑DiK 11. CLIENT NOTIFICATION/RESOLUTION Person Contacted: Comment.;/Sample Discrepancy: Project Manager SCURF Review: Project Manager SRF Review: Field Data Required? (Yes nNo Date/Time: Date: i(i;', I I / Date: Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent -to the North Carolina DEHNR Certification Office (Le, Out of hold, incorrect preservative, out of temp, Incorrect containers) Page 12 of 14 Document Name: Document Revised: Sept. 21, 2016 Sample Condition Upon Receipt(SCUR) Page 2 of 2 aceAnalytical Document No.: Issuing Authority: i F-CAR-CS-033-Rev.01 Pace Quality Office *Check mark top half of box if pH and/or dechlorination Project # WO# :�� 113 is verified and within the acceptance range for preservation samples. PM: MWB Due Date: 07/27/17 **Bottom half of box is to list number of bottles CLIENT: 92-A1 lvac NC u 4 v ^ Z v `✓ z v -. n z Z z a v o 2 N cv Z 2 m z of ry rt _ a c z v v a 2 ^� v N Y x z V v x d z Z m �o I a m m v Q � Z G x = a N p, a Z z Q Z O m za o N Q ° j O °Z" ° Z g Ln 2 - jo .Si U u U N N N •_ V1 t) u S C1 .D N .fl 'E S z M F ui 0 c� F I ! o a (� G M n _ o � � .1 �� }Q 6 m tq 0 �n _ _ n`i _ ,� i� G o e g Y, LA mM L rI 0 a a a n a a a a " a l7 a l a C7 a t� a t7 a l7 a t7 o [7 > :5 t7 > , U c w4 > > N a Ln to U11 > c� CO COra CO CD m to CO3 1 N \N t NN 3 4 l NI 1\1\N 5 t \\N1 6 \\N N \N 8 9 10 11 12 --- -- ----- pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lotft Page 13 of 14 (N/A) w Q J ) pelul saldweS _ N % •, Ur O Q aleas Jaloo0 sno z Z o O— F.. 0 D LO w F ❑ O a J w J (polsn0 L L to a >_ (NIA)e0l w uo panlesag 7-1i��9 CZ( (N/A) auijoWO lenplsaa 0• ul dway ❑ i A a i U UJ = O <z Of 0 w '' r�l a L L rt 0 to _ ............. o lu ga y�U. LU Ud kN/ X t asal SISAle(�uf/yt m 1 4 Jau)o Ct w louey)aN EO'eS�eN j HOEN E .9 itil iu ` M m m L ;� w } IOH �C EONH �C V C` 4 rd6zl l paruesaiduN SC u a E OvLu _`,�• 2 a rna m w=¢ U MONNINOO 30 # n N0110311001tl dW313ldtNVS Mr _ r w J w J w 4 pp O a 4 Q0 1• 1 NLu z . a rn a N • _ m N� Z Q a E W z LU � W r z (A) V/ IU o ice' I ' t p w a N Q u b V • F LL Q N ppN F f(1 ui o W 6 E o z a+ Z � (dW00=0 9b@i0=0) UAi 31dWdS V � � � 3000XR11VW a(llalols'pmPlle-as) J m a o m <C = 0 d r co33°'w03<r0 o N Z Z H� JJpp..ff v�r IJ Z sr U a' 0 a o a Mcm c M �? E CE U � k X 3 ``y V n a duo d � Ada V) o3�a�ioai=o O Ic Z w 0 0 _ 'mot. u ❑ z = J LLI m J Irl ri Z CL 0 Q p C v n Q U� n 0 v E ZQ v, Pa e 14 of 14 in 0 a w a # W311