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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20180215STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. o}GS o00 DOC TYPE ❑ FINAL PERMIT )� MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ Zaa • 02 • IS YYYYM M D D February 9, 2018 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: P.O. Box 5030 2020 Ashcraft Avenue Monroe, NC 28111-5030 Phone: (704) 289-4511 Fax: (704) 290-5194 Email: Joe.Hinkle@atimetals.com Attached,, please. find stormwater monitoring data for Permit No NCS000330. The originals anld one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number I Start End Year 9 — Period 1 17 1 September 1, 2017 February 28, 2018 Stornnwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. qe 'erely, Hinkle EHS Manager RECEIVED FEB 15 2U1a OFNTRAL rII.CS DWR SECTIQPJ "0 Allvac - Monroe Plant -0ow-ATI Allvac Stormwater Monitoring Report Form Sample Date: SampleTime: Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analvsis: Stonnwater Discharge Outfall #2 Drainage Area = 272,590sq. ft. = 6.25 acres % Impervious = 36% es M0scr PlILe- 41)�'�zf I Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 120 TSS 100 Cadmium O 0.001 Chromium, total recoverable 1 Lead, total recoverable 0.03 Nickel, total recoverable 0.26 Zinc, total recoverable 0.067 Oil mid Orease 30 PH (std units) 6-9 (std units) Storm Date: Storm Duration: - 4 A (Hrs.) Inches of Rainfall: L'6n Duration of time preceding rain event exceeding 0.1": Mrs.) Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x.64) +.9 x inches rain/12inches/ft. x 6.25 x.36) Q(TotaI,cf§)=.l333x 0, <A (Inches of rain) +.1688 x0,50 (Inches of rain) cfs Q o � odd 0 a � a 0 A � w s° � v v O �• o 4o� b cn � b ILI w w� Oz a o LL C 'O o O °To o O h C 0 0 0 0 0 o � w � ° o " w con w � � o 6 W, T p a CD 0 A A NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Foi guidunce on filling out this foi in, Please visit: I1LLW / jPui taLiicdem.urg/web/wgjws/su jnpdessw#itah-4 Permit No.: N Facility Name: County: �1 Inspector: i Date of Inspection: j - -/Y Time of Inspection: 9`36) AM Total Event Precipitation (inches): Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 0 Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative nonitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event " However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. ............................................................. ........................................................................................................ ......... _...................... ............................ _....................... ........... ..... ............... ........... .................... ......... ........................ ............................................................... .......... -....... _.......... _........................ _..... By this signa re, I certify that this report is accurate and complete to the best of my knowledge: �— 1. Outfall Description- 0 Outfall No. —��� Structure pipe, ditch, etc.) / Receiving Stream: (1 ( 7 Describe the indu,strY activities that occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: h -i ' a l-y a j J 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): fir) A10 4. Clarity: Choose the number which best describes the clarity of the discharge, where! 1 is clear and 5 is very cloudy- 1 4D 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 0 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 (2) 3 4 5 7. Is there any foam in the stormwater discharge? Yes No B. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Lidicatois of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 �� NEDENR St®rmwater Discharge ®utfall (SD®) Qualitative Monitoring Report Forguidance on lillinq out this form, Please visit: http://porttal,ncdenr.org/web/wq/ws/su/npdessw##tab-4 Permit No.: N/C//C/Q/�/,/.�/�/. or Certificate of Coverage No.: Facility Name: County: Z//1 i"1?Q Phone No.�i�9' Inspector: 1 me-s M6-se-r Date of Inspection: Time of Inspection: 8,'l 7,411 Total Event Precipitation (inches): OX Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) l`-' Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). (qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "rrieasureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWO Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall vDeauition: Outfall No. St uctu Receiving Stream: AAf - /'' Describe the industrial activities the z etc.) occur within the outfall drainage area: 2. Color: Describe the color of the dis (light, medium, dark) as descriptors: %/' using basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 1764 e- 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 a 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 0 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes S 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 A4j;A A NCDENR Stormwater Discharge Outtall (SDO) Qualitative Monitoring Report Forguidance on filling out this form, please vi.sit� http_/lnortal:nrdunr,urgublw ws s ln►2dassw#tab 4 r Permit No.: N/C/,,:� j Facility Name: County: Z14 1,0/7 Inspector: Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 0. or CertifCatelof C Phone No. No.: N/C/Q/ / / / / / / Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) 0 Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative inonitoi ing I equii elnents vary. Must pei iiiits i cquii c qualitativc rnonituriiig tube performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. .................. ......................... ......................................._.................................. _........................ .................................................................... .................................. _................................................................... .............................. ............................ _.................... ..................... ........................................................................ By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. C Structu} e (pipe, Receiving Stream: j 6hI r ..Sot-i h, etc..)) iioe / Describe the industrial activities that occur within the outfall r area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: `� A-1) &J a 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Z20/7F 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and S is very cloudy- 1 V 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 @2 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 AL� NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report. Fut guidance on filling out this forut, please visit. liLLW;//poi-tal.iicdeiir.org/web/wq/ws/su/npdossw#tab-4 Permit No.: N/C/,S/ Facility Name: �Q County: Inspector: Date of Inspection: _ Time of Inspection: _ J/1.5/,0/, or Certificate of Coverage No.: Total Event Precipitation (inches): 'p, q6 Phone No. 72) Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) wr Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative tttouitot ittg i equii citiculs vary. Mosl pei ►nits i equiie qualitative mottilot hig Lobe performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee ob. ..............................................................................................._.._..........................._............................................................._.................................................................................................................................................................................................................................................................................... By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Descri tion: Outfall No. so � Receiving Stream: _1 Descri e the industrial ff ctivi, (pipe, ditch, etc.) e, //1 1/c, z )4 C-reeK --1441 that occur within 2. Color: Describe the color of the discharge using b (light, medium, dark) as descriptors: V i r � h"- area: colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /WRe' 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 l_l 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 AQ= NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Fur guidunce un filling out this fur ni, pleuse visit: lily://portal.ncdenr.org/web jwq/ws jsu jnpdessw#Lab -4 Permit No.: N/C Pr Certi[�ale,o['Cover4ge No.: N/(;/G Facility Name: fR i County: /.fir'2 r a/t Phone No. Inspector: .JCL /'1 6 p, 14p S, r Date of Inspection: _4 - 4-19 Time of Inspection: 9 --�4 A14 Total Event Precipitation (inches): 0096, Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) Y`J Yes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). (qualitative monitoring requirernerrts vary. Most perinits require qualitative rnoniloring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1. inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. .. ..... ....... -............................................. _........................... ................................................................................................................................................. .......................................... _................................................... ............................... ............. ........................................... ......... ... .................. ............................................... By this signatyre, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: ,% C Outfall No. truct}�re (pipe, ditch, etc.) �t % "rGA Receiving Stream: ' ✓'Cl 'LIl-eelk Describe the industrial a tivities that oc ur wit in the outfall drainage area: f ® l / D < a Q i n 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: i "T ti 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 17,0A f 4-. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 t„/ 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 0 3 4 5 7. Is there any foam in the stormwater discharge? Yes No 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious liidlcalurs of Storinwater Pollullon: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 NCDENR Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report Foi guidunce on filling out this foi in, pleuse visit: hLLp://poi Lai.iicdem .oi g jweb/wy/ws/su/►1Wdcssw#Lab-4 Permit No.: N/C/s/�)/LI/ Facility Name: 7-s County: ZJ4 I Dil Inspector: _ 1 Am,,, q Date of Inspection: Time of Inspection: .�/1/.6/` or Certifi�ateiof Coverige No.: N Total Event Precipitation (inches): 7 Phone No. 7d V 2,?.YV -"1Si Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) VYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ............................ Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event " However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signatufe, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall No. < Receiving Stream: If (pipe, ditch,,etc.) d 'Iek 2. Color: Describe the color of the discharge u ing basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: %2 l6 it) n 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /'?0/2 if 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy! "1 6) 3 4 5 S. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2� 3 4 5 7. Is there any foam in the stormwater discharge? Yes 49 8. Is there an oil sheen in the stormwater discharge? Yes No 9. Is there evidence of erosion or deposition at the outfall? Yes No 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 W e z aceAnalj4ical o www.pacelabs.com February 01, 2018 Mr. Joe Hinkle Allvac R[-: Project* MUNkOE- 8 I ()RMWAi [-P\ Pace Project No.: 92370463 Pace Analytical Services, LLC 9800 Kincey Ave. Suite loo Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)€375-9092 Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 18 1�;a'ceAnalj4ical' www.pacelabs.com t Project: MONROE STORMWATER Pace Project No.: 92370463 Pace Analytical Services, LLC 9800 KinceyAve. -Suite 100 V Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDS 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #. E87048 Massachusetts; Certification #: WI NC 0'SU North Carolina Drinklna Water Certification #: 3//12 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Vlrglnla/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VLLAI I Certification #: 4OU222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 18 T' p ;ceAnalj&al r www.pacelabs.com t SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: MONROE STORMWATER 92370463 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92370463001 MSW 02 BOD SM 5210B ECH 1 PASI-A 92370463002 MSW 02 COD SM 5220D NAL 1 PASI-A 92370463003 MSW 02 TSS SM 2540D MJP 1 PASI-A 92370463004 MSW 02 MSTALS LPA2UU.l 81-11 5 PASI-A 92370463005 MSW 02 OIL & GREASE FPA 1664H JMS 1 PASI C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 18 aceAnalytical www.pacelabs.com I ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. -Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92370463 Sample: MSW 02 BOD Lab ID: 92370463001 Collected: 01/23/18 01:15 Received: 01/23/18 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method Collected By J.Moser 1 01/24/18 09:42 Collected Date 1123/18 1 01/24/18 09:42 Collected Time 1:25 1 01/24/18 09:42 NI 1 7.4 Sid. Units 0.10 1 01/24/18 09.42 Tcmpomture 1:2.7 deg C 0.50 1 01/24/10 09:42 621(lH HOD, 5 day Analytical Method: 5M 5210N BOD, 5 day 4.8 Ing/L 2.0 1 01/24/18 13:00 01/29/18 10:09 L2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18 aceAnaIX cal www.paWabs.com (f I ANALYTICAL RESULTS Project: MONROE STORMWATER Pace Project No.: 92370463 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MSW 02 COD Lab ID: 92370463002 Collected: 01/23/18 01:16 Received: 01/23/18 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 41.0 mg/L 25.0 .1 01/31/18 20:21 Date: 02/01/2018 06:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 18 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS S Pace Analytical Services, LLC 9800 Kincey Ave. -Suite lo0 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92370463 Sample: MSW 02 TSS Lab ID: 92370463003 Collected: 01/23/18 01:19 Received: 01/23/18 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 9.3 mg/L 2.5 1 01/25/18 08:02 Date: 02/01/2018 06:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 18 aceAnalytical' www.pacelabs.com r ' ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92370463 Sample: MSW 02 METALS Lab ID: 92370463004 Collected: 01/23/18 01:21 Received: 01/23/18 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 01/24/18 06:30 01/28/18 03:51 7440-43-9 Chromium 85.6 u0/t 50 1 01/24/18 0630 01/28/18 03:51 7440-47-3 Lead ND ug/L 5.0 1 01/24/18 06:30 01/28/18 03:5,1 7439-92-'I Niolcol 370 ug/L 5.0 1 01/24/18 00:30 01/28/18 03 51 7440-02-0 Zinc 2G7 ug/L 10.0 1 01/24/18 00.30 01/28/18 03.51 T440-66-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 18 aceAnalytical www.pacelabs.mm i ANALYTICAL RESULTS Project: MONROE STORMWATER Pace Project No.: 92370463 Pace Analytical Services, LLC 9800 Kincey Ave. 'Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MSW 02 OIL & GREASE Lab ID: 92370463005 Collected: 01/23/18 01:18 Received: 01/23/18 11:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 01/31/18 05:04 Date: 02/01/2018 06:14 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 18 aceftlytical www.pacelabs.com I QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92370463 QC Batch: 396117 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92370463005 ML I HUD BLANK: 2196042 Associated I ab Samples: 92370463005 Parameter Units Oil and Grease lay/L LABORAI URY GUN I ROL SAMPLE: 2196043 Parameter Units Oil and Grease mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporliny Result I imit Analyzed Qualifiers ND 5.0 U 113 1/18 Ub:UU Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 40 37.4 94 78114 MATRIX SPIKE SAMPLE: 2196044 92370638001 Spike MS MS % Rec Paromotor Units Result Cone. Result % Reo Limits Quanners Oil and Grease mg/L ND 40 35.9 90 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18 ZAnalytical wwvl.pacelabs.00m QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. 'Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92370463 QC Batch: 395229 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92370463004 METHOD BLANK: 2191021 Matrix: Water Associated Lab Samples: 92370463004 Blank Repul tiny parameter Units Result Limit Analyzed Qualiriels Cadmium ug/L NU 1.0 01/28/18 02:48 Chromium ug/L ND 6.0 01/28/18 02.48 Lead ug/L NU 5.0 01/28/18 02:48 Nickel ug/L NU 13.0 U1/28/18 02:48 Zinc ug/L ND 10.0 01/28/18 02:48 LABORATORY CONTROL SAMPLE: 2191022 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 495 99 85-115 Chromium ug/L 600 500 102 85115 Lead ug/L 500 491 98 85-115 Nickel ug/L 500 500 100 85-115 Zinc ug/L 500 502 100 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191023 2191024 MS MSD 92370439001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua[ Cadmium ug/L ND 500 500 397 406 79 81 70-130 2 Chromium ug/L 259 500 500 609 633 70 75 70-130 4 Lead ug/L 129 500 500 487 485 72 71 70-130 0 Nickt:[ uy/L 132 500 500 490 500 72 74 70-130 2 Zinc uy/L 424 500 500 780 716 73 59 70-130 9 MI MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2,19,1025 2,19,1026 MS MSD 92370463004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua] Cadmium ug/L ND 500 500 522 547 104 109 70-130 5 Chromium ug/L 85.6 500 500 612 636 105 110 70-130 4 Lead ug/L ND 500 500 503 522 100 104 70-130 4 Nickel ug/L 370 500 500 891 896 104 105 70-130 1 Zinc ug/L 267 500 500 801 796 107 106 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01 /2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 18 ' 9 a aceAnalytical —pacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92370463 QC Batch: 395443 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92370463003 METHOD BLANK: 2192164 Associated Lab Samples: 92370463003 Parameter Units fbtal Suspended Solids mg/L LABORAf ORY GON I ROL SAMPLE: 2192165 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2192166 Paramoter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2192167 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Rlaiik Refuuthig Result Limit Analyzed Qualifiers NU 2.5 01/25/18 08:00 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 242 97 90-110 923/0593001 Uup Result Result 4.9 5.3 92370518001 Dup Result Result ND ND RrD Qualifiers 7 D6 RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01 /2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18 aceAnalytical www.pacelabs.com f t m, Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92370463 QC Batch: 395280 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92370463001 METHOD BLANK: 2191164 Associated t ah Samples' 92370463001 Parameter Units BOD, 5 day my/L LABOPAI OPY CON I POL SAMPLE: 2191165 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NO 2.0 01/29/18 09:58 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 162 82 84.6-115.4 L2 SAMPLE DUPLICATE: 2191166 92370494001 Dup Paramoter Units Result Result BOD, 5 day mg/L 113 126 RhD Qualifiers; 11 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 18 .y aceAnalyticai® f vww.pacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92370463 QC Batch: 396112 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92370463002 METHOD BLANK: 2196020 Associated Lab Samples: 92370463002 Parameter Units Chemical Oxygen Demand mg/L Matrix: Water Blank Rupotllny Result Limit Analyzed Qualifiers ND 25.0 01/31/18 20:21 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY" CONTROL SAMPLE. 2190021 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 753 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196022 2196023 MS MSD 92370468001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 114 100 100 220 223 106 109 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196024 2196025 MS MSD 92370760001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Cone Result Result % Rec % Rec L imits RPD Qual Chemical Oxygen Demand mg/L 4490 100 100 5050 5160 560 672 90-110 2 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 18 aceAnalytical www.pacelabs.com QUALIFIERS Project: MONROE STORMWATER Pace Project No.: 92370463 DEFINITIONS 4 O' Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. I N I C - too Numerous to Count ,l - Fstimated concentration above the adjusted method detection limit and below the adjusted reporting limit. M(X - Adjusted Method Detection t Imit PQL- Practical Quantitation Limit. RL - Reporting Limit. S - Sulugate 1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS U8 Ilie precision between [lie sample and sample duplicate exceeded laboratory control limits. 12 Anolyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18 aceAna1j4 cal' www.pacelabs.corn t QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MONROE STORMWATER Pace Project No.: 92370463 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92370463001 MSW 02 BOD 92370463005 MSW 02 OIL & GREASE EPA 1664E 396117 92370463004 MSW 02 METALS EPA200.7 395229 EPA200.7 92370463003 MSW 02 TSS SM 2540D 305443 92370463001 MSW 02 BOD RM 5210C3 395280 SM 5210B f kitU463UU4 MSW ok UUU 810 b220U 306112 I�F.1�[iYaLdllf�,ZiS[ i�Ic9fiCl��I REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Analytical Batch 395247 395324 Page 15 of 18 /q Document Name: Document Revised: August 4, 2017 �- Go Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: ! F-CAR-CS-033-Rev.04 Pace Quality Office Laboratory receiving samples: Asheville R Eden❑ Sample iiCondition � Client Name: Upon Re .Courier:---- .-....... _._._..❑Fed Ex❑UPS GreenwoodEl Huntersviile Raleigh❑ Mechanim-,111,.r1 l Project: Wo# : 9237a463 # ... Iititr111 flit fit Custody Seal Present? ❑Yes Seals Intact? ❑yes Cr Date/Initials Person Examining Contents: Packing Material: ❑aubblo Wrap ubbie Begs ❑ Non a ❑ Other Biological Tissue Frozme 7 berm I [ [_I IR. - ` ❑Yes ❑N/A IRGun iO: � �_�L'( 'wet ❑Blue ❑None Typo of Ica: Correction Factor: Cooler Temp Corrected ('Cl! . , j Tomp should be above freezing to 6'C 115ampi81 Out of ternp criteria. Surnpius on Ice, cooling proees: as begun USDA Regulated Soll N/A, water sample) Old samples angi a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source tinter Tonally, I—lYac Nn us —dil mm rU6rio f%Jcv)r LJyeS �LJNO Commems/Discre ancy: Chain of Custody Present? N/A 1. Samples Arrived within Hold Time? es Cho ❑N/A 2. Short Hold Time Analysis (02 hr.)? es ONO []N/A 3. NO turn Arounr! Time Requested? Ymc Pl< N/A 4 S. Sufficient Volume? Yes .. ONO N/A Correct Containers Used? ❑No ❑N/A 6. -Pace Containers Used? �Yes -i des No []NIA Containers Intact? EJ es ❑NO ON A 7. Dissolved analysis: Samples Field Filtered? Dyes", o N/A 8, Sample Labels Match COC? es ❑No ❑N/A' 9. -includes Date/Time/iD/Analysis Matrix: Heads ace in VOA Vials (>s-6mm ? ❑Yes DNO /A 10. Trip Blank Present? Dyes CIP ❑N/A 11. I rip [Sunk Lustody Seals Present.? Yes [ENO f (�11/A Person Contacted: Comments/Sample Discrepancy: Lot ID Of split containers: Date/Time: Field Oats Required? _ ❑YCS ONO Project Manager SCURF Review: j V by Date-, l 2� Project Manager SRF Review: N 1. 4 Date: Z Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 16 of 18 Document Natvte: Document No.: '"Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. "Bottom half of box is to list number of bottles Document Revised: August4, 2017 it(SCUR) Page 2 of 2 Issuing Authority: Pace Quality Office Project # WO# : J237Q46- f:M: MWB Due Date: 02/ovla CLIENT: 92411vac NC Ion UUMM U 0 MEN M ME 0 0 M OMEN 0 0 MEN me Monson MINES a—EMMOMME Monsoon L-IL-1000 EMOOMMOM MEN on son 0 OLIN OLIN ENSIMMODOMEN SON 0 on OMEN 0 on EMMONS MESON 0 on M on MONSOON MESON NOM 0 M 0 MML 10 INONE ■0 M 0 ME 0 1�ONOMME on a MEMO 0 NOMEMEMME NONE on ME , 0 0 0 M 0 0 M 0 1 pH Adjustment Log for Preserved Samples Sample Ib Type of Preservative pH upon receipt bate preservation adjusted Time preservation adjusted Amount of Preservative added Lot It Page 17 of 18 N o w v m N. A W N ITEM # a o m m �Rr r O n a I co G m o a 1 7 a 19j s a W o ep c7 a z- O m Z ... • • z w r M m P m n p c x T n a W ` g Q z m ; n� n a i fn� IT,p (� •S� OaqD-O rn a��Cs,v p A m o m m CO a o M ® A. P. c m ( o a 3 lA MATRIX OODE (sesvafd codes to left) . �_. III SAME L( ±INYPE (G=GRAB C=COMP) o Q ` IT u p ql S D d IO y m. n l m O s -�, z . Z V z R •.. w •► �,+ -. �' to r m m n c d m • Z H x T q :D'�� p]j3° M 7l h " • • y �^ 7P„ L o a v. a..1'- �.hi m c Q N s m SAMPLE TEMP AT COLLECTION 0 a t ` ... y" .- .� •.+ r # OF CONTAINERS m m a �' SL s p m Unpreserved Q g HNOa' m c a HGI 2 t_ Z ; s NaOH Methanol �. c Other O %, . jAnafysPsTest j':' Y/N Z a a113 0 1 +� o y R s ICD O rt• mu �' Y' � � y �S fl% 9 v n �33 �. �• v,. o' ai v a n m � 3 000 Q -71 z ` Tn Temp in °C 4v 0 Ste°. Residual Chlorine (Y%N) D ra, Recelved on t~ m N Ice (YIN) D t J � Custody m 7 r r> � h Sealed Cooler 0 .;Z7 Q7 (YIN) o m alai Z m — 2 al X (Zri a Samples Intact y (Y/N) c m v � Pa e18of18