HomeMy WebLinkAboutNCS000330_Monitoring Reports_20180215STORMWATER DIVISION CODING SHEET
NCS PERMITS
PERMIT NO.
o}GS o00
DOC TYPE
❑ FINAL PERMIT
)� MONITORING REPORTS
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ Zaa • 02 • IS
YYYYM M D D
February 9, 2018
Attn: Central Files
N.C. Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Central Files:
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: (704) 289-4511
Fax: (704) 290-5194
Email: Joe.Hinkle@atimetals.com
Attached,, please. find stormwater monitoring data for Permit No NCS000330. The originals anld
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
I Start
End
Year 9 — Period 1
17
1 September 1, 2017
February 28, 2018
Stornnwater sampling for Outfall # 02(M) has been determined to be the representative outfall
through prior correspondence.
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
qe
'erely,
Hinkle
EHS Manager
RECEIVED
FEB 15 2U1a
OFNTRAL rII.CS
DWR SECTIQPJ
"0
Allvac - Monroe Plant -0ow-ATI Allvac
Stormwater Monitoring Report Form
Sample Date: SampleTime:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Stonnwater Discharge Outfall #2
Drainage Area = 272,590sq. ft. = 6.25 acres
% Impervious = 36%
es M0scr
PlILe- 41)�'�zf
I
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
O
0.001
Chromium, total recoverable
1
Lead, total recoverable
0.03
Nickel, total recoverable
0.26
Zinc, total recoverable
0.067
Oil mid Orease
30
PH
(std units)
6-9 (std units)
Storm Date: Storm Duration: - 4 A (Hrs.) Inches of Rainfall: L'6n
Duration of time preceding rain event exceeding 0.1": Mrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., cfs) = (A x inches rain/12 inches/ft. x 6.25 acres x.64) +.9 x inches rain/12inches/ft. x 6.25 x.36)
Q(TotaI,cf§)=.l333x 0, <A
(Inches of rain) +.1688 x0,50 (Inches of rain)
cfs
Q
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A
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Foi guidunce on filling out this foi in, Please visit: I1LLW / jPui taLiicdem.urg/web/wgjws/su jnpdessw#itah-4
Permit No.: N
Facility Name:
County: �1
Inspector: i
Date of Inspection: j - -/Y
Time of Inspection: 9`36) AM
Total Event Precipitation (inches):
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
0 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative nonitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event " However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
............................................................. ........................................................................................................ ......... _...................... ............................ _....................... ........... ..... ............... ........... .................... ......... ........................ ............................................................... .......... -....... _.......... _........................ _.....
By this signa re, I certify that this report is accurate and complete to the best of my knowledge:
�—
1. Outfall Description- 0
Outfall No. —��� Structure pipe, ditch, etc.) /
Receiving Stream: (1 ( 7
Describe the indu,strY activities that occur within the outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: h -i ' a l-y a
j J
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): fir) A10
4. Clarity: Choose the number which best describes the clarity of the discharge, where! 1 is
clear and 5 is very cloudy-
1 4D 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 0 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 (2) 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
B. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Lidicatois of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
��
NEDENR
St®rmwater Discharge ®utfall (SD®)
Qualitative Monitoring Report
Forguidance on lillinq out this form, Please visit: http://porttal,ncdenr.org/web/wq/ws/su/npdessw##tab-4
Permit No.: N/C//C/Q/�/,/.�/�/. or Certificate of Coverage No.:
Facility Name:
County: Z//1 i"1?Q Phone No.�i�9'
Inspector: 1 me-s M6-se-r
Date of Inspection:
Time of Inspection: 8,'l 7,411
Total Event Precipitation (inches): OX
Was this a 'Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
l`-' Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
(qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "rrieasureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWO Regional Office.
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall vDeauition:
Outfall No. St uctu
Receiving Stream: AAf - /''
Describe the industrial activities the
z
etc.)
occur within the outfall drainage area:
2. Color: Describe the color of the dis
(light, medium, dark) as descriptors: %/'
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 1764 e-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 (D 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2 a 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 0 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes S
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
A4j;A
A
NCDENR
Stormwater Discharge Outtall (SDO)
Qualitative Monitoring Report
Forguidance on filling out this form, please vi.sit� http_/lnortal:nrdunr,urgublw ws s ln►2dassw#tab 4
r
Permit No.: N/C/,,:� j
Facility Name:
County: Z14 1,0/7
Inspector:
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches): 0.
or CertifCatelof C
Phone No.
No.: N/C/Q/ / / / / / /
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
0 Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative inonitoi ing I equii elnents vary. Must pei iiiits i cquii c qualitativc rnonituriiig tube
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
.................. ......................... ......................................._.................................. _........................ .................................................................... .................................. _................................................................... .............................. ............................ _.................... ..................... ........................................................................
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall Description:
Outfall No. C Structu} e (pipe,
Receiving Stream: j 6hI r ..Sot-i
h, etc..)) iioe
/
Describe the industrial activities that occur within the outfall r
area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: `� A-1) &J a
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): Z20/7F
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and S is very cloudy-
1 V 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 @2 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
AL�
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report.
Fut guidance on filling out this forut, please visit. liLLW;//poi-tal.iicdeiir.org/web/wq/ws/su/npdossw#tab-4
Permit No.: N/C/,S/
Facility Name: �Q
County:
Inspector:
Date of Inspection: _
Time of Inspection: _
J/1.5/,0/, or Certificate of Coverage No.:
Total Event Precipitation (inches): 'p, q6
Phone No. 72)
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
wr Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative tttouitot ittg i equii citiculs vary. Mosl pei ►nits i equiie qualitative mottilot hig Lobe
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
ob. ..............................................................................................._.._..........................._............................................................._....................................................................................................................................................................................................................................................................................
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall Descri tion:
Outfall No. so �
Receiving Stream: _1
Descri e the industrial ff ctivi,
(pipe, ditch, etc.) e, //1 1/c, z
)4 C-reeK --1441
that occur within
2. Color: Describe the color of the discharge using b
(light, medium, dark) as descriptors: V i r � h"-
area:
colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /WRe'
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 l_l 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
AQ=
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Fur guidunce un filling out this fur ni, pleuse visit: lily://portal.ncdenr.org/web jwq/ws jsu jnpdessw#Lab -4
Permit No.: N/C Pr Certi[�ale,o['Cover4ge No.: N/(;/G
Facility Name: fR i
County: /.fir'2 r a/t Phone No.
Inspector: .JCL /'1 6 p, 14p S, r
Date of Inspection: _4 - 4-19
Time of Inspection: 9 --�4 A14
Total Event Precipitation (inches): 0096,
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Y`J Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
(qualitative monitoring requirernerrts vary. Most perinits require qualitative rnoniloring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1. inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
.. ..... ....... -............................................. _........................... ................................................................................................................................................. .......................................... _................................................... ............................... ............. ........................................... ......... ... .................. ...............................................
By this signatyre, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall Description: ,% C Outfall No. truct}�re (pipe, ditch, etc.) �t % "rGA
Receiving Stream: ' ✓'Cl 'LIl-eelk
Describe the industrial a tivities that oc ur wit in the outfall drainage area: f ® l / D < a Q i n
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: i "T ti
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): 17,0A f
4-. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 t„/ 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious liidlcalurs of Storinwater Pollullon:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
Foi guidunce on filling out this foi in, pleuse visit: hLLp://poi Lai.iicdem .oi g jweb/wy/ws/su/►1Wdcssw#Lab-4
Permit No.: N/C/s/�)/LI/
Facility Name: 7-s
County: ZJ4 I Dil
Inspector: _ 1 Am,,, q
Date of Inspection:
Time of Inspection:
.�/1/.6/` or Certifi�ateiof Coverige No.: N
Total Event Precipitation (inches): 7
Phone No. 7d V 2,?.YV -"1Si
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
VYes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
............................
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event " However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
By this signatufe, I certify that this report is accurate and complete to the best of my knowledge:
1. Outfall Description:
Outfall No. <
Receiving Stream: If
(pipe, ditch,,etc.) d 'Iek
2. Color: Describe the color of the discharge u ing basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: %2 l6 it) n
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /'?0/2 if
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy!
"1 6) 3 4 5
S. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
0 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2� 3 4 5
7. Is there any foam in the stormwater discharge? Yes 49
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012
W
e
z aceAnalj4ical o
www.pacelabs.com
February 01, 2018
Mr. Joe Hinkle
Allvac
R[-: Project* MUNkOE- 8 I ()RMWAi [-P\
Pace Project No.: 92370463
Pace Analytical Services, LLC
9800 Kincey Ave. Suite loo
Huntersville, NC 28078
(704)875-9092
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
(704)€375-9092
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 18
1�;a'ceAnalj4ical'
www.pacelabs.com
t
Project: MONROE STORMWATER
Pace Project No.: 92370463
Pace Analytical Services, LLC
9800 KinceyAve. -Suite 100 V
Huntersville, NC 28078
(704)875-9092
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #. E87048
Massachusetts; Certification #: WI NC 0'SU
North Carolina Drinklna Water Certification #: 3//12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Vlrglnla/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VLLAI I Certification #: 4OU222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 18
T'
p
;ceAnalj&al
r www.pacelabs.com
t
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Project:
Pace Project No.:
MONROE STORMWATER
92370463
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92370463001
MSW 02 BOD
SM 5210B
ECH
1
PASI-A
92370463002
MSW 02 COD
SM 5220D
NAL
1
PASI-A
92370463003
MSW 02 TSS
SM 2540D
MJP
1
PASI-A
92370463004
MSW 02 MSTALS
LPA2UU.l
81-11
5
PASI-A
92370463005
MSW 02 OIL & GREASE
FPA 1664H
JMS
1
PASI C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 18
aceAnalytical
www.pacelabs.com
I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. -Suite 100
Huntersville, NC 28078
(704)875-9092
Project: MONROE STORMWATER
Pace Project No.: 92370463
Sample: MSW 02 BOD Lab ID: 92370463001 Collected: 01/23/18 01:15 Received: 01/23/18 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Field Data Analytical Method
Collected By
J.Moser
1 01/24/18 09:42
Collected Date
1123/18
1 01/24/18 09:42
Collected Time
1:25
1 01/24/18 09:42
NI 1
7.4 Sid. Units
0.10 1 01/24/18 09.42
Tcmpomture
1:2.7 deg C
0.50 1 01/24/10 09:42
621(lH HOD, 5 day
Analytical Method: 5M 5210N
BOD, 5 day
4.8 Ing/L
2.0 1 01/24/18 13:00 01/29/18 10:09 L2
REPORT OF LABORATORY ANALYSIS
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(f
I
ANALYTICAL RESULTS
Project: MONROE STORMWATER
Pace Project No.: 92370463
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MSW 02 COD Lab ID: 92370463002 Collected: 01/23/18 01:16 Received: 01/23/18 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 41.0 mg/L 25.0 .1 01/31/18 20:21
Date: 02/01/2018 06:14 PM
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
S
Pace Analytical Services, LLC
9800 Kincey Ave. -Suite lo0
Huntersville, NC 28078
(704)875-9092
Project: MONROE STORMWATER
Pace Project No.: 92370463
Sample: MSW 02 TSS Lab ID: 92370463003 Collected: 01/23/18 01:19 Received: 01/23/18 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 9.3 mg/L 2.5 1 01/25/18 08:02
Date: 02/01/2018 06:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: MONROE STORMWATER
Pace Project No.: 92370463
Sample: MSW 02 METALS Lab ID: 92370463004 Collected: 01/23/18 01:21 Received: 01/23/18 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0
1
01/24/18 06:30 01/28/18 03:51
7440-43-9
Chromium
85.6
u0/t
50
1
01/24/18 0630 01/28/18 03:51
7440-47-3
Lead
ND
ug/L
5.0
1
01/24/18 06:30 01/28/18 03:5,1
7439-92-'I
Niolcol
370
ug/L
5.0
1
01/24/18 00:30 01/28/18 03 51
7440-02-0
Zinc
2G7
ug/L
10.0
1
01/24/18 00.30 01/28/18 03.51
T440-66-5
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: MONROE STORMWATER
Pace Project No.: 92370463
Pace Analytical Services, LLC
9800 Kincey Ave. 'Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MSW 02 OIL & GREASE Lab ID: 92370463005 Collected: 01/23/18 01:18 Received: 01/23/18 11:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 01/31/18 05:04
Date: 02/01/2018 06:14 PM
REPORT OF LABORATORY ANALYSIS
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Page 8 of 18
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I
QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92370463
QC Batch: 396117 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92370463005
ML I HUD BLANK: 2196042
Associated I ab Samples: 92370463005
Parameter Units
Oil and Grease lay/L
LABORAI URY GUN I ROL SAMPLE: 2196043
Parameter Units
Oil and Grease mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix: Water
Blank Reporliny
Result I imit Analyzed Qualifiers
ND 5.0 U 113 1/18 Ub:UU
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
40 37.4 94 78114
MATRIX SPIKE SAMPLE: 2196044
92370638001 Spike MS MS % Rec
Paromotor Units Result Cone. Result % Reo Limits Quanners
Oil and Grease mg/L ND 40 35.9 90 78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 18
ZAnalytical
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. 'Suite 100
Huntersville, NC 28078
(704)875-9092
Project: MONROE STORMWATER
Pace Project No.: 92370463
QC Batch: 395229
Analysis
Method:
EPA
200.7
QC Batch Method: EPA 200.7
Analysis
Description:
200.7 MET
Associated Lab Samples: 92370463004
METHOD BLANK: 2191021
Matrix:
Water
Associated Lab Samples: 92370463004
Blank
Repul tiny
parameter
Units
Result
Limit
Analyzed Qualiriels
Cadmium
ug/L
NU
1.0
01/28/18 02:48
Chromium
ug/L
ND
6.0
01/28/18 02.48
Lead
ug/L
NU
5.0
01/28/18 02:48
Nickel
ug/L
NU
13.0
U1/28/18 02:48
Zinc
ug/L
ND
10.0
01/28/18 02:48
LABORATORY CONTROL SAMPLE:
2191022
Spike
LCS
LCS % Rec
Parameter
Units
Cone.
Result
% Rec Limits Qualifiers
Cadmium
ug/L
500
495
99 85-115
Chromium
ug/L
600
500
102 85115
Lead
ug/L
500
491
98 85-115
Nickel
ug/L
500
500
100 85-115
Zinc
ug/L
500
502
100 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2191023
2191024
MS
MSD
92370439001
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits
RPD Qua[
Cadmium
ug/L
ND
500
500
397
406 79 81
70-130
2
Chromium
ug/L
259
500
500
609
633 70 75
70-130
4
Lead
ug/L
129
500
500
487
485 72 71
70-130
0
Nickt:[
uy/L
132
500
500
490
500 72 74
70-130
2
Zinc
uy/L
424
500
500
780
716 73 59
70-130
9 MI
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2,19,1025
2,19,1026
MS
MSD
92370463004
Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result % Rec % Rec
Limits
RPD Qua]
Cadmium
ug/L
ND
500
500
522
547 104 109
70-130
5
Chromium
ug/L
85.6
500
500
612
636 105 110
70-130
4
Lead
ug/L
ND
500
500
503
522 100 104
70-130
4
Nickel
ug/L
370
500
500
891
896 104 105
70-130
1
Zinc
ug/L
267
500
500
801
796 107 106
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01 /2018 06:14 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 18
' 9
a
aceAnalytical
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QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92370463
QC Batch: 395443 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92370463003
METHOD BLANK: 2192164
Associated Lab Samples: 92370463003
Parameter
Units
fbtal Suspended Solids
mg/L
LABORAf ORY GON I ROL SAMPLE:
2192165
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2192166
Paramoter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 2192167
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix: Water
Rlaiik Refuuthig
Result Limit Analyzed Qualifiers
NU 2.5 01/25/18 08:00
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 242 97 90-110
923/0593001 Uup
Result Result
4.9 5.3
92370518001 Dup
Result Result
ND ND
RrD Qualifiers
7 D6
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01 /2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 18
aceAnalytical
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f
t
m,
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92370463
QC Batch: 395280 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day
Associated Lab Samples: 92370463001
METHOD BLANK: 2191164
Associated t ah Samples' 92370463001
Parameter Units
BOD, 5 day my/L
LABOPAI OPY CON I POL SAMPLE: 2191165
Parameter Units
BOD, 5 day mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 2.0 01/29/18 09:58
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 162 82 84.6-115.4 L2
SAMPLE DUPLICATE: 2191166
92370494001 Dup
Paramoter Units Result Result
BOD, 5 day mg/L 113 126
RhD Qualifiers;
11 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 18
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QUALITY CONTROL DATA
Project: MONROE STORMWATER
Pace Project No.: 92370463
QC Batch: 396112 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92370463002
METHOD BLANK: 2196020
Associated Lab Samples: 92370463002
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Rupotllny
Result Limit Analyzed Qualifiers
ND 25.0 01/31/18 20:21
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
LABORATORY" CONTROL SAMPLE. 2190021
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 753 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196022 2196023
MS MSD
92370468001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 114 100 100 220 223 106 109 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2196024 2196025
MS MSD
92370760001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Cone Result Result % Rec % Rec L imits RPD Qual
Chemical Oxygen Demand mg/L 4490 100 100 5050 5160 560 672 90-110 2 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: MONROE STORMWATER
Pace Project No.: 92370463
DEFINITIONS
4
O'
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
I N I C - too Numerous to Count
,l - Fstimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
M(X - Adjusted Method Detection t Imit
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Sulugate
1,2-Diphenythydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
U8 Ilie precision between [lie sample and sample duplicate exceeded laboratory control limits.
12 Anolyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 02/01/2018 06:14 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 18
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MONROE STORMWATER
Pace Project No.: 92370463
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92370463001
MSW 02 BOD
92370463005
MSW 02 OIL & GREASE
EPA 1664E
396117
92370463004
MSW 02 METALS
EPA200.7
395229
EPA200.7
92370463003
MSW 02 TSS
SM 2540D
305443
92370463001
MSW 02 BOD
RM 5210C3
395280
SM 5210B
f kitU463UU4
MSW ok UUU
810 b220U
306112
I�F.1�[iYaLdllf�,ZiS[ i�Ic9fiCl��I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
395247
395324
Page 15 of 18
/q
Document Name:
Document Revised: August 4, 2017
�- Go
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
!
F-CAR-CS-033-Rev.04
Pace Quality Office
Laboratory receiving samples:
Asheville R Eden❑
Sample iiCondition
� Client Name:
Upon Re
.Courier:---- .-....... _._._..❑Fed Ex❑UPS
GreenwoodEl Huntersviile Raleigh❑ Mechanim-,111,.r1
l Project: Wo# : 9237a463
# ... Iititr111 flit fit
Custody Seal Present? ❑Yes Seals Intact? ❑yes Cr
Date/Initials Person Examining Contents:
Packing Material: ❑aubblo Wrap ubbie Begs ❑ Non a ❑ Other Biological Tissue Frozme
7 berm I [ [_I IR. - ` ❑Yes ❑N/A
IRGun iO: � �_�L'( 'wet ❑Blue ❑None
Typo of Ica:
Correction Factor: Cooler Temp Corrected ('Cl! . , j Tomp should be above freezing to 6'C
115ampi81 Out of ternp criteria. Surnpius on Ice, cooling proees:
as begun
USDA Regulated Soll N/A, water sample)
Old samples angi a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source tinter Tonally,
I—lYac Nn
us —dil mm rU6rio f%Jcv)r LJyeS �LJNO
Commems/Discre ancy:
Chain of Custody Present?
N/A
1.
Samples Arrived within Hold Time?
es
Cho
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
es
ONO
[]N/A
3.
NO turn Arounr! Time Requested?
Ymc
Pl<
N/A
4
S.
Sufficient Volume? Yes .. ONO N/A
Correct Containers Used?
❑No
❑N/A
6.
-Pace Containers Used?
�Yes
-i des
No
[]NIA
Containers Intact?
EJ es
❑NO
ON A
7.
Dissolved analysis: Samples Field Filtered?
Dyes",
o
N/A
8,
Sample Labels Match COC?
es
❑No
❑N/A'
9.
-includes Date/Time/iD/Analysis Matrix:
Heads ace in VOA Vials (>s-6mm ?
❑Yes
DNO
/A
10.
Trip Blank Present?
Dyes
CIP
❑N/A
11.
I rip [Sunk Lustody Seals Present.?
Yes
[ENO
f
(�11/A
Person Contacted:
Comments/Sample Discrepancy:
Lot ID Of split containers:
Date/Time:
Field Oats Required? _ ❑YCS ONO
Project Manager SCURF Review: j V by Date-, l 2�
Project Manager SRF Review: N 1. 4 Date: Z
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 16 of 18
Document Natvte:
Document No.:
'"Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles
Document Revised: August4, 2017
it(SCUR) Page 2 of 2
Issuing Authority:
Pace Quality Office
Project # WO# : J237Q46-
f:M: MWB Due Date: 02/ovla
CLIENT: 92411vac NC
Ion
UUMM
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0
0
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0
0
M
0
1
pH Adjustment Log for Preserved Samples
Sample Ib
Type of Preservative
pH upon receipt
bate preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot It
Page 17 of 18
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