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HomeMy WebLinkAboutNCS000330_Monitoring Reports_20181126STORMWATER DIVISION CODING SHEET NCS PERMITS PERMIT NO. j��SQCp 2�aj� DOC TYPE ❑FINAL PERMIT MONITORING REPORTS ❑ APPLICATION ❑ COMPLIANCE ❑ OTHER DOC DATE ❑ 7.0l SS • U • "L& YYYYMMDD r November 15, 2018 *ATI P.O. Box 5030 2020 Ashcraft Avenue Monroe, NC 28111-5030 Attn: Central Files Phone: (704) 289-4511 N.C. Division of Water Quality ��'� Fax: (704)2.VJe@a4 ��Email: Joe.Hinkle@atimetals.com 1617 Mail Service Center E'D Raleigh, NC 27699-1617 NOV 2 6 2018 CEN Central Files: OWR SECTION M�o Attached, please, find stormwater monitoring data foi Pwiiiit No NCS000330. The oliglrlals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start End Year 10 —Period 1 19 September 1, 2018 February 28, 2019 Stormwater sampling for Outfall # 02(M) has been determined to be the representative outfall through prior correspondence. If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sincerely, k., ( jk J e Hinkle EHS Manager Allvac e Monroe Plant ' I AIIvac &2 water Mlonitorin Report Form Sample Date: / 0 - � 6 - / ? Sample Time: 5 : /a q n Sample Location: SW Person Collecting Samples: O Stormwater Discharge Outfall #2 Drainage Area = 272,590sa. ft. = 6.25 acres % Impervious = 360/9 Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: 40 CFR ftt 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 120 TSS b 100 Cadmium NO 0.001 n Chromium, total recoverable O,Vo116 1 Lead, total recoverable 0.03 Nickel, total recoverable 0.1.09 0.26 Zinc, total recoverable e 0355 0.067 Oil and Grease NO 30 N 6-9 (std units) pH (std units) Storm Date: l0 -o16 - / 2 Storm Duration: M 7„S (Hrs.) Inches of Rainfall: 1.90►' Duration of time preceding rain event exceeding 0.111: 1JA(Hrs.) Estimated Flow Calculation: Q = CIA Q(Tota1) = Q(Pervious Area) + Q(Impervious Area) Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 6.25 acres x ,64) + .9 x inches rain/12inches/ft. x 6.25 x .36) Q(Total, cfs) =. 1333 x J . 'y (Inches of rain) + .1688 x 1 • y (Inches of rain) _ 0, q23 cfs V 0 mmM) w W z W a x 0 w � W rr rl V W w z z0 Oa C7 w �� V th 0 C ee o� o UO O c � L 2 cj E � O y 3 O O . LC z MI 0 0 3 G 0 0 I Wo W L o� zo R 0 r fi � � v C o � w CL � L j E- A Lin U E oz 0 a 14(3 QFW v w a w C � O�•g p•�vpir'" eo 0 a bL a�"ia w a� �d waA8� ad ego°° PC �.���� a c a A� d =�' o o a Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deg.nc.gov/about/divisions/energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: /3 / O/ or Certificates of Coverage No.: N/C/G/_ Facility Name: /q % .S,QBG% ry%, / ► tq �-6/C ! ri. 3 County: ✓V ��y �/ Phone No. 7441 -a 89 - y-V 1 Inspector: JAM�K5 MCL5, l2 Date of Inspection- 1 Time of Inspection: e? ; l 3 Qm Total Event Precipitation (inches): Q . y,5 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72 hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. nutfall Description: Outfall No. sw o Structure (pipe, ditch, etc.): Receiving Slleetln: /��'ch aa�so.✓ Gr�'�/�' Describe the industrial activities that occur within the outfall drainage area: l eiw% „f�6ri!E Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: VP-- ZL4 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): nZo,y 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Q2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 i 7. Is there any foam in the stormwater discharge? ® Yes 9 No. 8. Is there an oil sheen in the stormwater discharge? C)Yes No. 9. Is there evidence of erosion or deposition at the outfall? n Yes 0o. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit h=s://deg.nc.aov/about/divisions/energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: N/C/_✓I" / 0/ ©/ O/ 3/3/ 0✓ or Certificate of Coverage No.: N/C/G/_/_/_/_/—/_/ Facility Name: /'% Tr MAAA%e ig15 County: V V � @ dV Phone No. 70 Z —p299 Inspector: q� Date of Inspection- //- Time of Inspection: 9 : a I nrr'1 Total Event Precipitation (inches): 0 . 416 All permits require qualitative monitoring to be performed during a "measurable storm event." ,. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous ieasurable storin event must have been at least 72 hours prior. The 72 hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. ......... ..._.... ......... ........ _.................................... ....................... By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. j .� Structure (pipe, ditch, etc /` ; ;0� Receiving Stlzalri. cti,�adsaN CrcE,� Describe the industrial activities that occur within the outfall drainage area: Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 4 ¢ brouoAf 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 4ZO All 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 (D 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: ^ 1 2 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? () Yes WNo. 8. Is there an oil sheen in the stormwater discharge? ()Yes GKNO. 9. Is there evidence of erosion or deposition at the outfall? 0 Yes eKNo. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: N/C/S/�7 /�/ Dl3 /3/ C'� or Certificate of Coverage No.: N/C/G/_/_/_/_/_/_/ FacilityName: A T.z��`,gf County: L%/V 1'0 AJ Phone No. 76 4/ -,R8M - 41SI I Inspector: 3-Arr-e-f 6Jet Dato of In.spoc.tion• // - C/ - / Time of Inspection: &.' e2 7 4r!'7 Total Event Precipitation (inches): 6. q.5 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous ineasutahle stoup event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or Des 1. Outfall Description: Outfall No..5W 0,3 Structure (pipe, ditch, etc.): f d �G Receiving Stream: Describe the industrial activities that occur within the outfall drainage area: Pagel of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the jis (light, medium, dark) as descriptors: I basic colors (red, brown, blue, etc.) and tint 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 426A E 4. Clarity: Choose the number which best describes the clarity of the discharge, where I is clear and 5 is very cloudy: 1 <0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 i 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 2 3 4 5 7. Is there any foam in the stormwater discharge? Q Yes 0"'No. 8. Is there an oil sheen in the stormwater discharge? ()Yes EJ No. _ 9. Is there evidence of erosion or deposition at the outfall? o Yes Gr 90. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit htgps://deq.nc.cov/about/divisions/ener.gy-mineral-land- resources/energymineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: NlCI„�101�l Dll,�l Ol or !Certificate ofLCoverage No.: N/C/G/_/ /_/_/_/_/ Facility Name: 4 Tl ..Sa6�r'r� 11'N I�A59i r9//S County: V / i' Phone No. 70 Inspector: 3t4," u3 G e- Data of Inspection: f.• g Time of Inspection: Total Event Precipitation (inches): 0. 4/3 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous treasurable storm event inust have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR Regional Office. _. ......... ......... ........ ......... ........ ............................... ... By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. 5LO 0 Structure (pipe, ditch, etc.): Receiving Stream: 4; CAN a <nV Cr cc% Describe the industrial activities that occur within the outfall drainage area: A ;esg,ivJA-4!j /'.a Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: L— P1 h P'O WAL 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): Aj 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 QU 3 4 5 7. Is there any foam in the stormwater discharge? 0 Yes o. 8. Is there an oil sheen in the stormwater discharge? ®Yes o. 9. Is there evidence of erosion or deposition at the outfall? 9 Yes Gwl�o. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: or Certificate of Coverage No.: N_/C/G/_/_/_/_/_/_/ Facility Name: 11 %Z SSDE G inn l �A My �--nei /s-01 us County: L;V"8Al Phone No. 70 y - Q99 - y 11 Inspector: Q At"0"J_.,z—M--.D.3G-"!2 Date of Inspection: / l • q - % Time of Inspection: 6 6 /4 .,-n Total Event Precipitation (inches) a.L15 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least '72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DEMLR al Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. y�-� Structure (pipe, ditch, etc.): ,L./ jG1) Receiving Stream: /�►' oh�� sow CrG�,'% Describe the industrial activities that occur within the outfall drainage area: l' a u erg vU�- ✓l h!5,-xG e5 . CISAW Page 1 of 2 SWU-242, Last modified 07/28/2017 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: / ��h, it 12! QWV 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): /VO V GF 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 0 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with Gloating solids• 63 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: I 1 2 3 4 5 7. Is there any foam in the stormwater discharge? () Yes 8. Is there an oil sheen in the stormwater discharge? ()Yes No. 9. Is there evidence or erosion or deposition at the outfalI? o Yes �To. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 3 Environmental Quality Stormwater Discharge Outfall (SDO) Qualitative Monitoring Report For guidance on filling out this form, please visit https://deq.nc.gov/about/divisions/energy-mineral-land- resources/energy-mineral-land-permits/stormwater-permits/npdes-industrial-sw#tab-4 Permit No.: N/C/ 5/ 0/0 / 0 /3 / 3 / o/ or Certificate of Coverage No.: N_/C/G/_/_/_/_/_/_/ Facility Namc: lq / I jpf r—i R41 %1kUkC/L1,A915 County: _s(�/j/! 4/ Phone No. 76) 41- A $q -'Y5 // Inspector: :IAm L.S InO f 6I2 Bate of Inspection• // - El Time of Inspection: ; .3 5 .4m Total Event Precipitation (inches): 0 , y5 All permits require qualitative monitoring to be performed during a "measurable storm event." A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous ineasui able 5tottn event inust have been at least 72 houis piioi. The 72-houi stotut interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local D MLR Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: (Signature of Permittee or 1. Outfall Description: Outfall No. JU) b Receivin Streant Structure (pipe, ditch, etc.): Do'�-L, h g Alcbfmdso,✓ C Describe the industrial activities that occur within SWU-242, Last modified 07/28/2017 outfall drainage area: 4A6r-Ae.x' Page I of 2 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): IVOAA G 4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: r 1 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 0 2 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 .2 3 4 5 7. Is there any foam in the stormwater discharge? () Yes No. 8. Is there an oil sheen in the stormwater discharge? ()Yes o. 9. Is there evidence of erosion or deposition at the outfall? O Yes 0<0. 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 07/28/2017 aceAnalytical www.pacelabs.com f November 06, 2018 Mr. Preston Baucom Allvac 2020 Ashcraft Ave Monroe, NC 28110 RE: Project: MONROE S I ORMWAI ER Pace Project No.: 92404952 Dear Mr. Baucom: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on October 26, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Mr. Joe Hinkle, Allvac Mr. Tommy Long, Allvac Scott Ryan, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 14 aceAnalytical www.pacelabs.com r Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: MONROE STORMWATER Pace Project No.: 92404952 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2226 Riverside Drivo, Aehovillo, NC 28804 North Carolina Wastewator C:ortifcntion * 40 Florida/NELAP Certification #: E81648 South Carolina Certification #: 99030001 Massachusetts Certification #: M-NC030 VirginiaNELAP Certification #: 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 14 ;acieAnalytical Pace Analytical Services, LLC a 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com I (704)875-9092 SAMPLE ANALYTE COUNT Project: MONROE STORMWATER Pace Project No.: 92404952 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92404952001 SW02 EPA 1664B JMS 1 PASI-C EPA 200.7 Rev 4.4 1994 DS 5 PASI-A SM 2540D-2011 CEH 1 PASI-A SM 521OB-2011 RLO 1 PASI-A SM 52201) 2011 rC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 14 Pace Analytical Services, LLC © 9800Suite ceAnalytical Hunte svlle, C28078 a www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: MONROE STORMWATER Pace Project No.: 92404952 Sample: SW02 Lab ID: 92404952001 Collected: 10/26/18 05:20 Received: 10/26/18 10:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By JM 1 10/26/18 05:21 Collected Date 10/26/18 1 10126/18 05:21 Collected Time 05:10 1 10/26/18 05:21 pH 7.0 Std. Units 0.10 I 10/26/18 05:21 Temperature 14 deg C 0.50 1 10/26/18 05:21 HEM, Oil and Grease Analytical Method. EPA 1004E Oil and Grease 5.1 mg/L 4.8 1 11/06/18 05:16 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Cadmium ND ug/L 1.0 1 10/27/18 05:34 10/29/18 03:07 7440-43-9 Chromium 21.6 ug/L 5.0 1 10/27/18 05:34 10/29/18 03:07 7440-47-3 Lead ND ug/L 5.0 1 10/27/18 05:34 10/29/18 03:07 7439-92-1 Nickel 109 ug/L 5.0 1 10/27/18 05:34 10/29/18 03:07 7440-02-0 Zinc 355 ug/L 10.0 1 10/27/18 05:34 10/29/18 03:07 7440-66-6 2840D total Suspended Solids Analytical Method: SM 2540U-201 1 Total Suspended Solids 386 mg/L 50 1 10/30/18 01:59 5210E BOD, 5 day Analytical Method: SM 521 OB-2011 BOD, 5 day 16.0 mg/L 2.0 1 10/27/18 01:32 11/01/18 02:12 L2 5220D COD Analytical Method: SM 5220D-2011 Preparation Method: SM 5220D-2011 Chemical Oxygen Demand 73.6 mg/L 25.0 1 10/31/18 15:00 11/01/18 17:23 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 14 aceAnalXical www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 440476 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92404952001 METHOD BLANK: 2419432 Matrix: Water Associated Lab Samples: 92404952001 Mink Repurlhig Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/1 ND 48 11106/18 05-13 LABORATORY CONTROL SAMPLE: 2419433 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 38.5 36.4 95 78-114 MATRIX SPIKE SAMPLE: 2419434 92404994002 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Llmlts Qualifiers Oil and Grease mg/L ND 38.5 37.6 97 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 14 Pace Analytical Services, LLC �100 ce AHnalytical@ 9800 Kincey Ave. Suite Huntersville, NC 28078078 f www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 438752 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Associated Lab Samples: 92404952001 METHOD BLANK: 2412034 Matrix: Water Associated Lab Samples: 92404952001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cadmium ug/L ND 1.0 10/29/18 03:51 Chromium ug/L ND 5.0 10/29/18 03:51 Lead ug/L ND 5.0 10/29/18 03:51 Nickel ug/L ND 5.0 10/29/18 03:51 Zinc ug/L ND 10.0 10/29/18 02:14 LABORATORY CONTROL SAMPLE: 2412035 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Cadmium ug/L 500 497 99 85-115 Chromium ug/t 600 401 08 85116 Lead ug/L 500 497 99 85-115 Nickel uq/L 500 496 99 85-115 Zinc ug/L 500 516 103 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2412036 2412037 MS MSD 92404821001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 486 483 97 96 70-130 1 Chromium ug/L ND 500 500 476 476 95 95 70-130 0 Lead ug/L ND 500 500 472 470 94 94 70-130 0 Nickel ug/L 7.4 500 500 480 476 94 94 70-130 1 Line ug/L 3/9 bo0 500 862 852 9/ 9b /0-130 1 MAIRIX SPIKE & MAIKIX SPIKE DUPLICATE. 2412038 MS 92404952001 Spike Parameter Units Result Cone. Cadmium ug/L ND 500 Chromium ug/L 21.6 500 Lead ug/L ND 500 Nickel ug/L 109 500 Zinc ug/L 355 500 2412039 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 500 493 484 99 97 70-130 2 500 505 497 97 95 70-130 1 500 485 476 97 95 70-130 2 500 602 588 99 96 70-130 2 500 853 850 100 99 70-130 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Qua] Page 6 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 439068 Analysis Method: SM 2540D-2011 QC Batch Method: SM 2540D-2011 Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92404952001 METHOD BLANK: 2413197 Associated Lab Samples: 92404952001 raromotor Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 2413198 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 2413199 Parameter Unit6 Total Suspended Solids mg/L SAMPLE DUPLICATE: 2413200 Parameter Total Suspended Solids Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 m'10/30/18 01:51 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 254 101 90-110 92404991002 Dup Rebuil Rubull RPD Qualiners 10.4 13.4 25 D6 92404958002 Dup Units Result Result mg/L 40.8 41.6 RPD Qualifiers 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 14 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 438745 Analysis Method: SM 521 OB-2011 QC Batch Method: SM 521 OB-2011 Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92404952001 METHOD BLANK: 2412018 Associated Lab Samples: 92404952001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 2412019 Parameter Units BOD, 5 day mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result t imit Analyzed Qualifiers ND 2.0 11/01/18 02:08 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 198 153 77 84.6-115 L2 SAMPLE DUPLICATE: 2412021 92405075001 Dup Parameter Units Result Result BOD, 5 day mg/L 685 676 RPD Qualifiers 1 B1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall riot be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 14 an eAnalytical j www.pacelabs.com I Project: MONROE STORMWATER Pace Project No.: 92404952 QC Batch: 439481 QC Batch Method: SM 5220D-2011 Associated Lab Samples: 92404952001 METHOD BLANK: 24.15039 Associated Lab Samples: 92404952001 Parameter Units Chemical Oxygen Dwnarid rng/L QUALITY CONTROL DATA Analysis Method: SM 5220D-2011 Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 'I'I/01PI8 '1 /:20 Pace Analytical Services, LLC 9800 KinceyAve. Suite too Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 2415040 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 748 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2415041 2415042 MS MSD 92404515005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 92.2 100 100 193 186 101 93 90-110 4 R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2415043 2415044 MS MSD 92405151001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD QUal Chemical Oxygen Demand mg/L 52.2 100 100 151 140 99 88 90-110 7 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 14 aceAnaljltical www.pacelabs.com QUALIFIERS Project: MONROE STORMWATER Pace Project No.: 92404952 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantltatlon Limit. RL Reporting Lii nit The luwust ouncentrutlun value that meets project requirements for quantitative data with known precision and blab ror a bpeulno analyte In a spucitic matrix. - Surrogate 1,2-Uiphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SO Silica Gal Clean Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyi ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS 131 Less than 1.0 mq/L DO remained for all dilutions Fret. The reported value is an estimated greater than value and is calculated for the dilution using the least amount of sample. U6 the precision between the sample and sample duplicate exceeded laboratory control limits. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/06/2018 01:03 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 14 �- aceAnaIX cal ( www.pacelabs.com I QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: MONROE STORMWATER 92404952 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92404952001 SW02 92404952001 SW02 EPA 1664B 440476 92404952001 SW02 EPA 200.7 Rev 4.4 1994 438752 EPA 200.7 Rev 4.4 1994 438781 92404952001 SW02 SM 2b40U-2011 439068 92404952001 SW(12 SM 521OB-2011 438745 SM 521OB-2011 438770 92404962001 SW02 SM 5220D-2011 439481 SM 5220D-2011 439841 Date: 11/06/2018 01:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 14 Document Name: Document Revised: February 7, 2018 M aceAnalytical 5ampte Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: FCAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville.[Q Raleigh❑ Mechanicsville❑ Client Name: Project R '" o 9 04952 Courier: []Fed Ex ❑UPS QUSPS QCiient ❑ Commercial [)Pace ❑Other: 92404952 Custody Seal Present? QYes ONo sea is intact? ❑Yes []No,,it Date/Initials Person Examining Contents: ( c) Packing Material: nBubbte Wrap DBubble Bags (1None n Other Biological Tissue Frozen? Thermometer: QYes FlNo ❑N/A IR lion ID. 92TO45 Type of Ice: ❑Wet ❑Blue (-)Nona Cooler Tamp ('C): Correction Factor! Add/vubtract (°C) 1 � } Temp should be above freezing to 6°C Cooler Temp Corrected ('C): i,,, ❑Samples out of temp criteria. Samples on ice, cooling process has begun USDA Regulated Soil (0 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, nYes nNo including Hawaii and Puerto Rico)? nYes f_1No Cam ments/Discrepancy: Chain of Custody Present? Elves ❑Nu ❑N/A 1. Samples Arrived within Hold Time? ❑Yes ❑No N/A 2. Short Hold Time Analysis (<72 hr.? _ . Rush Turn Around Time Requested? Yes 0yes LJNo DNo QN/A ❑N/A 3. 4. Sufficient Volume? 0-Yes No ❑N/A S. Correct Containers Used? -Pace Containers Used? ❑ves 0 Yes ❑No []No []N/A ❑N/A 6. Containers Intact? °- ves No N/A 7• Dissolved analysis: Samples Field Filtered? ❑Yes ❑No ❑N/A 8. Sample Labels MatchCOC? -Includes Date/Time/ID/Analysis Matrix: ❑Yes []No []NIA 9. Headspace in VOA Vials (>5-6mm)? ❑Yes No - N%A 10. Trip Blank Present? Trip Blank Custody Seals Present? nYms ❑Yes (�[N0 QNo nN/A ❑N/A 11 COMMENTS/SAMPLE [DISCREPANCY Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Field Data Required? (-(Yes nNo Project Manager SCURF Review: r`l Date: ;� f. t Ztf, IF -i 9 Project Manager SRF Review:_ Date: �, ;✓i � Page 12 of 14 Document Name: Document Revised: February 7, 2018 aceAnaixieal a Sample Condition Upon Recef t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev,OG Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechiorination Is Project verified and within the acceptance range for preservation samples, Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle WO#:92404952 IoN: MWB Due Date: 11/06/18 CLIENT: 92-Allvae NC a E a a� a V a tttlllE 3 v a m 077 a V a of NVet 3 M t� yyZ a li a N a m -J m w rt .+ a m V N E J v a m V g U a J o N a to a co bit ai U.. E eN-1 H 4 L m n V r' J E ,�., u v a m ° E E vz i u= V, Vy Q ; rf v E Q ;; ,-1 x N t7 z Q J o N m t? C. N Q t w1 Jj l9 fP yi J o N•M.r J� t7 v ", t7 0 > E 2 m t7 `r � E r- Ot W > J E m Q > t > E m W C a � a Q 0 ? 3 d � ? " t7 \ > A J E ervi f n a h G z u J E rq N a rn M g� U ^ J o f�V a. m Bp 95 w IL '-f E '�' Q c� Ln J E N D it p �! E o�+ G 1 t 2 i 3 ! i 4 5 \� I X, 5- 7 8 9 1D 11 12 N N\ Tt- -11 pH Adjustment Log for Preserved Samples Sample ID Type of preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Note, Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le, Out of hold, incorrect preservative, out of temp, incorrect containers. Page 13 of 14 E 0 B 0 U) cr a) E z 0 L.O 0 Zl 9 2 x L) cCS L ci ----------- Qvm 0 z z C) (NIA) Ei z 7--4 0 P31COS — (L w Apolno .gym iL (WOODI in 110 POA!03.36 (N/,k) allIJOILIO lenpIsaH o� ui dwal Av? N /A Ilse L SISAleuvt JaqlO HOBN IOH w ul IL 'bNH '><i "US'H I wasaidun r- pant Ix I xI I SUDNIVINOO JO # — —1 —1 —1 E NOUDE11100 IV dN31. 31dV%VS '-_A w CL 4� w Z3 z 0 0 X LU 2 L) w " 46 0 x Z w Ili W 3000 XWIVN S4 V) z w tu z :D Q 0 i�� V) w w In o IN #wall rN M o NPage 14 of