NCS000315_MONITORING INFO_20180327

STORMWATER DIVISION CODING SHEET
PERMIT NO.
CODzj�
DOC TYPE
❑FINAL PERMIT
'� MONITORING INFO
❑ APPLICATION
❑ COMPLIANCE
❑ OTHER
DOC DATE
❑ 201 � D�j
YYYYMMDD

?je5WW3/50
nexeo•
solutions
March 27, 2018
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center
Raleigh, North Carolina 27699-1612
Re: Semi -Annual Storm Water Sampling Results for Year 9, Period 1
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
RECEIVED
APR 0 4 2018
DENR-LAND QUALIFY
STORMWATER PERMITTING
RECEIVED
To Whom It May Concern: APR 0 4 2018
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring ev��l;L, Fin 1 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, Nort aro rna, on March 6,
2018, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315). Per
the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001 during a
representative storm event that consisted of 0,49 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at Harding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table 1.
Table 1
scharge Chara'ctcristic` �� 4 4
Inspection Result
Color
Slight brown
Odor
None observed
Clarity
Slightly cloudy
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Stormwater Pollution
No significant change
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
NexeoSolutions.com ( Connect.

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nexeoe
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value with the exception of pH of 3.62 detected in the field, which is unusual compared to previous
monitoring events from the past three years. Records indicate that the field meter used to analyze pH was properly
calibrated. The lab reported pH as 7.2, and although outside of 15 minute hold time, this result is more consistent
with previous monitoring events. No spills or significant change in operations was identified and all other
parameters were within benchmark values. Thus, the low field pH detected on March 6, 2018, appears to be an
anomalous pH reading. However, in accordance with Tier One benchmark protocol, the facility will conduct a
stormwater inspection to identify possible causes of the pH exceedance and follow the corrective action procedure
accordingly.
All of the results of the storm water sample analyses along with their corresponding benchmark values as listed in
the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
DischArge Characteristic
u.. n...
Result
.;
Benchmark Value
Total Suspended Solids
43 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<2.6 mg/L
30 mg/L
Chemical Oxygen Demand
31 mg/L
120 mg/L
Toluene
<0.00I mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
3.62 (field reported) / 7.2 (lab reported)
6-9
Total Rainfall
0.49 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 9, Period 2) between July 1 and December 31, 2018, and will
submit the results per the requirements of the permit. Should you have any questions or require additional
information, please'contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions, LLC
NexeaSolutions.com 1 Connect.

TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT P�fl
TestAmerica Laboratories, Inc.
TestAmerica Savannah r'7'
5102 LaRoche Avenue L -�
Savannah, GA 31404
Tel: [phone]
o-
TestAmerica Job ID: 680-149643-1 r--
Client Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
For:
EHS Support, LLC
100 Georgia Ave
Daphne, Alabama 36526
Attn: Amy Bauer
Authorized for release by:
311512018 4:05:19 PM
Jerry Lanier, Project Manager I
[phone] e.3410
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNl requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: EHS Support, LLC TestAmerica Job U 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Table of Contents
Cover Page ..............................................
1
Table of Contents .........................................
2
Case Narrative......................I.....................
3
Sample Summary .........................................
5
Method Summary ...........................................
6
Definitions/Glossary .......................................
7
Detection Summary ........................................
8
Client Sample Results ......................................
9
Surrogate Summary .......................................
10
QC Sample Results ........................................
11
QC Association Summary ...................................
14
Lab Chronicle ............................................
15
Chain of Custody ..........................................
16
Receipt Checklists .........................................
17
Certification Summary ......................................
18
TestAmerica Savannah
Page 2 of 18 3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Job ID: 680-149643-1
Laboratory: TestAmerica Savannah
Narrative
Case Narrative
CASE NARRATIVE
Client: EHS Support, LLC
Project: Nexeo - Charlotte, N.C. (Outfall 001
Report Number: 680-149643-1
TestAmerica Job ID: 680-149643-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In the event of interference or analytes present at high concentrations, samples may be diluted. For diluted samples, the
reporting limits are adjusted relative to the dilution required.
RECEIPT
The samples were received on 03/07/2018; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.5 C.
VOLATILE ORGANIC COMPOUNDS (GC -MS)
Samples Outfall 001 (680-149643-1) and Trip Blank (680-149643-2) were analyzed for Volatile Organic Compounds (GC -MS) in
accordance with EPA Method 624. The samples were analyzed on 03/11/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch
680-515382.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
OIL AND GREASE AND TPH
Sample Outfall 001 (680-149643-1) was analyzed for Oil and Grease and TPH in accordance with EPA Method 1664A. The samples were
prepared and analyzed on 03113/2018.
Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MSIMSD/DUP) associated
with preparation batch 680-515578.
No analytical or quality issues were noted, other than those described above or in the Definition slGlossary page.
TOTAL SUSPENDED SOLIDS
Sample Outfall 001 (680-149643-1) was analyzed for total suspended solids in accordance with SM 2540D. The samples were analyzed
on 03/13/2018.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CHEMICAL OXYGEN DEMAND
Sample Outfall 001 (680-149643-1) was analyzed for chemical oxygen demand in accordance with SM 5220D. The samples were
analyzed on 03/13/2018,
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
CORROSIVITY (PH)
Sample Outfall 001 (680-149643-1) was analyzed for corrosivity (pH) in accordance with SM 4500 H+ B. The samples were analyzed on
TestAmerica Savannah
Page 3 of 18 3/15/2018

Case Narrative
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.G. (Outfall 001)
Job ID: 680-149643-1 (Continued)
Laboratory: TestAmerica Savannah (Continued)
03/1412018.
TestAmerica Job ID: 680-149643-1
This analysis is normally performed in the field and has a method -defined holding time of 15 minutes. This sample(s) was performed in
the laboratory outside the 15 minute timeframe.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TestAmerica Savannah
Page 4 of 18 3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Lab Sample ID Client Sample ID
680-149643-1 Outfali 001
680-149643-2 Trip Blank
Sample Summary
Matrix
Water
Water
TestAmerica Job ID: 680-149643-1
Collected Received
03/06/ 88 13:46 03/07/18 09:20
03/06/18 13:46 03/07/18 09:20
TestAmerica Savannah
Page 5 of 18 3/15/2018

Method Summary
Client: EHS Support, LLC
ProjeGUSite: Nexeo - Charlotte, N.C. (Outfall 001)
Method
Method Description
624
Volatile Organic Compounds (GC)MS)
1664A
HEM and SGT-HEM
SM 2540D
Solids, Total Suspended (TSS)
SM 4500 H+ B
pH
SM 5220D
COD
12
TestAmerica Job ID: 680-149643-1
1664A
SM
SM
SM
Protocol References:
1664A = EPA-821-98-002
40CFR136A = "Methods for Organic Chemical Analysis of Municipal Industrial Wastewater', 40CFR, Part 136, Appendix A, October 26, 1984 and
subsequent revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater,
Laboratory References:
TAIL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
-
;
Laboratory
TAL SAV
TAL SAV
TAL SAV
TAL SAV
TAL SAV R11
[Ifl
`�I
TestAmerica Savannah
Page 6 of 18
3/15/2018

Definitions/Glossary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (outfall 001)
Qualifiers
General Chemistry
Qualifier Qualifier Description
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present In this report.
o Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DOD/DOE)
LOQ Limit of Quantitation (DcD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
NO Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
Rt. Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEO Toxicity Equivalent Quotient (Dioxin)
TestAmerica Job ID: 680-149643-1
TestAmerica Savannah
ff 19
Page 7 of 18 3/15/2018

Detection Summary
RI
Client: EHS Support, LLC
TestAmerica Job ID: 680-149643-1
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
F
Client Sample ID: Outfall 001
Lab Sample ID: 680-149643-1
Analyte
Result Qualifier NONE NONE
Unit
Di Fac D Method Prep Typo
Rffl
pH
7.2 HF
SU
1 SM 4500 H+ B TotallNA
Analyte
Result Qualifier RL MDL
Unit
DI Fac D Method Prep Type
Chemical Oxygen Demand
31 10
mg1L
1 SM 5220D Total/NA
Analyte
Result Qualifier RL RL
Unit
Di Fac D Method Prop Type
Total Suspended Solids
43 5.0
mg/L
1 SM 2540D TotallNA
L
Client Sample ID: Trip Blank
Lab Sample ID: 680-149643-2
.
LTI)
C No Detections.
This Detection Summary does not include radiochemical test results.
TestAmerica Savannah
RM
E�Ij
Page 8 of 18 3/15/2018

Client Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: Outfall 001
Date Collected: 03106/1813:46
Date Received: 03107118 09:20
Method: 624 - Volatile Organic Compounds (GC1MS)
Analyte
Result Qualifier
RL
MDL Unit D
Toluene
<1.0
1.0
ug/L
Toluene
<1.0
1.0
ug/L
Xylenes, Total
<2.0
2.0
ug1L
Xylenes, Total
<2.0
2.0
ug/L
Surrogate
Toluenetl8 (Surr)
Toluene -dB (Surr)
1,2-Dichloroethane-d4 (Surr)
1,2-Dichloroethane-d4 (Surr)
4-8romoRuorobenzene (Surr)
4-BromoRuorobenzene (Surr)
Dibromofluoromethane (Surr)
Dibromofiuoromethane (Surr)
General Chemistry
Analyte
pH
Analyte
HEM (Oil & Grease)
Chemical Oxygen Demand
Analyte
Total Suspended Solids
%Recovery Qualifier
9B
101
104
103
100
97
96
99
Limits
79 - 119
79 - 119
70 - 130
70 - 130
71 - 121
71 - 121
77 - 129
77 - 129
Result Qualifier
NONE
7.2 HF
Result Qualifier
RL
<2.6
2.6
31
10
Result Qualifier
RL
43
5.0
NONE Unit D
Su
E
TestAmerica Job ID: 680-149643-1
Lab Sample ID: 680-149643-1
121
Matrix: Water
E
Prepared Analyzed
Dil Fac
03/11/18 16:37
1
03111/1817:00
1
03/11/18 1
1
03111118 17::0000
1
Prepared Analyzed
Dil Fac
C
a
03/1 }/18 1b:37
1
03111118 17:00
1
�J
03111118 16:37
1
w
0311111817,00
1
03/11/18 16:37
1
03/11/18 17. 00
1
03111118 16:37
1
03/11/18 17: 00
1
Prepared Analyzed
Dil Fac
03/14118 17:14
1
U.
MDL Unit D Prepared Analyzed Di Fac
mg/L 03/13118 08:21 03/13/18 11:07 1
mg/L 03/13/18 15:26 1
RL Unit D Prepared Analyzed DII Fac
mg/L 0311311813:15 1
Client Sample ID: Trip Blank Lab Sample ID: 680-149643-2
Date Collected: 03/06118 13:46 Matrix: Water
Date Received: 03107M8 09:20
Method: 624 - Volatile Organic Compounds (GC1MS)
Analyte Resutt Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Toluene <1.0 1.0 ug/L 03/11/1813:56 1
Xylenes, Total <2.0 2.0 ug/L 03/11/18 13:56 1
Surrogate
Toluene -de (Surr)
1,2-Dichloroethane-d4 (Surr)
4-Bromolluorobenzene (Surr)
Dibromolluoromethane (Surr)
%Recovery Qualifier
Limits
Prepared Analyzed
Dil Fac
99
79 - 119
03111118 13:56
1
103
70 - 130
03/11/18 13:56
1
97
71-121
03111118 13:56
1
96
77- 129
03111118 13:56
1
TestAmerica Savannah
Page 9 of 18 3/15/2018

Surrogate SummaryTestAmerica
HI
Client: EHS Support, LLC
Job ID: 680-149643-1
�-
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
I ;1
Method: 624 - Volatile Organic Compounds (GC/MS)
Matrix: Water
Prep Type: Total/NA
El
Percent Surrogate Recovery (Acceptance Limits)
TOL
DCA
BFB
DBFM
Lab Sample ID Client Sample ID
(79.119)
(70-130)
(71-121)
(77-129)
680-149643-1 Outfall001
98
104
100
96
680-149643-1 Oulall001
101
103
97
99
0
680-149643-2 Trip Blank
LCS 680-515382l3 Lab Control Sample
99
95
103
95
97
97
96
91
L
LCSD 680-51538214 Lab Control Sample Dup
98
99
101
95
MB 680-51538218 Method Blank
100
103
97
97
Surrogate Legend
51
TOL = Toluene-d8 (Surr)
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
j
DBFM = Dibromofluoromethane (Surr)
TestAmerica Savannah
Page 10 of 18 3/15/2018

QC Sample Results
7
Client: EHS Support, LLC
TestAmerica Job ID: 680-149643-1
r-
ProjectlSite: Nexeo - Charlotte, N.C. (Outfall 001)
{
Method: 624 -Volatile Organic Compounds (GC/MS)
Lab Sample ID: MB 680-51538218
Client Sample ID: Method Blank
R
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 515382
M
MB MB
Analyte
Result Qualifier
RL MDL Unit
D Prepared Analyzed Dil Fee
ICE
usne
<1.0
1.0 ugiL
03/11/1813:10 1
Xylenes, Total
<2.0
2.0 uglL
03111/18 13:10 1
yy�
IJ
ma ma
Surrogate
%Recovery Qualifier
Limits
Prepared Analyzed Dil Fac
r --
Toluen"S (Surr)
100
79 - 119
03/11/18 13:10 1
1,2-Oichloroethane-d4 (Surf)
103
70 - 130
03/11/18 13:10 1
4-Bromoftuorobenzene (Surr)
97
71 - 121
03/11/18 13:10 1
DibromoRuoromethane (Surr)
97
77 - 129
03/11/18 13AD 1
'I
Lab Sample ID: LCS 680-51538213
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: TOtalINA
Analysis Batch: 515382
Spike
LCS LCS
Analyte
Added
Result Qualifier
Unit
Toluene
20.0
19.2
uglL
Xylenes, Total
40.0
39.9
uglL
LCS LCS
Surrogate %Recovery Qualifier
Limits
roluene-d8 (Surr)
95
79 - 119
1,2-0ichloroethane-d4 (Stirr)
95
70 - 130
4-Sromolluorobenzene (Surr)
97
71 - 121
Dibromohuoromethane (Surr)
91
77- 129
Lab Sample ID: LCSD 680-515382I4
Matrix: Water
Analysis Batch: 515382
Spike
LCSD LCSD
Analyte
Added
Result Qualifier
Unit
Toluene
20.0
19.9
ugtL
Xylenes, Total
40,0
41.7
uglL
LCSD LCSD
Surrogate %Recovery Qualifier Limits
Toluene-d& (Surr) 98 79 - 119
1,2-Dichloroethana-d4 (Surr) 99 70- 130
4.Sromotiuorobenzene (Surr) 101 71 - 121
Dibromoffuoromethane (Surr) 95 77.129
Method: 1664A - HEM and SGT-HEM
Lab Sample ID: MB 680-51557811-A
Matrix: Water
Analysis Batch: 615643
Analyte
HEM (Oil & Grease)
IUIB MB
Result Qualifier RL MDL Unit
<5.0 5.0 mglL
% Rec.
NAM
D %Rec Limits
96 47 - 154
100 78 - 119
Client Sample ID: Lab Control Sample Dup
Prep Type: TOtalINA
%Rat. RPD
D %Roc Limits RPD Llmit
100 47 - 150 4 30
104 78-119 4 30
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 515578
D Prepared Analyzed DII Fee
03/13/18 08:21 03/13/18 11:07 1
TestAmerica Savannah
Page 11 of 18 3/15/2018

Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
QC Sample Results
TestAmerica Job ID: 680-149643-1
i i71.
L_._1
Method: 1664A - HEM and SGT-HEM (Continued)
Lab Sample ID: LCS 680-515578/2-A
Client Sample ID: Lab Control Sample
11A
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 515643
Prep Batch: 515578
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Roe Limits
He
HEM (Oil & Grease)
40.0
34.60
mglL 86 78 - 114
Lab Sample ID: LCSD 680-515578/3-A
Client Sample ID: Lab Control Sample Dup
!
Matrix: Water
Prep Type: TotalINA
Analysis Batch: 515643
Prep Batch: 515578
RE
Analyte
Spike
Added
LCSD LCSD
Result Qualifier
%Rec. RPD
Unit D %Rec Limits RPD Limft
HEM (Oil & Grease)
40.0
33.20
mglL 83 78 - 114 4 18
1'Uii1i
Method: SM 2540D - Solids, Total Suspended (TSS) --
Lab Sample ID: MB 680-51568911 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 516689
MB MB
Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Far -
Total Suspended Solids c1.0 1.0 mglL 03/13/18 13:15 1
Lab Sample ID: LCS 680-51568912 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type. Total/NA
Analysis Batch: 515689
Spike LCS LCS %Rec.
Analyte Added Result Quallfier Unit D %Rec Limits
LTotal Suspended Solids
Lab Sample ID: LCSD 680-51568913
Matrix: Water
Analysis Batch: 615689
Analyte
Total Suspended Solids
Lab Sample ID: 680-149643-1 DU
Matrix: Water
Analysis Batch: 615689
Sample Sample
Analyto Result Qualifier
Total Suspended Solids 43
20.0 24.0 mglL 120 80 - 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD %Rec. RPD
Added Result Qualifier Unit D %Rec Limits RPD Limit
20.0 24.0 mglL 120 80 - 120 0 25
Client Sample ID: Outfall 001
Prep Type: Total/NA
DU DU RPD
Result Qualifier Unit D RPD Limit
42.5 mglL T 1 5
Method: SM 4500 H+ B - pH
Lab Sample ID: LCS 680-515940/6 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 515940
Spike LCS LCS %Rec.
Analyte Added Result Qualifier Unit D %Rec Limits
pH 7,00 7,1 SU 101 63 - 158
TestAmerica Savannah
Page 12 of 18
3/15/2018

QC Sample Results
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfali 001)
TestAmerica Job ID: 680-149643-1
f �
Method: SM 5220D - COD
'
FLab Sample ID: M8 680-51572413
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 515724
MB MB
Analyte Result Qualifier RL MDL Unit
D Prepared Analyzed DII Fac
FC.
Chemical Oxygen Demand <10 10 mg/L
03/13118 15:26 1
Lab Sample ID: LCS 680-51572414
Client Sample ID: Lab Control Sample
C�
Matrix: Water
Prep Type: TotaVNA
Analysis Batch: 515724
j
Spike LCS LCS
Anaiyte Added Result Qualifier Unit
%Rec.
0 %Rec Limits
Chemical Oxygen Demand 50,o 51.3 mg1L
103 90 - 110
W `d
s
,h
TestAmerica Savannah
Page 13 of 18 3/15/2018

QC Association Summary
Client: E=HS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
GCIMS VOA
Analysis Batch: 515382
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-149643-1
Outfall 001
Total/NA
Water
624
680-149643-1
Outfall 001
Total/NA
Water
624
680-149643-2
Trip Blank
Total/NA
Water
624
MB 680-51538218
Method Blank
Total/NA
Water
624
LCS 680-515382/3
Lab Control Sample
TotalINA
Water
624
LCSD 680-51538214
Lab Control Sample Dup
Total/NA
Water
624
General Chemist
Prep Batch: 515578
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method .
680-149643-1
Ouffall001
TotaYNA
Water
1664A
MB 680-51557811-A
Method Blank
Total/NA
Water
1664A
LCS 680-515578/2-A
Lab Control Sample
Tota11NA
Water
1664A
LCSD 680-51557a13-A
Lab Control Sample Dup
Tota11NA
Water
1664A
Analysis Batch: 515643
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-149643-1
Ouffall001
Total/NA
Water
1664A
MB 680.51557811-A
Method Blank
TotalINA
Water
1664A
LCS 680-51557812-A
Lab Control Sample
Total/NA
Water
1664A
LCSD 680-51557813-A
Lab Control Sample Dup
Total/NA
Water
1664A
Analysis Batch: 515689
Lab Sample ID
Cl lent Sample ID
Prep Type
Matrix
Method
68D-149643-1
Outfall 001
Total/NA
Water
SM 2540D
MB 680-515689/1
Method Blank
Total/NA
Water
SM 2540D
LCS 680-51568912
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-51568913
Lab Control Sample Dup
Total/NA
Water
SM 2540D
680-149643-1 DU
Outfall 001
Total/NA
Water
SM 2540D
Analysis Batch: 515724
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
68D-149643-1
Outfall 001
Total/NA
Water
SM 52200
MB 680-515724/3
Method Blank
Total/NA
Water
SM 52200
LCS 680-51572414
Lab Control Sample
TotalINA
Water
SM 5220D
Analysis Batch: 515940
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
680-149643-1
Outfall 001
Total/NA
Water
SM 4500 H+ B
LCS 680-51594016
Lab Control Sample
Total/NA
Water
SM 4500 H+ B
RI
TestAmerica Job ID: 680-149643-1 [j]3
Prep Batch IN
V
Prep Batch m
Prep Batch I
515578
515578
515578
515578
Prep Batch
Prep Batch
Pren Ra+ch
TestAmerica Savannah
Page 14 of 18 3/15/2018

.. ., .', l: � � ...
.. :'�.:�
J _
{
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y.

Client: EHS Support, LLC Lab Chronicle TestAmerica Job ID: 680-149643-1 [i]
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Client Sample ID: Qutfall 001
Date Collected: 0310611813:46
Date Received: 03107/18 09:20
Batch Batch DII Initial Final Batch
Prep Type Typo Method Run Factor Amount Amount Number
TataVNA Analysis 624 1 5 mL 5 mL 515382
Instrument ID: CMSC
Total/NA Analysis 624
1
5 mL
Instrument ID: CMSC
Total/NA Prep 1664A
965 mL
Total/NA Analysis 1664A
1
Instrument ID: NOEQUIP
Total/NA Analysis SM 2540D
1
2D0 mL
Instrument ID: NOEQUIP
TotaIINA Analysis SM 4500 H+ 6
1
Instrument ID: MANTECH
Total/NA Analysis SM 52200
1
2 mL
Instrument ID: SPC7
Client Sample ID: Trip Blank
Date Collected: 0310611813:46
Date Received: 03/07/18 09:20
Batch Batch
Dil
Initial
Prop Type Type Method Run
Factor
Amount
TotaI1NA Analysis 624
1
5 mL
Instrument Q: CMSC
Laboratory References:
TAL SAV = TestAmerica Savannah, 5102 LaRoche Avenue, Savannah,
GA 31404, TEL [phone]
Page 15 of 18
5 mL 515382
500 mL 515578
515643
1000 mL 515689
515940
2 mL 515724
Final Batch
Amount Number
5 mL 515382
Lab Sample ID: 680-149643-1
Matrix: Water
Prepared
or Analyzed
Analyst
Lab'
TAL SAV
03111l18 16:37
WAS
03I11118 17:00
WAS
TAL SAV
03/13118 08:21
JAS
TAL SAV
o
=13M8 11:07
JAS
TAL SAV
(❑
i~J
03113118 13:15
JEC
TAL SAV
03/14/18 17:14
JEC
TAL SAV
03/13118 15:26
JER
TAL SAV
4�
Lab Sample ID: 680-149643-2
Matrix: Water
Prepared
or Analyzed Analyst Lab
03/11/18 13;56 WAS TAL SAV
TestAmerica Savannah
3/15/2018

CO
NE
TestAmerica Savannah
5102 LaRoChe Avenue
Savannah, GA 31404
Phone [phone]a Fax [phone]
Chain of Custody Record
TestAmedca
%*+E t EAVES +N [ur+pptruE`� AL iC 11+M1
samcter
Lao PM.
Coma Trac-m rtols)
COC No:
Client Information
Adam Michalak .
Jerry Lanier
ct n" contact-
1(251)
PhOM
E-Mat'
Pape.
Amy Bauer
533.6949
[e-mail]
Page 1 of 1
Ganparq.
EHS Support• LLC
Anal sis Requested
Job a.
Address,
728S:Green Street
Doe Oate Reaucsted:„,
.
�
PreservasionCddY
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TAT Requested (days):
State. Z+a:
NC, 27101
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F - M*CIH R - Ma25251 �
Pr�1,�e;
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[phone]
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sample
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sae Identification
Special InstructionslNoto:
_
• �
Preservation Code:
Outfatl 001
Mlid
G
Water
N
X
X
X
X
X
Subsampte p8 from TSS bottle
Trip Blank
3I6118
�5� 0'
G
Water
N
X
i
680-149643 Chain of Custody
Possible Hazard identification
Sa©le Disposal (A for mays assessed il' samples aretained longer than 1 month)
© Non -Hazard (:3 I Flammable '-Skin+ Irritant lrorson 8 Unkrmvm Ra0 diological
Return To Client Disposal By Lab Archive For Months
Delivefable Requested: I, fl, III, IV, Other (specify)
Special InstrvrtionVOC Requirements:
Empty Kit Relinquished by: hate: Time: aktrua of SnOrent
Reh..wistsd e'y: Adam "Mfialak
OR WrmB:
6I18 ��. 1Z
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Aoie4 f ug
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Custody Seats Intact:
Custody Seal No,,.
C w'rra' ;s)'C one OUW Remar`s O L, V
�4. Yes No
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116+� + I �PgP7.�-1 s'i S 1,:'. 3 i..U`_
l l r _. t. - - ..9 , __J t._,-.�..t I....a

Login Sample Receipt Checklist
Client: EHS Support, LLC Job Number: 680-149643-1
Login Number: 149643
List Source: TestAmerica Savannah
List Number: 1
Creator: Anderson, Jordan K
Question
Answer Comment
Radioactivity wasn't checked or is <1= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present. '
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
N/A
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
NIA
There is sufficient vol. for all requested analyses, incl. any requested
True
MSIMSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (114"),
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
NIA
TestAmerica Savannah
Page 17 of 18 3/15/2018

Accreditation/Certification Summary
Client: EHS Support, LLC
Project/Site: Nexeo - Charlotte, N.C. (Outfall 001)
Laboratory: TestAmerica Savannah
The accreditationsloertificationa listed below are applicable to this report.
Authority Program
North Carolina (VW/SW) State Program
EPA Region Identification Number
TestAmerica Job ID: 680-149643-1
Explratlon Data
12-31-18
TestAmerica Savannah
Page 18 of 18 3/15/2018

n m. X e a
solutions
March 6, 2017
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
I617 Mail Service Center
Raleigh, NC 27699-1617
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
SI CS 0',6 -0 3/S
Re: Semi -Annual Storm Water Sampling Results for Year 8, Period 1
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
RECEIVED
MAR 2 1 2017
CENTRAL FILES DWR SECTION
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 8, Period 1 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on February
15, 2017, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315).
Per the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001
during a representative storm event that consisted of 0.44 inches of total rainfall, as measured by the local United
States Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at Harding High School,
Charlotte, North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table 1.
Table 1
Diseharge Charactenstic ,",�
Inspeetaan,Result r
Color
Clear
Odor
None observed
Clarity
Clear -Cloudy
Floating Solids
None observed
Suspended Solids
None observed
Foam
Low
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Storm water Pollution
No significant change
NexeoSolutions.com I Connect.

jr' .
nexeo°
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value. The results of the stone water sample analyses along with their corresponding benchmark values
as listed in the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Disehs5arge Cliaracteiristki
_. .ud
rty�53A 91.3i.„+tl A ; r_-; P-
Result i "� R , ",
-� dL[.,rr',�,2,.`•-,l'��.'°�".4=Ei''",
Benchmark Value x, uL
xu..�.s..r=e.tr:-+-sn� nn, ...elf.
Total Suspended Solids
26 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<2.6 mg/L
30 mg/L
Chemical Oxygen Demand
22 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
6.2
6-9
Total Rainfall
0.44 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 8, Period 2) between July 1 and December 3I, 2017, and will
submit the results per the requirements of the permit. Should you have any questions or require additional
information, please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
���c/
✓7 Timothy ightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions, LLC
NexeoSolutions.com l Connect.

neAvveo°
solutions
January 8, 2018
3 Waterway Square Place
Suite 1000
The Woodlands. TX 77380
Division of Energy, Mineral and Land Resources
Stormwater Permitting Program
1612 Mail Service Center 0'(Raleigh, North Carolina 27699-1612
p,N 1
Re: Semi -Annual Storm Water Sampling Results for Year 8, Period 2 , WNGVNC�
Nexeo Solutions, LLC �NFflR��1oNp�6 1
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID ##NCD 061 263 315
To Whom It May Concern:
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 8, Period 2 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Car'o , on Dece r
5, 2017, as prescribed in the National Pollutant Discharge Elimination System (NPDES) perm' (NCS000315), P r
the requirements, the storm water sample was collected from the storm water discharge outfall • g a
representative storm event that consisted of 0.32 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at Harding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented below in Table 1.
Table 1
Discharge Characteristic
., Inspection Result
Color
Light (milky)
Odor
None observed
Clarity
Medium
Floating Solids •
None observed
Suspended Solids
None observed
Foam
Minimal
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Storm water Pollution
No significant change
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
NexeoSolutions.com I Connect,

neAveo°
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value. The results of the storm water sample analyses along with their corresponding benchmark values
as listed in the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Discha�rrge CharacEerts icwa
Result �„
Bench�mark�Ualu ���;"
Total Suspended Solids
22 milligrams/liter (mg/L)
100 nig/L
Oil and Grease
<4.6 mg/L
30 mg/L
Chemical Oxygen Demand
17 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0,002 mg/L
6.7 mg/L
pH
7
6-9
Total Rainfall
0.32 inches
Required to be> 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 9, Period 1) between January l and June 30, 2018, and will submit
the results per the requirements of the permit. Should you have any questions or require additional information,
please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexco Solutions, LLC
NexeoSolutivns.com ! Connect.

nexeo�
solutions
January 5, 2017
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
JAN I A 2017
CENTRAL FILES
DWR SECTION
Re: Semi -Annual Storm Water Sampling Results for Year 7, Period 2
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Nexco Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 7, Period 2 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on November
29, 2016, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315).
Per the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001
during a representative storm event that consisted of 0.35 inches of total rainfall, as measured by the local United
States Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at Harding High School,
Charlotte, North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table 1.
Table 1
Discharge Characteristic ..
Inspection Result
Color
Clear
Odor
None observed
Clarity
Clear
Floating Solids
None observed
Suspended Solids
None observed
Foam
Negligible
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Storm water Pollution
No significant change
NexeoSolutions.com I Connect.

4 �.
no,7, Ave, o�
solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value. The results of the storm water sample analyses along with their corresponding benchmark values
as listed in the permit are presented below in Table 2, and the laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
}::"; Result
'Benchmark Value
Total Suspended Solids
27 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<2.7 mg/L,
30 mg/L
Chemical Oxygen Demand
37 mg/L
120 mg/L
Toluene
<0.001 mg/L
0.055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
7.3
6-9
Total Rainfall
0.35 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 8, Period 1) between January 1 and June 30, 2017, and will submit
the results per the requirements of the permit. Should you have any questions or require additional information,
please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions, LLC
NexeoSolutions.com I Connect.

nexeo�
solutions
May 10, 2016
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Reel V
MAY 01016
Sr RMWA s'D Q�q�lrl,
pERI 17-rjNG
Re: Semi -Annual Storm Water Sampling Results for Year 7, Period 1
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
To Whom It May Concern:
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 7, Period 1 at the
Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North Carolina, on April 22,
2016, as prescribed in the National Pollutant Discharge Elimination System (NPDES) permit (NCS000315): Per
the requirements, the storm water sample was collected from the storm water discharge outfall (SDO) 001 during a
representative storm event that consisted of 0.16 inches of total rainfall, as measured by the local United States
Geological Survey (USGS) rain gage (number 351412080541245 CRN-53 at Harding High School, Charlotte,
North Carolina). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in Table 4 of
the NPDES permit. No atypical conditions were noted during the field inspection. In accordance with Section C. of
the permit, in the event that an atypical condition is noted at a stormwater discharge outfall, the permittee shall
document the suspected cause of the condition and any actions taken in response to the discovery in the Stormwater
Pollution Prevention Plan (SPPP). The inspection results are presented in Table 1.
Table 1
Discharge Characte'rishc it,y
Inspection Result
Color
Clear
Odor
None observed
Clarity
Clear -Cloudy
Floating Solids
None observed
Suspended Solids
None observed
Foam
Low
Oil Sheen
None observed
Erosion/Deposition at the Outfall
No significant change
Other Obvious Indicators of Storm water Pollution
No significant change
NexeoSolutions.eom ( Connect.

nexeo'D
Solutions
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip blank to the
Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total suspended solids, oil
and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the results exceeded its corresponding
benchmark value. The results of the storm water sample analyses along with their corresponding benchmark values
as listed in the permit are presented below in Table 2, and the laboratory results are included as Enclosure I .
Table 2
,, w� ': . � wo. k:.xw . � �,
Discharge Characteristic 1, w
• TYy* ',r ,„, a'y�„",x"rat"
.�
k t Resalt r _ *, h.i u
.fir s
f J g`rk hR. �-- � 4� 4. q € i£:_ +M
" Valae
. _ y=tBe�nchmark, d
Total Suspended Solids
10 milligrams/liter (mg/L)
100 mg/L
Oil and Grease
<4.7 mg/L
30 mg/L
Chemical Oxygen Demand
33 mg/L
120 mg/L
Toluene
<0.001 mg/L
0,055 mg/L
Xylenes, Total
<0.002 mg/L
6.7 mg/L
pH
7.35
6-9
Total Rainfall
0.16 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit is issued.
We will conduct the next monitoring event (Year 7, Period 2) between July I and December 31, 2016, and will
submit the results per the requirements of the permit. Should you have any questions or require additional
information, please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions
NexeoSolutions.com I Connect.

nexeo�
solutions
December 14, 2015
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
RECEIVED
DEC 1 '1.Z01S
CENTRAL FILES
DWR SECTION �0
Re: Semi -Annual Storm Water Sampling Results for Year 6, Period 2
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
Dear Ms. Cannon:
ino
ao�
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 6, Period
2 at the Nexco facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North
Carolina, on November 18, 2015, as prescribed in the National Pollutant Discharge Elimination System
(NPDES) permit CS000315). Per the requirements, the storm water sample was collected from the
storm water discharge out a ) 001 during a representative storm event that consisted of 0.67 inches
of total rainfall, as measured by the local United States Geological Survey (USGS) rain gage (number
351412080541245 CRN-53). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in
Table 4 of the NPDES permit. No atypical conditions were noted during the field inspection. In
accordance with Section C. of the permit, in the event that an atypical condition is noted at a stormwater
discharge outfall, the permittee shall document the suspected cause of the condition and any actions taken
in response to the discovery in the Stormwater Pollution Prevention Plan (SPPP). The inspection results
are presented in Table 1.
Table 1
Discharge Characteristic
Inspection Result
Color
Clear
Odor
None observed
Clarity
Clear
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
NexeoSolutions.com l Connect.

hc 5-0 0 0 C-3/ 5—
nexeo�
solutions
RECEIVED
DEC 17 Zu��
CENTRAL FILES
DWR SECTION
Table 1 (cont.)
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Discharge Characteristic
Inspection Result
Oil Sheen
None observed
Erosion/Deposition at the
Outfall
No significant change
Other Obvious Indicators
of Storm water Pollution
No significant change
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip
blank to the Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total
suspended solids, oil and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the
results exceeded its corresponding benchmark value. The results of the storm water sample analyses along
with their corresponding benchmark values as listed in the permit are presented below in Table 2, and the
laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
<1.0 milli rams/liter m /L)
100 m L
Oil and Grease
<4.7 m /L
30 m /L
Chemical Oxygen Demand
10 mg/L
120 m L
Toluene
<0.001 m L
0.055 m L
X lenes, Total
<0.002 m L
6.7 m /L
H
7.93
6-9
Total Rainfall
0.67 inches
Required to be > 0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit
is issued. We will conduct the next monitoring event (Year 7, Period 1) Between January 1 and June 30,
2016, and will submit the results per the requirements of the permit. Should you have any questions or
require additional information, please contact me at 704-391-6877.
Sincerely,
Nexeo Solutions, LLC
Awl,
Timothy Nightwine
Facility Manager
cc: Ed Graves, Nexeo Solutions
NexeoSolutions.com I Connect.

C5oaOL31r
9 e 3 Waterway Square Place
nexveoo The WOQo
the Woadfands, TX 77380
solutions
January 8, 2015 -�
fires auo-3/s
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVED
Re: Semi -Annual Storm Water Sampling Results for Year 5, Period 2
JAN 14 2015
Nexeo Solutions, LLC
CENTRAL FILES
3930 Glenwood Avenue
DWR SECTION
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
Dear Ms. Cannon:
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 5, Period
2 at the Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North
Carolina,_0 December 6, 2014 as prescribed in the National Pollutant Discharge Elimination System
(NPDES} permit er the requirements, the storm water sample was collected from the
storm water disc arge outfall (SDO) 001 during a representative storm event that consisted of 0.13 inches
of total rainfall, as measured by the local United States Geological Survey (USGS) rain gage (number
351412080541245 CRN-53). More than 72 hours of 0.00 inches of rainfall occurred prior to the sampling.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in
Table 4 of the NPDES permit. No atypical conditions were noted during the field inspection. In
accordance with Section C. of the permit, in the event that an atypical, condition is noted at a stormwater
discharge outfal I, the permittee shall document the suspected cause of the condition and any actions taken
in response to the discovery in the Stormwater Pollution Prevention Plan (SPPP). The inspection results
are presented in Table 1,
Table 1
Discharge Characteristic
Inspection Result
Color
Clear
Odor
No odor detected
Clarity
Clear
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
NexeoSolutions.coni I Connect,

crJ3 0,0

neAvve o ID
solutions
Table 1 (cont.)
3 Waterway Square Place
`Suite 1000
The Woodlands, TX 77380
Discharge Characteristic
Inspection Result
Oil Sheen
None observed
Erosion/Deposition at the
Outfal l
None observed
Other Obvious Indicators
of Storm water Pollution
None observed
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip
blank to the Test America, Inc. laboratory in Savannah, Georgia. The sample was then analyzed for total
suspended solids, oil and grease, chemical oxygen demand, toluene, total xylenes, and pH. None of the
results exceeded its corresponding benchmark value. The results of the storm water sample analyses along
with their corresponding benchmark values as listed in the permit are presented below in Table 2, and the
laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
6.5 milli rams/liter m /L
100 m /L
Oil and Grease
<2.5 m /L
30 m /L
Chemical Oxygen Demand
25 m /L
120 m /L
Toluene
<0.0010 m /L
0.055 m /L
X lenes, Total
<0.0020 m /L
6.7 m /L
H
7.20
6-9
Total Rainfall
0.13 inches
Required to be >
0.1 inches
Nexeo will continue semi-annual monitoring under the expired permit NCS000315 until the new permit
is issued. We will conduct the next monitoring event (Year 6, Period l) between January 1 and June 30,
2015, and will submit the results per the requirements of the permit. Should you have any questions or
require additional information, please contact me at 704-392-2121.
Sincerely,
Nexeo Solutions, LLC
��La 31A_1
Michael Trull
Plant Manager
NexeoSolutions.com I Connect,

:< " .
\ . y
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a

neAveom
solutions
April 7, 2014
Division of Water Quality
Surface Water Protection Section
Attention: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Semi -Annual Storm Water Sampling Results for Year 5, Period 1
Nexeo Solutions, LLC
3930 Glenwood Avenue
Charlotte, Mecklenburg County, North Carolina
EPA ID #NCD 061 263 315
Dear Ms. Cannon:
W/
3 Waterway Square lace
Suite 1000
The Woodlands, TX 77380
RECEIVED
APR 11 2014
CENTRAL FILES
DWQ/BOG
Nexeo Solutions, LLC (Nexeo) conducted the semi-annual analytical monitoring event for Year 5, Period
1 at the Nexeo facility located at 3930 Glenwood Drive in Charlotte, Mecklenburg County, North
Carolina, on March 3, 2014 as prescribed in the National Pollutant Discharge Elimination System
(NPDES) permit (NCS000315). Per the requirements, the sample of the stormwater discharge was
collected from the stormwater discharge outfall (SDO) 001 during a representative storm event that
measures greater than 0.1 inches of rainfall, as measured by the local United States Geological Survey
(USGS) rain gage (number 351412080541245 CRN-53). The representative storm event was preceded
by at least 72 hours in which no storm event measuring greater than 0.1 inches occurred.
During the sampling event, a visual inspection for qualitative monitoring was conducted as specified in
Table 4 of the NPDES permit. No atypical conditions were noted during the field inspection. In
accordance with Section C. of the permit, in the event that an atypical condition is noted at a stormwater
discharge outfall, the permittee shall document the suspected cause of the condition and any actions taken
in response to the discovery in the Stormwater Pollution Prevention Plan (SPPP). The inspection results
are presented in Table 1.
Table 1
Discharge Characteristic
Inspection Result
Color
Clear
Odor
None observed
Clarity
Clear
Floating Solids
None observed
Suspended Solids
None observed
Foam
None observed
Nexeo5olutions.com i Connect,

I
neAveo°
solutions
Table 1 (cont.)
3 Waterway Square Place
Suite 1000
The Woodlands, TX 77380
Discharge Characteristic
Inspection Result
Oil Sheen
None observed
Erosion/Deposition at the
Outfall
None observed
Other Obvious Indicators of
Storm water Pollution
None observed
The sample was collected in laboratory -supplied bottles, preserved with ice, and transported with a trip
blank overnight to the TestAmerica Laboratories, Inc. laboratory in Savannah, Georgia. The sample was
then analyzed for total suspended solids, oil and grease, chemical oxygen demand, toluene, total xylenes,
and pH. None of the results exceeded its corresponding benchmark value. The results of the stormwater
sample analyses along with their corresponding benchmark values as listed in the permit, and the total
rainfall amount, are presented below in Table 2. The laboratory results are included as Enclosure 1.
Table 2
Discharge Characteristic
Result
Benchmark Value
Total Suspended Solids
7 milli rams/liter m
100 m
Oil and Grease
<2.9 mgJL
30 m
Chemical Oxygen Demand
<10 m
120 m
Toluene
<0.0010 m
0.055 m L
X lenes, Total
<0.0020 m L
6.7 m
H
7.19
6-9
Total Rainfall
0.17 inches
Required to be
greater than 0.1
inches
Nexeo will conduct the Year 5, Period 2 monitoring event between July 1 and December 31, 2014, and
will submit the results per the requirements of the permit. Should you have any questions or require
additional information, please contact me at 704-392-2121.
Sincerely,
Nexeo Solutions, LLC
Michael Trull
Plant Manager
NexeoSolutrons.com I Connect.

Ashland Chemical
qlW
Environmental, Health & Safety
G. W. Hammer
Vice President
[phone]
October 17, 1995
Mr. Bill Mills
NC DEHNR
DEM1Water Quality Section
Permits & Engineering Unit
512 N. Salisbury Street
Raleigh, North Carolina 27604
Ashland Chemical Company Address Reply:
Division of P.O. Box 2219
Ashland Inc. Columbus, Ohio 43216
Fax: [phone]
FEDERAL EXPRESS
Re: NPDES Stormwater Data Required by Section VII of Form 2F
Ashland Chemical Co. (Ashland) - Charlotte, NC Facility
Dear Mr. Mills:
eD
The purpose of this memo is to submit the remaining stormwater sampling data required
for our individual NPDES Stormwater application Section VII of Form 2F. Our October
12th submittal was VOC data, this submittal includes BOD, SS, COD, TKN, Total
Phosphorus, Nitrate/Nitrite, Copper, Lead, Nickel, Zinc, and Chromium, Oil & Grease,
=
and pH. The application itself was submitted to DEHNR on February 15, 1995.
?-
As you can see, the outfall showed 0.17 mgh of Zinc, which is above State Surface Water
rem°,
Standards of 0.050 r l (Title 15A, Chapter 2, subchapter 2B). Ashland will address
0
reducing Zinc levels in our Stormwater Pollution Prevention Plan,
Q7
PQ
Ashland Chemical's Charlotte facility sampled on September 11, 1995. We request that
the DEHNR consider the enclosed data to the end that the permit be based on the actual
facility stormwater runoff.
'!
We appreciate your consideration of this matter. If any additional information is needed,
please call meat [phone]. Thank you for your assistance.
Sincerely,
Terri Weckenbrock
Environmental Engineer
Enclosure
Headquarters:
Cable Address: Aroplaz OH
quAurtr ° -
5200 Blazer Parkway
Telex: 245385
Dublin, Ohio 43017
Answerback: ASHCHEM
Ashland Chemical's
[phone]
Fax; [phone]
Commitment to
Quality and Productivity
comp"

SAVANNAH LABORATC)RIES
S L & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
�� �[�/�2 LQG N0: 55-55032
f Received: 12 SEP 95
MS. Terri Weckenbrock OCT - 3 1995
Ashland Chemical Company
P. 0. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull Project: NPDES
Sampled By: Client
REPORT OF RESULTS Page 1
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES DATE SAMPLED
------------------------------------------------------------- -----------------------
55032-1 Outfall 002 Grab 09-11-95
------------------------------------------------------------- -----------------------
PARAMETER 55032-1
-------------------------------------------------------------------------------
Oil & Grease , mg/1 5.1
PH, units 7.2
-------------------------------------------------------------------------------
3nft ' u?
r-
W
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA

SAVANNAH LABORATORIES'
S L & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S5-55032
Received: 12 SEP 95
Ms. Terri weckenbrock
Ashland Chemical Company
P. O. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull Project: NPDES
Sampled By: Client
REPORT OF RESULTS
Page 2
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
-----------
DATE SAMPLED
--------------------------------------------------
55032-2 Outfall 002 Composite
-----------
-----------------------
09-11-95
--------------------------------------------------
PARAMETER
55032-2
-----------------------
-------------------------------------------------
Biochemical Oxygen Demand (5 Day) (405.1), mg/l
----------
7.1
--------------------
Suspended Solids (160.2), mg/l
70
Chemical Oxygen Demand, mg/l
51
Total Kjeldahl Nitrogen-N, mg/l
1.6
Total Phosphorus (365.4) , mg/l
0.39
Nitrate + Nitrite-N, mg/l
0.54
Copper (200.7), mg/l
<0.025
Lead (239.2), mg/1
0.014
<
Nickel (200.7), mg/l
<0.040
Zinc (200.7), mg/l
0.17
Chromium (200.7), mg/1
<0.010
x'
-------------------------------------------------
----------
-----------------��--
"�
IV
i�f
Cn
Cn
f--
TI
W
Laboratories In Savannah, GA • Tallahassee, FL 9 Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA

SAVANNAH LABORATORIES'
S L & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 + [phone] • Fax [phone]
Ms. Terri Weckenbrock
Ashland Chemical Company
P. O. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES
55032-3 Method Blank Liquid
55032-4 Accuracy (Mean lk Recovery)
55032-5 Precision (W RPD)
55032-6 Date Analyzed
LOG NO: S5-55032
Received: 12 SEP 95
Project: NPDES
Sampled By: Client
Page 3
-------------------------------------------------------------
PARAMETER
55032-3
----------------------
55032-4
55032-5
55032-6
-----------------------------
Oil & Grease , mg/1
----------
--------------------
<5.0
86
----------
W
0
----------
W
09.21.95
pH, units
---
96
%-
1.0
%-
09.12.95
Biochemical Oxygen Demand
(5 Day)
<2.0
107
1.9
W
09.12.95
(405.1), mg/l
Suspended Solids (160.2),
mg/1
<5.0
96
W
1.0
09.13.95
Chemical Oxygen Demand, mg/1
<20
96
%-
1.0
W
09.19.95
Total Kjeldahl Nitrogen-N,
mg/1
<0.10
100
%-
10
96
09.14.95
Total Phosphorus (365.4) ,
mg/l
<0.10
98
W
3.1
$
09.14.95
Nitrate + Nitrite-N, mg/1
<0.050
108
%-
2.8
$
09.20.95
Copper (200.7), mg/1
<0.025
100
W
1.0
%7
09.25.95
Lead (239.2), mg/l
<0.0050
105
W
5.7
%-
09.20.95
Nickel (200.7), mg/1
<0.040
98
%-
1.0
%
09.25.95
zinc (200.7), mg/1
<0.020
96
W
1.0
%-
09.25.95
Chromium (200.7), mg/l
<0.010
98
%-
1.0
%-
09.25.95
Methods: EPA 40 CFR Part 136
Kar4i L. Derr
Page Of Report
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA

,'�
Ashland Chemical
Environmental, Health & Safety
G. W. Hammer
Vice President
[phone]
October 12, 1995
Mr. Bill Mills
NC DEHNR
DEM\Water Quality Section
Permits & Engineering Unit
512 N. Salisbury Street
Raleigh, North Carolina 27604
Ashland Chemical Company Address Reply:
Division of P.O. Box 2219
Ashland Inc. Columbus, Ohio 43216
Fax: [phone]
FEDERAL EXPRESS
Re: NPDES Stormwater Data Required by Section VII of Form 2F
Ashland Chemical Co. - Charlotte, NC Facility
Dear Mr. Mills:
The purpose of this memo is to submit the stormwater sampling data required for our
individual NPDES Stormwater application Section VII of Form 2F. The application itself
was submitted to DEHNR on February 15, 1995,
Ashland Chemical's Charlotte facility sampled on September 11, 1995. We request that
the DEHNR consider the enclosed data to the end that the permit be based on the actual
facility stormwater runoiT x'
rw
Fes,
We appreciate your consideration of this matter. If any additional information is needed, --o
please call meat [phone]. Thank you for your assistance. Cn
Sincerely,
�1
f
Terri Weckenbrock
Environmental Engineer
Enclosure
waurr
Ashland Chemical's
Commitment to
Quality and Productivity
Headquarters:
5200 Blazer Parkway
Dublin, Ohio 43017
[phone]
Cable Address: Aroplaz OH
Telex: 245385
Answerback: ASHCHEM
Fax: [phone]
A Reapomlbk Cale'
C-Parry
in

SAVANNAH LABORATORIES
S & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
Me. Terri Weckenbrock
Ashland Chemical. Company
P. O. Box 2219
Columbus, OH 43216
CC: Mr. Mike
Cg ra qq �
I l SEP 2 2 I995
REPORT OF RESULTS
LOG NO: S5-55056
Received: 13 SEP 95
Project: ACI-Charlotte, NC
Sampled By: Client
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
----------- --------------------------------------------------
55056-1 Outfall 002 Composite
----------- --------------------------------------------------
PARAMETER 55056-1
Purgeables (624)
Page 1
DATE SAMPLED
-----------------------
UNKNOWN
-----------------------
Benzene, ug/l
<5.0
Bromodichloromethane, ug/1
<5.0
Bromoform, ug/l
<5.0
Bromomethane, ug/l
<10
Carbon tetrachloride, ug/1
<5.0
Chlorobenzene, ug/l
<5.0
Chloroethane, ug/1
<10
2-Chloroethylvinyl ether, ug/1
<50
Chloroform, ug/l
<5.0
Chloromethane, ug/l
<10
A
Dibromochloromethane, ug/1
<5.0
`t0
1,2-Dichlorobenzene, ug/l
<5.0
ry
1,3-Dichlorobenzene, ug/l
<5.0
al
1,4-Dichlorobenzene, ug/l
<5.0
1,1-Dichloroethane, ug/1
<5.0
c3�
1,2-Dichloroethane, ug/1
<5.0
1,1-Dichloroethene, ug/l
<5.0
trans-1,2-Dichloroethene, ug/1
<5.0
1,2-Dichloropropane, ug/l
<5.0
cis-1,3-Dichloropropene, ug/1
<5.0
trans-1,3-Dichloropropene, ug/l
<5.0
Ethylbenzene, ug/1
<5.0
Methylene chloride (Dichloromethane), ug/1
-------------------------------------------------
<5.0
--------------------
----------
Laboratories in Savannah, GA • Tallahassee, FL • Tampa, FL 9 Deerfield Beach, FL 9 Mobile, AL 9 New Orleans, LA

. SAVANNAH LABORATORIES
S L & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] + Fax [phone]
Ms. Terri Weckenbrock
Ashland Chemical Company
P. 0. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull
REPORT OF RESULTS
LOG NO: S5-55056
Received: 13 SEP 95
Project: ACI-Charlotte, NC
Sampled By: Client
Page 2
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES
DATE SAMPLED
-------------------------------------------------------------
55056-1 Outtall 002 Composite
-----------------------
UNKNOWN
-------------------------------------------------------------
PARAMETER
-----------------------
55056-1
-------------------------------------------------
1,1,2,2-Tetrachloroethane, ug/l
------------------------------
<5.0
Tetrachloroethene, ug/l
<5.0
Toluene, ug/l
<5.0
1,1,1-Trichloroethane, ug/l
<5.0
1,1,2-Trichloroethane, ug/l
<5.0
Trichloroethylene, ug/l
<5.0
Trichlorofluoromethane, ug/l
<5.0
vinyl chloride, ug/l
<10
Xylenes, ug/l
-------------------------------------------------
<5.0
------------------------------
ry
rn
Laboratorles in Savannah, GA • Tallahassee, FL • Tampa, FL • Deerfield Beach, FL • Mobile, AL • New Orleans, LA

SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue * Savannah, GA 31404 * [phone] * Fax [phone]
Ms. Terri Weckenbrock
Ashland Chemical Company
P. 0. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull
REPORT OF RESULTS
LOG NO: S5-55056
Received: 13 SEP 95
Project: ACI-Charlotte, NC
Sampled By: Client
Page 3
LOG NO SAMPLE DESCRIPTION , QC REPORT
-------------------------------------------------------------
FOR LIQUID
SAMPLES
55056-2 Method Blank Liquid
----------------------
55056-3 Accuracy (Mean W Recovery)
55056-4 Precision (W RPD)
55056-5 Date Analyzed
-------------------------------------------------------------
PARAMETER
55056-2
----------------------
55056-3
55056-4 55056-5
-------------------------------------------------
Purgeables (624)
----------
----------
----------
Benzene, ug/l
<5.0
91
0.0 W 09.14.95
Bromodichloromethane, ug/1
<5.0
---
--- 09.14.95
Bromoform, ug/1
<5.0
---
--- 09.14.95
Bromomethane, ug/l
<10
---
--- 09.14.95
Carbon tetrachloride, ug/l
<5.0
---
--- 09.14.95
Chlorobenzene, ug/l
<5.0
98 %.
3.0 $ 09.14.95
Chloroethane, ug/l f
<10
---
--- 09.14.95
2-Chloroethylvinyl ether, ug/l
<50
---
--- 09.14.95
Chloroform, ug/1
<5.0
---
--- 09.14.95.
Chloromethane, ug/1
<10
---
--- 09.14.95 u
Dibromochloromethane, ug/l
<5.0
---
--- 09.14.9�,'
1,2-Dichlorobenzene, ug/l
<5.0
---
--- 09.14.95-n
1,3-Dichlorobenzene, ug/l
<5.0
---
--- 09.14.9�0
1,4-Dichlorobenzene, ug/l
<5.0
---
--- 09.14.9-
1,1-Dichloroethane, ug/l
<5.0
---
--- 09.14.95
1,2-Dichloroethene, ug/l
<5.0
---
--- 09.14.95
1,1-Dichloroethene, ug/l
<5.0
98 W
5.1 $ 09.14.95
trans-1,2-Dichloroethene, ug/I
<5.0
---
--- 09.14.95
1,2-Dichloropropane, ug/l
<5.0
---
--- 09.14.95
cis-1,3-Dichloropropene, ug/l
-------------------------------------------------
<5.0
----------
---
----------
--- 09.14.95
----------
03
Laboratories in Savannah, GA * Tallahassee, FL 9 Tampa, FL * Deerfield Beach, FL * Mobile, AL * New Orleans, LA

SAVANNAH LABORATORIES
S L & ENVIRONMENTAL SERVICES, INC.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S5-55056
Received: 13 SEP 95
Ms. Terri Weckenbrock
Ashland Chemical Company
P. O. Box 2219
Columbus, OH 43216
CC: Mr. Mike Trull Project: ACI-Charlotte, NC
Sampled By: Client
REPORT OF RESULTS
Page 4
LOG NO SAMPLE DESCRIPTION , QC REPORT
FOR LIQUID
SAMPLES
-------------------------------------------------------------
55056-2 Method Blank Liquid
----------------------
55056-3 Accuracy (Mean W Recovery)
55056-4 Precision ($ RPD)
55056-5 Date Analyzed
-------------------------------------------------------------
PARAMETER
55056-2
----------------------
55056-3
55056-4 55056-5
-------------------------------------------------
trans-1,3-Dichloropropene, ug/l
----------
<5.0
----------
---
----------
--- 09.14.95
Ethylbenzene, ug/l
<5.0
---
--- 09.14.95
Methylene chloride (Dichloromethane), ug/l
<5.0
---
--- 09.14.95
1,1,2,2-Tetrachloroethane, ug/l
<5.0
---
--- 09.14.95
Tetrachloroethene, ug/1
<5.0
---
--- 09.14.95
Toluene, ug/1
<5.0
93 %-
2.2 W 09.14.95
1,1,1-Trichloroethane, ug/1
<5.0
---
--- 09.14.95
1,1,2-Trichloroethane, ug/1
<5.0
---
--- 09.14.95
Trichloroethylene, ug/l
<5.0
100 W
.2.0 $ 09.14.95
Trichlorofluoromethane, ug/1
<5.0
---
--- 09.14.95
Vinyl chloride, ug/1
<10
---
--- 09.14.95
Xylenes, ug/1
-----------------------------
<5.0
---
--- 09.14.95
--------------------
Methods: EPA 40 CFR Part 136
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Final Page Of Report
Laboratories in Savannah, GA 9 Tallahassee, FL • Tampa, FL 9 Deerfield Beach, FL • Mobile, AL 9 New Orleans, LA

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Ashland Chemical
Environmental, Health & Safety
G. W. Hammer
Vice President
[phone]
August 25, 1995
Mr. Tony Evans
NC DEHNR
DEM\Water Quality Section
Permits & Engineering Unit
512 N. Salisbury Street
Raleigh, North Carolina 27604
Ashland Chemical Company Address Reply:
Division of P.O. Box 2219
Ashland Inc. Columbus, Ohio 43216
Fax: [phone]
FEDERAL EXPRESS
Re: NPDES Stormwater Data Required by Section VII of Form 2F
Ashland Chemical Co. - Charlotte, NC Facility
Dear Mr. Evans:
The purpose of this memo is to confirm your verbal extension of the due date for the
required Section VII stormwater sampling data to September 1, 1995,
Ashland Chemical's Charlotte facility is prepared to sample, but has not had a rainfall
event since July. We intend to meet the September I deadline, but if there is not a rainfall M
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event by then, we will sample the first rainfall event. We would request at that time that v
we can submit the data for consideration. We realize that the permit may already have co
been issued with the group and Mecklenburg County data by that time; but request that
TII
the permit be written based on the facility stormwater runoff. cr
We appreciate your consideration of this matter. If any additional information is needed,
please call me at [phone]. Thank you for your assistance.
Sincerely,
Terri Weckenbrock
Environmental Engineer
cc: Bill Mills - NC DEHNR
Coleen Sullins, PE - NC DEHNR
- - - - - - i Headquarters: Cable Address: Aroplaz OH
i0uALlrr' 5200 Blazer Parkway Telex: 245385
Dublin, Ohio 43017 Answerback: ASHCHEM
Ashland Chemical's [phone] Fax: [phone]
Commitment to ARfipOMlWIGn'
Quality and Productivity Company

State of North Carolina
Department of Environment,.
Health and Natural Resources
Division of Environmental Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
A. Preston Howard, Jr., P.E., Director
July 24, 1995
Mr. Edward Graves, Environmental Engineer
Ashland Chemical Company
P. O. Box 2219
Columbus, Ohio 43216
Dear Mr. Graves:
A
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D FEHNF=1
Subject: NPDES Stormwater Permit Application
Ashland Chemical Company
Charlotte
Mecklenburg County
On February 15, 1995 the Division of Environmental Management received an individual
NPDES Stormwater application for stormwater discharges from the subject facility. After
reviewing the application, we find that the application is incomplete Therefore, processing of the
application cannot begin. The following information is needed to make the application complete:
The stormwater data required in Section VII of Form 2F has not been provided.
Your transmittal letter of February 15, 1995 advised that sampling had not been
conducted at that time but would be accomplished a9 soon as weather conditions
allow. Mr. Bill Mills of my staff called you in June, 1995 to inquire about the sample
results and was told that sampling had still not been conducted.
rn
The information cited above needs to be submitted at a very early date in o'er far a
complete review and application processing to begin. Unless the above cited informa�01 isfiled
with our Division by August 25, 1995 we will draft the permit using the Mecklenburg ntyluata
and the group application data. 1
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If you have any questions, please contact Bill Mills at [phone] ext . 548. '
Sincerely,
cc: Mooresville Regional Office
GPermits-and-Erigineeririg Units
Central Files
P.O. Box 29535, Raleigh, North Carolina 27626-0535
An Equal Opportunity Affirmative Action Employer
oleen Sullins, PE
Supervisor, Permits and Engineering Unit
Telephone [phone] FAX [phone]
50% recycled/ 10% post -consumer paper