HomeMy WebLinkAboutWQ0000543_Residual Annual Report 2018_20190315INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0000543
SUBMITTAL DATED: 2/28/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
Ifinnerty@synagro.com
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0000543
Permittee *
Facility Name *
City of Sanford
City of Sanford
Phone Number*
4434899086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
2018 Annual Report
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Hans, Specifications, Calculations, Etc.)
Sanford NC 2018 Annual Report.pdf 16.68MB
Upload only 1 RDF document. NUltiple documents must be corrbined into one RDF file.
For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at: 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/28/2019
435 ` whams Court, Suite 100
Baltimore, MD 21220
wwwsynagro.com
FEBRUARY 275 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Centex
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0000543
Dear NCDEQ:
Synagxo is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Sanford, NC.
If you have any
questions
ox need additional
information, please do not hesitate to contact Scott
Siletzky at (919)
775-8305 or Melinda Boyd at
(336) 909-8627.
Sincerely,
Derrick Shivax
Environmental Compliance Manager
Enclosures
ec: Melinda Boyd, Synagxo
Scott Siletzlcy, City of Sanford
YOUR PARTNER FORA CLEANER, GREENERWORLD
CITY OF SANFORD
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0000543
2018 ANNUAL REPORT
City of Sanford, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analysis,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNectorRttraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses
SECTION 1
ANNUAL LAND APPLICATION CERTIFICATION FORM
WQPermit#: WO0000543 County Carteret Year 2018
Facility Name (as shown on permit) City of Sanford W WTP NPDES No. NC0024147
Land Application Operator Synagro Phone# L336)998-7150
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Annlication Summarv:
Total number of application fields in the permit: 43
Total number of fields utilized For land application during the year: 13
Total amount of dry tons applied during the year for all application sites: 450.84
Total number of acres utilized for land application during the year: 271.20
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all condifions of the ]and application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
I.
Part C —Cert
Only residuals approved for this permit were applied to the permitted sites.
2.
Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3.
Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4.
Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5.
All other monitoring was performed in accordance with the permit and reported during the you as required and three (3)
copies of certified laboratory results are attached.
6.
The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7.
All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8,
All monitoring and reporting requirements in 15A NCAC 02T.1 11 I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9.
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10.
No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediation.
11.
Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12.
No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13.
All buffer requirements as specified on the permit were maintained during each application of residuals.
ification:
"L certify, under penalty
of law, that the above information is, to the best of rr
am aware that there are signifieanY penalties for submitting false information,
knowing violations."
Hal Heewer, Public City Man
ager
Permittee Name and Title (type or print) Si
a ► �1
Signature of Preparer* 0 D to Si
if different from Permittee) (if different
and belief, true, accurate, and complete. I
possibility of fines and imprisonment forFaffmW
Preparer)
*Pranarer is defined in 40 CFR Part SOi 9lrl and ISA NCAC 02T .1102 061 ➢RNR FnRM ACF !12/20061
2018 ANNUAL OPERATIONS SUMMARY = LAND APPLICATION IN NC
SANFORD,NC
SANFORD, NC BUFFALO CREEK WWTP AEROB, DIG. LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
April 2018
1,264,800.00
G
133.44
D
121.03
May 2018
9541800.00
G
100.72
D
91.37
June 2018
725,400.00
G
70.18
D
63.65
July 2018
663,400.00
G
73.03
D
66.24
October 2018
3902600.00
G
47.23
D
42.84
November 2018
217,000.00
G
26.24
D
23.80
YEARLY TOTAL
4,216,000.00 G 450.84 D 408.93
1 /22/2019
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0gm at
Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 2/8/2018 1/1/2018-5131/2018 0.8377
AEROB. DIG, LIQUID
Na mg/I = (Na mg/kg x % Solids) _ 100 = (3150 x 2.5300) + 100 = 79.695
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (17300 x 2.5300) - 100 = 437.69
Mg mg/I = (mg mg/kg x % Solids) + 100 = (5850 x 2.5300) - 100 = 148.005
Na meq = Na mg/I + Molec.Wgt.Na = 79.695 + 23 = 3.465
Ca meq = Ca mg/I + MoleaWgLCa = 437.69 + 20 = 21.8845
Mg meq = Mg mg/1 + Molec.Wgt.Mg = 148.005 : 12 = 12.3338
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.465 = SgrRoot[0.5(21.8845+12.3338)] = 0.837702
Printed: 1/25/2019
Page 1 08:27
t, --e
Waypoint a
ANALYTICAL
6/18/2018
Synagro Central LLC/ Sanford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointa na lytics I. com
Ref: Analytical Testing
Report Number: 18-159-0203
Project Description: Sanford
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 6/8/2018 for the analyses presented in the fallowing
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were pertormed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p a� c. -r
Pauric McGroary
Agronomist
Laboratory's liability in any c/aim relating to analyses performed shall be limited to,. at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid forpertormance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida Eg71087 North Carolina 257 South Carolina 93007
Page 1 of 8
Wa OI �� M® 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
Y ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-159-0203
Client Project Description: Sanford
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61070
Sanford
Solids
06/07/2018
14:45
06/08/2018
61070
Sanford
Solids
06/07/2018
14:45
06/08/2018
6010D
WiN
WTN: Waypoint Analytical - TN, Memphis, TN, Certifcation: #1354
Page 2 of 6
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ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointanalytical.tom
Cooler Receipt Form
Customer Number: 48489
Customer Name: Synagro Central LLC/ Sanford
Report Number: 18-159-0203
Shipping Method
Q Fed Ex Q US Postal Q Lab Q Other:
UPS. Q Client Q Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received r 1
Custody seals intact on shipping container/cooler? Q Yes Q No t, Not Required
Custody seals intact on sample bottles? Q Yes Q No � Not Required
Chain of Custody (COC) present? � Yes Q No
COC agrees with sample label(s)? � Yes Q No
COC properly completed � Yes Q No
Samples in proper containers? � Yes Q No
Sample containers intact? � Yes Q No
Sufficient sample volume for indicated test(s)? � Yes Q No
All samples received within holding time? � Yes Q No
Cooler temperature in compliance? � Yes Q No
Cooler/Samples arrived at the laboratory on ice. � Yes Q No
Samples were considered. acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes Q No Q N/A
Water -VOA vials free of headspace Q Yes Q No � N/A
Trip Blanks received with VOAs � Yes Q No � N/A
Soil VOA method 5035 —compliance criteria. met Q Yes Q No � N/A
High concentration container (48 hr) � Law concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low cont pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? (� Yes � No
Comments:
Signature: Brandi Watson Date:&Time: 06/08/201813:56:06
Page 5 of 6
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Product Code Product Name Sample as Report Range Ratio
2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 6/7/2018 6/1/2018-6/30/2018 1.0293
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x % Solids) . 100 = (3620 x 2.3200) + 100 = 83.984
Ca mg/I = (Ca mg/kg x % Solids) + 100 = (15100 x 2.3200) + 100 = 350.32
Mg mg/I = (mg mg/kg x % Solids) + 100 = (3960 x 2.3200) + 100 = 91.872
Na meq = Na mg/I + Molec. Wgt.Na = 83.984 + 23 = 3.65148
Ca meq = Ca mg/I + MolecWgLCa = 350.32 + 20 = 17.516
Mg meq = Mg mg/I + Molec.Wgt.Mg = 91.872 = 12 = 7.656
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.65148 + SgrRoot[0.5(17.516+7.656)] = 1.02926
Printed: 1/25/2019
Page 1 08:27
Waypoint
ANALYTICAL
17(IC:i%I�7iE�3
Synagro Central LLC/ Sanford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointa n alytica I.co m
Ref: Analytical Testing
Report Number: 18-184-0200
Project Description: Sanford
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples} on 7/3/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite....) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any feld parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results far solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only tc
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
p a•r r
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid far performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
'�•'
Page 1 of 7
Waypoint.
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypoi nta nalytica Isom
Client: Synagro Central LLC/ Sanford CASE NARRATIVE
Project: Sanford
Lab Report Number: 18-184-0200
Date: 7/18/2018
TKN (Titration) Method SM�500-NH3C-TKN
Analyte: TKN
OC Batch No: E64890
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MOL. The actual
result was
XXJ which calculates to a recovery of XX°/ .
Analyte was flagged for 0% recovery in the LCS and/or LCSD .The actual result was
0.870 which calculates to a recovery of 85%.
QC Batch No: E84890
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Nitrate+ Nitrite Nitrogen Method SM-4500NO3F
Sample 61491 (Sanford 3 of 4)
Analyte: NO3+NO2-N
ClG Batch No: E84942/E64892
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Solids Total Mercury Analysis - CVAA Method SW -7471 B
Analyte: Hg
QC Batch No: E84928/E84889
MS/MSD Recovery failed, PDS confirmed matrix interference
Page 2 of 7
Waypoi nt.., 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-184-0200
Client Project Description: Sanford
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61491
Sanford 3
of 4
Solids
06/27/ZO18
10:30
07/03/2018
61491
Sanford 3
of 4
Solids
06/27/2018
10:30
07/03/2018
6010C
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 3 of 7
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Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypointa nalydca I. com
Cooler Receipt Form
Customer Number: 46489
Customer Name: Synagrd Central LLC/ Sanford
Report Number: 18-184-0200
Shipping Method
Q Fed Ex Q US Postal Q Lab Q Other
UPS Q Client Q Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes Q No
Number of coolers received
Custody seals intact on shipping container/cooler? Q Yes (� No � Not Required
Custody seals intact on sample battles? Q Yes Q No � Not Required
Chain of Custody (COC) present? � Yes Q No
COC agrees with sample label(s)? � Yes (� No
GOC properly completed � Yes (� No
Samples in proper containers? � Yes Q No
Sample containers intact? � Yes Q No
Sufficient sample volume for indicated test(s)? � Yes Q No
All samples received within holding time? � Yes Q No
Cooler temperature in compliance? � Yes Q No
Cooler/Samples arrived at the laboratory on ice. � Yes Q No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved Q Yes Q No � N/A
Water-VOAvials free of headspace Q Yes Q No � N/A
Trip Blanks received with VOAs Q Yes Q No � N/A
Soil VOA method 5035 —compliance criteria met Q Yes Q No � N/A
� High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low concyre-weighed vials (Sod Bis -14 d)
Special precautions or instructions included? Q Yes � No
Comments:
Signature: Brandi Watson Date &Time: 07/03/2018 13:34:48
Page 6 of 7
�
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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2039-01-AEDLIQ-NC
SANFORD, NC BUFFALO CREEK WWTP
6/27/2018
7/1/2018-9130/2018
1.1161
AEROB. DIG. LIQUID
Na mg/I = (Na mg/kg x %Solids) + 100 = (3890 x 2.6400) + 100 = 102.696
Ca mg/I = (Ca mg/kg x %Solids) :100 = (17900 x 2.6400) = 100 = 472.56
Mg mg/I = (mg mg/kg x %Solids) :100 = (3810 x 2.6400) + 100 = 100.584
Na meq = Na mg/I - Molec.Wgt.Na = 102.696 + 23 = 4.46504
Ca meq = Ca mg/I + Molec.Wgt.Ca = 472.56 + 20 = 23.628
Mg meq = Mg mg/I _ Molec.Wgt.Mg = 100.584+ 12 = 8.382
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.46504 + SgrRoot[0.5(23.628+8.382)] = 1.11609
Printed: 1/25/2019
Page 1 08:27
Wal(Do
point,
nt
ANALYTICAL
1 011 6/2 01 8
Synagro Central LLC/ Sanford
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-278-0223
Project Description: Sanford WWTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-94010 Fax 804-271-6446
www.waypo intana lytica I. co m
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/5/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
f applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Anal
ysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating fo analyses performed shall be limited to, at laboratory's option, repeating the.
analysis in question at laboratory's expense,. or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
4A
Page 1 of 6
Waypoint.. 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-278-0223
Client Project Description: Sanford WWTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63033
Sanford
WWTP
Solids
10/01/2018
14:30
6010D
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Soltds
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
63033
Sanford
WWTP
Solids
10/01/2018
14:30
10/05/2018
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
SM-4500-NH3C
WTN
9045D
WTN
4500NO3F-2011
WTN
6010D
WTN
SW -74718
WTN
SM-4500-NH3C-TKN
WTN
SM -2540G
WTN
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Waypoint..''�W^���t'�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax 804-271-6446
www.waypoi nta nalyH ca Isom
Cooler Receipt Form
Customer Number: 46489
Customer Name: Synagro Central LLC/ Sanford
Report Number: 18-278-0223
Shipping Method
Fed Ex � US Postal � Lab � Other : �—
UPS (� Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes Q No
Number of coolers received r 1
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Nat Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
COCproperlycompleted � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes 0 No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cooler/Samples. arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No � N/A
Water-VOAvialsfree ofheadspace � Yes � No � N/A
Trip Blanks received with VOAs a Yes � No � WA
Soil VOA method 5035 –compliance criteria met � Yes � No � N/A
� High concentration container (48 hr) � Law concentration Encore samplers (48 hr)
� High concentration pre -weighed (methanol -14 d) � Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson Date &Time: 10/05/2018 14:23:19
Page 5 of 6
�
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\(
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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2039-01-AEDLIQ-NC
SANFORD, NC BUFFALO CREEK WWTP
10/1/2018
101112018-1/31/2019
0.7776
AEROB, DIG. LIQUID
Na mg/I = (Na mg/kg x %Solids) + 100 = (2680 x 2.9000) + 100 = 77.72
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (18100 x 2.9000) = 100 = 524.9
Mg mg/I = (mg mg/kg x %Solids) + 100 = (4770 x 2.9000) + 100 = 138.33
Na meq = Na mg/I - Molec.Wgt.Na = 77.72 : 23 = 3.37913
Ca meq = Ca mg/I - Molec.Wgt.Ca = 524.9 + 20 = 26.245
Mg meq = Mg mg/I - Molec.Wgt.Mg = 138.33 + 12 = 11.5275
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.37913 + SgrRoct[0.5(26.245+11.5275)] = 0.777557
Printed: 1/25/2019
Page 1 08:28
SECTION 3
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SECTION 4
q9SUMM111
Anaf y6cal Laboramries
March 07. 2018
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: (336) 998-7150
FAX: (336) 998-8450
RE: Sanford
Dear Will Varner:
SummitE vironmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL (330) 253-8211 FAX: (330) 253-4489
Website httn:/Anvw.settek.com
Order No.: 18020868
Summit Environmental Technologies, Inc. received 1 samples) on 2!16/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report
unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
j
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Californ
ia 07256CA, Colorado, Connecticut PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, lllinvis
200061, Indiana C -OH -13, Kansas &10347, Kentucky (Uvdergrouvd Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota
4097I1,.New Hampshire 2996, New Jersey OH006, New Yolk 11777, Noah Ceraliva 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 27
SUMMIT suinnaftEnvironmentai Te hao WinInc. Case Narrative
331010 ,�a sr.
CNVIRONMENTAL TECHNOLOOlES, 1NC. Cuyahoga Falls, Ohio 44223 WO#: 18020868
Analytical LaboraNOPq TEL: (330) 253-8211 RIX- (330) 253-4489
Website: h_lo.-I viv settek.00m Date: 3/7/2018
CLIENT: Synagro
Project: Sanford
WorkOrder Narrative:
18020868: This report in its entirety consists of the following documents: Cover Letter; Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples.
are reported
on an
"as received" or
"wet weight" basis unless indicated as
"dry weight" using the "-dry"
designation
on the
reporting units.
with this report are
This report is
believed
to meet all of the requirements of the
accrediting agency,
where applicable.
Any
comments or
problems
with the analytical events associated
with this report are
noted below.
Analytical Sequence Salnple Notes:
18020868-OOla tclp-voc-mstr_tclp(8260): Sample extracted in methanol.
18020868-001a tclp-voc-mstr_tclp(8260): VOC Reporting Limit elevated due to sample being treated
as waste dilution due to matrix.
Oeiginal
Page 2 of 27
M1su 'll Suninit Environmental Technologies, In Qualifiers and Acronyms
33/0 Win 5
RWIRONMENTAL I£CHNOL.0mrs, We Cuyahoga Falls, Ohio 4421 W04: 18020868
Anafytfcal taborstio6es TEL: (330) 253-82// FAX: (330) 253-445
Website; huv:/hvww.settek.co Date: 3/7/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
II
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration oris estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response.
it
Manual integration in which peak was deleted
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GUMS.
X
The result was not confirmed when GC/MS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amountsof analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QLr/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCI. Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimum Compound Limit
1CV
Initial Calibration Verification RA Reanalysis
1CB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Cheek CF Calibration Factor
DF
Dilution Factor RF Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 27
SU 111_ Summit Environmental Technologies, Inc. workOPCIer
3310 Win St.
MVIRONh1ENTAL TECHUOLOWES,+NC Cuyahoga Falls, Ohio 44223 Sample Summary
Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18020868
Website: huP71Aviviv.settek.com 07 -Mar -18
CLIENT: Synagro
Project: Sanford
Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix
18620868-001 Sanford 2/8/2018 11:15:00 AM 2/16/2018 10:10:00 AM Solid
Page 4 of 27
YOUMMI T unit Environmental Teehaal10WinS. Analytical Report
3310 wa sr.
rNVIR0NIAEN7ALTECHN0L0G,E5, INC Cuyahoga Falls, Ohio 44223 (base report)
Anafyf:r-af Laharaosrhi TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18020868
Website.: htta./Avivw settek.com Date Reported: 3/7/2018
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 2/8/2018 11:15:00 AM
Lab ID: 18020868-OOIA
Project: Sanford
Client Sample ID Sanford
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SWI 31117470)
TCLP Mercury ND 0.00500 mg/L 1 2/21/2018 4:07:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW6010D Analyst: KMS
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND 0.500 mgfL 1 2/21/2018 9:23:33 PM
TCLP Barium(Ba) ND 5.00 mg/L 1 2/21/2018 9:23:33 PM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 2/21/2018 9:23:33 PM
TCLP Chromium(Cr) ND 0.200 mg/L 1 2/21/2018 9:23:33 PM
TCLP Lead(Pb) ND 0.500 mg/L 1 2/21/2018 9:23:33 PM
TCLP Selenium(Se) ND 0.0500 mg/L 1 2/21/2018 9:23:33 PM
TCLP Silver(Ag) ND 0.500 mg/L 1 2121/2018 9:23:33 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW82700 SW361OC Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene ND 0.0800 mg/L 2 2/22/2018 5:48:00 PM
2,4,5-Trichlorophenol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM
2,4,6-Trichlorophenol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM
2,4-Dinitiotoluene ND 0.0400 mg/L 2 2/22/2018 5:48:00 PM
o-Cresol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM
m/p-Cresol(s) ND 0.200 mg/L 2 2/22/2018 5:48:00 PM
Cresols, Total ND 4.00 mg/L 2 2/22/20185:48:00 PM
Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 2/22/2018 5:48:00 PM
Hexachlorobenzene ND 0.0400 mg/L 2 2/22/2018 5:48:00 PM
Hexachloroethane ND 0.0800 mg/L 2 2/22/2018 5:48:00 PM
Nitrobenzene ND 0.0800 mg/L 2 2/22/20185:48:00 PM
Pentachlorophenol ND 0.200 mg/L 2 2/22/20185:48:00 PM
Pyridine ND 0.200 mg/L 2 2/22/2018 5:48:00 PM
Surr: 2-Fluorophenol 55.6 10-109 %Rec 2 2/22/2018 5:48:00 PM
Surr Phenol-d6 52.2 10-109 % Rec 2 2/22/2018 5:48:00 PM
Surr: Nitrobenzene-d5 .91.4 19-120 % Rec 2 2/22/2018 5:48:00 PM
Surr: 2,4,6-Tribromophenol 59.1 10-120 % Rec 2 2/22/2018 5:48:00 PM
Surr: 2-Fluorobiphenyl 99.8 22-117 % Rec 2 2/22/2018 5:48:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 6 of 27
HISUMMInt Suarmir Environmental Technologies, WSt.
3310 Win St.
rf&VIRONNIENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Anafythcal Laboratories TEL: (330) 253-8211 FAX. (330) 253-4489
Website: hHoWwwwsefiekcore
CLIENT: Synagro
Matrix: SOLID
Lab ID: 18020868-OOIA
Project: Sanford
Client Sample ID Sanford
Analyses Result
Analytical Report
(base report)
WO#: 18020868
Date Reported: 3/7/2018
Tag Number:
Collection Date: 2/8/2018 11:15:00 AM
RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
Surr: p-Terphenyl-d14 111 34-116
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total
ND
Toxaphene
ND
Endrin
ND
gamma -BHC
ND
Heptachlor
ND
Heptachlor epoxide
ND
Methoxychlor
ND
Burr: TCMX
65.8
Surr: DCB
40.0
SW8270D SW3510C Analyst: BJH
%Rec 2 2/22/2018 5:48:00 PM
SW8081 SW3510C Analyst: JBN
0.0200
mg/L
2
2122/2018 5:38:00
MEK
ND
PM
0.0400
mg/L
2
2/22/2018 5:38:00
ND'
Chloroform
PM
0.00200
mg/L
2
2/22/2018 5:38:00
Vinyl chloride
ND
PM
0.00200
mg/L
2
2/22/2018 5:38:00
mg/L
1000
PM
0.00200
mg/L
2
2/22/2018 5:38:00
mg/L
PM
0.00200
mg/L
2
2/22/2018 5:38:00
5.00
PM
0.00200
mg/L
2
2/22/2018 5:38:00
PM
5.00
PM
10 - 119
% Rec
2
2122/2018 5:38:00
PM
PM
10 - 119
%Rec
2
2122/2018 5:38:00
PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
SW8151A SW8151A Analyst: JBN
2,4-D ND 1.00
21415 -TP ND 0.500 It
Surr: DCAA 85.4 20-140
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
1,2-Dichloroethane
ND
MEK
ND
Benzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND'
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Qualifiers:
* Value exceeds Maximum Contaminant. Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minunuin Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
mg/L
1
2/28/2018 7:54:00
1000
2/21/20184:44:00
PM
mg/L
1
2/28/2018 7:54:00
mg/L
1000
PM
%Rec
1
2/28/2018.7:54:00
25.0
PM
SW8260B SW1311M Analyst: CTB
5.00
H Value above quantitation
mglL
1000
2/21/20184:44:00
PM
5.00
mg/L
1000
2/21/20184:44:00
PM
25.0
mg/L
1000
2/21/20184:44:00
PM
5.00
mg/L
1000
2/21/2018
4:44:00
PM
5.00
mg/L
1000
2/21/2018
4:44:00
PM
5.00
m9/L
1000
2/21/20184:44:00
PM
5.00
mg/L
1000
2/21/2018
4:44:00
PM
5.00
mg/L
1000
2/21/20184:44:00
PM
5.00
mg/L
1000
2121/20184:44:00
PM
2.00
mg/L
1000
2/21/20184:44:00
PM
range
M Manual Integration used to detemrine area response
N Tenmtively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 27
Summit Environmental TeclmolInc.
SUMMIT
331010Win St.
FNVIROWENTALT£CHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
AnafyWaf Laborsiorles TEL: (330) 253-8211 FLY.. (330) 253-4489
Website: hap.,Uvwvv.seaek.com
CLIENT: Synagro
Matrix: SOLID
Lab ID: 18020868-001A
Project: Sanford
Client Sample ID Sanford
Analyses Result
TCLIP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Surr; 4-Bromofluorobenzene
80.8
Sum Dibromofluoromethane
101
Surr: Toluene -d8
86.6
NOTES:
PM
Sample treated as waste dilution due to
matrix.
RCI -SOLID -W/ IGNITABILITY1030
1000
REACTIVE CYANIDE (9014/7.3.3.2) -SOLID
Not Detected
Cyanide, Reactive
ND
RCI -SOLID -W/ IGNITABILITY1030
130
IGNITABILITY OF SOLIDS (SW -846:
1030)
Ignitability
non-flammable
RCI -SOLID -W/ IGNITABILITY1030
PM
PH (SW9046D)
pH
7.6
RCI -SOLID -W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
40.0
QuaOSers:
Analytical Report
(basereport)
WO#: 18020868
Date Reported: 3/7/2018
Tag Number:
Collection Date: 2/8/2018 11:15:00 AM
RL Qual Units DF Date Analyzed
SW8260B SW1311M Analyst: CTB
70 -
130
%Rec
1000
2/21 /2018 4:44:00
SWI 030
Analyst:
PM
70 -
130
% Rec
1000
2/21/2018 4:44:00
Not Detected
0
PM
70 -
130
% Rec
1000
2/21/2018 4:44:00
RPD outside accepted recovery limits
RL
PM
SW9014 Analyst: MS
0.500
mg/Kg
1
2/22/20184:49:00 PM
SW9045D
SWI 030
Analyst:
Analyst: AJT
s.u.@79.2C 1 3/1/201811:19:00 AM
SW9034 Analyst: MS
25.0 mg/Kg 1 2122/2018 4:49:00 PM
*
1
2/21/2018 10:30:00
AM
SW9045D
Holding times for preparation or analysis exceeded
Analyst:
DHC
s.u.@79.2C 1 3/1/201811:19:00 AM
SW9034 Analyst: MS
25.0 mg/Kg 1 2122/2018 4:49:00 PM
*
Value exceeds Maximum Contaminant Level
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
0
RSD is greaterthan RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 8 of 27
I�s„mm;tEruironmentalTechnologies, Inc. Accreditation Program
3310 Win St. Analytes Report
04VIRONhtENTALTECHNOLOCIE3, INc Cryahoga Falls, Ohio 44223 Y P
Arralyficerl Laboratories TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 18020868
Website: hM.11imv3v.setiekconn 07-Mar48
Client: Synagro State: NW
Project: Sanford Program Name: NC—WW—SCM
Sample ID Ma[rix
Test Name
Analyte
Sta[us
18020868-001A Solid
Ignitability of Solids (SW -846: 1030)
Ignitability
A
Solid
pH(SW9045D)
Hydrogen Ion (PH)
A
Solid
Reactive Cyanide (9014/7.33.2) -Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides Analysis(SW1311/8151)
214,5 -TP
A
Solid
TCLP Herbicides Analysis (SW1311/8151)
2,4-1)
A
Solid
TCLP Herbicides Analysis(SW1311/8151)
DCAA
A
Solid
TCLPMercury Analysis(SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis(SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis(SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis(SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW 1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis(SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/808 1)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Solid
TCLP Pesticides Analysis (SW1311/808 1)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma -BHC
A
Solid.
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW 1311/808 1)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SWI 311/8081)
Tetraehlore-m-xylene
A
Solid
TCLP Pesticides Analysis (SWI 311/8081)
Toxaphene
A
Solid
TCLP Semi -Volatiles Analysis(SWI311/8270)
1,4 -Dichlorobenzene
A
Solid
TCLP Semi -Volatiles Analysis (SW1311/8270)
2,4,5 -Trichlorophenol
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6-Tribromophenol
A
Solid
TCLP Semi -Volatiles Analysis (SWI 311/8270)
2,4,6 -Trichlorophenol
A
Solid
TCLP Semi -Volatiles Analysis (SW 1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
2-Fluorobiphenyl
A
Solid
TCLP Semi -Volatiles Analysis (SW 1311/8270)
2-Fluorophenol
A
NC_WW_SCM A Accredited NC_WW_SCM U Unavailable
Version #2
Page 9 of 27
S U 1 11 SummitEnvi onmentalTechnologies, Inc. Accreditation Program
3310 win St. Analytes Report
MVIRONMAENTAL T2CONOLOGIES, INC Cxryahoga Falls, Ohio 44223 y P
dnaPyfiraf Lahm'atwTs TEL: (330) 253-8211 FIX: (330) 253-4489 WO#: 18020868
Website: hov:lAviviv settelceom 07 -Mar -18
Client: Synagro State: NW
Project: Sanford Program Name: NC—WW—SCM
Sample ID Matrix
Test Name
Analyte
Status
18020868-001A Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
2-Methylpbenol
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
3,4-Methylphenol
A
Solid
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi -Volatiles Analysis(SWI311/8270)
Hexaehlorobutadiene
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Hexachloroothane
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Nitrobenzene -d5
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Phenol -d6
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
p-Terphenyl-d14
A
Solid
TCLP Semi -Volatiles Analysis(SW1311/8270)
Pyridine
A
Solid
TCLP Volatiles Analysis
1,1-Dicliloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
4-Bromolluorobenzene
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Dibromofluoromethane
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Toluene -d8
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl cldoride
A
NC_WW_SCM A Accredited NC_WW_SCM U Unavailable
Version #2
Page 10 of 27
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Summie Environmental Technologies, Inc.
3310 Win St.
"MRONhtENTAL IECHMOLOGrEs,;NC- Cuyahoga Falls, Ohio 44223 Sample Log -in Check List
Analytical Latw atorfes TEL: (330) 253-8211 FAX (330) 253-4489
Website: hily.11mvm.settekconr
Client Name: SYN -NC -27028
Logged by: Christopher Livengood
Completed By: Antonio Betscakos
Reviewed By: Jennifer Woolf
Chain of Custody
1, Is Chain of Custody complete?
2, How was the sample delivered?
Log In
3_ Coolers are present?
Work Order Number: 18020868
2/1612018 10:10:00 AM
2/16/2618 3:34:3fi PM
2/19/2018 4:28:11 PM
4. Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
5. Were all samples received at a temperature of >0' C to 6.0°C
�. Sample(s) in proper container(s)?
6. Sufficient sample volume for indicated test(s)?
9_ Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11, Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
12. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
Yes ❑�/
FedEx
as
as
Yes ElSigned By:
as 0
Yes 0
Yes
Yes
Yes❑
Yes ❑
Yes ❑
as El
Yes WY
es
Yes 66Yes W
Rcip o:
El11ElElL11
No ❑ Not Present ❑
Na ❑
NA
❑
Noi Present
0
NA
❑
NA
El
NA ❑�
NA
No VOA Vials R1
17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑�
Person Notified: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
16. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition Seal Intact
Seal No
Seal
1
4.3
Good Not Present
Date Signed By
Page 27 of 27
SECTION 5
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
W WTP Name: Big Buffalo W WTP NPDES Number: NCO024147
Monitoring Period: From 01/01/18 To 03/31/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.11061 -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (timehemp)
Alt. 4/D (No Prior Test)
Alt.2B (Alk Treatment)
Alt. 5/Process to Further Reduce Pathogens
Alt 3/C (Prior Testing]
Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alkernative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If aoulicable to alternative performed (Class A or Class Bl comolete the followine manitorine data:
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 61h
CFU
<29800
<30900
<32500
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g.
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction) X
Option/Alt, 5
(14 -Day Aerobic)
Option/Alt. 9
(Injection)
ption
(40 -day bench)
O/Alt. 2
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requvements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in
ption/Alt.
(30 -day bench)
O 3
Option/Alt. 7
(Drying — Stable)
No vector att
(Spec.
Option/Alt 4
02 uptake)
Option/Alt. 8
(Drying—Unstable)
raction reduction alternatives were performed
40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that theppathogen requirements in 40 CFR 503.32115ANCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that thepathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzky,WWTPSuperintendent MaiIy�o c .1�x16k jock JPrkL4r. SOPcialrs�—
Preparer Name and Title type or print) Land Applier Name and Title (if applicable) (type or p int)
e�4� 1� (9 q i�VIO ` al'►1
Signature of Preparer* Dat Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part .503.9(r) an
d 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc. Laboratory Report
Synagro LOTS Pf
Sanford A eykllaC
Sample Information
W. Varner pai 01/08/18 Aeaa1>r `,
„a
Analyses and Results
NC DENR#654
NC PHHS #37799
US EPA #NC01918
1$0023
as
M. Sims
Data 01!08118
180023 -1 swage cr Fec. Coliform -S <30900 cFu/g 30900 01!98!18 SB 9222D - MF
-2 <30300 CFUI9 30300
-3 <31200 CFUI9 31200
-4 <31200 CFU/9 31200
-5 <30800 CFUIg 30800
-6 <32500 CFUI9 32500
_7 <29800 CFUI9 29800
Geomean <30900
180023 -1 =wage Gr TS (% } 3.26% % 0.01 01112/18 SB 2540 G -TS
-2 3.30% /c 0.01
-3 3,21% % 0,01
4 3,21% % 0.01
-5 3.25% % 0.01
-6 3.08% % 0.01
-7 3.36% % 0.01
Report
ReviewQ / /q/p
Lab Director r,r,Le . Date
219 S. Sl9elc Sll. 919-208-0240
Sanford NC 27330 chrisQcamerontesting.cnm
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VSR
LebTech'sinitials: L/
RAS (IN) DIGESTER
Sample OUT
Volume 100 Mis, 100 MIs.
Dish 4
113.0-113
Lt2, L�S�
1t3.5sq`�
1 ! 22�--
Crucible Weight
Crucible 6 Liquid
Dried
t3umoo
3m
;m
;m
am
Datetl'ime In: 3`�-r� / 9 ' 2 y Drying Oven
DateMme Out $-11 / q•.`{$ Temp: Iny °C
Time In: 11 O•titi Muffle Furnace
Time Out I I .4 8 Temp: °C
Were the samples well mixed before analyzing? Yes ✓ No�
Was the temp of the drying oven in the proper operating range? Yes ✓No_
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes ✓✓ No�
If not what were the corrective actions?
Samplers J rr _ .
Lei
W
W1
DISH
113.0743
W2
WET
212.2151
W3
DRY
113.5594
W4
ASH
113.2222
OUT
City of Sanford
Big Buffalo WWTP
Sludge Calculations
PERCENT VOLITILE SOLIDS 0.695114
W1 DISH 118.751Q
W2 WET 217.9440
W3 DRY 128.1152
W4 ASH 125.1075
PERCENT SOLIDS 9,440010
PERCENT VOLtT1LE SOLIDS 0.321205
PERCENT YOLITII.E SOL.IUS REDUCTION 79.24492
Is it above
VSR c 79.24452
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
WWTPName: Big Buffalo WWTP NPDESNumber: NCO024147
Monitoring Period: From 04/01/18 To 06/30/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens — Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If applicable to alternative performed Class A or Class B complete the following monitorin data:
Parameter Allowable Level in Sludge Path
Vector Attraction Reducti
(40 CFR 503.33/15A NCAC 02T.1107)
ogen Density
No. of
Frequency
Sample
Analytical
Option/Alt. 4
(VS reduction) X
(40 -day bench)
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10 to the 61"
CFU
<40200
130214
300000
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MEN
1000 MEN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 WN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
on
Opti
(40 CFR 503.33/15A NCAC 02T.1107)
-Please indicate option/alternative performed:
Option/Alt. 1
Opfion/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction) X
(40 -day bench)
(30 -day bench)
(Spec. 02 uptake)
on/Alt. 5. Option/Alt. 6
Option/Mt.9 Option/A1t.10
(Injection) (Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503 33/15A
Option/Alt, 7 Option/Alt. 8
(14 -Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying—Unstable)
No vector attraction reduction alternatives were performed
NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the ppathogen requhemems m 40 CFR 503.32/iSA 11 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have not been met" (Please note if you check this statement attach an
explanation why you havenot met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have
been met. I am aware that there ate significant penalties for false certification
"
inoludin,/g fine an^d�7imprisonment
Scott Siletzky, WWTP Superintendent 6Qtir\U� llOV TCC h. esP MlC-L-
Preparer Name and Title (type rint) Land Applier Name and Tit e (if applicable) (type or print)
r� tts ��T t �l /� 211
Signature of Preparer* ate Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) an
d 15A NCAC 2T.1102 (26)
Cameron'resting Services, Inc. Laboratory Report
NG DENR#654
NC PHHS #37799
US EPA #NC01918
Synagro cfaPdj 180600
TProj'dl�ta F' Sanford 'Ft�9ul�tgtY , Yes
Sample Information
1 9 W. Varner Date _ 04/10/18 �Ra `ria; C. Cameron p4te = 04110!18
M
Analyses and Results
180600 -1 swaae Gr Fec. Coliform -S 28$100 cFw9 41200 04!10118 SB 92220 - MF
-2 300000 CFU19 42900
_3 183000 CFw9 45700
4 157000 CFUl9 39200
-5 157000 crura 39400
-6 <40500 cFu,9 40500
-7 <40200 Cr -U19 40200
Geomean 130214
180600 -1 >ludge Gr TS (%) 2.43% 001 04110/18 SS 2540 G -TS
-2 2.33% 001
-3 2.19% 9.01
4 2.55% 0.01
_5 2.54% 0.01
-6 2.47% 0.01
_7 2.49% 0,01
Report/ e
Review )1
a
A�rtznnanrk
Date (
919-208-4240
219 5. Steele Str.
Sanford NC 2!330 cM1ris�aeamer0ntesting.0om
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Grab Date:ff
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Lab Tech's Initials: cl
Samples �I�)
Volume 100 MIS.
Dish #�
Crucible Weight
Crucibfa & Liquid
r 13, 0�J3?
113.498b'
1t L�bC
gm
gm
gm
gm
aDaterFime In: l Y 169Yo Drying Oven
Date/Time Out 4-Zp.7g I 1:4a Temp: /Oq °C
Time In: 10:4Y
Muffle Furnace
Time Out (/. a3 Temp: rPO °C
Were the samples well mixed before analyzing? Ye No./
Was the temp of the drying oven in the proper operating range? Yes_ No.
If not what were the corrective actions?
Was the temp of the Muffle Furnace In the proper operating range? Yes.ZNo_____
If not what were the corrective actions?
Samplers .7"b
,U
W1
W2
W3
74
w1
W2
W3
W4
1N
DISH
WET
DRY
ASH
aur
DISH
WET
DRY
ASN
City of Sanford
Big Buffalo WWTP
Sludge Calculations
y-11► 18
113.0737
213.1344
113.4888
113.2160
PERCENT VOLITILE SOLIDS
112.1619
212.4611
131.2530
126.9007
PERCENT SOL]DS
PERCENT VOLITILE SOLIDS
PERCENT VOLITILE 5OLlDS REDUCTION
Is it above
0.414$4$
0.657191
19.03415
6.227975
84.59658
VSR = 84.59658
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Sanford WQ Permit Number: W00000543
WWTPName: Big Buffalo WWTP NPDESNumber: NCO024147
Monitoring Period: From 07/01/18 To 09/30/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Tosting)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf nnnlienhle to alternntive nerfinryned (Class A or Class Rl camnlete the following monitoring data:
Parameter Allowable Level in Sludge Pathogen Density
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
OppPion/Ah. 1 .
Option/Alt. 2
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10. to. the 6`h
CFU
<36800
<39900
<40500
CFU/g
0
4xyear
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
MPN
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
OppPion/Ah. 1 .
Option/Alt. 2
(VSreduetion) X
(40- day bench)
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15ANCAC
(30 -day bench) (Spec.
Option/Alt, 5 Option/Alt. 6
(14 -Day Aerobic) (Alk Stabilization)
Option/Alt.9 Option/Alt. 10
(Injection) (Incorporation)
Option/Alt3 Option/Alt. 4
02 uptake)
Option/Alt 7 Option/Alt. 8
(Drying—Stable) (Drying—Unstable)
No vector attraction reducti
on alternatives were performed
02T.1107 have been met "
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that thepathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment"
Scott Siletzky, WWTP Superintendent lr cD( Iol, lCC K 9,_.A "C k,
ZPre aver Name and Title (typ r print) Land Applier Name an Title (if applicable) (type or print)
- A. �� Kat � *UAAv .Com- ail �
Signature of Preparer* Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) an
d 15A NCAC 2T.1102 (26)
Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
US EPA#NC01918
�laent Synagro %GTS P.roj: 181099
Project:'; Sanford Regu►afory , Yes
Sample Information
spinpleil„% %, C. F. ;Date 06/27/18 Received J. Cameron Data 06/27/18
Analyses and Results
181099 1 swaee Gr Fec. Coliform -S <36800 CFU/0 36800 06/27/18 SB/CW 9222D - MF
-2 <39200 CFU/9 39200
-3 <38300 CFU/9 38300
-4 <38600 CFUg 38600
-5 <40500 CFU/9 40500
-6 <39100 M19 39100
-7 <40200 CFU/9 40200
Geomean <38900
181099 -1 sludge Gr TS (%) 2.72% 0.01 06/27/18 SB/CW 2540 GTS
-2 2,55% 0.01
-3 2,61% 0.01
-4 2.59% 0.01
-5 2.47% 0.01
-6 2.56% 0.01
"7 2949% 0.01
Report
Review
Project Manager Date 64
219 S. S[eele Str.
Sanford NC 27330 919-208-4240
Chris r(licamcrontesting,com
T
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VSR
Grab Date: 77- t peo 1I y
Lab Tech's Idais: (/(/
Sample RAS {IN) DIGESTER
OUT
Volume 100 Nils. 100 Mis.
Dish#� — —J
Crucible WetgM
4U001e & liquid
Drfed
Bumed
i 13, 0766
gm
2t1.6�03 am
It7.4sp ?
am
tIP5 Y3
gm
t
tt 1.3991 gm
2
ale 3Oo
120. 031-x.
t-7_ ae99
y
Datett'1me In: 7-t 0-IY/ t o:vy
Dateirme Out w I Y / to4 iq r Oven p� Y Tem 10 'C
Time in: _1zt33
Time Out: o Y Muffle Furnace
—1' Temw. Y ro 'G
Were the samples well mixed before analyzing? Yes�/Noy
Was the temp of the drying oven in the proper operating range? Yes � No�
If not what were the corrective actions?
Was the temp of the Muftie Furnace In the proper operaL•ng range? Yes ✓No.
if notwhat were the corrective actions?
Samplers s're t I C�
City of Sanford
Big Buffalo WWTP
Sludge Calculations
111
W1
pISH
113.0786
W2
WET
211.6303
W3
DRY
113.4593
W4
ASH
113.1683
VSR = 54.86063
0.388316
PERCENT VOLITILE SOLIDS 0.760387
W1
DISH
111.3991
W2
WET
209.3004
W3
DRY
120.0312
W4
ASH
117.2299
PERCENT SOLIpS S.S17145
PERCENT VOLITILE SOLIDS 0.324521
P>=RGENT VOLtT]LE SOLIpS REAUCTION 84.88063
Is it above
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility
Name:
City
of Sanford
WQ Permit Number:
WQ0000543
Analytical
(Alk Stabilization)
Option/Alt, 9
WWTPName:
Excee-
Big
Buffalo WWTP
NPDESNumber:
NCO024147
Minimum Geo. Mean Maximum Units
dentes
Monitoring Period: From 10/01/18 To 12/31/18
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. UA (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tf......i:..ohlo t...,itor.,"t:.," nArf"rrnAd trinvc A ..r Clace Rl rmmnlptp the fallowing monitoring data:
Parameter
Vector Att
Allowable Leve] in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
(Alk Stabilization)
Option/Alt, 9
Option/Alt. 10
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2xlOto the 61"
CFU
<40300
<42000
<44100
CFU/g
0
4 x year
Grab
9222D
Coliform
power per gram
of total solids
MPN/g
WN
1000 WN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1 ptiop/Alt.
bench)
Opfion/Alt. 2
(VS reduction) %
(40-daybench)(30-day
Option/Alt. 5
Option/Alt. 6.
(14 -Day Aerobic)
(Alk Stabilization)
Option/Alt, 9
Option/Alt. 10
(Injection)
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
O 3
Option/Alt. 7
(Drying —Stable)
No vector att
Option/Alt. 4
(Speo. 02 uptake)
Option/Alt. 8
(Drying—Unstable)
raction reduction alternatives were performed
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15ANCAC 02T:1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please nate if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination hasbeen made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Scott Siletzkv WWTP Superintendent tn(>l0` �BO I!A (e(SeY-"tk�
Preparer Name and Title (typ r print) LLand App�lier Name and Title (if applicable) (Type or print)
C5 I A1 1.WDeE ani
Signature of Preparer* Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and ISA NCAC
2T.1102 (26)
Cameron Testing Services, Inco Laboratory Report
Synagro
Sanford WWTP
Sample. Information
M. Soya '. 10/01/18
ON
RM
Analyses and Results
NC OENR #654
NC PHHS #37798
US 6PA #NCQ1918
181767
Yes
M, Sims 10!01!18
181707 1 31w 9e G Fec, COIIJOmF$ <43300 CFWO 43300 10/02/18 ERP 9222@ -MF
2 <44100 cFuA2 44100
3 <40500 CFWO 40500
4 X40700 CFUk 40700
5 <40300 CFWm 403U0
6 <43300 CFWg 43390
7 <41700 CFWD 41700
Geomean <42000
181707 1 None cr. TS t /0) 2.31% 007 1p102118 ERP 2540 G •TS
2 2.27% 0.01
3 2.47% 001
4 2.46% 0.01
5 2.48% 0.01
6 2,31% 0.01
7 2.40% a01
Report
Ravlew
Odle «rfl /
219 S. SteeleSlr,
3xiilaad N4 27330 91ri-208-d240
cl�ris(;0gmcranReSting.c0m
i
VSR
Grab Date: 10 � i 5� / $
Lab Tech's Initials: [z i
Sample RAS (IN)
Volume 100 MIs.
Dish #0
Crucible Weight
Crucible & Liquid
Dried
Burned
(12.437`
2iz,4y7S
13.0 ►��
3m
3m
3m
3
DIGESTER
OUT
94
2(1.6'10?
122.6 q! $
118. yGcy
Date/Time In: (�-t1 "�� / f Z�� Drying Oven
DatelTime Out: IDgI 1b / ))12 ,10+ Temp: /04 °C
Time In: l0 1�-IY oCr 04 Muffle Furnace
Time Out:►u-(6.rk . 2:23 Temp: tp o C
v
Were the samples well mixed before analyzing? Yes_ No_
Was the temp of the drying oven in the proper operating range? Yes No_
If not what were the corrective actions?
Was the temp of the Muffle Furnace in the proper operating range? Yes_ No.
If not what were the corrective actions?
Samplers �Wr
City of Sanford
Big Buffalo WWTP
Sludge Calculations
IL'
VSR = 39.88332
W1
DISH
112.7376
W2
WET
212.7475
W3
DRY
113.0127
W4
ASH
112.8870
0.275073
PERCENT VOLITILE SOLIDS 0.456925
OUT
W1
DISH
111.3991
W2
WET
211.6707
W3
DRY
122.0418
W4
ASH
118.4669
PERCENT SOLIDS 10.61387
PERCENT VOLITILE SOLIDS 0.335902
PERCENT VOLITILE SOLIDS REDUCTION 39.88332
Is it above 38%
0
Agricultural Lime Application Log
Year: 2018
Project: Sanford
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
I onsimcre
Applied
Date Applied
n/a
NC
-CH -49-6
6.0
0.0
NC -CH -49-7
6.1
0.0
n/a
NC -CH -49-8
6.2
0.0
n/a
NC -CH -60-1
6.0
0.0
n/a
NC -CH -60-3
6.1
0.0
n/a
NC -CH -60-7
5.7
0.7
0.0
NC -CH -60-11
5.4
1.3
0.0
NC -CH -66-1
5.8
0.4
n/a
NC -CH -66-3
5.9
0.0
n/a
NC -CH -66-4
6.2
0.0
n/a
NC -CH -66-6
6.0
0.0
n/a
NC -CH -66-8
6.1
0.0
n/a
NC -CH -66-11
6.2
0.0
n/a
*Lime to be spread in first quarter 2019
SECTION 7
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