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HomeMy WebLinkAboutWQ0000543_Residual Annual Report 2018_20190315INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0000543 SUBMITTAL DATED: 2/28/2019 Project Contact Information Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Lisa Finnerty Email Address* Ifinnerty@synagro.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0000543 Permittee * Facility Name * City of Sanford City of Sanford Phone Number* 4434899086 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. 2018 Annual Report Please attach all information required or requested for this submittal to be review here. Application Form Engineering Hans, Specifications, Calculations, Etc.) Sanford NC 2018 Annual Report.pdf 16.68MB Upload only 1 RDF document. NUltiple documents must be corrbined into one RDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at: 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/28/2019 435 ` whams Court, Suite 100 Baltimore, MD 21220 wwwsynagro.com FEBRUARY 275 2019 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Centex Raleigh, NC 27699-1617 Re: 2018 Annual Report for Permit No. WQ0000543 Dear NCDEQ: Synagxo is submitting one copy and one electronic copy of the above referenced report on behalf of the City of Sanford, NC. If you have any questions ox need additional information, please do not hesitate to contact Scott Siletzky at (919) 775-8305 or Melinda Boyd at (336) 909-8627. Sincerely, Derrick Shivax Environmental Compliance Manager Enclosures ec: Melinda Boyd, Synagxo Scott Siletzlcy, City of Sanford YOUR PARTNER FORA CLEANER, GREENERWORLD CITY OF SANFORD RESIDUALS LAND APPLICATION PROGRAM Permit No. WQ0000543 2018 ANNUAL REPORT City of Sanford, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen ReductionNectorRttraction Reduction 6. Soil pH &Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQPermit#: WO0000543 County Carteret Year 2018 Facility Name (as shown on permit) City of Sanford W WTP NPDES No. NC0024147 Land Application Operator Synagro Phone# L336)998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A—Residuals Annlication Summarv: Total number of application fields in the permit: 43 Total number of fields utilized For land application during the year: 13 Total amount of dry tons applied during the year for all application sites: 450.84 Total number of acres utilized for land application during the year: 271.20 Part B —Annual Compliance Statement: Facility was compliant during calendar year 2018 with all condifions of the ]and application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I. Part C —Cert Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the you as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.1 105(a) or the Pollutant Loading Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8, All monitoring and reporting requirements in 15A NCAC 02T.1 11 I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediation. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. ification: "L certify, under penalty of law, that the above information is, to the best of rr am aware that there are signifieanY penalties for submitting false information, knowing violations." Hal Heewer, Public City Man ager Permittee Name and Title (type or print) Si a ► �1 Signature of Preparer* 0 D to Si if different from Permittee) (if different and belief, true, accurate, and complete. I possibility of fines and imprisonment forFaffmW Preparer) *Pranarer is defined in 40 CFR Part SOi 9lrl and ISA NCAC 02T .1102 061 ➢RNR FnRM ACF !12/20061 2018 ANNUAL OPERATIONS SUMMARY = LAND APPLICATION IN NC SANFORD,NC SANFORD, NC BUFFALO CREEK WWTP AEROB, DIG. LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS April 2018 1,264,800.00 G 133.44 D 121.03 May 2018 9541800.00 G 100.72 D 91.37 June 2018 725,400.00 G 70.18 D 63.65 July 2018 663,400.00 G 73.03 D 66.24 October 2018 3902600.00 G 47.23 D 42.84 November 2018 217,000.00 G 26.24 D 23.80 YEARLY TOTAL 4,216,000.00 G 450.84 D 408.93 1 /22/2019 SECTION 2 ru C d Y W U W Z Q O 0 J O LL C\[ LL �U)z m O `m o ci Q N d R .. 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L O C N N N N ro C o 0 C N U c U N N .m � N O 0 R N0 y 'y o a a N ro N a) N C ro L O 3 m m c c ° o 'O ro Y O U ro C C N c E c O y � N N Q a,o E Nro� E c 0 o ro o � � U N w N.L' _ O N N _ E n m w W N � N o oe � a N O (6 y �a m ro N c � c 3?'c `m E Q O E O i U � O � C C C N w y N N � D_ E c� O 6 N J N .. L O C N N N N ro C o 0 C N U c U N N .m � N t R y 'y o a a m m Y 6J N ao ao �FEE(n W W nU cc E E c E a v mEmma� �aooa m ro 2 o o N ro N a) N C ro L O 3 m m c c ° o 'O ro Y O U ro C C N c E c O y � N N Q a,o E Nro� E c 0 o ro o � � U N w N.L' _ O N N _ E n m w W N � N o oe � a N O (6 y �a m ro N c � c 3?'c `m E Q O E O i U � O � C C C N w y N N � D_ E c� O 6 N J N .. L O C N N N N ro C o 0 C N U c U N N .m � N t 3 'C Y 6J W W E E c E a E E Q? m ro 2 o o a < C) n D. cn N ro N a) N C ro L O 3 m m c c ° o 'O ro Y O U ro C C N c E c O y � N N Q a,o E Nro� E c 0 o ro o � � U N w N.L' _ O N N _ E n m w W N � N o oe � a N O (6 y �a m ro N c � c 3?'c `m E Q O E O i U � O � C C C N w y N N � D_ E c� O 6 N J N .. L O C N N N N ro C o 0 C N U c U N N .m � N e% a6 c 3 \22eeeReeeReae\/\ //7755{§§§}§§§$e/ \\ i B5\ )\] � $7! G!( \\((\\\\(\\}}\ !§§Q<((f!!fa ) ) � 0 ( � 0 E e � � - f; ' _ 2#542:[! {Er:%z) ! r U) IL U) 0 2 U) <C f N 0 W } /)//)/]))]]///#0 � §�j }§{ � % ) \\� /}k §\\ k§(} k)( k)) (ilk \� ƒ]) /!§§ e% a6 c 3 \22eeeReeeReae\/\ //7755{§§§}§§§$e/ \\ i B5\ )\] � $7! G!( \\((\\\\(\\}}\ !§§Q<((f!!fa ) ) � 0 ( � 0 E e � � - f; ' _ 2#542:[! {Er:%z) ! r U) IL U) 0 2 U) <C f N 0 W } /)//)/]))]]///#0 � � % ) /}k k§(} k)( k)) (ilk ƒ]) /!§§ e% a6 c 3 \22eeeReeeReae\/\ //7755{§§§}§§§$e/ \\ i B5\ )\] � $7! G!( \\((\\\\(\\}}\ !§§Q<((f!!fa ) ) � 0 ( � 0 E e � � - f; ' _ 2#542:[! {Er:%z) ! r U) IL U) 0 2 U) <C f N 0 W } /)//)/]))]]///#0 � k§(} (ilk /!§§ e% a6 c 3 \22eeeReeeReae\/\ //7755{§§§}§§§$e/ \\ i B5\ )\] � $7! G!( \\((\\\\(\\}}\ !§§Q<((f!!fa ) ) � 0 ( � 0 E e � � - f; ' _ 2#542:[! {Er:%z) ! r U) IL U) 0 2 U) <C f N 0 W } /)//)/]))]]///#0 � m:§ >4 777 =�_ \\§/Q k�\ \\\ (\/\ t \\ eet 3§A ]2 {§' {\0 \� \�\- \\\\\\\\\ CL= \)§(\j§ ¥ §\§)! I ca§ - �. a, } a �j o , \ % \\ w / - \ \ \\ \ w / ` \ / §\ % \ ) ) { \ |2� «!§§\�:{\! / ) �k{ § 2)!)\ \ C.)\ (/ \ §$ 2 n u } ) /12 12§§ \\ E°) 0gm at Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 2/8/2018 1/1/2018-5131/2018 0.8377 AEROB. DIG, LIQUID Na mg/I = (Na mg/kg x % Solids) _ 100 = (3150 x 2.5300) + 100 = 79.695 Ca mg/I = (Ca mg/kg x % Solids) = 100 = (17300 x 2.5300) - 100 = 437.69 Mg mg/I = (mg mg/kg x % Solids) + 100 = (5850 x 2.5300) - 100 = 148.005 Na meq = Na mg/I + Molec.Wgt.Na = 79.695 + 23 = 3.465 Ca meq = Ca mg/I + MoleaWgLCa = 437.69 + 20 = 21.8845 Mg meq = Mg mg/1 + Molec.Wgt.Mg = 148.005 : 12 = 12.3338 SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.465 = SgrRoot[0.5(21.8845+12.3338)] = 0.837702 Printed: 1/25/2019 Page 1 08:27 t, --e Waypoint a ANALYTICAL 6/18/2018 Synagro Central LLC/ Sanford Mary Brewer 284 Boger Road Mocksville, NC, 27028 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypointa na lytics I. com Ref: Analytical Testing Report Number: 18-159-0203 Project Description: Sanford Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received samples) on 6/8/2018 for the analyses presented in the fallowing report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were pertormed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, p a� c. -r Pauric McGroary Agronomist Laboratory's liability in any c/aim relating to analyses performed shall be limited to,. at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid forpertormance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida Eg71087 North Carolina 257 South Carolina 93007 Page 1 of 8 Wa OI �� M® 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 Y ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-159-0203 Client Project Description: Sanford Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61070 Sanford Solids 06/07/2018 14:45 06/08/2018 61070 Sanford Solids 06/07/2018 14:45 06/08/2018 6010D WiN WTN: Waypoint Analytical - TN, Memphis, TN, Certifcation: #1354 Page 2 of 6 m a V Z rni o p U' C7 U 2 U N 2 ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ Z F- LL GO m d' O to N Z O O O O O O O O O O O O� M E m C m o oO tp0: fOO (pD (pO (p0 (pp (OO t00 (00 t00 aT J o LL O N N fn co m a p Ol 3 r (p (p (n a 3 0 0 0 to co co co �o � co co m <o o o o m W W 3 p• ,a Q E u a ri of i+i ih ri ri of ri i+i ni ri ai iii m of Cri 0 0 o p o 0 0 0 0 0 0 0 0' o c- 3 'm N K K ao co M m m m ro M m m m m ro w m m m N N N N � ❑ p ❑ m m V O V 7 V a V d' V V V N O O O O O O O O O O O O O O O O O a o ❑ ❑ ❑ y�y�� gygy ❑ U y Y Y Y Y Y Y Y Y Y 0 N 0 L y m co Z J Q O O O O O O O O O O O O O O O O O O LL O O O O O O O O p Lq p O O M O O O t[J .o Q O Qz a a w W M a r O M N M V O W N M O L J r p N N m K m 0 U � � +`• o Z • a rn m m s m� � ami E ao cn N 2 a v m Y N N `z? Z a rn ZZ E ' �E izm o 'mv N3 ° u Eum ma 0 mm o o K¢ n F 2 H na o U MW q _ Q:2 U N Q O Z V A� r �- O W N M O L J r p N N m K m 0 U � � +`• o Z • a rn m m s m� � ami E ao cn N 2 a v m Y N N `z? Z a rn ZZ E ' �E izm o 'mv N3 ° u Eum ma 0 mm o o K¢ n F 2 H na o U MW q _ Q:2 U N Q O Z V A� M N +� M �D u N �y — @ � N -d e Z c � � � y a a x « L J � LL 'O z 0 2 U O Z G � e 3 O1 o � a 3 C m 3 � .n « °0 - c 3� F D N n fn O +� � O � � d @ m � � Z � .. y a a E ro J � Z � z c � U O Z G d U a 0 0 m N � J O J N m � U O Z G d. 0 N m m N F D fn 0 O � � O (ep O D D D d d d N (O (O (O [O (D O (O E o a o 0 0 0 0 o 0 0 d 0 0 0 0 0 0 d m 0 0 0 ❑❑❑ V 7 'd' V V' V V a f0 (O (O (O (O (D (O <O (O O O O O O O O O O • I y1V \V�,� Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypointanalytical.tom Cooler Receipt Form Customer Number: 48489 Customer Name: Synagro Central LLC/ Sanford Report Number: 18-159-0203 Shipping Method Q Fed Ex Q US Postal Q Lab Q Other: UPS. Q Client Q Courier Thermometer ID: Shipping container/cooler uncompromised? � Yes � No Number of coolers received r 1 Custody seals intact on shipping container/cooler? Q Yes Q No t, Not Required Custody seals intact on sample bottles? Q Yes Q No � Not Required Chain of Custody (COC) present? � Yes Q No COC agrees with sample label(s)? � Yes Q No COC properly completed � Yes Q No Samples in proper containers? � Yes Q No Sample containers intact? � Yes Q No Sufficient sample volume for indicated test(s)? � Yes Q No All samples received within holding time? � Yes Q No Cooler temperature in compliance? � Yes Q No Cooler/Samples arrived at the laboratory on ice. � Yes Q No Samples were considered. acceptable as cooling process had begun. Water -Sample containers properly preserved � Yes Q No Q N/A Water -VOA vials free of headspace Q Yes Q No � N/A Trip Blanks received with VOAs � Yes Q No � N/A Soil VOA method 5035 —compliance criteria. met Q Yes Q No � N/A High concentration container (48 hr) � Law concentration Encore samplers (48 hr) High concentration pre -weighed (methanol -14 d) � Low cont pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? (� Yes � No Comments: Signature: Brandi Watson Date:&Time: 06/08/201813:56:06 Page 5 of 6 W Q Z U W O a o❑IL r\�Jj IL ❑a o¢ Fw wW it EL a i w ❑g N Z� J a �w O � N ¢ W Z oa Z U 9 bo g abed N V N h m of z O U LL NU1 co LL Z � J U Q W U COil z 0 C7 � O J w Z 2 J O 2 h W � d N U W Q Z U W O a o❑IL r\�Jj IL ❑a o¢ Fw wW it EL a i w ❑g N Z� J a �w O � N ¢ W Z oa Z U 9 bo g abed N V N h m of z O U LL NU1 co LL Z � J U Q W U COil z 0 z U d N O � U U� m x CL in 2 h® tl 6 z U U o` Z O Z 2 a Z . ti! J � � I ® a i h V) Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample as Report Range Ratio 2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 6/7/2018 6/1/2018-6/30/2018 1.0293 AEROB. DIG. LIQUID Na mg/I = (Na mg/kg x % Solids) . 100 = (3620 x 2.3200) + 100 = 83.984 Ca mg/I = (Ca mg/kg x % Solids) + 100 = (15100 x 2.3200) + 100 = 350.32 Mg mg/I = (mg mg/kg x % Solids) + 100 = (3960 x 2.3200) + 100 = 91.872 Na meq = Na mg/I + Molec. Wgt.Na = 83.984 + 23 = 3.65148 Ca meq = Ca mg/I + MolecWgLCa = 350.32 + 20 = 17.516 Mg meq = Mg mg/I + Molec.Wgt.Mg = 91.872 = 12 = 7.656 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.65148 + SgrRoot[0.5(17.516+7.656)] = 1.02926 Printed: 1/25/2019 Page 1 08:27 Waypoint ANALYTICAL 17(IC:i%I�7iE�3 Synagro Central LLC/ Sanford Mary Brewer 284 Boger Road Mocksville, NC, 27028. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypointa n alytica I.co m Ref: Analytical Testing Report Number: 18-184-0200 Project Description: Sanford Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received samples} on 7/3/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite....) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any feld parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results far solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only tc the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, p a•r r Pauric McGroary Agronomist Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid far performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 257 South Carolina 93007 '�•' Page 1 of 7 Waypoint. ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypoi nta nalytica Isom Client: Synagro Central LLC/ Sanford CASE NARRATIVE Project: Sanford Lab Report Number: 18-184-0200 Date: 7/18/2018 TKN (Titration) Method SM�500-NH3C-TKN Analyte: TKN OC Batch No: E64890 Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MOL. The actual result was XXJ which calculates to a recovery of XX°/ . Analyte was flagged for 0% recovery in the LCS and/or LCSD .The actual result was 0.870 which calculates to a recovery of 85%. QC Batch No: E84890 The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Nitrate+ Nitrite Nitrogen Method SM-4500NO3F Sample 61491 (Sanford 3 of 4) Analyte: NO3+NO2-N ClG Batch No: E84942/E64892 The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory duplicates. Solids Total Mercury Analysis - CVAA Method SW -7471 B Analyte: Hg QC Batch No: E84928/E84889 MS/MSD Recovery failed, PDS confirmed matrix interference Page 2 of 7 Waypoi nt.., 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-184-0200 Client Project Description: Sanford Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61491 Sanford 3 of 4 Solids 06/27/ZO18 10:30 07/03/2018 61491 Sanford 3 of 4 Solids 06/27/2018 10:30 07/03/2018 6010C WTN WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 3 of 7 Z o O O U 2 O N M 0 �= U U U U U U U U U U U Z F 0 0 In N Z 0 0 0 0 0 O O O O O O� MLL coo coo m. coo coo coo coo coo too m 0 o O N N N co 0 Q O D D D w j v o 0 o m ro ro ro co m m m m m m o o r Lh LD Lo 6 6 6 6 Lb 6� e- O O H N_ N_ 00 N_ N N in LLJ in iri N in Lf) O O lrm ya: m m ro ro ro ro N m m co m m m m m m m ❑ ❑ ❑ i+l M N (� N c� a N N_ N N N [� (� � � � 0 0 0 O O O r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 �� ❑ Z Z Z Z Z Z Z Z Z Z Z p �' Y Y Y Y Y Y Y Y Y Y Y N K m m m m m m m m m m m� � J Z Q O O O O O O O o O 0 0 0 0 0 0 OJ 0 0 0 0 0 0 o 0 o co 0 6 o v O W O O O O O O O O N l0 0 0 0 d M D c m a v � m m � Z .. z E n o D E o E m m Z z Z E cn H ° a a in U U) °¢ ci N Q O z 4 D E 0 � � u N - m > ' � o�� N Or J x E c m o U o O. o Z K � D V o m 3 � a 3 c � 3 m Z• � d pip C E 3� c b n Z o O O U 2 O N M 0 �= U U U U U U U U U U U Z F 0 0 In N Z 0 0 0 0 0 O O O O O O� MLL coo coo m. coo coo coo coo coo too m 0 o O N N N co 0 Q O D D D w j v o 0 o m ro ro ro co m m m m m m o o r Lh LD Lo 6 6 6 6 Lb 6� e- O O H N_ N_ 00 N_ N N in LLJ in iri N in Lf) O O lrm ya: m m ro ro ro ro N m m co m m m m m m m ❑ ❑ ❑ i+l M N (� N c� a N N_ N N N [� (� � � � 0 0 0 O O O r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 �� ❑ Z Z Z Z Z Z Z Z Z Z Z p �' Y Y Y Y Y Y Y Y Y Y Y N K m m m m m m m m m m m� � J Z Q O O O O O O O o O 0 0 0 0 0 0 OJ 0 0 0 0 0 0 o 0 o co 0 6 o v O W O O O O O O O O N l0 0 0 0 d M D c m a v � m m � Z .. z E n o D E o E m m Z z Z E cn H ° a a in U U) °¢ ci N Q O z 4 0 m m � N Or J N m o U +� o Z K m m o m Z• � c Z o O O U 2 O N M 0 �= U U U U U U U U U U U Z F 0 0 In N Z 0 0 0 0 0 O O O O O O� MLL coo coo m. coo coo coo coo coo too m 0 o O N N N co 0 Q O D D D w j v o 0 o m ro ro ro co m m m m m m o o r Lh LD Lo 6 6 6 6 Lb 6� e- O O H N_ N_ 00 N_ N N in LLJ in iri N in Lf) O O lrm ya: m m ro ro ro ro N m m co m m m m m m m ❑ ❑ ❑ i+l M N (� N c� a N N_ N N N [� (� � � � 0 0 0 O O O r 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 �� ❑ Z Z Z Z Z Z Z Z Z Z Z p �' Y Y Y Y Y Y Y Y Y Y Y N K m m m m m m m m m m m� � J Z Q O O O O O O O o O 0 0 0 0 0 0 OJ 0 0 0 0 0 0 o 0 o co 0 6 o v O W O O O O O O O O N l0 0 0 0 d M D c m a v � m m � Z .. z E n o D E o E m m Z z Z E cn H ° a a in U U) °¢ ci N Q O z 4 )(§ ExM / 6w :E )$\ ~ � )/ a- \> 2 2 7 7 'rWW' » , °= 00m $) G!� \}\ § §kk.=\\j\\\\\\ 7z z z z !/f2J \ M � (L a - z § \ - » ƒ .�\ \ \\ LU a -,,,,� , Lq \ - ` \ \ \\ t _ \ / - ( WE ° - \ \ \_ \7{/ - §§ \®/0 �® ) $ £ ° £ m) §jn §§ e `z{�{)k � � §0 t\\ \VW$ a6,!!) - \ ;« L) // Waypoint ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypointa nalydca I. com Cooler Receipt Form Customer Number: 46489 Customer Name: Synagrd Central LLC/ Sanford Report Number: 18-184-0200 Shipping Method Q Fed Ex Q US Postal Q Lab Q Other UPS Q Client Q Courier Thermometer ID: Shipping container/cooler uncompromised? � Yes Q No Number of coolers received Custody seals intact on shipping container/cooler? Q Yes (� No � Not Required Custody seals intact on sample battles? Q Yes Q No � Not Required Chain of Custody (COC) present? � Yes Q No COC agrees with sample label(s)? � Yes (� No GOC properly completed � Yes (� No Samples in proper containers? � Yes Q No Sample containers intact? � Yes Q No Sufficient sample volume for indicated test(s)? � Yes Q No All samples received within holding time? � Yes Q No Cooler temperature in compliance? � Yes Q No Cooler/Samples arrived at the laboratory on ice. � Yes Q No Samples were considered acceptable as cooling process had begun. Water -Sample containers properly preserved Q Yes Q No � N/A Water-VOAvials free of headspace Q Yes Q No � N/A Trip Blanks received with VOAs Q Yes Q No � N/A Soil VOA method 5035 —compliance criteria met Q Yes Q No � N/A � High concentration container (48 hr) � Low concentration Encore samplers (48 hr) � High concentration pre -weighed (methanol -14 d) � Low concyre-weighed vials (Sod Bis -14 d) Special precautions or instructions included? Q Yes � No Comments: Signature: Brandi Watson Date &Time: 07/03/2018 13:34:48 Page 6 of 7 � y \/& +\l \ § _ z0Z9 a § / Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 6/27/2018 7/1/2018-9130/2018 1.1161 AEROB. DIG. LIQUID Na mg/I = (Na mg/kg x %Solids) + 100 = (3890 x 2.6400) + 100 = 102.696 Ca mg/I = (Ca mg/kg x %Solids) :100 = (17900 x 2.6400) = 100 = 472.56 Mg mg/I = (mg mg/kg x %Solids) :100 = (3810 x 2.6400) + 100 = 100.584 Na meq = Na mg/I - Molec.Wgt.Na = 102.696 + 23 = 4.46504 Ca meq = Ca mg/I + Molec.Wgt.Ca = 472.56 + 20 = 23.628 Mg meq = Mg mg/I _ Molec.Wgt.Mg = 100.584+ 12 = 8.382 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.46504 + SgrRoot[0.5(23.628+8.382)] = 1.11609 Printed: 1/25/2019 Page 1 08:27 Wal(Do point, nt ANALYTICAL 1 011 6/2 01 8 Synagro Central LLC/ Sanford Mary Brewer 284 Boger Road Mocksville, NC, 27028 Ref: Analytical Testing Report Number: 18-278-0223 Project Description: Sanford WWTP 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypo intana lytica I. co m Dear Mary Brewer: Waypoint Analytical Virginia, Inc. received sample(s) on 10/5/2018 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table f applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Anal ysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Pauric McGroary Agronomist Laboratory's liability in any claim relating fo analyses performed shall be limited to, at laboratory's option, repeating the. analysis in question at laboratory's expense,. or the refund of the charges paid for performance of said analysis. Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014 Florida E871087 North Carolina 257 South Carolina 93007 4A Page 1 of 6 Waypoint.. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 18-278-0223 Client Project Description: Sanford WWTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 63033 Sanford WWTP Solids 10/01/2018 14:30 6010D 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Soltds 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 63033 Sanford WWTP Solids 10/01/2018 14:30 10/05/2018 WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354 Page 2 of 6 SM-4500-NH3C WTN 9045D WTN 4500NO3F-2011 WTN 6010D WTN SW -74718 WTN SM-4500-NH3C-TKN WTN SM -2540G WTN \ ( )t\0 [ /10 - )) ( co E; - _ _ f! ' _ _mE K e2 - «�k ( !E \\{}iw#)G L 0 0E -=;r[2m:« ƒk2 n /;)//\//7£kla,#7$ k�§ \ }( E49 77/ =ee . . .. k§! {\k \\\\ \ D0@0@d@@@ � ;,r,,, , LU � cc •§§(§/(\ / � \ \ )t{}LR f a ;! ;§ e §# )® 2 !� - t`-0Io0 ff ]\z If U) ko Waypoint..''�W^���t'� ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 °Fax 804-271-6446 www.waypoi nta nalyH ca Isom Cooler Receipt Form Customer Number: 46489 Customer Name: Synagro Central LLC/ Sanford Report Number: 18-278-0223 Shipping Method Fed Ex � US Postal � Lab � Other : �— UPS (� Client � Courier Thermometer ID: Shipping container/cooler uncompromised? � Yes Q No Number of coolers received r 1 Custody seals intact on shipping container/cooler? � Yes � No � Not Required Custody seals intact on sample bottles? � Yes � No � Nat Required Chain of Custody (COC) present? � Yes � No COC agrees with sample label(s)? � Yes � No COCproperlycompleted � Yes � No Samples in proper containers? � Yes � No Sample containers intact? � Yes 0 No Sufficient sample volume for indicated test(s)? � Yes � No All samples received within holding time? � Yes � No Cooler temperature in compliance? � Yes � No Cooler/Samples. arrived at the laboratory on ice. � Yes � No Samples were considered acceptable as cooling process had begun. Water -Sample containers properly preserved � Yes � No � N/A Water-VOAvialsfree ofheadspace � Yes � No � N/A Trip Blanks received with VOAs a Yes � No � WA Soil VOA method 5035 –compliance criteria met � Yes � No � N/A � High concentration container (48 hr) � Law concentration Encore samplers (48 hr) � High concentration pre -weighed (methanol -14 d) � Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? � Yes � No Comments: Signature: Brandi Watson Date &Time: 10/05/2018 14:23:19 Page 5 of 6 � )\ �\ ��� � �� � ,ua; \( / \§ � )\ �\ ��� � �� � ,ua; Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2039-01-AEDLIQ-NC SANFORD, NC BUFFALO CREEK WWTP 10/1/2018 101112018-1/31/2019 0.7776 AEROB, DIG. LIQUID Na mg/I = (Na mg/kg x %Solids) + 100 = (2680 x 2.9000) + 100 = 77.72 Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (18100 x 2.9000) = 100 = 524.9 Mg mg/I = (mg mg/kg x %Solids) + 100 = (4770 x 2.9000) + 100 = 138.33 Na meq = Na mg/I - Molec.Wgt.Na = 77.72 : 23 = 3.37913 Ca meq = Ca mg/I - Molec.Wgt.Ca = 524.9 + 20 = 26.245 Mg meq = Mg mg/I - Molec.Wgt.Mg = 138.33 + 12 = 11.5275 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.37913 + SgrRoct[0.5(26.245+11.5275)] = 0.777557 Printed: 1/25/2019 Page 1 08:28 SECTION 3 r N N 0 a o � o w w w 6 0 5 0 Ln O Q r N N 0 o � o w w w 0 N 0 Ln O U � W L' a w O r N N o � w w w 0 N 0 Ln U � L' z A p m m � .z 0 O 0 F. q N qF v v o w U V U V 0 d�z N a a F. c a g V4 zd w r N N w w w N zv Ln z m m .z Jb O F. q N qF a a U V V d�z N a a F. c a g V4 zd w q o F o 0 F � r rod E. O g 'Q1 U o 0..p N 5 .�aax q O v U vF y o U C � gHw4� N U qu a r N N N w N Ln z m O x q N a a U V V a a c a g V4 zd w q o r rod E. 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F � V z�z as V o0 0 o� z z N N N o � � U O o C o 0 to N a N 1 F M a a a v v F'� v �aaxo8 0 a Q q ca �N caHw¢ � W a vOQi o � � �d a 0.. N N z N V x P. F � V V o � � U k 0 48 u a a U a O Y+ U U U U a a �rti�r] a W 48 u a a U a O Y+ U U U U �rti�r] W W W W U W www w a z m a U C o W U U N W a W U U F4 .Ni U 4 z�z U 48 u a a U a U U U U �rti�r] W W W W U W www w a z m a U C V U p N W a b U F4 .Ni U 4 z�z U r1 �' 0 Q9 w N a Y H � U d�z m m m m � C a i � ;:'� P O o 0 0 .L x N N N N 0.ry �3yaaaa Q Q Q Q p U rn Q a a a a a Q Q Q Q Q W¢WQW¢w¢W¢' .dam o U U U o U Q O o NF+F MMMNN N vM CJv C7 C�Cv C7Cv �% p N O N Q N N i �a w 6 a z m a U C V U p N W a b U F4 .Ni U 4 0 U r1 �' 0 Q9 w N Y H � U �a m U C U F4 4 0 r1 �' w w �a x w W a U U W o W W a U w w ch A x w W U U W o W W U w w ch N y 0. M � z n v N N u� ^ o rr+ U z�z W 4 0. 0. �m U lV v a .a a a a �z w � M o 0. O m ^ p � � 6 U g o z 0 N I O 5wwx a IM :'=caq U U m � b b N N U � � a 00 0 � o x w W N ch N y M � z n ^ o rr+ U W 4 �m U lV v a .a a a a Q w � o m ^ p � F 6 U x ch N M ^ o U 4 a .a a a a Q w � x I C9 w P a U U o N Q W Nco v w w Q C9 w U U o N W W Nco v w w z wy N NN � ry N � x N ? 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Q N e N N � so F N 3 N 0 z a N w N N z N z V y N N x U w tl oV s H V N b �a ra N V a N w o A � N a N V y N U A a s b p� �a ra N � a w I w p V a W �(y z w 6 v 6 a � O Q N H q W w V W �(y z w v 6 NO° � O Q N H N W b w V W N U w v 6 NO° w � N N a b v b N z z N M qc N �z N x A U pp m a e �� Na U =. c ro w >a o a U ,ob w � V a Q o ' �aax o 0 3 N 0 U Q 7 Q Vp� v = V � u ` o � N a� so a �H 0 �3 ck N N dQ 0 v d w N NO° N 0 N M z N x A U pp m a e N U c w � a U w � V N Q o p F 7 Q Vp� N M A U pp a e c w � a w � V Q a SECTION 4 q9SUMM111 Anaf y6cal Laboramries March 07. 2018 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Sanford Dear Will Varner: SummitE vironmental Technologies, Inc. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL (330) 253-8211 FAX: (330) 253-4489 Website httn:/Anvw.settek.com Order No.: 18020868 Summit Environmental Technologies, Inc. received 1 samples) on 2!16/2018 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, j Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, Californ ia 07256CA, Colorado, Connecticut PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, lllinvis 200061, Indiana C -OH -13, Kansas &10347, Kentucky (Uvdergrouvd Storage Tank) 3, Kentucky 90146, Louisiana 04061, Maryland 339, Minnesota 4097I1,.New Hampshire 2996, New Jersey OH006, New Yolk 11777, Noah Ceraliva 39705 and 631, North Dakota R-201, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 27 SUMMIT suinnaftEnvironmentai Te hao WinInc. Case Narrative 331010 ,�a sr. CNVIRONMENTAL TECHNOLOOlES, 1NC. Cuyahoga Falls, Ohio 44223 WO#: 18020868 Analytical LaboraNOPq TEL: (330) 253-8211 RIX- (330) 253-4489 Website: h_lo.-I viv settek.00m Date: 3/7/2018 CLIENT: Synagro Project: Sanford WorkOrder Narrative: 18020868: This report in its entirety consists of the following documents: Cover Letter; Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples. are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. with this report are This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Salnple Notes: 18020868-OOla tclp-voc-mstr_tclp(8260): Sample extracted in methanol. 18020868-001a tclp-voc-mstr_tclp(8260): VOC Reporting Limit elevated due to sample being treated as waste dilution due to matrix. Oeiginal Page 2 of 27 M1su 'll Suninit Environmental Technologies, In Qualifiers and Acronyms 33/0 Win 5 RWIRONMENTAL I£CHNOL.0mrs, We Cuyahoga Falls, Ohio 4421 W04: 18020868 Anafytfcal taborstio6es TEL: (330) 253-82// FAX: (330) 253-445 Website; huv:/hvww.settek.co Date: 3/7/2018 These commonly used Qualifiers and Acronyms may or may not be present in this report Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. II The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration oris estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. it Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amountsof analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QLr/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCI. Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit 1CV Initial Calibration Verification RA Reanalysis 1CB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Cheek CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 27 SU 111_ Summit Environmental Technologies, Inc. workOPCIer 3310 Win St. MVIRONh1ENTAL TECHUOLOWES,+NC Cuyahoga Falls, Ohio 44223 Sample Summary Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18020868 Website: huP71Aviviv.settek.com 07 -Mar -18 CLIENT: Synagro Project: Sanford Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 18620868-001 Sanford 2/8/2018 11:15:00 AM 2/16/2018 10:10:00 AM Solid Page 4 of 27 YOUMMI T unit Environmental Teehaal10WinS. Analytical Report 3310 wa sr. rNVIR0NIAEN7ALTECHN0L0G,E5, INC Cuyahoga Falls, Ohio 44223 (base report) Anafyf:r-af Laharaosrhi TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18020868 Website.: htta./Avivw settek.com Date Reported: 3/7/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 2/8/2018 11:15:00 AM Lab ID: 18020868-OOIA Project: Sanford Client Sample ID Sanford Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: EAM TCLP MERCURY ANALYSIS (SWI 31117470) TCLP Mercury ND 0.00500 mg/L 1 2/21/2018 4:07:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW6010D Analyst: KMS TCLP METALS ANALYSIS (SW131116010) TCLP Arsenic(As) ND 0.500 mgfL 1 2/21/2018 9:23:33 PM TCLP Barium(Ba) ND 5.00 mg/L 1 2/21/2018 9:23:33 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 2/21/2018 9:23:33 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 2/21/2018 9:23:33 PM TCLP Lead(Pb) ND 0.500 mg/L 1 2/21/2018 9:23:33 PM TCLP Selenium(Se) ND 0.0500 mg/L 1 2/21/2018 9:23:33 PM TCLP Silver(Ag) ND 0.500 mg/L 1 2121/2018 9:23:33 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW82700 SW361OC Analyst: BJH TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270) 1,4-Dichlorobenzene ND 0.0800 mg/L 2 2/22/2018 5:48:00 PM 2,4,5-Trichlorophenol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM 2,4,6-Trichlorophenol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM 2,4-Dinitiotoluene ND 0.0400 mg/L 2 2/22/2018 5:48:00 PM o-Cresol ND 0.200 mg/L 2 2/22/2018 5:48:00 PM m/p-Cresol(s) ND 0.200 mg/L 2 2/22/2018 5:48:00 PM Cresols, Total ND 4.00 mg/L 2 2/22/20185:48:00 PM Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 2/22/2018 5:48:00 PM Hexachlorobenzene ND 0.0400 mg/L 2 2/22/2018 5:48:00 PM Hexachloroethane ND 0.0800 mg/L 2 2/22/2018 5:48:00 PM Nitrobenzene ND 0.0800 mg/L 2 2/22/20185:48:00 PM Pentachlorophenol ND 0.200 mg/L 2 2/22/20185:48:00 PM Pyridine ND 0.200 mg/L 2 2/22/2018 5:48:00 PM Surr: 2-Fluorophenol 55.6 10-109 %Rec 2 2/22/2018 5:48:00 PM Surr Phenol-d6 52.2 10-109 % Rec 2 2/22/2018 5:48:00 PM Surr: Nitrobenzene-d5 .91.4 19-120 % Rec 2 2/22/2018 5:48:00 PM Surr: 2,4,6-Tribromophenol 59.1 10-120 % Rec 2 2/22/2018 5:48:00 PM Surr: 2-Fluorobiphenyl 99.8 22-117 % Rec 2 2/22/2018 5:48:00 PM Qualifiers: * Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit N Tentatively identified compounds ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 27 HISUMMInt Suarmir Environmental Technologies, WSt. 3310 Win St. rf&VIRONNIENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Anafythcal Laboratories TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hHoWwwwsefiekcore CLIENT: Synagro Matrix: SOLID Lab ID: 18020868-OOIA Project: Sanford Client Sample ID Sanford Analyses Result Analytical Report (base report) WO#: 18020868 Date Reported: 3/7/2018 Tag Number: Collection Date: 2/8/2018 11:15:00 AM RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP SEMI -VOLATILES ANALYSIS (SW131118270) Surr: p-Terphenyl-d14 111 34-116 TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND Toxaphene ND Endrin ND gamma -BHC ND Heptachlor ND Heptachlor epoxide ND Methoxychlor ND Burr: TCMX 65.8 Surr: DCB 40.0 SW8270D SW3510C Analyst: BJH %Rec 2 2/22/2018 5:48:00 PM SW8081 SW3510C Analyst: JBN 0.0200 mg/L 2 2122/2018 5:38:00 MEK ND PM 0.0400 mg/L 2 2/22/2018 5:38:00 ND' Chloroform PM 0.00200 mg/L 2 2/22/2018 5:38:00 Vinyl chloride ND PM 0.00200 mg/L 2 2/22/2018 5:38:00 mg/L 1000 PM 0.00200 mg/L 2 2/22/2018 5:38:00 mg/L PM 0.00200 mg/L 2 2/22/2018 5:38:00 5.00 PM 0.00200 mg/L 2 2/22/2018 5:38:00 PM 5.00 PM 10 - 119 % Rec 2 2122/2018 5:38:00 PM PM 10 - 119 %Rec 2 2122/2018 5:38:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP HERBICIDES ANALYSIS (SW1311/8151) SW8151A SW8151A Analyst: JBN 2,4-D ND 1.00 21415 -TP ND 0.500 It Surr: DCAA 85.4 20-140 TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 1,2-Dichloroethane ND MEK ND Benzene ND Carbon tetrachloride ND Chlorobenzene ND' Chloroform ND Tetrachloroethene ND Trichloroethene ND Vinyl chloride ND Qualifiers: * Value exceeds Maximum Contaminant. Level. H Holding times for preparation or analysis exceeded MC Value is below Minunuin Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits mg/L 1 2/28/2018 7:54:00 1000 2/21/20184:44:00 PM mg/L 1 2/28/2018 7:54:00 mg/L 1000 PM %Rec 1 2/28/2018.7:54:00 25.0 PM SW8260B SW1311M Analyst: CTB 5.00 H Value above quantitation mglL 1000 2/21/20184:44:00 PM 5.00 mg/L 1000 2/21/20184:44:00 PM 25.0 mg/L 1000 2/21/20184:44:00 PM 5.00 mg/L 1000 2/21/2018 4:44:00 PM 5.00 mg/L 1000 2/21/2018 4:44:00 PM 5.00 m9/L 1000 2/21/20184:44:00 PM 5.00 mg/L 1000 2/21/2018 4:44:00 PM 5.00 mg/L 1000 2/21/20184:44:00 PM 5.00 mg/L 1000 2121/20184:44:00 PM 2.00 mg/L 1000 2/21/20184:44:00 PM range M Manual Integration used to detemrine area response N Tenmtively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 7 of 27 Summit Environmental TeclmolInc. SUMMIT 331010Win St. FNVIROWENTALT£CHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 AnafyWaf Laborsiorles TEL: (330) 253-8211 FLY.. (330) 253-4489 Website: hap.,Uvwvv.seaek.com CLIENT: Synagro Matrix: SOLID Lab ID: 18020868-001A Project: Sanford Client Sample ID Sanford Analyses Result TCLIP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS Surr; 4-Bromofluorobenzene 80.8 Sum Dibromofluoromethane 101 Surr: Toluene -d8 86.6 NOTES: PM Sample treated as waste dilution due to matrix. RCI -SOLID -W/ IGNITABILITY1030 1000 REACTIVE CYANIDE (9014/7.3.3.2) -SOLID Not Detected Cyanide, Reactive ND RCI -SOLID -W/ IGNITABILITY1030 130 IGNITABILITY OF SOLIDS (SW -846: 1030) Ignitability non-flammable RCI -SOLID -W/ IGNITABILITY1030 PM PH (SW9046D) pH 7.6 RCI -SOLID -W/ IGNITABILITY1030 REACTIVE SULFIDE (9034)/7.3.4.2 Sulfide, Reactive 40.0 QuaOSers: Analytical Report (basereport) WO#: 18020868 Date Reported: 3/7/2018 Tag Number: Collection Date: 2/8/2018 11:15:00 AM RL Qual Units DF Date Analyzed SW8260B SW1311M Analyst: CTB 70 - 130 %Rec 1000 2/21 /2018 4:44:00 SWI 030 Analyst: PM 70 - 130 % Rec 1000 2/21/2018 4:44:00 Not Detected 0 PM 70 - 130 % Rec 1000 2/21/2018 4:44:00 RPD outside accepted recovery limits RL PM SW9014 Analyst: MS 0.500 mg/Kg 1 2/22/20184:49:00 PM SW9045D SWI 030 Analyst: Analyst: AJT s.u.@79.2C 1 3/1/201811:19:00 AM SW9034 Analyst: MS 25.0 mg/Kg 1 2122/2018 4:49:00 PM * 1 2/21/2018 10:30:00 AM SW9045D Holding times for preparation or analysis exceeded Analyst: DHC s.u.@79.2C 1 3/1/201811:19:00 AM SW9034 Analyst: MS 25.0 mg/Kg 1 2122/2018 4:49:00 PM * Value exceeds Maximum Contaminant Level E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected 0 RSD is greaterthan RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 8 of 27 I�s„mm;tEruironmentalTechnologies, Inc. Accreditation Program 3310 Win St. Analytes Report 04VIRONhtENTALTECHNOLOCIE3, INc Cryahoga Falls, Ohio 44223 Y P Arralyficerl Laboratories TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 18020868 Website: hM.11imv3v.setiekconn 07-Mar48 Client: Synagro State: NW Project: Sanford Program Name: NC—WW—SCM Sample ID Ma[rix Test Name Analyte Sta[us 18020868-001A Solid Ignitability of Solids (SW -846: 1030) Ignitability A Solid pH(SW9045D) Hydrogen Ion (PH) A Solid Reactive Cyanide (9014/7.33.2) -Solid Cyanide, Reactive U Solid Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Solid TCLP Herbicides Analysis(SW1311/8151) 214,5 -TP A Solid TCLP Herbicides Analysis (SW1311/8151) 2,4-1) A Solid TCLP Herbicides Analysis(SW1311/8151) DCAA A Solid TCLPMercury Analysis(SW1311/7470) Mercury A Solid TCLP Metals Analysis (SW1311/6010) Arsenic A Solid TCLP Metals Analysis(SW1311/6010) Barium A Solid TCLP Metals Analysis(SW1311/6010) Cadmium A Solid TCLP Metals Analysis(SW1311/6010) Chromium A Solid TCLP Metals Analysis (SW 1311/6010) Lead A Solid TCLP Metals Analysis (SW1311/6010) Selenium A Solid TCLP Metals Analysis(SW1311/6010) Silver A Solid TCLP Pesticides Analysis (SW1311/808 1) 2,2',3,3',4,4',5,5',6,6'- A Decachlorobiphenyl Solid TCLP Pesticides Analysis (SW1311/808 1) Chlordane, total A Solid TCLP Pesticides Analysis (SW1311/8081) Endrin A Solid TCLP Pesticides Analysis (SW1311/8081) gamma -BHC A Solid. TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Solid TCLP Pesticides Analysis (SW 1311/808 1) Heptachlor epoxide A Solid TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Solid TCLP Pesticides Analysis (SWI 311/8081) Tetraehlore-m-xylene A Solid TCLP Pesticides Analysis (SWI 311/8081) Toxaphene A Solid TCLP Semi -Volatiles Analysis(SWI311/8270) 1,4 -Dichlorobenzene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4,5 -Trichlorophenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-Tribromophenol A Solid TCLP Semi -Volatiles Analysis (SWI 311/8270) 2,4,6 -Trichlorophenol A Solid TCLP Semi -Volatiles Analysis (SW 1311/8270) 2,4-Dinitrotoluene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorobiphenyl A Solid TCLP Semi -Volatiles Analysis (SW 1311/8270) 2-Fluorophenol A NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Version #2 Page 9 of 27 S U 1 11 SummitEnvi onmentalTechnologies, Inc. Accreditation Program 3310 win St. Analytes Report MVIRONMAENTAL T2CONOLOGIES, INC Cxryahoga Falls, Ohio 44223 y P dnaPyfiraf Lahm'atwTs TEL: (330) 253-8211 FIX: (330) 253-4489 WO#: 18020868 Website: hov:lAviviv settelceom 07 -Mar -18 Client: Synagro State: NW Project: Sanford Program Name: NC—WW—SCM Sample ID Matrix Test Name Analyte Status 18020868-001A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Methylpbenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 3,4-Methylphenol A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Cresols, Total A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobenzene A Solid TCLP Semi -Volatiles Analysis(SWI311/8270) Hexaehlorobutadiene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachloroothane A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Nitrobenzene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Nitrobenzene -d5 A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Pentachlorophenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Phenol -d6 A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) p-Terphenyl-d14 A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) Pyridine A Solid TCLP Volatiles Analysis 1,1-Dicliloroethene A Solid TCLP Volatiles Analysis 1,2-Dichloroethane A Solid TCLP Volatiles Analysis 2-Butanone A Solid TCLP Volatiles Analysis 4-Bromolluorobenzene A Solid TCLP Volatiles Analysis Benzene A Solid TCLP Volatiles Analysis Carbon tetrachloride A Solid TCLP Volatiles Analysis Chlorobenzene A Solid TCLP Volatiles Analysis Chloroform A Solid TCLP Volatiles Analysis Dibromofluoromethane A Solid TCLP Volatiles Analysis Tetrachloroethene A Solid TCLP Volatiles Analysis Toluene -d8 A Solid TCLP Volatiles Analysis Trichloroethene A Solid TCLP Volatiles Analysis Vinyl cldoride A NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Version #2 Page 10 of 27 » \\ � )\ )! {E _3N }5/!)))//{„ co )[> ) )\ ) } §q) � )\ )! {E _3N }5/!)))//{„ co )[> ) ) } §q) )/ kk\ \ �k\ !y r �!\ {) \ \k) \ ) ) \} /\ \ \\\ &>!> }§ \\ � )\ )! {E _3N }5/!)))//{„ co )[> ) ) } §q) )/ kk\ \ �k\ !y r \� {) \ \k) \ ) ) \} /\ \ \\\ &>!> }§ \\ 2 ;J&« �{\ CY < =>e, § Of � )\ )! {E _3N }5/!)))//{„ co )[> ) ) } §q) )/ kk\ \ �k\ !y r \� {) \ tm\ \ ) ) \} /\ \ \\\ &>!> (§£ \\ ;J&« �{\ CY ;)»2 =>e, � )\ )! {E _3N }5/!)))//{„ co #»- ) ) } §q) )/ kk\ \ \] !y r \� {) \ U) \ � )\ )! {E _3N }5/!)))//{„ co #»- ) ) } ;m! )/ kk\ \ !y r \� \ U) \ ) � )\ )! {E _3N }5/!)))//{„ co Ce� Lo #»- ) ) } ;m! )/ kk\ \ !y r \� );} \ ) ) \} /\ \ &>!> Ce� Lo #»- ) ) } ;m! )/ kk\ !y \� );} \ ) ) \} /\ \ &>!> (§£ \\ ;J&« �{\ CY ;)»2 =>e, \ 0 #»- ) ) ;m! )/ kk\ !y \� );} ) \} /\ \ &>!> \\ ;J&« CY \ 0 ) ) ;m! )/ !y \� ) \} i§±{ &>!> \\ ;J&« )»2} ;)»2 =>e, \ 0 ) ) ) )/ !y \} i§±{ &>!> \\ ;J&« )»2} ;)»2 =>e, ) )/ !y \} \\ \\\/ 772/ m -y: \ % \ � d d ' 0 U � m E W 0 m 0 d w J r m E � 46 m 0 d N n A. 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a a+ > E w O 0 N a ❑ cl ❑ 0 o a a � 0 N N W F O O o m au 0 a to (9 o U = ai Q Y m_ 0 a ❑ ❑ d ~ E m N � � 3 U � � a E Z J F C E a Q c J 42 C w Q c E U :i rn U � E0 0 - a a+ > E w 0 0 N � ❑ cl ❑ 0 o a a � 0 N N W F O O o m au 0 U to (9 o U K z Q Y x 0 a ro ui d ~ e m Z U � ❑ U � � a E Z a F E E :i Y p � E 0 0 a a+ Z E ro 0 0 m 0 E cl ❑ 0 o a 0 � 0 N N N E O O m m au 0 U to :i � w °10 E 0 0 0 Z Z a Z 0 0 m 0 E a ❑ 0 o a 0 � 0 N N N a O O m au 0 U to (9 U U :i � w °10 E 0 0 0 Z Z Z Z 0 0 0 0 � W ❑ � o a 0 0 0 0 :i � w °10 E o d Z Z Z Z Z Z Z m 0 � W ❑ � o a � ❑ N :i � w °10 E o d N E t U E M w 0 � W ❑ � o a � ❑ N m N a a O O m ❑ 0 U to U K z Q ° x 0 a ro ui d ~ e m o > Z ❑ U E m E Z U L E E a c J 42 C Q c E U D a z O F W m 2 = 2a 0 :i � w E o d N E t U E M w 0 � W ❑ � o a � ❑ N m N a a O v) m ❑ 0 U to U K z Q ° a 3 = ro ui d ~ e :i � w E o - N E t U ❑ M w 0 � W K � � ❑ N m N a a O v) m a 0 U to U osaib a 3 = ro ui d ~ e 0 o > Z E U E m �5. � in in u � a a J 42 C Q U :i � w E o - N E � U > M w 0 � W K � � ❑ N m c a a O v) m 0 U to U osaib a 3 Y u N d ~ e > Z a U E m �5. � in in E � a W :i a w m � N E � U M � 0 U n � � ❑ N N c a � O O m n U to :i a w m � ° E N yob J 0 U 0 � ❑ N N c mE O O O n U Q :i a w � ° E 0 0 0 0 C a N N O O O O :i a w � ° E 0 0 0 0 C :i a w � ° E X C a � b o _ `o a U osaib ❑ 3 � u v ~ e > a a a E m �5. w in in E W 42 g :i w � ° E C a � b a � osaib � 3 � o e > a a w O w :i w v C a � 3 o e a E 42 g a z w m 2a 0 :i v m a � o E � 0 x � a :i Ic e M E s F� a N Y = ❑ O w °q' U s F� a N Y = ❑ v m °q' o M a o U W s F� a N Y = ❑ O m m ��2 0 M a o � J a � a O U N m d W � m E t° ❑ O m (q w 0 M m " � J a � a ❑ J N ❑ d W � m E t° N m N m U Q ❑ O m (q w Um M M N � J a a o J J FT m A W U E t° N m N � C � ❑ O m (q w �L M M N o a a U U J J ❑ m A W ❑ E N v N N C � (A U Q ❑ O m (q w �L M a o o a a 0 U O E m A in N N C � Q p� 3 N � v U � d a .E m � ca m ❑ O N ❑ a w E � m E w m iii U Q ❑ O m 41 w � M o o a a 0 E m A in N C � Y p� 3 N � c � a .E m � ca m ❑ O � O a w E w m x W U Q N O m w � o a p w . a 0 v A o C � Y p� 3 N � c � a .E � � ca cPa� w O c4 w . a 0 o C � 3 � c � a .E � 5 0 a 7 a x � a W . a 0 o C � a .E � 5 0 7 a x � a d § « \\ ) tk )3 ) \)}i $)»3 !)2{ ±6»§ )\ »j() )) \))\ ,l:a ) )) \) )\ )) /))) 11§, ]\2) 11 n — a b ?� a o � J s U Aw N c-� r-� a E N n — a c y a c � J s � n K 0 0 m o y C � a U v J m � ❑ N � N c-� r-� a E N n — a c y a c � 0 s � n 0 K 0 m o y C U U v J J � ❑ N � E v m a rn U 4 N c-� r-� a E N n — a c y a c � o s � n 0 0 m o a C E m v � m � a A p a 3 � 4 C p O b 'o O d t o m 00 m ❑ N � d � E � m E ` a o > w U Q N c-� r-� a E N c-� m E E c I n — a o y a c N o s � n o 0 m o a C E m v E m � a A p Q 3 � 4 C p O b b d t o m 00 m ❑ N � d � E � m v1 U Q c-� m E E c I n N w a c N o � � s7 N 0 m a a C � � v E m � in A p Q 3 � 4 C p U b b d t o m O � a d E y m o > (A U Q N w O v e s7 N m a a v e H C � � v o � A p 3 � C p b b G t v � H C � � v ro � 3 � C p b b �b _ o > > � � v �b _ o > > x rn a E E 0 m i0 d v m a ' d ❑ rc ro U a` E E 0 m i0 a � m a o d ❑ rc ro n � E ti p J y a ❑ F ti � r r x �m o N N E o � ❑ m N y J a a C z Y c Q N � = N N N N_ o Z ❑ E E 0 m i0 a � m a o d ❑ rc ro n � E ti p ❑ y a a F ti � r r x �m o N N E n o E w N y J a N C z Y z z N � = N N N N_ o Z ❑ ❑ " d E � o � o ro m m m o ro a ❑ o a` � w N w N E m w E d m U E E 0 m i0 a � m a o d ❑ rc ro n � E ti p Y y a a F ti � r r x �m o N r E n o E w N y J a > C z Y z z N � W Nai= 0 N N_ o Z ❑ U " d E � o � o ro m E E 0 m i0 a � m a o d ❑ rc ro n � E ti p ❑ N a cl F ti a �m r x �m o N r E a a E m N y J a a m z � z z o � z Nai= 0 N N_ N V ❑ oU a d E E o � o ro m m m o ro a ❑ o d � w N J N E m w E d m U Sm w U Q E E 0 m i0 a � m w rc d ❑ rc ro n � E n � ❑ N a cl n � a �m r x � o N r E a a E m N y J a a m z � z z o � z Nai= 0 N N_ N V ❑ E E 0 m N a � m w rc 45 ❑ rc ro n � E n � ❑ N a a n � � �m r � �m o N N E a a E 'c N y J a N m z � z Q o � z Nai= 0 N N_ N V ❑ o 0 d E E N o ro E m o 67 a ❑ o d ❑ w C J N E m w E C) o U Sm A 0 Q 0 E E 0 m N a � m w rc d ❑ rc ro n � E n � J N a a n � � �m r � �m o N N E a a E 'c y � a N m z � z Q o � z = 0 N N V E o 0 d F= E u o ro � m o 67 ❑ � d ❑ w N N E m w E m_ o U Sm A U Q E E 0 r-� T m N a o � w K d v rc ro n � E n � J N a a � � �m r � � o N N E a a E 'c y � a N z z � z Q o � z = 0 N r-� T m N a o � w K 0 v rc ro n � E n � Y N a a � � �m � � o N N E a iu E 'c y � a N N � z � o o z = 0 N H F E 0 0 d F= E u o ro � C o 67 ❑ � d a` w m E m w E o U r-� T m N a o � w K 0 v rc ro n � E n � Y N a a � a �m � � o N r E a iu ❑ 'c y � w N N � z � o o z 0 o H F E CY d F= a r-� T m N a o � K d v rc ro n � E n � a y a ❑ � a �m � � c N r E a iu ❑ m rn w a � z � o o z 0 o U E CY E a u o ro � C J 67 ❑ � d � w m E m a E o U A U Q r-� T m N a c K d � ro � E n � a y a ❑ � a a � � c m r E iu ❑ m rn w a � z � o o z 0 o O E r-� T m - a c K O � ro � ❑ n � a y a � O a m m c m E iu rn w a = N o z 0 o O E N E a o m C J � d w E m a r-� T m - a c K O � ro � c n � y y a � O a m m c m rn w a o z O ~ r a a r-� T m - a c K O W ro � c n � hq pj � O a m m N 3 c � O a m � d N E m m (q U r-� T N O W ro c ❑ � hq pj � O a r-� T �7 � c 3 c � a �7 ! \ / / # \\ i )! \ / / # i )! 46 \ / / # i 46 CK )) \ {\ \) m \� E \ \ ) /\ \ ) aj 4j )} ((2 )�) �{) ))!) \}{/ LU \\ \ \ / / # i )) \ {\ \) m \� E \ \\ ) /\ \ ) )} )�) ))!) \}{/ LU \\ \ \/\ j#2� \ / / # i )) \ {\ \) m E \ \\ ) /\ \ ) )} \ / / # )) {\ \) E \ \\ ) /\ \ ) )} )�) ))!) \}{/ LU \ / / # )) {\ \) E \\ /\ \ ) )} )�) \ / / # )) {\ \) E \\ ) )} ))!) \}{/ \\ \ j#2� \ / / # )) \) \\ )} ))!) \}{/ j#2� =,2: m % \ 2 ■ § § § [® {\ ) ;2! )Z ) ;2! i] ))§$ \� i j49 EE!! \ ±{\] \}$2 CY \))/ \\ ;y:* \1§, 7]>) \\\ \\ \ ) i] ))§$ i j49 EE!! \ ±{\] \}$2 \))/ \\ ;y:* \1§, 7]>) \\ \ ) i] ))§$ i j49 EE!! ±{\] \}$2 \))/ ;y:* ) i] \� \\ \}$2 \1§, 7]>) (a {w )Z ) )Z )/ ) )/ & ƒ �§ 3 \ \) cl E \ \\ \ \\ ) )/ & ƒ \\ 3 \ \) \\ \ \\ ) )/ & ƒ 3 \ ) )/ })) \) \\ )[\� \\\2 \\!) 7\§: \\\\ =,(a })) )[\� )\)� )})) \\\\ \\\\ \ M 0 N p v o O m O v w N p v o N m O v w N o o N m O E K � N ❑ an p� � � O � 0 n Q E m m in m N � Q Q 3 U 0 o p W b O c4 m 9 o ..Of v E � m E m m m v N o m O F K N N ❑ an p� � � O a 0 v Q E m N m N � v Q 3 U 0 5 p W b O c4 C3" o ..Of v v E m m m U Q N O N � N an p� � � O a � E 0 v Q � c o• � v 3 5 p W b O c4 � E � c 3 5 p ti b v v � (® } {w \ Cf )/ � } \ Cf )/ \) � } \ Cf \) \( (*/! iD k§ \0 m , / }� / d)} j E \\ § \ \/ } 6E!§ (\2 3z\\ (\2 � } \ \) \( (*/! \ k§ \0 m , / }� / d)} j E \\ § \ \/ } 6E!§ (\2 3z\\ (\2 I:22 �{\ \{\) { ) ,»_« \#J« \�{ � ) \ \) \( (*/! \ k§ \0 m , / }� / d)} j E \\ / \ \/ } 6E!§ (\2 3z\\ � ) \ \) \( (*/! k§ \0 , / }� / j E \\ / \ \/ } 6E!§ (\2 3z\\ I:22 �{\ \{\) , ,»_« \#J« � � \ / ) \ \) \( (*/! k§ \0 , / }� / )§0 \\ / \ \/ } 6E!§ 3z\\ I:22 \{\) , ,»_« \#J« \�{ \ \ \ U)L6 co 0 a L6 � \ / ) \ \) \( (*/! k§ \0 \� }� ))!! )§0 � \ / ) \ \) \( (*/! k§ \0 i# }� ))!! )§0 \\ \ \/ } � \ / ) \ \) \( (*/! \0 i# }� ))!! )§0 � \ / ) \ \) \( (*/! \0 i# cl ))!! )§0 \/ } 6E!§ � \ / ) ) \ \) (*/! \0 i# ))!! )§0 #;!{ 6E!§ 3z\\ I:22 \{\) »/:2 ,»_« ) \) \0 i# )§0 \\ 23 \)\� \{\) \#J« \ % Q / \0 )§0 \\)\ \)\� \\\/ \ % Q / J±;T) `\\\ ( f\} / °5= \ � �$ DO k §! �0 A({ � ) ! Lq ) \ { ) 46 \ (;\ \o. /*) \}� jL) \\ \ _ \ / ) � }a\\ tj)} \\\\ j)\\ ;»_C4 ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) )! Lq ) \ { ) 46 \ (;\ \o. /*) \}� jL) \\ \ _ \ / ) � }a\\ tj)} \\\\ j)\\ ;»_C4 ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) ) \ { ) 46 \ (;\ \o. /*) \}� jL) \\ \ _ \ / ) � }a\\ tj)} \\\\ j)\\ ;»_C4 ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) \}� jL) \\ \ _ \ / ) � }a\\ tj)} \\\\ j)\\ ;»_C4 ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) _ \ / ) � }a\\ tj)} \\\\ j)\\ ;»_C4 ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) ) {) \) \} \/ ))j) f}j) ]4«: =,ya \\0 ]!/0 }\)) ))!) \\0 ]!/0 }\)) ))!) � ca ) k )/ ())( � ca ) k ())( \§ ,2\ \� ) \ \\ \ }\/\ \\ f:(y � ) k ())( \§ �2\ \� ) \ \\ \ }\/\ \\ f:(y }§ { { ) \/ J);@ �{\ to \\!/ \/ \ ( ( 44J: co $§; $;f /(\ /\ \ � ) k ())( \§ �2\ \� § \\ \ � ) k ())( \§ �2\ § \\ \ }\/\ � � / ) k ())( �2\ § \ }\/\ \\ f:(y � / ) k ())( ));» § \ }\/\ \\ f:(y { ) \/ J);@ to \\!/ \/ \ ( 44J: $§; /(\ � / ) k ())( ));» }\/\ \\ f:(y \/ J);@ \\!/ \/ \ � / / ) k ())( ));» }\/\ \\ f:(y J);@ / f) §; \\ \) \\!/ 44J: sill 011111 LL LL IN�tF�ti�t� t Y smile frSUMMIT Summie Environmental Technologies, Inc. 3310 Win St. "MRONhtENTAL IECHMOLOGrEs,;NC- Cuyahoga Falls, Ohio 44223 Sample Log -in Check List Analytical Latw atorfes TEL: (330) 253-8211 FAX (330) 253-4489 Website: hily.11mvm.settekconr Client Name: SYN -NC -27028 Logged by: Christopher Livengood Completed By: Antonio Betscakos Reviewed By: Jennifer Woolf Chain of Custody 1, Is Chain of Custody complete? 2, How was the sample delivered? Log In 3_ Coolers are present? Work Order Number: 18020868 2/1612018 10:10:00 AM 2/16/2618 3:34:3fi PM 2/19/2018 4:28:11 PM 4. Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? No. Seal Date: 5. Was an attempt made to cool the samples? 5. Were all samples received at a temperature of >0' C to 6.0°C �. Sample(s) in proper container(s)? 6. Sufficient sample volume for indicated test(s)? 9_ Are samples (except VOA and ONG) properly preserved? 10. Was preservative added to bottles? 11, Is the headspace in the VOA vials less than 1/4 inch or 6 mm? 12. Were any sample containers received broken? 13. Does paperwork match bottle labels? (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? 15. Is it clear what analyses were requested? 16. Were all holding times able to be met? (If no, notify customer for authorization.) Special Handling (if applicable) Yes ❑�/ FedEx as as Yes ElSigned By: as 0 Yes 0 Yes Yes Yes❑ Yes ❑ Yes ❑ as El Yes WY es Yes 66Yes W Rcip o: El11ElElL11 No ❑ Not Present ❑ Na ❑ NA ❑ Noi Present 0 NA ❑ NA El NA ❑� NA No VOA Vials R1 17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑� Person Notified: Date By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 16. Additional remarks: Cooler Information Cooler No Temp °C Condition Seal Intact Seal No Seal 1 4.3 Good Not Present Date Signed By Page 27 of 27 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Sanford WQ Permit Number: W00000543 W WTP Name: Big Buffalo W WTP NPDES Number: NCO024147 Monitoring Period: From 01/01/18 To 03/31/18 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.11061 -Please indicate level achieved and alternative performed: Class A: Alt. 1/A (timehemp) Alt. 4/D (No Prior Test) Alt.2B (Alk Treatment) Alt. 5/Process to Further Reduce Pathogens Alt 3/C (Prior Testing] Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alkernative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If aoulicable to alternative performed (Class A or Class Bl comolete the followine manitorine data: Parameter Allowable Level in Sludge Pathogen Density No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10to the 61h CFU <29800 <30900 <32500 CFU/g 0 4 x year Grab 9222D Coliform power per gram of total solids MPN/g MPN 1000 MPN per gram of MPN/g. total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: Option/Alt. 1 (VS reduction) X Option/Alt, 5 (14 -Day Aerobic) Option/Alt. 9 (Injection) ption (40 -day bench) O/Alt. 2 Option/Alt. 6 (Alk Stabilization) Option/Alt. 10 (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) "1 certify, under penalty of law, that the pathogen requvements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in ption/Alt. (30 -day bench) O 3 Option/Alt. 7 (Drying — Stable) No vector att (Spec. Option/Alt 4 02 uptake) Option/Alt. 8 (Drying—Unstable) raction reduction alternatives were performed 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that theppathogen requirements in 40 CFR 503.32115ANCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that thepathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Siletzky,WWTPSuperintendent MaiIy�o c .1�x16k jock JPrkL4r. SOPcialrs�— Preparer Name and Title type or print) Land Applier Name and Title (if applicable) (type or p int) e�4� 1� (9 q i�VIO ` al'►1 Signature of Preparer* Dat Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part .503.9(r) an d 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report Synagro LOTS Pf Sanford A eykllaC Sample Information W. Varner pai 01/08/18 Aeaa1>r `, „a Analyses and Results NC DENR#654 NC PHHS #37799 US EPA #NC01918 1$0023 as M. Sims Data 01!08118 180023 -1 swage cr Fec. Coliform -S <30900 cFu/g 30900 01!98!18 SB 9222D - MF -2 <30300 CFUI9 30300 -3 <31200 CFUI9 31200 -4 <31200 CFU/9 31200 -5 <30800 CFUIg 30800 -6 <32500 CFUI9 32500 _7 <29800 CFUI9 29800 Geomean <30900 180023 -1 =wage Gr TS (% } 3.26% % 0.01 01112/18 SB 2540 G -TS -2 3.30% /c 0.01 -3 3,21% % 0,01 4 3,21% % 0.01 -5 3.25% % 0.01 -6 3.08% % 0.01 -7 3.36% % 0.01 Report ReviewQ / /q/p Lab Director r,r,Le . Date 219 S. Sl9elc Sll. 919-208-0240 Sanford NC 27330 chrisQcamerontesting.cnm T o m co o O�QQ®OO r� r U rn vi a 4} m m A U t o'. azo d m }� iaylo ci U V) i i Z sseJE)'Zo g N a W V j w apseld l L m o v sselo'1 L j o v �j rn 0 le!AlW Ob w N N 1 Na Z epaloeH. - N o Z ~ 009 C � fU v j leJ 2/l E .p C U w a z (N/A) aal z o xiaaelN E qejE) /dwoo V Q awi� i CL N L .0 a .. v Egs N in a m c �. y. m o v N cr � VSR LebTech'sinitials: L/ RAS (IN) DIGESTER Sample OUT Volume 100 Mis, 100 MIs. Dish 4 113.0-113 Lt2, L�S� 1t3.5sq`� 1 ! 22�-- Crucible Weight Crucible 6 Liquid Dried t3umoo 3m ;m ;m am Datetl'ime In: 3`�-r� / 9 ' 2 y Drying Oven DateMme Out $-11 / q•.`{$ Temp: Iny °C Time In: 11 O•titi Muffle Furnace Time Out I I .4 8 Temp: °C Were the samples well mixed before analyzing? Yes ✓ No� Was the temp of the drying oven in the proper operating range? Yes ✓No_ If not what were the corrective actions? Was the temp of the Muffle Furnace in the proper operating range? Yes ✓✓ No� If not what were the corrective actions? Samplers J rr _ . Lei W W1 DISH 113.0743 W2 WET 212.2151 W3 DRY 113.5594 W4 ASH 113.2222 OUT City of Sanford Big Buffalo WWTP Sludge Calculations PERCENT VOLITILE SOLIDS 0.695114 W1 DISH 118.751Q W2 WET 217.9440 W3 DRY 128.1152 W4 ASH 125.1075 PERCENT SOLIDS 9,440010 PERCENT VOLtT1LE SOLIDS 0.321205 PERCENT YOLITII.E SOL.IUS REDUCTION 79.24492 Is it above VSR c 79.24452 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Sanford WQ Permit Number: W00000543 WWTPName: Big Buffalo WWTP NPDESNumber: NCO024147 Monitoring Period: From 04/01/18 To 06/30/18 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens — Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If applicable to alternative performed Class A or Class B complete the following monitorin data: Parameter Allowable Level in Sludge Path Vector Attraction Reducti (40 CFR 503.33/15A NCAC 02T.1107) ogen Density No. of Frequency Sample Analytical Option/Alt. 4 (VS reduction) X (40 -day bench) Excee- of Type Technique Minimum Geo. Mean Maximum Units dentes Analysis Fecal 2x10 to the 61" CFU <40200 130214 300000 CFU/g 0 4 x year Grab 9222D Coliform power per gram of total solids MPN/g MEN 1000 MEN per gram of MPN/g total solids (dry weight) Salmonella 3 WN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform on Opti (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: Option/Alt. 1 Opfion/Alt. 2 Option/Alt. 3 Option/Alt. 4 (VS reduction) X (40 -day bench) (30 -day bench) (Spec. 02 uptake) on/Alt. 5. Option/Alt. 6 Option/Mt.9 Option/A1t.10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503 33/15A Option/Alt, 7 Option/Alt. 8 (14 -Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying—Unstable) No vector attraction reduction alternatives were performed NCAC 02T.1107 have been met." "I certify, under penalty of law, that the ppathogen requhemems m 40 CFR 503.32/iSA 11 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have not been met" (Please note if you check this statement attach an explanation why you havenot met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there ate significant penalties for false certification " inoludin,/g fine an^d�7imprisonment Scott Siletzky, WWTP Superintendent 6Qtir\U� llOV TCC h. esP MlC-L- Preparer Name and Title (type rint) Land Applier Name and Tit e (if applicable) (type or print) r� tts ��T t �l /� 211 Signature of Preparer* ate Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) an d 15A NCAC 2T.1102 (26) Cameron'resting Services, Inc. Laboratory Report NG DENR#654 NC PHHS #37799 US EPA #NC01918 Synagro cfaPdj 180600 TProj'dl�ta F' Sanford 'Ft�9ul�tgtY , Yes Sample Information 1 9 W. Varner Date _ 04/10/18 �Ra `ria; C. Cameron p4te = 04110!18 M Analyses and Results 180600 -1 swaae Gr Fec. Coliform -S 28$100 cFw9 41200 04!10118 SB 92220 - MF -2 300000 CFU19 42900 _3 183000 CFw9 45700 4 157000 CFUl9 39200 -5 157000 crura 39400 -6 <40500 cFu,9 40500 -7 <40200 Cr -U19 40200 Geomean 130214 180600 -1 >ludge Gr TS (%) 2.43% 001 04110/18 SS 2540 G -TS -2 2.33% 001 -3 2.19% 9.01 4 2.55% 0.01 _5 2.54% 0.01 -6 2.47% 0.01 _7 2.49% 0,01 Report/ e Review )1 a A�rtznnanrk Date ( 919-208-4240 219 5. Steele Str. Sanford NC 2!330 cM1ris�aeamer0ntesting.0om h p -0 I. y N U o `o a> t U rn E� a h p hl N m� a> E� VSR Grab Date:ff / l/ Lab Tech's Initials: cl Samples �I�) Volume 100 MIS. Dish #� Crucible Weight Crucibfa & Liquid r 13, 0�J3? 113.498b' 1t L�bC gm gm gm gm aDaterFime In: l Y 169Yo Drying Oven Date/Time Out 4-Zp.7g I 1:4a Temp: /Oq °C Time In: 10:4Y Muffle Furnace Time Out (/. a3 Temp: rPO °C Were the samples well mixed before analyzing? Ye No./ Was the temp of the drying oven in the proper operating range? Yes_ No. If not what were the corrective actions? Was the temp of the Muffle Furnace In the proper operating range? Yes.ZNo_____ If not what were the corrective actions? Samplers .7"b ,U W1 W2 W3 74 w1 W2 W3 W4 1N DISH WET DRY ASH aur DISH WET DRY ASN City of Sanford Big Buffalo WWTP Sludge Calculations y-11► 18 113.0737 213.1344 113.4888 113.2160 PERCENT VOLITILE SOLIDS 112.1619 212.4611 131.2530 126.9007 PERCENT SOL]DS PERCENT VOLITILE SOLIDS PERCENT VOLITILE 5OLlDS REDUCTION Is it above 0.414$4$ 0.657191 19.03415 6.227975 84.59658 VSR = 84.59658 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Sanford WQ Permit Number: W00000543 WWTPName: Big Buffalo WWTP NPDESNumber: NCO024147 Monitoring Period: From 07/01/18 To 09/30/18 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Tosting) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf nnnlienhle to alternntive nerfinryned (Class A or Class Rl camnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: OppPion/Ah. 1 . Option/Alt. 2 No. of Frequency Sample Analytical Excee- of Type Technique Minimum Geo. Mean Maximum Units dences Analysis Fecal 2x10. to. the 6`h CFU <36800 <39900 <40500 CFU/g 0 4xyear Grab 9222D Coliform power per gram of total solids MPN/g MPN 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: OppPion/Ah. 1 . Option/Alt. 2 (VSreduetion) X (40- day bench) CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/I SA NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15ANCAC (30 -day bench) (Spec. Option/Alt, 5 Option/Alt. 6 (14 -Day Aerobic) (Alk Stabilization) Option/Alt.9 Option/Alt. 10 (Injection) (Incorporation) Option/Alt3 Option/Alt. 4 02 uptake) Option/Alt 7 Option/Alt. 8 (Drying—Stable) (Drying—Unstable) No vector attraction reducti on alternatives were performed 02T.1107 have been met " "I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have not been met" (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that thepathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Scott Siletzky, WWTP Superintendent lr cD( Iol, lCC K 9,_.A "C k, ZPre aver Name and Title (typ r print) Land Applier Name an Title (if applicable) (type or print) - A. �� Kat � *UAAv .Com- ail � Signature of Preparer* Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) an d 15A NCAC 2T.1102 (26) Cameron Testing Services, Inc. Laboratory Report NC DENR#654 NC PHHS #37799 US EPA#NC01918 �laent Synagro %GTS P.roj: 181099 Project:'; Sanford Regu►afory , Yes Sample Information spinpleil„% %, C. F. ;Date 06/27/18 Received J. Cameron Data 06/27/18 Analyses and Results 181099 1 swaee Gr Fec. Coliform -S <36800 CFU/0 36800 06/27/18 SB/CW 9222D - MF -2 <39200 CFU/9 39200 -3 <38300 CFU/9 38300 -4 <38600 CFUg 38600 -5 <40500 CFU/9 40500 -6 <39100 M19 39100 -7 <40200 CFU/9 40200 Geomean <38900 181099 -1 sludge Gr TS (%) 2.72% 0.01 06/27/18 SB/CW 2540 GTS -2 2,55% 0.01 -3 2,61% 0.01 -4 2.59% 0.01 -5 2.47% 0.01 -6 2.56% 0.01 "7 2949% 0.01 Report Review Project Manager Date 64 219 S. S[eele Str. Sanford NC 27330 919-208-4240 Chris r(licamcrontesting,com T a a m 3 N N m lQ L U N C D 'O Q l0 O a a m 0 Q a� v m 3 Y O 3 L N VSR Grab Date: 77- t peo 1I y Lab Tech's Idais: (/(/ Sample RAS {IN) DIGESTER OUT Volume 100 Nils. 100 Mis. Dish#� — —J Crucible WetgM 4U001e & liquid Drfed Bumed i 13, 0766 gm 2t1.6�03 am It7.4sp ? am tIP5 Y3 gm t tt 1.3991 gm 2 ale 3Oo 120. 031-x. t-7_ ae99 y Datett'1me In: 7-t 0-IY/ t o:vy Dateirme Out w I Y / to4 iq r Oven p� Y Tem 10 'C Time in: _1zt33 Time Out: o Y Muffle Furnace —1' Temw. Y ro 'G Were the samples well mixed before analyzing? Yes�/Noy Was the temp of the drying oven in the proper operating range? Yes � No� If not what were the corrective actions? Was the temp of the Muftie Furnace In the proper operaL•ng range? Yes ✓No. if notwhat were the corrective actions? Samplers s're t I C� City of Sanford Big Buffalo WWTP Sludge Calculations 111 W1 pISH 113.0786 W2 WET 211.6303 W3 DRY 113.4593 W4 ASH 113.1683 VSR = 54.86063 0.388316 PERCENT VOLITILE SOLIDS 0.760387 W1 DISH 111.3991 W2 WET 209.3004 W3 DRY 120.0312 W4 ASH 117.2299 PERCENT SOLIpS S.S17145 PERCENT VOLITILE SOLIDS 0.324521 P>=RGENT VOLtT]LE SOLIpS REAUCTION 84.88063 Is it above ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Sanford WQ Permit Number: WQ0000543 Analytical (Alk Stabilization) Option/Alt, 9 WWTPName: Excee- Big Buffalo WWTP NPDESNumber: NCO024147 Minimum Geo. Mean Maximum Units dentes Monitoring Period: From 10/01/18 To 12/31/18 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. UA (time/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion Tf......i:..ohlo t...,itor.,"t:.," nArf"rrnAd trinvc A ..r Clace Rl rmmnlptp the fallowing monitoring data: Parameter Vector Att Allowable Leve] in Sludge Pathogen Density No. of Frequency Sample Analytical (Alk Stabilization) Option/Alt, 9 Option/Alt. 10 Excee- of Type Technique Minimum Geo. Mean Maximum Units dentes Analysis Fecal 2xlOto the 61" CFU <40300 <42000 <44100 CFU/g 0 4 x year Grab 9222D Coliform power per gram of total solids MPN/g WN 1000 WN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: Option/Alt. 1 ptiop/Alt. bench) Opfion/Alt. 2 (VS reduction) % (40-daybench)(30-day Option/Alt. 5 Option/Alt. 6. (14 -Day Aerobic) (Alk Stabilization) Option/Alt, 9 Option/Alt. 10 (Injection) (Incorporation) CERTIFICATION STATEMENT (please check the appropriate statement) O 3 Option/Alt. 7 (Drying —Stable) No vector att Option/Alt. 4 (Speo. 02 uptake) Option/Alt. 8 (Drying—Unstable) raction reduction alternatives were performed "I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15ANCAC 02T:1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15ANCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15ANCAC 02T.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please nate if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination hasbeen made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Scott Siletzkv WWTP Superintendent tn(>l0` �BO I!A (e(SeY-"tk� Preparer Name and Title (typ r print) LLand App�lier Name and Title (if applicable) (Type or print) C5 I A1 1.WDeE ani Signature of Preparer* Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and ISA NCAC 2T.1102 (26) Cameron Testing Services, Inco Laboratory Report Synagro Sanford WWTP Sample. Information M. Soya '. 10/01/18 ON RM Analyses and Results NC OENR #654 NC PHHS #37798 US 6PA #NCQ1918 181767 Yes M, Sims 10!01!18 181707 1 31w 9e G Fec, COIIJOmF$ <43300 CFWO 43300 10/02/18 ERP 9222@ -MF 2 <44100 cFuA2 44100 3 <40500 CFWO 40500 4 X40700 CFUk 40700 5 <40300 CFWm 403U0 6 <43300 CFWg 43390 7 <41700 CFWD 41700 Geomean <42000 181707 1 None cr. TS t /0) 2.31% 007 1p102118 ERP 2540 G •TS 2 2.27% 0.01 3 2.47% 001 4 2.46% 0.01 5 2.48% 0.01 6 2,31% 0.01 7 2.40% a01 Report Ravlew Odle «rfl / 219 S. SteeleSlr, 3xiilaad N4 27330 91ri-208-d240 cl�ris(;0gmcranReSting.c0m i VSR Grab Date: 10 � i 5� / $ Lab Tech's Initials: [z i Sample RAS (IN) Volume 100 MIs. Dish #0 Crucible Weight Crucible & Liquid Dried Burned (12.437` 2iz,4y7S 13.0 ►�� 3m 3m 3m 3 DIGESTER OUT 94 2(1.6'10? 122.6 q! $ 118. yGcy Date/Time In: (�-t1 "�� / f Z�� Drying Oven DatelTime Out: IDgI 1b / ))12 ,10+ Temp: /04 °C Time In: l0 1�-IY oCr 04 Muffle Furnace Time Out:►u-(6.rk . 2:23 Temp: tp o C v Were the samples well mixed before analyzing? Yes_ No_ Was the temp of the drying oven in the proper operating range? Yes No_ If not what were the corrective actions? Was the temp of the Muffle Furnace in the proper operating range? Yes_ No. If not what were the corrective actions? Samplers �Wr City of Sanford Big Buffalo WWTP Sludge Calculations IL' VSR = 39.88332 W1 DISH 112.7376 W2 WET 212.7475 W3 DRY 113.0127 W4 ASH 112.8870 0.275073 PERCENT VOLITILE SOLIDS 0.456925 OUT W1 DISH 111.3991 W2 WET 211.6707 W3 DRY 122.0418 W4 ASH 118.4669 PERCENT SOLIDS 10.61387 PERCENT VOLITILE SOLIDS 0.335902 PERCENT VOLITILE SOLIDS REDUCTION 39.88332 Is it above 38% 0 Agricultural Lime Application Log Year: 2018 Project: Sanford Field (state -county -site -field) Soil pH Lime Requirement (from soil analysis) I onsimcre Applied Date Applied n/a NC -CH -49-6 6.0 0.0 NC -CH -49-7 6.1 0.0 n/a NC -CH -49-8 6.2 0.0 n/a NC -CH -60-1 6.0 0.0 n/a NC -CH -60-3 6.1 0.0 n/a NC -CH -60-7 5.7 0.7 0.0 NC -CH -60-11 5.4 1.3 0.0 NC -CH -66-1 5.8 0.4 n/a NC -CH -66-3 5.9 0.0 n/a NC -CH -66-4 6.2 0.0 n/a NC -CH -66-6 6.0 0.0 n/a NC -CH -66-8 6.1 0.0 n/a NC -CH -66-11 6.2 0.0 n/a *Lime to be spread in first quarter 2019 SECTION 7 r N MO _W t O C UN o N Q a O N N o N z v N d EE� 0 O `cZ p Z Z y N a W N d 0 ' A� CZ N Z Z y 0 a W W N d 0 E� p CZ N Z Z v) N on N 00 7 x POP O Z m m Mo G1 O Co o O d M d M d M Z (n N 2 p z z o z o o. o Of `d Vo _ Q v v m a`S No Q M No Q f0 No C a N M C r N N m m m d `m `d O M O O N N N N N m m d K m .. 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