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WQ0001800_Residual Annual Report 2018_20190314
INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0001800 SUBMITTAL DATED: 2/26/2019 Project Contact Information Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Lisa Finnerty Email Address* Ifinnerty@synagro.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0001800 Permittee * Facility Name * Town of Yadkinville Town of Yadkinville Phone Number* 4434899086 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Eic.) Yadkinville NC 2018 Annual Report.pdf 7.51 MB upload only 1 PDF docurrent. NLltiple documents must be corrbined into one RDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/26/2019 435 Aill.iams Court, Suite 100 Baltimore, XM 21220 NvwW svizagro.com FEBRUARY 26, 2019 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2018 Annual Report for Permit No. WQ0001800 Dear NCDEQ: SYNAGRO Synagro is submitting one copy and one electronic copy of the above referenced report on behalf of the Town of Yadkinville, NC. If you have any questions or need additional information, please do not hesitate to contact Perry Williams at (336) 679-8732 or Erik Bruce at (336) 909-8627. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Perry Williams — Town of Yadkinville Erik Bruce, Synagro YOUR PARTNER FORA CLEANER, GREENERWORLD TOWN OF YADKIN MLLE, NC RESIDUALS LAND APPLICATION PROGRAM Permit No. W00001800 2018 ANNUAL REPORT Town of Yadkinvine, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analyses, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms &Metal Field Loading Summary Forms 4. TCLP Analyses 5. Pathogen ReductionNector Attraction Reduction 6. Soil pH &Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQPermit#: WO00o1800 County Yadkin Year 2018 t' Facility Name (as shown on permit) Town of Yadkinville W WTP & WTP NPDES No. NC0020338. NC0079260 \ Land Application Operator Svnaaro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO, skip Part A, and Part B and proceed to Part C, Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A— Residuals Application Summary: Total number of application fields in the permit: 14 Total number of fields utilized for land application during the year: 7 Total amount of dry tons applied during the year for all application sites: 56_50 Total number of acres utilized for land application during the year: 31.7 Part B —Annual Compliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediation. 11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on the permit were maintained during each application of residuals. Part C —Cert ification: "I certify, under penal ty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ] am aware that there are significant penalties for submitting false information, including the possibility of fines and hnprisontnent for knowing violations." y �/J / Peny Williams, Director of Public Works l/U-AL ab 1'/� Permittee Name and Title (type or prhit)ignature of PC nnie n Date Signature of Preparer* Date Signad'o1'La nd AppI�i r Date (if different from Permittee) (if different fro Permittee and Preparer) *Preparer is defined in 40 CFR Patt 503.9(r) and l5A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC YADKINVILLE, NC YADKINVILLE, NC WWTP LIQUID vzzr2o�s DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS June 2018 3135600.00 G 29.30 D 26.58 YEARLY TOTAL 313,600.00 G 29.30 D 26.58 YADKINVILLE, NC WTP LIQUID DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS March 2018 40,200.00 G 4.66 D 4.23 June 2018 79200.00 G 9.18 D 8.34 August 2018 72,000.00 G 8.35 D 7.57 December 2018 431200.00 G 5.01 D 4.54 YEARLY TOTAL 2341600.00 G 27.20 D 24.68 vzzr2o�s SECTION 2 E®. � co (D cu 2 d \�c cj 2 )&{ / \\a \ . 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N c6 = 0 �aooa R¢0mou Com] WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354 Page 1 of 4 Wa 7621 Whitepine Road, Richmond, VA 23237 � OI ■ ■�,.® Main 804-743-9401 °Fax 804-271-6446 � ANALYTICAL www.waypointanalyticaLcom Sample Summary Table Report Number: iS-073-0217 Client Project Description: Yadkinville WTP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 59185 Yadkinville WTP Solids 03/09/2018 08:30 03/14/2018 59185 Yadkinville WTP Solids 03/09/2018 08:30 03/14/2018 7471A WTN 59185 Yadkinville WTP Solids 03/09/2018 08:30 03/14/2018 6010C WTN WTN: Waypoint Analytical -TN, Memphis, TN, Certification: #1354 Page 1 of 4 m $ Z U Z .c - NF (D U = U N coo m coo coo coo coo coo m coo coo m v C o U U Q o o- o a? 0 0 o m m m m cn v� cn m o cn co 0 o M R W E d (D t0 d) cV N N N N N N m N iV O7 m N�— (q R R R N N N N N N N N N N N N N N N N N M m C7 u O O O O O O O O O O O O O O O O O N a p K 2 K K K K cG �- Y :5F 0 � � o J a Z u J Q 0 0 0 0 0 Lj o� m � •O J Q O �z Q W V- � N V N N G 46 Y N r m d N c+> r a U d W m mY i16 O 3 N w 0 E o z � Z to � N Z o E Q v No m ,2. ca m -o o a z z nom. in U in Q U N o c a v M N m m m m m m ro m m m m m m o d K Q N J F S H h� F° F2 I2 I—o I2 3 p- ^ •� O E O O M mm �n u N i _ y r OJ m N N N O T � � 0 c � ^ O r 0 0 N x J E m c �LLo O v N m v o U Ql W o s c s E E m � 3 � ,h 3 a � 3 c � 3 V 0 0 � m m N Z N Y � Q 3 N r° a n 7 �C m O 0 O O M 0 0 M O uri y r OJ m N N N O m IL o 0 O � ^ D r 0 0 N o J (D m (D J O v N m v o U Ql W o s c s E E m � z � z m N 0 0 N Y 3 V 0 0 � m m N Z N Y � Q 7 �C m O 0 O O M 0 0 M O uri � of OJ O v N J O m m o 0 O N N- D U (D N o J (D D) r J O O N m v o U Ql W o Z c m C� E m a � d m N 0 0 N o d V N mm � m m N Z N Y r° a N O O 0 O O M 0 0 M O uri � of OJ O v N J O O m o 0 O N N- D (D (D N � N (D D) O M O O b c0 v v aai Ql W oD OJ E v a � d m N 0 0 N w d V N N � � 0 J U U U U Q U❑ U 0 0 0 o M o o n uri uri r v N J O O O O V O 0 0 D (D (D (D ID r (D D) O 0 0 0 o M o o n uri uri v N N M Y N 0 O N V O N N N N O D N b c0 of W W Ql W oD OJ 7 0 0 0 0 0 0 0 0 V N N N N N N N N 0 0 0 o M o 0 N N M Y 0 0 0 0 0 0 o M o 0 N N M 0 0 0 0 c O O D kF, /§ cn Ir §) ./ § L z \ �\ � e k £ §§ kF, /§ cn Ir §) ./ § 4 \ \. \\ }{ q( }j 2/ \\ §\ co E5 'a co z \ � e £ � .»a L R ; 4 \ \. \\ }{ q( }j 2/ \\ §\ co E5 'a co z � e £ � .»a L R ; �- .- ) CL « a � a « � z z k \ U)ri $ Ll Sodium Absorption Ratio Calculation (SAR) Product Code Product Name SamPle Date Report Range Ratio 2056-02-WPL-NC YADKINVILLE, NC WTP LIQUID 3/9/2018 111/2018-1213112018 0.2538 Na mg/I = (Na mg/kg x % Solids) + 100 = (322 x 2.7800) _ 100 = 8.9516 Ca mg/I = (Ca mg/kg x % Solids) - 100 = (1980 x 2.7800) + 100 = 55.044 Mg mg/I = (mg mg/kg x % Solids) = 100 = (842 x 2.7800) . 100 = 23.4076 Na meq = Na mg/I + Molec.Wgt.Na = 8.9516 = 23 = 0.3692 Ca meq = Ca mg/I + Molec.Wgt.Ca = 55.044 - 20 = 2.7522 Mg meq = Mg mg/I + Malec.Wgt.Mg = 23.4076 = 12 = 1.95063 SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.3892 + SgrRoot[0.5(2.7522+1.95063)] = 0.25381 Printed: 1/23/2019 Page 1 12:32 SECTION 3 a m M a a w a A N m M a w N w v w cin rn z N AJ N o b � a x zaz w A m U N z U N v m y A 4 �p N o aq A* � � P4 A � A o a.� rs . y 6 U aN \ .9aax� b�Ya Q rnUq � b � � "o a� Q�wQ� N V e o N m M w N rn z N x w A m U N U N v m y 4 � A o U m M ANN CJAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkinville, NC Total Dry Tons Applied (Annual): 6.95 #: WQ0001800 Cation Exchange Capacity (non 503 only): 10 �=rmit 12 Solids 2.24 � Billy Griffin Owner: Billy Griffin Predominant Soil Series: Poplar Forest _aerator: Acres Used: 4.1 Acres Permitted: 4.2 Site #: NC YK 00008 Field #: YK 00008 0001 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date � 1/11/18 2 3 4 5 6 7 9 9 10 11 12 Solids 2.24 8 9 10 11 12 Arsenic 3.23 Cadmium 2 Copper 1060 Chromi 49.4 � Lead 25.2 Mercury 0.4 Molyb- denum 5 0.000 0.000 0.000 0.000 0.000 Nickel 41 0.000 0.000 0.000 0.000 0.000 0.011 Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 2260 0.000 0.000 0.000 0.000 0.000 0.007 Total Phos- Torus 20700 0.000 0.000 0.000 0.000 0.000 �_ .rnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App. � Event 1.70 Arsenic 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 3.593 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.593 Chromium 0.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.167 Lead 0.085 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.085 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 denum Nickel 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 Selenium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Zinc 7.661 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.661 Total Phos- 70.173 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 70.173 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and �risonment foryk�nowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) C � W o V q w w a µw�yk b0 .a Gi PJ N N N No N v q o 0 �oK p 'r'vav v sa o 0 a z�� b H z ..� Q W a Ly Ly N o q p o J < ry` P4 O O o ' O l? N 6 W b V N d A y y W g Y e rv� N N On 0.� qow Ln V o dkj .g. a.Wx o F 3 y 04 z w o U o y Fa Q Q `� S RWO �^ �HW6 0 •• r. a q m a'S C W .� o C N F o R 'O ., a o 4 Q U v W N il Z .? Wiz° m E a- z W'6a W H m w opo '1" -21 �pp II 6 0 W ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkinville, NC Total Dry Tons Applied (Annual): 5.21 T'ermit #: W00001800 Cation Exchange Capacity (non 503 only): 10 r aerator: Billy Griffin Owner: Billy Griffin Predominant Soil Series: 2.24 Poplar Forest Acres Used: 2.1 Acres Permitted: 2.1 Site #: NC YK 00008 Field #: 10 YK 00008 0003 11 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample Or Com- posite Date 1 1/11/18 2 3 4 5 6 7 8 9 10 11 12 Solids 2.24 lbs/acre): 9 10 11 12 Arsenic 3.23 Cadmium 2 y Copper 1060 Chromim 49.4 � Lead 25.2 Mercury 0.4 w Molyb- denum 5 Nickel 41 �� Selenium 5 0.000 0.000 0.000 0.000 0.000' Zinc 2260 0.000 0.000 0.000 0.000 0.000 0.016 Total Phos- porus 20700 0.000 0.000 0.000 0.000 0.000 Total 1 2 3 4 5 ennal Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ � App w Event 2.48 �� Arsenic 0.016 0.000 0.000 0.000 0.000 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 5.262 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 5.262 Chromi 0.245 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.245 Lead 0.125 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.125 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 denum Nickel 0.204 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.204 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Zinc 11.219 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 11.219 Total Phos- 102.755 0.000 0.000 0.000 D.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 102.755 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and �risonment for knowing violations". Signature of L plier l Dat DENR FORM MFLSF (12/2006) W7 a 'a e � H F W N � N y P U U z Q W7 e � H F W N � N y P U U z M v O VJ N rUy W w � o U U W v zQ v W U b w W u7 O h W7 � H F W N � N y U U z M v N rUy W w U W v zQ v W U b W a N U 7 p N N o z�z w a d m z 0 0 a d � o 7 q'� v V o QA 0 � m QHa.6 o 0 � � a N N N fV ti Ci P. M vNi N N 00 6 C5 o N o NN Q� W N � N y z M v N x v W U v U o d ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkinville, NC Total Dry Tons Applied (Annual): 7.08 Dermit #: W00001800 Cation Exchange Capacity (non 503 only): 10 '� � erator: Billy Griffin Owner: Billy Griffm Predominant Soil Series: 2.24 Poplar Forest Acres Used: 4.2 Acres Permitted: 4.2 Site #: NC YK 00008 Field #: YK 00008 0004 i ,tnual Heavy Metal Field Loadings (Calculated in lbs/acre): Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 1/11/18 2 3/9/18 3 3/9/18 4 5 6 7 8 9 10 11 12 Solids 2.24 2.78 2.78 9 10 11 12 Arsenic 3.23 1 1 Cadmium 2 4.8 4.8 y Copper 1060 63.3 63.3 Chromi 49.4 21 21 � Lead 25.2 38.8 38.8 Mercury 0.4 0.0846 0.0846 Molyb- denum 5 2.34 2.34 0.89 Nickel 41 12.4 12.4 �� Selenium 5 0.5 0.5 0.002 0.000 0.000 0.000 Zinc 2260 196 196 0.000 0.000 0.000 0.000 0.006 Total Phos- horns 20700 2670 2670 0.009 0.000 0.000 0.000 Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ � App. Event 0.49 0.30 0.89 �� Arsenic 0.003 0.001 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Cadmium 0.002 0.003 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 1.047 0.038 0.113 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.198 Chromi 0.049 0.013 0.038 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099 Lead 0.025 0.023 0.069 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.005 0.001 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 denum Nickel 0.041 0.007 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.070 Selenium 0.005 0.000 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Zinc 2.233 0.117 0.350 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.700 Total Phos- 20.452 1.591 4.774 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 26.817 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and �risonment for knowing violations". C\� Signature of Lan pplier DENR FORM MFLSF (12/2006) I f-9 0 N z a a a �Ww1 w�1 U Q `Y cf rt}: W W U A W f-9 0 N z a �Ww1 w�1 U U `Y cf rt}: W W U W W a a z a a w N N 0 0 � N Y v z z�� N N Np � q �z p .. y a a U � q m qs � � 0 0 �« Na :9 Q Q iYiUq� �h Q Fw600 N N e N N ti b � O C7 C7 U H o N b b N < Q f-9 0 N z a i M N IY m k N `Y cf rt}: N a 0 0 N v N N Np p y U i M N IY m k ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkinville, NC Total Dry Tons Applied (Annual): 1.74 � "�rmit #: W00001800 Cation Exchange Capacity (non 503 only): ierator: Billy Crriffin Owner: Larry Styers Predominant Soil Series: Clifford Acres Used: 2.1 Acres Permitted: 2.1 Site #: NC Yl� 00008 Field #: YK 00008 0006A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample ox Com- posite Date 1 1/11/18 2 3 4 5 6 7 8 9 10 11 12 Solids 2.24 6 9 10 11 12 Arsenic 3.23 Cadmium 2 H Copper 1060 Chromi 49.4 ° Lead 25.2 Mercury 0.4 y Molyb- demm� 5 Nickel 41 �� Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 2260 0.000 0.000 0.000 0.000 0.000 0.005 Total Phos- 4orus 20700 O.00b 0.000 0.000 0.000 0.000 v. ,mual Heavy Metal FY'eld Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 6 9 10 11 12 H DT/Ac./ ° App. y Event 0.83 �� Arsenic 0.005 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.005 Cadlnium 0.003 O.00b 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 1.755 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.755 Chromi 0.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.082 Lead 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 denwn Nickel 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.068 Selenium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Zinc 3.743 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.743 Total Phos- 34.279 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 34.279 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 7 am aware that there are significant penalties for submitting false information, including the possibility of fines and �risonment for knowing violations". Signature of Lan pplier ID e l DENR FORM MFLSF (12/2006) O T�2 a O U q W Q w wLiz o oo,a w �J= A O T�2 O U W U w wLiz o oo,a w �J= N =o N O Q V W b w w O C F T�2 O W U w wLiz w �J= N N V b & � N G z6 O G N � O M �z N a 0 x a N m a 6 r4 U q 0 o � � N U d N U o 5 Q a awwx a A C O7 q Q v�UQ� y a o W'" N � N � � Q U o H c3 Q� C F z a T�2 wLiz O N N V � O N z6 O N O M N a 0 x N m a 6 r4 U � N U d N U N Q a A C O7 q z a ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: rmit #: �.erator: Acres Used: �� _ _.mual Heavy Metal Field Loadings (Calculated in lbs/acre): Yadkinville, NC Total Dry Tons Applied (Annual): 2.90 WQ0001800 Cation Exchange Capacity {non 503 only): Billy Griffin Owner: Billy Griffin Predominant Soil Series: Clifford Acres Permitted: Site #: NC YK 00008 Field #: YK 00008 0006E Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 1/11/18 2 3 4 5 6 7 8 9 10 11 12 Solids 2.24 8 9 10 11 12 Arsenic 3.23 Cadmium 2 y Copper 1060 Chromi 49.4 � Lead 25.2 Mercury 0.4 Molyb- denum 5 Nickel 41 Selenium 5 Zinc 2260 Total Phos- 'torus 20700 0.000 0.000 0.000 0.000 0.000 Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ � APP• Event 2.90 Arsenic 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Caduuum 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Copper 6.140 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 6.140 Chromi 0.286 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.286 Lead 0.146 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.146 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 denum Nickel 0.237 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.237 Selenium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 13.090 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 13.090 Total Phos- 119.894 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 119.894 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and prisonment for knowing violations". Signahtre of Land pie^ Z �� � Date DENR FORM MFLSF (12/2006) I H 'a T�l a Q M o ra � A w H T�l a � M o w U w v z N N W ,Aj N a z �b� d x C w �z N U N Ci 0 a C6y��o A O c O � Q N �+ dwwx .r Q m U � d o caFwQ �N N U � 6 t5 ° so F �3 � H d T�l M z N N z x w N U N Ci a A O c ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: �rmit #: \ ,erator: Acres Used: Yadkinville, NC WQ0001800 Jack Adams Owner: Total Dry Tons Applied (Annual): 10.42 Cation Exchange Capacity (non 503 only): Jack Adams Predominant 5oil5eries: Clifford 6.7 Acres Permitted: 7.5 Site #: NC YIC 00009 Field #: YK 00009 0001 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 1/11/18 2 3 4 5 6 7 6 9 10 11 12 %Solids 2.24 8 9 10 11 12 Arsenic 3.23 Cadmium 2 y Copper 1060 Chromi 49.4 � Lead 25.2 Mercury 0.4 w Molyb- denum 5 Nickel 41 �� Selenium 5 0.000 0.000 0.000 0.000 0.000 Zinc 2260 0.000 0.000 0.000 0.000 0.000 0.010 Total Phos- porus 20700 0.000 0.000 0.000 0.000 0.000 _nnual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 y DT/Ac./ � App. w Event 1.56 �� Arsenic 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 3.299 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.299 Chromi 0.154 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.154 Lead 0.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.078 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 denum Nickel 0.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128 Selenium 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.016 Zinc 7.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 7.033 Total Phos- 64.418 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 64.418 porus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. T am aware thatthere are significant penalties for submitting false information, including the possibility of fines and prisonment for knowing violations". Signature of pplier DENR FORM MFLSF (12/2006) )\ \ \ \ \ \ \ ) \r8 ` t2: 25 G Q%/ \\ ( ( ( \ ( \ \w O/ \\ # \/«w9aZsaa; N ra U a z�z N C Qy �z 9 E q Q � ra U z�z N C �z E q � C* N LL .� �aax N a� 0 e R F Fi 00 c7 E a E c3 o H 0 Q N W N 0 z Fi a �ry U N V b o U �r 6 0 m ^ A � O E � U ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Yadkinville, NC Total Dry Tons Applied (Anneal): 22.19 r �rmit #: l aerator: Acres Used: WQ0001800 Cation Exchange Capacity (non 503 only): Town of Yadkinville Owner: Town of Yadkinville Predominant Soil Series: Clifford 11.5 Acres Permitted: 11.5 Site #: NC YK 00029 Field #: YK 00029 0001 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, %Solids use Raw Percent #): Sample or Com- posite Date 1 3/9/18 2 3 4 5 6 7 6 9 10 11 12 Solids 2.78 in lbs/acre): 9 10 11 12 Arsenic 1 Cadmium 4.8 Copper 63.3 Chromi 21 Lead 38.8 Mercury 0.0846 w Molyb- denum 2.34 Nickel 12.4 Selenium 0.5 0.000 0.000 0.000 0.000 0.000 Zinc 196 0.000 0.000 0.000 0.000 0.000 0.004 Total Phos- porus 2670 0.000 0.000 0.000 0.000 0.000 Total 1 2 3 4 5 � anual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ App w Event 1.93 Arsenic 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Cadmium 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Copper 0.244 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.244 Chromi 0.081 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.081 Lead 0.150 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.150 Mercury 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Molyb- 0.009 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.009 denum Nickel 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Selenium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Zinc 0.756 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.756 Total Phos- 10.296 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 10.296 porus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. i am aware that there are significant penalties for submitting false information, including the possibility of fines and 2risonment for knowing violations". J � �1 SignatureofLandApplier (Date DENR FORM MFLSF (12/2006) ���C�7TC! ' Summit Environmental Technologies,Inc. U3310 Win St. PNVIRONIAENTALT€CHNOLGG1E5, ING Cuyahoga Falls, Ohio 44223 Arraiytical Loborgiorlea TEL: (330) 253-8211 FAX. (330) 253-4489 Website: hap.'Mioviv.settekcam February 03, 2017 Erik Bruce Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336)998-7150 FAX: (336) 998-8450 RE: Yadkinville Dear Erik Bruce: Order No.: 17010155 Summit Environmental Technologies, Inc. received 2 samples) on 1/5/2017 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted n the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, t Jennifer Woolf Project Man ager 3310 Win St. Cuyahoga Falls, Ohio 44223 Alabama 41600, Arkansas 88-0735, California 07256CA, Colomdn, Co®eclicmt PH -0105, Delawaze, Florida NELAC E87688, Georgia E67688, Idaho OH00923, Illinois 200061, Indiana C -OH -13, Kansas E-10347, Kentucky (Underg<omd Stooge Tank) 3, Kentuclry 90146, Louisiana 04061, Maryland 339, Massachusetts M-OPH923, Minnesota 409711, New Hempsh¢e 2996, New Sersey OH006, New York 11777, North Cazolina 39705 and 631, North Dakota R-201, Ohio Drinking Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Region 8 8TMS-L, USDA/APHIS P330-11-00244, Utah OH009232011-1, Vermont VT -87688, Virginia 00440 and 1581, Washington C891, West Virgjnie 9957C Page 1 of 48 Page 1 of 42 Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. Case Narrative RMPIONMENTALT€CH NOLaCuEs, WQ- Cuyahoga Falls, Ohio 44223 WO#: 17010155 Analytical Lflhara3arles TEL: (330) 253-8211 FAX: (330) 253-4489 Website: hM.11w1vwsettekcom Date: 2/3/2017 CLIENT: Synagro Project Yadkinville WorkOrder Narrative: 17010155: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples This report is believed to meet all P+1, are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. noted below. Original Page 2 of 42 Page 2 of 48 e requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Original Page 2 of 42 Page 2 of 48 ilt Summit Enviromeatarzeennorina Qualifiers and Acronyms 331010Win 5 summ WWRONMENTAL TECnN4Lacics, tree Cuyahoga. Falls, Ohio 442< W04: 17010155 .hrra:ytisat Lnhorotarlet TEL: (330) 253-8211 FAX. (330) 253-445 Date: 2/3/2017 Website: http..11aww.settek.co These commonly used Qualifiers and Acronyms may or may not be present in this report. Qualifiers U The compound was analyzed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit, H The hold time for sample preparation and/or analysiswas exceeded. D The result is reported from a dilution. F The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. LCS The result exceeds the Regulatory Limit or Maximum Contamination Limit. In Manual integration was used to determine the area response. N The result is presumptive based on aMass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. .X The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+), R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for RF additional information Acronyms ND This list of Quali Not Detected RL Reporting Limit QC Quality Connol MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MinCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RF Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor fiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 42 Page 3 of 48 MSUMMINt Summit Environmental Technologies,lnc. workorder 3310 Win St. FffVRONIA€ NTAL TECHE40 LOVIES, INC Cuyahoga Falls, Ohio 44223 Sample Summary Arwdytical Lahoraiorhes TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 17010155 Website: http.lAvivw.settek.com 03-Feb-17 CLIENT: Synagro Project: Yall1mville Lab SampleID Client Sample lD Tag No Date Collected Date Received Matrix 17010155-001 Yadkinville WNTP 1/3/2017 1.00:00 PM 1/5/2017 9:45:00 AM Sludge 17010155-002 Yadkinville WTP 1/3/2017 2:00:00 PM 1/5/2017 9:45:00 AM Sludge Page 4 of 48 Page 4 of 42 AI 0 0 65n o O � m r ti N N Ri CP CD CP Z6 ZB a HLIE a w A q x U 6 y a n U HLIE w A q x U 6 HLIE 6 SUMMITsummitEnvironmental Teenaoro�tes, Inc.ffJ 3310 Win St. Analytical Report OYVIAONMENTflL T€Z=rIPdBLaGIeS, 111q. Cuyahoga Falls, Ohio 44223 (consolidated) Arudy.tical Ladoraiaries TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 17010155 Website: htip.://www.settek.com Date Reported: 2/3/2017 CLIENT: Synagro Collection Date: 1/3/2017 1:00:00 PM Project: Yadkinville Lab ID: 17010155-001 Matrix: SLUDGE Client Sample 11) YadkinvilleWWTP Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ALJ TCLP MERCURY ANALYSIS (1311/7470) TCLP Mercury ND 0.00200 mg/L 1 1/6/20174:31:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW6010C SW3010A Analyst: VVK TCLP METALS ANALYSIS (6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/6/2017 3:55:11 PM TCLP Barium(Ba) ND 5.00 mg/L 1 1/6/20173:55:11 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/6/2017 3:55:11 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 1/6120173:55:11 PM TCLP Lead(Pb) ND 0.500 mg/L 1 1/6/20173:55:11 PM TCLP Selenium(Se) ND 0.500 mg/L 1 1/6/20173:55:11 PM TCLP Silver(Ag) ND 0.500 mg/L 1 1/6/2017 3:55:11 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270C SW3510C Analyst: MSM SVOC 8270 TCLP BNA LIST 1,4-Dichlorobenzene ND 0.0800 mg/L 2 1/9/2017 11:47:00 PM 2,4,5-Trichlorophenol ND 0.200 mg/L 2 1/9/2017 11:47:00 PM 2,4,6-Trichlorophenol ND 0.200 mg/L 2 1/9/201711:47:00 PM 2,4-Dinitrotoluene ND 0.100 mg/L 2 1/9/2017 11:47:00 PM Cresols, Total ND 4.00 mg/L 2 1/91201711:47:00 PM Hexachloro-1,3-butadiene ND 0.100 mg/L 2 1/9/201711:47:00 PM Hexachlorobenzene ND 0.100 mg/L 2 119/201711:47:00 PM Hexachloroethane ND 0.0800 mg/L 2 1/9/2017 11:47:00 PM Nitrobenzene ND 0.0800 mg/L 2 1/9/201711:47:00 PM Pentachlorophenol ND 0.200 mg/L 2 1/9/201711:47:00 PM Pyridine ND 0.200 mg/L 2 1/9/2017 11:47:00 PM Surr. 2-Fluorophenol 51.4 10-109 %Rec 2 1/9/2017 11:47:00 PM Surr: Phenol-d6 53.9 10-109 %Rec 2 1/9/2017 11:47:00 PM Surr. Nitrobenzene-d5 59.5 19-120 %Rec 2 1/9/2017 11:47:00 PM Surr: 2,4,6-Tribromophenol 53.8 10-VO %Rec 2 1/9/2017 11:47:00 PM Surr: 2-Fluorobiphenyl 65.1 22 - 117 %Rec 2 1/9/2017 11:47:00 PM Surr: p-TerphenylA14 84.1 34-116 %Rec 2 1/9/2017 11:47:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081A SW3610C Analyst: JBN SVOC SW-846:8081-TCLP PESTICIDES Qa811t1f:r5: H Holdmn Mmes forprepmation or analysis exceeded M Maausllntegrafion used to tle[emane area response IJD Nor retested a[IM1e Repa,M1ng Limit PL Permit Limi[ R APD oatside accepted rewvery limits RL Reportmn Detection Limit W Sample ramaiaer temperatweis outoflimittespeciGed attesup a Original Page 6 of 42 Page 6 of 48 c. RINUMMly svmmitEnvirrnmentalTechnologtes,ln 3310 Win St. Ana lytical Report Fid91EONMENTALTECHNOLOGIES, ING- Cuyahoga Falls, Ohio 44223 (consolidated) Arialyttral Labaratudes TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 17010155 Website: ht4n.11www settelccom Date Reported: 2/3/2017 CLIENT: Synagro Collection Date: 1/3/2017 1:00:00 PM Project: Yadkinville Lab ID: 17010155-001 Matrix: SLUDGE Client Sample ID Yadkinville W WTP Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081A SW3510C Analyst: JBN SVOC SW-846: 8081-TCLP PESTICIDES Chlordane, total ND 0.0100 mg/L 1 1/9/2017 8:37:00 PM Toxaphene ND 0.0200 mg/L 1 1/9/20178:37:00 PM Endrin ND 0.00100 mg/L 1 1/9/20178:37:00 PM gamma-BHC ND 0.00100 mg/L 1 1/9/2017 8:37:00 PM Heptachlor ND 0.00100 mg/L 1 1/9/20178:37:00 PM Heptachlor epoxide ND 0.00100 mg/L 1 1/9/2017 8:37:00 PM Methoxychlor ND 0.00100 mg/L 1 1/9/2017 8:37:00 PM Sort: TCMX 72.3 10-119 %Rec 1 1/9/2017 8:37:00 PM Surr: DCB 55.9 10-119 %Rec 1 1/9/2017 8:37:00 PM �. TCLP HERBICIDES ANALYSIS (SW846 131118151) LSW8151A SW8151A Analyst: JBN SVOC SW-846: 8151 HERBICIDES-TCLP 234-D ND 1.00 mg/L 1 1/18/20172:19:00 AM 2,435-TP ND 0.500 mg/L 1 1/18/2017 2:19:00 AM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8260B Analyst: MES VOC BY GCIMS (8260)-TCLP 1,1-Dichloroethene ND 0.100 mg/L 1 1/6/20176:19:00 PM 1,2-Dichloroethane ND 0.100 mg/L 1 1/612017 6:19:00 PM MEK ND 2.00 mg/L 1 1/6/20176:19:00 PM Benzene ND 0.100 mg/L 1 1/6/20176:19:00 PM Carbon tetrachloride ND 0.100 mg/L 1 1/6/2017 6:19:00 PM Chlorobenzene ND 0.100 mg/L 1 1/6/20176:19:00 PM Chloroform ND 0.100 mg/L 1 1/6/2017 6:19:00 PM Tetrachloroethene ND 0.100 mg/L 1 1/6/2017 6:19:00 PM Trichloroethene ND 0.100 mg/L 1 1/6/20176:19:00 PM Vinyl chloride ND 0.200 mg/L 1 1/6/2017 6:19:00 PM Sort: 4-BromoOuorobenzene 97.9 70-130 %Rec 1 1/6/2017 6:19:00 PM Surr: Dibromo0uoromethane 101 70-130 %Rec 1 1/6/2017 6:19:00 PM Sort, Toluene-d8 98.8 70-130 %Rec 1 1/6/2017 6:19:00 PM RCI SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2) Cyanide, Reactive ND 0.500 mg/Kg 1 1/6120172:48:00 PM Qualifiers: H llol"gbmesforprepaationormdysis celled M Mminellntegmfion usedto de[emune arearesponsa /' ND No[De[ected at the Reporting Limi[ PL Permit Limi[ A AYD outside eccepfed recovery limits RL Reportingramaioo Liadt W Sample confsinarterrem[ure is out oflimit as specified at cascade Original Page 7 of 42 Page 7 of 48 SUMMIT Summit Environmental Technologies, Inc. 3310 Win St. C A Analytical Report F.KVIRONMENTAL TECHNOLociEs,]INC- Cuyahoga Falls, Ohio 44223 (consolidated) hnatytical tahoralorfes TEL: (330) 253-8211 FAX: (330) 253-4489 WD#: 17010155 Website: htm.//vivtvsettekcom Date Reported: 2/3/2017 CLIENT: Synagro Collection Date: 1/3/2017 1:00:00 PM Project: Yadkinville Lab ED: 17010155-001 Matrix: SLUDGE Client Sample ID Yadkinville W WTP Analyses - Result PQL Qual its DF Date Analyzed IGNITABILITY OF SOLIDS (SW -846:1030) SW1030 Analyst: RMT Ignitability Non-flammable. 1 2/1/2017 10:15:00 AM RCI SW9045D Analyst: DHC PH (SW9045D) pH 7.46 s.u.@19.9C 1 1/9/20174:53:00 PM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034) Sulfide, Reactive ND 25.0 mg/Kg 1 1/6/2017 2:48:00 PM Qaal(IICC9: H Holding rimes forpreparelion or snalysa exceeded M Manuel lnregranon asedto detemune area cesponsa ND Nol Deterred at fha Reporting Limit PL Permit Limit R RPD outside accepted recowrylimik RL Aeportiag Detection Limit W Sample mntsiner temperature is our of limit as specified at notmde Original Page 8 of 42 SUMMITSummit Environmental Technologies, Inc. 3310 Whn St. Analytical Report ENVIRONMENTAL TECH NOL061ES,INC',-Cuyahoga Falls, Ohio 44223 (consolidated) d) Labnysturles TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 17010155 Website: httn lAvrvw.settekcom. Date Reported: 2/3/2017 CLIENT: Synagro Collection Date: 1/3/2017 2:00:00 PM Project: Yadkinville Lab ID: 17010155-002 Matrix: SLUDGE Client Sample ID Yadkinville WTP Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: ALJ TCLP MERCURY ANALYSIS (131117470) TCLP Mercury ND 0.00200 mg1L 1 1/6/2017 4:34:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW6010C SW3010A Analyst: VVK TCLP METALS ANALYSIS (6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/6/2017 3:55:11 PM TCLP Barium(Ba) ND 5.00 mg/L 1 1/6/20173:55:11 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/6/20173:55:11 PM TCLP Chromium(Cr) ND 0.200 mg/L 1 1/6/20173:55:11 PM TCLP Lead(Pb) ND 0.500 mg/L 1 1/6/20173:55:11 PM TCLP Selenium(Se) ND 0.500 mg/L 1 116/20173:55:11 PM TCLP Silver(Ag) ND 0.500 mg/L 1 116/2017 3:55:11 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270C SW351OC Analyst: MSM SVOC 8270 TCLP BNA LIST 1,4-Dichlorobenzene ND 0.0800 mg/L 2 1/10/201712:17:00 AM 2,4,5-Trichlorophenol ND 0.200 mg/L 2 1/10/2017 12:17:00 AM 2,4,6-Trichlorophenol ND 0.200 mglL 2 1/101201712:17:00 AM 2,4-Dinitrotoluene ND 0.100 mg/L 2 1/10/201712:17:00 AM Cresols, Total ND 4.00 mg/L 2 1/10/2017 12:17:00 AM Hexachloro-1,3-butadiene ND 0.100 mg1L 2 1/10/201712:17:00 AM Hexachlorobenzene ND 0.100 mg/L 2 1/10/201712:17:00 AM Hexachloroethane ND 0.0800 mg/L 2 1/10/201712:17:00 AM Nitrobenzene ND 0.0800 mg/L2 1/10/201712:17:00 AM Pentachlorophenol ND 0.200 mg/L 2 1/10/201712:17:00 AM Pyridine ND 0.200 mg/L 2 1/10/201712:17:00 AM Surf: 2-Fluorophenol 37.5 10-109 %Rec 2 1/10/201712:17:00 AM Surr: Phenol-d6 48.4 10-109 %Rec 2 1/10/2017 12:17:00 AM Surr: Nitrobenzene-d5 68.0 19-120 %Rec 2 1/10/2017 12:17:00 AM Surr: 2,4,6-Tribromophenol 42.1 10-120 %Rec 2 1/1012017 12:17:00 AM Surr: 2-Fluoroti phenyl 72.8 22-117 %Rec 2 1/10/2017 12:17:00 AM Surr. p-Terphenyl-d14 104 34-116 %Rec 2 1/10/201712:17:00 AM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081A SW351OC Analyst: JBN SVOC SW-846: 8081-TCLP PESTICIDES Qualifiers: H Holding times Corpreparatian or analysis exceeded M Manual lntegredonused to deteemme arearespoue ND Not Detected at o Reporting Limit PL Perot Limit I- R RPD outside accepted recovery limits ItL Reposing Detection Limit W Sample tontainer outpemtura ta out ofunuit as specified at tutmde Original Page 9 of 42 Page 9 of 48 U I•r summa nv,ronme,ttarTe hnorWSt. Analytical Report 331010Win St. r1sWIR4NMENTALTECHNOLnclES, ING- Cuyahoga Falls, Ohio 44223 (consolidated) ArrafyBr-sl t-abara?rries TEL: (330) 253-8211 FAX: (330) 253-4489 Wo#: 17010155 Website: htto.lAvwdv sette%com Date Reported: 2/3/2017 CLIENT: Synagm Collection Date: 1/3/2017 2:00:00 PM Project: Yadldriville Lab ID: 17010155-002 Matrix: SLUDGE Client Sample ID Yadkinville WTP Analyses Result PQL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081A SW3510C Analyst: JBN SVOC SW -846: 8081-TCLP PESTICIDES Chlordane, total ND 0.0100 mg/L 1 1/9/2017 9:04:00 PM Toxaphene ND U200 mg/L 1 1/9/2017 9:04:00 PM Endrin ND 0.00100 mg/L 1 1/9/2017 9:04:00 PM gamma -BHC ND 0.00100 mg/L 1 1/9120179:04:00 PM Heptachlor ND 0.00100 mg/L 1 1/9/2017 9:04:00 PM Heptachlor epoxide ND 0.00100 mg/L 1 1/9/20179:04:00 PM Methoxychlor ND 0.00100 mg/L 1 1/9/20179:04:00 PM Surr. TCMX 89.9 10-119 %Rec 1 1/9/2017 9:04:00 PM Surr: DCB 81.3 10-119 %Rec 1 1/9/2017 9:04:00 PM TCLP HERBICIDES ANALYSIS (SW846 1311/8151) SW8151A SW8151A Analyst: JBN SVOC SW -846: 8151 HERBICIDES-TCLP 2,4-D ND 1.00 mg/l. 1 1/18/2017 2:48:00 AM 214,5 -TP ND 0.500 mg/L 1 1/18/2017 2:48:00 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW82608 Analyst: MES - VOC BY GC/MS (8260)-TCLP 1,1-Dichloroetheree ND 0.100 mg/L 1 1/6/2017 6:53:00 PM 1,2-Dichloroethane ND 0.100 mg/L 1 1/6/2017 6:53:00 PM MEK ND 2.00 mg/L 1 1/6/20176:53:00 PM Benzene ND 0.100 mg/L 1 1/6/2017 6:53:00 PM Carbon tetrachloride ND 0.100 mg/L 1 1/6/2017 6:53:00 PM Chlorobenzene ND 0.100 mg/L 1 1/6/20176:53:00 PM Chloroform ND 0.100 mg/L 1 1/6/2017 6:53:00 PM Tetrachloroethene ND 0.100 mg/L. 1 1/6/2017 6:53:00 PM Trichloroethene ND 0.100 mg/L 1 1/6/2017 6:53:00 PM Vinyl chloride ND 0.200 mg/L 1 1/6/2017 6:53:00 PM Surr: 4-Bromofluorobenzene 96.9 70-130 %Ree 1 1/6/2017 6:53:00 PM Surr: Dibromofluoromethane 103 70-130 %Rec 1 1/6/20176:53:00 PM Surr: Toluene -d8 104 70-130 %Ree 1 1/612017 6:53:00 PM RCI SW9014 - Analyst: MS REACTIVE CYANIDE (9014/7.3.3.2) Cyanide, Reactive ND 0.500 mg/Kg 1 1/10/2017 12:17:00 PM Qualifiers: H Holding times for preparation or analysis exceeded M Manual lndegmdon used to determine am, response ND Not Detected at Ne Reporting Limit PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit W Sample wnteinertempenture is out of limit as specified at tesicnde Original Page 10 of 42 Page 10 of 48 summlySummit Environmental Technolowin St. Analytical Report 33100 Win St. Hi GNVIRONIdeNYALYfCHN4L¢GiE ,frtE- - Cuyahoga Falls, Ohio 44223 (consolidated) Analytical Lahoralodes TEL.: (330) 253-8211 FAX: (330) 253-4489 WO#: 17010155 Website: http://wiviv settekcom Date Reported: 2/3/2017 CLIENT: Synagro Collection Date: 1/3/2017 2:00:00 PM Project: Yadkinville Lab ID: 17010155-002 Matrix: SLUDGE Client Sample ID Yadkinville WTP Analyses Result PQL Qual Units DF Date Analyzed IGNITABILITY OF SOLIDS (SW -846:1030) Pemut Limit SWI 030 � R Analyst: RMT Ignitability Non-flammable. 1 2/1/2017 10:15:00 AM RCI _ W SW9045D Analyst: DHC PH (SW9045D) Original pH 6.35 s.u.@19.3C 1 1/9/2017 4:56:00 PM RCI SW9034 Analyst: MS REACTIVE SULFIDE (9034) Sulfide, Reactive ND 25.0 mg/Kg 1 1/10/2017 12:17:00 PM Qualifie[S: H Flolding times forpreparetion or analysis ecceeded M Manuallntegmrion usedto detetmma areatesponse � ND Not Detectedazd�e Repotting Limit PL Pemut Limit � R RPD ootsida accepted tewvaryllnufs RL Reporting Defactiou Limit _ W Sample confainerietnpetafweu out of limit as specified at fesfcode Original Page 11 of 42 Page 11 of 48 le' Lqa � — d m y E O (moi � U Qi Lqa � — O y E O (moi � N K N � E m J � N ❑ c � a o m Y E m a � m in E a ❑ a J O _ z z o F z = di N Or m � Lqa � — O y E O O � N K N � ❑ m a � N � c � N o m Y E m a � m in E a ❑ J J O _ U c _ F z = di N m_ p � ❑ ❑ E o Z U `9 ~ a C J F- J Q U' K 0) Lqa � — O y E O O � N K N � > m 46 � N a ❑ � N o m Y E m a E m in a ❑ Q J O _ U c _ F z > N � p � 0 o E o Z U `9 ~ a F- J J � — m y m Q O � N K N � E m N � a a p � N o m Y E m a E m in J n — m J Q O � N � E m N � a a p N N v m Y �- a E m N In U Q J n — m J Q O � p O E N h y a N N N E m Y �- J n — m J Q O E p O E U y a N N N E m Y �- a N E a ❑ a J O ? 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P. h h 0 O h t0 V m m d' o D m 0 (00 m N N N N N V N N N N m N (m0 m f�O m 0 0 0 0 0 0 0 0 0 O O O O O O o m n c v o r m0 0Y cT N N O N N 6 N _ G o E — p o o o LL .`- 0 U_ _ `o0 N — N d Z N N O N O N O N N N O CT fn N U7 fn N V) N U 2 z S= 6. d :i �o O N m w :i w �a C .pp .a 7 o E a � �ro�a :i u N rs rra T 0 0 Y N d N N 0 q d o ?: N a 0 v w rra T 0 0 Y N d r-r-� Tr m o .n _n N N 0 U O N N a 0 D] � � r-r-� Tr m o .n _n 0 U G ❑ N a 0 D] H E z z N ❑ v m � � m 9 m E d P" E m n v U Q a ao o d ❑ v U 0 N ra o P4 N A ti o D N o Gl W a O G a Q0 E � m n U Q o > > za u U x � a E A m m NE r 0 U G ❑ N a 0 D] H E � am N ❑ v m � m m 9 m E d P" E m n v r U G ❑ N a 0 � H E U U N v v N N m r U G ° N a 0 � N N U U N d J ❑ N m m 9 U P" E m J U Q LUOf U G ° � a 0 � N N h N d N N N m v o � U G w � o 0 � N N h N a � N [V m ~ U P" E m J 5 a ao o d ❑ v U 0 N ra o P4 N A ti 4 a N o Gl W � m G a Q0 E � m n U Q v o � U G w v no 0 N h N � N [V m G w v no 0 N � N m a P" J 5 a ao o d ❑ w� 0 N ra o P4 N 5 ti 4 a N o W � m G a Q0 w o x v w a J 5 a ao w� 0 N ra o P4 N 5 ti 4 a N o W � m G a a� 15 o > > za x W"za x � a v a J , c a o W � q C o > > x x � a A a ( ( � 75 \\ f§! §/ � 75 \\ f§! )) 2\ \ ^/$ R \\\ \\\ ? ) \ \i)[ \k\ co ))(� � \\ f§! )) 2\ ^/$ \\\ \\\ ? ) \ \i)[ \k\ co ))(� } ) tg!{ £E)4 ±j[) )))\ }{!j&«2, >k\ � § \\ f§! )) 2\ ^/$ \\\ ? ) \ \i)[ \k\ co ))(� tg!{ £E)4 ±j[) )))\ }{!j&«2, >k\ \/ \ :aG \} \ /* C3 § \\ f§! )) 2\ ^/$ \\\ ? ) \ \i)[ 0 co ))(� tg!{ £E)4 ±j[) )))\ }{!j&«2, \/ \ § ) \\ )) 2\ ^/$ \\\ ? ) \ \i)[ 0 co ))(� tg!{ £E)4 ±j[) )))\ }{!j&«2, ) )) ^/$ \\\ ? 0 co /)( }{!j&«2, \ ■ � _ ■ (\ \ \ ,ƒ) 3\ � _ ■ }\ \ \ 3\ /\\ \ \\\( % \� ) \ \/\ \\ E&<§ \ )(\ \� f)§) )\ � _ ■ }\ \ \ 3\ /\\ \\\( \� ) \ � \\ E&<§ \ )(\ \� f)§) )\ }( £ \\)[ �{\ ;==a � _ ■ }\ \ \ 3\ /\\ \\\( \� \{j{ \\ E&<§ \ )(\ \� f)§) )\ \\)[ � _ ■ }\ \ \ 3\ /\\ \\\( \� \{j{ � _ ■ }\ \ \ 3\ /\\ \\\( \{j{ \\ E&<§ \ \� � _ ■ ■ }\ \ \ 3\ /\\ ■ \ \ /\\ \\\( \{j{ E&<§ \� f)§) )\ \\)[ ;==a ■ /\\ ))\\ \� )\ \\/) ■ .-. 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D d N v __ s r a 6 L E C E p Y `o `o v (q (n N m U U U 9 F- ow v _ m w E K - � m m d rJ oY ❑ H U �w ti E r Y .Q N N N o y � iDa E m � E o fD � m N V a ui a N .. y ° � O o Z E U o v O w' a` - o m a 9 P J ¢ v ❑ U r N O V v n U Q 12 � v z z o 7 � � o > 9 x i x � w � m m v _ m w E K - � m m d rJ oY ❑ H U �w ti E r Y .Q a d y o y � N E m � E o � m N V = ui a N .. y ° ° O o Z E U W O w' a` - o m a 9 P J ¢ v U o � E v m v _ m 00 E K - � m m d rJ oY O H U �w ti E m Y .Q a d y o y � m � E o � m N V y a N .. y O o Z U W O w' y 9 m a 9 P m v _ 00 y K � � m m d rJ oY O H U �w ti E m .Q a � o 9 E o N y N V C N U o O `o W O w' 9 m N 9 P o v O o � E v n U Q A N [O 00 Z O v n m m H d cY 00 Z O v n m m id cY 00 Z O N o N � rJ oY O O id cY 00 Z O O o N � rJ id cY Z rn O o o � rJ id cY rn O N o � rJ oY W �w ti .Q a � o 00 o y N V C o C id cY rn O N o � rJ �bc'a W o � rJ �bc'a �w ti .Q a � o 00 o V C o C o O W O w' o � rJ F .Q a � o 00 V C o C o O 9 � N P N O o � � f6 12 Ei C 7 � � o > 9 x i x � w a � V C o C 9 � O o � � C 7 � � o > 9 x i x � w c o = rn m � v E a � U w c o = rn m N E E a � o r�i O > ry rNi ❑ a u 0 p � a E n Y o a a W m ` E U o m 0 a C � z z o Q 0 = a O N N N_ c o = rn m N E E 46 � o r�i O > ry rNi ❑ a u a p � .- E n Y o a a W m ` E U o m 0 iDS C � N z o Q 0 = a O N N N_ o ❑ O o Z E U CO c w 35 J F N o a ❑ c J N Q o U E d m K w U Q d o = rn m N E E - � o r�i O > ry rNi v a u a p � .- E m Y o a a W m ` ❑ U o m 0 a C � N z o Q 0 = a O N N U N D O o Z E U CO c w a J F N 04 a d o = o m N N E a' � o r�i � ry rNi v a u a p � .- E m r o a a W m ` ❑ m � 0 0 a C � N z o Q 0 = a O N N U � D O O E o CO c w a Fes- F N 04 a ❑ c J N � o U E d m K w U Q m N N N N N N N N O m V o m m V 0 E a' � v r�i � ry rNi v O m V o m m V 0 E a' � J r N M r N a a N � .- r n r O m V o m m V 0 E a' J E w 0 a a O m V o m m E E E a' J E w 0 a a A � v n � o a a W `t ` ❑ m � 0 0 a C � z z o Q 0 = a O N O � D O Z E CO c w a Fes- Ci � 04 a c J Q o U � K - w � N W — — o 0 m - d E r < < o o x N w s N N m € `o 0 0 O 0 0 a o o N U U E F F o m m E E E a' J E w 0 a a A � v n � o a a W `t ` ❑ m � 0 0 a � � z z o Q 0 = N (n N O o m m E E E - J 0 w 0 a a A � 0 n Y o a a W U ` E U m 0 0 J � � N Q 0 = N (n N O � D O Z E CO c w a Fes- Ci � 04 a c J Q o U � K o m m E E E - J w 0 a C A 0 � Y o a a W U m _ U m 0 0 � � N Q 0 t w (n N O U Q O Z CO c w a Fes- Ci � 04 a o � m E E I J a 0 a C A 0 � o a N P4 U m _ J 0 0 � m E E I J a N a C A 0 3 b a N P4 U � _ J 0 0 0 � � N 0 0 t o wo � O U Q m E E � N o C A b b a N P4 O � 0 0 0 0 0 m E E � F C A b b a N P4 C � co 0 0 t o � O O o CO c v a W N O 04 cu o � � N W — — o v m U E < < > x � w E E � F C A b b a N P4 C � co t o O O o CO c v a W N O 04 w � F a N a co o O O o CO c v a N cu o � � zw o v m > x > x � w a N a C o � � o v > x > x � w R J v — v d N m a 0 L U P. 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C3 6q O K � d ❑ ❑ O � ~ o 00 E m m o ❑ d' o r o Z Z o N � � o FL 'b � W pp O a d. 6q O K � d ❑ ❑ a ~ U 00 E m m � E d' o r o a = m O w' m_ ❑ ❑_ 1 d E N �co d q ryq a o a C J Q m U W OR � U � > N N E m_ Gm vJ U Q vva- Y o a � 0 a v z � ro > i W a Z F d a � � o FL 'b � W pp O a d. 6q O K � d ❑ ~ U 00 E m m m d' o o a W O w' 1 d d q ryq z a m OR > � > N N E m_ Gm vJ U Q � � o FL 'b � W pp O M 6q � � o FL 'b C 00 O d' o o W O w' � � o FL 'b 00 O d' o M 1 d q ryq z a OR > x > fes• 0 N m C N °q' o CY � U Py 0 N m C N m CY � K Y Q p E Y E ❑ F v o � r n. m rn N h w m N M N o E E c .J — U a `o — Q Z z o N z o F N_ G� 0 m 0 N m C N m CY � K Y Q p 0 Y E ❑ F Y 0 � r � m rn N h w m N M N � E E c .J — U a `o — Q z z = N z o F N_ 0 0 m a 0 E � o � b z a - o m - o ❑ 'ra m Q J m U W Q W E m K N � (V 0 N m C N m CY � K Y Q p z Y E ❑ F Y 0 � r K m rn N h w m N M N � ❑ E c � — U a `o — Q z z o Z z o F N_ K in m 0 N m C N m C3 � K Y Q p z Y E ❑ F Y ❑ � r K m rn N m w m N M E � E E E � — U a `o — Q U 2 Z z o F N_ ❑ ❑_ m a 0 E � o 7 b z a C1 E m - o ❑ 'ra m Q J m J W Q = E m N N � (V n U K 0 N m C N m C3 � K Y Q p E Y E ❑ F Y ❑ � r d m rn N m w m M E � ❑ E E � — U a `o — Q U = Z z o F U ❑ ❑ m z 0 E 0 N m C N m � � K Y Q p ❑ Y E ❑ F Y � r � m rn N m w m M E � E E E � — U E `o — Q U = N r ❑ F U ❑ ❑ m v � E � o 7 b z o C1 E m e yP) ❑ 'ra m � ❑ m J W Q = E m N N � (V n U K 0 N m C N m � � K Y Q p ❑ Y E M F Y � m — m rn N m w m M E � — E E � — U E `o — Q U Y46 r ❑ F U O m v � O � o 7 b z o C1 E m e yP) ❑ 'ra m � ❑ m W O = E m N N � (V n U Q 0 o a Y Y a E Y Z a` - 3 U W J m d O Q m U o W K � 0 v a vv U fn U Q U !q U fO V fn Z ZZ Z o U ° UU N. J 'J H CJ I- d N F V 0 N m C N m � � K � Q p ❑ E M F � cLi — m 0 N m w m M 0 N N V w m � � K K n � ❑ E M tl1 � a — J 0 9 m w m M w � m E v � N U N N N V w J � � K K n � ❑ E M H J ren — J 0 9 m w m M N N V w a � K K KN ❑ E M H J ren — J 0 9 w m M w � m E v � M N `o U Q N V w W � K K ui ❑ E M H � ren — m 0 m w m M w � r � N `o U Y46 r ❑ F U O m v � O � o 7 b z o C1 E m e yP) ❑ 'ra m � ❑ m W O = E m N N � (V n U Q 0 0 �o ❑ E M � ren — m 0 w n M � � r � N U Y46 r ❑ C � m v � O � o 7 Z z o ate' Y 0 �o ❑ E M � ren — w r � U Y46 b Q � m v � O � o 7 m a a ate' E m e yP) � 'ra m a ❑ 3 W O = N N � (V N 0 o a pm a E Z a` - 3 U W J m d O Q m U o W K � 0 Y "' �o ❑ E M � ren — w U Y46 b Q � m v � O � o m a a ate' E m e yP) � 'ra m a ❑ 3 W O mi RT � (V N V a pm Z U W J m d O m m Yo "' �o ❑ o M � ren w U o b Q � v O � o m a a ate' E m e yP) 'ra m ❑ ❑ W O mi (V a d � O m m � m v U fn U Q U �o o M w U o b Q � O � m a a ate' e yP) 'ra 7 ❑ ❑ W O mi U � O � a a ate' e yP) (V a � < ■ )Z \ � /\ \\\0 \ � \\\0 ) )) am®` Ja!! f]§) )))\ * ) )) \\\� \)(� r2/) §}2y ,m\, Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J m ' 0 m � U p. Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N 1 m � d J d E a � E n N J E M ❑ n w a M M K N n N N ❑ V 1O r ❑ 1�D c a N a a n Z o � Z o 45 N ❑ m_ r K in E Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N 1 m � 46 J d E a � E n N ❑ E d o n W K M M K N m N N ❑ V 1O r E E a N a n Z o � U = 45 N ❑ m_ r � ❑ E m U E N y � d Z a m o a � J W C 0 QJ J ❑ Q U � U N d � o Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N 1 m � O J d E a � E n N ❑ E d o n W a M M K N m N N ❑ V 1O r ❑ E a N a n Z o � U S 0 N ❑ Y r Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N 1 m � a J d E a � J n N ❑ E M a n r � � n w N m N N ❑ 1pp r E E J N a n Z o � U S 0 N ❑ Y r 0 o E m U E N y � d Z o T 3 a � J W C 0 Q J ❑ Q U � U N d � o Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N J m � a J d E a � J n N ❑ E M a n n � � n w N m N N ❑ 1pp r E E a N a n Z o � U 2 0 N ❑ Y r Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d N J N J m � N J d � a � rn n � E � E n n � � m w N m N N n m ❑ E E � N a n U Q � U 2 0 ❑ Y r 0 0 E m U E N o d Z o T u a � o W O 0 m J ❑ Q N � U N d � o E 9 a Y Y Y E - E - 0 E - Y Y Y N Z o Z o Z UU o U J d dN �I N H d OfmSE N J N J m � N J d � a � rn n � E � E n N ' � m w N m N � n OfmSE N b W m a N J d � � rn n � E m E m N ' � a w E m N � n m ❑ N E � N a n U Q '�' N b W m a N J d � � rn n � E m E N ' o U w E m E m n m ❑ N 46a. N b W � N y d O rn a' E m E N ' U U w J J E m n ❑ ❑ N M � N a o 'd N{ � U Q 46a. N b W � N y d O rn E E N ' w - E m n ❑ a M � N a o 'd N{ a � w 0 ❑ Y r a � E m U (V N o d Z o u n � � W O 0 m ❑ N � N d � o E 9 a m V 9 U Q 46a. N b W �pq Y d O rn E E N ' w - n ❑ a M � M a o 'd N{ r � w 0 ❑ Y r a � E m V (V Z Z o N b W �pq Y > O rn E N ' w - n ❑ a M a o 'd � r � w o Y C o ❑ E m V 9 a u E � W O 0 J N qa d d � o 0 9 a m V = N f N j x > ❑ ❑ � a o CY E � v Z o o C)N m ~ J Q U w M � 0 N b W �pq Y O rn E w - n ❑ a M 46 o 'd � � vv❑�� w o Y C o ❑ E m V 9 a u x W O 0 N qa d d � o 0 9 a m V N f j x > N N � a o CY N Z o o C)N m ~ a N b W �pq O O M cn w n ❑ a M o 'd � vv❑�� w o 0 C o ❑ E m V 9 W O 0 N qa d 0 9 a f x > d U � a o CY P a m E m 0 a 0 U Q to N b W �pq O O M cn w Q T a M o 'd vv❑�� w o 0 C o ❑ V V 9 W O m Q T a M o 0 C o ❑ V V 9 qa d 0 9 f x > x � a a T a y o C ❑ V V 9 0 9 o x > x � a P a \ ) J j ) ) ®3\OD ]$.:3 i\4§ \\\ 0 \))/ /\\ =:o; j ®3\OD \\\ 0 /\\ , \\\J / \{}) V �l m E E E a v � d o � a U a m E E E a v � o d � a y � v ❑ K ~ U O. E m � U a 6 a a m a E m a a � K H 5 0 v E a 0 o O o a a W o Q 3 o Y r 9 n wC o } ❑ N } N a o E � m Y � in U Q m E E E � d � a y � n � K 2 � O. E m � U a 6 a E m a E m � a � K H 5 0 v E a 0 o O o a a W Q 3 o Y •- m n wC o } � n } � a o E v a Y � W U N n E w u � x q U Q V � K � a y � n � U O. E m � a a a a a E m � o � in 5 0 v E o 0 o O o a a W Q 3 o Y •- m n wC } � N � � a o E v a Y n U Q V i E E C a y � o a � a a a c a E m � o � in 5 0 a E o 0 o O o a a W Q 3 v CO wC � � a o Y c 9 n w E � x > w � Z d E v in U Q i E E C o � a � a a c a 'a � o � o 5 0 E o 0 o O o a a W o � v CO wC � � a w E ❑ x o � a � a T a 'a W o � o 5 0 E o 0 o O o W o � CO wC � � a E � o > w > Z a a � a T o o 0 E U o U o � wC E � o > w > a a' r � rn � o � d ' 0 v K � rn � v a d ' 0 v K a P` � rn � ca a d m � K a a v a N K E ❑ ❑ W N ❑ I o, a E n � s — m n E m m ❑ 1O � E _ N a a _ Cf N z o N= N _ N a � rn 'E � rn � — a d m � K � a v a N K E ❑ ❑ W � ❑ I o, � E n � s — m n E a m ❑ 1O N E _ N a a _ N N Q = N= N _ N a U U 'E ❑ H d c C a o Y 5 = d W N m w' a` Q J 9 ¢ o U O ¢ W m a E � LU � rn � — a d m � K � a v a N K E ❑ Y W � ❑ I o, y E m � s — m n E a m ❑ 1O N E _ N a a _ N N Q 5 N= Z _ N ,43 U U J ❑ H d c C a o Y 5 � rn � — a d m � K � a v a N K E ❑ J W � ❑ 2 o, a E m � a m m n E a m ❑ 1O r E _ N a a _ U c Q 5 N= Z _ N ,43 Uy U d ❑ ~ l c C E o Y 5 = d W N m w' a` r o 9 ¢ o U O ¢ W m a E � LU n U Q � rn � — a d 0 0 K N a v a o K E ❑ J W Q ❑ I o, a E m � a m m n E � m ❑ 1O r E _ N a a _ U c Q 5 N= Z _ N ,43 Uy U d � rn � — a d a 0 K N a v a o K ❑ ❑ J W ❑ � I r U E n 0 a m m E E m ❑ � � E _ N a a _ U c o 5 N= Z _ N ,43 Uy U d ❑ ~ l c z E o U 5 = d W N m w' a` — o ❑ ¢ o U O ¢ W m K 0 � LU � rn � — a d a 0 K N a v a o K Y ❑ J W ❑ a I m U E n 0 a m m � E m ❑ � � E _ N a a _ U c o 5 � Z _ N w Uy U d ❑ ~ l c z E o U 5 � rn � — a d a 0 K N a v a o K � ❑ J oa ❑ ❑ I m a E n 0 a m b E m ❑ � � E I H N a a _ � c o 5 o Z _ N w m U d ❑ ❑ l c z E o U 5 = d W N m w' a` — o ❑ 0 o n O ¢ m U 0 � LU n U Q o m J w 9 ¢ ¢E T fn U Q � rn � — a d a 0 K � � a on E ❑ J N � ❑ I m a E n 0 a m b e a ❑ � � E I H N a � _ � c o 5 o Z _ N w m U d � rn � — a d 0 K � � a on ❑ ❑ N � d I � E n 0 a m b a a � � E I H N n � _ � �b z 5 o Z _ N w m U d ❑ ❑ c z E o d 5 = W N m w' a` — o ❑ 0 o n O ¢ U E � LU n U Q � rn � — a d 0 K � � a on ❑ Y N � d I U E z 0 a m b a a � � Y I H N n � _ � �b z 5 o Z U w m U d N Q c z P4 � rn � — a d 0 K � � a on ❑ y H � o I N E z 0 a m in a a � T � I H N n � _ � �b z 5 rn U a m U d N Q c z P4 o d 5 = W N m w' o cm ❑ 0 o n O E o E � m n U Q � rn � — N 0 o a 7 a on ❑ y E o I N 2 � 0 a m a r a � T � OD N n � _ � �b z 5 rn U a a F� d N z z P4 � rn :J � — N w o a 7 a on ❑ y E o I N 2 � A a - � r a � T � OD N m � _ � �b z 5 rn U a J F� d N P4 d 5 = W N O w' o cm 0 o n O E o E o m J w 9 ¢ ¢E T U W .� x K a E m O - :J � — N w o a 7 a on ❑ y E o I N 2 � A a - m a � T � OD N m � _ � �b z 5 rn U a o F� d Fa P4 :J � — N y o a v a on ❑ w E o b 2 � A a T OD E m _ � �b 5 rn a o P4 d 5 W O w' o cm U n O o E o m z w 9 ¢E ¢E T .� x � a E m O - n U Q — :J .. o o on w :J o b A a T OD � �b 5 0 o P4 d 5 W O w' :J a T OD � 5 0 o P4 d 5 cm w o E o z w � ¢E ¢E o :J a T w o E o � � o x � a :J u V E E .. N v a m ro O � E E .. N v a m d O � U W E E .. N a a d O o a � o � � n ❑ a ❑ n � M n� � v o m a E m a ro m F y E m a t m � o a A cl b 0 CEi o a U a U N O N � o Cd F 4 m m o � O U m U n m � m Eami m in r m ❑ E E .. N a d H O o a � 0 oa n � a ❑ n � M n� v E m a C a E m F a E m 00 t m � o a A cl b 0 CEi O a U a Q y� � yaC N � o Cd F 4 m o � O U m U n m � m o in r m ❑ m � N m Z ❑ � v m w N P� N (q U Q E E .. N m a H O a a � 0 oa n � n � M n� C E m a C a o� F a E m 00 t � o is C A a b 0 CEi O H U a Q y� � yaC N � o Cd F 4 m U m E � m o in U Q n m .- m Z ❑ � w N P� N E m n 0 V J T .. N m a y O o K � n � M n� C E m a C a in F a 00 t � o is C A P4 b 0 CEi O N U a o y� � yaC N � o Cd F 4 m � m E � m in U Q V J T .. N m O pp 5 M C . a C a F 00 t � o is C A P4 b CEi O � N y� � yaC N � o F 4 m 5 C . a 00 CEi O F 4 .a Z a w ti P� a f•_•1 ro E a o w v �o m � D� U m E o ro E a y w v �o 0 � D� U w ro E a y w a � 0 � D� a � E o ❑ a N E 0 i o a E m � a m � o j a m o � ❑ a E a � N J c v U c Q E o Z = � m ro E a y w a � � � D� a � E o ❑ a N E d i � � E r � a m � o j a o ❑ a E E � N J Q N U c Q E o Z = N N_ U (.) 0 o a v O E H H aZ � = d T 3� o m J a C . o Q J Q U o W E v m E � K 9 U a ro E a y N a � � � D� a � E o ❑ Y N E d i � m E m � a m � o j a o ❑ a E Y � N � Q N U c Q E o Z = N N_ U (.) N F a v O E H y aZ ro E a y N a � � � D� a � E o ❑ Y H E a F � a E m � a m � o j a o ❑ a E Y ❑ N � Q N � c Q E N Z = N N_ N (.) v CY d v O E o y aZ � = d m" 3 o m J a C . o Q a U o Q E v m E � a 9 U Q ro E a y N a � U � D� ❑ �pp E o ❑ Y N E a F o a T m � a N o j v o ❑ a E Y ❑ N � o N � c Q E N Z = N N_ � m ro E a y N a � v>- � D� ❑ �pp E o ❑ Y N E a F ti J T m o a N o j O � ❑ a E Y ❑ N � o N � Q z E N Z = N N_ U N ❑ ❑ d v O E o y aZ � = d T 3 o m J a C . o Q a U o Q o K E � a ro E a y N a � 0 � D� ❑ �pp E o ❑ Y N E d F ti J T m o a N o j O � ❑ a E Y ❑ N � o N � Q z E N Z o N_ U N N H d v O z o R aZ ro E a y N a � 0 � D� ❑ �pp E o ❑ Y m E ❑ F ti J T m o a m m - O � ❑ a E m � b o N � Q z E N C o N_ 0 N N is E v O z o R aZ = N o m m a . o Q a E o Q o E � m ti p a7 U Q ro E T a y w K 0 � O �pp E Y m E ❑ a � J T m o a a - a � ❑ E m � b o N � z E N C o N_ 0 N � d E z z o R aZ = N o m m a T a y w K 0 � �pp E Y m r ❑ a � Y T m o a S - a � ❑ E m � b o N � z E N C o N_ 0 N � d E Q o R aZ = N o 0 v Q ~ a 0 o Q a E o Q o ti p a` o m w 0 � Q o W • E m m T a y w K 0 � �pp E Y m r ❑ a � Y T m o a - a � ❑ E m � b o N � z e N C o N_ 0 N � d E Q o R aZ 9 o 0 v Q ~ a � U Q a w T a y w K 0 � �pp E Y m r ❑ a � a T m o - a � ❑ E m � a - N � z e N a o N_ � N � d E Q o R a 9 o 0 v Q r U Q a w o Q o ti p z m w 0 o • E m m W in U T a E N a y w K 0 � �pp E Y m r ❑ 2 o a T m o - � H ❑ r iDS � a - N � z e N o N_ � N a E N a y w K q � �pp O Y m � a 2 m T m o - A H E iDS � Y - N � N o N_ ❑ ❑_ � d E � o R a 9 o 0 v Q E Q a w U Q o a E N a y w K q � �pp O Y m � a 2 m T m o - A bq � Y - N � N o Z 5 � d c � o R a a E N a y K q ❑ �pp O � 2 O E m o a bq Q W U 5 o d c b � R 9 o 0 v Q E a U Q a E N .. N q 0 �pp O O � o bq W 5 c b � o o 0 v Q o p z w o • x � a W O w' a E N o 00 5 c b � N p z w 5 c p • x � a N Page 43 of 48 _ k17 OD e M e q� a s x wanl�euasara .7 z _ � z d 1;7WA MUT' xo=MQ WV=V `a8Pni5-'is J o WD �4 w vi ;i � a kt •°2 qy oo u U, v v 13 a Co Page 43 of 48 omray. 16 r uaiaiiE. �nrF;., �rsr.:oli:rl Tc-c.�f:nEngi�s, Enr,. en�aroo nerd Gu+ate Initials of person inspeeCing cooler end semplas:� ""tom. Otani. � ' L I' Order Numlmr�__ _ Data Reoelved,- ±± Time P.eceivad- Date cooler(s) opened and samples irspocted:-, Number of Coale-WBoxes: NIA Shipper. ED UPS DHL Airborne US Postal Walk-in Pickup Ofber. Packaging: Peanuts Bub a Paper Foam None Other. Tape on cooleribox N NfA Custody Seals intact y N FO -C in plastic r �ri N Nil,, lca� Slue ice ! res • i absent I melted NIA SamPla Temrrperature IR Gun fk1fia2ti4Gg CF �,0°C 3' ! g>G NIA Radiolagtcal Testing Inabrumentserial1136727 Y N 'Cp' (see pegs 2 far scan results} CC�'' "Use i sheat par sample far Radlologicat TesLng. lieample is HOT, ilia Radlotogica(Safafy Orficer must be notiric3 immediately. /,r+ C -O -C filled oui properly d N NIA Samples In separate bags N WA Sample containers intact' N NIA `If no, list broken sampla(s):-- Sample labels} complete (iD, date, ele.) � N N1A Labels) agree wlth C -O -C �e N N[A Gufract containers used (/ N - WA Suffrclent sample received Y N NIA Sample$ rocelved within -holding time LY N Bubbles absent from 44 mL vials"' Y N "Samples with buBbles amm are acceptable. bullcateibubble size it>6mm. WaA Client contacted abeutsanlPles Y N VYllclient Send now samples; Y N C)ient contact; Logged in Page 1 oft Page 44 of 48 Page 1 of 4 Page 45 of 48 LO E a m U Claw mz� 199s I'z3a1*2a 929=0 3=09n lz� va oig o a¢vwig �Sids aa¢�g 9i Li �$ p5 ¢ Q N¢ i m g m f m � Mf p ?� m i i Mp] w��" °mm o °° � I.: ti�mm�mo ¢L W a4. ¢ N W y N W iA h y� F N Q W W W tail a W h W N g W N W tail 6m W h W N m W N § d E Z aaaj y .a% m q_ ? o W N a g o m a m o °1 v ^ v G a W Z G 6 a 5❑ W`yyN°cz� �aJ m`¢W°cWgpaa NWq fyNO Wrr a oWOrr gy$ry OWrr aY5t�nq CaleE¢� CIra, a+ v al!aam w ^¢50 ai y KZ N W O w KLLF 2 6ZC cs dmZ 6yraa � w Lj UT O O ¢ O vO aWa 0 OJOWW Vi y z z Page 2 of 4 E h r= m O 3 'c v LL W _ g � E Claw mz� 199s I'z3a1*2a 929=0 3=09n lz� va oig o a¢vwig �Sids aa¢�g 9i Li �$ p5 ¢ Q N¢ i m g m f m � Mf p ?� m i i Mp] w��" °mm o °° � I.: ti�mm�mo ¢L W a4. ¢ N W y N W iA h y� F N Q W W W tail a W h W N g W N W tail 6m W h W N m W N § d E Z aaaj y .a% m q_ ? o W N a g o m a m o °1 v ^ v G a W Z G 6 a 5❑ W`yyN°cz� �aJ m`¢W°cWgpaa NWq fyNO Wrr a oWOrr gy$ry OWrr aY5t�nq CaleE¢� CIra, a+ v al!aam w ^¢50 ai y KZ N W O w KLLF 2 6ZC cs dmZ 6yraa � w Lj UT O O ¢ O vO aWa 0 OJOWW Vi y z z Page 2 of 4 h r= m O 'c N LL W _ g � E r N U ro Claw mz� 199s I'z3a1*2a 929=0 3=09n lz� va oig o a¢vwig �Sids aa¢�g 9i Li �$ p5 ¢ Q N¢ i m g m f m � Mf p ?� m i i Mp] w��" °mm o °° � I.: ti�mm�mo ¢L W a4. ¢ N W y N W iA h y� F N Q W W W tail a W h W N g W N W tail 6m W h W N m W N § d E Z aaaj y .a% m q_ ? o W N a g o m a m o °1 v ^ v G a W Z G 6 a 5❑ W`yyN°cz� �aJ m`¢W°cWgpaa NWq fyNO Wrr a oWOrr gy$ry OWrr aY5t�nq CaleE¢� CIra, a+ v al!aam w ^¢50 ai y KZ N W O w KLLF 2 6ZC cs dmZ 6yraa � w Lj UT O O ¢ O vO aWa 0 OJOWW Vi y z z Page 2 of 4 z q R7 I 2 E' P Q¢ Q¢h am¢aua v¢usg 4 omp r,-�$w^m m> ew Q,00 si0 rw°pmDom�^o°S� o�m € m g m z ma a anm a o m o 11 0 o m o m? o g 3w'o'��'o"�mrv�zN`g°cmi$wR�ry � W N W s E S K E 8 `e 3 d » H m v N N c S S ¢ 4F :S no gw o` o - - - - - a¢¢$ a o a 3 a 3 a 3 a 3 a 3 a 3 a 3 a 3 a a 3 a p a 3¢ a 3 a 3 s a Page 3 of 4 Page 47 of 48 E E m .. O U W O IL z q R7 I 2 E' P Q¢ Q¢h am¢aua v¢usg 4 omp r,-�$w^m m> ew Q,00 si0 rw°pmDom�^o°S� o�m € m g m z ma a anm a o m o 11 0 o m o m? o g 3w'o'��'o"�mrv�zN`g°cmi$wR�ry � W N W s E S K E 8 `e 3 d » H m v N N c S S ¢ 4F :S no gw o` o - - - - - a¢¢$ a o a 3 a 3 a 3 a 3 a 3 a 3 a 3 a 3 a a 3 a p a 3¢ a 3 a 3 s a Page 3 of 4 Page 47 of 48 T E Z Q p « NM � U W W O N Z O N U ^ Z Z o m 0 m _ a u S¢ W K JJ U Q g 4 i O0 Fn a U � ❑ �Nm m oZ v°r�i. mC6a o w a m a o$ z m w m m UW Z 6W. W N 0. W N a W N O N F N F N e C E F W E U Vk $ ay � � � E � O g a g a g z o¢L6 a v¢ a 'v a h a 'a awi a N= J ❑ ❑ i p i i p i m i❑ i m g? o Yci v p¢ a a 3 pa 3 d 3 o a 3 a J 3 N w N a 3 a 3 M O W N W N W N x W N W N Z W N Q W N Z W www? p N p 6 W N Z N Page 4 of 4 �m U '� Summit Environmental TechnoloWine. 33100 w�nSt. rfdVIRONIA€NTALTEClit4OLGGtES,]IaG Cuyahoga Fails, Ohio 44223 Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 Website: htto://www.settekcom February 27, 2018 Erik Bruce Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Yadkinville WWTP Dear Erik Bruce: Order No.: 18010568 Summit Environmental Technologies, Inc. received 1 sample(s) on 1/12/2018 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, California 07256CA, Colorado, Covnectiwt PH -0108, De]awaze, Florida NELAC E87688, Geor�aE87688, Idaho OH00923, lllinois 200061, Indiana C -OH -13, Kansas )x10347, Kentu cky (Uvdergromd Storage Tarek) 3, Kentucky 90146, Lotisiarm 04061, Mary]and 339, Mimesoh 409711, New Harnpslure 2996, New jersey OH006, New York 11777, North Carolina 39705 avd 631, NoRh Dakota R-201, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-11-5, Utah. OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 24 Summit Environmental Technologies, Inc. SUMMIT 3310 Win St. Case Narrative "VIRONMENTALTECHHOLBGIES, mr- Cuyahoga Falls, Ohio 44223 WO#: 18010568 Arrafytical Lnhgrstarle€ TEL: (330) 253-8211 FAX (330) 253-4489 Date: 2/27/2018 Website: hito.//viv settekcom CLIENT: Synagro Project: Yadkinville WWTP WorkOrder Narrative: 18010568: This report in its entirety consists of the following documents: Cover Letter, Case Narrative; Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence Sample Notes: 18010568-OOla TCLP-SVOC-CPest(8081B): The Pesticide MS and MSD pair exhibited high RPDs for Endrin and Methoxychlor; Recoveries were within acceptance limits for all analytes individually in both the MS and the MSD. Original Page 2 of 24 Summit Environmental Technologies, In U1� Qualifiers and Acronyms \ 3310 wtn MVIRONktENTALTECHNO LOG] ES, INC Cuyahoga Falls, Ohio 4422 WO#: 18010568 Anziytical Lahora3urles TEL.: (330) 253-8211 FAX: (330) 253-446 Website: hao.//ivwwsettekco Date: 2/27/2018 These commonly used Qualifiers and Acronyms may or may not be present in this report. Qual�ers U This list of Qualifiers and Acronyms reflects the most commonly utilized Quali The compound was analysed for but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. H The hold time for sample preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GUMS. X The result was not confirmed when GUMS Analysis was performed. 1180+ The analyte was detected in the, associated blank. G The ICB or CCB contained reportable amounts of analyte. QC-/+ The CCV recovery failed low (-) or high (+). R/QDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+). QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low (-) or high (+). QMR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms ND Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different M1nCL Minimum Compound Limit ICV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor fiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 24 t MIS-- �� Summit Environmental Technologies, Inc. WOrkorder UMM3310 Win St. MVIA0N1.1@NTAL TECHNOLOGt'cS, mc; Cuyahoga Falls, Ohio 44223 Sample Summary Anatytlral Laboraiorles TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 18010568 Website: htto:/Avivivsettekcom 27-Feb48 CLIENT: Synagro Project: Yadkinville WWTP Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix 18010568-001 Yadldnvlle WWTP 1/11/2018830:00 AM 1/12/201912:20.00 PM Solid Page 4 of 24 \ \ 3 / Summit Environmental Technologies, Inc. m y 331OWinSt. Analytical Report ILJFNVIR0 NNIENTAL TECWJ0 LOUPE S, INC Cuyahoga Falls, Ohio 44223 (base report) Arrarlytiral Lataaratorlea TEL: (330) 253-8211 FAX (330) 253-4489 WO#: 18010568 Website: h0.11mwivsettekcom Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/11/20188:30:00 AM Lab ID: 18010568-OOIA Project: Yadkinville WWT Client Sample ID Yadkinville W WTP Analyses Result RL Quad Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW7470A SW7470A Analyst: EAM TCLP MERCURY ANALYSIS (SW131117470) TCLP Mercury ND 0.00200 mg/L 1 1/16/2018 2:55:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW601OD SW301OA Analyst: KMS TCLP METALS ANALYSIS (SW1311/6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/16/2018 2:59:00 PM TCLP Barium(Ba) ND 5.00 mg/L 1 1/16/2018 2:59:00 PM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/16/2018 2:59:00 PM TCLP Chro rdum(Cr) ND 0.200 mg/L 1 1/16/2018 2:59:00 PM TCLP Lead(Pb) ND 0.500 mg/L 1 1/16/2018 2:59:00 PM TCLP Selenium(Se) ND 0.0500 mg/L - 1 1/16/20182:59:00 PM TCLP Silver(Ag) ND 0.500 mg1L 1 1116/2018 2:59:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D SW351OC Analyst: BJH TCLP SEMI-VOLATILES ANALYSIS (SW131118270) 1,4-Dichlorobenzene ND 0.0800 mg/L 2 111812018 10:45:00 AM 2,4,5-Trichlorophenol ND 0.200 mg/L 2 1/181201810:45:00 AM 2,4,6-Trichlorophenol ND 0.200 mg/L 2 1/181201810:45:00 AM 2,4-Dinitrotoluene ND 0.0400 mg/L 2 1/18/201810:45:00 AM o-Cresol ND 0.200 mg/L 2 1/18/2018 10:45:00 AM m/p-Cresol(s) ND 0.200 mg/L 2 11181201810:45:00 AM Cresols, Total ND 4.00 mg/L 2 1/18/2018 10:45:00 AM Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 1/18/ 201810:45:00 AM Hexachlorobenzene ND 0.0400 mg/L 2 1118/201810:45:00 AM Hexachloroethane ND 0.0800 mg/L 2 1/181201810:45:00 AM Nitrobenzene ND 0.0800 mg/L 2 1/18/2018 10:45:00 AM Pentachlorophenol ND 0.200 mg/L. 2 1118/201810:45:00 AM Pyridine ND 0.200 mg/L 2 1/18/2018 10:45:00 AM Surr: 2-Fluorophenol 42.0 10-109 %Rec 2 1/18/201810:45:00 AM Surr: Phenol-d6 21.2 10-109 % Rec 2 1/18/2018 10:45:00 AM Surr: Nitrobenzene-d5 66.3 19-120 % Rec 2 1/1812018 10:45:00 AM Surr: 2,4,6-Tribromophenol 47.3 10-120 % Rec 2 1/18/2018 10:45:00 AM Surr: 2-Fluorobiphenyl 64.5 22-117 % Rec 2 1/18/2018 10:45:00 AM Qualifiers: � Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding times for prepazation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds �.. ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds PL Pennit Limit Original, R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 24 Summit Environmental Technologies, Inc. Msummint 3310 Win St. Analytical Report RNIFtONld@NTALTPCONOLQGIES, INC Cuyahoga Falls, Ohio 44223 (basereport) Analytical LabPraOrms TEL: (330) 253-8211 FAX. (330) 233-4489 WO#: 18010568 Website: hgQ llwwiv.settek.com Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/11/20188:30:00 AM Lab ID: 18010568-OOIA Project: Yadkinville WWTP Client Sample ID Yadkinville W WTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D SW3510C Analyst: BJH TCLP SEMI-VOLATILES ANALYSIS (SW131118270) Burr: p-Terphenyl-dl4 74.1 34-116 %Rec 2 1/18/201810:45:00 AM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: JBN TCLP PESTICIDES ANALYSIS (SW1311/8081) Chlordane, total ND 0.0100 mg/L 1 1/17/2018 3:18:00 PM Toxaphene ND 0.0200 mg/L 1 1/17/2018 3:18:00 PM Endrin ND 0.00100 OMR mg/L 1 1/17/2018 3:18:00 PM gamma-BHC ND 0.00100 mg/L 1 1/17/20183:18:00 PM t' Heptachlor ND 0.00100 mg/L 1 1/17/2018 3:18:00 PM � Heptachlor epoxide ND 0.00100 mglL 1 1/17/2018 3:18:00 PM Methoxychlor ND 0.00100 QMR mg/L 1 1/17/20183:18:00 PM Surr: TCMX 78.0 10-119 %Rec 1 1117120183:18:00 PM Sur, DCB 61.8 10-119 %Rec 1 1/17/2018 3:18:00 PM NOTES: The Pesticide MS and MSD pair exhibited high RPDs for Endrin and Methoxychlor, Recoveries were within acceptance limits for all analyte individually in both the MS and the MSD. TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8151A SW8151A Analyst: JBN TCLP HERBICIDES ANALYSIS (SW1311/8151) 2,4-D ND 1.00 mg/L 1 1/23/2018 5:14:00 PM 21415-TP ND 0.500 mg/L 1 1/23/2018 5:14:00 PM Sort: DCAA 91.0 20-140 %Rec 1 1/23/2018 5:14:00 PM TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8260B SW1311M Analyst: CTB TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 0.0500 mg/L 10 1/16/20184:43:00 PM 1,2-Dichloroethane ND 0.0500 mg/L 10 1/16/20184:43:00 PM MEK ND 0.250 mg/L 10 1/16/20184:43:00 PM Benzene ND 0.0500 mg/L 10 1/16/2018 4:43:00 PM Carbon tetrachloride ND 0.0500 mg/L 10 1/16/2018 4:43:00 PM Chlorobenzene ND 0.0500 mg/L 10 1/16/20184:43:00 PM Chloroform ND 0.0500 mg/L 10 1/16/20184:43:00 PM Qualifiers: ' Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 7 of 24 U IT Summit Environmenta(Teehnoles, St. Analytical Report 331010 ll'<'n St. IT CNVIRONMENTALTECHN01,00IE5, ING Cuyahoga Falls, Ohio 44223 (basereport) Areary+tical L,aharefurles TEL.: (330) 253-8211 FAX. (330) 253-4489 WO#: 18010568 Website: hQ.11wwivsettelteom Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SOLID Collection Date: 1/11/2018 8:30:00 AM Lab ID: 18010568-o01A Project: Yadkinville WWTP Client Sample ID Yadkinville W WTP Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: CTB TCLP VOLATILES ANALYSIS Tetrachloroethene ND 0.0500 mglL 10 1/16/20184:43:00 PM Trichloroethene ND 0.0500 mg/L 10 1/16/20184:43:00 PM Vinyl chloride ND 0.0200 mg/L 10 1/16/2018 4:43:00 PM Surr. 4-Bromofluorobenzene 94.3 70-130 %Rec 10 1/16/2018 4:43:00 PM Surr: Dibromofluoromethane 104 70-130 %Rec - 10 1/16/20184:43:00 PM Surr: Toluene -d8 93.6 70-130 %Rec 10 1/16/20184:43:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2) -SOLID Cyanide, Reactive ND 0.500 mg/Kg 1 1/19/2018 4:48:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW -846:1030) Ignitability non-flammable 1 1/25/2018 1:00:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW9045D Analyst: DHC PH (SW9045D) pH 7.8 s.u.@18.3C 1 1/17/2018 11:55:00 AM RCI -SOLID -W/ IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)17.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 1/19/2018 4:48:00 PM Qualifiers: * Value exceeds Maximum Contaminant Level. H Holding times for prepazation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine azea response N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 8 of 24 summ.itEnvlrownentaf Technologies, Inc. Accreditation Program MSUMMIEF 3310 Win St. Analytes P es Report FNVIROhIMEN'TALTECISNBLr1G'ESr'UC; Cuyahoga Falls, Ohio 44223 .7` Analytical Lxhoratorfes TEL: (330) 253-8211 FAX., (330) 253-4489 WO#: 18010568 Website: him Ilaww.settekcom 27-Feb-18 Client: Synagro State: NW Project: YadklnvilleWWTP Program Name: NC-WW-SCM Sample ID Matrix Test Name Analyte Status 18010568-001A Solid C Ignitability of Solids (SW -846. 1030) Ignitability A Solid pH(SW9045D) Hydrogen Ion (pH) A Solid Reactive Cyanide (9014/7.3.3.2) -Solid Cyanide, Reactive U Solid Reactive Sulfide (9034)17.3 4.2 Sulfide, Reactive U Solid TCLP Herbicides Analysis (SW1311/8151) 2,415 -TP A Solid TCLP Herbicides Analysis (SW1311/8151) 234-D A Solid TCLP Herbicides Analysis (SW1311/8151) DCAA A Solid TCLP Mercury Analysis (SW1 311/7470) Mercury A Solid TCLP Metals Analysis (SW1311/6010) Arsenic A Solid TCLP Metals Analysis (SW1311/6010) Barium A Solid TCLP Metals Analysis(SW1311/6010) Cadmium A Solid TCLP Metals Analysis (SW131116010) Chromium A Solid TCLP Metals Analysis (SW1311/6010) Lead A Solid TCLP Metals Analysis(SW1311/6010) Selenium A Solid TCLP Metals Analysis(SW1311/6010) Silver A Solid TCLP Pesticides Analysis(SW1311/8081) 2,2',3,3',4,4'15,5',6,6'- A Decachlorobiphenyl Solid TCLP Pesticides Analysis(SW1311/8081) Chlordanes total A Solid TCLP Pesticides Analysis (SW1311/808 1) Endrin A Solid TCLP Pesticides Analysis (SWI 311/8081) gamma -BHC A Solid TCLP Pesticides Analysis (SW131118 08 1) Heptachlor A Solid TCLP Pesticides Analysis (SW1311/8081) Heptachlor epoxide A Solid TCLP Pesticides Analysis (SW1311/8081) Methoxychlor A Solid TCLP Pesticides Analysis (SW1311/808 1) Tetrachloro-m-xylene A Solid TCLP Pesticides Analysis (SW131 1/808 1) Toxapbene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 1,4 -Dichlorobenzene A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,5 -Trichlorophenol A Solid TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-Tribromophenol A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4,6 -Trichlorophenol A Solid TCLP Seini-Volatiles; Analysis(SW1311/8270) 2,4-Dinifrotoluene A Solid TCLPSeini-Volatiles Analysis(SW1311/8270) 2-Fluorobiphenyl A Solid TCLP Semi -Volatiles Analysis (SWI 311/8270) 2-Flurimphenol A Kcy Key NC WW SCM A Accredited NC WW SCM U Unavailable Original #1 Page 9 of 24 UI%M1. Summit Environmental Technologies, Inc.Accreditation Program 3310 Win Ohio4422. Analytes Report fFiVIR[FNMENTftL TECHtipL¢Gles, !htG Cuyahoga Falls, Ohio 94223 Anaiytiral Laboralgrleg TEL: (330) 253-8211 FAX. (330) 253-4489 WO#: 18010568 Website: hnn /ftvww.set ekcom 27 -Feb -18 Client: Synagro State: NW Project: YadkinvilleWWTP Program Name: NC—WW—SCM Sample 11) Matrix Test Name Analyte Status 18010568-OOlA Soli d TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Methylphanol A Solid TCLP Send -Volatiles Analysis (SW1311/8270) 3,4-Methylphanol A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Cresols, Total A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachlorobenzene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachlorobutadiene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachloroethane A Solid TCLP Semi -Volatiles Analysis (SW1311/9270) Nitrobenzene A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene -d5 A Solid TCLP SemiVolatilesAnalysis (SW1311/8270) Pentachlorophenol A Solid TCLP Semi-Volaflles Analysis (SW1311/8270) Phenol -d6 A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) p-Terphenyl-d14 A Solid TCLP Semi -Volatiles Analysis (SW1311/8270) Pyridine A Solid TCLP Volatiles Analysis 1,1-Dichloreethene A Solid TCLP Volatiles Analysis 1,2-Dichloroethane A Solid TCLP Volatiles Analysis 2-Butanone A Solid TCLP Volatiles Analysis 4-Bromofluorobenzenc A Solid TCLP Volatiles Analysis Benzene A Solid TCLP Volatiles Analysis Carbon tetrachloride A Solid TCLP Volatiles Analysis Chlorobenzene A Solid TCLP Volatiles Analysis Chloroform A Solid TCLP Volatiles Analysis Dibromofluoromethaue A Solid TCLP Volatiles Analysis Tetrachloroethene A Solid TCLP Volatiles Analysis Toluene -d8 A Solid 'TCLP Volatiles Analysis Trichloroethene A Solid TCLP Volatiles Analysis Vinyl chloride A NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Original #1 Page 10 of 24 a n ro ❑ Qo a a o ?; a v > v a" a n ro ❑ Qo a a a a a v > M N v � N � � N ❑ d N � N o � N o y N N m � c ❑ F n Q i d cJ � Z Z o o d a iD R_ in K m E a n � ❑ Qo a a a - a v > M N v � N � � K a d N � N o st ❑ Qo y N N m n � E F n Q i E cJ � 2 N = o d a iD R_ in ❑ ❑ E U " E � ~ Z� o y w bj= m ~ V 0 o 2 � W E Z J U E m m O U ~ aF� K 3 K d t= a n � ❑ Qo a a a - a v > M N v � N � � K Y d N a N o st ❑ Qo y J K m n � � F n Q i E cJ � 2 N � o m_ a iD ❑ in o Z E U " J � ~ Z� o y w Y n � ❑ Qo a o a C3 a a 46 M N v > N 5 � K ❑ � N J N o st ❑ Qo y E K m n � (n a Q i E cJ � 2 th ❑ o m_ a iD ❑ in U a E U " J � ~ Z� o y w bj= m ~ V 0 2 � W E Y n � ❑ Qo a o °' C3 a a 46 M N v > N 5 � K ❑ � N a N o � Y Qo y E K m n � (n a Q i E cJ � 2 d E o m_ a iD ❑ in U i E U " J � ~ a H y w bj= m ~ V 0 2 ❑ ❑ E Z U E m m O r4 ~ aF� K 3 d t= A o W LL1 J U U _ m E d Y n � ❑ Qo a o °' C3 a a - M N v > N 5 � K ❑ � N a N o � Y Qo y E a N m n � (n a Q i E cJ � 2 d o m_ a ❑ ❑ in U i E U " J � ~ a H y U a m ~ V 0 2 o E Z U CC) m m O r4 ~ aF� K 3 d t= Y n � ❑ Qo n � °' C3 a a 46 M N ❑ m N 5 � a ❑ ❑ J a N o � a Qo J E m m n � (n U Q i E m o 2 d o m_ a ❑ ❑ in U Q E U " J � ~ a H T U a m ~ V 0 2 o E Z U U E m O r4 E m K 3 d t= A W LL1 c r•� 0 Qo a a C3 a a 46 M N ❑ m N 5 � a ❑ ❑ J a N o � a Qo J E m m n � (n U Q r•� a Qo a a C3 a a 46 ❑ � N 5 fO ❑ � J a N o � a Qo J J m E n � F n e i E m o 2 d o m_ a ❑ ❑ in U Q r•� a Qo a a C3 a a 46 ❑ � N 5 fO ❑ � J a N o � a Qo F J m E n � F n a i > Z o 2 ai o m_ a ❑ ❑ m r•� a Qo a a 46 a a 46 ❑ � N 5 ❑ Y � J a ~ U ❑ a Qo F J m E O � F n m i > E = 2 ai o m_ a ❑ ❑ m Z E U " J � ~ a H T p a m o W 0 ❑ o E Z U U U J O r4 E � K 3 r•� a Qo a a - a a > 6 � N 5 ❑ Y � J a ~ U ❑ a Qo F J m O � F n m i > E I� 2 CO) o C a V m Z c U " J � ~ a H b p m � r•� a N w a M K O N 5 5 ❑ � J a ~ U ❑ Y F � m O � a` m C E I� m c ❑ o C a V m O c o = � m x b p m � W 0 ❑ o E Z U U w J O r4 E � m 3 d t= r•� r.. a o w a a L8 O > 5 5 ❑ � J a C ❑ Y F a y O � a` m C E I� m c ❑ C a � m c o = � m x m p � W 0 r.. a o w a L8 O > 5 5 ❑ � N a C Y F V y n a` m C E N to C � m 3 = � m x m p 0 0 o E Z U U w J O r4 ~ a 3 d t= A s,sq LL1 c U _ m r.. a o w a - O > 5 5 � N � C Y F V y n a` m C oJ N to C � m 3 � Q x m p � o o Z U U w J O r4 ~ a d t= r.. w 5 5 N C F V E m C to C � m 3 � Q C p o U who O r4 o d A s,sq LL1 c _ m E d m U Q r.. w 5 5 C a C C � m 3 � C p who r4 r.. w 5 5 C � m 3 � C p d s,sq c r.. ) ! [§m \ )/ � 46 �k\ (()� � \ ))»: \� r k \ \ ;\\{ (\\CY JE#! }a;7 }52 J)m@ ;»o» \ ) \/ \ ) ! \ a [§m \ )/ � 46 \ a [§m \ � 46 �k\ (()� ))»: \� k \ \ ;\\{ (\\CY JE#! }a;7 }52 J)m@ ;»o» \ ) \/ \ \ a [§m \ � �k\ (()� ))»: \� ;\\{ (\\CY JE#! }a;7 J)m@ \ a \ � (()� ))»: \� ;\\{ JE#! }a;7 J)m@ ;»o» \/ \ \ a \ � (()� ))»: ;\\{ JE#! }a;7 J)m@ ;»o» \ � - kr E \\:(\ \\\\\\\\ \ / )!, ) � )/ CD - kr E \\:(\ \\\\\\\\ \ / )!, ) � 4 CD \\� 03 (j\\ \ � k\ ; \\ \� ;\f« \ )§\� k\ \ \{ \� �\ \(\ b3 - kr E \\:(\ \\\\\\\\ \ / )!, ) � 4 CD \\� 03 (j\\ � k\ \\ \� ;\f« \ )§\� k\ \ \{ \� �\ \(\ b3 3j[) (45 \F \)(� \))\ \\k\ »G«± - kr E \\:(\ \\\\\\\\ \ / )!, ) � \\� 03 (j\\ � k\ \\ \� ;\f« \ )§\� E \{ \� �\ \(\ gE)s 3j[) \)(� \))\ - kr E \\:(\ \\\\\\\\ \ / ) � \\� 03 (j\\ \\ \� ;\f« \ )§\� - kr E \\:(\ \\\\\\\\ \ / ) � 03 (j\\ \\ \\ ;\f« \ )§\� - kr E \\:(\ \\\\\\\\ \ / j ) � (j\\ \\ ;\f« )§\� \{ \� �\ E»!§ gE)s 3j[) \)(� \))\ j \\ )§\� \{ \� �\ gE)s \j \)(� \\k\ »G«± ##2) =°Re )§\� \� �\ gE)s \)(� ')/\7 »G«± \ / ) / �)7 /) {\� }\\ \ kkj fe : { \\ \� \(\ 2\!! - ) 0_ �k\ \\\cy }(2 £E\\{\\ / ) / �)7 /) {\� }\\ kkj fe { \\ \� \(\ 2\!! - ) 0_ �k\ \\\cy }(2 £E\\{\\ \\ �{\ ){\: Ik:!! _;\ �k\ \\\{ \\< ${0 >m*= #2.2, =,ee \ �� }§! }( 0 £ �{\ :2:p / ) / �)7 /) {\� }\\ kkj fe { \\ \� \(\ 2\!! - 3\[) 0_ �k\ \\\cy }(2 £E\\{\\ \\ �{\ ){\: Ik:!! �k\ \\\{ \\< ${0 >m*= #2.2, =,ee \ �� }§! / ) / �)7 /) {\� }\\ kkj }\A { \\ \� \(\ 2\!! 3\[) �k\ \\\cy }(2 £E\\{\\ \\ �{\ ){\: Ik:!! \\\{ \\< ${0 >m*= #2.2, =,ee \ �� :2:p / (4 ! < / ) / �)7 /) {\� }\\ kkj }\A { \\ \� \(\ 2\!! 3\[) �k\ \\\cy }(2 £E\\{\\ \\ �{\ ){\: Ik:!! \\\{ / ) / �)7 /) {\� }\\ kkj }\A { \\ \� 2\!! 3\[) �k\ \\\cy £E\\{\\ \\ ){\: Ik:!! / ) / /) {\� }\\ }\A { \\ \� 2\!! 3\[) �k\ £E\\{\\ \\ ){\: Ik:!! \\\{ \\< ${0 >m*= / ) / /) }\\ }\A { \\ 2\!! 3\[) £E\\{\\ \\ ){\: Ik:!! \\\{ / \ ) / /) }\\ }\A { \\ 2\!! 3\[) \)(\ \\ \ /) }\\ \\ \/\\ \\ \\ ){\: \\\{ ${0 >m*= #2.2, =,ee }\\ \/\\ §\\ ){\: \\\{ >m*= �1 u N n m N rra Zit m W � a 0 o ❑ N a � U w` N N o m E a o Mo a C b m y n m N rra Zit g m W p ?� 0 o ❑ N a � U w` g m W U 0 O ❑ N a � � ` a o m E a N N C b J y a.� m E T Co 0 Q m E (n U Q m U N V .ro E P4 W d N. N C m p r a U U } o � p i m i v] m • x � a m � U Q a � d m W U 0 O ❑ N a � � ` a o m E a N N C b J y a.� m E T Co 0 Q m N U O ❑ N a � Hn ` ❑min o m v v N N m N U O ❑ N a � 0 N ❑min o m � o N U C b J y a.� ❑ U T E � m E (n U Q N U O ❑ N a � r t ❑min o m � o N N N U O N O � � eo � o m M v m p C b Q y a.� H U T E m N F m U N V .ro E P4 W d N. N C m p r a } � i m i v] • x � a � U Q N U O LO N eo p o m v v N N N O LO N eo p o m CL � 9 . C b Q y a.� a T C m U 3 V .ro E P4 W O N. � 9 . a.� a T m U 3 V .ro E m p r a i rri i v] . a.� a T op U V .ro m p r a i rri i v] • x � a a d \ \ a \, )/ \ a \, _)CNI \\� :! ly \\ )® k\\ )/ \{ \k \ \ a \, _)CNI \\� :! \\ )® k\\ )/ \{ \k \ \\ �\\ \\k) \\ \ \ a \, _)CNI \\� :! \\ )® )/ \{ \k \ \\ \\k) \\ \ ;,2 Lq /§ \ \ a \, _)CNI \\� :! \\ )® )/ \{ \\ \\k) \\ \ \ a \, _)CNI :! \ a 3 \ � \, :! \\ \{ \\ \\k) 3 \ � ; 3 � )3 / ; 3 � )) / \ \3 \ §� \) \� \\ \ ; 3 � )) / \ \3 \ §� \) \\ \ ; 3 � )) / \ \3 CL \) {\){ \\ $/() \)(/ w=:a \\\j ]!J: \ 0\ ; 3 � )) / \ \3 CL ; � )) \ \) {\){ \\ $/() \)(/ w=:a ; )) \) \\ \\\j ]!J: J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y va ca � w 0] � C N J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y va ca � w 0] � c� ci a� ❑ E K ❑ FT N ❑ � a a E n � N � � o a m � \ ❑ c J 0 U Q N z o z z o N N r J m 0 0 J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y ca � w 0] � a ci a� ❑ K ❑ FT E a � a ❑ E m � a � � o a m � \ � J 0 U Q N z o � = N N r J 0 0 E z 6 0 a - o ca J Q J a` a K 0 J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y ca � en 0] � a ci a� ❑ K J FT E ❑ � a ❑ E m � a � � o a m � r � a 0 U Q N z o � ❑ N " r J 0 a E z 6 0 > 3 ca 0a J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y J � en 0] � a a� ❑ K J FT t ❑ � a ❑ E m � a � � m � m � � r ❑ a 0 U Q N z o ` = N J 0 o E > 3 ca 0a J a` a W a � J Q W K J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y J � en 0] � a a� ❑ K J FT t ❑ � a d E m � m � � n ` m � � r ❑ a 0 U Q Z z o = N J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y J � en 0] � a� ❑ K ❑ FT t � a E m m � � in ` m E iDE 0 U Q = N 0 o E > 3 ca 0a J a` W J J J E - E - E - > > > L- N N W 7 K Z Y Y Y a a a � x s -o c > > c i U N d U N d o N d p Z o Z 90 Z CO � a F -M a Y J � en 0] � a� ❑ K FT t � a E m m � � in ` m n 3 J K � 2 � a U m K 3 J J g m � m E � m (q U Q m m Q � E m n O v N Gl m a E m � U Q 3 d ❑ n � N c d N z Z 49 ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W K 07 pj � a 9 m � � ` m E 0 U Q n 3 J K � 2 � a U m K 3 J J g m � m E � m (q U Q m m Q � E m n O v N Gl m a E m � U Q 3 d ❑ n � N c d N z Z 49 ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W K 3 J J g m � m E � m (q U Q m m Q � E m n O v N Gl m a E m � U Q 3 d ❑ n � N c d N z Z 49 ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W m m Q � E m n O v N Gl m a E m � U Q 3 d ❑ n � N c d N z Z 49 ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W 3 d ❑ n � N c d N z Z 49 ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W ❑ a w � _ E J N = m n � a` U Mo W K 0 N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W N E > Y � a � v � 9 — o > U N a o Z UIT cy CS i- o ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W ❑ m N K d FT r E m y 0 r UCy A 07 N U in U Q U ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W ICTN O gg W N C o" C5 n. q tb W O 04 w C p b b rva q ❑z a f4 ^ z W q tb W O 04 w C p b b rva q ❑z a f4 ^ z W w C p b b rva q ❑z a f4 ^ z W \ J s § ■ ) � }}j{ \))\ w::: ■ u� i v N qT - N m � N O O m N U W K � � O d v N n - � m � N n K � U W K � � d � v E m e � q _ ❑ v EmM x a C a ETis tb d U Q d m � o m � Ql K � ❑ N ❑ U V v N n - � m � N n K � U W v N n - � m n K � 6 J K � � d � m E m M � a ❑ EmM � a N a ETis d U Q v N n - � m � K � 6 J K � � d � E m M N EmM N a a r d tl m m Ql K � ❑ N ❑ U V J J N N (n U Q � o N n v < E m m in U Q v N n - � m � K � 6 � 0 � 2 E m M N N a a d tl u m Ql N ❑ N ❑ ❑ � N N N (n U Q v N � m N 0 E m N a tl N m ❑ � N N E o n v < % ] � za \ 0 / k ) (}$( )$&� tj)f EEl! 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UMMIT 3310 Win S[. FTfVIR4NhIENT4LTECHN0I,GGiE3,INC- Cuyahoga Falls, Ohio 44223 Sample Log -in Check List Anaryticirl Lahorafor7es TEL: (330) 253-8211 FLY (330) 253-4489 Website: hay11www.settek.com Client Name: SYN -NC -27028 Work Order Number: 18010668 RcptNo: 1 1/12/2018 12:20:00 PM Logged by: Antonio Betscakos , r Completed By: Antonio Betscakos 1/16/2018 2:32:22 PM Reviewed By: Chain of Custody 1. Is Chain of Custody complete? Yes J❑ No ❑ Not Present ❑ 2, How was the sample delivered? FedEx Log In 3. Coolers are present? Yes 0 No ❑ NA ❑ 4, Shipping container/cooler in good condition? Yes 0 No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present J❑ No. Seal Date: Signed By: 5, Was an attempt made to cool the samples? Yes W No ❑ NA ❑ 6, Were all samples received at a temperature of >0" C to 6.0°C Yes 0 No ❑ NA ❑ 7, Samples) in proper container(s)? Yes � No ❑ 1 6. Sufficient sample volume for indicated test(s)? Yes No ❑ g. Are samples (except VOA and ONG) properly preserved? Yes 0 No ❑ 10. Was preservative added to bottles? Yes ❑ No ❑ NA NA 11. Is the headspace in the VOA vials less than 114 inch or 6 mm? Yes ❑ No ❑ No VOA Vials ❑� 12. Were any sample containers received broken? Yes ❑ No J❑ 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes No ❑ 15. Is it clear what analyses were requested? Yes No ❑ 16, Were all holding times able to be met? Yes No ❑ (If no, notify customer for authorization.) Special Handling (if applicable) 17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑1 Person Notified: Date By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 16. Additional remarks: Cooler Information Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed By 1 4.5 Good Not Present Page 24 of 24 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Town of Yadkinville WQ Permit Number: W00001800 ( WWTP Name: Town of Yadkinville WWTP NPDES Number: NCO020338 Monitoring Period: From 01/01/18 To 12/31/2018 Pathogen Redaction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt. 4/1) (No Prior Test) Alt. 5/1rocess to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment _ Thermophilic Beta Ray Gamma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If a licable to alternative erformed Class Vector Attraction Reduction (40 CFR 503.33/I5A NCAC 02T.11 07) A or Class is corn fete tue touowm monuonn aara: Parameter Allowable Level in Sludge Pathogen DensityNo. of Excee- Frequency of Sample Type Analytical Technique Option/Alt. 7 Option/Alt. 8 Minimum Geo. Mean Maximum Units dances Analysis (Drying—Unstable) Option/Alt.9 Fecal 2x10 to the 6`h MPN <1149 <1207 <1316 MPN/g 0 Annual grab SM12210E Coliform power per gram of total solids CFU/g CFU 1000 MPN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) -Please indicate option/alternative performed: 0 tion/Alt. 1 Option/Alt.2 Option/Alt. 3 Option/Alt. 4 (VS reduction) X (40 -day bench) (30 -day bench) (Spec. 02 uptake) Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14 -Day Aerobic) (Alk Stabilization) (Drying—Stable) (Drying—Unstable) Option/Alt.9 Option/Alt. 10 (Iniection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction reduction requirement to 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note i£ you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnelproperly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Perry Williams Director of Public Works � r parer Name and T/iJtype or print) Q Land Appliex Name and Title (if applicable) (type or print) SignatuofPreparer* Date Signature of Lan *Prepazer is defined in 40 CFR Put 503.9(x) and 15A NCAC 2T.1102 (26) d Appliex (if applicable) Date Analytical Results Town of Yadkinville PO Box 816 Yadkinville, NC 27055 Receive Date: 02120/2018 Reported: 02122/2018 For: Holding Tank Comments: Geometric Mean <1,207 MPN/g Sample Numher .Parameter Sample ID Result Unit Method Analyzed Analyst 180220.16.01 Fecal Coliforms 1 <1316 MPN/g SM92210E,2" 02/21/2018 WC 180220-16-01 Percent Solids 1 1,52 % SM25648-1947 02/20/2018 WC 180220.16-02 Fecal Coliforms 2 <1170 MPN/g SM92=e,2005 0221/2018 WC 180220-16-02 Percent Solids 2 1,71 % SM2540B-1997 02/2012018 WC 180220-16-03 Fecal Coliforms 3 <1220 MPN/g SMMICE$ 6 02212016 WC 180220-1&03 Percent Solids 3 1.64 % SM25408-1947 02/202018 WC 180220-16-04 Fecal Coliforms 4 <1149 MPN/g SM9221EE-2006 02/212018 WC 1802201&N Percent Solids 4 1.74 % SM2540B-1997 021202018 WC 1 802 20-1 6.05 Fecal Coliforms 5 <1190 MPN/g sM922tcE-2995 02/21/2018 1VC 160220-16-05 Percent Solids 5 1.68 % sM25405-1991 02120/2018 WC 18022046.06 Fecal Coliforms 6 <1242 MPN/g SM92210E-2005 02/21/2018 WC 180220-16-06 Percent Solids 6 1.61 % SM25400.1997 02/202018 WC 180220-16-07 Fecal Coliforms 7 <1170 MPN/g SM92210E-2C05 02/21/2018 WC 180220-16-07 Percent Solids 7 1.71 %, SM25 001W 02120/2018 WC Respectfully submitted, Dena Myers NG Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 22$ •Statesville, NC 28687 •704J872J4697 Page 7 of 4 Condition of Receipt Sample Number 180220-16-01 Temp on Arrival; Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 180220-16-02 Temp on Arrival: Parameter Scheduler Percent Solids Received an Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 180220-16-03 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Scheduler Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 180220-16-04 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fewk Coliforms Sodium Thiosulfate Received on Ice Sample Numher 180220-16-05 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 180220-16-06 Tamp on Arrival: PO Box 228 • 5tatesville, NC 28687 + 704/872!4647 Page 2 of 4 Parameter Schedule; Percent Solids Received on Ice Parameter Schedule; Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 180220-16.07 Temp on Arrivah .�� Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiesulfate Received on Ice PO box 228 •Statesville, NC 28687 •704/872/4697 Page 3 oro �. i � .1 k9 m a m �� � $ m m m m m m S �, � �� g � � �i m �. � B. � a 6. C i�� g� g g \ ��.c Iii' III rn Q a p E m � � I z `��z I l �N-6W N._, D 3 3 3 3 Di 3 � 3 v - � Z ^ 1' �� �� � < ���� �_ � �_ z �� Quo aoo�� o�®Cd$a� _, a � t o� � � � g1° c m � m w 'c m f I � \ Ce � `C ` I I � � � � � i � 3 � 3 3 x � � R m `\� t � k �� k' I_ I� I � ��' J � � � � � w ` I` I €� � o � c � � 3 9 O 1 � D m � C Q H� � 1 y T 7�7 '� Jn�z C\ I � p -fin � 4' b ��j �° \ G �4 �� PQ Box 228 •Statesville, NC 28687 • 704/872/4fi97 Page 4 of 4 volatilesolidsxis 212106 % TOTAL SOLIDS % VOLATILE SOLIDS SM 2,540 G Analyzed By: h Calculated By. Date In 103105 oven: L7 {' i Date In 550 furnace: Z (�{Tf Time In 103-105 oven: i (1 Time in 550 furnace: i ,,,r, alfA Time Out 103-105 oven; r)—7� Time Out 550 furnace: �v Sample ID ISL ME INITIAL RAS 1 f INITIAL RAS (dup) D wt. . s 3 Dish wt. Dish wt. Sample vol. LStvti Sample VDI. Ts%j,� Ts% Dish # • P.I Dish # I D wt. `6�.l•�3 `s Ash wt. t 757 vs % 1 6 ° 171) Lk oivide Vs w %vofetde % rr , Sample ID FINAL j5-3� HoldingTank FINAL Holding Tank (dup) D wt. Dish wt. 5 Sample vol. LStvti Ts%j,� 3 y� Dish # D wt.3,..I Ash wt. `s vs % a iwde VS% by TS% %vowe V d S-!57. ffatlO[t %vowe Calculation for TS% and VS%: Dry wt. -Dish wt. X 100' . Uv -en Sample vol. U o RAGE: ,`1`i 15 FENAL VERAGE; j Qvteli USE INITIAL AND FINAL AVERAGES OF YOUR %VOLATILE FRACTION TO CALGULATE THE PERCENT REDUCTION (USE THE VAN KLEECK FORMULA) Van Kfeeck Reduction: initial °k voi. frac -Fina! °k val. frac. X 100 = reduction Initial %vol. frac. -(Initial %vof-fracx Final %vol. frac.) &,I 1.rj minus k O t G 1(3 I X100 = Gehl q l minus R G: times Gb(p'(('? A 6 L __7 (4f Do multiplication inside [{ )] before you subtract on twtom of equation. SECTION 6 Agricultural Lime Application Log i— Year: 2018 Project: Yadkinville Field (state -county -site -field) Soil pH (from Lime Requirement soil analysis) TonslAcre Applied Date Applied yk-08-01 5.1 1.4T/Ac. yk-08-02 6.0 O.OT/Ac. yk-08-03 5.7 0.71T/Ac. yk-08-04 6.3 O.OT/Ac. yk-08-6a 6.2 O.OT/Ac. yk-08-6b 5.7 0.5T/Ac. ** yk-09-01 5.9 0.8T/Ac. 1.5T/ac 06/18/18 k-29-1 5.8 0.3T/Ac. O.OT/Ac. O.OT/Ac. O.OT/Ac. * Lime will be spread when conditions improve SECTION 7 ^ oJro ? t N 0 N d o E 0 O Z Z z w N O0 o E Z Z z y W N O0 € C N Z z _ �NLL w m O N ro Co o Z ro N ro N ro N `m m O Z o Z o Z d 0 m"> O 0 O O O 3 O IDm p •p Lu U) N Q m r U U U w N o Q N o Q N p Q m Q m m m m m m a a 8 a (n 'yy V1 M N ro a a a r z rn Wiz' m Mz' rn .E = O K Z 0 o c m U 0] N i- (n 7 N M V7 ro a �• a U .. � N .. � N .. rn� a v v Z Z Z m N 0 N N (D N ro N N C ro a o 0 o C U C U U Z Z Z LU O _ co Z Y o n v E a E N o `" E N o " E N •- `" ro d J U J O J U N C C 0 C C1 o D O _ N 6. 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W U) U U W z o 0 m S f -'- m 0 Y L m 0 no O `� F- C O O m U U O O O E a ) a a x) x -o m c c v'o y m m U m cco m m U m m R CE E E 2 2 �WWWW, N OI 'Z c C C w v -a 0 w WE m 2' m m aEi c c o w ._ .t EE'c C Z E N rt) Z �'N.o E w c`o O Z w m 0) K O w m j oaaw S m o IWWWw r o L — a, oxi s a O L 7 O — a V) x u a m N 3N U) Z N x c m x U E 'N c WWW -c N N o4WWWW @ _o m w NE pTjaW 160 w m N a Q c c mWWWWWWW, y L 4:2 O c O�a L~ O w= U C CWP O 0 SO o 0o o Z W o 0 E - ° E .E 0 a .c M o (7 m cnar_ 'm0 �ac,� s3 m "--ah S c opt c O E c E m ya > - us_ mU) m U) p 01 E U h O C a C 'O p 'O E a V WO a ` m m a c 0 0 c N o O uE —_>o� E0 =rnc Wim¢ -oW 3 CWWWWWW O) G N N C O y M 0 l9 w N C 0 Z °� G - '0 0 `m v c Y a o 0 'c m r o y- w w N 'C- C c R E mm m >, 3' o (D CQ j aa) fn 7$ c w m �- 0 0 0 o R o cE E m aGi m w— +- E E L c w — c u a s U) 'u3 s _ > y m o m E w w E w- c R E R p -m.., _> y m v E E fa'� 3 o a m E a �',� U o ioo'w= a.E�ma m a cw mUZ � •Q CU m 3 R E o>� w N w m c N c o .0 -d vi o E m m N m a m o R (v N w R WWWWWW =) > C N V) Z� E w m m 0 m `0 QN E'WWWWJ- E �w aSa 0z- w WE 0 M Q >wm UUZ_)N !+I N a m VI V O m`OO�NO EO3 E a - ` m o E a. oE o Q. . N >G WE L WO WWWWWWvmO lR 0 W. 6 O , •Cq" E OZ( WW EWWWWWW o y m .WWW4 E 0 O RO 0w 0 .O 0� E O O Y 0 _ C O NE O . a o sO co moy m6 _°�°o° o a0oawo°om c m . E aa)) O w O 0 LO E E@ lw6 d UN m NU j WWWWN O w.0 o —E CL a N o N^ E WE b U '0 i N E 0 m N m y 0 5 N y O N k 2 0 a) T- N N p" a) m 0— m U y y U WE o 610 mo c rC ( �E c mY w o 0)a) o c •R w 3 0 0 L 00 4 0 >a v m(9 -o o '-0_ 0 a -Roc o w > o WWWWWW c w 4= o_ C m C O O m R (V m w m >' 3 m E "- 0 n 'o E o 0- 0 O) .::z mO > 0 0 o L v c m . _ N E O 0 0 o) E X L C �) m K m LZc `0 m� :E 0 m W. m �. m o' in m E 'm w E °:c E w m m m m R w o w 9 c c O m 0 .7 K � w- W- !`-) t� � co m 0 It c c c �' w E F I-