WQ0014885_Residual Annual Report 2018_20190314

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0014885
SUBMITTAL DATED: 2/27/2019
Project Contact Information
Hease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0014885
Permittee * HARNETT COUNTY
Facility Name * HARNETT COUNTY REGIONAL WTP
Phone Number*
443-489-9086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Hans, Specifications, Calculations, Etc.)
2018 ANNUAL REPORT FOR HARNETT COUNTY
18.35MB
WTP NC.pdf
Upoad only 1 HDF docurrent. NLltiple docurrents must be combined into one HJF file.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/27/2019

435 "I'illiams Court, Suite 100
Baltimore, ISD 21220
www synagro. coni
FEBRUARY 27, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 276994617
Re: 2018 Annual Report for Permit No. WQ0014885
Dear NCDEQ:
Enclosed are one copy and one electronic copy of the, above referenced report on behalf of
Harnett WTP Class A Residuals under Permit No. WQ0014885D
If you have any questions or comments, please contact Steve Ward at [phone] or Melinda
Boyd at [phone].
Sincerely,
DeYricl� Sllivar
Environmental Compliance Manager
Enclosures
cc: Steve Ward, Harnett County
Melinda Boyd, Synagro

HARNETT COUNTY WTP, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0014885
2018 ANNUAL REPORT

Harnett County WTP, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00014885 County Harnett Year 2018
Facility Name (as shown on permit) Harnett. County Utilities Regional WTP PWS ID No. 00-076-84
Land Application Operator Synaaro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO, If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 528.26
Total number of acres utilized for land application during the year: 154.60
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
143 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(6) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit werecomplied with (applicable to 40 CFR Part 503
regulated facilities).
_ 8. All monitoring and reporting requirements in 15A NCAC 02T.1 111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirementsin the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoringwell or explanations of violations are
attached to include appropriate actions and remediation.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge an elief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information,. including the p sibility of fines and imprisonment for
knowing violations."
Steve Ward Director of Public Utilities
Perm' ame Titer pe or t) Signature of Per itt Date
r
Signature of Prego �er* Dat Signam d Appli Date
(if different frot( Permittee) (if different from rmittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T.] 102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
HARNETT CO. UTILITIES, NC
HARNETT CO. UTIL., NC COH REGIONAL WP LIQUID
DRY METRIC
MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS
January 2018
1,091,200.00
G
40.95
D
37.14
February 2018
116981800.00
G
63.75
D
57.83
March 2018
11035,400.00
G
38.86
D
35.24
April 2018
8062000.00
G
30.24
D
27.44
May 2018
15233,800.00
G
46.30
D
41.99
June 2018
11537,600.00
G
57.70
D
52.34
July 2018
9301000.00
G
31.02
D
28.14
August 2018
11450,800.00
G
48.38
D
43.89
September 2018
111535200.00
G
38.48
D
34.90
October 2018
9235800.00
G
30.82
D
27.95
November 2018
211015800.00
G
70.11
D
63.59
December 2018
9481600.00
G
31.65
D
28.70
YEARLY TOTAL 14,911,000.00 G 528.26 D 479.15
vivzois

SECTION 2

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2037-01-WPL-NC
HARNETT CO. UTIL., NC COH REGIONAL
WTP LIQUID
1/16/2018
1/112018-613012018
1.1234
Na mg/I = (Na mglkg x %Solids) + 100 = (1810 x 0.9000) + 100 = 16.29
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (1080 x 0.9000) = 100 = 9.72
Mg mg/I = (mg mg/kg x %Solids) - 100 = (412 x 0.9000) + 100 = 3.708
Na meq = Na mg/I = Molec. Wgt. Na = 16.29 + 23 = 0.708261
Ca meq = Ca mg/I + Molec. Wgt.Ca = 9.72 + 20 = 0.486
Mg meq = Mg mg/I _ MolecWgt.Mg = 3.708 + 12 = 0.309
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.708261 = SgrRoot[0.5(0.486+0.309)] = 1.12337
Printed: 2/8/2019
Page 1 13:52

Waypoint ���
ANALYTICAL
7/17/2018
Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville, NC, 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypo intanalylica I. com
Ref: Analytical Testing
Report Number: 18-187-0208
Project Description: Harnett WTP
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 7/6/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were. performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2D12) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating fhe
analysis in question atlaboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
:;
Page 1 of 9

• ' `��
Waypoint `-
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Mein 804-743-9401 °Fax [phone]
www.waypo intanaly6ca Isom
Client: Synagro Central LLC/ Harnett CASE NARRATIVE
Project: Harnett VVTP
Lab Report Number: 18-187-0208
Date: 7/17/2018
Nitrate +Nitrite Nitrogen Method 4500NO3F-2011
Sample 61522
Analyte: NO3+NO2-N
OC Batch No: E64963
The MS/MSD recoveries are considered insignifcant due to the level of analyte present in the parent sample
relative to the spike level .RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Metals Analysis Method 6010D
Sample 61559
Analyte: AI
QC Batch No: L390694
MS and/or MSD spike recovery failed. Analyte concentration >25X the MOL. Dilution test within method limits.
No matrix interference is suspected.
Analyte: As
C2C Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Ca
OC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration >25X the MQL. Dilution test within method limits.
No matrix interterence is suspected.
Analyte: Cd
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Cr
QC Batch Nc: L390422
MS and/or MSD spike recovery failed. Analyte concentration >25X the MQL. Dilution test within method limits.
No matrix interterence is suspected.
Analyte: Cu
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interterence is suspected.
Analyte: Fe
QC Batch No: L390422
Page 2 of 9

WaypointN
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.way pointan al ytica I.co m
MS
and/or MSD spike
recovery failed.
Analyte concentration >25X the MQL. Dilution test within method limits.
No
matrix interference
is suspected.
Analyte: K
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration >25X the MQL. Dilution test within method limits.
No matrix interference is suspected.
Analyte: Mg
C2C Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration >25X the MQL. Dilution testwithin method limits.
No matrix interference is suspected.
Analyte: Mn
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration >25X the MQL. Dilution test within method limits.
No matrix interference is suspected.
Analyte: Mo
ClC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Na
QC Batch Nc: L390422
MS andlor MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Ni
CSC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyfe: P
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Pb
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: S
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MC3L. Post Digestion Spike within
method limits. No matrix interference is suspected.
Page 3 of 9

Wa oint
Y -ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743.9401 °Fax [phone]
www.way pointan al yti ca I. com
Analyte: Se
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Analyte: Zn
QC Batch No: L390422
MS and/or MSD spike recovery failed. Analyte concentration < 25X the MQL. Post Digestion Spike within
method limits. No matrix interference is suspected.
Page 4 of 9

Waypoi nt . 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-187-0208
Client Project Description: Harnett WTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61528
Harnett WTP
Solids
07/03/2018
12:30
07/06/2018
61528
Harnett WTP
Solids
07/03/2018
1230
07/06/2018
6010D
WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 5 of 9

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Waypoint. -�
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9901 °rax 804-271-6446
www.waypointana lyttca l.com
Cooler Receipt Form
Customer Number: 46460
Customer Name: Synagro Central LLC/ Harnett
Report Number: 18-187-0208
Shipping Method
O Fed Ex O US Postal O Lab O Other
UPS O Client O Courier Thermometer ID: �—
Shipping container/cooler uncompromised? � Yes O No
Number of coolers received r 1
Custody seals intact on shipping container/cooler? O Yes � No � Nat Required
Custody seals intact on sample bottles? O Yes O No � Not Required
Chain of Custody (COC) present? � Yes O No
COC agrees with sample label(s)? � Yes O No
COC properly completed � Yes O No
Samples in proper containers? � Yes O No
Sample containers intact? � Yes O No
Sufficient sample volume for indicated test(s)? � Yes O No
All samples received within holding time? � Yes O Nc
Cooler temperature in compliance? � Yes O No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved O Yes O No � N/A
Water -VOA vials free of headspace O Yes O No � N/A
Trip Blanks received with VOAs O Yes O No � N/A
Soil VOA method 5035 –compliance criteria met O Yes O No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low cone pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? Q Yes � No
Comments:
Signature: Brandi Watson � Date &Time: 07/06/201$ 13;14:02
Page 8 of 9

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2037-01-WPL-NC
HARNETT CO. UTIL., NC COH REGIONAL
WTP LIQUID
7/312018
7/112018-12131/2018
0.6769
Na mg/I = (Na mg/kg x % Solids) - 100 = (1410 x 0.8000) - 100= 11.28
Ca mg4 = (Ca mg/kg x %Solids) + 100 = (1230 x 0.8000) - 100 = 9.84
Mg mg/I = (mg mg/kg x %Solids) + 100 = (837 x 0:8000) _ 100 = 6.696
Na meq = Na mg/I + Molec.Wgt.Na = 17.28 +23 = 0.490435
Ca meq = Ca mg/I + Molec. Wgt.Ca = 9.84 + 20 = 0.492
Mg meq = Mg mg/I + Molec.Wgt.Mg = 6.696 + 12 = 0.558
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.490435 + SgrRoot[0.5(0.492+0:558)] = 0.676864
Printed: 2!8/2019
Page 1 13:52

Waypoint,�
ANALYTICAL
10/8/2018
Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville, NG, 27028
Ref: Analytical Testing
Report Number: 18-271-0205
Project Description: Harnett VVTP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.way pointa na IyNca Isom
Dear Mary Brewer:
Waypoint Analytical Virginia,. Inc. received samples) oh 9/28/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
v,�- K'�--i'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at /aboratory's expense, or the refund. of the charges paid for performance of said analysis.
Arizona A20629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
Y•:
Page 1 of 6

W^� /�®' �� M 7621 Whitepine Road, Richmond, VA 23237
QY Main 809.743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-271-0205
Client Project Description: Harnett WTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
62903
Harnett WTP
Solids
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
09/25/2018
14:30
09/28/2018
09/25/2018
14:30
09/28/2018
09/25/2018
14:30
09J28/2018
09/25/2018
14:30
09/28/2018
09/25/2018
14:30
09/28/2018
09/25/2018
14:30
09/28/2018
09/25/2018
14:30
09/28/2018
Page 2 of 6
SM-4500-NH3C-TKN WTN
4600NO3F-2011
WTN
6010D
WTN
SW -74716
WTN
9046D
WiN
SM-4500-NH3C
WTN

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Waypoint �����
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypoi ntana lyri ca I. tom
Cooler Receipt Form
Customer Number: 46460
Customer Name: Synagro Central LLC/ Harnett
Report Number: 18-271-0205
Shipping Method
O Fed Ex O US Postal (� Lab O Other: �i
UPS O Client � Courier Thermometer ID: �—
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received
Custodyseals intact on shipping container/cooler? O Yes O No � Not Required
Custody seals intact on sample bottles? O Yes O No � Not Required
Chain of Custody (COC) present? � Yes O No
COC agrees with sample label(s)? � Yes O No
COC properly completed � Yes O No
Samples in proper containers? � Yes O No
Sample containers intact? � Yes O No
Sufficient sample volume for indicated test(s)? � Yes O No
All samples received within holding time? � Yes O No
Cooler temperature in compliance? � Yes O No
Cooler/Samples arrived at the laboratory on ice. � Yes Q No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved O Yes O No � N/A
Water -VOA vials free. of headspace O Yes O No � N/A
Trip Blanks received with VOAs O Yes O No � N/A
Soil VOA method 5035 –compliance criteria met O Yes O No � N/A
High concentration container (48 hr) O Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low cont pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? O Yes t♦ No
Comments:
Signature; Brandi Watson � Date &Time: 09/28!2018 12:20:16
Page 5 of 6

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2037-01-WPL-NC
HARNETT CO. UTIL., NC COH REGIONAL
WTP LIQUID
9/25/2018
/ / - / /
1.6631
Na mg/I = (Na mglkg x %Solids) + 100 = (1560 x 5.0000) + 100 = 78
Ca mg/I = (Ca mg/kg x %Solids) - 100 = (1660 x 5.0000) - 100 = 83
Mg mg/I = (mg mg/kg x %Solids) + 100 = (1000 x 5.0000) + 100 = 50
Na meq = Na mg/I = Molec.Wgt.Na = 78 - 23 = 3.3913
Ca meq = Ca mg/I + Molec. W gt. Ca = 83 + 20 = 4.15
Mg meq = Mg mg/1 = Molec.Wgt.Mg = 50 + 12 = 4.16667
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 3.3913 + SgrRoot[0.5(4.15+4.16667)] = 1.66306
Printed: 2/8/2019
Page 1 13:52

("q
Waypoint °
ANALYTICAL
1/11/2019
Synagro Central LLC/ Harnett
Mary Brewer
County
284 Boger Road
Mocksville, NC, 27025
Ref: Analytical Testing
Report Number: 19-003-0203
Project Description: Harnett WTP #3
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypotnta n alytica I, com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 1/3/2019 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time..
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pauric McGrcary
Agronomist
Laboratory's liability in any claim relating to analyses pertormed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZ0629 New Jersey VA011 Pennsylvania 68-03109 Virginia 460014
Florida E871087 North Carolina 257 South Carolina 93007
;�,:
Page 1 of 6

Waypoi nt,, 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-003-0203
Client Project Description: Harnett WTP #3
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
64264
Harnett
WTP
#3
Solids
12/31/2018
15:00
WTN
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2018
15:00
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2018
15:00
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2016
15:00
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2016
15:00
01/03/2019
69264
Harnett
WTP
#3
Solids
12/31/2018
15:00
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2018
15:00
01/03/2019
64264
Harnett
WTP
#3
Solids
12/31/2018
15:00
01/03/2019
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 2 of 6
SM-4500-NH3C
WfN
9045D
WTN
4600NO3F-2011
WTN
6010D
WTN
SW -74718
WTN
SM-4500-NH3C-TKN
WTN
SM -2640G
WTN

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Waypoint.�®
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalyHca I. co m
Cooler Receipt Form
Customer Number: 46460
Customer Name: Synagro Central LLC/ Harnett
Report Number: 19-003-0203
Shipping Method
Fed Fac � US Postal � Lab � Other
UPS � Client � Courier Thermometer ID: ��®
Shipping container/cooler uncompromised? � Yes 0 No
Number of coolers received I '
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes � No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agreeswith sample label(s)? � Yes 0 No
COC properly completed � Yes � No
Samples in proper containers? � Yes 0 No
Sample containers intact? � Yes � No
Sufficient sample volume for indica#ed test(s)? � Yes � No
All samples received within holding time? � Yes 0 No
Cooler temperature in compliance? � Yes � No
Cooler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No � N/A
Water -VOA vials free of headspace � Yes � No � N/A
Trip Blanks received with VOAs � Yes � No � N/A
Soil VOA method 5035 —compliance criteria met � Yes � No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low cont pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson � Date &Time: 01/03/2019 13:50:40
Page 5 of 6

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Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date
Report Range
Ratio
2037-01-WPL-NC
HARNETT CO. UTIL., NC COH REGIONAL
WTP LIQUID
12/31/2018
/ / - / /
0.3552
Na mg/I = (Na mg/kg x %Solids) + 100 = (2480 x 0.2300) + 100 = 5.704
Ca mg/I = (Ca mg/kg x %Solids) - 100 = (5310 x 0.2300) + 100 = 12.213
Mg mg/I = (mg mg/kg x %Solids) - 100 = (1900 x 0.2300) - 100 = 4.37
Na meq = Na mg/I - Molec.Wgt.Na = 5.704 - 23 = 0.248
Ca meq = Ca mg/I - Molec.Wgt.Ca = 12.213 + 20 = 0.61065
Mg meq = Mg mg/I + Molec. Wgt.Mg = 4.37 - 12 = 0.364167
SAR = Na meq _ SgrRoot[0.5 x (Ca meq + Mg meq)] = 0.248 + SgrRoot[0.5(0.61065+0.364167)] = 0.355226
Printed: 2 /1 512 0 1 9
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HINUMMIT
FNVIRONIAEN1'AL TECHNOLOGIES, ING
Analytical Labmniorlea
February 27, 2018
Will Varner
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Harnett
smm�n7En,�ironmenm7Teohnologies,7 C.
3310 Win St.
Coyahoga Falls, Ohio 44223
TEL [phone] FAX: [phone]
Websile: hiln.,IA11 lu.sellek.eom
Dear Will Varner: Order No.; 18011117
Summit Enviromnental Technologies, Inc. received 2 samples) on 1/24/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
l�W)
Jennifer Woolf
Project Man
ager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 0725fiCA, Vol
Cormecticut PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C -OH -l3, Kansas E-10347, Kentucky (Undergound Stornge Tank) 3, KenNcky 90146, Louisiana 04061, Marylavd 339, Mimesota
409711, New Harnpshire 2996, New Iersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahonu 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas 1104704466-11-5, Utah OH0092320114, Virginia VELAP 9456., Washington
C891
Page 1 of 33
unless noted
in the
Case
Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
l�W)
Jennifer Woolf
Project Man
ager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 0725fiCA, Vol
Cormecticut PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho OH00923, Illinois
200061, Indiana C -OH -l3, Kansas E-10347, Kentucky (Undergound Stornge Tank) 3, KenNcky 90146, Louisiana 04061, Marylavd 339, Mimesota
409711, New Harnpshire 2996, New Iersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Oklahonu 9940, Oregon
OH2O0001, Rhode Island LA000317, South Carolina 92016001, Texas 1104704466-11-5, Utah OH0092320114, Virginia VELAP 9456., Washington
C891
Page 1 of 33

ffl������ Summa Environmental Technologies, fnc, 3310 Win St. Case Narrative
fNVlftoNMENTAL TFOHNOLOWEs, iNq. Cuyahoga Falls, Ohio 44223 WO#: 18011117
Anity0ca1 LAboratnrles TEL: [phone] FAX: [phone]
Website: htto.Vemno.settekcom Date: 2/2712018
CLIENT: Synagro
Project: Harnett
WorkOrder Narrative:
18011117: This report
in its entirety consists of the following documents: Cover Letter, Case. Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples
are reported
on an
"as received" or
"wet weight" basis unless indicated as
"dry weight" using the "-dry"
designation
on the
reporting units.
with this report are
This report is
Analytical
believed
to meet all of the requirements of the
accrediting agency,
where applicable. Any
comments or
problems
with the analytjeal events associated
with this report are
noted below.
Sequence Sample Notes:
18011117-002A SVOC-BNA_TCLP(8270D): Sample exhibited low recovery for Surrogate: phenol -d6
due to matrix effect.
Analytical Sequence QC Notes:
ccv 40ng S8- svoc-mstr_s(8270): CCV exhibited high recovery for Hexachloroethane. Associated
samples are ND for these analytes.
Original
Page 2 of 33

fnSU IEF SuninrrEmaronmentalYachnologres,In Qualifiers and Acronyms
3310 Win 6
rNigaONMENTAL I ECANOLOGIES, are Cuyahoga Falls, Ohio 442E WO#: 18011117
,hnalyPral taborawries TEL: [phone] FAX: [phone] Date: 2/27/2018
Website: httn://ivir settek.co
These commonly used Qualifiers and Acronyms may or may not be present in this report
QualiFers
U
This list
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response.
d
Manual integration in which peak was deleted
N
The result is presumptive based on aMass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GUMS.
X
The result was not confirmed when GC/MS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+),
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QN
The ICV recovery failed low (-) or high (+),
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimum Compound Limit
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
priginal
Page 3 of 33

SU
�� SummirEmdramnenraf'fechnolo0 Win St. Workorder
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 Sample Summary
A. dyflcal LaborffiorJes TEL: [phone] FAX.[phone] WO#: 18011117
Website: hthc.-/Avivw settek com 27-Feb-18
CLIENT: Synagro
Project: Harnett
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
18011117-001 WTP 1/16/201812:15:00 PM 1/24/201811:00:00 AM Sludge
W
18011117-002 WTP 1/16/20181:30:00 PM 1/24/201811:00:00 AM Sludge
Page 4 of 33

5ul"MI Summit Environmental Technologies,Inc. An`alytical Report
3310 Win SJ.
rNVIRONMEWALTECHNOLOGrEs, WC Cuyahoga Falls, Ohio 44223 (base report)
AnaryOral Laboratories TEL: [phone] FAX-: [phone] WO#: 18011117
Website: http://ivww.settek.coni Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 12:15:00 PM
Lab ID: 18011117-OOIA
Project: Harnett
Client Sample ID WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND 0.00200 mg/L 1 1/26/2018 4:25:00 PM
TCLP METALS, VOCs BNA, PEST,. HERB -SOLID SW6010D SW3010A Analyst: KMS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As) ND 0.500 mg/L 1 1/31/2018 1:15:19 AM
TCLP Barium(Ba) ND 5.00 mg/L 1 1/31/2018 1:15:19 AM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/31120181:15:19 AM
TCLP Chromium(Cr) ND 0.200 mg/L 1 1/31/2018 115:19 AM
TCLP Lead(Pb) ND 0.500 mg/L 1 1/31/2018 1:15:19 AM
TCLP Selenium(Se) ND 0.0500 mg/L 1 1/31/20181:15:19 AM
TCLP Silver(Ag) No 0.500 mg/L 1 1/31/2018 1:15:19 AM
TCLP METALS, VOC, BNA, PEST, HERBSOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
1,4 -Dichlorobenzene ND 0.0800 mg/L 2 1/30/2018 12:09:00 AM
2,4,5 -Trichlorophenol ND 0.200 mg/L 2 1/30/2018 12:09:00 AM
2,4,6 -Trichlorophenol ND 0.200 mg/L 2 1/30/2018 12:09:00 AM
2,4-Dinitrotoluene - ND 0.0400 mg/L 2 1/30/2018 12:09:00 AM
o -Cresol ND 0.200 mg/L 2 1/30/201812:09:00 AM
mlp-Cresol(s) ND 0,200 mg/L 2 1130/201812:09:00 AM
Cresols, Total ND 4.00 mg/L 2 1/30/2018 12:09:00 AM
Hexachloro-1,9-butadiene ND 0.0160 mg/L 2 1/30/2018 12:09:00 AM
Hexachlorobenzene ND 0.0400 mg/L 2 1/30/201812:09:00 AM
Hexachloroethane ND 0.0800 QC+ mg/L 2 1/30/201812:09:00 AM
Nitrobenzene ND 0.0800 mg/L 2 1/30/201812:09:00 AM
Pentachlorophenol ND 0.200 mg/L 2 1/30/201812:09:00 AM
Pyridine ND 0.200 mg7L 2 1/30/201812:09:00 AM
Sort: 2-Fluorophenol 25.6 10-109 % Rec 2 1/30/2018 12:09:00 AM
Sort: Phenol -d6 11.0 10-109 % Rec 2 1/30/2018 12:09:00 AM
Sort: Nitrobenzene -d5 54.4 19-120 % Rec 2 1/30/2018 12:09:00 AM
Sort: 2,416-Tribromophenol 28.9 10-120 % Rec 2 1/30/2018 12:09:00 AM
Sort: 2-Fluorobiphenyl 75.5 22-117 %Rec 2 1/30/2018 12:09:00 AM
Qualifiers:
'
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times f'or prepazation or analysis exceeded
M
Manual Integration used to determineazea response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 6 of 33

SUs", ", Ea ` o"a,en ° T noS2a , Win St
3310 Analytical Repo91 rt
FNVIRONRIENTAL IEGHNOLQGies, INC Cuyahoga Falls, Ohio 44223 (basereport)
Analytical tabaraY0Ne9 TEL: [phone] FAX: [phone] WO#: 18011117
Website: into /Amviv settek coin Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 12:15:00 PM
Lab ID: 18011117-001A
Project: Harnett
Client Sample ID WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
Surr: p-Terphenyl-d14 89.2 34-116 %Ree 2 1/30/2018 12:09:00 AM
NOTES:
CCV exhibited high recovery for Hexachloroethane. Associated samples are ND for these analytes.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total ND 0.0200 mg/L 2 1/29/2018 10:20:00 PM
Toxaphene ND 0.0400 mg/L 2 1/29/2018 10:20:00 PM
Endrin ND 0.00200 mg1L 2 1/29/201810:20:00 PM
gamma -BHC ND 0.00200 mglL 2 1/29/2018 10:20:00 PM
Heptachlor ND 0.00200 mg/L 2 1/29/2018 10:20:00 PM
Heptachlor epoxide ND 0.00200 mg/L 2 1/29/201810:20:00 PM
Methoxychlor ND 0.00200 mg/L 2 1/29/201810:20:00 PM
Surr: TCMX 56.8 10-119 %Rec 2 1/29/2018 10:20:00 PM
Surr: DCB 46.9 10 - 119 %Rec 2 1/29/2018 10:20:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW131118151)
214-D ND 1.00 mg/L 1 1/31/2018 5:44:00 PM
2,415 -TP ND 0.500 it mg/L 1 1/31/2018 5:44:00 PM
Surr.. DCAA 88.1 20-140 %Rec 1 1/31/2018 5:44:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.0500 mg/L 10 1/30/2018 5:10:00 PM
1,2-Dichloroethane ND 0.0500 mg/L 10 1130120185:10:00 PM
MEK ND 0.250 mg/L 10 1/30/2018 5:10:00 PM
Benzene ND 0.0500 mg/L 10 1/30/2018 5:10:00 PM
Carbon tetrachloride ND 0.0500 mg/L 10 1/30/2018 5:10:00 PM
Chlorobenzene ND 0.0500 mgrL 10 1/30/2018 5:10:00 PM
Chloroform ND 0.0500 mg/L 10 1/30/2018 5:10:00 PM
Tetrachlomethene ND 0.0500 mg/L 10 1130/20185:10:00 PM
Qualifiers: � Value exceeds Maximmn Contaminant bevel.
B Value above quantitation range
H Holdingtimes For prepazation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 7 of 33

prsummly Summit Ettvironmental Technol10 Wi SV.t. Analytical Report
33]0 Win St.
nM1VIRONhfENTAl 1fCHNtl L6Glfs, WCCuyahoga Falls, Ohio 44223 (basereport)
AnAytiaal Laboratories TEL: [phone] FAX: [phone] WO#: 18011117
Website: Into 11www settek com Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 12:15:00 PM
Lab ID: 18011117-OOIA
Project: Harnett
Client Sample ID WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Trichloroethene ND
Vinyl chloride ND
Surr: 4-Bromofluorobenzene 93.8
Surr. Dibromofluoromethane 106
Surr: Toluene -d8 93.6
RCI -SOLID -WI IG NITABI LITY1030
REACTIVE CYANIDE (901417.3.3.2) -SOLID
Cyanide, Reactive ND
SW8260B SW1377M Analyst: CTB
0.0500
mg/L
10
1/30/2018 5:10:00
MC
Value sueelow Minimum Compound Lunit.
PM
0.0200
mg/L
10
1/30/2018 5:10:00
RPD outside accepted recovery limits
PM
70 - 130
%Rec
10
1/30/2018 5:10:00
PM
70-130
%Rec
10
1/30/20185:10:00
PM
70 - 130
%Rec
10
113012018 5:10:00
PM
SW9014
Analyst:
MS
0.500 mg/Kg 1 1/30/20182:59:00 PM
RCI -SOLID -WI IGNITABILITY1030 SW1030 Analyst: AJT
IGNITABILITY OF SOLIDS (SW -846: 1030)
Ignitability non-flammable 1 1/25/2018 1:00:00 PM
RCI -SOLID -WI IGNITABILITY1030 SW9046D Analyst: DHC
PH (SW9045D)
pH 6.0 s.u.@18.5C 1 2/8/201811:41:00 AM
RCI -SOLID -W/ IGNITABILITY1030 SW9034 Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND 25.0 mg/Kg 1 1/30/20182:59:00 PM
Qualifiers: `
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value sueelow Minimum Compound Lunit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integrntion used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 33

SunEE mrit Envlronmenml Techno/agiesn St. AII'dlytlC`[Il ep
RlD
i.rt
3310 Wn St.
"VIHONMENTAL 1ECW40LOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
4nalyRrat Laticamiories TEL: [phone] FAX: [phone] WO#: 18011117
Website: him /hviviv settek cwn Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 1:30:00 PM
Lab ID: 18011117-002A
Project: Hamett
Client Sample ID W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM
TCLP MERCURY ANALYSIS (SW131117470)
TCLP Mercury ND 0.00500 mg/L 1 1/26/2018 4:27:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMS
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND 0.500 mg/L 1 1/31/2018 1:19:38 AM
TCLP Barium(Ba) ND 5.00 mg/l. 1 1/31/2018 1:19:38 AM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/31/20181:19:38 AM
TCLP Chromium(Cr) No 0.200 mg/L 1 ' 1/31/20181:19:38 AM
TCLP Lead(Pb) No 0.500 mg/L 1 1/31/20181: 19:38 AM
TCLP Selenium(Se) No 0.0500 mg/L 1 1/31/20181:19:38 AM
TCLP Silver(Ag). ND 0.500 mg/L 1 1/31/2018 1:19:38 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270)
1,4 -Dichlorobenzene ND 0.0800 mg/l. 2 1/30/201812:42:00 AM
2,4,5 -Trichlorophenol ND 0.200 mg/L 2 1/30/201812:42:00 AM
2,4,6 -Trichlorophenol ND 0.200 mg/l. 2 1/30/2018 12:42:00 AM
2,4-Dinitrotoluene No 0.0400 mg/L 2 1/30/2018 12:42:00 AM
o -Cresol ND 0.200 mg/L 2 1/30/2018 12:42:00 AM
m/p-Cresol(s) ND 0.200 mg/L 2 1/30/2018 12:42:00 AM
Cresols, Total ND 4.00 mg/L 2 1/30/2018 12:42:00 AM
Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 1/30/201812:42:00 AM
Hexachlorobenzene No 0.0400 mg/L 2 1/30/201812:42:00 AM
Hexachloroethane No 0.0800 QC+ mg/L 2 1/30/201812:42:00 AM
Nitrobenzene No 0.0800 mg/L 2 1/30/201812:42:00 AM
Pentachlorophenol No 0.200 mg/L 2 1130/201812:42:00 AM
Pyridine No 0.200 mg/L 2 1/30/201812:42:00 AM
Surr: 2-Fluorophenol 18.6 10-109 %Rec 2 1/30/2018 12:42:00 AM
Son: Phenol -d6 7.44 10-109 S % Rec 2 1/30/2018 12:42:00 AM
Son: Nitrobenzene -d5 48.5 19-120 % Rec 2 1/30/2018 12:42:00 AM
Surr. 2,4,6-Tribromophenol 19.0 10-120 % Rec 2 1/30/2018 12:42:00 AM
Son: 2-Fluorobiphenyl 64.2 22-117 % Rec 2 1/30/2018 12:42:00 AM
Qualifi
ers: ` Value exceeds Maximum Contaminant Level.
E Value above cumulation range
H Holding times for preparatien or analysis exceeded M Manual Integration used to determine area response
MC Value is below Mini mum Compound Limit.
ND Not Detected
P Second column confirmation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDlimlt
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 33

ffIUIT
S°""""F"";'o""e^la, eehaol10WinaeAnalyticalReport
33]0 W;n Sr.
FNVI801AL 3EC"NOLOGI, Cuyahoga Falls, Ohio 44223 (liase report)
Analytical Labora3urler. TEL: [phone] FAX: [phone] WO#: 18011117
Websne.: htro.'//ivunrvsertekeom Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 1:30:00 PM
Lab ID: 18011117-002A
Project: Harnett
Client Sample ID W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI-VOLATILES ANALYSIS (SW131118270)
Surr. p-Terphenyl-dl4 66.0 34-116 %Rec 2 1/30/2018 12:42:00 AM
NOTES:
CCV exhibitedhigh recovery for Hexachloroethane. Associated samples are ND for these analytes.
Sample exhibited low recovery for Surrogate: phenol-d6 due to matrix effect.
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8081 SW3510C Analyst: JBN
TCLP PESTICIDES ANALYSIS (SW131118081)
Chlordane, total No 0.0200 mg/L 2 1/29/2018 10:47:00 PM
Toxaphene ND 0.0400 mg1L 2 1/29/2018 10:47:00 PM
Endrin ND 0.00200 mg/L 2 1/29/2018 10:47:00 PM
gamma-BHC ND 0.00200 mg/L 2 1/29/2018 10:47:00 PM
Heptachlor ND 0.00200 mg/L 2 1/29/2018 10:47:00 PM
Heptachlor epoxide ND 0,00200 mg/L 2 1/29/201810:47:00 PM
Methoxychlor No 0.00200 mg1L 2 1/29/2018 10:47:00 PM
Surr. TCMX 61.4 10-119 %Rec 2 1/29/2018 10:47:00 PM
Surr. DCB 47.4 10-119 %Rec 2 1/29/2018 10:47:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8151A SW8151A Analyst: JBN
TCLP HERBICIDES ANALYSIS (SW131118151)
23¢D ND 1.00 d mg/L 1 1/31/2018 6:25:00 PM
21415-TP ND 0.500 d mg1L 1 1/31/2018 6:25:00 PM
Surr: DCAA 84.2 20-140 %Rec 1 1/31120186:25:00 PM
TCLP METALS, VOC, BNA, PEST, HERB-SOLID SW8260B SW1311M Analyst: CTB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.0500 mg1L 10 1/30120185:42:00 PM
1,2-Dichloroethane ND 0.0500 mg/L 10 1/30/2018 5:42:00 PM
MEK ND 0.250 mg/L 10 1/30/20185:42:00 PM
Benzene ND 0.0500 mg/L 10 1/30/2018 5:42:00 PM
Carbon tetrachloride ND 0.0500 mg/L 10 1/30/20185:42:00 PM
Chlorobenzene ND 0.0500 mg/L 10 1/30120185:42:00 PM
Chloroform ND 0.0500 mg/L 10 1/30/20185:42:00 PM
Qualifiers: ` Value exceeds Maximum Contaminant
Level.
H Holding tunes for preparation or analysis exceeded
E Value above quantitation range
M Manual Integration used to determine area response
MC Value is below Mmunum Compound Limit
ND Not Detected
P Second column confmnation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL
Permit Limit Original
RL Reporting Detection Limit
Page 10 of 33

EH y
U1%M11 Summit Em'ironmentol Technologies,Inc.
3370 Win C. Analytical Report
rN+41RONh1EN1'4L1ECAt10Lr3GIES, TNC Cuyahoga Falls, Ohio 44223 (base report)
AnaPyRcat Lahirarogaa TEL: [phone] FAX: [phone] WO#: 18011117
Website: h1&R.1Avuno.seue1c.com Date Reported: 2/27/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 1/16/2018 1:30:00 PM
Lab ID: 18011117-002A
Project: Harnett
Client Sample ID W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
Value exceeds Maximum Contaminant Level.
SW8260B
SW1311 M Analyst: CTB
TCLP VOLATILES ANALYSIS
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
Tetrachloroethene
ND
0.0500
mg/L
10
1/30/2018 5:42:00 PM
Trichloroethene
ND
0.0500
mg/l.
10
1/30/2018 5:42:00 PM
Vinyl chloride
ND
0.0200
mg/L
10
1/30/2018 5:42:00 PM
Surr: 4-Bromofluorobenzene
94.7
70-130
% Rec
10
1/30/2018 5:42:00 PM
Surr. Dibromofluoromethane
103
70-130
% Rec
10
1/30/2018 5:42:00 PM
Surr: Toluene -d8
93.9
70-130
% Rec
10
1/30/2018 5:42:00 PM
RCI -SOLID -W/ IGNITABILITY1030
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)SOLID
Cyanide, Reactive
ND
0.500
mg/Kg
1
1/30/2018 2:59:00 PM
RCI -SOLID -WI IGNITABILITY1030
SW1030
Analyst: AJT
IGNITABILITY OF SOLIDS (SW -846:1030)
Ignitability non-flammable
1
1/25/2018 1:00:00 PM
RCI -SOLID -W/ IGNITABILITY1030
SW9045D
Analyst: DHC
PH (SW9045D)
pH
7.4
s.u.@18.8C
1
2/8/201811:43:00 AM
RCI -SOLID -W/ IGNITABILITY1030
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive
30.0
25.0
mg/Kg
1
1/30/2018 2:59:00 PM
Qualifiers: `
Value exceeds Maximum Contaminant Level.
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 11 of 33

Sn,nnot Eneironinental Technolog es, Inc. Accreditation Program
frSUMMIT 3310 Win St. Analytes Report
rVlRONhIEN1'AL1cCHUOLOOlE5, INC Cuyahoga Falls, Ohio 44223 y P
Analytical LRbarntorons TEL: [phone] FAX: [phone] WO#: 18011117
Website: htto.-/Avivul settek. com 27-Feb-18
Client: Synagro State: NW
Project: Harnett Program Name: NC—WW—SCM
SampleID Matrix
Test Name
Analy[e
Status
18011117-OOIA Sludge
Ignitability of Solids (SW -846: 1030)
Ignitabdity
A
Sludge
pH(SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2) -Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide. (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis(SW1311/8151)
27435 -TP
A
Sludge
TCLP Herbicides Analysis(SW1311/8151)
2y1 -D
A
Sludge
TCLP Herbicides Analysis(SW1311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis(SW131116010)
Cadmium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
2,2',3,3',4,4',5,5',6,6'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
gamma -BHC
A
Sludge
TCLP Pesticides Analysis (SWI 311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SWI 311/8081)
Heptachlor epoxide.
A
Sludge
TCLP Pesticides Analysis(SWI 311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Tetrachloro-m-xylene
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Toxaphene
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
1,4-Dicldorobenzene
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,5 -Trichlorophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6 -Trichlorophenol
A
Sludge
TCLP Semi -Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi -Volatiles Analysis (SW1311/8270)
2-Fluorabipbenyl
A
Sludge
TCLP Semi -Volatiles Analysis(SWL311/8270)
2-Fluorophenol
A
Version #2
Page 12 of 33
Key
Key
NC
WW
SCM
A
Accredited
NC
WW
SCM
U
Unavailable.
Version #2
Page 12 of 33

M� SUMMIT Summit Environmental Technologies, Inc. ACCre(11tatI0II PPOgraID
33`OWin St.
Analytes Report
fNVIRONhIENTALTECtiNOLOCIES, We Cuyahoga Falls, Ohio 44223 J 1�
Anafykcal Lattoratartes TEL: [phone] FAX:: [phone] WO#: 18011117
Website: hrrp.11 vmw seaekcom 27 -Feb -18
Client: Synagro State: NW
Project: Harnett Program Name: NC—WW—SCM
Sample ID Matrix Test Name Analyte Status
18011117-OOIA Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Methylphenol A
Sludge TCLP Semi-VolatilesAnalysis (SW1311/8270) 3,4-Methylphenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270). Hexachlorobenzene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi -Volatiles Analysis (SW 1311/8270) Hexachloroethane A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene-dS A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Phenol -d6 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) p-Terphenyl-dl4 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-Dichlovoethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A
Sludge TCLP Volatiles Analysis Benzene A
Sludge. TCLP Volatiles Analysis. Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge. TCLP Volatiles Analysis Dibromofluoromethane A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Toluene -d8 A
Sludge TCLP Volatiles Analysis Trichloroethene A
Sludge TCLP Volatiles Analysis Vinyl chloride A
18011117-002A Sludge Ignitability of Solids (SW -846: 1030) Ignitability A
Sludge pH (SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2) -Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide,. Reactive U
Sludge TCLP Herbicides Analysis (SWI 311/8151) 22425 -TP A
Sludge TCLP Herbicides Analysis(SW1311/8151) 254-D A
Sludge TCLP Herbicides Analysis(SW1311/8151) DCAA A
Key Key
NC -WW -SCM A Accredited NC -WW -SCM U Unavailable
Version #2
Page 13 of 33

summit Environmental Technologies, Inc. ACereditation Program
SUMMIT 331oWinst. Analytes Report
I'MVIRONMENTAL rECHNOLOGiE51 Inc Cuyahoga FglIs, Ohio 44223
Analytical Laboratories TEL: [phone] FAX: [phone] W04: 18011117
Website: htto /Avrmv settekcoin 27 -Feb -18
Client: Synagro State: NW
Project: Hamett Program Name: NC—WW—SCM
Sample ID Matrix Test Name Analyte Status
18011117-002A Sludge. TCLP Mercury Analysis(SW1311/7470) Mercury A
Sludge TCLP Metals Analysis (SW1311/6010) Arsenio A
Sludge TCLP Metals Analysis (SW1311/60 10) Barium A
Sludge TCLP Metals Analysis (SW 1311/6010) Cadmium. A
Sludge TCLP Metals Analysis (SWI 311/6010) Chromium A
Sludge TCLP Metals Analysis (SW 1311/6010) Lead A
Sludge TCLP Metals Analysis (SWI 311/6010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver A
Sludge TCLP Pesticides Analysis(SW1311/9081) 2,2',3,3174,4',525,656'- A
Decachlorobiphenyl
Sludge TCLP Pesticides Analysis(SW1311/8081) Chlordane, total A
Sludge TCLP Pesticides Analysis (SW131 1/808 1) Endrin A
Sludge TCLP Pesticides Analysis (SWI 311/8081) gamma -BHC A
Sludge TCLP Pesticides Analysis (SW1311/808 1) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/808 1) I-Ieptaeldor epoxide A
Sludge TCLP Pesticides Analysis (SWI 311/8081) Methoxychlor A
Sludge TCLP Pesticides Analysis (SWI 311/8081) Tetrachloro-m-xylene A
Sludge TCLP Pesticides Analysis (SW1311/8081) Toxaphene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 1,4 -Dichlorobenzene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,5 -Trichlorophenol A
Sludge TCLP Seini-Volatiles Analysis (SW1311/8270) 2,4,6-Tribromophenol A
Sludge TCLP Semi -Volatiles Analysis (SW13l l/8270) 2,4,6 -Trichlorophenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorobiphenyl A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Fluorophenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Methylphenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 3,4-Methylphenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Cresols, Total A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachlorobenzene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Hexachlomethane A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene A
— Key Key
NC WW SCM A Accredited NC WW_SCM U Unavailable
V eYsion #2
Page 14 of 33

PO
Sunlit Environmental Technologies, Inc. Accreditation Program
SUMMIT 331°W"'S` AnalytesReport
fFlVIROMbIEN'I'AL7ECttt4OLOGlE5, INC Cuyahoga Falls, Ohio 44213 p
Analytical Laboratories TEL: [phone] FAX. [phone] WO#: 18011117
Website: gam.11wwivsettekcom 27 -Feb -18
Client: Synagro State: NW
Project: Harnett Program Name: NC—WW—SCM
Sample LD Matrix Test Name Analyte Status
18011117-002A Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Nitrobenzene -d5 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi-Volatfles Analysis(SW1311/8270) Phenol -d6 A
Sludge TCLP Semi- Volatiles Analysis(SW1311/8270) p-Terphenyl-d14 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Pyridine A
Sludge TCLP Volatiles Analysis 1,1-DieWoroethene A
Sludge TCLP Volatiles Analysis 1,2-1)ichloroethane A
Sludge TCLP Volatiles Analysis 2-13utanone A
Sludge TCLP Volatiles Analysis 4-13romofluorobenzcne A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenzene A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Dibromofluoromethane A
Sludge TCLP Volatiles Analysis Tetraehioroethene A
Sludge TCLP Volatiles Analysis Toluene -d8 A
Sludge TCLP Volatiles Analysis Trichloroethene. A
Sludge TCLP Volatiles Analysis Vinyl chloride A
Kcy Key
NC_WW_SCM A Accredited NC WW_SCM U Unavailable
Version #2
Page 15 of 33

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SUMMIT Summit Environmenta(Teehnolag(es. Inc.
3310 Win Sr.
rMVIROMMENTAL TECHMOLOCIES, SMO. Cuyahoga Falls, Ohio 44213 Sample Logon Check List
Anal yfrcal Laboraicines TEL: [phone] FAX. [phone]
Website: htto 11www.settek.com
Client Name: SYN -NC -27028 Work Order Number: 18011117 RcptNo: 1
Logged by: Christopher Livengood 112412018 11:00:00 AM
Completed By: Christopher Livengood 1/24/2016 4:12:50 PM
Reviewed By: Jennifer Woolf - 2 1126/2018 5:33:25 PM•'�^'�"
Chain of Custody
1. Is Chain of Custody complete? Yes No ❑ Not Present ❑
2, How was the sample delivered? FedEx
Log In
3. Coolers are present? Yes ❑ No ❑ NA ❑
4, Shipping container/cooler in good condition? Yes No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present❑
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes No ❑ NA ❑
6. Were all samples received at a temperature of >00 C to 6.0°C Yes No ❑ NA ❑
7. Sample(s) in proper container(s)? Yes © No ❑
8. Sufficient sample volume for indicated test(s)? Yes No ❑
9, Are samples (except VOA and ONG) properly preserved? Yes 0 No ❑
10. Was preservative added to bottles? Yes ❑ No ❑ NA ❑1
NA
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑ No ❑ No VOA Vials 0
12. Were any sample containers received broken? Yes ❑ No ❑�
13. Does paperwork match bottle labels? Yes ❑1 No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody? Yes R5 No ❑
15. Is it clear what analyses were requested? Yes No ❑
16. Were all holding times able to be met? Yes 0 No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA
Person Nobfied: Date
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
16, Additional remarks:
Cooler Information
p°
Cooler No Tem C Condition Seal Intact Seal No Seal pate Sig
red B
Y
1 5.1 Good Not Present _
Page 33 of 33

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name:
Harnett County
WTP
WQ Permit Number:
Frequency
Sample
W WTP Name:
Harnett County
Regional WTP
NPDES Number: _
Excee-
of
Monitoring Period:
From
01/01/18
To 3/31/18
WQ0014885
00-076-84
Pathogen Reduction (40 CFR 503s32/15A NCAC 02T.1106) - Please iudicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
.. A .. R\.. nle4e 4Rn inlln.n:nnm nifnvinn rin4n•
Parameter
Vector Att
Allowable Level in Sludge
Pathogen Density
No, of
Frequency
Sample
Analytical
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Excee-
of
Type
Technique
(Drying — Stable) _
(Drying—Unstable)
Minimum Geo. Mean Maximum Units
dences
Analysis
(Injection) _
Fecal
2x10 to the 6a'
CFU
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
1150
1150
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 NUN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: - N/A
Option/Alt 1
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40 -day bench)
(30 -day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying — Stable) _
(Drying—Unstable)
Option/Alt.9
Option/Alt. 10
(Injection) _
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I cert
ify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen reqquirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503:33/15ANCAC 02T.1107 have not been met" (Please note if you check this statement attach an
explanation why you have not. met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attracti
on reduction requirements have
been met. I am awaze that there are significant penalties for false certification including. fine and imprisonment."
Allan Rex O'Briant, WTP Su erintendent W V"
Pr d tit r yry L App lierIQaitjAnd Title
(if applicable) (type or print)
ignature of Preparer* at r Signature of Land Applier (if applicable) aDate
*Preparer is defined in CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report NC DENR#654
NC PHHS #37799
US EPA#NC01916
Client: Synagro=iTSfFojt _ 180080
Prdject: Harnett WTP LRegulator y vee
Sample Information
Sampled W. Varner Date 01/16/18 Received J. Zubeck Date 01/16/18
Analyses and Results
%Lab ID. , Sample ID - 0 8 Analyte Result C1 a � ,, ,�+, , Std. Methods
U
t7 i._. ,'P..,_'' r Reference
a
180080
01
#1
�wdgE
cr
Fec. Coliform -S
1150
MPNIg
10
01/16/18
ERP
9223 -MPN
Sludge
Sludge
Gr
TS ( %)
0.800%
%
O.o1
01116118
ERP
2540 G -TS
02
#2
iludgE
Gr
Fea
Coliform -5
683
MPNrg
+0
01!16118
ERP
9223-MPN
Sludge
Gr
TS (%)
0.770%
%
0.01
01116/18
ERP
2540 G -TS
Report
Review
Lab Director
219 S. Stcete Str.
Sanford NC 27330
Date
919-208-4240
chris�ucamerontes[in8.com

V
C

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WIT WQPermit Number: W00014885
WWTPName: Harnett County Regional WIT DES Number:
Monitoring Period: From 4/01/18 To 6/30/18
00-076-84
Pathogen Reduction (40 CFR 503.32/15A NCAC 021.1106) -Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt.l/A(time/temp)
Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/13 (No
Prior Test)
Heat Treatment
Alt.
5/Process to Further Reduce Pathogens Alt.
6 (Equivalent to PFRP)
If applicable to
alternative
performed
(Class A
only) indicate "Process to Further Reduce Pathogens":
Compost
lla ncaUe LU macAUuLivc cJ.". uacv ...wo0.�... ......... .. ....... ...... "W I.
Parameter Allowable Level in Sludge Path
Heat Drying
Heat Treatment
Thermophilic
Beta Ray
Gamma Ray
Pasteurization
Class B:
ogen Density
of
Alt. (1) Fecal Density
Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative
performed (Class B only)
indicate "Process to Significantly
Reduce Pathogens":
Lime Stabilization
Air Drying
Composting
Aerobic Digestion
Anaerobic Digestion
dentes
Analysis
.. ___.e__u_ ._ _..____.:_._
__-e,.......:d lln...... A ,.. cinvo
n\ e..."AaI rho fnnnwing monitoring dsts,
Vector Att
No.
Frequency
Sample
Analytical
ogen Density
of
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10to the 6`1
CFU
CFU/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
<87
<87
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 021.1107) -Please indicate option/alternative performed: - N/A
Option/Alt. 1
(VS reduction) (40 -day bench)
Option/Alt. 5
(14 -Day Aerobic)
Option/Alt. 9
(Injection)
ption/Alt.
O 2
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
STATEMENT (please check the appropriate statement)
ption/Alt.
O 3 Option/Alt. 4
(30 -day bench) (Spec. 02 uptake)
Option/Alt. 7 Option/Alt. 8
(Drying—Stable) (Drying—Unstable)
No vector attraction reduction altern
atives were performed
"I certify, under penalty of raw, that the pathogen requirements in 40 CFR 503.32/1 SA NCAC 021.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 021.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.) — See Tab 91
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certificatiioo(n� including fine and imprisonment."
AILan Rex O'Briant, WTP 5u erintendent 1 Y W`th'd`O�- 1Sn 1 C% e C�
PrZr(V
e txyp' L Applier N d itle (if applicable) (type or print)
�
a, �' M W a�
ignature of Preparer* D Signature of Land Applier (if applicable) Date
*Preparer is defined ' 40 CFR Part 503.9(r) and 15A NCA 2T. 1102 (26)

Cameron Testing Services, Inc. Laboratory Report
Synagro tlTs Wr j
t Harnett WTPRegulatory
Sample Information
180625
Yes
apYpe ,
Fecal2
W, Varner
__Batu
04112118 Recelvec{
J. Zubeck
Coliform -S
<gD
MPNIB
tc
04/13/18
ERP
1$0625
D1
Fecal1
1wdeE
cr
Fee.
Coliform -S
<$�
Mr+Nio to
Analyses
and Results
9223-MPN
ERP
2540 G -TS
l
cr
NC DENR #654
NC PHHS #37799
US EPA#NC01918
-;bate�; 04/12/18
02
Fecal2
iwaoc
cr
Fec.
Coliform -S
<gD
MPNIB
tc
04/13/18
ERP
1$0625
D1
Fecal1
1wdeE
cr
Fee.
Coliform -S
<$�
Mr+Nio to
04/13/18
ERP
9223-MPN
ERP
2540 G -TS
sWdoe
cr
TS (%)
2.D6%
o.m
04/13/18
ERP
2540 G -TS
02
Fecal2
iwaoc
cr
Fec.
Coliform -S
<gD
MPNIB
tc
04/13/18
ERP
9223-MPN
swne�
cr
TS (%)
2.24%
°�
c.ot
04!13/18
ERP
2540 G -TS
Review 7 / �P
Pr ject Manager Date
219 S. Steele Str. 919-2UK-4240
Snnf'ord NC 27330 chris�cameronlesting.com

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett County WTP WQ Permit Number: W00014885
W WTP Name: Harnett County Regional WTP NPDES Number.
Monitoring Period: From 07/01/18 To 09/30/18
00-076-84
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Tes0ng
Alt. I/A (time/temp)
Alt 2/B (A0c Txeabnem) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost
Beta Ray
Class B:
Alt. (1) Fecal Density
amma Ray
HeatDrying
G
Heat Treatment
Pasteurization
Alt (2) Process to Significantly Reduce Pathogens
Thermophilic
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
.. A �..l�I.,�eR\..n...nlnfn 4ha fnllnwina mnniFnrin"dAtA:
lla nl:AnlG
Vector Attraction Reduction (40 CFR 503.33/I5A NCAC 02T.1107)
l.n illl.ci uuurc ci iv�u...0 •..uw
in Sludge
n... ....+....-� -..... ._-_--.-__.._.. _._ .._________
Pathogen Density
No. of
Frequency
Sample
Analytical
Parameter
Allowable Level
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying—Stable)
(Drying—Unstable)
Option/Alt. 9
(Injection)
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6"
CFU
CFU/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 NIPper gram of
<208
<208
CFU/g
0
4/yr
Grab
9222D
total solids (dry weight)
Salmonella
3 MPN per 4grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
CERTIFICATION STATEMENT (please check the appropriate statement)
`T certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in
40 CFR 503.33/ISA NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement 1n 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification me oiling fine and imprisonment." .}-
AllanRexO'Briant WTP Superintendent IYx C\A& � 1�0�� IfC �K<,ZMtk_
Prep itle ( to Land
�A�pp�liiee�r�Name and Tiff (if applicable) (type or print) ja��
nature of Preparer* D Signature of Land Applier (if applicable) Date
*Preparer is defined in 4 FR Part 503.9(r) and 15ANCAC 2T.1102 (26)
-Please indicate option/alternative
performed: - N/A
Option/Alt. 1
(VS reduction)
Option/Alt 2
(40 -day bench)
Option/Alt. 3
(30-daybench)
Option/Alt. 4
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying—Stable)
(Drying—Unstable)
Option/Alt. 9
(Injection)
Option/Alt. 10
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
`T certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in
40 CFR 503.33/ISA NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement 1n 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification me oiling fine and imprisonment." .}-
AllanRexO'Briant WTP Superintendent IYx C\A& � 1�0�� IfC �K<,ZMtk_
Prep itle ( to Land
�A�pp�liiee�r�Name and Tiff (if applicable) (type or print) ja��
nature of Preparer* D Signature of Land Applier (if applicable) Date
*Preparer is defined in 4 FR Part 503.9(r) and 15ANCAC 2T.1102 (26)

Cameron Testing Services, Inc. Laboratory Report
Client: Synagro CTS Proj,
Project: Harnett WTP- Class A Fecal Regulatory
Sample Information
Sampled M. Boyd Date 07/03/18 Received
Analyses and Results
NC DENR #654
NC PHHS #37799
US EPA #NC01918
181136
as
J. Zubeck Date 07/03/18
N
Lab ID Sample ID e N Analyte Result v ,E = 6 4 Std. Methods
V c o = Reference
181136
01
swage
cr
Fec.
Coliform -S
<208 MPN/g
io
07/04/18
ERP
9223 -MPN
Sludge
Gr
TS (%)
0.865%
c.m
07/04/18
ERP
2540 G -TS
Review
Project Manager
Date
219 S. Stcele Str. 919-208-4240
Samford NC 27330 ehris©camerontesting.com

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Harnett. County WTP WQ Permit Number: W00014885
W WTP Name: Harnett County Regional WTP NPDES Number: 00-076-84
Monitoring Period: From 10/01/18 To 12/31/18 _.
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A: Fecal Coliform Testing
Alt. 1/A (time/temp) _ Alt. 2/B (Alk Treatment) _ Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Processto Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying _ Heat Treatment Thermophilic
Beta Ray _ Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If a licable
Vector Att
to alternative
erformed Class
A or Class B corn rete the touowm monrtor�n
Pathogen Density
ua�a:
.
Exeee-
Frequency
of
Sample
Type
Analytical
Technique
Parameter
Allowable Level in Sludge
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
CFU
CFU/g
Coliform
power per gram
of total solids
CFU
CFU/g
—Grab
1000 MPN per gram of34100
34100
CFU/g
0
4/yr
9222D
total solids (dry weight)
Salmonella
3 WN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed: - N/A
Option/Alt. 1
(VS reduction)
Option/Alt. 5
(14 -Day Aerobic)
Option/Alt. 9
(Injection)
Option/Alt. 2
(40 -day bench)
Option/Alt. 6
(Alk Stabilization)
Option/Alt. 10
(Incorporation)
CERTIFICATION STATEMENT (please check the appropriate statement)
ption/Alt.
(30 -day bench)
O 3
Option/Alt. 7
(Drying— Stable)
Option/A1t. 4
(Spec. 02 uptake)
Option/Alt. 8
(Drying—Unstable)
were
performed
No. vector attraction reduction alternatives
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/ISA NCAC 02T.1106 and the vector attraction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 at) vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for f Ise certificat/ifo�n'j including fin�eT and imprisonment."
Allan Rex O'Briant WTP Su endent
Pre r n e (ty e n + Land Applier Name ard Title (if applicable) (type or print) 1
LoWg'nature ofPreparer* ay Signature Applpplicable) Date
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCA 2T,1102(26)

Cameron Testing Services, Inc. Laboratory Report
Client: Synagro CTS Proj.
Project: Harnett WTP Regulatory
Sample Information
Sampled M. Boyd Date 12/18/18 Recelved
Analyses and Results
NC DENR #654
NC PHHS #37799
US EPA #NC01918
182204
Yea
M. Slms Date ' 12/18/18
CL a N
Lab ID Sample IDU Analyte Result ME_E o Std. Methods
ar Reference
1822174 01 Harnett VVrP Smdge Or Fec. Coliform -S 34100 MPNrg m 12/19/18 ERP 9223-MPN
Sludge Or TS (%) 0.410% % 0.0 12/19/18 ERP 2540 G -TS
Report -/
Review /A/ C5111 4
Project Manager Date
219 S. Steele Str. 919-208-4240
Snnford NC 27330 chris�cameron(csling.com

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