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HomeMy WebLinkAboutWQ0005135_Residual Annual Report 2018_20190314INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0005135 SUBMITTAL DATED: 2/27/2019 Project Contact Information Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Robert T. Branch Email Address* bbranch@branchrs.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0005135 Permittee * Von Drehle Corporation Facility Name * Von Drehle Corporation Cordova, NC Phone Number* 336 312-9007 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Rans, Specifications, Calculations, Etc.) VD DEQ 2018 Class B ar.pdf 5.09MB upload only 1 RDF docurrent. IVUltiple documents must be corrbined into one RDF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/27/2019 2018 ANNUAL REPORT VON DREHLE CORPORATION CLASS B CORDOVA, NORTH CAROLINA PERNUT #WQ0005135 Prepared For: Von Drehle Corporation 126 First Street Cordova, North Carolina 28330 Prepared By: Branch Residuals & Soils, LLC 8646 West Market Street- Suite 111 Greensboro, North Carolina 27409 February 2019 BRANCH RESIDUALS & SOILS, LLC 8646 W. Market St. — Suite 111 • Greensboro, NC 27409 PHONE (336) 510-0340 • Fax (336) 510-0341 February 26, 2019 North Carolina Department of Environmental Quality Division of Water Resource — Non -discharge Permitting Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Reference: 2018 LAND APPLICATION ANNUAL REPORT Von Drehle. Corporation Cordova, North Carolina Permit No. WQ0005135 Branch Residuals & Soils Project No. 2014-110 Information Processing Unit: Branch Residuals & Soils is submitting all monitoring and reporting information as required in the referenced permit on behalf of the Von Drehle Corporation. This data includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Reduction Forms, 8) Fecal and Salmonella Results, 9) Soils Lab Data, 10) 2018 Application Summary Table, and 11) 2018 Application Condition Summaries. Total production for 2018 was 6,379.88 wet tons for this facility. Disposal/applications were as follows: • 2,912.98 wet tons being sent to the landfill, • 28,718.77 wet tons sent for application in South Carolina under Belger farms permit • 643.94 wet tons applied as Class A under separate permit, and • 31,517.19 wet tons applied to the farms in North Carolina. A total of 31,517.19 wet tons (11,667.38 dry tons) of residual by-product paper were land applied to the farms at US and Hamlet (432.65 acres). Hamlet sites received 60 lbs/acre nitrogen topdressing in March 2018. The US -1 site received 25 lbs/acres nitrogen, 12 lbs/acres Manganese, and 2 lbs/acre iron in August 2018 for the soybean crop. Soybeans were planted on the US -1 site in July. If any further information is required regarding this land application program, please do not hesitate to contact me at (336) 312-9007. Sincer , Robert T. Branch, L.S.S. Land Application/Residuals Operator #15676 RTB Attachment M. Von Drehle Corporation TABLE OF CONTENTS SECTION NO. TITLE I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary Forms V Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Forms VIII Fecal and Salmonella Documentation and Results IX Soil Analysis Reports X 2018 Application Summary Table XI 2018 Application Condition Summaries CERTIFICATION FORM ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0005135 County: Richmond Year: 2018 Facility Name (as shown onpermit): von Drehle Corporation Land Application Operator: Belger Farms Phone: (803) 424-4731 Land application of residuals as allowed by the permit occurred during the past calendar year? ❑ Yes p No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in thepermit: 18 Total number of fields utilized for land application during the year: 18 Total amount of dry tons applied during the year for all application sites: 11,667.38 Total number of acres utilizes for land application during the year: 432.65 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. C7 Yes '' No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Mr. Justin Dawkins, Cordova Plant Manager Permittee Name and Title (type or print) 2G � S' tore of ttee bate Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (1212006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM �4 a U O O U �5 a O � � W a A 3w a N b •r b O R 6t V V N ¢ z O o C� M V Ln M_ O O O U to I.., 4� ej a.. id c O O 0 O O A U � a � r V (ey N O V U O N O � � W a A 3w a 6 0 O gD O N b •r b O R 6t V V N ¢ z O o 09 M M V CD O O W R cc r.+ O � I.., 4� ej a.. id c O O O O y � r V (ey N O V O O N Q �-" h V ~O V V O [n C (V O V 00p � M n r h 00 00 V G � O A N tg o r- or d o°°a civ r- rr+, a C 0 a M o o DO IR O r- V p \ N U O 0 00 Nd' N � cn V T m_� V O z V V1 N OV V M V M V O e N OV e l04 M 00 h V N 00 c, z v o N n v M N� CD o to ti �. by Q kn CD �z� O O O o Q Q Q v�az 6 bA y �t U ro ca � O 6 0 O gD O •r b O R r 6� v d iri CU CD 41 46, 20 4i W R cc r.+ O � I.., 4� ej a.. id c O O O O y � y iM .o 41 co N N_ LL N O LL Of Z W iri y CD W R cc r.+ O � y � PC .o pa 42 � O � G � O tg r 'O ;v p � o cu co N N_ LL N O LL Of Z W ANNUAL METALS FIELD LOADING SUMMARY FORMS ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 613.78 n/a WcB 22.8 Acres Permitted: 22.8 Site #: 3 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-3 MB 2018-4 MB Sample or Com- posite Date 5/29/18 7/10/18 % Solids 40.40 29.10 Arsenic 3.39 2.08 Cadmium 0.34 0.17 Chromium 0.00 0.00 Copper 5.18 9.07 Lead 3.39 0.88 Mercury 0.24 0.23 Molyb- denum 3.39 3.47 Nickel 1.35 1.97 Selenium 3.39 0.94 Zinc 40.50 133.00 Total Phos- horus 0 11 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 143.64 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB Acres Used: 9.3 Acres Permitted: 9.3 Site #: 3 Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): ,a ?n 1 R -A MR .i 1Non monsoons • t t t _---__-____ i t t Total Phos- phorus,00MENEEMENEE Annual Heavv Metal Field Loadings Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including gtthe possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) • t t t _---__-____ i t t Total Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including gtthe possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 427.30 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB Acres Used: 13.2 Acres Permitted: 13.2 Site #: 3 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-3 MB 2018-4 MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): � 1 Tolal, h 1 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of flues and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) � 1 Total ' . 11 M 1'. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of flues and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): 210.45 WQ0005135 Cation Exchange Capacity (non 503 only): n/a von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series WcB 11.1 Acres Permitted: 11.1 Site #: 3 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 20184 MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): i ® Total Phos- phorus s. . Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) Total Phos- �, 1• .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 582.53 n/a WcB 18.9 Acres Permitted: 18.9 Site #: 3 Field #: 3A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): A 2018-3 MB 20184 MB � +u ' : 1 Total Phos- phorusiMENEEMENEENE Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.2 Acres Permitted: 37.2 Site #: 3 Field # 1,346.62 n/a WcB 3B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-3 MB 20184 MB � �u Total Phos- • • rusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" c d-- Signature of Land Applier _ ZG.I5 Date Author Daryl D. Merritt DENR FORM MFLSF (712002) Total ' • 1 1 1 .ENEENEENEE i . • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" c d-- Signature of Land Applier _ ZG.I5 Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 24.6 Acres Permitted: 24.6 Site #: 3 Field #: 664.19 n/a WcB 6A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent ft vd 20194 MB Sample or Com- 7/10/18 posite Date % Solids 29.10 Arsenic 2.08 Cadmium 0.17 Chromium 0.00 Copper 9.07 Lead 0.88 Mercury 0.23 Molyb- 3.47 denum Nickel 1.97 Selenium 0.94 Zinc 133.00 Total Phos- 11 horus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" ;2_�- 2G- g Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) 11 Total Phos - 1 1 + "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" ;2_�- 2G- g Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.5 Acres Permitted: 37.5 Site #: 3 Field #: 829.18 n/a WcB 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-4 MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): f Total . 1 1 —ruSENEEMENEENER Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" (2= ��2-- Signature of Land Applier Author Daryl D. Merritt Z-'�S,jg Date DENR FORM MFLSF (712002) 1 . � 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" (2= ��2-- Signature of Land Applier Author Daryl D. Merritt Z-'�S,jg Date DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual) WQ0005135 Cation Exchange Capacity (non. 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 19.1 Acres Permitted: 19.1 Site #: 4 Field #: n/a TbB 509.50 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-1 MB 2018-2 MB �r Mull Total Phos- phorusEENEENEENEEN Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" CC, I `Z` d----_ z.-2- 1�--^ Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 37.4 Acres Permitted: 37.4 Site #: 4 Field #: 901.61 n/a TbB Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-2 MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- phoruSEENEENEEMENE Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 2 Z C, -,.E Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) Total Phos - 1 1 " "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 2 Z C, -,.E Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 634.41 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series ThA Acres Used: 22.4 Acres Permitted: 22.4 Site #: 4 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Yd 2018-1 MB Sample or Com- 1126118 posite Date % Solids 45.00 Arsenic 0.02 Cadmium 0.00 Chromium 0.00 Copper 8.06 Lead 0.79 Mercury 0.55 Molyb- 1.47 denum Nickel 0.00 Selenium 0.01 Zinc 30.10 Total Phos- 1 porus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier 'k 2 G -/C7 Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) Total Phos- 11' 14 phorus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier 'k 2 G -/C7 Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 1,468.05 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series ThA Acres Used: 53.15 Acres Permitted: 53.15 Site #: 4 Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-1 MB 2018-2 MB ample or Com- posite Date 1126118 3114118 % Solids 45.00 38.90 Arsenic 0.02 0.84 � Cadmium 0.00 0.00 Chromium 0.00 0.00 Copper 8.06 10.70 Lead 0.79 1.04 Mercury 0.55 0.76 Molyb- denum 1.47 4.44 Nickel 0.00 1.11 Selenium 0.01 0.13 Zinc 30.10 73.20 Total Phos- horus 1 5 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) - s � Total • 1 1 1 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 277.50 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series ThA Acres Used: 11.1 Acres Permitted: 11.1 Site #: 4 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-2 MB Annual HeavV Metal Field Loadings Calculated in lbs/acre): NMI • � 1 11 __-_-__-___ 1 11 Total Phos- phorusEENEENEENEEN Annual HeavV Metal Field Loadings Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) NMI • � 1 11 __-_-__-___ 1 11 Total Phos- phorusEEMENEEMENEEM. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 566.20 n/a ThA 19.2 Acres Permitted: 19.2 Site #: 4 Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-1 MB Sample or Com- 1126/18 posite Date % Solids 45.00 Arsenic 0.02 Cadmium 0.00 Chromium 0.00 Copper 8.06 Lead 1 0.79 Mercury 0.55 Molyb- 1.47 denum Nickel 0.00 Selenium 0.01 Zinc 30.10 Total Phos- 1 horus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) Phos- phorus r "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: von Drehle Corporation Total Dry Tons Applied (Annual): 716.56 Permit #: WQ0005135 Cation Exchange Capacity (non 503 only): n/a Operator: von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series TbA Acres Used: 289 Acres Permitted: 28.9 Site #: 4 Field #: 8 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-1 MB 2018-2 MB Sample or Com- posite Date 1/26/18 3/14/18 % Solids 45.00 38.90 Arsenic 0.02 0.84 Cadmium 0.00 0.00 Chromium 0.00 0.00 Copper 8.06 10.70 Lead 0.79 1.04 Mercury 0.55 0.76 Molyb- denum 1.47 4.44 Nickel 0.00 1.11 Selenium 0.01 0.13 Zinc 30.10 73.20 Total Phos- horus 1 5 Annual Heavy Metal Field Loadings Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" ( ?/, j: - Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) Total ' 1 11 1 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" ( ?/, j: - Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (7/2002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 28.6 Acres Permitted: 28.6 Site #: 4 Field #: 731.98 nla TbA 9 Residual Analysis Data (Heavy Metals and Total Phosphorus use mglkg, % Solids use Raw Percent #): vd 2018-2 MB r ' r ru r• ' Total Phos- . r Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier 2 —zc it Date Author Daryl D. Merritt DENR FORM MFLSF (712002) Total ' r 1 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier 2 —zc it Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 18.9 Acres Permitted: 18.9 Site #: 4 Field #: 557.72 n/a ThA 6A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-I MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total Phos- phorUSEEMENEENEENE Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includingthepossibility of fines and imprisonment for knowing violations" 2::� - _ Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) . . ' s f� M "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, includingthepossibility of fines and imprisonment for knowing violations" 2::� - _ Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL METALS FIELD LOADING SUMMARY FORM Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: von Drehle Corporation Total Dry Tons Applied (Annual): WQ0005135 Cation Exchange Capacity (non 503 only): von Drehle Corporation Owner: von Drehle Corporation Predominant Soil Series 19.3 Acres Permitted: 19.3 Site #: 4 Field #: 486.15 n/a TbA 6B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): vd 2018-2 MB Annual Heavy Metal Field Loadings (Calculated in lbs/acre): "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) Total ' . 1 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date Author Daryl D. Merritt DENR FORM MFLSF (712002) ANNUAL LAND APPLICATION FIELD SUMMARY FORMS ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND All nutrients and metals concentrations listed on the following annual land application field summary forms are on a pound per acre basis. The following is a list of symbols and abbreviations used on the field loading rate report: %TS — Percent Solids DT/ACRE — Dry Tons Applied per Acre lb/ac — Pounds per Acre Metals (lbs/ac) As — Arsenic Cd — Cadmium Cr — Chromium Cu — Copper Pb — Lead Hg — Mercury Mo — Molybdenum Ni — Nickel Se — Selenium Zn — Zinc Nutrients (lbs/ac) PAN — Plant Available Nitrogen P — Phosphorus K — Potassium Annual Totals — lbs/ac applied during the calendar year. 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C EA • iF C a1 LA G sv a *�4 oo d e y a W O O O a c d n O n co 4� v a a a g N A W o Ca p t,j 0 0 in o 0 T n *POWW 0 o uor�Bo-tiddd a a > o g uon'3Z-'211;![On Z aw aw oo o uo!l=-Iunutw ° � o ° w opo N �p °O n2 B[uolutuv tQ �d Q "til O N N Q n � o � n R. `O N N -W 0" n d A i erg• A v 10 0 0 0 w U i r. d CD V V Gy O Cb b �?m uOI l H m e -.1 ° � bdn�� t .Io V;6a K 5 CD a _ Q p mg z =C G � W n o n n m O cn o N � O Pd O C5 ro N V V Gy O uOI l H .Io V;6a K CD a _ Pd rb�� ro „wmp^Go�. . l'-" N (D Lh c� cn � CD V O ca ao a W 0 0 0 a d Y O � � cat 'cJ coo o °• d Yt7a O W O b � w�th0 th kA00' 0� N O b 6 ro 5 J oo ? lOir N .a 0 0 0 x :rnocpw uogEo-iIddV z z z a s Y p uouEz-FIfMoA 7- c z CD ? ch N a+• p UoP3ZE-IEmul O O Q '0 '-� CD om oma w N J Eluowtuv z� z uj P. yyy z C O h tNGn G N N �• N N F z RESIDUAL ANALYSIS LAB SHEETS Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2018-1 MB Date Sampled: 1/26/2018 Date Reported: 2/16/2018 Reporting Period: Jan - Feb 2018 Parameter % PPM Dry Weight EPA Monthly Solids Nitrogen (TKN) aog 1 813.000 Phosphorus V.vi►v 0.620 Potassium 0.007 69.800 Sulfate 19.10 0.000 Calcium 191,000.000 Magnesium 0.178 1,780.000 Sodium 0.096 --- --- 956.000 1.f1] 0A)OO Iron Aluminum Manganese --- Copper --- 8.060 1,500 Zinc --- 30-100 2,800 Ammonia Nitrogen 3.008 � � 79.000 Nitrate N 1 Nitrite N --- 0.5250 Cadmium --- 0,0010 39 Chromium --- 1,200 Nickel --- 0,0011) 420 Lead --- 0.7860 300 Arsenic --- 0,0200 41 Mercury --- 0,5500 17 Selenium --- 0.0100 100 pH 7.300 Calcium Carbonate Eq. 0.000 0.0000 Organic Nitrogen 0.073 Molybdenum --- ° A'�"^ 75 Chloride --- Boron Available P205 Industrial von Drehle Paper Cordova, North Carolina Jan - Feb 2015 Date Reported: 2/16/2018 Report No: vd 2018-1 MB Note All Units ' Pounds Per Dry' Macro Nutrients PAN Surf. 0.667 PAN Ini. 0.746 P 0.001 K 0.140 Lime 0.000 Secondary Nutrients Calcium 382.000 Magnesium 3.560 Sodium 1.912 SAR 0.400 Chloride 0.000 Iron 0.000 Alumium 2.020 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 45.00 pH 7.800 Min Rate 0.400 Metals Arsenic 0.000 Cadmium 0.000 Chromium 0.000 Copper 0.016 Lead 0.002 Mercury 0.001 Molybdenum 0.003 Nickel 0.000 Seleniun 0.000 Zinc 0.060 *MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0774 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project/ PO Number: NIA 126 First Street Received: 01/26/2018 Cordova, NC 28330 Reported: 02/16/2018 Analytical Testing Parameters Client Sample 10: Residual from Paper Plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0774-01 Collection Date: 01/26/2018 11:56 Result RL Units Note Prepared Analyzed Lab Method: Calculation Plant Available Nitrogen 260 mg/kg 02/16/18 1640 02/16/16 1545 FAY Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N x0.0250 0.0250 mg/kg 01/26/18 1534 01/29/18 1430 FAY Nitrile as N <0.500 0.500 mg/kg 01/26/18 1534 01/29/18 1430 FAY Method: SM 2540 G-2011 % Solids 45.0 1,00 % 01/31/18 1349 FAY Method: SM 4500 H+B-2011 (Non -Aqueous) pH at 25 °C 7.8 1.0 pH Units H 01/29/18 1200 FAY Method: SM 4500 NH3 C-2011 Ammonia as N 77.9 0.100 mg/kg Y 01/30/16 0934 FAY Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: SM 4500 P F-2011 Phosphorus, Total (as P) Metals Method: EPA 200.7 Rev 4.41994 Aluminum 1010 2.46 mg/kg Arsenic <0.020 0.020 mg/kg Cadmium <0.001 0.001 mg/kg Calcium 191000 0.983 mg/kg Copper 8.06 0.005 mg/kg Lead 0.786 0.003 mg/kg Magnesium 1760 0.983 mg/kg Molybdenum 1.47 0.001 mg/kg Nickel x0.001 0.001 mg/kg Potassium 69.8 1.97 mg/kg Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Result RL Units Note Prepared Analyzed Lab 0.420 mg/kg 02/161181640 021161181645 FAY 0.62 Result 0.25 mg/kg 02/02/18 1411 FAY RL Units Note Prepared Analyzed Lab 02/14/18 0942 FAY 02/14118 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY 02/14/18 0942 FAY Page 1 of 4 (VMJCROBAC@ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0774 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0774-01 Collection Date: 01/2612018 11:56 Metals Result RL Units Note Prepared Analyzed Lab Selenium <0.010 0.010 mg/kg 02/14/18 0942 FAY Sodium 956 4.92 mg/kg 02/16118 1007 021161181506 FAY Zinc 30.1 0.010 mg/kg 02/14/18 0942 FAY Analyses Subcontracted to: ECI Result RL Units Note Prepared Analyzed Method: SM 4500-N org B Total Kjeldahl Nitrogen 813 0.5 mg/kg 02/15/18 0000 Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Mercury Result RL Units Note Prepared Analyzed Method: SW7471A Mercury, Total <0.550 0.550 mg/kg DRY 02/05/18 0733 02/05/18 1227 PCB SOLID Result RL Units Note Prepared Analyzed Method: 0082A Arodor-1016 <38.4 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Aroclor-1221 <38.4 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Aroclor-1232 <38.4 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Arodor--1242 143 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Arodor-1248 <38.4 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Arodor-1254 <38.4 38.4 ug/kg DRY 01/31/18 0903 01/31/18 1737 Arodor-1260 <38A 38.4 ug/kg DRY 01/31/18 0903 01131/18 1737 Surrogate: 2,4,5,6-Tetrachloro-m-Xylene 69.9 Limit: 29-133 % Ree 01/31/18 0903 01131/18 1737 Surrogate: Decachlorobiphenyl 44.6 Limit: 60-125 % Ree 01/31/18 0903 01/31/18 1737 Percent Solids Result RL Units Note Prepared Analyzed Method: D2216 Percent Solids 44.5 1.00 weight % 02102/18 0735 Laboratory FAY: Microbac Laboratories, Inc. - Fayetteville Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p ' www.microbac.com Page 2 of 4 OMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0774 Definitions *: Surrogate or spike compound out of range H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. AL� The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included bonnie.sanders@microbac.com 0211 81201 8 17:23 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 4 5' W C g S C I IT t GI G1 1{� �y 3 d C a CD z 3 a 40 r In C g a a �f Q z N M c 5' si m c 0 t 0 O 3 Z cNr� O N �l 2 n $ C O v � < a M n 0 w O m rt O S M z 0 N po W O M Page 4 of 4 ; �y D r M a CD z �f Q z N M Z CO co �. n S a r* CD W a c c 0 3 3 m i O o '6 m m 3 91 m x p ) N M G W -n a CA x 4 5 � 0 v a a m W M c m c n O M X m -4 p py p T D D Aluminum, Cadmium D D rsenic, Selenium D D Calcium, Copper D D Lead, Magnesium T D D Nickel, Potassium M 0 D D Sodium, Zinc,MO,HG a D D NH3, No3+No2, {SAR) D D TKN, T Phos, PAN w D % Total Solids, pH D 1> PCBs Q = -nm Q C7 0o D y M uj P n Z m S Z o m oN m v S n ? + n A + + 0 :0 C1 n 4. A °0 0 C;0 m a' si m c 0 t 0 O 3 Z cNr� O N �l 2 n $ C O v � < a M n 0 w O m rt O S M z 0 N po W O M Page 4 of 4 Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2018-2 MB Date Sampled: 3/14/2018 Date Reported: 4/10/2018 Reporting Period: Apr - May 2018 Parameter % PPM Dry Weight EPA Monthly Limits Solids s8 'V 127.000 Nitrogen (TKN) _ 0.013 I 0.001 Phosphorus 5.300 Potassium 0.016 162.000 Sulfate 0.000 Calcium 10 400 104,000.000 Magnesium 0.195 1,950.000 Sodium 0,,096 959.000 Iron --- Aluminum --- 53,110(] Manganese --- Copper --- 10,700 1,500 Zinc --- 73100 2,800 Ammonia Nitrogen i 0.005 47.400 Nitrate N 1 Nitrite N --- 5.f1826 Cadmium --- 0. 00 10 39 Chromium --- 1,200 Nickel --- 1 H OO 420 Lead --- l.Cl400 300 Arsenic --- 0.8330 41 Mercury --- 0.75 70 17 Selenium --- 0.13 20 100 pH I 7.500 Calcium Carbonate Eq. 0.000 0.0000 Organic Nitrogen 0.008 Molybdenum --- 4_4400 75 Chloride --- Boron Available P2O5 Industrial von Drehle Paper Cordova, North Carolina Apr - May 2018 Date Reported: 4/10/2018 Report No: vd 2018-2 MB Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 0.121 PAN Inj. 0.169 P 0.011 K 0.324 Lime 0.000 Secondary Nutrients Calcium 208.000 Magnesium 3.900 Sodium 1.918 SAR 0.502 Chloride 0.000 Iron 0.000 Alumium 1.064 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 38.90 pH 7.500 Min Rate 0.400 Metals Arsenic 0.002 Cadmium 0.000 Chromium 0.000 Copper 0.021 Lead 0.002 Mercury 0.002 Molybdenum 0.009 Nickel 0.002 Seleniun 0.000 Zinc 0.146 0MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8C0417 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project 1 PO Number: NIA 126 First Street Received: 03/14/2018 Cordova, NC 28330 Reported: 04/10/2018 nalytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0417-01 Collection Date: 03/14/2018 12:10 Method: Calculation Plant Available Nitrogen Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2540 G-2011 % Solids Method: SM 4500 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: SM 4500 H+B-2011 (Non Aqueous) pH at 25 °C Method: SM 4500 P F-2011 Result RL Units 48.3 mglkg Note Prepared Analyzed Analyst 04/04/18 1518 04!04/18 1518 JMo x0.242 0.242 mg/kg 03/16/18 0958 03116/18 1614 DSK X4.84 4.84 mg/kg 03/16/18 0958 03/16/18 1614 DSK 38.9 1.00 % 03/18/18 1239 MT 47.4 0.100 mg/kg Y 03/16/18 0910 DSK 127 0.500 mg1kg Cadmium 03/19/18 0832 TAB Result RL Units Note Prepared Analyzed Analyst 0.570 mg/kg (dry) mg/kg 04/04/18 1518 04104/18 1518 JMO 7.5 1.0 pH Units H 03/19/18 1529 DC Phosphorus, Total (as P) 5.3 0.25 mg/kg 03/19/18 1144 DSK Metals Result RL Units Note Prepared Analyzed Analyst Method: Metals Solid/EPA 200.7 Rev 4.4 1994 Arsenic 0.838 0.020 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Cadmium X0.001 0.001 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Calcium 104000 0.985 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Copper 10.7 0.005 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Lead 1.04 0.003 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Magnesium 1950 0.985 mg/kg (dry) 04102118 1153 04/02/18 1153 TAB Molybdenum 4.44 0.001 mg/kg (dry) 04/02/18 1153 04/02/18 1153 TAB Microbac Laboratories, Inc. 2592 Hope Mills Rd ; Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3 OMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8C0417 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0417-01 Collection Date: 0311412018 12:10 Metals Nickel Potassium Selenium Sodium Zinc Metals Method: EPA 200.7 Rev 4.4 1994 Aluminum Mercury Method: SW7471A Mercury, Total Percent Solids Method: D2216 Percent Solids Result RL Units 1.11 0.001 mglkg (dry) 162 1.97 mg/kg (dry) 0.132 0.010 mg/kg (dry) 959 0.985 mg/kg (dry) 73.2 0.010 mglkg (dry) Analyses Subcontracted to: ECI Result RL Units Note Prepared Analyzed Analyst 04/02/18 1153 04/02118 1153 TAB 04/02/18 1153 04/02118 1153 TAB 04/02/18 1153 04/02118 1153 TAB 04/02/18 1153 04/02118 1153 TAB 04/02/18 1153 04/02118 1153 TAB Note Prepared Analyzed Analyst 532 2.5 mg/kg (dry) 04/08/10 0000 TD Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley RL: Reporting Limit Result RL Units Note Prepared Analyzed Analyst 00.757 0.757 mglkg DRY J 03/19/18 0759 03/21/16 1056 PDM Result RL Units Note Prepared Analyzed Analyst 32.0 1.00 weight % 03120/18 0814 KMG Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time J: The analyte was positively identified, but the quantitation was below the RL MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted The data and information on this, and other accompanying documents, represents Bonnie K Sanders only the sample(s) analyzed. This report is incomplete unless a8 pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bonnie.sanders@microtsac.00m 04/10/2018 09:37 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061 910.864.1920 p I www.microbac.com L Page 2 of 3 g jo £abed ti > a � U r OD a Y OD 0 rn It - 4 d to CD 0 rn .1 O M 00 N Q ar' U. ca 0 CL 0 x 0) N C 3 N T LL 0X U I O V w } D O D v LL. O z R V i; z m �U m CL T 0 12 0 E 0 U w Z O r`l v 0 a v V + + '' f 9 Z Q v U + n a Z= S Z N M O w 4 m U ltl LL IX o O U E- Hd 'Sp11oS MO. % ¢ ¢ N } NVd 'SO4d 1 'N)ll ¢ ¢ zWVS) 'ZoN+EoN '£HN ¢ ¢ OWOW'OuIZ 'wnlpoS Q ¢ Q wrnsse;od '1913iN Q ¢ w a- wrns9u6sW 'pea -1 ¢ ¢ ~ aaddoO 'wnialeO ¢ ¢ wnlualaS 'awasay ¢ ¢ wnlwpeO 'wnuiwnly ¢ ¢ L6 O m O w M ar [V r x IL a N C7 2_��f O � O r l7p U4 � O N -2a W 0 CL U `N W ;1 1 �1 M 0 A L L a U W W � W a S°u�a r Oz p F ca rn�WJ CL m a 0 nl 0 a� a U co .e Qf co Z r i N_ j Z ii D N J ¢ J J O i; z m �U m CL T 0 12 0 E 0 U Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: von Drehle Corporation von Drehle Paper Cordova, North Carolina Belger Farms Industrial vd 2018-3 MB 5/29/2018 6/11/2028 May - Jun 2018 Parameter % PPM Dry Weight EPA Monthly Limits Solids 1 Nitrogen (TKN) _40---10 _ ____0.004_ 0.000 41.400 Phosphorus 0.250 Potassium _ 0.003 34.700 Sulfate 0.000 Calcium _ 55,700.000 Magnesium _5.570 0.059 589.000 Sodium 0.017 174.000 Iron --- Aluminum Manganese --- Copper --- 5.1801 1 1,500 Zinc --- 411.519) 2,800 Ammonia Nitrogen 009 ; � .60 0 Nitrate N / Nitrite N --- S.5580 Cadmium --- ` 0.33t)U 39 Chromium --- 1,200 Nickel --- 1.3500 420 Lead --- 33900 300 Arsenic --- 3.3900 41 Mercury --- 02350 17 Selenium --- 3.3.900 100 pH 7.�i;-,t Calcium Carbonate Eq. 0.000 0.0000 Organic Nitrogen 0.001 Molybdenum ---: 75 Chloride --- Boron Available P205 Industrial von Drehle Paper Cordova, North Carolina May - Jun 2018 Date Reported: 6/11/2028 Report No: vd 2018-3 Ms Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 0.051 PAN Inj. 0.087 P 0.001 K 0.069 Lime 0.000 Secondary Nutrients Calcium 111.400 Magnesium 1.178 Sodium 0.348 SAR 0.128 Chloride 0.000 Iron 0.000 Aiumiurn 0.690 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 40.40 pH 7.400 Min Rate 0.400 Metals Arsenic 0.007 Cadmium 0.001 Chromium 0.000 Copper 0.010 Lead 0.007 Mercury 0.000 Molybdenum 0.007 Nickel 0.003 Seleniun 0.007 Zinc 0.081 *MICROBAC@ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8E0505 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project/ PO Number: NIA 126 First Street Received: 05/29/2018 Cordova, NC 28330 Reported: 06/11/2018 Case Narrative SAR DATA: 0.14 mg/kg nalytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K817,0505-01 Collection Date: 05/29/2018 15:35 Result RL Units Note Prepared Analyzed Analyst Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N 0.678 0.244 mg/kg 05131/18 1239 05/31/18 1600 DSK Nitrite as N <4.88 4.88 mglkg 05/31/18 1239 05/31/18 1600 DSK Method: SM 2540 G-2011 % Solids 40.4 1.00 % 05/31/18 1133 Method: SM 4500 NI -13 C-2011 Ammonia as N 35.6 0.100 mglkg Y 06/05/18 0923 MT Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen 41.4 0.500 mg/kg 06/06/18 0834 TAB Wet Chemistry Result RL Units Note Prepared Analyzed Analyst Method: SM 4500 H+13-2011 (Non -Aqueous) PH at 25 °C 7.4 1.0 pH Units H 06/01/18 1201 JR Method: SM 4500 P F-2011 Phosphorus, Total (as P) <0.25 0.25 mg/kg 06/08/16 1012 DSK Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Mercury Result RL Units Note Prepared Analyzed Analyst Method: SW7471A Mercury, Total <0.235 0.235 mglkg DRY 06/05/18 0903 06/06/18 1002 PDM Metals by 6010 Result RL Units Note Prepared Analyzed Analyst Method: SW6010C Aluminum, Total 345 13.5 mglkg DRY 06/04/18 0751 08/04/18 1515 PDM Arsenic, Total <3.39 3.39 mglkg DRY 06/04/18 0751 06/05/18 1402 PDM Cadmium, Total <0.339 0.339 mglkg DRY 06/04/16 0751 06/04/18 1515 PDM Microbac Laboratories, Inc. 2592 Hope Mills Rd Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 3 OMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8E0505 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0505-01 Collection Date: 05/29/2018 15:35 Metals by 6010 Result RL Units Note Prepared Analyzed Analyst Calcium, Total 55700 33.9 mg/kg DRY I 06!04!18 0751 06/04/18 1515 PDM Copper, Total 5.16 0.677 mg/kg DRY 06/04/18 0751 06104118 1515 PDM Lead, Total X3.39 3.39 mg/kg DRY 06/04/18 0751 06/04/18 1515 PDM Magnesium, Total 589 16.9 mgft DRY 06/04/18 0751 06/04118 1515 PDM Molybdenum, Total X3.39 3.39 mg/kg DRY 06/04/18 0751 06/04/18 1515 PDM Nickel, Total <1.35 1.35 mg/kg DRY J 06/04118 0751 06/04/18 1515 PDM Potassium, Total 34.7 33.9 mglkg DRY 06/04/18 0751 06/05/18 1402 PDM Selenium, Total X3.39 3.39 mg/kg DRY 06/04/18 0751 06/04/18 1515 PDM Sodium, Total 174 16.9 mg/kg DRY 06104/16 0751 06/04/16 1515 PDM Zinc, Total 40.5 0.677 mg/kg DRY 06/04/18 0751 06/08/18 1254 PDM Definitions H: Analyte was prepared andlor analyzed outside of the analytical method holding time I: Semiquantitative result (out of instrument calibration range) J: The analyte was positively identified, but the quantitation was below the RL MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents Jeanne Overstreet only the sample(s) analyzed. This report is incomplete unless all pages indicated Client Relationship Specialist, Environmental in the footnote are present and an authorized signature is included jean n e.overstreetQmlcrobac. com 06/11/2018 09:23 Microbac Laboratories, Inc. 2892 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3 L w 00 � OD ago U Z as" �a LL I V 0 N r CL 0 CM a ca LL k. t Irl 0 a u i.0 �I W [y v O F s + ^' o x Z N 0: _ R l4d 'SplloS 18401 % a ¢ NVd '804d 1 "N)I1 ¢ a WVS) 'ZON+£oN '£HN ¢ aJH'OW'oulZ `wrpS ¢ ¢¢ wnlsse;od'IM PI aO a¢ lwnlsau6en'pea ¢¢ jaddoo `wnlole ¢ wnlueleg'olumV 4 wn+wpeo 'wnulwnlV m o N¢ X � v F � Ln b � � o is 6 M C d CL ` 0.18 '2 N Ta - Li to zd-13-2 c� N L+ co O N d Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2018-4 MB Date Sampled: 7/10/2018 Date Reported: 7/27/2018 Reporting Period: Jul - Aug 2018 Parameter % PPM Dry Weight 280.000 11.000 2.000 0.000 67,800.000 755.000 _ 540.000 1 NAM EPA Monthly Limits Solids Nitrogen (TKN) 0.628 Phosphorus 0.00' Potassium O.000 Sulfate Calcium 6.73SO Magnesium 0.076 Sodium 0,054 Iron --- Aluminum --- Manganese --- Copper --- 9.070 1,500 Zinc --- 1 T3,0Q0 2,800 Ammonia Nitrogen 0 mo I 1 +■i!i 106.00(} Nitrate N / Nitrite N --- _ 5.77001 (1. I €7�} 39 Cadmium --- Chromium --- 1,200 Nickel --- 1.5 7M 420 Lead --- (L9 ! 0 300 Arsenic --- 2.MOO 41 Mercury --- 0-2340 17 Selenium --- 0.93.70 100 pH '7,800 Calcium Carbonate Eq. 0.000 0.0000 Organic Nitrogen 0.017 Molybdenum --- = -.171 Fc 75 Chloride --- Boron Available P2O5 Industrial von Drehle Paper Cordova, North Carolina Jul - Aug 2018 Date Reported: 7/27/2018 Report No: vd 2018-4 MB Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 0.257 PAN In'. 0.363 P 0.022 K 0.004 Lime 0.000 Secondary Nutrients Calcium 135.600 Magnesium 1.510 Sodium 1.080 SAR 0.305 Chloride 0.000 Iron 0.000 Alumium 0.388 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 29.10 pH 7.800 Min Rate 0.400 Metals Arsenic 0.004 Cadmium 0.000 Chromium 0.000 Copper 0.018 Lead 0.002 Mercury 0.000 Molybdenum 0.007 Nickel 0.004 Seleniun 0.002 Zinc 0.266 OMICROBAC® Microbac Laboratories, Inc. - Fayetteville Revised Report. Amended -See CERTIFICATE OF ANALYSIS Case Narrative. K800085 Von Dnehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project / PO Number: NIA 126 First Street Received: 07/10/2018 Cordova, NC 28330 Reported: 07/27/2018 Case Narrative PAN Calculation: 44.01 mg/kg SAR Calculation: 0.40 mglkg Report amended an July 26, 2018 for work order IOJG0085 that was originally relwrbed an July 24, 2018; The sample was rerun on 0712512018. Rerun result indicates a poor recovery in the initial anlaysis due to matrix Interference. New result supersedes prior analysis. Analytical Testing Parameters Client Sample ID: Reoidual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0085-01 Collection Date: 07/10/2018 12:06 Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2540 G-2011 % Solids Method: SM 4500 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: SM 4500 H+B-2011 (Non -Aqueous) pH at 25 °C Method: SM 4500 P F-2011 Result RL Units Note Prepared Analyzed Analyst 0.790 0.249 mg/kg 07/12116 0937 07/12118 1653 DSK <4.98 4.98 mg/kg 07/12118 0937 07/12118 1653 DSK 29.1 1.00 % 07113!18 1618 MT 106 0.100 mg/kg y 07/13/18 0935 07113/18 1516 MT 280 0.500 mg/kg 07/17/18 0845 TAB Result RL Units Note Prepared Analyzed Analyst 7.8 1.0 pH Units H 07/13/18 1108 TAB Phosphorus, Total (as P) 11 0.25 mg/kg Metals Result RL Units Note Prepared Method: Metals Solid/EPA 200.7 Rev 4.4 1994 TAB 071201181152 Arsenic 2.08 0.020 mglkg (dry) Cadmium 0.167 0.001 mg/kg (dry) Calcium 67800 0.999 mg/kg (dry) Copper 9.07 0.005 mg/kg (dry) Lead 0.881 0.003 mg/kg (dry) Magnesium 765 0.999 mg/kg (dry) Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com 07116118 1135 DSK Analyzed Analyst 07120/18 1152 TAB 07/20/18 1152 TAB 07120118 1152 TAB 071201181152 TAB 07120/181152 TAB 071201181152 TAB Page 1 of 3 (9MICROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8G0085 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0085-01 Collection Date: 07/10/2018 12:06 Metals Result RL Units Note Prepared Analyzed Analyst Molybdenum 3.47 0.001 mg/kg (dry) 07/20/18 1152 TAB Nickel 1.97 0.001 mg/kg (dry) 07/20/18 1152 TAB Potassium X2.00 2.00 mg/kg (dry) 07/20/18 1152 TAB Selenium 0.937 0.010 mg/kg (dry) 07/20/18 1152 TAB Sodium 540 0.999 mg/kg (dry) 07/20/18 1152 TAB Zinc 133 0.010 mg/kg (dry) 07/20/18 1152 TAB Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Mercury Result RL Units Note Prepared Analyzed Analyst Method: SW7471A Mercury, Total X0.234 0.234 mg/kg 07/17/18 0819 07/18/18 1450 JST Metals by 6010 Result RL Units Note Prepared Analyzed Analyst Method: SW6010C Aluminum, Total 194 13.9 mg/kg 07/16/18 0845 07/16/18 2008 PDM Definitions H: Analyte was prepared andlor analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) anaWed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Reviewed and Approved By: �.E6L-11X' Jeanne Overstreet Client Relationship Specialist, Environmental jeenne.overstreet@microbac.com 07/271201811:30 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3 co O 04T 4. rn 0 2 U Z Ui t •a 0 N 0I O. 0 z N F u 0 M ry O L) W W. G O P - U) U IL O Z U G v V + � 0 z Z N X W U in W U. a Qp U a Hd'smoS Ie4oL'yo ¢ ¢ w NVd 'sOgd 'l '01 ¢ ¢ 4 (UVS) 'ZON+£oN '£HN <1 Q OH'OVf uVWnipoS ¢ ¢ LL © Wnisselod '10MOiN ¢ ¢ wroseuBTaW 'peo-I ¢ ¢ aaddoo unwo ¢ ¢ Wnivalas lol.unov ¢ ¢ WniWpeO'Wnui.WnIV ¢ ¢ LL w o f N -J W w at N r a X w ro 2 o a 0 4 � � o W a 'O 0 G U r. s w 0 .G T' WL. L Q (f 4 E ~i 7 O c� N m w U � U a m co) Z W c >0 Q w a p J CL 4 d E E 0 U 0 46 0 M m om m CL Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2018-5 MB Date Sampled: 9/11/2018 Date Reported: 10/31/2018 Reporting Period: Sept - Oct 2018 Parameter % PPM --- _ Dry Weight Chromium --- Nitrogen (TKN) 0.077 774.000 Phosphorus 0,004 36.000 Potassium 0.131 1,510.000 Sulfate Zinc 0.000 1. Calcium 18.100 181,000.000 Magnesium _ 0.172 1,720.000 Sodium 0.151 1,510.000 EPA Monthly Limits ll ull - - - Aluminum --- Manganese --- Copper --- 27,100 1,500 Zinc --- _ 96.83 2,800 Ammonia Nitrogen 0.01f) 156,000 Nitrate N / Nitrite N --- t8.7300 Cadmium --- 0.49W 39 Chromium --- 1,200 Nickel --- 2.000o 420 Lead --- 1. 50.0u 300 Arsenic --- ..QL)OO 41 Mercury --- 0.0140 17 Selenium --- 3.W00 100 pH 7.800 Calcium Carbonate Eq. 0.000 0.0000 Organic Nitro en 0.062 Molybdenum --- I {.'rs+.7tx 75 vailable P2O5 Industrial von Drehle Paper Cordova, North Carolina Sept - Oct 2018 Date Reported: ##### Report No: vd 2018-5 MB Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 0.688 PAN Inj. 0.844 P 0.072 K 3.020 Lime 0.000 Secondary Nutrients Calcium 362.000 Magnesium 3.440 Sodium 3.020 SAR 0.507 Chloride 0.000 Iron 0.000 Alumium 3.040 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 27.40 pH 7.800 Min Rate 0.400 Metals Arsenic 0.006 Cadmium 0.001 Chromium 0.000 Copper 0.054 Lead 0.003 Mercury 0.000 Molybdenum 0.007 Nickel 0.004 Seleniun 0.006 Zinc 0.194 OMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K810151 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project/ PO Number: NIA 126 First Street Received: 0911 1 120 1 8 Cordova, NC 28330 Reported: 10/31/2018 Case Narrative Report amended on October 9, 2018 for work order KBI0151 that was originally reported on October 9, 2018; Dupliate result for % Solid was removed. Report amended on October 18, 2018 for work order K8I0151 that was originally reported on October 9, 2018; Solid results from OVD was removed as the analysis was outside hold time, not a vatlid result. 10/31/2018: Client requested the metals rerun as the 601 OD method as required by the permit. Mercury run as method EPA 7471 B. Y qualifier for Ammonia is incorrrect due to an IT issue currently being resolved. Analytical Testing Parameters Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Lab Sample ID: K810151-01 Method: Calculation Plant Available Nitrogen Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2540 G-2011 % Solids Method: SM 4500 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: SM 4500 H+B-2011 (Non -Aqueous) pH at 25 °C Method: SM 4800 P F-2011 Result RL Units 72.6 mg/kg 1.58 0.862 mglkg dry vvt. dry a17.2 17.2 mglkg dry wt. dry 27.4 1.00 % 156 774 Result 0.690 7.9 Collected By: Client Collection Date: 09/11/2018 12:00 Note Prepared Analyzed Analyst 10/09/18 0926 10!09118 0927 JMO 3.65 mg/kg dry wt. Y dry 1.83 mg/kg dry wt. dry RL Units Nol mg/kg 1.0 pH Units H 09/12/18 0916 09/12/18 1603 DSK 09/12/18 0918 09/12/18 1603 DSK 09/18/16 1415 MT 09/12/18 1005 MT 09/12/18 0845 TAB Prepared Analyzed Analyst 10/31/18 0904 10/31/18 0905 JMO Phosphorus, Total (as P) 36 0.87 mg/kg dry wt. dry Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910-864-1920 p I www.microbac.com 09/12/18 1219 JR 09/20/18 1404 DSK Page 1 of 3 0MICROBACU Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K810151 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Client Lab Sample ID: K810151-01 Collection Data: 09/11/2018 12:00 Wet Chemistry 6010 MET ICP Method: 6010D Aluminum Arsenic Cadmium Calcium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc 7471 B Method: 7471 B Mercury Result RL Units Note Prepared Analyzed Analyst Analyses Subcontracted to: Pace Analytical Result RL Units Note Prepared Analyzed Analyst 1520 30.2 mg/kg dry wt. 10M/118 0000 DS X3.0 3 mg/kg dry wt. 10/28/18 0000 DS OA9 0.3 mg/kg dry wt. 10/28/18 0000 DS 181000 605 mg/kg dry wt. 1012s118 0000 DS 27.1 1.5 mg/kg dry wt. 10/28/18 0000 DS <1.5 1.5 mglkg dry wt. 10/28/18 0000 DS 1720 30.2 mglkg dry wt. 10/28/18 0000 DS 3.7 1.5 mglkg dry wt. 10/28/18 0000 DS 2 1.5 mg/kg dry wt. 10/28/18 0000 DS <1510 1510 mg/kg dry wt. 10/28/16 0000 DS <3.0 3 mglkg dry wt. 10128118 0000 DS <1510 1510 mg/kg dry wt. 10/28/18 0000 DS 95.8 3 mglkg dry wt. 10/26/18 0000 DS Result <0.014 RL Units Note Prepared Analyzed Analyst 0.014 mglkg dry wt. 10/30/18 0000 JMW Definitions H: Analyte was prepared and/or analyzed outside of the analytical method holding time MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Reviewed and Approved By: Jeanne Overstreet Client Relationship Specialist, Environmental Reported: 1013112018 09:23 Microbac laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 2 of 3 0 N rn 'ct (fl ao 4 cQ M Go N U z a� $i LI� m C. O N rn LO 04 W I�If�f 0 u 541, a a w re Q U LL O z a s en 0 c E E 0 W a 6 0 W O O U U Itv U v e N � � i w V + + v a to 1 V Y + v d A Q a + W M Y u W .Z ? x Z N Y r r it n u r R n W a to U O w LL- Lo 0 a U s8�d d 41 lid 'sp!1Os lelol % Q NVd 'sOud '1 `N7ii < '£HN d WVS) 'ZON+£aN ¢ ac E)HbW'aur,� `wn!pos 4 LL O wnl9s%0d 'la)loiN wnlseuDEV9 'Peal 0. 'wn!Oleo jaddoo wnlueles b!uesiv d wnlwpeo'wnu!wnld a m o a u N X Le en C ti CD o o D mTE T 04 U- o' oC " ca T CI CLW 0. cm IL O E 0 m d co m U m U m C/3 Z ik A 1! o LL W mq J CD as� s en 0 c E E 0 M 46 O m m EL 6 0 N � � i w a to A F W c S M 46 O m m EL Facility: von Drehle Corporation Source: von Drehle Paper Location: Cordova, North Carolina Contractor: Belger Farms Type of Analysis: Industrial Report No: vd 2018-6 MB Date Sampled: 11/6/2018 Date Reported: 11/18/2018 Reporting Period: Nov - Dec 2018 Parameter % PPM Dry Weight EPA Monthly Limits Solids 3&60 Nitrogen (TKN) €x.012 115.000 Phosphorus 0.000 1.100 Potassium 0.972 9,720.000 Sulfate 0.000 Calcium 10A00 164,000.000 Magnesium UJ 83 1,830.000 Sodium. {1 1 o7 1,070.000 Iron --- T Aluminum --- Y.656,00 Manganese --- Copper --- 2&400 1,500 Zinc --- `2:51(.) 2,800 Ammonia Nitrogen i i. t ){k7 72.100 Nitrate N / Nitrite N --- I -k .57€ ) Cadmium --- 0.1900 39 Chromium --- 1,200 Nickel --- 3 .7�k[1(} 420 Lead --- 1.310{} 300 Arsenic --- 1-9[}f11 41 Mercury --- {). X11-50 17 Selenium --- 1-9000 100 pH;.'r�c: Calcium Carbonate Eq. 0.000 0.0000 Organic Nitrogen 0.004 Molybdenum --- r�t,3.lir 75 Chloride --- Boron Available P2O5 Industrial von Drehle Paper Cordova, North Carolina Nov - Dec 2018 Date Reported: ##"ft*u# Report No: A 2018-6 MB Note All Units in Pounds Per Dry Ton Macro Nutrients PAN Surf. 0.134 PAN In'. 0.206 P 0.002 K 19.440 Lime 0.000 Secondary Nutrients Calcium 328.000 Magnesium 3.660 Sodium 2.140 SAR 0.447 Chloride 0.000 Iron 0.000 Alumium 4.100 Manganese 0.000 Boron 0.000 Sulfur 0.000 Physical Characteristics % Solids 38.60 13 8.200 Min Rate 0.400 Metals Arsenic 0.004 Cadmium 0.000 Chromium 0.000 Copper 0.057 Lead 0.003 Mercury 0.000 Molybdenum 0.008 Nickel 0.063 Seleniun 0.004 Zinc 0.185 OMICROBAC@ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8 K0080 Von Drehle Corporation Project Name: Residuals Sample - 60 day Mr. Chris Fowler Project/ PO Number: NIA 126 First Street Received: 11/06/2018 Cordova, NC 28330 Reported: 11/18/2018 Analytical Testing Parameters Client Sample ID: Residual from Paper PlAnt Sample Matrix: Solid Lab Sample ID: K81<0030-01 Method: Calculation Plant Available Nitrogen Method: EPA 300.0, Rev. 2.1 (1993) Nitrate as N Nitrite as N Method: SM 2640 G-2011 % Solids Method: SM 4600 NH3 C-2011 Ammonia as N Method: SM 4500-Norg C-2011 Total Kjeldahl Nitrogen Wet Chemistry Method: Calculation Sodium Adsorption Ratio, SAR Method: SM 4600 H+8-2011 (Non -Aqueous) PH at 25 °C Method: SM 4600 P F-2011 Phosphorus, Total (as P) 7471B Method: 7471B Mercury Result RL Units 49.6 mg/kg 0.676 0.643 mg/kg dry wt. dry X12.9 12.9 mg/kg dry wt. dry Collected By: Wright Collection Date: 11/06/2018 11:00 Note Prepared Analyzed Analyst 11/14/18 1433 11/14/18 1448 JMO 11/07/18 1224 11/08/18 1034 DSK 11/07/18 1224 11/08/18 1034 DSK 38.6 1.00 % 11/12118 1417 MT 72.1 2.59 mg/kg dry wt. y 11/07/18 1314 MT dry 115 1.29 mg/kg dry wt. I 11/08/18 0832 TAB dry Result RL Units Note Prepared Analyzed Analyst 0.510 mg/kg 11/14/18 1433 11114/18 1448 JMd 8.2 1.0 pH Units H 11/07/18 1420 TAB 1.1 0.65 mg/kg dry wt. Al2 11/09/18 1024 DSK dry Analyses Subcontracted to: Pace Analytical Result RL Units Note Prepared Analyzed Analyst X0.016 mg/kg dry wt. 11110118 0000 D5 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.11920 p I www.microbac.com Page 1 of 2 O)MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8K0080 Client Sample ID: Residual from Paper Plant Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8K0080-01 Collection Date: 11/06/2018 11:00 SPLP Metals Result RL Units Note Prepared Analyzed Analyst Method: SW -846 6010B Aluminum 2050 19.4 mglkg dry wt. 11/10/18 0000 DS Arsenic <1.9 1.9 mg/kg dry wt. 11/10/18 0000 DS Cadmium X0.19 0.19 mg/kg dry wt. 11110!18 0000 DS Calcium 164000 389 mg/kg dry wt. 11/10/18 0000 DS Copper 28.4 0.97 mglkg dry wt. 11/10/18 0000 DS Lead 1.3 0.97 mglkg dry wt. 11/10/18 0000 DS Magnesium 1830 19.4 mg/kg dry wt. 11/10/18 0000 DS Molybdenum 3.8 0.97 mg/kg dry wt. 11110/18 0000 DS Nickel 31.7 0.97 mg/kg dry wt. 11/10/18 0000 DS Potassium <972 972 mg/kg dry wt. 11/10/18 0000 DS Selenium <1.9 1.9 mg/kg dry wt. 1111o/1e oo0o DS Sodium 1070 972 mg/kg dry wt. 11/10/18 0000 DS Zinc 92.5 1.9 mg/kg dry wt. 11/10118 0000 DS Definitions Al2: MS/MSD fail recovery, but the LCS passes criteria. H: Analyte was prepared and/or analyzed outside of the analytical method holding time I: Spike recovery outside control limits due to sample matrix interFerenoe or high analyte concetration MDL: Minimum Detection Limit RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments North Carolina DENR NPDES Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Reviewed and Approved By: Jeanne Overstreet Client Relationship Specialist, Environmental Reported: 11/18/2018 16:38 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 2 of 2 TOXICITY CHARACTERISTICS LEACHING PROCEDURE (TCLP) ANALYSIS REPORT ONICROBAC ° Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Project description Residuals Sample -Annual For: Mr. Chris Fowler Von Drehle Corporation 126 First Street Cordova, NC 28330 Bonnie K. Sanders Senior Project Manager Wednesday, February 7, 2018 Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require further assistance regarding this report, please contact your service representative listed above. I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil samples are reported on a'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported results are related only to the samples analyzed as received. Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 1 of 8 OMICROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KBA0694 Von Drehle Corporation Project Name: Residuals Sample - Annual Mr. Chris Fowler Project 1 PO Number: 2030767 126 First Stmt Received: 01/24/2018 Cordova, NC 28330 Reported: 02/07/2018 Sample Summary Report Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received Residual from paper plant K8A0694-01 Solid Grab 01/24/18 11:45 01/24/18 14:50 Page 2 of 13 OMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Analytical Testing Parameters Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0694-01 Collection Date: 01124/2018 11:45 Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Result RL Units Note Prepared Analyzed Method: SW9045 Corrosivity pH 8.58 UNITS 01/26/18 1508 Temperature At Determination (C) 17.2 UNITS 01/26/18 1508 8270 TC Result RL Units Note Prepared Analyzed Method: SW8270C 1,4 -Dichlorobenzene <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 2,4,5 -Trichlorophenol <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 2,4,6 -Trichlorophenol <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 2,4-Dinitrotoluene <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 Hexachlorobenzene <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 Hexachlorobutadiene <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 Hexachloroethane <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 m -,p -Cresol <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 Nitrobenzene <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 o -Cresol <50.0 50.0 ug/L 01/30/18 1430 01/31/18 1013 Pentachlorophenol <250 250 ug/L 01/30/18 1430 01/31/18 1013 Pyridine <250 250 ug/L 01/30/18 1430 01/31/18 1013 Surrogate: 2,4,6-Tribromophenol 97.0 Limit: 10-123 % Rec 01/30/18 1430 01/31/18 1013 Surrogate: 2-Fluorobiphenyl 81.6 Limit: 43-116 % Rec 01/30/18 1430 01/31!18 1013 Surrogate: 2-Fluorophenol 49.7 Limit: 21-100 % Rec 01/30/18 1430 01/31/18 1013 Surrogate: NitrobenzeneA5 73.0 Limit: 35-114 % Rec 01/30/18 1430 01/31/18 1013 Surrogate: p-Terphenyl-d14 90.7 Limit: 33-141 % Rec 01/30/18 1430 01/31/18 1013 Surrogate: Phenol -d5 33.7 Limit: 10-94 % Rec 01/30/18 1430 01/31/18 1013 Ignitabiiity of Solids Result RL Units Note Prepared Analyzed Method: 1030 Bumrate - 1030 <2.20 2.20 mm/sec 01/30/18 1140 Mercury Result RL Units Note Prepared Analyzed Method: SW7470A Mercury <0.00200 0.00200 mg/L 01/30/18 0957 01/31/18 1133 Metals by 6010 Result RL Units Note Prepared Analyzed Method: SW6010C Arsenio, TCLP <1.00 1.00 mg/L 01/30!18 1029 01/31/18 1353 Barium, TCLP 0.272 0.100 mg/L 01/30/18 1029 01/31/18 1353 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac-com Page 3 of 8 6)MICROBACL Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Client Sample ID: Residual from paper plant Sample Matrix: Solid Lab Sample ID: KSA0694-01 Collected By: Marin Collection Date: 01/24/2018 11:45 Metals by 6010 Result RL Units Note Prepared Analyzed Cadmium, TCLP <0.100 0.100 mg1L 01130/18 1029 01/31/18 1353 Chromium, TCLP <0.200 0.200 mg1L 01/30/18 1029 01/31/18 1353 Lead, TCLP <1.00 1.00 mg/1- 01/30/18 1029 01!31116 1353 Silver, TCLP <0.100 0.100 mg/L 01/30/18 1029 01/31/16 1353 Metals by 6020 Result RL Units Note Prepared Analyzed Method: SW6020A Selenium, TCLP <0.500 0.500 mg/L 01/30/16 1029 01/31/18 1549 Reactivity, Cyanide Result RL Units Note Prepared Analyzed Method: SW9014 Reactivity, Cyanide <9.98 9.98 mg/kg 01/31/18 1520 Sulfide (Reacitivity) Result RL Units Note Prepared Analyzed Method: SW9034 Reactivity, Sulfide <100 100 mg/kg 01/31/18 1700 TCLP HERBICIDES Result RL Units Note Prepared Analyzed Method: SW8151A 2,4-D <20.0 20.0 ug/L 01/31/18 1213 02/01/18 2006 2,4,5 -TP (Silvex) <2.00 2.00 ug/L 01/31/18 1213 02/01/18 2006 Surrogate: 2,4-Dichlorophenylacetic acid 41.3 Limit: 20-144 % Rec 01/31/18 1213 02/01/18 2006 TCLP Pesticides Result RL Units Note Prepared Analyzed Method: SW80818 Endrin <0.500 0.500 ug/L 01/30/18 1215 02!02118 0520 Lindane <0.500 0.500 ug/L 01/30/18 1215 02/02/18 0520 Methoxychlor <0.500 0.500 ug/L 01/30/18 1215 02/02/18 0520 Toxaphene <10.0 10.0 ug/L 01/30/18 1215 02/02/18 0520 Chlordane <10.0 10.0 ug/L 01/30/18 1215 02/02/18 0520 Heptachlor <0.500 0.500 ug/L 01/30/18 1215 02/02/18 0520 Heptachlor Epoxide <0.500 0.500 ug/L 01/30/18 1215 02/02/18 0520 alpha Chlordane <0.500 0.500 ug1L 01/30/18 1215 02/02/18 0520 gamma Chlordane <0.500 0.500 ug1L 01/30/15 1215 02/02/18 0520 Surrogate: 2,4,5,6-Tetrachloro-m-xylene 53.3 Limit: 20-180 % Rec 01/30/18 1215 02/02/18 0520 Surrogate: Decachlorobiphenyl 20.1 Limit: 25-140 % Rec 01/30/18 1215 02/02/18 0520 VOIatIIe Organics Result RL Units Note Prepared Analyzed Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864A920 p I www.microbac.com Page 4 of 8 OMICROBACa Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Client Sample ID: Residual from paper plant Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0694-01 Collection Date: 01/24/2018 11:45 Volatile Organics Result RL Units Note Prepared Analyzed Method: SW8260B 1,1-Dichloroethene <50.0 50.0 uglL 01/31/18 1655 1,2-Dichloroethane <50.0 50.0 uglL 01/31/18 1655 Benzene <50.0 50.0 uglL 01/31/18 1655 Carbon tetrachloride <50.0 50.0 uglL 01/31/18 1655 Chlorobenzene <50.0 50.0 uglL 01/31/18 1655 Chloroform <50.0 50.0 uglL 01/31/18 1655 Methyl Ethyl Ketone <100 100 uglL 01/31/18 1655 Tetrachloroethene <50.0 50.0 uglL 01131!18 1655 Trichloroethene <50.0 50.0 uglL 01131/181655 Vinyl chloride <100 100 uglL 01/31/18 1655 Surrogate: 1,2-Dichloroelhane-l4 101 Limit: 80-120 % Rec 01/31/18 1655 Surrogate: 4-Bromofluorobenzene 103 Limit: 86-115 % Rec 01/31/18 1655 Surrogate: Dibromofluoromethane 97.8 Limit: 86-118 % Rec 01/31/18 1655 Surrogate: Toluene -d8 99.9 Limit: 88-110 % Rec 01/31/18 1655 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com page 5 of 8 Batch Quality Control Summary 6)MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley Spike Source %REC RPD Metals by 6020 Result RL Units Level Result %REC Limits RPD Limit Notes Batch WG647263 - METHOD - SW6020A BILK (WG646866-02) Selenium, TCLP BS (WG646865-03) Selenium, TCLP Reactivity, Cyanide BS (WG646993-01) Reactivity, Cyanide Prepared: 01/30/2018 Analyzed: 01/31/2018 ND 0.0500 mg/L - U Prepared: 01/30/2018 Analyzed: 01/31/2018 0.237 0.0500 mg/L 94.9 80-120 20 Spike Source %REC RPD Result RL Units Level Result %REC Limits RPD Limit Notes ND 100 Prepared: Analyzed: 01/31/2018 mg/kg 4.96 .5-110 50 U Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 6 of 8 0MICROBAC' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0694 Laboratory FAY: Microbac Laboratories, Inc. - Fayetteville Definitions Cooler Receipt Log Cooler ID: Default Cooler Cooler Inspection Checklist Custody Seals Intact and/or No Evidence of Tampering COC/Labels Agree Received on Ice (or not required) Project Requested Certifications) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments Temp: 4.1 °C Yes Containers Intact Yes Yes Preservation Correct (or not required) Yes Yes North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. All� The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bonnie.sanders@microhac.com 0210712018 12:26 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061970.864.1920 p I www.microbac.com Page 7 Of $ Surrogate or spike compound out of range J: [Undefined] MDL: Minimum Detection Limit RL: Reporting Limit RPD: Relative Percent Difference U: Not detected at or above adjusted sample detection limit Cooler Receipt Log Cooler ID: Default Cooler Cooler Inspection Checklist Custody Seals Intact and/or No Evidence of Tampering COC/Labels Agree Received on Ice (or not required) Project Requested Certifications) Microbac Laboratories, Inc. - Fayetteville 11 Report Comments Temp: 4.1 °C Yes Containers Intact Yes Yes Preservation Correct (or not required) Yes Yes North Carolina DENR NPDES Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. All� The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bonnie.sanders@microhac.com 0210712018 12:26 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061970.864.1920 p I www.microbac.com Page 7 Of $ C7 C m p� i e� m ti. x W n. V 0 N N 2 a ro w X a F Z _, m z C3 cc w 0 j Q N O OD O j co 5 0 �7 6 1 W 4h m (D n O N .-. co W to N CL d C N fA (D ca 9 s co o a a m a d C? x � m N to m r -4 i O a R.C.1 TCLP, PEST y JTCLP, HERB D JTCLP, RCRA m D JTCLP. VOLATILE -0e1 y JTCLP, SEMI -VOL z r y �fA S M V X -n m v n m a 0 c o u n u p tl g z m z m ) Q O 0 3 s 2 w O a -1 + +0 As0 h m m n. V 0 N N 2 a ro w X a F Z _, m z C3 cc w 0 j Q N O OD O PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 1/1/2018 To 2/28/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C {Prior Testing) ❑ A1t.D (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermophilic❑ Beta Ray Gamma Ra ❑ Pasteurization ❑ Class B: Alt. 11 Fecal Density El Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑Compostin L3Aerobic Di estion L3 ..................... Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density NUMber ot Excee- Frequenc of Analysis Sample Type Analytical Tech - inimu Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 4 $6.24714 1300 MPNI Gram 0 imonthl Grab SM 9221 C CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MON per 4 grams total solid (dry weight) vector Attraction KeUTICAOn ("A INUAU ULT .iiu /) - iricase rnuicate atternative pertormea: Alt. l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization[] Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." _ © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the "This determination has been made under my direction and accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier ame and Title (if applicable)(type or print) 5/1 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WWTP Name: Cordova Facility Monitoring Period: From 3/1/2018 To WQ Permit Number: WQ0005135 NPDES Number: NA 4/30/2018 Pathoeen Reduction (15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ ALt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermophilic❑ Beta Ray ❑ Gamma Ra ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density El I Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ I Composting ❑ 1 Aerobic Digestion ❑ Anaerobic Di cstion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level Sludge Pathogen Density `mer ° Excein denre- Frequency of Analysis Sample Type na ytica Tech - Minim Geo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 19 110.2651 570 MPN/ Gram 0 irnonthl Grab SM 9221 C CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 NON per 4 grams total solid (dry weight) Vector Attraction KeauCUOn (13A A% -AC, UZ l .jum t) - rlease mulcam aiLernanve perrormeu: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ I Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying -Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) 0 No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature o Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DFNR FORM PVRF 02T (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WWTP Name: Cordova Facility Monitoring Period: From 5/1/2018 To WQ Permit Number: WQ0005135 NPDES Number: NA 6/30/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) [IAlt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Therm hilic❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B; Alt. (1) Fecal Density El Alt. (2) Process to Signific!atly SignificantlyReduce Pathogens- ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ Aerobic Di estion ❑ Anaerobic Digestion El- If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density Number ol Excee- Frequency of Analysis y Sample Type Analytical Tech - nioue Minim Geo. Mean Maximum Unitsences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 19000 48333.98 130000 MPN/ Gram 0 imonthl Grab SM 9221 C CFU 1000 mpn per gram of total solid (dry WeiLt) Salmonella bacteria (in lieu of fecal coliform 3 N2N per 4 grams total solid (dry wei t v ector Attracuon Keaucuon [1,A INUAU UG 1 .11U t) - ricase inuicate anernauve perrormen: Alt. I (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ 1 Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Apppiiieeerr Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (12/2006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 7/1/2018 To 8/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate Ievel achieved and alternative performed: Class A: Alt. A (time/temp) ❑ IT Alt B (Alk Treatment) © Alt. C (Prior Testing) ❑ ARD (No Prior Test) ❑ Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment[] Thermophilic❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density El Alt. (2) Process to Significantly Reduce Patho ens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ :.:. ..........;.,._ Anaerobic Digestion 11 ..:.......:...:...::..:....:. .:..., .,... I . ...... I ............. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample Type Analytical Tech - Minimum Geo. Mean Maximurri Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 860 18898.41 200000 MPN/ Gram 0 imonthl Grab SM 9221 C CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) vector Attracnon meaucnon (1,A .NUAl: ULT .11U-/) - rtease maicate alternanve performed: Alt.1 (VS reduction) ❑ Alt. 2 (40 -day bench) I Alt. 3 (30 -day bench) ❑ Alt. 4 (Spec- Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ JAlt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El INo vector attraction reduction alternatives were perforated ❑ CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the J vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer Name and Title (type or print) Land Applier a and Title (if applicable)(type or print) (��K :;�) cc, --,/ � Z_/_ -/If Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WQ Permit Number: WQ0005135 WWTP Name: Cordova Facility NPDES Number: NA Monitoring Period: From 9/1/2018 To 10/31/2018 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (timehem) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) D A1t.D (No Prior Test) ❑ I Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ Thermophilic❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density El Alt. (2) Process to Sigpificantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air ]2E&g ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic Digestion ❑ .... , . .. _ .. If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- Frequency of Analysis Sample T Type Analytical Tech - nioue inim Geo. Mean MaximumUnits Fecal Coliform 2 x 10 to the 6th power per gram of total solids NTN CFU 1000 mpn per grain of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) < 0.6 NA C 0.6 GraNin's 0 imonthl3 Grab E PA 682 Vector Attraction Reduction (15A iNUAU UZ I .11W) - riease inaicate aiternauve perrormea: Alt. l (VS reduction) ❑ Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ Alt. 4 (Spec. 02 uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ I Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed El CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparqr Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) (:2�-, )- -2- 71C "-et Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: von Drehle Corporation WWTP Name: Cordova Facility Monitoring Period: From 10/1/2018 To WQ Permit Number: NPDES Number: 12/31/2018 WQ0005135 NA Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ I Alt B (Alk Treatment) ❑ I Alt. C (Prior Testing) El Alt.D (No Prior Test) ❑ 1 Process to Further Reduce Pathogens ❑ If applicable to alternative performed (Class A only) indicate `Trocess to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment❑ I Thermophilic❑ Beta Ra ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alt. (1) Fecal Density El I Alt_ (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ 1 Aerobic Digestion ❑ Anaerobic Digestion ❑ .. ..:.....::...:.:... ;:...............:...... - If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number of Excee- Frequency of Analysis Sample Type Analytical Tech - inimGeo. Mean Maximumences Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN CFU 1000 mpn per gram of total solid (dry wei ht Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry wei t < 0.6 NA < 0.6 41 Gr ms 0 imonthl Grab PA 1682 Vector Attraction Reduction (15A NCAU UZ .11W) - rlease indicate alternative pertormea: Alt. l (VS reduction) 13 Alt. 2 (40 -day bench) ❑ Alt. 3 (30 -day bench) ❑ JAIL 4 (Spec. Oz uptake) ❑ Alt. 5 (14 -Day Aerobic) ❑ Alt. 6 (Alk. Stabilization❑ Alt 7 (Drying - Stable) ❑ jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) El No vector attraction reduction alternatives were performed D CERTIFICATION STATEMENT (please check the appropriate statement) ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." © "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Mr. Chris Fowler, Facility Manager Mr. Chris Fowler, Land Application ORC Preparer me and Title (type or print) Land Ap ier Nance and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (1212006) FECAL COLIFORM AND SALMONELLA DOCUMENTATION Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jan -18 Microbac Laboratories Lab # Date Analyzed Most Probable Number per gram Log 1 1/24/18 1,300 3.114 2 1/24/18 200 2.301 3 1/24/18 43 1.633 4 1/24/18 270 2.431 5 1/24/18 4 0.602 6 1/24/18 140 2.146 7 1/24/18 21 1.322 Totall 13.550 Averagel 1.936 Most Probable Number / Gram 86 Fecal Coliform Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. OMICROBAC@ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0665 Von Drehle Corporation Project Name: Sludge Sample - Class B Mr. Chris Fowler Project I PO Number: 2030767 126 First Street Received: 01/24/2018 Cordova, NC 28330 Reported: 02/02/2018 lalytical Testing Parameters Client Sample ID: 1 Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-01 Collection Date: 01/24/2018 11:26 Client Sample ID: 2 Sample Matrix: Solid Collected By: Marin Lab Sample ID: KBA0665-02 Collection Date: 01/24/2018 11:28 Result RL Units Note Prepared Analyzed Lab Method: SM 2540 G-2011 Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Units Note Coliform, Fecal 200 % Solids 43.0 1.00 % B,Y 01/25/18 1348 FAY General Microbiology Result RL Units Note Prepared Analyzed Lab Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 1300 2.0 MPNIg 01/25/18 0851 FAY Client Sample ID: 2 Sample Matrix: Solid Collected By: Marin Lab Sample ID: KBA0665-02 Collection Date: 01/24/2018 11:28 RL Result Method: SM 2540 G-2011 Lab % Solids 40.6 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Units Note Coliform, Fecal 200 RL Units Note Prepared Analyzed Lab 1.00 % By 01/25/18 1348 FAY RL Units Note Prepared Analyzed Lab 2.0 MPNIg 01/25/18 0851 FAY Client Sample ID: 3 Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-03 Collection Date: 01/24/2018 11:30 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 Result RL Units Note Prepared Analyzed Lab Method: SM 2540 G-2011 % Solids 39.1 1.00 % BY 01/25/18 1348 FAY General Microbiology Result RL Units Note Prepared Analyzed Lab Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 43 2.0 MPNIg 01/25/18 0851 FAY Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 VM1CROBAC'& Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0665 Client Sample ID: 4 Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-04 Collection Date: 01124/2018 11:32 Result Method: SM 2640 G-2011 % Solids 41.1 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 603 Coliform, Fecal 270 RL Units Note Prepared Analyzed Lab 1.00 % B,Y 011251181348 FAY RL Units Note Prepared Analyzed Lab 2.0 MPNIg 01/25/18 0851 FAY Client Sample ID: 5 Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-05 Collection Date: 01/24/2018 11:34 Client Sample ID: 6 Sample Matrix: Solid Collected By: Poythress Lab Sample ID: K8A0665-06 Collection Date: 01/24/2018 11:36 Result RL Units Note Prepared Analyzed Lab Method: SM 2540 G-2011 FAY % Solids 39.6 1.00 % % Solids 41.9 1.00 % B,Y 01/25/18 1348 FAY General Microbiology Result RL Units Note Prepared Analyzed Lab Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal a4.0 4.0 MPNlg 01/25/18 0851 FAY Client Sample ID: 6 Sample Matrix: Solid Collected By: Poythress Lab Sample ID: K8A0665-06 Collection Date: 01/24/2018 11:36 Note Prepared Analyzed Result RL Units Method: SM 2640 G-2011 Lab 01/25/18 0851 FAY % Solids 39.6 1.00 % General Microbiology Result RL Units Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 140 2.0 MPN1g Note Prepared Analyzed Lab B,Y 01/25/18 1348 FAY Note Prepared Analyzed Lab 01/25/18 0851 FAY Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4 V M I C R O BAC-' Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8A0665 Client Sample ID: 7 Sample Matrix: Solid Collected By: Poythress Lab Sample ID: K8A0665-07 Collection Date. 01/24/2018 11:38 Client Sample ID: Geometric Means Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-08 Collection Date: 01/24/2018 General Microbiology Result RL Units Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 85 2.0 MPNIg Laboratory FAY: Microbac Laboratories, Inc. - Fayetteville Note Prepared Analyzed Lab 02/62/18 1143 FAY Definitions B: Detected in the associated Method Blank RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certificadon(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bvnnie.sanders@micrvbac.wm 02/02/2018 15:45 Microbac Laboratories, Inc. 2592 Hope Mills Rd 1 Fayetteville, NC 283081910.864.1920 p I wwwmicrobac.com Page 3 of 4 Result RL Units Note Prepared Analyzed Lab Method: SM 2540 G-2411 % Solids 36.9 1.00 % B,Y 01/25/18 1348 FAY General Microbiology Result RL Units Note Prepared Analyzed Lab Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 21 2.0 MPNIg 01/25/18 0851 FAY Client Sample ID: Geometric Means Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8A0665-08 Collection Date: 01/24/2018 General Microbiology Result RL Units Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 85 2.0 MPNIg Laboratory FAY: Microbac Laboratories, Inc. - Fayetteville Note Prepared Analyzed Lab 02/62/18 1143 FAY Definitions B: Detected in the associated Method Blank RL: Reporting Limit Y: This analyte is not on the laboratory's current scope of accreditation. Project Requested Certificadon(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager in the footnote are present and an authorized signature is included. bvnnie.sanders@micrvbac.wm 02/02/2018 15:45 Microbac Laboratories, Inc. 2592 Hope Mills Rd 1 Fayetteville, NC 283081910.864.1920 p I wwwmicrobac.com Page 3 of 4 2 � 3 � Go 0 � 2 � � � k � LL � � � A x Cb C%j 4 Logo 11— @ � Im �■ ��■ � 2 g u� IT @ m & 0 f � ! ■ I § 60 G f ƒ �. _ \in 0 2\ � tv � � k , W $ ■ ■ 2 _ § I z $ I N § a LO LL IL 0Lu 0 ` Lo � � $ U. 0 w a � m� ] U- U. U- U- LL U- § o j . _ $ e k E 2 O J § B 2 � � k 0 ■ g � E G8 § ƒ. 77 L § &§ G2 ■ � � B 66k § 2�_ §« & §0 Q Lo LLo _ 11— @ � . �■ ��■ � C14 IT @ m & K � ! ■ I 60 �. _ n p � tv � � k , W $ ■ ■ Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Mar -18 Microbac Laboratories Lab # Date Analyzed Most Probable Number per gram Log 1 3/14/18 19 1.279 2 3/14/18 130 2.114 3 3/14/18 120 2.079 4 3/14/18 43 1.633 5 3/14/18 570 2.756 6 3/14/18 88 1.944 7 3114/18 310 2.491 Totall 14.297 Averagel 2.042 Most Probable Number / Gram 1 110 Fecal Coliform Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. OMICROBAC@ Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8CO415 Von Drehle Corporation Project Name: Sludge Sample - Class B Mr. Chris Fowler Project/ PO Number: 2030767 126 First Street Received: 03/14/2018 Cordova, NC 28330 Reported: 03/20/2018 Analytical Testing Parameters Cllent5amplelD: 1, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: KBC0415-01 Collection Date: 03/14/2018 11:45 Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-02 Collection Date: 03/14/2018 11:47 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 Analyst Method: SM 2540 G-2011 % Solids 41.4 1.00 % 03/15/18 1546 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Result RL Units Note Prepared Coliform, Fecal 19 2.0 MPNIg 03114/18 1620 JR Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-02 Collection Date: 03/14/2018 11:47 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, INC 283061910.864.1920 p I www.microbac.com Page 1 Of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 38.8 1.00 % 03/15/18 1546 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 130 2.0 MPNIg 03/14/18 1620 JR Client Sample ID: 3, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-03 Collection Date: 03/14/2018 11:49 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 42.1 1.00 % 03/15/18 1548 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 120 2.0 MPNIg 03114/18 1620 JR Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, INC 283061910.864.1920 p I www.microbac.com Page 1 Of 4 OMICROBAC`. Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8C0415 Client Sample ID: 4, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: KBC0415-04 Collection Date: 03/14/2018 11:51 Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-05 Collection Date: 03/14/2018 11:53 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 39.1 1.00 % 03/15/18 1546 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 603 Coliform, Fecal 43 2.0 MPNIg 03/14/18 1620 JR Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-05 Collection Date: 03/14/2018 11:53 Client Sample ID: 6, grab Sample Matrix: Solid Collected By: Marin Lab Sample ib: K8C0415-06 Collection Data: 03/14/2018 11:55 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 42.3 1.00 % 03/15/18 1546 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 570 2.0 MPNIg 03/14/18 1820 JR Client Sample ID: 6, grab Sample Matrix: Solid Collected By: Marin Lab Sample ib: K8C0415-06 Collection Data: 03/14/2018 11:55 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2640 G-2011 % Solids 37.6 1.00 % 03/15/18 1546 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 603 Coliform, Fecal 88 2.0 MPNIg 03/14/18 1620 JR Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4 OMICROBACO Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS KBC0415 Client Sample ID: 7, grab Sample Matrix: Solid Collected By: Marin Lab Sample ID: K8C0415-07 Collection Date: 03/14/2018 11:57 Method: SM 2540 G-2011 % Solids General Microbiology Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal Client Sample ID: Geometric Means Sample Matrix: Solid Lab Sample ID: K8C0415-08 Result RL Units Note Prepared Analyzed Analyst 42.0 1.00 % 0311511 a 1548 Result RL Units Note Prepared Analyzed Analyst 310 2.0 MPNIg 031141181620 JR General Microbiology Result RL Units Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 110 2.0 MPNIg Definitions RL: Reporting Limit Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 Collected By: Marin Collection Date: 03/2012018 Note Prepared Analyzed Analyst 03/20/18 1038 03/20/18 1035 JTL North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. Aul� The data and information on this, and other accompanying documents, represents Bonnie K. Sanders only the sample(s) analyzed. This report is incomplete unless all pages indicated in the footnote are present and an authorized signature is included. Senior Project Manager donnie.sanders(omicxohac,com 03/20/2018 11:25 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 28306 ; 910.864.1920 p I www.microbac.com Page 3 of 4 #pt7,aL k k O 2 � � ƒ k 2 k 0 _ CV N C b k � LL �� M w O U W � } O O CO) � U LL O Z_ « Z U O k � % / | ■ ■ � g ; � k0 2 o m a Nr o co k � ! � ! d � � | z ¥� \ $ a 2 k/ E k m L 0} m 0 o o< e , . E v I£ z� 2 2 U)¢ LU m o o w LL Ix 0 0 . L � � ¢ 3 O w � � 1L LL LL ± L LL LL 2 . o _ . . f - CD§ a. § / / S § ƒ ...00, 0 k L ` ? / 0 / 0. — 0 Q§ .. �� �� ® § � CD §�'' �■ - 0 ,§ §E 6 Ga R § ) — (N m # m o r - a q B 5 ® � v § kLLJ § d � k 0 ! } 1 | V- & O k � % / | ■ ■ � � 2 q Nr o co k k ! � ! � � | � ■ ■ _ m L ¥ , . E Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 May -18 Microbac Laboratories Lab # Date Analyzed Most Probable Number per gram Log 1 5/29/18 19,000 4.279 2 5/29/18 84,000 4.924 3 5/29118 51,000 4.708 4 5/29/18 56,000 4.748 5 5/29/18 130,000 5.114 6 5/29/18 40,000 4.602 7 5/29/18 26,000 4.415 Totall 32.790 Averagel 4.684 Most Probable Number / Gram 1 48,334 Fecal Coliform Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. VMICROBAC® Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8E0504 Von Drehle Corporation Project Name: Sludge Sample - Class B Mr. Chris Fowler Project 1 PO Number: 2030767 126 First Street Received: 05/29/2018 Cordova, NC 28330 Reported: 06/11/2018 Analytical Testing Parameters Client Sample ID: 1, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-01 Collection Date: 05/29/2018 15:40 Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-02 Collection Date: 05/29/2018 15:40 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 41.5 1.00 % 05/31/18 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 19000 2.0 MPNIg 05/30/18 1202 JR Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-02 Collection Date: 05/29/2018 15:40 Client Sample ID: 3, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-03 Collection Date: 05/29/2018 15:40 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 41.5 1.00 % 05/31/18 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 84000 2.0 MPNIg 05130!18 1202 JR Client Sample ID: 3, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-03 Collection Date: 05/29/2018 15:40 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 43.3 1.00 % 05/31/18 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPNj, 24hr. 503 Coliform, Fecal 51000 2.0 MPNIg 05/30/18 1202 JR Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 (5>MICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8E0504 Client Sample ID: 4, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-04 Collection Date: 05/29/2018 15:40 Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-05 Collection Date: 06129/2018 15:40 Result Method: SM 2540 G-2011 % Solids 41.4 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 130000 RL Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 MT RL Units Note Prepared Analyzed Analyst % Solids 42.6 1.00 % 05/31/18 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 56000 2.0 MPNIg 05/30/18 1202 JR Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-05 Collection Date: 06129/2018 15:40 Result Method: SM 2540 G-2011 % Solids 41.4 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 130000 RL Units Note Prepared Analyzed Analyst 1.00 % 05131118 1133 MT RL Units Note Prepared Analyzed Analyst 2.0 MPNIg 051301181202 JR Client Sample ID: 6, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-06 Collection bate: 05/29/2018 15:40 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 42.3 1.00 % 05131118 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 40000 2.0 MPNIg 05/30/18 1202 JR Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4 (5>MICR0BAC` Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8E0504 Client Sample ID: 7, grab Sample Matrix: Solid Lab Sample ID: K8E0504-07 Collected By: Wright Collection Date: 05/29/2018 15:40 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 42.2 1.00 % 05/31/18 1133 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 603 Coliform, Fecal 26000 2.0 MPNlg 05/30/18 1202 JR Client Sample ID: Geometric Means Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8E0504-08 Collection Date: 05/29/2018 General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 48000 2.0 MPNlg 05/30/18 1202 JR Definitions RL: Reporting Limit Project Requested Certification(s) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted.. The data and information on this, and other accompanying documents, represents Jeanne Overstreet only the sample(s) analyzed. This report is incomplete unless all pages indicated Client Relationship Specialist, Environmental in the footnote are present and an authorized signature is included. jeanne.overstreel@microbaacom 06/1112018 12:37 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 3 of 4 to V) co U Z m U! LO N O IL W o Y� D U LL 0 vJ V u 0 u r� rLi O v 0 z r s a F + e + z R! a o W n n u n n e( to U O 1L W T-- N O W lew:j IL LL U LL ti LL m O F F , W W N- ir C UQO g N [17 w ` r � CO go F W 8 2E 09 d c v 12 12ob I -Li $� p o0 Sm 7 N Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Jul -18 Microbac Laboratories Lab # Date Analyzed Most Probable Number per gram Log 1 7/13/18 8,200 3.914 2 7/13/18 84,000 4.924 3 7/13/18 200,000 5.301 4 7/13/18 130,000 5.114 5 7/13/18 43,000 4.633 6 7/13/18 1,300 3.114 7 7/13/18 860 2.934 Totall 29.935 Averagel 4.276 Most Probable Number / Gram 1 18,898 Fecal Coliform Fecal Coliform values are less than 2,000,000 and meets the Class B pathogen reduction requirement Data provided in this summary have been used for the values and geometric means reported on the Annual Pathogen and Vector Attraction Reduction Form for this land application event. (VMICROBAC'v Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8G0087 Von Drehle Corporation Project Name: Sludge Sample - Class B Mr. Chris Fowler Project 1 PO Number: 2030767 126 First Street Received: 07/10/2018 Cordova, NC 28330 Reported: 07/19/2018 lalytical Testing Parameters Client Sample ID: 1, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8GO087-01 Collection Date: 07/10/2018 11:57 Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-02 Collection Date: 07/10/2018 11:57 Result RL Units Note Prepared Analyzed Analyst Method: SM 2640 G-2011 % Solids 39.5 % Solids 40.1 1.00 % 07/13/18 1618 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 84000 2.0 MPNIg 07/11/18 1054 JR Coliform, Fecal 8200 2.0 MPNIg 07111118 1054 JR Client Sample ID: 2, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-02 Collection Date: 07/10/2018 11:57 Client Sample ID: 3, grab Sample Matra: Solid Collected By: Wright Lab Sample ID: K8G0087-03 Collection Date: 07/10/2018 11:59 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 Method: SM 2540 G-2011 % Solids 39.5 1.00 % 07/13/18 1618 General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 603 Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 84000 2.0 MPNIg 07/11/18 1054 JR Client Sample ID: 3, grab Sample Matra: Solid Collected By: Wright Lab Sample ID: K8G0087-03 Collection Date: 07/10/2018 11:59 Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 39.3 1.00 % 07/13/18 1618 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 200000 2.0 MPNIg 07/11/18 1054 JR Microbac Laboratories, Inc. 2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 1 of 4 (5>M1CR0BAC% Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8G0087 Client Sample ID: 4, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-04 Collection Date: 07/10/2018 11:59 Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KBG0087-05 Collection Date: 07110/2018 11:59 Result Method: SM 2540 G-2011 % Solids 39.2 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 43000 RL Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 MT RL Units Note Prepared Analyzed Analyst % Solids 39.0 1.00 % 07/13/18 1618 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 130000 2.0 MPNIg 07/11/18 1054 JR Client Sample ID: 5, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: KBG0087-05 Collection Date: 07110/2018 11:59 Result Method: SM 2540 G-2011 % Solids 39.2 General Microbiology Result Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 43000 RL Units Note Prepared Analyzed Analyst 1.00 % 07/13/18 1618 MT RL Units Note Prepared Analyzed Analyst 2.0 MPNIg 07/11/18 1054 JR Client Sample ID: 6, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-06 Collection Date: 07/10/2018 12:02 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbse.com Page 2 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 39.0 1.00 % 07113/18 1618 MT General Microbiology Result RL Units Nobe Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 1300 2.0 MPNIg 07/11/16 1054 JR Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbse.com Page 2 of 4 OMICROBAC" Microbac Laboratories, Inc. - Fayetteville CERTIFICATE OF ANALYSIS K8GO087 Client Sample ID: 7, grab Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-07 Collection Date: 07/10/2018 12:02 Client Sample ID: Geometric Means Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-08 Collection Date: 0711012018 General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 19000 2.0 MPNIg 07/11/18 1054 JR Definitions RL: Reporting Limit Project Requested Certifications) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. <i ��r The date and information on this, and other accompanying documents, represents Jeanne Overstreet only the sample(s) analyzed. This report is incomplete unless all pages indicated Client Relationship Specialist, Environmental in the footnote are present and an authorized signature is included. jeanne.overstreetiffimicrobac.com 0711 812015 10:27 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 3 of 4 Result RL Units Note Prepared Analyzed Analyst Method: SM 2540 G-2011 % Solids 38.1 1.00 % 07/13/18 1618 MT General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 860 2.0 MPNIg 07/11/18 1054 JR Client Sample ID: Geometric Means Sample Matrix: Solid Collected By: Wright Lab Sample ID: K8G0087-08 Collection Date: 0711012018 General Microbiology Result RL Units Note Prepared Analyzed Analyst Method: SM 9221 C E-2006 (MPN), 24hr. 503 Coliform, Fecal 19000 2.0 MPNIg 07/11/18 1054 JR Definitions RL: Reporting Limit Project Requested Certifications) Microbac Laboratories, Inc. - Fayetteville 11 North Carolina DENR NPDES Report Comments Reviewed and Approved By: Samples were received in proper condition and the reported results conform to applicable accreditation standard unless otherwise noted. <i ��r The date and information on this, and other accompanying documents, represents Jeanne Overstreet only the sample(s) analyzed. This report is incomplete unless all pages indicated Client Relationship Specialist, Environmental in the footnote are present and an authorized signature is included. jeanne.overstreetiffimicrobac.com 0711 812015 10:27 Microbac Laboratories, Inc. 2692 Hope Mills Rd I Fayetteville, NC 283061910.864.1920 p I www.microbac.com Page 3 of 4 co 0 c+1 OD N U Z as '5 a� fA rL O z C) UD N 0 Ix u 0 19 U W U) U. 0 I jig v 0 w qo I a N 'V' V + e } N� 0. C oza�r + E 0ao 0 Q o =p r ih LA m Z Z N Ip o C p W 11 a ➢ 11 11 11 d to U 0 w >L � Ul � n a U a It O za Imazi Il V- I- LL U- LL U. fl ■ D t L U_Lu ra �o LL V p LL r Vco tp ILO 0 �� w 0 Uz U V- 6� c N C J N Rh iF Lo 0 1 - IL a us o m E' N 4 F N N '� 4h l0 LL �J CD 2 O N 0 U � � qo a N 'V' t0 00 e C 4 M E 0 r ih LA !+ C p @ R .J Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Sep -18 Biological Consulting Services Lab # Date Analyzed Primary Value Salmonella MPN per ml Secondary Value Salmonella MPN per 4 grams Dry 1809056 9114118 < 0.07 < 0.6 1809057 9114118 < 0.07 < 0.6 1809058 9114/18 < 0.07 < 0.6 1809059 9114118 < 0.07 < 0.6 1809060 9114118 < 0.07 < 0.6 1809061 9/14118 < 0.07 < 0.6 1809062 9/14/18 < 0.07 < 0.6 Exceedances 1 0 All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. Inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. September 14, 2018 Robert Branch Branch Residuals and Soils 8646 W. Market St. Suite 111 Greensboro NC 27409 336-510-0340 bbranch@branchrs.com Client ID: VD -1, VD -2, VD -3, VD -4, VD -5, VD -6, VD -7 BCS ID: 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova NA alysis IMethod monella JEPA 1682; BCS SOP M-4 (15017025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, -I L"-��l L& Bonnie Mull, MPH Laboratory Operations Manager Page i of 8 Final Report BCS ID 1809056,1849057,1809058,1809059,1809060,1809061,1809062 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT HE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -1 Sample Date/Time: September 10, 2018 13:33 BCS Sample ID: 1809056 Sample Description: Biosolids Date Received: September 11, 2018 09:26 Amount Submitted:100mi bottle 96 Solids: 42.3 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -2 Sample Date/Time: September 10, 2018 13:37 BCS Sample ID: 1809057 Sample Description: Biosolids Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 40.6 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1809056,1849057,1809058,1809059,1809060,1809061,1809062 BCS LABORATORIES, INC. — GAINESVIL.L.E 4609 NW 6TH STREET, STE. A, GAINESV[LLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP## 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ��S"� a{{htb,tto Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -3 Sample Date/Time: September 10, 2018 13:41 BCS Sample ID: 1809058 Sample Description: Biosolids Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 39.3 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed ,I Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units ' Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -4 Sample Date/Time:September 10, 2018 13:45 BCS Sample ID: 1809059 Sample Description: Biosolids Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 41.4 Amount Analyzed: 30.00 g Analysis Start: September 11, 2018 09:40 Analyst: Greta Pallack, B.A. Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Stop Date: September 14, 2018 11:10 Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3of8 Fina[ Report BCS ID 1809056, 1809057, 1809058,1809059,1809060,1809061,1809062 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES. COM FL DOH #E82924, ISO/IEC 17025:2005 L.2422 (ANAB), PA DER# 68-03950, EPA# F'LO 1 147 TH[S REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT TME WRITTEN CONSENT OF BCS LABORATORIES ot"I'gn '•� J }v ate'—� ' 3' Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -5 Sample Date/Time: September 10, 2018 13:47 BCS Sample ID: 1809060 Sample Description: Bliosolids Date Received: September 11, 2018 09:26 Amount Submitted:100mi bottle % Solids: 40.9 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.6 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -6 Sample Date/Time: September 10, 2018 13:50 BCS Sample ID: 1809061 Sample Description: Biosolids Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 40.1 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Valve: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4of8 Final Report BCS 10 1809056, 1809057,1809058,1809059,1809060,1809061,1809062 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROSIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 6&03950, EPA# FLO 1 147 THIS REPORT SHALL, NOT HE REPRODUCED, EXCEPT W FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES n AAWI wecwio,rao �. ~, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NA Client Sample ID: VD -7 Sample Date/Time: September 10, 2018 13:52 BCS Sample ID: 1809062 Sample Description: Biosollds Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 39.5 Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams (Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 1809056, 1809057, 1809058, 1809059, 1809060, 1,909061, 1809062 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW. MICROBIOSERV[CES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES e %\ AAM s .teweu+tiaa Client: Branch Residuals and Soils Project: Cordova NA Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #EB2924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES f At" I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date. . September 14, 2018 Page 7 of 8 Final Report BCS ID 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.M[CROBIOSERV[CES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES 'y �jAL[latoiL 6 DATA QU ALI FIER CODES SYMBOQMEANING _ B "Results based on counts outside the acceptable range. - Sample received without prior notification or delayed delivery. Analysis performed outside of X j associated method required QC data set (1 QC data set per 20 samples -per 168 hours). �- --� _ I rValue is between the laboratory method detection limit & laboratory practical quantitation limit. J1_ -;The sample matrix Interfered with the ability to make any accurate determination. M J2 No Quality Control criteria exist for the component. J3 !:The data are questionable because of improper laboratory or field protocols. _ L Off scale high. Actual value is known to be greater than value given. Presumptive evidence for the presence of material. There is an indication that the analyte is present, i N _ 1{ i but the confirmation requirement was not met. 0 Sampled, but analysis not performed - Q Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected. The specified component was not —� `detected. The reported value is the method detection limit. an V Analyte was detected in both sampled associated method blank. Data -- — -- Y- _._..,...-.---- -- -- � - _ -- may not be accurate. Y The laboratory analysis was from an improperly preserved sample. The data mav not be accurate. I Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that ' can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. ^ BCS is not currently accredited for this analyte. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A. GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES. COM FL DOH #1^82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 66-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES n�^I'Vn .`�W`J k RCt Mtb,teu y � m � = 3 C. � CJS O M � m O d C j .J rn ID rh m t ma `m m a � 07 g n` '� CL in �,� ZEA M C d' � Z �01 R A y .• Date Sampled Time Sampled No. of containers shipped Grab Composite Field Filtered FH at election -emnarsture at collection I frozen too packs �9 ' Groundwater C) n aro Wastewater w � 3 e � J J N 0NIL1 0 a a n o Blosolld/Sludge/Soli (circle) O s y• � � c i� � m O d C j .J rn ID rh m t ma `m m a � 07 g n` '� CL in �,� ZEA M C d' � Z �01 R A y .• Date Sampled Time Sampled No. of containers shipped Grab Composite Field Filtered FH at election -emnarsture at collection I frozen too packs �9 ' Groundwater C) n Wastewater � 3 e � J J N 0NIL1 0 1i 1"V+" o Blosolld/Sludge/Soli (circle) O s y• 1. � � Other (specify): F 1_ T m W a o m o c Cutlure EntemvlruseslEnteric virus to ge in CD P4 a m or EPA 1816 enterovirus d m d m h7 7 0 aCLEPA UP 1615 Noroviruses O H 3 a H Cryptosporldium & Glardia N E. coli � m O d C j .J rn ID rh m t ma `m m a � 07 g n` '� CL in �,� ZEA M C d' � Z �01 R A y .• Date Sampled Time Sampled No. of containers shipped Grab Composite Field Filtered FH at election -emnarsture at collection I frozen too packs Total Coliform y Yeast & Mold Fecal coliform sA Helminth Ove Plate Count 11acterla (HPC) Salmonella spp M AJ t Legionella (Culture or Genetic) fowieri TAT (Fee Applies) P N p rn 0 ro 01 X 0 700 v �9 ' Groundwater C) n Wastewater � m Drinking Water 0 1i 1"V+" o Blosolld/Sludge/Soli (circle) O s M I OV � 0 N Other (specify): g o{ a o m o c Cutlure EntemvlruseslEnteric virus to ge in CD P4 a m or EPA 1816 enterovirus d m d m h7 7 0 aCLEPA UP 1615 Noroviruses O H 3 a H Cryptosporldium & Glardia in E. coli Total Coliform y Yeast & Mold Fecal coliform sA Helminth Ove Plate Count 11acterla (HPC) Salmonella spp M AJ t Legionella (Culture or Genetic) fowieri TAT (Fee Applies) P N p rn 0 ro 01 X 0 700 v �9 C) n � O 0 1i 1"V+" tD 0 N Cn W A. Z" Q a ElZ 0 Von Drehle Corporation Cordova, NC City of Rockingham IUP 0015 Nov -18 Biological Consulting Services `Lab # Date Analyzed Primary Value Salmonella MPN per ml Secondary Value Salmonella MPN per 4 grams Dry 1811051 11/9/18 < 0.6 1811052 11/9/18 < 0.07 < 0.6 1811053 11/9/18 < 0.07 < 0.6 1811054 11/9/18 < 0.07 < 0.6 1811055 11/9/18 < 0.07 < 0.6 1811056 11/9/18 <_ 0.07 < 0.6 1811057 11/9/18 < 0.07 < 0.6 Exceedances 0 All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen requirement for distribution. Data provided in this summary have been used for the values reported on the Annual Pathogen and Vector Attraction Reduction Form for Class A and Class B options. Inc. BIOLOGICAL CONSULTING SERVICES �./ OF NORTH FLORIDA, INC. November 15, 2018 Robert Branch Branch Residuals and Soils 8646 W. Market St. Suite 111 Greensboro NC 27409 336-510-0340 bbranch@branchrs.com Client ID: VD -1, VD -2, VD -3, VD -4, VD -5, VD -6, VD -7 BCS ID: 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Cordova NC Anal sis Method Salmonella JEPA 1682; BCS SOP M-4 (15017025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, �7 c9�1��r Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 6803950, EPA# FLO 1 147 THIS REPORT SMALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �' i Y ''� Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -1 Sample Date/Time: November 05, 2018 13:50 BCS Sample ID: 1811051 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 38.3 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: ; l Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard re} pang units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -2 BCS Sample ID: 1811052 Sample Date/Time: November 05, 2018 13:53 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 35.6 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: D Primary Value: !90.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP; 6803950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, Wr7HOUT THE WRITTEN CONSENT OF BCS LABORATORIES d Al�&B �1� wccw[oiido Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -3 Sample Date/Time: November 05, 2018 13:56 BCS Sample ID: 1811053 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 35.8 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units L _ - Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -4 Sample Date/Time: November 05, 2018 14:00 BCS Sample ID: 1811054 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 37.3 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed I Secondary Value: 550.7 Salmonella MPN/4 dry grams I Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW. MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP; 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE wRITTEN CONSENT OF BCS LABORATORIES A " t A M ' ' '}��= wccnco,rro k M}tMpNM4rEM, Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -5 Sample Date/Time: November 05, 2018 14:03 BCS Sample ID: 1811055 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 37.8 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: !90.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams ,Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -6 Sample Date/Time: November 05, 2018 14:06 BCS Sample ID: 1811056 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 37.6 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 09, 2018 12:00 Analyst: Greta Pallack, B.A. Qualifier: U Primary Value: 50.07 Salmonella MPN/mL sample analyzed Secondary Value: :90.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units: Page 4of8 Final Repoli BGS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #EB2924, ESO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, ,EXCEPT IN FULL, wrrHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A + ; ►it Mt o, rb •Ne r\fin �-� 1 Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Cordova NC Client Sample ID: VD -7 Sample Date/Time: November 05, 2018 14:09 BCS Sample ID: 1811057 Sample Description: Biosolids Date Received: November 06, 2018 09:49 Amount Submitted:100ml bottle % Solids: 43.3 Amount Analyzed: 30.00 g Receipt Temperature: 6.0 deg C Preserved: Yes Analysis Start: November 06, 2018 13:20 Analysis Stop Date: November 14, 2018 14:50 Analyst: Greta Pallack, B.A. Qualifier: None Primary Value: 0.07 Salmonella MPN/mL sample analyzed Secondary Value: 0.7 Salmonella MPN/4 dry grams Analysis Notes: None L Page 5 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL,. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DON #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DER# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES N.J 4 wt Cnrb.t�� n7.,h,1u+ x Client: Branch Residuals and Soils Project: Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROSIOSERVICES.COM FL DOH #E82924, ISO/lEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES �5 w i k 4 ' I certify that I have examined I am familiar with the information submitted herein. The results pertain only to analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted documents. The analysis was authorized commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date. , November 15, 2018 Page 7 of 8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056,1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 VAA W.MICROSIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA#F FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES P7s'1'yy g I DATA QUALIFIER CODES SYMBOL ;MEANING B Results based on counts outside the acceptable ranges -� Sample received without prior notification or delayed delivery. Analysis performed outside of X p associated method required QC data set (1 QC data set per 20 samples per 168 hours). I IVa1ue is between the laboratory method detection limit & laboratory practical quantitation limit. J m J1 The sample matrix interfered with the ability to make any accurate determination. J2 No Quality Control criteria exist for the component.�_ J3 W !The data are questionable because of improper laboratory or field protocols.�— _ L Off scale high. Actual value is known to be greater than value given N Presumptive evidence for the presence of material. There is an indication that the analyte is present, i but the confirmation requirement was not met. O - Sampled, but analysis not performed._ Q _ Sample held beyond the accepted holding time. Indicates that the compound was analyzed for but not detected. The specified component was not I U +detected. The reported value is the method detection limit. V _ Analyte was detected in both sample and associated method blank. Data may not be accurate. — 1 Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate. 'Too many colonies present (TNTC); the numeric value given represents the upper end of the value that Z can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. R ** Not reported due to interference. - A 1 BCS is not currently accredited for this analyte, # BCSLab specificqualifier.See _laboratory analysis notes. Page 8of8 Final Report BCS ID 1811051, 1811052, 1811053, 1811054, 1811055, 1811056, 1811057 BCS LABORATORIES, INC. -- GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES AAM.`' I 1 t�+ A w �7 .% � y a v m M 0 Date Sampled a.- m i 3 i :r Time Sampled i i � � o 0i Q -- ym a m -4 t�+ A w �7 .% � y a v m M 0 Date Sampled a.- m n i :r Time Sampled 4YLr1�carip i o 0i Q .v -- ym a m -4 ai O .110 -�L Grab d $ G 261 o 7= 3 j Composite N 4 Field Mitered tl° w w pH at collection PL ° di a $ a o Ne 7hicsulfate r C -I— W -� �y Ice / frozen Ice packs - r Z1 126 in t�+ A w �7 .% � v m M 0 Date Sampled a.- m n i i Time Sampled i i o 0i Q .v -- No. of containers shipped i � ai O .110 -�L Grab d $ G 261 o 7= 3 a Composite 0 4 Field Mitered tl° w w pH at collection emperature at collection 4 Ne 7hicsulfate r C -I— S' �y Ice / frozen Ice packs - r Other (alcilft in Groundwater Wastewater WCn a Drinking Water 70 —47 !r_ i� 8inselidlSludoelSoil fcircl� 1 L l 1 - Other (specify); vulture EntaroviruseslEnteric virus EPA 1615 enterovirus :PA 1815 Noroviruses Iryptosperldium & Giardia E. 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V n 0 m m OCD CL O a a ° V Cr a n m — w 3a a oV �_ C) O V C �a E Co Cal M I— ell •p Z � o o 7 E 0 HfIJ� x • 7 C a g 2 w CL M a a E w o' a 8 M 3 a > C baa L a°rs E. m m C m E co 0 CL O O a o E 3 .a a j m a o p 10 V It V LO 11 V a c00 V CL CL C3 0 r z z c W C O Co cA U ° = E r`D i C Q IL E N N O O CL to 7 I J 7 � a1 C J ro Y E u M U C ro c m n CL c g E CL c) U z CL _ LQ tl e N N M � u a a Ci V Z CCL (0 E = N a n N Z = r a CL I cr � Z a EL a na r 2 � o 9L a o Z W_ M C Z — � Z {0 3 Co 0 � tm1 G p� N as �Z � Y� Mo O g a o.a as QY m w1i w w ii rn m� m � C c m J CL c5PL 0 �0 C �' gm a@ Z� m CL m�Zo '*> N c�MmU ==w WTO N z O z W U W J W LL J N Go 00 a` a mi g o o m — 3a a oV �_ O O V C �a C Q COM M I— ell 7 o 0 HfIJ� 7 C 2 .0 0 i CM o _ CL o' a 8 M m a C baa L z ma 0 0 C O O 0 0 C7 0 0 .a a M o C e v a z z c W C O cA U ° mo C ,g N O O lC E m CL m CL E o a m rn a c E i D C v � Q T E cc Z O a m c C O a of m O C E E E CD 0 r 2018 APPLICATION SUMMARY TABLE 'Z W) O�t 00 QN O) --O N 00 [ Oo N M N O Ln �o w; v) 00 00 Z to 4 �D r � oo O N Nq N t- m N N W y W W w W ra y U5 may+ wL N") 0 V U vCe 0 0 0 U 0 0 SS 0 0 0 0 0 0 0 0 0 0 0 n V0 UD ON 0, � O� to -4 N m 0% T 00 M 00 O to O O O 00 N W)N � �D � 00 � 00 r- O Vl •-y kn O• �0 't 't � Vl N D1 l •-+ N M M M C -; O D O 4 O; 4 V ri gy m= Cl- 110 n 7a (U\ N W)t- kn M O qr �o N O O O M Ln O [-- ID M M V1 00 u M v) N vi %0 %D It O -4 l r. N I --� to "l:O O M l: � 01 � CIN F V M n � do l� � c M 00 O O1 �-�. M %0 •--! N n -1 Gfl 00 In -4 O M M .--i [� cV C kn W �O �--i vi 0< N N W) (3N to -- -- -- N �-- N N N N N N� 4 , 4 N N N N N N Q 0 0 0 0 0 0 0 0 0 O 00 0 0 0 0 0 C C C C C C 0 0 �O0,0,000�rngOa�rnc13, ri O O; ON o a1 01 O O% O O� O� QN kn 00 00 kn kn 00 ao kn kn 00 00 kn 00 D N CA "d- N Nd- N d' N N N T m M 'T M M'T'T M M M* M C M to kn kn .-- O O !� CJ o0 %D N N O i- kn C O �n oo -- M' n O N .-- cV M " �D O C d O L 00 t �D c•1 N O� [ M l- -- oo cV � N 01 [� 01 0\ IT 00 M Ln M O1 .--i M ,--i 01 A .--i 00 � +--i O O �D M " N � 00 M � � N N Vi N oo to 00 M 01 V1 C% N n 00 N N M � [� -- N .-- N N N r" ~ r -i "O o0 00 00 00 0o w 00 00 m 0p o0 00 00 00 W 00 Da 00 M 00 w 00 00 MW O O O O O 0 0 0 O O to 0 0 0 0 0 0 m m N : +-y -I (V M N M .--i 01 00 00 00 N M N M -+ m N kn N "C M to l- 00 f� cn A 2018 APPLICATION CONDITION SUMMARIES von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 19.1 Site/Tract: 4 Application Method: Incorporated Field: 1 Percent Solids: 45 Residual Report No.: va 2018-1 Ms Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 1/25/18 1 176.80 Cool, Fair Dry 0.00 1126118 1 277.70 Cool, Fair Dry 0.00 Total Wet Tons 454.50 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 22.4 Site/Tract: 4 Application Method: Incorporated Field: 3 Percent Solids: 45 Residual Report No.: vd 2018-1 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 1/22/18 3 187.94 wane, cloudy Dry 0.00 1/23/18 3 727.70 cool, Partly cloudy Moist 0.00 1/24/18 3 383.66 warm, Fair Dry 0.00 1/25/18 3 110.50 cool, Fair Dry 0.00 Total Wet Tons 1,409.80 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 53.15 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 45 Residual Report No.: vd 2018-1 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 2/19/18 4 566.85 cool, cloudy Dry 0.00 2/20/18 4 205.92 cool, cloudy Dry 0.00 2/23/18 4 163.87 warm, Fair Dry 0.00 2/26/18 4 435.56 warm, cloudy Moist 0.00 2/27118 4 339.32 Wann, Cloud3 Moist 0.00 2128/18 4 198.26 Cool, Fair Moist 0.00 Total Wet Tons 1,909.78 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 19.2 Site/Tract: 4 Application Method: Incorporated Field: 7 Percent Solids: 45 Residual Report No.: vd 2018-1 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 1/29/18 7 313.61 wane, Cloudy Moist 0.00 1/30/18 7 425.05 warm, Cloudy Moist 0.00 1/31/18 7 0.00 Cool, Partly Cloudy Moist 0.00 2/1/18 7 190.23 cool,Paraycioudy Moist 0.00 2/2/18 7 165.11 ol, Partly Cloi Moist 0.00 2/3118 7 164.22 Cool, Fair Dry 0.00 i i Total Wet Tons 1,258.22 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 18.9 Site/Tract: 4 Application Method: Incorporated Field: 6A Percent Solids: 45 Residual Report No.: Vd 2018-1 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 2/3/18 6A 93.84 Cool, Fair Dry 0.00 2/5/18 6A 96.04 Cool, Cloudy Moist 0.00 2/6/18 6A 271.28 Cool, Fair Moist 0.00 2/20/18 6A 160.16 cool, cloudy Dry 0.00 2/21/18 6A 466.03 Warm, Fair Dry 0.00 2/22/18 6A 152.02 Warm, Fair Dry 0.00 Total Wet Tons 1,239.37 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jan - Feb 2018 von Drehle Paper Farmer: Wayne Belger Acres: 28.9 Site/Tract: 4 Application Method: Incorporated Field: 8 Percent Solids: 45 Residual Report No.: vd 2018-1 Ms Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 217118 8 172.12 cool, Fair Moist 0.00 Total Wet Tons 172.12 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 19.1 Site/Tract: 4 Application Method: Incorporated Field: 1 Percent Solids: 38.9 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Prev. 24 Hour Conditions Rainfall 3/16118 1 387.01 Warm, Fair Dry 0.00 3/19118 1 244.95 Warm, Fair Dry 0.00 3/20118 1 152.044 Warm, Cloud3 Moist 0.00 Total Wet Tons 784.00 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 37.4 Site/Tract: 4 Application Method: Incorporated Field: 2 Percent Solids: 38.9 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Weather Subfield Wet Tons Conditions Soil Conditions Prev. 24 Hour Rainfall 3/20/18 2 65.16 Wann, Cloud3 Moist 0.00 3/21/18 2 0.00 Wann, Cloud3 Moist 0.00 3/22/18 2 473.56 Cool, Cloudy Moist 0.00 3/23/18 2 92.81 0l, Partly Cloi Moist 0.00 3126/18 2 242.50 Cool, Fair Dry 0.00 3/27/18 2 317.02 Cool, Fair Dry 0.00 3/28/18 2 393.97 Cool, Fair Dry 0.00 3/29/18 2 244.01 Warm, Fair Dry 0,00 3/30/18 2 176.59 Warm, Cloud Moist 0.00 4/2/18 2 312.15 Warm, Fair Dry 0.00 Total Wet Tons 2,317.77 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 53.15 Site/Tract: 4 Application Method: Incorporated Field: 4 Percent Solids: 38.9 Residual Report No.: vd 2418-2 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/1/18 4 132.10 Cool, Cloudy Moist 0.00 3/2/18 4 84.07 Warm, Cloud3 Moist 0.00 3/5/18 4 450.36 Cool, Fair Dry 0.00 3/6/18 4 361.14 ol, Partly Clot Dry 0.00 3/13/18 4 352.96 ol, Partly Clot Moist 0.00 3/14/18 4 44.33 0l, Partly Clot Dry 0.00 4/30/18 4 139.70 Warm, Cloud Moist 0.00 Total Wet Tons 1,564.66 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 11.1 Site/Tract: 4 Application Method: Incorporated Field: 5 Percent Solids: 38.9 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Subfield Weather Wet Tons Conditions Soil Conditions Prev. 24 Hour Rainfall 317118 5 44.01 ol, Partly Cloi Dry 0.00 3/8/18 5 427.79 Cool, Fair Dry 0.00 3/9/18 5 196.21 Cool, Fair Dry 0.00 4/30/18 5 45.36 Warm, CIoud3 Moist 0.00 Total W et Tons 713.37 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 28.9 Site/Tract: 4 Application Method: Incorporated Field: 8 Percent Solids: 389 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 4/9/18 8 244.20 Cool, Cloudy Moist 0.00 4/10/18 8 200.43 Cool, Fair Moist 0.00 4/23/18 8 81.44 rm, Partly Clc Moist 0.00 4/24/18 8 354.51 Warm, Cloud Moist 0.00 4/25/18 8 423.49arm, Cloud Moist 0.00 4/26/18 8 181.13 arm, Cloud Moist 0.00 4/27/18 8 135.06 arm, Cloud Moist 0.00 4/30/18 8 22.68 arm, Cloud3 Moist 0.00 Total Wet Tons 1,642.94 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 28.6 She/Tract: 4 Application Method: Incorporated Field: 9 Percent Solids: 38.9 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Prev. 24 Hour Conditions Rainfall 4/10118 9 200.43 Cool, Fair Moist 0.00 4/11/18 9 163.16 Cool, Fair Dry 0.00 4/12/18 9 131.21 Cool, Fair Dry 0.00 4/13/18 9 160.42 Warm, Fair Dry 0.00 4/17/18 9 383.71 Cool, Fair Moist 0.00 4/18/18 9 345.09 Cool, Fair Moist 0.00 4/19/18 9 280.12 Warm, Fair Moist 0.00 4/20/18 9 176.84 Warm, Fair Dry 0.00 4/23/18 9 40.72 nn, Partly Clo Moist 0.00 Total Wet Tons 1,881.70 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Apr - May 2018 von Drehle Paper Farmer: Wayne Belger Acres: 19.3 Site/Tract: 4 Application Method: Incorporated Field: 6B Percent Solids: 38.9 Residual Report No.: vd 2018-2 MB Crop: Soybeans Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 3/12/18 6B 221.51 ol, Partly Cloi Moist 0.00 3/13/18 6B 132.36 ol, Partly Cloi Moist 0.00 3/14/18 6B 0.00 ol, Partly Cloi Dry 0.00 4/2/18 6B 83.24 Warm, Fair Dry 0.00 4/3/18 6B 292.73 , Partly Clo Dry 0.00 4/4/18 6B 116.47 Warm, Fair Dry 0.00 4/9/18 6B 222.00 Cool, Cloudy Moist 0.00 4/30/18 6B 181.44 Warm, Cloud Moist 0.00 Total Wet Tons 1,249.75 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 May - Jun 2018 von Drehle Paper Farmer: Wayne Belger Acres: 22.8 She/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 40.4 Residual Report No.: vd 2018-3 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Soil Conditions Conditions Prev. 24 Hour Rainfall 6126118 1 125.52 Hot, Cloudy Moist 0.40 6127118 1 347.98 Hot, Fair Moist 0.00 Total Wet Tons 473.50 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 May - Jun 2018 von Drehle Paper Farmer: Wayne Belger Acres: 13.2 Site/Tract: 3 Application Method: Incorporated Field: 4 Percent Solids: 40.4 Residual Report No.: A 2018-3 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 6128118 4 153.91 Hot, Fair Moist 0.00 6129118 4 225.83 Hot, Fair Dry 0.00 6130118 4 0.00 Hot, Fair Dry 0.00 Total Wet Tons 379.74 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 May - Jun 2018 von Drehle Paper Farmer: Wayne Belger Acres: 18.9 Site/Tract: 3 Application Method: Incorporated Field: 3A Percent Solids: 40.4 Residual Report No.: vd 2018-3 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 6/20/18 3A 271.57 Hot, Fair Dry 0.00 6/21/18 3A 240.77 Hot, Cloudy Moist 0.43 6/22/18 3A 170.10 Hot, Fair Moist 0.00 6125118 3A 143.01 Hot, Cloudy Moist 0.40 6/26/18 3A 292.88 Hot, Cloudy Moist 0.40 Total Wet Tons 1,118.33 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 May - Jun 2018 von Drehle Paper Farmer: Wayne Belger Acres: 37.2 Site/Tract: 3 Application Method: Incorporated Field: 3B Percent Solids: 40.4 Residual Report No.: vd 2018-3 MB Crop: Rye Date Field No. Subfield Weather Wet Tons Conditions Soil Conditions Prev. 24 Hour Rainfall 6/11/18 3B 461.68 Hot, Fair Dry 0.00 6/12/18 3B 370.86 Hot, Cloudy Moist 0.10 6/13/18 3B 361.67 A, Partly Clou Moist 0.06 6/14/18 3B 249.06 Warm, Fair Moist 0.00 6/15/18 3B 47.00 Hot, Fair Dry 0.00 6/18/18 3B 278.64 Hot, Fair Dry 0.00 6119/18 3B 390.18 Hot, Cloudy Dry 0.05 6/20/18 3B 83.56 Hot, Fair Dry 0.00 1 Total Wet Tons 2,242.65 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 22.8 Site/Tract: 3 Application Method: Incorporated Field: 1 Percent Solids: 29.1 Residual Report No.: vd 20184 Ms Crop: Rye Date Field No. SubfieId Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/31/18 1 323.41 Hot, Cloudy Moist 0.47 8/1/18 1 319.83 Hot, Cloudy Moist 0.14 8/2/18 1 216.37 Wane, Fair Moist 0.00 8/3/18 1 374.82 Warm, Cloud3 Moist 0.60 8/4/18 1 104.11 Wann, Cloud3 Moist 0.32 8/9/18 1 1 113.29 Hot, Cloudy Moist 0.22 Total Wet Tons 1,451.85 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 9.3 Site/Tract: 3 Application Method: Incorporated Field: 2 Percent Solids: 29.1 Residual Report No.: vd 2018-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7125118 2 45.76 Hot, Fair Dry 0.00 7126118 2 157.85 Hot, Fair Dry 0.05 7127118 2 181.89 Hot, Fair Dry 0.00 7128118 2 108.11 Hot, Fair Dry 0.00 Total Wet Tons 493.61 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 13.2 Site/Tract: 3 Application Method: Incorporated Field: 4 Percent Solids: 29.1 Residual Report No.: vd 2018-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/2/18 4 443.50 Hot, Fair Dry 0.00 8/13/18 4 181.47 Hot, Cloudy Moist 0.42 8/14/18 4 22.01 Hot, Fair Moist 0.00 8/17/18 4 184.76 Hot, Cloudy Moist 0.20 8/20/18 4 109.45 Hot, Fair Dry 0.00 Total Wet Tons 941.20 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 11.1 Site/Tract: 3 Application Method: Incorporated Field: 5 Percent Solids: 29.1 Residual Report No.: vd 2018-4 Ms Crop: Rye Date Field No. Subfield Wet Tons Feather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/23118 5 186.64 Hot, Fair Dry 0.00 7/24118 5 399.29 Hot, Fair Dry 0.08 7/25118 5 137.28 Hot, Fair Dry 0.00 Total Wet Tons 723.21 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 18.9 Site/Tract: 3 Application Method: Incorporated Field: 3A Percent Solids: 29.1 Residual Report No.: vd 2018-4 Ms Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/6/18 3A 254.31 Hot, Cloudy Moist 0.20 8/7/18 3A 194.90 Hot, Cloudy Moist 0.02 Total Wet Tons 449.21 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 37.2 Site/Tract: 3 Application Method: Incorporated Field: 3B Percent Solids: 29.1 Residual Report No.: vd 20184 Ms Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 8/9/18 3B 203.77 Hot, Cloudy Moist 0.22 8/10/18 3B 252.60 Hot, Cloudy Moist 0.00 8/13/18 3B 272.59 Hot, Cloudy Moist 0.42 8/14/18 3B 293.76 Hot, Fair Moist 0.00 8/15/18 3B 258.33 Hot, Fair Moist 0.00 8/16/18 3B 232.99 Hot, Fair Moist 0.00 Total Wet Tons 1,514.05 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 24.6 Site/Tract: 3 Application Method: Incorporated Field: 6A Percent Solids: 29.1 Residual Report No.: vd 2018-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/11/18 6A 295.32 Hot, Fair Dry 0.00 7/12/18 6A 324.32 Hot, Fair Dry 0.00 7/13/18 6A 374.29 Hot, Fair Dry 0.02 7/16/18 6A 277.70 Hot, Fair Dry 0.00 7/17/18 6A 231.44 Hot, Fair Dry 0.00 7/18/18 6A 68.58 Hot, Fair Dry 0.00 8/21/18 6A 224.24 Hot, Fair Dry 0.00 8/22/18 6A 229.66 Hot, Fair Dry 0.00 8/23/18 6A 256.89 Hot, Fair Dry 0.00 Total Wet Tons 2,282.45 von Drehle Corporation Cordova, North Carolina Belger Farms WQ0005135 Jul - Aug 2018 von Drehle Paper Farmer: Wayne Belger Acres: 37.5 Site/Tract: 3 Application Method: Incorporated Field: 6B Percent Solids: 29.1 Residual Report No.: vd 2018-4 MB Crop: Rye Date Field No. Subfield Wet Tons Weather Conditions Soil Conditions Prev. 24 Hour Rainfall 7/3/18 6B 251.27 Hot, Fair Dry 0.00 7/5/18 6B 302.69 Hot, Fair Dry 0.00 7/6/18 6B 45.31 Hot, Cloudy Dry 0.04 7/9/18 6B 319.82 Hot, Fair Dry 0.00 7/10/18 6B 327.41 Hot, Fair Dry 0.00 7/18/18 6B 137.16 Hot, Fair Dry 0.00 7/19/18 6B 188.29 Hot, Fair Dry 0.00 7/20/18 6B 138.74 Hot, Fair Dry 0.00 7/23/18 6B 163.31 Hot, Fair Dry 0.00 7/24/18 6B 284.69 Hot, Fair Dry 0.08 8/20/18 6B 246.71 Hot, Fair Dry 0.00 8/21/18 6B 22.01 Hot, Fair Dry 0.00 8/22/18 6B 222.00 Hot, Fair Dry 0.00 8/24/18 6B 199.99 Hot, Fair Dry 0.00 Total Wet Tons 2,849.41