WQ0039924_2018 Residual Annual Report_20190314

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0039924
SUBMITTAL DATED: 2/27/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Robert T. Branch
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0039924
Permittee * Von Drehle Corporation
Facility Name * Von Drehle Corporation Cordova, NC
Phone Number*
336 312-9007
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
vd 2018 class a ar.pdf 1019.44KB
upload only 1 RDF docurrent. NUltiple docurrents must be corrbined into one RDF file.

For neiv and modif cation permit applications, the paper copy is required to be submitted to the
Di,,isiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ping:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,,ision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942 M
512 N_ Salisbury St_ Raleigh, NC 27604
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
* I40 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/27/2019

F�;
Branch Residuals: & So11s, LLC
8646 West Market Street, Siiite 111- Greensboro, NC 27409
PHONE [phone] • FAX [phone]
RECEIVEDINCDEOIDWR
Letter of Transmittal
To: NCDENR Information Processing Section
From: Bob Branch
CC:
Date: 2/27/2019
Re: von Drehle 2018 Class A Annual Land Application Report Permit No. WQ0039924
The following copies of this report have been sent to you: .
FEB 2 8 2019
Non -Discharge
Permitting Unit
• WCDENR/Aquifer Protection Section/Infomiation Procession Unit-1 copy+ 1 electronic, .
• Von Drehle — 2 copies, and
• Wayne Belger —I copy (sent to von Drehle).
Please give me a call at (336)"3,12-9007 if you have any questions.,
Robert T. Branch
RECEIVED
DEQIDWR
MAR 18 20.19
WO-ROS
FAYETTEVILLE; ;EGIONX6r—F10E
RFrPI\/RD
FEB 2 8 2019
DWR SECTION
INFORMATION PROCESSING UNIT

2018 ANNUAL REPORT
VON DREHLE CORPORATION
FIBER CLAY RESIDUAL
CORDOVA, NORTH CAROLINA
PERMIT #WQ0039924
Prepared For:
Von Drehle Corporation
126 First Street
Cordova, N.C. 28330
Prepared By:
Branch Residuals & Soils, LLC
8646 West Market Street- Suite 111
Greensboro, North Carolina 27409
February 2019

BRANCH RESIDUALS & SOILS, LLC
8646 W. Market St. — Suite 111 • Greensboro, NC 27409
PHONE [phone] • Fax [phone]
February 26, 2019
North Carolina Department of Environmental Quality
Division of Water Resources
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Reference: 2018 LAND APPLICATION ANNUAL REPORT
Von Drehle Corporation.
Cordova, North Carolina
Permit No. WQ0039924
BR&S Project No. 2014-110
Information Processing Unit:
Branch Residuals & Soils is submitting all monitoring and reporting information as required in
the referenced permit on behalf of Von Drehle Corporation for their facility in Cordova, North
Carolina. This report includes: 1) Distribution and Marketing Certification and Summary Forms,
2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms,
4) Annual land application Field Summary Forms, 5) Residual Analysis Lab Sheets, 6) TCLP
Lab Sheets, 7) Pathogen & Vector Attraction Form, 8) Pathogen and Vector Attraction
Reduction Documentation, 9) Soils Lab Data 10) 2018 Application Summary Table, and 11)
2018 Application Condition Summaries.
A total of 643.94 wet tons (187.39 dry tons) of Fiber Clay Residuals were distributed to sites on
the Valley Protein Spray fields in Wadesboro, NC in August of 2018.
If any further information is required regarding this land application program, please do not
hesitate to contact me at [phone].
Sincerely,
Robert T. Branch, L.S.S.
Land Application/Residuals Operator
#15676
RTB
Enclosures

TABLE OF CONTENTS
SECTION NO. TITLE
I Distribution and Marketing Certification and Summary
Forms
II Annual Residual Sampling Summary Form
III Annual Metals Field Loading Summary Form
IV Annual Land Application Field Summary Form
V Residual Analysis Lab Sheets
VI Toxicity Characteristics Leaching Procedure
(TCLP) Analysis Report
VII Pathogen and Vector Attraction Reduction
Form
VIII Pathogen and Vector Attraction Reduction Documentation
IX Soil Analysis Report
X 2018 Application Summary Table
XI 2018 Application Condition Summary

DISTRIBUTION AND MARKETING CERTIFICATION AND SUMMARY FORM

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0039924 FACILITY NAME: von Drehle Corporation
PHONE: [phone] �. COUNTY: Richmond OPERATOR: Belger Farm
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
v❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes El No ❑ If No skip parts A, B, C and certify form below
Part A*•
Part B*•
Month
Sources(s) (include NPDES # if
applicable)
Volumed tons
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
intended use(s)
January
February
March
April
Ma
June
Jul
August
von Drehle Cordova Fiber Clay
0
187.39
187.39
Belger Farms
187.39
Soil Amendment
September
October
November
December
Total from FORM DMSDF (su }
0
0
0
0
Totals: Annual d tons :
0
187.39
187.39
18739
Amendments used: 1
Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)):
Part C:
Total Number of Form DMSDF (Supp)l
Facility was compliant during the past calendar year with all conditions of the land application permit p Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No 10 If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
- it ra--� D2-6/19 :�O�- <;z,-
Si ature of PermKee Date Signature of Preparer.. - Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
WQ0039924
Facility Name: von Drehle Corporation
Residual Source WQ # or
NPDES #:
WWTP Name: Von Drehle Fiber Clay Cordova, NC
Residual Analysis Data
Laboratory: 1) Microbac Labs
2)
3)
4)
5)
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sam le or Composite Date
7/10/2018
Percent Solids (%)
NA
29.10
Arsenic
75
2.08
Cadmium
85
0.17
Copper
4,300
9.07
Chromium
NA
NA
Lead
840
0.88
Mercury
57
<0.234
Molybdenum
75
3.47
Nickel
420
1.97
Selenium
100
0.94
Zinc
7,500
133.00
Total Phosphorus
NA
11
TKN
NA
280
Ammonia -Nitrogen
NA
106
Nitrate and Nitrite
NA
45.77
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals Iimits,
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer *
,Ze.1 --/ S
Date
*Preparer is defined in 40 C1R Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM

ANNUAL METALS FIELD LOADING SUMMARY FORM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
von Drehle Corporation Total Dry Tons Applied (Annual): 187.39
WQ0039924 Cation Exchange Capacity (non 503 only): nla
Belger Farms Owner: Valley Protein Predominant Soil Series PwB3
101.97 Acres Permitted: 101.97 Site #: VP Field #: S1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
vd 2018-4 MB
1
Annual Heavy Metal Field Loadings (Calculated in lbslacre):
1-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Sl ature of Land Applier
d-2e
Date
Author Daryl D. Merritt DENR FORM MFLSF (712002)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM

ANNUAL LAND APPLICATION FIELD SUMMARY FORMS LEGEND
All nutrients and metals concentrations listed on the following annual land application field
summary forms are on a pound per acre basis.
The following is a list of symbols and abbreviations used on the field loading rate report:
%TS — Percent Solids
DTIACRE — Dry Tons Applied per Acre
lb/ac — Pounds per Acre
Metals (lbs/ac)
As
— Arsenic
Cd
— Cadmium
Cr —
Chromium
Cu
— Copper
Pb
— Lead
Hg
— Mercury
Mo
— Molybdenum
Ni —
Nickel
Se —
Selenium
Zn
— Zinc
Nutrients (lbs/ac
PAN — Plant Available Nitrogen
P — Phosphorus
K — Potassium
Annual Totals — lbs/ac applied during the calendar year.
Cumulative Totals — lbs/ac applied during the lifetime of field use.

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "NIA" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: von Drehle Corporation WQ Permit #: WQ0039924 Field #: VP Acres Utilized:
Owner: Valley Protein Annual Dry Tons Applied: 187.39 Site #: Si Acres Permitted:
Operator: Belger Farms Predominat Soil Series PwB3 Cation Exchange Capacity (non 503):
Crop 1 Name: Wheat Crop 1 Max PAN: 67.00 Crop 2 Name: #NIA Crop 2 Max. PAN
101.97
101.97
NA
#NIA
C7
p ?r
C°
Specify
Totals
Per Acre
% Solids
As
Decimal
Volume
Applied per
Acre
DT/Ac
Residual Sources
(NPDES #, WQ#,
Fert., Animal Waste,
SitePrecip.
Cond.
{Dry'
Wet,
Moist)
Past 24
Hrs.
Inches
� d
w
a ELL.
o
w EP
# N
*
°
TKN
m
Z �
o
m
m
Nitrate
and
Nitrite
m
PAN Applied
(lbs/acre)
Must Select
Crop 1 or Crop 2
Wet Tons
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
Crop 1
Crop 2
Aug-18
643.94
6.31
29.10
1.84
von Drehle Paper
INC
1.00
0.40
280
106
6
0.67
X
TOTALS:
6
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.01
0.00
0.00
0.03
0.00
0.00
1 0.01
0.01
0.00
0.49
0.04
0.67
1 0.00
Date
lbs/ac
Current Cumulative lbs/acre
0.01 0.00 NA 0.03 0.00 0.00 NA 0.01 0.00 0.49
0.00 0.00 NA 0.00 0.00 0.00 NA 0.00 0.00 0.00
36 34 NA 1,338 267 15 NA 374 89 2,498
67.00
Aug-18
I,474
Prior Years Cumulative lbs/acre
Permitted C. P. L. R****
Permit PAN Limit lst/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of flues and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation ,2 0,0 � **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0
Signature of Land Applier Date ***Mineralization Rates: Compost - 0.1, Anaerobically Digested - 0.2,
Aerobically Digested - 0.3, Raw Sludge - 0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (1212006)

RESIDUAL ANALYSIS LAB SHEETS

Facility:
von Drehle Corporation
Source:
von Drehle Paper
Location:
Cordova, North Carolina
Contractor:
Belger Farms
Type of Analysis:
Industrial
Report No:
vd 2018-4 MB
Date Sampled:
7/10/2018
Date Reported:
7/27/2018
Reporting Period:
Jul - Aug 2018
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids
29.10�
Nitrogen (TKN)
0, 02 Q
280.000
Phosphorus
0.001
11.000
Potassium
0.000
2.000
Sulfate
0.000
Calcium
6780
67,800.000
Magnesium
U'076
755.000
Sodium
0,054
540.000
Iron
Aluminum
---
194,000
Manganese
---
Copper
---
9,070
1,500
Zinc
---
[33_000
2,800
Ammonia Nitrogen
I u6.00(
Nitrate N / Nitrite N
---
5.77011
Cadmium
---
0-1670
39
Chromium
---
— — 1.9700
1,200
Nickel
---
420
Lead
---
i}_10
300
Arsenic
---
2.0800
41
Mercury
---
'0.2340
17
Selenium
---
0.9 70
100
pH
40.106
Calcium Carbonate Eq.
401,000.0000
Organic Nitrogen
0.017
_
Molybdenum
---
75
Chloride
_
Boron
Available P205

Industrial
von Drehle Paper
Cordova, North Carolina
Jul - Aug 2018
Date Reported: 7/27/2018 Report No: vd 2018-4 MB
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
0.257
PAN Inj.
0.363
P
0.022
K
0.004
Lime
802.000
Secondary Nutrients
Calcium
135.600
Magnesium
1.510
Sodium
1.080
SAR
0.305
Chloride
0.000
Iron
0.000
Alumium
0.388
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
29.10
pH
7.800
Min Rate
0.400
Metals
Arsenic
0.004
Cadmium
0.000
Chromium
0.000
Copper
0.018
Lead
0.002
Mercury
0.000
Molybdenum
0.007
Nickel
0.004
Seleniun
0.002
Zinc
0.266

OMICROBAC®
Microbac Laboratories, Inc. - Fayetteville
Revised Report: Amended- See CERTIFICATE OF ANALYSIS
Case Narrative. KBG0085
Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project 1 PO Number: NIA
126 First Street Received: 07/10/2018
Cordova, NC 28330 Reported: 07/27/2018
Case Narrative
PAN Calculation: 44.01 mglkg
SAR Calculation: 0.40 mg/kg
Report amended on July 26, 2018 for work order KlIG0085 that was originally reported on July 24, 2018; The sample was rerun on
07125/2018. Rerun result Indicates a poor recovery in the initial anaaysis due to matrbi interference. New result supersedes prior analysis.
Analytical Testing Parameters
Client Sample ID: Rcsidual from I gaper Plant
Sample Matrix: Solid Collected By: Wright
Lab Sample ID: K8G0085-01 Collection Date: 07/10/2018 12:06
Method: EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
Nitrite as N
Method: SM 2540 G-2011
% Solids
Method: SM 4500 NH3 C-2011
Ammonia as N
Method: SM 4500-Norg C-2011
Total Kjeldahl Nitrogen
Wet Chemistry
Method: SM 4500 H+B-2011 (Non -Aqueous)
pH at 25 °C
Method: SM 4600 P F 2011
Result
RL
Units
Note Prepared
Analyzed
Analyst
0.790
0.249
mg/kg
07/12/18 0937
0711218 1653
DSK
<4.98
4.98
mg/kg
07/12/18 0937
07/12/15 1653
DSK
29.1
1.00
%
07l13/18 1mie
MT
106
0.100
mg/kg
Y 07/1 all 0935 07/13118 1516
MT
280
0.500
mg/kg
07/17/18 0845
TAB
Result
RL
Units
Note Prepared Analyzed
Analyst
7.8
1.0
pH Units
H 07/13/18 1108
TAB
Phosphorus, Total (as P)
11
0.25
mg/kg
Metals
Result
RL
Units Note Prepared
Method: Metals Solid/EPA 200.7 Rev 4.4 1994
Arsenic
2.08
0.020
mglkg (dry)
Cadmium
0.167
0.001
mg/kg (dry)
Calcium
67800
0.999
mg/kg (dry)
Copper
9.07
0.005
mg/kg (dry)
Lead
0.881
0.003
mg/kg (dry)
Magnesium
766
0.999
mg/kg (dry)
Microbac Laboratories,
Inc.
2592 Hope Mills Rd I Fayetteville, NC 283061910.864.1920
p I www.microbac.com
07116/18 1135 DSK
Analyzed Analyst
07/20/18 1152
TAB
07120118li52
TAB
07/20116 1152
TAB
07/20/18 1152
TAB
07/20/18 1152
TAB
07/20/18 1152
TAB
Page 1 of 3

6)MICROBAC®
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
KBG0085
Client Sample ID: Residual from raper Plant
Sample Matrix: Solid Collected By: Wright
Lab Sample ID: K800085--01 Collection Date: 07/10/2018 12:06
Metals
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Mercury
Method: SW7471A
Mercury, Total
Metals by 6010
Method: 5W6010C
Aluminum, Total
Definitions
H:
MDL:
RL:
Y:
Result
RL
Units Note
Prepared Analyzed
Analyst
3.47
0.001
mg/kg (dry)
07/20/18 1152
TAB
1.97
0.001
mg/kg (dry)
07/20/18 1152
TAB
<2.00
2.00
mg/kg (dry)
07/20/18 1152
TAB
0.937
0.010
mg/kg (dry)
07/20/15 1152
TAB
540
0.999
mg/kg (dry)
07/20/18 1152
TAB
133
0.010
mg/kg (dry)
07/20/18 1152
TAB
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Result RL Units Note Prepared Analyzed Analyst
<0.234
0.234
mg/kg
07/17/15 0819
07/18/18 1450
JST
Result
RL
Units
Note Prepared
Analyzed
Analyst
194
13.9
mg/kg
07/16/18 0845
07/16/15 2008
PDM
Analyse was prepared and/or analyzed outside of the analytical method holding time
Minimum Detection Limit
Reporting Limit
This analyte is not on the laboratory's current scope of accreditation.
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENT? NPOES
Report Comments
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents
only the sample(s) analyzed. This report is incomplete unless all pages indicated
in the footnote are present and an authorized signature is included.
Reviewed and Approved By:
Jeanne Overstreet
Client Relationship Specialist, Environmental
jeanne.overstreet@microbaacom
07/27/2018 11:39
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 2 Of 3

Fayettevilie Division 2592 Hope Mills Road — Fayetteville, NC 28306 [phone] ! 86 " ---' '--
M I C R O B A C- *K$G0085-
CHAIN OF CUSTODY RECORD
CLIENT NAME& ADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO10
I
PROJECT I LOCATION:
Cordova - 60-dayseries
%OF
s
o
T
L
E
$
TYPE OF
ANALYSIS
PRESERVATION C"DE
E
U Mc
E
C.
E.
Q
=
2 CD
CO
m
"M
a
V
E
'I
U
=
N
�
2
2
rai
O
o_
Y
Z
=:<
2
ci
N
1
.�
Z
M
o
Z
Z
Z
a
(L
F-
Z
ie
rn
3E
CODE: A = None
B = HNO3 (pH<2) + -WC
c = x2saa (pH<2) + �•4•C
D= NaOH + t4'G
E = ZN Acetate + <4°C
F = HCI
coNTACT PERSdN.
Mr. Chris Fowler
PHONE,r
910A 10-9131
SAMPLER
DATE! METHOD OFSHIPMBVr.
Microbac
LA9 ID
SAMPLE TYPE
DATE
TIME
COMP
GRAB
pH
D.O.1
EMP •c
R IL
Residual from paper plant
�df
� 0
X
2
A
A
A
A
A
A
A
A
A
%
��•a
1
A
A
A
A
A
A
A
A
A
Tlme
Received twe lsi9�e)
DateTIM
"two�/�
f
I3:1-*
2
EEEDate
FnqWsMh.d
Date
tr
-*-d bx: (Signature)
Date
Time
3
4
Rate
ime
RecefvW by: (alyntr
Otte
me
51
81
r
Comments or Special xazards:
Page 3 of 3

TOXICITY CHARACTERISTICS LEACHING PROCEDURE
(TCLP) ANALYSIS REPORT

OMICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
KBA0694
Project Description
Residuals Sample - Annual
For:
Mr. Chris Fowler
Von Drehle Corporation
126 First Street
Cordova, NC 28330
Bonnie K. Sanders
Senior Project Manager
Wednesday, February 7, 2018
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac laboratories, Inc. - Fayetteville. If you have any questions, comments, or require
further assistance regarding this report, please contact your service representative listed above.
1 certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil
samples are reported on a'dry-weight' basis unless specified otherwise. Analytical results forwater and wastes are reported on
a 'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This
laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported
results are related only to the samples analyzed- as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864A920 p I www.microbac.com
Page 1 of 8

�VMICROBAC®
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Von brehle Corporation Project Name: Residuals Sample -Annual
Mr. Chris Fowler Project 1 PO Number: 2030767
126 First Street Received: 01/24/2018
Cordova, NC 28330 Reported: 02/07/2018
Sample Summary Report
Sample Laboratory IB Client Matrix Sample Impe Sample Begin Sample Taken Lab Received
Residual from paper plant KBA0694-01 Solid Grab 01/24/18 11:45 01/24/18 14:50
Page 2 of 8

OMICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Analytical Testing Parameters
Client Sample 10: Residual from paper plant
Sample Matrix: Solid Collected By; Marin
Lab Sample ID: KBA0694-01 Collection Date: 01/24/2018 11:45
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Result RL Units Note Prepared Analyzed
Method: SW9045
Corrosii ty pH 8.68 UNITS 01/26/18 1508
Temperature At Determination (C) 17.2 UNITS 01/26/16 1508
8270 TC
Result
RL Units Note
Prepared
Analyzed
Method: SW8270C
1,4-Dichlorobenzene
<50.0
50.0 uglL
01/30/18 1430
01/31/18 1013
2,4,5-Trichlorophenol
<50.0
50.0 uglL
01/301181430
01/311181013
2,4,6-Trichlorophenol
<50.0
50.0 uglL
011301181430
01/311181013
2,4-Dinitrotoluene
<50.0
50.0 ug/L
011301181430
01/31/181013
Hexachlorobenzene
<50.0
50.0 ug/L
011301181430
011311181013
Hexachlorobutadiene
<50.0
50.0 ug/L
011301181430
011311181013
Hexachloroethane
<50.0
50.0 ug/L
01/30/18 1430
011311181013
m-,p-Cresol
<50.0
50.0 ug/L
01/30/18 1430
01131/18 1013
Nitrobenzene
<50.0
50.0 ug/L
01/30/18 1430
01131/181013
0-Cresol
<50.0
50.0 uglL
01/30/18 1430
01/31/18 1013
Pentachlorophenol
<250
250 ug/L
01/30/18 1430
01/31/18 1013
Pyridine
<250
250 ug1L
01/30/18 1430
01/31118 1013
Surrogate: 2,4,6-Tribromophenol
97.0
Limit: 10-123 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: 2-Fluorobiphenyl
81.6
Limit: 43-116 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: 2-Fluorophenol
49.7
Limit: 21-100 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: Nitrobenzene-d5
73.0
Limit: 35-114 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: p-Terphenyl-d14
90.7
Limit: 33-141 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: Phenol-d5
33.7
Limit: 10-94 % Rec
01/30/18 1430
01/31/18 1013
Ignitability of Solids
Result
RL Units Note
Prepared
Analyzed
Method: 1030
Burnrate - 1030
<2.20
2.20 mmisec
01/30/18 1140
Mercury
Method: SW7470A
Mercury
Metals by 6010
Method: SW6010C
Arsenic, TCLP
Barium, TCLP
Result RL Units
<0.00200 0.00200 mg/L
Note Prepared Analyzed
01/30/18 0957 01/31/18 1133
Result RL Units Note Prepared
Analyzed
<1.00 1.00 mg/L 01/30/18 1029
01/31/18 1353
0.272 0.100 mg/L 01/$0/16 1029
01131/181353
Microbac Laboratories, Inc.
2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 3 of 8

O)MICROBACO
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0694--01 Collection Date: 01/24/2018 11:45
Metals by 6010
Result
RL
Units
Note
Prepared
Analyzed
Cadmium, TCLP
<0.100
0.100
mg1L
01/30MO 1029
01/31/18 1353
Chromium, TCLP
<0.200
0.200
mg/L
011=18 1029
01/31/18 1353
Lead, TCLP
<1.00
1.00
mg1L
01/30118 1029
01/31/18 1353
Silver, TCLP
<0.100
0.100
mg1L
01/30118 1029
01/31/18 1353
Metals by 6020
Result
RL
Units
Note
Prepared
Analyzed
Method: SW6020A
Selenium, TCLP
<0.500
0.500
mg1L
01/30/18 1029
01/31/18 1549
Reactivity, Cyanide
Result
RL
Units
Note
Prepared
Analyzed
Method: SW9014
Reactivity, Cyanide
<9.98
9.98
mg/kg
01131/18 1520
Sulfide (Reacttivity)
Result
RL
Units
Note
Prepared
Analyzed
Method: SW9034
Reactivity, Sulfide
<100
100
mg/kg
01/31/18 1700
TCLP HERBICIDES
Result
RL
Units
Note
Prepared
Analyzed
Method: SW8151A
2+1)
<20.0
20.0
ugA-
01/31118 1213
02101/18 2006
2,4,5-TP (Silvex)
<2.00
2.00
uglL
01/31/18 1213
02/01/18 2006
Surrogate: 2,4-Dichlorophenylacetic acid
41.3
Limit: 20-144 % Rec
01/31/18 1213
02/01/18 2006
TCLP Pesticides
Result
RL
Units
Note
Prepared
Analyzed
Method: SW6081B
Endrin
<0.500
0.500
ug1L
01/30/18 1215
02/02/18 0520
Lindane
<0.500
0.500
ug1L
01/30/18 1215
02/02H8 0620
Methoxychlor
<0.500
0.500
ug1L
01130H8 1215
02/02/18 0620
Toxaphene
<10.0
10.0
ug1L
01/30/18 1215
02/02118 0520
Chlordane
<10.0
10.0
ug1L
01/30/18 1215
02/02118 05220
Heptachlor
<0.500
0.500
uglL
01/30/18 1215
02/02118 0520
Heptachlor Epoxide
<0.500
0.500
uglL
01/30/18 1215
02JO2118 0520
alpha Chlordane
<0.500
0.500
uglL
01/30/18 1215
02102118 0520
gamma Chlordane
<0.500
0.500
ug1L
01/30/18 1215
02102118 0520
Surrogate:2,4,5,6-Tetrachloro-m-xylene
53.3
Limit:20-180 °%Rec
01/30/18 1215
0210211a o52o
Surrogate: Decachlorobiphenyl
20.1
Limit: 25-140 °% Rec
01/30/18 1215
02102/18 0520
Volatile Organics
Result
RL
Units
Note
Prepared
Analyzed
Microbac
Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC
28306 1910.864.1920 p I
www.microbac.com
Page 4 of 8

OMIC:ROBAC®
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
KBA0694
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0694-01 Collection Date: 01/24/2018 11:45
Volatile Organics
Result
RL Units Note
Prepared Analyzed
Method: SW82608
1,1-Dichloroethene
<50.0
50.0 uglL
011311181555
1,2-Dichloroethane
<50.0
50.0 ug1L
01131/181655
Benzene
<50.0
50.0 ug/L
01/31/18 1655
Carbon tetrachloride
<50.0
50.0 ug/L
01/31/18 1655
Chlorobenzene
<50.0
50.0 ug1L
01/311181655
Chloroform
<50.0
50.0 ug/L
01/31/18 1655
Methyl Ethyl Ketone
<100
100 ug1L
01/31/18 1655
Tetrachloroethene
<50.0
50.0 uglL
01131118 1655
Trichloroethene
<50.0
50.0 uglL
01/31/18 1655
Vinyl chloride
<100
100 ug1L
01/31/18 1655
Surrogate: 1,2-Dichloroethane-d4
101
Limit: 80-120 % Rec
01/31/18 1655
Surrogate: 4-Bromofluorobenzene
103
Limit: 86-115 % Rec
01/31/18 1655
Surrogate: Dibromofluoromethane
97.8
Limit: 86-118 % Rec
01/31/18 1655
Surrogate: Toluene-d8
99.9
Limit: 88-110 % Rec
01/31/18 1655
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1 910.864.1920 p I www.microbac.com page 5 of 8

Batch Quality Control Summary
&)MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Spike Source %REC
Metals by 6020 ResuH RL Units Level Result %REC Limits
Batch W0647253 - METHOD - SW6020A
BLK (WG646865-02)
Selenium, TCLP
BS (WG646865-03)
Selenium, TCLP
Reactivity, Cyanide
Batch WG646993 - SW7.33 - SW9014
BS (WG646993-01)
Reactivity, Cyanide
Prepared: 01/30/2018 Analyzed: 01/31/2018
RPD
RPD Limit Notes
ND 0.0500 mg/L - U
Prepared: 01/30/2018 Analyzed: 01/31/2018
0.237 0.0500 mg1L 94.9 80-120 20
Spike Source %REC RPD
Result RL Units Level Result %REC Limits RPD Limit Notes
Prepared: Analyzed: 01/31/2018
ND 100 mglkg 4.96 .5-110
50 U
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page6nf8

O)MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Laboratory
FAY: Microbac Laboratories, Inc. - Fayetteville
Definitions
*: Surrogate or spike compound out of range
J: [Undefined)
MDL: Minimum Detection Limit
RL: Reporting Limit
RPD: Relative Percent Difference
U: Not detected at or above adjusted sample detection limit
Cooler Receipt Log
Cooler ID: Default Cooler
Cooler Inspection Checklist
Custody Seals Intact and/or No Evidence of Tampering
COC/Labels Agree
Received on Ice (or not required)
Project Requested Certifications)
Microbac Laboratories, Inc. - Fayetteville
11
Report Comments
Temp; 4.1 °C
Yes Containers Intact Yes
Yes Preservation Correct (or not required) Yes
Yes
North Carolina DENR NPDES
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted.
The data and information on this, and other accompanying documents, represents Bonnie K. Sanders
only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager
in the footnote are present and an authorized signature is included.
bonnie.sandersomicrobac.com
02/07/2018 12:26
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, INC 28306 910.864.1920 p I www.microbac.com Page 7 of 8

VonDrehle Corp.
126 First Street
Cordova. NC 28330
LM ID 0
U ) Res
Fayetteville Division 2592 Hope Mills Road -- Fayetteville, NC 28306 [phone]
CHAIN OF CUSTODY RECORD
Cordova - Yearly
CONTACT MOON:
Mr_ Chris Fowler
PHONE:
910-410-9131 -
SAMPLE TYPE I DATE
I-2q'(�
Microhac
TIME FFX�
'�5
#OF
s
7 TF't
Ur ANA
O
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f-
w
w
L
LU
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0-
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o:
UI
-j
-j
a
-j
21AIAIAIAIAIA
DaleYg8r
imer5�I� 1 sD
by
pqw
Dots
,Tiffis
rJ
IE-
e�
by:
ime
by:
111111111111
CODE: A = eVC ONLY
B = HNO3.(ph<2) + a4°C
C = H2SO4 (ph<2) + 40C
D = NaOH + <4°C
E = ZN Acetate + <4"C
F w Sodium Thio.
PH 1 D.O. I TEMP'C
M
Comments or Special Hazards:
�i� Page 8 of 8
l�-r1a�

PATHOGEN AND VECTOR
ATTRACTION REDUCTION FORM

PATHOGEN REDUCTION AND VECTOR ATTRACTION REDUCTION
The current permit, WQ0039924, does not have vector attraction requirements but does have Class
A requirements for pathogens. The form is marked to reflect these requirements.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: von Drehle Corporation
WWTP Name: Von Drehle Fiber Clay Cordova, NC
Monitoring Period: From 1/1/2018 To
WQ Permit Number: WQ0039924
NPDES Number:
12/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/tem) ❑
1 Alt B (Alk Treatment) ❑
I Alt. C &or Testing) El
Alt.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion
.................................................
..... .
. --
If applicable to alternative pe med Class A or Class B complete the followin
monitoring
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
um er 01
Excee-
Frequency
of Anal sis
Y
I Sample
Type
Analytical
Tech-
item
Geo. Mean
axing
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
< 0.6
NA
< 0.6
Grams
0
Yearly
Grab
1682
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.l (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
jAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
jAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
El "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mr. Chris Fowler, ORC
Preparer Name and Title (type or print)
Signature of Preparer*
- 6/ 1
Date
Land Applier Name and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

PATHOGEN AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION

PATHOGEN REDUCTION AND VECTOR
ATTRACTION REDUCTION DOCUMENTATION
The current permit, WQ0039924, does not have vector attraction requirements but does have Class
A requirements for pathogens. Documentation is attached to reflect these requirements.

Von Drehle Corporation
Cordova, NC
City of Rockingham IUP 0015
Sep-18
Biological Consulting Services
vLab #
Date Analyzed
Primary Value Salmonella
MPN per ml
Secondary Value Salmonella
MPN per 4 grams Dry
1809056
9/14/18
< 0.07
1809057
9/14/18
< 0.07
< 0.6
1809058
9/14/18
< 0.07
< 0.6
1809059
9/14/18
< 0.07
< 0.6
1809060
9/14/18
< 0.07
< 0.6
1809061
9/14/18
< 0.07
< 0.
1809062
9/14/18
< 0.07
< 0.6
Exceedances 0
All Samples are less then 3 MPN per 4 grams dry weight. Samples meet Class A pathogen
requirement for distribution.
Data provided in this summary have been used for the values reported on the Annual Pathogen
and Vector Attraction Reduction Form for Class A and Class B options.

Icnc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
September 14, 2018
Robert Branch
Branch Residuals and Soils
8646 W. Market St. Suite 111
Greensboro NC 27409
336-510-0340
[e-mail]
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Cordova NA
Imonella
ethod
1682; BCS SOP M-4 (15017025 and TNi Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
LQi
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS M 1809056, 1809057, 1809058,1809059,1809060,1809061,1809062
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, wrrHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AW
1 wCtR��
A i
7.,1 „4 rt►+N �+1bu�M'r

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-1 Sample Date/Time: September 10, 2018 13:33
BCS Sample ID: 1809056 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 42.3
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A.
Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-2
Sample Date/Time: September 10, 2018 13:37
BCS Sample ID: 1809057 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 40.6
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1809056, 1809057,1809058, 1809059, 1809060, 1809061, 1809062
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW. MICROBI OSERVICES.COM
FL DOH #E82924. ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE wRITTEN CONSENT OF BCS LABORATORIES
�5� h
IItCA,:9I

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-3
Sample Date/Time: September 10, 2018 13:41
BCS Sample ID: 1809058 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 39.3
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Paliack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/ml- sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
knalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-4
Sample Date/Time: September 10, 2018 13:45
BCS Sample ID: 1809059 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 41.4
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/ml- sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
knalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1809056, 1809057,1809058, 1909059, 1809060, 1809061, 1809062
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW. MICROBIOSERVICES.COM
FL DOH #EB2924, ISOAEC 17025:2005 L2422 (ANAS), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED.. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AM
j�� wttwio,�co ,p

Client: Branch Residuals and Soils
Analysis: Salmonello
Project Name: Cordova NA
Client Sample ID: VD-5 Sample Date/Time:September 10, 2018 13:47
BCS Sample ID: 1809060 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 40.9
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-6 Sample Date/Time: September 10, 2018 13:50
BCS Sample ID: 1809061 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 40.1
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting unit:
Page 4 of 8
Final Report BCS ID 1809056,1809057, 1809058, 1809059,1809060,1809061,1809062
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW. MICROBIOSERVICES. COM
FL DOH #E82924, ISO/IEC 17025:2005 L.2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
"r�.� wtcncartco ITOR Tld

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-7 Sample Date/Time: September 10, 2018 13:52
BCS Sample ID: 1809062 Sample Description: Biosolids
Date Received: September 11, 2018 09:26 Amount Submitted:100ml bottle % Solids: 39.5
Amount Analyzed: 30.00 g Receipt Temperature: 5.6 deg C Preserved: Yes
Analysis Start: September 11, 2018 09:40 Analysis Stop Date: September 14, 2018 11:10
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5of8
Final Report BCS ID 1809056,1809057, 1809058,1809059, 1809060,1809061, 1809062
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROB[OSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68.03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED. EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
%� `✓ w[cnablsro �
r„i,a�ti Tll

Client: Branch Residuals and Soils
Project: Cordova NA
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6of8
Final Report BCS ID 1809056, 1809057, 1809058, 1809059, 1809060, 1809061, 1809062
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW. MICROSIOSERVICES.COM
FL DOH #E82924, [SO/IEC 17025:2005 L2422 (ANAB), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AAn
wttw:40
'�d.l,hr efb��BN��bn+

I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH
Environmental Laboratory Certification Program, as applicable unless otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date: September 14, 2018
Page 7of8
Final Report BCS ID 1809056,1809057, 1809058, 1809059, 1809060, 1809061,1809062
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET, STE. A, GAINESVfLL,E, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS !REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
Atom -
.ester rr .
'•,/ lye„10,�~ MdIW9 VlMY'9M

DATA QUALIFIER CODES
SYMBOL MEANING I
B Results based on counts outside the acceptable range. _ — -
X Sample received without prior notification or delayed delivery. Analysis performed outside of
associated method required QC data set (1 QC data set per 20 samples per 168 hours).
I Value is between the laboratory method detection limit & laboratory practical quantitation limit.
J1 The sample matrix interfered with the ability to make any accurate determination.
J2 No Quality Control criteria exist for the component. r_ m
A 'The data are questionable because of improper laboratory or field protocols. •`
L Off scale high. Actual value is known to be greater than value given. Y
Presumptive evidence for the presence of material. There is an indication that the analyte is present, s
N
but the confirmation requirement was not met.
O Sampled, but analysis not performed.
Q Sample held beyond the accepted holding time.
Indicates that the compound was analyzed for but not detected. The specified component was not
U
detected. The reported value is the method detection limit.
V Anal was detected in both sample and associated method blank. Data may not be accurate. ;
Yta .. p _
Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate.
z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that ;
can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
Presence or absence of analyte could not be confirmed.
Not reported due to interference._._ .....
** p
A BCS is not currently accredited for this analyte.
# BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1809056, 1809057, 1909058, 1809059, 1809060, 1809061, 1809062
BCS LABORATORIES, INC. -- GAINESVILL.E
4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (ANAB), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
AAW
Y wCCN[o1Teo iy +` 0%~ N

CHAIN OF CUSTODY RECORD
1p www.microbioservices-com
" FL DOH Laboratory #E82924, EPA# FLd1147
Client Name and Address: A2A-id, z5U4 r 5
CitylStatelzip: a kie, 3hawo "C- Z 590 Q Project ID:
Project Manager: ROA WA66A FeellitylSlte:
Telekphone Number. 4 3/2- op Fax Na.: Report To:
Sampler Name: (Print) '4 Email:
Sampler Signature: Invoice To:
B —5. Res' mservati+reI Matrix
BCSLaboratories
4609 NW 6th street, Building A
Gainesville, FL 32609
Tel. [phone], Pax. [phone]
Compliance Mogitoring? ErYes❑ No
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AL S. L. ►
ra Mums and Soils
VDT y 0. �
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09/11/2019 9.26 � '
Q g v 1Lu v, 0 U X G.
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1809060 �—�' gis c�i p g w Q m o 1✓
26 _ o % �s^ _U _j 09/1112018 9:.. I
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Sample ID ! Description o z . c� . {i r� g o o S w w 0 ui W } _ ii `�, z O
r , :33Branch Residuals and Soils
1 VD-1
1809866
`V' + 09/1112018 9:26
I tl " I Branch Residuals and Sails
1r "' -3 VD-2
091i11x018 9:26 ,gyp
Branch Residuals and Soils `Q
V11-3
1809068
Branch Residuals and Soils Branch Residuals and Soils 0911112018 9:26
VDT VD 7
i809061 1809062 Laboratory Comments:
091111201a 9:26 09H 112018 9:26
Method of Sh t: Pnstal OHL FEDEX Other. Temp. @ reclet: � Cwr �
� nq Date Time Reaeived:by: Date Time IR-
of +ro Custody Seat: Intact 13rotmn W
(© !S Presence of vlsabie ice
Date Time Presence of i Y
ReVnquislled by: Date Time .Received by BCS Laboratories: eks
I Hold rime
tG

SOIL ANALYSIS REPORT

SOIL ANALYSIS REPORT
Soil Samples were sent to a lab for testing. Results are not available at the time of the report.
Soil samples will be provided as soon as they are available from the lab.

2018 APPLICATION SUNEVIARY TABLE

VON DREHLE CORPORATION
LAND APPLICATION PROGRAM
PERMIT NO. WQ0039924
2018 CLASS A APPLICATION SUMMARY
Tract
/Site Field
Acres
Date
Spread
Wet Tons % Solids
Dry Tons /
Acre
Dry Tons
Crop PAN
VP SI
101.97
Aug-18
643.94 29.1
1.84
187.39
Wheat 0.47
101.97
von Drehle
Wet Tons
Dry Tons
Permit
Limit
643.94
187.39
16,499
Branch Residuals Soils, LLC Confidential 2/25/2019 Page 1

2018 APPLICATION CONDITION SUMMARY

von Drehle Corporation
Cordova, North Carolina
Belger Farms
WQ0005135
Jul - Aug 2018
von Drehle Paper
Farmer: Wayne Belger
Acres: 101.97
Site/Tract: VP
Application Method: Incorporated
Field: SI
Percent Solids: 29.1
Residual Report No.: vd 2018-4 MB
Crop: Wheat
Date
Field No.
Subfield
Wet Tons
Weather
Conditions
Soil
Conditions
Prev. 24 Hour
Rainfall
8/27/18
SI
138.08
Hot, Fair
Dry
0.00
8/28/18
SI
368.20
Hot, Fair
Dry
0.00
8/29/18
SI
137.66
Hot, Fair
Dry
0.00
Total Wet Tons
643.94