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HomeMy WebLinkAboutWQ0003919_Residual Annual Report 2018_20190314INITIAL REVIEW Reviewer Williams, Kendall Project Number* WQ0003919 SUBMITTAL DATED: 2/27/2019 Project Contact Information Hease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues. ...................................................................................................................................................................................................................................................................................................................................................................................................... Name * Lisa Finnerty Email Address* Ifinnerty@synagro.com Project Information Application Type* r New r Renewal r Annual Report Permit Type * r Wastewater Irrigation r Other Wastewater • Closed -Loop Recycle r Single -Family Residence Wastewater Irrigation Is a paper copy of the application being submitted?* r Yes r Nor N/A Permit Number* WQ0003919 Permittee * CITY OF KINSTON Facility Name * KINSTON REGIONAL WRF Phone Number* 443-489-9086 r Modification (Major or Minor) • Additional Information r Other • High -Rate Infiltration r Reclaimed Water r Residuals r Other Please provide comments/notes on your current submittal below. Please attach all information required or requested for this submittal to be review here. Application Form Engineering Hans, Specifications, Calculations, Etc.) 2018 ANNUAL REPORT FOR CITY OF KINSTON 11.66MB NC.pdf Upload only 1 HDF docurrent. NLltiple docurrents must be combined into one HJF file. For nein and modif cation permit applications, the paper copy is required to be submitted to the Di, risiom Be advised, applications will not be considered complete until both the paper and electronic applications. have been received_ The paper copy shall include the follm ging: • Application Farm • All relevant attachments (talcs, soils report, specs, etc_) • 1 full-size engineering plan set • 2 11-17" engineering plan sets • 1 extras set of specifications (in addition to the set of specifications Provided in the attachments) • Fee (if required) This shall be mailed to the following address: By US_ Postal Service- Di,vision of Water Resources- Non -Discharge Branch 1617 Mail Service Center Raleigh NC 27699-1617 By Courier, -Special Delivery: Division of Water Resources- Non -Discharge Branch Nathaniel Thornburg- 9th Floor, Office #942M 512 N_ Salisbury St_ Raleigh, NC 27644 For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov. *140 By checking this box I am acknowledging that I have read the above statement and agree to send these documents as required to one of the address given above. Signature Submission Date 2/27/2019 435 Vvfdaams Court, Suite 100 Baltimore, LVID 21220 Nvwwv synagro. corn FEBRUARY 27, 2019 NCDEQ Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, NC 276994617 Re: 2018 Annual Report for Permit No. WQ0003919 Dear NCDEQ: Synagro is submitting one copy: and one electronic copy of the above referenced report on behalf of City of Kinston, NC. If you have any questions or comments, please contact Kenneth Stevens at (252) 939-3375 or Melinda Boyd at (336) 909-8627. Sincerely, Derrick Shivar Environmental Compliance Manager Enclosures cc: Kenneth Stevens, City of Kinston Melinda Boyd, Synagro CITY OF HINSTON9 NC RESIDUALS LAND APPLICATION PROGRAM PermitNo. WQ0003919 2018 ANNUAL REPORT City of Kinston, NC Residuals Land Application Program 2018 Annual Report TABLE OF CONTENTS 1. Certification Form and Annual Operations Summary 2. Annual Residual Sampling Summary Forms, Residuals Analysis, & SAR Calculation Pages 3. Annual Land Application Field Summary Forms 4. TCLP Analysis 5. Pathogen Reduction/Vector Attraction Reduction 6. Soil pH &Lime Application Records 7. Soil Analyses SECTION 1 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit #: W00003919 County Lenoir Year2018 Facility Name (as shown on permit) Kinston Regional WRF & Peachtree W WTP NPDES No. NC0024236, NCO020541 Land Application Operator Synapro Phone# (336) 998-7150 Land application of residuals as allowed by the above permit occurred during the past calendar year? X YES NO. If NO,. skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A—Residuals Application Seminary: Total number of application fields in the permit: 53 Total number of fields utilized for land application during the year: 3 Total amount of dry tons applied during the year for all application sites: 95_51 Total number of acres utilized for land application during the year: 28.6 Part B —Annual Compliance Statement: Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality X YES NO. If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the pemdt and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading Rates in 15A NCAC. 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All monitoring and reporting requirements in 15ANCAC 02T. I I 11 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11. Vegetative cover wasmaintained and proper crop management was performed on each site receiving residuals, as specified in the permit. 12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13. All buffer requirements as specified on. the permit were maintained during each application of residuals. Part C —Cert ification: "I cert ify, under penalty of law, that the above information is, to the best of my lmowledge and belief, true, accurate, and complete. ] am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Kenneth Stevens, WRF Superintendent Permittee Name and Title (type or print) Signature of Preparer* Date Signage of Land App&@r Date (if different from Permittee) (if different from Permittee and Preparer) *Prepuer is defined in 40 CFR Part 5O3.9(r) and l5A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) 2018 ANNUAL OPERATIONS SUMMARY= LAND APPLICATION IN NC KINSTON, NC KINSTON, NC KINSTON REGIONAL WRF AEROB. DIGESTED CAKE DRY METRIC MONTHNEAR AMOUNT UNIT DRY TONS UNIT TONS May 2018 725.00 Y 95.51 D 86.61 YEARLY TOTAL 725.00 Y 95.51 D 86.61 1 /28/2019 SECTION 2 0 L_ C O a N R E E N m a 0 D- N O w f0 0 Y as �C R c O Q O m -- a o� 0 E N R N R O d U � 0 0 o E R C N C L O U @ E I. Q NO. 0 O m y d 0 C O N z _0 U C7 w rnz� M z Nz O 0 N 0 0 O Z U Z �YZ Y T C O m `0 CD BOOM E E E 7 Z ••ORION R ZZyU) ON IRWIN W ELF LINp aURIz `o1 N N <n M� to •ti m o 0 o M r�i V r V M V N N M M N W bi M rl Q N l0 d' V N N N •-I l0 N j� rl rl N to �o .0 tm i r o m p N Y T o M a E R A N N N a Q y K o 0 N N -O wFINN E,L Z RFEEmo w E E o m� �U)0 Q� �' E a—'' a o 0 Na0E �m�E o na TY mem Z Em d R f0 o a i m of o o y oY E.-_- G'aooa dQU2U0 2 CD NFFQz U t� N� m 61 O M l0 ❑ � V ri ri ri 1p Oi N N Gj � � N lO O N N <n M� to •ti m o 0 o M r�i V r V M V N N M M N W bi M rl Q N l0 d' V N N N •-I l0 N j� rl rl N to �o .0 tm i r o m p N Y T o M a E R A N N N a Q y K o 0 N N -O wFINN E,L Z RFEEmo w E E o m� �U)0 Q� �' E a—'' a o 0 Na0E �m�E o na TY mem Z Em d R f0 o a i m of o o y oY E.-_- G'aooa dQU2U0 2 CD NFFQz R® \/\ \ ;)) \ r 2 )Q{ / )/{ ) / \,0 :lU) /Z\ Co &m ` [a\ LL, ,a „: §22 ® ° D(j \- 22e \ - - \U0 4T ) \ ° tm - \/\ LOU /§g�( 2 / \\) } ^0 U) § { E _ } kk IB $ \_� 2 \)/ ca Q z \k_} ]/{\$ �e ■ e OWE e Im§§FOOO ��§! «§ ¥% Jƒ>0$ $;"§ $\-am00 �_, W=3l= o<o;=CLm 52§ z \§{ : o;( oReeeee§(C� |F ] f _ &/§§§§§§§§§§§(\ 0 \ ¥ 7!° %b3w \k( « ` §P 0 ~ {\ ., {0 6666! „ me,,,,,,,,,, ;� !66 \� �\/._\\\\\\\\\\\\\\\\\ !;=00000000000 §j co ` a - �g \ C/ k U \ \\ � {\ , )\f\7/§§) // \ \\ \_ )sof \ `® -]m § m§ \\ //m {]§a) i§ - - §o§ m } / _ !± ' _ _^/a;\a;>r[0 zg § 0 § z � JJC)U) a,«:)# /k2 A !� } F2 FF/ /<0z \\ O NI m �' �a fJ � y 7Z� �� U 4 � ��Nn <b � � � __ � n �_ � -- __ U �NY F 'a> 1 Z J Q °= v a fowl ul �.Ec o J u � � N N ¢`r° U C Z a y o U, 1 Z J Z LL a fowl F � g u � � �I � `1 W Q e M V M � W i O i a D �� .3 0 W W W � � a w c� � Rt z� Y Ja N Q .� �. N LL2 � F U w as a� N ZO F R N � 11� OW N � C U y Y Q Q W LL a m Q 7 EM �M M m On 'O m L N ._ d _� a 1 Z O z O a fowl a 3y' �N Z D �� .3 0 W W W � � a w c� � Rt z� Y Ja N Q .� �. N LL2 � F U w as a� N ZO F R N � 11� OW N � C U y Y Q Q W LL a m Q 7 EM �M M m On 'O m L N ._ d _� a o mZ � o E z O Z �� 2 � N Z O z O `o U LL .� Z N U � `` 1 \ J VVV m y '-°o >N o? vd �- � 1 N N W � _ \ \ � ���111 W 2 y Q � \ fq T a a a z Q z � \ � � 3 1 i U o mZ � o E z O Z �� 2 � N Z O `o U LL .� � N m H s � z � J Q d W `J �� N N d a U N U] m E� N � o � aQD c 0 �� o E L Ua) O o � a� \ o :a � z E \ m v \J � U �� -� Jm cn j N O �' � J N� N m �� h � N � F° 0] NN Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 1/15/2018 1/1/2018-3/31/2018 2.0697 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x %Solids) = 100 = (2830 x 16.3400) + 100 = 462.422 Ca mg/I = (Ca mg/kg x %Solids) + 100 = (14700 x 16.3400) + 100 = 2401.98 Mg mg/I = (mg mg/kg x %Solids) + 100 = (5040 x 16.3400) + 100 = 823.536 Na meq = Na mg/I + Molec.Wgt.Na = 462.422 + 23 = 20.1053 Ca meq = Ca mg/I - Molec.WgtCa = 2401.98 + 20 = 120.099 Mg meq = Mg mg/I + Molec. Wgt.Mg = 823.536 = 12 = 68.628 SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 20.1053 = SgrRoot[0.5(120.099+68.628)] = 2.06971 Printed: 2/6/2019 Page 1 09:05 )2 \)j)) &\ »^K E §/ -&G«f0\I)dR2\_ 0Zr \{\))« /) ){)///))/]//) / J )/] )_ OO iO E m 0 N N �y — a � N O C N IL V Y C � C O 0 � Y LL G u �O ° a O a a m v a E Of O C M z n a 3 'a a o v 00 K Q t c 3� o - L O 0 o N N m y n OO O 0 N a o � N O C IL Y � m M 0 � � J O a y J a E ry � z z z a v K Q OO O 0 m O C Y � J O J ry z o - L O 0 o N m y 0 n N N a N N N OO O m O N N N N M O O V v v v a a a l0 (O f0 (O a O v 0 0 0 O 6 O E ro ro id cq io c io m o N� K m ro ro o� co m co ao m a 0 0 0 0 0 0 0 0 0 a a O O O O O O O O O U U U U U U U U N N !p [ ( N N J Z Q 0 o 0 0 0 0 o o O N N N N M W N v v o v O W U z J a 0 O U ir 0 0 0 Z W 0 0 O o z rn U n 'y Z J Q .E y 'E o Y a .N L 0 T O E o o z' E C) � 'z z n N 2 11 N m N " u A m E �o _cFa * E < F2 F lo- F F E W Z) U E U 7 U Z N >.y ®1.J 014CC 0 easy ®LLI¢ %O av �W V CC =0 as ao N J W r 0 W z O\, Q a Z $4? U d N O U CO) Z W =0 as ao N J W r 0 W z O\, Q a Z Z U d N O U CO) Z W � o U o a d ami Q Cl) U = > N n Y =0 as ao N J W r 0 W z O\, Q a Z Z d N O U CO) Z W 0 O o Ir o a d ami Q Cl) U =0 as ao N J W r W z O\, Q .-. Z d Z U CO) w 0 O c Ir o d =0 as ao N J W r p F w N N n a U ai m ro E� E z O\, \ d Z CO) ami a°i c aUi p F w N N n a U ai m ro E� E z O\, \ Z CO) d N > N O? a 1 V N N W \ \ D W u, a (A J Q � IL \ Z \ \ U U , \ c 7z � \ 0 Z Zz t _ Z z � � y J N W 1 J a� _ Z Sodium Absorption Ratio Calculation (SAR) Product Code Product Name Sample Date Report Range Ratio 2060-02-AEDCAK-NC KINSTON, NC KINSTON REGIONAL WRF 413/2018 4/1/2018-6/3012018 1.3430 AEROB. DIGESTED CAKE Na mg/I = (Na mg/kg x %Solids) = 100 = (1860 x 15.6400) = 100 = 290.904 Ca mg/I = (Ca mg/kg x %Solids) + 100 = (14600 x 15.6400) _ 100 = 2283.44 Mg mg/I = (mg mglkg x %Solids) + 100 = (4850 x 15.6400) _ 100 = 758.54 Na meq = Na mg/I = Molec.Wgt.Na = 290.904 - 23 = 12.648 Ca meq = Ca mg/I - Molec.Wgt.Ca = 2283.44 + 20 = 114.172 Mg meq = Mg mg/I + Molec.Wgt.Mg = 758.54 + 12 = 63.2117 SAR = Na meq + SgrRoot[0.5 x (Cameq + Mg meq)] = 12.648 + SgrRoot[0.5(114.172+83.2117)] = 1.34301 Printed: 2/6/2019 Page 1 09:05 SECTION 3 15 a 4 z Q a s N 4 15 4 z Q N 4 W W U 0.l ttl h zQ rg z ri N a a b x 0 Ei A d a 4 0. P4 a m U N W p a a z Its v o 4 R U N W a _, C o �aC6 1N c o �F � U v�Uq QFa; o o R d N u U 0 0 _ H s cl 4 N Ln h z ri N b x 0 Ei A d a P4 P4 a m U N .a p a a Its v o a U N W a C o �F � U Ln b 0 Ei P4 P4 .a p a a Q W a 'a Q w 6 o W U W A E Q w o W U W 7a- E n wg z- b b zE a x C y '0 E a a a �z U a a a � P U a a b U o @ a F C o N 6 a � N ci N a � p � p o doh e Q � U a zoo e ra a 00 w N z- U x a a a U a a � P U a a b U o @ a o N a � p � p o e � U U a a a a � P a a o @ a 0 0 pm a F4 N N 6 E a W U � q 0 0 pm a F4 N N 6 0. W U � O � V z q" ,3 N 1 + zC9 N W o vi GC U °O U w m o a � 3� � a 2 Uax66 0 0 pm a F4 N N 6 0. W U � V N ,3 N zC9 N R GC U m a � � a 2 Uax66 o U a a v Q a y QRa� 'v d ? N s � y 5aw i a mad Q V]Uo a 79 � F 6 U QF~a � e oV a v 0 o V N ry Q a N N 0. V N ZC5 N U a � � a Uax66 U a a v Q a y 'v i a a 79 � F 6 U U a � � a a a Q a SECTION 4 TSUMM111- "WIRONNIENTALUCHNOLOales, NG fArtafyfical Laboisfw'W5 February 27, 2018 Will Varner Synagro 284 Boger Rd. Mocksville, NC 27028 TEL: (336) 998-7150 FAX: (336) 998-8450 RE: Kinston Dear Will Varner: Sammti Eni onmenxal Technologies, lnC. 3310 Win St. Cuyahoga Falls, Ohio 44223 TEL (330) 253-8211 FAX. (330) 253-4489 Website: h11o'Apoviusettek.com Order No.: 18011115 Summit Environmental Technologies, Inc, received 1 samples) on 1/24/2018 for the analyses presented in the following report. There were no problems with the analytical events associated with this report unless noted in the Case Narrative. Quality control data is within laboratory defined or method specified acceptance limits except where noted. If you have any questions regarding these tests results, please feel free to call the laboratory. Sincerely, Jennifer Woolf Project Manager 3310 Win St. Cuyahoga Falls, Ohio 44223 Arkansas 88-0735, Galif nia 07256CA, Colorado, Connecticut PH -0108, Delaware, Florida NELAC E87688, Oeorga E87688, Idaho OH00923, Llinois 20006 1, Indiana C -OH -l3, Kansas E-10347, KorLLucky (Uvdergouud srorage Tank) 3, KenNcky 90146, Lotisiana 04061, Maryland 339, Mivuesota 409711, New Hampshire 2996,New Sersey OH006, New York ] 1777, North Carolina 39705 and 631, Nort1r Dakota 2-201, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Carolina 9201600t, Texas T104704466-11-5; Utah OH009232011-1, Virginia VELAP 9456, Washington C891 Page 1 of 28 msummly Summit Environmental Technologies, Wi St. Case Narrative 3310 Win St. MVIRONMIENTAL TACIMOLQGIE57 INC. Cuyahoga Falls, Ohio 44223 WO#: 18011115 Anafyfiral Laborafones TEL: (330) 253-8211 FAX: (330) 253-4489 Website: htto7/Avirmsenek.com Date: 2/27/2018 CLIENT: Synagro Project: Kinston WorkOrder Narrative: 18011115: This report in its entirety consists of the following documents: Cover Letter, Case Narrative, Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody, Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit Environmental Technologies, Inc., Work Order Number assigned to this report. Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation are attached as applicable. Results provided in this report for any parameter not listed on the Scope of Accreditation should be considered "not certified." The information contained in this. analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results contained in this report are only representative of the samples received. Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible for use or interpretation of the data included herein. All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as "dry weight" using the "-dry" designation on the reporting units. noted below. This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any comments or problems with the analytical events associated with this report are noted below. Analytical Sequence QC Notes: ecv 40ng S8- svoc-mstr_s(8270): CCV exhibited high recovery for Hexachloroethane. Associated samples are ND for these analytes. Original Page 2 of 28 U'Nt Summit Environmental Technologies, In Qualifiers and Acronyms Ffl S3310 Win 3 rNVIRONMENTO.L TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 4422 WOk: 18011115 Arralyterat Laboratories TEL: (330) 2534211 FAX,, (330) 253-443 Website: hup:/hvlrw.senekco Date: 2/27/2018 These commonly used Qualifiers and Acronyms mayor may not be present in this report Qualifiers U The compound was analyzed fox but was not detected. J The reported value is greater than the Method Detection Limit but less than the Reporting Limit. I -I The hold time for simple preparation and/or analysis was exceeded. D The result is reported from a dilution. E The result exceeded the linear range of the calibration or is estimated due to interference. MC The result is below the Minimum Compound Limit. * The result exceeds the Regulatory Limit or Maximum Contamination Limit. in Manual integration was used to determine the area response. d Manual integration in which peak was deleted N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response. P The second column confirmation exceeded 25% difference. C The result has been confirmed by GC/MS. % The result was not confirmed when GC/MS Analysis was performed. B/MB+ The analyte was detected in the associated blank. G The ICB or CCB contained reportable amounts of analyte, QC-/+ The CCV recovery failed low (-) or high (+), UQDR The RPD was outside of accepted recovery limits. QL-/+ The LCS or LCSD recovery failed low (-) or high (+), QLR The LCS/LCSD RPD was outside of accepted recovery limits. QM-/+ The MS or MSD recovery failed low () or high (+). )MR The MS/MSD RPD was outside of accepted recovery limits. QV-/+ The ICV recovery failed low (-) or high (+). S The spike result was outside of accepted recovery limits. Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for additional information Acronyms M Not Detected RL Reporting Limit QC Quality Control MDL Method Detection Limit MB Method Blank LOD Level of Detection LCS Laboratory Control Sample LOQ Level of Quantitation LCSD Laboratory Control Sample Duplicate PQL Practical Quantitation Limit QCS Quality Control Sample CRQL Contract Required Quantitation Limit DUP Duplicate PL Permit Limit MS Matrix Spike RegLvl Regulatory Limit MSD Matrix Spike Duplicate MCL Maximum Contamination Limit RPD Relative Percent Different MInCL Minimum Compound Limit iCV Initial Calibration Verification RA Reanalysis ICB Initial Calibration Blank RE Reextraction CCV Continuing Calibration Verification TIC Tentatively Identified Compound CCB Continuing Calibration Blank RT Retention Time RLC Reporting Limit Check CF Calibration Factor DF Dilution Factor RF Response Factor This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting. Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this list or for additional information regarding the use of these Qualifiers on reported data. Original Page 3 of 28 su ill_ Summit Environmental Technologies, Inc. Warkorder 3310 Win St. rNVIRONl.1ENUL TPCHNOLOtn Es, INC. Cuyahoga Falls, Ohio 44223 Sample Summary Analytical LaharaYoKes TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18011115 Website: htm:/hvnvnv.settekcom 27 -Feb -18 CLIENT: Synagro Project: Kinston Lab Samplell) Client Sample ID Tag No Date Collected Date Received Matrix 18011115-001 Kinston 1/15/20182: 20: 00 PM 1/24/201811:00:00 AM Sludge Page 4 of 28 \\ \\\\\\ } ©((\\« \ 18 ca Z5 94 !la:3mmlmm^, a/f;/eseee\§ ) } j \ ! }\ \: 3 / ;e!\ \ c 5umm'� SummitEnvironmental Technol10Wi St. Analytical Report 3310 Win SC. Report rrWRONMENTAL TECHNOLOGIES, VNC. Cyahoga Falls, Ohio 44223 (basereport) Analp6cal Laboratooes TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18011115 Website: hrtorl/www.settek.com Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/1 5/201 8 2:20:00 PM Lab ID: 18011115-OOIA Project: Kinston Client Sample ID Kinston Analyses Result RL Qual Units DF Date Analyzed TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: EAM TCLP MERCURY ANALYSIS (SW131117470) TCLP Mercury ND 0.00200 mg/L 1 1/26/2018 4:11:00 PM TCLP METALS, VOC, BNA, PEST, HERBSOLID SW6010D SW301OA Analyst: KMS TCLP METALS ANALYSIS (SW1311/6010) TCLP Arsenic(As) ND 0.500 mg/L 1 1/31/2018 12:50:34 AM TCLP Barium(Ba) ND 5.00 mg/L 1 1/31/201812:50:34 AM TCLP Cadmium(Cd) ND 0.100 mg/L 1 1/31/201812:50:34 AM TCLP Chromium(Cr) ND 0.200 mg/L 1 1131/201812:50:34 AM TCLP Lead(Pb) ND 0.500 mg/L 1 1/31/201812:50:34 AM TCLP Selenium(Se) ND 0.0500 mg/L 1 1!31/201812:50:34 AM TCLP Silver(Ag) ND 0.500 mg/L 1 1/31/201812:50:34 AM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW351OC Analyst: BJH TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270) 1,4 -Dichlorobenzene ND 0.0800 mg/L 2 1/29/2018 10:27:00 PM 2,4,5 -Trichlorophenol ND 0.200 mglL 2 11291201810:27:00 PM 2,4,6 -Trichlorophenol ND 0.200 mg/L 2 1/29/2018 10:27:00 PM 2,4-Dinitrotoluene ND 0.0400 mg/L 2 1/29/2018 10:27:00 PM o -Cresol ND 0.200 mg/L 2 1/29/2018 10:27:00 PM m/p-Cresol(s) ND 0.200 mg/L 2 1/29/2018 10:27:00 PM Cresols, Total ND 4.00 mg1L 2 1/29/2018 10:27:00 PM Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 1/29/2018 10:27:00 PM Hexachlorobenzene ND 0.0400 mg/L 2 1/29/2018 10:27:00 PM Hexachloroethane ND 0.0800 OC+ mg/L 2 1/29/2018 10:27:00 PM Nitrobenzene ND 0.0800 mg/L 2 1/29/2018 10:27:00 PM Pentachlorophenol ND 0.200 mg/L 2 1/29/2018 10:27:00 PM Pyridine ND 0.200 mg/L 2 1/29/2018 10:27:00 PM Surr: 2-Fluorophenol 27.8 10-109 %Rec 2 1/29/201810:27:00 PM Surr. Phenol -d6 11.5 10-109 %Rec 2 1/29/2018 10:27:00 PM Surr: Nitrobenzene -d5 50.8 19-120 %Rec 2 1/29/2018 10:27:00 PM Surr: 2,4,6-Tribromophenol 33.5 10-120 %Rec 2 1/29/2018 10:27:00 PM Surr: 2-Fluorobiphenyl 69.0 22-117 %Rec 2 1/29/2018 10:27:00 PM Qualifiers: ' Value exceeds Maximum Contaminant Level. E Value above quantitation range H Holding timesfor preparation or analysis exceeded M Manual lntegation usedto. detemrore area response MC Value is below Minimum Compound Limit. N Tentatively identified compounds ND Not Detected O RSD is greater than RSDlimit P Second column confirmation exceeds PL Permit Limit Original R RPD outside accepted recovery limits RL Reporting Detection Limit Page 6 of 28 R1 NUMMIll Summit Ersviranmental Technologies, 331010 es, Incc t. rNVIRON MENTAL TECHNOLOGIES, IPIC Cuyahoga Falls, Ohio 44223 Anatyticel Lehoreiorles TEL: (330) 253-8211 FAX: (330) 253-4489 Website: him:/hvwm.settekeom Analytical Report (base report) WO#: 18011115 Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date; 1/15/2018 2:20:00 PM Lab ID: 18011115-OOIA Project: Kinston Client Sample ID Kinston Analyses Result RI. QAaI IInits DF Date Analyzed TCLP METALS, VOC, BNA, PEST,. HERB -SOLID SW8270D SW3510C Analyst: BJH TCLP SEMI -VOLATILES ANALYSIS (SWI 31118270) gamma -BHC ND Sort: p-Terphenyl-d14 80.7 34-116 %Ree 2 1/29/2018 10:27:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP PESTICIDES ANALYSIS (SW131118081) Chlordane, total No SW8087 SW3510C Analyst: JBN 0.0200 Toxaphene ND Endrin ND gamma -BHC ND Heptachlor ND Heptachlor epoxide ND Methoxychlor ND Sort: TCMX 66.9 Sort: DCB 61.4 SW8087 SW3510C Analyst: JBN 0.0200 mg/L 2 1/29/2018 8:59:00 MEK ND PM 0.0400 mg/L 2 1/29/2018 8:59:00 ND Chloroform PM 0.00200 mg/L 2 1/29/2018 8:59:00 Vinyl chloride ND PM 0.00200 mg/L 2 1/29/2018 8;59:00 PM PM 0.00200 mg/L 2 1/29/2018 8:59:00 PM PM 0.00200 mg/L 2 1/29/2018 8:59:00 PM PM 0.00200 mg/L 2 1/29/2018 8:59:00 PM PM 10 -119 %Rec 2 1129/2018 8:59:00 PM PM 10 -119 % Rec 2 1/29/2018 8:59:00 PM PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP HERBICIDES ANALYSIS (SW1311/8151) SW8151A SW8151A Analyst: JBN 254-D ND 1.00 25415 -TP ND 0.500 d Surr: DCAA 80.1 20-140 TCLP METALS, VOC, BNA, PEST, HERB -SOLID TCLP VOLATILES ANALYSIS 1,1-Dichloroethene ND 1,2-Dichloroethane ND MEK ND Benzene ND Carbon tetrachloride ND Chlombenzene ND Chloroform ND Tetrachloroethene ND Trichloroethene ND Vinyl chloride ND mg/L 1 1/31/2018 3:42:00 10 1/29/2018 7:07:00 PM mg/L 1 1/31/2018 3:42:00 mg/L 10 PM °(o Rec 1 1/31/2018 3:42:00 mg/L. 10 PM SW8280B SW1311M Analyst: CTB 0.0500 mg/L 10 1/29/2018 7:07:00 PM 0.0500 mg/L 10 1/29/2078 7:07:00 PM 0.250 mg/L. 10 1/29/2018 7:07:00 PM 0.0500 mg/L 10 1/29/2018 7:07:00 PM 0.0500 mg/L 10 1/29/2018 7:07:00 PM 0.0500 mg/L 10 1/29/2018 7:07:00 PM 0.0500 mg/L. 10 1/29/2018 7:07:00 PM 0.0500 mg/L. 10 1/29/2018 7:07:00 PM 0.0500 mg/L.10 1/29/2018 7:07:00 PM 0.0200 mg/L.10 1/29/2018 7:07:00 PM Qualifiers:* Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC E Value above quantitation range Value is below Minimum Compound Limit ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits M Manual Integration used to determine area response N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 7 of 28 UMM I SpmmitEm�ironmental Technologies, Inc.MIS3310 Win St. Analytical Report F14VIRON6IENTAL rECONOLOG1E5, INC. Cuyahoga Falls, Ohio. 44223 (base report) Analytical Laboratories TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18011115 Website: htto7/Avinvsettek.com Date Reported: 2/27/2018 CLIENT: Synagro Tag Number: Matrix: SLUDGE Collection Date: 1/15/2018 2:20:00 PM Lab ID: 18011115-OOIA Project: Kinston Client Sample ID Kinston Analyses Result RL Qual Units DF Date Analyzed Cyanide, Reactive No 0.500 mg/Kg 1 1/29120184:46:00 PM TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SW1311M Analyst: CTB TCLP VOLATILES ANALYSIS Ignitability non-flammable 1 1/25/2018 1:00:00 PM Surr: 4-Bromofluorobenzene 100 70-130 %Rec 10 1/2912018 7:07:00 PM Surr: Dibromofluoromethane 97.4 70-130 %Rec 10 1/29/2018 7:07:00 PM Surf: Toluene -d8 96.8 70-130 %Rec 10 1/29120187:07:00 PM RCI-SOLID-W/IGNITABILITY7030 SW9014 Analyst: MS REACTIVE CYANIDE (901417.3.3.2) -SOLID Cyanide, Reactive No 0.500 mg/Kg 1 1/29120184:46:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW1030 Analyst: AJT IGNITABILITY OF SOLIDS (SW -846: 1030) Ignitability non-flammable 1 1/25/2018 1:00:00 PM RCI -SOLID -W/ IGNITABILITY1030 SW9045D Analyst: DHC PH (SW9045D) pH 6.4 s.u.@19.1C 1 2/81201811:37:00 AM RCI -SOLID -W/ IGNITABILITY1030 SW9034 Analyst: MS REACTIVE SULFIDE (9034)17.3.4.2 Sulfide, Reactive ND 25.0 mg/Kg 1 1/29/2018 4:46:00 PM Qualifiers: " Value exceeds Maximum Contaminant Level. H Holding times for preparation or analysis exceeded MC Value is below Minimum Compound Limit. ND Not Detected P Second column confirmation exceeds R RPD outside accepted recovery limits E Value above quantitation range M Manual Integration used to determine area msponse N Tentatively identified compounds O RSD is greater than RSDlimit PL Permit Limit Original RL Reporting Detection Limit Page 8 of 28 SU 111StamnitEnvionmentalTechnologies,Inc. Accreditation Program 3310 win St. Analytes Rep ort fTWIRONhIENTAL 1£�LIINOLOOI£S, INC Cuyahoga Falls, Ohio 44223 J C Analyflral l.shorsrm7es TEL: (330) 253-8211 FAX: (330) 253-4489 WO#: 18011115 ffebsite: huallwirip.seuekewm 27 -Feb -18 Client: Synagro State: NW Project: Kinston Program Name: NC—WW—SCM Sample ID Matriz Test Name Analyte Status 18011115-OOIA Sludge Ignitability of Solids (SW -846: 1030) Igritability A Sludge pH(SW9045D) Hydrogen Ion (pH) A Sludge. Reactive Cyanide (9014/7.3.3.2) -Solid Cyanide, Reactive U Sludge. Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U Sludge TCLP Herbicides Analysis (SWI 311/8151) 2,475 -TP A Sludge TCLP Herbicides Analysis (SWI 311/8151) 234-D A Sludge TCLP Herbicides Analysis(SW1311/8151) DCAA A Sludge TCLP Mercury Analysis(SW131 V7470) Mercury A Sludge TCLP Metals Analysis (SW1311/6010) Arsenic A Sludge TCLP Metals Analysis(SWI311/6010) Barium A Sludge TCLP Metals Analysis (SWI 311/6010) Cadmium A Sludge TCLP Metals Analysis(SW1311/6010) Chromium A Sludge TCLP Metals Analysis(SW1311/6010) Lead A Sludge TCLP Metals Analysis(SW1311/6910) Selenium A Sludge TCLP Metals Analysis(SW1311/6010) Silver A Sludge TCLP Pesticides Analysis (SW1311/8081) 2,2',3,3',4,4',5,5',6,6'- A Decachlorobiphenyl Sludge TCLP Pesticides Analysis (SW 1311/8081) Chlmilme, total A Sludge TCLP Pesticides Analysis (SW 1311/8081) Endrin A Sludge TCLP Pesticides Analysis(SW1311/8081) gamma-BIIC A Sludge TCLP Pesticides Analysis (SW1311/8081) Heptachlor A Sludge TCLP Pesticides Analysis (SW1311/808 1) Heptachlor epoxide A Sludge TCLP Pesticides Analysis (SWI 31 U8081) Metboxychlm A Sludge TCLP Pesticides Analysis (SW13 [1/808 1) Tetcachloro-m-xylene A Sludge TCLP Pesticides Analysis (SWI 311/8081) Toxaphene A Sludge TCLP Semi -Volatiles Analysis (SWI 311/8270) 1,4-Diclilorobenzene A Sludge TCLP Semi -Volatiles Analysis (SWI 311/8270) 2,4,5 -Trichlorophenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-Tribromophenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4,6-'Friehlorophenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2,4-Dinitrotoluene A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Fluorobiphenyl A Sludge TCLP Semi-Volatites Analysis (SW1311/8270) 2-Fluorophenol A Key Key NC—WW—SCM A Accredited NC—WW—SCM U Unavailable Version #2 Page 9 of 28 S U IEF SunsnitEnvironmentalTechnologies, Inc. Accreditation Program EI3310 Win St. Analytes Report MVIRONMENTAL rECBNOLaWE5, INC Cuyahoga Falls, Ohio 44223 y P Analytical Laharetewes TEL: (330) 253-8211 FA"... (330) 253-4489 WO#: 18011115 Website: huv.,1Avww.seuekc°n' 27 -Feb -18 Client: Synagro State: NW Project: Kinston Program Name: NC—WW—SCM Sample ID Matrix Test Name Analyte Status 18011115-o01A Sludge TCLP Semi -Volatiles Analysis (SWI 311/8270) 2-Methylphenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 3,4-Methylphenol A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Cresols, Total A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobenzene A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachloroethane A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Nitrobenzene A Sludge TCLP Semi -Volatiles Analysis (SW 1311/8270) Nitrobenzene -d5 A Sludge TCLP$ami-Volatiles Analysis(SW1311/8270) Pentachlorophenol A Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Phenol -d6 A Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) p-Terphenyl-dl4 A Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) Pyridine A Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A Sludge TCLP Volatiles Analysis 1,2-Dichloroethane A Sludge TCLP Volatiles Analysis 2-Butanone A Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A Sludge TCLP Volatiles Analysis Benzene A Sludge TCLP Volatiles Analysis Carbon tetrachloride A Sludge TCLP Volatiles Analysis Chlorobenzene A Sludge TCLP Volatiles Analysis Chloroform A Sludge TCLP Volatiles Analysis Dibromolluoromethane A Sludge TCLP Volatiles Analysis Tetrachloroethene A Sludge TCLP Volatiles Analysis Toluene -d8 A Sludge TCLP Volatiles Analysis Trichloroethene A Sludge TCLP Volatiles Analysis - Vinyl ebloride A NC_WW_SCM A Accredited NC_WW_SCM U Unavailable Version #2 Page 10 of 28 y r� H 7 d J N 0 ❑1 � U a`" 7 00 J N y ❑1 � � rG M � � y � d � 10 � a 9 U p v q m C6 m E d m E m 7 00 N y � � 0 m � � y � OD 0 10 � a 9 J ❑ v q m U m E d m E m in U Q 7 00 N y � � U m � q M � J 0 10 U U J J ❑ v q m U m o m E m m � y U Q 7 00 N � 0 m KrL q M � D) 0 10 U U J J ❑ v q m � m O m E m � y U Q 7 3'S 00 N � y m KrL q M � D) 0 10 d � d [ v q U O E m � rn 7 � ❑ 3 F U O A Ql ❑ m ❑ � m d m E v - y U Q 3'S 00 N O y m q � � D) 0 10 d EL y � Y � Z d � [ v q A m � 7 � ❑ 3 F O y � d � A m ❑ 3 F O m ❑ E v - m U y � d � E m ❑ O m ❑ E v - m U ; �y ({ ) &s � )Z �y \ 0 ) � )Z \ 0 \ ) � }\\� \j§) \))j \ J � o O d w > E ' d N J � o d w > E ' d N y � 0 P. 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If L v� 12, 01 z l a Sl z A.4If i4 .wL 'r,�l ao iri=f[MI ,qp if y `? f W vv �a A m c'iS E n ` a 1 4 -,� a' W r t a CL i Y sO son q w No' _ a r> Q 0 o MIMI 3 III �o❑aux.- 8 ba r ; $n No Iy Zr y,1 E .1 U V U SUMMIT S emit Ehvirenmenta7 Technologies, Inc. ffl3310 Win St. rNviRONMFN1'AL 1aCHNOLOrlts, INC_ Cuyahoga Palls, Ohio 44223 Sample Log -in Check List Analytical Lebarsiorlgs TEL: (330) 253-8211 FAX: (330) 253-4489 Website: htty.Iliviviv.seuck.coni Client Name: SYN -NC -27028 Work Order Number: 18011115 RcptNo: 1 Logged by: Christopher Livengood Completed By: Christopher Livengood Reviewed By: Jennifer Woolf 112412018 11:00:00 AM 112412018 3:57:45 PM E Iii:7 iAS E:I �i E Fi F1r7 9 i4 l Chain of Custody 1. Is Chain of Custody complete? Yes W No ❑ Not Present ❑ 2. How was the sample delivered? FedEx Lop In 3. Coolers are present? Yes No ❑ NA ❑ ¢, Shipping. container/cooler in good condition? Yes ❑� No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑�. No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑ g, Were all samples received at a temperature of >0° C to 6.0°C Yes ❑� No ❑ NA ❑ 7, Samples) in proper container(s)? Yes © No ❑ Signed By 8. Sufficient sample volume for indicated testis)? Yes © No ❑ g, Are samples (except VOA and ONG) properly preserved? Yes No ❑ 10. Was preservative added to bottles? Yes ❑ No ❑ NA ❑+� NA 11, Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes. ❑ No W No VOA Vials 0 12, Were any sample containers received broken? Yes ❑ No ❑� 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14. Are matrices correctly identified on Chain of Custody? Yes No ❑ 15. Is it clear what analyses were requested? Yes W No ❑ 16. Were all holding times able to be met? Yes 0 No. ❑ (If no, notify customer for authorization.) $Aecial Handling (if applicable) 17, Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA 0 Person Notified: Date By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person Regarding: Client Instructions: 1g, Additional remarks: Cooler Information Cooler No Temp °C Condition Seal Intact Seal No Seal Date Signed By 1 5.7 Good Not Present Page 28 of 28 SECTION 5 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility. Name: City of Kinston, NC WQ Permit Number: W00003919 W WTP Name: Kinston Regional WRF NPDES Number: NC0024236 Monitoring Period: From 01/01/2018 To 12/31/2018 Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed: Class A: Alt. I/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing) Alt 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP) If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying Heat Treatment Thermophilic Beta Ray Gramma Ray Pasteurization Class B: Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying Composting Aerobic Digestion Anaerobic Digestion If nnnlirahle to alternative nerformed iCla.es A nr Cln.es Rl comnlete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Vector Attracti No. of Frequency Sample Analytical (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Excee- of Type Technique (Drying—Stable) (Drying—Unstable) Minimum Geo. Mean Maximum Units dences Analysis (Injection) Fecal 2x10 to the 611 NIPN MPN/g Coliform power per gram of total solids CFU 61,700 185,522 445,000 CFU/g 0 Annually Grab SM9222D 1000 NUN per gram of MPN/g total solids (dry weight) Salmonella 3 MPN per 4 grams total bacteria (in solids (dry weight) lieu of fecal coliform) on Reduction (40 CFR 503.33/15A NCAC 02T:1107) -Please indicate option/alternative performed Option/Alt. 1 Option/Alt, 2 Option/All. 3 Option/AIT. 4 (VS reducti CERTIFICATION STATEMENT (please check the appropriate statement) "I cert ify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T1106 and the vector attraction R reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements m 40 CFR 503.32/15A NCAC 021.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector att raction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Kenneth Stevens, WWTP Superintendent Prep ame and Title (type. or print) Land Applier Name and Title (if applicable) (type or print) Signature ofPreparer* Date Signature of Land Appliee (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date on) (40 -day bench) (30 -day bench) (Spec. 02 uptake) X Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8 (14 -Day Aerobie) (Alk Stabilization) (Drying—Stable) (Drying—Unstable) Option/Alt. 9 Option/Alt. 10 (Injection) (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I cert ify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T1106 and the vector attraction R reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met." "I certify, under penalty of law, that the pathogen requirements m 40 CFR 503.32/15A NCAC 021.1106 and the vector attraction reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector att raction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment" Kenneth Stevens, WWTP Superintendent Prep ame and Title (type. or print) Land Applier Name and Title (if applicable) (type or print) Signature ofPreparer* Date Signature of Land Appliee (if applicable) *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26) Date Cameron ing Services, Inc. Laboratory Report NC DENR #654 NC PHHS #37799 U5 EPA #NC0191a Synagro QTS Proj. 180558 Kinston Regulatory Yes Sample Information W. Varner Date 04/03/18 ')teceived E. Puckett Date 04/04/18 Analyses and Results 1805581 D1 180558 01 Report Revlew 219 S. Steel Str, Sanford NC 27330 a �mdar cr Fec. Coliform -S h c d e f 9 Geomean 61700 cFwe 617D 04104/18 SB/6RP 9222D -MF 232000 CFwe 6100 135000 CFU1a 6410 386000 CFU/g 6210 224000 CFUra 5880 102000 cmg 5990 445000 CFU/9 6100 185522 a swdue Gr TS (%) 16,2% 0.0t (14!05115 SB b 16.4% c.o1 c 15.6% 0.01 d 16.1% 0,o1 e 17.0% 0.01 f 16.7% 401 9 16,4% 0.01 V 71ia/-/ Date 2540 G -T8 919-2084240 chis n cantarontesting.cnm 0 M N N O a m a z Z u1 rn o N o � m o � I� I m a 60 Cl - ✓ll ! U I� I i E' z" C hi O o > 4i N W IlL 7 C p I a Loa f� z bd m � Vri t o' O V IE I I , 4 w vz �a41O sselO zo O I - j � opseld l L I c4, . �i I v � 6i .04 sselO l L O OOA-lw Ob h E `� eiaeloeg 009 'le'J zl l • w a z F. o xis;eW � I /dwoo 6�b 00 1^!n CD awil Nm ` `— 0) o U �I Z ry ` alea c� SII � 1. oI Ll z . �I j m MOM O T (11 z C NLS m d ..9 Q �I dRL E sl E p v a U Time minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name. Riosolids Permit Number, Date Digester Temperature; Sampling Date/Time; Sampled By. Analysis DateMrre; Analyzed By: Sample volume; Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Ima/li KRWRF 40008919 3/23/2018 12 3/23/18 7:57am SF 3/23/18 8:00am SF 9.37 300 1.9 12,97 9.82 8.95 8.75 9.07 9.22 9.4 9.4 9.4 9.37 9.23 9.15 9.07 8.98 8.92 8.95 8.88 8.81 Slope: Intercept; Correlation Coefficient: milliliters %a Dry Solids degrees Celsius 9egrees Celsius Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygen/glhr Average Temperature: 11.4 degrees Celsius Temperature Correction Factor: 1,72 Temperature Corrected Specific Oxygen Uptake Rate' 0.32 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The GalcuNatien and the Spreadsheet execute automatically. it Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Speoific Oxygen Uptake Rake SOUR Facility Name Biosclids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis Date/Time, Analyzed By. Sample volume Total Solids Beginning Temperature End Temperature Dissolved Oxygen Level I mall! 8.92 8.99 9.54 9.87 9.98 10 9,97 9.89 9,89 9.84 9.7 9.54 9.52 9.4 9.4 9,28 Slope: Intercept: Correlation Coefficient: KRWRF WQ00039;am 3/ 3!23/18 8 SF 3/23118 8 SF 300 1,9 13.7 9,53 milliliters %Dry Solids Jag Celsius Jag Celsius Oxygen Uptake Rate: mg oxygen/hr Ambient Specific ©xygen Uptake Rake: mg Qxygen/g/hr Average Temperature: 11.6 degrees Celsius Temperature Correction Factor: 1.72 Temperature Corrected Specific Oxygen Uptake hate: 0.46 mg Oxygen/g/hr Instructiens: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 2 Time minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name Biosolids Permit Number Date Digester Temperature Sampling DatelTime Sampled By Analysis DateRime Analyzed By Sample Volume Total Solids Beginning Temperature End Temperature pissolved Oxygen bevel Ima/11 8.53 9.5 9.92 10.1 10.19 10.25 10.23 10.24 10.13 10.09 9.99 9.98 9.96 9.89 9.83 9.76 Slope; Intercept: Correlation Coefficient: KRWRF 'millilit VQ WQ0003919 3/2312018 12 3123/18 9:01am SF 3123/18 9:05am SF 300 1.9 14.27 9.58 ers Dry Solids leg Celsius Jog Celsius Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: mg Oxygen/g/hr Average Temperature: 11.9 degrees Celsius Temperature Correction Factor: 1.72 Temperature Corrected Specific Oxygen Uptake Rate: 0.28 mg Oxygen/g/hr Inskruatians: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. 3 Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 specific Oxygen Uptake Rate SOUR Facility Name 6iosalids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis DateMme: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Ima/Il 7.64 8.84 9.22 9,5 9.54 9.81 9.86 9.87 9.85 9,6 9.85 9.61 9.49 9.52 9.38 9.37 Slope : Intercept; Correlation Coefficient: ICRWRF milliliters WQ0003919 3/23/2018 12 3/23118 9:39am SF 3123/18 9:43am SF 300 1.9 14.36 10.25 Dry Solids leg Celsius iegrees Celsius Oxygen Uptake Rate; mg Dxygen/hr Ambient Specifio Oxygen Uptake Rate: mg Dxygen/glhr Average Temperature: 12.3 degrees Celsius Temperature Correction Factor: 1,72 Temperature Correotad Specific Oxygen Uptake Rate: 0.36 mg Oxygen/glhr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 0 Tima (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 16 Specific Oxygen Uptake Rate SOUR Facility Name 8iosolids Permit Number' Date. Digester Temperature. Sampling Date/Time, Sampled By. Analysis DatelTime: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: ❑issoived Oxygen Level Wail) 6.12 6.58 9.05 9.91 9.46 9.47 9.5 9.51 9.56 9.49 9.44 9.31 9.24 9,18 9.07 9,02 Slope: Intercept: Correlation Coefficient milliliters KRWRF WQ0003919 3/23/2018 12 3/23/18 10.12am SF 3/23/18 10:17am SF 300 1.9 14.19 10.32 YO Solids leg Celsius leg Celsius Oxygen Uptake Rate: mg Oxygen/hr Ambient Specific Oxygen Uptake hate: mg Oxygenlg/hr Average Temperature: 12.3 degrees Celsius Temperature Correction Factor: 1.72 Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically. l•� SECTION 6 Lime Recommendation Calculation Using A&L Soil Report Soil pH Target pH Acidity Lime Recommendation Soil pH Target pH Acidity 0.4 tons per acre Lime Recommendation 0.6 tons per acre JO -8790-5 JO -8790-6 Lime Recommendation Calculation Using A&L Soil Report On pH Target pH Acidity Lime Recommendation Soil pH Target pH Acidity 0.9 tons per acre Lime Recommendation 0.0 tons per acre JO -8790-7 Agricultural Lime Application Log E'er Project: Kinston, NC *Lime is ordered for first quarter 2019 Field (state -county -site -field) Soil pH Lime Requirement Tons/Acre Date Applied (tons/acre) Applied NC -JO -8790-5 5.4 0.4 NC -JO -8790-6 5.2 0.6 NC -JO -8790-7 5.0 0.9 =E====� *Lime is ordered for first quarter 2019 SECTION 7 3 w z C u. v N a $ m �o N rl N N '�+ o c � � v o ELL x O w o z C) o 0 n 3 a m ¢ m n 3 3 c 'n b o a eo w ym m s y fn�N(n� N CO n 3 w z C u. v O w N h o � y rn v O w o z C) 0 n a � ¢ 3 w z C u. 2 O w N h y 2 0 C) n U mo w ym m y fn�N(n� 2 O 2 h y 2 h W U y CO WN r U v v Lo U c � N C V h N g r y Y d M Q N G N 4 m L6 3 x C5 6 n U z z z y O 0 ICL`o r N L �l 2 m J