WQ0014868_Residual Annual Report 2018_20190314

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0014868
SUBMITTAL DATED: 2/28/2019
Project Contact Information
Hease provide inforrration on the person to be contacted by MB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Brent Collins
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0014868
Permittee * Donovan Owens
Facility Name * Smithfield Fresh Meats Corp.
Phone Number*
336-751-1441
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Hans, Specifications, Calculations, Etc.)
Smithfield Fresh Meats Annual Report -
3.17M6
WQ0014868. pdf
l pload only 1 HDF docurrent. NLltiple docurrents must be combined into one H7F file.

For neiv and modif cation permit applications, the paper copy is required to be submitted to the
Di,,isiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ping:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,,ision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942 M
512 N_ Salisbury St_ Raleigh, NC 27604
For questions or problems contact Tessa Monday at: 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
* I40 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/28/2019

Smithfield Fresh Meats RECE1VEDmCDEO1D%R
Tar Heel Facility MAR - 4 2019
2018 Annual Report Non -Discperm�ttan9h U pit
Residuals Land Application
Permit No. WQ0014868
RECEIVED
DEQ1DVVR
MAR 18 2019
WOOS
Prepared By:
EMA Resources, Inc.
Phone [phone] —Fax [phone]
755 Yadkinville Rd;-- Mocksville, NC 27028
WrP9 RI)
MAR 0 4 2010
D1112 3[fifl9il
fNFOIKIAPON FR(fOW16 Uf113

February 28, 2019
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
RL-u IVtu
DEOIDWR
MAR 18 2019
WOROS
FAYETT ,.':.' ` Ci:.' OFFICE
Re: 2018 Annual Report — Smithfield Packing Co.
Treatment and Land Application of Residuals
Permit No. WQ0014868
Dear Sir or Madam:
RECEIVEDlNCpr^IDWR
Enclosed is one copy of the 2018 Annual Report for the above referenced land
application permit. The report has also been submitted online.
MAR - 4 2019
Nan-Discn:,r.; j
Permitting Unit
During 2018 EMA Resources, Inc. land applied 143.76 dry tons of wastewater residuals
to 71.7 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sinc ely,
rto
ent Collins
Director of Technical Services
brent.collinsna.emaresourcesine.com
Phone [phone] — Fax [phone]
755 Yadkinville Road — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0014868 County:
Facility Name (as shown on permit):
Land Application Operator:
Bladen
Year: 2018
Smithfield Fresh Meats Corp.
EMA Resources Inc. Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
0 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in thepermit:
37
Total number of fields utilized for land application during the year:T
5
Total amount ofdry tons applied during the year for all application site—s.F
143.76
Total number of acres utilizes for land application during the year: 1
71.7
Part tt - Annual C;ompiance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. O Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T . 1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in I SA NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified
in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the possibility
of fines and imprisonment for knowing violations."
Donovan Owens - General Manager
Name and Title (type or print)
Signature of Permittee Date
Z; 2/5/2019
Signature of Preparer* Date Signature of Land Applier
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T 1 102 (26)
Date
DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0014868
Facility Name: Smithfield Fresh Meats Corp.
Residual Source WQ # or
NPDES #:
NCO078344
WWTP Name: Tarheel Plant W WTP
Residual Analysis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Conc.
Limit
m k a
Sample or Com osite Date
North
4/4/18
North
4/23/18
Average
Percent Solids (%)
NA
3.51
2.47
2.99
Arsenic
75
3
3.19
3.095
Cadmium
85
2
2
2
Copper
4,300
1140
1210
1175
Chromium
NA
41.7
37.5
39.6
Lead
840
8.02
7.61
7.82
Mercury
57
0.4
0.4
0.4
Molybdenum
75
15.1
14.2
14.7
Nickel
420
33.3
32.5
32.9
Selenium
100
5.25
5.51
5.4
Zinc
7,500
2410
2440
2425
Total Phosphorus
NA
14700
12400
13550
TKN
NA
84400
54400
69400
Ammonia -Nitrogen
NA
11900
13300
12600
Nitrate and Nitrite
NA
2.27
2.35
2.31
4- — 1--1 MV cclu!!g cvm:culrauvn omits usiea in mis form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
a
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
'! / 1�
Date
DENR FORM RSSF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0014868 Laboratory:
Facility Name: Smithfield Fresh Meats Corp.
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analvsis Data
NCO078344
Tarheel Plant W WTP
1) Waypoint Analytical
2)
3)
4)
5)
�r
..Calciu.Magnesium ...
Ill
„
•' l l
_________
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series:
Acres Used: 21.6 Acres Permitted: 21.6 Site #: SF03 Field #:
Residual Analvsis Data (Heavv Metals and Tnt.l --a_ ni
23.50
8.5
LaB
1
Sample
1
2
3
4
- - ----
5
-------i---••_
.,.., ......,
...5„�S,
iv Nvaauo
u�G
i�sivr 1 Gr�;Glll
thy:
or
6
7
8
9
10
11
12
Com-
April
posite
Average
Date
% Solids
2.99
Arsenic
3.1
Cadmium
2
Copper
1175
Chromium
39.6
Lead
7.82
Mercury
0.4
Molyb-
denum
14.65
Nickel
32.9
Selenium
5.38
Zinc
2425
al
s-
Lh
13550
rus
A"".,.I
Total
121
3
141
1 5
6
7
8
9
10
11
12
DT/Ac./
�-3
App.
0
>v
Event
1.09
Arsenic
0.007
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.007
Cadmium
0.004
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.004
Copper
2.557
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0. 000
0.000
0.000
2.557
Chromium
0.086
0.000
0.000
0.000
O.OpO
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.086
Lead
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.001
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
enum denum
0.032
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.032
Nickel
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Selenium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
Zinc
5.277
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.277
Total
Phos-
29.485
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
29.485
horus
11-F PartiA7
1-11-
-- ­.., ... ,,,,., uVb4L-k Ty"O y1cV"1vu u..uGr,ny uirection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2!:f-e 2/5/2019
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp.
Land Owner:
Operator:
Steve Dunham
Steve Dunham
Crop 1 Name: Bermuda -Pasture
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 23.50 Site #:
Predominant Soil Series:
LaB
Crop 1 Max. PAN: 147 Crop 2 Name:
Acres Utilized:
SF03 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
21.6
21.6
8.5
0 =
Volume applied
PP �
Volume
Residual Sources
Soil
Cond.
Precip.
>
o
'�
Z a
Nitrate
Name of CropT
U �
(enter one) Solids/
%
Applied per
PP P
(NPDES #, WQ#,
Past 24
w ,
�
TKN
o
and
PAN Applied
Receiving Residua
Q
Liquid
Solids
Acre
Fert., Animal
(Dry,
Hrs.
o m
N'
CD
+� -
°Q
o
Nitrite
(lbs/acre)
Application
Cu. Yds Gallons
(Dry Tons/Ac)
etc
Waste, )
Wet,
Moist)
inches
o
*
mg/kg
69400
mg/kg
12600
mg/kg
2.31
Crop 1
Crop 2
Crop 1
Crop 2
4/26
188500
1 2.99
1.088
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
38.436
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
o.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this
form):
TOT�t
01 1885001...:
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
0.000
Lime Applied
Annuallbs/acre
0.007
0.004
2.557
0.086
0.017
0.001
0.032
0.072
0.012
5.277
29.485
'38.4361
::
Date lbs/ac
Prior Years Cumulative lbs/ac
0.183
0.190
0.084
0.088
9
38.475
41.032
250
2.17
2.256
0.596
0.613
1000
0.021
0.022
1.184
1.216
3.486
3.558
250
0.257
0.269
163.314
168.591
500
.........
,Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
14 7
-1. cerniy, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2019 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series:
Acres Used: 13.3 Acres Permitted: 13.3 Site #: SF03 Field #:
Residual Analvsis Data (Heavv Metalc anti Tntzl Ph-h-..
31.11
8.6
Ce
2
Sample or
1
2
3
4
5]
ua�a�s9
i� uviaua
uac
AVAW r V1
cent ff):
161
7
8
9
1101
111112
Com-
April
posite
Average
Date
% Solids
2.99
Arsenic
3.1
Cadmium
2
Copper
1175
Chromium
39.6
Lead
7.82
Mercury
0.4
Molyb-
denum
14.65
Nickel
32.9
Selenium
5.38
Zinc
2425
Total
Phos-
13550
horus
Ann»�1
17en 1%4-,&.1
T.S..Ia
i __J•__--
�i._■
,.
Total
1
21
3
1 41
5
1 61
7 7
1 8
9
10
11
12
DT/Ac./
y
App.
0
Event
2.34
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
j 0.000
0.000
0.000
1 0.000
0.000
0.000
0.009
Copper
5.497
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.497
Chromium
0.185
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.185
Lead
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Nickel
0.154
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
0.154
Selenium
0.025
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.025
Zinc
11.344
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.344
Total
Phos-
63.387
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
63.387
horus
-. -- 1------J __ -^•• f ....v --l- --a P,vpaicu uuuC.- my ulrection or supervision In accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing
Lviolations".
2�z 2/5/2019
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 2 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 31.11 Site #: SF03 Acres Permitted:
Steve Dunham Predominant Soil Series: Ce Cation Exchange Capacity (non 5031:
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 168 Cron 2 Name: Oran') Mn PAN.
13.3
13.3
8.6
o +�
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
PP p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)Wet,
Soil
Cond.
(Dry.
Moist)
Precip.
Past 24
Hrs.
inches
>
o
o
a
C
o
;U
* N'
;d
CD ?y
TKN
mg/kg
69400
Z y
o
°° °
mg/kg
12600
Nitrate
and
Nitrite
mg/kg
2.31
1
PAN Applied
(]bs/acre)
Name of Crop Type
Receiving Residual
g
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/21
65000
2.99
0.609
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
21.525
NA
Bermuda
4/22
132500
2.99
1.242
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
69400
12600
2.31
43.878
NA
Bermuda
4/23
52000
2.99
0.487
Tarheel WWTP
Dry
<•5"
S
0.5
0.2
69400
12600
2.31
17.220
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
Annual
0 24gsoo ::::::::...
lbs/acre
As
0.015
0.175
0.190
Cd
0.009
0.063
0.072
9 1250
Cu
5.497
37.819
43.316
Cr
0.185
1.665
1.850
Pb
0.037
0.651
0.688
1000
N
0.002
0.019
0.021
Mo I
0.069
1.041
1.110
Ni
0.154
3.751
3.905
250
Se I
0.025
0.218
0.243
Zn
11,344
153.511
164.855
500
P 82.624 0.000
63.387
Lime A lied
Date ]bs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.
Permit PAN Limit 1 st/2nd Crop
168
- ---.71 r-•== .7 ­', --" 1■; uU%�u■.,r, L was pi-epareu unaer my airection or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2019 **Volatilization Rate: Surface - 0.5, Injection/incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual): 51.06
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only): 5.7
Operator: Steve Dunham Owner: Steve Dunham Predominant Soil Series: Ce
Acres Used: 21.3 Acres Permitted: 21.3 Site #: SF03 Field #: 3
Residual Analvsis Data tApavv MPtate anti Tn+al -1 - r
M
©
©
©
in0
Com-
•.
posite._�
Date
Total
,0
Total
Llj
2
3
4
5
6
7
8
9
10
11
12
DT/Ac./
► q
App.
0
iv
Event
2.40
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.015
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
5.633
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.633
Chromium
0.190
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.190
Lead
0.037
0.000
0.000 1
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.037
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
enum
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Nickel
0.158
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.158
Selenium
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Zinc
11.625
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.625
Total
Phos-
64.959
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
64.959
horus
Tv as yi cyaJIcu UHUCI- Illy Ulrrcuon or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2/5/2019
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
Operator:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Smithfield Farmland Corp. WQ Permit #: WQ0014868 Field #: 3 Acres Utilized:
Steve Dunham Annual Dry Tons Applied: 51.06 Site #: SF03 Acres Permitted:
Steve Dunham Predominant Soil Series: Ce Cation Exchange Capacity (non 503):
Crop I Name: Bermuda -Pasture Crop I Max. PAN: 168 Cron 2 Narne! r...,.,')n r.,., D A XT.
21.3
21.3
5.7
O
d °
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
PDES #, W #,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
n "a
o� o
5
C
o
"
*
e
p
*
TKN
mg/kg
69400
69400
69400
z a
�o °
mg/kg
1 12600
12600
12600
Nitrate
and
Nitrite
mg/kg
2.31
2.31
2.31
1
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/18
4/19
4/20
71500
201500
136500
2.99
2.99
2.99
0.419
1.180
0.799
Tarheel WWTP
Tarheel WWTP
Tarheel WWTP
Dry
Dry
Dry
<.5^
<.5"
<.51,
S
S
S
0.5
0.5
0.5
0.2
0.2
0.2
14.785
41.666
28.225
NA
NA
NA
Bermuda
Bermuda
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM
FSF supp (attach FORM
FSF supp to this
form):
.. .
TOTALS:
Annuallbs/acre
0 409500 ::::;:::::::
As
0.015
0.143
0.158
Cd
0.010
0.071
0.081
9
Cu
5.633
30.22
35.853
250
Cr
0.190
1.215
1.405
Pb
0.037
0.491
0.528
1000
H
0.002
0.015
0.017
Mo
0.070
0.82
0.890
Ni
0.158
2.849
3.007
250
Se
0.026
0.173
0.199
Zn
11.625
123.082
134.707
500
P 1 84.676 0.000
64.959 ::
:::.....::::
............................
Lime Applied
Date lbs/ac
Prior Years Cumulative Ibs/ac
2000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit I st/2nd Crop
6411 ,. 4:r_, ..a.
168
_ ___ ---.I______ 1....... I -- .w.., „ -- <u,- -"V U111C111 VV45 P1 Upal CU uuuer my uirection or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Zf 4; ", ,,. *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2019 **Volatilization Rate: Surface - 0.5, Injection/incorporation -1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
20.26
9.7
LaB
Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosnhorus use mfr/ku- %. galid.v uVP Raw PPr..Pnt ffl•
Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
WQ0014868 Cation Exchange Capacity (non 503 only):
Steve Dunham Owner: Steve Dunham Predominant Soil Series:
8
Acres Permitted: 8 Site #:
SF03
M..Com-
ERM
MENNEWEENUffil
Non
Date
Total
•o
_phorus'MENEENEENEEN
wnnuai heavy lvletal riela Loadings (Calculated in lbs/acre):
Total
1 11
1213
4
5
161
L 7j
L8J9
10
11
12
DT/Ac./
c
App.
Event
2.53
Arsenic
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.016
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
5.953
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.953
Chromium
0.201
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.201
Lead
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molyb-
denum
0.074
0.000
0.000
0.000
D.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.074
Nickel
0.167
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0167
Selenium
0.027
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.027
Zinc
12.285
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000 1
12.285
Total
Phos-
68.644
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
68.644
horus
I certify, under penalty of iaw, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z�f 2/5/2019
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp.
Land Owner: Steve Dunham
Operator: Steve Dunham
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 20.26 Site #:
Predominant Soil Series: LaB
Crop 1 Name: Bermuda -Hay Crop 1 Max. PAN: 196 Crop 2 Name:
Acres Utilized:
SF03 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
9.7
° y
Volume applied
Volume
Residual Sources
Soil
Cond.
Precip.
a
��
o
Z a
Nitrate
PAN Applied
Name of CropType
yP
y o
(enter one) Solids/
%
Applied per
(NPDES #, WQ#,
Past 24
1
;o
m
TKN
9 n
and
ReceivingResidual
Liquid
Solids
Acre
Fert., Animal
D
(Dry,
Hrs.
=' o
o�
"
N'
°Q
g
Nitrite
]bslacre
( )
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc )
Wet
Moist)
inches
*
*
0
*
mg/kg
69400
mg/kg
12600
mg/kg
1 2.31
Crop 1
Crop 2
Crop 1
Crop 2
4/20
32500
2.99
0.507
Tarheel W WTP
Dry
<.5"
S
0.5
0.2
17.893
NA
Bermuda
4/21
130000
2.99
2.026
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
69400
12600
2.31
71.571
NA
Bermuda
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
.........
0.000
0.000
0.000
......
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this
form):
TOTALS:
Of
162500
::::::::::::::
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
89.464
0.000
Lime Applied
Annuallbs/acre
0.016
0.099
0.115
0.010
0.052
0.062
9
5.953
19.406
25.359
250
0.201
0.984
1.185
0.040
0.286
0.326
1000
0.002
0.011
0.013
0.074
0.581
0.655
0.167
1.932
2.099
250
0.027
0.129
0.156
12.285
86.717
99.002
500
68.644
Date
Ibs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
196
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Z� 4y ". *Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2019 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Smithfield Farmland Corp. Total Dry Tons Applied (Annual):
Permit #: WQ0014868 Cation Exchange Capacity (non 503 only):
Operator: Steve Dunham Owner: JW Burney Predominant Soil Series:
Acres Used: 7.5 Acres Permitted: 7.5 Site #: SF07 Field #:
17.83
7.2
LaB
14
Residual Analysis Data (Heavy Metals and Total Phosnhorus use mu/ku- %, Cnlidv nee Raw Per,•an* ffl.
Com-
••
posite
non
Date
Total
Phos-
__phorus;MEEEEEEEEEEE
tinnuai heavy ivietat r .eta .Loadings (Ualculated in lbs/acre):
Total
1 21
1 31
1 4 v
L5
6
L 71
81
L9
10
11
12
DT/Ac./
c
App.
Event
2.38
y
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
1 0.000
0.015
Cadmium
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Copper
5.586
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
5.586
Chromium
0.188
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.188
Lead
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.002
Molyb-
denum
0.070
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.070
Nickel
0.156
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.156
Selenium
0.026
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.026
Zinc
11.528
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.528
Total
Phos-
64.417
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
64.417
horus
tT.-
t cei-my, under penalty of law, inat this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
z; 2/5/2019
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Smithfield Farmland Corp.
Land Owner:
Operator:
JW Burney
Steve Dunham
WQ Permit #: WQ0014868 Field #:
Annual Dry Tons Applied: 17.83 Site #:
Predominant Soil Series: LaB
Crop 1 Name: Bermuda -Pasture Crop 1 Max. PAN: 147 Crop 2 Name:
14
Acres Utilized: 7.5
SF07 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
7.5
7.2
° Y
Q
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, W #,
Fert., Animal
etc)
Soil
Cond.
WetWaste,
Moist)
Precip.
Past 24
Hrs.
inches
Y
°
°�
o
?:
*
o'
w `�
*
0
TKN
mg/kg
69400
Z >
o
mg/kg
12600
Nitrate
and
Nitrite
mg/kg
2.31
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/23
71500
2.99
1.189
Tarheel WWTP
Dry
<.5"
S
0.5
0.2
41.988
NA
Bermuda
4/26
71500
2.99
1.189
Tarheel W WTP
Dry
<.5"
S
0.5
0.2
69400
12600
2.31
41.988
NA
Bermuda
0.000
1
0.000
1 0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM
FSF supp ( attach FORM FSF supp
to this form):
.........
..........
TOTALS:
0
l4300W.:::::.:.:::i
As
Cd
Cu
Cr
Pb
Mo
Ni
Se
Zn
P
83.977
0.000
Lime A lied
Annuallbs/acre
0.015
0.144
0.159
0.010
0.065
0.075
9
5.586
33.907
39.493
250
0.188
2.333
2.521
0.037
0.626
0.663
1000
IH
0.070
0.967
1.037
0.156
3.011
3.167
250
0.026
0.208
0.234
11.528
134.708
146.236
500
64.417 ::
:: ':: :::::::::::::...........
......................
............................
Date
lbs/ac
Prior Years Cumulative lbs/ac
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
147
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/5/2019 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Report Number: 18-095-0201
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 59540
Sample Id : Smithfield TarHeel North
Waypoint0
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project : Smithfield Tarheel
REPORT OFANALYSIS Date Sampled: 4/4/2018 08:30:00
Date Received: 04/05/2018 00:00
Date Reported: 04/16/2018
Total Solids "
3.51
35100
100.0
JM
04/05/2018 14:35
SM-254OG
Moisture `
96.48
100.0
JM
04/05/2018 14:35
SM-254OG
Total Kjeldahl Nitrogen
8.44
84400
50.0
R D
04/09/2018 08:30
SM4500-NH3C-TKN
Total Phosphorus
1.47
14700
100
SMC
04/10/2018 18:02
6010C
Total Potassium
0.36
3590
100
SMC
04/10/2018 18:02
6010C
Total Sulfur
1.72
17200
100
SMC
04/12/2018 15:22
6010C
Total Calcium
1.30
13000
100
SMC
04/10/2018 18:02
6010C
Total Magnesium
0.15
1520
100
SMC
04/10/2018 18:02
6010C
Total Sodium
0.91
9100
100
SMC
04/10/2018 18:02
6010C
Total Iron
10800
100
SMC
04/10/2018 18:02
6010C
Total Aluminum
6090
100
SMC
04/13/2018 15:44
6010C
Total Manganese
294
5.00
SMC
04/10/2018 18:02
6010C
Total Copper
1140
5.00
SMC
04/10/2018 18:02
6010C
Total Zinc
2410
50.0
SMC
04/13/2018 17:10
6010C
Ammonia Nitrogen
1.19
11900
50.0
R D
04/09/2018 08:30
SM-4500-NH3C
Organic N
7.25
72500
50.0
04/09/2018 08:30
CALCULATION
Nitrate+Nitrite-N
<2.27
2.27
MMT
04/10/201813:12
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Pam«
imp 610wri''
Our reports anti letters are for the exslosive
and confidential usa of our elierrts. and
may not be reproduced
in whofe or part, norrnay
any reference be made
to the wnrk, the results. of the corm .n, in
it y advertising. news release, or ;they
perolic announcements without obtaining out hr!trr watterr authorization
Pauric McGroary
Agronomist
Page 1 of 4

Report Number: 18-095-0201
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Lab Number: 59540
Sample Id : Smithfield TarHeel North
Waypoint(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Smithfield Tarheel
REPORT OF ANALYSIS Date Sampled: 4/4/2018 08:30:00
Date Received: 04/05/2018 00:00
Date Reported: 04/16/2018
Total Cadmium
<2.00
2.00
SMC
04/10/2018 18:02
6010C
Total Chromium
41.7
5.00
SMC
04/12/2018 15:22
6010C
Total Nickel
33.3
5.00
SMC
04/12/2018 15:22
6010C
Total Lead
8.02
5.00
SMC
04/10/2018 18:02
6010C
Total Arsenic
<3.00
3.00
SMC
04/10/2018 18:02
6010C
Total Mercury
<0.400
0.400
SMC
04/12/2018 12:51
SW-7471 B
Total Selenium
5.25
5.00
SMC
04/12/2018 15:22
6010C
pH *
7.9
1.0
JM
04/09/2018 08:30
9045D
Total Volatile Solids
83.33 833300
100.0
JM
04/05/2018 14:35
SM-2540G
Total Molybdenum
15.1
5.00
SMC
04/12/2018 15:22
6010C
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our - ports ar J iettcfs are for the exc-tuswe and confidentra; use or our clients. and may oot be reproduced in wneie or par, no, may any reforence bt� made Wr-
Ac 60Wr
to the wark ite re tufts, t., the cororany rn any advertisrna. -,tws rcl asn. Brother public a,nrounceaterds mahout obtauwq ourpdo. woii err a tth.a. zatior?,
Pauric McGroary
Agronomist
'age 2 of 4

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Smithfield Tarheel
Lab Report Number: 18-095-0201
Date: 4/16/2018
7621 Whitepine Road, Richmond, VA 23237
Main $04-743-9401 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Nitrate + Nitrite Nitrogen Method SM-450ONO3F
Sample 59540 (Smithfield TarHeel North)
Analyte: NO3+NO2-N
QC Batch No: E63250/E63198
The MS/MSD recoveries are considered insignificant due to the level of analyte present in the parent sample
relative to the spike level . RPD is based on the MS/MSD results and should be evaluated as laboratory
duplicates.
Page 3 of 4

BIOSOLIDS SAWLF - ' `T,`v„ A T rnn 1k ArIOLY A YXT ('I CUSTODY
t
7621 Whitepine Road R EW Resout s inc 2oszota ,[e-mail]
Smithfield Tarheel 12,4722
Submitted By Copy To
EMA Resources Inc
ENIA Resources Inc
755 Yadkinville Rd
755 Yadkinville Rd
Mocksville, NC 27028
Mocksville, NC 27028
1-7
Sample lnformaliorj
Lab Number
Colleeiion lntormation
Gorttairler Iriftirmatlori Please Chec
Simple lD
(Lab Use
Only).
Fype'.. Date7YPe
°; Volurt.. - SLi . >S ;503 Nib
of $ottles fiAehals . Si
�rab
Composite
y%�l�s
S 3a
_ G
— oz
qt
— Grab
Glass
— oz
Composite
_
Plastic
___pint
t
Grab
Glass—
oz
_—Composite
_
Plastic
--pint
t
_ Grab
Glass
— oz
Composite
_
plastic
--pint
i' d 0 gnatj—j—�Tine
Received t3 : (S' nature
6% tl , u 1
/9 ' 5-nj
Test Package Details
SLI : Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SLI plus Sulfur. Calcium, Magnesium,Sodium, Iron, Aluminum, Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in SL2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen,
CIE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
Account #
sired Tests:,
U pH OEr` Ag a. VAS Others'
Date ' Tine
IT
IT
a)
to
tri
0-

Page: 1 of 2
Report Number: 18-114-0207
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
Waypoi nt.M(2)
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Smithfield Tar Heel
REPORT OFANALYSIS Date Sampled: 4/23/2018 11:55:00
Lab Number: 60200 Date Received: 04/24/2018 00:00
Sample Id : Smithfield Tar Heel Date Reported: 05/04/2018
WWI Dumb
ZAt
24100
100.0
R D
04/24/2018 14:30
SM-254OG
Moisture '
97.52
100.0
R D
04/24/2018 14:30
SM-2540G
Total Kjeldahl Nitrogen
5.44
54400
50.0
JM
04/25/2018 09:00
SM-4500-NH3C-TKN
Total Phosphorus
1.24
12400
100
BKN
05/04/2018 00:00
6010C
Total Potassium
0.34
3410
100
SMC
04/26/2018 19:04
6010C
Total Sulfur
1.56
15600
100
SMC
04/26/2018 19:04
6010C
Total Calcium
1.23
12300
500
BKN
05/04/2018 00:05
6010C
Total Magnesium
0.14
1390
100
SMC
04/26/2018 19:04
6010C
Total Sodium
0.81
8100
100
SMC
04/26/2018 19:04
6010C
Total Iron
14200
100
SMC
04/26/2018 19:04
6010C
Total Aluminum
5640
100
SMC
04/26/2018 19:04
6010C
Total Manganese
288
5.00
BKN
05/04/2018 00:00
6010C
Total Copper
1210
25.0
BKN
05/04/2018 00:05
6010C
Total Zinc
2440
25.0
BKN
05/04/2018 00:05
6010C
Ammonia Nitrogen
1.33
13300
50.0
R D
04/25/2018 09:00
SM-4500-NH3C
Organic N
4.11
41100
50.0
04/25/2018 09:00
CALCULATION
Nitrate+ N itrite-N
<2.35
2.35
MMT
04/27/2018 09:28
4500NO3F-2011
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is
on a wet basis.
Our repots and letters ate for the exclusive and confide niia!
to the work, the resulfs or,l e eor,rpany In any 0vemsaig, news
use of our cNeots. and may
release. nr stne,; tuna,
nct be reproduced
arznouncc me
in whOie or part, nonnay any re,ereerce
Its wfthvut obtainiog out pnor written aL1fh0r1Zab09
be made
Pauric McGroary
Agronomist

Page: 2 of 2
Report Number: 18-114-0207
Account Number: 46245
Send To: EMA Resources Inc
755 Yadkinville Road
Mocksville , NC 27028
•
Waypoint
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Project: Smithfield Tar Heel
REPORT OFANALYS/S
Date Sampled: 4/23/2018 11:55:00
Lab Number: 60200
Date Received: 04/24/2018 00:00
Sample Id : Smithfield Tar Heel
Date Reported: 05/04/2018
PARAMETER
RESULT RESULT
QUANTITATION
ANALYSIS
.
•.
�,
Total Cadmium
<2.00
2.00
BKN
05/04/2018 00:00 6010C
Total Chromium
37.5
5.00
BKN
05/04/2018 00:00 6010C
Total Nickel
32.5
5.00
BKN
05/04/2018 00:00 6010C
Total Lead
7.61
5.00
BKN
05/04/2018 00:00 6010C
Total Arsenic
3.19
3.00
BKN
05/04/2018 00:00 6010C
Total Mercury
<0.400
0.400
SMC
04/25/2018 16:39 SW-7471 B
Total Selenium
5.51
5.00
BKN
05/04/2018 00:00 6010C
pH °'
7.8
1.0
R D
04/25/2018 09:00 9045D
Total Volatile Solids
83.87 838700
100.0
R D
04/24/2018 14:30 SM-2540G
Total Molybdenum
14.2
5.00
BKN
05/04/2018 00:00 6010C
Comments:
NC CERT#257
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES.
All values are on a dry weight basis except as noted by asterisk_ Detection limit on all N series is on a wet basis.
Ow the exc'us;✓e a; id confide: iz'al use of ow clients. and may t,ot he reprod iced is; whole orparY, nor may any rate eoce be made
to the wod,, 1h , OSUiZS, n� rt e a}mpany in any adverts g. news release. orother pubhc announcements without obtain -,g our prior writtea authoazat'ori,
Pauric McGroary
Agronomist

A18-114-0207LA A&L Easter ���� � � 6245
7621 Whitt pine Road Richmond VA 23237 Tel: [phone]
EMA Resources Inc 13:19:17
Smithfield Tar Heel
CustorrNer In%rmE
Stibmltted By ..
.� IV
Gop}r To'
EMA Resources Inc EMA Resources Inc
755 Yadkinvilie Rd 755 Yadkinville Rd
Moc(ksvilte, NC 27028 Mocksville, NC 27028
5 Kk V211.1r,-�,
010,
lrG>�lectart.lfamlalwrl Contatlt 1
47 f?tease CIJesad
'tlrise Tests
Y
>a
uAa;...
'r"... ;. ._.f?. .,. 'r .''n A: eTj>. ,+�... '�S'M.A+rv^ cS,y,r F,+. 45 'P9 .'.l,.a S. 3' 'a : L"•�• C �.x,
s
z:. A. r?..a,., w * TM;a.(jnl�}\:. ; w ;1c, r. ,,,,, •� •, „r;,',:.. s:;.., �:,'r. A�+'^,p'-�'v'r'(s'.�,+'' . '� ; u ,•5, u. 's' ',,?�c. s .ate` �> i„t t x y t
a''+
�r•,r�>
YV oR.t tT' .. ,. „w rrn7rgr� /
_ Grab t = c _ 1 / ✓ I/
oz
Composite I C.� t-,st; 1/
_ qt
Grab Glass — oz
O_Composite —Plastic __pint
t
— Grab Glass — oz
— Composite — plastic __pint
t
Grab _ Glass — oz
_—Composite Plastic ___pint
t
n u �' fiat ba,Trrie Received :.{S' naiure Date Time
Test Package Details SPecial Instructions or Remarks
SLt: Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potassium
SL2: Basic Test SL I plus Sulfur, Calcium, Magnesittm,Sodium, Iron, Aluminum, Manganese, Copper And Zinc
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium.
(Copper & Zinc included in St2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & Organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For lime Treated Sludge)

*ESC ANALYTICAL REPORT m CSC
April 13, 2018
a s�brJeranol,�q�yy' a:✓bNOury al
wur+r '
EMA Resources
Sample Delivery Group
Samples Received:
Project Number. -
Description:
L983488
04/0 5/2 018
Smithfield Tar Heel
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By:
Cassandra Foster
Technical Service Representative
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is
performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
T c: Table of Contents
Ss: Sample Summary
3
Cn: Case Narrative
4
Sample Results
5
FSSr:
SMITHFIELD TAR HEEL L983488-01
5
Qc: Quality Control Summary
7
Fnj
Wet Chemistry by Method 9012 B
7
FrWet
Chemistry by Method 9034-9030B
g
Wet Chemistry by Method 9045D
9
RC
Wet Chemistry by Method D93/1010A
10
�GI
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
Volatile Organic Compounds (GC/MS) by Method 8260B
13
Chlorinated Acid Herbicides (GC) by Method 8151A
15
a
Sc
Pesticides (GC) by Method 8081B
16
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
17
GI: Glossary of Terms
19
AI: Accreditations & Lea "tio ,,s
.<:•.�i
Sc: Sample Chain of Custody
21
ACCOUNT: PROJECT: SDG:
DATEMME: PAGE:
EMA Resources L983488
04113/1816:19 2 of 21

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
SMITHFIELD TAR HEEL L983488-01 Waste Roy Whitaker 04/04/1808:30 04/05/1808:45
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
Preparation by Method 1311
WG1095373
1 04/08/1813:45
04/08/1813:45
KK
Preparation by Method 1311
WG1095939
1 04/10/1811:15
04/101811:15
RT
Wet Chemistry by Method 9012 B
WG1095472
1 04/10/18 09:39
04/11/1810:53
KK
Wet Chemistry by Method 9034-90308
WG1096347
1 04/11/18 23:20
04/11/18 23:20
JLJ
Wet Chemistry by Method 9045D
WG1094518
1 04/06/18 09:45
04/06/1811:30
MLW
Wet Chemistry by Method D93/1010A
WG1095365
1 04/10/1810:10
04/101810:10
TH
Rn
Mercury by Method 7470A
WG1095542
1 04/09/1811:16
04/09/1817:05
EL
Metals (ICP) by Method 6010D
WG1095571
1 04/09/1811:20
04/09/1815:39
ST
FrVolatile
Organic Compounds (GC/MS) by Method 8260B
WG1096448
1 04/11/1816:18
04/11/1816:18
JBE
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1096408
1 04/11/18 08:36
04/12/1812:09
KLM
s
QC
Pesticides (GC) by Method 8081B
WG1096466
1 04/12/18 07:14
04/12/1817:33
TD
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
WG1095680
1 04/09/1818:12
04/10/18 08:01
AO
�GI
FC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L983488
04/13/18 16:19
3 of 21

CASE NARRATIVE ONE LAB NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All radiochemical sample results for
solids are reported on a dry weight basis with the exception of tritium, carbon-14 and radon, unless wet
weight was requested by the client. All Method and Batch Quality Control are within established FS
criteria except where addressed in this case narrative, a non-conformance form or properly qualified
within the sample results. By my digital signature below, I affirm to the best of my knowledge, all
problems/anomalies observed by the laboratory as having the potential to affect the quality of the data
have been identified by the laboratory, and no information or data have been knowingly withheld that
would affect the quality of the data.
El
F C
Cassandra Foster
Technical Service Representative
Project Narrative
FC
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034/9030B.
ACCOUNT: PROJECT: sDG: DATE/TIME: PAGE:
EMA Resources L983488 04113/1816:19 4 of 21

SMITHFIELD TAR HEEL SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected dateltime: 04/04/18 08:30 L983488
Preparation by Method 1311
Result
Qualifier
Prep
Batch
Analyte
date / time
TCLP Extraction
4/8/20181:45:21 PM
WG1095373
TCLP ZHE Extraction
4/10/201811:15:32 AM
WGIO95939
t--- _--
Fluid 1
4/8/20181:45:21 PM
WG1095373
Initial pH 7.54
4/8/20181:45:21 PM
WG1095373
I qs
Final pH 4.88
4/8/20181:45:21 PM
WG1095373
FC
Wet Chemistry by Method 9012 B
Result
Qualifier
RDL Dilution
Analysis Batch
Analyte mg/kg
mg/kg
date / time
Reactive Cyanide ND
0.250 1
04/11/201810:53
FIC
Wet Chemistry by Method 9034-9030B
Result
Qualifier
RDL Dilution
Analysis Batch
FGI
Analyte mg/kg
mg/kg
date / time
Reactive Sulfide 42.5
25.0 1
04/11/2018 23:20
Wet Chemistry by Method 9045D
9
Sc
Result
Qualifier
Dilution Analysis
Batch
Analyte su date / time
Corrosivity by pH 7.08 TB 1 04/06/201811:30
Sample Narrative:
L983488-01 WG1094518: 7.08 at 20.9C
Wet Chemistry by Method D93/1010A
Result Qualifier Dilution Analysis Batch
Analyte Deg. F date / time
Ignitability DNI at 170 1 04/10/201810:10
Mercury by Method 7470A
Result Qualifier RDL
Analyte mg/I mg/I
Mercury ND 0.0100
Metals (ICP) by Method 6010D
Limit Dilution Analysis Batch
mg/I date / time
0.20 1 04/09/201817:05
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte
mg/I
mg/I
mg/I
date / time
Arsenic
ND
0.100
5
1 04/09/201815:39
Barium
ND
0.100
100
1 04/09/201815:39
Cadmium
ND
0.100
1
1 04/09/201815:39
Chromium
ND
0.100
5
1 04/09/201815:39
Lead
ND
0.100
5
1 04/09/201815:39
Selenium
ND
0.100
1
1 04/09/201815:39
Silver
ND
0.100
5
1 04/09/201815:39
Volatile Organic Compounds (GC/MS) by Method 8260B
Result
Qualifier RDL
Limit
Dilution Analysis Batch
Analyte
mg/I
mg/I
mg/I
date / time
Benzene
ND
0.0500
0.50
1 04/11/201816:18
Carbon tetrachloride
ND
0.0500
0.50
1 04/11/201816:18
Chlorobenzene
ND
0.0500
100
1 04/11/201816:18
Chloroform
ND
0.250
6
1 04/11/201816:18
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04113/1816:19 5 of 21

SMITHFIELD TAR
HEEL
SAMPLE RESULTS
- 01
ONE LAB. NATIONWIDE.
Collected date/time: 04/04/18
08:30
L983488
Volatile Organic Compounds
(GC/MS) by Method 8260B
Result
Qualifier RDL Limit Dilution
Analysis
Batch
Analyte
mg/1
mg/1 mg/I
date / time
1,2-Dichloroethane
ND
0.0500 0.50 1
04/11/201816:18
�-
1,1-Dichloroethene
ND
0.0500 0.70 1
04/111201816:18
2-Butanone (MEK)
ND
0.500 200 1
04/11/201816:18
Tetra chloroethene
ND
0.0500 0.70 1
04111/201816:18
�
I qs
Trichloroethene
ND
0.0500 0.50 1
04/11/201816:18
Vinyl chloride
ND
0.0500 0.20 1
04/11/201816:18
(S) Toluene-d8
98.8
80.0-120 120
041111201816.18
FCn]
(S) Dibromofluoromethone
104
76.0-123 123
04111120181618
(S) o, a, o-Trifluorotoluene
97.5
80.0-120 120
041111201816.18
(S) 4-Bromofluorobenzene
94.2
80.0-120 120
041111201816:18
Chlorinated Acid Herbicides (GC) by Method 8151A Rc
Result
Analyte mg/I
2,4,5-TP (Silvex) ND
2,4-D ND
(S) 2,4-Dichlorophenyl Acetic Acid 75.6
Pesticides (GC) by Method 8081B
Qualifier RDL
mg/I
0.00200
0.00200
14.0-158
Limit
mg/I
1
10
158
Dilution Analysis
date / time
1 04/12/201812:09
1 04/12/201812:09
041121201812:09
Batch
�-
�GI
-
9Sc
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1 04/12/201817:33
Endrin
ND
0.00500
0.02
1 04/12/201817:33
Heptachlor
ND
0.00500
0,0080
1 04/12/201817:33
Lindane
ND
0.00500
0.40
1 04/12/201817:33
Methoxychlor
ND
0.00500
10
1 04/12/201817:33
+
Toxaphene
ND
0.0100
0,50
1 04/12/201817:33
(S) Decochlorobiphenyl
72.0
10.0-144
144
04112120181733
(S) Tetrachloro-m-aylene
53.1
10.0-135
135
041121201817.33
Semi Volatile Organic Compounds
(GC/MS) by Method 8270D
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/1
mg/I
date / time
1,4-Dichlorobenzene
ND
0.100
7.50
1 04/10/2018 08.01
2,4-Dinitrotoluene
ND
0.100
0.13
1 04/10/2018 08:01
Hexachlorobenzene
ND
0.100
0.13
1 04/10/2018 08:01
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 04/10/2018 08:01
Hexachloroethane
ND
0.100
3
1 04/10/2018 08:01
Nitrobenzene
ND
0.100
2
1 04/10/2018 08:01
Pyridine
ND
0,500
5
1 04/10/2018 08:01
3&4-Methyl Phenol
ND
0.100
400
1 04/10/2018 08:01
2-Methylphenol
ND
0.100
200
1 04/10/2018 08:01
Pentachlorophenol
ND
0.100
100
1 04/10/2018 08:01
2,4,5-Trichlorophenol
ND
0.100
400
1 04/10/2018 08:01
2,4,6-Trichlorophenol
ND
0.100
2
1 04/10/2018 08:01
(S) 2-Fluorophenol
45.9
10.0-120
120
0411012018 08:01
(S) Phenol-d5
26.1
10.0-120
120
0411012018 08:01
(S) Nitrobenzene-6
59.6
10.0-126
126
0411012018 08:01
(S) 2-Fluorobiphenyl
65.0
22.0-127
127
0411012018 08:01
(5) Z,4,6-Tribromophenol
55.7
10.0-153
153
0411012018 08:01
(S) p-Terphenyl-d14
65.0
29.0-141
141
0411012018 08:01
d
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/13/18 16:19 6 of 21

WG1095472 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Wet Chemistry by Method 9012 B 9S3+48 6-61
Method Blank (MB)
(MB) R3300807-1 04/11/18 10:37}
MB Result MB Qualifier MB MDL MB ROL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
FS
L983429-01 Original Sample (OS) - Duplicate (DUP)
(OS) L983429-01 04111J1810:50 - (DUP) R3300807-4 04/11/13 10:51
FCn]
DUP RPD
Original Result DUP Result Dilution DUP RPD DUP Qualifier _
Limits
5r
Analyte mg/kg mg/kg % %
Reactive Cyanide 0.311 0A73 1 41.4 P1 20
L983914-05 Original Sample (OS) • Duplicate (DUP)
FG
(OS) L983914-05 04/11/18 11:02 - (DUP) R3300807-7 04/11/18 11:03
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
3
Analyte mg/kg mg/kg % %
Reactive Cyanide ND 0.000 1 0.000 20 9
SC
Laboratory Control Sample (LCS) - Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300807-2 04/11/18 10:39 - (LCSD) R3300807-3 04/11/18 10:40
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg % % % % %
Reactive Cyanide 2.50 2.57 2.68 103 107 50.0-150 4.20 20
L983493-01 Original Sample (OS) - Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L983493-01 04/11/1810:54 - (MS) R3300807-5 04/11/1810:55 - (MSD) R3300807-6 04/11/1810:56
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg nrg/kg mg/kg mg/kg % % % % %
Reactive Cyanide 1.67 ND 0.776 0.928 46.6 55.7 1 75.0-125 J6 J6 17.7 20
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/13/1816:19 7 of 21

WG1096347 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE
Wet Chemistry by Method 9034-9030B 3 6 _-
Method Blank (MB)
(MB) R3301064-1 04/11/18 23:20
MB Result
Analyte mg/kg
Reactive Sulfide U
MB Qualifier MB MDL M8 RDL
mg/kg mg/kg
7.63 25.0
L984329-02 Original Sample (OS) • Duplicate (DUP)
(OS) L984329-02 04/11/18 23:20 - (DUP) R3301064-4 04/11/18 23:20
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Sulfide ND ND 1 0.000 20
Laboratory Control Sample (LCS) - Laboratory Control Sample Duplicate (LCSD)
(LCS) R3301064-2 04/11/18 23:20 - (LCSD) R3301064-3 04/11/18 23:20
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg % % % % %
Reactive Sulfide 100 72.9 72.9 72.9 72.9 70.0-130 0.000 20
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
8of21

WG1094518 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D �8;8S-J1
L983492-02 Original Sample (OS) • Duplicate (DUP)
(OS) L983492-02 04/06/1811:30 - (DUP) R3299676-4 04/06/1811:30
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte Su su % %
Corrosivity by pH 6.24 6.20 1 0.643 1
Sample Narrative:
OS: 6.24 at 20.9C
DUP: 6.2 at 21C
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3299676-1 04/06/1811:30 • (LCSD) R3299676-2 04/06/1811:30
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD
Analyte Su Su Su % % % %
Corrosivity by pH 10.0 9.98 9.98 99.8 99.8 99.0-101 0.000
Sample Narrative:
LCS: 9.98 at 19.6C
LCSD: 9.98 at 19.6C
RPD Limits
1
ONE LAB. NATIONWIDE. *
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
9 of 21

WG1095365 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE.
Wet Chemistry by Method D93/1010A 933458-�1
L983409-01 Original Sample (OS) • Duplicate (DUP)
(OS) L983409-01 04/10/1810:10 • (DUP) R3300424-3 04/10/1810:10
Original Result DUP Result Dilution DUP RPD
DUP Qualifier
DUP RPD
Limits
Analyte Deg. F Deg. F %
%
Ignitability DNI at 170 DNI at 170 1 0.000
10
FS]
L983488-01 Original Sample (OS) • Duplicate (DUP)
Fln
(OS) L983488-01 04/10/1810:10 • (DUP) R3300424-4 04/10/1810:10
Original Result DUP Result Dilution DUP RPD
DUP Qualifier
DUP RPD
Limits
s
S r
Analyte Deg. F Deg. F %
Ignitability DNI at 170 DNI at 170 1 0.000
%
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
�GI
(LCS) R3300424-1 04/10/1810:10 • (LCSD) R3300424-2 04/10/18 10:10
- --""---
Spike Amount LCS Result LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F %
%
% % %F
-
Ignitability 82.0 83.5 83.5 102
102
96.0-104 0.000 10
a
qc
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
10 of 21

WG1095542 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Mercury by Method 7470A 9e34S8-�:
Method Blank (MB)
(MB) R3300323-1 04/09/18 16:26
MB Result
Analyte mg/I
Mercury U
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00333 0.0100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300323-2 04/09/1816:28 • (LCSD) R3300323-3 04/09/1816:37
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/1 % % % % %
Mercury 0.0300 0.0307 0.0309 102 103 80.0-120 0.678 20
L982896-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L982896-04 04/09/18 16:40 • (MS) R3300323-4 04/09/18 16:42 • (MSD) R3300323-5 04/09/1816:44
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I mg/I % % % % %
Mercury 0.0300 ND 0.0318 0.0320 106 107 1 75.0-125 0.884 20
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
11 of 21

WG1095571 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. 40
Metals (ICP) by Method 6010D L983`4a3-1)1
Method Blank (MB)
(MB) R3300298-1 04/09/18 14:27
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Arsenic
u
0.0333
0.100
Barium
U
0.0333
0.100
Cadmium
U
0.0333
0100
Chromium
U
0.0333
0.100
Lead
U
0.0333
0.100
Selenium
0.0339
J 0.0333
0.100
Silver
U
0.0333
0.100
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300298-2 04/09/1814:30 - (LCSD) R3300298-3 04/09/18 14:33
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
Arsenic
10.0
9.86
9.77
98.6
97.7
80.0-120
Barium
10.0
10.3
10.2
103
102
80.0-120
Cadmium
10.0
9.81
9.69
98.1
96.9
80.0-120
Chromium
10.0
9.87
9.79
98.7
97.9
80.0-120
Lead
10.0
10.1
9.90
101
99.0
80.0-120
Selenium
10.0
9.85
9.77
98.5
97.7
80.0-120
Silver
2.00
1.84
1.83
92.2
91.5
80.0-120
LCS Qualifier LCSD Qualifier RPD
RPD Limits
0.914
20
1.01
20
1.18
20
0.768
20
1.49
20
0.829
20
0.729
20
L982896-04 Original Sample (OS) - Matrix Spike (MS) - Matrix Spike Duplicate (MSD)
(OS) L982896-04 04/09/18 14:37 - (MS) R3300298-5 04/09l18 14:44 - (MSD) R3300298-6 04/09/18 14:47
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
10.3
10.1
103
101 1
Barium
10.0
0.117
10.0
9.98
99.2
98.7 1
Cadmium
10.0
ND
10.0
9.95
99.4
98.8 1
Chromium
10.0
ND
9.77
9.72
97.7
97.2 1
Lead
10.0
ND
10.1
10.0
101
100 1
Selenium
10.0
ND
10.4
10.3
103
103 1
Silver
2.00
ND
1.89
1.88
94.5
94.1 1
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
75.0-125
1.29
20
75.0-125
0.547
20
75.0-125
0.618
20
75.0-125
0.465
20
75.0-125
0.823
20
75.0-125
0.412
20
75.0-125
0 416
20
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
12 of 21

WG1096448 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B L_
Method Blank (MB)
(MB) R3300881-3 04/11/1812:10
MB Result
Analyte
mg/I
Benzene
U
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
U
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
101
(S) Dibromofluoromethane
100
(S) a,a,a-rrifluorotoluene
99.8
(S) 4-Bromofluorobenzene
92.8
MB Qualifier
MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
0.0167
0.0167
0.0167
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
76.0-123
80.0-120
80.0-120
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300881-1 04/11/1810:54 • (LCSD) R3300881-2 04/11/1811:13
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Benzene
0.0250
0.0261
0.0259
104
104
69.0-123
0.575
20
Carbon tetrachloride
0.0250
0.0259
0.0251
104
100
63.0-122
3.04
20
Chlorobenzene
0.0250
0.0287
0.0275
115
110
79.0-121
4.19
20
Chloroform
0,0250
0.0256
0.0256
103
102
72.0-121
0.0114
20
1,2-Dichloroethane
0.0250
0.0255
0.0255
102
102
67.0-126
0.165
20
1,1-Dichloroethene
0.0250
0.0246
0.0245
98.3
97.8
64.0-129
0.509
20
2-Butanone (MEK)
0.125
0.119
0.122
95.5
9T8
37.0-158
2.39
20
Tetrachloroethene
0.0250
0.0302
0.0288
121
115
70.0-127
4.48
20
Trichloroethene
0.0250
0.0296
0.0290
118
116
78.0-120
2.09
20
Vinyl chloride
0.0250
0.0267
0.0265
107
106
64.0-133
0.981
20
(S) Toluene-d8
98.9
96.8
80.0-120
(S) Dibromofluoromethane
93.9
93.3
76.0-123
(S) a,a,a-Tnfluorotoluene
104
102
80.0-120
(S) 4-Bromofluorobenzene
84.6
85.7
80.0-120
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/13/1816:19 13 of 21

WG1096448 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260B �Sn3&58-0;
L983661-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L983661-01 04/11/18 18:12 • (MS) R3300881-4 04/11/1818:31 • (MSD) R3300881-5 04/11/18 18:51
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. limits
MS Qualifier MSD Qualifier
RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
nigh
%
%
%
%
%
Benzene
1.25
ND
0.716
0.874
57.3
69.9
1 34.0-147
19.9
20
Carbon tetrachloride
125
ND
0.698
0.795
55.8
63.6
1 41.0-138
13.0
20
El
Chlorobenzene
125
ND
0.887
1.02
71.0
81.9
1 52.0-141
14.3
20
Chloroform
1.25
ND
0.815
0.940
65.2
75.2
1 50.0-139
14.2
20
4
1,2-Dichloroethane
1.25
ND
0.895
1.00
71.6
80.3
1 47.0-141
11.4
20
Cn
1,1-Dichloroethene
1.25
ND
0.553
0.691
44.2
55.3
1 31.0-148
J3
22.3
20
2-Butanone (MEK)
6.25
ND
5.40
5.40
86.4
86.3
1 12.0-149
0.142
24
Fr
Tetrachloroethene
1.25
ND
0.723
0.857
57.8
68.5
1 38.0-147
16.9
20
Trichloroethene
1.25
ND
0.721
0.892
5T6
71.3
1 32.0-156
J3
21.2
20
Vinyl chloride
1.25
ND
0.534
0.669
42.7
53.5
1 24.0-153
J3
22.5
20
(S) Toluene -dB
99.8
99.6
80.0-120
(S) Dibromofluoromethane
98.7
99.1
76.0-123
G
(S) a,a,a-Triiluorotoluene
97.1
970
80.0-120
(S)4-Bromofluorobenzene
86.9
870
80.0-120
I qC
ACCOUNT: PROJECT: SDG:
EMA Resources L983488
DATE/TIME:
04/13/1816:19
PAGE:
14 of 21

WG1096408 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3301342-1 04/12/18 09:57
MB Result
Analyte mg/I
2,4-D U
2,4,5-TP (Silvex) U
(S)2,4-DichlorophenylAcetic 77.9
Acid
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
0.000667
0.00200
0.000667
0.00200
14.0-158
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3301342-2 04/12/18 10:10 • (LCSD) R3301342-3 04/12/1810:23
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
2,4-D
0.00500
0.00429
0.00444
85.8
88.8
56.0-120
2,4,5-TP (Silvex)
0.00500
0,00466
0.00412
93.2
82.4
55.0-120
(S) 2,4-Dichlorophenyl Acetic
91.1
104
14.0-158
Acid
LCS Qualifier LCSD Qualifier RPD RPD Limits
3.48 20
12.3 20
ACCOUNT:
EMA Resources
PROJECT:
SDG: DATE/TIME:
L983488 04/13/1816:19
PAGE:
15 of 21

WG1096466 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE.
Pesticides (GC) by Method 8081E a4.a-u1
Method Blank (MB)
(MB) R3301393-1 04/12/18 15:40
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Gamma BHC
U
0,00167
0.00500
Endrin
U
0.00167
0.00500
Heptachlor
U
0.00167
0.00500
Methoxychlor
U
0.00167
0.00500
Chlordane
U
0.00167
0.00500
Toxaphene
U
0.00333
0.0100
(S) Decachlorobiphenyl
72.3
10.0-144
(S) Tetrachloro-m-xylene
50.1
10.0-135
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3301393-2 04/12/1815:52 • (LCSD) R3301393-3 04/12/1816:05
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
Gamma BHC
0.00100
0.000850
0.000825
85.0
82.5
56.0-133
Endrin
0-00100
0.000976
0.000939
97.6
93.9
58.0-135
Heptachlor
0.00100
0.000555
0.000482
55.5
48.2
37.0-134
Methoxychlor
0.00100
0.00108
0.00103
108
103
44.0-160
(S) Decachlorobiphenyl
78.9
72.6
10.0-144
(S) Tetrachloro-m-xylene
48.2
34.8
10.0-135
LCS Qualifier
LCSD Qualifier RPD
2.93
3.82
14.0
4.36
RPD Limits
20
20
24
22
ACCOUNT: PROJECT:
EMA Resources
SDG:
L983488
DATE/TIME:
04/13/1816:19
PAGE:
16 of 21

WG1095680 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270D s334a 6!
Method Blank (MB)
(MB) R3300441-3 04110/18 00:55
MB Result
Analyte mg/I
1,4-Dichlorobenzene
U
2,4-Dinitrotoluene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachloroethane
U
Nitrobenzene
U
Pyridine
U
2-Methylphenol
U
3&4-Methyl Phenol
U
Pentachlorophenol
U
2,4,5-Trichlorophenol
U
2,4,6-Trichlorophenol
U
(S) Nitrobenzene-d5
56.8
(S) 2-Fluorobiphenyl
618
(S) p-Terphenyl-d14
65.0
(S)Phenol-d5
275
(S) 2-Fluorophenol
47.5
(S) 2,4,6-Tribromophenol
62.1
MB Qualifier
MB MDL
mg/I
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
0.0333
MB RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
0.100
10.0-126
22.0-127
29.0-141
10.0-120
10.0-120
10.0-153
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300441-1 04/09/18 23:44 • (LCSD) R3300441-2 04/10/18 00:08
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0,0500
ND
ND
63.0
60.6
26.0-120
2,4-Dinitrotoluene
0.0500
0.0456
0.0406
91.3
81.3
47.0-127
Hexachlorobenzene
0.0500
0.0387
ND
77.4
66.4
41.0-124
Hexachloro-1,3-butadiene
0.0500
ND
ND
66.0
61.3
26.0-120
Hexachloroethane
0.0500
ND
ND
60.9
64.6
22.0-120
Nitrobenzene
0.0500
ND
ND
63.5
58.2
31.0-120
Pyridine
0.0500
ND
ND
31.2
31.4
10.0-120
2-Methylphenol
0.0500
ND
ND
59.5
55.0
26.0-120
3&4-Methyl Phenol
0.0500
ND
ND
56.9
58.7
27.0-120
Pentachlorophenol
0.0500
0.0383
0.0372
76.5
74A
20.0-126
2,4,5-Trich lorophenol
0.0500
0.0415
0.0376
83.0
75.2
44.0-124
2,4,6-Trichlorophenol
0.0500
0.0409
0.0388
81.9
77.5
40.0-122
(S) Nitrobenzene-d5
72.7
57.3
10.0-126
(S) 2-Fluorobiphenyl
83.9
74.5
22.0-127
(S)p-Terphenyl-d14
77.5
70.7
29.0-141
LCS Qualifier LCSD Qualifier RPD
RPD Limits
3.87
30
11.6
21
15.4
21
7.43
31
5.86
34
8.79
28
0.596
39
7.94
27
3.10
28
2.78
32
9.87
24
5.47
24
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/1311816:19 17 of 21

WG1095680 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. a
Semi Volatile Organic Compounds (GC/MS) by Method 8270D
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3300441-1 04/O9/18 23:44 • (LCSD) R3300441-2 04/10/18 00:08
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec,
Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/I mg/I mg/I
%
%
% % %
(S) Phenol-6
31.7
25.6
10.0-120
(S) 2-Fluorophenol
53.3
417
10.0-120
(S)2,4,6-Tribromophenol
76.2
69.0
10.0-153
L981398-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L981398-01 04/10/18 04:28 • (MS) R3300441-4 04/10/18 04:52 • (MSD) R3300441-5 04/10/18 05:16
Spike Amount
Original Result
MS Result
MSD Result
MS Rec,
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.332
0.308
66.3
61.6
1 12.0-125
2,4-Dinitrotoluene
0.500
ND
0.409
0.394
81.9
78.7
1 30.0-156
Hexachlorobenzene
0.500
ND
0.357
0.342
71.5
68.5
1 29.0-144
Hexachloro-1,3-butadiene
0.500
ND
0.357
0.329
71.5
65.8
1 18.0-122
Hexachloroethane
0.500
ND
0.337
0.316
67.4
63.2
1 12.0-120
Nitrobenzene
0.500
ND
0.319
0.306
63.8
61.3
1 14.0-134
Pyridine
0.500
ND
0.153
0155
30.6
31.1
1 10.0-120
2-Methylphenol
0.500
ND
0.271
0.267
54.2
53.4
1 14.0-120
3&4-Methyl Phenol
0.500
ND
0.277
0.269
55.4
53.8
1 13.0-124
Pentachlorophenol
0.500
ND
0.385
0.374
77.0
74.8
1 10.0-160
2,4,5-Trichlorophenol
0.500
ND
0.404
0.376
80.9
75.2
1 15.0-160
2,4,6-Trichlorophenol
0.500
ND
0.421
0.372
84.2
74.5
1 10.0-153
(S)Nitrobenzene-d5
67.8
61.2
10.0-126
(S) 2-Fluorobiphenyl
72.8
72.7
22.0-127
(S) p-Terphenyl-d14
66.4
56.5
29.0-141
(S) Phenol-6
273
24.7
10.0-120
(S) 2-Fluorophenol
47.2
38.9
10.0-120
(S)2,4,6-Tribromophenol
66.5
62.3
10.0-153
MS Qualifier MSD Qualifier RPD
RPD Limits
7.34
23
3.94
29
4.27
33
8.33
35
6.35
36
4.13
32
1.61
40
1.47
29
2.91
26
2.96
40
7.22
27
12.2
29
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/13/1816:19 18 of 21

GLOSSARY OF TERMS ONE LAB. NATIONWIDE. 4*
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
MDL
ND
Method Detection Limit.
Not detected at the Reporting Limit (or MDL where applicable).
FIS
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
Fn
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
s
Sr
S
OYt
Matrix Spike/Duplicate; used to evaluate analytical efficiency b measuring recovery. Surrogates are not expected to be
Y Y 9 ry 9 P
detected in all environmental media.
u
Not detected at the Reporting Limit (or MDL where applicable).
e
QC
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Analyte
reported.
If the sample matrix contains an interfering material, or if concentrations of analytes in the sample are higher than the
Dilution
highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value
different than 1 is used in this field, the result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
Original Sample
sample. The Original Sample may not be included within the reported SDG.
SC a
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Control
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
P1
RPD value not applicable for sample concentrations less than 5 times the reporting limit.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L983488 04/13/18 16:19 19 of
21

ACCREDITATIONS & LOCATIONS ONE LAB, NATIONWIDE.
ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab
is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences.
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZ0612
New Hampshire
2975
Arkansas
88.0469
New Jersey—NELAP
TNO02
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky"
90010
South Carolina
84004
Kentucky '
16
South Dakota
n/a
Louisiana
A130792
Tennessee' "
2006
Louisiana'
LA180010
Texas
T 104704245-17-14
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A2LA
A2LA— ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100799
A2LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461,01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water Z Underground Storage Tanks
'Aquatic Toxicity
° ChemicaVMicrobiological 5 Mold 5 Wastewater n/a Accreditation not applicable
ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please
contact our main office. ESC Lab Sciences performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L983488 04/13/18 16:19 20 of 21

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp. WQ Permit Number: WQ0014868
WWTP Name: Tarheel WWTP NPDES Number: NCO078344
Monitoring Period: From 4/6/2018 To 4/6/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (titne/tern) ❑I
Alt B (Alk Treatment)❑
I Alt. C (Prior Testing)❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAII. (1) Fecal Density 211
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) Indicate "Process to Si niScantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
jAcrobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludgexcee-
g
Pathogen Density
um r ol
dendences
Frequency
of Analysis
Sample
Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maxaximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
2041
14467
89474
MPN/G
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry
%+eight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ®
Alt. 2 (40-day bench)
JAIt. 3 (30-day bench) ❑
Alt. 4 (Spec. Oz uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑ JAIt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
JNo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC
PreparfName and Title type or print)
Signature of Preparer* Date
Brent Collins; Director of Technical Services
Land Applier Name and TT�e(�
itle(if applicable)(type or print)
�l 4;2- 2/5/2019
Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM PVRF 02T (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Smithfield Fresh Meats Corp.
WWTP Name: Tarheel WWTP
Monitoring Period: From 4/23/2018 To
WQ Permit Number: WQ0U14868
NPDES Number: NCO078344
4/23/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment)❑
I Alt. C (Prior Testing)[]
A1t.D (No Prior Test)
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilie ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alt. (1) Fecal Density ®
Alt. (2) Process to Significantly Reduce Patho ens ❑
If applicable to alternative pe -formed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAeroble Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number of
Excee-
d n e
Frequency
of Analysis
y
Sample
Type
Analytical
Tech-ni ue
q
inimu
Geo. Mean
aximu
Units
Fecal Colifortn
2 x 10 to the
6th power
per gram of
total solids
MPN
7958
8515
9311
MPN/g
0
Quarterly
G
SM92210E-
2006
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ®
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
JAlt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
L7 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Dwayne Russ - ORC
Preparer Name and Title (type or print)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
9J7 2/5/2019
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 04/06/2018
Reported: 04/09/2018
For: Smithfield Tar Heel
Comments: Geometric Mean 14,467 MPN/g
Sample Number
Parameter
Sample ID
Result
Unit
Method
Analyzed
Analyst
180406-02-01
Fecal Coliforms
1
69519
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-01
Percent Solids
1
1.87
%
SM254OB-1997
04/06/2018
WC
180406-02-02
Fecal Coliforms
2
2286
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-02
Percent Solids
2
1.75
aka
SM254OB-1997
04/06/2018
WC
180406-02-03
Fecal Coliforms
3
2041
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-03
Percent Solids
3
1.96
%
SM254OB-1997
04/06/2018
WC
180406-02-04
Fecal Coliforms
4
11404
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-04
Percent Solids
4
1.14
%
SM254OB-1997
04/06/2018
WC
180406-02-05
Fecal Coliforms
5
89474
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-05
Percent Solids
5
1.90
%
SM254OB-1997
04/06/2018
WC
180406-02-06
Fecal Coliforms
6
15873
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-06
Percent Solids
6
1.89
%
SM2540B-1997
04/06/2018
WC
180406-02-07
Fecal Coliforms
7
25252
MPN/g
SM92210E-2006
04/06/2018
WC
180406-02-07
Percent Solids
7
1.98
%
SM254OB-1997
04/06/2018
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 180406-02-01 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-02 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-03 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-04 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-05 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-06 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 180406-02-07 Temp on Arrival: 3.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Client: /
L! -Sklcegc , S .•�Wc
STATESv[LLEAHALYUCAL
122 Cowl Street • P.O. Box 228
Statesville. NC 28687
Address: (
S' //�, i(r�i �G L r`�-fY/�
s
DfeS /ZL GG' C 17 6 Z g
[phone]
I
contact Person: PI1On° 3 A -73% - / Sf r/ _'ye - 5 % -/ Y el
Chain of
Custody Record
PO * J;u z Requisitioned by: (� tee) I
Customer
IDa
_mom
�eb�os
TimeSampled
(Grp OtNy)
Dare Sampled
(Grab Only)
a
Matrlx
vara�a«smaeisbdroraalycis
ar
ww
a;,? M
=cr+L.
SPI
1: 05 PrLl
F 3
0
• o M
" F If
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6 : o Pft,�.
7, POA
Relinquished by: Time 9: o0 4opm Date . y I &W /l8' Sampled by: a Et�A�E;Z
Received by: Time 9:v0 Date � l!� IL
_-- ---_----- Transported by:
Relinquished by:__ Time /,z.v5 ( Date -ALJ 4 ljX Holding times met:
Received by:W `��� • Time 2� �j am, J&late y /� 1 O i
Compliance work:
Composite Sampling #1:
Time begin am, pm Date _/ ! Non-compliance work:
Time end am, pm Date _/� Lab Corrxnertts: SamplasTramported On Ice:
Composite SaWlIng #21
Time begin am, pm Date _!_I
Time end _ am, pm Date
kdtials:

Analytical Results
EMA Resources, Inc.
755 Yadkinville Rd.
Mocksville, NC 27028
Receive Date: 04/23/2018
Reported: 04/25/2018
For: Smithfield Tarheel
Comments: Geometric Mean 8,515 MPN/g
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
180423-08-01
Fecal Coliforms
1
8014
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-01
Percent Solids
1
2.87
%
SM254OB-1997
04/24/10:00
WC
180423-08-02
Fecal Coliforms
2
9275
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-02
Percent Solids
2
2.48
%
SM254OB-1997
04/24/10:00
WC
180423-08-03
Fecal Coliforms
3
8303
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-03
Percent Solids
3
2.77
%
SM25408-1997
04/24/10:00
WC
180423-08-04
Fecal Coliforms
4
7958
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-04
Percent Solids
4
2.89
%
sM25408-1997
04/24/10:00
WC
180423-08-05
Fecal Coliforms
5
8333
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-05
Percent Solids
5
2.76
%
SM254OB-1997
04/24/10:00
WC
180423-08-06
Fecal Coliforms
6
8519
MPN/g
SM92210E-2006
04/24/2018
WC
180423-08-06
Percent Solids
6
2.70
%
SM25408-1997
04/24/10:00
WC
180423-08-07
Fecal Coliforms
7
9311
MPN/g
SM92210E-2oo6
04/24/2018
WC
180423-08-07
Percent Solids
7
2.47
%
SM2540B-1997
04/24/10:00
WC
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 - Statesville, NC 28687 - 704/872/4697
Page 1 of 2

Client: z'--mw
e oalwES C
SPATF-WWEANALYTICAL
122 CourtStreci • PO. Box 228
Statesville, NC 29697
[phone]
Chain of
Custody Record
Address: �j
Ss �� /C2�i✓N�C C C /?0�4�
-
a V-f e-L G
Contact Person: a
Phone # FAXN
33 -7sl _1S(14/
PO #s sc--_ .� l
Regt>isitioned by: (Time Date)
cuato"Wr
IDY
Lac rD r
The sampled
(Oretr Only)
Dale sampled
((grab ON/y)
Malriz
w vnr
P®ammeferx equested for analysis
�y
C-A L. s
M
-
_ o
KA
n
s�-
o
Relinquished by:
Time a►l}�p� Date
V Sampled by: o
Received by:
Time am,(gDate Y"r? 4 Transported by: 8
Relinquished by:
------�
Time am, pm Date _!—l� Holding times met:
Received by:
Time am, pm Date _l_ /_
Compliance work:
Composite Samping
#1:
Time begin am, pm Date l_h
Non-compliance work:
Time end am, pm Date ��/�
Lab Comments: Samples Transported On Ice:
composite Semolina
#z --
Time begin—,__ _ am, pm Date _/_!_
Time end am, pm Date _!_/_
Initials:
KI

Land App ANL Volatile Solids In

Volatile Solids Out
Volatile Solids IN average
% Reduction
4/4/18 North
83.33
94.21
69.28
4/23/18 North
83.87
94.21
68.04

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY18-SL036704
Predictive Client: EMA Resources, Inc. Advisor:
f
755 Yadkinville Rd
Mehlich-3 Extraction Mocksville, NC 27028
Soil Re o
Sampled County: Bladen
Links to Helpful Information Sampled: Not Provided
Received: 06/06/2018
Farm: SF03-WILLIAM DUNHAM Completed: 06/12/2018 Client ID: 405413 Advisor ID:
Agronomist's Comments:
ATTENTION: This report was flagged with a "C" and/or "Z" to alert you that copper and/or zinc have accumulated in the soil and are approaching a level that could be detrimental to crop
production. The C and Z symbols are printed on your report for soil test Zn and Cu index levels of 2000 or more for agronomic crops; for peanuts with zinc, the level is 250. This note is
designed to be a "trigger" that allows enough time to either reduce the rate of application or find another field for application of biosolids and/or waste water. The CTL (critical toxic level) for
Cu and Zn is set at a 3000 index; for peanuts with zinc, the level is 500. Maintaining a pH of 6.0 or higher may reduce potential for toxicity, especially for Zn. These levels are used by
DENR as a benchmark to determine when application of waste products should be stopped. The CTL for copper and zinc was set to prevent levels from accumulating to the point where
they become toxic to crops rown on a field.
Sample ID: 00001
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0 120 0 0 pH$ Z 0 0
Note 12 Note
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cnT3; NO3-N in mg/ddl: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-Al Cu-I Na ESP SS-1 NO3-N
0.36 1.31 8.5 89 1.0 6.6 538 45 78 8 41 76 54 2320 2320 475 0.3 4
Sample ID: 00002
Recommendations: Lime Nutrients (lb/acre)
More
Crop (tons/acre) N P2O6 K2O Mg S Mn Zn Cu B
Information
Lime History:
1 -Bermuda hay/past., M 0.0 180-220 0 150 0 0 pH$ 0 0 0
Note: 12 Note.
2-
Test Results [units - WN in gled; CEC and Na in meq/100 cm3; NO3-N in mg/dd]: Soil Class: Mineral
HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N
0.92 1.35 8.6 94 0.5 7.0 499 36 78 15 38 53 33 1337 1337 462 0.3 3
North Carolina
A- ;
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDABCS Agronomic Division Phone: [phone]
Website: www.neagr.gov/agronomi/
Report No. FY18-SL036704
Page 2 of 3
Sample ID: 00003
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Bermuda hay/past., M
0.4
180-220 0
190
0
0
0
0
0 0
Note: 12
2-
Test Results [units - WN in
9/carp; CEC and Na in meg1100 cnP; NO3-N
in mgldnf]:
Soil Class:
Mineral
HM%a W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.36 1.40 5.7
81 1.1 5.6
566 21
65 14
30
72
60
1835
1835
588 0.3 5
Sample ID: 00005
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1 -Bermuda hay/past., M
0.0
180-220 0
110
0
0
pH$
0
0 0
Note. 12 Nate:
2-
Test Results [units - W/V in
g/cO; CEC and Na in meq/100 cm3; NO3-N
in mg/dnr3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH
P-1 K-1
Ca% Mg%
S-1
Mn-1
Mn-All
Mn.Al2
Zn-I
Zn-AI
Cu-1 Na ESP
SS-1 NO3-N
1.02 1.25 9.7
87 1.2 6.6
349 53
69 16
58
41
33
1507
1507
513 0.5 5

NCDABCS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY18-SL036705
Predictive
`O
Client:
EMA Resources, Inc.
755 Yadkinville Rd
Advisor:
Soil Report
Mehlich-3 Extraction
Mocksville, NC 27028
J� ��
Sampled County: Bladen
,. Links to Helpful Information
Sampled: Not Provided
Received: 06/06/2018
Farm: SF07-JW BURNEY
Completed: 06/11/2018
Client ID: 405413
Advisor ID:
Sample ID: 00012
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M
0.0 180-220 0
60 0
0
0
0
0
0
Note 12
2-
Test Results [units - WN in g/cm; CEC and Na in meq/100 cnr3; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-1 Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na
ESP SS-1 NO3-N
0.56 1.19 9.3 81 1.8 6.2
499 74 63 13
68 123 88
1827
1827
1353 0.2
2
Sample ID: 00013
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tons/acre) N P2O6
K2O Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1- Bermuda hay/past., M
0.0 180-220 0
210 0
0
0
0
0
0
Note 12
2-
Test Results [units - WN in g/cd; CEC and Na in meq/100 crrP; NO3-N in mg/ddl:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-1 Na
ESP SS-1 NO3-N
0.36 1.35 6.5 76 1.6 6.0
414 13 63 13
36 66 57
1630
1630
1004 0.2
3
Sample ID: 00014
Recommendations:
Lime
Nutrients (lb/acre)
More
Crop
(tonslacre) N P2O6
K2O Mg
S
Mn
Zn
Cu
B
Information
Lime History:
1-Bermuda hay/past., M
0.0 180-220 0
220 0
0
0
0
0
0
Note, 12
2-
Test Results [units - WN in g/crrr3; CEC and Na in meq/100 c0; NO3-N in mglddl:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH
P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All
Mn-Al2
Zn-1
Zn-AI
Cu-I Na
ESP SS-1 NO3-N
0.51 1.32 7.2 79 1.5 6.1
315 10 67 12
33 48 45
1257
1257
363 0.2
3
North Carolina
Tobacco Trust Fund Commission
Reprogramming of the laboratory -information -management system that makes this report possible is
being funded through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture