WQ0002883_2018 Residual Annual Report_20190314

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0002883
SUBMITTAL DATED: 3/5/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Drew Matthews
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0002883
Permittee * City of Elizabeth City
Phone Number*
2528839301
Facility Name * Elizabeth City WTP & Elizabeth City WWTP
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
2018 Elizabeth City Annual Report.pdf 12.05MB
1pload only 1 RDF docurrent. IVLltiple documents must be corrbined into one RDF file.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 3/5/2019

CITY OF ELIZABETH
CITY
2018 ANNUAL LAND APPLICATION OF
RESIDUAL BIO -SOLIDS REPORT
CLASS B PROGRAM
WQ0002883
Submitted by:
Soil Plus
PO Box 1396
Oxford, NC 27565
March 5, 2019
SOIL PLUS

SOIL PLUS
March 5, 2019
NCDEQ-DWR
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: 2018 LAND APPLICATION ANNUAL REPORT
Elizabeth City "Class B" Program
NC Permit No.: WQ0002883
Soil Plus Project No. 200704.A10
Information Processing Unit:
Soil Plus, LLC (Soil Plus) is submitting all monitoring and reporting requirements as
specified in the above referenced permit for the City of Elizabeth City on behalf of Atlantic
OBX. Soil Plus compiled this report using data gathered during the compliance year. This
data includes (1) certification form, (2) residual sampling, (3) field loading calculations, (4)
pathogen and vector attraction reduction documentation.
No biosolids from Elizabeth City's WWTP were land applied under this Class B permit,
however 4,614,000 gallons or 936.12 dry tons were land applied to permitted fields in
Currituck and Perquimans counties under Atlantic OBX's Class B permit (WQ0000974).
No residuals from Elizabeth City's WTP were land applied as a Class B product, however a
total of 2,704,000 gallons or 1,297.13 dry tons of Water Treatment Plant residuals were
land applied under Granville Farms' Class A Permit (WQ0033587) in Currituck County for
Agricultural uses. No Water Treatment Plant residuals were taken to the City of Elizabeth
City's Surface Disposal Unit (WQ0014808).
If there is any further information required or questions regarding this annual report please
do not hesitate to contact me or the Elizabeth City (252-337-6628) for further assistance.
Respectfully,
Drew Matthews, Soil Plus
Amanda Boone, City of Elizabeth City
PO Box 1396
Oxford, NC 27565
[phone]
dmatthews @s oilplus. net
www.soilplus.net

City of Elizabeth
City 2018 Annual
Land Application of
Residual Bio -Solids
Report
WQ0002883
Elizabeth City, NC
ANNUAL
CERTIFICATION FORM
RESIDUAL SAMPLING
SUMMARY FORM
Elizabeth City WTP
RESIDUAL SAMPLING
SUMMARY FORM
Elizabeth City WWTP
PATHOGEN & VECTOR
REDUCTION FORMS
Elizabeth City WWTP

City of Elizabeth City
2018 Class B Annual Report
WQ Permit# WQ0002883
Annual Certification Form

PermitNumber
WQ0002883
-ar: 2018
ANNUAL LAND APPLICATION CERTIFICATION FORM
FacilityName Land Application Operator County Phone Number
City of Elizabeth City Atlantic OBX Pasquotank [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year? If No, skip Part A, and Part yes No
B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the
residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit: 48
Total number of fields utilized for land application during the year: 0
Part B - Annual Compliance Statement:
Facility was compliant during calendar year with all conditions of the land application permit? Yes No
Including but not limited to items 1-13 below) issued by the Division of Water Quality RJ El
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites
2. Soil pH was adjusted as specified in the permit and lime was applied (f needed) to achieve a soil pH of at least 6
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory
results are attached
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of
--rtified laboratory results are attached
he facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T
7. All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated
facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with (applicable to 40 CFR Part 503 regulated
facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was
received from the Division of Water Quality
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to
include appropriate actions and remediation.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations."
Amanda Boone, Public Utilities Director
Permittee Name and Title (type or rint):
Signature of Preparer*
(if different from Permittee)
Date
�reparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T.1102 (26)
Tuesday, February 26, 2019
,I 05MAR19
Signature of Permittee
3-5-19
Signature of Land Applier Date
(if different from Permittee)

City of Elizabeth City
2018 Class B Annual Report
WQ Permit# WQ0002883
Residual Sampling Summary Form
Elizabeth City WTP
Field Loading Calculations
2018 Analytical
2018 TCLP

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 1/23/2018
% Solids 14.49
Mineralization Rate 0
Gallons per DT 1,654.99
PH 10.45
Sodium Absorpotion 0.11 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 284 lbs./1,000 gal 0.34
Ammonia Nitrogen (mg/Kg) 3.95 lbs./1,000 gal 0.00
Nitrate -Nitrite (mg/Kg) 5.92 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 8 lbs./1,000 gal 0.01
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 10 lbs./1,000 gal 0.01
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.30
Phosphorus lbs./1,000 gal 0.61
Calcium lbs./1,000 gal 383.70
Magnesium lbs./1,000 gal 17.80
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
2.50
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.50
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
5.00
Copper lbs./1,000 gal
0.01
Lead (mg/Ig)
2.50
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.30
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
5.00
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
5.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
276
0 0.00
Total 8 0.02
Total 10 0.02
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
284
8 0.02
276
284
10 0.02
274
276
0 0.00
276
274
0 0.00
274
276
0 0.00
276
274
0 0.00
274
276
0 0.00
276
274
0 0.00
274
276
0 0.00
276
274
0 0.00
274
Total 8 0.02
Total 10 0.02
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

Environment 1,11
P.O. BOX 7085, 114 OAMMONT DRIVE
GREENVILLE, N.C. 27835-7085
ELIZABETH CITY (WATER PLANT)
EMAIL RESULTS AND COC ONLY111
lS@d
Water Plant Analysis Method
PARAMETERS Sludge Date Analyst Code
Aluminum, (dry wt. basis), mg/kg
14434
02/09/18
LFJ
EPA200.7
Arsenic (dry wt. basis), mg/kg
<2.5
02/14/18
MTM
311313-04
Calcium (dry wt, basis), mg/kg
317507
02/09/18
LFJ
EPA200.7
Cadmium (dry wt. basis), mg/kg
<0.5
02/13/18
MTM
3113E-04
Copper (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA200.7
Chromium, T.(dry wt. basis),mg/kg
<2.5
02/09/18
LFJ
EPA200A
Lead (dry weight basis), mg/kg
<2.5
02/12/18
MTM
3113B-04
Magnesium (dry wt. basis), mg/kg
14726
02/09/18
LFJ
EPA200.7
Mercury (dry wt. basis), mg/kg
0.30
02/12/18
LFJ
EPA7471B
Nickel (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA20097
Potassium (dry wt. basis), mg/kg
<250
02/09/18
LFJ
EPA200.7
Selenium (dry wt, basis), mg/kg
<5.0
02/14/18
MTM
3113B-04
Sodium (dry wt. basis), mg/kg
625
02/09/18
LFJ
EPA200v7
Zinc (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA200.7
Total Solids, %
14.49
01/25/18
MAR
2540G11
TKN (dry wt.), mg/kg
c 283.8
02/12/18
CML
351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg
c 3.945
02/19/18
CLO
350.1 R243
Phosphorus, T. (dry wt.), mg/kg
c 508.7
02/16/18
CML
365.4-74
Chloride (dry wt. basis), mg/kg
c 7800
02/12/18
SEJ
4500CLB41
Nitrate -Nitrite (dry wt.), mg/kg
c 5.92
02/13/18
MF
353.2 R2-93
Sulfate (dry weight), mg/kg
c 1510
02/09/18
SEJ
4500802EII
Molybdenum (dry wt. basis), mg/kg
<5.0
02/09/18
LFJ
EPA200.7
waeteaaaer rD:
PHONE [phone]
FAX [phone]
DATE COLLECTED: 01/23/18
DATE REPORTED : 02/20/18
REVIEWED BY:
n llnaerti Eied data, DWa does not oPEer non -aqueous aertlEio at ion For Ghia analyt Joel pros adore.

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 3/21/2018
% Solids 20.5
Mineralization Rate 0
Gallons per DT 1,169.80
PH 10.58
Sodium Absorpotion 0.44 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 244 lbs./1,000 gal 0.42
Ammonia Nitrogen (mg/Kg) 39.40 lbs./1,000 gal 0.07
Nitrate -Nitrite (mg/Kg) 9.60 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 29 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 49 lbs./1,000 gal 0.08
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.86
Phosphorus lbs./1,000 gal 0.41
Calcium lbs./1,000 gal 653.11
Magnesium lbs./1,000 gal 24.96
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
4.50
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
0.45
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
2.30
Copper lbs./1,000 gal
0.00
Lead (mg/Ig)
2.30
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
2.30
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
4.50
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
4.50
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
215
0 0.00
Total 29 0.06
Total 49 0.10
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
244
29 0.06
215
244
49 0.10
195
215
0 0.00
215
195
0 0.00
195
215
0 0.00
215
195
0 0.00
195
215
0 0.00
215
195
0 0.00
195
215
0 0.00
215
195
0 0.00
195
Total 29 0.06
Total 49 0.10
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bi -Monthly Residuals
Pace Project No.: 92378031
Sample: Water Plant Sludge 1-6
Lab ID: 92378031001 Collected: 03/21/18 08:08
Received: 03/21/18 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method:
EPA 6010
Preparation Method: EPA 3050
Aluminum
14400
mg/kg
45.2
1
03/25/1810:10
03/28/1818:04
7429-90-5
Arsenic
ND
mg/kg
4.5
1
03/25/1810:10
03/28/1818:04
7440-38-2
Cadmium
ND
mg/kg
0.45
1
03/25/1810:10
03/28/1818:04
7440-43-9
Calcium
382000
mg/kg
2260
50
03/25/18 10:10
03/28/18 23:24
7440-70-2
Chromium
ND
mg/kg
2.3
1
03/25/1810:10
03/28/1818:04
7440-47-3
Copper
ND
mg/kg
2.3
1
03/25/1810:10
03/28/1818:04
7440-50-8
Lead
ND
mg/kg
2.3
1
03/25/1810:10
03/28/1818:04
7439-92-1
Magnesium
14600
mg/kg
45.2
1
03/25/1810:10
03/28/1818:04
7439-95-4
Molybdenum
ND
mg/kg
2.3
1
03/25/1810:10
03/28/1818:04
7439-98-7
Nickel
ND
mg/kg
2.3
1
03/25/1810:10
03/28/1818:04
7440-02-0
Potassium
ND
mg/kg
2260
1
03/25/1810:10
03/28/1818:04
7440-09-7
Selenium
ND
mg/kg
4.5
1
03/25/1810:10
03/28/1818:04
7782-49-2
Sodium
ND
mg/kg
2260
1
03/25/1810:10
03/28/1818:04
7440-23-5
Zinc
ND
mg/kg
4.5
1
03/25/1810:10
03/28/1818:04
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
ND
mg/kg
0.021
1
03/27/1819:11
03/28/1813:07
7439-97-6 M1
8260 MSV TCLP
Analytical Method:
EPA 8260
Leachate Method/Date: EPA 1311; 03/26/18
12:07
Benzene
ND
ug/L
50.0
10
04/04/1815:20
71-43-2
2-Butanone (MEK)
ND
ug/L
100
10
04/04/18 15:20
78-93-3
Carbon tetrachloride
ND
ug/L
50.0
10
04/04/18 15:20
56-23-5
Chlorobenzene
ND
ug/L
50.0
10
04/04/1815:20
108-90-7
Chloroform
ND
ug/L
50.0
10
04/04/1815:20
67-66-3
1,4 -Dichlorobenzene
ND
ug/L
50.0
10
04/04/1815:20
106-46-7
1,2-Dichloroethane
ND
ug/L
50.0
10
04/04/1815:20
107-06-2
1,1-Dichloroethene
ND
ug/L
50.0
10
04/04/1815:20
75-35-4
Tetrachloroethene
ND
ug/L
50.0
10
04/04/1815:20
127-18-4
Trichloroethene
ND
ug/L
50.0
10
04/04/1815:20
79-01-6
Vinyl chloride
ND
ug/L
50.0
10
04/04/18 15:20
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
70-130
10
04/04/18 15:20
17060-07-0
Toluene -d8 (S)
117
%
67-135
10
04/04/18 15:20
2037-26-5
4-Bromofluorobenzene (S)
105
%
70-130
10
04/04/18 15:20
460-00-4
2540G Total Percent Solids
Analytical Method:
SM 2540G
Total Solids
20.5
%
0.000010
1
03/22/18 18:48
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
79.5
%
0.10
1
03/23/18 08:15
1010 Flash poi nt,Closed Cup
Analytical Method:
EPA 1010
Flashpoint
>200.0
deg F
70.0
1
03/26/18 11:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2018 10:11 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 26

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bi -Monthly Residuals
Pace Project No.: 92378031
Sample: Water Plant Sludge 1-6
Lab ID: 92378031001 Collected: 03/21/18 08:08 Received: 03/21/18 11:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared
Analyzed
CAS No. Qual
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
9.9 Std. Units 0.10 1
03/26/18 14:53
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
ND mg/kg 39.4 1
03/27/18 08:41
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
ND mg/kg 244 1
04/03/18 05:10
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg 9.6 1
04/03/1823:55
M1,R1
Nitrogen, Nitrite
ND mg/kg 4.8 1
04/03/1823:55
M1,R1
Nitrogen, NO2 plus NO3
ND mg/kg 9.6 1
04/03/18 23:55
M1,R1
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
242 mg/kg 9.4 1
03/26/1816:40
7723-14-0
4500 Chloride in Soil
Analytical Method: SM 4500 -CI -E
Chloride
ND mg/kg 242 1
03/27/18 00:35
16887-00-6
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW -846 7.3.3.2
Cyanide, Reactive
ND mg/kg 4.9 1 03/28/18 23:03
03/29/18 01:58
734S Reactive Sulfide
Analytical Method: SM4500S2F-00 Preparation Method: SW -846 7.3.4.2
Sulfide, Reactive
ND mg/kg 48.6 1 03/28/18 23:03
03/29/18 00:03
9056 IC Anions
Analytical Method: EPA 9056A Preparation Method: EPA 9056A
Sulfate
821 mg/kg 244 1 03/29/1816:05
03/30/1818:36
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2018 10:11 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 26

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 5/23/2018
% Solids 6
Mineralization Rate 0
Gallons per DT 3,996.80
PH 10.2
Sodium Absorpotion 0.64 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 663 lbs./1,000 gal 0.33
Ammonia Nitrogen (mg/Kg) 148.00 lbs./1,000 gal 0.07
Nitrate -Nitrite (mg/Kg) 32.10 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 106 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 180 lbs./1,000 gal 0.09
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.10
Phosphorus lbs./1,000 gal 0.21
Calcium lbs./1,000 gal 197.66
Magnesium lbs./1,000 gal 8.06
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
12.40
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
1.20
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
6.20
Copper lbs./1,000 gal
0.00
Lead (mg/Ig)
6.20
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.06
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
6.20
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
12.40
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
12.40
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
557
Total 106 0.21
Total 180 0.36
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
663
106 0.21
557
663
180 0.36
483
557
0 0.00
557
483
0 0.00
483
557
0 0.00
557
483
0 0.00
483
557
0 0.00
557
483
0 0.00
483
557
0 0.00
557
483
0 0.00
483
Total 106 0.21
Total 180 0.36
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: Bi -Monthly Residuals
Pace Project No.: 92385890
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Water Plant Sludge 1 Lab ID: 92385890001 Collected: 05/23/18 09:05 Received: 05/23/18 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
14600
mg/kg
124
1
06/05/18 02:30
06/05/18 21:39
7429-90-5
Arsenic
ND
mg/kg
12.4
1
06/05/18 02:30
06/05/18 21:39
7440-38-2
Cadmium
ND
mg/kg
1.2
1
06/05/18 02:30
06/05/18 21:39
7440-43-9
Calcium
395000
mg/kg
620
5
06/05/18 02:30
06/06/18 13:24
7440-70-2
Chromium
ND
mg/kg
6.2
1
06/05/18 02:30
06/05/18 21:39
7440-47-3
Copper
ND
mg/kg
6.2
1
06/05/18 02:30
06/05/18 21:39
7440-50-8
Lead
ND
mg/kg
6.2
1
06/05/18 02:30
06/05/18 21:39
7439-92-1
Magnesium
16100
mg/kg
124
1
06/05/18 02:30
06/05/18 21:39
7439-95-4
Molybdenum
ND
mg/kg
6.2
1
06/05/18 02:30
06/05/18 21:39
7439-98-7
Nickel
ND
mg/kg
6.2
1
06/05/18 02:30
06/05/18 21:39
7440-02-0
Potassium
ND
mg/kg
6200
1
06/05/18 02:30
06/05/18 21:39
7440-09-7
Selenium
ND
mg/kg
12.4
1
06/05/18 02:30
06/05/18 21:39
7782-49-2
Sodium
ND
mg/kg
6200
1
06/05/18 02:30
06/05/18 21:39
7440-23-5
Zinc
ND
mg/kg
12.4
1
06/05/18 02:30
06/05/18 21:39
7440-66-6
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 0.059 1 06/05/1812:10 06/05/1814:35 7439-97-6
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 94.5 % 0.10 1 06/07/18 16:19
Sample: Water Plant Sludge 2 Lab ID: 92385890002 Collected: 05/23/18 09:05 Received: 05/23/18 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture
Percent Moisture
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
Nitrogen, NO2 plus NO3
365.1 Phosphorus, Total
Phosphorus
Date: 06/07/2018 04:30 PM
Analytical Method: ASTM D2974-87
94.0 %
0.10
1
06/07/1816:19
Analytical Method: EPA 350.1 1993
Rev 2.0
ND mg/kg
148
1
05/30/1811:57 7664-41-7
Analytical Method: EPA 351.2
ND mg/kg
663
1
05/31/18 01:31 7727-37-9
Analytical Method: EPA 353.2
ND mg/kg
32.1
1
05/30/1813:01
ND mg/kg
16.0
1
05/30/1813:01
ND mg/kg
32.1
1
05/30/1813:01
Analytical Method: EPA 365.1
429 mg/kg
291
10
06/01/18 21:33 7723-14-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: Bi -Monthly Residuals
Pace Project No.: 92385890
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Water Plant Sludge 3 Lab ID: 92385890003 Collected: 05/23/18 09:05 Received: 05/23/18 14:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture
Percent Moisture
4500 Chloride in Soil
Chloride
9056 IC Anions
Sulfate
Date: 06/07/2018 04:30 PM
Analytical Method: ASTM D2974-87
94.2 % 0.10 1 06/07/1816:20
Analytical Method: SM 4500 -CI -E
682 mg/kg 170 1 06/04/1812:31 16887-00-6 M1
Analytical Method: EPA 9056A Preparation Method: EPA 9056A
164 mg/kg 49.8 1 05/31/1813:28 06/01/1814:37 14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 7/19/2018
% Solids 13.2
Mineralization Rate 0
Gallons per DT 1,816.73
PH 11.16
Sodium Absorpotion 0.56 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 291 lbs./1,000 gal 0.32
Ammonia Nitrogen (mg/Kg) 56.40 lbs./1,000 gal 0.06
Nitrate -Nitrite (mg/Kg) 15.10 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 43 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 72 lbs./1,000 gal 0.08
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.30
Phosphorus lbs./1,000 gal 0.44
Calcium lbs./1,000 gal 289.53
Magnesium lbs./1,000 gal 13.87
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
6.00
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
0.60
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
3.00
Copper lbs./1,000 gal
0.00
Lead (mg/Ig)
3.00
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
3.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
6.00
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
6.00
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
248
0 0.00
Total 43 0.09
Total 72 0.14
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
291
43 0.09
248
291
72 0.14
220
248
0 0.00
248
220
0 0.00
220
248
0 0.00
248
220
0 0.00
220
248
0 0.00
248
220
0 0.00
220
248
0 0.00
248
220
0 0.00
220
Total 43 0.09
Total 72 0.14
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
-pacelabs.com
ANALYTICAL RESULTS
Project: Bi -Monthly Residuals
Pace Project No.: 92392656
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Water Plant Sludge 1 Lab ID: 92392656001 Collected: 07/19/18 09:43 Received: 07/19/18 10:33 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
10900
mg/kg
60.0
1 07/24/18 12:04
07/25/18 20:07
7429-90-5
Arsenic
ND
mg/kg
6.0
1 07/24/18 12:04
07/25/18 20:07
7440-38-2
Cadmium
ND
mg/kg
0.60
1 07/24/18 12:04
07/25/18 20:07
7440-43-9
Calcium
263000
mg/kg
300
5 07/24/18 12:04
07/25/18 20:26
7440-70-2
Chromium
ND
mg/kg
3.0
1 07/24/18 12:04
07/25/18 20:07
7440-47-3
Copper
ND
mg/kg
3.0
1 07/24/18 12:04
07/25/18 20:07
7440-50-8
Lead
ND
mg/kg
3.0
1 07/24/18 12:04
07/25/18 20:07
7439-92-1
Magnesium
12600
mg/kg
60.0
1 07/24/18 12:04
07/25/18 20:07
7439-95-4
Molybdenum
ND
mg/kg
3.0
1 07/24/18 12:04
07/25/18 20:07
7439-98-7
Nickel
ND
mg/kg
3.0
1 07/24/18 12:04
07/25/18 20:07
7440-02-0
Potassium
ND
mg/kg
3000
1 07/24/18 12:04
07/25/18 20:07
7440-09-7
Selenium
ND
mg/kg
6.0
1 07/24/18 12:04
07/25/18 20:07
7782-49-2
Sodium
ND
mg/kg
3000
1 07/24/18 12:04
07/25/18 20:07
7440-23-5
Zinc
ND
mg/kg
6.0
1 07/24/18 12:04
07/25/18 20:07
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury
ND
mg/kg
0.021
1 07/23/1813:56
07/24/1812:36
7439-97-6
2540G Total Percent Solids
Analytical Method:
SM 254OG-2011
Total Solids
13.2
%
0.000010
1
07/23/18 16:12
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
86.8
%
0.10
1
07/23/18 16:02
350.1 Ammonia
Analytical Method:
EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
ND
mg/kg
56.4
1 07/24/18 11:00
07/24/18 16:41
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
ND
mg/kg
291
1 07/24/18 11:30
07/25/18 02:21
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method:
EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND
mg/kg
15.1
1 07/26/18 21:50
07/27/18 05:59
Nitrogen, Nitrate
ND
mg/kg
15.1
1 07/26/18 21:50
07/27/18 05:59
14797-55-8
Nitrogen, Nitrite
ND
mg/kg
7.6
1 07/26/18 21:50
07/27/18 05:59
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus
398
mg/kg
14.8
1 07/24/18 22:15
07/25/18 02:44
7723-14-0
9056 IC Anions
Analytical Method:
EPA 9056A Preparation Method: EPA 9056A
Sulfate
1390
mg/kg
376
1 07/25/18 10:19
07/27/18 01:20
14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/02/2018 04:10 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 18

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 9/17/2018
% Solids 18.2
Mineralization Rate 0
Gallons per DT 1,317.63
PH 10.37
Sodium Absorpotion 0.57 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 250 lbs./1,000 gal 0.38
Ammonia Nitrogen (mg/Kg) 49.10 lbs./1,000 gal 0.07
Nitrate -Nitrite (mg/Kg) 10.90 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 35 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 60 lbs./1,000 gal 0.09
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.66
Phosphorus lbs./1,000 gal 0.31
Calcium lbs./1,000 gal 347.59
Magnesium lbs./1,000 gal 15.18
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
4.80
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
0.48
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
2.40
Copper lbs./1,000 gal
0.00
Lead (mg/Ig)
2.40
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.02
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
2.40
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
4.80
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
4.80
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
215
0 0.00
Total 35 0.07
Total 60 0.12
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
250
35 0.07
215
250
60 0.12
190
215
0 0.00
215
190
0 0.00
190
215
0 0.00
215
190
0 0.00
190
215
0 0.00
215
190
0 0.00
190
215
0 0.00
215
190
0 0.00
190
Total 35 0.07
Total 60 0.12
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
-pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Bi -Monthly Residuals
Pace Project No.: 92399624
Sample: Water Plant Sludge
Lab ID: 92399624001 Collected:
09/17/18
08:56
Received: 09/17/18 10:53 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture,
sample size and any dilutions.
Parameters
Results Units Report
Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
8580 mg/kg
48.2
1
09/21/1814:01
09/23/1819:27
7429-90-5
Arsenic
ND mg/kg
4.8
1
09/21/1814:01
09/23/1819:27
7440-38-2
Cadmium
ND mg/kg
0.48
1
09/21/1814:01
09/23/1819:27
7440-43-9
Calcium
229000 mg/kg
482
10
09/21/18 14:01
09/24/18 04:26
7440-70-2
Chromium
ND mg/kg
2.4
1
09/21/1814:01
09/23/1819:27
7440-47-3
Copper
ND mg/kg
2.4
1
09/21/1814:01
09/23/1819:27
7440-50-8
Lead
ND mg/kg
2.4
1
09/21/1814:01
09/23/1819:27
7439-92-1
Magnesium
10000 mg/kg
48.2
1
09/21/1814:01
09/23/1819:27
7439-95-4
Molybdenum
ND mg/kg
2.4
1
09/21/1814:01
09/23/1819:27
7439-98-7 P8
Nickel
ND mg/kg
2.4
1
09/21/1814:01
09/23/1819:27
7440-02-0
Potassium
ND mg/kg
2410
1
09/21/1814:01
09/23/1819:27
7440-09-7
Selenium
ND mg/kg
4.8
1
09/21/1814:01
09/23/1819:27
7782-49-2
Sodium
ND mg/kg
2410
1
09/21/1814:01
09/23/1819:27
7440-23-5
Zinc
ND mg/kg
4.8
1
09/21/1814:01
09/23/1819:27
7440-66-6
7471 Mercury
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
Mercury
ND mg/kg
0.021
1
09/20/1818:32
09/21/1812:43
7439-97-6
2540G Total Percent Solids
Analytical Method: SM 254OG-2011
Total Solids
18.2 % 0.000010
1
09/18/18 15:23
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
81.8 %
0.10
1
09/18/18 15:16
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod.
Preparation
Method:
EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
ND mg/kg
49.1
1
09/22/18 16:30
09/22/18 17:29
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
ND mg/kg
250
1
09/20/18 14:22
09/21/18 05:47
7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND mg/kg
10.9
1
09/22/18 09:37
09/22/18 15:29
Nitrogen, Nitrate
ND mg/kg
10.9
1
09/22/18 09:37
09/22/18 15:29
14797-55-8
Nitrogen, Nitrite
ND mg/kg
5.4
1
09/22/18 09:37
09/22/18 15:29
14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
Phosphorus
203 mg/kg
10.4
1
09/20/18 12:28
09/21/18 01:34
7723-14-0
4500 Chloride in Soil
Analytical Method: SM 4500 -CI -E-2011
Preparation
Method:
SM 4500 -CI -E-2011
Chloride
194 mg/kg
54.8
1
09/25/18 16:19
09/25/18 20:41
16887-00-6
9056 IC Anions
Analytical Method: EPA 9056A Preparation Method:
EPA 9056A
Sulfate
941 mg/kg
273
1
09/20/18 15:25
09/28/18 00:54
14808-79-8
Date: 09/28/2018 01:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 19

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AGMAN
FIELD LOADING ESTIMATES
Facility Elizabeth City WTP
Sampling Date 11/16/2018
% Solids 6.5
Mineralization Rate 0
Gallons per DT 3,689.36
PH 10.36
Sodium Absorpotion 3.54 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 487 lbs./1,000 gal 0.26
Ammonia Nitrogen (mg/Kg) 122.00 lbs./1,000 gal 0.07
Nitrate -Nitrite (mg/Kg) 32.60 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 94 lbs./1,000 gal 0.05
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 155 lbs./1,000 gal 0.08
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 7.16
Phosphorus lbs./1,000 gal 0.39
Calcium lbs./1,000 gal 33.77
Magnesium lbs./1,000 gal 1.95
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.01
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
26.50
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.60
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
13.20
Copper lbs./1,000 gal
0.01
Lead (mg/Ig)
13.20
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.09
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
13.20
Nickel lbs./1,000 gal
0.01
Selenium (mg/Kg)
26.50
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
26.50
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
393
Total 94 0.19
Total 155 0.31
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
487
94 0.19
393
487
155 0.31
332
393
0 0.00
393
332
0 0.00
332
393
0 0.00
393
332
0 0.00
332
393
0 0.00
393
332
0 0.00
332
393
0 0.00
393
332
0 0.00
332
Total 94 0.19
Total 155 0.31
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BiMonthly Residuals +Full TCLP
Pace Project No.: 92407889
Sample: WTP Sludge Lab ID: 92407889001 Collected: 11/16/18 09:55 Received: 11/16/18 14:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
mg/kg
265
1
Leachate Method/Date: EPA 1311; 11/26/18 12:05
Initial
pH: ; Final pH:
5
ND
gamma -BHC (Lindane)
ND
ug/L
0.50
1
11/27/18 13:19
11/29/18 16:35
58-89-9
Chlordane (Technical)
ND
ug/L
3.0
1
11/27/18 13:19
11/29/18 16:35
57-74-9
Endrin
ND
ug/L
0.50
1
11/27/1813:19
11/29/1816:35
72-20-8
Heptachlor
ND
ug/L
0.50
1
11/27/1813:19
11/29/1816:35
76-44-8
Heptachlor epoxide
ND
ug/L
0.50
1
11/27/18 13:19
11/29/18 16:35
1024-57-3
Methoxychlor
ND
ug/L
1000
1
11/27/1813:19
11/29/1816:35
72-43-5
Toxaphene
ND
ug/L
3.0
1
11/27/1813:19
11/29/1816:35
8001-35-2
Surrogates
13.2
1
11/26/18 15:09
11/28/18 01:12
7439-98-7
Nickel
ND
Decachlorobiphenyl (S)
77
%
10-138
1
11/27/18 13:19
11/29/18 16:35
2051-24-3
Tetrachloro-m-xylene (S)
73
%
10-110
1
11/27/18 13:19
11/29/18 16:35
877-09-8
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
3150
mg/kg
265
1
11/26/18 15:09
11/28/18 01:12
7429-90-5
Arsenic
ND
mg/kg
26.5
1
11/26/18 15:09
11/28/18 01:12
7440-38-2
Cadmium
ND
mg/kg
2.6
1
11/26/18 15:09
11/28/18 01:12
7440-43-9
Calcium
62300
mg/kg
265
1
11/26/18 15:09
11/28/18 01:12
7440-70-2
Chromium
ND
mg/kg
13.2
1
11/26/18 15:09
11/28/18 01:12
7440-47-3
Copper
ND
mg/kg
13.2
1
11/26/18 15:09
11/28/18 01:12
7440-50-8
Lead
ND
mg/kg
13.2
1
11/26/18 15:09
11/28/18 01:12
7439-92-1
Magnesium
3600
mg/kg
265
1
11/26/18 15:09
11/28/18 01:12
7439-95-4
Molybdenum
ND
mg/kg
13.2
1
11/26/18 15:09
11/28/18 01:12
7439-98-7
Nickel
ND
mg/kg
13.2
1
11/26/18 15:09
11/28/18 01:12
7440-02-0
Potassium
ND
mg/kg
13200
1
11/26/18 15:09
11/28/18 01:12
7440-09-7
Selenium
ND
mg/kg
26.5
1
11/26/18 15:09
11/28/18 01:12
7782-49-2
Sodium
ND
mg/kg
13200
1
11/26/18 15:09
11/28/18 01:12
7440-23-5
Zinc
ND
mg/kg
26.5
1
11/26/18 15:09
11/28/18 01:12
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010D
Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 11/29/18 21:42 Initial
pH: 9.9; Final pH: 5
Arsenic
ND
mg/L
0.050
1
11/30/1819:12
12/02/1819:16
7440-38-2
Barium
ND
mg/L
0.25
1
11/30/1819:12
12/02/1819:16
7440-39-3
Cadmium
ND
mg/L
0.0050
1
11/30/1819:12
12/02/1819:16
7440-43-9
Chromium
ND
mg/L
0.050
1
11/30/1819:12
12/02/1819:16
7440-47-3
Lead
ND
mg/L
0.025
1
11/30/1819:12
12/02/1819:16
7439-92-1
Selenium
ND
mg/L
0.10
1
11/30/1819:12
12/02/1819:16
7782-49-2
Silver
ND
mg/L
0.025
1
11/30/1819:12
12/02/1819:16
7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470A
Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 11/29/18 21:42 Initial
pH: 9.9; Final pH: 5
Mercury
ND
mg/L
0.00020
1
12/01/18 22:26
12/03/18 10:49
7439-97-6
7471 Mercury
Analytical Method: EPA 7471 B
Preparation Method: EPA 7471 B
Mercury
ND
mg/kg
0.089
1
11/28/1814:27
11/29/1812:55
7439-97-6
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except
in full,
Date: 12/17/2018 03:27 PM
without
the written consent
of Pace Analytical Services,
LLC.
Page 4 of 39

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: BiMonthly Residuals +Full TCLP
Pace Project No.: 92407889
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WTP Sludge Lab ID: 92407889001 Collected: 11/16/18 09:55 Received: 11/16/18 14:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270D Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 11/26/18 12:05
Initial pH: ; Final pH:
5
1,4 -Dichlorobenzene
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
106-46-7
2,4-Dinitrotoluene
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
121-14-2
Hexachloro-1,3-butadiene
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
87-68-3
Hexachlorobenzene
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
118-74-1
Hexachloroethane
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
67-72-1
2-Methylphenol(o-Cresol)
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
15831-10-4
Nitrobenzene
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
98-95-3
Pentachlorophenol
ND
ug/L
100
1
11/27/18 08:36
11/27/18 17:38
87-86-5
Pyridine
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
110-86-1
2,4,5 -Trichlorophenol
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
50.0
1
11/27/18 08:36
11/27/18 17:38
88-06-2
Surrogates
Nitrobenzene -d5 (S)
62
%
12-102
1
11/27/18 08:36
11/27/18 17:38
4165-60-0
2-Fluorobiphenyl (S)
64
%
13-107
1
11/27/18 08:36
11/27/18 17:38
321-60-8
Terphenyl-d14 (S)
76
%
21-132
1
11/27/18 08:36
11/27/18 17:38
1718-51-0
Phenol -d6 (S)
18
%
10-110
1
11/27/18 08:36
11/27/18 17:38
13127-88-3
2-Fluorophenol (S)
27
%
10-110
1
11/27/18 08:36
11/27/18 17:38
367-12-4
2,4,6-Tribromophenol (S)
45
%
27-108
1
11/27/18 08:36
11/27/18 17:38
118-79-6
8260 MSV TCLP
Analytical Method:
EPA 8260B
Leachate Method/Date: EPA 1311; 11/28/18 08:35
Benzene
ND
ug/L
100
20
12/03/1817:53
71-43-2
2-Butanone (MEK)
ND
ug/L
200
20
12/03/18 17:53
78-93-3
Carbon tetrachloride
ND
ug/L
100
20
12/03/18 17:53
56-23-5
Chlorobenzene
ND
ug/L
100
20
12/03/1817:53
108-90-7
Chloroform
ND
ug/L
100
20
12/03/1817:53
67-66-3
1,4 -Dichlorobenzene
ND
ug/L
100
20
12/03/1817:53
106-46-7
1,2-Dichloroethane
ND
ug/L
100
20
12/03/1817:53
107-06-2
1,1-Dichloroethene
ND
ug/L
100
20
12/03/1817:53
75-35-4
Tetrachloroethene
ND
ug/L
100
20
12/03/1817:53
127-18-4
Trichloroethene
ND
ug/L
100
20
12/03/1817:53
79-01-6
Vinyl chloride
ND
ug/L
100
20
12/03/18 17:53
75-01-4
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
20
12/03/18 17:53
17060-07-0
Toluene -d8 (S)
109
%
67-135
20
12/03/18 17:53
2037-26-5
4-Bromofluorobenzene (S)
107
%
70-130
20
12/03/18 17:53
460-00-4
254OG Total Percent Solids Analytical Method: SM 2540G-2011
Total Solids 6.5 % 0.000010 1 11/21/18 17:13
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 93.5 % 0.10 1 11/21/18 17:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 03:27 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 39

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BiMonthly Residuals +Full TCLP
Pace Project No.: 92407889
Sample: WTP Sludge
Lab ID: 92407889001 Collected: 11/16/18 09:55 Received: 11/16/18 14:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010A
Flashpoint
>200 deg F 70.0 1 11/25/18 13:13
9045 pH Soil
Analytical Method: EPA 9045D
pH at 25 Degrees C
9.7 Std. Units 0.10 1 11/26/18 13:31 H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
Nitrogen, Ammonia
ND mg/kg 122 1 12/01/18 09:31 12/02/18 16:02 7664-41-7 M1
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
487 mg/kg 480 1 11/26/18 14:30 11/28/18 02:12 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
32.6 mg/kg 30.3 1 12/03/18 11:57 12/04/18 05:55
Nitrogen, Nitrate
32.6 mg/kg 30.3 1 12/03/18 11:57 12/04/18 05:55 14797-55-8
Nitrogen, Nitrite
ND mg/kg 15.2 1 12/03/18 11:57 12/04/18 05:55 14797-65-0
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Phosphorus
721 mg/kg 27.9 1 11/21/18 22:00 11/22/18 02:57 7723-14-0
4500 Chloride in Soil
Analytical Method: SM 4500 -CI -E-2011 Preparation Method: SM 4500 -CI -E-2011
Chloride
525 mg/kg 152 1 11/28/18 17:30 11/29/18 00:11 16887-00-6
733C S Reactive Cyanide
Analytical Method: EPA 9014 Preparation Method: SW -846 7.3.3.2
Cyanide, Reactive
ND mg/kg 15.3 1 12/13/18 16:12 12/13/18 18:35
734S Reactive Sulfide
Analytical Method: SM4500S2F-00 Preparation Method: SW -846 7.3.4.2
Sulfide, Reactive
ND mg/kg 153 1 12/13/18 16:12 12/13/18 16:25
9056 IC Anions
Analytical Method: EPA 9056A Preparation Method: EPA 9056A
Sulfate
3470 mg/kg 765 1 11/29/1815:34 11/30/1812:39 14808-79-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 03:27 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 39

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ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
November 30, 2018
Angela Baioni
Pace Analytical Services, Inc.
9800 KINCEY AVE STE 100
HUNTERSVILLE NC 28078-8400
RE: 92407889
Dear Angela Baioni: Order No: 1811K19
Analytical Environmental Services, Inc. received 1 samples on November 21, 2018 9:52 am
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the
analyses contained herein will be noted and submitted in the form of a project Case Narrative. AES'
certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/18-06/30/19.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/18.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/19.
These results relate only to the items tested. This report may only be reproduced in full and with written
permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Jessica Shilling
Project Manager
3080 Presi4ential Drive • Atlanta, Georgia 30340 -Tel: [phone] • Fax: 770.457-S 188 • Toll F.,e:800.972.4889
www.aesatlanta.com
Page 35 of 39
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Analytical Environmental Services, Inc
Date: 30 -Nov -18
Client:
Pace Analytical Services, Inc.
Client Sample ID:
WTP SLUDGE
Project Name:
92407889
Collection Date:
11/16/2018 9:55:00 AM
Lab ID:
1811K19-001
Matrix:
Solid
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
HERBICIDES, TCLP SW1311/8151A
2,4,5 -TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 76.6 49.4-120
Qualifiers: • value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW3510C)
mg/L 270683 1 11/29/201812:48 UH
mg/L 270683 1 11/29/201812:48 UH
%REC 270683 1 11/29/201812:48 UH
E
Estimated (value above quantitation range)
S
Spike Recovery outside limits due to matrix
Nan'
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NC
Not confirmed
<
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J
Estimated value detected below Reporting Limit
Page 37 of 39
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City of Elizabeth City
2018 Class B Annual Report
WQ Permit# WQ0002883
Residual Sampling Summary Form
Elizabeth City WWTP
Field Loading Calculations
2018 Analytical
2018 TCLP

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Facility Elizabeth City WWTP
FIELD LOADING ESTIMATES
Sampling Date 2/13/2018
% Solids 4.93
Mineralization Rate 0.3
Gallons per DT 4,864.26
PH 12.31
Sodium Absorpotion 0.31 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 38,690 lbs./1,000 gal 15.91
Ammonia Nitrogen (mg/Kg) 80.18 lbs./1,000 gal 0.03
Nitrate -Nitrite (mg/Kg) 83.87 lbs./1,000 gal 0.03
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 11,707 lbs./1,000 gal 4.81
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 11,747 lbs./1,000 gal 4.83
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 1.69
Phosphorus lbs./1,000 gal 8.58
Calcium lbs./1,000 gal 51.19
Magnesium lbs./1,000 gal 2.16
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
3.70
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
1.10
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
186.00
Copper lbs./1,000 gal
0.08
Lead (mg/Ig)
13.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.31
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.00
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
5.00
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
626.00
Zinc lbs./1,000 gal
0.26
RESIDUAL NITROGEN CALCULATION
26,983
Total 18,653 37.31
Total 18,683 37.37
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
38,690
11,707
23.41
26,983
38,690
11,747 23.49
26,943
26,983
4,047
8.09
22,936
26,943
4,041 8.08
22,902
22,936
1,720
3.44
21,215
22,902
1,718 3.44
21,184
21,215
796
1.59
20,420
21,184
794 1.59
20,390
20,420
383
0.77
20,037
20,390
382 0.76
20,007
Total 18,653 37.31
Total 18,683 37.37
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CITY OF ELIZABETH CITY
MR. TRAVIS TUCKER
ATTN: WWTP
P.O. BOX 347
ELIZABETH CITY ,NC 27907-0404
Sludge Analysis Method
PARAMETERS Sample Date Analyst Code
Aluminum, (dry wt. basis), mg/kg 8706 03/07/18 LFJ EPA200.7
Arsenic (dry wt. basis), mg/kg 3.7 03/07/18 MTM 3113B-04
Calcium (dry wt. basis), mg/kg 124504 03/07/18 LFJ EPA200.7
Cadmium (dry wt. basis), mg/kg 1.1 03/08/18 MTM 3113B-04
Copper (dry wt. basis), mg/kg 186 03/07/18 LFJ EPA200.7
Chromium, T.(dry wt. basis),mg/kg 15 03/07/18 LFJ EPA200.7
Lead (dry weight basis), mg/kg 13 03/06/18 MTM 3113B-04
Magnesium (dry wt. basis), mg/kg 5258 03/07/18 LFJ EPA200.7
Mercury (dry wt. basis), mg/kg 0.31 02/27/18 MTM EPA7471B
Nickel (dry wt. basis), mg/kg 10 03/14/18 LFJ EPA200.7
Potassium (dry wt. basis), mg/kg 4100 03/07/18 LFJ EPA200.7
Selenium (dry wt. basis), mg/kg <5.0 03/07/18 MTM 3113B-04
Sodium (dry wt. basis), mg/kg 1835 03/07/18 LFJ EPA200.7
Zinc (dry wt. basis), mg/kg 626 03/07/18 LFJ EPA200.7
Total Solids, % 4.93 02/15/18 KDS 2540G-11
TKN (dry wt.), mg/kg c 38690 02/28/18 MF 351.2 R2-93
Ammonia Nitrogen (dry wt.),mg/kg c 80.18 03/13/18 DTL 350.1 R2-93
Phosphorus, T. (dry wt.), mg/kg c 20860 03/08/18 DTL 365.4-74
Chloride (dry wt. basis), mg/kg c 9840 03/05/18 KAC 4500CLB-11
Nitrate -Nitrite (dry wt.), mg/kg c 83.87 03/09/18 MF 353.2 R2-93
Molybdenum (dry wt. basis), mg/kg < 5.0 03/07/18 LFJ EPA200.7
Drinking
Water
ID:
37715
Wastewater
ID:
10
PHONE [phone]
FAX [phone]
ID#: 1054
DATE COLLECTED:
DATE REPORTED
REVIEWEiD
02/13/18
03/28/18
c Uncertified data. DWR does not offer non -aqueous certification for this analytical Brocedure.

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Facility Elizabeth City WWTP
FIELD LOADING ESTIMATES
Sampling Date 5/9/2018
% Solids 4.7
Mineralization Rate 0.3
Gallons per DT 5,102.30
PH 11.5
Sodium Absorpotion 0.31 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 14,700 lbs./1,000 gal 5.76
Ammonia Nitrogen (mg/Kg) 251.00 lbs./1,000 gal 0.10
Nitrate -Nitrite (mg/Kg) 2.00 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 4,462 lbs./1,000 gal 1.75
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 4,588 lbs./1,000 gal 1.80
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 0.15
Phosphorus lbs./1,000 gal 0.25
Calcium lbs./1,000 gal 1.91
Magnesium lbs./1,000 gal 0.09
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
0.75
Arsenic lbs./1,000 gal
0.00
Cadmium (mg/Kg)
0.09
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
9.10
Copper lbs./1,000 gal
0.00
Lead (mg/Ig)
0.69
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.04
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
0.51
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
0.75
Selenium lbs./1,000 gal
0.00
Zinc (mg/Kg)
30.80
Zinc lbs./1,000 gal
0.01
RESIDUAL NITROGEN CALCULATION
10,238
Total 7,098 14.20
Total 7,191 14.38
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
14,700
4,462 8.92
10,238
14,700
4,588 9.18
10,112
10,238
1,536 3.07
8,702
10,112
1,517 3.03
8,595
8,702
653 1.31
8,049
8,595
645 1.29
7,951
8,049
302 0.60
7,748
7,951
298 0.60
7,653
7,748
145 0.29
7,602
7,653
143 0.29
7,509
Total 7,098 14.20
Total 7,191 14.38
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92384202
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WASTEWATER PLANT Lab ID: 92384202002 Collected: 05/09/18 09:26 Received: 05/09/18 16:00 Matrix: Solid
SLUDGE #4
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
350.1 Ammonia Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia 251 mg/kg 9.4 1 05/24/18 15:39 7664-41-7
365.1 Phosphorus, Total Analytical Method: EPA 365.1
Phosphorus 636 mg/kg 23.3 20 05/16/18 07:15 7723-14-0
Date: 05/25/2018 02:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 30

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92384202
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WASTEWATER PLANT Lab ID: 92384202003 Collected: 05/09/18 09:26 Received: 05/09/18 16:00 Matrix: Solid
SLUDGE #5
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 95.3 % 0.10 1 05/15/18 11:55
Date: 05/25/2018 02:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
CAS No. Qual
Page 6 of 30

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92384202
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WASTEWATER PLANT Lab ID: 92384202004 Collected: 05/09/18 09:26 Received: 05/09/18 16:00 Matrix: Solid
SLUDGE #6& #8
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>212 deg F 75.0 1 05/14/18 14:29
734S Reactive Sulfide
Analytical Method: SW -846 7.3.4.2 Preparation Method: SW -846 7.3.4.2
Sulfide, Reactive
ND mg/kg 50.0 1 05/14/18 08:30 05/14/18 14:55
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
11.5 Std. Units 0.010 1 05/15/18 14:57
733C S Reactive Cyanide
Analytical Method: SW -846 7.3.3.2 Preparation Method: SW -846 7.3.3.2
Cyanide, Reactive
ND mg/kg 25.0 1 05/14/18 08:30 05/15/18 12:37
CAS No. Qual
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/25/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 30

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92384202
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WASTEWATER PLANT Lab ID: 92384202005 Collected: 05/09/18 09:26 Received: 05/09/18 16:00 Matrix: Solid
SLUDGE #7
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Percent Moisture
Percent Moisture
4500 Chloride in Soil
Chloride
9056 IC Anions
Sulfate
Date: 05/25/2018 02:07 PM
Analytical Method: ASTM D2974-87
94.6 % 0.10 1 05/18/1810:48
Analytical Method: SM 4500 -CI -E
634 mg/kg 99.8 10 05/15/1812:11 16887-00-6
Analytical Method: EPA 9056 Preparation Method: EPA 9056
ND mg/kg 922 1 05/17/18 05:30 05/17/18 08:15 14808-79-8 M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 30

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92384202
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WASTEWATER PLANT
Lab ID: 92384202006 Collected: 05/09/18 09:26
Received: 05/09/18 16:00 Matrix: Solid
SLUDGE #3
Results reported on a "wet -weight"
basis
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
14700 mg/kg
500
10
05/16/18 02:46 7727-37-9
353.2 Nitrogen, NO2/NO3
Analytical Method: EPA 353.2
Nitrogen, Nitrate
ND mg/kg
2.0
1
05/16/18 21:37
Nitrogen, Nitrite
1.4 mg/kg
1.0
1
05/16/18 21:37
Nitrogen, NO2 plus NO3
ND mg/kg
2.0
1
05/16/18 21:37
Date: 05/25/2018 02:07 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SLUDGE
Pace Project No.: 92384202
Sample: WASTEWATER PLANT
Lab ID: 92384202007
Collected: 05/09/18 09:26
Received: 05/09/18 16:00 Matrix: Solid
SLUDGE 1& 2
Results reported on a "wet -weight"
basis
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010
Preparation Method: EPA 3050
Aluminum
409
mg/kg
7.5
1
05/22/1813:40
05/23/1813:20
7429-90-5
Arsenic
ND
mg/kg
0.75
1
05/22/1813:40
05/23/1813:20
7440-38-2
Cadmium
0.090
mg/kg
0.075
1
05/22/1813:40
05/23/1813:20
7440-43-9
Calcium
4870
mg/kg
7.5
1
05/22/1813:40
05/23/1813:20
7440-70-2
Chromium
0.86
mg/kg
0.37
1
05/22/1813:40
05/23/1813:20
7440-47-3
Copper
9.1
mg/kg
0.37
1
05/22/1813:40
05/23/1813:20
7440-50-8
Lead
0.69
mg/kg
0.37
1
05/22/1813:40
05/23/1813:20
7439-92-1
Magnesium
228
mg/kg
7.5
1
05/22/1813:40
05/23/1813:20
7439-95-4
Molybdenum
ND
mg/kg
0.37
1
05/22/1813:40
05/23/1813:20
7439-98-7
Nickel
0.51
mg/kg
0.37
1
05/22/1813:40
05/23/1813:20
7440-02-0
Potassium
ND
mg/kg
373
1
05/22/1813:40
05/23/1813:20
7440-09-7
Selenium
ND
mg/kg
0.75
1
05/22/1813:40
05/23/1813:20
7782-49-2
Sodium
ND
mg/kg
373
1
05/22/1813:40
05/23/1813:20
7440-23-5
Zinc
30.8
mg/kg
0.75
1
05/22/1813:40
05/23/1813:20
7440-66-6
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
0.043
mg/kg
0.0032
1
05/16/1817:10
05/18/1814:17
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/25/2018 02:07 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30

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Facility Elizabeth City WWTP
FIELD LOADING ESTIMATES
Sampling Date 10/1/2018
% Solids 5
Mineralization Rate 0.3
Gallons per DT 4,796.16
PH 12.05
Sodium Absorpotion 1.69 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 1,710 lbs./1,000 gal 0.71
Ammonia Nitrogen (mg/Kg) 209.00 lbs./1,000 gal 0.09
Nitrate -Nitrite (mg/Kg) 2.00 lbs./1,000 gal 0.00
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 557 lbs./1,000 gal 0.23
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 661 lbs./1,000 gal 0.28
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 4.13
Phosphorus lbs./1,000 gal 0.35
Calcium lbs./1,000 gal 50.46
Magnesium lbs./1,000 gal 2.11
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
19.80
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
2.00
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
252.00
Copper lbs./1,000 gal
0.11
Lead (mg/Ig)
24.00
Lead lbs./1,000 gal
0.01
Mercury (mg/Kg)
0.29
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
10.70
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
19.80
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
810.00
Zinc lbs./1,000 gal
0.34
RESIDUAL NITROGEN CALCULATION
1,153
Total 854 1.71
Total 931 1.86
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN
PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
1,710
557
1.11
1,153
1,710
661 1.32
1,049
1,153
173
0.35
980
1,049
157 0.31
891
980
74
0.15
907
891
67 0.13
825
907
34
0.07
873
825
31 0.06
794
873
16
0.03
856
794
15 0.03
779
Total 854 1.71
Total 931 1.86
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92401901
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WW PLANT SLUDGE Lab ID: 92401901001 Collected: 10/01/18 14:51 Received: 10/03/18 13:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Aluminum
10700
mg/kg
198
1
10/08/1811:23
10/09/1816:18
7429-90-5
Arsenic
ND
mg/kg
19.8
1
10/08/1811:23
10/09/1816:18
7440-38-2
Cadmium
ND
mg/kg
2.0
1
10/08/1811:23
10/09/1816:18
7440-43-9
Calcium
121000
mg/kg
198
1
10/08/1811:23
10/09/1816:18
7440-70-2
Chromium
23.6
mg/kg
9.9
1
10/08/1811:23
10/09/1816:18
7440-47-3
Copper
252
mg/kg
9.9
1
10/08/1811:23
10/09/1816:18
7440-50-8
Lead
24.0
mg/kg
9.9
1
10/08/1811:23
10/09/1816:18
7439-92-1
Magnesium
5060
mg/kg
198
1
10/08/1811:23
10/09/1816:18
7439-95-4
Molybdenum
ND
mg/kg
9.9
1
10/08/1811:23
10/09/1816:18
7439-98-7
Nickel
10.7
mg/kg
9.9
1
10/08/1811:23
10/09/1816:18
7440-02-0
Potassium
ND
mg/kg
9910
1
10/08/1811:23
10/09/1816:18
7440-09-7
Selenium
ND
mg/kg
19.8
1
10/08/1811:23
10/09/1816:18
7782-49-2
Sodium
ND
mg/kg
9910
1
10/08/1811:23
10/09/1816:18
7440-23-5
Zinc
810
mg/kg
19.8
1
10/08/1811:23
10/09/1816:18
7440-66-6
7471 Mercury Analytical Method: EPA 7471 B Preparation Method: EPA 7471 B
Mercury 0.29 mg/kg 0.083 1 10/06/18 20:34 10/09/18 10:08 7439-97-6
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 95.0 % 0.10 1 10/04/18 14:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2018 09:36 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 23

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SLUDGE
Pace Project No.: 92401901
Sample: WW PLANT SLUDGE Lab ID: 92401901002 Collected: 10/01/18 14:51 Received: 10/03/18 13:40 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
4500 Chloride in Soil Analytical Method: SM 4500 -CI -E-2011 Preparation Method: SM 4500 -CI -E-2011
Chloride 259 mg/kg 9.9 1 10/08/18 18:16 10/09/18 00:57 16887-00-6
Date: 10/15/2018 09:36 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 23

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92401901
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WW PLANT SLUDGE Lab ID: 92401901003 Collected: 10/01/18 14:51 Received: 10/03/18 13:40 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total 1710 mg/kg 83.3 2 10/09/18 09:57 10/10/18 00:16 7727-37-9
353.2 Nitrogen, NO2/NO3 Analytical Method: EPA 353.2 Rev 2.0 1993 Preparation Method: EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3 ND mg/kg 2.0 1 10/08/18 17:20 10/09/18 11:35
Nitrogen, Nitrate ND mg/kg 2.0 1 10/08/18 17:20 10/09/18 11:35 14797-55-8
Nitrogen, Nitrite 2.1 mg/kg 0.99 1 10/08/18 17:20 10/09/18 11:35 14797-65-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/15/2018 09:36 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: SLUDGE
Pace Project No.: 92401901
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: WW PLANT SLUDGE Lab ID: 92401901004 Collected: 10/01/18 14:51 Received: 10/03/18 13:40 Matrix: Solid
Results reported on a "wet -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540G Total Percent Solids
Total Solids
1010 Flash point,Closed Cup
Flashpoint
350.1 Ammonia
Nitrogen, Ammonia
365.1 Phosphorus, Total
Phosphorus
Date: 10/15/2018 09:36 AM
Analytical Method: SM 2540G-2011
5.0 % 0.000010 1 10/04/1814:33
Analytical Method: EPA 1010A
>200 deg F 70.0 1 10/07/18 13:56
Analytical Method: EPA 350.1 Rev 2.0 1993 Mod. Preparation Method: EPA 350.1 Rev 2.0 1993 Mod.
209 mg/kg 10.0 1 10/08/18 08:40 10/08/18 14:31 7664-41-7
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
829 mg/kg 18.5 10 10/05/18 21:34 10/05/18 23:35 7723-14-0 M6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 23

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Facility Elizabeth City WWTP
FIELD LOADING ESTIMATES
Sampling Date 12/3/2018
% Solids 4.9
Mineralization Rate 0.3
Gallons per DT 4,894.04
PH 12.24
Sodium Absorpotion 1.58 <5.0 Safe 5.0 - 10.0 Careful Management >15.0 Do Not Land Apply
Ratio
NITROGEN APPLICATION
TKN (mg/Kg) 35,800 lbs./1,000 gal 14.63
Ammonia Nitrogen (mg/Kg) 718.00 lbs./1,000 gal 0.29
Nitrate -Nitrite (mg/Kg) 42.20 lbs./1,000 gal 0.02
PLANT AVAILABLE NITROGEN SURFACE APPLIED
PAN (mg/Kg) 10,926 lbs./1,000 gal 4.46
PLANT AVAILABLE NITROGEN INJECTED/INCORPORATED APPLIED
PAN (mg/Kg) 11,285 lbs./1,000 gal 4.61
Volatization Rate= 0.5 Surface Application
1.0 Injection/ Incorporation
EPA METAL LIMITS
Class A Ceiling
Class B Ceiling
Limits (mg/Kg)
Limits (mg/Kg)
41
75
39
85
1,500
4,300
300
840
17
57
420
420
100
100
2,800
7,500
1st Year
2nd Year
3rd Year
4th Year
5th Year
NUTRIENT APPLICATION
Potassium lbs./1,000 gal 3.49
Phosphorus lbs./1,000 gal 5.31
Calcium lbs./1,000 gal 41.27
Magnesium lbs./1,000 gal 1.59
Manganese lbs./1,000 gal
Sulfur lbs./1,000 gal
Molybdenum lbs./1,000 gal 0.00
HEAVY METAL CONCENTRATION HEAVY METAL LOADING
Arsenic (mg/Ig)
17.10
Arsenic lbs./1,000 gal
0.01
Cadmium (mg/Kg)
1.70
Cadmium lbs./1,000 gal
0.00
Copper (mg/Ig)
130.00
Copper lbs./1,000 gal
0.05
Lead (mg/Ig)
9.20
Lead lbs./1,000 gal
0.00
Mercury (mg/Kg)
0.24
Mercury lbs./1,000 gal
0.00
Nickel (mg/Kg)
8.50
Nickel lbs./1,000 gal
0.00
Selenium (mg/Kg)
17.10
Selenium lbs./1,000 gal
0.01
Zinc (mg/Kg)
382.00
Zinc lbs./1,000 gal
0.16
RESIDUAL NITROGEN CALCULATION
24,874
Total 17,329 34.66
Total 17,596 35.19
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)
Surface Application
Injection/Incorporation Application
Remaining
Remaining
Organic
Organic
PAN PAN
Nitrogen
PAN PAN
Nitrogen
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
TKN
(mg/kg) (lbs/DT)
(mg/Kg)
35,800
10,926 21.85
24,874
35,800
11,285 22.57
24,515
24,874
3,731 7.46
21,143
24,515
3,677 7.35
20,838
21,143
1,586 3.17
19,557
20,838
1,563 3.13
19,275
19,557
733 1.47
18,824
19,275
723 1.45
18,552
18,824
353 0.71
18,471
18,552
348 0.70
18,204
Total 17,329 34.66
Total 17,596 35.19
Equations
1st Yr. PAN (mg/Kg)=(MR x (TKN-NH3))+(VR x NH3)+NOx
2nd Yr PAN (mg/Kg)= 2nd Yr. TKN x (MR/2)
3rd Yr PAN (mg/Kg)= 3rd Yr. TKN x (MR/4)
4th Yr PAN (mg/Kg)= 4th Yr. TKN x (MR/8)
5th Yr PAN (mg/Kg)= 5th Yr. TKN x (MR/16)

aceAnalytical
-pacelabs.com
ANALYTICAL RESULTS
Project: Residuals Quarterly WWTP
Pace Project No.: 92409272
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Residuals/Quarterly Lab ID: 92409272001 Collected: 12/03/18 14:00 Received: 12/04/18 10:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
7471 Mercury
Mercury
2540G Total Percent Solids
Total Solids
Percent Moisture
Percent Moisture
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3
Nitrogen, NO2 plus NO3
Nitrogen, Nitrate
Nitrogen, Nitrite
365.1 Phosphorus, Total
Phosphorus
4500 Chloride in Soil
Chloride
9056 IC Anions
Sulfate
Date: 12/18/2018 02:54 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
7510
mg/kg
171
1
12/12/1811:42
12/13/1810:21
7429-90-5
ND
mg/kg
17.1
1
12/12/1811:42
12/13/1810:21
7440-38-2
ND
mg/kg
1.7
1
12/12/1811:42
12/13/1810:21
7440-43-9
101000
mg/kg
171
1
12/12/1811:42
12/13/1810:21
7440-70-2
12.4
mg/kg
8.5
1
12/12/1811:42
12/13/1810:21
7440-47-3
130
mg/kg
8.5
1
12/12/1811:42
12/13/1810:21
7440-50-8
9.2
mg/kg
8.5
1
12/12/1811:42
12/13/1810:21
7439-92-1
3890
mg/kg
171
1
12/12/1811:42
12/13/1810:21
7439-95-4
ND
mg/kg
8.5
1
12/12/1811:42
12/13/1810:21
7439-98-7
ND
mg/kg
8.5
1
12/12/1811:42
12/13/1810:21
7440-02-0
ND
mg/kg
8530
1
12/12/1811:42
12/13/1810:21
7440-09-7
ND
mg/kg
17.1
1
12/12/1811:42
12/13/1810:21
7782-49-2
ND
mg/kg
8530
1
12/12/1811:42
12/13/1810:21
7440-23-5
382
mg/kg
17.1
1
12/12/1811:42
12/13/1810:21
7440-66-6
Analytical Method: EPA 7471 B Preparation Method:
EPA 7471 B
0.24
mg/kg
0.088
1
12/05/1818:42
12/06/1814:18
7439-97-6
Analytical Method:
SM 254OG-2011
4.9
% 0.000010
1
12/05/1816:32
Analytical Method: ASTM D2974-87
95.1
%
0.10
1
12/05/1816:25
Analytical Method:
EPA 350.1 Rev 2.0 1993 Mod.
Preparation Method:
EPA 350.1 Rev 2.0 1993 Mod.
718
mg/kg
201
1
12/11/1816:21
12/12/1814:44
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation
Method: EPA 351.2 Rev 2.0 1993
35800
mg/kg
1640
2
12/06/18 01:26
12/07/18 06:34
7727-37-9
Analytical Method:
EPA 353.2 Rev 2.0 1993 Preparation
Method: EPA 353.2 Rev 2.0 1993
42.2
mg/kg
40.8
1
12/05/18 23:04
12/06/18 00:38
H1,M1
ND
mg/kg
40.8
1
12/05/18 23:04
12/06/18 00:38
14797-55-8
H1
38.6
mg/kg
20.4
1
12/05/18 23:04
12/06/18 00:38
14797-65-0
H1,M1
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation
Method: EPA 365.1 Rev 2.0 1993
13000
mg/kg
394
10
12/06/18 16:20
12/06/18 22:05
7723-14-0
Analytical Method:
SM 4500 -CI -E-2011
Preparation
Method: SM 4500 -CI -E-2011
5220
mg/kg
203
1
12/17/18 07:19
12/17/18 11:20
16887-00-6
Analytical Method: EPA 9056A Preparation Method:
EPA 9056A
ND
mg/kg
1020
1
12/10/1815:16
12/11/1810:50
14808-79-8
M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 19

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aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Project: TCLP Sludge WWTP
Pace Project No.: 92407539
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: Sludge Lab ID: 92407539001 Collected: 11/15/18 00:00 Received: 11/15/18 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8081 TCLP Pesticides RVE
gamma -BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
8151 Chlorinate Herbicide TCLP
2,4-D
2,4,5 -TP (Silvex)
Surrogates
2,4-DCAA (S)
PCB -1016 (Aroclor 1016)
PCB -1221 (Aroclor 1221)
PCB -1232 (Aroclor 1232)
PCB -1242 (Aroclor 1242)
PCB -1248 (Aroclor 1248)
PCB -1254 (Aroclor 1254)
PCB -1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
Date: 12/05/2018 10:20 AM
Analytical Method: EPA 8081 B Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 11/21/18 12:27
ND
ug/L
0.50
1
11/26/18 09:36
11/29/18 15:57
58-89-9
ND
ug/L
3.0
1
11/26/18 09:36
11/29/18 15:57
57-74-9
ND
ug/L
0.50
1
11/26/18 09:36
11/29/18 15:57
72-20-8
ND
ug/L
0.50
1
11/26/18 09:36
11/29/18 15:57
76-44-8
ND
ug/L
0.50
1
11/26/18 09:36
11/29/18 15:57
1024-57-3
ND
ug/L
1000
1
11/26/18 09:36
11/29/18 15:57
72-43-5
ND
ug/L
3.0
1
11/26/18 09:36
11/29/18 15:57
8001-35-2
64
%
10-138
1
11/26/18 09:36
11/29/18 15:57
2051-24-3
55
%
10-110
1
11/26/18 09:36
11/29/18 15:57
877-09-8
Analytical Method: EPA 8151 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 11/21/18 16:08 Initial pH: 10; Final pH: 4
ND mg/L 0.010 1 11/26/1816:40 11/28/1810:11 94-75-7
ND mg/L 0.010 1 11/26/1816:40 11/28/1810:11 93-72-1
105 % 39-139 1 11/26/1816:40 11/28/1810:11 19719-28-9
Analytical Method: EPA 8082A Preparation Method: EPA 3510C
Leachate Method/Date: EPA 1311; 11/21/18 12:27
M1
M1
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
12674-11-2 M1
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
11104-28-2
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
11141-16-5
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
53469-21-9
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
12672-29-6
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
11097-69-1
ND
ug/L
1000
1
11/26/18 09:37
11/26/18 17:52
11096-82-5 M1
7
%
10-132
1
11/26/18 09:37
11/26/18 17:52
2051-24-3 S2
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 11/26/18 21:57 Initial pH: 11.19; Final pH: 4.5
ND
mg/L
0.050
1
11/27/18 20:35
11/29/18 06:20
7440-38-2
ND
mg/L
0.25
1
11/27/18 20:35
11/29/18 06:20
7440-39-3
ND
mg/L
0.0050
1
11/27/18 20:35
11/29/18 06:20
7440-43-9
ND
mg/L
0.050
1
11/27/18 20:35
11/29/18 06:20
7440-47-3
ND
mg/L
0.025
1
11/27/18 20:35
11/29/18 06:20
7439-92-1
ND
mg/L
0.10
1
11/27/18 20:35
11/29/18 06:20
7782-49-2
ND
mg/L
0.025
1
11/27/18 20:35
11/29/18 06:20
7440-22-4
Analytical Method:
EPA 7470A
Preparation Method:
EPA 7470A
Leachate Method/Date: EPA 1311; 11/26/18 21:57
Initial
pH: 11.19; Final pH: 4.5
ND
mg/L
0.00020
1
11/27/18 22:46
11/28/18 11:56
7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 25

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TCLP Sludge WWTP
Pace Project No.: 92407539
Sample: Sludge
Lab ID: 92407539001 Collected:
11/15/18 00:00
Received: 11/15/18 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV TCLP Sep Funnel
Analytical Method:
EPA 8270D Preparation
Method:
EPA 3510C
Leachate Method/Date:
EPA 1311; 11/21/18 12:27
1,4 -Dichlorobenzene
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
106-46-7
2,4-Dinitrotoluene
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
121-14-2
Hexachloro-1,3-butadiene
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
87-68-3
Hexachlorobenzene
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
118-74-1
Hexachloroethane
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
67-72-1
2-Methylphenol(o-Cresol)
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
95-48-7
3&4 -Methyl phenol (m&p Cresol)
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
15831-10-4
Nitrobenzene
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
98-95-3
Pentachlorophenol
ND
ug/L
1000
10
11/20/18 10:44
11/20/18 20:32
87-86-5
Pyridine
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
110-86-1
2,4,5 -Trichlorophenol
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
95-95-4
2,4,6 -Trichlorophenol
ND
ug/L
500
10
11/20/18 10:44
11/20/18 20:32
88-06-2
Surrogates
Nitrobenzene -d5 (S)
0
%
12-102
10
11/20/18 10:44
11/20/18 20:32
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
13-107
10
11/20/18 10:44
11/20/18 20:32
321-60-8
S4
Terphenyl-d14 (S)
0
%
21-132
10
11/20/18 10:44
11/20/18 20:32
1718-51-0
S4
Phenol -d6 (S)
0
%
10-110
10
11/20/18 10:44
11/20/18 20:32
13127-88-3
S4
2-Fluorophenol (S)
0
%
10-110
10
11/20/18 10:44
11/20/18 20:32
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-108
10
11/20/18 10:44
11/20/18 20:32
118-79-6
S4
8260 MSV TCLP
Analytical Method: EPA 8260B Leachate
Method/Date:
EPA 1311; 11/28/18 08:35
Benzene
ND
ug/L
100
20
12/03/1812:34
71-43-2
M1
2-Butanone (MEK)
ND
ug/L
200
20
12/03/18 12:34
78-93-3
Carbon tetrachloride
ND
ug/L
100
20
12/03/18 12:34
56-23-5
M1
Chlorobenzene
ND
ug/L
100
20
12/03/1812:34
108-90-7
M1
Chloroform
ND
ug/L
100
20
12/03/1812:34
67-66-3
M1
1,4 -Dichlorobenzene
ND
ug/L
100
20
12/03/1812:34
106-46-7
M1
1,2-Dichloroethane
ND
ug/L
100
20
12/03/1812:34
107-06-2
M1
1,1-Dichloroethene
ND
ug/L
100
20
12/03/1812:34
75-35-4
M1
Tetrachloroethene
ND
ug/L
100
20
12/03/1812:34
127-18-4
M1
Trichloroethene
ND
ug/L
100
20
12/03/1812:34
79-01-6
Vinyl chloride
ND
ug/L
100
20
12/03/18 12:34
75-01-4
M1
Surrogates
1,2-Dichloroethane-d4 (S)
103
%
70-130
20
12/03/18 12:34
17060-07-0
Toluene -d8 (S)
107
%
67-135
20
12/03/18 12:34
2037-26-5
4-Bromofluorobenzene (S)
99
%
70-130
20
12/03/18 12:34
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
93.1
%
0.10
1
12/04/18 11:36
1010 Flash poi nt,Closed Cup
Analytical Method: EPA 1010
Flashpoint
>200
deg F
60.0
1
11/19/18 19:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 25

aceAnalytical
—pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: TCLP Sludge WWTP
Pace Project No.: 92407539
Sample: Sludge Lab ID: 92407539001 Collected: 11/15/18 00:00 Received: 11/15/18 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
9045 pH Soil Analytical Method: EPA 9045C
pH in water at 25 degrees C 12.1 Std. Units 2.0 1 11/16/18 22:24 H3
733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW -846 7.3.3.2
Cyanide, Reactive ND mg/kg 14.5 1 11/20/18 00:19 11/20/18 18:33
734S Reactive Sulfide Analytical Method: SM4500S2F-00 Preparation Method: SW -846 7.3.4.2
Sulfide, Reactive ND mg/kg 145 1 11/20/18 00:19 11/20/18 00:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/05/2018 10:20 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 25

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Page 25 of 25

City of Elizabeth City
2018 Class B Annual Report
WQ Permit# WQ0002883
Pathogen & Vector Attraction Reduction Form
Elizabeth City WWTP
Lime Stabilization Records

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWTP NPDES Number: NCO025011
Monitoring Period: 01 /01 /2018 to 03/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry
Weight) 0 0 Continuous Grab Samples
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T.1107): Alt. 6 (Alk. Stabilization)
0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
F1 requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Rebecca Miller, WWTP Superintendent
Preparer Name and Title (type or print)
Signature of Preparer*
J. Bryan Smith, President
Land Applier Name and Title (if applicable)(type or print)
3-5-19
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 26, 2019

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWTP NPDES Number: NC0025011
Monitoring Period: 04/01/2018 to 06/30/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to altemative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T.1107): Alt. 6 (Alk. Stabilization)
Q "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Rebecca Miller, WWTP Superintendent
Preparer Name and Title (type or print)
-A, & - 05 k
Signature of Preparer*
J. Bryan Smith, President
Land A plier Name and Title (if applicable)(type or print)
3-5-19
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 26, 2019

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWT13 NPDES Number: NC0025011
Monitoring Period: 07/01/2018 to 09/30/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry 0 0 Continuous Grab Samples
Weight)
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T.1107): Alt. 6 (Alk. Stabilization)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Rebecca Miller, WWTP Superintendent
Preparer Name and Title (type or print)
4W AN 1',r O5l'1/� f
Signature of Preparer*
J. Bryan Smith, President
Land Applier Name and Title (if applicable)(type or print)
r/d�OWNC-XL 3-5-19
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 26, 2019

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Elizabeth City WQ Permit Number: WQ0002883
WWTP Name: Elizabeth City WWTP NPDES Number: NCO025011
Monitoring Period: 10/01 /2018 to 12/31/2018
Pathogen Reduction (15A NCAC 02T .1106) - Please Indicate level achieved and alternative performed:
"Class A" Alternative: Not Applicable
If applicable to alternative performed ("Class A" only) indicate "Process to Further Reduce Pathogens": Not Applicable
"Class B" Alternative: Alternative 2
If applicable to alternative performed ("Class B" only) indicate "Process to Further Reduce Pathogens": Lime Stablization
Fecal Coliform Minimum Geo. Mean Maximum # of Exceedences Frequency Sample Type
Colonies Per Gram of
Total Solids(Dry Grab ab Sam les
Weight) 0 o P
Analytical Technique
Vector Attraction Reduction Performed (15A NCAC 02T.1107): Alt. 6 (Alk. Stabilization)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction
requirement in 15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction
F1 requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why
you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment."
Rebecca Miller, WWTP Superintendent
Preparer Name and Title (type or print)
I At"
44" 0/',vI �
Signature of Preparer*
J. Bryan Smith, President
Land Applier Name and Title (if applicable)(type or print)
3-5-19
Date Signature of Land Applier (if applicable Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Tuesday, February 26, 2019

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