WQ0021826_Residual Annual Report 2018_20190313

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0021826
SUBMITTAL DATED: 2/26/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0021826
Permittee *
Facility Name *
City of Roxboro
City of Roxboro
Phone Number*
4434899086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
City of Roxboro NC 2018 Annual Report.pdf 9AMB
Upload only 1 RDF docurrent. IVLltiple documents must be corrbined into one RDF file.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/26/2019

435 Williams Court, Suite 100
Baltimore, MD 21220
wwNusynagro.co«
FEBRUARY 22, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0021826
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Roxboro, NC.
If you have any questions or need additional information, please do not hesitate to contact
Thomas Warren at [phone] ext. 22 or Nate Roth at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Thomas Warren, City of Roxboro
Nate Roth, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF ROXBORO3 NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0021826
2018 ANNUAL REPORT

City of Roxboro, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQPermit #: WO0021826 County Person Year 2018
Facility Name (as shown on permit) City of Roxboro W WTP & WTP NPDES No. NC0021024
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Annlication Summazv:
Total
number
of appliea6on fields
in the permit: 16
Total
number
of fields utilized for
land application during the year: 1
Total
amount
of dry tons applied during the year for all application sites: 135.03
Total
number
of acres utilized for
land application during the year: 23_30
PatY B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken,
I.
Part C —Cert
Only residuals approved for this permit were applied to the permitted sites.
2.
Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pFI of at least 6.0 or the
limit specified in the permit.
3.
Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4.
Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5.
All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6.
The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T. I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7.
All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8.
All monitoring and reporting requirements in 15A NCAC 02T. I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9.
All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10.
No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11.
Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12.
No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13.
All buffer requirements as specified on the permit were maintained during each application of residuals.
ification:
"1 cert
ify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware Yhat there u'e significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Thomas S. Warren, Assistant Citv Man
aeer
Permittee Name and Title (type or print)
Com=, t�--
Signature ofPreparer* Date
(if different from Permittee)
Signature of Permittee - Date
ao ,ce
Sign - 'e ppl'' Date
(if different frot ermr tee and P arer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY - LAND APPLICATION IN NC
ROXBORO,NC
ROXBORO, NC WWTP/WTP MIX
DRY METRIC
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT TONS
October 2018 240.00 Y 135.03 D 122.47
YEARLY TOTAL 240.00 Y 135.03 D 122.47
1 /28/2019

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Wa aint
y ANALYTICAL
7flfllyF:l
Synagro Central LLC/ Roxboro
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 18-240-0206
Project Description: Roxboro
7621 Whttepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www,waypointa n alytica I. com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received samples) on 8/28/2018 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Pw�• a• rm-!'
Pauric McGroary
Agronomist
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Arizona AZOfi29 New Jersey VA031 Pennsylvania 68-03109 Virginia 4fi0014
Florida E871087 North Carolina 257 South Carolina 93007
?:
Page 1 of 6

Waypoi nt.. 7621 Whitepfne Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-240-0206
Client Project Description: Roxboro
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62499
62499
62499
62499
62499
62499
62499
62499
Roxboro WWiP Drying Bed
Roxboro WWiP Drying Bed
Roxboro WWiP Drying Bed
Roxboro WWiP Drying Bed
Roxboro WWTP Drying Bed
Roxboro WWiP Drying Bed
Roxboro WWiP Drying Bed
Roxboro WWiP Drying Bed
Solids
Solids
Solids
Solids
Solids
Solids
Solids
Solids
WTN: Waypoint.Analytical - TN, Memphis, TN, Certification: #1354
08/27/2018
10;45
08/28/2018
08/27/2018
10:45
08/28/2018
D8/27/2018
10:46
08/28/2018
08/27/2018
10:45
08/28/2018
08/27/2018
10:45
08/28/2016
08/27/2018
10:45
08/28/2018
08/27/2018
10:46
08/28/2018
08/27/2018
10;45
08/28/2018
Page 2 of 6
SM-4500-NH3C
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WiN
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WiN
SW -74716
WTN
SM-4500-NH3C-TKN
WTN
SM -2640G
WTN

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Waypoint..®
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 °Fax [phone]
www.waypointa nalytica Isom
Cooler Receipt Form
Customer Number: 46487
Customer Name: Synagro Central LLCI Roxboro
Report Number: 18-240-0206
Shipping Method
Fed Ex a US Postal � Lab � Other
UPS 0 Client � Courier Thermometer ID:
Shipping container/cooler uncompromised? � Yes � No
Number of coolers received I '
Custody seals intact on shipping container/cooler? � Yes � No � Not Required
Custody seals intact on sample bottles? � Yes Q No � Not Required
Chain of Custody (COC) present? � Yes � No
COC agrees with sample label(s)? � Yes � No
GOC properly completed � Yes � No
Samples in proper containers? � Yes � No
Sample containers intact? � Yes 0 No
Sufficient sample volume for indicated test(s)? � Yes � No
All samples received within holding time? � Yes � No
Cooler temperature in compliance? � Yes � No
Cocler/Samples arrived at the laboratory on ice. � Yes � No
Samples were considered acceptable as cooling
process had begun.
Water -Sample containers properly preserved � Yes � No � N/A
Water -VOA vials free of headspace � Yes � Nc � N/A
Trip Blanks received with VOAs � Yes � No � N/A
Soil VOA method 5035 —compliance criteria met � Yes � No � N/A
High concentration container (48 hr) � Low concentration Encore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) � Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? � Yes � No
Comments:
Signature: Brandi Watson � Date &Time: 108/28/2018 12 7 54 7 �
.Page 5 of 6

, o E) :

Sodium Absorption Ratio Calculation (SAR)
Product Code
Product Name
Sample Date Report Range Ratio
2102 -01 -MIX -NC
ROXBORO, NC WWTP/WTP MIX
8/27/2018 1/1/2018-12/31/2018 0.6795
Na mg/I = (Na
mg/kg x % Solids) + 100 =
(250 x 66.8000) +
100 = 167
Ca mg/1= (Ca
mg/kg x % Solids) + 100 =
(2470 x 66.8000)
+ 100 = 1649.96
Mg mg/I = (mg
mg/kg x % Solids) + 100
= (2620 x 66.8000)
+ 100 = 1750.16
Na meq = Na mg/I + Molec.Wgt.Na = 167 = 23 = 7.26087
Ca meq = Ca mg/I + Molec.Wgt.Ca = 1649.96 + 20 = 82.498
Mg meq = Mg mg/I + Molec.Wgt.Mg = 1750.16 + 12 = 145.847
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 7.26087 = SgrRoot[0.5(82.498+145.847)] = 0.679529
Printed: 2/6/2019
Page 1 09:35

SECTION 3

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SECTION 4

TINUIWMITI,
Analytical Laboratories
September 19, 2018
Clay Fisackerly
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Roxboro WWTP
Summit Environmenlal Technologies, Inc.
3310 win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX [phone]
1e bsue: htto://em .settekeom
Dear Clay Fisackerly: Order No.: 18081870
Summit Environmental Technologies, Inc. received 1 sample(s) on 8/31/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report
unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you haue any questions regarding these tests results, please feel flee to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win 5t.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, Cam mia 07256CA, Colorado, Connecticut PH -0108, Delawaz'e, Florida NELAC 1187688, Gem'gia ER7688, Idaho OH00923, Rlineis
200061, Indiana C -OH -13, Kan
sas E-10347, Kentucky (Dnderg�.'ound Stm'age Tank) 3, ICenNcky 90146, Louisiana 04061, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OHOOb,. New York l 1777, North Carolina 39705 and 637, NorUn Dakota R-201, Oklahoma 9940, Oregon
11200001, Rhode Island I,A000317, South Carolina 92016001, Texas T104704466-11-5, Utah 011009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 27
Page 1 of 28

SUMMIT
S°"""`Environmental Technologies, bac.ffl 3310 Win St. Case Narrative
ENVIRONMENTAL TECNN0LGG1rr, WC Cuyahoga Falls, Ohio 44223 WOM 18081870
Analytical Laboratories TEL: [phone] FAX [phone]
Website: huo llw w.settekco n Date: 9/19/2018
CLIENT: 5ynagro
Project: Roxboro WWTP
WorkOrder Narrative:
18081870: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary, All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples
are reported
on
an
"as received" or
"wet weight" basis unless indicated as
"dry weight" using the "-dry"
designation
on
the
reporting units.
This report is
believed to meet all of the requirements of the
accrediting agency,
where applicable. Any
comments or
problems with the analytical events associated
with this report are
noted below.
Prep Sample Comments:
18081870-OOlA 402482: Prep Comments for MtlPrep_TCLP(3010A), Sample 18081870-OOlA: TCLP
was filtered after digestion.
18081870-001A 403198: Prep Comments for SVPrep_BNATot_TCLP(3510), Sample 18081870-
001A: Sample is a soapy solution, Matrix caused excessive emulsion to form
18081870-OOIA 403773: Prep Comments for SVPrep_CPest TCLP(3510), Sample 18081870-OOIA:
Sample is a soapy solution, Matrix caused excessive emulsion to form
Analytical Sequence Sample Notes:
18081870-OOlA SVOC-BNA TCLP(8270D): Possible low bias for Pyridine due. to low recovery in the
Original
Page 2 of 27
Page 2 of 28

YOU M1 T s n„»uE"vlron,neatatTeanuomWin t. Case Narrative
33700Win St.
ENVIRONMENTAL MCHN01 OGIFS� INC Cuyahoga Falls, Ohio 44223 WO#: 18081870
Annlyf7caf La6aratorKes TEL: [phone] FAX [phone]
Website: htto:/lw .settekcom Date: 9/19/2018
CLIENT: Synagro
Project: Roxboro WWTP
CCV.
18081870-001A SVOG-BNA_TCLP(8270D): The CCV (Batch R88817) exhibited high recoveries for
2,4,5 -Trichlorophenol, 2-Methylphenol, Hexachloroethane, Pentachlorophenol. The associated samples
are ND for 2,4,5 -Trichlorophenol, 2-Methylphenol, Hexachloroethane, Pentachlorophenol.
18081870-OOIA SVOC-BNA_TCLP(8270D): The sample exhibited low recovery for Surrogate:
Phenol -db. All other Surrogates are within the acceptance limits.
Analytical Sequence QC Notes:
18081870-OOIAMS TCLP-SVOC-HERB_TCLP(8i51): Spike recovery indicates matrix interference.
The method is in control as indicated by the laboratory control sample (LCS).
18081870-OOIAMSD TCLP-SVOC-HERB_TCLP(8151): High RPD due to suspected sample
inhomogeneity.
18081870-OOIAMSD TCLP-SVOC-HERB TCLP(8151): Spike recovery indicates matrix interference.
The method is in control as indicated by the laboratory control sample (LCS).
Original
Page 3 of 27
Page 3 of 28

UMM1ll Summit Environmental Technologies, lit Qualifiers and Acronyms
3310 Win 3
ENVIIIONIdENTAL TEGuN01,0r1FS, INC Cuyahoga Falls, Ohio 4422 WO#: 18081870
ArralpUcal Laboratories TEL: [phone] FAX' (330) 253-446
Website: h tv:11w .senek.co. Date: 9/19/2018
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Nates in the Case Narrative for any Qualifiers
The compound was analyzed for but was not detected.
7
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded. Not 47CFR32 compliant.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
In
Manual integration was used to determine the area response.
it
Manual integration in which peak was deleted
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GC/MS.
X
The result was not confirmed when GC/MS Analysis was performed..
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCS contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low O or high (+).
S
The spike result was outside of accepted recovery limits.
W
Sampleswere received outside temperature limits (00 — 6° C). Not 47CSR32 compliant for W.V.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quantitation Limit
ICS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike Duplicate MCL Maximum Contamination Limit
RPD
Relative. Percent Different MinCL Minimum Compound Limit
1CV
Initial Calibration Verification RA Reanalysis
1CB
Initial Calibration Blank RE Reexnaction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCB
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 27
Page 4 of 28

NUMMI, Summit EnvironmentalTec)nolagies,b2c. Workorder
3310 Win St.
ENVIRONhIENTAL TECM01.oeir-S, iryr Cuyahoga Falls, Ohio 44223 Sample Summary
Ana?y(lcai taboralorlog TEL: [phone] FAX [phone] WOM 18081870
Website: htto://w settek.com 19-Sep4i?
CLIENT: Synagro
Project: Roxboro WWTP
Lab SamplelD Client Sample ID Tag No
18081870-001 Roxboro WWTP
Date Collected
8/29/2018 1:00:00 PM
Date Received Matrix
/2018 1 0:00:00 AM Sludge
Page 5 of 27
Page 5 of 28

\
2
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es,
N U I _ sa n nilEnvhnnmenta7Teelmul10 Win Sl. St.
3310 Win Analytical Report
En
ENVIt10NFALWAL rZcflNOI. crier, INC Cuyahoga Falls, Ohio 44223 (base report)
Anafyticat Laboratories TEL: [phone] FAX.. [phone] WO#: 18081870
Website: huy.-Ilwww.settekcom Date Reported: 9/19/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/29/2018 1:00:00 PM
Lab ID: 18081870-OOIA
Project: Roxboro WWTP
Client Sample ID Roxboro W WTP
Analyses Result RL Quad Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury ND 0.00500 mg/L 1 917/2018 3:49:00 PM
TCLP METALS., VOC, BNA, PEST, HERB -SOLID SW6010D SW3010A Analyst: KMO
TCLP METALS ANALYSIS (SW131116010)
TCLP Arsenic(As) ND 2.50 mg/L 1 9/10/2018 12:26:22 PM
TCLP Barmm(Ba) ND 25.0 mg/L 1 9/7/2018 6:08:37 PM
TCLP Cadmium(Cd) ND 0.500 mg/L 1 9/7/2018 6:08:37 PM
TCLP Chromium(Cr) ND 1,00 mg/L 1 917/2018 6:08:37 PM
TCLP Lead(Pb) ND 2.50 mg/L 1 9/7/2018 6:08:37 PM
TCLP Selenium(Se) ND 0.250 mg/L 1 9/101201812:26:22 PM
TCLP Silver(Ag) ND 2.50 mg/L 1 9/10/2018 12:26:22 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW3510C Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270)
1,4 -Dichlorobenzene ND 0.0800 mg/L 2 9/14/2018 5:42:00 PM
2,4,5 -Trichlorophenol ND 0.200 QC+ mg/L 2 9/14/2018 5:42:00 PM
2,4,6 -Trichlorophenol ND 0200 mg/L 2 9/14/2018 5:42:00 PM
2,4-Dinitrotoluene ND 0.0400 mg/L 2 9/14/2018 5:42:00 PM
o -Cresol ND 0.200 QC+ mg/L 2 9/14/2018 5:42:00 PM
m/p-Cresol(s) ND 0.200 mg/L 2 9/14/2018 5:42:00 PM
Cresols, Total ND 4.00 mg/L 2 9/14/2018 5:42:00 PM
Hexachloro-1,3-butadiene ND 0.0160 mg/L 2 9/14/2018 5:42:00 PM
Hexachlorobenzene ND 0.0400 mg/L 2 9/14/2018 5:42:00 PM
Hexachloroethane ND 0.0800 QC+ mg/L 2 9/14/20185:42:00 PM
Nitrobenzene ND 0.0800 mg/L 2 9/14/2018 5:42:00 PM
Pentachlorophenol ND 0.200 QC+ mg/L 2 9/14/2018 5:42:00 PM
Pyridine ND 0.200 QC- mg/L 2 9/14/2018 5:42:00 PM
Surr: 2-Fluorophenol 12.6 10-109 %Rec 2 9/1412018.5:42:00 PM
Surr. Phenol -d6 8.08 10 - 109 S %Rec 2 9/14/2018 5:42:00 PM
Surr: Nitrobenzene -d5 37.4 19 - 120 %Rec 2 9/14/2018 5:42:00 PM
Sour: 2,4,6-Tribromophenol 37.0 10 - 120 %Rec 2 9/14/2018 5:42:00 PM
Surr: 2-Fluorobiphenyl 52.7 22 - 117 %Rec 2 9/14/2018 5:42:00 PM
Qualifiers: Value exceeds Maximum Contaminant Level. E Value above quantitation range
H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit. N Tentatively identified compounds
ND Not Detected O RSD is greater than RSDlimit
P Second colmim continuation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 7 of 28

R1SUMMIT SammltEnvbomnentalTechnoWinSt. Analytical Report
331010Win St.
ENVII14NhtENTAL rECON01GGIES, !Nr. Cuyahoga Falls, Ohio 44223 (basereport)
Analytical Laboratories TEL: [phone] FAX... [phone] wok 18081870
Website: htm.'11www.se9,&com Date Reported: 9/19/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/29/2018 1:00:00 PM
Lab ID: 18081870-OOIA
Project: Roxboro WWTP
Client Sample ID Roxboro W WTP
Analyses
Result
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270)
RL Qusl
Units
DF Date
Analyzed
SW3510C Analyst: RIS
SW8270D
SW3510C
Analyst: BJH
Surr: p-Terphenyl-d14 89.2 34 - 116 %Rec 2 9/14/2018 5:42:00 PM
NOTES:
Possible low bias for Pyridine due to low recovery in the CCV.
The CCV (Batch R88817) exhibited high recoveries for 2,4,5 -Trichlorophenol, 2-Methylphenol, Hexachloroethane, Pentachlorophenol. The
associated samples are ND for 2,4,5 -Trichlorophenol, 2-Methylphenol, Hexachloroethane, Pentachlorophenol.
The sample exhibited low recovery for Surrogate: Phenol -d6. All other Surrogates are within the acceptance limits.
TCLP METALS, VOC,
BNA, PEST, HERB -SOLID
0,500
SW8081
SW3510C Analyst: RIS
TCLP PESTICIDES ANALYSIS (SW93't9/8081)
2,4,5 -TP
ND
0.500
mg/L
10
9/13/20187:21:00 PM
Surr: DCAA
Chlordane, total
ND
0.0200
mg/L
10
9/14/2018 9:17:00
HERB -SOLID
PM
Toxaphene
ND
0.400
mg/L
10
9/14/2018 9:17:00
1,1-Dichloroethene
PM
Endrin
ND
0.00400
mg/L
10
9/14/20189:17:00
0.250
mg/L
PM
gamma -BHC
ND
0.00400
mg/L
10
9/14/2018 9:17:00
9/7/2018 6:24:00 PM
Benzene
PM
Heptachlor
ND
0.00400
mg/L
10
9/14/2018 9:17:00
0.250
mg/L
PM
Heptachlor epoxide
ND
0.00400
mg/L
10
9/14/2018 9:17:00
PM
Methoxychlor
ND
0.00400
mg/L
10
9/14/20189:17:00
PM
Surr. TCMX
44.2
10-119
%Rec
10
9/14/2018 9:17:00
PM
Surr: DCB
70.4
10-119
%Rec
10
9/14/2018 9:17:00
PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP HERBICIDES ANALYSIS (SW1311/8151)
SW8151A SW8151A Analyst: MES
214-D
Qualifiers: ` Value exceeds Maximum Contaminant
ND
0,500
mg/L
10
9/13/2018 72100 PM
2,4,5 -TP
ND
0.500
mg/L
10
9/13/20187:21:00 PM
Surr: DCAA
74.0
20-140 an
%Rec
10
9/13/2018 7:21:00 PM
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8260B
SWI 311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50
9/7/20186:24:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50
9/7/2018 6:24:00 PM
MEK
ND
1.25
mg/L
50
9/7/2018 6:24:00 PM
Benzene
ND
0250
mg/L
50
9/7/2018 6:24:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50
9[7/2018 6:24:00 PM
Level.
E. Value above quantitation range
H Bolding times forpreparation m -analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
ND Not Detected
P Second column cow nation exceeds
R RPD outside accepted recovery limits
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 8 of 28

SUMMIT SammftEnv;ronmentalTenhnol10WinSt.RI AnalyticalReport
3310 l�'n St.
ENVIRONMENTAL TiCIMMO MS, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratarf2s TEL. [phone] FAX: [phone] WO#: 18081870
Website: htto:/7www.settek.com Date Repotted: 9/19/2018
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 8/29/2018 1:00:00 PM
Lab TD: 1 808 1 970-00 1A
Project: Roxboro WWTP
Client Sample ID Roxboro W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Chlorobenzene
ND
Chloroform
ND
Tetrachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
103.
Surr: Dibromofluoromethane
103
Surr: Toluene -d8
105
RCI -SOLID -W/ IGNITABILITY1030
REACTIVE CYANIDE (9014/7,3.3.2) -SOLID
Cyanide, Reactive ND
RCI -SOLID -W/ IGNITABILITY1030
IGNITABILITY OF SOLIDS (SW -846: 1030)
Ignitability non-flammable
RCISOLI D -W / IGNITABILITY1030
PH (SW9045D)
pH 7.4
RCI
SOLID-W/ IGNITABILITY1030
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
SW82608 SW1311M Analyst: MES
0.250
mg/L
50
9!7/2018 8:24:00
PM
0.250
m9/1-
50
917/2018 6:24:00
PM
0.250
mg/L
50
9/7/2018 6:24:00
PM
0.250
mg/L
50
9/7/2018 6:24:00
PM
0.100
QC+ mg/1.
50
9/712018 6:24:00
PM
70 .130
% Ree
50
9h7/2018 6:24:00
PM
70 .130
% Rae
50
9/7/2018 6:24:00
PM
70 -130
% Rec
50
9/7/2018 6:24:00
PM
SW9014
Analyst:
MS
0.500
mg/Kg
1
9/16/2018 10:00:00
AM
SWI 030
Analyst:
AJT
Qualifiers: `
Value xceeds Maximum Conkaminant Level.
H
Holding tunes far preparation or analysis exceeded
MC
Value is below Minimmn Compound Limit.
ND
Not Detected
P
Second corman confirmation exceeds
R
RPD outside accepted recovery limits
SW9045D
s.u.@20,4C
SW9034
25.0 mg/Kg
1 9/12/2018 2:30:00 PM
Analyst: DHC
1 9/17/2018 11:18:00 AM
Analyst: MS
1 9/16/2018 10:00:00 AM
H Value above quantitation range
M Manual Integration used to detumine area response
N 'fentativety identified compounds
O BSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit
Page 9 of 28

summing- Summit Environmental Technologies, Inc. Accreditation Program
3310 win Analytes Report.
ffI ENVNtON1,1Ci1d7AL racnNoipel=;, iNr, Cuyahoga Falls, Ohio 4422323
AnnlyHcal Laboralorles TEL [phone] FAX• [phone] WOM 18081870
website: into.// w.settekcom 19-Sep-18
Client: Synagro State: NW
Project: Roxboro WWTP Program Name: NC WW SCM
Sample ED Matrix Test Name Analyte Status
18081870-OOIA Sludge
Ignitabillty of Solids (SW -946:1030)
Ignitability
A
Sludge
PH(SW9045D)
Hydrogen Ion (PH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2) -Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides Analysis (SW 1311/8151)
2,455 -TP
A
Sludge
TCLP Herbicides Analysis(SW1311/8151)
2,4-D
A
Sludge
TCLP Herbicides Analysis (SWI 311/8151)
DCAA
A
Sludge
TCLP Mercury Analysis(SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis(SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW 131 t/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW 1311/6010)
Clucmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis(SWI31l/6010)
Silver
A
Sludge
TCLP Pesticides Analysis(SW1311/8081)
2,2'13,3',414'555503656'-
A
Decachlorobiphenyl
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Endrin
A
Sludge
'TCLP Pesticides Analysis (SW1311/808 1)
gamma -BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/808 1)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SWI 311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis(SW1311/8081)
Tetrzchloro-nr-xylene
A
Sludge
TCLP Pesticides Analysis(SW1311/8081)
Toxaphene
A
Sludge
TCLP Somi-Volatiles Analysis (SW1311/8270)
1,4-Diehlorobenzene
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,5 -Trichlorophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2,4,6-Tribromophenol
A
Sludge
TCLP Semi -Volatiles Analysis (SWI 311/8270)
2A&Tdclilorophenol
A
Sludge
TCLP Semi -Volatiles Analysis(SW13 t 1/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi -Volatiles Analysis (SW1311/8270)
2-Fluombiphenyl
A
Sludge
TCLP Semi -Volatiles Analysis(SW1311/8270)
2-Flucrophenol
A
Key
Key
NC -WW -SCM A Accredited
NC -WW -SCM U Unavailable
Page 1 of
Version #2
Page 10 of 28

Summit Environmental Technologies, Inc. Accreditation Program
r T ' S u 'EF.. 3310 i Analytes Report
I � ENVIROWM�NTAL ri-cHNOIAS;lf3, INCINCCuyahoga Falls, Ohio 442234223 y 1)
Anafyflcaf tab6ramr76e TEL: [phone] FAX [phone] WO#: 18081870
Website: htm://www.sellok.com 19 -Sep -18
Client: Synagro State: NW
Project: RoxboroWWTP Program Name: NC -WW -SCM
SamplelD Matrix
Test Name
Analyte
Status
18081870-OOIA Sludge
TCLP Serm-Volatiles Analysis
(SW1311/8270)
2-Mctlrylpbenol
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
3,4-Methylphenol
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Hexachlorobenzebe
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Hexacblorobutadiene
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Hexachloroetbane
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Nitrobenzened5
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Send -Volatiles Analysis
(SW1311/8270)
Phenol -db
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
p-TmphcnyI-d14
A
Sludge
TCLP Semi -Volatiles Analysis
(SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichlorvethme
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
4-Bromofluorobenzene
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Dibromofluoromethane
A
Sludge
TCLP Volatiles Analysis
Tetracbloroetheue
A
Sludge
TCLP Volatiles Analysis
Toluene -d8
A
Sludge_
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
A Accredited
NC_W W_SCM
Key
U Unavailable
Page 2 of 2
Version #2
Page 11 of 28

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SUMM,y Summit Environmental Technologies, Inc.
PI3310 )A'n Si.
(ENVIRONMENTAL ICC14NOI 0GIr3, INC Cuyahoga Falls, Ohio 44223 Sample Log -In Check List
Analytical Laboratories TEL: [phone] FAX' [phone]
Website. httP711ww.settek.com
Client Name: SYN -NC -27028 Work Order Number: 18081870 RcptNo: 1
Logged by: Nick Cleer
Completed By: Christopher Livengood
Reviewed By: Jennifer Wooif
8/31/2018 10:00:00 AM
8/3112018 4:35:27 PM
8/31/2018 4:44:27 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑ No V Not Present ❑
2, How was the sample delivered? UPS
Lon ►n
Sample(s) in proper container(s)?
Yes
0
No
3, Coolers
are present?
Yes VV
No ❑
NA ❑
¢, Shipping container/cooler in good condition? Yes 0 No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present❑
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes V No ❑ NA ❑
5, Were all samples received at a temperature of >0° C to 6.0°C Yes © No ❑ NA ❑
�,
Sample(s) in proper container(s)?
Yes
0
No
❑
Seal Date
8.
Sufficient sample volume for indicated test(s)?
Yes
0
No
❑
g.
Are samples (except VOA and ONG) properly preserved?
Yes
0
No
❑
10.
Was preservative added to bottles?
Yes
❑
No
❑
NA 0
NA
11.
Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
V
No
❑
No VOA Vials ❑�
12,
Were any sample containers received broken?
Yes
❑
No
W
13.
Does paperwork match bottle labels?
Yes
0
No
❑
(Note discrepancies on chain of custody)
14.
Are matrices correctly identified on Chain of Custody?
Yes
©
No
❑
15.
Is it clear what analyses were requested?
Yes
V
No
❑
16.
Were all holding times able to be met?
Yes
V
No
❑
(If no, notify customer for authorization.)
Special Handllnp (if applicable)
17.
Was client notified of all discrepancies with this order?
Yes
❑
No
❑
NA W
Person Notified: Date
By Whom: Via:
❑ rival ❑
Phone ❑
Fax
V In Person
Regarding:
Client Instructions:
18.
Additional remarks:
Cooler Information
Page 27 of 27
Page 28 of 28
Cooler No
Temp °C
Condition
Seal Intact
_ S_eal No
Seal Date
Signed By
h
2.9
Good
Not Present
Page 27 of 27
Page 28 of 28

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxboro WWTP WQ Permit Number: WQ 0021826
WWTP Name: Roxboro WWTP NPDES Number: NC 0021024
Monitoring Period: From 01/01/2018 To 3/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp) Alt 2/B (Alk Treannent) ALt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Claes A only) indicate "Process to Farther Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray GammaRay Pasteurization
I. c� NO Land Application this Period
Parameter
Vector Attraction Reduction (40 CFR 503.33/I5A NCAC 02T.1107) -Please indicate option/alternati
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Excee-
of
Type
Technique
(Drying—Stable)
(Drying—Unstable)
Minimum Geo. Mean Maximum Units
dentes
Analysis
(Injection)
Fecal
2x10 to the 6"i
CFU
CFU/g
Coliform
power per gram of
total solids
CFU/ug
CFU
2x10 to the 61s
CFU
CFU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
ve performed
Option/Alt. 1
Option/Att. 2
Option/Alt. 3
Option/Ait. 4
(VS reduction)
(40 -day bench)
(30 -day bench)
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying—Stable)
(Drying—Unstable)
Option/Alt.9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen re uirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector amaction
A reduction requiremenC in
40 CFR 503.33/15A NCAC 02T.1107 have been met"
"I certify, under penalty of law, that the pathogen requu'ements in 40 CFR 503.32/ISA NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly Bother and evaluate the information used Co determine that the pathogen and
vecIor air 'acCton reduction requirements have been met. I am aware that there are signifi
cant penalties or false
certification including fine and imprisonment."
Derek Clayton WWTP Superintendent
Prepares Name and Title Land Applies Name and Title (if applicable) (type or print)
( e� `—U 2-12N l4
Signature ofPreparer* I Date Signature of Land Applier(if applicable)
Date
*Preparer is defined in 40 CFR Part 5039(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxboro W WTP Wy Permit Number: WQ 0021826
W WTP Name: Roxboro W WTP NPDES Number: NC 0021024
Monitoring Period: From 04/01/2018 To 06/30/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1 /A (tune/temp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Claes A only) indicate "Process to Further Reduce Pathogens":
Cmnpost Heat Drying
Beta Ray Gamma Ray
Class B:
Heat Treatment Thermophilic
Pasteurization
Alt (1)
(40 CFR 503.33/15A NCAC 02T.1107)
-Please indicate option/alternative
performed:
NO Land Application this
Period
IfappHc
OptimilAlt. 4
(VS reduction)
Lime
(30 -day bench)
(Spec. 02 uptake)
Anaerob
Opfimr/Alt, 6
Option/Att. 7
If a h
(14 -Day Aerobic)
(Alk Stabilization)
Puamet
_Sample
Analytical
Option/Alt. 10
Excee- of Type Technique
(Injection)
Minimum Geo. Mean Maximum
Units dences Analysis
Fecal
2x10 to the 611
CFU
CPU/g
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 6's
CFU
CFU/g
power per gram of
total solids I solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction
(40 CFR 503.33/15A NCAC 02T.1107)
-Please indicate option/alternative
performed:
Option/AIC. I
Option/Alt. 2
Option/Alt. 3
OptimilAlt. 4
(VS reduction)
(40 -day bench)
(30 -day bench)
(Spec. 02 uptake)
Option/Alt. 5
Opfimr/Alt, 6
Option/Att. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying—Unstable)
Option/Alt.9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction
alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, underpenalty of Law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector amaction
X reduction requirement in
40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properlyy ather and evaluate the information used to determine that the ppathogen and
vector attraction reduction requirements ave been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
� repa
rer Name and Title Land Applier Name and Title (if applicable) (type or print)
Signature of Preparer t Date Signature of Land Applier (if applicable)
*Preparer is defined in 40 CFR Put 503.9(r) and 15A NCAC 2T.1102 (26)
Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Roles)
Facility Name:
City of Roxboro W WTP
WQ Permit Number^
WQ 0021826
40 CFR 503.33/15A NCAC 02T.1107
WWTPName:
Roxboro WWTP
NPDES Number: NC
0021024
Option/Alt. 7
Option/Alt. 8
Monitoring Period:
From 07/01/2018
To 09/30/2018
(Drying—Unstable)
Pathogen Reduction (AO CFR 503.32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/ternp) Alt. 2/13 (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process Co Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal DensiTy Alt. (2) Process to Significantly Reduce Pathogens
If app ca
Vector Attr
NO Land Application this Period
Lime Sta
40 CFR 503.33/15A NCAC 02T.1107
Anaerobic
(Spec. 02 uptake)
Option/Alt. 5
If a licab
Option/Alt. 7
Option/Alt. 8
Parameter
Sample
Analytical
(Drying—Unstable)
Option/Alt.9
Type
Technique
(Injection)
(Incorporation)
No vector attraction reduction
alternatives were performed
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 61h
CFU
CFU/g
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 611
CFU
CFU/g
power per gram of
total solids I solids
Salmonella
3 MPN per 4 grains total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
action Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed
OptionOptionOption/Alt. 3 Option/Alt. 4
(VS reduction) (40 -day bench) (30-daybench)
CERTIFICATION STATEMENT (please check the
40 CFR 503.33/15A NCAC 02T.1107
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying—Unstable)
Option/Alt.9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction
alternatives were performed
appropriate statement)
`T certify, raider penalty of law, that the pathogen re uirements in 40 CFR 50332/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel properly gother and evaluate the information used to determine that the pathogen
40 CFR 503.33/15A NCAC 02T.1107
have
been met."
`T certify,
under penalty of law, that the pathogen requirements
in 40
CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction
requirement in 40 CFR 503.33/15A NCAC 02T.1107
have
not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
and
vector attraction reduction xequrrements have been met. I am aware that there ora significant penalties for false
certification including fine and imprisonment."
Derek Clayton, WWTP Superintendent
Prepares Nune and Title Land Applier
Name and Title (if applicable) (type or print)
Signature of Preparer* Date Signature of ,Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Put 503.9(r) and 15A NCAC 2T.1102 (26)

ANNUAL PATHOGEN AND VECTOR ATTRACTION
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Roxbom WWTP
WWTP Name: Roxboro WWTP
WQ Permit Number: WQ 0021826
NPDES Number: NC 0021024
Monitoring Period: From 10/01/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503,32/15A NCAC 02T.1106) -Please indicate level achieved and alternative performed:
Class A:
Alt 1/A (time/temp) Alt. 2/B (Alk Treamient) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt (I) Fecal Density X Alt (2) Process to SignificanCly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If aoolicable to alternative performed !Class A or Class Bl complete the following monitoring
data:
Parameter
Vector Att
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
X (Spec. 02 uptake)
Option/Alt 5
Option/Alt. 6
Excee-
of
'Type
Technique
(Drying— Stable)
(Drying—Unstable)
Minimum Geo. Mean Maximum Units
dences
Analysis
check this statement attach an
(Injection)
Fecal
2x10 to the 611
CFU
149
154
164
CFU/g
0
1/yr
Grab
9222D
Coliform
power per gram of
total solids
CFU/g
CFU
2x10 to the 61h
CFU
CPU/g
power per gram of
total solids 1 solids
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1
Option/Alt. 2
Option/Alt 3
Option/Alt. 4
(VS reduction)
(40 -day bench)
(30 -day bench)
X (Spec. 02 uptake)
Option/Alt 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14 -Day Aerobic)
(Alk Stabilization)
(Drying— Stable)
(Drying—Unstable)
Option/Alt.9
Option/Alt. 10
not been met." (Please note if you
check this statement attach an
(Injection)
(Incorporation)
No vector attraction
reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/ISA NCAC 02T.1106 and Che vector attraction
X reduction requirement in
"This determination has been made under my direction and supervision in accordance with the system designed to
ensure that qualified personnel proper!� ether an
40 CFR 503.33/15A NCAC 02T.1107
have
been met."
(if applicable)
"I certify,
under penalty of law, that the pathogen requirements
in 40
CFR 503.32/15A NCAC 02T.1106
and the vector attraction
reduction
requirement in 40 CFR 503.33/15A NCAC 02T.1107
have
not been met." (Please note if you
check this statement attach an
explanation why you have not met one or both of the requirements.)
d evaluate the information used to determine that the ppathogen and
vector attraction reduction regmrements ave been met. I am aware that there are significant penalties for false
certification including fine and imprisonment."
Derek Clairton, WWTP Superintendent
Propazer Name and Title Land Applier Name and Title
L
(if applicable)
(type
or print)
Q
Signature ofPreparer* Date Signature of Land Applier (if applicable)
Date
*Preparer is defined in 40 CPR Part 503.9(x) and 15A NCAC 2T.1102 (26)

1/28/2019 Fecals 2018 - Dropbox
FECAL DATA SHEET.......
Lab result Log
154 2.187520721 Min 149
151 2.178976947 Max. 164
149' 2.173186268 Geometric Mean 154.
.153 2.184691431 _ -
155' 2.190331698
...152 2.181843588...
..1.64 2.214843848: I
Average _ 2.187342072.....
https://www.dropbox.com/sh/5xzx78flcbjlkzwn/AACibLA3ycCAa1 kL9zU 1 MxEfalRoxboro_Soil_Reports/Fecals % 202018?d1=0&preview=Roxboro+w�Arf... 1 /1

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Contact: Clay Fisackerly Report Date: 9/5/2018
Client: Synagro
284 Boger Road Project: Roxboro WWTP
Mocksville, NC 27028 Date Sample Rcvd: 8/27/2018
Meritech Work Order # 08271818 Sample: Roxboro WWTP - 1 Grab 8/27/18
Parameters Results Analysis Dateorti Limit Method
%Total Solids 59.0 % 8/28/18 0-100 % SM 254.OB
Fecal Coliform (Sludge) <154 col/g dry wt 8/27/18 154 col/g dry wt SM 9222D
Meritech Work Order # 08271819 Sample: Roxboro WWTP - 2 Grab 8/27/18
azameters esults Analysis Date Renortin� Limit Method
%Total Solids 60.1 % 8/28/18 0-100 % SM 254.OB
Fecal Coliform (Sludge) <151 col/g dry wt 8/27/18 151 col/g dry wt SM 9222D
Meritech Work Order # 08271820 Sample: Roxboro WWTP - 3 Grab 8/27/18
Parameters Resu is Analysis Date Reporting Limit Method
%Total Solids 61.0
% 8/28/18 0-100 % SM 25408
Fecal Coliform (Sludge) <149 col/g dry wt 8/27/18 149 CU U, dry wt SM 9222D
Meritech Work Order # 08271821 Sample: Roxboro WWTP - 4 Grab 8/27/18
Parameters Results Analysis Date Renortingl.imit Method
%Total Solids 59.6 % 8/28/18 0-100 % SM 25408
Fecal Coliform (Sludge) <153 col/g dry wt B/27/18 153 col/g dry wt SM 9222D
Meritech Work Order # 08271822 Sample: Roxboro WWTP - 5 Grab 8/27/18
Parameters Results Analysis Date Reporting Limit Method
%Total Solids 58,8
% 8/28/18 0-100 % SM 25408
Fecal Coliform (Sludge) <155 col/g dry wt 8/27/18 155 col/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Caro]ina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 2
Contact: Clay Fisackerly Report Date: 9/5/2018
Client: Synagro
284 Boger Road Project: Roxboro WWTP
Mocksville, NC 27028 Date Sample Rcvd: 8/27/2018
Meritech Work Order # 08271823 Sample: Roxboro WWTP - 6 Grab 8/27/18
Parameters Results Analysis Date Reporting Limi Method
%Total Solids 5918 % 8/28/18 0-100 % SM 2540B
Fecal Coliform (Sludge) <152 col/g dry wt 8/27/18 152 col/g dry wt SM 9222D
Meritech Work Order # 08271824 Sample: Roxboro WWTP - 7 Grab 8/27/18
Parameters Results Analysis Date ReuortingLimit Method
%Total Solids 55.5 % 8/28/18 0-100 % SM 2940B
Fecal Coliform (Sludge) <164 col/g dry wt 8/27/18 164 cal/k dry wt SM 9222D
I hereby certify that I have reviewed and approve these data �������
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[336)342-4748 fax.(336)342-i522

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1/2s/2o1s
DIGESTER
"COOLER'
30 Day Bench 2018 - Dropbox
ROXBORO VVWTP LAB _ _. _
%TOTAL RESIDUE and VOLATILE SOLIDS
_ _ BTANDARD METHODS 18TH EB 25498 antl 2540E
Analyst Nicki Dal[on, Crys[al Shotwell.. _ _ _
GATE (TIME
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SAMPLE
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DISH
#
VOL.
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WEIGHT
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SOLIDS
(Total)
Time
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(Total)
Time
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WEIGHT
DISH+DRV
SOLIDS
WEIGHT
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SOLIDS
%
TOTAL
501105
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Time
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Time
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AN s
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1/912016
1/9/2018
7
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61rfi764
115.7253
34.0469
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1000
81.6704
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61.6788
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1130
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6:45 AM
1/812018
9
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73.4471
109.0715
35.6244
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73.8184
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1/1fi/2016
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110.2203
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1/15/2018
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1/2312018
1/23/2018
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81.6]92
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7:00 AM
1/2212018
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107.5629
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73.4480
107.9514
34.5034
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73.7797
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0.96
73.5749
.2048
82
1130
1145
ND
1130/2018
113012018
7
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81.8784
118:0417
34.3633
900
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81.fi782
.0000
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7:00 AM
1/29/2018
9
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34.1438
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216/2016
7
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81.6778
115:6560
34.1704
840
1010
81.6775
-.0001
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01.6776
-.0001
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1200
ND
7:00 AM
215/2018
9
35
73.4467
107.1658
33.7191
840
1010
73.7351
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0.86
73.5592
.1759
61
1145
1200
ND
215/2018
9h
35
72.5536
107.0912
34.5376
640
1010
72.8489
.2953
0.86
72.6885
.1804
81
1145
1200
ND
2/13/2016
2113/2018
7
35
81.6783
11 6.3376
34.6593
820
950
81.6781
-.0002
Blank
81.6779
,0002
Blank
1130
1145
N❑
7:00 AM
2/1212016
9
35
73.447]
107.8692
34.4215
020
950
73.6460
.2003
0.58
73.5179
.1301
fi5
1130
1145
ND
2/t212018
9U
35
72.5545
106.5161
33.9616
820
950
]2:7472
.1927
0.57
72.823
.1242
64
t130
7145
ND
2114!2016
2/14/2018
7
35
Bt.6]81
118.1041
36.4260
830
1000
81.8781
.0000
Blank
81.678
.0001
Blank
1727
1147
ND
7:00 AM
211212010
9
35
73.4473
107.4187
33.9714
830
1000
73.6406
.1933
0.57
73:5163
.1243
fi4
1 P36
114]
ND
211212018
9b
35
72.5545
105:8913
33.3366
030
1000
72.7486
.1941
6,se
72.6228
.1280
65
1127
1147
NO
-
Blan
2018 (First Quarter) VECTOR ATTRACTION CALCULATIONS _ _ __
https://www.dropbox.com/sh/5xzx78flcbjlkzwn/AACmRXhYVU2b-h-kjxfBlbgYa/Roxboro_Soil_Reports/30 % 20Day%20Bench % 202018?d1=0&preview=V... 1 /1

ROXBORO VVWiP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 25409 and 2540E
DIGESTER Analyst: Nicht Dalton, Crystal Sholviell
OOLER"
SLUDGE
2018 (Second Quarter) VECTOR ATTRACTION CALCULATIONS
SAMPLE
DATE
DISH
#
VOL.
ML
INITIAL
DISH
WEIGHT
WEIGHT
DISH +WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
(Total)
Time
Out
Oven
WEIGHT
DISH+DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
m
(gras)
WEIGHT
VOLATILE
SOLIDS
as)
m
%
VORK
Sou
(Volaele)(VolaOle)
Time
Time ANoYarl
WITIALS
1
RPO's
ITNeeded
DATEITIME
OF
TEST
4/32018
40DD18
7
35
01.67]8
115.6470
33.9892
900
1030
61.6]]9
0001
Blank
01.6702
NO
630
422018
9b
35
72.5532
107.9074
35.4342
900
1030
721931
2399
0.68
72.6352
.1579
66
1200
1215
ND
422018
9
35
73.4461
106.7175
33.2714
900
1030
73.6714
.2253
068
73,5235
.1479
Bit
1200
1215
NO
4/102018
4/102018
7
35
81.6768
116.7905
35.1217
945
1115
81,6771
Blank
81.677
0001
Blank
1245
1300
NO
630
482018
9b
35
72.5529
1066428
34.0899
945
1115
72.0280
2759
0:01
72.8454
,1834
6S
1243
130D
ND
4192016
I B
1 35
73.4459
1 106.na
1 33.3209
945
1 1115
1 73.7027
1 .2560
0,77 1
73.5327
1 1700
66
1245
130D
ND
41122018
4/122016jgb�
81.6776
118.1261
MA405
910
1040
81.6774
:0002
Blank
816774
Blank
1200
NO
700
4/92010
73.4483
107.5061
34.0596
910
1040
]3.]208
.2745
0.81
73.5303
.1825
1100
1215
ND
recheck
4/92010
72.5530
105.9162
910
1040
72.8102
.2572
0.]]
72,6400
.1699
12W
1215
NO
41172010
4/17201801.6»8
115.7030
34.0254
81.6773
-.0003
Blank
01.6]]3
0000
Blank
TO
1134
CS
704
4/102018
]25531
107.0180
34.4629
72.7240
.1709
0.50
]28093
.114]
6]
1114
1134
CS
4/182010)3.4464
10].7978
34.3515
73.81]3
.1709
0.50
]3.6922
.1151
67
1114
1134
CS
4242016
4242010
81.8781
116.3384
34.6583
1005
01.6702
.0001
Blank
81.6]81
0001
Blank
1140
1155
ND
701
4232016
73.4473
107.3429
1005
73.8361
.1680
0.56
]3.5166
.1195
W
1140
1165
ND
4232016
)2:5540
106.5561
34.0021
1005
7274)4
.1936
0.5]
72.6245
.1229
64
1140
1155
ND
4262DIB
4262018
01.9778
115.7997
34.1218
1039
81.6782
0004
Blank
81.6]]9
.0003
Blank
1217
1237
CS
700
4232018
72.5538
107.2338
34.6000
1039
72.7467
.1929
0.56
72.6232
.1235
64
1217
1237
CS
recheck
2018
73.4472
107.7763
34.3291
1039
73.6411
.1939
VSS
]3.5165
.1246
64
1217
1237
CS
5/12018
5/12018
7
81.6]74
116,2240
34.5466
815
6T7d
Blank
81.BT71
.0003
Blank
1115
1130
ND
703
41302018
9
35
73.4468
1D82890
34.8424
615
945
73.6184
.1718
GAS
73.5043
.1141
fie
1115
1130
ND
4/302018
Am
35
725531
107.4355
815
845
72.7283
.1732
0.50
72:8119
.1144
68
1116
1130
ND
5102018
9182018
7
81.6]03
114.3710
32.6927
1.6780
lank
Blank
1115
1130
ND
706
5220189
35
734403
107.1591
33.7108
800
930
73.8076
.1583
0,47
73.5021
.1055
66
1115
1130
ND
522018
725541
1002001930
72.7123
.1582
0.47
72.6075
.1048
66
1115
1130
ND

ROXBORO WWTP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS LOTH E0.2540B and 2540E
DIGESTER Analysis shod Dalton, Crystal Shoovell
OOLEW
SLUDGE
DATE/TIME
OF
TEST
SAMPLE
GATE
DISH
#
VOL
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH +WET
SOLIDS
(grams)
WEIGHT
WET
SOLIDS
(grams)
(Total)
Time
In
Oven
Rare)
Time
Out
Oven
WEIGHT
DISH +DRY
SOLIDS
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITEDVOILATSUE
WEIGHT
(grams)
WEISHT
SOLIDS
(grams)
VOLATILE
SOU
Solaule)(volatile)
Time
lneINITIALS
1
"D's
if Needed
1132018
7/32018
62
35
75.9825
110.2713
34.2000
850
1022
75,9826
0001
Brook
75.9825
.0001
Blank
1202
1222
CS
631
722018
9b
35
72.5505
106.3917
33.8412
ago
1022
72.0948
,3443
142
72.6988
.1960
57
1202
1222
CS
722010
9
35
73.4463
107.8544
34.4001
850
1022
73.7967
3504
1.02
73s97
.1997
57
1202
1222
CS
7/102018
7/102010
52
35
75.9824
110.3466
34,3642
025
1004
75.9024
lank
1143
1205
CS
634
7192010
9b
35
72.5502
10.2640
33,8138
825
1004
72.8546
.3044
ISO
72.6727
,1819
60
1443
1205
CS
7A2010
1 9
1 35
73.4462
1 107,5000 1
34,0530
825
1 1004
1 73,7497
1 soas
0.89
1 73.569
1143
1205
CS
7/172010
7/172010
62
35
75.9824
110.2224
342400
043
1015
75.9825
.0001
Blank0001
1152
1212
CS
532
]/102010
35
73.4460
107.6097
34,2437
043
1015
73.7303
.2923
7355645
.1738
59
1152
1212
CS
7/162010
gb
'35
72.5502
105.4643
33.9141
043
1015
72.0301
2879
0+85
72.6665
1212
CS
7242018
7242018
5
35
77.8309
112.3110
34.4001
B13
943
77.8310
0001
Blank
7/.0307
1117
1138
CS
7232018
9
35
73.4458
108.1968
34.7512
813
943
73.7313
.2057
0,02
73.5593
.1720
60
1117
1138
CS
]232016
9b
35
72,5499
106.5303
33.9884
013
943
72.8278
.2779
0,82
72.6606
1138
CS
]/312010
7212018
5
35
7/.8307
112.3751
34.5444
010
940
77.0307
Blank
77.830]
CS
636
7/302018
35
73.4154
108.9691
33.5237
010
940
73.7077
2623
D.78
73,5497
,1580
1158
CS
7202018
9b
35
725497
108.4370
0881
B10
940
72.8155
2658
0.7e
72.6554
.1601
1130
CS
8/!2010
8/72010
62
35
75.9021
110.2892
34.3071
835
1005
75.9821
Blank
75.902
0001
Blank
1156
1216
CS
632
8/82018
9b
35
72.5407
108.0835
34.3340
835
1005
72.8017
.290
0.74
72.6509
.1508
60
1156
1216
CS
8182018
9
35
73.4450
100.0574
346224
835
1005
73.6992
.2542
0,73
73.5472
.1520
60
1166
1216
CS
2018 (Third
Ouerterl VECTOR
ATTRACTION
CALCULATIONS

ROXBORO W WTP LAB
%TOTAL RESIDUE and VOLATILE SOLIDS
STANDARD METHODS 18TH ED. 254OB and 2540E
DIGESTER Analyst Nick] Dalttar Crystal Shoteell
COOLER"
SLUDGE
DATEITIME
OF
TEST
a- Blank
1078 (Fourth Ouattar) VECTOR ATTRACTION CALCULATIONS
SAMPLE
OATS
DISH
#
VOL
ML
INITIAL
DISH
WEIGHT
(grams)
WEIGHT
DISH+WET
SOLIDS
(Seems)
WEIGHT
WET
SOLIDS
(grams)
(Tendo
Time
InOut
n
Total)
Time
Oven
WEIGHT
DISH +DRY
a
(grams)
WEIGHT
DRY
SOLIDS
(grams)
%
TOTAL
SOLIDS
IGNITED
WEIGHT
(grams
WEIGHT
VOLATILE
SOLIDS
grams
%
VOIAIILE
SOLIDS
walaffia(volatile)
Time
In
Time Ax
L8
if Needed
1022018
1022018
62
35
75.9816
110.3710
34.3894
927
1027
Blank
12:31
12:51
CS
5:32AM
10112018
9
35
73.4435
107.6077
34:1642
9:27
10:27
73+7304.2869
0.84
735689
.1615
56
12:31
12:51
CS
10112018
9h
35
Modal)
106.7797
34.2307
9:27
0:27
.845
.1614
56
12:31
12:51
CS
IOMM018
10192018
62
35
75.9815
109.1266
33.1451
930
1100
lank
75.9813
.0003
Blank
12:30
12:50
NO
724W
10182010
9
35
73.4421
107.4051
33.9640
1190
736860
.2439
0.72
73.5421
.1439
59
12:30
12:50
NO
10182010
I 9b
1 35
72.54T/
I IDT.1093
1 34.5616
9:30
1 1100
M.7960
.2483
0.72
72.6491
.1469
59
12:30
12:50
NO
101162010
101162018
62
35
75.9814
110.728
34,7914
8.30
10:00
75.9813
.9811
Blank
11:30
11:60
NO
8:35 AM
10/152018
9
35
73.4421
106.2741
32.8320
8i30
10:00
73.6550
73.528
.1270
W
11:30
11:50
NO
1WI52018
9b
35
72.5476
106.8290
342014
10:00
72.7693
.2217
OB5
72E372
.1321
Go
11:30
11:50
NO
10232018
10232010
62
AS
75.9815
109.5755
33,6940
10:0075.91112
-L003
Blank
75.9512
Dodd
Blank
11:50
12:10
NO
6:45 AM
10222010
9
35
73.4414
107.0179
3421
'830
10:00
73.5920
.1514
0.44
11:50
12:10
NO
10222018
9b
35
72.5466
106.8672
34.3206
8:30
MD
72.7003
0.45
72.8098
G905
59
11:50
12:10
NO
101302018
101302018
62
35
75.91106
110.1779
34.1973
9:00
10:30
75+9806+000001101
lank
12:30
12:60
NO
710M
/0292018
9
35
734400
100.1699
34.7291
9:00
1030
73.5250
.0842
0124
73.4788
.0484
57
12:30.
12:60
NO
10292018
96
35
]2.5461
106.2504
33.7043
9:00
1030
72.6359
12:30
12:60
NO
1182010
11182018
62
35
76.9812
110.7946
34.8134
9:00
10:30
75.9812
Blank
75,9814
Blank
12:17
12:38
NO
:30 AM
IVS2010
9
35
73.4417
106.4502
33.0085
9:00
10:30
73.5830
1413
0.43
73.5019
.0811
57
12:17
12:38
NO
IVI2918
9b
35
72.5471
105.9034
33.3563
9:00
10.30
72.6807
.1436
0.43
72A085
.0822
W
12:17
12:38
NO
VSR

SECTION 6

Agricultural Lime Application Log
Year: 2018
Project: Roxboro
FieldSoil
(state -county -site -field)
pH
Lime Requirement
(from soil analysisl
Tons/Acre
Applied
Date Applied
NC -PS -24-01
61
0.0 tons/ac.

SECTION 7

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