WQ0006101_Residual Annual Report 2018_20190313

INITIAL REVIEW
Reviewer Williams, Kendall
Project Number* WQ0006101
SUBMITTAL DATED: 2/26/2019
Project Contact Information
Rease provide inforrration on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other issues.
......................................................................................................................................................................................................................................................................................................................................................................................................
Name * Lisa Finnerty
Email Address*
[e-mail]
Project Information
Application Type* r
New
r
Renewal
r
Annual Report
Permit Type * r
Wastewater Irrigation
r
Other Wastewater
•
Closed -Loop Recycle
r
Single -Family Residence
Wastewater Irrigation
Is a paper copy of the application being submitted?*
r Yes r Nor N/A
Permit Number* WQ0006101
Permittee * City of Dunn
Facility Name * City of Dunn
Phone Number*
4434899086
r Modification (Major or Minor)
• Additional Information
r Other
• High -Rate Infiltration
r Reclaimed Water
r Residuals
r Other
Please provide comments/notes on your current submittal below.
Please attach all information required or requested for this submittal to be review here.
Application Form Engineering Rans, Specifications, Calculations, Etc.)
City of Dunn NC 2018 Annual Report.pdf 6.5MB
upload only 1 RDF docurrent. NUltiple documents must be corrbined into one RDF file.

For nein and modif cation permit applications, the paper copy is required to be submitted to the
Di, risiom Be advised, applications will not be considered complete until both the paper and electronic
applications. have been received_ The paper copy shall include the follm ging:
• Application Farm
• All relevant attachments (talcs, soils report, specs, etc_)
• 1 full-size engineering plan set
• 2 11-17" engineering plan sets
• 1 extras set of specifications (in addition to the set of specifications Provided in the
attachments)
• Fee (if required)
This shall be mailed to the following address:
By US_ Postal Service-
Di,vision of Water Resources- Non -Discharge Branch
1617 Mail Service Center Raleigh NC 27699-1617
By Courier, -Special Delivery:
Division of Water Resources- Non -Discharge Branch
Nathaniel Thornburg- 9th Floor, Office #942M
512 N_ Salisbury St_ Raleigh, NC 27644
For questions or problems contact Tessa Monday at 919.7073660 or Tessa_X%nday(dncdem_gov or
Sonia Graves at 919.707.3657 or Sonia Graves(dpcdenr.gov.
*140 By checking this box I am acknowledging that I have read the above statement and agree
to send these documents as required to one of the address given above.
Signature
Submission Date 2/26/2019

435 \VilHatns Court, Suite 100
Baltimore, NID 21220
wwwsynagro.com
FEBRUARY 22, 2019
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2018 Annual Report for Permit No. WQ0006101
Dear NCDEQ:
SYNAGRO
Synagro is submitting one copy and one electronic copy of the above referenced report on
behalf of the City of Dunn, NC.
If you have any questions or need additional information, please do not hesitate to contact
Heather Adams at [phone] or Melvin Goad at [phone].
Sincerely,
Derrick Shiva
Environmental Compliance Manager
Enclosures
cc: Heather Adams — City of Dunn
Melvin Goad - Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF DUNNI NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0006101
2018 ANNUAL REPORT

City of Dunn, NC
Residuals Land Application Program
2018 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms, Residuals Analyses,
& SAR Calculation Pages
3. Annual Land Application Field Summary Forms
4. TCLP Analyses
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH &Lime Application Records
7. Soil Analyses

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQPermit #: W00006 101 County Harnett Year 2018
Facility Name (as shown on permit) Dunn W WTP & City of Dunn WTP NPDES No. NC0043176 03-43-010
Land Application Operator Svnaero Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A—Residuals Anolication Summary:
Total number of application fields in the permit: 13
Total number of fields utilized for land application during the year: 3
Total amount of dry tons applied during the year for all application sites: 255.25
Total number of acres utilized for land application during the year: 125.6
Part B —Annual Compliance Statement:
Facility was compliant during calendar year 2018 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15ANCAC 02T.1 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40. CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediation.
IL Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C —Cert
ification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. ]
am aware that there are significant penalties for submitting false information, in ding the possibility of fines and imprisonment for
knowing violations." B
Heather Adams Utilities
Director
Permit e Name an Title (type or print) Sigi. e of Perm ee Date
Signaof PreparFr* Date Sign o and Ap 1 r Date
(if different from Permittee) (if different fro Permittee and repater)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006)

2018 ANNUAL OPERATIONS SUMMARY= LAND APPLICATION
DUNN, NC
DUNN, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT
April 2018 5455600.00 G 56.19 D
September 2018 601,400.00 G 61.94 D
YEARLY TOTAL 111473000.00 G 118.13 D
DUNN, NC WTP LIQUID
MONTH/YEAR AMOUNT UNIT DRY TONS UNIT
April 2018 737,800.00 G 104.60 D
October 2018 229,400.00 G 32.52 D
YEARLY TOTAL 967,200.00 G 137.12 D
DRY METRIC
TONS
50.97
56.18
107.15
DRY METRIC
TONS
94.87
29.50
124.37
1/31/2019

SECTION 2

a
(O Z M >
o Z o z
hoz o
O
N
a
E E cD E
ZZ Z
E« a
_W
L LL 0
m
N � N
N c
N N N
L O
3�
m c
c o
aEY
m
o— o
m � c
c _ E
c E c
O � p
y N
Z N O.
QpE
y N p
E �
O O 0
N
O C C_
U N �
N y
O
a N r
E � N
a�0
o_
a my
f0 N C
Q � �
� L �
N OJ C
32`c
� Qo
000
a€
U O
Y y N
N�
m p- rn
w
N = Q
„p cr N
Lp
N N
c O
Q LL
N c
,Z• � m
N U
c
� mw
a� rn
6 N

&
0
LLO
wo
«
■
�
7
e
e
z
�
&
«
e
J
«
�
D_
U)
w
«
7
z
«
\
� #
§ �
\ { f
) k7 D
�EI70 E
) \\j K§E, 5E
® 2\\ o ( )0
}00 <>Z£7
/
�
@
\
{y(co
ADO
\
$oz/o
k§
kt
2z..�z
•#§&a.
in
!ƒ
CL
z0
\
� #
§ �
\ { f
) k7 D
�EI70 E
) \\j K§E, 5E
® 2\\ o ( )0
}00 <>Z£7
/
�
@

W`,N � 7621 Whitepine Road, Richmond, VA 23237
aY NO' nt,- Main 804-743-9401 °Fax [phone]
i ANALYTICAL www.waypolntanalytical.com
Sample Summary Table
Report Number: 18-073-0214
Client Project Description: Dunn W WTP
Lab Na Client Sample ID Matrix Date Collected Date Received Method Lab ID
59182 Dunn WWTP Solids 03/13/201812:00 03/14/2018
59182 Dunn WWTP Solids 03/13/201812:00 03/14/2018 7471A WTN
59182 Dunn WWTP Solids 03/13/201812:00 03/14/2018 6010C WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 1 of 4

O
O
O
o
p
M
0
0
M
po
M
M
M
O
O
O
m
m
W
O
N
O
O
m
O
N
O
W
O
N
O
W
O
N
O
ON
m
O
N
O
O
m
O
N
O
N
W
O
N
O
m
O
N
O
m
O
N
O
W
O
N
O
m
O
N
O
m
O
N
O
�-
m
O
N
O
M
m
o
0
0
a
a°
:
Q
v
o
E
�
a
N
d
d
N
d
d
yd
�
O
�
Y
17 m ZO o
C7 C7 U 2 N
0 o M 0 0 0 U U U U U U U U Z~ LL
V V S O O O O O O O O O
o o o o o o o o v o
n N ^2 Q O
N U V
W
O
O
O
M
N
M
M
M
M
M
M
M
M
M
O
O
N
m
O
N
O
W
O
N
O
O
m
O
N
O
W
O
N
O
W
O
N
O
m
O
N
O
m
O
N
O
W
O
N
O
m
O
N
O
m
O
N
O
W
O
N
O
m
O
N
O
m
O
N
O
W
O
N
O
m
O
N
O
m
O
N
O
�-
m
O
N
O
CL
O
O
N
m
W
m
O
O
O
O
O
0
c
R
m
O
z' E E a��i o z
p Nd
r E aRi E 'c m Z 'c
N U R Z Z
0 o' a
i o c
in Y a. a° cn U cn m
¢ U N JE
"
m m
h Y m y
H, F H F H H IU- F° g I -o I -O 10- g Q O z

(((((Y(7(
\\k
a/ƒ
!kk
fy
\$\\
�§R
G
c`
(}\
f)
(
««§2
(
0o
ƒ)]
2
(((((Y(7(
\\k
a/ƒ
!kk
(((((Y(7(

oN m
FJ �m
ti
v Q Z 4 N
u.d{L�1 cam`
Z�¢ Eo
w � U
m
w
��d� 01
$�o� c
� b
� m
m
�3
��
�c�
U
Q
c �
—ho'
Q�Qm
b e
V
W
Q
Z
� �
v M
W m
O �
0
a a
ya
�a
W
c�
W
2r
a
�i
ZF
J
a
NQ
0
N
LL Z
oQ
'� z
V
J
0.}W
F
= Q
ao
W
y�
Uy
I�
0
a
a
m
a
Z
N
N
o
N
J
C
W
Z
�
o
a
F
N
U
V
W
Q
Z
� �
v M
W m
O �
0
a a
ya
�a
W
c�
W
2r
a
�i
ZF
J
a
NQ
0
N
LL Z
oQ
'� z
V
J
0.}W
F
= Q
ao
W
y�
Uy
I�
a
8
c
i
c
c
.�
�� E
J
N
Z
O
Z
a
W
a
a
m
�
N
N
•d
,C
C
a
8
c
i
c
c
.�
�� E
J
N
Z
O
Z
a
W
N
`m
d
U
��`�''
E`
2E
gg�
as
�o
2
o E
N O
O �
La E
®'
�m
Z�
-�o �
m U
��
�U
F° .2
mw
��
Ti
O
v�
fl) ~
U
��
Fm
(,!J N
z
•d
v
m q
1°
o
>N
op
7'
=a�Q
N
y
W
�
=
\
7
V
w
Q
N
�
�
`
\\
T
z�
a
`
�
\
Q
Z
`
`
\
V
V
D
Az
o
Z
`
\l
Z
a
S
Z
N
J
J
N
W
ao
1—
�
�
�
3
N
`m
d
U
��`�''
E`
2E
gg�
as
�o
2
o E
N O
O �
La E
®'
�m
Z�
-�o �
m U
��
�U
F° .2
mw
��
Ti
O
v�
fl) ~
U
��
Fm
(,!J N

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date ReportRange Ratio
2188.01-AEDLIQ-NC DUNN, NC WWTP AEROBICALLY DIGESTED 3113/2018 1/1/2018-12/31/2018 0.7641
LIQUID
Na mg/I = (Na mg/kg x %Solids) + 100 = (1960 x 2.4700) = 100 = 48.412
Ca mg/I = (Ca mg/kg x %Solids) _ 100 = (7640 x 2.4700) + 100 = 186.708
Mg mg/I = (mg mg/kg x %Solids) > 100 = (2790 x 2.4700) - 100 = 68.913
Na meq = Na mg/I + Molec.Wgt.Na = 48.412 _ 23 = 2.10487
Ca meq = Ca mg/I + Molec.Wgt.Ca = 188.708 _ 20 = 9.4354
Mg meq = Mg mg/I + Molec.Wgt.Mg = 68.913 - 12 = 5.74275
SAR = Na meq + SgrRoot[0.5 x (Ca meq + Mg meq)] = 2.10487 + SgrRoot[0.5(9.4354+5.74275)] = 0.764066
Printed: 1/28/2019
12:07
Page 1

`o
t
c
O
a
N
N
co
E
E
w
a
m
a
d
y
m
C
Q d
N N
N
C
� (0
c y
Q0
m N
a
C
o E
a
y R
d `m
o �
w C
0
o
E m
O C
Y C
U
U �
Q E
E
N
0
a
t
d
C
N
ayi
u
o
a
U
co
Z
o
Z
Z
�o
0
C
O
7
da
G1
Ew
�E
O
Z
..
R
Z
1
F
E�o
-
W
a
`O
a
u
z
W rl rl m
th rl N M N to ri rl N N m N N
o
o L
01
R 3
R
y Y
.y `0 01
T E
m c
C m fA o o
a.y � t Z
y a�
Fm
Dm❑oaa� Q E d z
E Eo c o W E E E movU
)Ea-
oon>•YmozE
ad.m N 0 v
Edm"r oYER om
d G. QU2UU � 2 z U) I-
I -P<2
N
c0
O C
o `
3 �
c R o ♦ V
v mY o
o_ o m
U �
(0 a C
c E EE
o n o
Z C d
ao E
`Ea
C
O _ R
O N
o c c
U N `i=
N ]C
O
a N w
T N
E �s
Fu
m
a d aC
ca o
a C
m u c
Baa
@ � C
3?'c
Q,o
O` co
O Q E
O O
V C C
C N
NCo
m
y � .
O 6 N
O
LL
C N y
N 0
w
Q N m
N C
m
O 00 d
O Co
0
c
a rn
�x
-am w

0
O
N
ca
E
E
f0/1
O
tr
N
0
C
N
Z w
0 U
N
�C
(0
c m
�a
� O
C N
a �
ca)
p E
O_
0 0
O O
U
YC
O
of
E m
O C
N C
.al O
U
U @
Q
E
N
n
0
O
M
w
Y
C
y
m
FL
o a
U
m Z
o Z Z
�o 0
T
O
3
y N 'C
s EcDE
E m .. E
Z z u Z
W Cj F
a LL z o
Y N C
N y O
0 L O
N
c o
O — O
U
(0 J C
C E E
O a p
y J Ul
� R
N E
0_ O
N E C
ON
O N
O � C
U N
NL.
O
vy�
T � -
E�
N
N 0
��Q
O C N
N 6 O
f0 N C
� a)
N � C
� O
O
QE
O
U N w
p C C
� C N
Y N N
N �
wa
mclrnr�- r\
O
m m s
u
p O' N
Tm o
Cw N
N N
N
O m N
N N C
(0
C p C
C U
U N C
al .m
7

pO' ■ ■��.® 7621 Whitepine Road, Richmond, VA 23237
Main R04-743-9401 °Fax [phone]
�� ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 18-073-0215
Client Project Description: Dunn WTP
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
59183 Dunn WTP Solids 03/13/2018 12:40 03/14/2018
59183 Dunn WTP Solids 03/13/2018 12:40 03/14/2018 7471A NfTN
59183 Dunn WTP Solids 03/13/2018 12:40 03/14/2018 6010C WTN
WTN: Waypoint Analytical - TN, Memphis, TN, Certification: #1354
Page 1 of 4

3
C
o
W
m
O
m
m
O
UO
d
O
m
N
�
o
m
�
N
m
N
d
V
�
—
C
W
N
d
m
�
0
N
=-
E
�
c
u
LL
O
l(j
(O
m
m
d
v
M
v
�
O
N
m
O)
3
a
m
C
s
E
m
d
�
d
c
'6
�
Z
0
U
Y
w
U
v
U
U
U
U
Z
3g
LL
O
O
O
O
O
N
N
ad'
as
rn
O
n
J
M
3
C
o
W
m
O
m
O
O
W
d
O
m
d
�
o
m
�
N
m
N
d
0
W
0
N
0
N
OOOOOOOOOO
�
a
�
N
N
m
�
0
�
=-
o
�
z
M
O
K
l(j
(O
m
m
d
v
M
v
�
O
N
m
`ol
..
a
N
C
s
E
m
d
d
d
N
�
Z
�
U
Y
w
U
v
U
U
U
U
Z
a
LL
O
O
O
O
O
O
N
ad'
as
rn
3
C
O
o
W
m
O
m
O
O
W
d
O
m
❑
O
o
m
W
m
m
N
J
m
0
N
0
N
O
W
0
N
0
N
OOOOOOOOOO
m
0
N
N
N
O
�
N
N
m
�
0
U
=-
o
z
M
O
K
l(j
(O
N
m
d
v
M
0
o
O
N
m
`ol
m
m
N
C
U
d
d
d
N
d
d
U
U
U
w
U
v
U
U
U
U
Z
a
LL
O
O
O
O
O
O
N
O
O
O
O
o
W
m
O
m
O
O
W
d
O
m
�
O
o
M
W
m
m
m
0
N
0
N
O
W
0
N
0
N
O
m
0
N
0
N
O
W
0
N
0
N
OOOOOOOOOO
m
0
N
N
N
O
�
N
N
�
�
ZO
�-
m
0
N
m
�
M
M
O
O
l(j
(O
N
m
d
v
M
0
o
m
N
N
N
d
d
C1
N
d
d
U
U
U
w
U
U
U
U
U
U
0
o
W
m
W
m
W
m
W
m
W
m
m
o
o
M
m
) o
J N
F 7
J
Y
W
0
N
0
N
O
m
0
N
0
N
O
W
0
N
0
N
O
m
0
N
0
N
O
W
0
N
0
N
OOOOOOOOOO
m
0
N
N
N
W
0
N
N
N
m
0
N
i*l
N
W
0
N
O
N
m
0
N
O
N
m
0
N
O
N
O
m
0
N
(D
ZO
�-
m
0
N
m
J
O
m
In
(fj
l(j
(O
N
N
V1
N
M
0
o
m
N
N
2
C1
N
=
U
U
U
U
U
U
U
U
U
U
U
Z
a
LL
O
O
O
O
O
O
O
O
O
O
O
O
J
M
Z
O
(00
(00
(00
(00
(00
(00
(00
(00
(00
(00
(Op
V
J
O
O
0
o
W
m
W
m
W
m
W
m
W
m
m
o
o
M
m
) o
J N
F 7
J
O
m
0
N
m
O
W
0
N
0
N
O
m
0
N
0
N
O
W
0
N
0
N
O
m
0
N
0
N
O
W
0
N
0
N
OOOOOOOOOO
m
0
N
N
N
W
0
N
N
N
m
0
N
i*l
N
W
0
N
O
N
m
0
N
O
N
m
0
N
O
N
O
m
0
N
(D
m
0
N
(D
�-
m
0
N
m
0
0
0
0
0
0
0
0
0
0
0
0
0
0
o
v
0
J
O
m
In
(fj
l(j
(O
N
N
V1
N
0
C1
m
N
N
C1
O m 0 0m � Ori � I� O O a0D 0 W c 0 N
rn m o
C
d
O
z 2 E D E m o z
0 o
(o o c
U��¢�
H 1-o H F2 O z

n
m
E
O
O
M
Mm
D
u
.
N
rl
N�
O
�
N
m
V
a
_
C
G
W
0
O
E
x
c
m
�
N
O
O
m
°
a
m
co
r
d
d
d
m
°
y
o
�
�
3
3
c
d
d
.Q
$
�
r
�
N
C
L
O
O
3�
n
O
O
O
M
O
O
d.
O
N�
O
co
m
0
0
0
O
O
O
O
m
�
N
O
O
m
o
0
m
co
r
d
d
d
°
y
o
ON
�
d
d
N
�
�
NN
N
N
�
O
O
T
N M d
7
U
Q
r -L
2
O
U
K
O
O
Z
ujO
0
U
E Q
E
E c o o O
0
N L U y N N O
U U Z J Q U N Z
m m m m m m m m c F
F° E w D
UJ
E U 7
U Z U
M
O
O
O
O
O
O
O
V
O
O
co
co
to
m
co
r
ro
m
co
T
N M d
7
U
Q
r -L
2
O
U
K
O
O
Z
ujO
0
U
E Q
E
E c o o O
0
N L U y N N O
U U Z J Q U N Z
m m m m m m m m c F
F° E w D
UJ
E U 7
U Z U
M
O
�
Op
N
m
W
m
CO
W
00
OJ
ON
ON
N
ON
NN
N
N
N
O
O
O
O
O
O
O
O
O
T
N M d
7
U
Q
r -L
2
O
U
K
O
O
Z
ujO
0
U
E Q
E
E c o o O
0
N L U y N N O
U U Z J Q U N Z
m m m m m m m m c F
F° E w D
UJ
E U 7
U Z U
M
O
�
T
N M d
7
U
Q
r -L
2
O
U
K
O
O
Z
ujO
0
U
E Q
E
E c o o O
0
N L U y N N O
U U Z J Q U N Z
m m m m m m m m c F
F° E w D
UJ
E U 7
U Z U

� H �,
O� ��
F J � ro
ya0 0"
'Z� �m
Clap �a"i
.c
QQW no
QTR a�
V �
Y YI °�-' o
C9 � L v
y
n
m
$�o�
0
u"r
�o
U
w
a
a,
�a ti
� N
o� u
�w •�
wN
E�
a ,�
J
R5
W .--
a� �
Q H �\
N QQ
LL $
OQ
� � L
O
U
w
J W
a�
U
Y
w
a
m
m
�V
2
E �"
F=
o"M
L �
2 O �.:
�F S
�� �
NO
4 q_ ct
Wo 3 3
O a L C a
Uy J S E
QN
n
m m
N N
J � �J �
�I C G
a ¢
a
E
F
m
L
N
._
C
0
a
o
n
a
V O
r
E
JE
�t
ii
J
LL
t
n
I
i
0
0
Z
o
�
a
}
�
N
0
J
V
z
w
�
J
a
�
N
ay
a v_
U'i
U
w
a
a,
�a ti
� N
o� u
�w •�
wN
E�
a ,�
J
R5
W .--
a� �
Q H �\
N QQ
LL $
OQ
� � L
O
U
w
J W
a�
U
Y
w
a
m
m
�V
2
E �"
F=
o"M
L �
2 O �.:
�F S
�� �
NO
4 q_ ct
Wo 3 3
O a L C a
Uy J S E
QN
n
m m
N N
J � �J �
�I C G
a ¢
a
E
F
m
L
N
._
C
0
a
o
n
a
V O
r
E
JE
�t
ii
J
LL
t
n
I
i
0
c
m
`m
a
0
U
d
m
m
Eg
��
C
o E
aQ
0
2
o E
nv
o �
LN
a 6
N N
w m
o �
Z ftl
�_ �
N �U _
�U
��
m (A
� N
o a
N N
'�
ai
U
.iq �
�m
NN
Z
o
�
\
\J
z
V
ay
a v_
oy
U
U
a
�
1
v
N
�
\h
W
OI
_
\
\
�
���111
W
N
4
1
�
N
T
a
\
$
``,
\
\ - `.
C1
U
�
\
C
m
\o`
2
Z
z
2
2
N
J
N
W
Q
1
ao
4-
�
N
c
m
`m
a
0
U
d
m
m
Eg
��
C
o E
aQ
0
2
o E
nv
o �
LN
a 6
N N
w m
o �
Z ftl
�_ �
N �U _
�U
��
m (A
� N
o a
N N
'�
ai
U
.iq �
�m
NN

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name Sample Date Report Range Ratio
2188-02-WPL-NC DUNN, NC WTP LIQUID 3113/2018 1/112018-72/31/2018 0.6787
Na mg/I = (Na mg/kg x %Solids) + 100 = (715 x 3.4000) = 100 = 24.31
Ca mg/I = (Ca mg/kg x %Solids) + 100 = (970 x 3.4000) - 100 = 32.98
Mg mg/I = (mg mg/kg x %Solids) + 100 = (1130 x 3.4000) - 100 = 38.42
Na meq = Na mgll - Molec.Wgt.Na = 24.31 +23 = 1.05696
Ca meq = Ca mgll + Molec.Wgt.Ca = 32.98' 20 = 1.649
Mg meq = Mg mg/I + Molec.Wgt.Mg = 38.42 + 12 = 3.20167
SAR = Na meq - SgrRoot[0.5 x (Ca meq + Mg meq)] = 1.05696 _ SgrRoot[0.5(1.649+3.20167)] = 0.67869
Printed: 1/28/2019
12:07
Page 1

SECTION 3

\
\\
\\
\\
\
\\
\\
\\
<
«*
\<
\\
()
\
)i
as
ww
\\
\\
)\
\\
)4\
22
zz
«\'»\
_)
ƒ\5
\\
)\\
_
\\
\\
#7\
)
\\
(\
}
j&C
[
-
;§(r3®®
5l
a
}
l2:2z2\
$\
ayEy}a

�I
a
44
N
E o
O
�I
44
N
E o
o
�
Q
d�z
Q
N
W
�
U
�
o
wg
�
N
x
E o
o
�
d�z
x
o
�
o
�
N
b
U
o
�o�
Q
�Uw
w�'
Q

9
G
w
n
0 GA
000
A
w
n
0 GA
000
0
z
z�U
x
a
m
a
nnn
�S
o�
Y
3A
Iz
3
U
x
F
0
e
o
00
�
C
b
N cV
cV N cV
y
p, N
h
�3
a
a
rL
qQ
QOQ
Q
F Pr
v
v
v
v M
o
N N
Cn
cn
x
6
d V
00
F
z�z
03
aPea
tN�
wzoN
a
w
N
<v
0
z
x
a
m
o�
Y
3A
3
U

09 10 8£ abed
96 bb b abed
� L✓ r� C K. � T b 5 � C R-
a..di
��s�a�uai>�w5ai� �❑ a 3 �m i�
i rn � w � N � Ui w n � w ✓I IJ Vl � W N w o � of D�
x 3
It
QIn
ti
m'tK-
R
1 n J IM
ILI-ILL 0 ILL IF v
T -m O G� $ m. ILI =L
C1 o b U' C9 m IJ a w o
It
o g
LL, wZ W w rxnz�mtwin t,nCwCaw'w ��47.c i1}
k
,4
-a
E
09 10 8£ abed
96 bb b abed
� L✓ r� C K. � T b 5 � C R-
a..di
��s�a�uai>�w5ai� �❑ a 3 �m i�
i rn � w � N � Ui w n � w ✓I IJ Vl � W N w o � of D�
x 3
It
QIn
ti
m'tK-
R
1 n J IM
ILI-ILL 0 ILL IF v
T -m O G� $ m. ILI =L
C1 o b U' C9 m IJ a w o
It
o g
LL, wZ W w rxnz�mtwin t,nCwCaw'w ��47.c i1}
k
,4
E
Z
�
❑
W
CIA
E
n.
ra
t�ww'o
09 10 8£ abed
96 bb b abed
� L✓ r� C K. � T b 5 � C R-
a..di
��s�a�uai>�w5ai� �❑ a 3 �m i�
i rn � w � N � Ui w n � w ✓I IJ Vl � W N w o � of D�
x 3
It
QIn
ti
m'tK-
R
1 n J IM
ILI-ILL 0 ILL IF v
T -m O G� $ m. ILI =L
C1 o b U' C9 m IJ a w o
It
o g
LL, wZ W w rxnz�mtwin t,nCwCaw'w ��47.c i1}
k
,4
CIA
E
n.
y
V
Z
6
e
09 10 8£ abed
96 bb b abed
� L✓ r� C K. � T b 5 � C R-
a..di
��s�a�uai>�w5ai� �❑ a 3 �m i�
i rn � w � N � Ui w n � w ✓I IJ Vl � W N w o � of D�
x 3
It
QIn
ti
m'tK-
R
1 n J IM
ILI-ILL 0 ILL IF v
T -m O G� $ m. ILI =L
C1 o b U' C9 m IJ a w o
It
o g
LL, wZ W w rxnz�mtwin t,nCwCaw'w ��47.c i1}
3
y
V
Z
6
e
9
' D
09 10 8£ abed
96 bb b abed
� L✓ r� C K. � T b 5 � C R-
a..di
��s�a�uai>�w5ai� �❑ a 3 �m i�
i rn � w � N � Ui w n � w ✓I IJ Vl � W N w o � of D�
x 3
It
QIn
ti
m'tK-
R
1 n J IM
ILI-ILL 0 ILL IF v
T -m O G� $ m. ILI =L
C1 o b U' C9 m IJ a w o
It
o g
LL, wZ W w rxnz�mtwin t,nCwCaw'w ��47.c i1}

05 10 g£ abed
96 10 5 abed
qj+gyp o K g; gP
W T 2 NY q G° J ip M1^ iG qCIO
a
w g RL
IN �P
uHw°'3w'w"y Q,a Dose 3 �w �S If t$
fIJ w Z W N d h v w ,n 't W til
C
a � Jul
S r
! o,ol
S? til
� z
Li
a as o n m �i m v a m a o y m
Q rc _ x ¢ o m a ci
@ ! wIM
Ks
TI
IN N
NN �e w61 1
0 °rif
d.
L u', w �n ui' n U i ,r w w u 'w ; 3 A. m w 0 y w NOo s w ,, J w
rti
n
a,
E
f
�
w
a
o
c
05 10 g£ abed
96 10 5 abed
qj+gyp o K g; gP
W T 2 NY q G° J ip M1^ iG qCIO
a
w g RL
IN �P
uHw°'3w'w"y Q,a Dose 3 �w �S If t$
fIJ w Z W N d h v w ,n 't W til
C
a � Jul
S r
! o,ol
S? til
� z
Li
a as o n m �i m v a m a o y m
Q rc _ x ¢ o m a ci
@ ! wIM
Ks
TI
IN N
NN �e w61 1
0 °rif
d.
L u', w �n ui' n U i ,r w w u 'w ; 3 A. m w 0 y w NOo s w ,, J w
rti
n
a,
E
a
o
c
Y
-
W
V
W
05 10 g£ abed
96 10 5 abed
qj+gyp o K g; gP
W T 2 NY q G° J ip M1^ iG qCIO
a
w g RL
IN �P
uHw°'3w'w"y Q,a Dose 3 �w �S If t$
fIJ w Z W N d h v w ,n 't W til
C
a � Jul
S r
! o,ol
S? til
� z
Li
a as o n m �i m v a m a o y m
Q rc _ x ¢ o m a ci
@ ! wIM
Ks
TI
IN N
NN �e w61 1
0 °rif
d.
L u', w �n ui' n U i ,r w w u 'w ; 3 A. m w 0 y w NOo s w ,, J w
rti
n
a,

\
}
t
�
k
G@»«q
& Joy d
)
{\#\
\£a!
G@»«q
& Joy d

pg }o 6b 96ed
9L Jo L 96ed
� w e
G
E
©� m
eiT wo gi
I A:
G � �
e
La w
n i m n x m L5 m > a m � m
a rb a ~ r u u
AD �
At
CA CA CA
z w N Ell
y a 0w w ww¢IL
-
$ h w w m wi
m',W w.
ww v
F A
IiiiN
WK
.. '.. A
o w
x a $ & a, •L a -'� L yF.
nq c Si5 is a c 8,3
R�qpm#O.<
z ¢ZO w.w mN w�m.��i P
1°a z. rc LR cros
�? e w$ w$° z $ z z $ w z `,j "a' m u
E m i Gre, N
z� s �Q ata oap�agaamQc° �aa�nang6� �g
O 3 Es qa. ra a a3F, a nas a � + Fn
6 F z'qm m t3 N u NGf Jll N I w 2 W N W W N a yr d W N d w G7 N K K F m

09 10 Zb abed
96 10 g abed
- r
s
°s
ME
n
� fl
Um
Ul
o
w a a o a
� � �' O ❑ G m � a i❑ m m o m >❑ gy mQ ❑o fi$
w J p.w c•u�d7' N mj.h a""ro `� v a�i$ �$w o..
.°`, q 3v4a2Z�aGja r, a �a�a:uia3'Laz u3u spa
'U. W�
D � �
Ll
Lo
� w m
rS a t
a � _
w � m
a u
S
c $
e
y p
E 4e
WA
ca ❑ �. m a o ❑ m ❑ A o ci o �...� e,Q
Q
,. 4 w r m; m r. w� � w.❑� a �$ ti wig $ � -s
L4 Mq
a asaza3 a mt 7i a d LLa a ZusL�a
u u�Jl w 0 w

)
k
k
3@ 9 «k
&1062@
f �
, \
\ 7 \) $
u i
- Ael !R ,
/$Q2:|�! {
{§f\!K§$\}\E{§\$))b k
/[ \
{/ 6
f |(!
: ) (
_ I
\! ;-
;
#� (a
k73 �` \# \! \/( ± as\\\
! ! -` - : - : :®E)!y! ®
*\\) 47 \i !) m �!I\fƒ«)#(f q
� \%7\ ) w0 )a t/\\ }t]«« %
[�§5§{)I/\tom ®fa/z j $ 2
r°\»w>:\ $ƒ%kf,§#l2fE�:*!:$!« ^ fƒ
3\ 9 i\\\\\w0w w 0 www !/#■§!;£!/a]j(kfa

February 7, 2p97
631
Ms. Meegan Dougherty
Summit Environmental Technologies, Inc.
3310 Win Street
Cuyahoga Falls, OH 44223
R,i1Y C iJ i7lrrl{
n9lcut.rtl. . K1--6AN
J A V 71 V1 AI G RM AN
Subject: NCWWlGW LC Srxty-I]ay Pareineter MBtlod-Deceitification Recommendation:
Zinc — EPA 2DO 7 and SW -846 6010 D
Boar ids. Dougherty:
The remedial Proiicloncy Testing (PT) result(s) for the below Parameter Methods) reported by your
laboratory for the North Carolina Wastewater! Groundwater Laboratory Certification (NC WWIGW I -C)
performance evaluation waslwere unacceptable and a sixty-day parameter method decertification will be
recommended The results reported and the true values as they appear In our retards are as foliows-
Study parameterPr`athnd Unts Red True Flcesptar
Value
pertcrmance
_ V81ue Value Rar. a
WPt6-30 SY/y 846 UEPA 0U171 n ❑ poll 600 495 441-569 NotAcceAtable
EPA 200.71
�92016C1 poll f66ll f4tl9 190-1610 Not Acceptable
S'JV-846 6090 D �__-_
'P writtanCwtadWe Enation Report (CAR) for each unagC9PldiZ 2; esull vdll be iequired Prior So Mkk9SU11)g Cerrlrleal)er,
This is to notify you that the Laboratory Certification Branch of the North Carolina Division of Water
Resources, Water Sciences Section, is considering recommending - a parameter method(s)
decertification to the Environmental Program Supervisur The recommendation concerns the above
mentioned vlolation(s). This is not a decertification; it Is a notification of our intent to consider
decertification. You will be informed in separate communication if decertification is issued.
Contact me immediately at [phone] ext 251 if your records do not agree with ours or if you have
questions.
Altachntar,t
cc: Daae 5attervrhde.
Jasnr. Srr,iih,
Hasler
Filo
trG31
Sincoroly,
IJ AO 6� `
Todd Crawford
Technical Assistance &Compliance 5pecialisY
NC WV'JI W Laboratory Certiltcanon Branch
�Nollr S[ir11cL:5 5CGi1011
—�- Page 10 of I ii
Page 44 of 50

February 7,47 r
631
Ms, Meegan Clougherty
Summit Environmental Technologies, Inc.
3310 Win Street
Cuyahoga Fails, OH 44223
lid)}° �C2U1'F_lk
Y11t'Il I i 5, Rli 4J it i\
Subject; NC V4M//GW LC Sixty -Pay Parameter Method Ri:cedfication f2ecvmmendation[
Selenium - EPA 204.7 and SW -848 6019 R
dear Ms_ nau9herty-.
The remedial Proficiency Testing i,PTj fesuttts) fior_tho below Pafarnater Method(9) reported t)y your
laboratory for the North Carolina Wastewater) Groundwater Laboratnry Certrfrcaiion (NC VtiM/!GW LG}
performance evalualion:rras!were unacceptable and a sixty-day Parameter method decenlficaLon will be.
recommended. The results reported and the true values as they appear in our records areas follows:
Study Parameter Meihod.
P if➢ -3B
�PA 200 in
Wr
+ane
o9201fiC1
Unds rcePcrr
Valor
t g!L 526
True
4-02 I 376-5d9
'Perin rmanae
Nat Acceptable
r irglL A71]I 3119 32$-444 Not Acceptable
Thar: is to notify you that the Laboratory Certification Branch of the North Carolina Rivisign of Water
Resources, Water Sciences Section, is considering recommending a parameter method(s)
dace tifiCation to the Environmental Program Supervisor. Ttle recommendation concerns the at;ove
mentioned violation(s). This is not a decertification; it is a notification of our intent to consider
decertification. You will be Informect in a separate communication if decertification is issued.
Contact me immediately at (919) 733=3903 ext. 251 if your records
d4 not agnea with curs or it you have
questions:
Sincerely,
hllachmenl
cm Cana $agcrwrrile, Jason �rniln,-PAaslul Fife 8B3'�
Todd Crawford
Technical Assistance & Compliance Specialist
NC VWJtG'JU Laboratory Certification Branch
Water sclsnrss Sreuon
Page 11 of 16
Page 45 of 50

February J, 2017
631
As. Meegan Clougherty
SllmmiiEnvironmental Technologiea, Inc.
3310 Win Street
Cuyahoga Falls, OH 44223
R(7" L DOPER
htls_liF.4Lti Rtii,irlN
t JIIl'/INl ltrl4 �'I r�li
Sutijcct; NC WV'J/GW LC Slxty-pay ParametorfAetnod pecertificativn Recornrnenda[ion:
Nickel - EPA 2007.and SW -846 6010 D
Rear Ivls• pertgherty•.
The remedial F roficiency Testing (PT) resultis), for 4he bolovv Parameter lvtelhtd(s) reprrteti by .your
laboratory tar the North Carolina Wastewater! Groundwater Laboratory Certification (NC VJW13W LC)
performance evaluation waslwere unacceptable and a sixty-day parameter method decertification will be
recommended. The results reported and the true values as they appear in our records are as follows:
Study Paramete Method
WP16-38 ^ EPA 200.71 R
0g2016C1
Units
pglL I
1CJ,58 � 918
Ng!L 1
1$26 1364.
isctt unacccplebre 'esull vrill be Yegt
Ac� p€cam iPedormance
$OS 030 Not Acceptable
1200-1520 Not Acceplabla
prior in reissuj
nq car!i1it8110r
This is to notify you Thai the Labora�oly Codification wench of the Ndrlh Carolina Division
of Wafer
Resources, Water Sc:ennes Section; is considering. recommending a parameter methodis)
decertification to the Environmental Program Supervisor. The recommendation concerns the above
-mentioned violation(s), This is nota decertification, it is -.a notifleatton of our intent to consider
clecartification, You will be informed in a separate communication if decertification is Issued.
Contact me immediately at [phone] ext, 261 if your records do not agree with ours or if
you have
questions,
hltachrn en!
rg: nsna:521tervlhila,
Jason Smllh,
Master
File N63i
Sincerely
>pw�'
Todd Crawford
Technical Assistance &
Compliance Specialist
NC V, OMv Laboratory Certification branch
Water scii+ces SeeJorl
Page 12 of 16
Page 46 of 50

BV-UU-Zr1lG ;y711527 1V'plf 36
Page
13
of
16
Page
47
SCCMA�ALCIA![H
50
(RTC;
ra 16i 3a
.
\,_T.
c:uu:l�dcl; La119120!f
MethmIX13A 200.7 5
0998) (Canlinuer)
Ann 1.�_
M�,91s AsaiynnJ
Arrepl,
7
B,a:uakiun
Units VAiOe.
1Vlurlurx
[ton, Fe"
1408 d(11L 1360
1150 to
9159
AccepuWo.
1590
I V, P+PLI132 061E 1Ail .1
F3A rrj
Evaivotion urtmd-;
A. xiy9n1r A IY IOU is
l9!r py.]'.'
0 > '! r3'
F,ia(xwC!oR.
l4rrytr, ares �,Y b0 +::a 03,nr]
L td, Ple1d
)9(j vs L 162
L_:i to 10I
2. (A
}rrypiaLle.
eu.-e "ML mLli1bl!A-s
FwNetmeI: R).r;u l
7'cr :flldn
iin anlC(e a jell OL rt rli„EiU
n I} LW"Fier I.I L a.
�nlf.n5-IYJ
d� y- ! ry.
hlzh0anesp, mn'”
11,20 ug1L 1140
945 to
1,a7
A•mepwLlm
I 'aU
1 tin PEI 131E 11 1.1
Mn'IWUMAawlusu baici
k1'lI'.3
201 G-fiif.tn
EV31,0II_I f''Ylem-I
❑lOfmvy
Cuvi1�.1 ,.�Pn�W
rn-tri ..1, liL t.:1.a9, J.L
Irlal)'i)Jflllkpl. }III"
ISO ngYL 132
1o] In 1:44
2.52
.lccuprab)e
I1f111')"flj; Ii`.IIL, Lit
I.MIS5i1:1
Fasivalrowcriteia-i
Evci i'lall
0 Mulenur11:0.90D 1-0.16; J,
W-.1te 1l 4V'i..vn 1>Is D.Ii.
3VI L.n9-19
`7l'dunlary
c-6.11372, r1:2-3555
Nkkul, Ni-'
105G uc111. al$
as 5 h,
3vJ
Nnl. �lcsnptihle
—
lucw
119.1 ,i Yllli3`461fLLftlLirynd'l
1:11alhelforl-:ldrenc !
P.1,111vefirm
Faildeporr-rr:1691`l uI :i YE.`,.
A441LSVTW k4elis.es Dam
r tY O; h if 39, .1,51
sckwuml, Sue-
)111 LgiL 9A2
376 r;Y.500
3:53
Not A=m[tWo
1119 efirl1] till Lul111
N,iTj
Fw?wUlon (17mnit 1
ElYejnlLiLahtf0'
Lo, a
A �alY�l•NA IY is ijvi.
2ne�.mtf
�]Irnri,ery
.re
$11t'CI', All
.1141 n§IL "lsu
213 W 203
-2 [0
ncxepl ablq
159 I Ii105 200] L IA.11
. 563E
jivc?u!9i6fl i! m 'f. -!
A a1y L1'A+A _Ir .I e--'-plc
0.11Z
rj}urntarl'
£Ycf.xriu
i?rro nztxr c:! b-0 ,C �9 .I.ti
'Fh211ku1n, 77"
1K2C'u4.14 549
4an'.a 640
2,39
Arcep;„isle
11 f;, P(i1�15..1ON1 4,a;
LliKgbP.3n
Eui(i lC l CnL."i/i - I
r.P
F9 1 1 .,9 a, G: U,Wje.
YIIJNJA� Analyvji U U.
A.illt=.UN 18
EllVai a:ry
+. ) it 1.1 d.I J-70!
Tin, 5n”
6%oq+S Gal
02 to 1195
0.0'7
.46eeptati4u
j h
[I'ifi 19'1 iF4 L rl
iKl A:
Li,anraoaij G rfn'u l
L ruula'I
!'rr r1e1+•r j1. L: :Id1CI, r1:0
!a kiAr*�A I Jain
�A111f::di-IR
❑1, 1.1179,,'y
BV-UU-Zr1lG ;y711527 1V'plf 36
Page
13
of
16
Page
47
of
50
i'eip:.la3.1i1 ror

SEMA-ALDRICH' tlt� wp1s-3B
_, Conclucod 0 Elf 91201 b
Final lot r iMi
loIeLkod:LPA 200.7 5 (19!1111 (CantllssH{II
IU:e:oLL :vslnm,•l I� L
Aili)-}'Ic k-1111129V,17.:v Y4'iiidaw '' Evniwaien
ilansum, "I" 209 r:gjl. 211 164 in 2,111 -0,73 Acceptable
]19?1 VEI lit'ZOML - IaIL M0,144ml Fanfn(! 1'111PIIV•7 FHl (If!a!i Pnllaelnr a! Lry .:'7.Gi, ,r]
urn Gl/st:Kr'..\oafs@ Crile �U13.nL'_!N �i'idarl:nlY . ..
V,lrad:um, 4" 141:611 nrllL 1`190' IG9,7 tG 1.00 ,rcvp:&iIL
1760
IWool
1•. uar ! a
I Iof II 1 -1
-�I'SLYR17 I. �L Ir _ Ih IH-I� Idr,r.l llt)
in{, LY. ' IM: DAr 475 421 ;o 111111 •1-23 Rnl r5erd0plc61g
I % ?DiI37nyl-Lai LIJCPti; Ila J.',oxiblAwn croolvteg !-y!uetm.'.P .,[r 'n.J.bi I-tl,pS; 1). 1)
1An.l}g 41A! p Wt.Z_a IG3b 3J ❑Velwi fail;
AJnmL win. ld" S69.ug1:. 1103 317 1n 49:1 2-19 Arcuplablp
Il C4 J Vii i] PT'oIt. r lot L[WWOr: koon?IJAWOTCntenu-I t .Igen l' mr-n:1J.:b'- u:J.ind'l.
IA-a)9ili4r&l MaLsjs lallul 281ii-(19 i0 [J Vhit'irtrm/- c.U.397S, d:1}ti: 110
klcl hndJ=.l'A 200.0 s i i 199N1 f 100 LINu91
Avl[yle
rmiiinuny, SG ,.
laps. I -L11052- Mi. -I 9
,ut IAidi)[li
r111YJ]VM.,inr 1 n Datr. to l sills. li
Iirsenis. As_''•
N.f90/ L'l• 116 [ti1,1L. Ur I Ibllaara
�. Ufl;cr1 Y Iv Irtrarvl�,:har,
llanao4 Ila'=
Ia!5 • i•L'Iirst-np!:. I+ai, Lil+.tlnC"se
d-J+=�r++ h r OeIn-:Li19{rl; I'
Ol;rillmn, 7P7'
I IFI:' 111 L tLtSe `)i_.r
1A ysl�r�Al Y Gal it -e_3p] VI! -l'%
Hnsu11 A53i{f n"�
ilLll'P1
�
[t�pti L3YIf1a
Una: &'clue-
14nI�lolx
of
50
S IEu011, 774
f1i to 904
107
hocopt 610
in llnen7enn,I
L 1uwl,..kA
fWampfelo-c', 9:9940 1 Do-, j Nor
I]FedunlarP
..
cu1>•lil ':5.1:.3P
741 is(fiL 76G.
633 to U79
0.13V4Eg
IJ.rz�10
5r"alloglyin CnJf.Ap-3
FIG4;o!nm
fOhRt_ 21D 11111 12&11:
N]� Ilkin, 162
oAu h1 4iY11
iG
,tapnpYa71lE
L 4allotlojol Lrlene.
L Lfu.rf IrJnI
III II•r-ri-! 1l -I ll;i i'tt
.214 uq.H. '231 109 m 263: -1 :l Accep744fle
F.al CnlFL-¢1.saRiorlP 1,'-nr]•l-_!:c':9,09.d:G
'Bpnn, N'�
❑1pinll19rir 1573 uni4 1430
1219 la 1.77
LE40
n0-U.2�0,1C -1'1771142'1 V\Tlll'3�S
Page
14
of
16
Page
48
of
50
,4ccpp[a6Je
1'.r.q�: 05 of 1?li

09
bo
617
abed
96
30
9L
abed
3
�Y
�
5
e
a
�
�
r
r.
ci
ci
It
atM
a
IM
N
IN
&
f
e
S
aIm
m
�
c�
Lq
¢
9
C)
C
cl
p
w
PID

\k
\w
09
)
6@Q
®@
#
§
k§
t�)
Fk\
&
\w
09
«q
6@Q
®@
#
§
t�)
&
;
&M
:
10
09
«q
6@Q
®@

ENYIRONMENTALt&CNN4LOG1kS, 3NC
Analyrtical Latioraiartaa
January 04, 2019
Nate Roth
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: Dunn WTP
Dear Nate Roth:
Summit Environmental Technologies, Inc.
33]0 Win S[.
Cuyahoga Falls, Ohio 44223
TEL: (330J 253-821] FilX: [phone]
Website: hn /huww sezzek co
Order No.: 18121225
Summit Environmental Technologies, Inc. received 1 samples) on 12/20/2018 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 07256CA, Colorado, Connecticut PH -0108, Delaware, Florida NELAC E87688, Georga E87688, Idalw OH00923, ]Oinois
200061, Indima C -OH -13, Kansas E-10347, Kentucky (Underground Storage Taok) 3, Kemucky 90146, Lotisiana 04067, Maryland 339, Minnesota
409711, New Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota It -201, Oklahoma 9940, Oregon
OH2O0001, Rhode Island LA000317, Soutlr Carolina 92016001, Texas TI047044GG-11-5, Utah OH009232011-1, Virginia VELAP 9456, Washington
C891
Page 1 of 29

SUmMSummit Environmental Technologies, Inc. 3310 Win St. Case NaTTai1VC
EiMorl ENVIRONMENTAL TrC"H0WQiVS, INC. Cuyahoga Falls, Ohio 44223 WO#: 18121225
AnalyBral Laboratories TEL: [phone] FAX. [phone] Date: 1/4/2019
W bsoe: htty.1119ww.sevekconi
CLIENT: Synagro
Project: Dunn WTP
WorkOrder Narrative:
18121225: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report
is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
18121225-OOlA SVOC-BNA_TCLP(8270d): MS/MSD exhibited high RPDs due to suspected sample
inhomogeneity.
18121225-001A SVOC-BNA TCLP(8270d): The sample MSD exhibited low recovery for 2,4-
Dinitrotoluene and Surrogates: 2,4,6-Tribromophenol and Pheol-d6. The sample MS and the LCS
exhibited control.
Analytical Sequence QC Notes:
pest ccv SOOppb svoc-CPEST_npw(8081): The CCV (Batch 892856) exhibited high recovery for
Methoxychlor. The associated samples are ND for Methoxychlor.
Original
Page 2 of 29

M>�1T SummitEn„ onmen a T hnorog es, n . Case Narrative
ffISU3310 Win St.
ENVIRONMENTAL MCNNOLQPI1 S; INC. Cuyahoga Falls, Ohio 44223 WO#: 15121225
Analytical Labaralorles TEL: [phone] FAX [phone] Date: 1/4/2019
Website: http://Www.settek.coni
CLIENT: Synagro
Project: Dunn WTP
CCV 40ng S8-341 SVOC-MSTR_S(8270): CCV exhibited high recovery of several analytes;
Associated samples are ND for all analytes of interest.
18121225-001AMSD SVOC-BNA_TCLP(8270d): High RPDs due to suspected sample inhomogeneity.
18121225-001AMSD SVOC-BNA_TCLP(8270d): The sample MSD exhibited low recovery for 2,4-
Dinitrotoluene and Surrogates: 2,4,6-Tribromophenol and Pheol-d6. The sample MS and the LCS
exhibited control.
LCS-35345 TCLP-svoc-herb_TCLP(8151): The LCS (Batch 35345/R92977) exhibited a high recovery
for Surrogate: DCAA. The LCS exhibited recoveries within the acceptance limits for all analytes of
interest.
18121225-OOIAMS TCLP-svoc-herb_TCLP(8151): Spike recovery indicates matrix interference. The
method is in control as indicated by the laboratory control sample (LCS).
18121225-OOIAMSD TCLP-svoc-herb_TCLP(8151): Spike recovery indicates matrix interference. The
method is in control as indicated by the laboratory control sample (LCS).
Original
Page 3 of 29

����� samraaEnv;ronmenralTeannorogies,In Qualifiers andAeronyms
3370 Wln 5
EFiVIttONMENTAL TCCIfnpL4Ft[S, INC Cuyahoga Farls, Ohio 9422 WO#: 18121225
Arratyllcal LatiaraloNas TEL: (330J 253-8211 FAX: (330J 253-448 Date: 1/4/2019
Website: h[rn://+wwse[[ek.co
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
This list of Qualifiers and Acronyms refl
The compound was analyzed for but was not detected.
J
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
E
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in
Manual integration was used to determine the area response.
d
Manual integration in which peak was deleted
N
The result is presumptive based on aMass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GUMS.
X
The result was not confirmed when GUMS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high (+).
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected RL Reporting Limit
QC
Quality Control MDL Method Detection Limit
MB
Method Blank LOD Level of Detection
LCS
Laboratory Control Sample LOQ Level of Quantitation
LCSD
Laboratory Control Sample Duplicate PQL Practical Quatiitation Limit
QCS
Quality Control Sample CRQL Contract Required Quantitation Limit
DUP
Duplicate PL Permit Limit
MS
Matrix Spike RegLvl Regulatory Limit
MSD
Matrix Spike. Duplicate MCL Maximum Contamination Limit
RPD
Relative Percent Different MinCL Minimam Compound Limit
ICV
Initial Calibration Verification RA Reanalysis
ICB
Initial Calibration Blank RE Reextraction
CCV
Continuing Calibration Verification TIC Tentatively Identified Compound
CCD
Continuing Calibration Blank RT Retention Time
RLC
Reporting Limit Check CF Calibration Factor
DF
Dilution Factor RF Response Factor
ects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any QuaB£iers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 29

����'� Summit Environmental Technologies,Ina WOT�OI'(leP
3310 Win St
ENVIRONMkNYAL TGCNNOLOSi�S, iNC Cuyahoga Falls, Ohio 44223 Sample SummaY'j'
pnalylfc8f L�tia�ralr3rlas TEL: (330J 253-8211 FAX (330J 253-4489 WO#: 18121225
Website: hita�//w viv settek com 04 -Jan -19
CLIENT: Synagro
Project: Dunn WTP
Lab SampleID Client Sample lD Tag No Date Collected Date Received Matrix
18121225-001 Dunn WTP 12/18/2018 2:30:00 PM 12/20/2018 11:50:00 AM Sludge
Page 5 of 29

� ; �EZ222!<7KE2iEy§
¢ q \
TIII
\\\\\\\\
% a `222--§eases -
2
\
/
:x„: /t\2)a/asses(/sera
) \
[ \ i
°{} 2
�) )
\
G\ |/
\
0
m
/
�

summ'll Summit Env;ronmentolTechnolog;es,ine. Ana lytiealReport
f1 3310 Win St.
ENVIRONMENTAL TVCHHOLGGIFS. INC Cuyahoga Falls, Ohio 44223 (base report)
ArWytfeal Laboralorlas TEL: [phone] FLY: [phone] Wit: 18121225
Website: htro // ttekcom Date Reported: 1/41
/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/18/2018 2:30:00 PM
Lab ID: 18121225-OOIA
Project: Dunn WTP
Client Sample ID Dunn WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST,
� Value exceeds Maximum Contaminant Level. E Value above quantitation range
Qualifiers:
H Holding times for prepazationor
HERB -SOLID
SW7470A
SW7470A Analyst: DNS
TCLP MERCURY ANALYSIS (SWI
31 11747 0)
analysis exceeded
M
Manual Integration used to determine area response
MC
TCLP Mercury
ND
0.00500
ND
mg/L
1
12/27/2018 4:36:00 PM
TCLP METALS, VOC, BNA; PEST,
HERB -SOLID
PL
Permit Limit Original
SW6010D
SW301OA Analyst: KMO
TCLP METALS ANALYSIS (SW131116
010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
12/28/2018 1:42:06 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
12/28/2018 1:42:06 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
12/28/2018 1:42:06 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
12/31/2018 6:34:16 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
12/28/2018 1:42:06 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
12/28/2018 1:42:06 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
12128/2018 1:42:06 PM
TCLP METALS, VOC, BNA, PEST,
HERB -SOLID
SW8270D
SW351OC Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW131118270)
1,4 -Dichlorobenzene
ND
0.0800
QMR
mg/L
2
1/3/20192:20:00 PM
2,4,5 -Trichlorophenol
ND
0.200
QMR
mg/L
2
113/20192:20:00 PM
2,4,6 -Trichlorophenol
ND
0.200
QMR
mg/L
2
113/20192:20:00 PM
2,4-Dinitfotoluene
ND
0.04007+QM-QAmg/L
2
1/3120192:20:00 PM
o -Cresol
ND
0.200
QMR
mg/L
2
1/3/2019 2:20:00 PM
nip-Cresol(s)
ND
0.200
QMR
- mg/L
2
113/2019 2:20:00 PM
Cresols, Total
ND
4.00
QMR
mg/L
2
1/3/20192:20:00 PM
Hexachloro-1,3-butadiene
ND
0.0160DC+QMRmg/1_
_
2
1/3/20192:20:00 PM
Hexachlorobenzene
ND
0.0400
QC+
mg/L
2
1/3/20192:20:00 PM
Hexachloroethane
ND
0.0800
QMR
mg/L
2
1/312019 2:20:00 PM
Nitrobenzene
ND
0.0800
QMR
mg/L -
2.
1/3120192:20:00 PM
Pentachlorophenol
NO
0.200
QC+
mg/L
2
1/3/20192:20:00 PM
Pyridine
ND
0.200QC+QMRmg11_
2
1/3/2019 2:20:00 PM
Surr: 2-Fluorophenol
26.2
10-109
%Rec
2
1/3/2019 2:20:00 PM
Surr: Phenol -d6
26.2
10-109
%Rec
2
1/3/20192:20:00 PM
Surr: Nitrobenzene -d5
73.4
19-120
%Rec
2
1/3/2019 2:20:00 PM
Surr: 2,4,6-Tribromophenol
28.8
10-120
%Rec
2
1/3120192:20:00 PM
Surr: 2-Fluorobiphenyl
74.8
22-117
%Rec
2
1/3/2019 2:20:00 PM
Page 7 of 29
analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7 of 29

UMMIT Summit Environmental Technologies,Ina Analytical Report
3310 Win S[.
ffIS
ENVIRONmEBYAL [e-mail]. INC Cuyahoga Falls, Ohio 44223 (basereport)
Analytical Laboralorlas TEL: [phone] FAX: [phone] WO#: 18121225
Website: hhup dhuww senekcom Date Report
ed: 1/4/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/18/2018 2:30:00 PM
Lab ID: 18121225-OOIA
Project: Dunn WTP
Client Sample ID Dunn WIT _
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270D SW351OC Analyst: BJH
TCLP SEMI -VOLATILES ANALYSIS (SW1311/8270)
Surr: p-Terphenyl-d14 112 34-116 %Rec 2 1/3/2019 2:20:00 PM
NOTES:
MS/MSD exhibited high RPDs due to suspected sample inhomogeneity.
The sample MSD exhibited low recovery for 2,4-Dinitrotoluene and Surrogates: 2,4,6-Tribromophenol and Pheol-d6. The sample MS and
the LCS exhibited control.
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8081 SW3510C Analyst: MES
TCLP PESTICIDES ANALYSIS (SW1311/8081)
Chlordane, total ND 0.0250 mg/L 1 12/30/2018 1:07:00 AM
Toxaphene ND 0.0500 mg/L 1 12/30/20181:07:00 AM
Endrin ND 0.00250 mg/L 1 12/30/2018 1:07:00 AM
gamma -BHC ND 0.00250 mg/L 1 12/30/2018 1:07:00 AM
Heptachlor ND 0.00250 mg/L 1 12/30/2018 1:07:00 AM
Heptachlor epoxide ND 0.00250 mg/L 1 12/3012018 1:07:00 AM
Methoxychlor ND 0.00250 dQC+ mg/L 1 12/30/2018 1:07:00 AM
Surr. TCMX 31.4 10-119 % Rec 1 12/30/2018 1:07:00 AM
Surr: DCB 24.1 10-119 % Rec 1 12/30/2018 1:07:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8151A SW8151A Analyst: MES
TCLP HERBICIDES ANALYSIS (SW1311/8151)
214-D ND 0.0500 mg/L 1 1/3/20194:39:00 PM
23415 -TP ND 0.0500 mg/L 1 1/3/20194:39:00 PM
Surr: DCAA 60.7 20-140 m % Rec 1 1/3/2019 4:39:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8260B SWI 311M Analyst: RMT
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND 0.0500 mg/L 10 12/27/20184:47:00 PM
1,2-Dichloroethane ND 0.0500 mg/L 10 12/27/20184:47:00 PM
MEK NO 0.250 mg/L 10 12/27120184:47:00 PM
Benzene ND 0.0500 mg/L 10 12/27/20184:47:00 PM
Carbon tetrachloride ND 0.0500 mg/L 10 12/27/2018 4:47:00 PM
Chlorobenzene ND 0.0500 mg/L 10 12/27/20184:47:00 PM
Qualifiers: * Value exceeds Maximum Contaminant Level E Value above quantitation range
H Holding tunes for preparation or analysis exceeded M Manual Integration used to determine area
Page 8 of 29
response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
O
RSD is greater than RSDlimtt
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 8 of 29

summly
Summit Envirorsmental TechnolWin St. Analytical Report
331010 Win St.
mn
ENVIRONMENTALTECnrapl,QS7E5,fN[: Cuyahoga Falls, Ohio 44223 (base report)
Arralytical Laboratories TEL: [phone] FAX [phone] WO#: 18121225
Website: &W lAvwivsettekcom Date Reported: 1/4/2019
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/18/2018 2:30:00 PM
Lab ID: 18121225-OOIA
Project: Dunn WTP
Client Sample ID Dunn WTP
Analyses
Result RL Qual Units DF Date Analyzed
TC LP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP VOLATILES ANALYSIS
Chloroform
ND
Tebachloroethene
ND
Trichloroethene
ND
Vinyl chloride
ND
Surr: 4-Bromofluorobenzene
86.7
Surr Dibromofluoromethane
93.0
Surr: Toluene -d8
92.9
RCI -SOLID -W/ IGNITABILITY7030
REACTIVE CYANIDE (901417.3.3.2) -SOLID
Cyanide, Reactive ND
SW8260B SW1311M Analyst: RMT
0.0500
SW7030
mglL
10
12/2712018 4:47:00
Holding times for preparation or analysis exceeded
PM
0.0500
Ignitability non-flammable
mg/L
10
12/27/2018 4:47:00
RCI -SOLID -W/ IGNITABILITY1030
PM
0.0500
VVK
mg/L
10
12/27/2018 4:47:00
PM
0.0200
12/21/20181:40:21
mg/L
10
12/27/2018 4:47:00
Analyst:
PM
70
-130
%Rec
10
12/27/2018 4:47:00
25.0 mg/Kg 1
PM
70
-130
% Rec
10
12/27/2018 4:47:00
PM
70
-130
% Rec
10
12/27/2018 4:47:00
PM
SW9014
Analyst:
MS
0.472 mg/Kg 1 12/2612018 1:30:00 PM
RCI -SOLID -WI IGNITABILITY1030
SW7030
Analyst:
AJT
IGVII TABILITY OF SOLIDS (SW -646: 1030)
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
Ignitability non-flammable
1
12/28/2018 4:00:00
PM
RCI -SOLID -W/ IGNITABILITY1030
SW9045D
Analyst:
VVK
PH (SW9045D)
pH 5.8
s.u.@20.4C 1
12/21/20181:40:21
PM
RCI -SOLID -W/ IGNITABILITY1030
SW9034
Analyst:
MS
REACTIVE SULFIDE (9034)17.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg 1
12/26/2018 1:30:00
PM
�
Value exceeds Maximum Contaminant Level.
Qualifiers:
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
P
Second column confirmation exceeds
R
RPD outside accepted recovery limits
Page 9 of 29
E Value above quantitation range
M Manual Integation used to determine area response
N Tentatively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit

Summit Enoironmental Technologies, Inc. Accreditation Program
����1� 3vowinst. Anal tesRe ort
EN41R0?JIdEN7AL rECDHpI,OGI€5, INC Cuyahoga Fa++s, Ohio 44223 y p
AnafyrtlCal La&ararorles TEL: [phone] FAX: [phone] WO#: 18121225
Website: htt �/Avww settekcom 04 -Jan -19
Client: Synagro State: NW
Project: Dunn WTP Program Name: NC_WW_SCM
Sample lD Matrix Test Name Analyte Status
18121225-OOlA SLudge Ignitabilily of Solids (SW -846'. 1030) ]Bnrtablhtl' A
Sludge pH (SW9045D) Hydrogen Ion (pH) A
Sludge Reactive Cyanide (9014/7.3.3.2) -Solid Cyanide, Reactive U
Sludge Reactive Sulfide (9034)/7.3.4.2 Sulfide, Reactive U
Sludge TCLP Herbicides Analysis (SW1311/8151) 2,4,5 -TP A
Sludge TCLP Herbicides Analysis (SW1311/8151) 2,4-D A
Sludge TCLP Herbicides Analysis (SW1311/8151) DCAA A
Sludge TCLP Mercury Analysis (SW131 V7470) Mercury A
Sludge TCLP Metals Analysis (SWI311/6010) Arsenic A
Sludge TCLP Metals Analysis (SW 1311/6010) Barium A
Sludge TCLP Metals Analysis (SW 1311/6010) Cadmium A
Sludge TCLP Metals Analysis (SW1311/6010) Chromium A
Sludge TCLP Mehals Analysis (SW 1311/6010) Lead A
Sludge TCLP Metals Analysis (SW1311/6010) Selenium A
Sludge TCLP Metals Analysis (SW1311/6010) Silver - A
Sludge TCLP Pesticides Analysis (SW 1311/8081) 2,2',3,3',4,4',5,5',6,6'- A
Decachlorobiphenyl
Sludge TCLP Pesticides Analysis (SW1311/8081) Chlordane, total A
Sludgy TCLP Pesticides Analysis (SWI311/8081) Endrin A
Sludge TCLP Pesticides Analysis (SW1311/8081) gamma -BHC A
Sludge TCLP Pesticides Analysis (SW 1311/8081) Heptachlor A
Sludge TCLP Pesticides Analysis (SW1311/6081) Heptachlor epoxide A
Sludge TCLP Pesticides Attalysis (SW13ll/8081) Methoxychlor A
Sludge TCLP Pesticides Malysis (SW1311/8081) Tetrachloro-m-xylene A
Sludge TCLP Pesticides Analysis (SW1311/808]) Toxaphene A
Sludge TCLP Semi -Volatiles Analysis (SW 1311!8270) 1,4 -Dichlorobenzene A
Sludge TCLP Semi -Volatiles Analysis (SWI311/8270) 2,4,5 -Trichlorophenol A
Sludge TCLP Sami-Volatiles Analysis (SW 1311/8270) 2,4,6-Tribromophenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4,6 -Trichlorophenol A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2,4-Dinitrotoluene A
Sludge TCLP Semi -Volatiles Analysis (SW1311/8270) 2-Fluorobiphenyl A
Sludge TCLP Semi -Volatiles Analysis (SW1311I8270) 2-Fluorophenol A
NC_WW_SCM
A Accredited
NC_WW_SCM
U Unavailable
Version
#2
Page 10 of 29

summit Environmental Technologies, Inc. Accreditation Program
SuM�mm1 3310 Anal tesRe ort
PHVIrtONMENrAL t[GHNp4CJSt£S; INC Cuyahoga Falls, OhioOhio 44 49223 y P
Analytical LaboYa prf98 TEL: [phone] FAX: [phone] WO#: 18121225
Website: hap11www settekcom 04 -Jan -19
Client: Synagro State: NW
Project: Dunn WTP Program Name: NC -WW -SCM
Sample lD Matrix Test Name Analyte Status
18121225-OOIA Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 2-Methylphenol A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) 3,4Wethylphenol A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Cresols, Total A
Sludge TCLP Semi -Volatiles Analysis (SW1 311/8270) Hexachlorobenzene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachlorobutadiene A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Hexachleroethane A
Sludge TCl3 Semi -Volatiles Analysis (SWI 311/8270) Nitrobenzene A
Sludge TCLP Semi -Volatiles Analysis (SW131118270) Nitrobenzene -d5 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Pentachlorophenol A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) Phenol -d6 A
Sludge TCLP Semi -Volatiles Analysis(SW1311/8270) p-TerphenyW14 A
Sludge TCLPSemi-Volatiles Analysis(SW1311/8270) Pyndine A
Sludge TCLP Volatiles Analysis 1,1-Dichloroethene A
Sludge TCLP Volatiles Analysis 1,2-Dichloroethene A
Sludge TCLP Volatiles Analysis 2-Butanone A
Sludge TCLP Volatiles Analysis 4-Bromofluorobenzene A
Sludge TCLP Volatiles Analysis Benzene A
Sludge TCLP Volatiles Analysis Carbon tetrachloride A
Sludge TCLP Volatiles Analysis Chlorobenosq e A
Sludge TCLP Volatiles Analysis Chloroform A
Sludge TCLP Volatiles Analysis Dibromofluorometbane A
Sludge TCLP Volatiles Analysis Tetrachloroethene A
Sludge TCLP Volatiles Analysis Toluene -d8 A
Sludge TCLP Volatiles Analysis Trichloroethane A
Sludge TCLP Volatiles Analysis Vinyl chloride A
----Key Key _
NC—WW—SCM A Accredited NC_WW_SCM U Unavailable
Version #2
Page 11 of 29

$
]
\
±
RaR
)
k
)
())(
)]
(+!\
\\
*j!)
�
))(\
\)
RaR
)
)]
\\
�
\)
\
0
}®k{

A
v a
r
�
a
Qo
r
W
J
m
F
F
Z
Ir
A
v a
Y
r
�
a
Qo
r
a
J
a
w
Z
Ir
f
r
E
M
y
!r
❑
n
0
g
❑
a
N
N
�
N
F
_
a
N
E
m
�
❑
=
r
Q
�
_
a
_
Q
Z
3
Q
°
N
N
D
0
o
E
V
J
E
Y
r
�
a
Qo
r
a
J
46
w
Z
Ir
f
r
-
M
y
!r
❑
n
�
g
❑
a
N
N
�
h
F
_
a
N
E
J
EI
o
=
r
Q
�
_
h
_
Q
Z
3
hi
2
N
N
D
0
o
E
V
J
E
Z
°
H
❑
_
N
�
a
3
a
5
o
f0
3
I
QJ
W
a
�
2
E
�
O
v
NO
K
5
~ Ci
Y
r
�
a
Qo
r
a
J
m
w
Z
Ir
f
r
-
�
y
!r
❑
n
Y
g
❑
a
�
N
�
h
F
_
a
N
E
J
EI
o
=
r
Q
�
_
h
_
Q
�
3
Y
2
N
N
D
❑
❑
E
V
J
o
Z
°
H
❑
_
N
�
a
3
a
-
f0
Y
r
�
a
c
r
a
J
m
w
Z
Ir
mN
N
E
c0
N
�
❑
n
0
g
❑
a
N
N
�
h
F
_
N
N
E
J
EI
❑
�
�
r
Q
16
E
_
Q
=
n
4B
o
P
r
D
❑
❑
E
Y
r
�
a
c
r
a
J
m
w
Z
Ir
mN
N
E
c0
N
�
❑
n
�
g
❑
a
N
N
N
n
F
_
N
N
E
J
EI
o
�
�
U
Q
m
E
_
=
n
4B
o
P
r
D
❑
❑
E
V
J
E
Z
°
❑
_
N
m
]
3
a
-
f0
3
I
Q
W
a
�
2
E
�
O
v
NO
K
5
~ Ci
Y
r
�
a
c
r
a
J
m
w
Z
W
mN
N
E
a
N
�
❑
n
Y
g
❑
a
�
N
n
F
m
a
Y
J
EI
o
�
�
U
Q
m
E
_
�
n
J o m
o
P
r
D
v
V
E
V
J
o
Z
°
❑
m
N
m
]
E
di di
(❑Wy
C4
f0
Y
r
�
❑
r
c
J
N
w
Z
W
mN
N
E
a
ra
!Y
�
n
0
g
❑
a
9
�
N
F
m
ET
Y
N
EI
❑
f9
U
Q
m
E
_
�
n
J o m
o
P
r
D
v
V
E
V
J
m
°
❑
m
=
m
]
E
di di
(❑Wy
C4
f0
3
I
W
a
�
LW
a
m
c
N
N
N
a -
mN
h
E
a
ra
!Y
�
a
0
g
❑
a
9
�
N
F
m
ET
Y
N
EI
❑
f9
U
Q
r
a
c
N
N
N
a -
M
h
E
a
ra
!Y
J
J
0
F
❑
a
9
�
N
m
�
Y
N
EI
❑
r
N
m
E
a
a
c
N
N
N
a -
-
n
E
a
ra
!Y
!Y
0
F
❑
a
�
N
m
�
Y
N
EI
❑
r
N
m
E
_
�
n
J o m
o
P
r
D
v
V
w
a
a
c
N
N
N
a -
-
n
a >
a
ra
!Y
!Y
o
F
❑
w a
m
�
Y
N
EI
N
m
E
_
�
n
J o m
o
P
r
D
v
V
w
V
J
c
°
❑
❑
=
]
E
di di
(❑Wy
C4
m
3
I
� Z
a
�
2
E
�
O
v
NO
5
~ Ci
N
N
a
N
�
Z
a —
J
Q
o
o
5
b
Q
m
a.a
wO
❑
d
u
a
L
~
H
F
v U Q
a
a
c
N
N
N
a -
-
n
a >
a
ra
!Y
E
o
F
� W �
Y
m
H
Y
N
EI
E m
m
E
a
�
n
J o m
o
P
r
D
v
V
w
V
J
c
°
❑
❑
Z N �
]
E
rLr��ljj
G4
(❑Wy
C4
m
3
I
� Z
a
-
2
� d
�
O
v
NO
5
~ Ci
N
N
a
N
�
Z
f=
Q
o
o
5
b
9
m
a
D
N
N
N
a
-
n
!r
a
ra
!Y
E
o
F
o
0
m
H
Y
N
EI
E m
m
E
�
n
❑
P
r
N
V
w
V
J
c
°
❑
❑
]
E
rLr��ljj
G4
(❑Wy
C4
m
3
I
3
a
-
2
� d
�
v
Q
5
N
N
b
b
�
Z
U
Q
o
5
b
9
m
a.a
wO
❑
d
u
a
E
~
H
F
v U Q
a
D
N
N
N
a
-
n
!r
a
ra
!Y
E
o
F
o
0
m
a
Y
N
EI
m
E
�
n
❑
P
r
a
V
w
V
J
c
°
❑
❑
]
E
rLr��ljj
G4
(❑Wy
C4
m
3
a
c
N
N
N
a
-
n
!r
a
ra
!Y
o
F
o
a
m
m
Y
N
EI
m
E
�
n
P
N
a
V
w
V
J
c
�
❑
❑
]
E
rLr��ljj
G4
(❑Wy
C4
m
3
I
3
a
-
2
N
�
v
Q
5
U
N
b
b
�
Z
U
Q
a
c
N
N
N
a
-
n
!r
a
ra
>
o
F
o
m
m
Y
N
EI
m
�
n
P
N
a
V
w
V
J
c
�
O
]
�
rLr��ljj
G4
(❑Wy
C4
m
3
I
9
2
N
�
v
3
5
n
N
b
b
�
Z
U
Q
o
5
b
7
o
a.a
wO
~
d
i
N
a
~
Z
w
o
:J
❑
N
N
N
0.1
n
!r
a
�
o
F
o
m
m
N
EI
m
y
P
N
�b
V
w
V
3
'�
v
i
�
rLr��ljj
G4
(❑Wy
C4
m
3
9
9
v
3
5
n
N
b
b
fn
U
Q
:J
0.1
o
b
o
�aaPEI�
?
o
EI
m
y
P
N
�b
V
w
V
3
'�
i
�
rLr��ljj
G4
(❑Wy
C4
3
:J
0.1
u�
5
a
?
N
V
w
V
O
3
3
5
n
N
b
b
a
00
o
5
b
7
o
a.a
>
rMi
i
vi
Z
w
2a
:J
a
?
V
w
V
3
�
00
5
b
7
o
>
rMi
i
vi
:J

o
E'
b
�3
C
N
�
F
F
N
�
m
L
V
�r
�
M
J
�
Cl
N
n
m
�
o
E'
b
�3
C
N
�
F
F
N
�
o
N
b
V
C
❑
M
o
N
V
❑
M
N
�
m
L
`
�
J
d
J
�
Cl
N
a
�
LLLD
m
E
J
co
U
¢
o
V
❑
N
a
�
m
L
`
�
d
'2
�
N
N
o
V
❑
N
a
�
m
N
N
�
d
'2
a
9
cV
a
�
LLLD
m
E
J
A
U
Q
o
V
❑
tll
a
�
�L
N
�
d
d
v
N
cV
o
V
❑
tll
a
�
�L
N
�
d
�
v
N
IV
a
�
o
n
q
J
N
m
N
�
o
o
M
o
O
O
e
!a-
n
�
N
N
o
�
N
G
3
>�a°d
m
❑
�
>
>
x
d
caE
0
Z
w
U
Q
❑
a
�
�
v
N
IV
v
�
a
o
�
q
J
T
N
�
o
o
M
o
O
e
n
�
�
N
o
�
w
3
>�a°d
v
�
a
�
J
T
N
�
o
M
o
O
e
n
a
N
o
�
w
3
>
>
x
d
y
0
Z
x
a
w
a
�
J
T
b
�
o
M
a
�
o
�
w
3
>
>
x
y
x
�
w
n
d

%
k
/
l
)
�
)/
(}\\
\)
\\)\
m
it4
\\
)][)
0
\)
\)\(
)
c)
l
)/
\)
m
\\
0
\)
)
7)7\
£
\}0
\/\\
■

a
M
R
A
R
- m N m N N N N m rn N d N � N N iM
� m m c`o � 0 0 w 0�
N N O N O O O O O N O
v e' m❑ O m �- v
C O 0
N o T
m L v N o v N a o d
oa ^ _ - ~ 0 E
- m n o m o a N r
w~ O 0 0'V — N d Z N
U F7 C 0 41 _ U U L o U C �`. C 6
N Vo a N N x p C T 0 N N m 0 0
C4 -N E0x=xzaa
W
v
�
a
.8
�
.1
p
o
o
CO
�
o
�
a
�
w
o
�
P
C
7
�
a��zw
0
0
o.
6
6
o
0
6
0
0
6
N N O N O O O O O N O
v e' m❑ O m �- v
C O 0
N o T
m L v N o v N a o d
oa ^ _ - ~ 0 E
- m n o m o a N r
w~ O 0 0'V — N d Z N
U F7 C 0 41 _ U U L o U C �`. C 6
N Vo a N N x p C T 0 N N m 0 0
C4 -N E0x=xzaa
:i
W
v
�
a
.8
�
.1
p
o
o
CO
�
o
�
a
�
w
o
�
P
C
7
�
a��zw
:i
a
�
.1
p
CO
o
CO
E
�
w
o
�
P
C
7
�
:i

C3 aC3 N N o
�W/ o p
Oct
m 0 0 0 0 0
q�
� m F
W vo rn •+ LT
��co
V Z zIs
v P�
tb
M v
N VO O GO O N (O p
mr <o m M„
000om o '�" 5
p K o 0 0 0, 0
U m >zq
a
x
OOT
p p E6
M N O N N N N N C O N N N
LD - o
J
Q i
�% a0 d'
<v
N
w NMVONNON oi Nn 4 �m N CN Nn "G
a
N
�e ho`GNNMFLCwL y�y' y so oidyC
� aFvPJFzrnE„cF-iN❑N
p
�mD
Jv°�"vTw0
ya.
av0c
o
O
_ OlO
0
o 0!0,00 00 0 0
> N d6
l
0.a
a 0
00
0 0400,N
O
0 000 0
004
Z Z
u co O O 6 0 0 0 0 O Oa O o of
0U
w O M oS `
OC 1
m � 6.
C U VV d Z cV N
o F7 F7 aN
Oct®� 6 w C) EcxZm

(/
ff
)A
z
wo
4
}
46
r),\
)A
z
wo
4
}
46
r),\
\ `
z
wo
4
}
46
r),\
\
/7)E
,
^t
\�
\�
\
E
\\);
\\
\\.
\j\)
\\
\
±
z
4
}
46
r),\
\
/7)E
,
^t
\�
\�
\
E
\\);
\\
\\.
\j\)
\\
\))\
){{)
�4
)2
))>j
\/
\
(
®()
/2)!
,;/,
=,2:
\\\
\
\
±
z
4
}
46
r),\
\
/7)E
,
^t
\�
\�
\
E
\\);
\\
\\:
\j\)
\\
\))\
){{)
�4
)2
))>j
\/
\
\
\
±
z
4
}
46
r),\
\
/7)E
,
^t
\�
\cl
\
E
\\);
\\
\
±
z
4
}
46
r),\
/7)E
^t
\�
\cl
\
E
\\);
\\
\\:
\j\)
j\
\))\
){{)
�4
)2
))>j
\
®()
/2)!
,;/,
=,2:
/\
\
\
±
z
4
}
r),\
/7)E
^t
\�
\cl
/
\
\
±
z
4
}
r),\
/7)E
^t
\cl
/
\
\
±
z
4
}
r),\
/7)E
^t
)\;{
\\);
\\
\j\)
j\
\))\
){{)
�4
4
))
^t
)\\\
\\
)�
j\
){{)
)2
))>j
§}«0
®()
/2)!
,;/,
=,2:
)\\\
)�
j\
){{)
))>j
§}«0
/2)!
,;/,

46
n
�
o
N
N
w
r
J
K
y
J
K
�
2
a
K
n
a
U
J
nL'
aCY
a
F
D
m
v
E
m
00)
b
J
m
_
N
�
�+
E
m
E
v
o
c
Q
E
E
�
O
E
3
�
S
E
fn
U
E
o
N
d
S
W
W
❑
❑
E
❑
J
E
J
E
�
J
o
�
p
�
a
T
O
o
a
O
�a�za
c
J
Q
U
U
�
U
x
K
a
N
�
m
pa
V
wo
N
N
N
—
N
>
r45
46>
S
�
m
7
Y
Y
N
a
v
w
❑
O�1
y�j
_
O
OI
v
—
r
O
�
>
2
I
N
Y
Z
Z
�
Z
Z
Z
m
Z
Z
o
c
C
Z
c
Q
N
U
�
J
0
~
U)
K
F=
K
m
(n
q
46
n
�
o
N
N
w
r
J
K
y
J
K
�
2
�
K
n
�
U
J
nL'
eo
a
F
D
m
v
E
m
00)
b
J
m
_
N
�
�+
E
m
E
v
o
c
Q
av
E
�
O
❑
3
�
S
_
fn
U
S
o
N
d
S
W
W
❑
❑
E
❑
❑
E
E
�
—
o
�
T
�
a
T
O
o
a
O
�a�za
c
J
Q
U
U
�
U
x
K
a
N
�
m
pa
V
wo
N
N
N
—
Q
>
r45
46>
S
�
7
Y
Y
N
a
v
w
❑
O�1
y�j
_
O
OI
v
—
r
O
�
>
2
I
N
Y
n
�
Z
m
U
Z
U
�
J
0
~
a
F=
46
n
�
o
N
N
N
r
J
K
y
J
K
�
2
�
❑
n
�
U
J
nL'
eo
❑
a
F
D
m
v
E
m
00)
b
J
m
_
N
�
�+
E
46
a
y
N
y
j
r
W
y
J
�
=
�
❑
n
�
U
J
C
eo
❑
a
F
D
m
v
N
00)
b
J
m
_
N
�
�+
E
m
E
v
o
c
46
a
y
N
y
j
r
�
J
�
=
�
❑
n
�
a
C
eo
a
F
D
m
v
N
00)
b
J
m
_
N
�
�+
E
m
E
v
o
c
Q
av
E
�
O
❑
3
�
S
_
fn
U
S
o
N
d
P
o
�
❑
❑
E
W�oa
E
�
—
o
v
T
�
a
—
O
o
J
�a�za
Q
U
W
�
U
x
�
a
N
�
m
pa
V
wo
N
N
N
—
Q
>
46>
S
�
7
Y
Y
N
a
a
N
❑
O�1
y�j
_
O
OI
v
—
r
O
N
Y
2
I
N
Y
nl
�
Z
m
U
Z
U
�
J
N
a
46
a
y
N
y
j
r
�
J
�
=
�
❑
n
�
a
C
eo
a�
F
D
NW'
v
N
00)
b
J
m
_
N
�
�+
E
m
J
v
46
a
y
N
y
j
r
�
K
=
U
❑
n
�
a
C
eo
a�
FT
D
NW'
v
N
00)
b
J
J
_
N
❑
�+
E
J
v
o
c
Q
av
E
�
O
❑
3
�
S
_
fn
U
Q
o
46
a
y
N
y
j
r
�
K
=
U
❑
n
�
a
C
eo
a�
FT
D
NW'
v
N
00)
b
E
N
_
N
�+
E
J
v
o
c
Q
av
O
❑
3
�
S
=
o
N
a
P
o
�
0
0
E
W�oa
E
a
—
o
v
T
�
a`
O
o
�a�za
a
W
m m
o
U
x
�
a
N
�
m
7
wo
N
N
N
>
Q
>
�
S
�
❑
Y
a
N
�/1
m
O�1
y�j
_
OI
0
>
O
N
Y
2
I
N
U)
2
�
Z
U
Z
FF-
�
J
46
a
y
y
7
�
=
U
n
�
C
eo
a�
FT
D
NW'
v
00)
b
E
N
N
_
E
v
o
a
Q
av
O
❑
3
�
V
=
o
N
a
P
a)
0
0
W�oa
E
o
v
T
�
a`
O
o
�a�za
a
m m
�
U
x
�
a
�
m
wo
N
U
Q
46
a
y
y
7
�
=
U
n
�
C
eo
a�
FT
D
NW'
v
00)
b
E
N
N
_
E
v
o
a
Q
av
O
❑
3
�
V
=
o
N
a
P
a)
0
0
W�oa
E
o
v
T
�
a`
O
o
�a�za
a
W
�
U
x
�
a
N
—
ca
>
C
�
❑
Y
a
a
O�1
y�j
V
—
O
�
>
I
N
2
�
vo
Z
U
�
J
r
a
y
y
7
�
=
U
n
�
C
b
A
FT
D
NW'
v
00)
b
E
m
N
ru
v
o
U
Q
r
a
m
=
U
U
J
C
b
A
D
NW'
v
00)
b
C
a
N
ru
v
o
U
Q
av
J
a
m
C
b
A
a
NW'
v
00)
b
C
a
N
v
o
o
av
O
❑
3
�
V
�
o
N
a
P
a)
W�oa
J
m
�
C
.
00)
b
C
N
v
o
av
O
❑
3
�
V
N
a
P
a)
o
v
�
o
�a�za
J
�
s
.
b
C
y
v
o
❑
Up
�
V
3
a
a
o
v
�
o
x
�
a
J

§
�
«
)
�
(®)�
))
\j)\
!e]§
\\
)a\n
=>:a
«
))
\\
\\�\
«#2:
■

«
§
a
\
a
\
k
cf
\
())(
\\
)/
\�
>).
§2:
\/
)}){
\
\
a
\
k
())(
\\
)/
\�
>).
§2:
\/
)}){
\
\\
\\.
\)(/
\)
\
�4
\)§/
\
\
}}))
;42�
�=-2y
/\\
\
a
\
k
())(
\\
)/
\�
>).
\
a
\
k
())(
\\
)/
>).
\/
)}){
\
\
a
\
k
())(
)/
>).
)}){
\\
\)(/
\)
\
�4
«
)/
>).
\\
\)
\
\)§/
\
}}))
;42�
�=-2y

N
❑
N
=
m -
❑
E
N
N
N
a
n
0
�
v
5
R'
T
d' K
C
�
A
E
m
p
y
c4
C
p
N
U
p
N
a
N
W
x
O
PG
N
❑
N
=
m -
❑
N
N
N
a
n
0
R'
T
d' K
E
m
p-
Co
o
C
a
N
H
0�6 �
m
q x u
d a
m d N J J
Q a E
y •o E d � E v T �
U F4 co 0 Q 0 (9 U Q U tO U Q U
T
=
N
N
N
a
n
0
T
b
E
m
p-
Co
o
C
a
N
U
p
N
a
N
x
m
w
�
O
�
O
E
in
U
Q
a
T
b
p-
Co
o
C
a
pvpi
p
x
�
w
O

f
\0
B
\
�
{\
\
�
\
))
(}\{
\
CY
\�
\
2
^�
§
2
\j)\
£E!!
})\
\
fj[0
0
)}\(
:(\ma
\)
f
f
\0
B
\
�
{\
\
�
\
))
(}\{
\
CY
\�
\
2
^�
\j)\
£E!!
})\
\
fj[0
0
)}\(
\*}
\)
f
\0
B
\
�
{\
\
�
))
(}\{
CY
\�
\
2
^�
f
\0
B
\
�
\
\
))
(}\{
CY
\
2
^�
\j)\
£E!!
\\
\
fj[0
f
\0
)�\
j
\
�
\
\
))
(}\{
\
2
^�
\j)\
£E!!
\
�CD
fj[0
0
)}\(
\)
)�\
/
j
\
�
\
\
/
\
�
))
(}\{
^�
\j)\
£E!!
\\
fj[0
0
)}\(
\)
#
))
^�
m
\\
0
\)
f
))7)
/
\}\}
)!2PL

J
m
s
O
Z
E
N
—
o
�
K
�
d
m
❑
a
a
�
d
F
a
-
�
a
°
E
m
r
E
u
_
a
�
r
m
y
in
E
=
N
N
X
o
K
v
❑
❑
d
�
E
E
9
o
E
�
-
E
w'
3
a
E
o
tll
.
E
Q
o
01
N
Z
-
N
U
Z
J
-
H
E-
J
>
�
T
a
N
�
—
°
F=
a
�
Q
aof
Z
_w
�
a
a
c
a
W^2;
E
rm
fL
m
0
Un
J
U
Q
OI
E
�
�
7
Y
�
❑
U
m
a
m
m
❑
K
y
v
o
a
a
o
aa
ai
w'
aY
..
..
af
N
�
Z
Z
Z
Z
Z
a
o
H
d
Lo
o
H
v
�
�
N
mo
J
m
s
O
Z
E
N
—
o
�
K
�
d
m
❑
❑
a
�
a
F
a
-
�
a
Y
E
m
r
E
u
_
a
�
r
m
y
in
E
=
N
N
X
o
K
v
❑
❑
d
�
;
E
9
o
Q
�
-
>
w'
3
a
_
o
tll
.
E
Q
o
01
N
Z
E
N
U
Z
J
-
H
E-
J
m
s
O
Z
E
N
—
o
�
K
�
d
m
K
❑
K
�
a
F
a
-
�
a
Y
E
m
Y
u
_
a
�
m
m
y
in
E
;
in
a
X
o
K
v
a
=
d
�
;
_
9
o
Q
n
O
>
w'
N
W
Y
P
tll
.
E
0
o
01
N
Z
E
N
U
Z
J
-
H
E-
d
>
�
T
a
N
�
—
Oa`
F=
U
�
J
m
s
O
Z
m
N
N
o
�
K
�
d
m
K
❑
K
�
a
F
a
-
�
a
Y
E
m
a
u
_
rn
�
in
m
E
J
m
s
O
E
N
—
o
m
K
K
d
m
K
❑
K
�
a
m
a
-
�
a
Y
Fr
m
a
u
_
rn
�
m
m
E
in
E
;
in
a
X
o
d
v
a
=
a
�
;
_
9
U
Q
n
J
m
s
O
E
N
—
o
m
K
K
d
�
K
❑
K
�
a
H
a
H
J
Y
Fr
m
a
u
_
rn
�
m
m
E
in
E
N
in
a
E
o
d
N
�
o
a
�
;
_
3
O
=
w'
N
W
E
P
N
a
E
0
o
01
N
Z
E
N
U
N
J
-
H
E-
d
>
�
T
a
N
�
—
Oa`
g
U
�
Q
d
Z
_w
U
a
W
W^2;
E
�
fL
U
0
Un
J
U
Q
J
m
s
O
E
N
—
o
m
K
K
d
�
K
❑
K
�
a
H
❑
H
J
Y
Fr
m
a
u
_
rn
�
m
m
E
in
_
N
in
a
E
o
d
o
�
o
a
�
;
_
3
O
Y
w'
❑
❑
E
P
N
a
E
2
o
01
N
Z
J
N
U
N
J
-
H
E-
d
>
�
T
a
N
�
Q
O
s
J
V
m
s
OI
E
N
45
d
m
K
K
d
�
K
❑
K
�
a
H
❑
H
J
Y
Fr
m
�
E
_
❑
�
E
m
E
in
_
N
in
E
s
J
V
s
OI
E
N
45
d
m
K
K
d
d
v
❑
K
�
a
H
❑
H
J
Y
J
m
�
E
_
❑
�
N
E
in
_
N
w
E
Fd
o
E
�
_
3
O
Z
w'
s
J
V
s
OI
E
N
45
d
m
K
K
d
d
v
❑
N
p
a
H
❑
H
m
Y
E
m
�
E
_
❑
�
N
E
in
_
N
w
E
Fd
o
v
a
a
3
O
Z
w'
❑
❑
E
P
N
a
E
2
o
01
N
V
J
N
i
N
-
o
o
>
�
T
J
N
d
Q
O
g
U
�
Q
d
Z
_w
W
a
K
W^2;
E
�
m
U
0
Un
J
U
Q
OI
E
7
Y
�
a
U
m
v
K
y
v
o
a
o
ai
w'
aY
"
Z
U
H
d
Lo
a
H
s
J
V
s
OI
E
N
w
d
m
K
>
d
d
v
N
N
p
H
❑
H
m
Y
E
m
�
E
m
❑
N
in
_
N
w
E
Fd
o
v
a
a
3
O
Z
w'
n
U
E
P
N
a
co
0
o
01
N
V
E
N
N
N
-
m
a
>
�
T
N
d
O
g
�
Q
d
Z
_w
a
W^2;
E
�
m
U
Q
Un
s
J
V
s
OI
E
v
P]
d
K
>
d
v
N
H
❑
m
Y
E
m
�
❑
N
m
_
N
w
E
o
v
a
a
3
O
Z
w'
N
E
P
u
co
0
o
01
a
Z
E
N
b
~
a
>
F
T
N
d
O
g
�
Q
d
Z
w
W^2;
E
�
m
�
r
A
U
Q
s
J
V
s
OI
E
v
P]
d
K
>
d
v
q
H
o
Y
E
m
❑
m
�b
w
o
v
a
a
3
O
O
w'
N
E
P
u
co
N
a
01
a
Z
N
b
~
a
>
F
m
N
c
0
s
v
P]
d
K
d
v
q
H
o
E
m
N
�b
w
o
a
O
3
O
O
w'
N
E
P
u
N
a
01
N
b
N
>
m
c
g
�
d
d
Z
w
W^2;
E
�
m
A
U
Q
0
s
v
P]
d
c
v
q
o
N
�b
o
a
O
3
W
O
w'
:I
P]
.e
N
O
3
tl7
N
E
P
01
b
CL
b
d
d
Z
w
W^2;
:I

§
!
\\
\
±
\
k
!
{
(}\[
�G\
\§\
\�
\
)
\/\
\\\
){){
(
!
!
\
\/
\j{)
\
±
\
k
!
{
(}\[
\§\
\§\
\�
\
)
\/\
\\\
){){
(
!
!
\
\/
\j{)
{
)
))(\
w
\
\
±
\
k
!
{
(}\[
\§\
\§\
\�
)
{
\/\
\\\
){){
(
!
!
\
\/
\j{)
\
±
\
k
!
{
(}\[
\�
\§\
\�
)
\
±
\
k
!
{
(}\[
\§\
\�
)
{
\/\
){){
(
!
!
\
±
\
k
!
{
(}\[
\§\
\�
)
{
){){
(
!
!
\
\/
\j{)
\
)
))(\
w
\
\\
\
wo
\\
\
±
\
k
!
{
(}\[
\§\
\�
)
{
){){
\\\
!
\/
\j{)
\
)
))(\
_«
\\
\
\\
\
±
\
k
(}\[
\§\
\�
)
{
){){
\\\
\j{)
\
)
))(\
_«
\
±
\
k
(}\[
\§\
\�
){){
\\\
\j{)
\
±
\
k
(}\[
\�
){){
\j{)
))(\
_«
\\
\
\
±
\
k
(}\[
){){
\j{)
))(\
_«

P5
PW
wa
\/
a k
%7�,;
7§]
�
�
m
\
2

summ,y Summit Environmental Technologies, Inc.
ff13310 Win St
FNVIRONMENTALITCHNOLOMIES,INC, Cuyahoga Falls, Ohio 44223 Sample Log -In Check List
Anafyllcal tabararorlea TEL: [phone] FAX. [phone]
Website: htto //www.settek.com
Client Name: SYN -NC -27028 Work Order Number: 18121225
Logged by: Antonio Betscakos
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
Chain of Custody
1. Is Chain of Custody complete?
Z. How was the sample delivered?
Loa In
3. Coolers are present?
RcptNo: 1
12120/2018 11:50:00 AM
12120/2018 6:48:14 PM
12/21/2018 9:46:28 AM
4, Shipping container/cooler in goad condition?
Custody seals intact on shipping container/cooler?
No. Seal Date:
5. Was an attempt made to cool the samples?
6. Were all samples received at a temperature of >0" C to 6.O�C
7, Samples) in proper container(s)?
g. Sufficient sample volume for indicated test(s)?
9. Are samples (except VOA and ONG) properly preserved?
10. Was preservative added to bottles?
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
14. Were any sample containers received broken?
13. Does paperwork match bottle labels?
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
15. Is it clear what analyses were requested?
16. Were all holding times able to be met?
(If no, notify customer for authorization.)
Special Handling (if applicable)
Yes❑
UPS
Yes
Yes ❑�
as ❑
Signed By:
Yes ❑�
Yes ❑�
Yes
as 0
Yes
Yes ❑
Yes El
Yes ElYes 0
Yes 0
Yes 0
Yes ❑�
No
❑
Not
Present
❑
No
13NA
1
5.7
11
No ❑
No ElNot Present❑
No ❑ NA ❑
No ❑ NA
11El❑
No ❑
No
No
No R1 NA ❑
No ElNo VOA Vials
El1:1El❑�
No❑
No ❑
No
No
No
17. Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA❑
Person Notified:
By Whom:
Date
Regarding:
Client Instructions:
16. Additional remarks:
Cooler Information
Cooler No
.Temp °C
Condition _Seal
Intact
Seal No
Seal Date.
Signetl By
1
5.7
Good Not Present
❑
eMail
❑
Phone
❑
Fax
❑
In
Person
Cooler No
.Temp °C
Condition _Seal
Intact
Seal No
Seal Date.
Signetl By
1
5.7
Good Not Present
Page 29 of 29

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City
of Dunn
WQ Permit Number:
W00006101
Compost
Heat Drying
WWTP Name: City
of Dunn WWTP
NPDES Number:
NC0043176
Pasteurization
Monitoring Period:
From 01/01/2018
To 12/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative
performed (Class A only)
indicate "Process to Further
Reduce Pathogens":
Compost
Heat Drying
Heat Treatment _
Thermophilic
Beta Ray _
Gamma Ray _
Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
ua ucau�ewaum
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
/Alt
0 tion/Alt. 1 Option/Alt.2 Optien t.3 Option
unuvc c..o, ...c., ..."�.,
.-.... .-..,.,.,-- ..�... ...-.. ...--....-..-.. .__________
-__.
No.
Frequency
Sample
Analytical
Parameter
Allowable Level in Sludge
Pathogen Density
of
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10 to the 61h
MPN
MPN/g
Coliform
power per gram
of total solids
<39100
<39500
<40200
CFU/g
0
Annually
grab
9222D -
CFU
MF
1000 NTN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 NUN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
.4
(Ureduction) reduction) x (40 -day bench) (30 -day bench) (Spec. 02 uptake)
Option[Mt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14 -Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying—Unstable)
Option/Alt.9 Option/A1t.10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 an
d the vector attraction
% reduction requirement m 40 CFR 503.33/15A NCAC 02T1107 have been met"
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T. 1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T. 1107 have not been met" (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Domie Dukes Wastewater Treatment Plan
t Supervisor
P er Name and Title e or print)
ONN.AA 0 VZ: —. A
Signature ofPreparer* DateWL J
Land Applier Name and Title (if applicable) (type or print)
Signature of Lan
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)
d Applier (if applicable)

Cameron Testing Services, Inc. Laboratory Report NC DENR #654
NC PHHS #37799
US EPA #NCO1918
71
W
:0.
Yes
Dunn WWTP
Sample Information
NCO
ffix
W Varner IW C)3113118 J.Zubeck 03/13/18
ti5y
Analyses and Results
180434 D1 R sw�e or Fee. Coliform -S x39700 OFwa 39700 03113!18 ERP 9222D -MF
b <39400 uuja 39400
C 39200 cFu/g 39200
d <39100 cFulg 39100
0 <40200 cFura 40200
f 39200 cFWa 39200
9 <39400 eF010 39400
Geonjean 39600
160434 01 a sludge Gr TS (010) 2,82% 0.01 03113M0 ERP 2540 G -T;
b 2.54% 9.01
0 2.55%u 0,01
d 2.56% 0.01
a 2.49% 0.01
f 2.56% 0.01
9 2,54% 0101
Review
Project Manager Date
919-203-4240
219 S. Stecle SV,
Sanford NC 27330 chrisncamerontes6ng.can

�T
p \
N
7
U
o
O
C
VI
m
L
U
rn
a
i
ILI^
N p
?
illli
1 'Svh
1IL
1��P
LI
o
z
u
nj
ppp
2L
LIP
10410
I.'
All
__
_
— ,, _.
. _...---�....
ss81O 'zo 6
I
lot.
E
�
' Q
OOA l Ob
�
ma@J
n
'�^i
8p81�e9�
__.-
.
..._.-.�
....;_.
009_..
��
'I8U ZIb
SL
r''+ILI
s
�v
5,7
(NIA) eel
I
XPION
�._
GLielt
I
J
JE)
jr
�dwoo
S
--
--- --�-
--
---___.�
-
N
y
ewil
N
r
4
\
o�sJ
ca
> m
y
aCL
OD
_
GC
E
K
rn
rnILL
I

Black River Wastewater Treatment Plant
City of Dunn
2018
April 2018 Vector Attraction
Rec.—.79
Holding Tank—.69
September 2018 Vector Attraction
Rec.—.81
Holding Tank --.72

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Dunn WQ Permit Number: W00006101
WWTP Name: City of Dunn WTP NPDES Number: 03-43-010
Monitoring Period: From 01/01/2018 To 12/31/2018
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt 1/A (time/temp) Alt. 2/B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens _ Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment _ Thermophilic
Beta Ray Gamma Ray _ Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If a licable to alternative erformed Class A or Class B tom tete the [auowm mumronn uxiN of
t
Vector Att
Pathogen Density
xi-
.
Exeee-
Frequency
of
Sample
Type
Analytical
Technique
Parameter
Allowable Level in Sludge
Minimum Geo. Mean Maximum Units
dentes
Analysis
Fecal
2x10 to the 6"
MPN
MPN/g
Coliform
power per gram
of total solids
CFU
<22100
<32100
<41000
CFU/g
0
Based on
Land App.
grab
9222D -
MF
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform
raction Reduction (40 CFR 503.33/15A NCAC 02T.1107) -Please indicate option/alternative performed:
Option/Alt. 1 Option/Alt. 2 Option/Alt. 3 Option/Alt. 4
(VS reduction) (40 -day bench) (30 -day bench) (Spec. 02 uptake)
Option/Alt. 5 Option/Alt. 6 Option/Alt. 7 Option/Alt. 8
(14 -Day Aerobic) (Alk Stabilization) (Drying — Stable) (Drying—Unstable)
Option/Alt. 9 Option/Alt. 10
(Injection) (Incorporation) No vector attraction reduction alternatives were performed x
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector att
raction
X reduction requirement m 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 50332/15A NCAC 02T.1106 and Lite vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met" (Please note if you check this statement attach an
_ explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. 1 am aware that there are significant penalties for false certification including fine and imprisonment"
Ian Stroud Wastewater Treatment Plant Supervisor
Preparer Name
rd Title ( or print) � � � � � � p
rgnature of reparer* Date
/�1LI1_
Land Applier Name and Title (if applicable) (type or print)
Signature of Land
*Preparer is defined in 40 CFR Part 503.9(x) and 15A NCAC 2T.1102 (26)
Applier (if applicable)
Date

II I NODENRJ
,ameron Testing Services, Inc. Laboratory Report NC PHHSln7a
US EPA ,.;
a, 1 1
4 t
� °� �13aYes
Sample Information
d ir.:Eli, r, ,.W. Varner- -
03/13/18 6 J.Zubeck 03113118
Analyses and Results
180433 01 8 �mder cr Fec. Coliform -S 431800 cFurO 31800 03!13/18 ERP 92220 - MF
b <22100 Uure 22100
C <31800 CFU/9 31800
d <31400 cFu10 31400
e 441000 cFU/9 41000
f <30700 OFwg 30700
9 <39500 cFWg 39500
Geom2an 432100
180433 01 a 3Iude4 or TS (%) 3.14% 0.01 03113/18 ERP 2540 G -TS
b 4.53% 001
C 3.14% 0.01
d 3.18% 0.01
e 2.44% 0.01
f 3.26% 0,01
g 2.53% 001
Report /
Review
Project Manager Date
21.9 B..Steele Str. ', 919-208-4290
Sanford NC 27330 ch�isQcamer0n[es[ing.com

aid, ^'
II
o
O
N
a
U
o
��
�
1SIL
t
F
U
rn
Yi
aid, ^'
s •�
��
�
t
F
Iota
2S
If
°� t
�Oft
TOOO
1y
o. sLTZ
a
��
ON
kL
�; Y
r
Zx
m
i
I.
TO','
yf
r'
TV
u. 17
Jg4a0
4.rL.+
cc
I F
SSI d20 g
�{
ji,-
-
jr—if
011s�ld l 4
It
8Of
2
I
m
m
Iwo;
°N
0
2
'
OOA 1w 04
,
E
m
eua{aeg
----
..i
.•..
004
i
rt�1
'ISE)Zf4
Lf
(N/A)801
' I
JT,o'
X14evq
}
-
q�dLui�
14
co
-
ryQ
ewil
o
c�
-
i
v
,
a}ep
OLC
01
I>
Oil
CL
Lo
N
EO
r V7
NIt
2
It
r-
�.
.,TO
a
ea
y
)a
£
r.
5
iPAU
i

Agricultural Lime Application Log
Year: 2018
Project: City of Dunn
Field
(state -county -site -field code)
NC -HA -08-8
Soil pH
6.1
Lime Requirement
(from soil analysis)
O.OT/AC
Tons/Acre
A plied
0.0 1
e Applied
N/A
F
NC -HA -08-9
6.0
O.OT/AC
0.0
N/A
NC
-HA -201-4
6.1
O.OT/AC
0.0
N/A

SECTION 7

\
\
\
(\
\(
\\
\
w
|
/
:E
7
\
\
\
\}{\
!§{
k
n
,z\
\(
)
k\(
;2
(
(
�
(�\
k
ZN
)
=
w
}
�\
�\j
\
\
(\
01
w
|
/
:E
7
\}{\
!§{
(\
|
/
:E
!§{
k
\(
)
k\(
;2
(�\

w
co 3 O O
W �
W
n
v
3
�
o
�
2
3
O
N
n
r/i
N
D
Ci
N
W
�
N
o
VI
0
ILI
o
0
ZS
n
N
W
N
O
N
ID
C
d
=
d
m
N
A
J
3•<
_
�
m
�
Z
O
N
o
N
�
O
a
n
�
_
0
m
J
C1
a
rn
a_
y
3
m
a
�
9
0
O
p
O
�
O
O
W
O
Z
m
w
e
3
o
Z
3a
N
Ip
u
UI
o
W
�
00
A
N
m
_
w
co 3 O O
W �
W
n
n
v
3
O
N
n
D
Ci
N
N
2
0
o
VI
0
ILI
o
0
ZS
n
N
W
N
O
N
ID
C
d
=
d
m
N
A
J
3•<
_
�
o
n�Oi
D
O
N
n
n
(n
o
N
n
J
a
?
2
0
o
0
ILI
o
0
ZS
n
N
W
N
O
N
ID
C
d
=
W
m
A
J
3•<
_
�
o
d
�
N

m
z
C
mCD CD
xw o
a 0 �
< m CD
o CD 0
N O N
fD N O
m m H
o CD 3
o
w 3 m
d 3 m
CD
H
n
n v
3 0 ?
v m
p CD h
m >
0
3 0 m
O
O {Q
d
v
0 H
� v
'N 0
M N N
a CDy
\n
w
w
O 0
n _
O A O
W^ 00
o �
m m m
CD o v
w
yam 3
S o m
O O' y y
w CD w 0
O O a d
o mao
0 0 m CD
3 O O N
9 CDD O_ O
n = 3 CD
�o 0 3
3 S 4 v
3 m v
O O a
o ? o
M n
CD c
CD
N O w
3
N p C
m a
vci"� m
0
a Q. CD
O O,
O 61
CD 2 w
v S. CD
0 >
d
d O. p
(D
y ; n
CD C 7
" c
N 7
w
CD M
CD
d w N
N. 0
- 'O
Tots
�a
(D
N
O O
o N
o M v o �
CD M
CD m v
X O = O o
° CD ° 3 m
'm m o o m
a a m 0
Wo f a m v
0
4 (D
N n O77 0
CD
} O 2 O
N 1
JJ CD O N
CD m
O O !? a p.
N N 0 n n
v o o n o
O 3 0 N
o a
CD M o
a w 0 0 0 o
0 o
0o m o 0 3 m
3 0 m
oy N d Co
3 0 ? m
mfO a° v
N N N y N
CD CD m 0 -
CD a
w w
o v v o v
a m 3 w
d CD 0
O N N
N a w G
N CD 0 0 0
w N ai N
W CD v s
Z 3 D N
O 3 C w
O CD y O CD0
CD CD O- 0
0
ao0W2)
w O c <D p
v
/7NO �a
CD �n
V N
< O T d c
w y C N
O N O
CD CD
N
-n M r
Dy 3 0 o m 3
a 0 m
CD
< I 'm
- o
- -. 0 0
CD 0su
G7 0 0 3
N N Q O
0 > a 3
CD
3 n x
o a -n _
3 ? o N
n 3 m o0
a C N
0
v m � m e
3 m c o
3 o w s
w ° ? 3 v
o
a N 0 N
a o m n
c 0 0
0 < O 0 w
d S D a
O N w N
o a v
3 N a o
a 3
n O O W
0
m 3. 0 °J o
v W O
o
O S N 3
(D O
CD
3 m
0 g.
f<p O (<D =
9 Cc
Dr
�. 0 3 ro
x m O <
o
O O N
S Q CD c
w � N
O
O w O
N
a
CD v �.
CD
w � (D
.. r0
NN�f/�ury vv Ozzz3333333xx'=m�00wDDD
NO - 3 N� c m e y 0
Z N
N
O
g 3 3 n D 3 3 o o o m x o DOi o x
p=Oj Q y y N N N n t� tD �p N N �p N m y N (D d N Oj m m d
m 0 0� S x o o
m v
o. o m o- o- 0 0 3 c 0 n 0 0 Doi
-:0 0a ao m x as o
m m m w
n w x x 0 x n n x m o o Q o' n
a 0
x 0
3 w 0 0
w o o m D 0 w w
y 0 0 m o .7' 4 w
E.
0 a - M
N � 3 0
N
n
3
a
N
N
YJ
N
d
�
O
0
O
d
�
0
O
Q
3
5-
m
�
5-
m m m
CD o v
w
yam 3
S o m
O O' y y
w CD w 0
O O a d
o mao
0 0 m CD
3 O O N
9 CDD O_ O
n = 3 CD
�o 0 3
3 S 4 v
3 m v
O O a
o ? o
M n
CD c
CD
N O w
3
N p C
m a
vci"� m
0
a Q. CD
O O,
O 61
CD 2 w
v S. CD
0 >
d
d O. p
(D
y ; n
CD C 7
" c
N 7
w
CD M
CD
d w N
N. 0
- 'O
Tots
�a
(D
N
O O
o N
o M v o �
CD M
CD m v
X O = O o
° CD ° 3 m
'm m o o m
a a m 0
Wo f a m v
0
4 (D
N n O77 0
CD
} O 2 O
N 1
JJ CD O N
CD m
O O !? a p.
N N 0 n n
v o o n o
O 3 0 N
o a
CD M o
a w 0 0 0 o
0 o
0o m o 0 3 m
3 0 m
oy N d Co
3 0 ? m
mfO a° v
N N N y N
CD CD m 0 -
CD a
w w
o v v o v
a m 3 w
d CD 0
O N N
N a w G
N CD 0 0 0
w N ai N
W CD v s
Z 3 D N
O 3 C w
O CD y O CD0
CD CD O- 0
0
ao0W2)
w O c <D p
v
/7NO �a
CD �n
V N
< O T d c
w y C N
O N O
CD CD
N
-n M r
Dy 3 0 o m 3
a 0 m
CD
< I 'm
- o
- -. 0 0
CD 0su
G7 0 0 3
N N Q O
0 > a 3
CD
3 n x
o a -n _
3 ? o N
n 3 m o0
a C N
0
v m � m e
3 m c o
3 o w s
w ° ? 3 v
o
a N 0 N
a o m n
c 0 0
0 < O 0 w
d S D a
O N w N
o a v
3 N a o
a 3
n O O W
0
m 3. 0 °J o
v W O
o
O S N 3
(D O
CD
3 m
0 g.
f<p O (<D =
9 Cc
Dr
�. 0 3 ro
x m O <
o
O O N
S Q CD c
w � N
O
O w O
N
a
CD v �.
CD
w � (D
.. r0
NN�f/�ury vv Ozzz3333333xx'=m�00wDDD
NO - 3 N� c m e y 0
Z N
N
O
g 3 3 n D 3 3 o o o m x o DOi o x
p=Oj Q y y N N N n t� tD �p N N �p N m y N (D d N Oj m m d
m 0 0� S x o o
m v
o. o m o- o- 0 0 3 c 0 n 0 0 Doi
-:0 0a ao m x as o
m m m w
n w x x 0 x n n x m o o Q o' n
a 0
x 0
3 w 0 0
w o o m D 0 w w
y 0 0 m o .7' 4 w
E.
0 a - M
N � 3 0
N
n
3
a
N
N
YJ

m
N
�
❑
❑
d
❑
❑
d
J
a
❑
UPk
a
�
❑
❑
❑
❑
❑
❑
J
a
❑
oW
of
n
n
E
�
M
E
E
m
0
o
0
0
�
r
0
0
0
0
0
0
0
m.La
e
e
>
❑
Z
❑
❑
❑
❑
❑
❑
J
a
❑
oW
of
n
n
E
�
M
E
❑
Z
❑
❑
❑
❑
❑
❑
J
a
❑
❑
of
n
n
E
�
M
E
E
m
0
N
Q
�
r
�
o
0
0
0
m.La
e
e
>
a
�
z
�
o
M
❑
Z
❑
❑
❑
❑
❑
❑
J
❑
❑
❑
of
n
n
r
�
M
E
E
m
in
�
U
A
o
0
0
0
m.La
p
e
>
LO
M
�
N
�
�
0
Y
9
b
0
N
Q
O
9
E
a
z
U
0
0
sem❑
o
a
N
d
z
w
C
L
6
T
N
U
uoi
a
voi
>
0
0
0
0
o
N
N
Y
Z
_
U
F-
d
a
F
LL
❑
Z
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
of
n
n
r
�
M
�
E
m
in
�
U
A
0
0
0
0
:i
N
�
m
w
U
9
J
N
N
J
FT
m
�
E
m
in
�
U
A
ee
m.La
p
e
LO
k4
YJ
�
0
9
b
0
N
9
E
a
sem❑
o
a
d
z
w
C
L
6
T
N
N
N
N
a-
_
--
LL
b
y
IL
F-
0
10
0
a
'z
_
_
�:,
cv
_
_=
--E
o
C?N
OEj
N
N
N
0
C
'T
N
N
(7
y
y
N
N
N
cq
U
2=
S
z
d
R
:i
N
�
m
w
U
9
J
N
N
J
FT
m
�
E
m
in
:i
m
w
N
9
J
J
m
�
5
�
U
:i
w
9
s
�
5
�
a
A
ee
m.La
p
e
LO
k4
YJ
�
0
9
:i
w
s
ee
m.La
LO
0
9
b
0
N
9
E
a
sem❑
d
z
w
0.l
:i

0 0 0
0 0 0 0 0 0 0 0 0 0 0
�
E
O
rC
N
O
o
�
N
n
ro
o
m
o
�
U
N
N
W
•-
•-
��
�-
M
M
T
0
0
0
O>
0
W
0 0 0
0 0 0 0 0 0 0 0 0 0 0
N
C O_ O N T
N O W C O O¢ N
a F
U O — N
— N LL N V li f-
E~N D Z V N
N~ C= U u U .n m t t t t a
N N N N W d 0 N C fn (n (n W (n
N U== 2 Z m d
.V
W
J_
>
�
E
O
rC
N
O
o
�
N
n
ro
o
m
�
U
N
N
W
(%J
z
U
0
0
0
0
0
0
0
N
C O_ O N T
N O W C O O¢ N
a F
U O — N
— N LL N V li f-
E~N D Z V N
N~ C= U u U .n m t t t t a
N N N N W d 0 N C fn (n (n W (n
N U== 2 Z m d
.V
W
J_
>
�
E
O
rC
N
O
o
�
N
n
ro
o
m
�
U
N
N
W
(%J
z
U
N
rC
N
O
o
M
O
d
M
n
ro
�
N
(%J
U

a
E
w
C3
N
E
o
m
0
❑
b
N
c
o
�
�
o
❑
C)
ry
m
�
o
0
6
6
6
p
m
30
of
0
W
W
` x 0 6 0 6 6 6 0 6 6
(O � r N❑� (O W N�❑� N r o �O
w
C3
N
E
o
m
0
❑
b
N
c
o
�
�
o
❑
C)
0
�
z
�
o
0
6
6
6
p
(O � r N❑� (O W N�❑� N r o �O
w
C3
E
❑
b
N
c
�
�
o
❑
C)
�
z
�
o
C
p
30
P
°tea
rn
v
a
—
o
q
z
o
!4
E
—
N
0W
c
—
N
N
N
N
6
O
0
—
O
a
0
-
`
s
=
a
ILL
0
0
0
N
V
[Li
N
d
Z
cV
N
_
to
x
ter,
in
mmm
d_a'v�
N
N
U
2
2
2
Z
m
m
C4
w
C3
E
❑
b
N
c
�
�
o
❑
C)
�
z
�
o
C
p
w
b
c
q
C)
Ln
C
C
p
30
P
w
C)
Ln
C
C
p
30
P
°tea
rn
a
a
q
a�a�za
!4

Ey d O
x M"
m M M M m
F� �A J
n ❑ O y
a
n � e
p ry y' m3 o c n w OaviMmoM�uivC6
FQ'�1 c o'
N m o n o
m m V 0 w
r V O 6b d
0 0 0 O O O O O o
> a
a P�
N =
❑ ❑ 'E N h N N N h N V m
Q
U m N (O r r m4 6 w c6
N O
M r W 4 �...
o «
JLO
v
E o —
�o�Wf�wi0l ��ij rydUowr`z">xJ rorymryMf`��C`m`1 ' �mo�e .0�"an°i w3Q•� FCUU~O�aNaMnE MNyFFNom-
Yad>¢
oa0oM�A0NmoLoNOL 0o0VO ' m0d❑ZAv: 0Mx 0MtNm0mx� 0ro0Mom
00rM-a00❑Zam
0`rai`otn roitn mV�i�°n 1 mrn0r�iotn
¢mrSy0�a l
'
Vy�6^.qqb�TxCa
O
oo -S 2 4N
i b
u toN
z a0 000 00 0 y o 0 0
N
Z 0ooNO
lk—
Z 0
=4 9
'cam 9
>x>
-o
°2 20 0 0_ o 7
N N NtUI7 F o a
x x c
U U) C) ¢N NcNi C-)xxxz

e�
Y
-
-
q
d
y
N
N
m
V
ak
J
2
rc
x
m
E
N
n
a
G
FT
q
�
o
m
F4
b
E
m
�
G
m
E
U
in
N
�
m
E
a
f7
aU
o
(n
U
Q
o
o
ao
r_
ro
>"
..
P4
W
O
P4
e�
Y
-
-
q
d
y
N
N
m
V
ak
Y
-
-
J
y
N
N
m
b
J
2
rc
x
m
❑
N
n
�
J
FT
r
�
o
m
E
m
N
m
m
E
U
in
�
-
o
N
�
N
m
J
�
�
K
H
N
n
�
J
J
N
�
o
m
�
a
N
m
m
E
U
N
�
m
E
a
f7
aU
o
(n
U
Q
�
-
o
N
�
N
m
J
�
�
K
H
N
n
�
J
J
�
o
d
9
N
m
m
E
U
N
U
Q
�
-
o
N
�
ui
�
H
N
J
J
�
d
9
N
�
m
E
N
U
Q
�
-
o
N
�
ui
H
t
m
�
N
N
U
a
f7
aU
o
�
o
o
ao
r_
ro
❑
..
E
m
E
�
m
q
U
Q
�
-
o
N
�
ai
H
m
�
N
aU
o
o
r_
ro
❑
..
E
�
m
fn
U
Q

\ƒ
}
q \76
@
S
\
\/
\
/
)
�
CY
/)
())\
j)m!
§\;
)#;
EE;!
2
){{
9
)7f
§
;>sa
;±a
&
)/))
2
@
S
\
\/
\
/
)
)
�
/)
())\
j)m!
§\;
)#;
EE;!
2
){{
9
)7f
§
;>sa
;±a
)
/)
§\;
)#;
2
){{
)7f
§
;±a
&
)/))
2
$f
15
;42,
=-§a
■

n
-
V
Y
-
p7
m
�
�
N
E
-
-
�
K
H
U
a
p
46
a
m
m
a
m
N
>_
�
a
Y
E
m
Y
9
m
m
�
m
W
K
�
7
N
K
m
c
d
O
-
N
9
O
Q
fn
N
>
W
y
Y
N
d
N
o
o
Z
0
Z
v
cl
y
J
o
Jo
1-m
d
0
a�
�
a
N
F-
o
a
N
�
v
E
E
m
c
W
U
Q
0
❑
❑
r
❑
c
❑
r
r
Z
a
Z
o
Z
Z
o
Z
a
v
Q
?
N
>
>
>
w
N
cl
t•i
M
M
Nl
t�"i
N
=
=
N
N
=
N
=
0
0
o
o
.E
o❑
.E
o
o
.E
E
US
J
J
J
Q
Q
Q
Q
W
W
w
W
M
m
rn
a
rn
n
—
V
Y
p7
m
�
�
N
E
�
-
�
K
H
U
rc
p
46
E
m
m
m
m
N
>_
�
a
Y
E
m
Y
9
m
m
�
m
W
K
�
7
N
K
m
c
d
O
-
N
9
O
Q
fn
N
>
W
y
Y
N
d
N
o
Z
Z
>
U
y
J
o
Jo
1-m
d
to
a�
�
a
N
F-
o
a
N
�
v
n
—
V
Y
p7
N
�
�
N
o
�
-
�
K
H
U
rc
p
46
E
m
m
m
m
N
>_
�
n
—
V
Y
N
e
�
�
N
E
�
-
�
K
>
rc
p
46
�
u
m
m
m
>_
�
a
Y
E
m
a
9
m
m
�
N
K
�
7
N
E
m
c
9
O
>
N
t%1
U
Q
fn
n
—
V
Y
N
m
�
�
N
E
�
-
�
K
>
K
p
46
�
u
m
�
J
E
u
Y
E
m
a
m
m
m
�
N
K
�
7
N
Q
9
O
>
N
9
�
>
N
Y
W
U
�
a
d
o
Z
ti
>
U
y
J
o
c
1-m
d
to
a�
a
N
F-
o
n
—
V
Y
N
N
�
�
N
E
�
-
�
K
�
K
p
46
�
u
m
HT
J
E
u
Y
E
m
a
�
m
m
�
—
V
Y
e
�
N
E
�
-
°
>
K
p
46
�
u
m
J
J
E
m
Y
E
m
a
9
m
m
�
N
i
Q
fn
U
Q
(9
—
V
Y
m
�
N
E
�
-
°
>
d
p
46
�
u
m
E
m
Y
E
m
a
u
m
W
N
i
Q
9
O
9
�
>
h
Y
N
U
�
a
d
o
Z
ti
>
U
y
J
o
c
F=
d
a
N
r
o
—
V
m
�
N
41
�
�
°
>
d
p
Q
�
u
m
E
m
Y
E
m
a
�
W
N
i
Q
9
O
9
�
>
�
U
�
a
d
o
Z_
ti
>
w
m
�
c
F=
d
a
N
�
o
v
E
E
m
c
W
U
Q
0
—
V
m
�
N
E
�
°
>
C
v
Q
�
u
m
E
m
Y
�
a
�
W
a
Q
9
O
9
�
>
N
N
�
a
C
o
Z_
ti
>
w
m
o
F=
d
a
N
�
—
V
�
N
�
°
8
C
v
Q
�
u
E
m
❑
N
Q
9
�
a
a
C
o
>
cW
m
E
m
c
A
0
Q
0
°
8
C
v
Q
'y
o
9
�
a

\
!
/
]
)
�
))
\
»#;
��
a
!f3LO
;]!!
E&i!
)\$
)!E>
0
)3±
f/@m
a
_*
]
))
»#;
!f3LO
)\$
0
)3±
a
±!!
\
}}!j
■

T
e
N
a
a
o
z
-
7
a
e
L
Y
0
�
N
0
N
6
�
o
C�
0
�
�
o
-
m
o
�
a
E
a
�
3
o
m
d'
a
❑
N
N
r
=
N
z
0
U
m
m
o
❑
a
Fa
m
r
F=
�
3
v
-
a
m
-
3
a
-
N
oz
a
Q
o
W
0
�
LU
�
b
K
�
U
Q
�i
0
3
0
x
�
w
A
d
z
�
aT
Q
n
v
a
�
m
r
P7
._
E
m
=
W
❑
❑_
E
a
-
o
J
w
T
e
N
a
w
o
z
-
7
a
e
L
Y
0
�
N
0
N
6
�
o
C�
o
�
�
o
-
m
o
�
a
E
n
�
3
Y
m
N
a
❑
N
N
r
=
N
z
0
U
m
c
z
❑
a
Fa
a
a
F=
�
3
T
e
N
a
w
o
z
-
7
a
e
L
Y
0
�
N
0
N
6
�
o
C�
m
E
a
M
-
m
o
�
a
E
n
�
3
Y
a
N
N
❑
=
N
r
=
N
N
0
o
m_
c
z
❑
a
Fa
a
E
m
�
3
v
-
m
-
3
a
-
N
a
a
W
U
H
LU
8
E
v
�
U
Q
0
3
0
x
�
w
d
z
a
aT
Q
n
v
m
T
e
N
a
w
o
z
�
7
46
a
L
Y
0
�
N
0
N
6
�
A
_
m
m
a
M
-
m
o
�
a
E
J
3
Y
a
N
N
❑
=
N
r
=
N
N
0
o
m_
c
z
❑
a
Fa
a
E
v
�
3
v
-
O
-
3
T
e
N
a
w
o
z
�
7
46
a
L
Y
0
�
N
U
N
6
�
A
_
m
m
a
M
-
m
o
�
a
E
J
3
Y
a
N
N
❑
=
N
N
=
N
N
0
o
m_
C
❑
❑
a
Fa
a
E
v
�
3
v
-
O
-
3
a
-
Na)
a
a
Q
U
LU
8
E
v
T
e
N
a
w
o
z
�
7
❑
a
L
Y
0
�
N
U
N
6
�
A
_
m
m
a
M
-
m
o
�
a
E
J
3
Y
a
N
N
❑
=
N
N
oZ
Z
0
o
❑
C
N
�
a
Fa
a
a
v
�
3
T
e
N
a
w
o
z
�
7
❑
a
L
Y
0
�
N
U
N
6
�
A
E
m
N
a
M
-
m
o
�
a
E
J
M
Y
a
N
�
❑
=
N
N
oZ
m_
0
o
❑
C
N
U
E
a
a
v
�
3
O
-
J
m
Na)
a
a
U
K
8
E
v
�
U
Q
T
T
m
E
E
�d
d
w
d
7
❑
Y
0
�
N
r
N
�
�
�
A
_
ro
N
a
M
-
m
o
�
o
E
J
M
Y
a
N
�
❑
=
N
N
oZ
m_
0
o
❑
C
z
o
E
a
a
v
-
3
a
-
J
T
m
E
E
�d
d
w
0.l
7
❑
Y
�
N
r
N
�
�
�
A
_
ro
N
'a
M
-
m
o
�
o
E
J
M
Y
a
N
�
❑
=
N
N
oZ
m_
0
o
❑
C
v
�
E
a
a
v
-
3
a
-
J
Na)
a
a
U
K
8
T
m
E
E
�d
d
w
0.l
7
❑
Y
a
N
0
N
�
�
�
A
_
ro
N
'a
M
-
m
o
�
o
E
J
3
Y
a
N
�
❑
=
N
N
oZ
Z
0
U
❑
C
v
�
❑
a
a
F
F
v
T
m
E
E
T
�d
d
w
0.l
7
❑
Y
d
N
0
N
�
�
�
A
ro
m
a
�
E
m
o
�
o
E
J
�
o
a
N
�
❑
=
N
N
oZ
0
0
❑
❑
C
z
o
E
a
d
Fa
F
v
LO
c
01Q
T
�d
w
0.l
7
❑
Y
d
N
N
�
�
�
A
ro
m
a
�
E
m
o
�
o
E
J
�
o
a
N
�
=
N
N
oZ
0
0
❑
❑
F
E
a
d
Fa
F
v
LO
c
01Q
Na)
a
v
U
K
8
T
�d
w
0.l
7
Y
d
N
N
�
�
�
A
ro
m
a
-
m
o
�
o
E
o
a
N
�
LOO
oZ
0
0
U
0
F
a
d
Fa
F
v
T
U
�d
0.l
o
�
A
.T
o
E
o
a
�
LOO
0
0
0
0
U
a
F
v
LO
c
o
Na)
a
v
8
U
�d
0.l
.G
.T
o
E
a
O
LOO
0
0
0
0
U
a
F
v
LO
c
o
Na)
a
v
8
x
�
w
d
z
a
.G
.T
0
0
0
0
U
�
F
v
o.
c
o0
8
x
�
w

O
O
b
E
E
0
o
�
w
a
�
d
7
a
�
❑
�
K
n
E
❑
N
E
❑
�
J
a
�
n
�
E
m
r
m
a
o
n
�
❑
C
c
y
m
N
a
_
N
K
Z
Z
o
c
r
x
ti
�
I �
N
o
E
E
0
o
�
w
a
�
7
a
�
❑
�
K
n
E
❑
N
E
a
�
J
�
�
r
�
E
m
r
m
a
o
n
�
E
C
�
y
m
N
a
_
N
N
a
❑
N
ro
r
x
ti
..
U
N
o
❑
❑
O
Z
Z
E
�
�
F
y
0'
N
m
K
N
o
Z
Q
J
9
a
U
�
�
N
K
a
K
�
m
m
E
E
0
o
�
w
a
�
7
a
�
❑
�
K
n
E
Y
N
E
a
�
J
N
�
r
�
E
m
r
m
a
o
n
�
C
�
y
m
N
a
_
N
N
a
❑
N
ro
r
=
ti
..
U
N
o
❑
F-
O
Z
Z
a
�
�
E
E
0
o
�
w
a
�
7
a
�
a
�
K
n
E
Y
N
E
a
N
J
�
�
r
�
E
m
r
a
a
o
n
�
a
a
E
rn
N
�
_
N
4
a
❑
N
ro
r
=
ti
ti
U
N
o
❑
❑
d
Z
Z
o
�
F
y
0'
N
m
K
N
o
Z
E
E
0
o
�
w
a
�
7
rc
�
a
�
K
n
E
Y
N
E
a
N
U
�
�
r
�
E
m
r
a
a
❑
n
H t
a
a
E
rn
o
�
_
N
4
a
❑
N
ro
r
=
ti
ti
U
N
o
❑
❑
d
t0
~
E
�
F
y
0'
N
m
a
A
o
Z
c
J
9
a
U
�
�
N
K
a
w
�
m
m
E
E
0
o
�
�
a
�
7
rc
�
a
�
K
n
E
Y
N
E
a
N
U
N
�
O
�
E
m
r
a
a
❑
n
H t
a
a
y
rn
o
�
_
N
4
a
❑
N
ro
r
a
z
U
N
o
H
r
d
t0
~
a
�
F
a
0'
E
E
0
o
�
�
a
�
o
rc
K
a
�
K
n
E
Y
N
E
a
�
U
N
o
O
�
E
m
r
m
a
❑
n
H t
a
a
y
rn
o
�
�
N
a
❑
x
ro
r
U
m
o
z
r
d
t0
a
x
�
a
0'
N
m
0
A
C?
Z
m
e
9
❑
U
�
�
N
K
a
�
m
m
5
o
Q
N
U
Q
E
E
0
o
�
�
�
d
j
d
K
a
�
K
n
E
Y
N
E
a
�
E
N
�
O
�
J
r
m
a
❑
n
H t
�
a
y
rn
o
�
�
N
�
❑
x
ro
r
U
m
o
z
r
d
t0
o
x
�
a
0'
N
m
0
o
C?
Z
Z
e
E
❑
E
E
o
�
�
�
d
j
d
K
�
K
n
E
Y
N
E
a
�
a
N
O
�
a
r
m
E
n
H t
�
3
y
rn
N
d
E
N
�
❑
x
ro
r
U
�
Z
z
r
d
e
o
x
�
0'
N
m
0
o
C?
9
a
E
❑
U
�
o a
K
a
5
o
Q
C
J
a
m"
U
�
a
fL
-
E
E
a
�
�
�
d
j
d
K
�
n
E
Y
N
E
a
�
0
N
O
a o
a
v
m
E
n
H t
�
3
y
rn
N
d
E m
N
�
❑
x
ro
r
U
�
Z
z
r
d
e
o
a
�
E
E
a
�
�
�
d
�
d
K
�
n
E
a
o w
E
E
�
0
E
O
a o
�
v
m
E
n
H t
�
N
�
_
o
N
E m
�
❑
x
ro
r
a
�
Z
z
o
E
e
o
a
�
0'
N
m
C?
9
a
U
❑
U
�
o a
K
F
(A
U
Q
m"
�
a
N
-
E
E
a
�
E
�
d
K
�
n
a
N
a
�
0
N
O
�
�
v
m
E
n
fY
�
N
a
LO
o
N
a
�
❑
x
ro
r
ft
�
Z
z
o
E
e
o
ad
�
0'
N
m
E
E
a
�
E
�
K
�
n
a
N
a
�
N
m
�
�
v
m
E
O
�
N
a
LO
o
N
a
�
z
x
ro
O
❑
�
a
d
E
o
ad
EN
m
J
9
a
❑
U
�
K
F
E
E
a
�
E
�
�
n
Y
N
a
�
N
m
�
�
v
m
a
O
�
N
a
LO
o
N
a
�
z
O
~
a
d
co
o
ad
E
E
a
�
E
o
�
n
F
�
v
m
�
�
v
A
a
O
LO
o
a
O
d
co
o
ad
EN
m
m
9
❑
�
NE
F
(A
U
Q
E
E
�
E
N
�
v
�
E
v
A
a
O
LO
o
5
O
co
o
ad
EN
m
N
�
�
E
a
O
LO
o
5
O
co
o
ad
EN
m
za

\
±
\
k
{
(®)J
))
:f\
))\i
£§4!
�
2j\\
\))/
){\
#!!!
_
*
i
)
{
))
:f\
\{\
�
){\
#!!!
:>!
\4\)
k
]\))
,e*=
_
2
\2f!
)
{
{
#!!!
\4\)
,e*=
_
\2f!
§}«)
)«j±
)
{

N
O
b
H
ra
d
E
N
❑
i
N
C
�
(a
N
❑
to
�
o
`rd
a
�
Ugi'
C
N
U
Q
!r
U
o
!Y
�
m
i
v
C
V
(a
5
o
`rd
�
Ugi'
m
N
U
!r
U
o
lya
N
�
o
❑
2
�
o
r
K
5
P
a
N
r
a
E
m
5
f:4N
'0
N
m^2
=
�
N
N
cl
J
on
o
a
o
0
0
n
m
°
3
c
J
¢
w
o—
m
n
o
o
�
L
m
rn
rn
❑
m
oo4'o�
m
E
o
0
0
0
>-
7
!r
W
Q
m
U
H
Y
a
I
m
o0
N
�
N
N
o
o
o
m
>
o
N
N
O
o
o
N
�
d
h
N
a
m
v
C
V
(a
5
o
`rd
�
Ugi'
m
N
U
'J
U
o
lya
N
�
o
2
�
o
r
P4
5
P
a
N
a
E
m
5
f:4N
'0
N
m^2
�
N
J
on
o
a
o
0
0
n
m
N
3
0
o
o—
J
L
m
—
❑
oo4'o�
W
Q
m
U
H
m
v
C
V
(a
5
o
`rd
�
Ugi'
m
N
U
'J
U
o
lya
N
�
o
o
m
v
�
5
'J
o
LO
o
r
P4
5
P
N
a
5
5
f:4N
'0
m^2

o
m
U
d d O
EiJ
N N N N
m �
� F
G ❑ ~
z z o o v 'q v
w'
a o No o a�
Y
7
a❑ ❑ ❑
mor�
o c4
n v M
i
J
S
Yl c0 n M O O c0 d; c0 ❑ ❑ N (O
m a m c6 c6� N m n �
J ❑
U
o NO tf1 N V M cO Mp LO Np W ' Fo
of OM1 co W m r
j LoO
LOO
00000000 E - 00 2P4 M
O > v N
H c
CK
0)
C3
0 0 0 N N o
0 o -
o N o N N o N o ) N o
C� Y
. V
Z
d
0 0 0 0 0 0 0 0 0 ~ a o 0
T .J
n 0 c0 N M W 7 0 w G b
u1 V i�r1 O o v
C
o � o ❑
H
C
m E
w
a m
a �
m E a
t c b
p a ? o
a > x >
N0 0W N
N N - p1 'O C rTi W
C �0 0� C N
L o L m O N r ❑ N L
v. m E a o 0 d' o �= O r t v
r r c c a o t
❑ a `o 076m

E- o a o
❑ m o m
z o N0 o
N z Z o v q
N
cl
�i
a a
a
c+ 'E <o m rn N r co m N W '�, O w
t•J L
W =
❑ ❑ " 6
v m
J
WM N W NM NO C
rn rn w rn m m
oa
u LO0
O
m S o M
0 0
> 9 ro y N
j K
o0 o v c m o 0 0 0 'z w
76 N o 0 0 N N 0 n 0
hi
o s Z
w d
v a
F' ❑ N C5 N V V o
N
ci 0 0 0 0 0 p C o C
'uFiv U m U o
❑ J a
46
tl ~
W U
2 a v y o C
w
o 0
0 o E m
W N O L m
p E o
••c o B 't
d v E
b w m n Amin in
i E
U A+ to U Q 0 U 0 F- 1� > a

\�&
\|I
)
/
)
�
&
]
«a.
}\)\
)$m:
\)\
S
;)){
£E�!
(\$
)\/\
7]()
§
a2I
%)\)
\))(
\!a
;!=a
{
]]!l
\}}}
\\\\
,=y,
CO
\
\
Z
�
�\
_{\`
\
\
/
\
b
\�&
\|I
)
/
)
�
«a.
}\)\
)$m:
\)\
S
;)){
£E�!
(\$
)\/\
7]()
§
a2I
%)\)
\))(
\!a
;!=a
{
\:
«a.
\\),
\)\
S
(\$
)\/\
§
a2I
%)\)
\!a
\\\\
{
]]!l
\}}}
\\\\
\\),
)\/\
%)\)
\\\\
\\\\
,=y,

saaa�uo� � aaqumN
an�ynaaasaad
geEa�J
0
Page 33 of 50
a�
N
O

pF1
ROJ. 16
Summit Envitorlmental Technologies, Inc.
Cooler Receipt Form
ennre.�u,,,� n nay,
Initials of person inspecting cooler and aamplesl
Client: SYP' order Number: eclAA
pate Radeived:'3 Time Received!
i3 t{O Date ceolar(s) opened and samples inspected?�,�1j�„_...
Number of Coolers/60%ea: 1 _ _ N/A
Shipper.EDEX UPS DHL Airborne US Postal 'lJalkdn Pickup Other'
Packaging: Peanuts sujbl Wr Paper Foam None Other:
r� N NIA
Tape on cgolerfbg%: l—�ll
y N NIA
Custody Seals intact
N NIA
C -O -C in
pl slit
Ica Blue ice presen absent I molted NfA
Sample Temperature IR Gun #7�r+02C459 CF _n_o °G
4. 'C NIA
Radiological Testing Instrument serial #39,127 Y
N NIA
(see page 2 for scan results)
'•Use 1 shoal per sample for Radiological Testing. If sample is HOT, Ute Radiological Safety officer must be emitted
Immediately.
N N/A
C -6C lilted out properly
N NIA
Samples in separate bags ���------���
Sample containers Intact' ( ' J N MA
9f no, list broken sumple(s).___._._.
Sample Iabel(s) e0rnpVete (ID, dale. ¢lc.) � N N1A
Label(s) agree with -C -O -C (3:)
/�/ N NIA
Correct containers used �-. y N NIA
Sufficient sample received N NIA
Samples received within holding time t N
Rubbles absent from 40 nal -viols" Y N NIn
"Samples with bubbles <rinm+ am acceptable. Indicate bubble size it >0mrn.
Was client contacted about samples V N
Will client send new samples Y N
Laggetl In
Pale 1 of z
Page 34 of 50

pg JO gg 06ed
96
10 6 abed
e
a -
I
s
E I �EE
o
U w ai fl F
m
g
+Ir.�r n
J w w r m IMlw �, @ H e o r
171
Jni H
`�.s � c��wui u�:n �Gw u:w n. �3Ld , i uViw6�
Mi £
L7 ti
id
n
n � b
t ?
a
- u a
- N
s IFa
N
a- 4 •` a O�� Q < FQ.ffi �Z ZC Q�Q �z
amy� fro
4� 4C1 y 1.ire
c
3n 4 C s c
J_.Q __:X.yN BVI; i.LL 4.'�.NZ(�=W��WVCg NnCW4-VIaW 9�1 ,_

m
a
05 do 9E a0ad
94 bo Z abed
m
Ki ,4 C v4 vi C ci C eiyr 6 -{ r C
D ❑ o v A r D
Qq
v UQ1 o E
w wui v�'i uw.F°��w 0 w v'= w w www 10
`ts i91t
h
9I
� _ I
E � 4 QQa
w v m E itir
E E
o g K K Y K S t 4y`
i gg 6 qn
4 - C
zv �'i iKu �mowr'znaasa3e tri x W.c °�ng3 3w4 n �'`a a yA
..or rn w w n o -mw 0 w w N
r`.
q
=aa
m
Ki ,4 C v4 vi C ci C eiyr 6 -{ r C
D ❑ o v A r D
Qq
v UQ1 o E
w wui v�'i uw.F°��w 0 w v'= w w www 10
`ts i91t
h
9I
� _ I
E � 4 QQa
w v m E itir
E E
o g K K Y K S t 4y`
i gg 6 qn
4 - C
zv �'i iKu �mowr'znaasa3e tri x W.c °�ng3 3w4 n �'`a a yA
..or rn w w n o -mw 0 w w N
r`.
q
r�
4
W
w
G
m
Ki ,4 C v4 vi C ci C eiyr 6 -{ r C
D ❑ o v A r D
Qq
v UQ1 o E
w wui v�'i uw.F°��w 0 w v'= w w www 10
`ts i91t
h
9I
� _ I
E � 4 QQa
w v m E itir
E E
o g K K Y K S t 4y`
i gg 6 qn
4 - C
zv �'i iKu �mowr'znaasa3e tri x W.c °�ng3 3w4 n �'`a a yA
..or rn w w n o -mw 0 w w N
r`.

OS JO LE abed
96 bo g abed
�$° -
u [�
S t f O i
of .q Itt
ly i� Y. ry
✓ Z
w C U V w �'. U' o a ca
O m q
ua w w
,n w F a
r a 2 3 a s 4 N a a 3 x 3 z 3
D �w n lu ui
©,nay y Ines
y�
F
N
0 b
S r.$ °°' O $zzOz sn
g 4 v h A 4q S T C 4
'S4 5� 8d Q4o Fv
Y 4 ry m C.. q ¢ K:.
.. �sto to cc 8t 0 Aga to to wIa � z Y
mow n;�wm d 3 oto 3 w0?uRwv�',%wNn:.i�ai vi It
E
I ml"C
C
E
R
to
OS JO LE abed
96 bo g abed
�$° -
u [�
S t f O i
of .q Itt
ly i� Y. ry
✓ Z
w C U V w �'. U' o a ca
O m q
ua w w
,n w F a
r a 2 3 a s 4 N a a 3 x 3 z 3
D �w n lu ui
©,nay y Ines
y�
F
N
0 b
S r.$ °°' O $zzOz sn
g 4 v h A 4q S T C 4
'S4 5� 8d Q4o Fv
Y 4 ry m C.. q ¢ K:.
.. �sto to cc 8t 0 Aga to to wIa � z Y
mow n;�wm d 3 oto 3 w0?uRwv�',%wNn:.i�ai vi It
E
E
E
R
to
ON
toL
OS JO LE abed
96 bo g abed
�$° -
u [�
S t f O i
of .q Itt
ly i� Y. ry
✓ Z
w C U V w �'. U' o a ca
O m q
ua w w
,n w F a
r a 2 3 a s 4 N a a 3 x 3 z 3
D �w n lu ui
©,nay y Ines
y�
F
N
0 b
S r.$ °°' O $zzOz sn
g 4 v h A 4q S T C 4
'S4 5� 8d Q4o Fv
Y 4 ry m C.. q ¢ K:.
.. �sto to cc 8t 0 Aga to to wIa � z Y
mow n;�wm d 3 oto 3 w0?uRwv�',%wNn:.i�ai vi It

������ sannitEnviYonn,entarTechnorogies,,ne. Analytical Report
3310 w�n St.
FNVIltONMENTAL TECHNO LOGES, 1FtG Cuyahoga Falls, Ohio 49223 (base report)
AnaFytica! La�orstvrfea TEL: [phone]L1 FAX: (330J 253-4989 WO#: 17030217
Website: htm �//vww settek.com Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-OOlA
Project: Dunn WWTP
Client Sample ID Dunn W W TP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8061A SW3510C Analyst: JBN
SVOC SW -846: 8081-TCLP PESTICIDES
Chlordane, total ND 0.0100 mg/L 1 319/2017 5:09:00 PM
Toxaphene ND 0.0200 mg/L 1 3/9/2017 5:09:00 PM
Endrin ND 0.00100 mglL 1 3/9120175:09:00 PM
gamma -BHC ND 0.00100 mg/L 1 3/9/20175:09:00 PM
Heptachlor ND 0.00100 mg/L 1 3/9120175:09:00 PM
Heptachlor epoxide ND 0.00100 mglL 1 3/9120175:09:00 PM
Methoxychlor ND 0.00100 mg/L 1 3/9/2017 5:09:00 PM
Surr: TCMX 73.7 10 - 119 %Rec 1 3/9/2017 5:09:00 PM
Surr: DCB 89.9 10 - 119 %Rec 1 3/9/2017 5:09:00 PM
TCLP HERBICIDES ANALYSIS (SW846 131118151) SW8151A SW8151A Analyst: JBN
SVOC SW -846: 8151 HERBICIDES-TCLP
2,4-D ND 1.00 mg/L 1 3/1012017 10:26:00 PM
2,4,5 -TP ND 0.500 mg/L 1 3/10/2017 10:26:00 PM
Surr: DCAA 75.8 20 - 140 %Rec 1 3/1012017 10:26:00 PM
TCLP METALS, VOC, BNA, PEST; HERB -SOLID SW8260B Analyst: MES
VOC BY GC/MS (8260)-TCLP
1,1-Dichloroethene ND 0.100 mglL 1 317/201711:51:00 PM
1,2-Dichloroethene ND 0.100 mglL 1 317/201711:51:00 PM
MEK ND 2.00 mg/L 1 3/7/2017 11:51:00 PM
Benzene ND 0.100 mglL 1 3/7/2017 11:51:00 PM
Carbon tetrachloride ND 0.100 mglL 1 317/2017 11:51:00 PM
Chlorobenzene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Chloroform ND 0.100 mglL 1 3/712017 11:51:00 PM
Telrachloroethene ND 0.100 mg/L 1 31712017 11:51:00 PM
Trichloroethene ND 0.100 mg/L 1 3/7/2017 11:51:00 PM
Vinyl chloride ND 0.200 QC+ mg/L 1 317/201711:51:00 PM
Surr: 4-Bromofluarobenzene 97.2 70 - 130 %Rec 1 317/2017 11:51:00 PM
Surr: Dibromofluoromethane 96.0 70 - 130 %Rec 1 3/7/2017 11:51:00 PM
Surr: Toluene -de 100 70 - 130 %Rec 1 317/2017 11:51:00 PM
Page 8 of 50
Value exceeds Mmdmmn Contaminant Level.
E
Value above quantitation range
Qualifiers:
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected at the Reporting Limit
O
R8D is greater Yhan RBDlimit
P
Second column confirmatien exceeds
PL
Permit Limit OCiginal
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 8 of 50

��'.r san,m;t Env;romnental Technolog;es, /ne. Analytical Report
3310 W1n St.
C aho a Falls, Ohio 44223 (base report)
CtiVIRONM€NTAL TECONOLOGI€5, INC �' S WO#: 17030217
Anafyticnl LwbAreiorles TEL. [phone]!! FAX: (330J 253-4489
Website: htro //www seuekcom Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matriz: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-OOIA
Project: Dunn WWTP
Client Sample ID Dunn W WTP
Analyses Result RL Qual Units DF Date Analyzed
RCI SW9014 Analyst: MS
REACTIVE CYANIDE (901417.3.3.2) -SOLID
Cyanide, Reactive ND 0.500 mglKg 1 3/6/2017 11:45:00 AM
IGNITABILITY OF SOLIDS (SW -846: 1030) SW1030 Analyst: RMT
Ignitabilily Non -Flammable. 1 318/2017 11:00:00 AM
RCI SW9045D Analyst: DHC
PH (SW9045D)
pH g,5 s.u.Q19.7C 1 3/10/20174:03:00 PM
RCI SW9034 Analyst: MS
REACTIVE SULFIDE (9034)
Sulfde, Reactive ND 25.0 mg/Kg 1 3/6/2017 11:45:00 AM
Qualifiers: " Value exceeds Maximum Contaminant Level.
H Holding times for preparation or analysis exceeded
MC Value is below Minimum Compound Limit.
ND Not Detected at the Reporting Limit
P Second column confirmation exceeds
R RPD outside accepted recovery limits
Page 9 of 50
E Value above quantitation range
M Manual Integration used to determine area response
N Tenmtively identified compounds
O RSD is greater than RSDlimit
PL Permit Limit Original
RL Reporting Detection Limit

ca
)
k
CY
f/
CY
.r\
\3\
\\){
2§y
EE!!
.2\
\)fLO
\))\
|§y
{
995§)5§
0
&
§
\sE �! $J(}aE
\\7£#/� \\Eo
\\ I\\\\\\/ w\ ®{
!a leeeeRee )2 7 eeeeeee
\
0
)
k
CY
f/
.r\
\3\
\\){
2§y
EE!!
\)fLO
\))\
\sE �! $J(}aE
\\7£#/� \\Eo
\\ I\\\\\\/ w\ ®{
!a leeeeRee )2 7 eeeeeee
\
0
)
k
(�(\()\)\
f/
\3\
\\){
EE!!
\)fLO
\))\
{
995§)5§
0
&
;7\\
=-pk
\
\sE �! $J(}aE
\\7£#/� \\Eo
\\ I\\\\\\/ w\ ®{
!a leeeeRee )2 7 eeeeeee
\
0
)
k
(�(\()\)\
f/
\3\
\\){
\sE �! $J(}aE
\\7£#/� \\Eo
\\ I\\\\\\/ w\ ®{
!a leeeeRee )2 7 eeeeeee
\
0
)
)
k
f/
\3\
\\){
EE!!
\)fLO
\))\
_>0
/\ƒ
)
f/
\3\
\)fLO
/\ƒ
0
&
;7\\
=-pk

a
m
N
a
=
❑
a
J
c
0
J
-
Ir
�
c
E
Vl
v
�
U
c
r
�
a
o
uai
�
E
m
a
a
N
n
e
a
E
iD
m
a
a
d
�
�
z
o
o
�
2
N
N
=
�
rn
n
a
=
❑
a
J
c
a
J
-
Ir
�
c
❑
Vl
v
�
U
c
r
�
�
7
u
Y
E
m
a
a
N
n
m
a
E
iD
m
a
m
d
�
�
U
J
o
�
2
N
N
=
m
~I
n
❑
❑
r
❑
❑
E
0
N
E
S
FI
�
-
o
a`
-
3
�
U
J
N
Q
Z
tll
Q
U
�
o
W
o
❑
fn
U
Q
F-
a
=
❑
a
c
c
a
J
-
�
�
c
>
Vl
v
�
U
c
�
�
�
7
u
Y
E
m
a
a
N
n
m
a
E
m
a
m
d
�
�
U
J
o
�
o
=
m
~I
n
>
J
r
❑
❑
o
0
N
E
S
FI
�
-
o
�
O
3
�
U
N
c
Z
tll
Q
�
o
N
o
❑
fn
U
Q
F-
�
d
a
Z
~
a
U
r
�
-
�
a
v
a
=
❑
a
w
c
m
J
a
�
�
N
�
Vl
v
�
U
n
A
�
�
H
u
a
E
m
a
v
N
E
m
a
E
m
a
m
d
�
�
U
a
=
a
w
c
a
J
a
�
-
E
Vl
v
J
U
❑
A
�
�
n
u
a
E
m
a
v
N
�
a
a
E
m
a
m
d
�
�
U
Q
c
o
o
=
m
N
tr'
J
r
❑
❑
o
0
M
E
V
FI
n
-
o
�
O
3
a
U
N
c
J
tll
Q
�
o
N
o
❑
fn
U
Q
F-
V
W
a
Z
~
a
=
a
w
c
a
J
a
�
-
E
Vl
v
J
U
❑
A
�
�
n
u
a
E
m
a
v
N
Y
o
a
E
m
a
m
d
a
�
U
Q
c
o
o
=
m
N
tr'
J
r
a
=
a
w
c
0
J
a
�
-
!r
Vl
v
>
U
a
A
�
�
n
r
a
E
m
a
v
N
Y
o
a
E
r
a
m
d
J
�
U
Q
C
z
o
=
m
N
tr'
J
r
❑
❑
o
0
M
E
V
FI
n
-
o
�
O
3
a
U
N
c
J
tll
Q
�
o
N
o
❑
N
�
a
N
E
Z
a
a
=
a
c
c
0
J
a
�
-
Vl
v
>
U
A
�
0
❑
❑
a
E
m
a
v
N
Y
o
a
E
a
m
d
a
�
U
Q
C
z
o
a
m
tr'
J
r
c
�
o
0
M
J
V
FI
n
>
o
�
O
a'
I
U
N
N
_Y
tll
N
�
o
N
o
❑
N
�
a
N
E
Z
a
Z
~
U
�
-
�
a
v
N
o
a
a`
-
vu
F=
Q
r
0
J
U
fn
Q
a
=
a
c
c
0
J
n
�
-
Vl
v
E
U
H
�
0
❑
❑
a
E
m
a
v
N
Y
o
a
a
=
a
c
c
0
a
-
Vl
v
E
U
�
❑
0
❑
❑
a
J
�
a
v
N
Y
o
a
E
`
m
a
a
(A
U
Q
a
=
a
c
c
0
a
-
Vl
v
E
w
❑
0
N
❑
a
J
a
a
❑
N
Y
o
a
a
�
a
a
m
�
z
z
o
a
m
tr'
rn
r
a
=
a
c
c
a
a
-
Vl
v
K
w
❑
N
❑
Y
J
a
a
❑
N
Y
o
a
a
�
a
m
m
�
a
m
E
m
r
?
o
M
M
J
V
FI
n
>
o
N
O
a'
=
U
N
N
N
Z_
�
o
N
o
❑
N
�
a
N
E
Z
a
m
~
�
-
a
v
�
o
C
a`
-
vu
a
Q
r
m
J
U
fn
Q
Q
IU -
�
K
V
9
W
m
❑
v
�
a
=
a
c
c
a
a
-
Vl
v
>
w
fL
N
❑
Y
J
a
a
❑
N
Y
o
a
a
�
a
m
m
�
a
m
E
m
c
?
o
U
r
_
V
FI
n
>
o
N
O
a'
Y
U
2
N
N
Z_
�
o
N
o
❑
N
�
a
N
E
Z
a
m
~
V
o
a
v
�
a
C
J
a
Q
r
m
U
fn
U
Q
IU -
�
E
=
a
c
a
-
a
Vl
rL
N
w
fL
N
❑
Y
J
a
a
❑
N
❑
o
a
�
H
m
�
E
m
E
m
�a
O
❑
2
�
o
N
O
a'
U
z
v
O
Z_
�
o
N
o
❑
N
�
a
N
E
a
m
~
V
o
a
C
J
E
Q
m
U
fn
U
Q
IU -
E
=
a
c
a
-
a
Vl
E
n
w
fL
c
Y
J
a
a
❑
N
❑
o
a
�
H
r
J
E
m
E
m
r
O
❑
2
�
W
N
O
a'
z
Z_
�
o
N
❑
❑
N
�
a
N
E
a
~
E
=
a
c
a
-
Vl
E
n
w
fL
c
Y
a
a
❑
a
a
o
a
�
H
r
J
E
m
E
r
O
❑
2
N
W
O
a'
C
Z_
N
❑
❑
N
�
a
N
E
a
~
V
o
a
C
J
Q
m
U
o
�
K
9
E
=
a
c
a
-
Vl
E
n
w
�
c
Y
a
a
a
a
a
o
O
H
�
J
E
m
o
O
❑
2
N
W
O
a'
C
Z_
N
J
O
N
�
a
N
a
~
V
o
J
=
r
Vl
E
�
c
A
a
a
a
a
o
�
H
�
0
E
m
o
O
❑
o
�
W
O
a'
C
d
V
Q
a
0
m
�
9
m
❑
v
�
J
(A
U
Q
IU -
J
�
E
q
c
A
a
a
a
a
o
�
0
o
O
�
o
�
W
O
a'
J
�
E
A
0
o
O
�
o
�
C
d
a
J

§
3
\
/
)
\
�
(}/ƒ
))
!)\i
f!\
iaa!
)(\0
)%)LO
E@]§
7j§)
\)%4
E`l
)({
))\\
\
){\°
*
)
))
f!\
)(\0
)%)LO
\)%4
E`l
)({
\
){\°
\\\{
\$/{
l;2�
=,§e
/\$
)(\0
\)%4
E`l
){\°
\\\{
,_),

�
Q
m
❑
D
m
m
0
Z
E
n
K
y
J
❑
v
❑
9
N
a
r
K
a
U
N
46
a
❑
m
�
a
LO
�
a
E
N
r
Z
Z
o
E
E
a
Y
30
d
K
U
Y
�
Q
❑
D
m
m
n
Z
E
n
K
y
J
❑
n
9
N
a
r
�
a
U
N
46
a
�
—
E
m
a
LO
�
�
E
N
r
Z
�
o
E
E
a
Y
30
d
ce)
°
Y
o
x
e
a
a
a
E
1O
❑
4q
0
o
O
N
t
a
E
m
n
E
o
a
d
NS
v
Ej
o>
T
a
n
o
W
>
C
J
a
4❑
a
N
a
w
U
o 0 0
Y
N
W
P�
V
N
�
d
>
x
.V+
m
E
E
N
N
�
Q
❑
D
m
m
n
Z
E
n
K
y
J
E
n
9
N
a
v
m
a
U
N
46
a
�
—
E
m
a
LO
o
�
�
N
�
Z
Z
o
E
E
a
Y
30
d
ce)
°
Y
o
e
a
a
a
E
1O
❑
4q
m
N
O
°
t
a
E
m
o
E
o
a
d
NS
v
Ej
o>
N
n
y
W
>
Q
c
a
4❑
3
N
a
w
n
U
Y
N
N
P�
V
N
a
>
x
.V+
.
E
E
N
N
?i
N
Z
U
"
J
a
—
CY
c
F
p
o
o
d
0o
O
M
m
W6Co
T
W
�
Q
❑
D
m
m
n
Z
E
n
K
y
J
E
n
9
N
a
v
m
a
U
N
a
a
�
—
E
m
a
LO
o
�
Z
Z
o
Z
Z
o
�
Q
❑
D
m
m
N
Z
U
�
�
y
J
E
❑
o
N
a
v
m
a
U
N
a
a
�
—
m
N
a
LO
o
�
Z
Z
o
Z
Z
o
E
E
a
Y
30
d
ce)
°
a
o
e
a
a
U
E
1O
❑
4q
E
N
O
°
a
E
m
o
E
o
a
�
NS
v
Ej
w
n
y
W
U
Q
c
a
4❑
3
N
a
w
A
U
a
N
N
P�
V
0
�
>
x
E
J
❑
D
m
m
N
Z
U
�
�
y
J
E
❑
o
N
a
v
m
a
U
a
a
�
—
m
N
a
LO
o
�
Z
Z
o
Z
Z
o
r
❑
Y
30
d
J
❑
❑
m
m
N
Z
U
�
�
y
N
E
a
o
N
a
v
m
a
U
a
a
�
—
E
N
�
LO
o
m
❑
K
Z
Z
o
r
❑
Y
30
d
ce)
°
a
o
e
a
a
m
E
1O
r
4q
E
N
O
a
a
E
E
o
N
�
NS
o
Ej
w
n
y
W
U
Q
o
a
a
3
Y
w
V
w
a
ro
ti
P�
0
0
�
>
x
E
E
N
N
?i
N
—
U
"
J
a
—
CY
c
O
a
O
M
m
W6Co
T
W
U
❑
co
o
a
�
J
❑
❑
m
m
N
Z
U
�
�
y
N
E
a
o
N
a
v
m
a
U
J
a
�
—
E
N
�
LO
o
m
❑
K
Z
Z
o
U
❑
Y
30
d
ce)
°
a
o
e
a
a
m
E
1O
r
4q
E
O
O
a
a
d
E
o
N
�
NS
o
Ej
w
n
y
W
U
Q
o
a
a
3
Y
w
V
w
a
ro
ti
P�
❑
.
�
>
x
E
x
m
N
?i
Z
—
U
"
J
o0
0
CY
O
�
O
J
❑
❑
m
m
N
Z
U
�
�
y
N
E
a
o
N
a
v
m
a
U
J
a
�
—
E
m
K
LO
o
m
,F
K
Z
Z
o
J
❑
❑
m
m
0
Z
E
a
y
J
E
N
N
a
v
m
a
U
J
a
�
—
J
r
K
LO
o
a
,F
K
Z
Z
o
U
❑
Y
30
d
ce)
°
o
o
e
F
a
E
1O
sm
4q
E
O
O
a
a
°y
E
�
v
NS
o
Ej
n
W
U
Q
a
di
J
❑
❑
m
0
Z
E
a
y
J
E
E
o
a
v
m
a
J
CD
❑
�
r
K
LO
o
a
,F
K
Z
Z
o
r
p
Y
30
d
ce)
o
J
❑
❑
m
y
Z
E
a
y
E
E
o
x
v
?
Ei
J
CD
v
�
N
K
LO
o
�
,F
K
C
r
p
Y
30
ce)
o
c
e
F
N
E
1O
sm
4q
E
O
O
a
a
�
�
v
NS
o
Ej
E
=
a
di
ui
Y
w
w
w
a
ro
ti
P�
❑
o
�
>
x
E
x
m
N
?i
Z
—
U
3
o0
0
CY
O
�
O
W6Co
T
N
U
❑
co
o
a
�
J
❑
❑
m
y
Z
E
a
y
E
E
o
x
v
?
Ei
J
CD
v
�
N
K
LO
o
�
,F
C
p
Y
30
ce)
o
c
e
F
E
1O
sm
4q
W
G
O
m
a
�
�
v
NS
o
Ej
E
Q
a
a
3
Y
w
w
w
a
ro
ti
P�
w
�
>
x
x
�
r
?i
Z
U
J
o0
0
CY
O
�
O
u
❑
❑
m
y
Z
Z
y
y
E
E
r
x
v
❑
Ei
J
CD
v
o
LO
o
�
,F
C
p
30
ce)
o
c
e
F
E
1O
tea.'
4q
W
G
O
m
�
�
v
NS
o
Ej
E
Q
a
a
w
za
o
a
ro
ti
P�
w
>
>
x
x
�
r
?i
O
�
O
U
❑
o
a
�
N
E
dwod
N
U
Q
N
u
w
y
E
v
❑
Ei
J
CD
LO
o
�
,F
C
p
30
ce)
o
c
e
F
>
tea.'
4q
W
G
O
w
u
w
y
o
Ei
J
CD
LO
,F
C
p
30
ce)
o
c
e
F
4q
G
o
�
v
NS
o
Ej
Q
a
a
w
za
o
a
ro
ti
P�
w
u
o
o
c
e
o
�
v
NS
o
w
o
a
a
>
>
x
x
�
a
u

�
§
k
\
\}
It
f;
-
=fCIE
�
{\
)k\
`
\
�
\�
\\\C
\)\
\m
(f
CY
It
f;
-
=fCIE
�
{\
)k\
\�
\\\C
\)\
\m
(f
CY
\\:
: \\
{
It
f;
-
=fCIE
�
{\
)k\
\�
\)\
\m
(f
CY
It
=fCIE
�
{\
\�
\m
(f
: \\
{
\
/
■
=fCIE
\
/
■

k
\
\/
)
)\
\
§
t;-
�§\
)(
))/
\\\CDLO
\))\
\}\\
\�
Ee#!
�§\
w,!!
3:
r«
\\)\
33*�
kk\
_(\
»)»m
=»=a
}}\7
\\\\
##2!
=-yk
.my,
k
\
\/
_
)
)\
\
§
t;-
�§\
)(
))/
\\\CDLO
\))\
\}\\
\�
Ee#!
w,!!
3:
r«
\\)\
33*�
kk\
_(\
»)»m
=»=a
}}\7
\\\\
_
k■ _ - �«
!e §:
;> a! m 20 cl \: !fI\((
I)\tk�Ne \ ItO \ 753 F- w m 1. ` CO { \ 7 3 \J7
)
)\
\
§
t;-
�§\
)(
66666
\\\CDLO
\))\
\}\\
\�
Ee#!
w,!!
3:
r«
\\)\
33*�
kk\
»)»m
=»=a
}}\7
\\\\
##2!
=-yk
.my,
\\�
ci
k■ _ - �«
!e §:
;> a! m 20 cl \: !fI\((
I)\tk�Ne \ ItO \ 753 F- w m 1. ` CO { \ 7 3 \J7
)
)\
\
§
®!i
�§\
)(
66666
\\\CDLO
\))\
\}\\
\�
Ee#!
w,!!
k■ _ - �«
!e §:
;> a! m 20 cl \: !fI\((
I)\tk�Ne \ ItO \ 753 F- w m 1. ` CO { \ 7 3 \J7
)
)\
\
§
®!i
)(
66666
\\\CDLO
\))\
\}\\
\�
Ee#!
w,!!
3:
k■ _ - �«
!e §:
;> a! m 20 cl \: !fI\((
I)\tk�Ne \ ItO \ 753 F- w m 1. ` CO { \ 7 3 \J7
)
)\
\
§
®!i
)(
66666
\\\CDLO
\))\
\}\\
k■ _ - �«
!e §:
;> a! m 20 cl \: !fI\((
I)\tk�Ne \ ItO \ 753 F- w m 1. ` CO { \ 7 3 \J7
]
)
)\
\
®!i
)(
\\\CDLO
\))\
\}\\
Ee#!
w,!!
3:
r«
\\)\
33*�
»)»m
=»=a
]
)\
®!i
\\\CDLO
\}\\
)2{LO
w,!!
\\)\
33*�
/
}}\7
\\\\
##2!
=-yk
\}\\
w,!!
\\)\
\\\\
.my,

�1
ro
C3 O
J
�n ❑
a
N
m � ❑ � � N o d �
m
Z Z o p b Q
G1
❑
M
n O
n m m
d ? A
N N =
1 N N N ❑ E N N N N �J
a c �
N N N
n m43w LO
0
J '0 O
a v a N
46
u A .
00 o o 0 o a 00
0 0 0 m o -a
N N O O O N N
O
U)0 0 0 0 c Y q
a w z w
m
Z
U N J
H O
F= a
0 0 0 o 0 0
0 0 0 0 0
E N
0 0 Q Q V« U ro
m �w�
n U > x > rn
X F O
Uw `o m ro U o `o 2 m
r U U ❑ _ `o L U U
.� E m o t c m E n o
o E a� m m CO E m
w ¢ c
w` xx� a

FNIIIRONMENTAL ifGHNOLGGIe5, 1ryG
Analyficel Lshoraiolfi's
March 15, 2017
Chad M. Hayes
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL: [phone]
FAX: [phone]
RE: DunnWWTP
Dear Chad M. Hayes:
Summit Environmenla] Technologies, Inc.
33]0 Win St.
Cuyahoga Falls, Ohio 44223
TEL: (330J 253-8211 FAX: [phone]
Website: h�//vww settekcom
Order No.: 17030217
Summit Environmental Technologies, I c. received 1 samples) on 3/3/2017 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Alabama 47600, Arkansas BS -0735, Cali£omia 07256CA, Colorado, Corurecticu[ PH -0108, Delaware, Florida NELAC E87688, Georgia E87688, Idaho
OH00923, Illinois 200061, Indiana C -OH -13, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Louisiana 04067, Maryland
339, Massachusetts M-OPH923, Minnesota 409711, New Harnpslvre 2996, New Sersey OH006, New York 11777, NoRh Carolina 39705 and 631, Nortb
Dakota R-201, Ohio Dririkivg Water 4170, Ohio VAP CL0052, Oklahoma 9940, Oregon OH2O0001, Rhode Island LA000317, South Cazolina 92016001,
Teras 7104704466-11-5, Aegion B BTMS-L, USDA/APHIS P330-11-00244, Utalr OH009232011-1, Vermont VT -87688, Vaginia 00440 and 1581,
Washington C891, West Virgirda 9957C
Page 1 of 50

������ Summit Environmental Technologies, Inc. CRJe. NaI'Yat1VC
3310 Win S[.
rNVIitDNMENTAL fiECHNOLOG1E5, 1NG: Cuyahoga Falls, Ohio 44223 WO#: 17030217
AnaPphcffi LahgraigrJas TEL: [phone] FiLY: (330J 253-4489 Date: 3/15/2017
Website: hap'// wsettek cony
CLI)JNT: Synagro
Proiect: Dunn WVJTP
WorkOrder Narrative:
17030217: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. State Certificates and Scopes of Accreditation
are attached as applicable. Results provided in this report for any parameter not listed on the Scope of
Accreditation should be considered "not certified."
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence QC Comments:
ccv 20ppb c0306/ 1096834: Analytical Comments for voc-MSTR_npw(8260), Sample ccv 20ppb
c0306/, Batch ID R66502 : The VOC CCV (Batch R66502) exhibited slightly high (120.5%) recovery
for Method -Specified CCC Vinyl chloride; All samples were ND for Vinyl chloride. All other Method -
Specified CCCs and SPCCs exhibited control.
mb-25849 1098253: Analytical Comments for tclp-svoc-cpest tclp(8081), Sample mb-25849, Batch ID
25849 : The TCLP Pesticides Method Blank (Batch 25849) exhibited high recovery for Surrogate:
DCB; MB was ND for all analytes of interest.
lcs-25849 1098254: Analytical Comments for tclp-svoc-cpest tclp(8081), Sample Ics-25849, Batch ID
25849 : The TCLP Pesticides LCS (Batch 25849) exhibited high recovery for Surrogate: DCB; All
Original
Page 2 of 50

CLIENT: Synagro
Prniect: DunttWWTP
other analytes of interest exhibited recoveries within acceptance limits.
Original
Page 3 of 50
snm,n. En , onmen a Te hno ogee , n .
Case
Narrative
�:, ���T
333 o win sr.
FPFVIROMMENTAL'fEGNNOVJCIES, tNG:
Cuyahoga Falls, Ohio 44223
WO#:
17030217
AnaPpticn7 tnborafvNes
TEL: (330J 253-8211 FAX: [phone]
Date:
3/15/2017
Website: httn //www settek com
CLIENT: Synagro
Prniect: DunttWWTP
other analytes of interest exhibited recoveries within acceptance limits.
Original
Page 3 of 50

������ SvmmitEnvironmenlalTechnologies,In Qualifiers and Acronyms
3310 Win S
FtiVIAONMFNTgL7ECNHOtAClES, tryC Cuyahoga Falls, Ohio 442: WO#: 17030217
AnaJyticar LnharaYorles TEL.' (330J 253-82]1 FAX: (330J 253-445 Date: 3/15/2017
Website: has //www settekeo
These commonly used Qualifiers and Acronyms may or may not be present in this report
Qualifiers
U
The compound was analyzed for but was not detected.
3
The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H
The hold time for sample preparation and/or analysis was exceeded.
D
The result is reported from a dilution.
F
The result exceeded the linear range of the calibration or is estimated due to interference.
MC
The result is below the Minimum Compound Limit.
*
The result exceeds the Regulatory Limit or Maximum Contamination Limit
in
Manual integration was used to determine the area response.
N
The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P
The second column confirmation exceeded 25% difference.
C
The result has been confirmed by GUMS.
X
The result was not confirmed when GUMS Analysis was performed.
B/MB+
The analyte was detected in the associated blank.
G
The ICB or CCB contained reportable amounts of analyte.
QC-/+
The CCV recovery failed low (-) or high (+).
R/QDR
The RPD was outside of accepted recovery limits.
QL-/+
The LCS or LCSD recovery failed low (-) or high (+).
QLR
The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+
The MS or MSD recovery failed low (-) or high M.
QMR
The MS/MSD RPD was outside of accepted recovery limits.
QV-/+
The ICV recovery failed low (-) or high (+).
S
The spike result was outside of accepted recovery limits.
Z
Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
RF
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Labomtory Conuol Sample
LOQ
Level of Quantitation
LCSD
Labomtory Control Sample Duplicate
PQL
Practical QuanCitation LimiC
QCS
QualiTy Control Sample
CRQL
ContracC Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Mahb: Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Mhrimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RF
Reextractimr
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
RLC
Repofing Limit Check
CF
Calibration Factor
DF
Dilution Pactor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 50

- ����� SummitEnviranmen[a7Technologies,Inc. WOrkOYder
3310 Winst. Sam le Summary
fNVIRONMENTgL�ECHNOLAGtes, SNC Cuyahoga Falls, Ohio 44223 P
Anafytienl Lnhoraigrle5 TEL: [phone] FiLY: (330J 253-4489 WO#: 17030217
Website: ht>n�//mwiv settek com ]5 -Mar -17
CLIENT: Synagro
Project: DunnWWTP
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
17030217-001 Dunn WWTP 3!2/2017 11:00:00 AM 3/3/2017 L40:00 PM Sludge
Page 5 of 50

/
/
2

����'� Summit Environmental Technologies, lnc. AIIa13'tlCal RCpOYi
3310 Win St,
FNVIRONMENTALTECHnOI,OGtEs, 1NG Cuyahoga Falls, Ohio 44223 (base report)
Analytical lafiaraP©rtes TEL: [phone]// FIX: (330J 253-4489 WO#: 17030217
Website: http �//rvwmsettek.corn Date Reported: 3/15/2017
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 3/2/2017 11:00:00 AM
Lab ID: 17030217-OOlA
Project: Dunn WWTP
Client Sample ID Dunn W WTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW7470A SW7470A Analyst: ALJ
TCLP MERCURY ANALYSIS (1 311174 7 0)
TCLP Mercury ND 0.00200 mg/L 1 317/2017 6:31:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW6010C SW3010A Analyst: VVK
TCLP METALS ANALYSIS (8010)
TCLP Arsenic(As) ND 0.500 mg/L 1 3/9/2017 10:09:47 AM
TCLP Barium(Ba) ND 5.00 mg/L 1 3/9/201710:09:47 AM
TCLP Cadmium(Cd) ND 0.100 mg/L 1 3/9/201710:09:47 AM
TCLP Chromium(Cr) ND 0.200 mglL 1 3/9/201710:09:47 AM
TCLP Lead(Pb) ND 0.500 mglL 1 3/9!2017 10:09:47 AM
TCLP Selenium(Se) ND 0.500 mg/L 1 3/9/2017 10:09:47 AM
TCLP Silver(Ag) ND 0.500 mg/L 1 3/9/201710:09:47 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID SW8270C SW3510C Analyst: CxA
SVOC 8270 TCLP BNA LIST
1,4 -Dichlorobenzene ND 0.0800 mg/L 2 3/13/20174:46:00 PM
2,4,5 -Trichlorophenol ND 0.200 mg/L 2 3/13/20174:46:00 PM
2,4,6 -Trichlorophenol ND 0.200 mglL 2 3/13/20174:46:00 PM
2,4-Dinitrotaluene ND 0.100 mg/L 2 3/13/2017 4:46:00 PM
Cresols, Total ND 4.00 mglL 2 3113/2017 4:46:00 PM
Hexachloro-1,3-butadiene ND 0.100 mg/L 2 3113120174:46:00 PM
Hexachlorobenzene ND 0.100 mg/L 2 3113/20174:46:00 PM
Hexachloroethane ND 0.0800 mg/L 2 3/1312017 4:46:00 PM
Nitrobenzene ND 0.0800 mg/L 2 3/13/2017 4:46:00 PM
Pentachlorophenol ND 0.200 mg/L 2 3/13/2017 4:46:00 PM
Pyridine ND 0.200 mg/L 2 3/13/20174:46:00 PM
Surr: 2-Fluorophenol 63.0 10 - 109 %Rec 2 3/13/2017 4:46:00 PM
Surr: Phenol -d6 64.2 10 - 109 %Rec 2 3/13/2017 4:46:00 PM
Surr: Nitrobenzene -d5 67.5 19 - 120 %Rec 2 3113/2017 4:46:00 PM
Surr. 2,4,6-Tribromophenol 77.6 10 - 120 %Rec 2 3/13!2017 4:46:00 PM
Surr. 2-Fluorobiphenyl 62.9 22 - 117 %Rec 2 317312017 4:46:00 PM
Surr: p-Terphenyl-d14 75.8 34 - 116 %Rec 2 3/13/2017 4:46:00 PM
Qualif7ers: `
Value exceeds Maximum Contaminant Level.
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used [o determine area response
MC
Value is below Minimum Compound Limit
N
Tentatively identified cornpounds
ND
Not Detected at the Reporting Limit
O
RSD is greater than RSDlimit
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 7 of 50