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HomeMy WebLinkAboutNCS000329_Monitoring Reports_20160921September 21, 2016 Attn: Central Files N.C. Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Central Files: SAP 2 � 2pi6 CENTRAL FILES DWR SECTION Attached, please find stormwater monito> ing data fur Permit No NCS000329 OATI P.O. Box 5030 2020 Ashciaft Avenue Monroe, NC 28111-5030 Phone: (704) 289-4511 Fax: (704) 290-5194 Email: joe.hinkle(a,atimetals.com 1'lie originals and one copy are included. The monitoring data is for the following monitoring schedule: Monitoring Period Sample Number Start End Year 7 — Period 1 13 March 1, 2016 August 31, 2016 Analytical monitoring includes: • Outfall #01 (B), commingled stormwater • Outfall #02 (B), non -commingled stormwater • Outfall #03 (B), non -commingled stormwater • Non Contact Cooling Water #1 - #8 If you have any questions or need additional information, please contact me at 704-289-4511. Thank you. Sine ely, V_ datt, .10 lnkle En ironmental Manager Bakers o, ' Fonn Person Collecting Samples: Laboratory Performing analysis: Analytical Techniques and Methods Results of Sample Analvcic- Sample Time: Stormwater Discharge Outfall #01 (Commingled) Drainage Area = 2,915,470sq. ft. = 69 acres % Impervious = 34% J 40 CFR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD o2 &. q 30 COD U.® 120 TSS 100 Cadmium P 0.001 Chromium, total recoverable 1 Copper, total recoverable ® 3 0.007 Nickel, total recoverable /'/P 0.26 Zinc, total recoverable / /,V 0.067 Oil and Grease 20 Temp (effluent) 3/. (deg C) n/a Temp (downstream) / (deg C) n/a Temp (upstream) 91.3 (deg C) n/a Total Residual Chlorine 3 0.017 pH (std units) 6-9 (std units) Storm Date: "/8 ' /lo Storm Duration: 3 D (Hrs.) Inches of Rainfall: ®• '1O Duration of time preceding rain event exceeding 0.111: r Estimated Flow Calculation: Q = CIA Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (.4 x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34) Q(Total, cfs) = 1.5180 x ®. yO (Inches of rain) + 1.7595 x Q. 110 (Inches of rain) = / j// cfs FHC — RW — Mnn4-4no R-4 Fnrn. — i?— 7 aceAnalytical www.pacWabs.com September 07, 2016 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92309568 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainardLpacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 19 aceAnalytical www.pacelabs.com CERTIFICATIONS Project: BAKERS STORMWATER Pace Project No.: 92309568 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 Massachusetts Certification * M. NCO30 Vir(linia/VEt AP Cortification #- 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 19 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309568 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92309568001 BSW01 SM 2540D ALC 1 PASI-A 92309568002 BSW01 SM 5210B CJH1 1 PASI-A 92309568003 BSW01 SM 5220D CJH1 1 PASI-A 92309568004 BSWO'I EPA 16648 JMS 1 PASI-C 92309568006 BSW01 EPA200.7 SH1 5 PASI-A 92309568006 BSWO1 8M 4600 01 G MDW I PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 19 Pace Analytical Services, Inc. e 9800Suite Hunte svlle, NC28078 ,�aneAnalytical wwwpacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309568 Sample: BSW01 Lab ID: 92309568001 Collected: 08/19/16 07:14 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By DPJ 1 08/18/16 07:20 Collected Date 08/18/16 1 08/18/16 07:20 Collected Time 07:12 1 08/18/16 07:20 Field pH 7.8 Std. Units 0.10 1 08/18/16 07:20 Field Temperature 31.1 deg C 0.50 1 08/18/16 07.20 2640D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 18.3 mg/L 8.3 1 08/22/16 15:26 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 19 acmnalXical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309568 Sample: BSW01 Lab ID: 92309568002 Collected: 08/19/16 07:15 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 26.4 mg/L 2.0 1 08/20/16 03:44 08/24/16 22:07 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 19 aceAnalytical wmpecefabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309568 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW01 Lab ID: 92309568003 Collected: 08/19/16 07:16 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 72.0 mg/L 25.0 1 08/30/16 06:30 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 19 aceAnalytical wwwpacelabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309568 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW01 Lab ID: 92309568004 Collected: 08/19/16 07:18 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Oil and Grease Date: 09/07/2016 09:46 AM Analytical Method: EPA 1664E ND mg/L 5.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 08/23/16 08:14 Page 7 of 19 aceAnalytical www.pacelabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309568 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: l3SW01 Lab ID: 92309568005 Collected: 08/19/16 07:19 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 08/22/16 21:55 08/23/16 11:43 7440-43-9 Chromium ND ug/L 5.0 1 08/22/16 21:55 08/23/16 11:43 7440-47-3 Copper 19.3 ug/L 5.0 1 08/22/16 21:55 08/23/16 11:43 7440-50-8 Nickel ND ug/L 5.0 1 08/22/16 21:55 08/23/16 11:43 7440-02-0 line NI) ug/I 100 1 08/72/10 21.55 08/23/10 11-4`t 7440-00-0 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 19 aceAnalytical wmpacelabs.c= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 I luntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309568 Sample: BSW01 Lab ID: 92309568006 Collected: 08/19/16 07:20 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500CL G Chlorine, Residual Chlorine, Total Residual Date: 09/07/2016 09:46 AM Analytical Method: SM 4500-CI G 0.043 mg/L 0.024 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 09/02/1616:35 7782-50-5 H1 Page 9 of 19 �- aceAnalytical www.pacelabs.com Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 325932 QC Batch Method: EPA 1664B Associated Lab Samples: 92309568004 METHOD BLANK: 1805587 Associated Lab Samples: 92309568004 Parameter Units 011 and Groano rn(1/t QUALITY CONTROL DATA Analysis Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Matrix: Water blank Reporting Result Limit Analyzed Qualifiers NCI 60 08/23/16 08-00 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunteroville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1805588 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.1 88 78-114 MATRIX SPIKE SAMPLE: 1805589 92309031001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 34.3 86 78-114 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 325888 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92309568005 METHOD BLANK: 1805455 Associated Lab Samples: 92309568005 Parameter Cadmium Chromium Copper Nickel Zinc Matrix: Water Units Blank Result Reporting Limit Analyzed Qualifiers up/t ND 10 08/23/1610.13 ug/L ND 5.0 08/23/1610:13 ug/L ND 5.0 08/23/1614:25 ug/L ND 5.0 08123/1610:13 ug/L ND 10.0 08/23/1614:25 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Iiuntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1805456 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cadmium ug/L 500 506 101 85-115 Chromium ug/L 500 494 99 85-115 Copper ug/L 500 520 104 85-115 Nickel ug/L 500 493 99 85-115 Zinc ug/L 500 512 102 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805457 1805458 MS MSD 92309373001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Cadmium ug/L ND 500 500 505 502 101 100 70-130 1 Chromium ug/L ND 500 500 471 458 94 91 70-130 3 Copper ug/L ND 500 500 519 507 103 101 70-130 2 Nickel ug/L ND 500 500 430 429 85 85 70-130 0 Zinc ug/L ND 500 500 473 472 93 93 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805503 1805504 MS MSD 92309549002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 467 455 93 91 70-130 3 Chromium ug/L ND 500 500 451 439 90 88 70-130 3 Copper ug/L ND 500 500 486 472 96 94 70-130 3 Nickel ug/L 8.9 500 500 462 451 91 88 70-130 2 Zinc ug/L 41.9 500 500 502 490 92 90 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 11 of 19 aceAnalj cal www.pecelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 325866 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92309568001 METHOD BLANK: 1805270 Matrix: Water Associated Lab Samples: 92309568001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers TotA 9u9.1'1011(f id 901idx Intl/L NI) 2 6 08/22/10 16.20 LABORATORY CONTROL SAMPLE: 1805271 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1805272 92309381001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 14.9 14.5 3 SAMPLE DUPLICATE: 1805273 92309570001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 12.2 12.4 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 19 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 326649 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92309568006 METHOD BLANK: 1809616 Associated Lab Samples: 92309568006 Parameter Units C'hlorino, Total Rosiduel mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NI) 0 024 09/021113, 16,16 SAMPLE DUPLICATE: 1809617 92309578001 Dup Parameter Units Result Result Chlorine, Total Residual mg/L ND ND RPD Qualifiers H1 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 19 lacmnalXicalo www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 325737 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210B BOD, 5 day Associated Lab Samples: 92309568002 METHOD BLANK: 1804788 Matrix: Water Associated Lab Samples: 92309568002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers ROD, 6 dvy 1110/1. ND 2 0 08/2.4/16 22.07 LABORATORY CONTROL SAMPLE: 1804789 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers ROD, 5 day mg/L 198 193 97 84.6-115.4 SAMPLE DUPLICATE: 1804790 92309572002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 2.0 ND Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 19 aceAnaIX cal www.pacelabs.com i Project: BAKERS STORMWATER Pace Project No.: 92309568 QC Batch: 326642 QC Batch Method: SM 5220D Associated Lab Samples: 92309568003 METHOD BLANK: 1809582 Associated Lab Samples: 92309568003 Parameter Units Ohemical OxYgen Domand mg/t LABORATORY CONTROL SAMPLE: 1809583 Parameter Units Chemical Oxygen Demand mg/L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed NI? 26 0 08/10/16 06:30 Spike LCS Conc. Result 750 741 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers LCS % Rec % Rec Limits Qualifiers 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809584 1809585 MS MSD 92308849002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 77.0 750 750 781 779 94 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809586 1809587 MS MSD 92309513002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 92.0 750 750 801 801 95 95 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 19 aceAnalytical www.pacelabs.corn ( QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92309568 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Hunlersville, NC 28078 (704)875-9092 8 Surrogate 1,2-Dlphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 82/0. T he result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 16 of 19 acmnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: BAKERS STORMWATER 92309568 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92309568001 BSW01 92309568004 BSW01 EPA1664B 325932 92309568005 BSW01 EPA200.7 325888 EPA200.7 325920 92309568001 BSW01 SM 2540D 325866 92309568008 BSW01 SM 4500-CI G 326649 92309560002 08W01 SM 5210B 325737 SM 5210B 325753 92309668003 BSW01 SM 5220D 326642 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 17 of 19 a Document Name: Document Revised:April 25, 2016 1�2'eAnalXical' Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CHR-CS-003-rev.19 Pace Huntersville Quality Office • • • Client (Name: I r `I` I Project #: I 1 Courier: ❑Fed Ex ❑UPS ❑LISPS ❑Client I II I 1 ( I) ❑ Commercial ❑Pace ❑Other: ; 92ZO9568 Custody Seal Present? Yes ❑ []No Seals Intact? ❑Yes [�]hro Packing Material; ❑Bubble Wrap [Bubble Bags ❑None ❑Other: Date/Initials Person Examining Contents: Thermometer: T1505 Type of Ice: ❑Wet ❑Blue ❑None Samples on ice, cooling process has begun Correction Factor: 0.0°C Cooler Temp Corrected (°C): /'. Biological Tissue Frozen? ❑Yes ❑No ❑N/A Temp should be above freezin t 6°C go USDA Regulated Soil (❑ N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? r-1„-- ^— Chain Of Custody Present? QYes ❑No Samples Arrived within Hold Time? ❑Yes ONO Short Hold Time Analysis (<72 hr.)? -1- ❑No Rush Turn Around Time Requested? ❑Yes )�Juo` Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Samples Field Filtered? Sample Labels Match COC? -includes Date/Time/ID/Analysis Matrix: \]'f All containers needing acid/base preservation have been checked? All containers needing preservation are found to be in compliance with EPA recommendation? (HNO3, H2SO4, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Exceptions: VOA, Coliform, TOC, Oil and Grease, Samples checked for dechlorination? Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? Paco Trip Blank Lot N (if purchased): _ CLIENT NOTIFICATION/RESOLUTION QYes [:]No ❑N/A Dyes ONO ❑N/A ©Yt#s ONO ❑N/A ❑Yes_ ❑No ON/A QYes ❑No ❑N/A 1. 2. 3. 4. 5. 6. Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? ❑Yes ONO Comments(Dlscrepancy: 7. 8. Note if sediment is visible in the dissolved container 9. lO. HNC3 pH<2 QYes ❑No ❑N/A Ha pw2 H2S" PH" ]Yes ONO ❑N/A Na(NpH>12 ❑Y,es ❑No nN/A 140H/Z.0AcpH,9 L_JYes LJNo I JN)A 11. ❑Yes ONO ®N/A, 12, ❑Yes ONO ❑"/ 13. ❑Yes ONO [ N/A Field Data Required? ❑Yes ONO Person Contacted: Date/Time: --Comments/Sample — — Discrepancy: Project Manager SCURF Review: t' Date: Project Manager SRF Review: m 7 Date:l� �J Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office {i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 18 of 19 w m (NIA) Ioelul salfteS z ui 6 z z 0 (NIA) z ui a: z j e) In 0 0 paleas Apolsno n. w m a. J y (NIA) ODI UO POA!000a (N/A) @u!jOlq7lL-plsZ r, 0, u! dwa_L >- L) z w z 0 w 0 LL c .2 lu 0 Cl) w 0� m 0 D z w 0 (U W cr N hk jss.L sisAleuV w A) ply laq)o w QQ loueqia vq cOzSz6N o. HOeN 10H 'ONH Ix E 3 E 'OSzH XI J. I 0 z c u SK pamasaidun 5 +Ix F T -2 .5 E 0 < E ti < a w Z-i L a SU3NIV1NOO JO # N011031100 IV dN31 BldlIVS w a. w m uj tw z 2 < L 0 0 2 LD Z z 0 E w w A I w 0 < W Z z LLJ 0,) ON M M -k�l z 0 w IL U) 0 w rL < (L E Zl Q w o D CY 6100=0 sv�jo=�O) 9dAI 31dNVS �bj -,�j z w 3C1OOXj�JjVjrj s <- -ad 7:�- - - , 0 E E w — --- 0 u 3: -0 < t'n0 0 C z w w z w L) < z CL in 0 < < C, C, E 0 Ea E ,)0 Q_ P; ige 19 of 19 U) 0: u Q w 2j w L LL Alvac - Bakers Plant Stormwater Monitoring Report Form Sample Date: R �/b �14_ Sample Location: Person Collecting Samples: Laboratory Performing Analysis: Analytical Techniques and Methods: Results of Sample Analysis: Sample Time: _ 7023�� . Stormwater Discharge Outfall #02 (Non -Commingled) Drainage Area = 212,952sq. ft. = 4.9 acres % Impervious = 12% 40 C'FR Part 136 Parameter Results (mg/1) Benchmark Values (mg/1) BOD a 0 30 COD ga 0 120 TSS / O0 100 Cadmium N- 0.001 Chromium, total recoverable Q.I 1 Copper, total recoverable 0.007 Nickel, total recoverable ®, ®1I/�0 0.26 Zinc, total recoverable 0.067 pH (std units) 6-9 (std units) Storm Date: S Storm Duration: a3• ® Mrs.) Inches of Rainfall: Duration of time preceding rain event exceeding 0.111: —� (Hrs.) Estimated Flow Calculation: Q=CIA Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (.4 x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/ft. x 4.9 x .12) Q(Total, cfs) = 0.1437 x ®• 410 (Inches of rain) + 0.0441 x D• YO _ (Inches of rain) = 0.0?,S cfs F.HC — CW — Mnnitni inv RPnnrt Fnn — RPv 1 aceAnalytical www.pacelahs.com August 30, 2016 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, incerely, Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 15 Pace Analytical Services, Inc. aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.p&celabs.com (704)875-9092 CERTIFICATIONS Project: BAKERS STORMWATER Pace Project No.: 92309572 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification #: 84 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NEL.AP Certification #: F87648 South Carolina Certification #• 99030001 Mab6aohubbil.6 GaIlilloallon M. M NU030 Virgtrda/VELAI' Cerlitloalion A". 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 15 t aceAnalytical wwwpacelabs.com SAMPLE ANALYTE COUNT Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92309572001 BSW02 SM 2540D ALC 1 PASI-A 92309572002 BSW02 SM 5210B CJH1 1 PASI-A 92309572003 BSW02 SM 5220D CJH1 1 PASI-A 92309572004 BSW02 EPA 200.7 SH1 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 15 acmnalytical www.pacelabs.corn ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW02 Lab ID: 92309572001 Collected: 08/18/16 07:25 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By DPJ 1 08/18/16 07:35 Collected Date 08/18/16 1 08/18/16 07:35 Collected Time 07:26 1 08/18/16 07:35 Field pH 7.6 Std. Units 0.10 1 08/18/16 07:35 Field Temperature 28.4 clog C 0 60 1 08/18/1F 07,15 2540D Total Suspended Solids Analytical Method: SM 2540D Total Suspended Solids 100 mg/L 6.2 1 08/22/16 15:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 aoAnalXical wwvw.pacelabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: ' BSW02 Lab ID: 92309572002 Collected: 08/18/16 07:27 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5210B BOD, 5 day Analytical Method: SM 5210B BOD, 5 day 2.0 mg/L 2.0 1 08/20/16 03:44 08/24/16 22:07 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 I eAnalytical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309572 Sample: BSW02 Lab ID: 92309572003 Collected: 08/18/16 07:28 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 82.0 mg/L 25.0 1 08/30/16 06:30 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 acmnalytical www.pacelabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW02 Lab ID: 92309572004 Collected: 08/18/16 07:29 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 08/22/16 21:55 08/23/16 18:14 7440-43-9 Chromium 19.1 ug/L 5.0 '1 08/22/16 21:55 08/23/16 18:14 7440-47-3 Copper 118 ug/L 5.0 1 08/22/16 21:55 08/23/16 18:14 7440-50-8 Nickel 14.6 ug/L 5.0 1 08/22/16 21:55 08/23/16 18:14 7440-02-0 71ne 116 ug/t 100 1 08/22/16 21 66 08/23/16 18 14 7440 66 6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309572 QC Batch: 325889 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92309572004 METHOD BLANK: 1805461 Matrix: Water Associated Lab Samples: 92309572004 Blank Reporting Parameter Units Result Limit Analyzed C'HldrflIUM ug/L N[1 1 () 08/23/16 18-(18 Chromium ug/L ND 5.0 08/23/1018.08 Copper ug/L ND 5.0 08/23/1618:08 Nickel ug/L ND 5.0 08/23/1618:08 Zinc ug/L ND 10.0 08/24/1615:43 LABORATORY CONTROL SAMPLE: 1805462 Parameter Units Cadmium ug/L Chromium ug/L Copper ug/L Nickel ug/L Zinc ug/L Qualifiers Spike Cone. LCS Result LCS % Rec % Rec Limits 500 465 93 85-115 500 462 92 85-115 500 479 96 85-115 500 455 91 85-115 500 467 93 85-115 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805463 MS 92309572004 Spike Parameter Units Result Cone. Cadmium ug/L ND 500 Chromium ug/L 19.1 500 Copper ug/L 118 500 Nickel ug/L 14.6 500 Zinc ug/L 116 500 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805501 MS 92309538002 Spike Parameter Units Result Cone. Cadmium ug/L ND 500 Chromium ug/L ND 500 Copper ug/L 0.0078 500 mg/L Nickel ug/L ND 500 Zinc ug/L 0.039 500 mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersvilie, NC 28078 (704)875-9092 Qualifiers 1805464 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 500 479 479 96 96 70-130 0 500 498 500 96 96 70-130 0 500 616 613 100 99 70-130 0 500 479 479 93 93 70-130 0 500 586 585 94 94 70-130 0 1805502 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 500 483 477 97 95 70-130 1 500 481 479 96 96 70-130 0 500 508 505 100 99 70-130 1 500 466 462 92 91 70-130 1 500 504 500 93 92 70-130 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Qual Qua[ Page 8 of 15 aceAnalytical wwwpacelabs.com Project: BAKERS STORMWATER Pace Project No.: 92309572 QC Batch: 325866 QC Batch Method: SM 2540D Associated Lab Samples: 92309572001 METHOD BLANK: 1805270 Associated Lab Samples: 92309572001 Parameter Units lulal Suspended 5olld8 rng/L LABORATORY CONTROL SAMPLE: 1805271 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersviile, NC 28078 (704)875-9092 QUALITY CONTROL DATA Analysis Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers NU 2.b 08/22/ 16 16:20 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 240 96 90-110 SAMPLE DUPLICATE: 1805272 92309381001 Dup Parameter Units Result Result Total Suspended Solids mg/L 14.9 14.5 SAMPLE DUPLICATE: 1805273 92309570001 Dup Parameter Units Result Result Total Suspended Solids mg/L 12.2 12.4 RPD Qualifiers 3 RPD Qualifiers 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15 (�IaceAnalyticalo www.pwelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309572 QC Batch: 325737 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92309572002 METHOD BLANK: 1804788 Associated Lab Samples: 92309572002 Parameter Units BOD, S day ing/L LABORATORY CONTROL SAMPLE: 1804789 Parameter Units BOD, 5 day mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 08/24/16 22:07 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 198 193 97 84.6-115.4 SAMPLE DUPLICATE: 1804790 92309572002 Dup Parameter Units Result Result BOD, 5 day mg/L 2.0 ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15 Pace Analytical Services, Inc. acmnalXical o Kincey Ave. te 100 9800Hunte svlle, NCi28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309572 QC Batch: 326642 Analysis Method: SM 5220D QC Batch Method: SM 5220D Analysis Description: 5220D COD Associated Lab Samples: 92309572003 METHOD BLANK: 1809582 Matrix: Water Associated Lab Samples: 92309572003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chemical Oxygoit Drdrnend mg/L ND 26.0 08/30/16 06i30 LABORATORY CONTROL SAMPLE: 1809583 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 741 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809584 1809585 MS MSD 92308849002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 77.0 750 750 781 779 94 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809586 1809587 MS MSD 92309513002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 92.0 750 750 801 801 95 95 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:49 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15 aceAnalytical mm..pacelabs.com QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92309572 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. Rl - Reporting t imit Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S - 8urrugaLe 1,2-Dipheny1hydraLine decomposes lu and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte Date: 08/30/2016 08:49 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 12 of 15 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER Pace Project No.: 92309572 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92309572001 BSW02 92309572004 BSW02 EPA 200.7 325889 EPA 200.7 325919 92309572001 BSW02 SM 2540D 325866 92309572002 BSW02 SM 5210B 325737 SM 5210B 325753 92309572003 RSW02 SM 52201) 326642 Date: 08/30/2016 08:49 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 15 --Ra"ceAnapical . 441vtl upon trecetpt(5CUR) Page 1 of 2 Document No.: issuing Authority: F-CHR-CS-OD3-rev.19 Pace Huntersville Quality Client Iilanle; Pao. 9 of 9 fnr lntarn,l i len nq WID# 92309572 j } -�- 4j' Projec • Courier: ❑Fed Ex ❑UPS nLISPS ❑ Commercial apace ❑Client ❑other: 92;109572 Custody Seal Present? ❑oYes EIN'" Seals Intact? ❑Yes QNo` e Parkin Material: Date/initials Person Examining Contents: �. Al 1 �l{b/�, g []Bubble Wrap ❑Bubble Bags Mt- Other: Thermometer: T1505 ❑slue []None Type of ice: ❑Wet [Samples on ice, cooling process has begur Correction Factor: 0.0°C Cooler Temp Corrected (°C): Biological Tissue Frozen? ❑Yes []No--[:]N/ATemp should be above freezing to 6°C USDA Regulated Soil ([�.fVjA, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source El yes j0t Including Hawaii and Puerto Ricoi7 i—IYes Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr.)? Rush Turn Around Time Reauested? Zorrect Containers Used? -Pace Containers Used? containers Intact? imples Field Filtered? ;ample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: VV tll containers needing acid/base preservation have been EIY6 0119 CIN/A 1 1_ a YC_ [IN. ❑N/A 12. Ures UKO UN/A 4. QY ss ❑No 3N/A 5. [DYe"s ❑No [jN/A 6. UNo ❑N/A 7. []No [:]N/A 8. ❑No 1771N/A 9. 111 containers needing preservation are found to be in ompliance with EPA recommendation? HN09i H2SO4, NCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) Yes []No®NJA xceptions: VOA, Coiiform, TOC, Oil and Grease, 7RO/11015 lwntarl nnr i i u,. amples checked for dechlorination? ❑Yes [:]No DN/A leadspace in VOA Vials (>5-6mm)? ❑Yes ❑No rip Blank Present? ❑Yes []No EJN`JA rip Blank Custody Seals Present? ❑Yes ❑No ONjA ace Trip Blank Lot # (if purchased): CLIENT NOTIFICATION/RFsoitlTION Person Contacted: Comments/Sample 04screpancy: Project Manager SCURF Review: Project Manager SRF Review: Note: Whenever there is a discrepancy affecting North Carolina comp Out of hold, incorrect preservative, out of temp, Incorrect containers) if 10. HNO pHe2 HOpH<2 .,. _... H2s04 pHa MON pH>12 MOH/2n0k pH>9 11. 12. 13, Date/Time: is visible in the dissolved Field Data Required? []Yes []No Ily, Date; Date: __'i C ! t t r e samples, a copy of this form will be sent to the North Carolina —DEHNR Certification Office (i.e. Page 14 of 15 ma C � O Vi tr E U 10 U IZ: U 4 o E E F o z z fL U a a a .ti -iJ j m 0 E Gd a w a a ON W m C7 z a (dW00=0 SV'd9=9) 3dAl aldNVS (yak of sap» peen aas) 9000 MUM V c +� G Q x a G o�3ain03ci=0 0 F W a ® Z W 2 ^J DLij V yy f -{gym to ? m �� L #Wall • cI rI v ut m r co -To •- e15of15 Allvac - Bakers Plant Sample Location: Laboratory Performing Analysis: AnslyficalTechniques and Methods: Results of Sample Analysis: Sample Time: W��Pmfll �M= I 1 61 - Drainage Area = 336,580sq. ft. = 7.8 acres %Impervious = 15% 40_QPR Part 146 Parameter Results (mg/1) Benchmark Values (mg/1) BOD 30 COD 120 TSS 100 Cadmium /VIP 0.001 Chromium, total recoverable ocq_37 I Copper, total recoverable 0.5's_r 0.Nickel, 0.007 total recoverable J. 00618 0.26 Zinc, total recoverable 0.(96 _r5? 0.067 pH (std unit-,) 6-9 (std units) Storm Date: �16 Storm Duration: Mrs.) Inches of Rainfall: _42. Duration of time preceding rain event exceeding 0.1 ": - - 16 8 Q = CIA Q(Total) = Q(Pervious Area) + Q(hnpervious Area) Q(tot., cfs) = (A x inches rain/1 2 inches/ft. x 7.8 acres x .85) +.9 x inches rain/1 2inches/ft. x 7.8 x .15) Q(Total,cf§)=0.22l0x 0.!Ya -(Inches of rain)+ 0.0878 x_-a. (Inches of rain) 6. IR 3 cfs aceAnalytical "mpacelabs.mm August 30, 2016 Mr. Joe Hinkle Allvac RE: Project: BAKERS STORMWATER Pace Project No.: 92309570 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard(t_)pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 15 Pace Analytical Services, Inc. Kincey Ave. te 100 laiAnalytical ® 9800Hunte svlle, NC128078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: BAKERS STORMWATER Pace Project No.: 92309570 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification M 84 North Carolina Wastewater Certification #: 12 Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40 Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001 MOSS-whIICOttS Certification # M-NC030 Virginia/VFt AP Certification #- 460222 North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 15 aceAnalytical www.pacelabs.com SAMPLE ANALYTE COUNT Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309570 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92309570001 BSW03 SM 2540D ALC 1 PASI-A 92309570002 BSW03 SM 5210B CJH1 1 PASI-A 92309570003 BSW03 SM 5220D CJH1 1 PASI-A 92309570004 BSW03 EPA200.7 SH1 5 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 15 aceAnalytical www.pacelab.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309570 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW03 Lab ID: 92309570001 Collected: 08/18/16 07:34 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Field Data Analytical Method: Collected By DPJ 1 08/18/16 07:40 Collected Date 08/18/16 1 08/18/16 07:40 Collected Time 07:33 1 08/18/16 07:40 Field pH 7.2 Std. Units 0.10 1 08/18/16 07:40 Field Temperature 26.8 deg C 0.50 1 08/18/16 07:40 2540D Total Suspended Solids Analytical Method. SM 2540D Total Suspended Solids 12.2 mg/L 5.0 1 08/22/16 15:24 Date: 08/30/2016 08:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 acmnalj6cal www.pacelabs.com ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309570 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BSW03 Lab ID: 92309570002 Collected: 08/18/16 07:35 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua[ 5210B BOD, 5 day BOD, 5 day Date: 08/30/2016 08:48 PM Analytical Method: SM 5210B 10.8 mg/L 2.0 1 08/20/16 03:44 08/24/16 22:07 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 15 Pace Analytical Services, Inc. aceAnaly4ilti[11® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: BAKERS STORMWATER Pace Project No.: 92309570 Sample: BSW03 Lab ID: 92309570003 Collected: 08/18/16 07:37 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5220D COD Analytical Method: SM 5220D Chemical Oxygen Demand 32.0 mg/L 25.0 1 08/30/16 06:30 110i ll-719I0*1"MII3Cfi�Pi1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 15 acmnalyiical www.pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309570 Sample: BSW03 Lab ID: 92309570004 Collected: 08/18/16 07:39 Received: 08/19/16 07:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Cadmium ND ug/L 1.0 1 08/22/16 21:55 08/23/16 11:46 7440-43-9 Chromium 23.7 ug/L 5.0 1 08/22/16 21:55 08/23/16 11:46 7440-47-3 Copper 58.8 ug/L 5.0 1 08/22/16 21.55 08/23/16 11.46 7440-50-8 Nickel 6.8 ug/L 5.0 1 08/22/16 21:55 08/23/16 11:46 7440-02-0 Zinc 65.9 ug/L 10.0 1 08l22/16 21:bb 08/23/10 11:40 1440-00-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 15 aceAnalXical www.pacelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309570 QC Batch: 325888 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Associated Lab Samples: 92309570004 METHOD BLANK: 1805455 Matrix: Water Associated Lab Samples: 92309570004 Blank Reporting Parameter Units Result Limit Analyzed Cadmium ug/L ND 1.0 08/23/1610.13 Chromium ug/L NU b.0 08/23/1610:13 Copper ug/L ND 5.0 08/23/1614:25 Nickel ug/L ND 5.0 08/23/1610:13 Zinc ug/L ND 10.0 08/23/1614:25 LABORATORY CONTROL SAMPLE: 1805456 Parameter Units Cadmium ug/L Chromium ug/L Copper ug/L Nickel ug/L Zinc ug/L Qualifiers Spike Cone. LCS Result LCS % Rec % Rec Limits 500 506 101 85-115 500 494 99 85-115 500 520 104 85-115 500 493 99 85-115 500 512 102 85-115 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805457 1805458 MS MSD 92309373001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Cadmium ug/L ND 500 500 505 502 101 100 70-130 1 Chromium ug/L ND 500 500 471 458 94 91 70-130 3 Copper ug/L ND 500 500 519 507 103 101 70-130 2 Nickel ug/L ND 600 500 430 429 85 85 70-130 0 Zinc ug/L ND 500 500 473 472 93 93 70-130 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1805503 MS 92309549002 Spike Parameter Units Result Cone. Cadmium ug/L ND 500 Chromium ug/L ND 500 Copper ug/L ND 500 Nickel ug/L 8.9 500 Zinc ug/L 41.9 500 1805504 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 500 467 455 93 91 70-130 3 500 451 439 90 88 70-130 3 500 486 472 96 94 70-130 3 500 462 451 91 88 70-130 2 500 502 490 92 90 70-130 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Qual Page 8 of 15 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: BAKERS STORMWATER Pace Project No.: 92309570 QC Batch: 325866 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92309570001 METHOD BLANK: 1805270 Associated Lab Samples: 92309570001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 1805271 Parameter Units Total Suspended Solids mg/L Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 08/22/16 '15-20 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 240 96 90-110 SAMPLE DUPLICATE: 1805272 92309381001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 14.9 14.5 3 SAMPLE DUPLICATE: 1805273 92309570001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 12.2 12.4 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15 aceAnaIXical" www.pacelabs.com QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: BAKERS STORMWATER Pace Project No.: 92309570 QC Batch: 325737 Analysis Method: SM 5210B QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day Associated Lab Samples: 92309570002 MEIHODBLANK: 1804188 Matrix: Water Associated Lab Samples: 92309570002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers DOD, 5 day mg/L ND 2.0 08/24/10 22:07 LABORATORY CONTROL SAMPLE: 1804789 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 193 97 84.6-115.4 SAMPLE DUPLICATE: 1804790 92309572002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 2.0 ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15 aceAnalytical www.pacelabs.com Project: BAKERS STORMWATER Pace Project No.: 92309570 QC Batch: 326642 QC Batch Method: SM 5220D Associated Lab Samples: 92309570003 METHOD BLANK: 1809582 Associated Lab Samples: 92309570003 Parameter Units Chemical Oxygen Demand rng/L QUALITY CONTROL DATA Analysis Method: SM 5220D Analysis Description: 5220D COD Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 08/30/ 16 06:30 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 1809583 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chemical Oxygen Demand mg/L 750 741 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809584 1809585 MS MSD 92308849002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 77.0 750 750 781 779 94 94 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1809586 1809587 MS MSD 92309513002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chemical Oxygen Demand mg/L 92.0 750 750 801 801 95 95 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 15 laneAnalytical" www.pacelabs.com QUALIFIERS Project: BAKERS STORMWATER Pace Project No.: 92309570 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL- Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S e Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PAST -A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/30/2016 08:48 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 15 4 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BAKERS STORMWATER Pace Project No.: 92309570 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92309670001 BSW03 92309570004 BSW03 EPA 200.7 325888 EPA 200.7 325920 92309570001 BSW03 SM 2540D 325866 92309570002 BSW03 SM 52IOB 325737 SM 52-IOB 325753 92309570003 BSW03 SM 5220D 326642 Date: 08/30/2016 08:48 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 13 of 15 I Document Name: Document Revised:April 25, 2016 11!;31C1eAna1j4ica1' Sample Condition Upon Receipt(SCUR) Page 1 of 2 — Document No.: Issuing Authority: F-CHR-CS-003-rev.19 Pace Huntersville Quality Office Client Name: WID#: 923U46�U Project I Courier: [:]Fed Ex E]UPS nUSPS nClient n Commercial []Pace�- nOther: 92'41,09570 Custody Seal Present? nYes OW6 Seals Intact? nYes nNo Date/initials Person Examining Contents: Packing Material: nBubble Wrap E]Bubble Bags EJNone P16ther: c, i f 1- /" i`,-) ) Thermometer: T1505 Type of Ice: FlWet []Blue nNone [:]Samples on ice, cooling process has begun Correction Factor: O.O*C Cooler Temp Corrected (*C): Biological Tissue Frozen? [-]Yes []NO' nN/A Temp should be above freezing to 6°C USDA Regulated Soil ( Q /A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, []Yes []Ncr-- including Hawaii and Puerto Rico)? E]Yes E]No -- Comments/Discrepancy: Llidin of Lustudy Pmsunt F ON. ON/A I. Samples Arrived within Hold Time? QY6 [IN. ON/A 2. Short Hold Time Analysis (<72 hr.)? QyOrs- ONO QN/A 3. Rush Turn Around Time Requested? OYes QN6' 1771N/A 4. Sufficient Volume? [:] Ke ON. ON/A 5. Correct Containers Used? [Yes FlNo ON/A 6. -Pace Containers Used? []Yfis [-]No 0 N/A Containers Intact? E]Yes ' ONo 171 N/A 7. Samples Field Filtered? OYes [:]No Z ®N/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? Oes nNo 171 N/A 9. -Includes Date/Time/ID/Analysis Matrix: All containers needing acid/base preservation have been 10' HNOPH4 checked? QYes nNo 17IN/A All containers needing preservation are found to be in H(3 PH`Z compliance with EPA recommendation? HZS04 pW2 (HNO3, H2SO4, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) QYe's ONo ON/A NaOHpH>12 Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOCLLHg OYes ONo OK/A MOH/ZnM pH,9 Samples checked for dechlorination? [:]Yes ONo ON/A 11. Headspace in VOA Vials (>5-6mm)? [:]Yes E]No F1 WJA 12, Trip Blank Present? oyes nNo M d1A 13. Trip Blank Custody Seals Present? E]Yes FINo ONKA' Pace Trip Blank Lot ft (if purchased): CLIENT NOTIFICATION/RESOLUTION Person Contacted: Discrepancy: Date/Time: Field Data Required? E]Yes E]No Project Manager SCURF Review: Date: Project Manager SRF Review: j l Date: Note: Whenever there Is a discrepancy affecting North Caro rtrLacompliance samples, a copy of this form will be sent to the North Carolina DEHNR-Certification Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers) Page 14 of 15 0 .2 0 U) E wwwaae LU 0 co W U LL — 0 S C? 2 ui M (NIA) m,_ tselul sajdweS x 'I C) z z 0 z a 2 (NIA) F- 0 0 IJ 0 0 L) J01000 paleas U0, 0. w Apoisno (u cc IL C\,] a. co (WA) P31 UO w PDA!OODU (N/,k) autiolqo lenp!s@8 z o. u! dLu,?i Z W 0< 0 w < 0 .2 U) 0 n 0 z W C < 9 1 1 1 0 A cr w 5-: F- N/A t JSq.L SISAIL'Uvt, ti 0 loueqlaV4 w VSzEN Y) a A :� \ HOeN IOH S Q) 'ONH r Z%� S) 'OS'H W P@Alesajdun 0 < E 0 81 E X E 2 a F- w w w S83NIVA03 =10 # N011031100 IV d[131 31dkIVS w z IL -1 2 < M 2 w 0 0 0 w 0 E z w W M w w 0 Ft < z W-- Q, OCJz I I 0 - Z M 0: m 0 W LU K -i 0 w C) 101 6< -2j w 6 z z (diV(.)J=J 8VNV=91 9dU 3ldvivs Q) Q) w Ojai of sspn p!IeA eas) 3003 X18iVVI tir 0 E E 0 0 c OC' u x 41 < 0 �i;i! P 0 z w w z w 0 ui CL 1� D z 0 1. %J V� E E -b 0 0 < E w a Page 15 of 15 10 m ®o 00 00 -_1 (011 CA •P W N Ci tf3 (� ` °� i d ' o b Ig d o ® O ® O ® O p CrJ I Na � o y � �. r O O ` "C o �A NI ® "s rA m � a A7 Cy fD y eo b fteD p• o °C -P C) n b V. o � A o � CD 1 � MOW A� 1eAnalyticalo —pecelabs.com September 07, 2016 Mr. Joe Hinkle Allvac RE: Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Dear Mr. Hinkle: Enclosed are the analytical results for sample(s) received by the laboratory on August 19, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com Project Manager Enclosures cc: Mr. Preston Baucom, Allvac Mr. Tommy Long, Allvac David Pope, Allvac REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 18 aceAnalj6cal wwwpacelabs.com Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Charlotte Certification IDS 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #• M-NC0;30 North Carolina drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VEt AP Certification # 400.222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 18 Pace Analytical Services, Inc. m acmnalytical a 9800 Kincey Ave. Suite100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92309578001 BAKERS NON CONTACT #1 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578002 BAKERS NON CONTACT #2 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578003 BAKERS NON CONTACT #3 EPA1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578004 BAKERS NON CONTACT #4 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578005 BAKERS NON CONTACT #5 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578006 BAKERS NON CONTACT #6 EPA 1664E JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309578007 BAKERS NON CONTACT #7 EPA 1664B JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A 92309678008 BAKERS NON CONTACT #8 EPA 1664E JMS 1 PASI-C SM 4500-CI G MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 18 aceAnalytical" www.pacelabs.com ANALYTICAL RESULTS Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 I Iuntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92309678001 Collected: 08/18/16 07:30 Received: 08/19/16 07:20 Matrix: Water #1 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 08/23/16 08:15 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI O Chlorine, Total Residual ND mg/t 0 024 1 09/02/16 16-35 7782-50-5 H1 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 18 aceAnalytical www.pacelabs.= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT Lab ID: 92309578002 Collected: 08/18/16 07:49 Received: 08/19/16 07:20 Matrix: Water #2 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/23/16 08:16 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI C Chlorine, Total Residual ND mg/1 0024 1 09/02/16 16-35 778.2-50-5 H1 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 18 Pace Analytical Services, Inc. aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT Lab ID: 92309578003 Collected: 08/18/16 08:05 Received: 08/19/16 07:20 Matrix: Water #3 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/23/16 08:16 45000L G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, dotal Residual NU mq/L 0.024 1 09/02/16 16:35 7782-50-5 H1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 6 of 18 aceAnalytical wwmpamlabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT Lab ID: 92309578004 Collected: 08/18/16 08:22 Received: 08/19/16 07:20 Matrix: Water #4 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664E Oil and Grease ND mg/L 5.0 1 08/23/16 08:16 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.047 m0/L 0 024 1 09/02/16 16-35 7782-50-5 H1 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 aceAnafytical www.pacelabs.com Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT #5 Parameters HEM, Oil and Grease Oil and Grease 4500CL G Chlorine, Residual Chlorine, Total Residual Date: 09/07/2016 09:46 AM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92309578005 Collected: 08/18/16 08:36 Received: 08/19/16 07:20 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 1664B ND mg/L 5.0 1 08/23/16 08:17 Analytical Method: SM 4500-CI G 0.(160 mg/L 0 074 1 09/0.2/16 16 36 7782 60 6 H1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 8 of 18 s aceAnaIXical www.pecelabs.com ANALYTICAL RESULTS Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: BAKERS NON CONTACT Lab ID: 92309578006 Collected: 08/18/16 08:50 Received: 08/19/16 07:20 Matrix: Water #6 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/23/16 08:18 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual 0.089 mg/L 0 024 1 09/02/16 16-35 7782-50-5 1-11 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 9 of 18 Pace Analytical Services, Inc. aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT Lab ID: 92309578007 Collected: 08/18/16 09:10 Received: 08/19/16 07:20 Matrix: Water #7 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/1 .5.0 1 08/23/16 08:18 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, total Residual 0.46 mg/L 0.024 1 09/02/16 16-35 7782-50-5 H1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 10 of 18 aceAnalytical www.pacelabs.c= ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Sample: BAKERS NON CONTACT Lab ID: 92309578008 Collected: 08/18/16 09:27 Received: 08/19/16 07:20 Matrix: Water #8 Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM, Oil and Grease Analytical Method: EPA 1664B Oil and Grease ND mg/L 5.0 1 08/23/16 08:19 4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G Chlorine, Total Residual ND m0/L 0 024 1 09/02/16 16 35 7782-50-5 H1 Date: 09/07/2016 09:46 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 11 of 18 aceAnalytical www.pacelabs.com QUALITY CONTROL DATA Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 I luntersville, NC 28078 (704)875-9092 QC Batch: 325932 Analysis Method: EPA 1664E QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007, 92309578008 METHOD BLANK: 1805587 Matrix: Water Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007, 92309578008 Blank Reporting Parameter units Result t imit Analyred OLialifier,; Oil and Grease rng/L ND 5.0 08/23/16 08:09 LABORATORY CONTROL SAMPLE: 1805588 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L 40 35.1 88 78-114 MATRIX SPIKE SAMPLE: 1805589 92309031001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Oil and Grease mg/L ND 40 34.3 86 78-114 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 12 of 18 aceAnalytical www.pacelebs.com QUALITY CONTROL DATA Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 326649 Analysis Method: SM 4500-CI G QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007, 92309578008 METHOD BLANK: 1809616 Matrix: Water Associated Lab Samples: 92309578001, 92309578002, 92309578003, 92309578004, 92309578005, 92309578006, 92309578007, 92309578008 Blank Reporting rvirametor Units R65UIt Unit Analyzed Qualifiers Chlorine, Total Residual mg/L NU 0.024 09/02/16 16:35 SAMPLE DUPLICATE: 1809617 92309578001 Dup Parameter Units Result Result RPD Qualifiers Chlorine, Total Residual mg/L ND ND H1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18 acmnalXical www.pacelabs.com QUALIFIERS Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL- Practical Quantitation Limit. RL - Reporting Limit. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 S Surrogate 1,2-Diphenylhydrazlne decomposes to and cannot be separated from Azobenzene using Method 82/0. I he result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS H1 Analysis conducted outside the EPA method holding time. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 14 of 18 �acmnalytical" www.pacelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: NONCONTACT COOLING WATER Pace Project No.: 92309578 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92309578001 BAKERS NON CONTACT #1 EPA 1664B 325932 92309678002 BAKERS NON CONTACT #2 EPA 1664B 325932 92309578003 BAKERS NON CONTACT #3 EPA 1664B 325932 92309578004 BAKERS NON CONTACT #4 EPA 1664E 325932 92309578005 BAKERS NON CONTACT #5 EPA1664B 325932 92309578006 BAKERS NON CONTACT#6 EPA 1664B 325932 92309570007 BAKERS NON CONTACT #7 ErA 1664D 325932 92309618008 BAKERS NUN GUN IA(;1 #8 EPA I664B 325932 92309578001 BAKERS NON CONTACT #1 SM 4500-CI G 326649 92309578002 BAKERS NON CONTACT #2 SM 4500-CI G 326649 92309578003 BAKERS NON CONTACT #3 SM 4500-CI G 326649 92309578004 BAKERS NON CONTACT #4 SM 4500-CI G 326649 92309578005 BAKERS NON CONTACT #5 SM 4500-CI G 326649 92309578006 BAKERS NON CONTACT #6 SM 4500-CI G 326649 92309578007 BAKERS NON CONTACT #7 SM 4500-CI G 326649 92309578008 BAKERS NON CONTACT #8 SM 4500-CI G 326649 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 09/07/2016 09:46 AM without the written consent of Pace Analytical Services, Inc.. Page 15 of 18 Document Name: Document Revised:April 25, 2016 I. ace Analidical' Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CHR-CS-003-rev.19 Pace Huntersville Quality Office Name: WN:92309578 MClient -/ALL ; v, /"(,* Project i Courier: ❑ Commercial [JFed Ex DPace OUPS nUSPS nOther: nCl —ient III III III III fl1111111 92-008578 Custody Seal Present? E]Yes No Seals intact? Elyes []No Packing Material: &Bubble Wrap / 11 DBubble Bags nNone/ FJOther: Date/initials Person Examining Contents: -`� Thermometer: T1505 Type of Ice: DWet nBlue ONone .Samples on ice, cooling Iocess has begun Correction Factor: 0.0°C Cooler Temp Corrected ('C): Fl Biological Tissue Frozen? ❑Yes ffN.FIN/A Temp should be above freezing to 6°C USDA Regulated Soil NIA, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, 0Yes [3ho including Hawaii and Puerto Ricol? f-1VP; 1771KI. Cs�mmentsjpissrpanc Chain of Custody Present? OYCS,- ONO ON/A 1. Samples Arrived within Hold Time? Oyes ONO, ON/A 2. Short Hold Time Analysis (<72 hr.)? r-lv-. Q ON/A 3. Rush Turn Around Time Requested? mv— r7lNo ON/A 4. Sufficient Volume? ©Yes. ONo ONJA, 5, Correct Containers Used? O'Yes ONo ON/A 6. -Pace Containers Used? Elye// ON. ON/A Containers Intact? Iles Q/ ON/A 7. Samples Field Filtered? OYes,' ONc, ON/A 8. Note if sediment is visible in the dissolved container Sample Labels Match COC? ®Yes ONo ON/A 9. -Includes Date/Time/ID/Analysis Matrix: I All containers needing acid/base preservation have been / 10' NNOpW2 checked? OYes ❑ ONo Oi�/A All containers needing preservation are found to be in Fla PW2 compliance with EPA recommendation? HZ504 pH,2 (HNO3, H2SO4, HCI<2; NaOH >9 Sulfide, NaOH>12 Cyanide) OYes-' ONo [361A Exceptions: VOA, Coliform, TOC, Oil and Grease, N.O" PH'12 DRO/8015 (water) DOC,LLHg Y�s f-INo N/A N.OH/ZnOft p14,9 Samples checked for dechlorination? OYes ONo ONIA 11, Headspace in VOA Vials (>5-6mm)? nv— r-1 ❑— 041A 12. 13. Trip Blank Present? Me, 04. ❑NJA Trip Blank Custody Seals Present? [:]Yes 177INo 0 /A Pace Trip Blank Lol. # (if purchased): Nu. JFKAJ 10141RESOLUTION Person Contacted: Date !rne: ---C �mments/S J�mpl`e-- Discrepancy: Field Data Required? E]Yes [:]No Project Manager SCURF Review: l'r � . .. ... W- Date: Project Manager SRF Review: � / &'f/';"' Date: Note: Whenever there Is a discrepancy affecting North Carolina complIlince samples, a copy of this form will be sent to the North Carolina DEHNR Certificat—ion Office (i.e. Out of hold, Incorrect preservative, out of temp, incorrect containers) Page 16 of 18 m Jater monApia Specialty Materials Stor (NON CONTACT) Baker North Chain of Custody Record Prninrt IM-1 Ito K I ­­ 1, .1 . page HI � . — � .. -. I. I Sampler's Signature: •U111c: water Project Location: Allvac Baker Date: Ci 77 E Imi a) CL (A "L cu aj M (U E a III a) .> (u U 7i C (D < CL Requested Test E ~ (D M 0 E Parameters 0, ca CL 0 LI) 0 0 G one Y Residual Residual Chlorine L, G G /9, None —ne Y 2 '�, 9- I s ChlorineCLi I G None Y -Residual - I s 1 61), Residual Chlorine 61,), G G /,P, None Y 11716 Chlorine U L ine G G /t_P _& None Y •101 5� 6t' Residual Chlorinej4 G /7,P None Y 376 - —Residual Chlorineal - G Y :7. —VI- Residual Chlorine 7,r- G G /,P None Y �X ;:28.76 Residual Chl Chlorine Meter Calibrated. j N IThermometer Calibrated IN Sampling and Field analysis completed by: Relinquished By: Received Date: ITime: Date: -4 Received Pate: ITime:-- Lf? Li EH5Baker South SWREV #2 5/10/2016 Page 17 of 18 T1 Specialty Materials 13 TIM. , 01"Im (NON CONTACT) Baker north Chain of Custody Record Project Number/Name: NonContact Cooling Water page V2 Project Location: Allvac Baker Sampler's Signature: -6ate- > 0 as 0bI (> w v CL Requested Test E M C M > M 0 E Parameters M it 0 w w CL CL & fa)o 0 G G HCL Y 30,3q, Oil& Grease G G HCL Y Oil& Grease b 5 L Y Oil & Grease eceb,&-� 8Y :L Y Oil & Grease G G HCL Y Oil & Grease sww ee,,A, G G HCL Y Oil & Grease e AW G G HCL Y Oil& Grease G G HCL Y 6,z P_2 Oil & Grease Meter Calibrated- N IThermometer Calibrated: ff) N Sampling and Field analysis. completed by: Z3— �-11'11111-k Relinquished By: lRelinquished By: zz Date :R-/9-//6 Time: at Relinquished By: IRelinquished JDate ITime: i Date ITime: Page 18 of 18 C O �i i C 0 m m o K p, y o 0 � �Oc w � a o. �o 0 gz m �R 0 K 1 y O n M 'Ok y H C7 O d M O d 1.U+: Mrypr y yC� Fi tw O p" � p A� eqr � p� M C•i O ISeL y CD v O y ••h � � A y y A i/i " .. 3 , y CL y n. A eD O p "O O CQj pa�yy O �y p 'n ems•► O P� tD C Ir ewe q ."f Or G agrc, is �. a CD A O � �• O A� N � � r' l O r�i.• C C CD p q C e v c !F • ' AQ NCDEN Stormwater Discharge Dutfall (SDQ) Qualitative Monitoring Report For guidance on filling out this form, please visit. httD://aortal.ncdenr.org/web/wg/ws/su�npdessw#tab-4 Permit No.: N/C/ 5/ O/ O/ O/j/o? /j/ or Certificate of Coverage No.: IV/C/G/_/_/_/_/_/_/ Facility Name: County: e Inspector: e Date of Inspection: 9-4-16 Time of Inspection: 7 •'020�0• Total Event Precipitation (inches): e- !AQ Phone No. 7eV -e489- V-rll Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) all"Y'es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ,..-......____.....___-.___..._._..-----_-...___-----......._..._..... - -.........__........... _._.._-.-.._.-.._-------- ------ _ __ — -_.... ...... ...--.--------._._...---- ......__...__..._..� _ . Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be j performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred: A single storm event may contain up to 10 consecutive hours of no precipitation. i i E A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 20� 1. Outfall Description: Outfall No. Receiving Stream: Describe the industrial activil ditch, etc.) C� occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: (_1ro2/ 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): %L®!I e 4. Clarity: Choose the number which hest describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 Q 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ® 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1� 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes B. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes 0 10. Other Obvious Indicators of Stormwater Pollution: List and describe Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 �,� •e `/ ��*A NCDEN� Stormwater Discharge Dutfall (SDD) Qualitative Monitoring Deport P'orguidance on filling out this Corm, please visit. http://pQrtal.fLcdenr.org/mLeh/yvq/ws/u/IlPde5, w##tab-4 Permit No.: N/C/ 5"/Q/Q/Q/3//Q/ or Certificate of Coverage No.: Facility Name: '47:r &/VAX -13aKcnr County: _ Inspector: ZZ171'017 Phone No. Date of Inspection: Time of Inspection: Total Event Precipitation (inches): 1L410 Was this a `Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) �es ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, some permits do not have this requirement. Please refer to these definitions, if applicable. A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter interval is representative for local storm events during the sampling period, and the permittee obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. OutfaIl Description: Outfall No.S'VStru Receiving Stream: Describe the industrial activities (pipe, ditch, etc.) Did e IdGl;e Gree,� occur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: /26w , f ih 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): 00/7 i2 4. Clarlty: Choose the number which best describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 1 2 ® 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 ® 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: 1 3 4 5 7. Is there any foam in the stormwater discharge? Yeso 8. Is there an oil sheen in the stormwater discharge? Yes 9. Is there evidence of erosion or deposition at the outfall? Yes N�o 10. Other Obvious Indicators of Stormwater Pollution: List and describe 002 Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012 NCQENR Stormwater Discharge Qutfaii (SDQ) Qualitative Monitoring Report Forguidance on filling out this form, please visit. hW- jpQrtal.n.Cdciir Qrg/web/wq/`wa/au/n-pdessw#tab-4 Permit No.: N/C/S/D/o J D/3/a/Q/ or Certificate of Coverage No.: Facility Name: -9;rz' 41100-c - ,Bo Ac,-s County: LGni017 Phone No. 7011o?89-S+s'// Inspector: -po"a %opt 67/eni2 Date of Inspection: Time of Inspection: Total Event Precipitation (inches): Q. YD Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit? (See information below.) EKYes ❑ No Please verify whether Qualitative Monitoring must be performed during a "representative storm event" or "measureable storm event" (requirements vary, depending on the permit). ...... .... --.......-..._..---._._......._.-_._.... -- .......-----..__......_..._.......... ---...... -- ............._.._...----..__._._.._._.. _ --_ — _ ----------- ----- ---- --..._...__._.-.._._..._._..-..... Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be performed during a "representative storm event" or during a "measureable storm event." However, I some permits do not have this requirement. Please refer to these definitions, if applicable. I A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than 0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no precipitation. I A "measurable storm event" is a storm event that results in an actual discharge from the permitted site outfall. The previous measurable storm event must have been at least 72 hours I prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter j interval is representative for local storm events during the sampling period, and the permittee j I obtains approval from the local DWQ Regional Office. By this signature, I certify that this report is accurate and complete to the best of my knowledge: 1. Outfall Description: Outfall Nose_ Stru Receiving Stream: 1 Describe the industrial activities (pipe ditch, etc.) / fd;Z C.I-eclQ- ,ccur within the outfall drainage area: 2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint (light, medium, dark) as descriptors: 614a 3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil, weak chlorine odor, etc.): xvew e 4. Clarity: Choose the number which hest describes the clarity of the discharge, where 1 is clear and 5 is very cloudy: 2 3 4 5 5. Floating Solids: Choose the number which best describes the amount of floating solids in the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids: 1 Q 3 4 5 6. Suspended Solids: Choose the number which best describes the amount of suspended solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy: ® 2 3 4 5 7. Is there any foam in the stormwater discharge? Yes 6) 8. Is there an oil sheen in the stormwater discharge? Yes 19 9. Is there evidence of erosion or deposition at the outfall? Yes 10. Other Obvious Indicators of Stormwater Pollution: List and describe A4® G Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition may be indicative of pollutant exposure. These conditions warrant further investigation. Page 2 of 2 SWU-242, Last modified 10/25/2012