NCS000329_Monitoring Reports_20150723

FIL
MJ
OPT
eo q
O
r
�
C
1�!-ll
V
i.
oz
'-F'I
3
cz
kn
v-,
aj
O
u
s
it
O
O �
zo
0
0
b
o
o
F ri ri
�
o
O `.
�
i
I
42
r �
�I a
p
� O
V
Cej
O
oz

V R
ec q
a�
W
q is EA
PC
oOG�
qd.b�
.d z q
� o c
44
3C,od
c, a
co
Co
�a
ad
au
m w
o a, � q
a � tj
a .q os.
41
cc cd a
w
° C o
ed
° O
0 ,oq�n
� � o
y a Cd
4
0
a
�r
N
0
w
A

August 25, 2015
Attn: Central Files RECEIVED
N.C. Division of Water Quality AUG 2 8 2015
1617 Mail Service Center
Raleigh, NC 27699-1617 CENTRAL FILES
DWR SECTION
Central Files:
-4*ATI
P.O. Box 5030
2020 Ashcraft Avenue
Monroe, NC 28111-5030
Phone: [phone]
Fax: [phone]
Email: joe.hinkle(&atimetals.com
Attached, please find stonnwale> nionftoliug data foi Petwit No NCS000329. The originals and
one copy are included. The monitoring data is for the following monitoring schedule:
Monitoring Period
Sample Number
Start
End
Year 6 — Period 1
11
March 1, 2015
1 August 31, 2015
Analytical monitoring includes:
• Outfall #01 (B), commingled stormwater
• Outfall #02 (B), non -commingled stormwater
• Outfall #03 (B), non -commingled stormwater
• Non Contact Cooling Water #1 - #8
If you have any questions or need additional information, please contact me at 704-289-4511.
Thank you.
Sincerely,
Jo Hinkle
Environmental Manager

ATI
AT I - Bakers Plant
Stormwater Monitoring Report Form
Sample Date:
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analysis:
Sample Time: 4 r,56 PM
Stormwater Discharge Outfall #01 (Commingled)
Drainage Area = 2,915,470sq. ft. = 69 acres
% Impervious = 34%
�Q Via, Ae-1ge-
40 CFR Part 136
Parameter
Results (mg/l)
Benchmark Values (mg/1)
BOD
30
COD
120
TSS
100
Cadmium
0.001
Chromium, total recoverable
1
Copper, total recoverable
,5
0.007
Nickel, total recoverable
Dr 6 64
0.26
Zinc, total recoverable
e
0.067
Oil and Grease
20
Temp (effluent)
(deg C)
n/a
Temp (downstream)
(deg C)
JJ[ (deg C)
n/a
Temp (upstream)
n/a
Total Residual Chlorine
0.017
pH
o (std units)
6-9 (std units)
n ra
Storm Date: - Storm Duration: JV41
(Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.111: —ZO—L- (Hrs.)
Estimated Flow Calculation:
Q = CIA
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 69 acres x .66) + .9 x inches rain/12inches/ft. x 69 x .34)
C--(Total, cfs) = 1.5180 x (0,, 9 (Inches of rain) + 1.7595 x _-Ot 80 (Inches of rain)
cfs
FHC — CW — Mnnitnrino Rmnrt Fnrm — Rev 7

llvac ® Bakers Plant
Stormwater Monitoring Report Form
Sample Date: / 3
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis-
Sample Time: : M
Stormwater Discharge Outfall #02 (Non -Commingled)
Drainage Area = 212,952sq. ft. = 4.9 acres
% Impervious = 12%
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
30
COD
"P
120
TSS
100
Cadmium
D
0.001
Chromium, total recoverable
1
Copper, total recoverable
Q� !
`
0.007
Nickel, total recoverable
0.26
Zinc, total recoverable
pH
6% %
t
0.067
6-9 (std units)
(std[units)
8, '�
M /
Storm Date: Storm Duration: (Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.111: _ 0 q.. (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(hnpervious Area)
Q(tot., cfs) _ (A x inches rain/12 inches/ft. x 4.9 acres x .88) + .9 x inches rain/12inches/ft. x 4.9 x .12)
Q(Total, cfs) = 0.1437 x _ (Inches of rain) + 0.0441 x d® 8D (Inches of rain)
cfs
FHC — CW — Mnnitnrinv RPnnrt Fnr -Rau 7

Stormwater Monitoring Report Form
Sample Date: IS
Sample Location:
Person Collecting Samples:
Laboratory Performing Analysis:
Analytical Techniques and Methods:
Results of Sample Analvsis:
Sample Time: / ,A,3 1 jQ ra
Stormwater Discharge Outfall #03 (Non -Commingled)
Drainage Area = 336,580sq. ft. = 7.8 acres
% Impervious = 15%
�VJ PQe r
40 CFR Part 136
Parameter
Results (mg/1)
Benchmark Values (mg/1)
BOD
a
30
COD
0
120
TSS
100
Cadmium
0.001
Chromium, total recoverable
AM
1
Copper, total recoverable
6,1031
0.007
Nickel, total recoverable
j�
0.26
Zinc, total recoverable
D
0.067
pH
(std units)
6-9 (std units)
/rry-� St r
Storm Date: urm Duration: `� (Hrs.) Inches of Rainfall:
Duration of time preceding rain event exceeding 0.1": _--./()- (Hrs.)
Estimated Flow Calculation:
Q=CIA
Q(Total) = Q(Pervious Area) + Q(Irapervious Area)
Q(tot., cfs) _ (.4 x inches rain/12 inches/ft. x 7.8 acres x .85) + .9 x inches rain/12inches/ft. x 7.8 x .15)
Q(Total, cfs) = 0.2210 x 0o go _ (Inches of rain) + 0.0878 x .... .. 0,90 _ (Inches of rain)
010 / cfs
FUR — SW — Monitnrino R Pnnrt Form — Rev 1

Elmin
oo
w
N)
JA
-. F-
I-W
m
0

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://porta1mcdennorg/web/wq/ws/su/npdessw#tab-4
Permit No.: N/C/d&w/ D/,
Facility Name: 1�
County: _
Inspector:
Date of Inspection:.5,ff-/5
Time of Inspection: /3e,`A
or Certificate of Coverage No.:
Total Event Precipitation (inches): D. 75
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
..............................._...................................................................................................................................................................................................................I.............
By this signatuV, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permittee4 Designee
Pagel of 2
SWU-242, Last modified 10/25/2012

1. Outfall Description:
Outfall No. &/J0 /� � Structure (pipe,
Receiving Stream: �1. -y /'orK �t�<
Describe the industrial a/c HVes that occur
2. Color: Describe the color of the
(light, medium, dark) as descriptors: /
etc.)
the outfall drainage area:
using basic colors (red, brown, blue, etc.) and tint
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /Ie/I e-
4. Clarity: Choose the number which best describes the clarity of the discharge, where 1 is
clear and 5 is very cloudy:
1 2 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
1 2� 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2 e 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes `No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe AlolI e
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit. http://portaimcdennorg/web/wa /ws/su/nndessw#tab-4
Permit No.: or Certificate of Coverage No.:
Facility Name: / % 1� 4%/1czL
County: d A i Otl Phone No. %V2wyy- 60C.5,//
Inspector: 1191,piIn c4 4!,
Date of Inspection:
Time of Inspection:
Total Event Precipitation (inches):-6.7
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
/Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
..............................................................................
By this signapire, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of PerTirtee or
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfajj Description:
Outfall No. . a Structure (pi,e
Receiving Stream: K /
Describe the indu trial acti ities that occur
/ . —5 eo'er el i, l'vI it ,1{) /79r
etc.) ./ZiL
thq outfall drainage area:
2. Color: Describe the color of the discharge using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors: li / 62"')t-
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): /2F, ✓e
4. Clarity: Choose the number which best describes the clarity of tho discharge, where 1 is
clear and 5 is very cloudy:
1 0 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
01 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 0 3 4 5
7. Is there any foam in the stormwater discharge? Yes No
8. Is there an oil sheen in the stormwater discharge? Yes �No
9. Is there evidence of erosion or deposition at the outfall? Yes No
10. Other Obvious Indicators of Stormwater Pollution:
List and describe
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

LTIFAA
I AffljA
NCDENR
Stormwater Discharge Outfall (SDO)
Qualitative Monitoring Report
For guidance on filling out this form, please visit: httl2:/112ortal.ncdenr.org/web/wq,/ws/su./nl2dessw#tab-4
Permit No.: N/C/d/ )/—e
Facility Name: f1�
County: 1,41, ern
Inspector: Ge
Date of Inspection:
Time of Inspection:
6/3/2/1/ or Certificate of Coverage No.:
%t2
Total Event Precipitation (inches): 0e
Phone No.
Was this a "Representative Storm Event" or "Measureable Storm Event" as defined by the permit?
(See information below.)
/Yes ❑ No
Please verify whether Qualitative Monitoring must be performed during a "representative storm
event" or "measureable storm event" (requirements vary, depending on the permit).
Qualitative monitoring requirements vary. Most permits require qualitative monitoring to be
performed during a "representative storm event" or during a "measureable storm event." However,
some permits do not have this requirement. Please refer to these definitions, if applicable.
A "representative storm event" is a storm event that measures greater than 0.1 inches of rainfall
and that is preceded by at least 72 hours (3 days) in which no storm event measuring greater than
0.1 inches has occurred. A single storm event may contain up to 10 consecutive hours of no
precipitation.
A "measurable storm event" is a storm event that results in an actual discharge from the
permitted site outfall. The previous measurable storm event must have been at least 72 hours
prior. The 72-hour storm interval does not apply if the permittee is able to document that a shorter
interval is representative for local storm events during the sampling period, and the permittee
obtains approval from the local DWQ Regional Office.
....................................................................................................................-......................._......_......_..............................._........................................................................................................._............................................._......_.._...._.................
By this signature, I certify that this report is accurate and complete to the best of my knowledge:
(Signature of Permi*e or Designee)
Page 1 of 2
SWU-242, Last modified 10/25/2012

1. Outfall Descri]
Outfall No.
Receiving Stream: C"I
Describe the industrial
ditch, etc.)
G�
occur within the outfall drainage area:
2. Color: Describe the color of the dischar a using basic colors (red, brown, blue, etc.) and tint
(light, medium, dark) as descriptors:
3. Odor: Describe any distinct odors that the discharge may have (i.e., smells strongly of oil,
weak chlorine odor, etc.): Z20/�e
4. Clarity: Choose the number which best describes L110 clarity of Lhe discharge, where 1 is
clear and 5 is very cloudy:
1 20 3 4 5
5. Floating Solids: Choose the number which best describes the amount of floating solids in
the stormwater discharge, where 1 is no solids and 5 is the surface covered with floating solids:
(D 2 3 4 5
6. Suspended Solids: Choose the number which best describes the amount of suspended
solids in the stormwater discharge, where 1 is no solids and 5 is extremely muddy:
1 2� 3 4 5
7. Is there any foam in the stormwater discharge? Yes S
8. Is there an oil sheen in the stormwater discharge? Yes No
9. Is there evidence of erosion or deposition at the outfall? Yes nio
10. Other Obvious Indicators of Stormwater Pollution:
List and describes e-
Note: Low clarity, high solids, and/or the presence of foam, oil sheen, or erosion/deposition
may be indicative of pollutant exposure. These conditions warrant further investigation.
Page 2 of 2
SWU-242, Last modified 10/25/2012

aceAnalytical
www.pacelabs.com
July 31, 2015
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 20

/�atceAnalyficalo
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Fiorida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification #: 357
North Carolina Wastewater Certification #: 12
VrginiaNELAP Certification #: 460221
South Carolina Certification #: 99006001
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 20

aceAnalj&al
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92260320001
SW01
SM 5220D
MJP
1
PASI-A
92260320002
SW01
SM 5210B
BRJ
1
PASI-A
92260320003
SW01
SM 2540D
SAM
1
PASI-A
92260320004
SW01
EPA 200.7
JDA
5
PASI-A
92260320005
SW01
SM 4500-CI G
MLS
1
PASI-A
92260320006
SW01
EPA 16648
JMS
1
PASI-C,
q
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 20

§ /71aceAnalj4ical
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01 Lab ID: 92260320001 Collected: 07/23/15 18:50 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 50.0 mg/L 25.0 1 07/27/15 15:45
Date: 07/31/2015 02:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 20

aceAnalytical
% www.pacelab&com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Sample: SW01 Lab ID: 92260320002 Collected: 07/23/15 18:51 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day
BOD, 5 day
a
Date: 07/31/2015 02:22 PM
Analytical Method: SM 5210B
25.4 mg/L 2.0 1 07/25/15 04:41 07/29/15 23:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 20

acmnalytical
www.pacelab&com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01 Lab ID: 92260320003 Collected: 07/23/15 18:52 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2640D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 14.7 mg/L 8.3 1 07/29/15 11:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM Without the written consent of Pace Analytical Services, Inc..
Page 6 of 20

aceAnalytical
www.pacelabs.wm
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01
Lab ID: 92260320004
Collected: 07/23/15 18:53
Received: 07/24/15 12:00 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Cadmium
ND
ug/L
1.0
1
07/27/15 19:00
07/28/15 20:20
7440-43-9
Chromium
ND
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:20
7440-47-3
Copper
33.5
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:20
7440-50-8
Nickel
6.6
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:20
7440-02-0
Zinc
19.8
ug/L
10.0
1
07/27/15 19:00
07/28/15 20:20
7440-66-6
Date: 07/31/2015 02:22 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 20

Ar
�atceAnal�j�'ical
J`
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01 Lab ID: 92260320006 Collected: 07/23/15 18:54 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff
4500CL G Chlorine, Residual
Chlorine, Total Residual
Date: 07/31/2015 02:22 PM
Analytical Method: SM 4500-CI G
0.11 mg/L 0.024 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
07/27/1512:55 7782-50-5
Page 8 of 20

8
ceAnalj6cal
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW01 Lab ID: 92260320006 Collected: 07/23/15 18:56 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 07/30/15 10:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 20

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: GCSV/22117
Analysis Method:
EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description:
1664 HEM, Oil and Grease
Associated Lab Samples: 92260320006
METHOD BLANK: 1521896
Matrix: Water
Associated Lab Samples: 92260320006
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Oil and Grease
mg/L
ND 5,0 07/30/15 10-14
LABORATORY CONTROL SAMPLE:
1521897
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Oil and Grease
mg/L
40 35.6
89 78-114
MATRIX SPIKE SAMPLE:
1521898
92269903005 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
Oil and Grease
mg/L
ND 40
37.4 94 78-114
Results presented on this page are in the units Indicated by the "Units" column except where an afternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 20

acmnalytkal
w ww.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260320
QC Batch: MPRP/19100 Analysis Method: EPA200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92260320004
METHOD BLANK: 1518994
Matrix: Water
Associated Lab Samples: 92260320004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
07/28/1519:37
Cllrornlurn
u9/1-
ND
5.0
07/28/1610:37
Copper
ug/L
NU
5.0
01/28/1519:3/
Nickel
ug/L
ND
5.0
07/28/1519:37
Zinc
ug/L
ND
10.0
07/28/1519:37
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1518995
Spike
L CS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
451
90
85-115
Chromium
ug/L
500
467
93
85-115
Copper
ug/L
500
464
93
85-115
Nickel
ug/L
500
448
90
85-115
Zinc
ug/L
500
441
88
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1518996
1518997
MS
MSD
92260382008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Quai
Cadmium
ug/L
ND
500
500
448
449
90
90
70-130
0
Chromium
ug/L
ND
500
500
466
465
93
93
70-130
0
Copper
ug/L
ND
500
500
462
461
92
92
70-130
0
Nickel
ug/L
ND
500
500
444
444
89
89
70-130
0
Zinc
ug/L
2.9J
500
500
435
436
86
87
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1518998
1518999
MS
MSD
92260178001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
2.3
500
500
457
453
91
90
70-130
1
Chromium
ug/L
13.0
500
500
475
473
92
92
70-130
1
Copper
ug/L
824
500
500
1340
1440
102
122
70-130
7
Nickel
ug/L
14.8
500
500
453
450
88
87
70-130
1
Zinc
ug/L
608
500
500
1040
1060
86
89
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 20

aceAnalytical
www.pacelabs.com
Project: BAKERS STORMWATER
Pace Project No.: 92260320
QC Batch: WET/39159
QC Batch Method: SM 2540D
Associated Lab Samples: 92260320003
METHOD BLANK: 1520840
Associated Lab Samples: 92260320003
Parameter
Units
Total Suspended Solids
mg/L
LABORATORY CONTROL SAMPLE: 1520841
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1520842
Parameter
Units
Total Suspended Solids
mg/L
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 07/29/1511:24
Spike LCS
Cone. Result
250 248
92260085003 Dup
Result Result
177 200
SAMPLE DUPLICATE: 1520916
92260247001 Dup
Parameter Units Result Result
Total Suspended Solids mg/L 6.4 6.4
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
99 90-110
RPD Qualifiers
12 D6
RPD Qualifiers
0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 20

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260320
QC Batch: WET/39116 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92260320005
METHOD BLANK: 1519021
Associated Lab Samples: 92260320005
Parameter Units
Chlorine, Total Residual mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.024 07/27/15 '12:55
SAMPLE DUPLICATE: 1519022
92260064001 Dup
Parameter Units Result Result
Chlorine, Total Residual mg/L 0.034 0.040
RPD Qualifiers
16
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31 /2015 02:22 PM without the written consent of Pace Analytical Services, Inc..
Page 13 of 20

eAn l i al acyt c a
www.pacetabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260320
QC Batch: WET/39092 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210D DOD, 5 day
Associated Lab Samples: 92260320002
METHOD BLANK: 1518626
Associated Lab Samples: 92260320002
Parameter
Units
ROD, 5 day
mg/L
LABORATORY CONTROL SAMPLE: 1518627
Parameter
Units
BOD, 5 day
mg/L
SAMPLE DUPLICATE: 1518628
Parameter
Units
BOD, 5 day
mg/L
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/29/15 23:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 175 88 84.6-115.4
92260323002 Dup
Result Result RPD Qualifiers
20.4 19.9 2
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 14 of 20

acmnal ticai®
J
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260320
QC Batch: WETA/23876 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92260320001
METHOD BLANK: 1519000
Associated Lab Samples: 92260320001
Parameter Units
Chemical Oxygen Demand mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 25.0 07/27/1515:45
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1519001
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 746 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519002 1519003
MS MSD
92260042002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 250 1500 1500 578 578 22 22 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004 1519005
MS MSD
92260382006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 750 750 76.0 76.0 9 9 90-110 0 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc..
Page 15 of 20

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92260320
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kinrey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,241lpheny1hydrazine decomposes to and cannot be separated from Azobenzene using Method 8210. [lie result for each arralyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chioroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
A_1=�a77�1fti7al�.
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31 /2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 20

aceAnalytical o
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92260320
Analytical
Lab lD Sample ID QC Batch Method QC Batch Analytical Method Batch
92260320006
SW01
EPA 1664B
GCSV/22117
92260320004
SW01
EPA200.7
MPRP/19100 EPA200.7 ICP/17179
92260320003
SW01
SM 2540D
WET/39159
92260320005
SW01
SM 4500-CI G
WET/39116
92260320002
SW01
SM 5210B
WET/39092 SM 5210B WET/39095
92260310001
SWO1
SM 6220D
WETA123676
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/31/2015 02:22 PM without the written consent of Pace Analytical Services, Inc.. Page 17 of 20

�KCOAflalj*d'
Condition Upon Recel
Document Number:
F-CHR-CS-003-rev.16
Page 1 of 2*
Issuing Authority:
Pace Huntersville Qualitv Office
Client Name:. AFCi2e4e, I f
* Page 2 of 2 Is for Internal Use Only
Courier: Ej Fed Ex El UPSE] USPSO Clientn CommercialF1 ace Other
Custody Seal on Cooler/Box Present: El no Seals intact: ,[yes n no,
Packing Material: Ej Bubble VDp E] Bubble Bags ;?(Non- F-1 Other
Thermometer Used: IR Gun T1401 Type of Ice: Z Blue None 01Samples on ice, cooling process has begun
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp.: q C
Biological Tissue Is Frozen: Yes No
Date and initial of perspn fining
contents: '4 0331
Temp should be above freezing to 6*C
Comments:
Chain of Custody Present:
es E]No
EIN/A
I
Chain of Custody Filled Out:
Pes DNo
ON/A
2.
Chain of Custody Relinquished:
KYes DNo
ON/A
3.
Sampler Name & Signature on COC;
JVYes []No
ON/A
4,
Samples Arrived within Hold Time:
9-1yes DNo
ON/A
5.
Short Hold Time Analysis (<72hr):
es DNo
ON/A
6.
Rush Turn Around Time Requested:
DYes )ErNo
ON/A
7.
Sufficient Volume:
es DNo
DNIA
3.
Correct Containers Used:
es DNo
DNIA
9.
-Pace Containers Used:
es DNo
DN/A
Containers Intact:
Res DNo
ON/A
10.
Filtered volume received for Dissolved tests
es DNo
ON/A
11.
Sample Labels match COC:
e� Yes ONo
ON/A
12.
-includes date/time/ID/Analysis Matrix:
to
All containers needing preservation have been checked.
- JKYAs ONo
EIN/A
13.
All containers needing preservation are found to be In
XY/es ONo
ON/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, W-DRO (water)
OYesZNo
Samples checked for dechlorination:
DYes DNo
�IA
14.
Headspace in VOA Vials (>6mrn):
DYes ONo
&A
15,
Trip Blank Present:
DYes DNo
ON/A
16.
Trip Blank Custody Seals Present
DYes E]No
N/A
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date rime:
Comments/ Resolution:
SCURF Review: —Date: WN:92260"320
SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification<Office ( i.e out of hold, Incorrect preservative, out of temp, 92260320
incorrect containers)
Page 18 of 20

j3
8
1-4
10)
Jul
to
ITEM
�-
(:�.Y
31
P
Na.
I w V;
a m
Zp
C-
�-A
co
w - a
0
.0
;;
9x
X-1.
T.
.0
- .0
P1 ;
to
>
C . 'U
W
>!
0
M
0
C
In
z
In
to
--f 1>.g 0 V
1
1
'U
'U
'a
0
0
X
X m3
(D
ct
0
z
z
r
0 5
0 CL
X
MATRIX CODE (see va!id codes to left)
z
p
6
SAMPLE TYPE (G=GRAB C=COMP)
m
0
'n
"n
'U
0
0
r
1\
m
r-
17,
"t
A
�2 X
o ;a z
z>
0
z
m
0
-q
z m
C w
V
0
m
:0 3 >
M 0
. .
a
0 0 W
Z
m
r r-
ij
In
SAMPLE TEMP AT COLLECTION
m C
m
8
>
0
(mo
o.
# OF CONTAINERS
In
5
Unpreserved
H-7SOA
6 0
p-e
HNO3
z1a,
X1:
t
HCI
�x
NaOH
I
Na2S2O3
m
Methanol
I
o
Other
Analysis Test
YINI
U
Ix
GOD
I
6 m
19
to
m
,
z
;-
ZN
&
C
>
m
><
r
D
C z a
Cb -0
0
m
X
CL
m—
—
—
X G) m
0 0;0 Z
z
>1
m
0 a
-4 X
m —Z
in
;U
z
G)
*1
>
—
—
—
00
W
0')
Temp in 'C
W
>
r
m
0
0
z
0
z
I
Residual Chlorine (YIN)
z
0
Received on
Ice (Y/N)
Custody
Sealed Cooler
(Y/N)
Samples Intact
m
(YIN)
X
e 19 of 20

;3--8-4004
0
ITEM #
.0
0
M
3
7�
0
CL
>
>
r
'U
z
o>
r
M
0r
M
c
—n
w
0
9
3
M
z
C
M
0 51i .0
Fr .
E
512 >1
x
0>
�1VPcn-u M
;U
0
A
0
C
a
0
-01
M
z
z
0
MATRIX CODE (see va!id codes to feft)
z
ID
co
0
4'�
SAMPLE TYPE (G=GRAB C=COMP)
M
0
0
M
01
m
0
to A ;U
E) z
z z >
-4
0
z
111
M
0
--I
M
?
�; z M
3 >
M
m
X
m
0 0
0
> > G)
>
>
mZ
r
rtt
SAMPLE TEMP AT COLLECTION
rn rn a
I
M
N OF CONTAINERS
>
A30 :1
Unpreserved
M
1-12SO,
N,
HNO3
X
HCI
NaOH
Na2S203
rn
Methanol
Other
Analysis Test j
YINI
>
r
CD
Cx
0
z
Q
CL
Ali. ZN
>
M
oil
Ln.
r
C z Cr
"o
0
'0
m
0
M
0
CL
ATr
M
M
0C 0
Temp in 'C
z <
0
A
m
;o
Residual Chlorine (Y/N)
Received on
Ice (YIN)
>
r
M
0 0
z
C�
'
0
w r
z
Custody
Sealed Cooler
(YIN)
z
0 if
m
;D
z
z
Samples Intact
M
(YIN)
LLLLLLLLLLLLLL
;0
20 of 20

aceAnalj cal
wwwpacelaimcom
July 30, 2015
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92260323
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
p,�,,t,,N �h,- ..
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 16

Pace Analytical Services, Inc.
aceAnalyticalg 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com
[phone]
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92260323
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification #: 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 16

aceAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
BAKERS STORMWATER
92260323
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92260323001
SW02
SM 5220D
MJP
1
PASI-A
92260323002
SW02
SM 5210B
BRJ
1
PASI-A
92260323003
SW02
SM 2540D
SAM
1
PASI-A
92260323004
SW02
EPA 200.7
JDA
5
PASI-A
t
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 16

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260323
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW02 Lab ID: 92260323001 Collected: 07/23/15 19:12 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand 57.0 mg/L 25.0 1 07/27/15 15:45
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 16

(�;aneAnalyticalo
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260323
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW02 Lab ID: 92260323002 Collected: 07/23/15 19:13 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day
BOD, 5 day
I
Date: 07/30/2015 02:30 PM
Analytical Method: SM 5210B
20.4 mg/L 2.0 1 07/25/15 04:41 07/29/15 23:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 16

acmnalytical
www.pacelabs.=
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260323
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW02 Lab ID: 92260323003 Collected: 07/23/15 19:14 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 82.0 mg/L 10.0 1 07/29/15 11:30
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 16

aceAnalytical
www.pacafabs.com
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92260323
Sample: SW02 Lab ID: 92260323004 Collected: 07/23/15 19:16 Received: 07/24/15 12:00 Matrix: Water
Parameters
200.7 MET ICP
Cadmium
Chromium
Cupper
Nickel
Zinc
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
ND
ug/L
1.0
1
07/27/15 19:00 07/28/15 20:23
7440-43-9
16.2
ug/L
5.0
1
07/27/15 19:00 07/28/15 20:23
7440-47-3
496
ug/L
5.0
1
07/27/15 19.00 07/28/15 20:23
7440-50-8
10
ug/L
5.0
1
07/27/15 19:00 07/28/15 20:23
7440-02-0
74.7
ug/L
10.0
1
07/27/15 19:00 07/28/15 20:23
7440-60-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 7 of 16

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260323
QC Batch: MPRP/19100
QC Batch Method: EPA 200.7
Associated Lab Samples: 92260323004
Analysis Method:
Analysis Description:
EPA 200.7
200.7 MET
METHOD BLANK: 1518994
Matrix: Water
Associated Lab Samples: 92260323004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Cadmium
ug/L
ND
1.0
07/28/1519:37
Chromium
ug/L
ND
5.0
07/28/1519:37
Copper
ug/L
ND
5.0
07/28/1519:37
Nickel
ug/L
ND
5.0
07/28/1519:37
Zinc
ug/L
ND
10.0
07/28/1519:37
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1518995
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Cadmium
ug/L
500
451
90
85-115
Chromium
ug/L
500
467
93
85-115
Copper
ug/L
500
464
93
85-115
Nickel
ug/L
500
448
90
85-115
Zinc
ug/L
500
441
88
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1518996
1518997
MS
MSD
92260382008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Cadmium
ug/L
ND
500
500
448
449
90
90
70-130
0
Chromium
ug/L
ND
500
500
466
465
93
93
70-130
0
Copper
ug/L
ND
500
500
462
461
92
92
70-130
0
Nickel
tip/L
ND
500
500
444
444
89
89
70-130
0
Zinc
ug/L
2.9J
500
500
435
436
86
87
70-130
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
'15,18998
15,18999
MS
MSD
92260178001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium
ug/L
2.3
500
500
457
453
91
90
70-130
1
Chromium
ug/L
13.0
500
500
475
473
92
92
70-130
1
Copper
ug/L
824
500
500
1340
1440
102
122
70-130
7
Nickel
ug/L
14.8
500
500
453
450
88
87
70-130
1
Zinc
ug/L
608
500
500
1040
1060
86
89
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 8 of 16

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: BAKERS STORMWATER
Pace Project No.: 92260323
QC Batch: WET/39159
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92260323003
METHOD BLANK: 1520840
Matrix: Water
Associated Lab Samples: 92260323003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 07/29/15 11:24
LABORATORY CONTROL SAMPLE: 1520841
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 248
99 90-110
SAMPLE DUPLICATE: 1520842
92260085003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
177
200 12 D6
SAMPLE DUPLICATE: 1520916
92260247001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
6.4
6.4 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 16

aceAnalytical
www.pacelabs.com
Project: BAKERS STORMWATER
Pace Project No.: 92260323
QC Batch: WET/39092
QC Batch Method: SM 5210B
Associated Lab Samples: 92260323002
METHOD BLANK: 1518626
Associated Lab Samples: 92260323002
Parameter Units
BOG, 5 day mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5210B
Analysis Description: 5210B BOD, 5 day
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/29/15 23:39
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1518627
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 175 88 84.6-115.4
SAMPLE DUPLICATE: 1518628
92260323002 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L 20.4 19.9 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 16

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260323
QC Batch: WETA/23876 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92260323001
METHOD BLANK: 1519000 Matrix: Water
Associated Lab Samples: 92260323001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand rng/L ND 25.0 07/27/15 15:45
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersv[ile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1519001
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 746 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519002 1519003
MS MSD
92260042002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Chemical Oxygen Demand mg/L 250 1500 1500 578 578 22 22 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004 1519005
MS MSD
92260382006 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L ND 750 750 76.0 76.0 9 9 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 16

Qo
aceAnalytical
ffmpacelabs.com
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92260323
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chioroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 16

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project:
BAKERS STORMWATER
Pace Project No.:
92260323
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92260323004
SW02
EPA 200.7
MPRP/19100 EPA 200.7
ICP/17179
92260323003
SW02
SM 2540D
WET/39159
92260323002
SW02
SM 5210B
WET/39092 SM 5210B
WET/39095
92260323001
SW02
SM 5220D
WETA/23876
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 16

Document Name: Document Revised: May 18, 2015
aceAn,1lytical* Sample Condition Upon Receipt (SCUR) Page 1 of 2"
Document Number: Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersville Qualitv Office
/A 1
Client Name: ,T S QfrL(i 0t f E9 *Page 2 of 2 is for Internal Use Only
Temp Correction Factor T1401 No Correction
Corrected Cooler Temp.: .0
Biological Tissue is Frozen: Yes Nov
Date and Initialsoe a intng
contents:
Temp should be above freezing to 6*C
Comments:
Chbih'of CUStUd Present:
'r''es ONo
ONIA
1.
Chain of Custody Filled Out:
firyes []No
ON/A
2.
Chain of Custody Relinquishod:
l?<YQ9 []No
ONIA
3
Sampler Name & Signature on COC:
Yes. ONo
❑NIA
4.
Samples Arrived within Hold Time:
Yes ❑ o
ONIA
5.
Short Hold Time Analysis (<72hr):
e o
ON/A
6.
Rush Turn Around Time Requested:
Dyes ONo
ON/A
7.
Sufficient Volume:
PKe. ❑No
ONIA
8.
Correct Containers Used:
p e's _0No
❑NIA
9.
-Pace Containers Used:
®Yes ONo
❑NIA
Containers Intact:
es ONo
❑N/A
10.
Filtered volume received for Dissolved tests
es ONo
❑NIA
11.
Sample Labels match COC:
Imes ONo
ON/A
12.
-Includes date/time/ID/Analysis Matrix:
ti()
All containers needing preservation have been checked.JI/
Yes ONo
ON/A
13.
All containers needing preservation are found to be in
[JYes ONo
ON/A
compliance with EPA recommendation.
exceptions: VOA, coli(orm, TOC, O&G, W-DRO (water)
❑Yes o
Samples checked for dechlorination:
❑O Yes No
NIA
14.
Headspace in VOA Vials(>6mm):
❑Yes ONo
r6NIA
15.
Trip Blank Present:
❑Yes ONo
N/A
16.
Trip Blank Custody Seals Present
❑Yes ONo
NA
Pace -Trip Blank LQ0 .(if umhased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date:
SRF Review: Date: 2
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
WO#:92260323
llunlmvillfi
Page 14 of 16

D
3
m
to z
a z+
d m
m
0
N
Div 3 z
z A
m
y Temp in °C
b
ro Received on
0 Ice (YIN)
0
Custody
cn Sealed Cooler
(Y/N)
0
O
Samples Intact
(Y/N)
J I m
� m
C? o
-.
ITEM #
o
3
v
n '
oDv
0
� tJ
CO o �
0_ m
m�
C
z
C
m
dd
d
- 05
t� d
0o
a
N
MATRIX CODE (see va'id codes to left)
i�
SAMPLE TYPE (G=GRAB C=COMP)
mD
A 1p
4 1p
-4
m
0
9
m
O
r
rn
m
0
z0
0
m
v
�
.1�
,T,
m m
SAMPLE TEMP AT COLLECTION
r.
# OF CONTAINERS
HNO3
m
HCI 2
NaOH
Na2S203 y
Methanol
Other
IAnalvsis Test lyl
Residual Chlorine
m
0.
z
O
d \�
G
c
z
H
1 • •
m
.-t
��,,,
Q
o m
-0 o `�
O
a
\a
n D
O
C,
-0 c
3
0
o
m
oto
c
z
o
C.
A
q
y�
d O
� a
3 W
0
R
M.
f
n
o
d D
a Z
0
m e
<' m
m
0g
Qa
r
o
d
C
0
3 �
z n
�
1 �
m
w n
m
Q X
3 M
c ,Q
W
1
a
c
CD
t3
G
a
y
.�
..
m
A
0
N
r
C
z
C
n
Ami
o
T
..
m
_
m
A
z
0
O
0
m
z
{
m
0
m
0
0,')
O
al
A
m
z
C. i
A
5E
I-_- l
X
15 of 16

%
;t
w
-4
0)
to
A
ITEIVI#
;0
M
91
F.
C0
a
lk�
R 00
CL
>
0 0
N
5�
T
0
z
>
r
m m
-n
00
Z
?i
m
C
m
z
On
0 -,1
-0
U
a
00
8
go
> 0 to
a
m
a
0
m
C
30
z
z
of
A
r
MATRIX CODE (see vald codes to left)
z
D
r
9AMPLETYPF (G=GRAB C=COMP)
Vi
x
m
m
-21
0
>
r
m
0
m
z
0
z
m
z
z
-1
>
g
.z 8
m
0
z
.
m
>
1
0
m
G)
>
z
m
r
Vi
re
SAMPLE TEMP AT COLLECTION
m
J-1 n
# OF CONTAINERS
v g
old —t.90
&
m
m 0
Qw
8 6
t
Unpreserved
X.-
H,SO,
HNO3
0
0
J
HCI
CD
>
NaOH
Na2S203
CD
j
j
Methanol
In
Other
Analysis Test j
Y/ N
�Nd
>
19,0D
o m
F
11
Ix
A oD.
CL
m
0
C z a
U) 'D
In
0
m 0
m
C <
z
0
T
Temp inC
>
Residual Chlorine (Y/N)
>
m
0�0
(1110
Received on
Ice (Y/N)
r
m
0
(D
-0
r,
Custody
Sealed Cooler
0
z
z
C-)
(YIN)
2
0
0
m
;D
z
6)
z
CA
L.-
r
Samples Intact
m
;o
i I p
0
o 3:
00
In
0
0
0 IC)
0
m >
z
.-q M
>
0
X
M
M•
r
ty
M
0
13
CD 0
CL o
@
le 16 of 16

aceAnalytical
wwwpacelabs.com
I
July 30, 2015
Mr. Joe Hinkle
Allvac
RE: Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite too
Huntersville, NC 28078
[phone]
Dear Mr. Hinkle:
Enclosed are the analytical results for sample(s) received by the laboratory on July 24, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless other se footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Allvac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 15

Pace Analytical Services, Inc.
aceAnalyticai® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
CERTIFICATIONS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification M 40
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
Massachusetts Certification M M-NC030 West Virginia Certification M 356
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 15

acmnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92260317001
SW03
SM 5220D
MJP
1
PASI-A
92260317002
SW03
SM 5210B
BRJ
1
PASI-A
92260317003
SW03
SM 2540D
SAM
1
PASI-A
92260317004
SW03
EPA200.7
JDA
5
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 15

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW03 Lab ID: 92260317001 Collected: 07/23/15 07:31 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
5220D COD Analytical Method: SM 5220D
Chemical Oxygen Demand ND mg/L 25.0 1 07/27/15 15:45
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 15

1aneAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW03 Lab ID: 92260317002 Collected: 07/23/15 07:32 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210E BOD, 5 day Analytical Method: SM 5210B
BOD, 5 day 4.9 mg/L 2.0 1 07/25/15 04:41 07/29/15 23:39
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 15

aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SW03 Lab ID: 92260317003 Collected: 07/23/15 07:33 Received: 07/24/15 12:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids 14.0 mg/L 3.6 1 07/29/15 11:30
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 15

Pace Analytical Services, Inc.
aceAnalytrcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Sample: SW03 Lab ID: 92260317004 Collected: 07/23/15 07:35 Received: 07/24/15 12:00 Matrix: Water
Parameters
200.7 MET ICP
Cadmium
Chromium
Copper
Nickel
Zinc
Date: 07/30/2015 02:30 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Analytical Method: EPA 200.7
Preparation Method: EPA 200.7
ND
ug/L
1.0
1
07/27/15 19:00
07/28/15 20:16
7440-43-9
ND
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:16
7440-47-3
31.0
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:16
7440-50-8
ND
ug/L
5.0
1
07/27/15 19:00
07/28/15 20:16
7440-02-0
23.3
ug/L
10.0
1
07/27/16 19:00
07/28/16 20:16
7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 15

acmnalytical o
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: MPRP/19100
QC Batch Method: EPA 200.7
Associated Lab Samples: 92260317004
Analysis Method:
Analysis Description:
EPA 200.7
200.7 MET
METHOD BLANK: 1518994
Matrix: Water
Associated Lab Samples: 92260317004
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Cadmium
ug/L
ND
1.0 07/28/1519:37
Clllornlurn
ug/L
NU
5.0 01/28/'I5 '19:31
Copper
ug/L
ND
5.0 07/28/1519:37
Nickel
ug/L
ND
5.0 07/28/1519:37
Zinc
ug/L
ND
10.0 07/28/1519:37
LABORATORY CONTROL SAMPLE: 1518995
Spike LCS
LCS %
Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Cadmium
ug/L
500 451
90
85-115
Chromium
ug/L
500 467
93
85-115
Copper
ug/L
500 464
93
85-115
Nickel
ug/L
500 448
90
85-115
Zinc
ug/L
500 441
88
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1518996
MS
92260382008
Spike
Parameter
Units
Result
Conc.
Cadmium
ug/L
ND
500
Chromium
ug/L
ND
500
Copper
ug/L
ND
500
Nickel
ug/L
ND
500
Zinc
ug/L
2.9J
500
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1518998
MS
92260178001
Spike
Parameter
Units
Result
Conc.
Cadmium
ug/L
2.3
500
Chromium
ug/L
13.0
500
Copper
ug/L
824
500
Nickel
ug/L
14.8
500
Zinc
ug/L
608
500
1518997
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
448
449
90
90
70-130
0
500
466
465
93
93
70-130
0
500
462
461
92
92
70-130
0
500
444
444
89
89
70-130
0
500
435
436
86
87
70-130
0
1518999
MSD
Spike
MS
MSD
MS
MSD
% Rec
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
500
457
453
91
90
70-130
1
500
475
473
92
92
70-130
1
500
1340
1440
102
122
70-130
7
500
453
450
88
87
70-130
1
500
1040
1060
86
89
70-130
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc..
Qual
Qual
Page 8 of 15

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260317
QC Batch: WET/39159 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92260317003
METHOD BLANK: 1520840
Associated Lab Samples: 92260317003
Parameter Units
Total Susponded Sulidc rng/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.6 07/20/16 11:24
LABORATORY CONTROL SAMPLE:
1520841
Spike
LCS
Parameter
Units
Conc.
Result
Total Suspended Solids
mg/L
250
248
SAMPLE DUPLICATE: 1520842
92260085003
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
177
200
SAMPLE DUPLICATE: 1520916
92260247001
Dup
Parameter
Units
Result
Result
Total Suspended Solids
mg/L
6.4
6.4
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LCS % Rec
% Rec Limits Qualifiers
99 90-110
RPD Qualifiers
12 D6
RPD Qualifiers
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 9 of 15

aceAnalXical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260317
QC Batch: WET/39092 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92260317002
METHOD BLANK: 1518626
Associated Lab Samples: 92260317002
Parameter Units
SOD, 6 day mg/L
LABORATORY CONTROL SAMPLE: 1518627
Parameter Units
BOD, 5 day mg/L
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/29/15 23:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
198 175 88 84.6-115.4
SAMPLE DUPLICATE: 1518628
92260323002 Dup
Parameter Units Result Result
BOD, 5 day mg/L 20.4 19.9
RPD Qualifiers
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 15

acmnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: WETA/23876
Analysis Method: SM 5220D
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92260317001
METHOD BLANK: 1519000
Matrix: Water
Associated Lab Samples: 92260317001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
ND 25.0
07/27/15 15:45
LABORATORY CONTROL SAMPLE: 1519001
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
750
746
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519002
1519003
MS
MSD
92260042002
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 250
1500
1500 578
578 22 22
90-110
0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1519004
1519005
MS
MSD
92260382006
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L ND
750
750 76.0
76.0 9 9
90-110
0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 15

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: BAKERS STORMWATER
Pace Project No.: 92260317
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation l Imit
RL - Reporting Limit.
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Ulpheny1hydrazlne decomposes to and cannot be separated from Azobenzene using Method 8210. 1 he result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/30/2015 02:30 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 15

,�aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BAKERS STORMWATER
Pace Project No.: 92260317
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92260317004
SW03
EPA 200.7
MPRP/19100 EPA 200.7
ICP/17179
92260317003
SW03
SM 2540D
WET/39159
92260317002
SW03
SM 5210B
WET/39092 SM 5210B
WET/39095
92260317001
SW03
SM 5220D
WETA/23876
Date: 07/30/2015 02:30 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 15

° . -� aceAn��lytical"
Client Name:
.5 rw r
Document Name:
Condition Upon Receil
Document Number:
F-CHR-CS-003-rev.16
Temp Correction Factor T1401 No Correction
Document Revised: May 18, 2015
Page 1 of 2*
issuing Autnority:
Pace Huntersville Qualitv Office
* Page 2 of 2 is for Internal Use Only
It . ./ Biological Tissue is Frozen: Yes No /
Corrected Cooler Temp.: 7 'C g 6
Date and Initials f p rsgn e fining
contents: y "
Temp should be above freezing to 6*C Comments:
Chain of Custod Present: j2fos ONv ON/A
1.
Chain of Custody Filled Out: k&s ONO ❑N/A
2.
Chain of Custod}+ Rellnqulshed: esI ONO ❑N/A
3.
Sampler Name & Signature on COC: �res ONO ❑N/A
4.
Samples Arrived within Hold Time: es [qNo ❑N/A
5.
Short Hold Time Analysis <72hr : Yes ❑N/A
6.
Rush Turn Around Time Requested: Dyes ,,2/❑N/A
7,
Sufficient Volume: es ONO ❑N/A
8.
Correct Containers Used: Q*es ONO ❑N/A
9.
-Pace Containers Used: Res ONO ❑N/A
Containers Intact: Z'Yes ONO ❑N/A
10.
Filtered volume received for Dissolved tests es ❑No ❑N/A
11.
Sample Labels match COC; es ONO ❑N/A
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been checked.
l�les ONO ❑N/A
13.
All containers needing preservation are found to be in Yes ❑No ❑N/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, W-DRO (water) Dyes Juno
Sam lo4 chookod for dochlorination: ❑Yea ONO /A
14.
Headspace in VOA Vials (>6mm): ❑Yes ONO G3 A
15.
Trip Blank Prosent: ❑Y®a ONO N/
16.
,
Trip Blank Custody Seals Present ❑Yes ❑No 1'JN/A
__L_rig
Pace T Blank Lot # if urchased
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted:
Comments/ Resolution:
DatefTime:
SCURF Review: Date: I
Iffi: SRF Review: Date: C 2
Note: Whenever there is a discrepancy affecting North Carolina compliance
-- samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
Incorrect containers)
- WO# : 922603ll
1111111111111111111111
to nu I............-.^--�
Page 14 of 15

ro
'o
to
w
w
ITEM #
CA
IlS.
O
�{y 6
u
kN
(C
V 9
m
O
..
D
1
3
�
a•
`
O
3
4
o
z
C o
D
N
>
m M
u
c•
0
p
= v
2
m
z
m
G.
rC
Cn,N�o�nv��o
f�
O
d
N 1A.i Cn
M
O
'O
'0
OO
C
O
G..
>b
$ }5�$
� In ;o '3 � r- � 2 �
W
�.
:C
d
`9C
-Qggi
G w
O
r'
c
w
a
w
MATRIX CODE (see valid codes to tell)
m
-��°-
�
n
n
l
SAMPLE TYPE (G=GRAB C=COMP)
Z
C
z
P
�,
Lt
o
o
M
^,o.
-
3
m
v
m
T
N
7
'c
i
m
n
O
m
A z
>
=
n
V
D 1 g
C z m
W
D
m°
° Q 3
M
(]
r
m 23 Z
m
N
> pC,
W
J
9 T>
'
RI
%
SAMPLE TEMP AT COLLECTION
m m A
m
a ; (on
..
# OF CONTAINERS
°
e
o
a
o
�
Unpreserved
m
a
#
m
H;
3
n
i
H2SO4
6
v
h
HNO3
1 o
HCI
m
n
NaOH
t7'
Na2S203Ou
y
i
Cj
m
Methanol
✓(
a
Other
3
CS
aAnalysis Testa
YIN a
cop;
v
m
0
O D
o m
5
r
(�
y
a
i...
0
v
4
N
,
V/
N
�C
NNit
�p
I�-
'S
m
m
6
m
rn
0
o.
1 ...)
>
..
m
-c
Z
Z
so
:?
t�
$ O
z
z
n�
Tamp in°C
Residual Chlorine (YIN)
v
M
M
X
-�
00
Received on
Ice (YIN)
D
:
G
y
C (
O ow
°
Custody
Sealed Cooler
ei
o
a
�•
_
"_.
`
M"�
'a A
Z
(YIN)
vz
co
w
O r
m
t7
Samples Intact
co
(YIN)
x
F
ge 15 of 15

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 07, 2015
Mr. Joe Hinkle
Alivac
RE: Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Dear Mr. Hinkle:
Fnclosed are the analytical results for sample(s) received by the laboratory on August 04, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
Project Manager
Enclosures
cc: Mr. Preston Baucom, Alivac
Mr. Tommy Long, Allvac
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
CERTIFICATIONS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
West Virginia Certification M 357
North Carolina Wastewater Certification #: 12
VirginiaNELAP Certification * 460221
South Carolina Certification #: 99006001
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804 North Carolina Wastewater Certification #: 40
Florida/NELAP Certification #. E87848 South Carolina Certification #: 99030001
Massachusetts Certification #: M-NC030 West Virginia Certification M 356
North Carolina Drinking Water Certification #: 37712 VrginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92261784001
BAKERS NONCONTACT #1
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92261784002
BAKERS NONCONTACT #2
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92261784003
BAKERS NONCONTACT #3
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92961184004
BAKERS NONCON IAC I #4
EPA 1604B
JMS
I
PASI-;
SM 4500-CI G
MLS
1
PASI-A
92261784005
BAKERS NONCONTACT #5
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92261784006
BAKERS NONCONTACT #6
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92261784007
BAKERS NONCONTACT #7
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
92261784008
BAKERS NONCONTACT #8
EPA 1664B
JMS
1
PASI-C
SM 4500-CI G
MLS
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #1 Lab ID: 92261784001 Collected: 08/03/15 08:50 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/07/15 08:47
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.12 mg/L 0.024 1 08/05/15 10:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 4 of 18

aceAnalyticai®
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #2 Lab ID: 92261784002 Collected: 08/03/15 09:15 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/07/15 08:48
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.17 mg/L 0.024 1 08/05/1510:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 5 of 18

aceAnaIXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #3 Lab ID: 92261784003 Collected: 08/03/15 09:35 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/07/15 08:48
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.41 mg/L 0.12 5 08/05/15 10:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 6 of 18

QD
aceAna1j cal
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #4 Lab ID: 92261784004 Collected: 08/03/15 10:00 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/07/15 08:49
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.12 mg/L 0.024 1 08/05/15 10:35 7782-50-5
Date: 08/07/2015 03:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #5 Lab ID: 92261784005 Collected: 08/03/15 10:20 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/07/15 08:49
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.18 mg/L 0.024 1 08/05/1510:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 8 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #6 Lab ID: 92261784006 Collected: 08/03/15 10:45 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/07/15 08:50
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.070 mg/L 0.024 1 08/05/15 10:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #7 Lab ID: 92261784007 Collected: 08/03/15 11:10 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664E
Oil and Grease ND mg/L 5.0 1 08/07/15 08:50
4600CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 0.093 mg/L 0.024 1 08/05/15 10:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 10 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Sample: BAKERS NONCONTACT #8 Lab ID: 92261784008 Collected: 08/03/15 11:35 Received: 08/04/15 15:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 08/07/15 08:51
4500CL G Chlorine, Residual Analytical Method: SM 4500-CI G
Chlorine, Total Residual 1.3 mg/L 0.24 10 08/05/15 10:35 7782-50-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 11 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
QC Batch: GCSV/22191
Analysis Method: EPA 1664B
QC Batch Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007,
92261784008
METHOD BLANK: 1528455
Matrix: Water
Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007,
92261784008
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Coil and Groaso mg/1 _
ND 6 0 08/07/16 08-46
LABORATORY CONTROL SAMPLE: 1528456
Spike LCS LCS % Rec
Parameter Units
Cone. Result % Rec Limits Qualifiers
Oil and Grease mg/L
40 35.1 88 78-114
MATRIX SPIKE SAMPLE: 1528457
92261950002 Spike MS MS % Rec
Parameter Units
Result Cone. Result % Rec Limits Qualifiers
Oil and Grease mg/L
ND 40 37.4 94 78-114
Results presented on this page are in the
units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM
without the written consent of Pace Analytical Services, Inc.. Page 12 of 18

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
QC Batch: WET/39292 Analysis Method: SM 4500-CI G
QC Batch Method: SM 4500-CI G Analysis Description: 4500CL G Chlorine, Total Residual
Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007,
92261784008
METHOD BLANK: 1526178 Matrix: Water
Associated Lab Samples: 92261784001, 92261784002, 92261784003, 92261784004, 92261784005, 92261784006, 92261784007,
92261784008
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chlorine, Total Residual mg/1 ND 0 024 08/05115 10,35
SAMPLE DUPLICATE: 1526179
92261784001 Dup
Parameter Units Result Result RPD Qualifiers
Chlorine, Total Residual mg/L 0.12 0.12 5
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
e
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 18

aceAnalj6cal
www.pacelab.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Repurtirig Llrntt.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
IA_1:101XN e771 9
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc..
Page 14 of 18

aceAnalytical
www.pacelab&com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BAKERS NON CONTACT COOLING
Pace Project No.: 92261784
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92261784001
BAKERS NONCONTACT #1
EPA 1664B
GCSV/22191
92261784002
BAKERS NONCONTACT #2
EPA 1664B
GCSV/22191
92261784003
BAKERS NONCONTACT #3
EPA 1664B
GCSV/22191
92261784004
BAKERS NONCONTACT #4
EPA 1664B
GCSV/22191
92261784006
BAKERS NONCONTACT #5
EPA 1664E
GCSV/22191
92261784006
BAKERS NONCONTACT #6
EPA 1664B
GCSV/22191
92261784007
BAKERS NONCONTACT #7
EPA 1664B
GCSV/22191
92261784008
BAKERS NONCONTACT #8
FPA 1664B
GCSV/22191
92261784001
BAKERS NONCONTACT #1
SM 4500-0I G;
WFT/39292
92261784002
BAKERS NONCONTACT #2
SM 4500-CI G
WET/39292
92261784003
BAKERS NONCONTACT #3
SM 4500-CI G
WET/39292
92261784004
BAKERS NONCONTACT #4
SM 4500-CI G
WET/39292
92261784005
BAKERS NONCONTACT #5
SM 4500-CI G
WET/39292
92261784006
BAKERS NONCONTACT #6
SM 4500-CI G
WET/39292
92261784007
BAKERS NONCONTACT #7
SM 4500-CI G
WET/39292
92261784008
BAKERS NONCONTACT #8
SM 4500-CI G
WET/39292
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/07/2015 03:02 PM without the written consent of Pace Analytical Services, Inc.. Page 15 of 18

IJOCument Name: Document Revisea: May Its, Gu 10
<�ceAlt<�lytical` Sample Condition Upon Receipt (SCUR) Page 1 of 2*
Document Number: Issuing Authority:
F-CHR-CS-003-rev.16 Pace Huntersville Qualitv Office
Temp Correction Factor T1401 No Oorrection
Corrected Cooler Temp.: 'C
Temp should be above freezing to 6°C
Biological Tissue is Frozen: Yes No N/A
5
Comments:
Date and Initials of person ex inin
contents: /.i � k ,. -_t
Chain of Custod Present:
0 es Nb
ON/A
1.
2.
Chain of Custody Filled Out: es 6' ON/A
Chain of Custody Relinquished:
, es ❑ cr ❑NIA
3.
4.
Sampler Name & Signature on COC: ❑ s t4ro ❑N/A
Samples Arrived within Hold Time:
❑ es ONo
N/A
5.
Short Hold Time Analysis (<72hr):
❑Yes El o
N/A
6.
Rush Turn Around Time Requested:
Dye s o
❑N/A
7.
Sufficient Vidal Ile.
Correct Containers Used:
-Pace Containers Used:
es :No
es
❑NJA
❑N/A
9.
Containers Intact:
es ONo
ON/A
Filtered volume received for Dissolved tests
Dyes -No
21 /A
11.
Sample Labels match COC:
-Includes date/time/ID/Analysis Matrix:
( is . ❑yo
ON/A
12.
All containers needing preservation have been checked.
All containers needing preservation are found to be in
compliance with EPA recommendation.
exceptions: VOA, colirorm, TOC, 0&G, Wl•DRO (water)
Dyes ONo DNA'
❑Yes /A
13Yes ❑No
1
Samples checked for dechlorination:
OYes ❑No
QlirA
4.
Headspace in VOA Vials (>6mm):
❑Yes ONo
❑ /
5.
Trip Blank Present:
Trip Blank Custody Seals Present
Pace Trip Blank Lot # (if purchased):
OYes ❑No
OYes ONo
ZA
16.
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: Date:
SRF Review: Date: l
Note: Whenever there is a discrepancy affecting North Carolina compliance
samptes, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
1111111111111111111111
92261784
Page 16 of 18

N
o
+o
w
N
m
In
A
w
ro
ITEM #
a1.
nit)
npJl
coC
A
N
_
O
N Eo
a
t
c� D
•�CZ
4 0
0
1
z
O
O^^
©
O
y o lu
i\.
d
o
` y
IN
C
Z
w
x
3
m
m
�•
�'
i`
HOO poTN N O
n3
1�
m n
F
17
'0
'0
'D
n
.8
xi
M
,'0 (n
m
9N7JV0r V2�2
z
z
4
{
a°
C'O
a=
MATRIX
C
3
9
70
O
W
In--N
y
CODE (sea va'Idcodes toletl)
p
'a
'�-
•+•
n
7"
ij
n
{
SAMPLE TYPE (G=GRAB C=COMP)
`
M
a
d
W
<>11l�
m
(�
D
p
Q
r
ra
m
a
N
X
z
o
Z
o
m
0
(�
`� ,
•,
,
�'+
1
+
z
+
C
S
+
zm
n
i
t^
Ok
`
,
,
Z
mo
m
0
z
�y
v
O
m
c
\
ra
i~
C�
cy
v
ti,
\
w
`
SAMPLE TEMP AT COLLECTION
8
a 4w
$
n
a
m#OF
o
CONTAINERS
oET
4'm
3
C
Unpreseed
HZSO,
n
HNO
HCI
2
G
1
NaOH
n
Na2S203
y
vMethanol
_
"
m
Other
Q
Test b
Y/ N j
m
.Analysis
I
'R
,
a
3
C 'C
1),
m
p m
3
N
v
,�
_
1 I
G)
o
Uelw /l L+ C
y.
cO
to
o
v
C
-(
-t
�5 iG uG `% er
z
`
m
z
v
o
0
Temp in `C
./ D( G
C
Residual Chlorine (Y/N)
'a
y
M
GO
GO
Received
Ice (YIN)
y
3
m
(i(
_
w
"o {�
I )
O
0
GO
Custody
Sealed Cooler
O
{
✓t
r
�/
A• `�1
01
0
O
V
O_
Samples Inta
(n
r " )
a _
I
Dct
(YJN)
�
LL1--
m (7
m
a X
3
r
Er (D
o N
�®
a
a
a
15 �
e17of18

N
o
ry
"MIt
A
\-&
L m
N
;O to
W
C
C
-�
CO) n p
a
nD
yy
?
C
7
v
>
9 3
m
o a
a
i
O
Q
C o T
ms 1„
E
•n
X
i
r
Qy
V
Z ®
i
3
C
m
In
I
y
0
` Op.
'D
'e
'D
p
;o
.ZI to
G)
D
O
O
c
O
Is
!
_
-1 to :U r r
>
c
In
i I
m
'1
1
MATRIX CODE (sea valid codes to left)
3
p
o
L�
co
O.
v W
�•
Z
,
z
°
1�
Cti1
SAMPLE TYPE (G=GRAB C=COMP)
�•
v
D
m
r<'
a1
t y
R
m
0
m
7
W
1,
.�
o
n
-r
G)
z
M
Z
Z
D
�
I°
Z
-Di
Z
m
1
7
l
m
o
m
m
3
0
z
®
�N
D
b
D
D
o�
Sg
im
Z
��
(•��.
n
SAMPLE TEMP AT COLLECTION
m
v\
m
rya
$
d m
_ $
o m
a
o<
f�D
j o
# OF CONTAINERS
�•
�
s
o s 'pom
= '
Unpresered
HZSO,
�`
o n
0
HNO3
m
v,
HCI
NaOH
Na2S203
`
r
0
Methanol
�
vI
�
ZI
I
Other
dAnalysis Test
Yt N J
r�
m
�i CcS
@
1�
-
- i aet I A to[; 4'
�1
o N
n
z
F'
) ' ._I m
mto
p�Y
i
(D
O
G:
N v C
-n
y
-i o
m
�
m
0
� o
i
l71CL
>
m
(�
OC
0 Z
t J
n
(
�o
o
Temp in °C
0
Residual Chlorine (Y/N)
In
00
Received on
(/
Ice (Y/N)
\
D
a
) .�
GX)
-3o
In
m
�•
O O
(
Custody
Sealed Cooler
O
n C—,
m Z
�-,
(YIN)
o
Z
4)
O �
G)
"iilaol.
Sample
(, t)
Cr
d
m
4
0
0 c
w
C)
o
m >
m
•-zi �
a S�1
m
m
m �
a /W
3
r
o N
3 ama'
v
m
a 0
n
o
c
m
ge 18 of 18